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HomeMy WebLinkAbout20006_Southern Wipers_ESA Phase II 2019.10.02SUMMIT ENGINEERING• LABORATORY. TESTING October 2, 2019 Mr. Wyatt Dixon Fountains NoDA Holdings, LLC 1420 East 7th Street, Suite 150 Charlotte, NC 28204 SUMMIT Engineering, Laboratory & Testing, P.C. 3575 Centre Circle Fort Mill, South Carolina 29715 www.SUMMIT-coMpanies.com Phone: (704) 504-1717 Fax: (704) 504-1125 Subject: Brownfields Phase II Environmental Site Assessment Southern Wipers 511 E. 25th Street Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 3586.01 Brownfields Project No. 20006-16-060 Dear Mr. Dixon SUMMIT ENGINEERING, LABRATORY & TESTING, P.C. (SUMMIT) is pleased to submit the following report of our Brownfields Phase 11 Environmental Site Assessment (ESA) of the Southern Wipers property, located in Charlotte, Mecklenburg County, North Carolina (Mecklenburg County Parcel ID: 08305308). This report includes a description of the methodology of our investigation and a summary of our findings and conclusions. If you have any questions regarding our assessment of the subject property or our conclusions, please do not hesitate to call us at (704) 504-1717. Sincerely, SUMMIT Patr7Wowery Senior Environmental Manager NC LG No: 2421 CA�+Oj' Cyr• F�3S10.��,:. 4d by � �4 SEAL '_ 03356� Michael D. Zavislak, NRCC-EAfi', . IH, P .' Environmental Department Man • SUMMIT's NC Engineering Firm License No. C-2530 ENGINEERING * LABORATORY • TESTING 3575 Centre Circle give j Fort Mill, Soudh Carolina 29715 1 (704) SW - 1717 1 (704) 504 - 1125 (Fax) WV1 VV. UMMIT-C OMPAN IE .COM SUMMIT ENGINEERING. f,ABORATORY+TESTING BROWNFIELDS PHASE II ENVIRONMENTAL SITE ASSESSMENT SOUTHERN WIPERS CHARLOTTE MECKLENBURG COUNTY NORTH CAROLINA SUMMIT PROJECT NO. 3586.01 BROWNFIELDS PROJECT NO.20006-16-060 Prepared For: Fountains NoDA Holdings, LLC 1420 East 7t" Street, Suite 150 Charlotte, NC 28204 Prepared By: SUMMIT ENGINEERING, LABRATORY & TESTING, P.C. 3575 Centre Circle Fort Mill, South Carolina 29715 704-504-1717 October 2, 2019 ENGINEERING IN * LABORATORY • TESTING 3575 Centre Circle give I Fort Mill, South Carolina 29715 1 (704) SW - 1717 1 (704) 504 - 1125 (Fax) WVI W. UMMIT- OMPANIE . OM Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 TABLE OF CONTENTS 1.0 EXECUTIVE SUMMARY......................................................................................................1 2.0 INTRODUCTION.................................................................................................................... 3 2.1. PURPOSE.............................................................................................................................3 2.2. SITE DESCRIPTION...........................................................................................................3 2.3. ASSESSMENT HISTORY..................................................................................................3 2.4. ASSESSMENT WORK PLAN OBJECTIVES...................................................................4 3.0 PROPERTY SETTING............................................................................................................. 5 3.1. TOPOGRAPHIC SETTING................................................................................................ 5 3.2. GEOLOGIC SETTING........................................................................................................5 3.3. HYDROLOGIC SETTING..................................................................................................6 4.0 SUMMARY OF FIELD ACTIVITIES.................................................................................... 7 4.1. SOIL ASSESSMENT........................................................................................................... 7 4. l .1. SOIL BORINGS........................................................................................................... 7 4.1.2. SOIL SAMPLING........................................................................................................ 8 4.2. GROUNDWATER ASSESSMENT.....................................................................................8 4.2.1. MONITORING WELL GUAGING/PURGING.........................................................9 4.2.2. GROUNDWATER MEASURMENTS.....................................................................10 4.2.3. GROUNDWATER SAMPLING................................................................................10 4.3. SURFACE WATER/SEDIMENT ASSESSMENT............................................................10 4.3.1. SURFACE WATER & SEDIMENT SAMPLING....................................................11 4.4. SAMPLE PACKING AND SHIPMENT...........................................................................11 4.5. DECONTAMINATION.....................................................................................................12 4.6. INVESTIGATIVE DERIVED WASTE.............................................................................12 5.0 SUMMARY OF LABORATORY ANALYSIS.....................................................................13 6.0 DATA QUALITY....................................................................................................................16 6.1. QUALITY CONTROL SAMPLES...................................................................................16 6.1.1. DUPLICATE SAMPLES...........................................................................................16 6.1.2. EQUIPMENT BLANK..............................................................................................16 6.1.3. FIELD BLANK..........................................................................................................16 6.1.4. TRIP BLANK.............................................................................................................16 6.1.5. SENSITIVITY............................................................................................................16 DAProject Fomis\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase H ESA 1 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 6.1.6. LABORATORY DATA EVALUATION....................................................................17 7.0 FINDINGS & CONCLUSIONS............................................................................................18 8.0 QUALIFICATION OF REPORT........................................................................................... 20 9.0 ADDITIONAL SERVICES.................................................................................................... 21 10.0 REFERENCES.......................................................................................................................22 APPENDICES Appendix L• FIGURES Appendix II: TABLES Appendix III: ANALYTICAL RESULTS Appendix IV: WELL RECORDS/PERMITS Appendix V: BORING LOGS Appendix VI: FIELD/CALIBRATION LOGS Appendix VIL• IDW DISPOSAL CERTIFICATE Appendix VIII: RECEPTOR SURVEY DAProject Fomis\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers - Phase H ESA ii Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 1.0 EXECUTIVE SUMMARY In summary, six (6) groundwater samples, eleven (11) soil samples, two (2) surface water samples two (2) sediment samples, appropriate duplicate samples and QC samples (trip/field blanks) were collected from the site. Samples were analyzed for the presence of Volatile Organic Compounds via EPA Method 8260, Semi -Volatile Organic Compounds (SVOCs) via EPA Method 8270 and RCRA 8 Metals plus Hexavalent Chromium by EPA Method 6020/7471/7196. Soil samples detected the presence of elevated concentrations of Arsenic and Hexavalent Chromium (Chromium VI) above IHSB Preliminary Site Remediation Goals (PSRGs) for residential use in multiple surface (0-2' bgs) samples. Arsenic concentrations ranged from 0.73 mg/kg to 4.4 mg/kg in samples SB-1 through SB-9, while SB-10 and BG-1 (background) reported concentrations of 240 mg/kg and 50 mg/kg respectively. Hexavalent Chromium analysis detected concentrations above PSRGs in soil samples SB-5 through SB-10 and BG-1, ranging from 0.41 mg/kg (SB-7) to 2.9 mg/kg (SB-10). No VOC or SVOC constituent was detected above its respective PSRG. Based on a review of the concentrations, SUMMIT considers the Arsenic detections in SB-1 through SB-9 to be naturally occurring and should be considered background concentrations for the subject site. The groundwater samples identified the presence of multiple VOC and Metal constituents reported above North Carolina Groundwater Standards (15A NCAC 02L). VOC constituents Benzene, cis- 1,2-Dichloroethene Trichloroethene and Vinyl Chloride were detected in samples collected from MW-18 and MW-19. These analytes were reported above NC 2L standards in MW 19 while only Vinyl Chloride was reported above NC 2L standards in MW-18. Additionally, Trichloroethene and Vinyl Chloride were reported above DMW Residential Vapor Intrusion Screening Concentrations in MW-19 and MW-18 (vinyl chloride only). Arsenic was detected above NC 2L standard of 10 ug/L at 1,200 ug/L and 13 ug/L in MW-23 and MW-24 respectively. Chromium and Hexavalent Chromium was detected above the NC 2L standard of 10 ug/L in MW-17/MW-17 DUP (total 18 ug/L/ Hex 16 ug/L) and MW-19 (total 7,500 ug/L / Hex 3,900 ug/L). VOC detections appear to be concentrated in the northern portion of the subject site. Hexavalent Chromium impacts appear to be concentrated in the northeastern portion of the subject site. Arsenic impacts appear to be concentrated in the eastern portion of the subject site. In general, the groundwater detections reported in this assessment closely match historical concentrations reported in the monitoring reports completed for the adjoining DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 1 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 Applied Research Group Inc (ARGI) site (Table 8, Appendix II), with the exception of MW-19 and MW-25 which appear to have decreased significantly with time. The surface water samples collected from the adjoining Little Sugar Creek identified Tetrachloroethylene, Trichloroethene and Vinyl Chloride at concentrations exceeding North Carolina Water Quality Standards for Surface Waters (NC 2B). The reported concentrations are consistent in the upstream (SW2) and downstream (SW-1) samples. Sediment Samples collected from Little Sugar Creek reported one (1) detection of Benzo(a)pyrene in sample SS-1 DUP exceeding IHSB PRSGs. Additionally, Arsenic detections were reported above IHSB PSRGs in the sediment samples. Based on a review of the concentrations, SUMMIT considers the Arsenic detections to be consistent with naturally occurring concentrations. SUMMIT concludes the presence of surficial (0-2 bgs) soil impacts with heavy metals (Arsenic, Hexavalent Chromium), groundwater impacts with VOCs (Benzene, cis-1,2-Dichloroethene Trichloroethene, Vinyl Chloride), heavy metals (Arsenic, Hexavalent Chromium) and surface water impacts (Tetrachloroethylene, Trichloroethene, Vinyl Chloride) at the subject site are likely a result of off -site operations and existing off -site contamination. VOC, Arsenic and Hexavalent Chromium groundwater and soil impacts have been documented to be associated with upgradient adjoining properties (Gibbs Electroplating & Applied Research Group, Inc). Additionally, no known operation at the subject site utilized hazardous materials or heavy metals. Surface water samples indicate VOC impacts originate upstream of the subject site. DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 2 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 3586.01 October 2, 2019 2.0 2.1. PURPOSE INTRODUCTION SUMMIT was retained by Fountains NoDa Holdings, LLC to perform the Brownfields Phase II ESA of the Southern Wipers property, located at 511 East 25th Street in Charlotte, Mecklenburg County, North Carolina. More specifically the site can be described as Mecklenburg County Parcel ID: 08305308. The Brownfields Phase II ESA was conducted based on NC DEQ requests for additional assessment for preparation of the Brownfields Agreement. This report presents the results of our Brownfields Phase II ESA of the Southern Wipers site. 2.2. SITE DESCRIPTION The site is irregular in shape and was noted to be comprised of the 2.8-acre Mecklenburg Tax Parcel 08305308. The subject site is currently developed with a former rag manufacturing facility consisting of a main building (multiple additions), associated warehouse buildings and an abandoned railroad spur. The site is accessible from E. 25th Street to the south and E. 26th Street to the north. Refer to the Site Location Map shown in Figure 2 of Appendix I for the location of the subject property. 2.3. ASSESSMENT HISTORY SUMMIT completed a Phase I ESA, dated March 30, 2015 for the subject site. The subject site appeared to be first developed in 1950 as Southern Wipers, a manufacturing operation making commercial and industrial rags. This operation grew as more warehousing buildings were added up through the 1960s and continued to be utilized for the same purpose through the 1990s. While the site was utilized for manufacturing purposes, the specialized knowledge provided by the property owner confirmed that no hazardous substances were utilized in the manufacturing processes (only cutting, washing and packaging). Additionally, historical research did not identify the presence of any hazardous substances or tanks on the property. Upgradient and adjoining industrial facilities were identified to have impacted the subject site during the completion of the 2015 Phase I ESA. The Applied Research Group (ARGI) documented arsenic and chromium soil impacts on the ARGI facility located adjoining to the southeast as well as the DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 3 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 subject site property. Assessment of this release included the installation of monitoring wells on the subject site as well as the ARGI facility. Groundwater sampling confirmed the presence of metals, Trichloroethene and various VOCs in the groundwater at the subject site. The VOCs have been attributed to the adjoining Gibbs Electroplating facility, located adjoining to the southeast of the site and adjacent to the north of the ARGI facility. No site -specific environmental assessment has been completed with respect to the Gibbs facility release at the time of this report other than offsite sampling affecting this property. Groundwater concentrations related to the site monitoring wells are reported in Table 8 in Appendix 11 of this report. Based on the Phase I ESA, SUMMIT recommended consultation with the Brownfields Program. 2.4. ASSESSMENT WORK PLAN OBJECTIVES SUMMIT proposed to perform a Brownfields Phase II ESA according to our approved assessment work plan, general accordance with the Inactive Hazardous Sites Branch Guidelines for Assessment and Cleanup (October 2015 edition) and EPA Region IV SESD Field Branches Quality System and Technical Procedures. The proposed scope of services included the collection of eleven (11) soil samples, six (6) groundwater samples, two (2) sediment samples and two (2) surface water samples from the subject site. The sampling locations were placed in accessible locations and in areas that represented the highest potential for disturbance for the planned development and in accordance with the approved July 27, 2018 Work Plan for Additional Assessment. All samples collected were scheduled to be relinquished to a NC certified laboratory for analysis of Volatile Organic Compounds by EPA method 8260, Semi -Volatile Organic Compounds EPA method 8270, RCRA Metals by EPA method 6020/7471 and Hexavalent Chromium by EPA method 7196. DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 4 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 3586.01 October 2, 2019 3.0 3.1. TOPOGRAPHIC SETTING PROPERTY SETTING The United States Geological Survey (USGS) Charlotte East topographic quadrangle map and the Mecklenburg County North Carolina GIS website were reviewed. According to the contour lines on the topographic maps, the elevation of the subject property ranges from approximately 680 feet (along southeastern site boundary) to approximately 675 feet (along Little Sugar Creek) above Mean Sea Level (MSL). The contour lines indicate the general direction of downward slope is to the northwest towards Little Sugar Creek. Little Sugar Creek empties into Sugar Creek. Sugar Creek flows into the Catawba River near Goat Island. 3.2. GEOLOGIC SETTING The property is located in Mecklenburg County, North Carolina, which is located in the south-central Piedmont Physiographic Province. The Piedmont Province generally consists of well-rounded hills and ridges which are dissected by a well -developed system of draws and streams. The Piedmont Province is predominantly underlain by metamorphic rock (formed by heat, pressure and/or chemical action) and igneous rock (formed directly from molten material) which were initially formed during the Precambrian and Paleozoic eras. The volcanic and sedimentary rocks deposited in the Piedmont Province during the Precambrian era were the host from the metamorphism and were changed to gneiss and schist. The more recent Paleozoic era had periods of igneous emplacement, with at least episodes of regional metamorphism resulting in the majority of the rock types seen today. The topography and relief of the Piedmont Province has developed from differential weathering of the igneous and metamorphic rock. Ridges and hills have been developed on the more easily weathered and erodible rock. Because of the continued chemical and physical weathering, the rocks in the Piedmont Province are now generally covered with a mantle of soil that has weathered in place from the parent bedrock. These soils vary in thickness and are referred to as residuum or residual soils. The residuum is typically finer grained and has higher clay content near the surface because of the advanced weathering. Similarly, the soils typically become coarser grained with increasing depth DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers - Phase II ESA Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 3586.01 October 2, 2019 because of decreased weathering. As the weathering decreases, the residual soils generally retain the overall appearance, texture, gradation and foliations of the parent rock. 3.3. HYDROLOGIC SETTING Based on a review of the United States Geological Survey (USGS) Charlotte East topographic quadrangle map, the inferred groundwater flow direction based on topography appears to be to the northwest towards Little Sugar Creek. Refer to Figure I in Appendix I for a topographic map for the subject property. DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 6 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 4.0 SUMMARY OF FIELD ACTIVITIES 4.1. SOIL ASSESSMENT On September 21, 2018, SUMMIT personnel conducted the soil assessment phase of the Brownfields Phase II ESA. The soil borings were conducted in order to obtain knowledge of the surface and subsurface environmental conditions. A total of ten (10) soil borings and one (1) background soil borings were completed for this soil assessment. 4.1.1. SOIL BORINGS Environmental Drilling and Probe Services (EDPS) mobilized to the subject site with a GeoProbe direct push machine for the completion of soil boring activities. At each boring location an acetate lined MacroCore sampler was advanced to the depth of 10 feet below ground surface (bgs). Soil cores were retrieved in 2 ft intervals, logged and field screened by field personnel utilizing a calibrated Photo -Ionizing Detector for the presence of Volatile Organic Compounds (VOCs). The locations of the soil borings/soil samples can be viewed on the attached Site Map, Figure 2, in Appendix I. Surface soil (0-2' bgs) samples were collected from all sampling locations (SB-1 through SB-10 & BG-1). Field screening of collected soil intervals from all borings did not detect the presence of VOCs, therefore subsurface soil samples were not collected during this assessment. All soil borings generally encountered Brown/Tan/Orange clayey medium grained Sand from the surface to depths ranging from 4 feet bgs to 10 feet bgs. This material is consistent with Fill. Soil borings SB-4 through SB-10 encountered a Tan/Grey sandy Clay beneath the fill material at depths from 6 feet bgs to 10 ft bgs. This material was considered native soils for the site area. Groundwater was encountered in borings SB-I, SB-2, SB-4, SB-5, SB-6, SB-8 and SB-9. No visual or olfactory evidence of a release or impact were noted in soil borings. Field screening utilizing a calibrated Photo -Ionizing Detector did not detect the presence of Volatile Organic Compounds (VOCs) in any sampling interval. Soil Boring Logs can be viewed in Appendix V of this report. DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers - Phase II ESA Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 3586.01 October 2, 2019 4.1.2. SOIL SAMPLING On September 21, 2018, SUMMIT personnel collected soil samples from soil borings SB-1 through SB-10. Background soil boring BG-1 was collected on September 25, 2018. Soil samples were collected in the laboratory provided vails and jars in general accordance with the EPA Field Branches Quality System and Technical Procedures. Each soil boring was located utilizing a hand-held GPS unit. The locations of the soil borings/soil samples can be viewed on the attached Site Map, Figure 2, in Appendix I. The following location data can be attributed to the collected soil samples. Sample ID Sample Location (Lat/Lon) Sample Interval (ft b s) SB-1 35.241425 /-80.815637 0-2 SB-2 35.241180 /-80.815811 0-2 SB-3 35.241082 /-80.815652 0-2 SB-4 35.240560 /-80.816031 0-2 SB-5 35.240579 /-80.815724 0-2 SB-6 35.240010 /-80.815351 0-2 SB-7 35.240873 /-80.815170 0-2 SB-8 35.240598 /-80.815216 0-2 SB-9 35.240337 /-80.815582 0-2 SB-10 35.240076 /-80.816008 0-2 BG-1 35.240390 /-80.816308 0-2 All collected soil samples were submitted to a North Carolina certified laboratory for the analysis of Volatile Organic Compounds via EPA Method 8260, Semi -Volatile Organic Compounds (SVOCs) via EPA Method 8270 and RCRA 8 Metals plus Hexavalent Chromium by EPA Method 6020/7471/7196. 4.2. GROUNDWATER ASSESSMENT On September 20, 2018 and September 21, 2018, SUMMIT personnel conducted the groundwater assessment phase of the Brownfields Phase II ESA. SUMMIT proposed to collect groundwater samples from the eight (8) existing monitoring wells on the Southern Wipers property and adjoining parcel owned by the City of Charlotte (PIN 08305315). SUMMIT received approval from the City of Charlotte to access these monitoring wells and a copy of this approval is included in Appendix IV of this report. The monitoring wells planned for this sampling event were MW-17, MW-18, MW- DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 8 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 19, MW-20, MW-21, MW-23, MW-24 and MW-25 associated with the assessment and monitoring of the adjacent ARGI site. During this assessment MW-20 and MW-21 could not be located. Therefore six (6) groundwater samples were collected during this assessment. 4.2.1. MONITORING WELL GAUGING/PURGING On September 20, 2018 SUMMIT personnel completed monitoring well gauging and purging on monitoring wells planned for sampling. Purging was conducted as the well histories were somewhat unknown and to ensure that each well was prepared for sampling the following day. At each well location, SUMMIT personnel observed the condition of the monitoring well, gauged the depth to water utilizing a decontaminated Heron water level indicator and obtained total depth of each well. If ID tags were found, the tags were recorded. Monitoring well field information was compared to well construction details provided in the 2011 ARGI Monitoring Report completed by others. Site observations appeared consistent with construction details provided in the 2011 monitoring report. Table 1 in Appendix II of this report summarizes the well construction details. Following well gauging, a decontaminated well pump capable of 2 gallon per minute flow rate was placed in the monitoring well and activated. Purge water was collected in 5-gallon buckets and transferred a 55-gallon DOT approved drum for disposal. SUMMIT personnel monitored the purging, recording observations such as color/turbidity, odor and depth to water. Purging was considered complete when three well volumes were purged and the groundwater appeared clear or when the well pumped dry following the second recharge. The following purge data was recorded and field Purge Records are included in Appendix VI of this report. Well ID DTW (ft b s) Approx. Purge Volume (gallons) Notes MW-17 2.75 15 7 well volumes removed, clear, never purged dry MW-18 9.15 15 7 well volumes removed, clear, never purged dry MW-19 10.90 10 6 well volumes removed, clear, never purged dry MW-23 2.30 14 7 well volumes removed, pumped dry twice MW-24 9.04 4 4 well volumes removed, pumped dry twice MW 25 9.42 12 6 well volumes removed, clear, never purged dry DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 9 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 4.2.2. GROUNDWATER MEASURMENTS The depth to groundwater measurements were recorded prior to groundwater sampling on September 21, 2018. Top of casing elevations reported in the 2011 ARGI Monitoring Report were utilized to determine the groundwater table elevations for this assessment. Groundwater table elevations are reported in Table 2 in Appendix II of this report. Additionally, a Potentiometric Map is provided as Figure 5 in Appendix I of this report. Groundwater measurements indicate a groundwater flow direction to the northwest and appear consistent with historical elevation data reported in ARGI reports. 4.2.3. GROUNDWATER SAMPLING On September 21, 2018, SUMMIT personnel mobilized to the site for the collection of a groundwater samples from MW-17, MW-18, MW-19, MW-23, MW-24 and MW-25. Prior to sample collection, the monitoring well was purged via the low -flow method using a variable speed peristaltic pump and new dedicated tubing. Purging continued until consistent values (i.e., less than 10% variance between consecutive readings) were obtained for dissolved oxygen, specific conductivity, temperature, and consecutive pH measurements were within f 0.2 pH units. Additionally, turbidity was monitored with a calibrated turbidity meter and purging was considered adequate when readings are consistently <10 NTUs. Field sampling logs are included in Appendix VI of this report. All purge and development water was placed in a DOT approved steel 55-gallon drum for disposal. Following the purging process, one (1) groundwater sample was collected from each well. A duplicate sample was collected from MW-17 (MW-17 DUP). The collected samples were submitted to a North Carolina certified laboratory for the prescribed laboratory analysis of Volatile Organic Compounds via EPA Method 8260, Semi -Volatile Organic Compounds (SVOCs) via EPA Method 8270 and RCRA 8 Metals plus Hexavalent Chromium by EPA Method 6020/7471/7196. 4.3. SURFACE WATER/SEDIMENT ASSESSMENT On September 25, 2018, SUMMIT personnel conducted the surface water and sediment assessment phase of the Brownfields Phase II ESA. SUMMIT proposed to collect surface water and sediment samples from two (2) locations in the adjoining Little Sugar Creek. Surface Water and Sediment D:\ProjectFonns\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 10 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 samples were collected in the laboratory provided vails and jars in general accordance with the EPA Field Branches Quality System and Technical Procedures. 4.3.1. SURFACE WATER & SEDIMENT SAMPLING On September 25, 2018, SUMMIT personnel mobilized to the site for the collection of a Surface Water and Groundwater samples from Little Sugar Creek which adjoins the subject site to the northwest. The downstream sample location (SS-1/SW-1) was collected prior to the upstream sample location (SS-2/SW-2). At each location, SUMMIT personnel waded to the center of Little Sugar Creek and faced upstream for the collection of the samples. Surface Water samples were collected at each location by placing the laboratory provided sample containers directly into the water body. Following Surface Water sampling, sediment sampling was conducted. Sediment samples for VOCs were collected utilizing a lab provided plunger and placed directly into the laboratory provided vials. Sediment samples for the remaining analysis was collected via decontaminated stainless -steel spoon and placed into the laboratory provided vials and jars. The following sampling location data can be attributed to the collected samples: Sample ID Sample Location (Lat/Long) Sample Media SW-1 35.240395 /-80.816384 Surface Water SS-1 Sediment SW-2 35.241454 /-80.815821 Surface Water SS-2 Sediment All collected samples were submitted to a North Carolina certified laboratory for the analysis of Volatile Organic Compounds via EPA Method 8260, Semi -Volatile Organic Compounds (SVOCs) via EPA Method 8270 and RCRA 8 Metals plus Hexavalent Chromium by EPA Method 6020/7471/7196. 4.4. SAMPLE PACKING AND SHIPMENT Upon securing the samples in laboratory provided containers, the vial and jar lids were tightly fastened, and the jars encapsulated in shock -resistant plastic bags. The samples were double -bagged in large plastic bags, tied off with rubber bands, and packed on ice in a cooler. The samples were DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers - Phase II ESA 11 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 picked up by Con -Test lab currier and shipped overnight to Con -Test Analytical Laboratory in East Longmeadow, Massachusetts. The vials, jars and canisters used for the collection of the samples at this site were prepared by Con -Test, and were pre -labeled and contained analyte-appropriate preservatives. A listing of the preservatives in the sample containers utilized for the collection of the samples at this site are cataloged in the Chain -Of -Custody record, attached in Appendix III of this report. The secured samples were relinquished to laboratory on the dates indicated on the Chain of Custody Records for laboratory analysis. 4.5. DECONTAMINATION Upon completion of the drilling activities, the drilling equipment was decontaminated by the well driller by use of a steam cleaner or Alconox and tap water wash, tap water rinse, isopropanol rinse (sampling equipment), and deionized water rinse. Decontamination of the drilling equipment was performed prior to starting drilling activities, and upon the completion of drilling activities at each boring/well location. Where applicable, new disposable materials (bailers, tubing, MacroCore sleeves, etc.) were utilized to limit the potential for cross -contamination. 4.6. INVESTIGATIVE DERIVED WASTE Soil cuttings produced during soil boring activities were placed back in the borehole following field screening and sampling. Purge water was collected in 55-gallon steel DOT approved drums for pick up by a third -party disposal contractor. The drum is picked up by EVO Corporation ad disposed of on March 25, 2019. A copy of waste disposal certificate is attached in Appendix VII of this report. D:\ProjectFonns\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 12 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 5.0 SUMMARY OF LABORATORY ANALYSIS Samples were relinquished to Con -Test Analytical Laboratories on September 21, 2018 and September 25, 2018. Tables located in Appendix II of this report summarizes all detections. The May 2019 NCDEQ IHSB Preliminary Soil Remediation Goals (PSRGs), 2013 NCAC 02L Groundwater Standards and the 2017 NCAC 02B Surface Water standards were utilized for regulatory comparison. The analytical detections are summarized below: Soil: • VOC constituents Acetone, Chloroform, Tetrachloroethylene and Trichloroethene were reported in various collected soil samples and sample duplicate at concentrations below NC DEQ reference values for Protection of Groundwater and IHSB PSRGs for residential use. • SVOC constituents Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(g,h,i)perylene, Benzoic Acid, Fluoranthene and Pyrene were detected in soil sample analysis from SB-1, SB-2, SB-9 and SB-10. These detections were reported at concentrations below NC DEQ reference values for Protection of Groundwater and the IHSB PSRGs for residential use with the exception of SB-2 which reported a concentration of Benzo(a)pyrene equal to the PSRGs for residential use (0.11 mg/kg). • Arsenic was detected in the collected soil samples from SB-1, SB-2, SB-3, SB-4, SB-5, SB- 6, SB-7, SB-8, SB-9, SB-10 and BG-1 (background) at concentrations exceeding the IHSB PSRGs for residential use. Concentrations detected in SB-1 through SB-9 ranged from 0.73 mg/kg to 4.4 mg/kg while SB-10 and BG-1 reported concentrations of 240 mg/kg and 50 mg/kg respectively. • Hexavalent Chromium was detected in the collected soil samples from SB-5, SB-6, SB-7, SB- 8, SB-9, SB-10 and BG-1 (background) at concentrations exceeding the IHSB PSRGs for residential use. Concentrations detected in soil samples ranged from 0.41 mg/kg to 2.9 mg/kg, exceeding the PSRG of .31 mg/kg. D:\ProjectFonns\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 13 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 3586.01 October 2, 2019 • Lead, Mercury, Silver, Barium and Cadmium were reported in various collected soil samples and sample duplicate at concentrations below NC DEQ reference values for Protection of Groundwater and IHSB Preliminary Soil Remediation Goals (PSRGs) for residential use. Groundwater: • Groundwater collected from MW-18 and MW-19 detected the presence of various VOC constituents at concentrations exceeding North Carolina Groundwater Quality Standards (NC 2L). Benzene, cis-1,2-Dichloroethene, Trichloroethene and Vinyl Chloride were detected above NC 2L in MW-19. Vinyl Chloride was additionally detected above NC 2L standards in MW-18. No other VOC detection exceeded its respective NC 2L standard. • Concentrations of Trichloroethene and Vinyl Chloride in MW-19 and Vinyl Chloride in MW- 18 exceed the DWM Residential Groundwater Vapor Intrusion Screening Concentrations (Table 7, Appendix II). • Arsenic was detected above NC 2L standard of 10 ug/L in MW-23 (1,200 ug/L) and MW-24 (13 ug/L). • Total Chromium was detected above NC 2L standard of 10 ug/L in MW-17 (18 ug/L) MW- 17 DUP (19 ug/L) and MW-19 (7,500 ug/L). • Hexavalent Chromium was detected above NC 2L standard of 10 ug/L in MW-17 (16 ug/L) MW-17 DUP (16 ug/L) and MW-19 (3,900 ug/L). • No NC 2L standards have been established for the following compounds detected in select groundwater samples: Diisopropyl Ether (DIPE). D:\ProjectFonns\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase H ESA 14 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 3586.01 October 2, 2019 Surface Water/Sediment: • Surface Water collected detected the presence of tetrachloroethylene, Trichloroethene and Vinyl Chloride at concentrations exceeding the North Carolina Water Quality Standards for Surface Waters (NC 2B). Various other VOC detections did not exceed NC 2B standards. • Benzo(a)pyrene was detected in SS-1 DUP at 0.15 mg/kg, exceeding the IHSB PSRG for residential use of 0.11 mg/kg. • Arsenic was detected in SS-1 at 0.85 mg/kg and SS-2 at 1.5 mg/kg, exceeding the IHSB PSRG for residential use of 0.68 mg/kg. • Hexavalent Chromium was not detected in the sediment samples. D:\ProjectFonns\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 15 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 6.0 DATA QUALITY 6.1. QUALITY CONTROL SAMPLES 6.1.1. DUPLICATE SAMPLES Duplicate groundwater, soil, surface water and sediment samples were collected during this assessment. All duplicate samples were submitted for matching analysis. Duplicate analytical results are included in the summary tables in Appendix II of this report. Duplicate samples appear similar in concentrations to the field collected sample. 6.1.2. EQUIPMENT BLANK An equipment blank was not collected during the completion of this assessment. 6.1.3. FIELD BLANK A field blank was collected during the completion of this assessment and submitted for VOC, SVOC RCRA Metals and Hexavalent Chromium. Field Blank analytical results are included in Table 4 in Appendix II of this report. Analysis did not detect any constituent above the laboratory reporting limits. 6.1.4. TRIP BLANK One (1) trip blank was collected for VOC analysis. No detections were reported above the laboratory reporting limits for the Trip Blank sample. 