19054_HD Supply_Final Grade Sampling Report 2020.11.10

Via Email

November 10, 2020

NC Department of Environmental Quality
Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646

Attention: Ms. Carolyn Minnich

Re: Final Grade Soil Sampling Report
South Tower
HD Supply Site
1414 South Tryon Street
Charlotte, North Carolina
Brownfields Project No. 19054-15-060
H&H Job No. BCP.064

Dear Ms. Minnich:

Enclosed please find the Final Grade Soil Sampling Report for the HD Supply Brownfields
property (Brownfields Project No. 19054-15-060) located at 1414 South Tryon Street in Charlotte,
NC.

Should you have any questions or need additional information, please do not hesitate to contact us
at [phone].

Very truly yours,
Hart & Hickman, PC

Trinh DeSa, PE Nathan O’Leary, CHMM
Senior Project Engineer Project Manager

Enclosure

cc: Ms. Jordan Thompson, NCDEQ (Via email)

Final Grade Soil Sampling Report

HD Supply Brownfields Site
1414 South Tryon Street
Charlotte, North Carolina

Brownfields Project No. 19054-15-060

November 9, 2020 H&H Job No. BCP-064

#C-1269 Engineering #C-245 Geology

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Final Grade Soil Sampling Report
HD Supply Brownfields Site
1414 South Tryon Street
Charlotte, North Carolina
Brownfields Project No. 19054-15-060
H&H Job No. BCP-064

Table of Contents

Section Page No.

1.0 Introduction ............................................................................................................................ 1
1.1 Site History ........................................................................................................................... 1
1.2 Previous Brownfields Assessment Activities ....................................................................... 2
2.0 Final Grade Soil Sampling Activities ................................................................................... 5
2.1 Soil Sampling Methodology ................................................................................................. 5
2.2 Quality Assurance/Quality Control ...................................................................................... 6
2.3 Boring Abandonment and Investigation Derived Waste ...................................................... 7
3.0 Final Grade Soil Sampling Results ....................................................................................... 8
3.1 Soil Sample Results .............................................................................................................. 8
3.3 QA/QC Sample Results ........................................................................................................ 9
4.0 Summary and Conclusions.................................................................................................. 11

List of Tables
Table 1 Summary of Final Grade Soil Analytical Results

List of Figures
Figure 1 Site Location Map
Figure 2 Site and Final Grade Soil Sample Location Map

List of Appendices
Appendix A Soil Boring Logs
Appendix B Laboratory Analytical Report
Appendix C Soil Risk Calculator Summary Pages

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Final Grade Soil Sampling Report
HD Supply Brownfields Site
1414 South Tryon Street
Charlotte, North Carolina
Brownfields Project No. 19054-15-060
H&H Job No. BCP-064

1.0 Introduction

On behalf of RailYard LLC (Beacon), Hart & Hickman, PC (H&H) has prepared this Final Grade
Soil Sampling Report summarizing final grade soil sampling activities completed at the HD Supply
Brownfields property (Brownfields Project No. 19054-15-060) located at 1414 South Tryon Street in
Charlotte, Mecklenburg County, North Carolina (Site). A Site location map is provided as Figure 1.

The HD Supply Brownfields property was initially comprised of one approximately 3.38-acre parcel
of land owned by RailYard LLC (formerly Beacon MPI, LLC). However, RailYard LLC sold an
approximately 0.74-acre area in the western portion of the Site to Centro RailYard LLC on
November 27, 2018. Currently, the HD Supply Brownfields property is comprised of two parcels.
The larger approximately 2.77-acres parcel (Parcel No. 07309204) is owned by RailYard LLC and
has been developed with two multi-purpose high-rise towers (retail and commercial office space)
and a parking deck. The smaller approximately 0.74-acre parcel (Parcel No. 07309217) is owned by
Centro RailYard LLC and has been developed with a multi-story building including retail
commercial units on the ground floor with multi-family residential apartment units above. A Site
map is provided as Figure 2.

1.1 Site History

Historically, the subject Site was developed with multiple residential structures prior to 1911 based
on review of historic Sanborn Fire Insurance maps. The southeastern portion of the Site was
redeveloped for commercial purposes in 1946 when an approximately 36,000 square foot (sq ft)
multi-use building was constructed. The multi-use building was used as a drycleaner and laundry
facility from initial construction to the late 1960s or early 1970s. From the early 1970s through
2017 when the building was demolished, the multi-use building was used as a furniture showroom,

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offices, and warehouse storage. The western portion of the Site was developed with an
approximately 7,700 sq ft warehouse building in 1984 and was occupied by HD Supply for office
space and electrical supply warehousing from 1984 until 2017 when the building was demolished.
A Site map is provided as Figure 2.

1.2 Previous Brownfields Assessment Activities

Details of previous assessment activities conducted at the Site are provided in the Brownfields
Assessment Report dated June 19, 2017 and the Soil Characterization Report dated January 11,
2019. A brief summary of previous assessment activities detailed in these reports is provided below:

Brownfields Assessment Report
During the Brownfields assessment activities, H&H advanced five soil borings and installed seven
soil gas vapor points to supplement assessment activities previously conducted at the Site. Based on
the results of the assessment activities, H&H concluded the following:

• Soil with compound concentrations above Residential and/or Industrial PSRGs was present
in shallow soil in the area of soil samples SB-4 and SB-6 on the southeastern portion of the
Site in the vicinity of the former dry-cleaner. Results of TCLP analysis of soil from this area
indicates that the soil is not a characteristically hazardous waste.

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• Results of the soil gas sampling indicated the presence of PCE and 1,2,4-trimethylbenzene at
concentrations above Residential VISCs in the sample from SG-6 located below the
southwestern portion of the residential apartments. Results of cumulative risk calculations
indicate that cumulative risks for this sample is in the range of acceptable lifetime
incremental carcinogenic risk (LICR) of 1 x 10-4 to 1 x 10-6 for potential carcinogenic risks
and below the cumulative hazard index (HI) of 1 for potential non-carcinogenic risks. No
other soil gas samples collected in the area of the apartment building indicated the presence
of analyzed compounds at concentrations above Residential SGSLs. Additionally, no soil
gas samples in the area of the north tower indicated the presence of analyzed compounds
concentrations above Non-Residential SGSLs.

Based on the historical use of the Site for dry-cleaning operations and the results of the soil gas
sample collected below the southwestern portion of the apartment building, H&H recommended that
a vapor intrusion mitigation system (VIMS) be installed below the southern tower and the southern
portion of the apartment building.

Details of the Brownfields assessment activities are provided in the Brownfields Assessment Report
dated June 19, 2017.

Soil Characterization Report
Prior to the start of development activities, H&H characterized soil at the Site to expedite soil
management during development activities. Results of the soil characterization activities are
provided below:

• Analytical results did not indicate the presence of VOCs, SVOCs, or RCRA metals in the
shallow or deep samples collected from Sections 1, 2, 3, or 4 at concentrations above
Residential or Commercial/Industrial PSRGs.

• The shallow soil sample collected from Section 5 (SC-5S) indicated the presence of several
SVOCs above laboratory reporting limits, but below Residential and Commercial/Industrial

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PRSGs. Additionally, the polynuclear aromatic hydrocarbons (PAHs) benzo(a)pyrene,
benzo(b)fluoranthene, and dibenz(a,h)anthracene were detected at concentrations above the
Residential PSRGs, but below the Commercial/Industrial PSRGs. Additionally, arsenic was
detected above Residential and Commercial/Residential PSRGs.

• The deeper sample collected from Section 5 did not indicate the presence of VOCs or
SVOCs at concentrations above Residential or Commercial/Industrial PSRGs. Arsenic was
detected at 1.8 J mg/kg in the deeper sample from Section 5 which is above the Residential
PSRG, but is below the Commercial/Industrial PSRG.

• The shallow soil sample collected from Section 6 indicated the presence of tetrachloroethene
(PCE) at a concentration of 0.0024 mg/kg which is below Residential and
Commercial/Industrial PSRGs. Additionally, arsenic was detected in the shallow sample at a
concentration of 2.2 J mg/kg which is above the Residential PSRG, but below the
Commercial/Industrial PSRG. No other VOCs, SVOCs, or RCRA metals were detected in
the shallow or deeper soil samples collected from Section 6 at concentrations above
Residential or Commercial PSRGs.

• Analytical results indicate the presence of PCE and trichloroethene (TCE) at low
concentrations below the Residential and Commercial/Industrial PSRGs in the shallow and
deeper samples collected from Section 7. No SVOCs or RCRA metals were detected above
Residential or Commercial PSRGs in the soil samples collected from Section 7.

Details of the soil characterization activities are provided in the Soil Characterization Report dated
January 11, 2019.

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2.0 Final Grade Soil Sampling Activities

The subject Site is predominately covered with hardscape surfaces with the exception of a small
grassed courtyard located between the two Site tower buildings. As such, the purpose of the final
grade sampling activities was to collect representative soil samples of the grassed area. The small
courtyard area is depicted on Figure 2.

The final grade soil sampling activities were performed in accordance with the DEQ-approved Final
Grade Sampling Work Plan (Work Plan) dated October 23, 2020.

Prior to conducting the field activities, H&H contacted North Carolina 811, the public utility locator,
to mark subsurface utilities located at the Site. In addition, H&H contracted Ground Penetrating
Radar Systems, LLC (GPRS), a private utility locator to mark utilities on the property. Several
utilities, including irrigation lines and electrical conduits, were identified and marked in the grassed
area. The final grade soil boring locations were selected to provide representative coverage of the
grassed area and to provide proper clearance from the utilities for safety reasons.

2.1 Soil Sampling Methodology

On October 28, 2020, H&H advanced three shallow soil borings (SB-1, SB-2, and SB-3) in the
grassed courtyard located between the northern and southern tower buildings. Soil borings were
advanced to approximately 2 feet (ft) below ground surface (bgs) at each boring location utilizing a
decontaminated stainless-steel hand auger. Continuous soil samples were collected from the center
of the hand auger bucket at each soil boring and described for lithologic purposes, observed for the
presence of staining, and field screened for the presence of organic vapors using a calibrated
photoionization detector (PID). Soil boring logs with lithologic and field screening information are
included as Appendix A.

Aliquots of soil from each boring were placed into a stainless-steel bowl and homogenized to form
one composite soil sample. No obvious evidence of impacts was observed in the soil at the boring
locations during field screening activities. In accordance with the Work Plan, H&H randomly

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selected a soil boring to collect a grab sample from the 1 ft to 2 ft bgs interval for laboratory analysis
of volatile organic compounds (VOCs). The grab sample was collected from soil boring SB-1
(Figure 2).

The final grade soil samples selected for laboratory analysis were collected directly into laboratory
supplied glassware, labeled with the sample identification, date, time, and requested analysis and
placed on ice in a laboratory supplied cooler. The samples were delivered to Pace Analytical
Laboratories (Pace) under standard chain of custody protocols. The grab sample (FG1-1-2) was
collected and submitted for analysis of VOCs by EPA Method 8260. The composite sample (FG-
102820) was collected and submitted for analysis of semi-volatile organic compounds (SVOCs) by
EPA 8270, and RCRA metals plus hexavalent chromium by EPA Methods 6020/7471/7199. The
laboratory analytical report and the chain of custody are included in Appendix B, and the analytical
data is summarized on Table 1. A summary of the analytical results is provided in Section 3.0.

2.2 Quality Assurance/Quality Control

For quality assurance / quality control (QA/QC) purposes, H&H collected a duplicate soil sample
(DUP-1). Additionally, H&H collected an equipment blank (RB-1) to evaluate the effectiveness of
the field equipment decontamination methods. To collect the equipment blank, laboratory supplied
analyte free water was poured over the decontaminated stainless-steel hand auger. The water was
collected off the hand auger directly into laboratory supplied sample containers. The duplicate soil
sample and the equipment blank were submitted to Pace for analysis of VOCs by EPA Method
8260, SVOCs by EPA 8270, and RCRA metals plus hexavalent chromium by EPA Methods
6020/7471/7199. H&H requested a Level II QA/QC data package from the laboratory that includes
compound detections to the laboratory-specified method detection limits (MDL) using J-flags. The
laboratory analytical report and the chain of custody are included in Appendix A, and the analytical
data is summarized on Table 1. A summary of the analytical results is provided in Section 3.0.

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2.3 Boring Abandonment and Investigation Derived Waste

During boring advancement and sampling, field screening indicated no evidence of significant
impact was observed in the soils. Therefore, the investigation derived waste (IDW) generated
during the sampling activities was thin spread in the area of generation. Following sampling
activities, the soil borings were properly abandoned using bentonite chips mixed with soils generated
from the sampling activities, and the surface was repaired to match pre-sampling conditions with
grass cover.

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3.0 Final Grade Soil Sampling Results

The analytical laboratory results for the surficial final grade soil samples are summarized in Table 1
and the analytical laboratory reports are included in Appendix B. The analytical results were
compared to the DEQ Residential and Non-Residential Health-Based PSRGs dated July 2020. The
area where the final grade sampling activities were conducted is used for non-residential purposes
(i.e. retail and office space), but due to the residential multi-family apartment located on the western
portion of the property (Centro Railyard), the results were also compared to the Residential PSRGs.

Metal analytical results were compared to Site-specific metals data summarized in the Soil
Characterization Report dated January 11, 2019. Additionally, the metals concentrations were
compared to regional background concentrations for North Carolina soils as published in Elements
in North American Soils by Dragun and Chekiri (2005) before comparison to the PSRGs.

3.1 Soil Sample Results

VOCs
Laboratory analytical results of FG-1 and DUP-1 do not indicate the presence of VOCs at
concentrations above Residential or Non-Residential PSRGs. It should be noted that several VOCs
were detected at low concentrations above laboratory method detection limits (MDLs), but well
below their respective PSRG values. Additionally, several of the detected compounds including
acetone and methylene chloride are common laboratory artifacts.

SVOCs
Laboratory analytical results indicate do not indicate the presence of SVOCs at concentrations above
laboratory MDLs in the sample or associated duplicate sample.

Metals
Analytical results indicate the presence of several metals at concentrations above laboratory MDLs
in the sample and associated duplicate sample, but below the Residential and Non-Residential
PSRGs, with the exception of arsenic. Arsenic was detected at a concentration of 2.91 mg/kg, which

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is above the Residential PSRG of 0.68 mg/kg, but below the Non-Residential PSRS of 3.0 mg/kg.
Arsenic is a prevalent metal found in soils in this region of North Carolina and the detected arsenic
concentrations is in the range of published regional background concentrations for North Carolina
soils (1.0 mg/kg to 18 mg/kg). Additionally, the concentrations of arsenic detected in the soil
sample and associated duplicate sample are consistent with the lower end of the range of arsenic
detected during the characterization activities. As such, the presence arsenic in the grassed area
between the two towers is likely naturally occurring.

3.2 Risk Calculation

To further evaluate the detected compounds, H&H input the highest concentration of each
compound detected in the soil samples (to simulate a worst-case scenario) into the DEQ Risk
Calculator (July 2020 version). Calculations were completed for both a Residential and Non-
Residential use scenario for the direct contact soil exposure pathway to calculate cumulative
potential carcinogenic and non-carcinogenic risks for the soil samples. To evaluate the worst-case
scenario, H&H used the highest detected concentration of each compound in either the parent or
duplicate sample. The completed risk calculator summary pages are provided in Appendix C.

The soil risk calculator for the worst-case scenario indicated that the non-carcinogenic HI for
residential use is 0.099 and the HI for non-residential workers is 0.0084, which are significantly
below the threshold of 1. Additionally, the soil risk calculator indicated that the LICR for residential
us is 4.3 x 10-6 and the LICR for non-residential workers is 9.7 x 10-7, which are significantly below
the acceptable risk of 1 x 10-4. As such, exposed surficial soil at the Site does not appear to pose an
unacceptable risk to future Site residents or non-residential workers.

3.3 QA/QC Sample Results

The results of the analytical data from the duplicate sample indicated that similar constituents and
concentrations were detected in the both the parent duplicate soil sample, with the exception of
acetone. Acetone was detected at a very low concentration in the duplicate sample, but was not
detected in the parent sample. Acetone is a common ingredient in cleaning solutions and thus is a

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common laboratory contaminant. The low concentration of acetone detected could be attributed to
laboratory contamination. Therefore, the duplicate sample results generally indicated good
laboratory repeatability.

The analytical data for the equipment blank sample indicated that VOC, SVOC, or metal
constituents were not detected above laboratory MDLs, with the exception of hexavalent chromium,
which was detected a low estimated J-flag concentration. Hexavalent chromium was not detected in
either the parent or duplicate soil sample above laboratory MDLs. Therefore, the results of the
equipment blank indicate that effective field equipment decontamination methods were performed
and did not appear to impact the analytical results of the soil samples.

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4.0 Summary and Conclusions

H&H has prepared this report to summarize final grade soil sampling conducted at the HD Supply
Brownfields property (Brownfields Project No. 19054-15-060) located at 1414 South Tryon Street in
Charlotte, Mecklenburg County, North Carolina. A brief summary of the final grade soil sampling
activities and results is provided below.

• The Site is developed with two commercial use high-rise towers (retail and commercial
office space) and a parking deck in the central portion of the Site. The western portion of the
Site and is developed with a multi-store building which includes retail commercial units on
the ground floor and multi-family residential apartment units above.

• The subject Site is predominately covered with hardscape surfaces with the exception of a
small grassed courtyard located between the two Site tower buildings. H&H collected
shallow grab and composite soil samples from the grassed area to evaluate potential risks to
future Site residents and/or workers from direct contact exposure to surficial soil at the Site.

• The results of analysis of the final grade soil samples do not indicate the presence of VOCs
at concentrations above Residential or Non-Residential PSRGs or SVOCs at concentrations
above laboratory MDLs. The results of the metals analysis indicate that arsenic was detected
in shallow soil at a concentration above the Residential PSRG, but below the Non-
Residential PSRG. This arsenic detection is consistent with published regional background
levels and previous site-specific sampling data. As such, the presence of arsenic is likely
naturally occurring.

• Cumulative risk calculations using DEQ’s risk calculator indicate that the calculated LICR
and HI values are below the DEQ and EPA acceptable risk levels. As such, surficial soil at
the Site does not appear to pose an unacceptable risk to future Site residents or non-
residential workers.

