23020 Beltex Mill Brownfields Assessment 20191114

Via E-Mail
November 14, 2019

NC Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646
Attn: Mr. Bill Schmithorst
Re: Brownfields Assessment Report
BFs Number 23020-19-036 130 Performance Drive Belmont, North Carolina
H&H Project No. DRY-003

Dear Bill:
On behalf of WXLY, LLC and Dry Pro Basement Systems, Inc., Hart & Hickman, PC (H&H)
has prepared the attached Brownfields Assessment Report in PDF format for the above-
referenced site. Should you have any questions or need any additional information, please feel
free to contact me.
Sincerely,
Hart & Hickman, PC
Matt Bramblett
Principal

Attachments Cc: Mr. Ron Weatherly, Dry Pro (via email)
Ms. Susan Cooper, WBD (via email)
Mr. Michael Cain, Foundry (via email)

i
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
Brownfields Assessment Report Beltex Mill
130 Performance Drive Belmont, North Carolina Brownfields Project No. 23020-19-036 H&H Job No. DRY-003
Table of Contents
1.0 Introduction .............................................................................................................................1
1.1 Background ............................................................................................................................1
1.2 Previous Environmental Assessments ...................................................................................2
1.3 Brownfields Program Eligibility ...........................................................................................2
2.0 Brownfields Assessment Activities ........................................................................................4
3.0 Soil Assessment Activities.......................................................................................................5
3.1 Soil Sampling Methodologies ................................................................................................5
3.2 Soil Analytical Results ...........................................................................................................6
4.0 Groundwater Sampling Activities ..........................................................................................7
4.1 Groundwater Sampling Methodologies ..................................................................................7
4.2 Groundwater Analytical Results .............................................................................................9
5.0 Quality Assurance – Quality Control ...................................................................................10
6.0 Summary and Conclusions...................................................................................................11

ii \\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
List of Tables
Table 1 Summary of Soil Analytical Data
Table 2 Summary of Temporary Well Construction
Table 3 Summary of Groundwater Analytical Data
List of Figures
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Sample Location Map
List of Appendices
Appendix A Boring Logs
Appendix B Laboratory Analytical Report
Appendix C Monitoring Well Sampling Form
1
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
Brownfields Assessment Work Plan Beltex Mill
130 Performance Drive Belmont, North Carolina Brownfields Project No. 23020-19-036 H&H Job No. DRY-003
1.0 Introduction

On behalf of WXLY, LLC and Dry Pro Basement Systems, Inc (Prospective Developer or PD),
Hart & Hickman, PC (H&H) has prepared this Brownfields Assessment for report documenting
additional soil and groundwater sampling activities conducted at the Beltex Mill Brownfields
property (Brownfields Project No. 23020-19-036) located at 130 Performance Drive in Belmont,
Gaston County, North Carolina (Site or subject Site). A Site location map is provided as Figure
1.

The Site is comprised of two contiguous parcels totaling approximately 22.45 acres of land. The
southern portion of the Site is developed with a 54,537 square foot (sq ft) office/warehouse
building with a basement. The remaining portions of the Site consist of asphalt parking areas
and driveways, concrete loading docks, curbing, and sidewalks, landscaped and naturally
vegetated areas, and wooded land. A Site Map is included as Figure 2.

1.1 Background

The Site consisted of agricultural land on the northwestern and southern portions of the Site with
wooded land on the central portion of the Site prior to the late-1930s. In the mid-1950s,
residential structures were developed on the southern portion of the Site until 1979 when the
original footprint of the current industrial building was developed as a textile spinning mill. This
mill was operating under the name Beltex when it closed in 2001. In the mid-1990s and mid-
2000s, the original building footprint was expanded to increase warehouse space and office
space, respectively. Wachs Services, a welding company, occupied the Site building from
approximately 2007 to 2018. Wachs Services vacated the Site in 2018 and the Site building is
currently being renovated for occupancy by the PD. In preparing for the renovation work, an
2
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
Environmental Management Plan (EMP) was submitted and approved by the North Carolina
Department of Environmental Quality (DEQ) Brownfields Program on July 16, 2019.

1.2 Previous Environmental Assessments

H&H conducted previous environmental assessment activities at the Site. The previous
assessment activities included the collection of soil, groundwater, sub-slab, and indoor air
samples. The results of the previous environmental assessment activities were provided to the
Brownfields Program in the Phase I and II Environmental Site Assessment Report dated
November 1, 2018, the Vapor Intrusion Assessment Report dated May 3, 2019, and the
Additional Groundwater Assessment Report dated May 20, 2019.

The results of the environmental assessment activities conducted by H&H indicated the presence
of tetrachloroethene (PCE) in groundwater in the vicinity of the manhole oil pit above the 15A
North Carolina Administrative Code 2L Groundwater Standard (2L Standard) and DEQ Division
of Waste Management (DWM) Non-Residential Vapor Intrusion Groundwater Screening Level
(GWSL).

Results of the soil sampling did not indicate the presence of volatile organic compounds (VOCs)
or polycyclic aromatic hydrocarbon (PAH) compounds above their respective IHSB Preliminary
Soil Remedial Goals (PSRGs). In addition, the results of the sub-slab and indoor air samples did
not indicate the presence of VOCs above their respective Division of Waste Management
(DWM) Non-Residential Soil Gas Screenings Levels (SGSLs) and DWM Non-Residential
Indoor Air Screening Levels (IASLs).

1.3 Brownfields Program Eligibility

Following the environmental assessment activities, the PD applied for eligibility with the DEQ
Brownfields Program. The Site received eligibility into the DEQ Brownfields Program via a
Letter of Eligibility dated May 28, 2019. The PD elected to participate in the Brownfields
Program Redevelopment Now option to expedite the Brownfields process. As part of this
3
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
process, a kick-off/data gap meeting was attended by H&H and the DEQ Brownfields Project
Manager on June 19, 2019 to discuss historical uses of the Site, available environmental
information, proposed redevelopment plans, and data gaps.

Based on the kick-off/data gap meeting, DEQ requested that the PD conduct additional soil and
groundwater assessment activities at the Site in an email dated July 11, 2019 and modified on
July 12, 2019. Based on this e-mail request, H&H prepared a Brownfields Assessment Work
Plan (Work Plan) dated August 26, 2019. The Brownfields Program approved the Work Plan via
e-mail on August 30, 2019. A summary of our additional soil and groundwater assessment
activities conducted in accordance with the approved Work Plan is provided in the following
sections.
4
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
2.0 Brownfields Assessment Activities

In September 2019, H&H conducted Brownfields assessment activities at the Site. The
Brownfields assessment activities included the collection three (3) soil samples and the
collection of one (1) groundwater sample. Prior to conducting subsurface field activities, H&H
contacted NC 811, the public utility locator, to mark subsurface utilities at the Site. H&H also
contracted with a private utility locator to mark utilities which were not identified by the public
locator. Additionally, H&H directed the drilling contractor to hand clear each boring to a depth
of approximately 5 feet (ft) below ground surface (bgs) to further screen the boring locations for
the presence of subsurface utilities.

The assessment activities were performed in general accordance with the DEQ Inactive
Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup (Guidelines) dated
October 2015, the DEQ Division of Waste Management (DWM) Vapor Intrusion Guidance (VI
Guidance) dated March 2018, most recent versions of the U.S. Environmental Protection Agency
(EPA) Region IV Science and Ecosystem Support Division (SESD) Field Branches Quality
System and Technical Procedures guidance, and the DEQ-approved Work Plan (Revision 1).

Details of the soil assessment activities are provided in Section 3.0; details of the groundwater
assessment activities are provided in Section 4.0; quality assurance and quality control
information is provided in Section 5.0; and conclusions based on results of the assessment
activities are provided in Section 6.0.
5
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
3.0 Soil Assessment Activities

On September 20, 2019, H&H contracted Innovative Environmental Technologies (IET) to
advance three (3) soil borings at the Site. To supplement previous sampling activities, one (1)
soil sample (SB-5) was collected adjacent to the manhole oil pit near the previous soil sample
location SB-1, one (1) soil sample (SB-6) was collected in the former septic system area near the
previous soil sample location SB-2, and one (1) soil sample (SB-7) was collected at the manhole
oil pit discharge location near the previous soil sample location SB-4. The Brownfields
assessment soil sample locations are shown on Figure 3.
3.1 Soil Sampling Methodologies The soil borings were advanced utilizing a decontaminated stainless-steel hand auger. During
boring advancement, continuous soil samples were collected from each boring from the hand
auger bucket. Soil samples were logged for lithological description and field screened for
indication of potential impacts by observation for staining, odors, and the presence of organic
vapors using a calibrated photoionization detector (PID). Field screening results did not indicate
the obvious presence of impacts. Soil boring logs are included in Appendix A.

Following boring advancement, a soil sample was collected from each soil boring. Per DEQ’s
request, and accordance with the approved Work Plan, a sample was collected from 3 ft to 4 ft
from SB-5, 5 ft to 6 ft from SB-6, and 1 ft to 2 ft from SB-7. The soil samples were placed
directly into dedicated laboratory supplied sample containers, labeled with the sample
identification, date, time, and requested analysis, and placed in a laboratory supplied cooler with
ice. Soil samples were submitted to Pace Analytical (Pace), a North Carolina certified laboratory
under standard chain of custody protocols for analysis of Resource Conservation and Recovery
Act (RCRA) metals by EPA Method 6020/7471B.

Following sampling activities, the soil borings were properly abandoned and the ground surface
was repaired to previous conditions.

6
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
3.2 Soil Analytical Results

Laboratory analytical results were compared to DEQ Residential and Industrial/Commercial
PSRGs dated May 2019 and published naturally occurring background metals concentrations in
North Carolina soils described in Elements in North American Soils by Dragun and Chekiri,
2005. A discussion of the laboratory analytical results for the September 2019 Brownfields
assessment soil samples is provided below, and a summary of the laboratory analytical data is
provided in Table 1. The laboratory analytical data report and chain of custody record are
included in Appendix B.

As expected, several metals were detected at concentrations above laboratory detection limits.
Arsenic was detected in each soil sample above the IHSB Residential PSRG. However, the
concentrations detected were within the range of naturally occurring background concentrations
(Dagun and Chekiri, 2005). No metals were detected at concentrations exceeding the published
background metals concentrations and/or DEQ Industrial/Commercial PSRGs at the Site.

7
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
4.0 Groundwater Sampling Activities

On September 20, 2019, under the direction of H&H, IET installed one (1) temporary
groundwater monitoring well at the Site (TMW-4). TMW-4 was installed northwest of the Site
building to assess groundwater quality topographically downgradient of the Site building. The
location of the temporary monitoring well is shown on Figure 3. A summary of the temporary
monitoring well installation, sampling, and results is provided below.
4.1 Groundwater Sampling Methodologies

Due to shallow boring refusal encountered during previous assessments, air rotary methods were
utilized to advance the temporary monitoring well boring to approximately 45 ft below ground
surface (bgs). The well construction record and well abandonment record for TMW-4 are
included in Appendix A. Following boring advancement, the temporary monitoring well was
constructed with a 20 ft section of 2-inch diameter PVC with 0.010-inch slotted screen set to
bracket the water table and connected to a 2-inch PVC riser installed in the boring up to the
ground surface. A sand filter pack was placed from the bottom of the boring to approximately 2
ft above the top of the well screen. The temporary well was completed by placing a minimum of
2 ft of hydrated bentonite seal above the sand filter pack.

Following installation, the temporary monitoring well was allowed to equilibrate to static
conditions, and a decontaminated electronic water level indicator was used to measure the depth
to the water table relative to the ground surface. The water level was measured at 33.28 ft bgs.
Well construction and water level information are provided on Table 2.

8
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
Following the depth to water measurement, the temporary monitoring well was developed
utilizing a decontaminated Tornado Sampling Pump. During development, approximately 8 well
volumes were removed from the well. However, following development, turbidity remained
above 10 NTUs. As such, H&H secured the temporary monitoring well and left the Site to allow
the temporary monitoring well time to equilibrate.