6.1.5. SENSITIVITY Laboratory RDLs and method detection limits (MDLs) were sufficient to report concentrations below regulatory standards for the majority of analytes. D:\ProjectFonns\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 16 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 6.1.6. LABORATORY DATA EVALUATION The laboratory completed validation and verification of laboratory processes and data, and delivered a laboratory report to SUMMIT. The laboratory report and the QC information provide documentation of compliance with the industry standards. In reviewing the laboratory results, several analytes are reported as detections with "J" data qualifiers, indicating the reported value is an estimate reported within the 95% confidence interval. These compounds were detected above the MDL, but below the RDL. The MDL is the lowest concentration at which an analyte can be detected in a sample by the particular laboratory method used. "Detected" indicates that the analyte can be distinguished from the blank with reasonable certainty. The RDL (also called practical quantitation limit, or PQL) is approximately five times the MDL or the lower calibration standard, whichever is higher. Results above the report limit can be distinguished from the blank and fall within applicable standard curves. For the purposes of this assessment, all "J" qualified data are considered acceptable for making site management decisions. D:\ProjectFonns\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 17 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 7.0 FINDINGS & CONCLUSIONS In summary, six (6) groundwater samples, eleven (11) soil samples, two (2) surface water samples two (2) sediment samples, appropriate duplicate samples and QC samples (trip/field blanks) were collected from the site. Samples were analyzed for the presence of Volatile Organic Compounds via EPA Method 8260, Semi -Volatile Organic Compounds (SVOCs) via EPA Method 8270 and RCRA 8 Metals plus Hexavalent Chromium by EPA Method 6020/7471/7196. Soil samples detected the presence of elevated concentrations of Arsenic and Hexavalent Chromium (Chromium VI) above IHSB Preliminary Site Remediation Goals (PSRGs) for residential use in multiple surface (0-2' bgs) samples. Arsenic concentrations ranged from 0.73 mg/kg to 4.4 mg/kg in samples SB-1 through SB-9, while SB-10 and BG-1 (background) reported concentrations of 240 mg/kg and 50 mg/kg respectively. Hexavalent Chromium analysis detected concentrations above PSRGs in soil samples SB-5 through SB-10 and BG-I, ranging from 0.41 mg/kg (SB-7) to 2.9 mg/kg (SB-10). No VOC or SVOC constituent was detected above its respective PSRG. Based on a review of the concentrations, SUMMIT considers the Arsenic detections in SB-1 through SB-9 to be naturally occurring and should be considered background concentrations for the subject site. The groundwater samples identified the presence of multiple VOC and Metal constituents reported above North Carolina Groundwater Standards (15A NCAC 02L). VOC constituents Benzene, cis- 1,2-Dichloroethene Trichloroethene and Vinyl Chloride were detected in samples collected from MW-18 and MW-19. These analytes were reported above NC 2L standards in MW-19 while only Vinyl Chloride was reported above NC 2L standards in MW-18. Additionally, Trichloroethene and Vinyl Chloride were reported above DMW Residential Vapor Intrusion Screening Concentrations in MW-19 and MW-18 (vinyl chloride only). Arsenic was detected above NC 2L standard of 10 ug/L at 1,200 ug/L and 13 ug/L in MW-23 and MW-24 respectively. Chromium and Hexavalent Chromium was detected above the NC 2L standard of 10 ug/L in MW-17/MW-17 DUP (total 18 ug/L/ Hex 16 ug/L) and MW-19 (total 7,500 ug/L / Hex 3,900 ug/L). VOC detections appear to be concentrated in the northern portion of the subject site. Hexavalent Chromium impacts appear to be concentrated in the northeastern portion of the subject site. Arsenic impacts appear to be concentrated in the eastern portion of the subject site. In general, the groundwater detections reported in this assessment closely match historical concentrations reported in the monitoring reports completed for the adjoining D:\ProjectFonns\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 18 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 Applied Research Group Inc (ARGI) site (Table 8, Appendix II), with the exception of MW-19 and MW-25 which appear to have decreased significantly with time. The surface water samples collected from the adjoining Little Sugar Creek identified Tetrachloroethylene, Trichloroethene and Vinyl Chloride at concentrations exceeding North Carolina Water Quality Standards for Surface Waters (NC 2B). The reported concentrations are consistent in the upstream (SW2) and downstream (SW-1) samples. Sediment Samples collected from Little Sugar Creek reported one (1) detection of Benzo(a)pyrene in sample SS-1 DUP exceeding IHSB PRSGs. Additionally, Arsenic detections were reported above IHSB PSRGs in the sediment samples. Based on a review of the concentrations, SUMMIT considers the Arsenic detections to be consistent with naturally occurring concentrations. SUMMIT concludes the presence of surficial (0-2 bgs) soil impacts with heavy metals (Arsenic, Hexavalent Chromium), groundwater impacts with VOCs (Benzene, cis-1,2-Dichloroethene Trichloroethene, Vinyl Chloride), heavy metals (Arsenic, Hexavalent Chromium) and surface water impacts (Tetrachloroethylene, Trichloroethene, Vinyl Chloride) at the subject site are likely a result of off -site operations and existing off -site contamination. VOC, Arsenic and Hexavalent Chromium groundwater and soil impacts have been documented to be associated with upgradient adjoining properties (Gibbs Electroplating & Applied Research Group, Inc). Additionally, no known operation at the subject site utilized hazardous materials or heavy metals. Surface water samples indicate VOC impacts originate upstream of the subject site. D:\ProjectFonns\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers -Phase II ESA 19 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 8.0 QUALIFICATION OF REPORT The Brownfields Phase II ESA was performed in general accordance with the approved assessment work plan, the Inactive Hazardous Sites Branch Guidelines for Assessment and Cleanup (October 2015 edition) and EPA Region IV SESD Field Branches Quality System and Technical Procedures. The findings detailed in this report are specific to the conditions in the immediate vicinity of the sample locations for this particular project. DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers - Phase II ESA 20 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 9.0 ADDITIONAL SERVICES This report does not include any environmental assessment of surface water, the determination of wetlands, the determination of noise impact, the assessment of air quality, the identification of cultural resources, or the identification of endangered species. These services are beyond the scope of services of this limited sampling and analysis. A NC DEQ Receptor Survey is included in Appendix VIII of this report. No additional services were provided. DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers - Phase II ESA 21 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 10.0 REFERENCES Phase I ESA Report, Southern Wipers Property, by SUMMIT ELT, P.C. dated March 30, 2015. Various Environmental Report —Applied Research Group, Inc, RH Bouligny, Safety-Kleen, General Latex & Chemical Co. United States Geological Survey (USGS) 7.5 minute Topographic Map of the Charlotte East Topographic Quadrangle, 2002. EPA National Primary Drinking Water Regulations - htt2://water.epa.gov/drink/contaminants/index.cfin 15A NCAC 2L Standards — hgl2s:Hdeq.nc. gov/about/divisions/water-resources/planning/classification- standards/,groundwater-standards NC Inactive Hazardous Site Branch, Preliminary Remediation Goals Table — May 2019 HTTPS:HFILES.NC.GOV/NCDEQ/WASTE%20MANAGEMENT/DWM/SF/IHS/GUIDANCE/FEB201 8 PSRGS.PDF NC DWM Residential SGSL — February 2018 hops://files.nc. gov/ncdeg/Waste%20Management/DWM/SF/RiskBasedRemediation/Feb2O 18_ Res_VISLs.pdf DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southern Wipers - Phase II ESA 22 Draft 10-2-19.docx Brownfields Phase II ESA —Southern Wipers Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 3586.01 October 2, 2019 APPENDIX I FIGURES D:\ProjectFomis\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\3586.01 Southem Wipers -Phase H ESA Draft 10-2-19.doex t;� y.._ - ?.► • t$ndo' 1 ungitin .� _ } � ram • i' ''h:. 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I Source: USGS Topographic 7.5' Quadrangle Prepared By\Date: PL/06/18 Checked By\Date: MZ/06/18 Site Location Map Southern Wipers 511 E. 25th Street SUMMIT Charlotte, North Carolina Fountians NoDa Holding, LLC Scale 1420 East 7th Street, Suite 150 As Shown Charlotte, NC 28204 Figure 1 623M • 2Mh ST. k VICINITY VAP - N.T.S. 2. ALL ONSTANCfb APE HO XKTA N)NOIRAO IWTANOES RI GECWAAA us SURIEY FEET. AOe3(sm1 AS r VO AN w5 /93 A AREA By COORMNAT' CCANAI ATGL SMTHCw Wms MC. T. THESE MMRTIEs WY BE &JBLCi ro AEpnGHAL FAWWNNTS M RFGINTS OF WAY. A ANINU Is 1-2 PEP WEN. 00. L 0. SIMVEY IS UA OH PHY9M EMUETKE AND EN G YpA/,g1TAnGN FnIK] usNG THE v.FnEY. 10. miAl AREA iH15 Pui 2�61 Af1fL �121,A00 oe JNE 92FE OM FLIINO MONUAVNTATFGN FS IMENT GANEKR 12. TNERE WAS NO OSSERfED ENOEMLE a dlME21T EMTX EMINE W B N QOM➢ G CONS�NIUOnC11 OR SLII MR ADOIl10NR IS HEM WAS NO OB9ER1E0 EN0E2NCE THAT ME 911E HAS EEIII usm As A souo WASTE WMY, SiAP GP sAMrurr I ti. EA"MU- iosow.wN.G 2NFa1NATNpN aNOWn Pnce,uE FRw pNp/Mp 5UF AN ONE FOGY OMMUW MI VA IERTr•i OA1MM is NAV BY NRS OPS A TM M THE MNT OF CONMFNfF]LNT. 19. WTE CUIYI 1 ITIE NSURANOE GdIPANY, cd, -NT No. Ir0e0lOGN; ERYCInR: — NAula1 .. 2m O. 1 110T A MATIER OF SUNAEY. 3. WTTENS OF SINIEY 910'A1N HIOEON. * SEE 25' AM R04T OF WAY M OW Or p,AftMM AS RECOROEG IN MO. I&M PALE M3 RUNmii C ILL AL[tJ0 THE WESTEB N 510E a SU& PROPERTA' AND CENWBI ] ON SEWFH S1RIICNRES. QY G s. MTN ST. MOH1 aP WAY N104D AH6 EON14E1Ea M SIX MIM14 IWIMM W. RE9ERVNC A 10' i 2W R/Vf FOR SE/SFN, 23' RIV FOR SOCAR LAFF][ G11F" i 10' R/W fEFN MvEP MAN F 031. Y]OY PO. i01 �Q s W N MOIT OF ftv W OIrE POrea mwAerr FOP avreli / ]. & 111 6 P'SSM 2,� 9 OOE°6 NOOTr,J'1R�C,°A CT " HFAEON. 5W-1 I BGNT OF my FOR SPUR 1RAGA CONSINR AC Xv AOL£BS PM M. 1l PG AOS AND SNA01rN ,NFR6aH RUNNNG ADJACENT TO SUe,EOT F TY ALONG FWOPEFNTr MOM OW1NE0 eT LTY OF CINA `R-- A NEABEMENT APER FRL1A G2NTEN OF UJ SUGYf CNmc A5 FECOPOEO 0.B. WN, Po. 075 MR wANMNNKC Wb ACCESS OF SAID CREV 10. M F EASEIE"NoNi 1ANO Di 1lEF11SAS PE AM1 D.B.SS0 OE9tlNBm R1 O.1PAGE 70TN AFFECTSM PHOPFR"BUT 1S NOT I 11. NO PO NS OF TNT PROPERTY UE A NN THE MNN UK RANAOAO R TD M1. ,z BnN,s oT � RpA�AM. A.p yTryRAL R MAY A FTNPSRTT BUT ARE BLANKET IN NAT MID HOT KIYTTABLE. IS MDT A MATTER OF 5LWYET. PRELIMINARY DRAFT Source: Drawn by SUMMIT 11A& SUMMIT BG-1 Site Plan Southern Wipers Property 511 E 25th Street Property Charlotte, NC e SW-2 SS-2 �► �� SB-1 'SB-2 SBA♦+\,\ I O- SB ` A q9 Rg L• 'I I—T �• SB-4 SB-50 T,Tp` 01 I � SB-9 KEY . Groundwater Sample from existing Monitoring Well (MW) O Soil Boring Location O Surface Water and Sediment Sample Location GRAPHIC SCALE I tN tEC7 1 i Ira - ea rr_ Fountains at NoDa Holding, LLC 1420 East 7th Street, Suite 150 Charlotte, NC 28204 Prepared By\Date: PL/11/18 Checked By\Date: MZ/11/18 Scale As Shown Figure 2 Sail & Sediment Sample COC Fxceedances 50-32-8 7440-38-2 7440-47-3 18540-29-9 All Values in mg/kgOpY Benzo a rene Arsenic Chromium (total) Hexavalent Chromium PSRG- Residential 0.11 0.68 0.31 0.31 SB-1 BDL 4.4 91 BDL SB-2 0.11 4.4 31 BDL SB-3 BDL 1 52 BDL SB-4 BDL 1.1 82 BDL SB-5 BDL 1 96 0.54 SB-6 BDL 1.6 1301 1.2 SB-7 BDL 1.1 36 0.41 SB-8 BDL 0.73 60 0.61 SB-8 DUP BDL 0.66 59 0.6 SB-9 BDL 1.7 49 0.51 SB-10 BDL 240 55 2.9 BG-1 BDL 50 19 1.6 SS-1 BDL 0.85 85 BDL SS-1 DUP 0.15 0.61 20 BDL SS-2 BDLj 1.51 42 BDL All Soil Samples (SB/BG) collected from the 0-2' bgs interval - See Summary Tables for a list of all laboratory detections PRELIMINARY DRAFT Source: Drawn by SUMMIT 11A& SUMMIT a SS-2,—.. r _' SB-1 KEY A Monitoring Well (MW) 0 Soil Sample Location 0 Surface Water and Sediment Sample Location • I � ` ®OM 'SB-2 SB-3 \, r 01/ SBSIR ` I � �f SB-4 SB-5 SB BG-1 ♦ 9� � i�nw Soil/Sediment COC Map Southern Wipers Property 511 E 25th Street Property Charlotte, NC j / 1 SB-9 , , ♦ GRAPHIC SCALE Fountains at NoDa Holding, LLC 1420 East 7th Street, Suite 150 Charlotte, NC 28204 Prepared By\Date: PL/11/18 Checked By\Date: MZ/11/18 Scale As Shown Figure 3 Groundwater Sample COC Exceedances 71-43-2 159-59-2 79-01-6 75-01-4 7440-38-2 7440-47-3 18540-29-9 All S alu es in ug`L Benzene cis-1.2- Diclila•oethene Trichloroethene - inyl chlm•ide Arsenic Cbronllnn] (total) Hexat-alert Clu•mrumn NC 2L CrW Standards 1, 0 70 3, 0 003 10 10 10 ]b1W-17 BDL BDL BDL BDL 0.98 181 16 NEW-17 DUP BDL BDL 0.21 BDL 1.1 19 16 NEW-18 BDL 0.9.7 BDL 2.8 1.1 5, 4 1.4 NEW-19 1.2 91 43 2.4 1 7500 3900 ]41W-23 BDL BDL BDL BDL 1200 4 2.8 ]41W-24 BDL BDL BDLI BDLI 13 4,1 BDL ]�1W-25 BDLI B Ll BDLI BDLI BDLI 121 BDL See Srmvnary Tables for H list of all laboratory detections 90,EC 6 - 9EO N - Ex PWNS N01 A MATTER W 91 .. 2 NOT A MAi OF 91RAEY. S WTTERS W SlRi1Er 91011N HEPEON. * SEE 25' AIM R04T OF w Y r0 Ott OF pu1ROTM AS RECOROEO M MB. 1d PACE 313 WN1 ILL ALO<JO THE 1fiESTFItrI SIDE a SU&EOT PRCPERTI' AND Ov11ER6n ON SENFR STRIIONRES. S. MW ST. H T aF WAY aLOSSn A EON4s1Ea m SIXITIERN IKFEA3. W. RE9ERN A 10' i 2W "FOR SE1'RT. 23' RIV FOR 9OCAR CREEIf MWAli, a 10•"FOR "G MM PEN O.& Y]6Y PO. i0.1 A 91OAN HEIEON. s ea WN R r D ftv r0 d1tE PEYEII tO1PAHY FOR PEYEA TAANSMISSM]N RECONOEIf IN MO. 1002 P0. 243 AM0 SHOINI REASON. M DA 10 PALE N9 0 S NOT AFFECr SI CT PROPERTY. I R T OF my FOR S AiAdf L S�AC Rv0 PER 0.& 1l PG W AND 9N011N NERlON RONM% AO.N T W SO0 = PROPERTY KO PROPS T' NON OMIRD er an O CNARL - 9. NEASENMT APER F OEN OF UJ Sy OAR ONED( AS fECOROEO 0.B. ekw Po. 675 rM m+ NrCNNAmM W ACCESS OF SAO CREEL Surface Water Samnle COC F.xceedancec J1C� J � • I SW-1 i dop, 127-18-4 79-01-6 75-01-4 All Values in ug/L Tetrachloroethylene Trichloroethene Vinylchloride NC 2B SWQ Standards 0.7 2.5 0.025 SW-1 4.4 15 0.4 SW-1 DUP 4.8 15 0.37 SW-2 4.7 15 0.4 SW-2 was collected upstream of SW-1 See Summary Tables for a list of all laboratory detections PRELIMINARY DRAFT Source: Drawn by SUMMIT 11A& SUMMIT sT SW-2 r Groundwater/Surface Water COC Map Southern Wipers Property 511 E 25th Street Property Charlotte, NC KEY . Groundwater Sample from existing Monitoring Well (MW) O Surface Water and Sediment Sample Location MW- `.�2s�` W-24 GRAPHIC SCALE [wrae'rr Fountains at NoDa Holding, LLC 1420 East 7th Street, Suite 150 Charlotte, NC 28204 Prepared By\Date: PL/11/18 Checked By\Date: MZ/11/18 Scale As Shown Figure 4 VICINITY MAP - N.T.S. r'1 1. CIIRPEIIT TAX PAP{i1a AS IISTED" J x ALL ASTANOEY A 14pl2ONTAL Q 13 MTAAC IN OECYAL US SNfIFi FEET. �. N«r„ NAsn au rcD nrH »rs os t ARFiI BY Ca]eDwAn' : 1 .y r :. aA51En u Es PIOICRTE SWM13IN w^fxs we i. THESE PROP Vm MAY W SO a TO ACCTICNAL ,. ;' :. .� EASIICTITS OR Ma1TS CF MAY. e. EflllD Is I-Y PER MMN. M, WS. 9. SAFYEY IS OAS ON GL ENYElKE AHD Ei051wc • 'o MON im,m-- c nu sw�r" 1a TTfTAL AREA rHls PLAr x�ev Aars I,21,am Si .�H, �' . 11. M1PE Sgs pa FvurlD ILFUNENYAf,d, It ouraoE drreren. 12 n MN xA8 NO OBSFXrED ENOENLE of N BUN T G MONNC NGRN, fAAXINNC a)IISTHUM OR fM ADpi1011S. l• , % STM 19, MM MAS HD CBsERND ENDENCE THAT THE 911E HAS ifEN VSEO AS A SaA MASTE OUYP, 51AP OR SANITARY 1 f 1 / LAN7)FlW I5. RPU4FARXC TIFF TWR My PPODUCE FRW %u 9 S1R1Er oEc FOOT p]IM w ,ERir•i CA1'u B NAwee r y I F F:' BY T PONT T V I OP& AND BIM m 1HE POINT OF .__�_ WPA 1a nnE MINT IYQlI 6Y f%NCA06 nn.E WSURAHf9' 0.^APANv. LOM,HTMO0 eo. tN; n,ecllre OATe M„RCH .� xa,a • i! : . %r� CTM 0 41 NOT A B - SEcnpl N - EFLEPlIDNB I. NOT A MA1TEl+ W SYDVET. x NOT A IMTIEA OF 9OIIVEY 1 ]. MATTERS SI M*T stow nEHEOH. 4. SEE 33' WON OF ro ptt OF puR{pr1E AS RE WI W f + w C.B" fe11 PACE .AN IelNlrlC ALL ALWC nc AE mff SIDE 0< IIM M OF SL PNO AND cF/!lt)vE]] ON �XER STPDLIO AT S. mart CF MAY AHC fSIEXYEL m SOOIHEMH WPEAS, 3. Srr m M' WC HEORNNC A 1I ! 25' R/Yf FOR 9E'AER, L DO. 27 91lCAR WQ 25' (FED[ IXRFALL, R 17 RJM FOR MAIQt 11AF PER D.B. ?TEP P0. 1W s 1 AHD SHCw HETff 6. 6C PChER ION CF MAT m O PCIETf L243 S` f . AND S14 TRAElSI� PA PEWAOED IN r 1904 PR '1�] AND SHO'M! HFREOIL N96NS I i. O.& OF PACE R DOEL Nor AFFECT UCVOCT PROPFRtt. L. R.0. Lf Nx1T FOR EPHR lllApf LDHSTPuOWNI At T PER PF 13 Y PO. G A/q SINNN HEREON RBY a OFf A1T To 9UB.eCi EPa'EDTT AT PDOR T' NOpf O Dr att OF CHUKhS { f \\ ' r' Zo, AN 91CM1 PIEER As 9. DO' ERSEYZHi MEA INCEI CENTER F J O 4, A AN 011M .I p.rt. ePD. Pa. an rcF HAX1IEHANCE AND Access OF SAC CY4EN NONN AND Shaw MID f . J, AW 16 EA9E11E/ii AIN N10 7M Di IN0 PETLSAL AS PE�RVB ANC OE N 0.9. 1]]SO PACE iN AFFECTS PRL'PFRtt BUT IS HOT 11. NO POIICF 1HI8 PROPERtt uE N11W/ 111E MAIN UKRAeROAO i 1�_ DHiTT OF OF AFFE INT T M DPASRN, AND ur,CDAL MAT CT D�D ,2 HHTs of ARE PRDPERTI' DDT APE el.AfacET IN HAINIE AND DNU NU PIARABIE. / Py'J\TI/I IZ NOT A MATTER OF SURVEY. \ J \ \ 3 PRELIMINARY DRAFT Source: Drawn by SUMMIT 11AA& SUMMIT Potentiometric Map Southern Wipers Property 511 E 25th Street Property Charlotte, NC Far KEY Groundwater Table 2 ft Elevation Contour ,i 0 • % \ 23 � L L V ` GRAPHIC SCALE ^ { IN F6Sf ] T mob_ eo a Prepared By\Date: PL/11/18 Checked By\Date: MZ/11/18 Fountains NoDa Holding, LLC 1420 East 7th Street, Suite 150 Scale Charlotte, NC 28204 1 As Shown Figure 5 Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 APPENDIX II TABLES DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\Appendix II.rtf Page 1 of 10 Table 1: Well Construction Summary Monitoring Well ID Installation Date Casing Diameter (inches) Well Material Total Depth (feet) Cased Interval (feet bgs) Screened Interval (feet bgs) MW-17 10/19/2000 2 PVC 20 0.0-5.0 5.0-20.0 MW-18 10/19/2000 2 PVC 20 0.0-5.0 5.0-20.0 MW-19 10/19/2000 2 PVC 20 0.0-5.0 5.0-20.0 MW-20 4/17/2006 Well Not Located MW-21 4/17/2006 Well Not Located MW-23 2/9/2007 2 PVC 13 0.0-3.0 3.0-13.0 MW-24 2/8/2007 2 PVC 13 0.0-3.0 3.0-13.0 MW-25 6/5/2007 2 PVC 20 0.0-10.0 10.0-20.0 Notes: bgs = below ground surface Well Construction Details obtained from 2011 Monitoring Report of the Former Applied Research Group, Inc. Site Total Depth and construciton materials confirmed in the field by SUMMIT on 9/20/18 Table 2: Groundwater Elevation Data Monitoring Well ID Top of Casing Elevation (ft MSL) Date Measured Depth to Groundwater (ft bgs) Groundwater Elevation (ft MSL) MW-17 661.93 9/21/2018 2.76 659.17 MW-18 658.44 9/21/2018 9.40 649.04 MW-19 659.31 9/21/2018 10.20 649.11 MW-20 Well Not Located MW-21 Well Not Located MW-23 660.23 9/21/2018 2.31 657.92 MW-24 659.79 9/21/2018 9.14 650.65 MW-25 660.40 9/21/2018 9.45 650.95 Notes: bgs = below ground surface * = Top of Casin Elevations obtained from 2011 Monitoring Report of the Former Applied Research Group, Inc. Site MSL = Elevation above Mean Seal Level Southern Wipers October 2, 2019 Charlotte, NC SUMMIT Project No: 3586.01 Page 2 of 10 All Values in mg/kg CAS VOC Analyte 67-64-1 Acetone 67-66-3 Chloroform 127-18-4 Tetrachloroethylene 79-01-6 Trichloroethylene CAS SVOC Analyte 56-55-3 Benzo(a)anthracene 50-32-8 Benzo(a)pyrene 205-99-2 Benzo(b)fluoranthene 191-24-2 Benzo(g,h,i)perylene 65-85-0 Benzoic Acid 206-44-0 Fluoranthene 129-00-0 Pyrene CAS Metals 7440-38-2 Arsenic 16065-83-1 Chromium (III)** 18540-29-9 Chromium (VI) 7439-92-1 Lead 7439-97-6 Mercury 7440-22-4 Silver 7440-39-3 Barium 7440-43-9 Cadmium Table 3: Soil Sample Detection Summary Table SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-7 DEQ Reference Values 9/21/2018 9/21/2018 9/21/2018 9/21/2018 9/21/2018 9/21/2018 9/21/2018 0-2' bgs 0-2' bgs 0-2' bgs 0-2' bgs 0-2' bgs 0-2' bgs 0-2' bgs Protection PSRG-Res of GW Result MDL Result MDL Result MDL Result MDL Result MDL Result MDL Result MDL 1.20E+04 2.50E+01 0.091 J 0.091 0.059 J 0.025 0.062 J 0.022 0.042 J 0.023 0.034 J 0.025 0.099 J 0.025 0.031 J 0.021 3.40E-01 3.90E-01 BDL 0.0006 BDL 0.0076 BDL 0.0006 0.0035 J 0.0007 BDL 0.0007 BDL 0.0008 BDL 0.0006 1.70E+00 6.30E-03 BDL 0.0012 BDL 0.0014 0.0031 0.0012 BDL 0.0013 BDL 0.0014 BDL 0.0014 BDL 0.0014 8.70E-01 2.10E-02 BDL 0.0009 BDL 0.0011 BDL 0.0009 BDL 0.001 BDL 0.0011 BDL 0.0011 0.0011 J 0.0009 Protection PSRG-Res of GW Result MDL Result MDL Result MDL Result MDL Result MDL Result MDL Result MDL 1.10E+00 3.50E-01 BDL 0.052 0.068 J 0.056 BDL 0.052 BDL 0.056 BDL 0.057 BDL 0.057 BDL 0.057 1.10E-01 1.20E-01 BDL 0.061 0.11 J 0.066 BDL 0.062 BDL 0.066 BDL 0.067 BDL 0.067 BDL 0.067 1.10E+00 1.20E+00 0.073 J 0.052 0.13 J 0.06 BDL 0.056 BDL 0.06 BDL 0.061 BDL 0.061 BDL 0.061 NA I 1.56E+04 BDL 0.087 0.1 J 0.094 BDL 0.087 BDL 0.093 BDL 0.095 BDL 0.095 BDL 0.095 5.10E+04 1.20E+02 BDL 0.21 BRL 0.23 BDL 0.21 BDL 0.23 BDL 0.23 BDL 0.23 BDL 0.23 4.80E+02 6.70E+02 0.071 J 0.065 0.086 J 0.07 BDL 0.065 BDL 0.07 BDL 0.071 BDL 0.071 BDL 0.071 3.60E+02 4.40E+02 BDL 0.065 0.1 J 0.07 BDL 0.065 BDL 0.07 BDL 0.071 BDL 0.071 BDL 0.071 Protection PSRG-Res of GW Result MDL Result MDL Result MDL Result MDL Result MDL Result MDL Result MDL 6.80E-01 5.80E+00 0.032 0.035 1 0.03 1.1 0.033 1 0.035 1.6 0.034 1.1 0.034 2.30E+04 3.60E+05 91 0.69 31 0.19 52 0.17 82 0.18 95.46 0.19 128.8 0.74 35.59 0.19 3.10E-0I 3.80E+00 BDL 0.23 BDL 0.097 BDL 0.09 BDL 0.098 0.54 0.1 1.2 0.1 0.41 0.1 NA 2.70E+02 25 0.063 22 0.069 17 0.061 10 0.067 10 0.07 9.5 0.068 7.5 0.069 2.30E+00 1.00E+00 0.036 0.0029 0.042 0.0032 0.039 0.0029 0.042 0.003 0.063 0.0031 0.061 0.0031 0.036 0.0034 7.80E+01 3.40E+00 0.091 0.0031 0.052 J 0.0034 0.038 J 0.003 0.12 0.0033 0.096 0.0034 0.091 0.0033 0.05 J 0.0033 3.10E+03 5.80E+02 120 1.6 63 0.43 78 0.38 120 1.7 90 0.44 110 1.7 100 0.43 1.40E+01 3.00E+00 0.42 0.012 0.049 J 0.013 BDL 0.012 BDL 0.013 BDL 0.014 BDL 0.013 BDL 0.013 BDL = Below Detection Limit J = Estimated Concentration MDL = Lab Detection Limit BOLD = Concentration Above Reference Values NT = Not Tested I = PSRG Appendix A Table ** -Chromium Speciation - Chromium (III) determined by subtracting Chromium (VI) from Total Chromium (7440-47-3) reported in analaytical reports Southern Wipers October 2, 2019 Charlotte, NC SUMMIT Project No: 3586.01 Page 3 of 10 All Values in mg/kg CAS VOC Analyte 67-64-1 Acetone 67-66-3 Chloroform 127-184 Tetrachloroethylene 79-01-6 Trichloroethylene CAS SVOC Analyte 56-55-3 Benzo(a)anthracene 50-32-8 Benzo(a)pyrene 205-99-2 Benzo(b)fluoranthene 191-24-2 Benzo(g,h,i)perylene 65-85-0 Benzoic Acid 206-44-0 Fluoranthene 129-00-0 Pyrene CAS Metals 7440-38-2 Arsenic 16065-83-1 Chromium (III)** 18540-29-9 Chromium (VI) 7439-92-1 Lead 7439-97-6 Mercury 7440-22-4 Silver 7440-39-3 Barium 7440-43-9 Cadmium Table 3: Soil Sample Detection Summary Table (continued) SB-8 SB-8 DUP SB-9 SB-10 BG-1 DEQ Reference Values 9/21/2018 9/21/2018 9/21/2018 9/21/2018 9/25/2018 0-2' bgs 0-2' bgs 0-2' bgs 0-2' bgs 0-2' bgs Protection PSRG-Res of GW Result MDL Result MDL Result MDL Result DL Result MDL 1.20E+04 2.50E+01 0.047 J 0.021 0.045 J 0.022 0.034 J 0.023 0.026 J 0.026 NT 3.40E-01 3.90E-01 BDL 0.0006 BDL 0.0007 BDL 0.0007 BDL 0.0008 NT 1.70E+00 6.30E-03 BDL 0.0012 BDL 0.0012 BDL 0.0013 BDL 0.0014 NT 8.70E-01 2.10E-02 BDL 0.0009 BDL 0.001 BDL 0.001 BDL 0.0011 NT Protection PSRG-Res of GW Result MDL Result DL Result MDL Result MDL Result MDL 1.10E+00 3.50E-01 BDL 0.051 BDL 0.052 BDL 0.055 BDL 0.06 NT 1.10E-01 1.20E-01 BDL 0.061 BDL 0.061 BDL 0.065 BDL 0.071 NT 1.10E+00 1.20E+00 BDL 0.055 BDL 0.055 0.65 J 0.059 0.13 J 0.064 NT NA I 1.56E+04 BDL 0.086 BDL 0.086 BDL 0.092 BDL 0.1 NT 5.10E+04 1.20E+02 BDL 0.21 BDL 0.21 BDL 0.22 0.32 J 0.24 NT 4.80E+02 6.70E+02 BDL 0.064 BDL 0.064 0.094 J 0.069 BDL 0.075 NT 3.60E+02 4.40E+02 BDL 0.064 BDL 0.064 0.082 J 0.069 0.082 J 0.075 NT Protection PSRG-Res of GW Result MDL Result MDL Result MDL Result MDL Result MDL 6.80E-01 5.80E+00 0.73 0.032 0.66 0.03 1.7 0.033 240 0.14 50 0.038 2.30E+04 3.60E+05 59.39 0.17 58.4 0.17 48.49 0.18 52.1 0.19 17.4 0.21 3.10E-0I 3.80E+00 0.61 0.1 0.6 0.091 0.51 0.09 2.9 0.1 1.6 0.11 NA 2.70E+02 11 0.064 8.1 0.061 15 0.066 19 0.07 4.9 0.077 2.30E+00 1.00E+00 0.03 0.0029 0.028 0.0027 0.042 0.0031 0.019 J 0.0034 0.0057 J 0.0034 7.80E+01 3.40E+00 0.087 0.0031 0.071 J 0.003 0.059 J 0.0032 0.038 J 0.0034 0.026 J 0.0037 3.10E+03 5.80E+02 92 0.39 110 1.5 140 1.6 46 0.44 76 0.48 1.40E+01 3.00E+00 0.016 J 0.012 BDL 0.012 BDL 0.013 0.8 0.014 0.12 0.015 BDL = Below Detection Limit J = Estimated Concentration MDL = Lab Detection Limit BOLD = Concentration Above Reference Values NT = Not Tested I = PSRG Appendix A Table ** -Chromium Speciation - Chromium (III) determined by subtracting Chromium (VI) from Total Chromium (7440-47-3) reported in analaytical reports Southern Wipers October 2, 2019 Charlotte, NC SUMMIT Project No: 3586.01 Page 4 of 10 All Values in ug/L CAS VOC Analyte 71-43-2 Benzene 67-66-3 Chloroform 106-46-7 1,4-Dichlorobenzene 159-59-2 cis-1,2-Dichloroethene 156-59-2 trans-1,2-Dichloroethene 108-20-3 Diisopropyl Ether (DIPE) 163-04-4 Methyl tert-Butyl Ether (MTBE) 91-20-3 Naphthalene 994-05-8 tert-Amyl Methyl Ether (TAME) 79-01-6 Trichloroethene 75-01-4 Vinyl chloride CAS SVOC Analyte All SVOC Compounds CAS Metals 7440-38-2 Arsenic 7440-39-3 Barium 7440-47-3 Chromium 7439-92-1 Lead 7439-97-6 Mercury 18540-29-9 Hexavalent Chromium Table 4: Groundwater Sample Detection Summary Table MW-17 MW-17 DUP MW-18 MW-19 MW-23 DEQ Reference Values 9/21/2018 9/21/2018 9/21/2018 9/21/2018 9/21/2018 NC 2L Groundwater Standards Result MDL Result MDL Result MDL Result MDL Result MDL 1.00E+00 BDL 0.12 BDL 0.12 BDL 0.12 1.2 0.12 BDL 0.12 7.00E+01 BDL 0.22 BDL 0.22 BDL 0.22 0.64 J 0.22 BDL 0.22 6.00E+00 BDL 0.15 BDL 0.15 BDL 0.15 1.9 0.15 BDL 0.15 7.00E+01 BDL 0.15 BDL 0.15 0.97 J 0.15 91 0.15 BDL 0.15 1.00E+02 BDL 0.15 BDL 0.15 1.8 0.15 17 0.15 BDL 0.15 NE BDL 0.18 BDL 0.18 0.34 J 0.18 0.41 J 0.18 BDL 0.18 2.00E+01 BDL 0.09 BDL 0.09 1.4 0.09 3.2 0.09 BDL 0.09 6.00E+00 BDL 0.12 BDL 0.12 BDL 0.12 0.25 J 0.12 BDL 0.12 I 1.28E+02 BDL 0.11 BDL 0.11 0.45 J 0.11 0.87 0.11 BDL 0.11 3.00E+00 BDL 0.2 0.21 J 0.2 BDL 0.2 43 0.2 BDL 0.2 3.00E-02 BDL 0.13 BDL 0.13 2.8 0.13 2.4 0.13 BDL 0.13 NC 2L Groundwater Standards Result MDL Result MDL Result MDL Result MDL Result MDL BDL BDL BDL BDL BDL NC 2L Groundwater Standards Result MDL Result MDL Result MDL Result MDL Result MDL 1.00E+01 0.98 0.72 1.1 0.72 1.1 0.72 1 0.72 1200 0.72 7.00E+02 56 11 57 11 300 11 53 11 25 II 1.00E+01 18 1 19 1 5.4 1 7500 1 4 1 1.50E+01 BDL 0.28 BDL 0.28 1.2 J 0.28 BDL 0.28 BDL 0.28 1.00E+00 0.034 J 0.034 BDL 0.034 BDL 0.034 0.039 J 0.034 BDL 0.034 1.00E+01 16 1 16 1 1.4 J 1 3900 1 2.8 J 1 BDL = Below Detection Limit J = Estimated Concentration MDL = Lab Detection Limit BOLD = Concentration Above Reference Values NT = Not Tested NE = Regulatory Concentration Not Established at this time Southern Wipers Charlotte, NC October 2, 2019 SUMMIT Project No: 3586.01 Page 5 of 10 All Values in ug/L CAS VOC Analyte 71-43-2 Benzene 67-66-3 Chloroform 106-46-7 1,4-Dichlorobenzene 159-59-2 cis-1,2-Dichloroethene 156-59-2 trans-1,2-Dichloroethene 108-20-3 Diisopropyl Ether (DIPE) 163-04-4 Methyl tert-Butyl Ether (MTBE) 91-20-3 Naphthalene 994-05-8 tert-Amyl Methyl Ether (TAME) 79-01-6 Trichloroethene 75-01-4 Vinyl chloride CAS SVOC Analyte All SVOC Compounds CAS Metals 7440-38-2 Arsenic 7440-39-3 Barium 7440-47-3 Chromium 7439-92-1 Lead 7439-97-6 Mercury 18540-29-9 Hexavalent Chromium Table 4: Groundwater Sample Detection Summary Table (continued) MW-24 MW-25 Trip Blank Field Blank DEQ Reference Values 9/21/2018 9/21/2018 9/25/2018 9/25/2018 NC 2L Groundwater Standards Result MDL Result MDL Result MDL Result MDL 1.00E+00 BDL 0.12 BDL 0.12 BDL 0.12 BDL 0.12 7.00E+01 BDL 0.22 0.27 J 0.22 BDL 0.22 BDL 0.22 6.00E+00 BDL 0.15 BDL 0.15 1.1 0.15 0.69 J 0.15 7.00E+01 BDL 0.15 BDL 0.15 BDL 0.15 BDL 0.15 1.00E+02 BDL 0.15 BDL 0.15 BDL 0.15 BDL 0.15 NE BDL 0.18 BDL 0.18 BDL 0.18 BDL 0.18 2.00E+01 BDL 0.09 BDL 0.09 BDL 0.09 BDL 0.09 6.00E+00 BDL 0.12 BDL 0.12 BDL 0.12 BDL 0.12 I 1.28E+02 BDL 0.11 BDL 0.11 BDL 0.11 BDL 0.11 3.00E+00 BDL 0.2 BDL 0.2 BDL 0.2 BDL 0.2 3.00E-02 BDL 0.13 BDL 0.13 BDL 0.13 BDL 0.13 NC 2L Groundwater Standards Result MDL Result MDL Result MDL Result MDL BDL BDL NT BDL NC 2L Groundwater Standards Result MDL Result MDL Result MDL Result MDL 1.00E+01 13 0.72 BDL 0.72 NT BDL 0.72 7.00E+02 18 J 11 27 11 NT BDL 11 1.00E+01 4.1 1 1.2 J 1 NT BDL 1 1.50E+01 0.31 J 0.28 1.2 J 0.28 NT BDL 0.28 1.00E+00 BDL 0.034 0.035 J 0.034 NT BDL 0.034 1.00E+01 BDL 1 BDL 1 NT BDL 1 BDL = Below Detection Limit J = Estimated Concentration MDL = Lab Detection Limit BOLD = Concentration Above Reference Values NT = Not Tested NE = Regulatory Concentration Not Established at this time Southern Wipers Charlotte, NC October 2, 2019 SUMMIT Project No: 3586.01 Page 6of10 Table 5: Sediment Sample Detection Summary Table All Values in mg/kg CAS VOC Analyte 106-46-7 1,4-Dichlorobenzene 79-01-6 Trichloroethylene CAS SVOC Analyte 56-55-3 Benzo(a)anthracene 50-32-8 Benzo(a)pyrene 205-99-2 Benzo(b)fluoranthene 207-08-9 Benzo(k)fluoranthene 191-24-2 Benzo(g,h,i)perylene 85-68-7 Butylbenzylphthalate 218-01-9 Chrysene 206-44-0 Fluoranthene 91-57-6 2-Methylnaphthalene 85-01-8 Phenanthrene 129-00-0 Pyrene CAS Metals 7440-38-2 Arsenic 16065-83-1 Chromium (III)** 18540-29-9 Chromium (VI) 7439-92-1 Lead 7439-97-6 Mercury 7440-22-4 Silver 7440-39-3 Barium 7440-43-9 Cadmium SS-1 SS-1 Dup SS-2 DEQ Reference Values 9/25/2018 9/25/2018 9/25/2018 Protection PSRG-Res of GW Result MDL Result MDL Result MDL 2.80E+00 1.20E-01 0.002 J 0.0009 BDL 0.0008 BDL 0.0008 8.70E-01 2.10E-02 0.0015 J 0.0011 BDL 0.001 BDL 0.001 Protection PSRG-Res of GW Result MDL Result MDL Result MDL 1.10E+00 3.50E-01 BDL 0.058 0.15 J 0.056 BDL 0.053 1.10E-01 1.20E-01 BDL 0.068 0.15 J 0.066 BDL 0.063 1.10E+00 1.20E+00 BDL 0.062 0.23 0.06 BDL 0.057 1.10E+01 1.20E+01 BDL 0.068 0.12 J 0.066 BDL 0.063 NA I 1.56E+04 BDL 0.097 0.087 J 0.094 BDL 0.089 2.90E+02 2.90E+02 BDL 0.1 3.3 0.1 BDL 0.096 1.10E+02 3.60E+01 BDL 0.068 0.21 J 0.066 BDL 0.063 4.80E+02 6.70E+02 BDL 0.072 0.46 0.07 0.092 J 0.067 4.80E+01 3.10E+00 BDL 0.076 0.075 J 0.074 BDL 0.07 NA I 1.34E+02 BDL 0.11 0.19 J 0.11 BDL 0.1 3.60E+02 4.40E+02 BDL 0.072 0.46 0.07 0.094 0.067 Protection PSRG-Res of GW Result MDL Result MDL Result MDL 6.80E-01 5.80E+00 0.85 0.036 0.61 0.036 1.5 0.034 2.30E+04 3.60E+05 85 0.2 20 0.19 42 0.18 3.10E-01 3.80E+00 BDL 0.1 BDL 0.025 BDL 0.1 NA 2.70E+02 4.6 0.072 3.8 0.071 6.1 0.067 2.30E+00 1.00E+00 0.0039 J 0.0031 0.0089 0.0032 0.0048 0.003 7.80E+01 3.40E+00 0.022 J 0.0035 0.014 0.0035 0.02 0.0033 3.10E+03 5.80E+02 39 0.44 16 0.44 18 0.42 1.40E+01 3.00E+00 BDL 0.014 0.02 0.014 0.018 J 0.013 BDL = Below Detection Limit J = Estimated Concentration MDL = Lab Detection Limit BOLD = Concentration Above Reference Values NT = Not Tested I = PSRG Appendix A Table ** -Chromium Speciation - Chromium (III) determined by subtracting Chromium (VI) from Total Chromium (7440-47-3) reported in analaytical reports Southern Wipers Charlotte, NC October 2, 2019 SUMMIT Project No: 3586.01 Page 7 of 10 Table 6: Surface Water Sample Detection Summary Table All Values in ug/L CAS VOC Analyte 106-46-7 1,4-Dichlorobenzene 75-35-4 1, 1 -Dichloroethylene 159-59-2 cis-1,2-Dichloroethene 156-59-2 trans-1,2-Dichloroethene 163-04-4 Methyl tert-Butyl Ether (MTBE) 127-18-4 Tetrachloroethylene 79-01-6 Trichloroethene 75-01-4 Vinyl chloride CAS SVOC Analyte All SVOC Compounds CAS Metals 7440-39-3 Barium SW-1 SW-1 Dup SW-2 DEQ Reference Values 9/25/2018 9/25/2018 9/25/2018 NCAC 2B SWQ Standards Result MDL Result MDL Result MDL 4.88E+02 0.96 J 0.15 0.87 J 0.15 0.93 J 0.15 02L* 3.50E+02 BDL 0.16 BDL 0.16 0.24 J 0.21 02L* 7.00E+01 6.8 0.15 7.3 J 0.15 7.4 0.15 02L* 1.00E+02 0.25 J 0.15 0.18 0.15 BDL 0.15 02L* 2.00E+01 0.62 J 0.09 0.66 J 0.09 0.58 J 0.09 7.00E-01 4.4 0.27 4.8 0.27 4.7 0.27 2.50E+00 15 0.2 15 0.2 15 0.2 2.50E-02 0.4 J 0.13 0.37 J 0.13 0.4 J 0.13 NCAC 2B SWQ Standards Result MDL Result MDL Result MDL BDL BDL BDL NCAC 2B SWQ Standards Result MDL Result MDL Result MDL 1.00E+03 48 11 52 J 11 50 11 BDL = Below Detection Limit J = Estimated Concentration MDL = Lab Method Detection Limit BOLD = Concentration Above Reference Values NCAC 2B SWQ Standards - NC 15A NCAC 02B Water Qulaity Standards for Surface Waters - September 2017 02L* - NCAC 02L Groundwater Standards utilized when surface water standards were not established. Southern Wipers October 2, 2019 Charlotte, NC SUMMIT Project No: 3586.01 Page 8 of 10 All Values in ug/L CAS VOC Analyte 71-43-2 Benzene 67-66-3 Chloroform 106-46-7 1,4-Dichlorobenzene 159-59-2 cis-1,2-Dichloroethene 156-59-2 trans-1,2-Dichloroethene 108-20-3 Diisopropyl Ether (DIPE) 163-04-4 Methyl tert-Butyl Ether (MTBE) 91-20-3 Naphthalene 994-05-8 tert-Amyl Methyl Ether (TAME) 79-01-6 Tichloroethene 75-01-4 Vinyl chloride CAS SVOC Analyte All SVOC Compounds Table 7: Groundwater Vapor Intrusion Screening Comparison Table DEQ Reference Values DWM Residential Vapor Intrusion GW Screening MW-17 9/21/2018 Result MDL MW-17 DUP 9/21/2018 Result MDL MW-18 9/21/2018 Result MDL MW-19 9/21/2018 Result MDL MW-23 9/21/2018 Result MDL 1.60E+01 BDL 0.12 BDL 0.12 BDL 0.12 1.2 0.12 BDL 0.12 8.40E+00 BDL 0.22 BDL 0.22 BDL 0.22 0.64 J 0.22 BDL 0.22 2.60E+01 BDL 0.15 BDL 0.15 BDL 0.15 1.9 0.15 BDL 0.15 NE BDL 0.15 BDL 0.15 0.97 J 0.15 91 0.15 BDL 0.15 NE BDL 0.15 BDL 0.15 1.8 0.15 17 0.15 BDL 0.15 1.40E+03 BDL 0.18 BDL 0.18 0.34 J 0.18 0.41 J 0.18 BDL 0.18 4.50E+03 BDL 0.09 BDL 0.09 1.4 0.09 3.2 0.09 BDL 0.09 3.50E+01 BDL 0.12 BDL 0.12 BDL 0.12 0.25 J 0.12 BDL 0.12 NE BDL 0.11 BDL 0.11 0.45 J 0.11 0.87 0.11 BDL 0.11 1.00E+00 BDL 0.2 0.21 J 0.2 BDL 0.2 43 0.2 BDL 0.2 1.50E+00 BDL 0.13 BDL 0.13 2.8 0.13 2.4 0.13 BDL 0.13 DWM Residential Vapor Intrusion GW Screening Result MDL Result MDL Result MDL Result MDL Result MDL BDL I BDL I BDL I BDL I BDL BDL = Below Detection Limit J = Estimated Concentration MDL = Lab Detection Limit BOLD = Concentration Above Reference Values NT = Not Tested NE = Regulatory Concentration Not Established at this time February 2018 - DWM Residential VISLs utiltized Southern Wipers Charlotte, NC October 2, 2019 SUMMIT Project No: 3586.01 Page 9 of 10 Table 7: Groundwater Vapor Intrusion Screening Comparison Table (continued) All Values in ug/L CAS VOC Analyte 71-43-2 Benzene 67-66-3 Chloroform 106-46-7 1,4-Dichlorobenzene 159-59-2 cis-1,2-Dichloroethene 156-59-2 trans-1,2-Dichloroethene 108-20-3 Diisopropyl Ether (DIPE) 163-04-4 Methyl tert-Butyl Ether (MTBE) 91-20-3 Naphthalene 994-05-8 tert-Amyl Methyl Ether (TAME) 79-01-6 Tichloroethene 75-01-4 Vinyl chloride CAS SVOC Analyte All SVOC Compounds DEQ Reference Values DWM Residential Vapor Intrusion GW Screening MW-24 9/21/2018 Result MDL MW-25 9/21/2018 Result MDL Trip Blank 9/25/2018 Result MDL Field Blank 9/25/2018 Result MDL 1.60E+01 BDL 0.12 BDL 0.12 BDL 0.12 BDL 0.12 8.40E+00 BDL 0.22 0.27 J 0.22 BDL 0.22 BDL 0.22 2.60E+01 BDL 0.15 BDL 0.15 1.1 0.15 0.69 J 0.15 NE BDL 0.15 BDL 0.15 BDL 0.15 BDL 0.15 NE BDL 0.15 BDL 0.15 BDL 0.15 BDL 0.15 1.40E+03 BDL 0.18 BDL 0.18 BDL 0.18 BDL 0.18 4.50E+03 BDL 0.09 BDL 0.09 BDL 0.09 BDL 0.09 3.50E+01 BDL 0.12 BDL 0.12 BDL 0.12 BDL 0.12 NE BDL 0.11 BDL 0.11 BDL 0.11 BDL 0.11 1.00E+00 BDL 0.2 BDL 0.2 BDL 0.2 BDL 0.2 1.50E+00 BDL 0.13 BDL 0.13 BDL 0.13 BDL 0.13 DWM Residential Vapor Intrusion GW Screening lResult MDL Result MDL Result MDL Result MDL BDL I BDL I NT I BDL BDL = Below Detection Limit J = Estimated Concentration MDL = Lab Detection Limit BOLD = Concentration Above Reference Values NT = Not Tested NE = Regulatory Concentration Not Established at this time February 2018 - DWM Residential VISLs utiltized Southern Wipers Charlotte, NC October 2, 2019 SUMMIT Project No: 3586.01 Page 10 of 10 Table 8: Historical Groundwater COCs Summary Table All Values in ug/L Sample Date* 71-43-2 159-59-2 79-01-6 75-014 7440-38-2 7440-47-3 18540-29-9 Benzene cis-1,2- Dichloroethene Trichloroethene Vinyl chloride Arsenic Chromium total Hexavalent Chromium NC 2L GW Standards 1.0 70 3.0 0.03 10 10 10 MW-17 Duplicate 4/20/2009 150.0 BDL BDL BDL BDL BDL BDL 4/21/2010 BDL BDL BDL BDL 8.1 12 BDL 4/29/2011 BDL BDL BDL BDL BDL 11 BDL 9/21/2018 BDL BDL BDL BDL 0.98 18 16 9/21/2018 BDL BDL 0.21 BDL 1.1 19 16 MW-18 4/20/2009 BDL BDL BDL 5 BDL BDL BDL 4/21/2010 1.4 BDL BDL 17 BDL 18 BDL 4/29/2011 BDL BDL BDL 3.9 BDL BDL BDL 9/21/2018 BDL 0.97 BDL 2.8 1.1 5.4 1.4 M"'-19 4/20/2009 3 470 1600 12 BDL 12000 12000 4/21/2010 <50 570 1200 <50 BDL 12000 12000 9/21/2018 1.2 91 43 2.4 1 7500 3900 7723 4/20/2009 BDL BDL BDL BDL 1100 BDL BDL 4/21/2010 NA BDL BDL BDL 1300 BDL BDL 4/29/2011 BDL BDL BDL BDL 1200 BDL BDL 9/21/2018 BDL BDL BDL BDL 1200 4 2.8 MW-24 4/20/2009 BDL BDL BDL BDL 1.1 BDL1 BDL 4/21/2010 NA BDL 1.2 BDL 1.5 10 11 4/29/2011 BDL BDL BDL BDL 2.1 16 BDL 9/21/2018 BDL BDL BDL BDL 13 4.1 BDL MW-25 4/20/2009 BDL BDL BDL BDL 40000 46 22 4/21/2010 NAI BDLI BDLI BDL 1.5 10 37 4/29/20111 BDLI BDLJ BDLI BDL 201 18 11 9/21/20181 BDLJ BDLJ BDLI BDLJ BDLJ 1.21 BDL Notes: bgs = below ground surface * = Historical sample results obtained from 2011 Monitoring Report of the Former Applied Research Group, Inc. Site Southern Wipers October 2, 2019 Charlotte, NC SUMMIT Project No: 3586.01 Brownfields Phase II ESA —Southern Wipers SUMMIT Project No. 3586.01 Charlotte, Mecklenburg County, North Carolina October 2, 2019 APPENDIX III ANALYTICAL RESULTS DAProject Forms\Projects\3586.01 Southem Wipers - Brownfields\Phase II Report Docs\10-2-19 Rev Docs\Appendix III.rtf icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 October 2, 2018 Patrick Lowery Summit Engineering 3575 Centre Circle Drive Fort Mill, SC 29715 Project Location: 511 East 25th Street, Charlotte, NC Client Job Number: Project Number: 3586.01 Laboratory Work Order Number: 18I1008 Enclosed are results of analyses for samples received by the laboratory on September 21, 2018. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Page 1 of 159 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 18I1008-01 18I1008-02 18I1008-03 1811008-04 1811008-05 1811008-06 1811008-07 1811008-08 1811008-09 18I1008-10 1811008-11 1811008-12 1811008-13 1811008-14 1811008-15 18I1008-16 18I1008-17 1811008-18 Sample Preparation Information QC Data Volatile Organic Compounds by GC/MS B213199 4 7 11 11 17 23 29 35 41 47 53 59 65 71 77 83 89 95 101 107 113 119 122 122 122 Page 2 of 159 Table of Contents Table of Contents (continued) B213538 Semivolatile Organic Compounds by GUMS B213246 B213417 Metals Analyses (Total) B213358 B213569 B213692 B213733 Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) B213102 B213410 B213636 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 126 132 132 136 142 142 142 142 143 145 145 145 145 146 147 155 Page 3 of 159 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Summit Engineering 3575 Centre Circle Drive REPORT DATE: 10/2/2018 Fort Mill, SC 29715 PURCHASE ORDER NUMBER: ATTN: Patrick Lowery PROJECT NUMBER: 3586.01 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18I1008 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 511 East 25th Street, Charlotte, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB SB-1 18I1008-01 Soil SM 254OG SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D SB-2 18I1008-02 Soil SM 254OG SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D SB-3 18I1008-03 Soil SM 254OG SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D SB-4 18I1008-04 Soil SM 254OG SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D SB-5 18I1008-05 Soil SM 254OG SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D SB-6 18I1008-06 Soil SM 254OG SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D Page 4 of 159 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Summit Engineering 3575 Centre Circle Drive REPORT DATE: 10/2/2018 Fort Mill, SC 29715 PURCHASE ORDER NUMBER: ATTN: Patrick Lowery PROJECT NUMBER: 3586.01 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18I1008 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 511 East 25th Street, Charlotte, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB SB-7 18I1008-07 Soil SM 254OG SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D SB-8 18I1008-08 Soil SM 2540G SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D SB-9 18I1008-09 Soil SM 2540G SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D SB-10 18I1008-10 Soil SM 2540G SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D SB-8 DUP 18I1008-11 Soil SM 2540G SW-846 6020B SW-846 7196A SW-846 7471B SW-846 8260B SW-846 8270D MW-18 18I1008-12 Ground Water SW-846 6020B SW-846 7196A SW-846 7470A SW-846 8260B SW-846 8270D MW-24 18I1008-13 Ground Water SW-846 6020B SW-846 7196A SW-846 7470A SW-846 8260B SW-846 8270D Page 5 of 159 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Summit Engineering 3575 Centre Circle Drive REPORT DATE: 10/2/2018 Fort Mill, SC 29715 PURCHASE ORDER NUMBER: ATTN: Patrick Lowery PROJECT NUMBER: 3586.01 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18I1008 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 511 East 25th Street, Charlotte, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB MW-19 18I1008-14 Ground Water SW-846 6020B SW-846 7196A SW-846 7470A SW-846 8260B SW-846 8270D MW-23 18I1008-15 Ground Water SW-846 6020B SW-846 7196A SW-846 7470A SW-846 8260B SW-846 8270D MW-25 18I1008-16 Ground Water SW-846 6020B SW-846 7196A SW-846 7470A SW-846 8260B SW-846 8270D MW-17 18I1008-17 Ground Water SW-846 6020B SW-846 7196A SW-846 7470A SW-846 8260B SW-846 8270D MW-17 DUP 18I1008-18 Ground Water SW-846 6020B SW-846 7196A SW-846 7470A SW-846 8260B SW-846 8270D Page 6 of 159 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method 6020, all dilutions were performed as per standard operating procedure. Page 7 of 159 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 SW-846 7196A Qualifications W-06 Elevated method reporting limit due to intense color of sample Analyte & Samples(s) Qualified: Hexavalent Chromium 18I1008-01[SB-1], 18I1008-02[SB-2], 18I1008-03[SB-3],18I1008-04[SB-4] SW-846 8260B Qualifications L-02 Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not affected since all results are 'hot detected" for associated samples in this batch and bias is on the high side. Analyte & Samples(s) Qualified: Acetone B213538-BS1, B213538-BSD1 Hexachlorobutadiene B213199-BSI, B213199-BSDI L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. Analyte & Samples(s) Qualified: 2-Butanone (MEK) B213538-BS1 SW-846 8270D Qualifications: L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side. Analyte & Samples(s) Qualified: Hexachlorocyclopentadiene 1811008-12[MW-18], 18I1008-13[MW-24], 1811008-14[MW-19], 1811008-15[MW-23], 18I1008-16[MW-25], 1811008-17[MW-17], 1811008-18[MW-17 DUP], B213417-BLKI, B213417-BSI, B213417-BSDI L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. Analyte & Samples(s) Qualified: Hexachloroethane B213417-BSDI L-07A Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for this compound. Analyte & Samples(s) Qualified: Benzidine B213246-BS1 Hexachlorobutadiene B213417-BSDI R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Analyte & Samples(s) Qualified: 1,2,4-TYichlorobenzene 18IlOO8-12[MW-18], 18I1008-13[MW-24], 18I1008-14[MW-19], 18I1008-15[MW-23], 18I1008-16[MW-25], 1811008-17[MW-17], 18I1008-18[MW-17 DUP], B213417-BLKI, B213417-BSI, B213417-BSDI Benzidine 18I1008-01[SB-1], 18I1008-02[SB-2], 18I1008-03[SB-3], 18I1008-04[SB-4], 18I1008-05[SB-5], 18I1008-06[SB-6], 18I1008-07[SB-7], 1811008-08[SB-8], 18I1008-09[SB-9], 18I1008-10[SB-10], 18I1008-11[SB-8 DUP], B213246-BLKI, B213246-BSDI Hexachlorobutadiene 18I1008-12[MW-18], 18I1008-13[MW-24], 18I1008-14[MW-19], 1811008-15[MW-23], 18I1008-16[MW-25], 18I1008-17[MW-17], 18I1008-18[MW-17 DUP], B213417-BLKI, B213417-BS1, B213417-BSDI Page 8 of 159 ,con-testo ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 ` TEL. 413/525-2332 V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method specified criteria. Reported result is estimated. Analyte & Samples(s) Qualified: 2,4-Dinitrophenol 18I1008-12[MW-18], 18I1008-13[MW-24], 18I1008-14[MW-19], 18I1008-15[MW-23], 18I1008-16[MW-25], 18I1008-17[MW-17], 18I1008-18[MW-17 DUP], B213417-BLKI, B213417-BSI, B213417-BSDI Benzidine 18I1008-12[MW-18], 18I1008-13[MW-24], 18I1008-14[MW-19], 18I1008-15[MW-23], 18I1008-16[MW-25], 18I1008-17[MW-17], 18I1008-18[MW-17 DUP], B213417-BLKI, B213417-BSI, B213417-BSDI Hexachlorocyclopentadiene 18I1008-12[MW-18], 18I1008-13[MW-24], 18I1008-14[MW-19], 18I1008-15[MW-23], 18I1008-16[MW-25], 18I1008-17[MW-17], 18I1008-18[MW-17 DUP], B213417-BLKI, B213417-BSI, B213417-BSDI V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound. Analyte & Samples(s) Qualified: Aniline 18I1008-01[SB-1], 18I1008-02[SB-21, 18I1008-03[SB-31, 18I1008-04[SB-41, 18I1008-05[SB-5], 18I1008-06[SB-61, 18I1008-07[SB-7], 18I1008-08[SB-81, 18I1008-09[SB-9], 18I1008-10[SB-10], 18I1008-11[SB-8 DUP], B213246-BLKI, B213246-BSI, B213246-BSDI Benzidine 18I1008-01[SB-1], 18I1008-02[SB-2], 18I1008-03[SB-3], 18I1008-04[SB-4], 18I1008-05[SB-5], 18I1008-06[SB-6], 18I1008-07[SB-7], 18I1008-08[SB-8], 18I1008-09[SB-9], 18I1008-10[SB-10], 18I1008-11[SB-8 DUP], 18I1008-12[MW-18], 18I1008-13[MW-24], 18I1008-14[MW-19], 18I1008-15[MW-23], 18I1008-16[MW-251, 18I1008-17[MW-171, 18I1008-18[MW-17 DUPI, B213246-BLKI, B213246-BSI, B213246-BSDI, B213417-BLKI, B213417-BSI, B213417-BSDI V-06 Continuing calibration did not meet method specifications and was biased on the high side for this compound. Analyte & Samples(s) Qualified: 2,4-Dinitrophenol B213246-BSI,B213246-BSDI 3,3-Dichlorobenzidine B213246-BS1,B213246-BSD1 4-Nitrophenol B213417-BLKI. B213417-BSI. B213417-BSDI Benzoic Acid B213246-BSI, B213246-BSDI V-19 Initial calibration did not meet method specifications. Compound was calibrated using linear regression with correlation coefficient <0.99. Reported result is estimated. Analyte & Samples(s) Qualified: 2,4-Dinitrophenol 18I1008-01[SB-11, 18I1008-02[SB-2], 18II008-03[SB-3], 18IlOO8-04[SB-41, 18I1008-05[SB-51, 18I1008-06[SB-61, 18I1008-07[SB-71, 18I1008-08[SB-81, 18I1008-09[SB-91, 18I1008-10[SB-101, 18I1008-11[SB-8 DUPI, B213246-BLKI, B213246-BSI, B213246-BSDI V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte Si Samples(s) Qualified: 2,4-Dinitrophenol 18I1008-01[SB-1], 18I1008-02[SB-2], 18I1008-03[SB-3], 18I1008-04[SB-4], 18I1008-05[SB-5], 18I1008-06[SB-6], 18I1008-07[SB-7], 18I1008-08[SB-8], 18I1008-09[SB-9], 18I1008-10[SB-10], 18I1008-11[SB-8 DUP], B213246-BLKI 3,3-Dichlorobenzidine 18I1008-01[SB-1], 18I1008-02[SB-2], 18I1008-03[SB-3], 18I1008-04[SB-4], 18I1008-05[SB-5], 18I1008-06[SB-6], 18I1008-07[SB-7], 18I1008-08[SB-8], 18I1008-09[SB-9], 18I1008-10[SB-10], 18I1008-11[SB-8DUP],B213246-BLKI 4-Nitrophenol 18I1008-12[MW-18], 18I1008-13[MW-24], 18I1008-14[MW-19], 18I1008-15[MW-23], 18I1008-16[MW-25], 18I1008-17[MW-17], 18I1008-18[MW-17 DUP] Benzoic Acid 18I1008-01[SB-1], 18I1008-02[SB-2], 18I1008-03[SB-3], 18I1008-04[SB-4], 18I1008-05[SB-5], 18I1008-06[SB-6], 18I1008-07[SB-7], 18I1008-08[SB-8], 18I1008-09[SB-9], 18I1008-10[SB-10], 18I1008-11[SB-8 DUP], B213246-BLKI Page 9 of 159 ,con-testo ANALYTICAL LABORATORY Table of Contents V-34 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 ` TEL. 413/525-2332 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. Analyte & Samples(s) Qualified: 4-Chloroaniline 18I1008-01[SB-1], 18I1008-02[SB-2], 18I1008-03[SB-3], 18I1008-04[SB-4], 18I1008-05[SB-5], 18I1008-06[SB-6], 18I1008-07[SB-7], 18I1008-08[SB-8], 18I1008-09[SB-9], 18I1008-10[SB-10], 18I1008-11[SB-8 DUP], 18I1008-12[MW-18], 18I1008-13[MW-24], 18I1008-14[MW-19], 18I1008-15[MW-23], 18I1008-16[MW-25], 18I1008-17[MW-17], 1811008-18[MW-17 DUP], B213246-BLKI, B213246-BSI, B213246-BSDI, B213417-BLKI, B213417-BSI, B213417-BSDI Aniline 18I1008-OI[SB-1], 18I1008-02[SB-2], 18I1008-03[SB-3], 18I1008-04[SB-4], 18I1008-05[SB-5], 18I1008-06[SB-6], 18I1008-07[SB-7], 18I1008-08[SB-8], 18I1008-09[SB-9], 18I1008-10[SB-10], 18I1008-11[SB-8 DUP], B213246-BLKI, B213246-BSI, B213246-BSDI Benzidine 18I1008-01[SB-1], 18I1008-02[SB-2], 18I1008-03[SB-3], 18I1008-04[SB-4], 18I1008-05[SB-5], 18I1008-06[SB-6], 18I1008-07[SB-7], 18I1008-08[SB-8], 1811008-09[SB-9], 18I1008-10[SB-10], 1811008-11[SB-8 DUP], 18I1008-12[MW-18], 18I1008-13[MW-24], 18I1008-14[MW-19], 18I1008-15[MW-23], 18I1008-16[MW-25], 18I1008-17[MW-17], 18I1008-18[MW-17 DUP], B213246-BLKI, B213246-BSI, B213246-BSDI, B213417-BLKI, B213417-BS1, B213417-BSDI The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Project Manager Page 10 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-1 Samnle ID: 1811008-01 Start Date/Time: 9/21/2018 9:30:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 9:35:OOAM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.091 0.091 0.021 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 9:02 MFF Acrylonitrile ND 0.0055 0.0023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF tert-Amyl Methyl Ether (TAME) ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Benzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Bromobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Bromochloromethane ND 0.0018 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Bromodichloromethane ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Bromoform ND 0.0018 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Bromomethane ND 0.0091 0.0038 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 2-Butanone (MEK) ND 0.037 0.016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF tert-Butyl Alcohol (TBA) ND 0.037 0.019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF n-Butylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF sec-Butylbenzene ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF tert-Butylbenzene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00091 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Carbon Disulfide ND 0.0055 0.0039 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Carbon Tetrachloride ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Chlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Chlorodibromomethane ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Chloroethane ND 0.018 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Chloroform ND 0.0037 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Chloromethane ND 0.0091 0.0059 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 9:02 MFF 2-Chlorotoluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 4-Chlorotoluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,2-Dibromoethane (EDB) ND 0.00091 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Dibromomethane ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,2-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,3-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,4-Dichlorobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF trans-1,4-Dichloro-2-butene ND 0.0037 0.0019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Dichlorodifluoromethane (Freon 12) ND 0.018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,1-Dichloroethane ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,2-Dichloroethane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,1-Dichloroethylene ND 0.0037 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF cis-1,2-Dichloroethylene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF trans-1,2-Dichloroethylene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,2-Dichloropropane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,3-Dichloropropane ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 2,2-Dichloropropane ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,1-Dichloropropene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF cis-1,3-Dichloropropene ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF trans-1,3-Dichloropropene ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Diethyl Ether ND 0.018 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Page 11 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-1 Sample ID: 1811008-01 Start Date/Time: 9/21/2018 9:30:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 9:35:OOAM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.00091 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,4-Dioxane ND 0.091 0.053 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Ethylbenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Hexachlorobutadiene ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 2-Hexanone (MBK) ND 0.018 0.010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Isopropylbenzene (Cumene) ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF p-Isopropyltoluene (p-Cymene) ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0037 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Methylene Chloride ND 0.018 0.0065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 4-Methyl-2-pentanone (MIBK) ND 0.018 0.0070 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Naphthalene ND 0.0037 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF n-Propylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Styrene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0018 0.0016 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 9:02 MFF 1,1,2,2-Tetrachloroethane ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Tetrachloroethylene ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Tetrahydrofirran ND 0.0091 0.0020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Toluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,2,3-Trichlorobenzene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,2,4-Trichlorobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,3,5-Trichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1, 1, 1 -Trichloroethane ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,1,2-Trichloroethane ND 0.0018 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Trichloroethylene ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Trichlorofluoromethane (Freon 11) ND 0.0091 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,2,3-Trichloropropane ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0091 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF 1,3,5-Trimethylbenzene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Vinyl Chloride ND 0.0091 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF m+p Xylene ND 0.0037 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF o-Xylene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:02 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 103 70-130 9/28/18 9:02 Toluene-d8 102 70-130 9/28/18 9:02 4-Bromofluorobenzene 102 70-130 9/28/18 9:02 Page 12 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-1 Samnle ID: 1811008-01 Start Date/Time: 9/21/2018 9:30:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 9:35:OOAM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.20 0.059 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Acenaphthylene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Acetophenone ND 0.39 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Aniline ND 0.39 0.11 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Anthracene ND 0.20 0.057 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Benzidine ND 0.76 0.49 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Benzo(a)anthracene ND 0.20 0.052 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Benzo(a)pyrene ND 0.20 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Benzo(b)fluoranthene 0.073 0.20 0.056 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 16:10 BGL Benzo(g,h,i)perylene ND 0.20 0.087 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Benzo(k)fluoranthene ND 0.20 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Benzoic Acid ND 1.2 0.21 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Bis(2-chloroethoxy)methane ND 0.39 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Bis(2-chloroethyl)ether ND 0.39 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Bis(2-chloroisopropyl)ether ND 0.39 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Bis(2-Ethylhexyl)phthalate ND 0.39 0.15 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 4-Bromophenylphenylether ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Butylbenzylphthalate ND 0.39 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Carbazole ND 0.20 0.051 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 4-Chloroaniline ND 0.76 0.090 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 4-Chloro-3-methylphenol ND 0.76 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2-Chloronaphthalene ND 0.39 0.074 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2-Chlorophenol ND 0.39 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 4-Chlorophenylphenylether ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Chrysene ND 0.20 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Dibenz(a,h)anthracene ND 0.20 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Dibenzofman ND 0.39 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Di-n-butylphthalate ND 0.39 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 1,2-Dichlorobenzene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 1,3-Dichlorobenzene ND 0.39 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 1,4-Dichlorobenzene ND 0.39 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 3,3-Dichlorobenzidine ND 0.20 0.060 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2,4-Dichlorophenol ND 0.39 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Diethylphthalate ND 0.39 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2,4-Dimethylphenol ND 0.39 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Dimethylphthalate ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 4,6-Dinitro-2-methylphenol ND 0.39 0.37 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2,4-Dinitrophenol ND 0.76 0.22 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2,4-Dinitrotoluene ND 0.39 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2,6-Dinitrotoluene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Di-n-octylphthalate ND 0.39 0.21 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.39 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Flumanthene 0.071 0.20 0.065 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 16:10 BGL Flumene ND 0.20 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Page 13 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-1 Samnle ID: 1811008-01 Start Date/Time: 9/21/2018 9:30:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 9:35:OOAM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Hexachlorobutadiene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Hexachlorocyclopentadiene ND 0.39 0.083 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Hexachloroethane ND 0.39 0.079 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Indeno(1,2,3-cd)pyrene ND 0.20 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Isophorone ND 0.39 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 1-Methylnaphthalene ND 0.20 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2-Methylnaphthalene ND 0.20 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2-Methylphenol ND 0.39 0.098 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 3/4-Methylphenol ND 0.39 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Naphthalene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2-Nitroaniline ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 3-Nitroaniline ND 0.39 0.057 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 4-Nitroaniline ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Nitrobenzene ND 0.39 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2-Nitrophenol ND 0.39 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 4-Nitrophenol ND 0.76 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL N-Nitrosodimethylamine ND 0.39 0.25 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL N-Nitrosodiphenylamine ND 0.39 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL N-Nitrosodi-n-propylamine ND 0.39 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Pentachloronitrobenzene ND 0.39 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Pentachlorophenol ND 0.39 0.095 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Phenanthrene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Phenol ND 0.39 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Pyrene ND 0.20 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Pyridine ND 0.39 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 1,2,4,5-Tetrachlorobenzene ND 0.39 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 1,2,4-Trichlorobenzene ND 0.39 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2,4,5-Trichlorophenol ND 0.39 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL 2,4,6-Trichlorophenol ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:10 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 48.2 30-130 9/26/18 16:10 Phenol-d6 52.6 30-130 9/26/18 16:10 Nitrobenzene-d5 54.9 30-130 9/26/18 16:10 2-Fluorobiphenyl 59.1 30-130 9/26/18 16:10 2,4,6-Tribromophenol 57.3 30-130 9/26/18 16:10 p-Terphenyl-dl4 63.6 30-130 9/26/18 16:10 Page 14 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-1 Sample ID: 18I1008-01 Start Date/Time: 9/21/2018 9:30:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 9:35:OOAM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 4.2 0.19 0.032 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:19 MJH Chromium 91 19 0.69 mg/Kg dry 20 SW-846 6020B 10/1/18 10/2/18 12:11 MJH Lead 25 1.9 0.063 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:19 MJH Mercury 0.036 0.029 0.0029 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:13 EJB Selenium ND 0.81 0.055 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:19 MJH Silver 0.091 0.085 0.0031 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:19 MJH Barium 120 39 1.6 mg/Kg dry 20 SW-846 6020B 10/1/18 10/2/18 12:11 MJH Cadmium 0.42 0.37 0.012 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:19 MJH Page 15 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-1 Samnle ID: 1811008-01 Start Date/Time: 9/21/2018 9:30:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 9:35:OOAM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium ND 0.92 0.23 mg/Kg dry 5 W-06 SW-846 7196A 9/27/18 9/28/18 10:42 MMH % Solids 85.0 % Wt 1 SM 2540G 10/1/18 10/1/18 21:47 DMP Page 16 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-2 Samnle ID: 1811008-02 Start Date/Time: 9/21/2018 9:45:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 9:50:OOAM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.059 0.11 0.025 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 9:28 MFF Acrylonitrile ND 0.0065 0.0027 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF tert-Amyl Methyl Ether (TAME) ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Benzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Bromobenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Bromochloromethane ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Bromodichloromethane ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Bromoform ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Bromomethane ND 0.011 0.0046 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 2-Butanone (MEK) ND 0.043 0.019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF tert-Butyl Alcohol (TBA) ND 0.043 0.023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF n-Butylbenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF sec-Butylbenzene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF tert-Butylbenzene ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0011 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Carbon Disulfide ND 0.0065 0.0047 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Carbon Tetrachloride ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Chlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Chlorodibromomethane ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Chloroethane ND 0.022 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Chloroform ND 0.0043 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Chloromethane ND 0.011 0.0069 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 9:28 MFF 2-Chlorotoluene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 4-Chlorotoluene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,2-Dibromoethane (EDB) ND 0.0011 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Dibromomethane ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,2-Dichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,3-Dichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,4-Dichlorobenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF trans-1,4-Dichloro-2-butene ND 0.0043 0.0023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Dichlorodifluoromethane (Freon 12) ND 0.022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,1-Dichloroethane ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,2-Dichloroethane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,1-Dichloroethylene ND 0.0043 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF cis-1,2-Dichloroethylene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF trans-1,2-Dichloroethylene ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,2-Dichloropropane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,3-Dichloropropane ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 2,2-Dichloropropane ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,1-Dichloropropene ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF cis-1,3-Dichloropropene ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF trans-1,3-Dichloropropene ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Diethyl Ether ND 0.022 0.0020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Page 17 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-2 Sample ID: 1811008-02 Start Date/Time: 9/21/2018 9:45:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 9:50:OOAM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0011 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,4-Dioxane ND 0.11 0.063 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Ethylbenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Hexachlorobutadiene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 2-Hexanone (MBK) ND 0.022 0.012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Isopropylbenzene (Cumene) ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF p-Isopropyltoluene (p-Cymene) ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0043 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Methylene Chloride ND 0.022 0.0077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 4-Methyl-2-pentanone (MIBK) ND 0.022 0.0083 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Naphthalene ND 0.0043 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF n-Propylbenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Styrene ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0022 0.0020 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 9:28 MFF 1,1,2,2-Tetrachloroethane ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Tetrachloroethylene ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Tetrahydrofirran ND 0.011 0.0024 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Toluene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,2,3-Trichlorobenzene ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,2,4-Trichlorobenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,3,5-Trichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1, 1, 1 -Trichloroethane ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,1,2-Trichloroethane ND 0.0022 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Trichloroethylene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Trichlorofluoromethane (Freon 11) ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,2,3-Trichloropropane ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.011 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF 1,3,5-Trimethylbenzene ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Vinyl Chloride ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF m+p Xylene ND 0.0043 0.0018 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF o-Xylene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:28 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 107 70-130 9/28/18 9:28 Toluene-d8 102 70-130 9/28/18 9:28 4-Bromofluorobenzene 103 70-130 9/28/18 9:28 Page 18 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-2 Samnle ID: 1811008-02 Start Date/Time: 9/21/2018 9:45:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 9:50:OOAM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.21 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Acenaphthylene ND 0.21 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Acetophenone ND 0.43 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Aniline ND 0.43 0.12 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Anthracene ND 0.21 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Benzidine ND 0.83 0.53 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Benzo(a)anthracene 0.068 0.21 0.056 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 16:41 BGL Benzo(a)pyrene 0.11 0.21 0.066 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 16:41 BGL Benzo(b)fluoranthene 0.13 0.21 0.060 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 16:41 BGL Benzo(g,h,i)perylene 0.10 0.21 0.094 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 16:41 BGL Benzo(k)fluoranthene ND 0.21 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Benzoic Acid ND 1.3 0.23 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Bis(2-chloroethoxy)methane ND 0.43 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Bis(2-chloroethyl)ether ND 0.43 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Bis(2-chloroisopropyl)ether ND 0.43 0.091 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Bis(2-Ethylhexyl)phthalate ND 0.43 0.17 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 4-Bromophenylphenylether ND 0.43 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Butylbenzylphthalate ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Carbazole ND 0.21 0.055 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 4-Chloroaniline ND 0.83 0.098 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 4-Chloro-3-methylphenol ND 0.83 0.091 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2-Chloronaphthalene ND 0.43 0.080 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2-Chlorophenol ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 4-Chlorophenylphenylether ND 0.43 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Chrysene ND 0.21 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Dibenz(a,h)anthracene ND 0.21 0.13 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Dibenzofman ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Di-n-butylphthalate ND 0.43 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 1,2-Dichlorobenzene ND 0.43 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 1,3-Dichlorobenzene ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 1,4-Dichlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 3,3-Dichlorobenzidine ND 0.21 0.065 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2,4-Dichlorophenol ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Diethylphthalate ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2,4-Dimethylphenol ND 0.43 0.079 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Dimethylphthalate ND 0.43 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 4,6-Dinitro-2-methylphenol ND 0.43 0.40 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2,4-Dinitrophenol ND 0.83 0.24 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2,4-Dinitrotoluene ND 0.43 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2,6-Dinitrotoluene ND 0.43 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Di-n-octylphthalate ND 0.43 0.22 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.43 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Flumanthene 0.086 0.21 0.070 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 16:41 BGL Flumene ND 0.21 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Page 19 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-2 Samnle ID: 1811008-02 Start Date/Time: 9/21/2018 9:45:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 9:50:OOAM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.43 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Hexachlorobutadiene ND 0.43 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Hexachlorocyclopentadiene ND 0.43 0.090 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Hexachloroethane ND 0.43 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Indeno(1,2,3-cd)pyrene ND 0.21 0.15 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Isophorone ND 0.43 0.083 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 1-Methylnaphthalene ND 0.21 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2-Methylnaphthalene ND 0.21 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2-Methylphenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 3/4-Methylphenol ND 0.43 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Naphthalene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2-Nitroaniline ND 0.43 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 3-Nitroaniline ND 0.43 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 4-Nitroaniline ND 0.43 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Nitrobenzene ND 0.43 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2-Nitrophenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 4-Nitrophenol ND 0.83 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL N-Nitrosodimethylamine ND 0.43 0.27 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL N-Nitrosodiphenylamine ND 0.43 0.088 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL N-Nitrosodi-n-propylamine ND 0.43 0.088 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Pentachloronitrobenzene ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Pentachlorophenol ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Phenanthrene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Phenol ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Pyrene 0.10 0.21 0.070 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 16:41 BGL Pyridine ND 0.43 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 1,2,4,5-Tetrachlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 1,2,4-Trichlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2,4,5-Trichlorophenol ND 0.43 0.096 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL 2,4,6-Trichlorophenol ND 0.43 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 16:41 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 65.6 30-130 9/26/18 16:41 Phenol-d6 69.0 30-130 9/26/18 16:41 Nitrobenzene-d5 67.8 30-130 9/26/18 16:41 2-Fluorobiphenyl 73.2 30-130 9/26/18 16:41 2,4,6-Tribromophenol 78.2 30-130 9/26/18 16:41 p-Terphenyl-dl4 78.3 30-130 9/26/18 16:41 Page 20 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-2 Sample ID: 1811008-02 Start Date/Time: 9/21/2018 9:45:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 9:50:OOAM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 4.4 0.21 0.035 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:22 MJH Chromium 31 5.3 0.19 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:22 MJH Lead 22 2.1 0.069 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:22 MJH Mercury 0.042 0.032 0.0032 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:14 EJB Selenium ND 0.89 0.060 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:22 MJH Silver 0.052 0.093 0.0034 mg/Kg dry 5 J SW-846 6020B 10/1/18 10/2/18 11:22 MJH Barium 63 11 0.43 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:22 MJH Cadmium 0.049 0.40 0.013 mg/Kg dry 5 J SW-846 6020B 10/1/18 10/2/18 11:22 MJH Page 21 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-2 Samnle ID: 1811008-02 Start Date/Time: 9/21/2018 9:45:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 9:50:OOAM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium ND 0.39 0.097 mg/Kg dry 2 W-06 SW-846 7196A 9/27/18 9/28/18 10:42 MMH % Solids 79.5 % Wt 1 SM 2540G 10/1/18 10/1/18 21:48 DMP Page 22 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-3 Sample ID: 1811008-03 Start Date/Time: 9/21/2018 10:00:00AM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:05:OOAM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.062 0.092 0.022 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 9:53 MFF Acrylonitrile ND 0.0055 0.0023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF tert-Amyl Methyl Ether (TAME) ND 0.00092 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Benzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Bromobenzene ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Bromochloromethane ND 0.0018 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Bromodichloromethane ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Bromoform ND 0.0018 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Bromomethane ND 0.0092 0.0039 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 2-Butanone (MEK) ND 0.037 0.016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF tert-Butyl Alcohol (TBA) ND 0.037 0.019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF n-Butylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF sec-Butylbenzene ND 0.0018 0.00092 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF tert-Butylbenzene ND 0.0018 0.00083 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00092 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Carbon Disulfide ND 0.0055 0.0040 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Carbon Tetrachloride ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Chlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Chlorodibromomethane ND 0.00092 