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Based on the results of the final grade sampling activities, compounds present in surficial soil at the
Site do not appear to pose an unacceptable risk to future residential occupants or non-residential
workers. As such, H&H does not recommend additional assessment or remedial activities be
completed.
Table 1
Summary of Final Grade Soil Sample Analytical Results
HD Supply Brownfields Site
1414 South Tryon St.
Charlotte, North Carolina
H&H Project No. BCP.064
Site
Site-Specific Metal
Concentrations (2)
Sample ID FG-102820 FG1-1-2 DUP-1
Sample Type Composite Grab Duplicate
Sample Date 10/28/2020 10/28/2020 10/28/2020
VOCs by EPA 8260 (mg/kg)
Acetone --<0.0495 0.418 12,000 140,000 ------
2-Butanone (MEK)--0.158 0.236 5,500 40,000 ------
Methylene Chloride --0.0961 0.0874 58 650 ------
Toluene --0.0065 J 0.0048 J 990 9,700 ------
SVOCs by 8270 (mg/kg)ND --ND ----------
Metals by 6020/7196/7471 (mg/kg)
Arsenic 2.91 --2.53 0.68 3.0 <1.3 - 27 1.0 - 18.0 4.8
Barium 85.8 --73.8 3,100 47,000 27 - 150 50 - 1,000 356
Cadmium <0.120 --<0.118 14 200 0.15 - 4.5 1.0 - 10*4.3
Lead 10.7 --12.3 400 800 <0.59 - 130 ND - 50 16
Mercury 0.0557 J --0.0901 2.3 9.7 0.037 - 0.30 0.03 - 0.52 0.121
Selenium 0.818 J --0.856 J 78 1,200 ND <0.1 - 0.8 0.42
Silver <0.122 --<0.120 78 1,200 <0.36 - 3.0 ND - 5.0 NS
Total Chromium 70.5 --44.0 NE NE 16 - 130 7.0 - 300 65
Hexavalent Chromium <0.359 --<0.353 0.31 6.5 NS NS NS
Notes:
1) NC Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Residential and Non-Residentila Health Based Soil Remediation Goals (PSRGs) - July 2020
2) Range of site-specific metal concentrations from pre-construction samples, as summarized in the Soil Characterization Report, dated January 11, 2019.
3) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005
* = Range and mean values of background metals for Southeastern USA soilsOnly those compounds detected in at least sample for VOCs and SVOCs shown; all results for metal analyses are shownSoil concentrations are reported in milligrams per kilogram (mg/kg)
Laboratory analytical methods are shown in parentheses
NS = Not Specified; -- = Not Applicable; NE = Not Established; ND = Non-detect
VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic CompoundsSoil samples for analysis of SVOCs and metals collected as composite samples
VOC sample collected as grab sample from 1-2 ft depth interval
J = estimated value between the laboratory detection limit and the laboratory reporting limit
Less than values indicate laboratory method detection limits
HD Supply PSRGs (1)Regional Background Metals
in Soil (3)
MeanRangeIndustrial/
CommercialResidential Range
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Table 1
Hart & Hickman, PC
SITE LOCATION MAP
HD SUPPLY BROWNFIELDS SITE1414 SOUTH TRYON STREETCHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
11/23/2020 0
1BCP-064
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP7.5 MINUTE SERIES (TOPOGRAPHIC)
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
CHARLOTTE EAST, NORTH CAROLINA 1991
SITE
S. TRYON STREETW
E
S
T

B
L
A
N
D

S
T
R
E
E
T
WINNIFRED STREETWI
N
O
N
A

S
T
R
E
E
T
THE RAILYARD(RAILYARD, LLC)
SOUTH
TOWER
NORTH
TOWER
PARKINGGARAGE
RAILYARD APARTMENTS(CENTRO RAILYARD, LLC)
POTENTIAL AREA OF
SOIL CONTAMINATION
SB-1
SB-2
SB-3
REVISION NO. 0
JOB NO. BCP-064
DATE: 11-09-20
FIGURE NO. 2
HD SUPPLY BROWNFIELDS SITE1414 SOUTH TRYON STREET
CHARLOTTE, NORTH CAROLINA
SITE AND FINAL GRADE SOIL SAMPLE
LOCATION MAP
LEGEND
RAILYARD APARTMENTS(CENTRO RAILYARD, LLC)
THE RAILYARD (RAILYARD, LLC)
FINAL GRADE SAMPLING SOILBORING LOCATION
POTENTIAL AREA OF SOIL
CONTAMINATION
GRASSED COURTYARD
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURGCOUNTY GIS, 2020.
2. SOIL SAMPLES WERE COLLECTED ON OCTBER 28, 2020.S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-064 1414 and 1422 S. Tryon\Brownfields\Final Grade Sampling Report\Site Map.dwg, 11/7/2020 8:20:21 PM, DWG To PDF.pc3

Appendix A

Soil Boring Logs
NOTES: A sample aliquot from each 1 ft interval was composited for analysis of SVOCs and metals.
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-064
1414 S. Tryon Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
10/28/2020
10/28/2020
Hart & Hickman
Hand Auger
MJW
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR
GR
1.00
1.00
(0') SILT with sand (ML); some fine-medium sand, very moist, black, some organics, wood debris
(0.85') CLAY (CL); some silt, medium plasticity, very moist, orange to red
0.9
1.2
0
1
2
3
4
5
A grab sample from the 1ft to 2ft interval at this location was collected for analysis of VOCs.
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-064
1414 S. Tryon Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
10/28/2020
10/28/2020
Hart & Hickman
Other
Hand Auger
MJW
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR
GR
1.00
1.00
(0') SILT with sand (ML); some fine-medium sand, very moist, black, some organics, wood debris
(0.85') Lean CLAY (CL); some silt, medium plasticity, very moist, orange
1.2
1.2
0
1
2
3
4
5
NOTES: A sample aliquot from each 1 ft interval was composited for analysis of SVOCs and metals.
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-064
1414 S. Tryon Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
10/28/2020
10/28/2020
Hart & Hickman
Other
Hand Auger
MJW
HHM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR
GR
1.00
1.00
(0') SILT with sand (ML); some fine-medium sand, very moist, black, some organics, wood debris
(0.85') Lean CLAY (CL); some silt, medium plasticity, very moist, orange
1.3
1.3
0
1
2
3
4
5
NOTES: A sample aliquot from each 1 ft interval was composited for analysis of SVOCs and metals.