On September 22, 2019, H&H remobilized to the Site to collect the groundwater sample. The
groundwater sample was collected utilizing low flow/low stress purging techniques utilizing a
bladder pump and dedicated polyethylene tubing. The intake point of the pump tubing was
placed in the approximate mid-portion of the screened interval of the temporary monitoring well
and groundwater was removed at a rate no greater than 200 milliliters per minute. H&H utilized
water quality meters to collect measurements of pH, temperature, dissolved oxygen, oxidation
reduction potential, turbidity, and specific conductivity at three to five-minute intervals during
the purging process. Purging was complete when the field parameters stabilized (pH ± 0.1 SU,
conductivity varied no more than 5%, and turbidity was less than 10 NTUs. The monitoring well
sampling record is provided in Appendix C.

Once groundwater parameters stabilized, the groundwater sample was collected directly into
laboratory supplied sample containers and submitted for laboratory analysis of VOCs by EPA
Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method 8270, and RCRA
metals by EPA Method 6020/7471. The sample containers were labeled with the sample
identification, date, time, and requested analysis, and placed in a laboratory supplied cooler with
ice. The groundwater samples were then delivered to Pace, a North Carolina certified laboratory
under standard chain of custody protocols.

Following installation and sampling activities, the temporary monitoring well was properly
abandoned by a licensed well driller, and the ground surface was repaired to previous conditions.

9
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
4.2 Groundwater Analytical Results
A tabular summary of the groundwater sample analytical results is presented in Table 3. The
laboratory analytical report and chain of custody record are provided in Appendix B.
Groundwater data were compared to the DEQ 15A NCAC 2L Groundwater Quality Standards
(2L Standards) dated April 2013 and the DEQ DWM Residential and Non-Residential Vapor
Intrusion Groundwater Screening Levels (GWSLs) dated February 2018.

PCE was detected in TMW-4 (1.4 µg/L) above the 2L Standard of 0.7 µg/L. The detected PCE
concentration is below the NC DEQ DWM Non-Residential GWSL of 48 µg/L. No additional
VOCs or SVOCs were identified in groundwater sample collected from TMW-4.

Low levels of barium, chromium, and lead were detected in the groundwater sample from TMW-
4. However, no metals were detected at concentrations exceeding 2L Standards. The metals
detected may be naturally occurring.

10
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
5.0 Quality Assurance – Quality Control

For field and laboratory QA/QC purposes, H&H collected one duplicate soil sample from soil
boring SB-5 (SB-DUP) and one duplicate groundwater sample from TMW-4 (TMW-DUP). The
duplicate samples were analyzed for the same compounds as the parent samples. The analytical
results of the duplicate samples are provided in the attached tables and generally comparable to
the results of the parent samples indicating good repeatability for the duplicate samples.

In addition, a laboratory supplied trip blank was placed into the laboratory supplied cooler that
was used for water samples and accompanied field personnel during groundwater sample
collection activities. The trip blank was analyzed for VOCs by EPA Method 8260. No
constituents were detected above laboratory detection limits in the laboratory supplied trip blank.
11
\\HHFS01\MasterFiles\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Brownfields Assesment\Brownfields Assessment _Beltex Mill (BPN 23020-19-036)_.doc
6.0 Summary and Conclusions

H&H has completed Brownfields assessment activities at the Beltex Mill Brownfields property
(Brownfields Project No. 23020-19-036) located at 130 Performance Drive in Belmont, Gaston
County, North Carolina. The purpose of the assessment was to supplement previous soil and
groundwater assessment activities conducted in October 2018 and April 2019. The assessment
activities included the collection of three (3) soil samples and one (1) groundwater sample. The
work was conducted in accordance with the DEQ-approved work plan. A summary of the soil
and groundwater assessment results is provided below.

• Laboratory analytical results of the soil sampling did not indicate the presence of
compounds above naturally occurring levels for metals and/or IHSB PSRGs.

• Laboratory analytical results of the groundwater sample indicated the presence of PCE
(1.4 µg/L) above the 2L Standard of 0.7 µg/L but below the DWM GWSL of 48 µg/L.

Based on these results, H&H does not recommend additional Brownfields assessment activities
at this time.

Table 1Summary of Soil Analytical DataBeltex MillBrownfields Project No. 23020-19-036130 Performance DriveBelmont, North CarolinaH&H Job No. DRY-003Northwest of the Site Sample IDSB-1 SB-5SB-DUP (3)SB-2 SB-6 SB-3 SB-4 SB-7Depth (ft)5-7 3-4 3-4 3-5 5-6 3-5 1-2 1-2Date Collected10/12/20189/20/2019 9/20/2019 10/12/2018 9/20/2019 10/12/2018 10/12/2018 9/20/2019TPH GRO (8015C) mg/kgGasoline Range Organics (C6-C10)------ND NA NA NA NA NA NA NATPH DRO (8015C) mg/kgDiesel Range Organics (C10-C28)------ND NA NA NA NA NA NA NAVOCs (8260B/5035A) mg/kgMethylene chloride0.025586506.2 J NA NA 5.5 J NA<23.07.5 J NARCRA Metals (6020 and 7471) mg/kgRangeAverageArsenic5.80.683.01 - 18 4.8 NA 0.494J 0.724 NA 0.683 NA NA 2.11Barium5803,10047,000 50 - 1,000 356 NA 20.0 21.6 NA 96.7 NA NA 82.9Cadmium3.0142001 - 10* 4.3* NA<0.0863 <0.0872NA 0.119 J NA NA<0.0980Chromium360,000 23,000100,000 7 - 300 65 NA 33.7 35.4 NA 23.2 NA NA 41.5Lead270400800ND - 50 16 NA 0.612 0.647 NA 3.64 NA NA 3.64Mercury1.02.33.10 0.03 - 0.52 0.121 NA 0.00345 J 0.00444 J NA 0.00540 J NA NA 0.0603Selenium2.17.81,200 <0.1 - 0.8 0.42 NA<0.205 <0.207NA<0.225NA NA 0.712Silver3.4781,200NS NS NA<0.167 <0.169NA<0.184NA NA<0.190PAHs (8270D) mg/kg------BRL NA NA BRL NA BRL BRL NANotes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (February 2018).2) Published background metals concentrations in North Carolina soils are provided from Elements in North American Soils by Dragun and Chekiri, 2005; * = value from southeast US3) SB-DUP was collected from the parent soil boring SB-5Constituents detected in at least one sample are shown above; with the exception of the 8 RCRA metals, refer to the laboratory report Methylene chloride is likely laboratory-introduced contaminantMethod number follows parameter in parenthesismg/kg = milligrams/kilogram; SB = Soil BoringTPH-GRO = gasoline range total petroleum hydrocarbonsTPH-DRO = diesel range total petroleum hydrocarbonsVOCs = volatile organic compoundsRCRA = Resource Conservation and Recovery Act PAHs = polycyclic aromatic hydrocarbonsBRL = below reporting limit; J = estimated value between reporting limit and method detection limitNA = not analyzed, -- = not applicable--Sample LocationAdjacent to Manhole Oil PitFormer Septic System AreaManhole Oil Discharge LocationDEQ IHSB Protection of Groundwater PSRGs (1) DEQ IHSB Residential Use PSRGs (1) DEQ IHSB Industrial/Commercial PSRGs (1)North Carolina Background Levels (2)S:\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Tables\FInal Tables11/1/2019Table 1Hart & Hickman, PC
Table 2Summary of Temporary Well ConstructionBeltex MillBrownfields Project No. 23020-19-036130 Performance DriveBelmont, North CarolinaH&H Job No. DRY-003Well Well Screen WaterDiameter Depth Interval Table Depth(inches) (ft) (ft) (ft bgs)TMW-110/12/20182 40 30-40 33.5TMW-2 4/17/2019 2 41 26-41 29.00TMW-3 4/18/2019 2 46 31-46 35.73TMW-4 9/20/2019 2 50 25.7-45.7 33.28Notes:bgs = below ground surfaceInstallation DateDepth to groundwater measurements collected from the monitoring wells on date of installationMonitoring Well IdentificationTMW = temporary monitoring wellS:\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Tables\FInal Tables11/1/2019Table 2Hart & Hickman, PC
Table 3Summary of Groundwater Analytical DataBeltex MillBrownfields Project No. 23020-19-036130 Performance DriveBelmont, North CarolinaH&H Job No. DRY-003Adjacent to Manhole Oil PitEast of the Site buildingSample IDTMW-1 TMW-2 TMW-3TMW-DUP (3)TMW-4TMW-DUP (4)Field BlankTrip BlankDateVOCs (8260B) µg/LTetrachloroethene0.74877.7<1.0<1.0<1.01.41.4<1.0<0.16Trichloroethene34.40.81 J<1.0<1.0<1.0<0.22<0.22<1.0<0.22Toluene600160000.27 J<1.0<1.0<1.0<0.24<0.24<1.0<0.24SVOCs (8270) µg/L----NABRLBRLNABRLBRLNANAPAHs (8270D SIM) µg/L----BRLNANANANANANANARCRA Metals (6020/7470) Total µg/LArsenic10--NA0.496 J0.526 JNA<0.250<0.250NANABarium700--NA67.211.1NA20.321.3NANACadmium2--NA<0.160<0.160NA<0.160<0.160NANAChromium10--NA4.386.57NA2.992.85NANALead15--NA1.02 J<0.240NA<0.2400.322 JNANAMercury10.75NA<0.0490<0.0490NA<0.0490<0.0490NANASelenium20--NA0.409 J0.718 JNA<0.380<0.380NANASilver20--NA<0.310<0.310NA<0.310<0.310NANARCRA Metals (6020/7470) Dissolved µg/LArsenic10--NA<0.2500.423 JNANANANANABarium700--NA26.67.81NANANANANACadmium2--NA<0.160<0.160NANANANANAChromium10--NA<0.5400.709 JNANANANANALead15--NA0.893 J<0.240NANANANANAMercury10.75NA<0.0490<0.0490NANANANANASelenium20--NA<0.380<0.380NANANANANASilver20--NA<0.310<0.310NANANANANANotes:1) North Carolina 15A NCAC 02L Groundwater Standards (NC 2L Standard) (April 2013) 2) North Carolina Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSL) (February 2018)3) TMW-DUP was collected from the parent monitoring well TMW-34) TMW-DUP was collected from the parent monitoring well TMW-4Bold values exceed NC 2L StandardsUnderline values exceed NC Non-Residential Vapor Intrusion GWSLsMethod detection limits are shown above for non-detectionsConstituents detected in at least one sample are shown above; with the exception of the 8 RCRA metals, refer to the laboratory report Method number follows parameter in parenthesisµg/L = micrograms/literVOCs = volatile organic compoundsSVOCs = semi-volatile organic compoundsPAHs = polycyclic aromatic hydrocarbonsRCRA= Resource Conservation and Recovery ActQA/QC= Quality Assurance/Quality ControlNA = not analyzed; BRL = below reporting limits-- = not applicable; J = estimated value between reporting limit and method detection limitDowngradient of Septic Systems Northwest of the Site BuildingSample Location9/22/2019QA/QCNC 2L Standard (1) (µg/L)NC Non-Residential Vapor Intrusion GWSL (2) (µg/L)10/13/2018 4/18/2019 4/19/2019 4/19/2019 9/22/2019 9/22/2019 4/19/2019S:\AAA-Master Projects\Dry Pro Basement Systems (DRY)\DRY-003\Tables\FInal Tables11/1/2019Table 3Hart & Hickman, PC
TITLE
PROJECT
SITE LOCATION MAP
BELTEX MILLBROWNFIELDSPROJECT NO. 23020-19-036130PERFORMANCE DRIVE
BELMONT, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
10-21-2019 0
1DRY-003
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
MOUNT HOLLY, NORTH CAROLINA, 1993
REVISION NO. 0
JOB NO. DRY-003
DATE: 10-18-19
FIGURE NO. 2
BELTEX MILL
BROWNFIELDS PROJECT NO. 23020-19-036
130 PERFORMANCE DRIVE
BELMONT, NORTH CAROLINA
SITE MAP
LEGEND
SITE PROPERTY BOUNDARY
FORMER LEACHFIELD LINES
CURRENT LEACHFIELD LINES
AIR COMPRESSOR
DUMPSTER
PAD-MOUNTED TRANSFORMER
POLE-MOUNTED TRANSFORMER
SEPTIC SYSTEM
WATER SUPPLY WELL
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
NOTES:
1. BASE MAP OBTAINED FROM NC ONEMAP.
MANHOLE OIL PIT
OIL PIT WATER
DISCHARGE TO DITCH
PER
F
O
R
M
A
N
C
E
D
RI
V
E
PERFORMANCE DR
IVE
MCAD
E
N
VI
L
L
E
R
O
A
D
PEACH ORCHARD ROADFORMER DRIVE-IN THEATER
RAMSEY PRODUCTS CORPORATION
(135 PERFORMANCE DRIVE)
MCADENVILLE DUMP
(332 MCADENVILLE ROAD)
FORMER BELTEX
CORPORATION
(345 MCADENVILLE ROAD)
INDUSTRIAL PROPERTY
(130 PERFORMANCE DRIVE)
RESIDENCE
(320 MCADENVILLE ROAD)
(PARCEL ID:
219017)
DU
K
E