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Chloroethane ND 0.018 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Chloroform ND 0.0037 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Chloromethane ND 0.0092 0.0059 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 9:53 MFF 2-Chlorotoluene ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 4-Chlorotoluene ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,2-Dibromoethane (EDB) ND 0.00092 0.00092 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Dibromomethane ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,2-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,3-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,4-Dichlorobenzene ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF trans-1,4-Dichloro-2-butene ND 0.0037 0.0019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Dichlorodifluoromethane (Freon 12) ND 0.018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,1-Dichloroethane ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,2-Dichloroethane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,1-Dichloroethylene ND 0.0037 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF cis-1,2-Dichloroethylene ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF trans-1,2-Dichloroethylene ND 0.0018 0.00083 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,2-Dichloropropane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,3-Dichloropropane ND 0.00092 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 2,2-Dichloropropane ND 0.0018 0.00083 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,1-Dichloropropene ND 0.0018 0.00083 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF cis-1,3-Dichloropropene ND 0.00092 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF trans-1,3-Dichloropropene ND 0.00092 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Diethyl Ether ND 0.018 0.0017 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Page 23 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-3 Sample ID: 1811008-03 Start Date/Time: 9/21/2018 10:00:00AM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:05:OOAM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.00092 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,4-Dioxane ND 0.092 0.053 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Ethylbenzene ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Hexachlorobutadiene ND 0.0018 0.00092 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 2-Hexanone (MBK) ND 0.018 0.010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Isopropylbenzene (Cumene) ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF p-Isopropyltoluene (p-Cymene) ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0037 0.00083 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Methylene Chloride ND 0.018 0.0065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 4-Methyl-2-pentanone (MIBK) ND 0.018 0.0070 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Naphthalene ND 0.0037 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF n-Propylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Styrene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0018 0.0017 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 9:53 MFF 1,1,2,2-Tetrachloroethane ND 0.0018 0.00083 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Tetrachloroethylene 0.0031 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Tetrahydrofirran ND 0.0092 0.0020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Toluene ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,2,3-Trichlorobenzene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,2,4-Trichlorobenzene ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,3,5-Trichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1, 1, 1 -Trichloroethane ND 0.0018 0.00092 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,1,2-Trichloroethane ND 0.0018 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Trichloroethylene ND 0.0018 0.00092 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Trichlorofluoromethane (Freon 11) ND 0.0092 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,2,3-Trichloropropane ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0092 0.00083 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0018 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF 1,3,5-Trimethylbenzene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Vinyl Chloride ND 0.0092 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF m+p Xylene ND 0.0037 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF o-Xylene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 9:53 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 108 70-130 9/28/18 9:53 Toluene-d8 101 70-130 9/28/18 9:53 4-Bromofluorobenzene 103 70-130 9/28/18 9:53 Page 24 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-3 Sample ID: 1811008-03 Start Date/Time: 9/21/2018 10:00:00AM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:05:OOAM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.20 0.059 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Acenaphthylene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Acetophenone ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Aniline ND 0.40 0.11 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Anthracene ND 0.20 0.057 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Benzidine ND 0.77 0.50 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Benzo(a)anthracene ND 0.20 0.052 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Benzo(a)pyrene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Benzo(b)fluoranthene ND 0.20 0.056 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Benzo(g,h,i)perylene ND 0.20 0.087 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Benzo(k)fluoranthene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Benzoic Acid ND 1.2 0.21 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Bis(2-chloroethoxy)methane ND 0.40 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Bis(2-chloroethyl)ether ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Bis(2-chloroisopropyl)ether ND 0.40 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Bis(2-Ethylhexyl)phthalate ND 0.40 0.15 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 4-Bromophenylphenylether ND 0.40 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Butylbenzylphthalate ND 0.40 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Carbazole ND 0.20 0.051 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 4-Chloroaniline ND 0.77 0.091 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 4-Chloro-3-methylphenol ND 0.77 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2-Chloronaphthalene ND 0.40 0.075 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2-Chlorophenol ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 4-Chlorophenylphenylether ND 0.40 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Chrysene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Dibenz(a,h)anthracene ND 0.20 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Dibenzofman ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Di-n-butylphthalate ND 0.40 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 1,2-Dichlorobenzene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 1,3-Dichlorobenzene ND 0.40 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 1,4-Dichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 3,3-Dichlorobenzidine ND 0.20 0.061 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2,4-Dichlorophenol ND 0.40 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Diethylphthalate ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2,4-Dimethylphenol ND 0.40 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Dimethylphthalate ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 4,6-Dinitro-2-methylphenol ND 0.40 0.38 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2,4-Dinitrophenol ND 0.77 0.23 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2,4-Dinitrotoluene ND 0.40 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2,6-Dinitrotoluene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Di-n-octylphthalate ND 0.40 0.21 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.40 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Flumanthene ND 0.20 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Flumene ND 0.20 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Page 25 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-3 Sample ID: 1811008-03 Start Date/Time: 9/21/2018 10:00:00AM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:05:OOAM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Hexachlorobutadiene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Hexachlorocyclopentadiene ND 0.40 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Hexachloroethane ND 0.40 0.079 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Indeno(1,2,3-cd)pyrene ND 0.20 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Isophorone ND 0.40 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 1-Methylnaphthalene ND 0.20 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2-Methylnaphthalene ND 0.20 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2-Methylphenol ND 0.40 0.099 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 3/4-Methylphenol ND 0.40 0.13 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Naphthalene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2-Nitroaniline ND 0.40 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 3-Nitroaniline ND 0.40 0.057 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 4-Nitroaniline ND 0.40 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Nitrobenzene ND 0.40 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2-Nitrophenol ND 0.40 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 4-Nitrophenol ND 0.77 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL N-Nitrosodimethylamine ND 0.40 0.25 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL N-Nitrosodiphenylamine ND 0.40 0.082 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL N-Nitrosodi-n-propylamine ND 0.40 0.082 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Pentachloronitrobenzene ND 0.40 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Pentachlorophenol ND 0.40 0.096 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Phenanthrene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Phenol ND 0.40 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Pyrene ND 0.20 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Pyridine ND 0.40 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 1,2,4,5-Tetrachlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 1,2,4-Trichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2,4,5-Trichlorophenol ND 0.40 0.090 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL 2,4,6-Trichlorophenol ND 0.40 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:12 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 57.8 30-130 9/26/18 17:12 Phenol-d6 60.7 30-130 9/26/18 17:12 Nitrobenzene-d5 61.8 30-130 9/26/18 17:12 2-Fluorobiphenyl 66.4 30-130 9/26/18 17:12 2,4,6-Tribromophenol 73.3 30-130 9/26/18 17:12 p-Terphenyl-dl4 74.9 30-130 9/26/18 17:12 Page 26 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-3 Sample ID: 1811008-03 Start Date/Time: 9/21/2018 10:00:00AM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 10:05:OOAM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 1.0 0.19 0.030 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:26 MJH Chromium 52 4.6 0.17 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:26 MJH Lead 17 1.9 0.061 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:26 MJH Mercury 0.039 0.029 0.0029 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:16 EJB Selenium ND 0.78 0.053 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:26 MJH Silver 0.038 0.082 0.0030 mg/Kg dry 5 J SW-846 6020B 10/1/18 10/2/18 11:26 MJH Barium 78 9.3 0.38 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:26 MJH Cadmium ND 0.35 0.012 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:26 MJH Page 27 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-3 Sample ID: 1811008-03 Start Date/Time: 9/21/2018 10:00:00AM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 10:05:OOAM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium ND 0.36 0.090 mg/Kg dry 2 W-06 SW-846 7196A 9/27/18 9/28/18 10:42 MMH % Solids 85.8 % Wt 1 SM 2540G 10/1/18 10/1/18 21:48 DMP Page 28 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB4 Sample ID: 1811008-04 Start Date/Time: 9/21/2018 10:20:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:25:OOAM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.042 0.097 0.023 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 10:19 MFF Acrylonitrile ND 0.0058 0.0024 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF tert-Amyl Methyl Ether (TAME) ND 0.00097 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Benzene ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Bromobenzene ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Bromochloromethane ND 0.0019 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Bromodichloromethane ND 0.0019 0.00058 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Bromoform ND 0.0019 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Bromomethane ND 0.0097 0.0041 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 2-Butanone (MEK) ND 0.039 0.017 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF tert-Butyl Alcohol (TBA) ND 0.039 0.020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF n-Butylbenzene ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF sec-Butylbenzene ND 0.0019 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF tert-Butylbenzene ND 0.0019 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00097 0.00058 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Carbon Disulfide ND 0.0058 0.0042 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Carbon Tetrachloride ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Chlorobenzene ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Chlorodibromomethane ND 0.00097 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Chloroethane ND 0.019 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Chloroform 0.0035 0.0039 0.00068 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 10:19 MFF Chloromethane ND 0.0097 0.0062 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 10:19 MFF 2-Chlorotoluene ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 4-Chlorotoluene ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0019 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,2-Dibromoethane (EDB) ND 0.00097 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Dibromomethane ND 0.0019 0.00058 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,2-Dichlorobenzene ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,3-Dichlorobenzene ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,4-Dichlorobenzene ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF trans-1,4-Dichloro-2-butene ND 0.0039 0.0020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Dichlorodifluoromethane (Freon 12) ND 0.019 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,1-Dichloroethane ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,2-Dichloroethane ND 0.0019 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,1-Dichloroethylene ND 0.0039 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF cis-1,2-Dichloroethylene ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF trans-1,2-Dichloroethylene ND 0.0019 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,2-Dichloropropane ND 0.0019 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,3-Dichloropropane ND 0.00097 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 2,2-Dichloropropane ND 0.0019 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,1-Dichloropropene ND 0.0019 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF cis-1,3-Dichloropropene ND 0.00097 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF trans-1,3-Dichloropropene ND 0.00097 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Diethyl Ether ND 0.019 0.0017 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Page 29 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB4 Sample ID: 1811008-04 Start Date/Time: 9/21/2018 10:20:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:25:OOAM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.00097 0.00058 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,4-Dioxane ND 0.097 0.056 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Ethylbenzene ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Hexachlorobutadiene ND 0.0019 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 2-Hexanone (MBK) ND 0.019 0.011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Isopropylbenzene (Cumene) ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF p-Isopropyltoluene (p-Cymene) ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0039 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Methylene Chloride ND 0.019 0.0069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 4-Methyl-2-pentanone (MIBK) ND 0.019 0.0074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Naphthalene ND 0.0039 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF n-Propylbenzene ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Styrene ND 0.0019 0.00058 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0019 0.0017 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 10:19 MFF 1,1,2,2-Tetrachloroethane ND 0.0019 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Tetrachloroethylene ND 0.0019 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Tetrahydrofuran ND 0.0097 0.0021 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Toluene ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,2,3-Trichlorobenzene ND 0.0019 0.00058 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,2,4-Trichlorobenzene ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,3,5-Trichlorobenzene ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1, 1, 1 -Trichloroethane ND 0.0019 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,1,2-Trichloroethane ND 0.0019 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Trichloroethylene ND 0.0019 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Trichlorofluoromethane (Freon 11) ND 0.0097 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,2,3-Trichloropropane ND 0.0019 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0097 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0019 0.00078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF 1,3,5-Trimethylbenzene ND 0.0019 0.00058 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Vinyl Chloride ND 0.0097 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF m+p Xylene ND 0.0039 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF o-Xylene ND 0.0019 0.00068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:19 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 100 70-130 9/28/18 10:19 Toluene-d8 102 70-130 9/28/18 10:19 4-Bromofluorobenzene 105 70-130 9/28/18 10:19 Page 30 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB4 Sample ID: 1811008-04 Start Date/Time: 9/21/2018 10:20:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:25:OOAM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.21 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Acenaphthylene ND 0.21 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Acetophenone ND 0.42 0.083 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Aniline ND 0.42 0.12 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Anthracene ND 0.21 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Benzidine ND 0.82 0.53 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Benzo(a)anthracene ND 0.21 0.056 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Benzo(a)pyrene ND 0.21 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Benzo(b)fluoranthene ND 0.21 0.060 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Benzo(g,h,i)perylene ND 0.21 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Benzo(k)fluoranthene ND 0.21 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Benzoic Acid ND 1.2 0.23 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Bis(2-chloroethoxy)methane ND 0.42 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Bis(2-chloroethyl)ether ND 0.42 0.083 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Bis(2-chloroisopropyl)ether ND 0.42 0.091 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Bis(2-Ethylhexyl)phthalate ND 0.42 0.16 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 4-Bromophenylphenylether ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Butylbenzylphthalate ND 0.42 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Carbazole ND 0.21 0.055 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 4-Chloroaniline ND 0.82 0.097 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 4-Chloro-3-methylphenol ND 0.82 0.091 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2-Chloronaphthalene ND 0.42 0.080 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2-Chlorophenol ND 0.42 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 4-Chlorophenylphenylether ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Chrysene ND 0.21 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Dibenz(a,h)anthracene ND 0.21 0.13 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Dibenzofman ND 0.42 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Di-n-butylphthalate ND 0.42 0.092 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 1,2-Dichlorobenzene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 1,3-Dichlorobenzene ND 0.42 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 1,4-Dichlorobenzene ND 0.42 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 3,3-Dichlorobenzidine ND 0.21 0.065 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2,4-Dichlorophenol ND 0.42 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Diethylphthalate ND 0.42 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2,4-Dimethylphenol ND 0.42 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Dimethylphthalate ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 4,6-Dinitro-2-methylphenol ND 0.42 0.40 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2,4-Dinitrophenol ND 0.82 0.24 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2,4-Dinitrotoluene ND 0.42 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2,6-Dinitrotoluene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Di-n-octylphthalate ND 0.42 0.22 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.42 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Flumanthene ND 0.21 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Flumene ND 0.21 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Page 31 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB4 Sample ID: 1811008-04 Start Date/Time: 9/21/2018 10:20:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:25:OOAM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Hexachlorobutadiene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Hexachlorocyclopentadiene ND 0.42 0.090 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Hexachloroethane ND 0.42 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Indeno(1,2,3-cd)pyrene ND 0.21 0.15 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Isophorone ND 0.42 0.082 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 1-Methylnaphthalene ND 0.21 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2-Methylnaphthalene ND 0.21 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2-Methylphenol ND 0.42 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 3/4-Methylphenol ND 0.42 0.13 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Naphthalene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2-Nitroaniline ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 3-Nitroaniline ND 0.42 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 4-Nitroaniline ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Nitrobenzene ND 0.42 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2-Nitrophenol ND 0.42 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 4-Nitrophenol ND 0.82 0.092 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL N-Nitrosodimethylamine ND 0.42 0.27 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL N-Nitrosodiphenylamine ND 0.42 0.087 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL N-Nitrosodi-n-propylamine ND 0.42 0.087 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Pentachloronitrobenzene ND 0.42 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Pentachlorophenol ND 0.42 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Phenanthrene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Phenol ND 0.42 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Pyrene ND 0.21 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Pyridine ND 0.42 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 1,2,4,5-Tetrachlorobenzene ND 0.42 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 1,2,4-Trichlorobenzene ND 0.42 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2,4,5-Trichlorophenol ND 0.42 0.096 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL 2,4,6-Trichlorophenol ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 17:42 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 62.8 30-130 9/26/18 17:42 Phenol-d6 64.0 30-130 9/26/18 17:42 Nitrobenzene-d5 65.2 30-130 9/26/18 17:42 2-Fluorobiphenyl 69.7 30-130 9/26/18 17:42 2,4,6-Tribromophenol 80.4 30-130 9/26/18 17:42 p-Terphenyl-dl4 71.7 30-130 9/26/18 17:42 Page 32 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB4 Sample ID: 1811008-04 Start Date/Time: 9/21/2018 10:20:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 10:25:OOAM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 1.1 0.20 0.033 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:29 MJH Chromium 82 5.1 0.18 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:29 MJH Lead 10 2.0 0.067 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:29 MJH Mercury 0.042 0.030 0.0030 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:18 EJB Selenium ND 0.85 0.058 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:29 MJH Silver 0.12 0.089 0.0033 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:29 MJH Barium 120 41 1.7 mg/Kg dry 20 SW-846 6020B 10/1/18 10/2/18 12:15 MJH Cadmium ND 0.39 0.013 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:29 MJH Page 33 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB4 Sample ID: 1811008-04 Start Date/Time: 9/21/2018 10:20:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 10:25:OOAM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium ND 0.39 0.098 mg/Kg dry 2 W-06 SW-846 7196A 9/27/18 9/28/18 10:42 MMH % Solids 80.1 % Wt 1 SM 2540G 10/1/18 10/1/18 21:48 DMP Page 34 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-5 Sample ID: 1811008-05 Start Date/Time: 9/21/2018 10:45:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:50:OOAM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.034 0.11 0.025 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 10:46 MFF Acrylonitrile ND 0.0064 0.0027 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF tert-Amyl Methyl Ether (TAME) ND 0.0011 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Benzene ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Bromobenzene ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Bromochloromethane ND 0.0021 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Bromodichloromethane ND 0.0021 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Bromoform ND 0.0021 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Bromomethane ND 0.011 0.0045 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 2-Butanone (MEK) ND 0.042 0.019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF tert-Butyl Alcohol (TBA) ND 0.042 0.022 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF n-Butylbenzene ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF sec-Butylbenzene ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF tert-Butylbenzene ND 0.0021 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0011 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Carbon Disulfide ND 0.0064 0.0046 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Carbon Tetrachloride ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Chlorobenzene ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Chlorodibromomethane ND 0.0011 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Chloroethane ND 0.021 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Chloroform ND 0.0042 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Chloromethane ND 0.011 0.0068 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 10:46 MFF 2-Chlorotoluene ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 4-Chlorotoluene ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0021 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,2-Dibromoethane (EDB) ND 0.0011 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Dibromomethane ND 0.0021 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,2-Dichlorobenzene ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,3-Dichlorobenzene ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,4-Dichlorobenzene ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF trans-1,4-Dichloro-2-butene ND 0.0042 0.0022 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Dichlorodifluoromethane (Freon 12) ND 0.021 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,1-Dichloroethane ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,2-Dichloroethane ND 0.0021 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1, 1 -Dichloroethylene ND 0.0042 0.0012 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 10:46 MFF cis-1,2-Dichloroethylene ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF trans-1,2-Dichloroethylene ND 0.0021 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,2-Dichloropropane ND 0.0021 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,3-Dichloropropane ND 0.0011 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 2,2-Dichloropropane ND 0.0021 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,1-Dichloropropene ND 0.0021 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF cis-1,3-Dichloropropene ND 0.0011 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF trans-1,3-Dichloropropene ND 0.0011 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Diethyl Ether ND 0.021 0.0019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Page 35 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-5 Sample ID: 1811008-05 Start Date/Time: 9/21/2018 10:45:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:50:OOAM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0011 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,4-Dioxane ND 0.11 0.061 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Ethylbenzene ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Hexachlorobutadiene ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 2-Hexanone (MBK) ND 0.021 0.012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Isopropylbenzene (Cumene) ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF p-Isopropyltoluene (p-Cymene) ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0042 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Methylene Chloride ND 0.021 0.0075 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 4-Methyl-2-pentanone (MIBK) ND 0.021 0.0081 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Naphthalene ND 0.0042 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF n-Propylbenzene ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Styrene ND 0.0021 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0021 0.0019 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 10:46 MFF 1,1,2,2-Tetrachloroethane ND 0.0021 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Tetrachloroethylene ND 0.0021 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Tetrahydrofuran ND 0.011 0.0023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Toluene ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,2,3-Trichlorobenzene ND 0.0021 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,2,4-Trichlorobenzene ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,3,5-Trichlorobenzene ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1, 1, 1 -Trichloroethane ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,1,2-Trichloroethane ND 0.0021 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Trichloroethylene ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Trichlorofluoromethane (Freon 11) ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,2,3-Trichloropropane ND 0.0021 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.011 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0021 0.00085 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF 1,3,5-Trimethylbenzene ND 0.0021 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Vinyl Chloride ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF m+p Xylene ND 0.0042 0.0018 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF o-Xylene ND 0.0021 0.00074 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 10:46 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 105 70-130 9/28/18 10:46 Toluene-d8 102 70-130 9/28/18 10:46 4-Bromofluorobenzene 106 70-130 9/28/18 10:46 Page 36 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-5 Sample ID: 1811008-05 Start Date/Time: 9/21/2018 10:45:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:50:OOAM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.22 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Acenaphthylene ND 0.22 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Acetophenone ND 0.43 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Aniline ND 0.43 0.12 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Anthracene ND 0.22 0.062 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Benzidine ND 0.84 0.54 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Benzo(a)anthracene ND 0.22 0.057 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Benzo(a)pyrene ND 0.22 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Benzo(b)fluoranthene ND 0.22 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Benzo(g,h,i)perylene ND 0.22 0.095 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Benzo(k)fluoranthene ND 0.22 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Benzoic Acid ND 1.3 0.23 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Bis(2-chloroethoxy)methane ND 0.43 0.082 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Bis(2-chloroethyl)ether ND 0.43 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Bis(2-chloroisopropyl)ether ND 0.43 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Bis(2-Ethylhexyl)phthalate ND 0.43 0.17 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 4-Bromophenylphenylether ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Butylbenzylphthalate ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Carbazole ND 0.22 0.056 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 4-Chloroaniline ND 0.84 0.099 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 4-Chloro-3-methylphenol ND 0.84 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2-Chloronaphthalene ND 0.43 0.081 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2-Chlorophenol ND 0.43 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 4-Chlorophenylphenylether ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Chrysene ND 0.22 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Dibenz(a,h)anthracene ND 0.22 0.13 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Dibenzofman ND 0.43 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Di-n-butylphthalate ND 0.43 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 1,2-Dichlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 1,3-Dichlorobenzene ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 1,4-Dichlorobenzene ND 0.43 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 3,3-Dichlorobenzidine ND 0.22 0.066 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2,4-Dichlorophenol ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Diethylphthalate ND 0.43 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2,4-Dimethylphenol ND 0.43 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Dimethylphthalate ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 4,6-Dinitro-2-methylphenol ND 0.43 0.41 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2,4-Dinitrophenol ND 0.84 0.25 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2,4-Dinitrotoluene ND 0.43 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2,6-Dinitrotoluene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Di-n-octylphthalate ND 0.43 0.23 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.43 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Flumanthene ND 0.22 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Flumene ND 0.22 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Page 37 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-5 Sample ID: 1811008-05 Start Date/Time: 9/21/2018 10:45:OOAM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 10:50:OOAM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Hexachlorobutadiene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Hexachlorocyclopentadiene ND 0.43 0.091 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Hexachloroethane ND 0.43 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Indeno(1,2,3-cd)pyrene ND 0.22 0.15 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Isophorone ND 0.43 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 1-Methylnaphthalene ND 0.22 0.082 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2-Methylnaphthalene ND 0.22 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2-Methylphenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 3/4-Methylphenol ND 0.43 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Naphthalene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2-Nitroaniline ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 