Appendix B

Laboratory Analytical Report
#=CL#
November 06, 2020
LIMS USE: FR - NATHAN O'LEARY
LIMS OBJECT ID: 92502685
92502685
Project:
Pace Project No.:
RE:
Mr. Nathan O'Leary
Hart & Hickman
2923 S. Tryon St
Charlotte, NC 28203
BCP-064
Dear Mr. O'Leary:
Enclosed are the analytical results for sample(s) received by the laboratory on October 28, 2020. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
Report revised 11/6/20 to correct a reporting error. 6020/7470 RCRA Metals and 7199 Hexavalent Chromium results for
RB-1 were mistakely uploaded for FG1-1-2. This report corrects that error.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 57
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92502685
BCP-064
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 57
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92502685
BCP-064
Lab ID Sample ID Matrix Date Collected Date Received
92502685001 FG-102820 Solid 10/28/20 11:00 10/28/20 14:20
92502685002 DUP-1 Solid 10/28/20 11:10 10/28/20 14:20
92502685003 FG1-1-2 Solid 10/28/20 11:00 10/28/20 14:20
92502685004 RB-1 Water 10/28/20 09:30 10/28/20 14:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 57
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92502685
BCP-064
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92502685001 FG-102820 EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92502685002 DUP-1 EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92502685003 FG1-1-2 EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92502685004 RB-1 EPA 6020B 7 PANLAT
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:FG-102820 Lab ID:92502685001 Collected:10/28/20 11:00 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.91 mg/kg 11/02/20 00:10 7440-38-210/30/20 19:331.41 0.141 5
Barium 85.8 mg/kg 11/02/20 00:10 7440-39-310/30/20 19:333.52 0.214 5
Cadmium ND mg/kg 11/02/20 00:10 7440-43-910/30/20 19:331.41 0.120 5
Chromium 70.5 mg/kg 11/02/20 00:10 7440-47-310/30/20 19:337.04 0.417 5
Lead 10.7 mg/kg 11/02/20 00:10 7439-92-110/30/20 19:332.81 0.139 5
Selenium 0.818J mg/kg 11/02/20 00:10 7782-49-2 J10/30/20 19:333.52 0.253 5
Silver ND mg/kg 11/02/20 00:10 7440-22-410/30/20 19:330.704 0.122 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0557J mg/kg 10/31/20 08:37 7439-97-6 J10/30/20 08:230.0563 0.0253 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 10/29/20 16:05 83-32-910/29/20 14:154711211
Acenaphthylene ND ug/kg 10/29/20 16:05 208-96-810/29/20 14:154711111
Aniline ND ug/kg 10/29/20 16:05 62-53-310/29/20 14:154711061
Anthracene ND ug/kg 10/29/20 16:05 120-12-710/29/20 14:154711221
Benzo(a)anthracene ND ug/kg 10/29/20 16:05 56-55-310/29/20 14:154711501
Benzo(a)pyrene ND ug/kg 10/29/20 16:05 50-32-810/29/20 14:154712041
Benzo(b)fluoranthene ND ug/kg 10/29/20 16:05 205-99-210/29/20 14:154711901
Benzo(g,h,i)perylene ND ug/kg 10/29/20 16:05 191-24-210/29/20 14:154711841
Benzo(k)fluoranthene ND ug/kg 10/29/20 16:05 207-08-910/29/20 14:154711981
Benzoic Acid ND ug/kg 10/29/20 16:05 65-85-0 L2,M010/29/20 14:1523505081
Benzyl alcohol ND ug/kg 10/29/20 16:05 100-51-610/29/20 14:159412501
4-Bromophenylphenyl ether ND ug/kg 10/29/20 16:05 101-55-310/29/20 14:154711241
Butylbenzylphthalate ND ug/kg 10/29/20 16:05 85-68-710/29/20 14:154711251
4-Chloro-3-methylphenol ND ug/kg 10/29/20 16:05 59-50-710/29/20 14:159412871
4-Chloroaniline ND ug/kg 10/29/20 16:05 106-47-810/29/20 14:159412881
bis(2-Chloroethoxy)methane ND ug/kg 10/29/20 16:05 111-91-110/29/20 14:154711261
bis(2-Chloroethyl) ether ND ug/kg 10/29/20 16:05 111-44-410/29/20 14:154711001
2-Chloronaphthalene ND ug/kg 10/29/20 16:05 91-58-710/29/20 14:154711051
2-Chlorophenol ND ug/kg 10/29/20 16:05 95-57-810/29/20 14:154711101
4-Chlorophenylphenyl ether ND ug/kg 10/29/20 16:05 7005-72-310/29/20 14:154711221
Chrysene ND ug/kg 10/29/20 16:05 218-01-910/29/20 14:154711371
Dibenz(a,h)anthracene ND ug/kg 10/29/20 16:05 53-70-310/29/20 14:154711881
Dibenzofuran ND ug/kg 10/29/20 16:05 132-64-910/29/20 14:154711181
1,2-Dichlorobenzene ND ug/kg 10/29/20 16:05 95-50-110/29/20 14:154711021
1,3-Dichlorobenzene ND ug/kg 10/29/20 16:05 541-73-110/29/20 14:154711061
1,4-Dichlorobenzene ND ug/kg 10/29/20 16:05 106-46-710/29/20 14:154711041
3,3'-Dichlorobenzidine ND ug/kg 10/29/20 16:05 91-94-110/29/20 14:159413281
2,4-Dichlorophenol ND ug/kg 10/29/20 16:05 120-83-210/29/20 14:154711551
Diethylphthalate ND ug/kg 10/29/20 16:05 84-66-210/29/20 14:154711021
2,4-Dimethylphenol ND ug/kg 10/29/20 16:05 105-67-910/29/20 14:154711171
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:FG-102820 Lab ID:92502685001 Collected:10/28/20 11:00 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 10/29/20 16:05 131-11-310/29/20 14:154711061
Di-n-butylphthalate ND ug/kg 10/29/20 16:05 84-74-210/29/20 14:154711161
4,6-Dinitro-2-methylphenol ND ug/kg 10/29/20 16:05 534-52-110/29/20 14:159417591
2,4-Dinitrophenol ND ug/kg 10/29/20 16:05 51-28-510/29/20 14:15235015001
2,4-Dinitrotoluene ND ug/kg 10/29/20 16:05 121-14-210/29/20 14:154711251
2,6-Dinitrotoluene ND ug/kg 10/29/20 16:05 606-20-210/29/20 14:154711231
Di-n-octylphthalate ND ug/kg 10/29/20 16:05 117-84-010/29/20 14:154712681
bis(2-Ethylhexyl)phthalate ND ug/kg 10/29/20 16:05 117-81-710/29/20 14:154711541
Fluoranthene ND ug/kg 10/29/20 16:05 206-44-010/29/20 14:154711421
Fluorene ND ug/kg 10/29/20 16:05 86-73-710/29/20 14:154711261
Hexachloro-1,3-butadiene ND ug/kg 10/29/20 16:05 87-68-310/29/20 14:154711141
Hexachlorobenzene ND ug/kg 10/29/20 16:05 118-74-110/29/20 14:154711201
Hexachlorocyclopentadiene ND ug/kg 10/29/20 16:05 77-47-410/29/20 14:154711881
Hexachloroethane ND ug/kg 10/29/20 16:05 67-72-110/29/20 14:154711071
Indeno(1,2,3-cd)pyrene ND ug/kg 10/29/20 16:05 193-39-510/29/20 14:154712151
Isophorone ND ug/kg 10/29/20 16:05 78-59-110/29/20 14:154711021
1-Methylnaphthalene ND ug/kg 10/29/20 16:05 90-12-010/29/20 14:154711251
2-Methylnaphthalene ND ug/kg 10/29/20 16:05 91-57-610/29/20 14:154711201
2-Methylphenol(o-Cresol)ND ug/kg 10/29/20 16:05 95-48-710/29/20 14:154711041
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/29/20 16:05 15831-10-410/29/20 14:154711181
Naphthalene ND ug/kg 10/29/20 16:05 91-20-310/29/20 14:154711131
2-Nitroaniline ND ug/kg 10/29/20 16:05 88-74-410/29/20 14:1523502371
3-Nitroaniline ND ug/kg 10/29/20 16:05 99-09-210/29/20 14:1523502501
4-Nitroaniline ND ug/kg 10/29/20 16:05 100-01-610/29/20 14:159412321
Nitrobenzene ND ug/kg 10/29/20 16:05 98-95-310/29/20 14:154711121
2-Nitrophenol ND ug/kg 10/29/20 16:05 88-75-510/29/20 14:154711451
4-Nitrophenol ND ug/kg 10/29/20 16:05 100-02-710/29/20 14:1523507501
N-Nitrosodimethylamine ND ug/kg 10/29/20 16:05 62-75-910/29/20 14:154711321
N-Nitroso-di-n-propylamine ND ug/kg 10/29/20 16:05 621-64-710/29/20 14:154711321
N-Nitrosodiphenylamine ND ug/kg 10/29/20 16:05 86-30-610/29/20 14:154711201
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/29/20 16:05 108-60-110/29/20 14:154711311
Pentachlorophenol ND ug/kg 10/29/20 16:05 87-86-510/29/20 14:159412151
Phenanthrene ND ug/kg 10/29/20 16:05 85-01-810/29/20 14:154711191
Phenol ND ug/kg 10/29/20 16:05 108-95-210/29/20 14:154711121
Pyrene ND ug/kg 10/29/20 16:05 129-00-010/29/20 14:154711301
Pyridine ND ug/kg 10/29/20 16:05 110-86-110/29/20 14:154711191
1,2,4-Trichlorobenzene ND ug/kg 10/29/20 16:05 120-82-110/29/20 14:154711081
2,4,5-Trichlorophenol ND ug/kg 10/29/20 16:05 95-95-410/29/20 14:154711221
2,4,6-Trichlorophenol ND ug/kg 10/29/20 16:05 88-06-210/29/20 14:154711181
Surrogates
Nitrobenzene-d5 (S)64 %10/29/20 16:05 4165-60-010/29/20 14:1521-130 1
2-Fluorobiphenyl (S)41 %10/29/20 16:05 321-60-810/29/20 14:1519-130 1
Terphenyl-d14 (S)76 %10/29/20 16:05 1718-51-010/29/20 14:1515-130 1
Phenol-d6 (S)58 %10/29/20 16:05 13127-88-310/29/20 14:1518-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:FG-102820 Lab ID:92502685001 Collected:10/28/20 11:00 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)62 %10/29/20 16:05 367-12-410/29/20 14:1518-130 1
2,4,6-Tribromophenol (S)64 %10/29/20 16:05 118-79-610/29/20 14:1518-130 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.8 %10/28/20 17:010.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.1 %11/01/20 05:2511/01/20 05:151
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 10/30/20 23:56 18540-29-910/30/20 16:231.41 0.359 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:DUP-1 Lab ID:92502685002 Collected:10/28/20 11:10 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.53 mg/kg 11/02/20 00:14 7440-38-210/30/20 19:331.38 0.138 5
Barium 73.8 mg/kg 11/02/20 00:14 7440-39-310/30/20 19:333.46 0.210 5
Cadmium ND mg/kg 11/02/20 00:14 7440-43-910/30/20 19:331.38 0.118 5
Chromium 44.0 mg/kg 11/02/20 00:14 7440-47-310/30/20 19:336.92 0.410 5
Lead 12.3 mg/kg 11/02/20 00:14 7439-92-110/30/20 19:332.77 0.137 5
Selenium 0.856J mg/kg 11/02/20 00:14 7782-49-2 J10/30/20 19:333.46 0.249 5
Silver ND mg/kg 11/02/20 00:14 7440-22-410/30/20 19:330.692 0.120 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0901 mg/kg 10/31/20 08:40 7439-97-610/30/20 08:230.0554 0.0249 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 10/29/20 16:58 83-32-910/29/20 14:154261101
Acenaphthylene ND ug/kg 10/29/20 16:58 208-96-810/29/20 14:154261011
Aniline ND ug/kg 10/29/20 16:58 62-53-310/29/20 14:1542695.7 1
Anthracene ND ug/kg 10/29/20 16:58 120-12-710/29/20 14:154261111
Benzo(a)anthracene ND ug/kg 10/29/20 16:58 56-55-310/29/20 14:154261361
Benzo(a)pyrene ND ug/kg 10/29/20 16:58 50-32-810/29/20 14:154261851
Benzo(b)fluoranthene ND ug/kg 10/29/20 16:58 205-99-210/29/20 14:154261721
Benzo(g,h,i)perylene ND ug/kg 10/29/20 16:58 191-24-210/29/20 14:154261671
Benzo(k)fluoranthene ND ug/kg 10/29/20 16:58 207-08-910/29/20 14:154261801
Benzoic Acid ND ug/kg 10/29/20 16:58 65-85-0 L210/29/20 14:1521304601
Benzyl alcohol ND ug/kg 10/29/20 16:58 100-51-610/29/20 14:158522261
4-Bromophenylphenyl ether ND ug/kg 10/29/20 16:58 101-55-310/29/20 14:154261121
Butylbenzylphthalate ND ug/kg 10/29/20 16:58 85-68-710/29/20 14:154261141
4-Chloro-3-methylphenol ND ug/kg 10/29/20 16:58 59-50-710/29/20 14:158522601
4-Chloroaniline ND ug/kg 10/29/20 16:58 106-47-810/29/20 14:158522611
bis(2-Chloroethoxy)methane ND ug/kg 10/29/20 16:58 111-91-110/29/20 14:154261141
bis(2-Chloroethyl) ether ND ug/kg 10/29/20 16:58 111-44-410/29/20 14:1542690.5 1
2-Chloronaphthalene ND ug/kg 10/29/20 16:58 91-58-710/29/20 14:1542694.9 1
2-Chlorophenol ND ug/kg 10/29/20 16:58 95-57-810/29/20 14:1542699.2 1
4-Chlorophenylphenyl ether ND ug/kg 10/29/20 16:58 7005-72-310/29/20 14:154261111
Chrysene ND ug/kg 10/29/20 16:58 218-01-910/29/20 14:154261241
Dibenz(a,h)anthracene ND ug/kg 10/29/20 16:58 53-70-310/29/20 14:154261701
Dibenzofuran ND ug/kg 10/29/20 16:58 132-64-910/29/20 14:154261071
1,2-Dichlorobenzene ND ug/kg 10/29/20 16:58 95-50-110/29/20 14:1542692.2 1
1,3-Dichlorobenzene ND ug/kg 10/29/20 16:58 541-73-110/29/20 14:1542696.0 1
1,4-Dichlorobenzene ND ug/kg 10/29/20 16:58 106-46-710/29/20 14:1542693.8 1
3,3'-Dichlorobenzidine ND ug/kg 10/29/20 16:58 91-94-110/29/20 14:158522971
2,4-Dichlorophenol ND ug/kg 10/29/20 16:58 120-83-210/29/20 14:154261411
Diethylphthalate ND ug/kg 10/29/20 16:58 84-66-210/29/20 14:1542692.5 1
2,4-Dimethylphenol ND ug/kg 10/29/20 16:58 105-67-910/29/20 14:154261061
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:DUP-1 Lab ID:92502685002 Collected:10/28/20 11:10 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 10/29/20 16:58 131-11-310/29/20 14:1542696.3 1
Di-n-butylphthalate ND ug/kg 10/29/20 16:58 84-74-210/29/20 14:154261051
4,6-Dinitro-2-methylphenol ND ug/kg 10/29/20 16:58 534-52-110/29/20 14:158526871
2,4-Dinitrophenol ND ug/kg 10/29/20 16:58 51-28-510/29/20 14:15213013601
2,4-Dinitrotoluene ND ug/kg 10/29/20 16:58 121-14-210/29/20 14:154261131
2,6-Dinitrotoluene ND ug/kg 10/29/20 16:58 606-20-210/29/20 14:154261111
Di-n-octylphthalate ND ug/kg 10/29/20 16:58 117-84-010/29/20 14:154262431
bis(2-Ethylhexyl)phthalate ND ug/kg 10/29/20 16:58 117-81-710/29/20 14:154261391
Fluoranthene ND ug/kg 10/29/20 16:58 206-44-010/29/20 14:154261291
Fluorene ND ug/kg 10/29/20 16:58 86-73-710/29/20 14:154261141
Hexachloro-1,3-butadiene ND ug/kg 10/29/20 16:58 87-68-310/29/20 14:154261041
Hexachlorobenzene ND ug/kg 10/29/20 16:58 118-74-110/29/20 14:154261081
Hexachlorocyclopentadiene ND ug/kg 10/29/20 16:58 77-47-410/29/20 14:154261701
Hexachloroethane ND ug/kg 10/29/20 16:58 67-72-110/29/20 14:1542697.1 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/29/20 16:58 193-39-510/29/20 14:154261951
Isophorone ND ug/kg 10/29/20 16:58 78-59-110/29/20 14:1542692.6 1
1-Methylnaphthalene ND ug/kg 10/29/20 16:58 90-12-010/29/20 14:154261141
2-Methylnaphthalene ND ug/kg 10/29/20 16:58 91-57-610/29/20 14:154261081
2-Methylphenol(o-Cresol)ND ug/kg 10/29/20 16:58 95-48-710/29/20 14:1542694.4 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/29/20 16:58 15831-10-410/29/20 14:154261071
Naphthalene ND ug/kg 10/29/20 16:58 91-20-310/29/20 14:154261021
2-Nitroaniline ND ug/kg 10/29/20 16:58 88-74-410/29/20 14:1521302141
3-Nitroaniline ND ug/kg 10/29/20 16:58 99-09-210/29/20 14:1521302261
4-Nitroaniline ND ug/kg 10/29/20 16:58 100-01-610/29/20 14:158522101
Nitrobenzene ND ug/kg 10/29/20 16:58 98-95-310/29/20 14:154261021
2-Nitrophenol ND ug/kg 10/29/20 16:58 88-75-510/29/20 14:154261321
4-Nitrophenol ND ug/kg 10/29/20 16:58 100-02-710/29/20 14:1521306791
N-Nitrosodimethylamine ND ug/kg 10/29/20 16:58 62-75-910/29/20 14:154261201
N-Nitroso-di-n-propylamine ND ug/kg 10/29/20 16:58 621-64-710/29/20 14:154261191
N-Nitrosodiphenylamine ND ug/kg 10/29/20 16:58 86-30-610/29/20 14:154261091
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/29/20 16:58 108-60-110/29/20 14:154261181
Pentachlorophenol ND ug/kg 10/29/20 16:58 87-86-510/29/20 14:158521951
Phenanthrene ND ug/kg 10/29/20 16:58 85-01-810/29/20 14:154261071
Phenol ND ug/kg 10/29/20 16:58 108-95-210/29/20 14:154261021
Pyrene ND ug/kg 10/29/20 16:58 129-00-010/29/20 14:154261171
Pyridine ND ug/kg 10/29/20 16:58 110-86-110/29/20 14:154261081
1,2,4-Trichlorobenzene ND ug/kg 10/29/20 16:58 120-82-110/29/20 14:1542697.6 1
2,4,5-Trichlorophenol ND ug/kg 10/29/20 16:58 95-95-410/29/20 14:154261111
2,4,6-Trichlorophenol ND ug/kg 10/29/20 16:58 88-06-210/29/20 14:154261071
Surrogates
Nitrobenzene-d5 (S)63 %10/29/20 16:58 4165-60-010/29/20 14:1521-130 1
2-Fluorobiphenyl (S)39 %10/29/20 16:58 321-60-810/29/20 14:1519-130 1
Terphenyl-d14 (S)68 %10/29/20 16:58 1718-51-010/29/20 14:1515-130 1
Phenol-d6 (S)59 %10/29/20 16:58 13127-88-310/29/20 14:1518-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:DUP-1 Lab ID:92502685002 Collected:10/28/20 11:10 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)59 %10/29/20 16:58 367-12-410/29/20 14:1518-130 1
2,4,6-Tribromophenol (S)61 %10/29/20 16:58 118-79-610/29/20 14:1518-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 418 ug/kg 10/29/20 23:53 67-64-110/29/20 14:4513449.9 1
Benzene ND ug/kg 10/29/20 23:53 71-43-210/29/20 14:456.7 4.7 1
Bromobenzene ND ug/kg 10/29/20 23:53 108-86-110/29/20 14:456.7 4.5 1
Bromochloromethane ND ug/kg 10/29/20 23:53 74-97-510/29/20 14:456.7 5.1 1
Bromodichloromethane ND ug/kg 10/29/20 23:53 75-27-410/29/20 14:456.7 4.4 1
Bromoform ND ug/kg 10/29/20 23:53 75-25-210/29/20 14:456.7 3.6 1
Bromomethane ND ug/kg 10/29/20 23:53 74-83-910/29/20 14:4513.4 10.5 1
2-Butanone (MEK)236 ug/kg 10/29/20 23:53 78-93-3 1g10/29/20 14:4513456.7 1
n-Butylbenzene ND ug/kg 10/29/20 23:53 104-51-810/29/20 14:456.7 3.6 1
sec-Butylbenzene ND ug/kg 10/29/20 23:53 135-98-810/29/20 14:456.7 4.2 1
tert-Butylbenzene ND ug/kg 10/29/20 23:53 98-06-610/29/20 14:456.7 3.6 1
Carbon tetrachloride ND ug/kg 10/29/20 23:53 56-23-510/29/20 14:456.7 3.0 1
Chlorobenzene ND ug/kg 10/29/20 23:53 108-90-710/29/20 14:456.7 4.3 1
Chloroethane ND ug/kg 10/29/20 23:53 75-00-3 IK10/29/20 14:4513.4 7.1 1
Chloroform ND ug/kg 10/29/20 23:53 67-66-310/29/20 14:456.7 3.3 1
Chloromethane ND ug/kg 10/29/20 23:53 74-87-310/29/20 14:4513.4 9.4 1
2-Chlorotoluene ND ug/kg 10/29/20 23:53 95-49-810/29/20 14:456.7 4.8 1
4-Chlorotoluene ND ug/kg 10/29/20 23:53 106-43-410/29/20 14:456.7 4.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/29/20 23:53 96-12-810/29/20 14:456.7 6.2 1
Dibromochloromethane ND ug/kg 10/29/20 23:53 124-48-110/29/20 14:456.7 3.6 1
1,2-Dibromoethane (EDB)ND ug/kg 10/29/20 23:53 106-93-410/29/20 14:456.7 4.7 1
Dibromomethane ND ug/kg 10/29/20 23:53 74-95-310/29/20 14:456.7 3.3 1
1,2-Dichlorobenzene ND ug/kg 10/29/20 23:53 95-50-110/29/20 14:456.7 4.0 1
1,3-Dichlorobenzene ND ug/kg 10/29/20 23:53 541-73-110/29/20 14:456.7 5.5 1
1,4-Dichlorobenzene ND ug/kg 10/29/20 23:53 106-46-710/29/20 14:456.7 5.0 1
Dichlorodifluoromethane ND ug/kg 10/29/20 23:53 75-71-810/29/20 14:4513.4 2.3 1
1,1-Dichloroethane ND ug/kg 10/29/20 23:53 75-34-310/29/20 14:456.7 2.9 1
1,2-Dichloroethane ND ug/kg 10/29/20 23:53 107-06-210/29/20 14:456.7 2.7 1
1,1-Dichloroethene ND ug/kg 10/29/20 23:53 75-35-410/29/20 14:456.7 2.1 1
cis-1,2-Dichloroethene ND ug/kg 10/29/20 23:53 156-59-210/29/20 14:456.7 3.8 1
trans-1,2-Dichloroethene ND ug/kg 10/29/20 23:53 156-60-510/29/20 14:456.7 2.9 1
1,2-Dichloropropane ND ug/kg 10/29/20 23:53 78-87-510/29/20 14:456.7 4.2 1
1,3-Dichloropropane ND ug/kg 10/29/20 23:53 142-28-910/29/20 14:456.7 4.6 1
2,2-Dichloropropane ND ug/kg 10/29/20 23:53 594-20-710/29/20 14:456.7 3.7 1
1,1-Dichloropropene ND ug/kg 10/29/20 23:53 563-58-610/29/20 14:456.7 3.2 1
cis-1,3-Dichloropropene ND ug/kg 10/29/20 23:53 10061-01-510/29/20 14:456.7 4.3 1
trans-1,3-Dichloropropene ND ug/kg 10/29/20 23:53 10061-02-610/29/20 14:456.7 5.7 1
Diisopropyl ether ND ug/kg 10/29/20 23:53 108-20-310/29/20 14:456.7 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:DUP-1 Lab ID:92502685002 Collected:10/28/20 11:10 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 10/29/20 23:53 100-41-410/29/20 14:456.7 6.3 1
Hexachloro-1,3-butadiene ND ug/kg 10/29/20 23:53 87-68-310/29/20 14:456.7 6.3 1
2-Hexanone ND ug/kg 10/29/20 23:53 591-78-610/29/20 14:4566.9 13.3 1
Isopropylbenzene (Cumene)ND ug/kg 10/29/20 23:53 98-82-810/29/20 14:456.7 4.2 1
p-Isopropyltoluene ND ug/kg 10/29/20 23:53 99-87-610/29/20 14:456.7 3.7 1
Methylene Chloride 87.4 ug/kg 10/29/20 23:53 75-09-2 B,C910/29/20 14:4526.7 9.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/29/20 23:53 108-10-110/29/20 14:4566.9 56.6 1
Methyl-tert-butyl ether ND ug/kg 10/29/20 23:53 1634-04-410/29/20 14:456.7 4.3 1
Naphthalene ND ug/kg 10/29/20 23:53 91-20-3 IK10/29/20 14:456.7 3.8 1