E
N
E
R
G
Y

R
I
G
H
T
-
O
F
-
W
A
Y
SEPTIC SYSTEMS (2)
RESIDENCE
(332 MCADENVILLE ROAD)
RESIDENCE
(330 MCADENVILLE ROAD)
BASEMENT
AREA
RESIDENTIAL
PER
F
O
R
M
A
N
C
E
D
RI
V
E
RAMSEY PRODUCTS
CORPORATION
(135 PERFORMANCE DRIVE)
DUKE ENERGY
RIGHT-OF-WAY
BASE
M
E
N
T
AREA
TMW-4
INDUSTRIAL PROPERTY
(130 PERFORMANCE DRIVE)
RESIDENCE
(320 MCADENVILLE
ROAD)
MANHOLE
OIL PIT
PERFORMANCE DR
IVE
SEPTIC SYSTEMS (2)
MCAD
E
N
VI
L
L
E
R
O
A
D
RESIDENCE
(332 MCADENVILLE ROAD)RESIDENCE
(330 MCADENVILLE ROAD)
SB-4 SB-7
SB-5
SB-6SB-2
SB-3
TMW-4/SB-1
TMW-3
TMW-2
PEACH ORCHARD ROADREVISION NO. 0
JOB NO. DRY-003
DATE: 10-18-19
FIGURE NO. 3
BELTEX MILL
BROWNFIELDS PROJECT NO. 23020-19-036
130 PERFORMANCE DRIVE
BELMONT, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
FORMER LEACHFIELD LINES
CURRENT LEACHFIELD LINES
SEPTIC SYSTEM
WATER SUPPLY WELL
PREVIOUS TEMPORARY MONITORING WELL
PREVIOUS SOIL BORING
BROWNFIELDS ASSESSMENT TEMPORARY
MONITORING WELL
BROWNFIELDS ASSESSMENT SOIL BORING
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
NOTES:
1. BASE MAP OBTAINED FROM NC ONEMAP.
2. PREVIOUS SOIL AND GROUNDWATER ASSESSMENT
OCCURRED IN OCTOBER 2018 AND APRIL 2019.

Appendix A
Boring Logs
NOTES: Sample collected for RCRA Metals.
generated using GroundLogs.online
Client:
Project:
Address:
Dry Pro Systems
DRY-003
130 Performance Drive, Belmont, NC
BORING LOG
Boring No.
Page:
SB-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
9/20/2019
9/20/2019
IET
Other
Hand Auger
Ayla Homer
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
4.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
GR 1.00
(0') SILT (ML); little fine-coarse gravel, very stiff, dry, brown
(1') SILT (ML); stiff, dry, brown
(3') SILT (ML); stiff, dry, brown
(4') Boring terminated
1.2
0.7
0.9
1.2 SB-5(3-4)
0
5
10
15
20
NOTES: Hole precleared by IET using hand auger. Sample collected for RCRA Metals.
generated using GroundLogs.online
Client:
Project:
Address:
Dry Pro Systems
DRY-003
130 Performance Drive, Belmont, NC
BORING LOG
Boring No.
Page:
SB-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
9/20/2019
9/20/2019
IET
Other
Hand Auger
Ayla Homer
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
GR 1.00
(0') SILT with sand (ML); some clay, very stiff, dry, brown
(0.5') SILT with sand (ML); stiff, dry, brown
(1') SILT (ML); stiff, dry, Light brown mottled with dark brown
(5') Elastic SILT (MH); stiff, dry, Brown mottled with Light brown
(6') Boring terminated
1.3
3.8
4.0
1.5
1.5 SB-6(5-6)
0
5
10
15
20
NOTES: Sample collected for RCRA Metals
generated using GroundLogs.online
Client:
Project:
Address:
Dry Pro Systems
DRY-003
130 Performance Drive, Belmont, NC
BORING LOG
Boring No.
Page:
SB-7
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
9/20/2019
9/20/2019
IET
Other
Hand Auger
Ayla Homer
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
GR 1.00
(0') SILT with sand (ML); trace fine-coarse gravel, hard, dry, brown
(1') SILT with sand (ML); very stiff, dry, light reddish-brown
(2') Boring terminated
1.3
0.7 SB-4(1-2)
0
5
10
15
20
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:

Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
one
9/20/2019 TMW-4
Wachs Services
130 Performance Dr.,Belmont 28012
Gaston
35 15 26 81 03 42
45
32
4
Air Rotary
9/20/2019
32 45 Brown silty soil/Rock
0 25 2 sch40 pvc
25 45 2 0.010 sch40 pvc
0
23
23
45
Bentonite
#2 Sand Poured
600LB/Poured
See Consultant Log
Supervised By Mike Tynan / Driller # 2725-A
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
Mike Tynan
2725-A one
<3
IET
94 lbs portland cement 6.5 gal water
9/23/19
Removed 5 feet of PVC casing. Filled entire well with neat cement
through rigid tremie pipe.
Wachs Services
130 Performance Dr, Belmont 28012 9/24/19
Gaston
35 15 26 81 03 42
TMW-4
45
4
32
25
20