3-Nitroaniline ND 0.43 0.062 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 4-Nitroaniline ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Nitrobenzene ND 0.43 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2-Nitrophenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 4-Nitrophenol ND 0.84 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL N-Nitrosodimethylamine ND 0.43 0.27 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL N-Nitrosodiphenylamine ND 0.43 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL N-Nitrosodi-n-propylamine ND 0.43 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Pentachloronitrobenzene ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Pentachlorophenol ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Phenanthrene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Phenol ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Pyrene ND 0.22 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Pyridine ND 0.43 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 1,2,4,5-Tetrachlorobenzene ND 0.43 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 1,2,4-Trichlorobenzene ND 0.43 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2,4,5-Trichlorophenol ND 0.43 0.098 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL 2,4,6-Trichlorophenol ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:11 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 41.2 30-130 9/26/18 18:11 Phenol-d6 42.5 30-130 9/26/18 18:11 Nitrobenzene-d5 39.4 30-130 9/26/18 18:11 2-Fluorobiphenyl 45.7 30-130 9/26/18 18:11 2,4,6-Tribromophenol 52.7 30-130 9/26/18 18:11 p-Terphenyl-dl4 52.2 30-130 9/26/18 18:11 Page 38 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-5 Sample ID: 1811008-05 Start Date/Time: 9/21/2018 10:45:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 10:50:OOAM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 1.0 0.21 0.035 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:33 MJH Chromium 96 5.4 0.19 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:33 MJH Lead 10 2.1 0.070 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:33 MJH Mercury 0.063 0.031 0.0031 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:19 EJB Selenium ND 0.90 0.061 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:33 MJH Silver 0.096 0.094 0.0034 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:33 MJH Barium 90 11 0.44 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:33 MJH Cadmium ND 0.41 0.014 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:33 MJH Page 39 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-5 Sample ID: 1811008-05 Start Date/Time: 9/21/2018 10:45:00AM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 10:50:OOAM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium % Solids 0.54 0.41 0.10 mg/Kg dry 2 77.6 % Wt 1 SW-846 7196A 9/27/18 9/28/18 10:42 MMH SM 2540G 10/1/18 10/1/18 21:48 DMP Page 40 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-6 Samnle ID: 1811008-06 Start Date/Time: 9/21/2018 11:05:OOAM Samnle Matrix: Soil StoD Date/Time: 9/21/2018 11:10:00AM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.099 0.11 0.025 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 11:11 MFF Acrylonitrile ND 0.0065 0.0027 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF tert-Amyl Methyl Ether (TAME) ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Benzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Bromobenzene ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Bromochloromethane ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Bromodichloromethane ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Bromoform ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Bromomethane ND 0.011 0.0045 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 2-Butanone (MEK) ND 0.043 0.019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF tert-Butyl Alcohol (TBA) ND 0.043 0.023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF n-Butylbenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF sec-Butylbenzene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF tert-Butylbenzene ND 0.0022 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0011 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Carbon Disulfide ND 0.0065 0.0046 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Carbon Tetrachloride ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Chlorobenzene ND 0.0022 0.00076 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:11 MFF Chlorodibromomethane ND 0.0011 0.00076 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:11 MFF Chloroethane ND 0.022 0.0016 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:11 MFF Chloroform ND 0.0043 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Chloromethane ND 0.011 0.0069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 2-Chlorotoluene ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 4-Chlorotoluene ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,2-Dibromoethane (EDB) ND 0.0011 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Dibromomethane ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,2-Dichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,3-Dichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,4-Dichlorobenzene ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF trans-1,4-Dichloro-2-butene ND 0.0043 0.0023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Dichlorodifluoromethane (Freon 12) ND 0.022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,1-Dichloroethane ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,2-Dichloroethane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,1-Dichloroethylene ND 0.0043 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF cis-1,2-Dichloroethylene ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF trans-1,2-Dichloroethylene ND 0.0022 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,2-Dichloropropane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,3-Dichloropropane ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 2,2-Dichloropropane ND 0.0022 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,1-Dichloropropene ND 0.0022 0.00097 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:11 MFF cis-1,3-Dichloropropene ND 0.0011 0.00076 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:11 MFF trans-1,3-Dichloropropene ND 0.0011 0.00076 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:11 MFF Diethyl Ether ND 0.022 0.0019 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:11 MFF Page 41 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-6 Samnle ID: 1811008-06 Start Date/Time: 9/21/2018 11:05:OOAM Samnle Matrix: Soil StoD Date/Time: 9/21/2018 11:10:00AM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPS) ND 0.0011 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,4-Dioxane ND 0.11 0.062 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Ethylbenzene ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Hexachlorobutadiene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 2-Hexanone (MBK) ND 0.022 0.012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Isopropylbenzene (Cumene) ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF p-Isopropyltoluene (p-Cymene) ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0043 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Methylene Chloride ND 0.022 0.0077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 4-Methyl-2-pentanone (MIBK) ND 0.022 0.0082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Naphthalene ND 0.0043 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF n-Propylbenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Styrene ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0022 0.0019 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 11:11 MFF 1,1,2,2-Tetrachloroethane ND 0.0022 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Tetrachloroethylene ND 0.0022 0.0014 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:11 MFF Tetrahydrofuran ND 0.011 0.0024 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Toluene ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,2,3-Trichlorobenzene ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,2,4-Trichlorobenzene ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,3,5-Trichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1, 1, 1 -Trichloroethane ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,1,2-Trichloroethane ND 0.0022 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Trichloroethylene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Trichlorofluoromethane (Freon 11) ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,2,3-Trichloropropane ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.011 0.00097 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0022 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF 1,3,5-Trimethylbenzene ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Vinyl Chloride ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF m+p Xylene ND 0.0043 0.0018 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF o-Xylene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:11 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 105 70-130 9/28/18 11:11 Toluene-d8 101 70-130 9/28/18 11:11 4-Bromofluorobenzene 102 70-130 9/28/18 11:11 Page 42 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-6 Samnle ID: 1811008-06 Start Date/Time: 9/21/2018 11:05:OOAM Samnle Matrix: Soil StoD Date/Time: 9/21/2018 11:10:00AM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.22 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Acenaphthylene ND 0.22 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Acetophenone ND 0.43 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Aniline ND 0.43 0.12 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Anthracene ND 0.22 0.062 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Benzidine ND 0.84 0.54 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Benzo(a)anthracene ND 0.22 0.057 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Benzo(a)pyrene ND 0.22 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Benzo(b)fluoranthene ND 0.22 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Benzo(g,h,i)perylene ND 0.22 0.095 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Benzo(k)fluoranthene ND 0.22 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Benzoic Acid ND 1.3 0.23 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Bis(2-chloroethoxy)methane ND 0.43 0.083 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Bis(2-chloroethyl)ether ND 0.43 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Bis(2-chloroisopropyl)ether ND 0.43 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Bis(2-Ethylhexyl)phthalate ND 0.43 0.17 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 4-Bromophenylphenylether ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Butylbenzylphthalate ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Carbazole ND 0.22 0.056 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 4-Chloroaniline ND 0.84 0.099 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 4-Chloro-3-methylphenol ND 0.84 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2-Chloronaphthalene ND 0.43 0.081 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2-Chlorophenol ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 4-Chlorophenylphenylether ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Chrysene ND 0.22 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Dibenz(a,h)anthracene ND 0.22 0.13 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Dibenzofman ND 0.43 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Di-n-butylphthalate ND 0.43 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 1,2-Dichlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 1,3-Dichlorobenzene ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 1,4-Dichlorobenzene ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 3,3-Dichlorobenzidine ND 0.22 0.066 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2,4-Dichlorophenol ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Diethylphthalate ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2,4-Dimethylphenol ND 0.43 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Dimethylphthalate ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 4,6-Dinitro-2-methylphenol ND 0.43 0.41 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2,4-Dinitrophenol ND 0.84 0.25 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2,4-Dinitrotoluene ND 0.43 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2,6-Dinitrotoluene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Di-n-octylphthalate ND 0.43 0.23 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.43 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Flumanthene ND 0.22 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Flumene ND 0.22 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Page 43 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-6 Samnle ID: 1811008-06 Start Date/Time: 9/21/2018 11:05:OOAM Samnle Matrix: Soil StoD Date/Time: 9/21/2018 11:10:00AM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Hexachlorobutadiene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Hexachlorocyclopentadiene ND 0.43 0.092 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Hexachloroethane ND 0.43 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Indeno(1,2,3-cd)pyrene ND 0.22 0.16 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Isophorone ND 0.43 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 1-Methylnaphthalene ND 0.22 0.083 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2-Methylnaphthalene ND 0.22 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2-Methylphenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 3/4-Methylphenol ND 0.43 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Naphthalene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2-Nitroaniline ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 3-Nitroaniline ND 0.43 0.062 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 4-Nitroaniline ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Nitrobenzene ND 0.43 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2-Nitrophenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 4-Nitrophenol ND 0.84 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL N-Nitrosodimethylamine ND 0.43 0.27 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL N-Nitrosodiphenylamine ND 0.43 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL N-Nitrosodi-n-propylamine ND 0.43 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Pentachloronitrobenzene ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Pentachlorophenol ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Phenanthrene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Phenol ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Pyrene ND 0.22 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Pyridine ND 0.43 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 1,2,4,5-Tetrachlorobenzene ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 1,2,4-Trichlorobenzene ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2,4,5-Trichlorophenol ND 0.43 0.098 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL 2,4,6-Trichlorophenol ND 0.43 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 18:41 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 64.0 30-130 9/26/18 18:41 Phenol-d6 66.2 30-130 9/26/18 18:41 Nitrobenzene-d5 64.9 30-130 9/26/18 18:41 2-Fluorobiphenyl 70.6 30-130 9/26/18 18:41 2,4,6-Tribromophenol 82.0 30-130 9/26/18 18:41 p-Terphenyl-dl4 78.1 30-130 9/26/18 18:41 Page 44 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-6 Sample ID: 1811008-06 Start Date/Time: 9/21/2018 11:05:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 11:10:00AM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 1.6 0.21 0.034 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:43 MJH Chromium 130 21 0.74 mg/Kg dry 20 SW-846 6020B 10/1/18 10/2/18 12:27 MJH Lead 9.5 2.1 0.068 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:43 MJH Mercury 0.061 0.031 0.0031 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:21 EJB Selenium ND 0.87 0.059 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:43 MJH Silver 0.091 0.091 0.0033 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:43 MJH Barium 110 41 1.7 mg/Kg dry 20 SW-846 6020B 10/1/18 10/2/18 12:27 MJH Cadmium ND 0.39 0.013 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:43 MJH Page 45 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-6 Samnle ID: 1811008-06 Start Date/Time: 9/21/2018 11:05:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 11:10:00AM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium % Solids 1.2 0.41 0.10 mg/Kg dry 2 78.2 % Wt 1 SW-846 7196A 9/27/18 9/28/18 10:42 MMH SM 2540G 10/1/18 10/1/18 21:48 DMP Page 46 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-7 Samnle ID: 1811008-07 Start Date/Time: 9/21/2018 11:45:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 11:50:OOAM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.031 0.092 0.021 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 11:36 MFF Acrylonitrile ND 0.0055 0.0023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF tert-Amyl Methyl Ether (TAME) ND 0.00092 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Benzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Bromobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Bromochloromethane ND 0.0018 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Bromodichloromethane ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Bromoform ND 0.0018 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Bromomethane ND 0.0092 0.0038 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 2-Butanone (MEK) ND 0.037 0.016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF tert-Butyl Alcohol (TBA) ND 0.037 0.019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF n-Butylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF sec-Butylbenzene ND 0.0018 0.00092 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF tert-Butylbenzene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00092 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Carbon Disulfide ND 0.0055 0.0039 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Carbon Tetrachloride ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Chlorobenzene ND 0.0018 0.00064 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:36 MFF Chlorodibromomethane ND 0.00092 0.00064 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:36 MFF Chloroethane ND 0.018 0.0014 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:36 MFF Chloroform ND 0.0037 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Chloromethane ND 0.0092 0.0059 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 2-Chlorotoluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 4-Chlorotoluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,2-Dibromoethane (EDB) ND 0.00092 0.00092 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Dibromomethane ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,2-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,3-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,4-Dichlorobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF trans-1,4-Dichloro-2-butene ND 0.0037 0.0019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Dichlorodifluoromethane (Freon 12) ND 0.018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,1-Dichloroethane ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,2-Dichloroethane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,1-Dichloroethylene ND 0.0037 0.0010 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 11:36 MFF cis-1,2-Dichloroethylene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF trans-1,2-Dichloroethylene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,2-Dichloropropane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,3-Dichloropropane ND 0.00092 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 2,2-Dichloropropane ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,1-Dichloropropene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF cis-1,3-Dichloropropene ND 0.00092 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF trans-1,3-Dichloropropene ND 0.00092 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Diethyl Ether ND 0.018 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Page 47 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-7 Samnle ID: 1811008-07 Start Date/Time: 9/21/2018 11:45:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 11:50:OOAM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.00092 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,4-Dioxane ND 0.092 0.053 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Ethylbenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Hexachlorobutadiene ND 0.0018 0.00092 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 2-Hexanone (MBK) ND 0.018 0.010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Isopropylbenzene (Cumene) ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF p-Isopropyltoluene (p-Cymene) ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0037 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Methylene Chloride ND 0.018 0.0065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 4-Methyl-2-pentanone (MIBK) ND 0.018 0.0070 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Naphthalene ND 0.0037 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF n-Propylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Styrene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0018 0.0016 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 11:36 MFF 1,1,2,2-Tetrachloroethane ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Tetrachloroethylene ND 0.0018 0.0012 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 11:36 MFF Tetrahydrofuran ND 0.0092 0.0020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Toluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,2,3-Trichlorobenzene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,2,4-Trichlorobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,3,5-Trichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1, 1, 1 -Trichloroethane ND 0.0018 0.00092 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,1,2-Trichloroethane ND 0.0018 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Trichloroethylene 0.0011 0.0018 0.00092 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 11:36 MFF Trichlorofluoromethane (Freon 11) ND 0.0092 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,2,3-Trichloropropane ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0092 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF 1,3,5-Trimethylbenzene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Vinyl Chloride ND 0.0092 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF m+p Xylene ND 0.0037 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF o-Xylene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 11:36 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 105 70-130 9/28/18 11:36 Toluene-d8 101 70-130 9/28/18 11:36 4-Bromofluorobenzene 107 70-130 9/28/18 11:36 Page 48 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-7 Samnle ID: 1811008-07 Start Date/Time: 9/21/2018 11:45:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 11:50:OOAM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.22 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Acenaphthylene ND 0.22 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Acetophenone ND 0.44 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Aniline ND 0.44 0.12 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Anthracene ND 0.22 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Benzidine ND 0.85 0.55 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Benzo(a)anthracene ND 0.22 0.058 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Benzo(a)pyrene ND 0.22 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Benzo(b)fluoranthene ND 0.22 0.062 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Benzo(g,h,i)perylene ND 0.22 0.096 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Benzo(k)fluoranthene ND 0.22 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Benzoic Acid ND 1.3 0.23 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Bis(2-chloroethoxy)methane ND 0.44 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Bis(2-chloroethyl)ether ND 0.44 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Bis(2-chloroisopropyl)ether ND 0.44 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Bis(2-Ethylhexyl)phthalate ND 0.44 0.17 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 4-Bromophenylphenylether ND 0.44 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Butylbenzylphthalate ND 0.44 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Carbazole ND 0.22 0.057 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 4-Chloroaniline ND 0.85 0.10 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 4-Chloro-3-methylphenol ND 0.85 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2-Chloronaphthalene ND 0.44 0.082 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2-Chlorophenol ND 0.44 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 4-Chlorophenylphenylether ND 0.44 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Chrysene ND 0.22 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Dibenz(a,h)anthracene ND 0.22 0.13 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Dibenzofman ND 0.44 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Di-n-butylphthalate ND 0.44 0.095 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 1,2-Dichlorobenzene ND 0.44 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 1,3-Dichlorobenzene ND 0.44 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 1,4-Dichlorobenzene ND 0.44 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 3,3-Dichlorobenzidine ND 0.22 0.067 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2,4-Dichlorophenol ND 0.44 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Diethylphthalate ND 0.44 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2,4-Dimethylphenol ND 0.44 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Dimethylphthalate ND 0.44 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 4,6-Dinitro-2-methylphenol ND 0.44 0.42 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2,4-Dinitrophenol ND 0.85 0.25 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2,4-Dinitrotoluene ND 0.44 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2,6-Dinitrotoluene ND 0.44 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Di-n-octylphthalate ND 0.44 0.23 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.44 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Flumanthene ND 0.22 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Flumene ND 0.22 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Page 49 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-7 Samnle ID: 1811008-07 Start Date/Time: 9/21/2018 11:45:OOAM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 11:50:OOAM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.44 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Hexachlorobutadiene ND 0.44 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Hexachlorocyclopentadiene ND 0.44 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Hexachloroethane ND 0.44 0.087 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Indeno(1,2,3-cd)pyrene ND 0.22 0.16 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Isophorone ND 0.44 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 1-Methylnaphthalene ND 0.22 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2-Methylnaphthalene ND 0.22 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2-Methylphenol ND 0.44 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 3/4-Methylphenol ND 0.44 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Naphthalene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2-Nitroaniline ND 0.44 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 3-Nitroaniline ND 0.44 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 4-Nitroaniline ND 0.44 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Nitrobenzene ND 0.44 0.082 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2-Nitrophenol ND 0.44 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 4-Nitrophenol ND 0.85 0.095 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL N-Nitrosodimethylamine ND 0.44 0.28 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL N-Nitrosodiphenylamine ND 0.44 0.090 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL N-Nitrosodi-n-propylamine ND 0.44 0.090 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Pentachloronitrobenzene ND 0.44 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Pentachlorophenol ND 0.44 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Phenanthrene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Phenol ND 0.44 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Pyrene ND 0.22 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Pyridine ND 0.44 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 1,2,4,5-Tetrachlorobenzene ND 0.44 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 1,2,4-Trichlorobenzene ND 0.44 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2,4,5-Trichlorophenol ND 0.44 0.099 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL 2,4,6-Trichlorophenol ND 0.44 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:11 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 52.2 30-130 9/26/18 19:11 Phenol-d6 53.5 30-130 9/26/18 19:11 Nitrobenzene-d5 55.2 30-130 9/26/18 19:11 2-Fluorobiphenyl 58.5 30-130 9/26/18 19:11 2,4,6-Tribromophenol 65.9 30-130 9/26/18 19:11 p-Terphenyl-dl4 65.4 30-130 9/26/18 19:11 Page 50 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-7 Sample ID: 1811008-07 Start Date/Time: 9/21/2018 11:45:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 11:50:OOAM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 1.1 0.21 0.034 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:47 MJH Chromium 36 5.2 0.19 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:47 MJH Lead 7.5 2.1 0.069 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:47 MJH Mercury 0.036 0.034 0.0034 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:31 EJB Selenium ND 0.88 0.059 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:47 MJH Silver 0.050 0.092 0.0033 mg/Kg dry 5 J SW-846 6020B 10/1/18 10/2/18 11:47 MJH Barium 100 10 0.43 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:47 MJH Cadmium ND 0.40 0.013 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:47 MJH Page 51 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-7 Samnle ID: 1811008-07 Start Date/Time: 9/21/2018 11:45:OOAM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 11:50:OOAM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium % Solids 0.41 0.41 0.10 mg/Kg dry 2 77.8 % Wt 1 SW-846 7196A 9/27/18 9/28/18 10:42 MMH SM 2540G 10/1/18 10/1/18 21:49 DMP Page 52 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 Sample ID: 1811008-08 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 12:25:OOPM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.047 0.091 0.021 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 12:01 MFF Acrylonitrile ND 0.0055 0.0023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF tert-Amyl Methyl Ether (TAME) ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Benzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Bromobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Bromochloromethane ND 0.0018 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Bromodichloromethane ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Bromoform ND 0.0018 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Bromomethane ND 0.0091 0.0038 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 2-Butanone (MEK) ND 0.036 0.016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF tert-Butyl Alcohol (TBA) ND 0.036 0.019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF n-Butylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF sec-Butylbenzene ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF tert-Butylbenzene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00091 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Carbon Disulfide ND 0.0055 0.0039 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Carbon Tetrachloride ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Chlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Chlorodibromomethane ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Chloroethane ND 0.018 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Chloroform ND 0.0036 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Chloromethane ND 0.0091 0.0058 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 12:01 MFF 2-Chlorotoluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 4-Chlorotoluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,2-Dibromoethane (EDB) ND 0.00091 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Dibromomethane ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,2-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,3-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,4-Dichlorobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF trans-1,4-Dichloro-2-butene ND 0.0036 0.0019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Dichlorodifluoromethane (Freon 12) ND 0.018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,1-Dichloroethane ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,2-Dichloroethane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,1-Dichloroethylene ND 0.0036 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF cis-1,2-Dichloroethylene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF trans-1,2-Dichloroethylene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,2-Dichloropropane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,3-Dichloropropane ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 2,2-Dichloropropane ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,1-Dichloropropene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF cis-1,3-Dichloropropene ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF trans-1,3-Dichloropropene ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Diethyl Ether ND 0.018 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Page 53 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 Sample ID: 1811008-08 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 12:25:OOPM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPS) ND 0.00091 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,4-Dioxane ND 0.091 0.052 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Ethylbenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Hexachlorobutadiene ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 2-Hexanone (MBK) ND 0.018 0.0099 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Isopropylbenzene (Cumene) ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF p-Isopropyltoluene (p-Cymene) ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0036 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Methylene Chloride ND 0.018 0.0065 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 4-Methyl-2-pentanone (MIBK) ND 0.018 0.0069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Naphthalene ND 0.0036 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF n-Propylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Styrene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0018 0.0016 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 12:01 MFF 1,1,2,2-Tetrachloroethane ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Tetrachloroethylene ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Tetrahydrofiran ND 0.0091 0.0020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Toluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,2,3-Trichlorobenzene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,2,4-Trichlorobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,3,5-Trichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1, 1, 1 -Trichloroethane ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,1,2-Trichloroethane ND 0.0018 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Trichloroethylene ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Trichlorofluoromethane (Freon 11) ND 0.0091 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,2,3-Trichloropropane ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0091 0.00082 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF 1,3,5-Trimethylbenzene ND 0.0018 0.00055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Vinyl Chloride ND 0.0091 0.0010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF m+p Xylene ND 0.0036 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF o-Xylene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:01 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 108 70-130 9/28/18 12:01 Toluene-d8 101 70-130 9/28/18 12:01 4-Bromofluorobenzene 103 70-130 9/28/18 12:01 Page 54 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 Sample ID: 1811008-08 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 12:25:OOPM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.19 0.058 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Acenaphthylene ND 0.19 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Acetophenone ND 0.39 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Aniline ND 0.39 0.11 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Anthracene ND 0.19 0.056 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Benzidine ND 0.76 0.49 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Benzo(a)anthracene ND 0.19 0.051 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Benzo(a)pyrene ND 0.19 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Benzo(b)fluoranthene ND 0.19 0.055 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Benzo(g,h,i)perylene ND 0.19 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Benzo(k)fluoranthene