n-Propylbenzene ND ug/kg 10/29/20 23:53 103-65-110/29/20 14:456.7 4.6 1
Styrene ND ug/kg 10/29/20 23:53 100-42-510/29/20 14:456.7 3.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/29/20 23:53 630-20-610/29/20 14:456.7 4.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/29/20 23:53 79-34-510/29/20 14:456.7 5.9 1
Tetrachloroethene ND ug/kg 10/29/20 23:53 127-18-410/29/20 14:456.7 3.3 1
Toluene 4.8J ug/kg 10/29/20 23:53 108-88-310/29/20 14:456.7 3.8 1
1,2,3-Trichlorobenzene ND ug/kg 10/29/20 23:53 87-61-6 IK10/29/20 14:456.7 4.1 1
1,2,4-Trichlorobenzene ND ug/kg 10/29/20 23:53 120-82-110/29/20 14:456.7 3.7 1
1,1,1-Trichloroethane ND ug/kg 10/29/20 23:53 71-55-610/29/20 14:456.7 2.7 1
1,1,2-Trichloroethane ND ug/kg 10/29/20 23:53 79-00-510/29/20 14:456.7 5.0 1
Trichloroethene ND ug/kg 10/29/20 23:53 79-01-610/29/20 14:456.7 4.2 1
Trichlorofluoromethane ND ug/kg 10/29/20 23:53 75-69-410/29/20 14:456.7 1.7 1
1,2,3-Trichloropropane ND ug/kg 10/29/20 23:53 96-18-410/29/20 14:456.7 5.4 1
1,2,4-Trimethylbenzene ND ug/kg 10/29/20 23:53 95-63-610/29/20 14:456.7 4.8 1
1,3,5-Trimethylbenzene ND ug/kg 10/29/20 23:53 108-67-810/29/20 14:456.7 4.0 1
Vinyl acetate ND ug/kg 10/29/20 23:53 108-05-410/29/20 14:4566.9 5.8 1
Vinyl chloride ND ug/kg 10/29/20 23:53 75-01-410/29/20 14:4513.4 2.6 1
Xylene (Total)ND ug/kg 10/29/20 23:53 1330-20-710/29/20 14:4513.4 3.8 1
m&p-Xylene ND ug/kg 10/29/20 23:53 179601-23-110/29/20 14:4513.4 10.3 1
o-Xylene ND ug/kg 10/29/20 23:53 95-47-610/29/20 14:456.7 3.8 1
Surrogates
Toluene-d8 (S)103 %10/29/20 23:53 2037-26-510/29/20 14:4570-130 1
4-Bromofluorobenzene (S)95 %10/29/20 23:53 460-00-410/29/20 14:4570-130 1
1,2-Dichloroethane-d4 (S)99 %10/29/20 23:53 17060-07-010/29/20 14:4570-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.6 %10/28/20 17:020.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.2 %11/01/20 05:2511/01/20 05:151
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:DUP-1 Lab ID:92502685002 Collected:10/28/20 11:10 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 10/31/20 00:02 18540-29-910/30/20 16:231.38 0.353 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:FG1-1-2 Lab ID:92502685003 Collected:10/28/20 11:00 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 10/30/20 00:11 67-64-110/29/20 14:4513349.5 1
Benzene ND ug/kg 10/30/20 00:11 71-43-210/29/20 14:456.6 4.7 1
Bromobenzene ND ug/kg 10/30/20 00:11 108-86-110/29/20 14:456.6 4.5 1
Bromochloromethane ND ug/kg 10/30/20 00:11 74-97-510/29/20 14:456.6 5.0 1
Bromodichloromethane ND ug/kg 10/30/20 00:11 75-27-410/29/20 14:456.6 4.4 1
Bromoform ND ug/kg 10/30/20 00:11 75-25-210/29/20 14:456.6 3.6 1
Bromomethane ND ug/kg 10/30/20 00:11 74-83-910/29/20 14:4513.3 10.4 1
2-Butanone (MEK)158 ug/kg 10/30/20 00:11 78-93-3 1g10/29/20 14:4513356.3 1
n-Butylbenzene ND ug/kg 10/30/20 00:11 104-51-810/29/20 14:456.6 3.6 1
sec-Butylbenzene ND ug/kg 10/30/20 00:11 135-98-810/29/20 14:456.6 4.2 1
tert-Butylbenzene ND ug/kg 10/30/20 00:11 98-06-610/29/20 14:456.6 3.6 1
Carbon tetrachloride ND ug/kg 10/30/20 00:11 56-23-510/29/20 14:456.6 2.9 1
Chlorobenzene ND ug/kg 10/30/20 00:11 108-90-710/29/20 14:456.6 4.3 1
Chloroethane ND ug/kg 10/30/20 00:11 75-00-3 IK10/29/20 14:4513.3 7.0 1
Chloroform ND ug/kg 10/30/20 00:11 67-66-310/29/20 14:456.6 3.3 1
Chloromethane ND ug/kg 10/30/20 00:11 74-87-310/29/20 14:4513.3 9.3 1
2-Chlorotoluene ND ug/kg 10/30/20 00:11 95-49-810/29/20 14:456.6 4.7 1
4-Chlorotoluene ND ug/kg 10/30/20 00:11 106-43-410/29/20 14:456.6 4.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/30/20 00:11 96-12-810/29/20 14:456.6 6.2 1
Dibromochloromethane ND ug/kg 10/30/20 00:11 124-48-110/29/20 14:456.6 3.6 1
1,2-Dibromoethane (EDB)ND ug/kg 10/30/20 00:11 106-93-410/29/20 14:456.6 4.7 1
Dibromomethane ND ug/kg 10/30/20 00:11 74-95-310/29/20 14:456.6 3.3 1
1,2-Dichlorobenzene ND ug/kg 10/30/20 00:11 95-50-110/29/20 14:456.6 3.9 1
1,3-Dichlorobenzene ND ug/kg 10/30/20 00:11 541-73-110/29/20 14:456.6 5.5 1
1,4-Dichlorobenzene ND ug/kg 10/30/20 00:11 106-46-710/29/20 14:456.6 5.0 1
Dichlorodifluoromethane ND ug/kg 10/30/20 00:11 75-71-810/29/20 14:4513.3 2.3 1
1,1-Dichloroethane ND ug/kg 10/30/20 00:11 75-34-310/29/20 14:456.6 2.9 1
1,2-Dichloroethane ND ug/kg 10/30/20 00:11 107-06-210/29/20 14:456.6 2.7 1
1,1-Dichloroethene ND ug/kg 10/30/20 00:11 75-35-410/29/20 14:456.6 2.1 1
cis-1,2-Dichloroethene ND ug/kg 10/30/20 00:11 156-59-210/29/20 14:456.6 3.8 1
trans-1,2-Dichloroethene ND ug/kg 10/30/20 00:11 156-60-510/29/20 14:456.6 2.9 1
1,2-Dichloropropane ND ug/kg 10/30/20 00:11 78-87-510/29/20 14:456.6 4.1 1
1,3-Dichloropropane ND ug/kg 10/30/20 00:11 142-28-910/29/20 14:456.6 4.6 1
2,2-Dichloropropane ND ug/kg 10/30/20 00:11 594-20-710/29/20 14:456.6 3.6 1
1,1-Dichloropropene ND ug/kg 10/30/20 00:11 563-58-610/29/20 14:456.6 3.2 1
cis-1,3-Dichloropropene ND ug/kg 10/30/20 00:11 10061-01-510/29/20 14:456.6 4.3 1
trans-1,3-Dichloropropene ND ug/kg 10/30/20 00:11 10061-02-610/29/20 14:456.6 5.6 1
Diisopropyl ether ND ug/kg 10/30/20 00:11 108-20-310/29/20 14:456.6 2.7 1
Ethylbenzene ND ug/kg 10/30/20 00:11 100-41-410/29/20 14:456.6 6.2 1
Hexachloro-1,3-butadiene ND ug/kg 10/30/20 00:11 87-68-310/29/20 14:456.6 6.3 1
2-Hexanone ND ug/kg 10/30/20 00:11 591-78-610/29/20 14:4566.3 13.2 1
Isopropylbenzene (Cumene)ND ug/kg 10/30/20 00:11 98-82-810/29/20 14:456.6 4.2 1
p-Isopropyltoluene ND ug/kg 10/30/20 00:11 99-87-610/29/20 14:456.6 3.7 1
Methylene Chloride 96.1 ug/kg 10/30/20 00:11 75-09-2 B,C910/29/20 14:4526.5 9.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:FG1-1-2 Lab ID:92502685003 Collected:10/28/20 11:00 Received:10/28/20 14:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/30/20 00:11 108-10-110/29/20 14:4566.3 56.1 1
Methyl-tert-butyl ether ND ug/kg 10/30/20 00:11 1634-04-410/29/20 14:456.6 4.2 1
Naphthalene ND ug/kg 10/30/20 00:11 91-20-3 IK10/29/20 14:456.6 3.7 1
n-Propylbenzene ND ug/kg 10/30/20 00:11 103-65-110/29/20 14:456.6 4.6 1
Styrene ND ug/kg 10/30/20 00:11 100-42-510/29/20 14:456.6 3.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/30/20 00:11 630-20-610/29/20 14:456.6 4.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/30/20 00:11 79-34-510/29/20 14:456.6 5.9 1
Tetrachloroethene ND ug/kg 10/30/20 00:11 127-18-410/29/20 14:456.6 3.3 1
Toluene 6.5J ug/kg 10/30/20 00:11 108-88-310/29/20 14:456.6 3.8 1
1,2,3-Trichlorobenzene ND ug/kg 10/30/20 00:11 87-61-6 IK10/29/20 14:456.6 4.1 1
1,2,4-Trichlorobenzene ND ug/kg 10/30/20 00:11 120-82-110/29/20 14:456.6 3.7 1
1,1,1-Trichloroethane ND ug/kg 10/30/20 00:11 71-55-610/29/20 14:456.6 2.7 1
1,1,2-Trichloroethane ND ug/kg 10/30/20 00:11 79-00-510/29/20 14:456.6 4.9 1
Trichloroethene ND ug/kg 10/30/20 00:11 79-01-610/29/20 14:456.6 4.1 1
Trichlorofluoromethane ND ug/kg 10/30/20 00:11 75-69-410/29/20 14:456.6 1.6 1
1,2,3-Trichloropropane ND ug/kg 10/30/20 00:11 96-18-410/29/20 14:456.6 5.4 1
1,2,4-Trimethylbenzene ND ug/kg 10/30/20 00:11 95-63-610/29/20 14:456.6 4.8 1
1,3,5-Trimethylbenzene ND ug/kg 10/30/20 00:11 108-67-810/29/20 14:456.6 4.0 1
Vinyl acetate ND ug/kg 10/30/20 00:11 108-05-410/29/20 14:4566.3 5.7 1
Vinyl chloride ND ug/kg 10/30/20 00:11 75-01-410/29/20 14:4513.3 2.5 1
Xylene (Total)ND ug/kg 10/30/20 00:11 1330-20-710/29/20 14:4513.3 3.8 1
m&p-Xylene ND ug/kg 10/30/20 00:11 179601-23-110/29/20 14:4513.3 10.2 1
o-Xylene ND ug/kg 10/30/20 00:11 95-47-610/29/20 14:456.6 3.8 1
Surrogates
Toluene-d8 (S)106 %10/30/20 00:11 2037-26-510/29/20 14:4570-130 1
4-Bromofluorobenzene (S)96 %10/30/20 00:11 460-00-410/29/20 14:4570-130 1
1,2-Dichloroethane-d4 (S)101 %10/30/20 00:11 17060-07-010/29/20 14:4570-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.0 %10/28/20 17:020.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Page 14 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:RB-1 Lab ID:92502685004 Collected:10/28/20 09:30 Received:10/28/20 14:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 11/02/20 01:40 7440-38-210/31/20 20:322.00 0.180 1
Barium ND ug/L 11/02/20 01:40 7440-39-310/31/20 20:3220.0 0.381 1
Cadmium ND ug/L 11/02/20 01:40 7440-43-910/31/20 20:321.00 0.150 1
Chromium ND ug/L 11/02/20 01:40 7440-47-310/31/20 20:322.00 1.24 1
Lead ND ug/L 11/02/20 01:40 7439-92-110/31/20 20:325.00 0.849 1
Selenium ND ug/L 11/02/20 01:40 7782-49-210/31/20 20:322.00 0.300 1
Silver ND ug/L 11/02/20 01:40 7440-22-410/31/20 20:322.00 0.0700 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 10/30/20 13:51 7439-97-610/30/20 09:050.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/30/20 11:42 83-32-910/29/20 06:5410.0 2.0 1
Acenaphthylene ND ug/L 10/30/20 11:42 208-96-810/29/20 06:5410.0 2.0 1
Aniline ND ug/L 10/30/20 11:42 62-53-310/29/20 06:5410.0 1.6 1
Anthracene ND ug/L 10/30/20 11:42 120-12-710/29/20 06:5410.0 2.3 1
Benzo(a)anthracene ND ug/L 10/30/20 11:42 56-55-310/29/20 06:5410.0 2.7 1
Benzo(a)pyrene ND ug/L 10/30/20 11:42 50-32-810/29/20 06:5410.0 2.8 1
Benzo(b)fluoranthene ND ug/L 10/30/20 11:42 205-99-210/29/20 06:5410.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 10/30/20 11:42 191-24-210/29/20 06:5410.0 2.8 1
Benzo(k)fluoranthene ND ug/L 10/30/20 11:42 207-08-910/29/20 06:5410.0 2.7 1
Benzoic Acid ND ug/L 10/30/20 11:42 65-85-010/29/20 06:5450.0 3.4 1
Benzyl alcohol ND ug/L 10/30/20 11:42 100-51-610/29/20 06:5420.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 10/30/20 11:42 101-55-310/29/20 06:5410.0 1.8 1
Butylbenzylphthalate ND ug/L 10/30/20 11:42 85-68-710/29/20 06:5410.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 10/30/20 11:42 59-50-710/29/20 06:5410.0 3.3 1
4-Chloroaniline ND ug/L 10/30/20 11:42 106-47-810/29/20 06:5420.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 10/30/20 11:42 111-91-110/29/20 06:5410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 10/30/20 11:42 111-44-410/29/20 06:5410.0 1.9 1
2-Chloronaphthalene ND ug/L 10/30/20 11:42 91-58-710/29/20 06:5410.0 1.7 1
2-Chlorophenol ND ug/L 10/30/20 11:42 95-57-810/29/20 06:5410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 10/30/20 11:42 7005-72-310/29/20 06:5410.0 2.0 1
Chrysene ND ug/L 10/30/20 11:42 218-01-910/29/20 06:5410.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 10/30/20 11:42 53-70-310/29/20 06:5410.0 3.0 1
Dibenzofuran ND ug/L 10/30/20 11:42 132-64-910/29/20 06:5410.0 2.1 1
1,2-Dichlorobenzene ND ug/L 10/30/20 11:42 95-50-110/29/20 06:5410.0 1.8 1
1,3-Dichlorobenzene ND ug/L 10/30/20 11:42 541-73-110/29/20 06:5410.0 1.6 1
1,4-Dichlorobenzene ND ug/L 10/30/20 11:42 106-46-710/29/20 06:5410.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 10/30/20 11:42 91-94-110/29/20 06:5420.0 8.1 1
2,4-Dichlorophenol ND ug/L 10/30/20 11:42 120-83-210/29/20 06:5410.0 1.4 1
Diethylphthalate ND ug/L 10/30/20 11:42 84-66-210/29/20 06:5410.0 2.0 1
2,4-Dimethylphenol ND ug/L 10/30/20 11:42 105-67-910/29/20 06:5410.0 1.7 1
Dimethylphthalate ND ug/L 10/30/20 11:42 131-11-310/29/20 06:5410.0 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Page 15 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:RB-1 Lab ID:92502685004 Collected:10/28/20 09:30 Received:10/28/20 14:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 10/30/20 11:42 84-74-210/29/20 06:5410.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 10/30/20 11:42 534-52-110/29/20 06:5420.0 3.4 1
2,4-Dinitrophenol ND ug/L 10/30/20 11:42 51-28-510/29/20 06:5450.0 26.0 1
2,4-Dinitrotoluene ND ug/L 10/30/20 11:42 121-14-210/29/20 06:5410.0 1.6 1
2,6-Dinitrotoluene ND ug/L 10/30/20 11:42 606-20-210/29/20 06:5410.0 1.7 1
Di-n-octylphthalate ND ug/L 10/30/20 11:42 117-84-010/29/20 06:5410.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/30/20 11:42 117-81-710/29/20 06:546.0 3.7 1
Fluoranthene ND ug/L 10/30/20 11:42 206-44-010/29/20 06:5410.0 2.2 1
Fluorene ND ug/L 10/30/20 11:42 86-73-710/29/20 06:5410.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 10/30/20 11:42 87-68-310/29/20 06:5410.0 1.8 1
Hexachlorobenzene ND ug/L 10/30/20 11:42 118-74-110/29/20 06:5410.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 10/30/20 11:42 77-47-410/29/20 06:5410.0 1.6 1
Hexachloroethane ND ug/L 10/30/20 11:42 67-72-110/29/20 06:5410.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/30/20 11:42 193-39-510/29/20 06:5410.0 2.9 1
Isophorone ND ug/L 10/30/20 11:42 78-59-110/29/20 06:5410.0 1.7 1
1-Methylnaphthalene ND ug/L 10/30/20 11:42 90-12-010/29/20 06:5410.0 2.0 1
2-Methylnaphthalene ND ug/L 10/30/20 11:42 91-57-610/29/20 06:5410.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 10/30/20 11:42 95-48-710/29/20 06:5410.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/30/20 11:42 15831-10-410/29/20 06:5410.0 1.2 1
Naphthalene ND ug/L 10/30/20 11:42 91-20-310/29/20 06:5410.0 2.1 1
2-Nitroaniline ND ug/L 10/30/20 11:42 88-74-410/29/20 06:5420.0 3.0 1
3-Nitroaniline ND ug/L 10/30/20 11:42 99-09-210/29/20 06:5420.0 3.8 1
4-Nitroaniline ND ug/L 10/30/20 11:42 100-01-610/29/20 06:5420.0 5.1 1
Nitrobenzene ND ug/L 10/30/20 11:42 98-95-310/29/20 06:5410.0 1.9 1
2-Nitrophenol ND ug/L 10/30/20 11:42 88-75-510/29/20 06:5410.0 1.4 1
4-Nitrophenol ND ug/L 10/30/20 11:42 100-02-710/29/20 06:5450.0 6.6 1
N-Nitrosodimethylamine ND ug/L 10/30/20 11:42 62-75-910/29/20 06:5410.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 10/30/20 11:42 621-64-710/29/20 06:5410.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 10/30/20 11:42 86-30-610/29/20 06:5410.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/30/20 11:42 108-60-110/29/20 06:5410.0 1.2 1
Pentachlorophenol ND ug/L 10/30/20 11:42 87-86-510/29/20 06:5420.0 3.8 1
Phenanthrene ND ug/L 10/30/20 11:42 85-01-810/29/20 06:5410.0 2.0 1
Phenol ND ug/L 10/30/20 11:42 108-95-210/29/20 06:5410.0 1.4 1
Pyrene ND ug/L 10/30/20 11:42 129-00-010/29/20 06:5410.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 10/30/20 11:42 120-82-110/29/20 06:5410.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 10/30/20 11:42 95-95-410/29/20 06:5410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 10/30/20 11:42 88-06-210/29/20 06:5410.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)106 %10/30/20 11:42 4165-60-010/29/20 06:5410-144 1
2-Fluorobiphenyl (S)90 %10/30/20 11:42 321-60-810/29/20 06:5410-130 1
Terphenyl-d14 (S)114 %10/30/20 11:42 1718-51-010/29/20 06:5434-163 1
Phenol-d6 (S)46 %10/30/20 11:42 13127-88-310/29/20 06:5410-130 1
2-Fluorophenol (S)61 %10/30/20 11:42 367-12-410/29/20 06:5410-130 1
2,4,6-Tribromophenol (S)92 %10/30/20 11:42 118-79-610/29/20 06:5410-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:RB-1 Lab ID:92502685004 Collected:10/28/20 09:30 Received:10/28/20 14:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 10/29/20 16:59 67-64-125.0 6.2 1
Benzene ND ug/L 10/29/20 16:59 71-43-21.0 0.15 1
Bromobenzene ND ug/L 10/29/20 16:59 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 10/29/20 16:59 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 10/29/20 16:59 75-27-41.0 0.26 1
Bromoform ND ug/L 10/29/20 16:59 75-25-21.0 0.62 1
Bromomethane ND ug/L 10/29/20 16:59 74-83-9 IK,v22.0 0.62 1
2-Butanone (MEK)ND ug/L 10/29/20 16:59 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 10/29/20 16:59 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 10/29/20 16:59 108-90-71.0 0.23 1
Chloroethane ND ug/L 10/29/20 16:59 75-00-31.0 0.49 1
Chloroform ND ug/L 10/29/20 16:59 67-66-35.0 2.3 1
Chloromethane ND ug/L 10/29/20 16:59 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 10/29/20 16:59 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 10/29/20 16:59 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 10/29/20 16:59 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 10/29/20 16:59 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 10/29/20 16:59 106-93-41.0 0.26 1
Dibromomethane ND ug/L 10/29/20 16:59 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 10/29/20 16:59 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 10/29/20 16:59 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 10/29/20 16:59 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 10/29/20 16:59 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 10/29/20 16:59 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 10/29/20 16:59 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 10/29/20 16:59 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 10/29/20 16:59 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 10/29/20 16:59 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 10/29/20 16:59 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 10/29/20 16:59 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 10/29/20 16:59 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 10/29/20 16:59 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 10/29/20 16:59 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 10/29/20 16:59 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 10/29/20 16:59 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 10/29/20 16:59 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 10/29/20 16:59 87-68-3 IK1.0 0.44 1
2-Hexanone ND ug/L 10/29/20 16:59 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 10/29/20 16:59 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 10/29/20 16:59 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/29/20 16:59 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 10/29/20 16:59 1634-04-41.0 0.28 1
Naphthalene ND ug/L 10/29/20 16:59 91-20-31.0 0.35 1
Styrene ND ug/L 10/29/20 16:59 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 10/29/20 16:59 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 17 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92502685
BCP-064
Sample:RB-1 Lab ID:92502685004 Collected:10/28/20 09:30 Received:10/28/20 14:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 10/29/20 16:59 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 10/29/20 16:59 127-18-41.0 0.16 1
Toluene ND ug/L 10/29/20 16:59 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 10/29/20 16:59 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 10/29/20 16:59 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 10/29/20 16:59 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 10/29/20 16:59 79-00-51.0 0.24 1
Trichloroethene ND ug/L 10/29/20 16:59 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 10/29/20 16:59 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 10/29/20 16:59 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 10/29/20 16:59 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 10/29/20 16:59 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 10/29/20 16:59 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 10/29/20 16:59 179601-23-12.0 0.41 1