Appendix B
Laboratory Analytical Report
#=CL#
October 17, 2019
LIMS USE: FR - MATT BRAMBLETT
LIMS OBJECT ID: 92446606
92446606
Project:
Pace Project No.:
RE:
Matt Bramblett
Hart & Hickman
2923 S.Tyron St.
Charlotte, NC 28203
DRY-003
Dear Matt Bramblett:
Enclosed are the analytical results for sample(s) received by the laboratory on September 23, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Per client request, report revised 10/17/19 to update sample ID from SB-4 (1-2) to SB-7 (1-2).
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 40
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92446606
DRY-003
Pace Analytical National Certification IDs
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 40
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92446606
DRY-003
Lab ID Sample ID Matrix Date Collected Date Received
92446606001 SB-5 (3-4)Solid 09/20/19 09:40 09/23/19 11:52
92446606002 SB-7 (1-2)Solid 09/20/19 10:00 09/23/19 11:52
92446606003 SB-6 (5-6)Solid 09/20/19 12:00 09/23/19 11:52
92446606004 TRIP BLANK Water 09/22/19 00:00 09/23/19 11:52
92446606005 TMW-4 Water 09/22/19 10:30 09/23/19 11:52
92446606006 TMW-DUP Water 09/22/19 00:00 09/23/19 11:52
92446606007 SB-DUP Solid 09/20/19 00:00 09/23/19 11:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 40
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92446606
DRY-003
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92446606001 SB-5 (3-4)EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
SM 2540G 1 PANJHH
92446606002 SB-7 (1-2)EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
SM 2540G 1 PANJHH
92446606003 SB-6 (5-6)EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
SM 2540G 1 PANJHH
92446606004 TRIP BLANK EPA 8260D 63 PASI-CDLK
92446606005 TMW-4 EPA 6020B 7 PANJPD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CDLK
92446606006 TMW-DUP EPA 6020B 7 PANJPD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CDLK
92446606007 SB-DUP EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
SM 2540G 1 PANJHH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:SB-5 (3-4)Lab ID:92446606001 Collected:09/20/19 09:40 Received:09/23/19 11:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 0.494J mg/kg 09/27/19 13:18 7440-38-2 J09/27/19 11:150.539 0.135 5
Barium 20.0 mg/kg 09/27/19 13:18 7440-39-309/27/19 11:151.08 0.173 5
Cadmium ND mg/kg 09/27/19 13:18 7440-43-909/27/19 11:150.539 0.0863 5
Chromium 33.7 mg/kg 09/27/19 13:18 7440-47-309/27/19 11:151.08 0.291 5
Lead 0.612 mg/kg 09/27/19 13:18 7439-92-109/27/19 11:150.539 0.129 5
Selenium ND mg/kg 09/27/19 13:18 7782-49-209/27/19 11:150.539 0.205 5
Silver ND mg/kg 09/27/19 13:18 7440-22-409/27/19 11:150.539 0.167 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.00345J mg/kg 09/29/19 21:49 7439-97-6 J09/27/19 12:580.0324 0.00302 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 92.7 %09/30/19 15:2609/30/19 15:181
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:SB-7 (1-2)Lab ID:92446606002 Collected:09/20/19 10:00 Received:09/23/19 11:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 2.11 mg/kg 09/27/19 13:35 7440-38-209/27/19 11:150.612 0.153 5
Barium 82.9 mg/kg 09/27/19 13:35 7440-39-309/27/19 11:151.22 0.196 5
Cadmium ND mg/kg 09/27/19 13:35 7440-43-909/27/19 11:150.612 0.0980 5
Chromium 41.5 mg/kg 09/27/19 13:35 7440-47-309/27/19 11:151.22 0.331 5
Lead 3.64 mg/kg 09/27/19 13:35 7439-92-109/27/19 11:150.612 0.147 5
Selenium 0.712 mg/kg 09/27/19 13:35 7782-49-209/27/19 11:150.612 0.233 5
Silver ND mg/kg 09/27/19 13:35 7440-22-409/27/19 11:150.612 0.190 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.0603 mg/kg 09/29/19 21:51 7439-97-609/27/19 12:580.0367 0.00343 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 81.6 %09/30/19 15:2609/30/19 15:181
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:SB-6 (5-6)Lab ID:92446606003 Collected:09/20/19 12:00 Received:09/23/19 11:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 0.683 mg/kg 09/27/19 13:38 7440-38-209/27/19 11:150.592 0.148 5
Barium 96.7 mg/kg 09/27/19 13:38 7440-39-309/27/19 11:151.18 0.189 5
Cadmium 0.119J mg/kg 09/27/19 13:38 7440-43-9 J09/27/19 11:150.592 0.0947 5
Chromium 23.2 mg/kg 09/27/19 13:38 7440-47-309/27/19 11:151.18 0.320 5
Lead 3.64 mg/kg 09/27/19 13:38 7439-92-109/27/19 11:150.592 0.142 5
Selenium ND mg/kg 09/27/19 13:38 7782-49-209/27/19 11:150.592 0.225 5
Silver ND mg/kg 09/27/19 13:38 7440-22-409/27/19 11:150.592 0.184 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.00540J mg/kg 09/29/19 21:59 7439-97-6 J09/27/19 12:580.0355 0.00332 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 84.4 %09/30/19 15:2609/30/19 15:181
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TRIP BLANK Lab ID:92446606004 Collected:09/22/19 00:00 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 09/27/19 03:06 67-64-125.0 6.2 1
Benzene ND ug/L 09/27/19 03:06 71-43-21.0 0.15 1
Bromobenzene ND ug/L 09/27/19 03:06 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 09/27/19 03:06 74-97-5 IK1.0 0.34 1
Bromodichloromethane ND ug/L 09/27/19 03:06 75-27-41.0 0.26 1
Bromoform ND ug/L 09/27/19 03:06 75-25-21.0 0.62 1
Bromomethane ND ug/L 09/27/19 03:06 74-83-9 IK,v22.0 0.62 1
2-Butanone (MEK)ND ug/L 09/27/19 03:06 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 09/27/19 03:06 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 09/27/19 03:06 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/27/19 03:06 75-00-3 IK1.0 0.49 1
Chloroform ND ug/L 09/27/19 03:06 67-66-35.0 2.3 1
Chloromethane ND ug/L 09/27/19 03:06 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 09/27/19 03:06 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 09/27/19 03:06 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 09/27/19 03:06 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 09/27/19 03:06 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 09/27/19 03:06 106-93-41.0 0.26 1
Dibromomethane ND ug/L 09/27/19 03:06 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 09/27/19 03:06 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 09/27/19 03:06 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 09/27/19 03:06 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 09/27/19 03:06 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 09/27/19 03:06 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 09/27/19 03:06 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 09/27/19 03:06 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 09/27/19 03:06 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 09/27/19 03:06 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 09/27/19 03:06 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 09/27/19 03:06 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 09/27/19 03:06 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 09/27/19 03:06 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 09/27/19 03:06 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 09/27/19 03:06 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 09/27/19 03:06 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 09/27/19 03:06 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 09/27/19 03:06 87-68-31.0 0.44 1
2-Hexanone ND ug/L 09/27/19 03:06 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 09/27/19 03:06 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 09/27/19 03:06 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/27/19 03:06 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 09/27/19 03:06 1634-04-41.0 0.28 1
Naphthalene ND ug/L 09/27/19 03:06 91-20-31.0 0.35 1
Styrene ND ug/L 09/27/19 03:06 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 09/27/19 03:06 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 09/27/19 03:06 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TRIP BLANK Lab ID:92446606004 Collected:09/22/19 00:00 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 09/27/19 03:06 127-18-41.0 0.16 1
Toluene ND ug/L 09/27/19 03:06 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 09/27/19 03:06 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 09/27/19 03:06 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 09/27/19 03:06 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 09/27/19 03:06 79-00-51.0 0.24 1
Trichloroethene ND ug/L 09/27/19 03:06 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 09/27/19 03:06 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 09/27/19 03:06 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 09/27/19 03:06 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 09/27/19 03:06 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 09/27/19 03:06 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 09/27/19 03:06 179601-23-12.0 0.41 1
o-Xylene ND ug/L 09/27/19 03:06 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)105 %09/27/19 03:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)79 %09/27/19 03:06 17060-07-070-130 1
Toluene-d8 (S)111 %09/27/19 03:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TMW-4 Lab ID:92446606005 Collected:09/22/19 10:30 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Arsenic ND ug/L 09/26/19 15:58 7440-38-209/26/19 09:482.00 0.250 1
Barium 20.3 ug/L 09/26/19 15:58 7440-39-309/26/19 09:485.00 0.360 1
Cadmium ND ug/L 09/26/19 15:58 7440-43-909/26/19 09:481.00 0.160 1
Chromium 2.99 ug/L 09/26/19 15:58 7440-47-3 B09/26/19 09:482.00 0.540 1
Lead ND ug/L 09/26/19 15:58 7439-92-109/26/19 09:482.00 0.240 1
Selenium ND ug/L 09/26/19 15:58 7782-49-209/26/19 09:482.00 0.380 1
Silver ND ug/L 09/26/19 15:58 7440-22-409/26/19 09:482.00 0.310 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 09/25/19 09:55 7439-97-609/24/19 20:400.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 09/24/19 19:22 83-32-909/24/19 12:0110.0 1.6 1
Acenaphthylene ND ug/L 09/24/19 19:22 208-96-809/24/19 12:0110.0 1.6 1
Aniline ND ug/L 09/24/19 19:22 62-53-309/24/19 12:0110.0 1.9 1
Anthracene ND ug/L 09/24/19 19:22 120-12-709/24/19 12:0110.0 1.7 1
Benzo(a)anthracene ND ug/L 09/24/19 19:22 56-55-309/24/19 12:0110.0 1.8 1
Benzo(a)pyrene ND ug/L 09/24/19 19:22 50-32-809/24/19 12:0110.0 2.1 1
Benzo(b)fluoranthene ND ug/L 09/24/19 19:22 205-99-209/24/19 12:0110.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 09/24/19 19:22 191-24-209/24/19 12:0110.0 1.4 1
Benzo(k)fluoranthene ND ug/L 09/24/19 19:22 207-08-909/24/19 12:0110.0 1.9 1
Benzoic Acid ND ug/L 09/24/19 19:22 65-85-009/24/19 12:0150.0 43.0 1
Benzyl alcohol ND ug/L 09/24/19 19:22 100-51-609/24/19 12:0120.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 09/24/19 19:22 101-55-309/24/19 12:0110.0 1.6 1
Butylbenzylphthalate ND ug/L 09/24/19 19:22 85-68-709/24/19 12:0110.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 09/24/19 19:22 59-50-709/24/19 12:0120.0 2.8 1
4-Chloroaniline ND ug/L 09/24/19 19:22 106-47-809/24/19 12:0120.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 09/24/19 19:22 111-91-109/24/19 12:0110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/24/19 19:22 111-44-409/24/19 12:0110.0 1.8 1
2-Chloronaphthalene ND ug/L 09/24/19 19:22 91-58-709/24/19 12:0110.0 1.5 1
2-Chlorophenol ND ug/L 09/24/19 19:22 95-57-809/24/19 12:0110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/24/19 19:22 7005-72-309/24/19 12:0110.0 1.6 1
Chrysene ND ug/L 09/24/19 19:22 218-01-909/24/19 12:0110.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 09/24/19 19:22 53-70-309/24/19 12:0110.0 1.6 1
Dibenzofuran ND ug/L 09/24/19 19:22 132-64-909/24/19 12:0110.0 1.5 1
1,2-Dichlorobenzene ND ug/L 09/24/19 19:22 95-50-109/24/19 12:0110.0 1.3 1
1,3-Dichlorobenzene ND ug/L 09/24/19 19:22 541-73-109/24/19 12:0110.0 1.5 1
1,4-Dichlorobenzene ND ug/L 09/24/19 19:22 106-46-709/24/19 12:0110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/24/19 19:22 91-94-109/24/19 12:0120.0 3.0 1
2,4-Dichlorophenol ND ug/L 09/24/19 19:22 120-83-209/24/19 12:0110.0 1.4 1
Diethylphthalate ND ug/L 09/24/19 19:22 84-66-209/24/19 12:0110.0 2.4 1
2,4-Dimethylphenol ND ug/L 09/24/19 19:22 105-67-909/24/19 12:0110.0 1.4 1
Dimethylphthalate ND ug/L 09/24/19 19:22 131-11-309/24/19 12:0110.0 1.6 1
Di-n-butylphthalate ND ug/L 09/24/19 19:22 84-74-209/24/19 12:0110.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/24/19 19:22 534-52-109/24/19 12:0120.0 15.2 1
2,4-Dinitrophenol ND ug/L 09/24/19 19:22 51-28-509/24/19 12:0150.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TMW-4 Lab ID:92446606005 Collected:09/22/19 10:30 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 09/24/19 19:22 121-14-209/24/19 12:0110.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/24/19 19:22 606-20-209/24/19 12:0110.0 1.4 1
Di-n-octylphthalate ND ug/L 09/24/19 19:22 117-84-009/24/19 12:0110.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/24/19 19:22 117-81-709/24/19 12:016.0 2.1 1
Fluoranthene ND ug/L 09/24/19 19:22 206-44-009/24/19 12:0110.0 1.7 1
Fluorene ND ug/L 09/24/19 19:22 86-73-709/24/19 12:0110.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 09/24/19 19:22 87-68-3 v109/24/19 12:0110.0 2.0 1
Hexachlorobenzene ND ug/L 09/24/19 19:22 118-74-109/24/19 12:0110.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 09/24/19 19:22 77-47-409/24/19 12:0110.0 1.7 1
Hexachloroethane ND ug/L 09/24/19 19:22 67-72-109/24/19 12:0110.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/24/19 19:22 193-39-509/24/19 12:0110.0 1.6 1
Isophorone ND ug/L 09/24/19 19:22 78-59-109/24/19 12:0110.0 1.6 1
1-Methylnaphthalene ND ug/L 09/24/19 19:22 90-12-009/24/19 12:0110.0 1.4 1
2-Methylnaphthalene ND ug/L 09/24/19 19:22 91-57-609/24/19 12:0110.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/24/19 19:22 95-48-709/24/19 12:0110.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/24/19 19:22 15831-10-409/24/19 12:0110.0 1.2 1
Naphthalene ND ug/L 09/24/19 19:22 91-20-309/24/19 12:0110.0 1.4 1
2-Nitroaniline ND ug/L 09/24/19 19:22 88-74-409/24/19 12:0120.0 4.2 1
3-Nitroaniline ND ug/L 09/24/19 19:22 99-09-209/24/19 12:0120.0 2.3 1
4-Nitroaniline ND ug/L 09/24/19 19:22 100-01-609/24/19 12:0120.0 2.2 1
Nitrobenzene ND ug/L 09/24/19 19:22 98-95-309/24/19 12:0110.0 2.1 1
2-Nitrophenol ND ug/L 09/24/19 19:22 88-75-509/24/19 12:0110.0 1.4 1
4-Nitrophenol ND ug/L 09/24/19 19:22 100-02-709/24/19 12:0150.0 3.5 1
N-Nitrosodimethylamine ND ug/L 09/24/19 19:22 62-75-909/24/19 12:0110.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/24/19 19:22 621-64-709/24/19 12:0110.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 09/24/19 19:22 86-30-609/24/19 12:0110.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/24/19 19:22 108-60-109/24/19 12:0110.0 2.8 1