ND 0.19 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Benzoic Acid ND 1.1 0.21 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Bis(2-chloroethoxy)methane ND 0.39 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Bis(2-chloroethyl)ether ND 0.39 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Bis(2-chloroisopropyl)ether ND 0.39 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Bis(2-Ethylhexyl)phthalate ND 0.39 0.15 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 4-Bromophenylphenylether ND 0.39 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Butylbenzylphthalate ND 0.39 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Carbazole ND 0.19 0.050 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 4-Chloroaniline ND 0.76 0.089 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 4-Chloro-3-methylphenol ND 0.76 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2-Chloronaphthalene ND 0.39 0.073 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2-Chlorophenol ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 4-Chlorophenylphenylether ND 0.39 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Chrysene ND 0.19 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Dibenz(a,h)anthracene ND 0.19 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Dibenzofman ND 0.39 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Di-n-butylphthalate ND 0.39 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 1,2-Dichlorobenzene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 1,3-Dichlorobenzene ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 1,4-Dichlorobenzene ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 3,3-Dichlorobenzidine ND 0.19 0.059 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2,4-Dichlorophenol ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Diethylphthalate ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2,4-Dimethylphenol ND 0.39 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Dimethylphthalate ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 4,6-Dinitro-2-methylphenol ND 0.39 0.37 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2,4-Dinitrophenol ND 0.76 0.22 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2,4-Dinitrotoluene ND 0.39 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2,6-Dinitrotoluene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Di-n-octylphthalate ND 0.39 0.20 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.39 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Flumanthene ND 0.19 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Flumene ND 0.19 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Page 55 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 Sample ID: 1811008-08 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Stoo Date/Time: 9/21/2018 12:25:OOPM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Hexachlorobutadiene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Hexachlorocyclopentadiene ND 0.39 0.082 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Hexachloroethane ND 0.39 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Indeno(1,2,3-cd)pyrene ND 0.19 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Isophorone ND 0.39 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 1-Methylnaphthalene ND 0.19 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2-Methylnaphthalene ND 0.19 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2-Methylphenol ND 0.39 0.097 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 3/4-Methylphenol ND 0.39 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Naphthalene ND 0.19 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2-Nitroaniline ND 0.39 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 3-Nitroaniline ND 0.39 0.056 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 4-Nitroaniline ND 0.39 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Nitrobenzene ND 0.39 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2-Nitrophenol ND 0.39 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 4-Nitrophenol ND 0.76 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL N-Nitrosodimethylamine ND 0.39 0.25 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL N-Nitrosodiphenylamine ND 0.39 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL N-Nitrosodi-n-propylamine ND 0.39 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Pentachloronitrobenzene ND 0.39 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Pentachlorophenol ND 0.39 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Phenanthrene ND 0.19 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Phenol ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Pyrene ND 0.19 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Pyridine ND 0.39 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 1,2,4,5-Tetrachlorobenzene ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 1,2,4-Trichlorobenzene ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2,4,5-Trichlorophenol ND 0.39 0.088 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL 2,4,6-Trichlorophenol ND 0.39 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 19:41 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 46.6 30-130 9/26/18 19:41 Phenol-d6 48.0 30-130 9/26/18 19:41 Nitrobenzene-d5 48.5 30-130 9/26/18 19:41 2-Fluorobiphenyl 53.0 30-130 9/26/18 19:41 2,4,6-Tribromophenol 57.4 30-130 9/26/18 19:41 p-Terphenyl-dl4 57.5 30-130 9/26/18 19:41 Page 56 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-8 Sample ID: 1811008-08 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 12:25:OOPM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 0.73 0.19 0.032 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:50 MJH Chromium 60 4.8 0.17 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:50 MJH Lead 11 1.9 0.064 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:50 MJH Mercury 0.030 0.029 0.0029 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:33 EJB Selenium ND 0.81 0.055 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:50 MJH Silver 0.087 0.085 0.0031 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:50 MJH Barium 92 9.7 0.39 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:50 MJH Cadmium 0.016 0.37 0.012 mg/Kg dry 5 J SW-846 6020B 10/1/18 10/2/18 11:50 MJH Page 57 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 Sample ID: 1811008-08 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 12:25:OOPM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium % Solids 0.61 0.37 0.093 mg/Kg dry 2 86.3 % Wt 1 SW-846 7196A 9/27/18 9/28/18 10:42 MMH SM 2540G 10/1/18 10/1/18 21:49 DMP Page 58 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-9 Samnle ID: 1811008-09 Start Date/Time: 9/21/2018 12:40:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 12:45:OOPM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.034 0.099 0.023 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 12:25 MFF Acrylonitrile ND 0.0059 0.0025 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF tert-Amyl Methyl Ether (TAME) ND 0.00099 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Benzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Bromobenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Bromochloromethane ND 0.0020 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Bromodichloromethane ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Bromoform ND 0.0020 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Bromomethane ND 0.0099 0.0042 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 2-Butanone (MEK) ND 0.040 0.017 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF tert-Butyl Alcohol (TBA) ND 0.040 0.021 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF n-Butylbenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF sec-Butylbenzene ND 0.0020 0.00099 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF tert-Butylbenzene ND 0.0020 0.00089 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00099 0.00059 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Carbon Disulfide ND 0.0059 0.0043 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Carbon Tetrachloride ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Chlorobenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Chlorodibromomethane ND 0.00099 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Chloroethane ND 0.020 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Chloroform ND 0.0040 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Chloromethane ND 0.0099 0.0063 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 12:25 MFF 2-Chlorotoluene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 4-Chlorotoluene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0020 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,2-Dibromoethane (EDB) ND 0.00099 0.00099 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Dibromomethane ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,2-Dichlorobenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,3-Dichlorobenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,4-Dichlorobenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF trans-1,4-Dichloro-2-butene ND 0.0040 0.0021 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Dichlorodifluoromethane (Freon 12) ND 0.020 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,1-Dichloroethane ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,2-Dichloroethane ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,1-Dichloroethylene ND 0.0040 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF cis-1,2-Dichloroethylene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF trans-1,2-Dichloroethylene ND 0.0020 0.00089 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,2-Dichloropropane ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,3-Dichloropropane ND 0.00099 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 2,2-Dichloropropane ND 0.0020 0.00089 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,1-Dichloropropene ND 0.0020 0.00089 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF cis-1,3-Dichloropropene ND 0.00099 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF trans-1,3-Dichloropropene ND 0.00099 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Diethyl Ether ND 0.020 0.0018 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Page 59 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-9 Samnle ID: 1811008-09 Start Date/Time: 9/21/2018 12:40:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 12:45:OOPM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.00099 0.00059 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,4-Dioxane ND 0.099 0.057 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Ethylbenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Hexachlorobutadiene ND 0.0020 0.00099 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 2-Hexanone (MBK) ND 0.020 0.011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Isopropylbenzene (Cumene) ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF p-Isopropyltoluene (p-Cymene) ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0040 0.00089 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Methylene Chloride ND 0.020 0.0070 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 4-Methyl-2-pentanone (MIBK) ND 0.020 0.0075 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Naphthalene ND 0.0040 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF n-Propylbenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Styrene ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0020 0.0018 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 12:25 MFF 1,1,2,2-Tetrachloroethane ND 0.0020 0.00089 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Tetrachloroethylene ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Tetrahydrofuran ND 0.0099 0.0022 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Toluene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,2,3-Trichlorobenzene ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,2,4-Trichlorobenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,3,5-Trichlorobenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1, 1, 1 -Trichloroethane ND 0.0020 0.00099 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,1,2-Trichloroethane ND 0.0020 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Trichloroethylene ND 0.0020 0.00099 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Trichlorofluoromethane (Freon 11) ND 0.0099 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,2,3-Trichloropropane ND 0.0020 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0099 0.00089 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF 1,3,5-Trimethylbenzene ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Vinyl Chloride ND 0.0099 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF m+p Xylene ND 0.0040 0.0017 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF o-Xylene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:25 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 104 70-130 9/28/18 12:25 Toluene-d8 102 70-130 9/28/18 12:25 4-Bromofluorobenzene 104 70-130 9/28/18 12:25 Page 60 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-9 Samnle ID: 1811008-09 Start Date/Time: 9/21/2018 12:40:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 12:45:OOPM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.21 0.062 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Acenaphthylene ND 0.21 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Acetophenone ND 0.42 0.082 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Aniline ND 0.42 0.12 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Anthracene ND 0.21 0.060 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Benzidine ND 0.81 0.52 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Benzo(a)anthracene ND 0.21 0.055 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Benzo(a)pyrene ND 0.21 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Benzo(b)fluoranthene 0.065 0.21 0.059 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 20:11 BGL Benzo(g,h,i)perylene ND 0.21 0.092 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Benzo(k)fluoranthene ND 0.21 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Benzoic Acid ND 1.2 0.22 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Bis(2-chloroethoxy)methane ND 0.42 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Bis(2-chloroethyl)ether ND 0.42 0.082 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Bis(2-chloroisopropyl)ether ND 0.42 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Bis(2-Ethylhexyl)phthalate ND 0.42 0.16 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 4-Bromophenylphenylether ND 0.42 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Butylbenzylphthalate ND 0.42 0.099 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Carbazole ND 0.21 0.054 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 4-Chloroaniline ND 0.81 0.095 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 4-Chloro-3-methylphenol ND 0.81 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2-Chloronaphthalene ND 0.42 0.078 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2-Chlorophenol ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 4-Chlorophenylphenylether ND 0.42 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Chrysene ND 0.21 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Dibenz(a,h)anthracene ND 0.21 0.13 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Dibenzofman ND 0.42 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Di-n-butylphthalate ND 0.42 0.091 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 1,2-Dichlorobenzene ND 0.42 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 1,3-Dichlorobenzene ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 1,4-Dichlorobenzene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 3,3-Dichlorobenzidine ND 0.21 0.064 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2,4-Dichlorophenol ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Diethylphthalate ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2,4-Dimethylphenol ND 0.42 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Dimethylphthalate ND 0.42 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 4,6-Dinitro-2-methylphenol ND 0.42 0.40 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2,4-Dinitrophenol ND 0.81 0.24 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2,4-Dinitrotoluene ND 0.42 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2,6-Dinitrotoluene ND 0.42 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Di-n-octylphthalate ND 0.42 0.22 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.42 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Flumanthene 0.094 0.21 0.069 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 20:11 BGL Flumene ND 0.21 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Page 61 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-9 Samnle ID: 1811008-09 Start Date/Time: 9/21/2018 12:40:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 12:45:OOPM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.42 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Hexachlorobutadiene ND 0.42 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Hexachlorocyclopentadiene ND 0.42 0.088 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Hexachloroethane ND 0.42 0.083 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Indeno(1,2,3-cd)pyrene ND 0.21 0.15 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Isophorone ND 0.42 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 1-Methylnaphthalene ND 0.21 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2-Methylnaphthalene ND 0.21 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2-Methylphenol ND 0.42 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 3/4-Methylphenol ND 0.42 0.13 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Naphthalene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2-Nitroaniline ND 0.42 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 3-Nitroaniline ND 0.42 0.060 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 4-Nitroaniline ND 0.42 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Nitrobenzene ND 0.42 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2-Nitrophenol ND 0.42 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 4-Nitrophenol ND 0.81 0.091 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL N-Nitrosodimethylamine ND 0.42 0.26 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL N-Nitrosodiphenylamine ND 0.42 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL N-Nitrosodi-n-propylamine ND 0.42 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Pentachloronitrobenzene ND 0.42 0.099 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Pentachlorophenol ND 0.42 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Phenanthrene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Phenol ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Pyrene 0.082 0.21 0.069 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 20:11 BGL Pyridine ND 0.42 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 1,2,4,5-Tetrachlorobenzene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 1,2,4-Trichlorobenzene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2,4,5-Trichlorophenol ND 0.42 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL 2,4,6-Trichlorophenol ND 0.42 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:11 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 55.2 30-130 9/26/18 20:11 Phenol-d6 57.5 30-130 9/26/18 20:11 Nitrobenzene-d5 56.2 30-130 9/26/18 20:11 2-Fluorobiphenyl 60.3 30-130 9/26/18 20:11 2,4,6-Tribromophenol 63.0 30-130 9/26/18 20:11 p-Terphenyl-dl4 65.2 30-130 9/26/18 20:11 Page 62 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-9 Sample ID: 1811008-09 Start Date/Time: 9/21/2018 12:40:OOPM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 12:45:OOPM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 1.7 0.20 0.033 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:54 MJH Chromium 49 5.0 0.18 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:54 MJH Lead 15 2.0 0.066 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:54 MJH Mercury 0.042 0.031 0.0031 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:34 EJB Selenium ND 0.84 0.057 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:54 MJH Silver 0.059 0.088 0.0032 mg/Kg dry 5 J SW-846 6020B 10/1/18 10/2/18 11:54 MJH Barium 140 40 1.6 mg/Kg dry 20 SW-846 6020B 10/1/18 10/2/18 12:31 MJH Cadmium ND 0.38 0.013 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:54 MJH Page 63 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-9 Samnle ID: 1811008-09 Start Date/Time: 9/21/2018 12:40:OOPM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 12:45:OOPM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium % Solids 0.51 0.38 0.096 mg/Kg dry 2 80.6 % Wt 1 SW-846 7196A 9/27/18 9/28/18 10:42 MMH SM 2540G 10/1/18 10/1/18 21:49 DMP Page 64 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-10 Samnle ID: 1811008-10 Start Date/Time: 9/21/2018 1:00:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 1:05:OOPM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.026 0.11 0.026 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 12:46 MFF Acrylonitrile ND 0.0066 0.0027 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF tert-Amyl Methyl Ether (TAME) ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Benzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Bromobenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Bromochloromethane ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Bromodichloromethane ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Bromoform ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Bromomethane ND 0.011 0.0046 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 2-Butanone (MEK) ND 0.044 0.019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF tert-Butyl Alcohol (TBA) ND 0.044 0.023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF n-Butylbenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF sec-Butylbenzene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF tert-Butylbenzene ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0011 0.00066 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Carbon Disulfide ND 0.0066 0.0047 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Carbon Tetrachloride ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Chlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Chlorodibromomethane ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Chloroethane ND 0.022 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Chloroform ND 0.0044 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Chloromethane ND 0.011 0.0070 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 12:46 MFF 2-Chlorotoluene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 4-Chlorotoluene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,2-Dibromoethane (EDB) ND 0.0011 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Dibromomethane ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,2-Dichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,3-Dichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,4-Dichlorobenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF trans-1,4-Dichloro-2-butene ND 0.0044 0.0023 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Dichlorodifluoromethane (Freon 12) ND 0.022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,1-Dichloroethane ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,2-Dichloroethane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1, 1 -Dichloroethylene ND 0.0044 0.0012 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 12:46 MFF cis-1,2-Dichloroethylene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF trans-1,2-Dichloroethylene ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,2-Dichloropropane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,3-Dichloropropane ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 2,2-Dichloropropane ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,1-Dichloropropene ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF cis-1,3-Dichloropropene ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF trans-1,3-Dichloropropene ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Diethyl Ether ND 0.022 0.0020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Page 65 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-10 Samnle ID: 1811008-10 Start Date/Time: 9/21/2018 1:00:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 1:05:OOPM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0011 0.00066 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,4-Dioxane ND 0.11 0.063 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Ethylbenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Hexachlorobutadiene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 2-Hexanone (MBK) ND 0.022 0.012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Isopropylbenzene (Cumene) ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF p-Isopropyltoluene (p-Cymene) ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0044 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Methylene Chloride ND 0.022 0.0078 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 4-Methyl-2-pentanone (MIBK) ND 0.022 0.0083 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Naphthalene ND 0.0044 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF n-Propylbenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Styrene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0022 0.0020 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 12:46 MFF 1,1,2,2-Tetrachloroethane ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Tetrachloroethylene ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Tetrahydrofuran ND 0.011 0.0024 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Toluene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,2,3-Trichlorobenzene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,2,4-Trichlorobenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,3,5-Trichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1, 1, 1 -Trichloroethane ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,1,2-Trichloroethane ND 0.0022 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Trichloroethylene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Trichlorofluoromethane (Freon 11) ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,2,3-Trichloropropane ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.011 0.00098 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF 1,3,5-Trimethylbenzene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Vinyl Chloride ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF m+p Xylene ND 0.0044 0.0019 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF o-Xylene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 12:46 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 102 70-130 9/28/18 12:46 Toluene-d8 101 70-130 9/28/18 12:46 4-Bromofluorobenzene 105 70-130 9/28/18 12:46 Page 66 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-10 Samnle ID: 1811008-10 Start Date/Time: 9/21/2018 1:00:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 1:05:OOPM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.23 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Acenaphthylene ND 0.23 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Acetophenone ND 0.45 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Aniline ND 0.45 0.13 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Anthracene ND 0.23 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Benzidine ND 0.88 0.57 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Benzo(a)anthracene ND 0.23 0.060 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Benzo(a)pyrene ND 0.23 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Benzo(b)fluoranthene 0.13 0.23 0.064 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 20:40 BGL Benzo(g,h,i)perylene ND 0.23 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Benzo(k)fluoranthene ND 0.23 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Benzoic Acid 0.32 1.3 0.24 mg/Kg dry 1 V-20, J SW-846 8270D 9/25/18 9/26/18 20:40 BGL Bis(2-chloroethoxy)methane ND 0.45 0.087 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Bis(2-chloroethyl)ether ND 0.45 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Bis(2-chloroisopropyl)ether ND 0.45 0.097 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Bis(2-Ethylhexyl)phthalate ND 0.45 0.18 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 4-Bromophenylphenylether ND 0.45 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Butylbenzylphthalate ND 0.45 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Carbazole ND 0.23 0.059 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 4-Chloroaniline ND 0.88 0.10 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 4-Chloro-3-methylphenol ND 0.88 0.097 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2-Chloronaphthalene ND 0.45 0.085 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2-Chlorophenol ND 0.45 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 4-Chlorophenylphenylether ND 0.45 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Chrysene ND 0.23 0.071 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Dibenz(a,h)anthracene ND 0.23 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Dibenzofman ND 0.45 0.079 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Di-n-butylphthalate ND 0.45 0.099 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 1,2-Dichlorobenzene ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 1,3-Dichlorobenzene ND 0.45 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 1,4-Dichlorobenzene ND 0.45 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 3,3-Dichlorobenzidine ND 0.23 0.069 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2,4-Dichlorophenol ND 0.45 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Diethylphthalate ND 0.45 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2,4-Dimethylphenol ND 0.45 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Dimethylphthalate ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 4,6-Dinitro-2-methylphenol ND 0.45 0.43 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2,4-Dinitrophenol ND 0.88 0.26 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2,4-Dinitrotoluene ND 0.45 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2,6-Dinitrotoluene ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Di-n-octylphthalate ND 0.45 0.24 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.45 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Flumanthene ND 0.23 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Flumene ND 0.23 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Page 67 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-10 Samnle ID: 1811008-10 Start Date/Time: 9/21/2018 1:00:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 1:05:OOPM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Hexachlorobutadiene ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Hexachlorocyclopentadiene ND 0.45 0.096 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Hexachloroethane ND 0.45 0.091 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Indeno(1,2,3-cd)pyrene ND 0.23 0.16 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Isophorone ND 0.45 0.088 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 1-Methylnaphthalene ND 0.23 0.087 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2-Methylnaphthalene ND 0.23 0.079 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2-Methylphenol ND 0.45 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 3/4-Methylphenol ND 0.45 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Naphthalene ND 0.23 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2-Nitroaniline ND 0.45 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 3-Nitroaniline ND 0.45 0.065 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 4-Nitroaniline ND 0.45 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Nitrobenzene ND 0.45 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2-Nitrophenol ND 0.45 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 4-Nitrophenol ND 0.88 0.099 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL N-Nitrosodimethylamine ND 0.45 0.29 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL N-Nitrosodiphenylamine ND 0.45 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL N-Nitrosodi-n-propylamine ND 0.45 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Pentachloronitrobenzene ND 0.45 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Pentachlorophenol ND 0.45 0.11 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Phenanthrene ND 0.23 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Phenol ND 0.45 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Pyrene 0.082 0.23 0.075 mg/Kg dry 1 J SW-846 8270D 9/25/18 9/26/18 20:40 BGL Pyridine ND 0.45 0.073 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 1,2,4,5-Tetrachlorobenzene ND 0.45 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 1,2,4-Trichlorobenzene ND 0.45 0.081 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2,4,5-Trichlorophenol ND 0.45 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL 2,4,6-Trichlorophenol ND 0.45 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 20:40 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 70.2 30-130 9/26/18 20:40 Phenol-d6 71.8 30-130 9/26/18 20:40 Nitrobenzene-d5 71.0 30-130 9/26/18 20:40 2-Fluorobiphenyl 75.9 30-130 9/26/18 20:40 2,4,6-Tribromophenol 87.8 30-130 9/26/18 20:40 p-Terphenyl-dl4 81.3 30-130 9/26/18 20:40 Page 68 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-10 Sample ID: 18I1008-10 Start Date/Time: 9/21/2018 1:00:OOPM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 1:05:OOPM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 240 0.86 0.14 mg/Kg dry 20 SW-846 6020B 10/1/18 10/2/18 12:35 MJH Chromium 55 5.4 0.19 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:57 MJH Lead 19 2.1 0.070 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:57 MJH Mercury 0.019 0.034 0.0034 mg/Kg dry 1 J SW-846 7471B 9/28/18 10/1/18 13:36 EJB Selenium ND 0.90 0.061 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:57 MJH Silver 0.038 0.094 0.0034 mg/Kg dry 5 J SW-846 6020B 10/1/18 10/2/18 11:57 MJH Barium 46 11 0.44 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:57 MJH Cadmium 0.80 0.41 0.014 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 11:57 MJH Page 69 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-10 Samnle ID: 1811008-10 Start Date/Time: 9/21/2018 1:00:OOPM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 1:05:OOPM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium % Solids 2.9 0.41 0.10 mg/Kg dry 2 74.8 % Wt 1 SW-846 7196A 9/27/18 9/28/18 10:42 MMH SM 2540G 10/1/18 10/1/18 21:49 DMP Page 70 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 DUP Samnle ID: 1811008-11 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 12:25:OOPM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 0.045 0.096 0.022 mg/Kg dry 1 J SW-846 8260B 9/28/18 9/28/18 13:11 MFF Acrylonitrile ND 0.0057 0.0024 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF tert-Amyl Methyl Ether (TAME) ND 0.00096 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Benzene ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Bromobenzene ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Bromochloromethane ND 0.0019 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Bromodichloromethane ND 0.0019 0.00057 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Bromoform ND 0.0019 0.0013 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Bromomethane ND 0.0096 0.0040 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 2-Butanone (MEK) ND 0.038 0.017 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF tert-Butyl Alcohol (TBA) ND 0.038 0.020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF n-Butylbenzene ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF sec-Butylbenzene ND 0.0019 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF tert-Butylbenzene ND 0.0019 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00096 0.00057 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Carbon Disulfide ND 0.0057 0.0041 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Carbon Tetrachloride ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Chlorobenzene ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Chlorodibromomethane ND 0.00096 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Chloroethane ND 0.019 0.0014 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Chloroform ND 0.0038 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Chloromethane ND 0.0096 0.0061 mg/Kg dry I SW-846 8260B 9/28/18 9/28/18 13:11 MFF 2-Chlorotoluene ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 4-Chlorotoluene ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0019 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,2-Dibromoethane (EDB) ND 0.00096 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Dibromomethane ND 0.0019 0.00057 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,2-Dichlorobenzene ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,3-Dichlorobenzene ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,4-Dichlorobenzene ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF trans-1,4-Dichloro-2-butene ND 0.0038 0.0020 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Dichlorodifluoromethane (Freon 12) ND 0.019 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,1-Dichloroethane ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,2-Dichloroethane ND 0.0019 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,1-Dichloroethylene ND 0.0038 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF cis-1,2-Dichloroethylene ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF trans-1,2-Dichloroethylene ND 0.0019 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,2-Dichloropropane ND 0.0019 