o-Xylene ND ug/L 10/29/20 16:59 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %10/29/20 16:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %10/29/20 16:59 17060-07-070-130 1
Toluene-d8 (S)102 %10/29/20 16:59 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.0584J ug/L 11/02/20 15:12 18540-29-9 J11/02/20 15:120.100 0.0400 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 18 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1568783
3015
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92502685004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3588281-1
Associated Lab Samples:92502685004
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 2.00 11/02/20 01:100.180
Barium ug/L ND 20.0 11/02/20 01:100.381
Cadmium ug/L ND 1.00 11/02/20 01:100.150
Chromium ug/L ND 2.00 11/02/20 01:101.24
Lead ug/L ND 5.00 11/02/20 01:100.849
Selenium ug/L ND 2.00 11/02/20 01:100.300
Silver ug/L ND 2.00 11/02/20 01:100.0700
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3588281-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 47.050.0 94.1 80.0-120
Barium ug/L 47.450.0 94.7 80.0-120
Cadmium ug/L 49.350.0 98.6 80.0-120
Chromium ug/L 46.950.0 93.9 80.0-120
Lead ug/L 45.450.0 90.8 80.0-120
Selenium ug/L 48.050.0 95.9 80.0-120
Silver ug/L 47.150.0 94.3 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3588387-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1278404-01
R3588387-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 50.0 97.4 75.0-12595.6 1.78 2050.00.209 48.9 48.0
Barium ug/L 50.0 98.8 75.0-125101 2.17 2050.04.61 54.0 55.2
Cadmium ug/L 50.0 98.9 75.0-125103 4.05 2050.0ND 49.4 51.5
Chromium ug/L 50.0 99.0 75.0-12599.0 0.093 2050.0ND 49.5 49.5
Lead ug/L 50.0 90.2 75.0-12593.8 3.93 2050.0ND 45.1 46.9
Selenium ug/L 50.0 113 75.0-125110 2.47 2050.0ND 56.5 55.1
Silver ug/L 50.0 97.0 75.0-125102 4.68 2050.0ND 48.5 50.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 19 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1568639
3050B
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92502685001, 92502685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3588147-1
Associated Lab Samples:92502685001, 92502685002
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 1.00 11/01/20 22:100.100
Barium mg/kg ND 2.50 11/01/20 22:100.152
Cadmium mg/kg ND 1.00 11/01/20 22:100.0855
Chromium mg/kg ND 5.00 11/01/20 22:100.297
Lead mg/kg ND 2.00 11/01/20 22:100.0990
Selenium mg/kg ND 2.50 11/01/20 22:100.180
Silver mg/kg ND 0.500 11/01/20 22:100.0865
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3588147-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 94.1100 94.1 80.0-120
Barium mg/kg 93.9100 93.9 80.0-120
Cadmium mg/kg 101100 101 80.0-120
Chromium mg/kg 96.9100 96.9 80.0-120
Lead mg/kg 95.3100 95.3 80.0-120
Selenium mg/kg 116100 116 80.0-120
Silver mg/kg 19.420.0 97.1 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3588147-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1279016-01
R3588147-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 22.4 90.1 75.0-12591.9 1.89 2022.45.09 106 108
Barium mg/kg 22.4 115 75.0-12595.6 10.1 2022.499.5 228 206
Cadmium mg/kg 22.4 98.0 75.0-125101 2.64 2022.40.503 110 113
Chromium mg/kg 22.4 100 75.0-12595.7 3.76 2022.416.9 129 124
Lead mg/kg MH,R122.4 399 75.0-125224 46.1 2022.474.2 520 325
Selenium mg/kg 22.4 112 75.0-125115 3.08 2022.40.414 126 129
Silver mg/kg 4.47 98.0 75.0-12598.9 0.845 204.470.140 22.0 22.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1568119
7470A
EPA 7470A
Mercury 7470A
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92502685004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3587602-1
Associated Lab Samples:92502685004
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.200 10/30/20 13:150.100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3587602-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.843.00 94.7 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3587602-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1279404-08
R3587602-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 3.00 90.9 75.0-12591.9 1.07 203.00ND 2.73 2.76
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1568187
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92502685001, 92502685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3587821-1
Associated Lab Samples:92502685001, 92502685002
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 10/31/20 07:310.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3587821-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.4660.500 93.2 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3587821-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1278273-02
R3587821-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.632 85.8 75.0-12590.8 5.28 200.6320.0418 0.584 0.615
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
576753
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92502685002, 92502685003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3052124
Associated Lab Samples:92502685002, 92502685003
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 10/29/20 22:423.3
1,1,1-Trichloroethane ug/kg ND 5.0 10/29/20 22:422.0
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 10/29/20 22:424.4
1,1,2-Trichloroethane ug/kg ND 5.0 10/29/20 22:423.7
1,1-Dichloroethane ug/kg ND 5.0 10/29/20 22:422.2
1,1-Dichloroethene ug/kg ND 5.0 10/29/20 22:421.6
1,1-Dichloropropene ug/kg ND 5.0 10/29/20 22:422.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 IK10/29/20 22:423.1
1,2,3-Trichloropropane ug/kg ND 5.0 10/29/20 22:424.1
1,2,4-Trichlorobenzene ug/kg ND 5.0 10/29/20 22:422.8
1,2,4-Trimethylbenzene ug/kg ND 5.0 10/29/20 22:423.6
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 10/29/20 22:424.6
1,2-Dibromoethane (EDB)ug/kg ND 5.0 10/29/20 22:423.5
1,2-Dichlorobenzene ug/kg ND 5.0 10/29/20 22:423.0
1,2-Dichloroethane ug/kg ND 5.0 10/29/20 22:422.0
1,2-Dichloropropane ug/kg ND 5.0 10/29/20 22:423.1
1,3,5-Trimethylbenzene ug/kg ND 5.0 10/29/20 22:423.0
1,3-Dichlorobenzene ug/kg ND 5.0 10/29/20 22:424.1
1,3-Dichloropropane ug/kg ND 5.0 10/29/20 22:423.5
1,4-Dichlorobenzene ug/kg ND 5.0 10/29/20 22:423.8
2,2-Dichloropropane ug/kg ND 5.0 10/29/20 22:422.8
2-Butanone (MEK)ug/kg ND 100 10/29/20 22:4242.4
2-Chlorotoluene ug/kg ND 5.0 10/29/20 22:423.6
2-Hexanone ug/kg ND 50.0 10/29/20 22:429.9
4-Chlorotoluene ug/kg ND 5.0 10/29/20 22:423.2
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 10/29/20 22:4242.3
Acetone ug/kg ND 100 10/29/20 22:4237.3
Benzene ug/kg ND 5.0 10/29/20 22:423.5
Bromobenzene ug/kg ND 5.0 10/29/20 22:423.4
Bromochloromethane ug/kg ND 5.0 10/29/20 22:423.8
Bromodichloromethane ug/kg ND 5.0 10/29/20 22:423.3
Bromoform ug/kg ND 5.0 10/29/20 22:422.7
Bromomethane ug/kg ND 10.0 10/29/20 22:427.9
Carbon tetrachloride ug/kg ND 5.0 10/29/20 22:422.2
Chlorobenzene ug/kg ND 5.0 10/29/20 22:423.2
Chloroethane ug/kg ND 10.0 IK10/29/20 22:425.3
Chloroform ug/kg ND 5.0 10/29/20 22:422.5
Chloromethane ug/kg ND 10.0 10/29/20 22:427.0
cis-1,2-Dichloroethene ug/kg ND 5.0 10/29/20 22:422.9
cis-1,3-Dichloropropene ug/kg ND 5.0 10/29/20 22:423.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3052124
Associated Lab Samples:92502685002, 92502685003
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 10/29/20 22:422.7
Dibromomethane ug/kg ND 5.0 10/29/20 22:422.5
Dichlorodifluoromethane ug/kg ND 10.0 10/29/20 22:421.7
Diisopropyl ether ug/kg ND 5.0 10/29/20 22:422.0
Ethylbenzene ug/kg ND 5.0 10/29/20 22:424.7
Hexachloro-1,3-butadiene ug/kg ND 5.0 10/29/20 22:424.7
Isopropylbenzene (Cumene)ug/kg ND 5.0 10/29/20 22:423.2
m&p-Xylene ug/kg ND 10.0 10/29/20 22:427.7
Methyl-tert-butyl ether ug/kg ND 5.0 10/29/20 22:423.2
Methylene Chloride ug/kg 17.1J 20.0 10/29/20 22:427.4
n-Butylbenzene ug/kg ND 5.0 10/29/20 22:422.7
n-Propylbenzene ug/kg ND 5.0 10/29/20 22:423.4
Naphthalene ug/kg ND 5.0 IK10/29/20 22:422.8
o-Xylene ug/kg ND 5.0 10/29/20 22:422.8
p-Isopropyltoluene ug/kg ND 5.0 10/29/20 22:422.8
sec-Butylbenzene ug/kg ND 5.0 10/29/20 22:423.2
Styrene ug/kg ND 5.0 10/29/20 22:422.4
tert-Butylbenzene ug/kg ND 5.0 10/29/20 22:422.7
Tetrachloroethene ug/kg ND 5.0 10/29/20 22:422.5
Toluene ug/kg ND 5.0 10/29/20 22:422.9
trans-1,2-Dichloroethene ug/kg ND 5.0 10/29/20 22:422.2
trans-1,3-Dichloropropene ug/kg ND 5.0 10/29/20 22:424.2
Trichloroethene ug/kg ND 5.0 10/29/20 22:423.1
Trichlorofluoromethane ug/kg ND 5.0 10/29/20 22:421.2
Vinyl acetate ug/kg ND 50.0 10/29/20 22:424.3
Vinyl chloride ug/kg ND 10.0 10/29/20 22:421.9
Xylene (Total)ug/kg ND 10.0 10/29/20 22:422.8
1,2-Dichloroethane-d4 (S)%102 70-132 10/29/20 22:42
4-Bromofluorobenzene (S)%93 70-130 10/29/20 22:42
Toluene-d8 (S)%102 70-130 10/29/20 22:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3052125LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12301250 99 70-130
1,1,1-Trichloroethane ug/kg 12801250 102 70-130
1,1,2,2-Tetrachloroethane ug/kg 12001250 96 55-130
1,1,2-Trichloroethane ug/kg 13001250 104 70-130
1,1-Dichloroethane ug/kg 13801250 111 68-130
1,1-Dichloroethene ug/kg 14301250 114 70-130
1,1-Dichloropropene ug/kg 13801250 111 70-130
1,2,3-Trichlorobenzene ug/kg 1210 IK12509770-130
1,2,3-Trichloropropane ug/kg 12301250 99 70-130
1,2,4-Trichlorobenzene ug/kg 13201250 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3052125LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12501250 100 69-130
1,2-Dibromo-3-chloropropane ug/kg 13701250 110 57-141
1,2-Dibromoethane (EDB)ug/kg 13301250 107 70-130
1,2-Dichlorobenzene ug/kg 13301250 106 70-130
1,2-Dichloroethane ug/kg 12801250 102 70-130
1,2-Dichloropropane ug/kg 13601250 109 70-130
1,3,5-Trimethylbenzene ug/kg 13101250 105 70-130
1,3-Dichlorobenzene ug/kg 13101250 105 70-130
1,3-Dichloropropane ug/kg 13101250 104 70-130
1,4-Dichlorobenzene ug/kg 12901250 103 70-130
2,2-Dichloropropane ug/kg 12901250 103 70-130
2-Butanone (MEK)ug/kg 27902500 112 60-130
2-Chlorotoluene ug/kg 13001250 104 70-130
2-Hexanone ug/kg 25602500 102 70-132
4-Chlorotoluene ug/kg 12701250 102 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 26302500 105 69-130
Acetone ug/kg 28402500 114 49-148
Benzene ug/kg 13001250 104 70-130
Bromobenzene ug/kg 13301250 106 70-130
Bromochloromethane ug/kg 14401250 115 70-130
Bromodichloromethane ug/kg 11801250 95 70-130
Bromoform ug/kg 12101250 97 68-136
Bromomethane ug/kg 14901250 119 60-140
Carbon tetrachloride ug/kg 12701250 102 70-130
Chlorobenzene ug/kg 12501250 100 70-130
Chloroethane ug/kg 1290 IK125010351-147
Chloroform ug/kg 12701250 102 70-130
Chloromethane ug/kg 11901250 96 48-130
cis-1,2-Dichloroethene ug/kg 13301250 107 70-130
cis-1,3-Dichloropropene ug/kg 13701250 109 70-130
Dibromochloromethane ug/kg 14001250 112 70-130
Dibromomethane ug/kg 13501250 108 70-130
Dichlorodifluoromethane ug/kg 13001250 104 49-130
Diisopropyl ether ug/kg 13301250 107 66-130
Ethylbenzene ug/kg 11901250 95 70-130
Hexachloro-1,3-butadiene ug/kg 12301250 99 70-130
Isopropylbenzene (Cumene)ug/kg 12101250 97 70-130
m&p-Xylene ug/kg 24902500 99 70-130
Methyl-tert-butyl ether ug/kg 13001250 104 70-130
Methylene Chloride ug/kg 13901250 111 50-137
n-Butylbenzene ug/kg 12701250 101 70-130
n-Propylbenzene ug/kg 12601250 101 70-130
Naphthalene ug/kg 1290 IK125010370-131
o-Xylene ug/kg 12501250 100 70-130
p-Isopropyltoluene ug/kg 12801250 102 70-130
sec-Butylbenzene ug/kg 12201250 98 70-130
Styrene ug/kg 12501250 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3052125LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 10101250 81 69-130
Tetrachloroethene ug/kg 11901250 95 56-130
Toluene ug/kg 12801250 103 70-130
trans-1,2-Dichloroethene ug/kg 13901250 111 70-130
trans-1,3-Dichloropropene ug/kg 12901250 103 70-130
Trichloroethene ug/kg 13301250 106 70-141
Trichlorofluoromethane ug/kg 10501250 84 67-130
Vinyl acetate ug/kg 29802500 119 10-136
Vinyl chloride ug/kg 10301250 82 67-130
Xylene (Total)ug/kg 37403750 100 70-130
1,2-Dichloroethane-d4 (S)%88 70-132
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3052127MATRIX SPIKE SAMPLE:
MSSpike
Result
92502210002
1,1,1,2-Tetrachloroethane ug/kg 650700 93 52-133ND
1,1,1-Trichloroethane ug/kg 678700 97 49-137ND
1,1,2,2-Tetrachloroethane ug/kg 624700 89 39-150ND
1,1,2-Trichloroethane ug/kg 761700 109 48-140ND
1,1-Dichloroethane ug/kg 686700 98 46-135ND
1,1-Dichloroethene ug/kg 773700 110 38-149ND
1,1-Dichloropropene ug/kg 702700 100 41-140ND
1,2,3-Trichlorobenzene ug/kg 542 IK7007710-158ND
1,2,3-Trichloropropane ug/kg 617700 88 33-157ND
1,2,4-Trichlorobenzene ug/kg 715700 102 10-155ND
1,2,4-Trimethylbenzene ug/kg 711700 101 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 496700 71 33-158ND
1,2-Dibromoethane (EDB)ug/kg 690700 99 40-136ND
1,2-Dichlorobenzene ug/kg 747700 107 27-146ND
1,2-Dichloroethane ug/kg 705700 101 49-140ND
1,2-Dichloropropane ug/kg 767700 109 44-143ND
1,3,5-Trimethylbenzene ug/kg 720700 103 40-144ND
1,3-Dichlorobenzene ug/kg 710700 101 33-140ND
1,3-Dichloropropane ug/kg 709700 101 47-147ND
1,4-Dichlorobenzene ug/kg 696700 99 35-139ND
2,2-Dichloropropane ug/kg 474700 68 41-140ND
2-Butanone (MEK)ug/kg 5761410 30 10-181155
2-Chlorotoluene ug/kg 716700 102 38-147ND
2-Hexanone ug/kg 6221410 44 18-169ND
4-Chlorotoluene ug/kg 707700 101 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 13701410 98 16-175ND
Acetone ug/kg 6391410 46 10-200ND
Benzene ug/kg 692700 99 46-136ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3052127MATRIX SPIKE SAMPLE:
MSSpike
Result
92502210002
Bromobenzene ug/kg 729700 104 38-149ND
Bromochloromethane ug/kg 756700 108 44-142ND
Bromodichloromethane ug/kg 653700 93 41-140ND
Bromoform ug/kg 589700 84 34-145ND
Bromomethane ug/kg 666 v27009514-162ND
Carbon tetrachloride ug/kg 627700 90 44-141ND
Chlorobenzene ug/kg 679700 97 39-141ND
Chloroethane ug/kg 178 IK7002510-182ND
Chloroform ug/kg 666700 95 45-140ND
Chloromethane ug/kg 742700 106 19-149ND
cis-1,2-Dichloroethene ug/kg 735700 105 38-150ND
cis-1,3-Dichloropropene ug/kg 717700 102 30-144ND
Dibromochloromethane ug/kg 697700 99 36-145ND
Dibromomethane ug/kg 752700 107 41-145ND
Dichlorodifluoromethane ug/kg 737700 105 16-146ND
Diisopropyl ether ug/kg 680700 97 41-143ND
Ethylbenzene ug/kg 652700 93 35-144ND
Hexachloro-1,3-butadiene ug/kg 738700 105 10-160ND
Isopropylbenzene (Cumene)ug/kg 660700 94 30-152ND
m&p-Xylene ug/kg 13301410 95 33-145ND
Methyl-tert-butyl ether ug/kg 665700 95 49-140ND
Methylene Chloride ug/kg 849700 106 10-174107
n-Butylbenzene ug/kg 680700 97 10-160ND
n-Propylbenzene ug/kg 714700 102 24-159ND
Naphthalene ug/kg 430 IK7006110-171ND
o-Xylene ug/kg 702700 100 31-150ND
p-Isopropyltoluene ug/kg 717700 102 21-154ND
sec-Butylbenzene ug/kg 696700 99 19-159ND
Styrene ug/kg 693700 99 15-152ND
tert-Butylbenzene ug/kg 568700 81 31-141ND
Tetrachloroethene ug/kg 611700 87 19-141ND
Toluene ug/kg 734700 104 31-1464.9J
trans-1,2-Dichloroethene ug/kg 766700 109 28-157ND
trans-1,3-Dichloropropene ug/kg 655700 94 25-146ND
Trichloroethene ug/kg 742700 106 34-149ND
Trichlorofluoromethane ug/kg 114700 16 10-167ND
Vinyl acetate ug/kg 13101410 94 10-200ND
Vinyl chloride ug/kg 639700 91 36-155ND
Xylene (Total)ug/kg 20302100 97 29-148ND
1,2-Dichloroethane-d4 (S)%112 70-132
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92502210001
3052126SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND IK30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30161
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND v230ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND IK30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92502210001
3052126SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 91.5 26 3070.4
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND IK30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 7.1 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%96100
4-Bromofluorobenzene (S)%9595
Toluene-d8 (S)%102103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
576679
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92502685004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3051826
Associated Lab Samples:92502685004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/29/20 11:220.34
1,1,1-Trichloroethane ug/L ND 1.0 10/29/20 11:220.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/29/20 11:220.22
1,1,2-Trichloroethane ug/L ND 1.0 10/29/20 11:220.24
1,1-Dichloroethane ug/L ND 1.0 10/29/20 11:220.27
1,1-Dichloroethene ug/L ND 1.0 10/29/20 11:220.24
1,1-Dichloropropene ug/L ND 1.0 10/29/20 11:220.21
1,2,3-Trichlorobenzene ug/L ND 1.0 10/29/20 11:220.34
1,2,3-Trichloropropane ug/L ND 1.0 10/29/20 11:220.35
1,2,4-Trichlorobenzene ug/L ND 1.0 10/29/20 11:220.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 10/29/20 11:220.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/29/20 11:220.26
1,2-Dichlorobenzene ug/L ND 1.0 10/29/20 11:220.29
1,2-Dichloroethane ug/L ND 1.0 10/29/20 11:220.34
1,2-Dichloropropane ug/L ND 1.0 10/29/20 11:220.19
1,3-Dichlorobenzene ug/L ND 1.0 10/29/20 11:220.22
1,3-Dichloropropane ug/L ND 1.0 10/29/20 11:220.16
1,4-Dichlorobenzene ug/L ND 1.0 10/29/20 11:220.26
2,2-Dichloropropane ug/L ND 1.0 10/29/20 11:220.27
2-Butanone (MEK)ug/L ND 5.0 10/29/20 11:223.3
2-Chlorotoluene ug/L ND 1.0 10/29/20 11:220.20
2-Hexanone ug/L ND 5.0 10/29/20 11:220.57
4-Chlorotoluene ug/L ND 1.0 10/29/20 11:220.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/29/20 11:224.5
Acetone ug/L ND 25.0 10/29/20 11:226.2
Benzene ug/L ND 1.0 10/29/20 11:220.15
Bromobenzene ug/L ND 1.0 10/29/20 11:220.22
Bromochloromethane ug/L ND 1.0 10/29/20 11:220.34
Bromodichloromethane ug/L ND 1.0 10/29/20 11:220.26
Bromoform ug/L ND 1.0 10/29/20 11:220.62
Bromomethane ug/L ND 2.0 IK,v210/29/20 11:220.62
Carbon tetrachloride ug/L ND 1.0 10/29/20 11:220.22
Chlorobenzene ug/L ND 1.0 10/29/20 11:220.23
Chloroethane ug/L ND 1.0 10/29/20 11:220.49
Chloroform ug/L ND 5.0 10/29/20 11:222.3
Chloromethane ug/L ND 1.0 10/29/20 11:220.39
cis-1,2-Dichloroethene ug/L ND 1.0 10/29/20 11:220.29
cis-1,3-Dichloropropene ug/L ND 1.0 10/29/20 11:220.30
Dibromochloromethane ug/L ND 1.0 10/29/20 11:220.41
Dibromomethane ug/L ND 1.0 10/29/20 11:220.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3051826
Associated Lab Samples:92502685004
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 10/29/20 11:220.23
Diisopropyl ether ug/L ND 1.0 10/29/20 11:220.22