Pentachlorophenol ND ug/L 09/24/19 19:22 87-86-509/24/19 12:0125.0 2.2 1
Phenanthrene ND ug/L 09/24/19 19:22 85-01-809/24/19 12:0110.0 1.7 1
Phenol ND ug/L 09/24/19 19:22 108-95-209/24/19 12:0110.0 0.92 1
Pyrene ND ug/L 09/24/19 19:22 129-00-009/24/19 12:0110.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 09/24/19 19:22 120-82-109/24/19 12:0110.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 09/24/19 19:22 95-95-409/24/19 12:0110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/24/19 19:22 88-06-209/24/19 12:0110.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)86 %09/24/19 19:22 4165-60-009/24/19 12:0113-130 1
2-Fluorobiphenyl (S)73 %09/24/19 19:22 321-60-809/24/19 12:0113-130 1
Terphenyl-d14 (S)92 %09/24/19 19:22 1718-51-009/24/19 12:0125-130 1
Phenol-d6 (S)48 %09/24/19 19:22 13127-88-309/24/19 12:0110-130 1
2-Fluorophenol (S)61 %09/24/19 19:22 367-12-409/24/19 12:0110-130 1
2,4,6-Tribromophenol (S)84 %09/24/19 19:22 118-79-609/24/19 12:0110-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 09/27/19 06:08 67-64-125.0 6.2 1
Benzene ND ug/L 09/27/19 06:08 71-43-21.0 0.15 1
Bromobenzene ND ug/L 09/27/19 06:08 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TMW-4 Lab ID:92446606005 Collected:09/22/19 10:30 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 09/27/19 06:08 74-97-5 IK1.0 0.34 1
Bromodichloromethane ND ug/L 09/27/19 06:08 75-27-41.0 0.26 1
Bromoform ND ug/L 09/27/19 06:08 75-25-21.0 0.62 1
Bromomethane ND ug/L 09/27/19 06:08 74-83-9 IK,v22.0 0.62 1
2-Butanone (MEK)ND ug/L 09/27/19 06:08 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 09/27/19 06:08 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 09/27/19 06:08 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/27/19 06:08 75-00-3 IK1.0 0.49 1
Chloroform ND ug/L 09/27/19 06:08 67-66-35.0 2.3 1
Chloromethane ND ug/L 09/27/19 06:08 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 09/27/19 06:08 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 09/27/19 06:08 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 09/27/19 06:08 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 09/27/19 06:08 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 09/27/19 06:08 106-93-41.0 0.26 1
Dibromomethane ND ug/L 09/27/19 06:08 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 09/27/19 06:08 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 09/27/19 06:08 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 09/27/19 06:08 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 09/27/19 06:08 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 09/27/19 06:08 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 09/27/19 06:08 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 09/27/19 06:08 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 09/27/19 06:08 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 09/27/19 06:08 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 09/27/19 06:08 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 09/27/19 06:08 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 09/27/19 06:08 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 09/27/19 06:08 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 09/27/19 06:08 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 09/27/19 06:08 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 09/27/19 06:08 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 09/27/19 06:08 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 09/27/19 06:08 87-68-31.0 0.44 1
2-Hexanone ND ug/L 09/27/19 06:08 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 09/27/19 06:08 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 09/27/19 06:08 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/27/19 06:08 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 09/27/19 06:08 1634-04-41.0 0.28 1
Naphthalene ND ug/L 09/27/19 06:08 91-20-31.0 0.35 1
Styrene ND ug/L 09/27/19 06:08 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 09/27/19 06:08 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 09/27/19 06:08 79-34-51.0 0.22 1
Tetrachloroethene 1.4 ug/L 09/27/19 06:08 127-18-41.0 0.16 1
Toluene ND ug/L 09/27/19 06:08 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 09/27/19 06:08 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TMW-4 Lab ID:92446606005 Collected:09/22/19 10:30 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 09/27/19 06:08 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 09/27/19 06:08 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 09/27/19 06:08 79-00-51.0 0.24 1
Trichloroethene ND ug/L 09/27/19 06:08 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 09/27/19 06:08 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 09/27/19 06:08 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 09/27/19 06:08 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 09/27/19 06:08 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 09/27/19 06:08 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 09/27/19 06:08 179601-23-12.0 0.41 1
o-Xylene ND ug/L 09/27/19 06:08 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)107 %09/27/19 06:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)84 %09/27/19 06:08 17060-07-070-130 1
Toluene-d8 (S)111 %09/27/19 06:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TMW-DUP Lab ID:92446606006 Collected:09/22/19 00:00 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Arsenic ND ug/L 09/26/19 16:01 7440-38-209/26/19 09:482.00 0.250 1
Barium 21.3 ug/L 09/26/19 16:01 7440-39-309/26/19 09:485.00 0.360 1
Cadmium ND ug/L 09/26/19 16:01 7440-43-909/26/19 09:481.00 0.160 1
Chromium 2.85 ug/L 09/26/19 16:01 7440-47-3 B09/26/19 09:482.00 0.540 1
Lead 0.322J ug/L 09/26/19 16:01 7439-92-1 B,J09/26/19 09:482.00 0.240 1
Selenium ND ug/L 09/26/19 16:01 7782-49-209/26/19 09:482.00 0.380 1
Silver ND ug/L 09/26/19 16:01 7440-22-409/26/19 09:482.00 0.310 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 09/25/19 09:57 7439-97-609/24/19 20:400.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 09/24/19 19:52 83-32-909/24/19 12:0110.0 1.6 1
Acenaphthylene ND ug/L 09/24/19 19:52 208-96-809/24/19 12:0110.0 1.6 1
Aniline ND ug/L 09/24/19 19:52 62-53-309/24/19 12:0110.0 1.9 1
Anthracene ND ug/L 09/24/19 19:52 120-12-709/24/19 12:0110.0 1.7 1
Benzo(a)anthracene ND ug/L 09/24/19 19:52 56-55-309/24/19 12:0110.0 1.8 1
Benzo(a)pyrene ND ug/L 09/24/19 19:52 50-32-809/24/19 12:0110.0 2.1 1
Benzo(b)fluoranthene ND ug/L 09/24/19 19:52 205-99-209/24/19 12:0110.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 09/24/19 19:52 191-24-209/24/19 12:0110.0 1.4 1
Benzo(k)fluoranthene ND ug/L 09/24/19 19:52 207-08-909/24/19 12:0110.0 1.9 1
Benzoic Acid ND ug/L 09/24/19 19:52 65-85-009/24/19 12:0150.0 43.0 1
Benzyl alcohol ND ug/L 09/24/19 19:52 100-51-609/24/19 12:0120.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 09/24/19 19:52 101-55-309/24/19 12:0110.0 1.6 1
Butylbenzylphthalate ND ug/L 09/24/19 19:52 85-68-709/24/19 12:0110.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 09/24/19 19:52 59-50-709/24/19 12:0120.0 2.8 1
4-Chloroaniline ND ug/L 09/24/19 19:52 106-47-809/24/19 12:0120.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 09/24/19 19:52 111-91-109/24/19 12:0110.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/24/19 19:52 111-44-409/24/19 12:0110.0 1.8 1
2-Chloronaphthalene ND ug/L 09/24/19 19:52 91-58-709/24/19 12:0110.0 1.5 1
2-Chlorophenol ND ug/L 09/24/19 19:52 95-57-809/24/19 12:0110.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/24/19 19:52 7005-72-309/24/19 12:0110.0 1.6 1
Chrysene ND ug/L 09/24/19 19:52 218-01-909/24/19 12:0110.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 09/24/19 19:52 53-70-309/24/19 12:0110.0 1.6 1
Dibenzofuran ND ug/L 09/24/19 19:52 132-64-909/24/19 12:0110.0 1.5 1
1,2-Dichlorobenzene ND ug/L 09/24/19 19:52 95-50-109/24/19 12:0110.0 1.3 1
1,3-Dichlorobenzene ND ug/L 09/24/19 19:52 541-73-109/24/19 12:0110.0 1.5 1
1,4-Dichlorobenzene ND ug/L 09/24/19 19:52 106-46-709/24/19 12:0110.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/24/19 19:52 91-94-109/24/19 12:0120.0 3.0 1
2,4-Dichlorophenol ND ug/L 09/24/19 19:52 120-83-209/24/19 12:0110.0 1.4 1
Diethylphthalate ND ug/L 09/24/19 19:52 84-66-209/24/19 12:0110.0 2.4 1
2,4-Dimethylphenol ND ug/L 09/24/19 19:52 105-67-909/24/19 12:0110.0 1.4 1
Dimethylphthalate ND ug/L 09/24/19 19:52 131-11-309/24/19 12:0110.0 1.6 1
Di-n-butylphthalate ND ug/L 09/24/19 19:52 84-74-209/24/19 12:0110.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/24/19 19:52 534-52-109/24/19 12:0120.0 15.2 1
2,4-Dinitrophenol ND ug/L 09/24/19 19:52 51-28-509/24/19 12:0150.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TMW-DUP Lab ID:92446606006 Collected:09/22/19 00:00 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 09/24/19 19:52 121-14-209/24/19 12:0110.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/24/19 19:52 606-20-209/24/19 12:0110.0 1.4 1
Di-n-octylphthalate ND ug/L 09/24/19 19:52 117-84-009/24/19 12:0110.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/24/19 19:52 117-81-709/24/19 12:016.0 2.1 1
Fluoranthene ND ug/L 09/24/19 19:52 206-44-009/24/19 12:0110.0 1.7 1
Fluorene ND ug/L 09/24/19 19:52 86-73-709/24/19 12:0110.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 09/24/19 19:52 87-68-3 v109/24/19 12:0110.0 2.0 1
Hexachlorobenzene ND ug/L 09/24/19 19:52 118-74-109/24/19 12:0110.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 09/24/19 19:52 77-47-409/24/19 12:0110.0 1.7 1
Hexachloroethane ND ug/L 09/24/19 19:52 67-72-109/24/19 12:0110.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/24/19 19:52 193-39-509/24/19 12:0110.0 1.6 1
Isophorone ND ug/L 09/24/19 19:52 78-59-109/24/19 12:0110.0 1.6 1
1-Methylnaphthalene ND ug/L 09/24/19 19:52 90-12-009/24/19 12:0110.0 1.4 1
2-Methylnaphthalene ND ug/L 09/24/19 19:52 91-57-609/24/19 12:0110.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/24/19 19:52 95-48-709/24/19 12:0110.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/24/19 19:52 15831-10-409/24/19 12:0110.0 1.2 1
Naphthalene ND ug/L 09/24/19 19:52 91-20-309/24/19 12:0110.0 1.4 1
2-Nitroaniline ND ug/L 09/24/19 19:52 88-74-409/24/19 12:0120.0 4.2 1
3-Nitroaniline ND ug/L 09/24/19 19:52 99-09-209/24/19 12:0120.0 2.3 1
4-Nitroaniline ND ug/L 09/24/19 19:52 100-01-609/24/19 12:0120.0 2.2 1
Nitrobenzene ND ug/L 09/24/19 19:52 98-95-309/24/19 12:0110.0 2.1 1
2-Nitrophenol ND ug/L 09/24/19 19:52 88-75-509/24/19 12:0110.0 1.4 1
4-Nitrophenol ND ug/L 09/24/19 19:52 100-02-709/24/19 12:0150.0 3.5 1
N-Nitrosodimethylamine ND ug/L 09/24/19 19:52 62-75-909/24/19 12:0110.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/24/19 19:52 621-64-709/24/19 12:0110.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 09/24/19 19:52 86-30-609/24/19 12:0110.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/24/19 19:52 108-60-109/24/19 12:0110.0 2.8 1
Pentachlorophenol ND ug/L 09/24/19 19:52 87-86-509/24/19 12:0125.0 2.2 1
Phenanthrene ND ug/L 09/24/19 19:52 85-01-809/24/19 12:0110.0 1.7 1
Phenol ND ug/L 09/24/19 19:52 108-95-209/24/19 12:0110.0 0.92 1
Pyrene ND ug/L 09/24/19 19:52 129-00-009/24/19 12:0110.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 09/24/19 19:52 120-82-109/24/19 12:0110.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 09/24/19 19:52 95-95-409/24/19 12:0110.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/24/19 19:52 88-06-209/24/19 12:0110.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)78 %09/24/19 19:52 4165-60-009/24/19 12:0113-130 1
2-Fluorobiphenyl (S)68 %09/24/19 19:52 321-60-809/24/19 12:0113-130 1
Terphenyl-d14 (S)91 %09/24/19 19:52 1718-51-009/24/19 12:0125-130 1
Phenol-d6 (S)43 %09/24/19 19:52 13127-88-309/24/19 12:0110-130 1
2-Fluorophenol (S)56 %09/24/19 19:52 367-12-409/24/19 12:0110-130 1
2,4,6-Tribromophenol (S)78 %09/24/19 19:52 118-79-609/24/19 12:0110-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 09/27/19 06:27 67-64-125.0 6.2 1
Benzene ND ug/L 09/27/19 06:27 71-43-21.0 0.15 1
Bromobenzene ND ug/L 09/27/19 06:27 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TMW-DUP Lab ID:92446606006 Collected:09/22/19 00:00 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 09/27/19 06:27 74-97-5 IK1.0 0.34 1
Bromodichloromethane ND ug/L 09/27/19 06:27 75-27-41.0 0.26 1
Bromoform ND ug/L 09/27/19 06:27 75-25-21.0 0.62 1
Bromomethane ND ug/L 09/27/19 06:27 74-83-9 IK,v22.0 0.62 1
2-Butanone (MEK)ND ug/L 09/27/19 06:27 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 09/27/19 06:27 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 09/27/19 06:27 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/27/19 06:27 75-00-3 IK1.0 0.49 1
Chloroform ND ug/L 09/27/19 06:27 67-66-35.0 2.3 1
Chloromethane ND ug/L 09/27/19 06:27 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 09/27/19 06:27 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 09/27/19 06:27 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 09/27/19 06:27 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 09/27/19 06:27 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 09/27/19 06:27 106-93-41.0 0.26 1
Dibromomethane ND ug/L 09/27/19 06:27 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 09/27/19 06:27 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 09/27/19 06:27 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 09/27/19 06:27 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 09/27/19 06:27 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 09/27/19 06:27 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 09/27/19 06:27 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 09/27/19 06:27 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 09/27/19 06:27 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 09/27/19 06:27 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 09/27/19 06:27 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 09/27/19 06:27 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 09/27/19 06:27 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 09/27/19 06:27 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 09/27/19 06:27 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 09/27/19 06:27 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 09/27/19 06:27 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 09/27/19 06:27 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 09/27/19 06:27 87-68-31.0 0.44 1