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,3-Dichloropropane ND 0.00096 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 2,2-Dichloropropane ND 0.0019 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,1-Dichloropropene ND 0.0019 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF cis-1,3-Dichloropropene ND 0.00096 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF trans-1,3-Dichloropropene ND 0.00096 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Diethyl Ether ND 0.019 0.0017 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Page 71 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 DUP Samnle ID: 1811008-11 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 12:25:OOPM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPS) ND 0.00096 0.00057 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,4-Dioxane ND 0.096 0.055 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Ethylbenzene ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Hexachlorobutadiene ND 0.0019 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 2-Hexanone (MBK) ND 0.019 0.010 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Isopropylbenzene (Cumene) ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF p-Isopropyltoluene (p-Cymene) ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0038 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Methylene Chloride ND 0.019 0.0068 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 4-Methyl-2-pentanone (MIBK) ND 0.019 0.0073 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Naphthalene ND 0.0038 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF n-Propylbenzene ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Styrene ND 0.0019 0.00057 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0019 0.0017 mg/Kg dry 1 SW-8468260B 9/28/18 9/28/18 13:11 MFF 1,1,2,2-Tetrachloroethane ND 0.0019 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Tetrachloroethylene ND 0.0019 0.0012 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Tetrahydrofiran ND 0.0096 0.0021 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Toluene ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,2,3-Trichlorobenzene ND 0.0019 0.00057 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,2,4-Trichlorobenzene ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,3,5-Trichlorobenzene ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1, 1, 1 -Trichloroethane ND 0.0019 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,1,2-Trichloroethane ND 0.0019 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Trichloroethylene ND 0.0019 0.00096 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Trichlorofluoromethane (Freon 11) ND 0.0096 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,2,3-Trichloropropane ND 0.0019 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0096 0.00086 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0019 0.00077 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF 1,3,5-Trimethylbenzene ND 0.0019 0.00057 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Vinyl Chloride ND 0.0096 0.0011 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF m+p Xylene ND 0.0038 0.0016 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF o-Xylene ND 0.0019 0.00067 mg/Kg dry 1 SW-846 8260B 9/28/18 9/28/18 13:11 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 106 70-130 9/28/18 13:11 Toluene-d8 101 70-130 9/28/18 13:11 4-Bromofluorobenzene 104 70-130 9/28/18 13:11 Page 72 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 DUP Samnle ID: 1811008-11 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 12:25:OOPM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.20 0.059 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Acenaphthylene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Acetophenone ND 0.39 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Aniline ND 0.39 0.11 mg/Kg dry 1 V-05, V-34 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Anthracene ND 0.20 0.056 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Benzidine ND 0.76 0.49 mg/Kg dry 1 V-34, R-05, V-05 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Benzo(a)anthracene ND 0.20 0.052 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Benzo(a)pyrene ND 0.20 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Benzo(b)fluoranthene ND 0.20 0.055 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Benzo(g,h,i)perylene ND 0.20 0.086 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Benzo(k)fluoranthene ND 0.20 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Benzoic Acid ND 1.1 0.21 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Bis(2-chloroethoxy)methane ND 0.39 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Bis(2-chloroethyl)ether ND 0.39 0.077 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Bis(2-chloroisopropyl)ether ND 0.39 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Bis(2-Ethylhexyl)phthalate ND 0.39 0.15 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 4-Bromophenylphenylether ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Butylbenzylphthalate ND 0.39 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Carbazole ND 0.20 0.051 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 4-Chloroaniline ND 0.76 0.090 mg/Kg dry 1 V-34 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 4-Chloro-3-methylphenol ND 0.76 0.084 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2-Chloronaphthalene ND 0.39 0.074 mg/Kg dry I SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2-Chlorophenol ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 4-Chlorophenylphenylether ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Chrysene ND 0.20 0.061 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Dibenz(a,h)anthracene ND 0.20 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Dibenzofman ND 0.39 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Di-n-butylphthalate ND 0.39 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 1,2-Dichlorobenzene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 1,3-Dichlorobenzene ND 0.39 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 1,4-Dichlorobenzene ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 3,3-Dichlorobenzidine ND 0.20 0.060 mg/Kg dry 1 V-20 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2,4-Dichlorophenol ND 0.39 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Diethylphthalate ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2,4-Dimethylphenol ND 0.39 0.072 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Dimethylphthalate ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 4,6-Dinitro-2-methylphenol ND 0.39 0.37 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2,4-Dinitrophenol ND 0.76 0.22 mg/Kg dry 1 V-19, V-20 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2,4-Dinitrotoluene ND 0.39 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2,6-Dinitrotoluene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Di-n-octylphthalate ND 0.39 0.20 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.39 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Flumanthene ND 0.20 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Flumene ND 0.20 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Page 73 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 DUP Samnle ID: 1811008-11 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Ston Date/Time: 9/21/2018 12:25:OOPM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Hexachlorobutadiene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Hexachlorocyclopentadiene ND 0.39 0.083 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Hexachloroethane ND 0.39 0.078 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Indeno(1,2,3-cd)pyrene ND 0.20 0.14 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Isophorone ND 0.39 0.076 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 1-Methylnaphthalene ND 0.20 0.075 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2-Methylnaphthalene ND 0.20 0.068 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2-Methylphenol ND 0.39 0.098 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 3/4-Methylphenol ND 0.39 0.12 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Naphthalene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2-Nitroaniline ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 3-Nitroaniline ND 0.39 0.056 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 4-Nitroaniline ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Nitrobenzene ND 0.39 0.074 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2-Nitrophenol ND 0.39 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 4-Nitrophenol ND 0.76 0.085 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL N-Nitrosodimethylamine ND 0.39 0.25 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL N-Nitrosodiphenylamine ND 0.39 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL N-Nitrosodi-n-propylamine ND 0.39 0.080 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Pentachloronitrobenzene ND 0.39 0.093 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Pentachlorophenol ND 0.39 0.094 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Phenanthrene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Phenol ND 0.39 0.067 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Pyrene ND 0.20 0.064 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Pyridine ND 0.39 0.063 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 1,2,4,5-Tetrachlorobenzene ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 1,2,4-Trichlorobenzene ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2,4,5-Trichlorophenol ND 0.39 0.089 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL 2,4,6-Trichlorophenol ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 9/25/18 9/26/18 21:10 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 54.2 30-130 9/26/18 21:10 Phenol-d6 56.4 30-130 9/26/18 21:10 Nitrobenzene-d5 56.2 30-130 9/26/18 21:10 2-Fluorobiphenyl 60.9 30-130 9/26/18 21:10 2,4,6-Tribromophenol 65.6 30-130 9/26/18 21:10 p-Terphenyl-dl4 67.1 30-130 9/26/18 21:10 Page 74 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: SB-8 DUP Sample ID: 1811008-11 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 12:25:OOPM Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 0.66 0.19 0.030 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 12:01 MJH Chromium 59 4.6 0.17 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 12:01 MJH Lead 8.1 1.9 0.061 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 12:01 MJH Mercury 0.028 0.027 0.0027 mg/Kg dry 1 SW-846 7471B 9/28/18 10/1/18 13:38 EJB Selenium ND 0.78 0.053 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 12:01 MJH Silver 0.071 0.082 0.0030 mg/Kg dry 5 J SW-846 6020B 10/1/18 10/2/18 12:01 MJH Barium 110 37 1.5 mg/Kg dry 20 SW-846 6020B 10/1/18 10/2/18 12:38 MJH Cadmium ND 0.35 0.012 mg/Kg dry 5 SW-846 6020B 10/1/18 10/2/18 12:01 MJH Page 75 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: SB-8 DUP Samnle ID: 1811008-11 Start Date/Time: 9/21/2018 12:20:OOPM Samnle Matrix: Soil Stop Date/Time: 9/21/2018 12:25:OOPM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium % Solids 0.60 0.37 0.091 mg/Kg dry 2 87.0 % Wt 1 SW-846 7196A 9/27/18 9/28/18 10:42 MMH SM 2540G 10/1/18 10/1/18 21:50 DMP Page 76 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-18 Sampled: 9/21/2018 14:30 Sample ID: 1811008-12 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 9.7 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Acrylonitrile ND 5.0 0.58 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF tert-Amyl Methyl Ether (TAME) 0.45 0.50 0.11 µg/L 1 J SW-846 8260B 9/25/18 9/25/18 17:19 MFF Benzene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Bromobenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Bromochloromethane ND 1.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Bromodichloromethane ND 0.50 0.30 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Bromoform ND 2.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Bromomethane ND 2.0 0.94 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 2-Butanone (MEK) ND 20 2.4 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF tert-Butyl Alcohol (TBA) ND 20 2.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF n-Butylbenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF sec-Butylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF tert-Butylbenzene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.50 0.095 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Carbon Disulfide ND 4.0 1.0 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Carbon Tetrachloride ND 5.0 0.25 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Chlorobenzene ND 1.0 0.16 µg/L I SW-846 8260B 9/25/18 9/25/18 17:19 MFF Chlorodibromomethane ND 0.50 0.10 µg/L I SW-846 8260B 9/25/18 9/25/18 17:19 MFF Chloroethane ND 2.0 0.28 µg/L I SW-846 8260B 9/25/18 9/25/18 17:19 MFF Chloroform ND 2.0 0.22 µg/L I SW-846 8260B 9/25/18 9/25/18 17:19 MFF Chloromethane ND 2.0 0.55 µg/L I SW-846 8260B 9/25/18 9/25/18 17:19 MFF 2-Chlorotoluene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 4-Chlorotoluene ND 1.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.37 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Dibromomethane ND 1.0 0.16 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,2-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,3-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,4-Dichlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Dichlorodifluoromethane (Freon 12) ND 2.0 0.28 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,2-Dichloroethane ND 1.0 0.19 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,1-Dichloroethylene ND 1.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF cis-1,2-Dichloroethylene 0.97 1.0 0.15 µg/L 1 J SW-846 8260B 9/25/18 9/25/18 17:19 MFF trans-1,2-Dichloroethylene 1.8 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,2-Dichloropropane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,3-Dichloropropane ND 0.50 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 2,2-Dichloropropane ND 1.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,1-Dichloropropene ND 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF cis-1,3-Dichloropropene ND 0.50 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF trans-1,3-Dichloropropene ND 0.50 0.11 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Diethyl Ether ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Page 77 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-18 Sampled: 9/21/2018 14:30 Sample ID: 1811008-12 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPS) 0.34 0.50 0.18 µg/L 1 J SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,4-Dioxane ND 50 26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Hexachlorobutadiene ND 0.60 0.59 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Isopropylbenzene (Cumene) ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF p-Isopropyltoluene (p-Cymene) ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Methyl tert-Butyl Ether (MTBE) 1.4 1.0 0.090 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Methylene Chloride ND 5.0 3.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 4-Methyl-2-pentanone (MIBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Naphthalene ND 2.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF n-Propylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Styrene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1, 1, 1,2-Tetrachloroethane ND 1.0 0.12 µg/L 1 SW-8468260B 9/25/18 9/25/18 17:19 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.16 µg/L 1 SW-8468260B 9/25/18 9/25/18 17:19 MFF Tetrachloroethylene ND 1.0 0.27 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Tetrahydrofirran ND 10 1.1 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Toluene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,2,3-Trichlorobenzene ND 5.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,2,4-Trichlorobenzene ND 1.0 0.19 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,3,5-Trichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1, 1, 1 -Trichloroethane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,1,2-Trichloroethane ND 1.0 0.24 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Trichloroethylene ND 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Trichlorofluoromethane (Freon 11) ND 2.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,2,3-Trichloropropane ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 1.0 0.18 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF 1,3,5-Trimethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Vinyl Chloride 2.8 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF m+p Xylene ND 2.0 0.26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF o-Xylene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:19 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 80.1 70-130 9/25/18 17:19 Toluene-d8 100 70-130 9/25/18 17:19 4-Bromofluorobenzene 97.9 70-130 9/25/18 17:19 Page 78 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-18 Sampled: 9/21/2018 14:30 Samnle ID: 1811008-12 Samnle Matrix: Ground Water Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 5.4 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Acenaphthylene ND 5.4 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Acetophenone ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Aniline ND 5.4 2.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Anthracene ND 5.4 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Benzidine ND 22 11 µg/L 1 V-04, V-05, V-34 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Benzo(a)anthracene ND 5.4 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Benzo(a)pyrene ND 5.4 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Benzo(b)fluoranthene ND 5.4 1.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Benzo(g,h,i)perylene ND 5.4 2.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Benzo(k)fluoranthene ND 5.4 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Benzoic Acid ND 11 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Bis(2-chloroethoxy)methane ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Bis(2-chloroethyl)ether ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Bis(2-chloroisopropyl)ether ND 11 2.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Bis(2-Ethylhexyl)phthalate ND 11 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 4-Bromophenylphenylether ND 11 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Butylbenzylphthalate ND 11 2.1 µg/L I SW-846 8270D 9/27/18 9/28/18 21:35 BGL Carbazole ND 11 1.7 µg/L I SW-846 8270D 9/27/18 9/28/18 21:35 BGL 4-Chloroaniline ND 11 1.6 µg/L I V-34 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 4-Chloro-3-methylphenol ND 11 1.5 µg/L I SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2-Chloronaphthalene ND 11 1.6 µg/L I SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2-Chlorophenol ND 11 1.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 4-Chlorophenylphenylether ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Chrysene ND 5.4 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Dibenz(a,h)anthracene ND 5.4 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Dibenzofman ND 5.4 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Di-n-butylphthalate ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 1,2-Dichlorobenzene ND 5.4 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 1,3-Dichlorobenzene ND 5.4 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 1,4-Dichlorobenzene ND 5.4 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 3,3-Dichlorobenzidine ND 11 2.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2,4-Dichlorophenol ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Diethylphthalate ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2,4-Dimethylphenol ND 11 4.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Dimethylphthalate ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 4,6-Dinitro-2-methylphenol ND 11 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2,4-Dinitrophenol ND 11 3.7 µg/L 1 V-04 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2,4-Dinitrotoluene ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2,6-Dinitrotoluene ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Di-n-octylphthalate ND 11 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 11 2.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Flumanthene ND 5.4 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Flumene ND 5.4 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Page 79 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-18 Sampled: 9/21/2018 14:30 Sample ID: 1811008-12 Samnle Matrix: Ground Water Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Hexachlorobutadiene ND 11 1.7 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Hexachlorocyclopentadiene ND 11 2.1 µg/L 1 L-04, V-04 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Hexachloroethane ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Indeno(1,2,3-cd)pyrene ND 5.4 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Isophorone ND 11 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 1-Methylnaphthalene ND 5.4 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2-Methylnaphthalene ND 5.4 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2-Methylphenol ND 11 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 3/4-Methylphenol ND 11 1.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Naphthalene ND 5.4 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2-Nitroaniline ND 11 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 3-Nitroaniline ND 11 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 4-Nitroaniline ND 11 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Nitrobenzene ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2-Nitrophenol ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 4-Nitrophenol ND 11 1.1 µg/L 1 V-20 SW-846 8270D 9/27/18 9/28/18 21:35 BGL N-Nitrosodimethylamine ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL N-Nitrosodiphenylamine ND 11 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL N-Nitrosodi-n-propylamine ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Pentachloronitrobenzene ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Pentachlorophenol ND 11 1.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Phenanthrene ND 5.4 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Phenol ND 11 1.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Pyrene ND 5.4 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Pyridine ND 5.4 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 1,2,4,5-Tetrachlorobenzene ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 1,2,4-Trichlorobenzene ND 5.4 1.7 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2,4,5-Trichlorophenol ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL 2,4,6-Trichlorophenol ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:35 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 47.6 15-110 9/28/18 21:35 Phenol-d6 31.7 15-110 9/28/18 21:35 Nitrobenzene-d5 61.4 30-130 9/28/18 21:35 2-Fluorobiphenyl 61.1 30-130 9/28/18 21:35 2,4,6-Tribromophenol 71.5 15-110 9/28/18 21:35 p-Terphenyl-dl4 79.3 30-130 9/28/18 21:35 Page 80 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: MW-18 Sampled: 9/21/2018 14:30 Sample ID: 18I1008-12 Samnle Matrix: Ground Water Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 1.1 0.80 0.72 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:52 MJH Barium 300 20 11 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:52 MJH Cadmium ND 1.0 0.19 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:52 MJH Chromium 5.4 2.0 1.0 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:52 MJH Lead 1.2 2.0 0.28 µg/L 2 J SW-846 6020B 9/28/18 10/2/18 8:52 MJH Mercury ND 0.00010 0.000034 mg/L 1 SW-846 7470A 9/26/18 9/28/18 11:47 EJB Selenium ND 10 4.2 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:52 MJH Silver ND 1.0 0.15 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:52 MJH Page 81 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-18 Sampled: 9/21/2018 14:30 Sample ID: 1811008-12 Samnle Matrix: Ground Water Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium 0.0014 0.0040 0.0010 mg/L 1 J SW-846 7196A 9/22/18 9/22/18 11:01 AA Page 82 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-24 Sampled: 9/21/2018 14:00 Sample ID: 18I1008-13 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 9.7 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Acrylonitrile ND 5.0 0.58 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF tert-Amyl Methyl Ether (TAME) ND 0.50 0.11 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Benzene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Bromobenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Bromochloromethane ND 1.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Bromodichloromethane ND 0.50 0.30 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Bromoform ND 2.0 0.21 µg/L I SW-846 8260B 9/25/18 9/25/18 17:45 MFF Bromomethane ND 2.0 0.94 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 2-Butanone (MEK) ND 20 2.4 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF tert-Butyl Alcohol (TBA) ND 20 2.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF n-Butylbenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF sec-Butylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF tert-Butylbenzene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.50 0.095 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Carbon Disulfide ND 4.0 1.0 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Carbon Tetrachloride ND 5.0 0.25 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Chlorobenzene ND 1.0 0.16 µg/L I SW-846 8260B 9/25/18 9/25/18 17:45 MFF Chlorodibromomethane ND 0.50 0.10 µg/L I SW-846 8260B 9/25/18 9/25/18 17:45 MFF Chloroethane ND 2.0 0.28 µg/L I SW-846 8260B 9/25/18 9/25/18 17:45 MFF Chloroform ND 2.0 0.22 µg/L I SW-846 8260B 9/25/18 9/25/18 17:45 MFF Chloromethane ND 2.0 0.55 µg/L I SW-846 8260B 9/25/18 9/25/18 17:45 MFF 2-Chlorotoluene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 4-Chlorotoluene ND 1.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.37 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Dibromomethane ND 1.0 0.16 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,2-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,3-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,4-Dichlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Dichlorodifluoromethane (Freon 12) ND 2.0 0.28 µg/L I SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,2-Dichloroethane ND 1.0 0.19 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,1-Dichloroethylene ND 1.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF cis-1,2-Dichloroethylene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF trans-1,2-Dichloroethylene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,2-Dichloropropane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,3-Dichloropropane ND 0.50 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 2,2-Dichloropropane ND 1.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,1-Dichloropropene ND 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF cis-1,3-Dichloropropene ND 0.50 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF trans-1,3-Dichloropropene ND 0.50 0.11 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Diethyl Ether ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Page 83 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-24 Sampled: 9/21/2018 14:00 Sample ID: 18I1008-13 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPS) ND 0.50 0.18 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,4-Dioxane ND 50 26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Hexachlorobutadiene ND 0.60 0.59 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Isopropylbenzene (Cumene) ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF p-Isopropyltoluene (p-Cymene) ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Methyl tert-Butyl Ether (MTBE) ND 1.0 0.090 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Methylene Chloride ND 5.0 3.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 4-Methyl-2-pentanone (MIBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Naphthalene ND 2.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF n-Propylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Styrene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1, 1, 1,2-Tetrachloroethane ND 1.0 0.12 µg/L 1 SW-8468260B 9/25/18 9/25/18 17:45 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.16 µg/L 1 SW-8468260B 9/25/18 9/25/18 17:45 MFF Tetrachloroethylene ND 1.0 0.27 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Tetrahydrofirran ND 10 1.1 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Toluene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,2,3-Trichlorobenzene ND 5.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,2,4-Trichlorobenzene ND 1.0 0.19 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,3,5-Trichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1, 1, 1 -Trichloroethane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,1,2-Trichloroethane ND 1.0 0.24 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Trichloroethylene ND 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Trichlorofluoromethane (Freon 11) ND 2.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,2,3-Trichloropropane ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 1.0 0.18 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF 1,3,5-Trimethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Vinyl Chloride ND 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF m+p Xylene ND 2.0 0.26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF o-Xylene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 17:45 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 80.7 70-130 9/25/18 17:45 Toluene-d8 98.4 70-130 9/25/18 17:45 4-Bromofluorobenzene 96.3 70-130 9/25/18 17:45 Page 84 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-24 Sampled: 9/21/2018 14:00 Samnle ID: 18I1008-13 Samnle Matrix: Ground Water Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Acenaphthylene ND 5.0 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Acetophenone ND 10 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Aniline ND 5.0 2.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Anthracene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Benzidine ND 20 9.7 µg/L 1 V-04, V-05, V-34 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Benzo(a)anthracene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Benzo(a)pyrene ND 5.0 1.5 µg/L I SW-846 8270D 9/27/18 9/28/18 21:57 BGL Benzo(b)fluoranthene ND 5.0 1.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Benzo(g,h,i)perylene ND 5.0 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Benzo(k)fluoranthene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Benzoic Acid ND 10 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Bis(2-chloroethoxy)methane ND 10 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Bis(2-chloroethyl)ether ND 10 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Bis(2-chloroisopropyl)ether ND 10 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Bis(2-Ethylhexyl)phthalate ND 10 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 4-Bromophenylphenylether ND 10 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Butylbenzylphthalate ND 10 1.9 µg/L I SW-846 8270D 9/27/18 9/28/18 21:57 BGL Carbazole ND 10 1.6 µg/L I SW-846 8270D 9/27/18 9/28/18 21:57 BGL 4-Chloroaniline ND 10 1.5 µg/L I V-34 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 4-Chloro-3-methylphenol ND 10 1.4 µg/L I SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2-Chloronaphthalene ND 10 1.5 µg/L I SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2-Chlorophenol ND 10 1.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 4-Chlorophenylphenylether ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Chrysene ND 5.0 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Dibenz(a,h)anthracene ND 5.0 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Dibenzofman ND 5.0 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Di-n-butylphthalate ND 10 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 1,2-Dichlorobenzene ND 5.0 1.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 1,3-Dichlorobenzene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 1,4-Dichlorobenzene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 3,3-Dichlorobenzidine ND 10 2.3 µg/L I SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2,4-Dichlorophenol ND 10 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Diethylphthalate ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2,4-Dimethylphenol ND 10 3.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Dimethylphthalate ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 4,6-Dinitro-2-methylphenol ND 10 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2,4-Dinitrophenol ND 10 3.4 µg/L 1 V-04 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2,4-Dinitrotoluene ND 10 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2,6-Dinitrotoluene ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Di-n-octylphthalate ND 10 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 10 2.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Flumanthene ND 5.0 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Flumene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Page 85 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-24 Sampled: 9/21/2018 14:00 Sample ID: 18I1008-13 Samnle Matrix: Ground Water Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND ]0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Hexachlorobutadiene ND ]0 1.5 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Hexachlorocyclopentadiene ND ]0 1.9 µg/L 1 L-04, V-04 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Hexachloroethane ND ]0 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Indeno(1,2,3-cd)pyrene ND 5.0 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Isophorone ND 10 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 1-Methylnaphthalene ND 5.0 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2-Methylnaphthalene ND 5.0 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2-Methylphenol ND 10 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 3/4-Methylphenol ND 10 1.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Naphthalene ND 5.0 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2-Nitroaniline ND 10 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 3-Nitroaniline ND 10 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 4-Nitroaniline ND 10 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Nitrobenzene ND 10 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2-Nitrophenol ND 10 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 4-Nitrophenol ND 10 1.0 µg/L 1 V-20 SW-846 8270D 9/27/18 9/28/18 21:57 BGL N-Nitrosodimethylamine ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL N-Nitrosodiphenylamine ND 10 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL N-Nitrosodi-n-propylamine ND 10 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Pentachloronitrobenzene ND 10 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Pentachlorophenol ND 10 1.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Phenanthrene ND 5.0 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Phenol ND 10 1.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Pyrene ND 5.0 1.6 µg/L, 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Pyridine ND 5.0 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 1,2,4,5-Tetrachlorobenzene ND 10 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 1,2,4-Trichlorobenzene ND 5.0 1.6 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2,4,5-Trichlorophenol ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL 2,4,6-Trichlorophenol ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 21:57 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 55.9 15-110 9/28/18 21:57 Phenol-d6 36.5 15-110 9/28/18 21:57 Nitrobenzene-d5 62.9 30-130 9/28/18 21:57 2-Fluorobiphenyl 54.5 30-130 9/28/18 21:57 2,4,6-Tribromophenol 60.6 15-110 9/28/18 21:57 p-Terphenyl-dl4 67.9 30-130 9/28/18 21:57 Page 86 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Date Received: 9/21/2018 Field Sample #: MW-24 Sampled: 9/21/2018 14:00 Sample ID: 18I1008-13 Samnle Matrix: Ground Water Work Order: 18I1008 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic 13 0.80 0.72 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:55 MJH Barium 18 20 11 µg/L 2 J SW-846 6020B 9/28/18 10/2/18 8:55 MJH Cadmium ND 1.0 0.19 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:55 MJH Chromium 4.1 2.0 1.0 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:55 MJH Lead 0.31 2.0 0.28 µg/L 2 J SW-846 6020B 9/28/18 10/2/18 8:55 MJH Mercury ND 0.00010 0.000034 mg/L 1 SW-846 7470A 9/26/18 9/28/18 11:49 EJB Selenium ND 10 4.2 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:55 MJH Silver ND 1.0 0.15 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:55 MJH Page 87 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-24 Sampled: 9/21/2018 14:00 Sample ID: 18I1008-13 Samnle Matrix: Ground Water Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium ND 0.0040 0.0010 mg/L 1 SW-846 7196A 9/22/18 9/22/18 11:01 AA Page 88 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-19 Sampled: 9/21/2018 15:15 Sample ID: 1811008-14 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 9.7 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Acrylonitrile ND 5.0 0.58 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF tert-Amyl Methyl Ether (TAME) 0.87 0.50 0.11 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Benzene 1.2 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Bromobenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Bromochloromethane ND 1.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Bromodichloromethane ND 0.50 0.30 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Bromoform ND 2.