Ethylbenzene ug/L ND 1.0 10/29/20 11:220.26
Hexachloro-1,3-butadiene ug/L ND 1.0 IK10/29/20 11:220.44
m&p-Xylene ug/L ND 2.0 10/29/20 11:220.41
Methyl-tert-butyl ether ug/L ND 1.0 10/29/20 11:220.28
Methylene Chloride ug/L ND 5.0 10/29/20 11:223.7
Naphthalene ug/L ND 1.0 10/29/20 11:220.35
o-Xylene ug/L ND 1.0 10/29/20 11:220.22
p-Isopropyltoluene ug/L ND 1.0 10/29/20 11:220.21
Styrene ug/L ND 1.0 10/29/20 11:220.27
Tetrachloroethene ug/L ND 1.0 10/29/20 11:220.16
Toluene ug/L ND 1.0 10/29/20 11:220.24
trans-1,2-Dichloroethene ug/L ND 1.0 10/29/20 11:220.25
trans-1,3-Dichloropropene ug/L ND 1.0 10/29/20 11:220.31
Trichloroethene ug/L ND 1.0 10/29/20 11:220.22
Trichlorofluoromethane ug/L ND 1.0 10/29/20 11:220.31
Vinyl acetate ug/L ND 2.0 10/29/20 11:221.4
Vinyl chloride ug/L ND 1.0 10/29/20 11:220.24
Xylene (Total)ug/L ND 1.0 10/29/20 11:220.63
1,2-Dichloroethane-d4 (S)%111 70-130 10/29/20 11:22
4-Bromofluorobenzene (S)%100 70-130 10/29/20 11:22
Toluene-d8 (S)%101 70-130 10/29/20 11:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3051827LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.450 105 70-130
1,1,1-Trichloroethane ug/L 56.650 113 70-130
1,1,2,2-Tetrachloroethane ug/L 51.150 102 70-130
1,1,2-Trichloroethane ug/L 49.850 100 70-130
1,1-Dichloroethane ug/L 52.650 105 70-130
1,1-Dichloroethene ug/L 49.850 100 70-132
1,1-Dichloropropene ug/L 56.750 113 70-131
1,2,3-Trichlorobenzene ug/L 52.450 105 70-134
1,2,3-Trichloropropane ug/L 52.150 104 70-130
1,2,4-Trichlorobenzene ug/L 50.450 101 70-130
1,2-Dibromo-3-chloropropane ug/L 58.250 116 70-132
1,2-Dibromoethane (EDB)ug/L 52.750 105 70-130
1,2-Dichlorobenzene ug/L 51.250 102 70-130
1,2-Dichloroethane ug/L 53.550 107 70-130
1,2-Dichloropropane ug/L 49.950 100 70-130
1,3-Dichlorobenzene ug/L 51.350 103 70-130
1,3-Dichloropropane ug/L 51.250 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3051827LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 52.350 105 70-130
2,2-Dichloropropane ug/L 56.450 113 70-130
2-Butanone (MEK)ug/L 110100 110 70-133
2-Chlorotoluene ug/L 50.650 101 70-130
2-Hexanone ug/L 110100 110 70-130
4-Chlorotoluene ug/L 51.850 104 70-130
4-Methyl-2-pentanone (MIBK)ug/L 105100 105 70-130
Acetone ug/L 107100 107 70-144
Benzene ug/L 51.250 102 70-130
Bromobenzene ug/L 50.650 101 70-130
Bromochloromethane ug/L 50.350 101 70-130
Bromodichloromethane ug/L 50.350 101 70-130
Bromoform ug/L 49.450 99 70-131
Bromomethane ug/L 48.5 IK,v3509730-177
Carbon tetrachloride ug/L 53.550 107 70-130
Chlorobenzene ug/L 49.550 99 70-130
Chloroethane ug/L 45.250 90 46-131
Chloroform ug/L 54.750 109 70-130
Chloromethane ug/L 40.750 81 49-130
cis-1,2-Dichloroethene ug/L 52.450 105 70-130
cis-1,3-Dichloropropene ug/L 53.950 108 70-130
Dibromochloromethane ug/L 53.950 108 70-130
Dibromomethane ug/L 50.050 100 70-130
Dichlorodifluoromethane ug/L 46.250 92 52-134
Diisopropyl ether ug/L 49.950 100 70-131
Ethylbenzene ug/L 50.050 100 70-130
Hexachloro-1,3-butadiene ug/L 48.3 IK509770-131
m&p-Xylene ug/L 99.3100 99 70-130
Methyl-tert-butyl ether ug/L 53.250 106 70-130
Methylene Chloride ug/L 44.550 89 68-130
Naphthalene ug/L 52.950 106 70-133
o-Xylene ug/L 50.050 100 70-130
p-Isopropyltoluene ug/L 53.450 107 70-130
Styrene ug/L 49.250 98 70-130
Tetrachloroethene ug/L 50.750 101 70-130
Toluene ug/L 50.750 101 70-130
trans-1,2-Dichloroethene ug/L 53.650 107 70-130
trans-1,3-Dichloropropene ug/L 53.350 107 70-130
Trichloroethene ug/L 53.150 106 70-130
Trichlorofluoromethane ug/L 48.650 97 61-130
Vinyl acetate ug/L 127100 127 70-140
Vinyl chloride ug/L 41.850 84 59-142
Xylene (Total)ug/L 149150 100 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3052869MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92502398004
3052870
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2500 116 70-135127 9 302500ND29003180
1,1,1-Trichloroethane ug/L 2500 116 70-148118 2 302500ND28902960
1,1,2,2-Tetrachloroethane ug/L 2500 109 70-131113 4 302500ND27202830
1,1,2-Trichloroethane ug/L 2500 109 70-136113 4 302500ND27102820
1,1-Dichloroethane ug/L 2500 103 70-147108 5 302500ND25702690
1,1-Dichloroethene ug/L 2500 111 70-158115 4 302500ND27702880
1,1-Dichloropropene ug/L 2500 117 70-149122 4 302500ND29303050
1,2,3-Trichlorobenzene ug/L 2500 118 68-140119 1 302500ND29402990
1,2,3-Trichloropropane ug/L 2500 116 67-137115 0 302500ND28902880
1,2,4-Trichlorobenzene ug/L 2500 113 70-139129 14 302500ND28103220
1,2-Dibromo-3-
chloropropane ug/L 2500 115 69-136114 1 302500ND28802840
1,2-Dibromoethane (EDB)ug/L 2500 117 70-137120 3 302500ND30403130
1,2-Dichlorobenzene ug/L 2500 120 70-133123 3 302500ND30003080
1,2-Dichloroethane ug/L 2500 101 67-138103 2 30250016326802740
1,2-Dichloropropane ug/L 2500 110 70-138113 2 302500ND27602810
1,3-Dichlorobenzene ug/L 2500 122 70-133129 6 302500ND30603240
1,3-Dichloropropane ug/L 2500 115 70-136120 4 302500ND28802990
1,4-Dichlorobenzene ug/L 2500 122 70-133123 0 302500ND30503060
2,2-Dichloropropane ug/L 2500 118 52-155122 3 302500ND29503040
2-Butanone (MEK)ug/L 5000 99 61-14798 1 305000ND55505490
2-Chlorotoluene ug/L 2500 124 70-141126 2 302500ND31003160
2-Hexanone ug/L 5000 107 67-139110 3 305000ND55805740
4-Chlorotoluene ug/L 2500 122 70-135124 2 302500ND30403090
4-Methyl-2-pentanone
(MIBK)ug/L 5000 98 67-136100 2 305000ND49105000
Acetone ug/L 5000 87 55-15989 2 305000ND57905880
Benzene ug/L 2500 70 67-15099 5 302500121001380014600
Bromobenzene ug/L 2500 123 70-134125 1 302500ND30803110
Bromochloromethane ug/L 2500 108 70-146119 10 302500ND27002970
Bromodichloromethane ug/L 2500 105 70-138109 4 302500ND26202720
Bromoform ug/L 2500 100 57-138101 1 302500ND25002530
Bromomethane ug/L 2500 105 10-200121 14 302500ND26203020
Carbon tetrachloride ug/L 2500 119 70-147120 0 302500ND29802990
Chlorobenzene ug/L 2500 110 70-137118 7 302500ND27502950
Chloroethane ug/L 2500 93 51-16699 6 302500ND23202480
Chloroform ug/L 2500 112 70-144117 4 302500ND27902920
Chloromethane ug/L 2500 91 24-16193 3 302500ND22702330
cis-1,2-Dichloroethene ug/L 2500 104 67-148106 2 302500ND25902640
cis-1,3-Dichloropropene ug/L 2500 111 70-142117 5 302500ND27802920
Dibromochloromethane ug/L 2500 115 68-138122 7 302500ND28603060
Dibromomethane ug/L 2500 112 70-134115 2 302500ND28002860
Dichlorodifluoromethane ug/L 2500 90 43-15596 6 302500ND22602400
Diisopropyl ether ug/L 2500 93 65-14697 4 30250032926502760
Ethylbenzene ug/L 2500 109 68-143124 8 302500167043804770
Hexachloro-1,3-butadiene ug/L IK250013362-151147 10 302500ND33303680
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3052869MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92502398004
3052870
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 5000 106 53-157126 8 30500074601280013800
Methyl-tert-butyl ether ug/L 2500 103 59-156107 3 30250078133603460
Methylene Chloride ug/L 2500 85 64-14888 3 302500ND24002470
Naphthalene ug/L 2500 113 57-150119 5 30250066934803650
o-Xylene ug/L 2500 98 68-143122 8 302500441068607470
p-Isopropyltoluene ug/L 2500 126 70-141132 4 302500ND31603300
Styrene ug/L 2500 112 70-136120 6 302500ND28102990
Tetrachloroethene ug/L 2500 111 70-139123 10 302500ND27803080
Toluene ug/L M12500-16 47-15735 6 302500213002090022200
trans-1,2-Dichloroethene ug/L 2500 107 70-149110 2 302500ND26802740
trans-1,3-Dichloropropene ug/L 2500 107 70-138113 6 302500ND26702820
Trichloroethene ug/L 2500 117 70-149119 1 302500ND29302970
Trichlorofluoromethane ug/L 2500 107 61-154107 0 302500ND26802680
Vinyl acetate ug/L 5000 103 48-156104 1 305000ND51405180
Vinyl chloride ug/L 2500 95 55-17298 3 302500ND23802460
Xylene (Total)ug/L 7500 104 66-145125 8 307500119001960021200
1,2-Dichloroethane-d4 (S)%94 70-13097
4-Bromofluorobenzene (S)%96 70-130100
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
576474
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92502685004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3050949
Associated Lab Samples:92502685004
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 10/29/20 12:401.7
1,2-Dichlorobenzene ug/L ND 10.0 10/29/20 12:401.8
1,3-Dichlorobenzene ug/L ND 10.0 10/29/20 12:401.6
1,4-Dichlorobenzene ug/L ND 10.0 10/29/20 12:401.7
1-Methylnaphthalene ug/L ND 10.0 10/29/20 12:402.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 10/29/20 12:401.2
2,4,5-Trichlorophenol ug/L ND 10.0 10/29/20 12:401.4
2,4,6-Trichlorophenol ug/L ND 10.0 10/29/20 12:401.6
2,4-Dichlorophenol ug/L ND 10.0 10/29/20 12:401.4
2,4-Dimethylphenol ug/L ND 10.0 10/29/20 12:401.7
2,4-Dinitrophenol ug/L ND 50.0 10/29/20 12:4026.0
2,4-Dinitrotoluene ug/L ND 10.0 10/29/20 12:401.6
2,6-Dinitrotoluene ug/L ND 10.0 10/29/20 12:401.7
2-Chloronaphthalene ug/L ND 10.0 10/29/20 12:401.7
2-Chlorophenol ug/L ND 10.0 10/29/20 12:401.2
2-Methylnaphthalene ug/L ND 10.0 10/29/20 12:401.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 10/29/20 12:401.9
2-Nitroaniline ug/L ND 20.0 10/29/20 12:403.0
2-Nitrophenol ug/L ND 10.0 10/29/20 12:401.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 10/29/20 12:401.2
3,3'-Dichlorobenzidine ug/L ND 20.0 10/29/20 12:408.1
3-Nitroaniline ug/L ND 20.0 10/29/20 12:403.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 10/29/20 12:403.4
4-Bromophenylphenyl ether ug/L ND 10.0 10/29/20 12:401.8
4-Chloro-3-methylphenol ug/L ND 10.0 10/29/20 12:403.3
4-Chloroaniline ug/L ND 20.0 10/29/20 12:403.6
4-Chlorophenylphenyl ether ug/L ND 10.0 10/29/20 12:402.0
4-Nitroaniline ug/L ND 20.0 10/29/20 12:405.1
4-Nitrophenol ug/L ND 50.0 10/29/20 12:406.6
Acenaphthene ug/L ND 10.0 10/29/20 12:402.0
Acenaphthylene ug/L ND 10.0 10/29/20 12:402.0
Aniline ug/L ND 10.0 10/29/20 12:401.6
Anthracene ug/L ND 10.0 10/29/20 12:402.3
Benzo(a)anthracene ug/L ND 10.0 10/29/20 12:402.7
Benzo(a)pyrene ug/L ND 10.0 10/29/20 12:402.8
Benzo(b)fluoranthene ug/L ND 10.0 10/29/20 12:402.6
Benzo(g,h,i)perylene ug/L ND 10.0 10/29/20 12:402.8
Benzo(k)fluoranthene ug/L ND 10.0 10/29/20 12:402.7
Benzoic Acid ug/L ND 50.0 10/29/20 12:403.4
Benzyl alcohol ug/L ND 20.0 10/29/20 12:402.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3050949
Associated Lab Samples:92502685004
Matrix:Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 10/29/20 12:401.8
bis(2-Chloroethyl) ether ug/L ND 10.0 10/29/20 12:401.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 10/29/20 12:403.7
Butylbenzylphthalate ug/L ND 10.0 10/29/20 12:403.1
Chrysene ug/L ND 10.0 10/29/20 12:402.8
Di-n-butylphthalate ug/L ND 10.0 10/29/20 12:402.2
Di-n-octylphthalate ug/L ND 10.0 10/29/20 12:403.9
Dibenz(a,h)anthracene ug/L ND 10.0 10/29/20 12:403.0
Dibenzofuran ug/L ND 10.0 10/29/20 12:402.1
Diethylphthalate ug/L ND 10.0 10/29/20 12:402.0
Dimethylphthalate ug/L ND 10.0 10/29/20 12:402.1
Fluoranthene ug/L ND 10.0 10/29/20 12:402.2
Fluorene ug/L ND 10.0 10/29/20 12:402.1
Hexachloro-1,3-butadiene ug/L ND 10.0 10/29/20 12:401.8
Hexachlorobenzene ug/L ND 10.0 10/29/20 12:402.2
Hexachlorocyclopentadiene ug/L ND 10.0 10/29/20 12:401.6
Hexachloroethane ug/L ND 10.0 10/29/20 12:401.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 10/29/20 12:402.9
Isophorone ug/L ND 10.0 10/29/20 12:401.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 10/29/20 12:401.3
N-Nitrosodimethylamine ug/L ND 10.0 10/29/20 12:401.9
N-Nitrosodiphenylamine ug/L ND 10.0 10/29/20 12:403.0
Naphthalene ug/L ND 10.0 10/29/20 12:402.1
Nitrobenzene ug/L ND 10.0 10/29/20 12:401.9
Pentachlorophenol ug/L ND 20.0 10/29/20 12:403.8
Phenanthrene ug/L ND 10.0 10/29/20 12:402.0
Phenol ug/L ND 10.0 10/29/20 12:401.4
Pyrene ug/L ND 10.0 10/29/20 12:402.2
2,4,6-Tribromophenol (S)%56 10-144 10/29/20 12:40
2-Fluorobiphenyl (S)%63 10-130 10/29/20 12:40
2-Fluorophenol (S)%45 10-130 10/29/20 12:40
Nitrobenzene-d5 (S)%67 10-144 10/29/20 12:40
Phenol-d6 (S)%31 10-130 10/29/20 12:40
Terphenyl-d14 (S)%94 34-163 10/29/20 12:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3050950LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 34.350 69 18-130
1,2-Dichlorobenzene ug/L 33.550 67 20-130
1,3-Dichlorobenzene ug/L 32.750 65 18-130
1,4-Dichlorobenzene ug/L 34.150 68 18-130
1-Methylnaphthalene ug/L 36.950 74 29-130
2,2'-Oxybis(1-chloropropane)ug/L 37.850 76 28-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Huntersville, NC 28078
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Page 36 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3050950LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 40.050 80 35-130
2,4,6-Trichlorophenol ug/L 38.250 76 31-130
2,4-Dichlorophenol ug/L 38.450 77 35-130
2,4-Dimethylphenol ug/L 43.450 87 34-130
2,4-Dinitrophenol ug/L 153250 61 10-153
2,4-Dinitrotoluene ug/L 45.150 90 37-136
2,6-Dinitrotoluene ug/L 47.750 95 33-136
2-Chloronaphthalene ug/L 39.950 80 26-130
2-Chlorophenol ug/L 35.350 71 37-130
2-Methylnaphthalene ug/L 38.450 77 29-130
2-Methylphenol(o-Cresol)ug/L 33.450 67 35-130
2-Nitroaniline ug/L 81.1100 81 37-130
2-Nitrophenol ug/L 38.250 76 32-130
3&4-Methylphenol(m&p Cresol)ug/L 35.450 71 34-130
3,3'-Dichlorobenzidine ug/L 88.0100 88 34-136
3-Nitroaniline ug/L 86.6100 87 37-138
4,6-Dinitro-2-methylphenol ug/L 77.0100 77 21-157
4-Bromophenylphenyl ether ug/L 39.950 80 38-130
4-Chloro-3-methylphenol ug/L 83.1100 83 37-130
4-Chloroaniline ug/L 79.1100 79 38-130
4-Chlorophenylphenyl ether ug/L 39.450 79 33-130
4-Nitroaniline ug/L 86.5100 87 42-137
4-Nitrophenol ug/L 133250 53 10-130
Acenaphthene ug/L 40.850 82 33-130
Acenaphthylene ug/L 41.050 82 35-130
Aniline ug/L 29.850 60 22-130
Anthracene ug/L 37.650 75 48-130
Benzo(a)anthracene ug/L 40.750 81 48-137
Benzo(a)pyrene ug/L 42.150 84 49-138
Benzo(b)fluoranthene ug/L 46.950 94 52-138
Benzo(g,h,i)perylene ug/L 44.050 88 48-140
Benzo(k)fluoranthene ug/L 44.550 89 48-139
Benzoic Acid ug/L 51.8250 21 10-130
Benzyl alcohol ug/L 64.6100 65 35-130
bis(2-Chloroethoxy)methane ug/L 38.750 77 34-130
bis(2-Chloroethyl) ether ug/L 38.950 78 36-130
bis(2-Ethylhexyl)phthalate ug/L 45.050 90 32-165
Butylbenzylphthalate ug/L 51.550 103 34-161
Chrysene ug/L 42.150 84 47-131
Di-n-butylphthalate ug/L 42.550 85 39-144
Di-n-octylphthalate ug/L 42.250 84 30-170
Dibenz(a,h)anthracene ug/L 43.450 87 49-138
Dibenzofuran ug/L 42.350 85 33-130
Diethylphthalate ug/L 45.250 90 38-131
Dimethylphthalate ug/L 43.550 87 37-130
Fluoranthene ug/L 39.750 79 46-137
Fluorene ug/L 41.750 83 37-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Huntersville, NC 28078
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Page 37 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3050950LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 31.350 63 11-130
Hexachlorobenzene ug/L 39.450 79 38-130
Hexachlorocyclopentadiene ug/L 31.550 63 10-130
Hexachloroethane ug/L 33.550 67 14-130
Indeno(1,2,3-cd)pyrene ug/L 44.550 89 41-130
Isophorone ug/L 41.550 83 33-130
N-Nitroso-di-n-propylamine ug/L 42.150 84 36-130
N-Nitrosodimethylamine ug/L 27.650 55 34-130
N-Nitrosodiphenylamine ug/L 42.450 85 37-130
Naphthalene ug/L 36.950 74 30-130
Nitrobenzene ug/L 41.150 82 36-130
Pentachlorophenol ug/L 73.5100 74 23-149
Phenanthrene ug/L 41.250 82 44-130
Phenol ug/L 22.550 45 18-130
Pyrene ug/L 42.750 85 47-134
2,4,6-Tribromophenol (S)%80 10-144
2-Fluorobiphenyl (S)%75 10-130
2-Fluorophenol (S)%50 10-130
Nitrobenzene-d5 (S)%79 10-144
Phenol-d6 (S)%39 10-130
Terphenyl-d14 (S)%94 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3050951MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92501672003
3050952
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 73 10-13071 2 30100ND72.9 71.3
1,2-Dichlorobenzene ug/L 100 68 10-13066 4 30100ND68.4 65.5
1,3-Dichlorobenzene ug/L 100 65 10-13062 4 30100ND64.5 62.2
1,4-Dichlorobenzene ug/L 100 66 10-13065 3 30100ND66.4 64.8
1-Methylnaphthalene ug/L 100 83 10-13081 3 30100ND83.3 80.6
2,2'-Oxybis(1-chloropropane)ug/L 100 87 12-14282 6 30100ND87.5 82.1
2,4,5-Trichlorophenol ug/L 100 104 10-14396 8 30100ND10495.8
2,4,6-Trichlorophenol ug/L 100 96 10-14781 17 30100ND95.7 80.8
2,4-Dichlorophenol ug/L 100 100 10-13895 5 30100ND99.7 94.9
2,4-Dimethylphenol ug/L 100 100 25-13097 3 30100ND10097.1
2,4-Dinitrophenol ug/L 500 14 10-16511 30500ND69.2J 55.9J
2,4-Dinitrotoluene ug/L 100 103 29-148106 3 30100ND103106
2,6-Dinitrotoluene ug/L 100 102 26-146103 0 30100ND102103
2-Chloronaphthalene ug/L 100 84 11-13084 1 30100ND84.4 83.6
2-Chlorophenol ug/L 100 89 10-13388 2 30100ND89.5 87.9
2-Methylnaphthalene ug/L 100 84 13-13082 2 30100ND83.9 81.9
2-Methylphenol(o-Cresol)ug/L 100 85 20-13085 0 30100ND85.1 84.9
2-Nitroaniline ug/L 200 95 24-13695 0 30200ND190190
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Huntersville, NC 28078
[phone]
Page 38 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3050951MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92501672003
3050952
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L 100 104 10-15397 6 30100ND10497.2
3&4-Methylphenol(m&p
Cresol)ug/L 100 81 16-13082 1 30100ND80.6 81.7
3,3'-Dichlorobenzidine ug/L 200 104 10-153105 1 30200ND208211
3-Nitroaniline ug/L 200 101 22-151105 4 30200ND203211
4,6-Dinitro-2-methylphenol ug/L 200 53 10-18040 27 30200ND10680.2
4-Bromophenylphenyl ether ug/L 100 96 25-13096 0 30100ND96.4 96.4
4-Chloro-3-methylphenol ug/L 200 98 25-13395 3 30200ND195190
4-Chloroaniline ug/L 200 95 14-13289 6 30200ND189178
4-Chlorophenylphenyl ether ug/L 100 97 19-13096 1 30100ND96.5 95.8
4-Nitroaniline ug/L 200 103 29-150109 5 30200ND207218
4-Nitrophenol ug/L 500 23 10-13020 11 30500ND114102
Acenaphthene ug/L 100 87 16-13085 3 30100ND87.0 84.7
Acenaphthylene ug/L 100 91 15-13788 3 30100ND90.8 88.5
Aniline ug/L 100 70 10-13071 2 30100ND69.5 70.9
Anthracene ug/L 100 86 37-13687 2 30100ND85.5 87.2
Benzo(a)anthracene ug/L 100 99 40-145101 2 30100ND99.4 101
Benzo(a)pyrene ug/L 100 102 41-146103 1 30100ND102103
Benzo(b)fluoranthene ug/L 100 102 39-151104 1 30100ND102104
Benzo(g,h,i)perylene ug/L 100 101 40-14799 2 30100ND10199.2
Benzo(k)fluoranthene ug/L 100 103 40-146106 3 30100ND103106
Benzoic Acid ug/L M1500010-1305 30500NDND23.7J
Benzyl alcohol ug/L 200 89 25-13091 1 30200ND179181
bis(2-Chloroethoxy)methane ug/L 100 99 23-13094 5 30100ND99.2 94.0
bis(2-Chloroethyl) ether ug/L 100 101 25-130101 1 30100ND101101
bis(2-Ethylhexyl)phthalate ug/L 100 110 28-166112 2 30100ND110112
Butylbenzylphthalate ug/L 100 105 33-165108 3 30100ND105108
Chrysene ug/L 100 99 38-141100 1 30100ND98.9 99.6
Di-n-butylphthalate ug/L 100 107 32-153110 3 30100ND107110
Di-n-octylphthalate ug/L 100 107 30-175107 1 30100ND107107
Dibenz(a,h)anthracene ug/L 100 104 39-148103 1 30100ND104103
Dibenzofuran ug/L 100 93 20-13091 2 30100ND93.2 91.1