2-Hexanone ND ug/L 09/27/19 06:27 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 09/27/19 06:27 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 09/27/19 06:27 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/27/19 06:27 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 09/27/19 06:27 1634-04-41.0 0.28 1
Naphthalene ND ug/L 09/27/19 06:27 91-20-31.0 0.35 1
Styrene ND ug/L 09/27/19 06:27 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 09/27/19 06:27 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 09/27/19 06:27 79-34-51.0 0.22 1
Tetrachloroethene 1.4 ug/L 09/27/19 06:27 127-18-41.0 0.16 1
Toluene ND ug/L 09/27/19 06:27 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 09/27/19 06:27 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:TMW-DUP Lab ID:92446606006 Collected:09/22/19 00:00 Received:09/23/19 11:52 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 09/27/19 06:27 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 09/27/19 06:27 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 09/27/19 06:27 79-00-51.0 0.24 1
Trichloroethene ND ug/L 09/27/19 06:27 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 09/27/19 06:27 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 09/27/19 06:27 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 09/27/19 06:27 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 09/27/19 06:27 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 09/27/19 06:27 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 09/27/19 06:27 179601-23-12.0 0.41 1
o-Xylene ND ug/L 09/27/19 06:27 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)107 %09/27/19 06:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)82 %09/27/19 06:27 17060-07-070-130 1
Toluene-d8 (S)112 %09/27/19 06:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92446606
DRY-003
Sample:SB-DUP Lab ID:92446606007 Collected:09/20/19 00:00 Received:09/23/19 11:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 0.724 mg/kg 09/27/19 13:52 7440-38-209/27/19 11:150.545 0.136 5
Barium 21.6 mg/kg 09/27/19 13:52 7440-39-309/27/19 11:151.09 0.174 5
Cadmium ND mg/kg 09/27/19 13:52 7440-43-909/27/19 11:150.545 0.0872 5
Chromium 35.4 mg/kg 09/27/19 13:52 7440-47-309/27/19 11:151.09 0.294 5
Lead 0.647 mg/kg 09/27/19 13:52 7439-92-109/27/19 11:150.545 0.131 5
Selenium ND mg/kg 09/27/19 13:52 7782-49-209/27/19 11:150.545 0.207 5
Silver ND mg/kg 09/27/19 13:52 7440-22-409/27/19 11:150.545 0.169 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.00444J mg/kg 09/29/19 22:01 7439-97-6 J09/27/19 12:580.0327 0.00305 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 91.7 %09/30/19 15:1609/30/19 15:081
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1351948
3015
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples:92446606005, 92446606006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3454978-1
Associated Lab Samples:92446606005, 92446606006
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 2.00 09/26/19 14:540.250
Barium ug/L ND 5.00 09/26/19 14:540.360
Cadmium ug/L ND 1.00 09/26/19 14:540.160
Chromium ug/L 0.612J 2.00 J09/26/19 14:540.540
Lead ug/L 0.260J 2.00 J09/26/19 14:540.240
Selenium ug/L ND 2.00 09/26/19 14:540.380
Silver ug/L ND 2.00 09/26/19 14:540.310
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3454978-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3454978-3
Arsenic ug/L 48.050.0 96.0 80.0-12096.348.2 0.273 20
Barium ug/L 48.450.0 96.8 80.0-12097.848.9 1.01 20
Cadmium ug/L 49.150.0 98.3 80.0-12099.849.9 1.51 20
Chromium ug/L 48.850.0 97.7 80.0-12098.749.4 1.03 20
Lead ug/L 49.250.0 98.4 80.0-12097.949.0 0.526 20
Selenium ug/L 47.250.0 94.4 80.0-12097.048.5 2.62 20
Silver ug/L 52.450.0 105 80.0-12010552.6 0.412 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3454978-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1142677-01
R3454978-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 50.0 94.0 75.0-12594.0 0.041 2050.0ND 47.0 47.0
Barium ug/L 50.0 98.2 75.0-12595.4 1.87 2050.026.5 75.6 74.2
Cadmium ug/L 50.0 101 75.0-125102 1.08 2050.0ND 50.6 51.2
Chromium ug/L 50.0 94.7 75.0-12594.1 0.646 2050.00.648 48.0 47.7
Lead ug/L 50.0 97.7 75.0-12596.4 1.26 2050.00.644 49.5 48.9
Selenium ug/L 50.0 102 75.0-125105 2.62 2050.0ND 50.9 52.3
Silver ug/L 50.0 106 75.0-125106 0.135 2050.0ND 53.0 53.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1353186
3051
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples:92446606001, 92446606002, 92446606003, 92446606007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3455321-1
Associated Lab Samples:92446606001, 92446606002, 92446606003, 92446606007
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 0.500 09/27/19 13:080.125
Barium mg/kg ND 1.00 09/27/19 13:080.160
Cadmium mg/kg ND 0.500 09/27/19 13:080.0800
Chromium mg/kg ND 1.00 09/27/19 13:080.270
Lead mg/kg ND 0.500 09/27/19 13:080.120
Selenium mg/kg ND 0.500 09/27/19 13:080.190
Silver mg/kg ND 0.500 09/27/19 13:080.155
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3455321-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3455321-3
Arsenic mg/kg 91.9100 91.9 80.0-12095.095.0 3.29 20
Barium mg/kg 94.2100 94.2 80.0-12093.793.7 0.500 20
Cadmium mg/kg 98.0100 98.0 80.0-120101101 2.85 20
Chromium mg/kg 97.0100 97.0 80.0-120100100 3.49 20
Lead mg/kg 96.6100 96.6 80.0-12098.498.4 1.85 20
Selenium mg/kg 96.4100 96.4 80.0-12098.498.4 2.01 20
Silver mg/kg 19.220.0 95.9 80.0-12098.519.7 2.71 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3455321-6MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92446606001
R3455321-7
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 21.6 90.6 75.0-12580.7 11.5 2021.60.494 98.2 87.5
Barium mg/kg 21.6 97.7 75.0-12587.1 9.55 2021.620.0 125 114
Cadmium mg/kg 21.6 101 75.0-12590.3 10.9 2021.6ND 109 97.4
Chromium mg/kg 21.6 99.2 75.0-12582.2 13.9 2021.633.7 141 122
Lead mg/kg 21.6 96.4 75.0-12583.4 14.3 2021.60.612 105 90.6
Selenium mg/kg 21.6 98.1 75.0-12587.6 11.3 2021.6ND 106 94.5
Silver mg/kg 4.31 97.2 75.0-12588.5 9.42 204.31ND 21.0 19.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1351504
7470A
EPA 7470A
Mercury 7470A
Associated Lab Samples:92446606005, 92446606006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3454332-1
Associated Lab Samples:92446606005, 92446606006
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.200 09/25/19 09:020.0490
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3454332-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3454332-3
Mercury ug/L 2.943.00 98.2 80.0-12096.22.89 1.97 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3454332-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1142598-01
R3454332-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 3.00 91.5 75.0-12584.5 7.98 203.00ND 2.75 2.54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1353452
7471A
EPA 7471B
Mercury 7471B
Associated Lab Samples:92446606001, 92446606002, 92446606003, 92446606007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3455753-5
Associated Lab Samples:92446606001, 92446606002, 92446606003, 92446606007
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0300 09/29/19 23:360.00280
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3455753-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3455753-2
Mercury mg/kg 0.4370.500 87.5 80.0-12086.60.433 0.976 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3455753-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1142466-01
R3455753-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.628 81.0 75.0-12579.5 1.71 200.6280.0495 0.558 0.549
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
500111
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples:92446606004, 92446606005, 92446606006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2690862
Associated Lab Samples:92446606004, 92446606005, 92446606006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/27/19 01:350.34
1,1,1-Trichloroethane ug/L ND 1.0 09/27/19 01:350.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/27/19 01:350.22
1,1,2-Trichloroethane ug/L ND 1.0 09/27/19 01:350.24
1,1-Dichloroethane ug/L ND 1.0 09/27/19 01:350.27
1,1-Dichloroethene ug/L ND 1.0 09/27/19 01:350.24
1,1-Dichloropropene ug/L ND 1.0 09/27/19 01:350.21
1,2,3-Trichlorobenzene ug/L ND 1.0 09/27/19 01:350.34
1,2,3-Trichloropropane ug/L ND 1.0 09/27/19 01:350.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/27/19 01:350.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/27/19 01:350.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/27/19 01:350.26
1,2-Dichlorobenzene ug/L ND 1.0 09/27/19 01:350.29
1,2-Dichloroethane ug/L ND 1.0 09/27/19 01:350.34
1,2-Dichloropropane ug/L ND 1.0 09/27/19 01:350.19
1,3-Dichlorobenzene ug/L ND 1.0 09/27/19 01:350.22
1,3-Dichloropropane ug/L ND 1.0 09/27/19 01:350.16
1,4-Dichlorobenzene ug/L ND 1.0 09/27/19 01:350.26
2,2-Dichloropropane ug/L ND 1.0 09/27/19 01:350.27
2-Butanone (MEK)ug/L ND 5.0 09/27/19 01:353.3
2-Chlorotoluene ug/L ND 1.0 09/27/19 01:350.20
2-Hexanone ug/L ND 5.0 09/27/19 01:350.57
4-Chlorotoluene ug/L ND 1.0 09/27/19 01:350.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/27/19 01:354.5
Acetone ug/L ND 25.0 09/27/19 01:356.2
Benzene ug/L ND 1.0 09/27/19 01:350.15
Bromobenzene ug/L ND 1.0 09/27/19 01:350.22
Bromochloromethane ug/L ND 1.0 IK09/27/19 01:350.34
Bromodichloromethane ug/L ND 1.0 09/27/19 01:350.26
Bromoform ug/L ND 1.0 09/27/19 01:350.62
Bromomethane ug/L ND 2.0 IK,v209/27/19 01:350.62
Carbon tetrachloride ug/L ND 1.0 09/27/19 01:350.22
Chlorobenzene ug/L ND 1.0 09/27/19 01:350.23
Chloroethane ug/L ND 1.0 IK09/27/19 01:350.49
Chloroform ug/L ND 5.0 09/27/19 01:352.3
Chloromethane ug/L ND 1.0 09/27/19 01:350.39
cis-1,2-Dichloroethene ug/L ND 1.0 09/27/19 01:350.29
cis-1,3-Dichloropropene ug/L ND 1.0 09/27/19 01:350.30
Dibromochloromethane ug/L ND 1.0 09/27/19 01:350.41
Dibromomethane ug/L ND 1.0 09/27/19 01:350.46
Dichlorodifluoromethane ug/L ND 1.0 09/27/19 01:350.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2690862
Associated Lab Samples:92446606004, 92446606005, 92446606006
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 09/27/19 01:350.22
Ethylbenzene ug/L ND 1.0 09/27/19 01:350.26
Hexachloro-1,3-butadiene ug/L ND 1.0 09/27/19 01:350.44
m&p-Xylene ug/L ND 2.0 09/27/19 01:350.41
Methyl-tert-butyl ether ug/L ND 1.0 09/27/19 01:350.28
Methylene Chloride ug/L ND 5.0 09/27/19 01:353.7
Naphthalene ug/L ND 1.0 09/27/19 01:350.35
o-Xylene ug/L ND 1.0 09/27/19 01:350.22
p-Isopropyltoluene ug/L ND 1.0 09/27/19 01:350.21
Styrene ug/L ND 1.0 09/27/19 01:350.27
Tetrachloroethene ug/L ND 1.0 09/27/19 01:350.16
Toluene ug/L ND 1.0 09/27/19 01:350.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/27/19 01:350.25
trans-1,3-Dichloropropene ug/L ND 1.0 09/27/19 01:350.31
Trichloroethene ug/L ND 1.0 09/27/19 01:350.22
Trichlorofluoromethane ug/L ND 1.0 09/27/19 01:350.31
Vinyl acetate ug/L ND 2.0 09/27/19 01:351.4
Vinyl chloride ug/L ND 1.0 09/27/19 01:350.24
Xylene (Total)ug/L ND 1.0 09/27/19 01:350.63
1,2-Dichloroethane-d4 (S)%83 70-130 09/27/19 01:35
4-Bromofluorobenzene (S)%109 70-130 09/27/19 01:35
Toluene-d8 (S)%110 70-130 09/27/19 01:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2690863LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.850 94 70-130
1,1,1-Trichloroethane ug/L 49.850 100 70-130
1,1,2,2-Tetrachloroethane ug/L 48.250 96 70-130
1,1,2-Trichloroethane ug/L 49.550 99 70-130
1,1-Dichloroethane ug/L 52.550 105 70-130
1,1-Dichloroethene ug/L 52.750 105 70-130
1,1-Dichloropropene ug/L 52.450 105 70-130
1,2,3-Trichlorobenzene ug/L 47.850 96 70-130
1,2,3-Trichloropropane ug/L 49.250 98 70-130
1,2,4-Trichlorobenzene ug/L 46.650 93 70-130
1,2-Dibromo-3-chloropropane ug/L 47.150 94 70-130
1,2-Dibromoethane (EDB)ug/L 48.950 98 70-130
1,2-Dichlorobenzene ug/L 46.450 93 70-130
1,2-Dichloroethane ug/L 50.150 100 70-130
1,2-Dichloropropane ug/L 53.250 106 70-130
1,3-Dichlorobenzene ug/L 45.250 90 70-130
1,3-Dichloropropane ug/L 51.050 102 70-131
1,4-Dichlorobenzene ug/L 46.150 92 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2690863LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 51.750 103 69-130
2-Butanone (MEK)ug/L 107100 107 64-135
2-Chlorotoluene ug/L 46.250 92 70-130
2-Hexanone ug/L 89.8100 90 66-135
4-Chlorotoluene ug/L 46.050 92 70-130
4-Methyl-2-pentanone (MIBK)ug/L 92.6100 93 70-130
Acetone ug/L 113100 113 61-157
Benzene ug/L 50.250 100 70-130
Bromobenzene ug/L 47.050 94 70-130
Bromochloromethane ug/L 51.2 IK5010270-130
Bromodichloromethane ug/L 50.750 101 70-130
Bromoform ug/L 46.950 94 70-130
Bromomethane ug/L 37.2 IK,v3507438-130
Carbon tetrachloride ug/L 48.250 96 70-130
Chlorobenzene ug/L 46.050 92 70-130
Chloroethane ug/L 42.6 IK508537-142
Chloroform ug/L 49.550 99 70-130
Chloromethane ug/L 52.550 105 48-130
cis-1,2-Dichloroethene ug/L 51.950 104 70-130
cis-1,3-Dichloropropene ug/L 54.150 108 70-130
Dibromochloromethane ug/L 47.750 95 70-130
Dibromomethane ug/L 48.950 98 70-130
Dichlorodifluoromethane ug/L 50.550 101 53-134
Diisopropyl ether ug/L 53.050 106 70-135
Ethylbenzene ug/L 46.450 93 70-130
Hexachloro-1,3-butadiene ug/L 44.650 89 68-132
m&p-Xylene ug/L 112100 112 70-130
Methyl-tert-butyl ether ug/L 53.450 107 70-130
Methylene Chloride ug/L 54.350 109 67-132
Naphthalene ug/L 48.350 97 70-130
o-Xylene ug/L 46.650 93 70-131
p-Isopropyltoluene ug/L 47.750 95 70-130
Styrene ug/L 46.950 94 70-130
Tetrachloroethene ug/L 43.950 88 69-130
Toluene ug/L 46.050 92 70-130
trans-1,2-Dichloroethene ug/L 52.250 104 70-130
trans-1,3-Dichloropropene ug/L 51.950 104 70-130
Trichloroethene ug/L 50.650 101 70-130
Trichlorofluoromethane ug/L 50.250 100 63-130
Vinyl acetate ug/L 108100 108 55-143
Vinyl chloride ug/L 52.650 105 70-131
Xylene (Total)ug/L 159150 106 70-130
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2692164MATRIX SPIKE SAMPLE:
MSSpike
Result
2623444002
1,1,1,2-Tetrachloroethane ug/L 18.620 93 73-134ND
1,1,1-Trichloroethane ug/L 20.120 101 82-143ND
1,1,2,2-Tetrachloroethane ug/L 20.120 101 70-136ND
1,1,2-Trichloroethane ug/L 19.620 98 70-135ND
1,1-Dichloroethane ug/L 23.520 113 70-1390.91J
1,1-Dichloroethene ug/L 23.520 117 70-154ND
1,1-Dichloropropene ug/L 20.120 101 70-149ND
1,2,3-Trichlorobenzene ug/L 19.220 96 70-135ND