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Bromomethane ND 2.0 0.94 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 2-Butanone (MEK) ND 20 2.4 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF tert-Butyl Alcohol (TBA) ND 20 2.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF n-Butylbenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF sec-Butylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF tert-Butylbenzene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.50 0.095 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Carbon Disulfide ND 4.0 1.0 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Carbon Tetrachloride ND 5.0 0.25 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Chlorobenzene ND 1.0 0.16 µg/L I SW-846 8260B 9/25/18 9/25/18 19:57 MFF Chlorodibromomethane ND 0.50 0.10 µg/L I SW-846 8260B 9/25/18 9/25/18 19:57 MFF Chloroethane ND 2.0 0.28 µg/L I SW-846 8260B 9/25/18 9/25/18 19:57 MFF Chloroform 0.64 2.0 0.22 µg/L I J SW-846 8260B 9/25/18 9/25/18 19:57 MFF Chloromethane ND 2.0 0.55 µg/L I SW-846 8260B 9/25/18 9/25/18 19:57 MFF 2-Chlorotoluene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 4-Chlorotoluene ND 1.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.37 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Dibromomethane ND 1.0 0.16 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,2-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,3-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,4-Dichlorobenzene 1.9 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Dichlorodifluoromethane (Freon 12) ND 2.0 0.28 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,2-Dichloroethane ND 1.0 0.19 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,1-Dichloroethylene ND 1.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF cis-1,2-Dichloroethylene 91 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF trans-1,2-Dichloroethylene 17 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,2-Dichloropropane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,3-Dichloropropane ND 0.50 0.13 µg/L I SW-846 8260B 9/25/18 9/25/18 19:57 MFF 2,2-Dichloropropane ND 1.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,1-Dichloropropene ND 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF cis-1,3-Dichloropropene ND 0.50 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF trans-1,3-Dichloropropene ND 0.50 0.11 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Diethyl Ether ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Page 89 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-19 Sampled: 9/21/2018 15:15 Sample ID: 1811008-14 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPS) 0.41 0.50 0.18 µg/L 1 J SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,4-Dioxane ND 50 26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Hexachlorobutadiene ND 0.60 0.59 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Isopropylbenzene (Cumene) ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF p-Isopropyltoluene (p-Cymene) ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Methyl tert-Butyl Ether (MTBE) 3.2 1.0 0.090 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Methylene Chloride ND 5.0 3.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 4-Methyl-2-pentanone (MIBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Naphthalene 0.25 2.0 0.12 µg/L 1 J SW-846 8260B 9/25/18 9/25/18 19:57 MFF n-Propylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Styrene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1, 1, 1,2-Tetrachloroethane ND 1.0 0.12 µg/L 1 SW-8468260B 9/25/18 9/25/18 19:57 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.16 µg/L 1 SW-8468260B 9/25/18 9/25/18 19:57 MFF Tetrachloroethylene ND 1.0 0.27 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Tetrahydrofirran ND 10 1.1 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Toluene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,2,3-Trichlorobenzene ND 5.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,2,4-Trichlorobenzene ND 1.0 0.19 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,3,5-Trichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1, 1, 1 -Trichloroethane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,1,2-Trichloroethane ND 1.0 0.24 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Trichloroethylene 43 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Trichlorofluoromethane (Freon 11) ND 2.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,2,3-Trichloropropane ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 1.0 0.18 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF 1,3,5-Trimethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Vinyl Chloride 2.4 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF m+p Xylene ND 2.0 0.26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF o-Xylene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 19:57 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 81.3 70-130 9/25/18 19:57 Toluene-d8 99.8 70-130 9/25/18 19:57 4-Bromofluorobenzene 98.4 70-130 9/25/18 19:57 Page 90 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-19 Sampled: 9/21/2018 15:15 Samnle ID: 1811008-14 Samnle Matrix: Ground Water Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Acenaphthylene ND 5.0 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Acetophenone ND 10 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Aniline ND 5.0 2.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Anthracene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Benzidine ND 20 9.7 µg/L 1 V-04, V-05, V-34 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Benzo(a)anthracene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Benzo(a)pyrene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Benzo(b)fluoranthene ND 5.0 1.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Benzo(g,h,i)perylene ND 5.0 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Benzo(k)fluoranthene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Benzoic Acid ND 10 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Bis(2-chloroethoxy)methane ND 10 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Bis(2-chloroethyl)ether ND 10 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Bis(2-chloroisopropyl)ether ND 10 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Bis(2-Ethylhexyl)phthalate ND 10 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 4-Bromophenylphenylether ND 10 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Butylbenzylphthalate ND 10 1.9 µg/L I SW-846 8270D 9/27/18 9/28/18 22:20 BGL Carbazole ND 10 1.6 µg/L I SW-846 8270D 9/27/18 9/28/18 22:20 BGL 4-Chloroaniline ND 10 1.5 µg/L I V-34 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 4-Chloro-3-methylphenol ND 10 1.4 µg/L I SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2-Chloronaphthalene ND 10 1.5 µg/L I SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2-Chlorophenol ND 10 1.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 4-Chlorophenylphenylether ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Chrysene ND 5.0 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Dibenz(a,h)anthracene ND 5.0 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Dibenzofman ND 5.0 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Di-n-butylphthalate ND 10 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 1,2-Dichlorobenzene ND 5.0 1.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 1,3-Dichlorobenzene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 1,4-Dichlorobenzene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 3,3-Dichlorobenzidine ND 10 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2,4-Dichlorophenol ND 10 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Diethylphthalate ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2,4-Dimethylphenol ND 10 3.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Dimethylphthalate ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 4,6-Dinitro-2-methylphenol ND 10 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2,4-Dinitrophenol ND 10 3.4 µg/L 1 V-04 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2,4-Dinitrotoluene ND 10 1.8 µg/L I SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2,6-Dinitrotoluene ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Di-n-octylphthalate ND 10 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 10 2.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Flumanthene ND 5.0 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Flumene ND 5.0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Page 91 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-19 Sampled: 9/21/2018 15:15 Sample ID: 1811008-14 Samnle Matrix: Ground Water Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND ]0 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Hexachlorobutadiene ND ]0 1.5 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Hexachlorocyclopentadiene ND ]0 1.9 µg/L 1 L-04, V-04 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Hexachloroethane ND ]0 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Indeno(1,2,3-cd)pyrene ND 5.0 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Isophorone ND 10 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 1-Methylnaphthalene ND 5.0 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2-Methylnaphthalene ND 5.0 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2-Methylphenol ND 10 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 3/4-Methylphenol ND 10 1.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Naphthalene ND 5.0 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2-Nitroaniline ND 10 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 3-Nitroaniline ND 10 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 4-Nitroaniline ND 10 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Nitrobenzene ND 10 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2-Nitrophenol ND 10 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 4-Nitrophenol ND 10 1.0 µg/L 1 V-20 SW-846 8270D 9/27/18 9/28/18 22:20 BGL N-Nitrosodimethylamine ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL N-Nitrosodiphenylamine ND 10 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL N-Nitrosodi-n-propylamine ND 10 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Pentachloronitrobenzene ND 10 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Pentachlorophenol ND 10 1.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Phenanthrene ND 5.0 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Phenol ND 10 1.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Pyrene ND 5.0 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Pyridine ND 5.0 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 1,2,4,5-Tetrachlorobenzene ND 10 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 1,2,4-Trichlorobenzene ND 5.0 1.6 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2,4,5-Trichlorophenol ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL 2,4,6-Trichlorophenol ND 10 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:20 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 37.7 15-110 9/28/18 22:20 Phenol-d6 24.8 15-110 9/28/18 22:20 Nitrobenzene-d5 54.3 30-130 9/28/18 22:20 2-Fluorobiphenyl 55.4 30-130 9/28/18 22:20 2,4,6-Tribromophenol 58.5 15-110 9/28/18 22:20 p-Terphenyl-dl4 68.4 30-130 9/28/18 22:20 Page 92 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-19 Sampled: 9/21/2018 15:15 Sample ID: 18I1008-14 Samnle Matrix: Ground Water Analyte Results RL DL Metals Analyses (Total) Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Arsenic 1.0 0.80 0.72 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:59 MJH Barium 53 20 11 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:59 MJH Cadmium ND 1.0 0.19 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:59 MJH Chromium 7500 20 10 µg/L 20 SW-846 6020B 9/28/18 10/2/18 9:41 MJH Lead ND 2.0 0.28 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:59 MJH Mercury 0.000039 0.00010 0.000034 mg/L 1 J SW-846 7470A 9/26/18 9/28/18 11:50 EJB Selenium ND 10 4.2 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:59 MJH Silver ND 1.0 0.15 µg/L 2 SW-846 6020B 9/28/18 10/2/18 8:59 MJH Page 93 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-19 Sampled: 9/21/2018 15:15 Sample ID: 1811008-14 Samnle Matrix: Ground Water Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium 3.9 0.10 0.025 mg/L 25 SW-846 7196A 9/22/18 9/22/18 11:01 AA Page 94 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-23 Sampled: 9/21/2018 15:50 Sample ID: 1811008-15 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 9.7 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Acrylonitrile ND 5.0 0.58 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF tert-Amyl Methyl Ether (TAME) ND 0.50 0.11 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Benzene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Bromobenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Bromochloromethane ND 1.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Bromodichloromethane ND 0.50 0.30 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Bromoform ND 2.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Bromomethane ND 2.0 0.94 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 2-Butanone (MEK) ND 20 2.4 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF tert-Butyl Alcohol (TBA) ND 20 2.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF n-Butylbenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF sec-Butylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF tert-Butylbenzene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.50 0.095 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Carbon Disulfide ND 4.0 1.0 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Carbon Tetrachloride ND 5.0 0.25 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Chlorobenzene ND 1.0 0.16 µg/L I SW-846 8260B 9/25/18 9/25/18 18:11 MFF Chlorodibromomethane ND 0.50 0.10 µg/L I SW-846 8260B 9/25/18 9/25/18 18:11 MFF Chloroethane ND 2.0 0.28 µg/L I SW-846 8260B 9/25/18 9/25/18 18:11 MFF Chloroform ND 2.0 0.22 µg/L I SW-846 8260B 9/25/18 9/25/18 18:11 MFF Chloromethane ND 2.0 0.55 µg/L I SW-846 8260B 9/25/18 9/25/18 18:11 MFF 2-Chlorotoluene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 4-Chlorotoluene ND 1.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.37 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Dibromomethane ND 1.0 0.16 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,2-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,3-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,4-Dichlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Dichlorodifluoromethane (Freon 12) ND 2.0 0.28 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-8468260B 9/25/18 9/25/18 18:11 MFF 1,2-Dichloroethane ND 1.0 0.19 µg/L 1 SW-8468260B 9/25/18 9/25/18 18:11 MFF 1, 1 -Dichloroethylene ND 1.0 0.21 µg/L 1 SW-8468260B 9/25/18 9/25/18 18:11 MFF cis-1,2-Dichloroethylene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF trans-1,2-Dichloroethylene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,2-Dichloropropane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,3-Dichloropropane ND 0.50 0.13 µg/L I SW-846 8260B 9/25/18 9/25/18 18:11 MFF 2,2-Dichloropropane ND 1.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,1-Dichloropropene ND 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF cis-1,3-Dichloropropene ND 0.50 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF trans-1,3-Dichloropropene ND 0.50 0.11 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Diethyl Ether ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Page 95 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-23 Sampled: 9/21/2018 15:50 Sample ID: 1811008-15 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPS) ND 0.50 0.18 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,4-Dioxane ND 50 26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Hexachlorobutadiene ND 0.60 0.59 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Isopropylbenzene (Cumene) ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF p-Isopropyltoluene (p-Cymene) ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Methyl tert-Butyl Ether (MTBE) ND 1.0 0.090 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Methylene Chloride ND 5.0 3.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 4-Methyl-2-pentanone (MIBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Naphthalene ND 2.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF n-Propylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Styrene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1, 1, 1,2-Tetrachloroethane ND 1.0 0.12 µg/L 1 SW-8468260B 9/25/18 9/25/18 18:11 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.16 µg/L 1 SW-8468260B 9/25/18 9/25/18 18:11 MFF Tetrachloroethylene ND 1.0 0.27 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Tetrahydrofirran ND 10 1.1 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Toluene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,2,3-Trichlorobenzene ND 5.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,2,4-Trichlorobenzene ND 1.0 0.19 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,3,5-Trichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1, 1, 1 -Trichloroethane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,1,2-Trichloroethane ND 1.0 0.24 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Trichloroethylene ND 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Trichlorofluoromethane (Freon 11) ND 2.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,2,3-Trichloropropane ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 1.0 0.18 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF 1,3,5-Trimethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Vinyl Chloride ND 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF m+p Xylene ND 2.0 0.26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF o-Xylene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:11 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 81.3 70-130 9/25/18 18:11 Toluene-d8 101 70-130 9/25/18 18:11 4-Bromofluorobenzene 96.6 70-130 9/25/18 18:11 Page 96 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-23 Sampled: 9/21/2018 15:50 Sample ID: 1811008-15 Samnle Matrix: Ground Water Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 5.7 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Acenaphthylene ND 5.7 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Acetophenone ND 11 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Aniline ND 5.7 2.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Anthracene ND 5.7 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Benzidine ND 23 11 µg/L 1 V-04, V-05, V-34 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Benzo(a)anthracene ND 5.7 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Benzo(a)pyrene ND 5.7 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Benzo(b)fluoranthene ND 5.7 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Benzo(g,h,i)perylene ND 5.7 2.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Benzo(k)fluoranthene ND 5.7 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Benzoic Acid ND 11 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Bis(2-chloroethoxy)methane ND 11 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Bis(2-chloroethyl)ether ND 11 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Bis(2-chloroisopropyl)ether ND 11 2.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Bis(2-Ethylhexyl)phthalate ND 11 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 4-Bromophenylphenylether ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Butylbenzylphthalate ND 11 2.2 µg/L I SW-846 8270D 9/27/18 9/28/18 22:42 BGL Carbazole ND 11 1.8 µg/L I SW-846 8270D 9/27/18 9/28/18 22:42 BGL 4-Chloroaniline ND 11 1.7 µg/L I V-34 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 4-Chloro-3-methylphenol ND 11 1.6 µg/L I SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2-Chloronaphthalene ND 11 1.7 µg/L I SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2-Chlorophenol ND 11 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 4-Chlorophenylphenylether ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Chrysene ND 5.7 1.6 µg/L I SW-846 8270D 9/27/18 9/28/18 22:42 BGL Dibenz(a,h)anthracene ND 5.7 2.4 µg/L I SW-846 8270D 9/27/18 9/28/18 22:42 BGL Dibenzofman ND 5.7 1.6 µg/L I SW-846 8270D 9/27/18 9/28/18 22:42 BGL Di-n-butylphthalate ND 11 2.1 µg/L I SW-846 8270D 9/27/18 9/28/18 22:42 BGL 1,2-Dichlorobenzene ND 5.7 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 1,3-Dichlorobenzene ND 5.7 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 1,4-Dichlorobenzene ND 5.7 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 3,3-Dichlorobenzidine ND 11 2.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2,4-Dichlorophenol ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Diethylphthalate ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2,4-Dimethylphenol ND 11 4.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Dimethylphthalate ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 4,6-Dinitro-2-methylphenol ND 11 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2,4-Dinitrophenol ND 11 3.9 µg/L 1 V-04 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2,4-Dinitrotoluene ND 11 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2,6-Dinitrotoluene ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Di-n-octylphthalate ND 11 2.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 11 2.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Flumanthene ND 5.7 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Flumene ND 5.7 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Page 97 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-23 Sampled: 9/21/2018 15:50 Sample ID: 1811008-15 Samnle Matrix: Ground Water Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Hexachlorobutadiene ND 11 1.8 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Hexachlorocyclopentadiene ND 11 2.2 µg/L 1 L-04, V-04 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Hexachloroethane ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Indeno(1,2,3-cd)pyrene ND 5.7 2.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Isophorone ND 11 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 1-Methylnaphthalene ND 5.7 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2-Methylnaphthalene ND 5.7 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2-Methylphenol ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 3/4-Methylphenol ND 11 1.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Naphthalene ND 5.7 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2-Nitroaniline ND 11 2.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 3-Nitroaniline ND 11 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 4-Nitroaniline ND 11 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Nitrobenzene ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2-Nitrophenol ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 4-Nitrophenol ND 11 1.2 µg/L 1 V-20 SW-846 8270D 9/27/18 9/28/18 22:42 BGL N-Nitrosodimethylamine ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL N-Nitrosodiphenylamine ND 11 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL N-Nitrosodi-n-propylamine ND 11 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Pentachloronitrobenzene ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Pentachlorophenol ND 11 1.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Phenanthrene ND 5.7 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Phenol ND 11 1.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Pyrene ND 5.7 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Pyridine ND 5.7 2.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 1,2,4,5-Tetrachlorobenzene ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 1,2,4-Trichlorobenzene ND 5.7 1.8 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2,4,5-Trichlorophenol ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL 2,4,6-Trichlorophenol ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 22:42 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 43.8 15-110 9/28/18 22:42 Phenol-d6 30.8 15-110 9/28/18 22:42 Nitrobenzene-d5 60.3 30-130 9/28/18 22:42 2-Fluorobiphenyl 64.1 30-130 9/28/18 22:42 2,4,6-Tribromophenol 76.2 15-110 9/28/18 22:42 p-Terphenyl-dl4 84.1 30-130 9/28/18 22:42 Page 98 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-23 Sampled: 9/21/2018 15:50 Sample ID: 1811008-15 Samnle Matrix: Ground Water Analyte Results RL DL Metals Analyses (Total) Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Arsenic 1200 4.0 3.6 µg/L 10 SW-846 6020B 9/28/18 10/2/18 9:44 MJH Barium 25 20 11 µg/L 2 SW-846 6020B 9/28/18 10/2/18 9:02 MJH Cadmium ND 1.0 0.19 µg/L 2 SW-846 6020B 9/28/18 10/2/18 9:02 MJH Chromium 4.0 2.0 1.0 µg/L 2 SW-846 6020B 9/28/18 10/2/18 9:02 MJH Lead ND 2.0 0.28 µg/L 2 SW-846 6020B 9/28/18 10/2/18 9:02 MJH Mercury ND 0.00010 0.000034 mg/L 1 SW-846 7470A 9/26/18 9/28/18 11:52 EJB Selenium ND 10 4.2 µg/L 2 SW-846 6020B 9/28/18 10/2/18 9:02 MJH Silver ND 1.0 0.15 µg/L 2 SW-846 6020B 9/28/18 10/2/18 9:02 MJH Page 99 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-23 Sampled: 9/21/2018 15:50 Sample ID: 1811008-15 Samnle Matrix: Ground Water Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexavalent Chromium 0.0028 0.0040 0.0010 mg/L 1 J SW-846 7196A 9/22/18 9/22/18 11:01 AA Page 100 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-25 Sampled: 9/21/2018 16:40 Sample ID: 18I1008-16 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 9.7 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Acrylonitrile ND 5.0 0.58 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF tert-Amyl Methyl Ether (TAME) ND 0.50 0.11 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Benzene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Bromobenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Bromochloromethane ND 1.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Bromodichloromethane ND 0.50 0.30 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Bromoform ND 2.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Bromomethane ND 2.0 0.94 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 2-Butanone (MEK) ND 20 2.4 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF tert-Butyl Alcohol (TBA) ND 20 2.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF n-Butylbenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF sec-Butylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF tert-Butylbenzene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.50 0.095 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Carbon Disulfide ND 4.0 1.0 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Carbon Tetrachloride ND 5.0 0.25 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Chlorobenzene ND 1.0 0.16 µg/L I SW-846 8260B 9/25/18 9/25/18 18:38 MFF Chlorodibromomethane ND 0.50 0.10 µg/L I SW-846 8260B 9/25/18 9/25/18 18:38 MFF Chloroethane ND 2.0 0.28 µg/L I SW-846 8260B 9/25/18 9/25/18 18:38 MFF Chloroform 0.27 2.0 0.22 µg/L I J SW-846 8260B 9/25/18 9/25/18 18:38 MFF Chloromethane ND 2.0 0.55 µg/L I SW-846 8260B 9/25/18 9/25/18 18:38 MFF 2-Chlorotoluene ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 4-Chlorotoluene ND 1.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.37 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Dibromomethane ND 1.0 0.16 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,2-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,3-Dichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,4-Dichlorobenzene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF trans-1,4-Dichloro-2-butene ND 2.0 0.31 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Dichlorodifluoromethane (Freon 12) ND 2.0 0.28 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,2-Dichloroethane ND 1.0 0.19 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,1-Dichloroethylene ND 1.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF cis-1,2-Dichloroethylene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF trans-1,2-Dichloroethylene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,2-Dichloropropane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,3-Dichloropropane ND 0.50 0.13 µg/L I SW-846 8260B 9/25/18 9/25/18 18:38 MFF 2,2-Dichloropropane ND 1.0 0.21 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,1-Dichloropropene ND 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF cis-1,3-Dichloropropene ND 0.50 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF trans-1,3-Dichloropropene ND 0.50 0.11 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Diethyl Ether ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Page 101 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-25 Sampled: 9/21/2018 16:40 Sample ID: 18I1008-16 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPS) ND 0.50 0.18 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,4-Dioxane ND 50 26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Ethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Hexachlorobutadiene ND 0.60 0.59 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Isopropylbenzene (Cumene) ND 1.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF p-Isopropyltoluene (p-Cymene) ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Methyl tert-Butyl Ether (MTBE) ND 1.0 0.090 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Methylene Chloride ND 5.0 3.2 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 4-Methyl-2-pentanone (MIBK) ND 10 1.5 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Naphthalene ND 2.0 0.12 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF n-Propylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Styrene ND 1.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1, 1, 1,2-Tetrachloroethane ND 1.0 0.12 µg/L 1 SW-8468260B 9/25/18 9/25/18 18:38 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.16 µg/L 1 SW-8468260B 9/25/18 9/25/18 18:38 MFF Tetrachloroethylene ND 1.0 0.27 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Tetrahydrofirran ND 10 1.1 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Toluene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,2,3-Trichlorobenzene ND 5.0 0.14 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,2,4-Trichlorobenzene ND 1.0 0.19 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,3,5-Trichlorobenzene ND 1.0 0.17 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1, 1, 1 -Trichloroethane ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,1,2-Trichloroethane ND 1.0 0.24 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Trichloroethylene ND 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Trichlorofluoromethane (Freon 11) ND 2.0 0.15 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,2,3-Trichloropropane ND 2.0 0.22 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 1.0 0.20 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 1.0 0.18 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF 1,3,5-Trimethylbenzene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Vinyl Chloride ND 2.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF m+p Xylene ND 2.0 0.26 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF o-Xylene ND 1.0 0.13 µg/L 1 SW-846 8260B 9/25/18 9/25/18 18:38 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 80.3 70-130 9/25/18 18:38 Toluene-d8 101 70-130 9/25/18 18:38 4-Bromofluorobenzene 97.0 70-130 9/25/18 18:38 Page 102 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-25 Sampled: 9/21/2018 16:40 Samnle ID: 18I1008-16 Samnle Matrix: Ground Water Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 5.6 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Acenaphthylene ND 5.6 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Acetophenone ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Aniline ND 5.6 2.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Anthracene ND 5.6 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Benzidine ND 22 11 µg/L 1 V-04, V-05, V-34 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Benzo(a)anthracene ND 5.6 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Benzo(a)pyrene ND 5.6 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Benzo(b)fluoranthene ND 5.6 1.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Benzo(g,h,i)perylene ND 5.6 2.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Benzo(k)fluoranthene ND 5.6 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Benzoic Acid ND 11 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Bis(2-chloroethoxy)methane ND 11 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Bis(2-chloroethyl)ether ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Bis(2-chloroisopropyl)ether ND 11 2.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Bis(2-Ethylhexyl)phthalate ND 11 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 4-Bromophenylphenylether ND 11 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Butylbenzylphthalate ND 11 2.2 µg/L I SW-846 8270D 9/27/18 9/28/18 23:04 BGL Carbazole ND 11 1.8 µg/L I SW-846 8270D 9/27/18 9/28/18 23:04 BGL 4-Chloroaniline ND 11 1.7 µg/L I V-34 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 4-Chloro-3-methylphenol ND 11 1.6 µg/L I SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2-Chloronaphthalene ND 11 1.7 µg/L I SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2-Chlorophenol ND 11 1.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 4-Chlorophenylphenylether ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Chrysene ND 5.6 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Dibenz(a,h)anthracene ND 5.6 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Dibenzofman ND 5.6 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Di-n-butylphthalate ND 11 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 1,2-Dichlorobenzene ND 5.6 1.5 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 1,3-Dichlorobenzene ND 5.6 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 1,4-Dichlorobenzene ND 5.6 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 3,3-Dichlorobenzidine ND 11 2.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2,4-Dichlorophenol ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Diethylphthalate ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2,4-Dimethylphenol ND 11 4.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Dimethylphthalate ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 4,6-Dinitro-2-methylphenol ND 11 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2,4-Dinitrophenol ND 11 3.8 µg/L 1 V-04 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2,4-Dinitrotoluene ND 11 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2,6-Dinitrotoluene ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Di-n-octylphthalate ND 11 2.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 11 2.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Flumanthene ND 5.6 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Flumene ND 5.6 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Page 103 of 159 Table of Contents icon-te O ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 511 East 25th Street, Charlotte, N Sample Description: Work Order: 18I1008 Date Received: 9/21/2018 Field Sample #: MW-25 Sampled: 9/21/2018 16:40 Sample ID: 18I1008-16 Samnle Matrix: Ground Water Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Hexachlorobutadiene ND 11 1.7 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Hexachlorocyclopentadiene ND 11 2.2 µg/L 1 L-04, V-04 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Hexachloroethane ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Indeno(1,2,3-cd)pyrene ND 5.6 2.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Isophorone ND 11 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 1-Methylnaphthalene ND 5.6 2.0 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2-Methylnaphthalene ND 5.6 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2-Methylphenol ND 11 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 3/4-Methylphenol ND 11 1.3 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Naphthalene ND 5.6 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2-Nitroaniline ND 11 2.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 3-Nitroaniline ND 11 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 4-Nitroaniline ND 11 2.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Nitrobenzene ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2-Nitrophenol ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 4-Nitrophenol ND 11 1.2 µg/L 1 V-20 SW-846 8270D 9/27/18 9/28/18 23:04 BGL N-Nitrosodimethylamine ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL N-Nitrosodiphenylamine ND 11 2.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL N-Nitrosodi-n-propylamine ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Pentachloronitrobenzene ND 11 1.9 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Pentachlorophenol ND 11 1.2 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Phenanthrene ND 5.6 1.6 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Phenol ND 11 1.1 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Pyrene ND 5.6 1.8 µg/L, 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Pyridine ND 5.6 2.4 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 1,2,4,5-Tetrachlorobenzene ND 11 1.8 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 1,2,4-Trichlorobenzene ND 5.6 1.8 µg/L 1 R-05 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2,4,5-Trichlorophenol ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL 2,4,6-Trichlorophenol ND 11 1.7 µg/L 1 SW-846 8270D 9/27/18 9/28/18 23:04 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 45.9 15-110 9/28/18 23:04 Phenol-d6 31.1 15-110 9/28/18 23:04 Nitrobenzene-d5 58.7 30-130 9/28/18 23:04 2-Fluorobiphenyl 57.8 30-130 9/28/18 23:04 2,4,6-Tribromophenol 61.5 15-110 9/28/18 23:04 p-Terphenyl-dl4 73.8 30-130 9/28/18 23:04 Page 104 of 159