Diethylphthalate ug/L 100 101 28-142105 4 30100ND101105
Dimethylphthalate ug/L 100 99 26-13698 0 30100ND98.6 98.3
Fluoranthene ug/L 100 102 39-143103 1 30100ND102103
Fluorene ug/L 100 94 24-13292 2 30100ND93.7 92.1
Hexachloro-1,3-butadiene ug/L 100 65 10-13066 1 30100ND65.4 65.9
Hexachlorobenzene ug/L 100 95 29-13098 2 30100ND95.5 97.6
Hexachlorocyclopentadiene ug/L 100 59 10-13062 5 30100ND59.3 62.1
Hexachloroethane ug/L 100 61 10-13058 4 30100ND61.0 58.4
Indeno(1,2,3-cd)pyrene ug/L 100 103 39-148103 0 30100ND103103
Isophorone ug/L 100 98 23-13093 5 30100ND97.7 92.8
N-Nitroso-di-n-propylamine ug/L 100 96 25-13092 4 30100ND96.2 92.0
N-Nitrosodimethylamine ug/L 100 67 22-13075 11 30100ND66.8 74.7
N-Nitrosodiphenylamine ug/L 100 98 26-13496 2 30100ND98.0 96.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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[phone]
Page 39 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3050951MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92501672003
3050952
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L 100 82 14-13077 6 30100ND82.1 76.9
Nitrobenzene ug/L 100 98 25-13093 6 30100ND98.2 92.8
Pentachlorophenol ug/L 200 70 10-17555 24 30200ND141111
Phenanthrene ug/L 100 95 36-13396 1 30100ND95.2 95.9
Phenol ug/L 100 50 10-13052 5 30100ND49.8 52.2
Pyrene ug/L 100 94 40-14398 4 30100ND93.7 97.8
2,4,6-Tribromophenol (S)%115 10-144107
2-Fluorobiphenyl (S)%97 10-13091
2-Fluorophenol (S)%63 10-13064
Nitrobenzene-d5 (S)%104 10-14495
Phenol-d6 (S)%48 10-13054
Terphenyl-d14 (S)%106 34-163107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Huntersville, NC 28078
[phone]
Page 40 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
576728
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92502685001, 92502685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3051993
Associated Lab Samples:92502685001, 92502685002
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 333 10/29/20 16:0576.4
1,2-Dichlorobenzene ug/kg ND 333 10/29/20 16:0572.1
1,3-Dichlorobenzene ug/kg ND 333 10/29/20 16:0575.1
1,4-Dichlorobenzene ug/kg ND 333 10/29/20 16:0573.3
1-Methylnaphthalene ug/kg ND 333 10/29/20 16:0588.8
2,2'-Oxybis(1-chloropropane)ug/kg ND 333 10/29/20 16:0592.6
2,4,5-Trichlorophenol ug/kg ND 333 10/29/20 16:0586.6
2,4,6-Trichlorophenol ug/kg ND 333 10/29/20 16:0583.7
2,4-Dichlorophenol ug/kg ND 333 10/29/20 16:05110
2,4-Dimethylphenol ug/kg ND 333 10/29/20 16:0583.0
2,4-Dinitrophenol ug/kg ND 1670 10/29/20 16:051060
2,4-Dinitrotoluene ug/kg ND 333 10/29/20 16:0588.3
2,6-Dinitrotoluene ug/kg ND 333 10/29/20 16:0587.2
2-Chloronaphthalene ug/kg ND 333 10/29/20 16:0574.2
2-Chlorophenol ug/kg ND 333 10/29/20 16:0577.6
2-Methylnaphthalene ug/kg ND 333 10/29/20 16:0584.8
2-Methylphenol(o-Cresol)ug/kg ND 333 10/29/20 16:0573.8
2-Nitroaniline ug/kg ND 1670 10/29/20 16:05168
2-Nitrophenol ug/kg ND 333 10/29/20 16:05103
3&4-Methylphenol(m&p Cresol)ug/kg ND 333 10/29/20 16:0583.8
3,3'-Dichlorobenzidine ug/kg ND 667 10/29/20 16:05232
3-Nitroaniline ug/kg ND 1670 10/29/20 16:05177
4,6-Dinitro-2-methylphenol ug/kg ND 667 10/29/20 16:05537
4-Bromophenylphenyl ether ug/kg ND 333 10/29/20 16:0587.5
4-Chloro-3-methylphenol ug/kg ND 667 10/29/20 16:05203
4-Chloroaniline ug/kg ND 667 10/29/20 16:05204
4-Chlorophenylphenyl ether ug/kg ND 333 10/29/20 16:0586.6
4-Nitroaniline ug/kg ND 667 10/29/20 16:05165
4-Nitrophenol ug/kg ND 1670 10/29/20 16:05531
Acenaphthene ug/kg ND 333 10/29/20 16:0585.8
Acenaphthylene ug/kg ND 333 10/29/20 16:0578.9
Aniline ug/kg ND 333 10/29/20 16:0574.8
Anthracene ug/kg ND 333 10/29/20 16:0586.5
Benzo(a)anthracene ug/kg ND 333 10/29/20 16:05106
Benzo(a)pyrene ug/kg ND 333 10/29/20 16:05144
Benzo(b)fluoranthene ug/kg ND 333 10/29/20 16:05134
Benzo(g,h,i)perylene ug/kg ND 333 10/29/20 16:05130
Benzo(k)fluoranthene ug/kg ND 333 10/29/20 16:05140
Benzoic Acid ug/kg ND 1670 10/29/20 16:05360
Benzyl alcohol ug/kg ND 667 10/29/20 16:05177
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Huntersville, NC 28078
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Page 41 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3051993
Associated Lab Samples:92502685001, 92502685002
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 333 10/29/20 16:0589.0
bis(2-Chloroethyl) ether ug/kg ND 333 10/29/20 16:0570.8
bis(2-Ethylhexyl)phthalate ug/kg ND 333 10/29/20 16:05109
Butylbenzylphthalate ug/kg ND 333 10/29/20 16:0588.8
Chrysene ug/kg ND 333 10/29/20 16:0596.8
Di-n-butylphthalate ug/kg ND 333 10/29/20 16:0582.2
Di-n-octylphthalate ug/kg ND 333 10/29/20 16:05190
Dibenz(a,h)anthracene ug/kg ND 333 10/29/20 16:05133
Dibenzofuran ug/kg ND 333 10/29/20 16:0583.3
Diethylphthalate ug/kg ND 333 10/29/20 16:0572.3
Dimethylphthalate ug/kg ND 333 10/29/20 16:0575.4
Fluoranthene ug/kg ND 333 10/29/20 16:05101
Fluorene ug/kg ND 333 10/29/20 16:0589.2
Hexachloro-1,3-butadiene ug/kg ND 333 10/29/20 16:0581.0
Hexachlorobenzene ug/kg ND 333 10/29/20 16:0584.6
Hexachlorocyclopentadiene ug/kg ND 333 10/29/20 16:05133
Hexachloroethane ug/kg ND 333 10/29/20 16:0576.0
Indeno(1,2,3-cd)pyrene ug/kg ND 333 10/29/20 16:05153
Isophorone ug/kg ND 333 10/29/20 16:0572.4
N-Nitroso-di-n-propylamine ug/kg ND 333 10/29/20 16:0593.3
N-Nitrosodimethylamine ug/kg ND 333 10/29/20 16:0593.7
N-Nitrosodiphenylamine ug/kg ND 333 10/29/20 16:0585.1
Naphthalene ug/kg ND 333 10/29/20 16:0579.8
Nitrobenzene ug/kg ND 333 10/29/20 16:0579.6
Pentachlorophenol ug/kg ND 667 10/29/20 16:05153
Phenanthrene ug/kg ND 333 10/29/20 16:0583.9
Phenol ug/kg ND 333 10/29/20 16:0579.6
Pyrene ug/kg ND 333 10/29/20 16:0591.7
Pyridine ug/kg ND 333 10/29/20 16:0584.3
2,4,6-Tribromophenol (S)%64 18-130 10/29/20 16:05
2-Fluorobiphenyl (S)%41 19-130 10/29/20 16:05
2-Fluorophenol (S)%62 18-130 10/29/20 16:05
Nitrobenzene-d5 (S)%64 21-130 10/29/20 16:05
Phenol-d6 (S)%58 18-130 10/29/20 16:05
Terphenyl-d14 (S)%76 15-130 10/29/20 16:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3051994LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10901670 65 47-130
1,2-Dichlorobenzene ug/kg 10801670 65 49-130
1,3-Dichlorobenzene ug/kg 10701670 64 48-130
1,4-Dichlorobenzene ug/kg 11101670 66 49-130
1-Methylnaphthalene ug/kg 11301670 67 54-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Page 42 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3051994LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 10801670 65 38-130
2,4,5-Trichlorophenol ug/kg 13401670 80 49-130
2,4,6-Trichlorophenol ug/kg 12201670 73 50-130
2,4-Dichlorophenol ug/kg 12501670 75 51-130
2,4-Dimethylphenol ug/kg 13001670 78 53-130
2,4-Dinitrophenol ug/kg 32808360 39 39-130
2,4-Dinitrotoluene ug/kg 12601670 75 53-130
2,6-Dinitrotoluene ug/kg 13001670 78 55-130
2-Chloronaphthalene ug/kg 11201670 67 48-130
2-Chlorophenol ug/kg 12001670 72 54-130
2-Methylnaphthalene ug/kg 11501670 69 57-130
2-Methylphenol(o-Cresol)ug/kg 12701670 76 50-130
2-Nitroaniline ug/kg 25703340 77 49-130
2-Nitrophenol ug/kg 12301670 73 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 12401670 74 50-130
3,3'-Dichlorobenzidine ug/kg 24003340 72 47-130
3-Nitroaniline ug/kg 24703340 74 45-130
4,6-Dinitro-2-methylphenol ug/kg 25003340 75 50-142
4-Bromophenylphenyl ether ug/kg 12001670 72 55-130
4-Chloro-3-methylphenol ug/kg 26903340 81 52-130
4-Chloroaniline ug/kg 22603340 68 49-130
4-Chlorophenylphenyl ether ug/kg 11801670 70 53-130
4-Nitroaniline ug/kg 25003340 75 51-130
4-Nitrophenol ug/kg 59308360 71 40-130
Acenaphthene ug/kg 11501670 69 56-130
Acenaphthylene ug/kg 11201670 67 58-130
Aniline ug/kg 9591670 57 44-130
Anthracene ug/kg 10701670 64 60-130
Benzo(a)anthracene ug/kg 12601670 75 59-130
Benzo(a)pyrene ug/kg 12201670 73 57-130
Benzo(b)fluoranthene ug/kg 12101670 72 54-130
Benzo(g,h,i)perylene ug/kg 11301670 68 59-130
Benzo(k)fluoranthene ug/kg 12801670 77 54-130
Benzoic Acid ug/kg 771J L28360919-130
Benzyl alcohol ug/kg 22703340 68 50-130
bis(2-Chloroethoxy)methane ug/kg 12001670 72 55-130
bis(2-Chloroethyl) ether ug/kg 12301670 74 53-130
bis(2-Ethylhexyl)phthalate ug/kg 13101670 78 58-130
Butylbenzylphthalate ug/kg 13201670 79 46-138
Chrysene ug/kg 13201670 79 57-130
Di-n-butylphthalate ug/kg 12201670 73 57-130
Di-n-octylphthalate ug/kg 13001670 78 57-130
Dibenz(a,h)anthracene ug/kg 11301670 67 60-130
Dibenzofuran ug/kg 12101670 72 54-130
Diethylphthalate ug/kg 12601670 75 55-130
Dimethylphthalate ug/kg 12901670 77 57-130
Fluoranthene ug/kg 11401670 68 57-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Page 43 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3051994LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 11401670 68 56-130
Hexachloro-1,3-butadiene ug/kg 11001670 66 41-130
Hexachlorobenzene ug/kg 11801670 70 53-130
Hexachlorocyclopentadiene ug/kg 6371670 38 23-130
Hexachloroethane ug/kg 10301670 62 48-130
Indeno(1,2,3-cd)pyrene ug/kg 11401670 68 61-130
Isophorone ug/kg 12701670 76 49-130
N-Nitroso-di-n-propylamine ug/kg 11901670 71 52-130
N-Nitrosodimethylamine ug/kg 10801670 65 45-130
N-Nitrosodiphenylamine ug/kg 12801670 77 56-130
Naphthalene ug/kg 11101670 67 56-130
Nitrobenzene ug/kg 12501670 75 50-130
Pentachlorophenol ug/kg 23803340 71 33-130
Phenanthrene ug/kg 12201670 73 60-130
Phenol ug/kg 10801670 65 54-130
Pyrene ug/kg 13001670 77 61-130
Pyridine ug/kg 9211670 55 35-130
2,4,6-Tribromophenol (S)%72 18-130
2-Fluorobiphenyl (S)%47 19-130
2-Fluorophenol (S)%61 18-130
Nitrobenzene-d5 (S)%62 21-130
Phenol-d6 (S)%62 18-130
Terphenyl-d14 (S)%72 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3051995MATRIX SPIKE SAMPLE:
MSSpike
Result
92502685001
1,2,4-Trichlorobenzene ug/kg 16002440 65 22-130ND
1,2-Dichlorobenzene ug/kg 15802440 65 23-130ND
1,3-Dichlorobenzene ug/kg 15602440 64 26-130ND
1,4-Dichlorobenzene ug/kg 16202440 66 27-130ND
1-Methylnaphthalene ug/kg 16502440 67 30-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 15802440 65 30-130ND
2,4,5-Trichlorophenol ug/kg 19602440 80 26-130ND
2,4,6-Trichlorophenol ug/kg 17902440 73 23-130ND
2,4-Dichlorophenol ug/kg 18302440 75 29-130ND
2,4-Dimethylphenol ug/kg 19002440 78 13-130ND
2,4-Dinitrophenol ug/kg 479012200 39 10-131ND
2,4-Dinitrotoluene ug/kg 18402440 75 28-130ND
2,6-Dinitrotoluene ug/kg 19002440 78 36-130ND
2-Chloronaphthalene ug/kg 16402440 67 27-130ND
2-Chlorophenol ug/kg 17502440 72 29-130ND
2-Methylnaphthalene ug/kg 16802440 69 29-130ND
2-Methylphenol(o-Cresol)ug/kg 18502440 76 20-130ND
2-Nitroaniline ug/kg 37504890 77 29-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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Huntersville, NC 28078
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Page 44 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3051995MATRIX SPIKE SAMPLE:
MSSpike
Result
92502685001
2-Nitrophenol ug/kg 17902440 73 26-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 18102440 74 10-176ND
3,3'-Dichlorobenzidine ug/kg 35104890 72 15-130ND
3-Nitroaniline ug/kg 36004890 74 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 36504890 75 15-132ND
4-Bromophenylphenyl ether ug/kg 17602440 72 35-130ND
4-Chloro-3-methylphenol ug/kg 39304890 81 30-130ND
4-Chloroaniline ug/kg 33004890 68 28-130ND
4-Chlorophenylphenyl ether ug/kg 17202440 70 32-130ND
4-Nitroaniline ug/kg 36504890 75 30-130ND
4-Nitrophenol ug/kg 865012200 71 17-130ND
Acenaphthene ug/kg 16802440 69 29-130ND
Acenaphthylene ug/kg 16302440 67 31-130ND
Aniline ug/kg 14002440 57 10-130ND
Anthracene ug/kg 15602440 64 33-130ND
Benzo(a)anthracene ug/kg 18402440 75 32-130ND
Benzo(a)pyrene ug/kg 17802440 73 32-130ND
Benzo(b)fluoranthene ug/kg 17702440 72 33-130ND
Benzo(g,h,i)perylene ug/kg 16502440 68 28-130ND
Benzo(k)fluoranthene ug/kg 18702440 77 31-130ND
Benzoic Acid ug/kg ND M012200110-130ND
Benzyl alcohol ug/kg 33104890 68 31-130ND
bis(2-Chloroethoxy)methane ug/kg 17502440 72 30-130ND
bis(2-Chloroethyl) ether ug/kg 18002440 74 68-130ND
bis(2-Ethylhexyl)phthalate ug/kg 19102440 78 40-130ND
Butylbenzylphthalate ug/kg 19302440 79 40-130ND
Chrysene ug/kg 19202440 79 30-130ND
Di-n-butylphthalate ug/kg 17802440 73 41-130ND
Di-n-octylphthalate ug/kg 19002440 78 42-130ND
Dibenz(a,h)anthracene ug/kg 16402440 67 27-130ND
Dibenzofuran ug/kg 17702440 72 32-130ND
Diethylphthalate ug/kg 18302440 75 40-130ND
Dimethylphthalate ug/kg 18902440 77 37-130ND
Fluoranthene ug/kg 16702440 68 26-130ND
Fluorene ug/kg 16602440 68 31-130ND
Hexachloro-1,3-butadiene ug/kg 16102440 66 20-130ND
Hexachlorobenzene ug/kg 17202440 70 29-130ND
Hexachlorocyclopentadiene ug/kg 9302440 38 10-130ND
Hexachloroethane ug/kg 15002440 62 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 16602440 68 28-130ND
Isophorone ug/kg 18502440 76 32-130ND
N-Nitroso-di-n-propylamine ug/kg 17402440 71 31-130ND
N-Nitrosodimethylamine ug/kg 15802440 65 20-130ND
N-Nitrosodiphenylamine ug/kg 18802440 77 32-130ND
Naphthalene ug/kg 16302440 67 30-130ND
Nitrobenzene ug/kg 18302440 75 25-130ND
Pentachlorophenol ug/kg 34804890 71 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 45 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3051995MATRIX SPIKE SAMPLE:
MSSpike
Result
92502685001
Phenanthrene ug/kg 17802440 73 34-130ND
Phenol ug/kg 15802440 65 14-130ND
Pyrene ug/kg 18902440 77 31-130ND
Pyridine ug/kg 13502440 55 10-130ND
2,4,6-Tribromophenol (S)%72 18-130
2-Fluorobiphenyl (S)%47 19-130
2-Fluorophenol (S)%61 18-130
Nitrobenzene-d5 (S)%62 21-130
Phenol-d6 (S)%62 18-130
Terphenyl-d14 (S)%72 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92502685001
3051996SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92502685001
3051996SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6664
2-Fluorobiphenyl (S)%4341
2-Fluorophenol (S)%6262
Nitrobenzene-d5 (S)%6564
Phenol-d6 (S)%6358
Terphenyl-d14 (S)%6876
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 47 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
576473
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92502685001, 92502685002, 92502685003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92502685001
3050946SAMPLE DUPLICATE:
Percent Moisture %27.4 12 2530.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
30389319004
3050947SAMPLE DUPLICATE:
Percent Moisture %24.4 1 2524.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1568505
7199
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92502685004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3588431-1
Associated Lab Samples:92502685004
Matrix:Drinking Water
AnalyzedMDL
Chromium, Hexavalent ug/L ND 0.100 11/02/20 13:220.0400
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3588431-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent ug/L 0.4750.500 95.1 90.0-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3588431-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
R3588431-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent ug/L E,P61.00 218 90.0-110285 0.422 201.00156 158 158
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92502685004
R3588431-3SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L 0.0556J J4.76 200.0584
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 49 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1568581
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92502685001, 92502685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3588368-1
Associated Lab Samples:92502685001, 92502685002
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 11/01/20 05:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3588368-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1278671-05
R3588368-3SAMPLE DUPLICATE:
Total Solids %92.2 1.00 1091.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92502685
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1567882
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92502685001, 92502685002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3587789-1
Associated Lab Samples:92502685001, 92502685002
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 10/30/20 21:020.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3587789-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.5410.0 95.4 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3587789-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1279129-03
R3587789-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg ML25.1 11.7 75.0-12511.1 4.34 2025.10.566 3.51 3.36
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3587789-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1279129-03
Chromium, Hexavalent mg/kg 573 ML83069.1 75.0-1250.566
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1279124-01
R3587789-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92502685002
R3587789-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 57
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92502685
BCP-064
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Lab Contaminant1g
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
Analyte concentration exceeded the calibration range. The reported result is estimated.E
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the
spike level.P6
RPD value was outside control limits.R1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 57
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92502685
BCP-064
ANALYTE QUALIFIERS
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 57
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92502685
BCP-064
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92502685004 1568783 1568783RB-1 3015 EPA 6020B
92502685001 1568639 1568639FG-102820 3050B EPA 6020B
92502685002 1568639 1568639DUP-1 3050B EPA 6020B
92502685004 1568119 1568119RB-1 7470A EPA 7470A
92502685001 1568187 1568187FG-102820 7471A EPA 7471B
92502685002 1568187 1568187DUP-1 7471A EPA 7471B
92502685004 576474 576628RB-1 EPA 3510C EPA 8270E
92502685001 576728 576887FG-102820 EPA 3546 EPA 8270E
92502685002 576728 576887DUP-1 EPA 3546 EPA 8270E
92502685002 576753 576798DUP-1 EPA 5035A/5030B EPA 8260D
92502685003 576753 576798FG1-1-2 EPA 5035A/5030B EPA 8260D
92502685004 576679RB-1 EPA 8260D
92502685001 576473FG-102820 ASTM D2974-87
92502685002 576473DUP-1 ASTM D2974-87
92502685003 576473FG1-1-2 ASTM D2974-87
92502685004 1568505 1568505RB-1 7199 EPA 7199
92502685001 1568581 1568581FG-102820 SM 2540 G SM 2540G
92502685002 1568581 1568581DUP-1 SM 2540 G SM 2540G
92502685001 1567882 1567882FG-102820 3060A EPA 7199
92502685002 1567882 1567882DUP-1 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 03:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 57
Page 55 of 57
Page 56 of 57
Page 57 of 57