1,2,3-Trichloropropane ug/L 18.720 93 71-137ND
1,2,4-Trichlorobenzene ug/L 18.820 94 73-140ND
1,2-Dibromo-3-chloropropane ug/L 17.620 88 65-134ND
1,2-Dibromoethane (EDB)ug/L 19.320 96 70-137ND
1,2-Dichlorobenzene ug/L 25.420 93 70-1336.8
1,2-Dichloroethane ug/L 19.720 99 70-137ND
1,2-Dichloropropane ug/L 21.220 106 70-140ND
1,3-Dichlorobenzene ug/L 21.020 100 70-1350.94J
1,3-Dichloropropane ug/L 19.320 97 70-143ND
1,4-Dichlorobenzene ug/L 24.820 91 70-1336.6
2,2-Dichloropropane ug/L 21.220 106 61-148ND
2-Butanone (MEK)ug/L 36.540 91 60-139ND
2-Chlorotoluene ug/L 20.120 101 70-144ND
2-Hexanone ug/L 37.640 94 65-138ND
4-Chlorotoluene ug/L 20.020 100 70-137ND
4-Methyl-2-pentanone (MIBK)ug/L 38.940 97 65-135ND
Acetone ug/L 42.840 107 60-148ND
Benzene ug/L 21.620 108 70-151ND
Bromobenzene ug/L 20.020 100 70-136ND
Bromochloromethane ug/L 22.3 IK2011170-141ND
Bromodichloromethane ug/L 20.620 103 70-138ND
Bromoform ug/L 18.220 91 63-130ND
Bromomethane ug/L 17.2 IK,v3208615-152ND
Carbon tetrachloride ug/L 20.420 102 70-143ND
Chlorobenzene ug/L 21.020 100 70-1381.0J
Chloroethane ug/L 22.5 IK2011252-163ND
Chloroform ug/L 20.820 104 70-139ND
Chloromethane ug/L 21.220 106 41-139ND
cis-1,2-Dichloroethene ug/L 21.620 108 70-141ND
cis-1,3-Dichloropropene ug/L 20.820 104 70-137ND
Dibromochloromethane ug/L 17.920 90 70-134ND
Dibromomethane ug/L 20.920 104 70-138ND
Dichlorodifluoromethane ug/L 21.520 108 47-155ND
Diisopropyl ether ug/L 19.920 100 63-144ND
Ethylbenzene ug/L 20.920 105 66-153ND
Hexachloro-1,3-butadiene ug/L 19.120 95 65-149ND
m&p-Xylene ug/L 43.340 108 69-152ND
Methyl-tert-butyl ether ug/L 18.620 93 54-156ND
Methylene Chloride ug/L 21.220 106 42-159ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2692164MATRIX SPIKE SAMPLE:
MSSpike
Result
2623444002
Naphthalene ug/L 19.320 92 61-1480.98J
o-Xylene ug/L 21.520 108 70-148ND
p-Isopropyltoluene ug/L 20.920 104 70-146ND
Styrene ug/L 20.820 104 70-135ND
Tetrachloroethene ug/L 20.520 98 59-1430.87J
Toluene ug/L 21.120 106 59-148ND
trans-1,2-Dichloroethene ug/L 21.820 109 70-146ND
trans-1,3-Dichloropropene ug/L 20.520 103 70-135ND
Trichloroethene ug/L 20.520 103 70-147ND
Trichlorofluoromethane ug/L 22.820 114 70-148ND
Vinyl acetate ug/L 34.740 87 49-151ND
Vinyl chloride ug/L 22.720 114 70-156ND
Xylene (Total)ug/L 64.860 108 63-158ND
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%105 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
2623444001
2692163SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L 8.3 22 306.7
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L 1.4 1 301.4
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L 16.7 27 3012.7
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L 2.0 28 301.5
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 8.2 D638305.5
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
2623444001
2692163SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND IK30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND IK,v230ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 0.77J 300.56J
Chloroethane ug/L ND IK30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L 5.5 27 304.2
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L 44.0 25 3034.1
o-Xylene ug/L 59.9 25 3046.4
p-Isopropyltoluene ug/L 7.8 D667303.9
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 4.1 D642302.7
Toluene ug/L 0.56J 300.51J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L 0.60J 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L 59.9 25 3046.4
1,2-Dichloroethane-d4 (S)%9289
4-Bromofluorobenzene (S)%107106
Toluene-d8 (S)%107112
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
499474
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Associated Lab Samples:92446606005, 92446606006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2687788
Associated Lab Samples:92446606005, 92446606006
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 09/24/19 16:511.5
1,2-Dichlorobenzene ug/L ND 10.0 09/24/19 16:511.3
1,3-Dichlorobenzene ug/L ND 10.0 09/24/19 16:511.5
1,4-Dichlorobenzene ug/L ND 10.0 09/24/19 16:512.1
1-Methylnaphthalene ug/L ND 10.0 09/24/19 16:511.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/24/19 16:512.8
2,4,5-Trichlorophenol ug/L ND 10.0 09/24/19 16:511.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/24/19 16:511.5
2,4-Dichlorophenol ug/L ND 10.0 09/24/19 16:511.4
2,4-Dimethylphenol ug/L ND 10.0 09/24/19 16:511.4
2,4-Dinitrophenol ug/L ND 50.0 09/24/19 16:5140.5
2,4-Dinitrotoluene ug/L ND 10.0 09/24/19 16:511.2
2,6-Dinitrotoluene ug/L ND 10.0 09/24/19 16:511.4
2-Chloronaphthalene ug/L ND 10.0 09/24/19 16:511.5
2-Chlorophenol ug/L ND 10.0 09/24/19 16:511.2
2-Methylnaphthalene ug/L ND 10.0 09/24/19 16:511.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/24/19 16:511.2
2-Nitroaniline ug/L ND 20.0 09/24/19 16:514.2
2-Nitrophenol ug/L ND 10.0 09/24/19 16:511.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/24/19 16:511.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/24/19 16:513.0
3-Nitroaniline ug/L ND 20.0 09/24/19 16:512.3
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/24/19 16:5115.2
4-Bromophenylphenyl ether ug/L ND 10.0 09/24/19 16:511.6
4-Chloro-3-methylphenol ug/L ND 20.0 09/24/19 16:512.8
4-Chloroaniline ug/L ND 20.0 09/24/19 16:512.8
4-Chlorophenylphenyl ether ug/L ND 10.0 09/24/19 16:511.6
4-Nitroaniline ug/L ND 20.0 09/24/19 16:512.2
4-Nitrophenol ug/L ND 50.0 09/24/19 16:513.5
Acenaphthene ug/L ND 10.0 09/24/19 16:511.6
Acenaphthylene ug/L ND 10.0 09/24/19 16:511.6
Aniline ug/L ND 10.0 09/24/19 16:511.9
Anthracene ug/L ND 10.0 09/24/19 16:511.7
Benzo(a)anthracene ug/L ND 10.0 09/24/19 16:511.8
Benzo(a)pyrene ug/L ND 10.0 09/24/19 16:512.1
Benzo(b)fluoranthene ug/L ND 10.0 09/24/19 16:511.9
Benzo(g,h,i)perylene ug/L ND 10.0 09/24/19 16:511.4
Benzo(k)fluoranthene ug/L ND 10.0 09/24/19 16:511.9
Benzoic Acid ug/L ND 50.0 09/24/19 16:5143.0
Benzyl alcohol ug/L ND 20.0 09/24/19 16:512.6
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/24/19 16:511.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2687788
Associated Lab Samples:92446606005, 92446606006
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 09/24/19 16:511.8
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/24/19 16:512.1
Butylbenzylphthalate ug/L ND 10.0 09/24/19 16:511.6
Chrysene ug/L ND 10.0 09/24/19 16:511.7
Di-n-butylphthalate ug/L ND 10.0 09/24/19 16:511.8
Di-n-octylphthalate ug/L ND 10.0 09/24/19 16:511.8
Dibenz(a,h)anthracene ug/L ND 10.0 09/24/19 16:511.6
Dibenzofuran ug/L ND 10.0 09/24/19 16:511.5
Diethylphthalate ug/L ND 10.0 09/24/19 16:512.4
Dimethylphthalate ug/L ND 10.0 09/24/19 16:511.6
Fluoranthene ug/L ND 10.0 09/24/19 16:511.7
Fluorene ug/L ND 10.0 09/24/19 16:511.6
Hexachloro-1,3-butadiene ug/L ND 10.0 v109/24/19 16:512.0
Hexachlorobenzene ug/L ND 10.0 09/24/19 16:511.7
Hexachlorocyclopentadiene ug/L ND 10.0 09/24/19 16:511.7
Hexachloroethane ug/L ND 10.0 09/24/19 16:512.0
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/24/19 16:511.6
Isophorone ug/L ND 10.0 09/24/19 16:511.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/24/19 16:512.2
N-Nitrosodimethylamine ug/L ND 10.0 09/24/19 16:511.2
N-Nitrosodiphenylamine ug/L ND 10.0 09/24/19 16:511.7
Naphthalene ug/L ND 10.0 09/24/19 16:511.4
Nitrobenzene ug/L ND 10.0 09/24/19 16:512.1
Pentachlorophenol ug/L ND 25.0 09/24/19 16:512.2
Phenanthrene ug/L ND 10.0 09/24/19 16:511.7
Phenol ug/L ND 10.0 09/24/19 16:510.92
Pyrene ug/L ND 10.0 09/24/19 16:512.1
2,4,6-Tribromophenol (S)%85 10-137 09/24/19 16:51
2-Fluorobiphenyl (S)%78 13-130 09/24/19 16:51
2-Fluorophenol (S)%70 10-130 09/24/19 16:51
Nitrobenzene-d5 (S)%86 13-130 09/24/19 16:51
Phenol-d6 (S)%60 10-130 09/24/19 16:51
Terphenyl-d14 (S)%106 25-130 09/24/19 16:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2687789LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2687790
1,2,4-Trichlorobenzene ug/L 39.150 78 30-1307034.8 12 30
1,2-Dichlorobenzene ug/L 33.150 66 30-1306231.0 6 30
1,3-Dichlorobenzene ug/L 33.550 67 20-1306130.7 9 30
1,4-Dichlorobenzene ug/L 33.150 66 30-1306130.6 8 30
1-Methylnaphthalene ug/L 39.850 80 30-1307035.1 12 30
2,2'-Oxybis(1-chloropropane)ug/L 39.550 79 20-1307336.3 8 30
2,4,5-Trichlorophenol ug/L 42.350 85 40-1307336.4 15 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2687789LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2687790
2,4,6-Trichlorophenol ug/L 43.250 86 40-1307637.8 13 30
2,4-Dichlorophenol ug/L 44.850 90 31-1308040.2 11 30
2,4-Dimethylphenol ug/L 42.950 86 30-1307838.9 10 30
2,4-Dinitrophenol ug/L 250250 100 30-13080200 22 30
2,4-Dinitrotoluene ug/L 43.650 87 49-1307537.4 15 30
2,6-Dinitrotoluene ug/L 41.250 82 50-1307135.5 15 30
2-Chloronaphthalene ug/L 33.750 67 30-1306029.9 12 30
2-Chlorophenol ug/L 36.650 73 30-1306833.9 8 30
2-Methylnaphthalene ug/L 40.850 82 30-1307135.5 14 30
2-Methylphenol(o-Cresol)ug/L 36.550 73 30-1306733.3 9 30
2-Nitroaniline ug/L 70.0100 70 40-1306060.5 15 30
2-Nitrophenol ug/L 39.850 80 20-1307336.4 9 30
3&4-Methylphenol(m&p Cresol)ug/L 34.450 69 20-1306331.7 8 30
3,3'-Dichlorobenzidine ug/L 90.6100 91 10-1508382.8 9 30
3-Nitroaniline ug/L 76.9100 77 40-1306766.7 14 30
4,6-Dinitro-2-methylphenol ug/L 113100 113 40-1309999.4 13 30
4-Bromophenylphenyl ether ug/L 49.750 99 30-1308944.7 11 30
4-Chloro-3-methylphenol ug/L 95.2100 95 30-1308281.7 15 30
4-Chloroaniline ug/L 75.4100 75 20-1307069.5 8 30
4-Chlorophenylphenyl ether ug/L 45.550 91 20-1308040.1 13 30
4-Nitroaniline ug/L 77.5100 77 40-1306564.9 18 30
4-Nitrophenol ug/L 161250 64 10-13056140 14 30
Acenaphthene ug/L 37.350 75 30-1306632.9 13 30
Acenaphthylene ug/L 40.350 81 30-1307135.6 12 30
Aniline ug/L 33.550 67 20-1306431.8 5 30
Anthracene ug/L 45.850 92 50-1308140.3 13 30
Benzo(a)anthracene ug/L 51.350 103 50-1309446.8 9 30
Benzo(a)pyrene ug/L 51.950 104 50-1309447.2 9 30
Benzo(b)fluoranthene ug/L 49.450 99 50-1309145.3 9 30
Benzo(g,h,i)perylene ug/L 49.750 99 50-1309246.1 7 30
Benzo(k)fluoranthene ug/L 51.250 102 50-1309145.4 12 30
Benzoic Acid ug/L 169 R12506810-1303792.1 59 30
Benzyl alcohol ug/L 73.6100 74 20-1306767.4 9 30
bis(2-Chloroethoxy)methane ug/L 39.050 78 30-1307035.0 11 30
bis(2-Chloroethyl) ether ug/L 40.450 81 30-1307638.1 6 30
bis(2-Ethylhexyl)phthalate ug/L 42.350 85 50-1307537.5 12 30
Butylbenzylphthalate ug/L 42.050 84 50-1507437.1 12 30
Chrysene ug/L 48.250 96 50-1308944.3 8 30
Di-n-butylphthalate ug/L 44.250 88 50-1307738.7 13 30
Di-n-octylphthalate ug/L 45.450 91 50-1308240.9 10 30
Dibenz(a,h)anthracene ug/L 51.450 103 40-1309447.1 9 30
Dibenzofuran ug/L 40.050 80 40-1306934.7 14 30
Diethylphthalate ug/L 38.850 78 40-1306632.9 16 30
Dimethylphthalate ug/L 40.450 81 40-1306934.7 15 30
Fluoranthene ug/L 55.550 111 30-1309849.0 12 30
Fluorene ug/L 41.750 83 20-1307236.1 14 30
Hexachloro-1,3-butadiene ug/L 42.9 v1508610-1307939.4 9 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2687789LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2687790
Hexachlorobenzene ug/L 44.550 89 30-1307839.1 13 30
Hexachlorocyclopentadiene ug/L 43.350 87 10-1507838.9 11 30
Hexachloroethane ug/L 31.150 62 10-1305828.8 8 30
Indeno(1,2,3-cd)pyrene ug/L 50.450 101 40-1309346.4 8 30
Isophorone ug/L 42.950 86 30-1307637.8 13 30
N-Nitroso-di-n-propylamine ug/L 38.350 77 30-1306934.6 10 30
N-Nitrosodimethylamine ug/L 32.650 65 10-1306231.0 5 30
N-Nitrosodiphenylamine ug/L 41.550 83 30-1307437.1 11 30
Naphthalene ug/L 39.350 79 20-1307035.0 12 30
Nitrobenzene ug/L 38.650 77 20-1306934.7 10 30
Pentachlorophenol ug/L 111100 111 10-1409897.5 13 30
Phenanthrene ug/L 46.950 94 50-1308441.9 11 30
Phenol ug/L 31.350 63 10-1305929.4 6 30
Pyrene ug/L 47.750 95 50-1308542.3 12 30
2,4,6-Tribromophenol (S)%103 10-13786
2-Fluorobiphenyl (S)%74 13-13063
2-Fluorophenol (S)%67 10-13060
Nitrobenzene-d5 (S)%85 13-13074
Phenol-d6 (S)%60 10-13053
Terphenyl-d14 (S)%104 25-13088
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1354564
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92446606001, 92446606002, 92446606003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3456264-1
Associated Lab Samples:92446606001, 92446606002, 92446606003
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 09/30/19 15:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3456264-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1142560-05
R3456264-3SAMPLE DUPLICATE:
Total Solids %85.8 0.946 1086.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92446606
DRY-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1354565
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92446606007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3456260-1
Associated Lab Samples:92446606007
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 09/30/19 15:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3456260-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1142573-03
R3456260-3SAMPLE DUPLICATE:
Total Solids %86.0 0.0546 1085.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 40
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92446606
DRY-003
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 40
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92446606
DRY-003
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92446606005 1351948 1351948TMW-4 3015 EPA 6020B
92446606006 1351948 1351948TMW-DUP 3015 EPA 6020B
92446606001 1353186 1353186SB-5 (3-4)3051 EPA 6020B
92446606002 1353186 1353186SB-7 (1-2)3051 EPA 6020B
92446606003 1353186 1353186SB-6 (5-6)3051 EPA 6020B
92446606007 1353186 1353186SB-DUP 3051 EPA 6020B
92446606005 1351504 1351504TMW-4 7470A EPA 7470A
92446606006 1351504 1351504TMW-DUP 7470A EPA 7470A
92446606001 1353452 1353452SB-5 (3-4)7471A EPA 7471B
92446606002 1353452 1353452SB-7 (1-2)7471A EPA 7471B
92446606003 1353452 1353452SB-6 (5-6)7471A EPA 7471B
92446606007 1353452 1353452SB-DUP 7471A EPA 7471B
92446606005 499474 499646TMW-4 EPA 3510C EPA 8270E
92446606006 499474 499646TMW-DUP EPA 3510C EPA 8270E
92446606004 500111TRIP BLANK EPA 8260D
92446606005 500111TMW-4 EPA 8260D
92446606006 500111TMW-DUP EPA 8260D
92446606001 1354564 1354564SB-5 (3-4)SM 2540 G SM 2540G
92446606002 1354564 1354564SB-7 (1-2)SM 2540 G SM 2540G
92446606003 1354564 1354564SB-6 (5-6)SM 2540 G SM 2540G
92446606007 1354565 1354565SB-DUP SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/17/2019 08:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 40
Page 37 of 40
Page 38 of 40
Page 39 of 40
Page 40 of 40

Appendix C
Monitoring Well Sampling Form
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling
Record Date: 4/2/2019
Job No:
Well ID:
Water Volume Pumping DO Temp.S. Cond.pH ORP Turbidity
Time Level Pumped Rate (mg/l)(oC)(µS/cm)(SU)(mV)(NTU)
Stabilization Criteria
Primary: Secondary:
LOW-FLOW GROUNDWATER
Other Sample Parameters:___________________________________________________________________________________________________
Sampled at:____________________________ Parameters taken with:
Sample Delivered to:________________________________ by ______________________________________ at ____________________________.
Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________
Sample Parameter Containers (Types, Number of Containers, Preservatives):
SAMPLING RECORD Well Location:
Facility Name: Date:
Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:
Total Well Depth (ft):_____________________ Depth to Water (ft):_________________________________ Well Diameter:
Sampling Personnel:___________________________, __________________________ Screen Interval (ft ): _____________-______________
Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.
Weather Conditions:_______________________________________________________ NOTES:
GROUNDWATER SAMPLING PARAMETERS
Stabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017.
Turb. +/- 10% (<10 NTUs for metals)
Water Level: slight or stable drawdown during purging
pH +/- 0.1 unit
S.Cond. +/- 5% ORP +/- 10mV
DO +/- 0.2 mg/L