Appendix C

Risk Calculator Summary Pages

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Final Grade Soil - Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
HD Supply Site
1414 South Tryon St, Charlotte, NC
Brownfields
19054-15-060
July 2020
May 2020 EPA RSL Table
11/9/2020
Prepared By:Hart & Hickman, PC
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 19054-15-060
Exposure Unit ID: Final Grade Soil - Worst Case
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration to Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 19054-15-060
Exposure Unit ID: Final Grade Soil - Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 19054-15-060
Exposure Unit ID: Final Grade Soil - Worst Case
Exposure Point
Concentration
(mg/kg)
Notes:CAS Number Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.418 67-64-1 Acetone mg/kg
2.91 7440-38-2 Arsenic, Inorganic mg/kg
85.8 7440-39-3 Barium mg/kg
12.3 7439-92-1 ~Lead and Compounds mg/kg
0.0901 7439-97-6 ~Mercury (elemental)mg/kg
0.236 78-93-3 Methyl Ethyl Ketone (2-Butanone)mg/kg
0.0961 75-09-2 Methylene Chloride mg/kg
0.856 7782-49-2 Selenium mg/kg
0.0065 108-88-3 Toluene mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 19054-15-060
Exposure Unit ID: Final Grade Soil - Worst Case
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 4.3E-06 9.9E-02 NO
Groundwater Use*NC NC NC
Soil 9.7E-07 8.4E-03 NO
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 19054-15-060
Exposure Unit ID: Final Grade Soil - Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.418 0.418 0.418 5.9E-06 8.9E-07 6.8E-06
7440-38-2 Arsenic, Inorganic 2.91 2.91 2.91 3.8E-06 5.3E-07 7.5E-11 4.3E-06 7.4E-02 8.8E-03 3.1E-06 8.3E-02
7440-39-3 Barium 85.8 85.8 85.8 5.5E-03 2.8E-06 5.5E-03
7439-92-1 ~Lead and Compounds 12.3 12.3 12.3 <SL**<SL**<SL**
7439-97-6 ~Mercury (elemental)0.0901 0.0901 0.0901 7.8E-03 7.8E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone)0.236 0.236 0.236 5.0E-06 3.5E-06 8.5E-06
75-09-2 Methylene Chloride 0.0961 0.0961 0.0961 1.3E-09 3.0E-10 1.6E-09 2.0E-04 4.9E-05 2.5E-04
7782-49-2 Selenium 0.856 0.856 0.856 2.2E-03 6.9E-10 2.2E-03
108-88-3 Toluene 0.0065 0.0065 0.0065 1.0E-06 2.7E-07 1.3E-06
Cumulative:4.3E-06 9.9E-02
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 19054-15-060
Exposure Unit ID: Final Grade Soil - Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.418 0.418 0.418 4.0E-07 2.1E-07 6.1E-07
7440-38-2 Arsenic, Inorganic 2.91 2.91 2.91 8.0E-07 1.7E-07 1.7E-11 9.7E-07 5.0E-03 1.1E-03 7.5E-07 6.0E-03
7440-39-3 Barium 85.8 85.8 85.8 3.7E-04 6.6E-07 3.7E-04
7439-92-1 ~Lead and Compounds 12.3 12.3 12.3 <SL**<SL**<SL**
7439-97-6 ~Mercury (elemental)0.0901 0.0901 0.0901 1.9E-03 1.9E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone)0.236 0.236 0.236 3.4E-07 8.3E-07 1.2E-06
75-09-2 Methylene Chloride 0.0961 0.0961 0.0961 5.9E-11 2.5E-11 8.4E-11 1.4E-05 1.2E-05 2.5E-05
7782-49-2 Selenium 0.856 0.856 0.856 1.5E-04 1.6E-10 1.5E-04
108-88-3 Toluene 0.0065 0.0065 0.0065 7.0E-08 6.5E-08 1.3E-07
Cumulative:9.7E-07 8.4E-03
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator