24040_Gary & Sarah Smith Properties_Phase II ESA_20191011

Privileged and Confidential
September 2019 Phase II Environmental Site Assessment
George and Sarah Smith Properties
1002 East Raleigh Street
Siler City, North Carolina 27344
October 11, 2019
Prepared For
Brian Rosenthal
Rose Law Firm
120 E. Fourth Sc
Little Rock, Arkansas 72201
For Use By
Ms. Tanya Rogers -Vickers
Director of Environmental Compliance
Mountaire Farms, Inc.
29292 John J. Williams Highway
P.O. Box 1320
Millsboro, Delaware 19966
Prepared By
Mr. Phillip Rahn P.G. RSM
Waters Edge Environmental, LLC
1434 Chester Road
Raleigh, North Carolina 27608
919.219.5820
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LMWATERS EDGE ENVIRONMENTAL, LLC
1434 CHESTER ROAD • RALEIGH, NC 27608 • PHONE [phone]
October 11, 2019
Mr. Brian Rosenthal
Rose Law Firm
120 E. Fourth St.
Little Rock, Arkansas 72201
For use by:
Ms. Tanya Rogers -Vickers
Director of Environmental Compliance
Mountaire Farms, Inc.
29292 John J. Williams Highway
P.O. Box 1320
Millsboro, Delaware 19966
Reference: Privileged and Confidential
September 2019 Phase II Environmental Site Assessment
Gary L. Smith and Sarah S. Smith, Trustees Properties
1002 East Raleigh Street
Siler City, North Carolina 27344
Dear Mr. Brian Rosenthal and Ms. Rogers -Vickers:
Waters Edge Environmental, LLC (Waters Edge) is pleased to submit this September 2019 Phase II
Environmental Site Assessment for the Gary L. Smith and Sarah S. Smith, Trustees Properties located at
1002 East Raleigh Street in Siler City, North Carolina. The following report documents the results of the
September 2019 Phase II ESA and presents our conclusions and recommendations for the property.
Waters Edge appreciates the opportunity to provide environmental consulting services to Mountaire Farms,
Inc. If you have any questions regarding the information contained herein, please do not hesitate to contact
me at 919.219.5820.
Sincerely,
WATERS EDGE ENVIRONMENTAL, LLC
Phillip L Rahn, P.G.
President
19-068/PLR/aht

Table of Contents
1 Introduction
2 September 2019 Phase II ESA Investigation
2.1 AOC-1 EPC Discharge Pipe
2.2 AOC-2 BA Parcels
2.3 AOC-3 Lynn's Florist Facility
2.4 AOC-4 DOT Facility
2.5 AOC-S Springs
3 Results, Conclusions and Recommendations
1 Project Location Map
2 Site Location Map
3 Sample Location Map
Figures
Tables
1 Surface Water/Spring Analytical Results
2 Sediment Analytical Results
3 Groundwater Analytical Results
A Standard Operating Procedures
B Laboratory Analytical Results
Appendix
1
2
2
2
3
3
3
3
V1

Acronym List
AOC
Area of concern
BA
Brownfields Agreement
D&D
Duncklee & Dunham
DEQ
Division of Environmental Quality
EPC
Engineered Plastic Components
ESA
Environmental Site Assessment
LUST
Leaking Underground Storage Tank
MFI
Mountaire Farms Inc. and its affiliates
MTBE
Methyl-Tert Butyl Ether
PAHs
Polyaromatic Hydrocarbons
POG
Protection of Groundwater
PFAS
Per- and polyfluoroalkyl substances
PWR
Partially Weathered Rock
PSRGs
Preliminary Soil Remediation Goals
SVOCs
semi -volatile organic compounds
VOCs
Volatile Organic Compounds
Waters Edge
Waters Edge Environmental, LLC
M

September 2019 Phase II Environmental Site Assessment
Gary L. Smith and Sarah S. Smith, Trustees Properties
1002 East Raleigh Street
Siler City, North Carolina 27344
October 11, 2019
Introduction
Waters Edge conducted a Phase I ESA on September 5, 2019 for the above -mentioned site
located in Siler City, North Carolina (see Figures 1-2). Based on the results of the Phase I ESA,
the following AOCs were identified:
AOC-1 EPC Discharge Pipe
There is an aqueous discharge emanating from this offsite concern onto the subject
property. Based on the materials produced at this offsite concern, we proposed sampling
the onsite surface water and sediment below this aqueous discharge for VOCs and
SVOCs.
AOC-2 BA Parcels
AOC 2 comprises all of the previous work conducted by Duncklee & Dunham on the
upgradient BA Parcels. The concerns mentioned in the Phase I ESA were as follows:
1. Surface Water and Sediment sampling conducted west of the Former Acme McCrary
building was ND for VOCs in the surface water but no SVOC sampling was found.
The sediment had some inorganics and PAHs detected. The inorganics (e.g. arsenic)
were felt due to background conditions in the D&D reports, and we agreed. The
PAHs were below PSRGs, but we still felt this warranted two sample locations in the
onsite north -south discharge feature to be analyzed for VOCs and SVOCs (both
surface water and sediment).
2. TMW-3 was a Geoprobe groundwater sample located on the south side of the former
Acme McCrary parcel which is immediately upgradient of the subject property. We
proposed one Geoprobe sampling point immediately downgradient of TMW-3 which
would be sampled for VOCs and SVOCs.
AOC-3 Lynn's Florist Facility
This building used to be a former gasoline service station, and there is another upgradient
LUST site. We proposed collecting one Geoprobe groundwater sample immediately
downgradient on the subject property which would be analyzed for VOCs (no MADEP
VPH in that you are contemplating a BA).
Page 1 of 5

Phase II Environmental Site Assessment
Gary L. Smith and Sarah S. Smith, Trustees Properties
1002 East Raleigh Street
Siler City, North Carolina 27344
19-068
October 11, 2019
AOC-4 DOT Facility
There is an aqueous discharge from the DOT facility onto the eastern side of the subject
property. Due to the past environmental incidents at the DOT facility, we proposed one
surface water, one sediment and one Geoprobe groundwater sample analyzed for VOCs
and SVOCs.
AOC-5 Springs
There are two and potentially three springs on the subject property. These were
considered to be relatively easy data collection points which we proposed analysis for
VOCs.
These items were included in a September 6, 2019 Phase II ESA Proposal which was accepted
by representatives of Mountaire. Herein, is contained an account of the September 2019 Phase
II ESA field work, laboratory analytical results and our conclusions and recommendations.
2 September 2019 Phase II ESA Investigation
On September 19, 2019 Waters Edge mobilized with a senior project manager, senior
environmental technician and a Geoprobe to the subject property. Sampling conducted in each
AOC is described below (see Figure 3 and SOPS in Appendix A):
2.1 AOC-1 EPC Discharge Pipe
Due to the dry conditions at the time of the Phase II ESA, the sample location had to be
shifted further downgradient (e.g. east) since there was no surface water near the western
property line (see AOC-1 in Figure 3). One surface water sample (AOC-I-SW) was
collected by hand dipping an empty sampling container into the surface water feature.
One sediment sample was collected in the same location with a decontaminated hand
auger (AOC-1-Sed). Both were analyzed for VOCs and SVOCs.
2.2 AOC-2 BA Parcels
The following work tasks were conducted:
1. Surface Water and Sediment Sampling - Both an upgradient and downgradient
surface water/sediment sample was collected in the onsite north -south discharge
feature transecting the central portion of the subject property (AOC-2-SW/Sed Up
and Down) via the same method as described in AOC-1. All samples were analyzed
for VOCs and SVOCs (e.g. both surface water and sediment).
2. Groundwater Sampling - A Geoprobe was utilized to collect one groundwater sample
(Geo-1) which was downgradient of past D&D sampling location TMW-3 located
Page 2 of 5

Phase II Environmental Site Assessment
Gary L. Smith and Sarah S. Smith, Trustees Properties
1002 East Raleigh Street
Siler City, North Carolina 27344
19-068
October 11, 2019
on the south side of the former Acme McCrary parcel. We had to offset the onsite
sample location further to the west due to encountering PWR on the first several
boring attempts. The groundwater was analyzed for VOCs and SVOCs
2.3 AOC-3 Lynn's Florist Facility
Several borings were attempted with the Geoprobe and all encountered shallow refusal
due to PWR. No groundwater samples were collected. The only feasible method to
collect groundwater samples would be to mobilize an air rotary drilling rig which would
not be cost effective.
2.4 AOC-4 DOT Facility
The following work tasks were conducted:
1. Surface Water and Sediment Sampling - One location was identified (AOC-4-
SW/Sed) and a surface water/sediment sample was collected via the same method as
described in AOC-I. Both samples were analyzed for VOCs and SVOCs (both
surface water and sediment).
2. Groundwater Sampling - Several borings were attempted with the Geoprobe along
the eastern property line that borders the DOT facility. All encountered shallow
refusal due to PWR. No groundwater samples were collected.
2.5 AOC-5Springs
Three springs were identified but Spring #1 (adjacent to the Residence) was dry. The
remaining two springs (Spring #2 and Spring #3) were samples with a decontaminated
stainless -steel scoop and decanted into laboratory provided containers. Both samples
were analyzed for VOCs.
Surface Water and Spring Results are summarized in Table 1, Sediment results in Table 2,
Groundwater results in Table 3 and documentation in Appendix B.
3 Results, Conclusions and Recommendations
We have the following results, conclusions and recommendations:
AOC-1 EPC Discharge Pipe
The surface water sample was below all applicable DEQ 2B Surface Water Standards.
The sediment sample had the following exceedances of DEQ PSRGs (DEQ Guidance
uses soil PSRGs for sediment):
Page 3 of 5

Phase 11 Environmental Site Assessment
Gary L. Smith and Sarah S. Smith, Trustees Properties
1002 East Raleigh Street
Siler City, North Carolina 27344
19-068
October 11, 2019
1. Benzo(a)anthracene BAA) detected 0.4 mg/kg which is in excess of the POG
PSRG at 0.35 mg/kg
2. Benzo(a)pyrene (BAP) detected 0.33 mg/kg which is in excess of the POG PSRG
of 0.12 mg/kg and residential PSRG of 0.11 mg/kg.
AOC-2 BA Parcels
1. Both surface water samples were below all applicable DEQ 2B Surface Water
Standards; however, we would still consider the issue of PCP being detected at 6.9
ug/L in AOC-2 Down to be an issue since there is no 2B Standard for PCP. Both
sediment samples were below all DEQ PSRGs for unrestricted use. The acetone and
carbon disulfide detected in AOC-2 Down is potentially a laboratory artifact.
2. Groundwater Sampling- The groundwater results had the following exceedances of
North Carolina 2L Groundwater Standards as follows:
a. MTBE was detected at 140 µg/L in excess of the 20 µg/L NC 2L Groundwater
Standard. MTBE was also detected in the offsite well on the Former Acme
McCrary parcel at 230 µg/L which is upgradient of Geo-1.
b. Pentachlorophenol (PCP) was detected at 7.0 µg/L in excess of the 0.3 µg/L NC
2L Groundwater Standard. PCP is a herbicide, insecticide, fungicide, algaecide,
and disinfectant and is used as an ingredient in antifouling paint. Some
applications were in agricultural seeds (for nonfood uses), leather, masonry,
wood preservation, cooling -tower water, rope and paper. Its use has declined due
to its high toxicity and slow biodegradation.
AOC-4 DOT Facility
The surface water sample was below all applicable DEQ 2B Surface Water Standards.
The acetone detected is potentially a laboratory artifact. The sediment sample was ND
or below all DEQ PSRGs for unrestricted use.
AOC-5 Springs
The spring samples were below all applicable DEQ 2B Surface Water Standards for
VOCs. The acetone detected in Spring #2 is potentially a laboratory artifact.
Our recommendations are as follows:
Enter the results in the DEQ Risk Calculator to determine whether the site poses either
a Carcinogenic Risk greater than lE-4 or a Hazard Quotient greater than 1 for all
constituents combined. This would give a preliminary indication whether site could be
closed out through the Risk -Based rules potentially with a groundwater Land Use
Restriction.
The site could be deemed to have a low enough risk to be assessed and remediated in
the REC Program.
Page 4 of 5

Phase II Environmental Site Assessment
Gary L. Smith and Sarah S. Smith, Trustees Properties
1002 East Raleigh Street
Siler City, North Carolina 27344
19-068
October 11, 2019
Mountaire could also considered a Brownfields Agreement for this parcel similar to the
approach taken for the parcels to the north. However, we would believe that this would
be a fairly expensive undertaking for a site that is not extensively impacted.
Finally, we would attempt to investigate any upgradient sources that could have caused
the PCP groundwater exceedance in Geo-1 and the surface water detection in AOC-2
Down. Further research should be conducted as to whether DEQ would consider the
detection of PCP in the surface water at 6.9 ug/L poses an undue risk for the site.
Page 5 of 5

FIGURES

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File Name Figure Scale Project George and Sarah Smith Properties
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File Name Figure Scale Project George and Sarah Smith Properties
R19-068.xls 3 1"=260' approx. Siler City, North Carolina

TABLES

Table 1
Surface Water/Spring Analytical Results
Smith Family Property
1002 East Raleigh Street
Siler City, North Carolina
Soil Sample Location:
Method
Units
2B
AOC-1
AOC-2
AOC-2
AOC-4
Spring #2
Spring #3
Sample Date:
m/d/y
-
9.19.19
9.19.19
9.19.19
9.19.19
9.19.19
9.19.19
Sample ID:
ft bgs
-
West P/L-SW
Up -SW
Down -SW
DOT -SW
Farmhouse
Framhouse
Volatile Organic Compounds (VOCs)
Acetone
8260C
ug/L
2,000
ND
ND
ND
21
13
ND
Bromodichloromethane
8260C
ug/L
NS
ND
0.87
ND
ND
ND
ND
2-Butanone (MEK)
8260C
ug/L
20,000 HH
ND
ND
ND
4.0
ND
ND
Chloroform
8260C
ug/L
5.6 WS
ND
2.9
ND
ND
ND
ND
1, 1 -Dichloroethene
8260C
ug/L
1,500
ND
1.1
ND
ND
ND
ND
Methyl-tert-Butyl Ether
8260C
ug/L
19 (HH)
0.47
ND
ND
ND
ND
ND
Toluene
8260C
ug/L
11
ND
ND
ND
ND
0.35
ND
Total VOCs
8260C
ug/L
NS
0.47
4.87
ND
25.0
13.35
ND
Semivolatile Organic Compounds (SVOCs)
Naphthalene
8270E
ug/L
12
ND
ND
3.6
ND
NA
NA
Pentachlorophenol
8270E
ug/L
NS
ND
ND
6.9
ND
NA
NA
Total SVOCs
8270E
ug/L
NS
ND
ND
10.5
ND
NA
NA
Note
All 2B Standards for Freshwater Aquatic Life unless otherwise specified
2B - North Carolina Surface Water Standards
HH - Standard for Human Health
WS - Standard for Water Supply
bgs - Below Ground Surface
ND - Non -Detect
NS - No Standard Available

Table 2
Sediment Analytical Results
Smith Family Residence
1002 East Raleigh Street
Siler City, North Carolina
ANALYTE
SAMPLE IDENTIFICATION
Protection of
Groundwater
PSRG
Residential
PSRG
Ind
PSRG
AOC-1
Sed
AOC-2
Sed Up
AOC-2
Sed Down
AOC-4
Sed
9.19.19
9.19.19
9.19.19
9.19.19
0' b s
0' b s
0' b s
0' b s
West P/L
North P/L
South P/L
East P/L
Volatile Organic Compounds (VOCs-Method
8260D- mg/kg)
2-Butanone (MEK)
ND
ND
0.0038
0.0009
17
5,500
40,000
Acetone
ND
ND
0.036
ND
25
12,000
140,000
Carbon Disulfide
ND
0.00054
0.0006
ND
4.1
160
740
4-Isopropyltoluene
0.0023
ND
ND
ND
NS
NS
NS
Total VOCs
1 0.0023
1 0.00054
1 0.0404
1 0.0009
1 NS
NS
NS
Semivolatile Organic Co m ounds (SVOCs- Method 8270E-mg/kg)
1-Methylnaphthalene
ND
ND
ND
ND
0.11
18
73
2-Methylnaphthalene
ND
ND
ND
ND
3.1
48
600
Acenapthene
ND
ND
ND
ND
16
720
9000
Anthracene
ND
ND
ND
ND
1,300
3,600
45,000
Benzo(a)anthracene
0.40
0.33
ND
ND
0.35
1.1
21
Benzo(a)pyrene
0.33
0.34
ND
ND
0.12
0.11
2.1
Benzo(b)fluoranthene
0.53
0.47
ND
ND
1.2
1.1
21
Benzo(g,h.i)perylene
ND
0.36
ND
ND
NS
NS
NS
Benzo(k)fluoranthene
ND
0.21
ND
ND
12
11
210
Chrysene
0.38
0.43
ND
ND
36
110
2,100
Di-n-butylphthalate
0.46
ND
ND
ND
NS
NS
NS
Dibenzo(a,h)anthracene
ND
ND
ND
ND
0.380
0.11
2.1
Fluoranthene
0.91
0.78
0.28
ND
670
480
6,000
Fluorene
ND
ND
ND
ND
110
480
6,000
Indeno(1,2,3-cd)pyrene
ND
0.30
ND
ND
3.9
1.1
210
Naphthalene
ND
ND
ND
ND
0.39
4.1
18
Phenanthrene
0.60
0.47
ND
ND
NS
NS
NS
Pyrene
0.72
0.58
ND
ND
440
360
4,500
Total SVOCs
4.33
4.27
0.28
ND
NS
NS
NS
Note:
NA - Not Analyzed Result Exceeds Protection of Groundwater PSRG
ND- Not Detected -Result Exceeds Residential PSRG
NS- No Standard -Result Exceeds Commercial/Industrial PSRG
-Result Exceeds Protection of Groundwater PSRG and Residential PSRG
-Result Exceeds Residential and CommAnd PSRG
Result Exceeds All PSRGs and SRGs
PSRG- Preliminary Soil Remediation Goal

Table 3
Groundwater Analytical Results
Smith Family Property
1002 East Raleigh Street
Siler City, North Carolina
Soil Sample Location:
Method
Units
2L
Geo-1
Sample Date:
m/d/y
-
9.19.19
Sample Depth:
ft bgs
-
-
Volatile Organic Compounds (VOCs)
1, 1 -Dichloroethene
8260C
ug/L
350
15
Isopropyl Ether
8260C
ug/L
70
5.6
Methyl-tert-Butyl Ether
8260C
ug/L
20
140
Total VOCs
8260C
ug/L
NS
160.6
Semivolatile Organic Compounds (SVOCs)
Diethylphthalate
8270E
ug/L
6,000
6.0
Naphthalene
8270E
ug/L
6
3.2
Pentachlorophenol
8270E
ug/L
0.3
7.0
Total SVOCs
8270E
ug/L
NS
16.2
Note:
2L- North Carolina Groundwater Standards (NCAC C. 0202)
bgs = Below Ground Surface
ND= Non -Detect
NS = No Standard Available

APPENDIX A

Geoprobe TM Sample Collection
he Geoprobe TM consists of a truck -mounted hydraulic system with a stainless
steel sampling probe that is directly pushed into the subsurface. The sampling
probe is made up of a stainless steel hollow core body with an internal Teflon
TM or polyethylene sample liner. Once the probe has been advanced to the
desired depth, a dummy tip is withdrawn from the core body. The sample is collected by
advancing the opened core body over a discrete interval, thereby filling the sample liner
with soil. The probe is subsequently withdrawn from the boring, and the liner containing
the soil sample removed and opened. Once the soil has been retrieved from the liner,
each soil sample may be split into two portions; one portion designated for headspace soil
gas screening to determine the presence, and the second portion transferred to a 100-m1
pre -cleaned glass jar, designated for potential laboratory analysis.
Headspace Screening:
Soils are typically screened with an organic vapor analyzer (OVA) for total volatile organic compounds
(VOCs), which may indicate organic or petroleum hydrocarbon contamination. A typical procedure for
screening soils involves filling a clean container (e.g., glass jar or plastic baggie) approximately halfway
with soil and sealing the container. This creates a headspace in which the VOCs in the soil accumulate and
equilibrate. After allowing approximately 10 to 15 minutes for this process to occur, the probe of the OVA
is inserted through the container's seal into the headspace of the container to obtain a VOC reading.
Soil Sample Collection for Analysis:
Geoprobe TM soil samples selected for laboratory analysis are placed into pre -cleaned containers supplied
by the laboratory for the analysis proposed for the particular site. The jars are the labeled appropriately
with the sampler's name, date of collection, sample number, analysis to be preformed, and project
designation before being stored and transported to the analytical laboratory in an insulated cooler chilled to
approximately 4.0 °C. To ensure sample integrity, all samples are transported in accordance with EPA
chain -of -custody protocols. All samples are typically transported to the laboratory within 48 hours of
sample collection, if possible.
Geoprobe TM Groundwater Sample Collection:
Groundwater samples are collected directly from the Geoprobe TM. During the sampling event, the sampler
is typically pushed to the desired depth with a screened unit sealed inside the sampler. At the desired
sampling depth, the screen is exposed by retracting the push rod. Once the open sampler fills with
groundwater, we use a peristaltic pump attached to either Teflon of polyethylene tubing which is advanced
inside the drill rods to the desired depth. During the purging process, we will typically initially purge until
the sample aliquot is relatively free of sediment. We then use low flow methodologies to collect field
parameter readings (pH, conductivity and temperature) and ultimately collect a sample for laboratory
analysis. During the purging process, we attempt to achieve repeat readings within 5% before collecting a
laboratory sample. The only exception to this methodology is if it appears that the boring is going dry
which would prevent obtaining any sample. If we believe the boring will purge to dryness, we will
immediately collect a sample.
All groundwater samples are decanted into laboratory provided containers appropriate for the parameters
being analyzed, preserved as required by the analytical technique, and labeled with the following
information: sampler's name, date of collection, sample number, analysis to be preformed, and project
designation. Samples are stored and transported to the analytical laboratory in an insulated cooler chilled to
approximately 4.0 °C. To ensure sample integrity, all samples are transported in accordance with EPA
chain -of -custody protocols. All samples are typically transported to the laboratory within 48 hours of
sample collection, if possible.
Waters Edge Environmental, LLC.
Standard Procedures: February 2001

APPENDIX
B

2�SENCO Laboratories
9g
Accurate. Timely. Respousive. luuavative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, October 4, 2019
WATERS EDGE ENVIRONMENTAL (WA020)
Attn: Phil Rahn
1434 Chester Road
Raleigh, NC 27608
RE: Laboratory Results for
Project Number: R19-39, Project Name/Desc: Smith Property FSA
ENCO Workorder(s): CC16129
Dear Phil Rahn,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, September 20, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Bill Scott
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of iJJ

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: GEO-1
Lab ID: CC16129-01
Sampled: 09/19/19 10:30
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
10/03/19
09/26/19 13:30
09/27/19 07:53
EPA 8270E
EPA 3510C_MS
09/26/19 10/31/19
09/21/19 07:54
09/23/19 21:08
Client ID: AOC-1 SW
Lab ID: CC16129-02
Sampled: 09/19/19 10:45
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
10/03/19
09/26/19 13:30
09/27/19 08:24
EPA 8270E
EPA 3510C_MS
09/26/19 10/31/19
09/21/19 07:54
09/23/19 21:38
Client ID: AOC-1 SED
Lab ID: CC16129-03
Sampled: 09/19/19 11:00
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5035_MS
10/03/19
10/02/19 12:41
10/02/19 19:21
EPA 8270E
EPA 3550C_MS
10/03/19 11/02/19
09/23/19 14:03
09/25/19 14:41
Client ID: AOC-2 UP SW
Lab ID: CC16129-04
Sampled: 09/19/19 11:15
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
10/03/19
09/26/19 13:30
09/27/19 08:56
EPA 8270E
EPA 3510C_MS
09/26/19 10/31/19
09/21/19 07:54
09/23/19 22:08
Client ID: AOC-2 UP SED
Lab ID: CC16129-05
Sampled: 09/19/19 11:20
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5035_MS
10/03/19
10/02/19 12:41
10/02/19 19:52
EPA 8270E
EPA 3550C_MS
10/03/19 11/02/19
09/23/19 14:03
09/25/19 17:14
Client ID: AOC-2 DOWN SW
Lab ID: CC16129-06
Sampled: 09/19/19 11:50
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
10/03/19
09/26/19 13:30
09/27/19 09:27
EPA 8270E
EPA 3510C_MS
09/26/19 10/31/19
09/21/19 07:54
09/23/19 22:38
Client ID: AOC-2 DOWN SED
Lab ID: CC16129-07
Sampled: 09/19/19 12:00
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5035_MS
10/03/19
10/02/19 12:41
10/02/19 20:23
EPA 8270E
EPA 3550C_MS
10/03/19 11/02/19
09/23/19 14:03
09/25/19 15:11
Client ID: AOC-4 SW
Lab ID: CC16129-08
Sampled: 09/19/19 13:15
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
10/03/19
09/26/19 13:30
09/27/19 09:58
EPA 8270E
EPA 3510C_MS
09/26/19 10/31/19
09/21/19 07:54
09/23/19 23:08
Client ID: AOC-4 SED
Lab ID: CC16129-09
Sampled: 09/19/19 13:25
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5035_MS
10/03/19
10/03/19 09:45
10/03/19 15:21
EPA 8270E
EPA 3550C_MS
10/03/19 11/02/19
09/23/19 14:03
09/25/19 15:42
Client ID: AOC-5 -SPRING #2
Lab ID: CC16129-10
Sampled: 09/19/19 13:50
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
10/03/19
09/26/19 13:30
09/27/19 10:29
Client ID: AOC-5 -SPRING #2
Lab ID: CC16129-10RE1
Sampled: 09/19/19 13:50
Received: 09/20/19 11:05
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
10/03/19
09/30/19 14:34
10/01/19 11:20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 65

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: AOC-5 -SPRING #3 Lab ID: CC16129-11 Sampled: 09/19/19 14:15 Received: 09/20/19 11:05
Parameter Preparation Hold Date/Time(s)
EPA 8260D EPA 5030B_MS 10/03/19
Prep Date/Time(s) Analysis Date/Time(s)
09/27/19 09:49 09/28/19 00:38
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of F)5

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SAMPLE DETECTION SUMMARY
Client ID: GEO-1
Lab ID:
CC16129-01
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
1,1-Dichloroethene
15
0.21
1.0
ug/L
EPA 8260D
Diethyl phthalate
6.0
J
2.4
10
ug/L
EPA 8270E
Isopropyl Ether
5.6
0.36
1.0
ug/L
EPA 8260D
Methyl-tert-Butyl Ether
140
0.16
1.0
ug/L
EPA 8260D
Naphthalene
3.2
J
2.8
10
ug/L
EPA 8270E
Pentachlorophenol
7.0
J
2.1
10
ug/L
EPA 8270E
Client ID: AOC-1 SW
Lab ID:
CC16129-02
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
Methyl-tert-Butyl Ether
0.47
J
0.16
1.0
ug/L
EPA 8260D
Client ID: AOC-1 SED
Lab ID:
CC16129-03
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
4-Isopropyltoluene
0.0023
0.00022
0.0014
mg/kg dry
EPA 8260D
Benzo(a)anthracene
0.40
JD
0.19
2.3
mg/kg dry
EPA 8270E
Benzo(a)pyrene
0.33
JD
0.23
2.3
mg/kg dry
EPA 8270E
Benzo(b)fluoranthene
0.53
JD
0.13
2.3
mg/kg dry
EPA 8270E
Chrysene
0.38
JD
0.21
2.3
mg/kg dry
EPA 8270E
Di-n-butylphthalate
0.46
JD
0.29
2.3
mg/kg dry
EPA 8270E
Fluoranthene
0.91
JD
0.25
2.3
mg/kg dry
EPA 8270E
Phenanthrene
0.60
JD
0.19
2.3
mg/kg dry
EPA 8270E
Pyrene
0.72
JD
0.26
2.3
mg/kg dry
EPA 8270E
Client ID: AOC-2 UP SW
Lab ID:
CC16129-04
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
1,1-Dichloroethene
1.1
0.21
1.0
ug/L
EPA 8260D
Bromodichloromethane
0.87
J
0.17
1.0
ug/L
EPA 8260D
Chloroform
2.9
0.18
1.0
ug/L
EPA 8260D
Client ID: AOC-2 UP SED
Lab ID:
CC16129-05
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
Benzo(a)anthracene
0.33
JD
0.17
2.0
mg/kg dry
EPA 8270E
Benzo(a)pyrene
0.34
JD
0.20
2.0
mg/kg dry
EPA 8270E
Benzo(b)fluoranthene
0.47
JD
0.11
2.0
mg/kg dry
EPA 8270E
Benzo(g,h,i)perylene
0.36
JD
0.29
2.0
mg/kg dry
EPA 8270E
Benzo(k)fluoranthene
0.21
JD
0.20
2.0
mg/kg dry
EPA 8270E
Carbon disulfide
0.00054
J
0.00036
0.0047
mg/kg dry
EPA 8260D
Chrysene
0.43
JD
0.18
2.0
mg/kg dry
EPA 8270E
Fluoranthene
0.78
JD
0.22
2.0
mg/kg dry
EPA 8270E
Indeno(1,2,3-cd)pyrene
0.30
JD
0.29
2.0
mg/kg dry
EPA 8270E
QV-01
Phenanthrene
0.47
JD
0.17
2.0
mg/kg dry
EPA 8270E
Pyrene
0.58
JD
0.23
2.0
mg/kg dry
EPA 8270E
Client ID: AOC-2 DOWN SW
Lab ID:
CC16129-06
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
Naphthalene
3.6
J
2.8
10
ug/L
EPA 8270E
Pentachloroohenol
6.9
J
2.1
10
ua/L
EPA 8270E
Client ID: AOC-2 DOWN SED
Lab ID:
CC16129-07
Anala
Results
Flag
MDL
POLL
Units
Method Notes
2-Butanone
0.0038
J
0.00091
0.0058
mg/kg dry
EPA 8260D
Acetone
0.036
0.016
0.023
mg/kg dry
EPA 8260D
Carbon disulfide
0.00060
J
0.00046
0.0058
mg/kg dry
EPA 8260D
Fluoranthene
0.28
JD
0.23
2.1
mg/kg dry
EPA 8270E
Client ID: AOC-4 SW
Lab ID:
CC16129-08
Anala
Results
Flag
MDL
POLL
Units
Method Notes
2-Butanone
4.0
J
1.3
5.0
ug/L
EPA 8260D
Acetone
21
10
20
ug/L
EPA 8260D
Client ID: AOC-4 SED
Lab ID:
CC16129-09
Anala
Results
Flag
MDL
POLL
Units
Method Notes
2-Butanone
0.00090
J
0.00052
0.0033
mg/kg dry
EPA 8260D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 65

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SAMPLE DETECTION SUMMARY
Client ID: AOC-S -SPRING #2 Lab ID: CC16129-30RE3
Anala Results Flag MDL POLL Units Method Notes
Acetone 13 1 10 20 ug/L EPA 8260D
Toluene 0.35 1 0.14 1.0 ug/L EPA 8260D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of 65

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ANALYTICAL RESULTS
Description: GEO-1 Lab Sample ID:CC16129-01 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 10:30 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,1,1-Trichloroethane [71-55-6]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,1,2-Trichloroethane [79-00-5]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,1-Dichloroethane [75-34-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,1-Dichloroethene [75-35-4]^
15
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,1-Dichloropropene [563-58-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
ug/L
1
0.012
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,2,3-Trichloropropane [96-18-4]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,2-Dibromoethane [106-93-4]^
ND
ug/L
1
0.66
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,2-Dichloroethane [107-06-2]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,2-Dichloropropane [78-87-5]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
ug/L
1
0.30
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,3-Dichloropropane [142-28-9]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
2,2-Dichloropropane [594-20-7]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
2-Butanone [78-93-3]^
ND
ug/L
1
1.3
5.0
9I26038
EPA 8260D
09/27/19
07:53
REF
2-Chloroethyl Vinyl Ether[110-75-8]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
07:53
REF
2-Chlorotoluene [95-49-8]^
ND
ug/L
1
0.081
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
2-Hexanone [591-78-6]^
ND
ug/L
1
0.88
5.0
9I26038
EPA 8260D
09/27/19
07:53
REF
4-Chlorotoluene [106-43-4]^
ND
ug/L
1
0.068
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
4-Isopropyltoluene [99-87-6]^
ND
ug/L
1
0.085
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
4-Methyl-2-pentanone [108-10-1]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Acetone [67-64-1]^
ND
ug/L
1
10
20
9I26038
EPA 8260D
09/27/19
07:53
REF
Benzene[71-43-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Bromobenzene [108-86-1]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Bromochloromethane [74-97-5]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Bromodichloromethane [75-27-4]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Bromoform [75-25-2]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Bromomethane [74-83-9]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Carbon disulfide [75-15-0]^
ND
ug/L
1
1.5
5.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Carbon tetrachloride [56-23-5]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Chlorobenzene [108-90-7]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Chloroethane [75-00-3]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Chloroform [67-66-3]^
ND
ug/L
1
0.18
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Chloromethane [74-87-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Dibromochloromethane [124-48-1]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Dibromomethane [74-95-3]^
ND
ug/L
1
0.27
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Dichlorodifluoromethane [75-71-8]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Ethylbenzene [100-41-4]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 65

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ANALYTICAL RESULTS
Description: GEO-1 Lab Sample ID:CC16129-01 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 10:30 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flao
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Isopropyl Ether [108-20-3]^
5.6
ug/L
1
0.36
1.0
9][26038
EPA 8260D
09/27/19
07:53
REF
Isopropylbenzene [98-82-8]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
m,p-Xylenes [108-38-3/106-42-3]^
ND
ug/L
1
0.17
2.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Methylene chloride [75-09-2]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Methyl-tert-Butyl Ether [1634-04-4]^
140
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Naphthalene [91-20-3]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
n-Butyl Benzene [104-51-8]^
ND
ug/L
1
0.058
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
n-Propyl Benzene [103-65-1]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
o-Xylene [95-47-6]^
ND
ug/L
1
0.065
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
sec-Butylbenzene [135-98-8]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Styrene [100-42-5]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
tert-Butyl benzene [98-06-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Tetrachloroethene [127-18-4]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Toluene [108-88-3]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Trichloroethene [79-01-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Trichlorofluoromethane [75-69-4]^
ND
ug/L
1
0.24
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Vinyl chloride [75-01-4]^
ND
ug/L
1
0.32
1.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Xylenes (Total) [1330-20-7]^
ND
ug/L
1
0.45
3.0
9I26038
EPA 8260D
09/27/19
07:53
REF
Surrogates
Results DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analvzed
" Notes
4-Bromofluorobenzene
44 1
50.0
87 %
53-136
9126038
EPA 8260D
09127119 07.•53
REF
Dibromofluoromethane
45 1
50.0
90 %
67-129
9126038
EPA 8260D
09127119 07.•53
REF
Toluene-d8
37 1
50.0
75 %
59-134
9126038
EPA 8260D
09127119 07.•53
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flaa
Units
DF
MDL
Q
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
2.4
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
1-Methylnaphthalene [90-12-0]^
ND
ug/L
1
2.7
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2,4,5-Trichlorophenol[95-95-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2,4,6-Trichlorophenol[88-06-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2,4-Dichlorophenol [120-83-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2,4-Dimethylphenol [105-67-9]^
ND
ug/L
1
2.3
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2,4-Dinitrophenol [51-28-5]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2,4-Dinitrotoluene [121-14-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2,6-Dinitrotoluene [606-20-2]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2-Chloronaphthalene [91-58-7]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2-Chlorophenol[95-57-8]^
ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]^
ND
ug/L
1
3.3
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2-Methylnaphthalene [91-57-6]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2-Methylphenol[95-48-7]^
ND
ug/L
1
2.0
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
2-Nitroaniline [88-74-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
FINAL
This report relates only to the
sample as received by the laboratory,
and may only be reproduced in full.
I Page 7 Of 65

(� �Eo
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ANALYTICAL RESULTS
Description: GEO-1 Lab Sample ID:CC16129-01 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 10:30 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
ND
ug/L
1
1.1
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
ND
ug/L
1
2.1
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
3,3'-Dichlorobenzidine [91-94-1]^
ND
ug/L
1
3.5
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
3-Nitroaniline [99-09-2]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
4-Bromophenyl-phenylether[101-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
4-Chloro-3-methylphenol[59-50-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
4-Chloroaniline [106-47-8]^
ND
ug/L
1
2.0
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
4-Nitroaniline [100-01-6]^
ND
ug/L
1
3.2
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
4-Nitrophenol[100-02-7]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Acenaphthene [83-32-9]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Acenaphthylene[208-96-8]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Anthracene [120-12-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Benzidine [92-87-5]^
ND
ug/L
1
1.6
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Benzo(a)anthracene [56-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Benzo(a)pyrene [50-32-8]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Benzo(b)fluoranthene [205-99-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Benzo(g,h,i)perylene [191-24-2]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Benzo(k)fluoranthene [207-08-9]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Benzoic acid [65-85-0]^
ND
ug/L
1
1.0
50
9I20004
EPA
8270E
09/23/19
21:08
DFM
Benzylalcohol [100-51-6]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Bis(2-chloroethyl)ether[111-44-4]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:08
DFM QV-01
Bis(2-ethylhexyl)phthalate [117-81-7]^
ND
ug/L
1
1.9
5.0
9I20004
EPA
8270E
09/23/19
21:08
DFM
Butyl benzylphtha late [85-68-7]^
ND
ug/L
1
3.8
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Chrysene [218-01-9]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Dibenzo(a,h)anthracene [53-70-3]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Dibenzofuran [132-64-9]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Diethylphthalate [84-66-2]^
6.0 J
ug/L
1
2.4
10
9120004
EPA
8270E
09/23/19
21:08
DFM
Dimethylphthalate [131-11-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Di-n-butylphthalate [84-74-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Di-n-octylphthalate [117-84-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Fluoranthene [206-44-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Fluorene [86-73-7]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Hexachlorobenzene [118-74-1]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Hexachlorocyclopentadiene [77-47-4]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Hexachloroethane [67-72-1]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Isophorone [78-59-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
Naphthalene [91-20-3]^
3.2 J
ug/L
1
2.8
10
9120004
EPA
8270E
09/23/19
21:08
DFM
Nitrobenzene [98-95-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
N-Nitrosodimethylamine [62-75-9]^
ND
ug/L
1
1.9
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
N-nitrosodiphenylamine/Diphenylamine
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:08
DFM
[86-30-6/122-39-4]^
Pentachlorophenol[87-86-S]^
7.0 J
ug/L
1
2.1
10
9120004
EPA
8270E
09/23/19
21:08
DFM
FINAL
This report relates only to the sample as received
by the
laboratory,
and may only
be reproduced in full.
I Page 8 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: GEO-1 Lab Sample ID:CC16129-01 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 10:30 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Phenanthrene[85-01-8]A ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
Phenol[108-95-2]A ND
ug/L
1
1.7
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
Pyrene [129-00-0]A ND
ug/L
1
3.5
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
Pyridine [110-86-1]A ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 21:08
DFM
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
2,4,6-Tribromophenol
89
1
100
89 %
10-179
9120004
EPA 8270E
09123119 21:08
DFM
2-Fluorobiphenyl
44
1
50.0
88 %
10-149
9120004
EPA 8270E
09123119 21:08
DFM
2-Fluorophenol
54
1
100
54 %
10-110
9120004
EPA 8270E
09123119 21:08
DFM
Nitrobenzene-d5
41
1
50.0
81 %
10-149
9120004
EPA 8270E
09123119 21:08
DFM
Phenol-d5
53
1
100
53 %
10-88
9120004
EPA 8270E
09123119 21:08
DFM
Terphenyl-d14
52
1
50.0
103 %
10-166
9120004
EPA 8270E
09123119 21:08
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 Of 65

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-1 SW Lab Sample ID:CC16129-02 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 10:45 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,1,1-Trichloroethane [71-55-6]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,1,2-Trichloroethane [79-00-5]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,1-Dichloroethane [75-34-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,1-Dichloroethene [75-35-4]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,1-Dichloropropene [563-58-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
ug/L
1
0.012
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,2,3-Trichloropropane [96-18-4]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,2-Dibromoethane [106-93-4]^
ND
ug/L
1
0.66
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,2-Dichloroethane [107-06-2]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,2-Dichloropropane [78-87-5]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
ug/L
1
0.30
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,3-Dichloropropane [142-28-9]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
2,2-Dichloropropane [594-20-7]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
2-Butanone [78-93-3]^
ND
ug/L
1
1.3
5.0
9I26038
EPA 8260D
09/27/19
08:24
REF
2-Chloroethyl Vinyl Ether[110-75-8]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
08:24
REF
2-Chlorotoluene [95-49-8]^
ND
ug/L
1
0.081
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
2-Hexanone [591-78-6]^
ND
ug/L
1
0.88
5.0
9I26038
EPA 8260D
09/27/19
08:24
REF
4-Chlorotoluene [106-43-4]^
ND
ug/L
1
0.068
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
4-Isopropyltoluene [99-87-6]^
ND
ug/L
1
0.085
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
4-Methyl-2-pentanone [108-10-1]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Acetone [67-64-1]^
ND
ug/L
1
10
20
9I26038
EPA 8260D
09/27/19
08:24
REF
Benzene[71-43-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Bromobenzene [108-86-1]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Bromochloromethane [74-97-5]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Bromodichloromethane [75-27-4]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Bromoform [75-25-2]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Bromomethane [74-83-9]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Carbon disulfide [75-15-0]^
ND
ug/L
1
1.5
5.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Carbon tetrachloride [56-23-5]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Chlorobenzene [108-90-7]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Chloroethane [75-00-3]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Chloroform [67-66-3]^
ND
ug/L
1
0.18
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Chloromethane [74-87-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Dibromochloromethane [124-48-1]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Dibromomethane [74-95-3]^
ND
ug/L
1
0.27
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Dichlorodifluoromethane [75-71-8]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Ethylbenzene [100-41-4]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 10 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-1 SW Lab Sample ID:CC16129-02 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 10:45 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flao
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Isopropyl Ether[108-20-3]^
ND
ug/L
1
0.36
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Isopropylbenzene [98-82-8]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
m,p-Xylenes [108-38-3/106-42-3]^
ND
ug/L
1
0.17
2.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Methylene chloride [75-09-2]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Methyl-tert-Butyl Ether [1634-04-4]^
0.47 J
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Naphthalene [91-20-3]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
n-Butyl Benzene [104-51-8]^
ND
ug/L
1
0.058
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
n-Propyl Benzene [103-65-1]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
o-Xylene [95-47-6]^
ND
ug/L
1
0.065
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
sec-Butylbenzene [135-98-8]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Styrene [100-42-5]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
tert-Butyl benzene [98-06-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Tetrachloroethene [127-18-4]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Toluene [108-88-3]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Trichloroethene [79-01-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Trichlorofluoromethane [75-69-4]^
ND
ug/L
1
0.24
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Vinyl chloride [75-01-4]^
ND
ug/L
1
0.32
1.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Xylenes (Total) [1330-20-7]^
ND
ug/L
1
0.45
3.0
9I26038
EPA 8260D
09/27/19
08:24
REF
Surrogates
Results DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analvzed
" Notes
4-Bromofluorobenzene
43 1
50.0
87 %
53-136
9126038
EPA 8260D
09127119 08:24
REF
Dibromofluoromethane
46 1
50.0
91 %
67-129
9126038
EPA 8260D
09127119 08:24
REF
Toluene-d8
37 1
50.0
73 %
59-134
9126038
EPA 8260D
09127119 08:24
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flaa
Units
DF
MDL
Q
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
2.4
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
1-Methylnaphthalene [90-12-0]^
ND
ug/L
1
2.7
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2,4,5-Trichlorophenol[95-95-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2,4,6-Trichlorophenol[88-06-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2,4-Dichlorophenol [120-83-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2,4-Dimethylphenol [105-67-9]^
ND
ug/L
1
2.3
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2,4-Dinitrophenol [51-28-5]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2,4-Dinitrotoluene [121-14-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2,6-Dinitrotoluene [606-20-2]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2-Chloronaphthalene [91-58-7]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2-Chlorophenol[95-57-8]^
ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]^
ND
ug/L
1
3.3
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2-Methylnaphthalene [91-57-6]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2-Methylphenol[95-48-7]^
ND
ug/L
1
2.0
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
2-Nitroaniline [88-74-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
FINAL
This report relates only to the
sample as received by the laboratory,
and may only be reproduced in full.
I Page 11 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-1 SW Lab Sample ID:CC16129-02 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 10:45 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl
Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
ND
ug/L
1
1.1
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
ND
ug/L
1
2.1
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
3,3'-Dichlorobenzidine [91-94-1]^
ND
ug/L
1
3.5
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
3-Nitroaniline [99-09-2]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
4-Bromophenyl-phenylether[101-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
4-Chloro-3-methylphenol[59-50-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
4-Chloroaniline [106-47-8]^
ND
ug/L
1
2.0
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
4-Nitroaniline [100-01-6]^
ND
ug/L
1
3.2
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
4-Nitrophenol[100-02-7]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Acenaphthene [83-32-9]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Acenaphthylene[208-96-8]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Anthracene [120-12-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Benzidine [92-87-5]^
ND
ug/L
1
1.6
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Benzo(a)anthracene [56-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Benzo(a)pyrene [50-32-8]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Benzo(b)fluoranthene [205-99-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Benzo(g,h,i)perylene [191-24-2]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Benzo(k)fluoranthene [207-08-9]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Benzoic acid [65-85-0]^
ND
ug/L
1
1.0
50
9I20004
EPA
8270E
09/23/19
21:38
DFM
Benzylalcohol [100-51-6]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Bis(2-chloroethyl)ether[111-44-4]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:38
DFM QV-01
Bis(2-ethylhexyl)phthalate [117-81-7]^
ND
ug/L
1
1.9
5.0
9I20004
EPA
8270E
09/23/19
21:38
DFM
Butyl benzylphtha late [85-68-7]^
ND
ug/L
1
3.8
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Chrysene [218-01-9]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Dibenzo(a,h)anthracene [53-70-3]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Dibenzofuran [132-64-9]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Diethylphtha late [84-66-2]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Dimethylphthalate [131-11-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Di-n-butylphthalate [84-74-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Di-n-octylphthalate [117-84-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Fluoranthene [206-44-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Fluorene [86-73-7]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Hexachlorobenzene [118-74-1]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Hexachlorocyclopentadiene [77-47-4]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Hexachloroethane [67-72-1]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Isophorone [78-59-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Naphthalene[91-20-3]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
Nitrobenzene [98-95-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
N-Nitrosodimethylamine [62-75-9]^
ND
ug/L
1
1.9
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
N-nitrosodiphenylamine/Diphenylamine
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
ND
ug/L
1
2.1
10
9I20004
EPA
8270E
09/23/19
21:38
DFM
FINAL
This report relates only to the sample as received
by the
laboratory,
and may only
be reproduced in full.
I Page 12 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-1 SW Lab Sample ID:CC16129-02 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 10:45 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Phenanthrene[85-01-8]A ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
Phenol[108-95-2]A ND
ug/L
1
1.7
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
Pyrene [129-00-0]A ND
ug/L
1
3.5
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
Pyridine [110-86-1]A ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 21:38
DFM
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
2,4,6-Tribromophenol
88
1
100
88 %
10-179
9120004
EPA 8270E
09123119 21:38
DFM
2-Fluorobiphenyl
44
1
50.0
88 %
10-149
9120004
EPA 8270E
09123119 21:38
DFM
2-Fluorophenol
49
1
100
49 %
10-110
9120004
EPA 8270E
09123119 21:38
DFM
Nitrobenzene-d5
40
1
50.0
80 %
10-149
9120004
EPA 8270E
09123119 21:38
DFM
Phenol-d5
42
1
100
42 %
10-88
9120004
EPA 8270E
09123119 21:38
DFM
Terphenyl-d14
50
1
50.0
100 %
10-166
9120004
EPA 8270E
09123119 21:38
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 13 Of 65

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-1 SED Lab Sample ID:CC16129-03 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 11:00 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 71.92
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
Q
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
mg/kg
dry
1
0.00022
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,1,1-Trichloroethane [71-55-6]^
ND
mg/kg
dry
1
0.00035
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
mg/kg
dry
1
0.00028
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,1,2-Trichloroethane [79-00-5]^
ND
mg/kg
dry
1
0.00035
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,1-Dichloroethane [75-34-3]^
ND
mg/kg
dry
1
0.00035
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,1-Dichloroethene [75-35-4]^
ND
mg/kg
dry
1
0.00042
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,1-Dichloropropene [563-58-6]^
ND
mg/kg
dry
1
0.00022
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
mg/kg
dry
1
0.00039
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,2,3-Trichloropropane [96-18-4]^
ND
mg/kg
dry
1
0.00089
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
mg/kg
dry
1
0.00038
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
mg/kg
dry
1
0.00024
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
mg/kg
dry
1
0.0011
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,2-Dibromoethane [106-93-4]^
ND
mg/kg
dry
1
0.00064
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,2-Dichlorobenzene [95-50-1]^
ND
mg/kg
dry
1
0.00038
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,2-Dichloroethane [107-06-2]^
ND
mg/kg
dry
1
0.00057
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,2-Dichloropropane [78-87-5]^
ND
mg/kg
dry
1
0.00036
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
mg/kg
dry
1
0.00028
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,3-Dichlorobenzene [541-73-1]^
ND
mg/kg
dry
1
0.00031
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,3-Dichloropropane [142-28-9]^
ND
mg/kg
dry
1
0.00040
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
1,4-Dichlorobenzene [106-46-7]^
ND
mg/kg
dry
1
0.00028
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
2,2-Dichloropropane [594-20-7]^
ND
mg/kg
dry
1
0.00032
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
2-Butanone [78-93-3]^
ND
mg/kg
dry
1
0.0011
0.0070
9302035
EPA 8260D
10/02/19
19:21
REF
2-Chloroethyl Vinyl Ether [110-75-8]^
ND
mg/kg
dry
1
0.00022
0.0070
9302035
EPA 8260D
10/02/19
19:21
REF
2-Chlorotoluene [95-49-8]^
ND
mg/kg
dry
1
0.00025
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
2-Hexanone [591-78-6]^
ND
mg/kg
dry
1
0.0010
0.0070
9302035
EPA 8260D
10/02/19
19:21
REF
4-Chlorotoluene [106-43-4]^
ND
mg/kg
dry
1
0.00036
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
4-Isopropyltoluene [99-87-6]^
0.0023
mg/kg
dry
1
0.00022
0.0014
9102035
EPA 8260D
10/02/19
19:21
REF
4-Methyl-2-pentanone [108-10-1]^
ND
mg/kg
dry
1
0.00079
0.0070
9302035
EPA 8260D
10/02/19
19:21
REF
Acetone [67-64-1]^
ND
mg/kg
dry
1
0.019
0.028
9302035
EPA 8260D
10/02/19
19:21
REF
Benzene [71-43-2]^
ND
mg/kg
dry
1
0.00024
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Bromobenzene [108-86-1]^
ND
mg/kg
dry
1
0.00031
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Bromochloromethane [74-97-5]^
ND
mg/kg
dry
1
0.00057
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Bromodichloromethane [75-27-4]^
ND
mg/kg
dry
1
0.00033
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Bromoform [75-25-2]^
ND
mg/kg
dry
1
0.00063
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Bromomethane [74-83-9]^
ND
mg/kg
dry
1
0.00044
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Carbon disulfide [75-15-0]^
ND
mg/kg
dry
1
0.00054
0.0070
9302035
EPA 8260D
10/02/19
19:21
REF
Carbon Tetrachloride [56-23-5]^
ND
mg/kg
dry
1
0.00031
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Chlorobenzene [108-90-7]^
ND
mg/kg
dry
1
0.00024
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Chloroethane [75-00-3]^
ND
mg/kg
dry
1
0.00035
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF QV-01
Chloroform [67-66-3]^
ND
mg/kg
dry
1
0.00025
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Chloromethane [74-87-3]^
ND
mg/kg
dry
1
0.00029
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
mg/kg
dry
1
0.00032
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
mg/kg
dry
1
0.00024
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Dibromochloromethane [124-48-1]^
ND
mg/kg
dry
1
0.00049
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Dibromomethane [74-95-3]^
ND
mg/kg
dry
1
0.00046
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Dichlorodifluoromethane [75-71-8]^
ND
mg/kg
dry
1
0.00063
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF QV-01
Ethylbenzene [100-41-4]^
ND
mg/kg
dry
1
0.00028
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-1 SED Lab Sample ID:CC16129-03 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 11:00 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 71.92
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flag
Units
DF
MDL
Q
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]^
ND
mg/kg
dry
1
0.00049
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Isopropyl Ether[108-20-3]^
ND
mg/kg
dry
1
0.00025
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Isopropylbenzene [98-82-8]^
ND
mg/kg
dry
1
0.00021
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
m,p-Xylenes [108-38-3/106-42-3]^
ND
mg/kg
dry
1
0.00051
0.0028
9302035
EPA 8260D
10/02/19
19:21
REF
Methylene Chloride [75-09-2]^
ND
mg/kg
dry
1
0.0010
0.0028
9302035
EPA 8260D
10/02/19
19:21
REF
Methyl-tert-Butyl Ether [1634-04-4]^
ND
mg/kg
dry
1
0.00042
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Naphthalene [91-20-3]^
ND
mg/kg
dry
1
0.00038
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
n-Butyl Benzene [104-51-8]^
ND
mg/kg
dry
1
0.00018
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
n-Propyl Benzene [103-65-1]^
ND
mg/kg
dry
1
0.00025
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
o-Xylene [95-47-6]^
ND
mg/kg
dry
1
0.00031
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
sec-Butylbenzene [135-98-8]^
ND
mg/kg
dry
1
0.0013
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Styrene [100-42-5]^
ND
mg/kg
dry
1
0.0014
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
tert-Butyl benzene [98-06-6]^
ND
mg/kg
dry
1
0.00024
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Tetrachloroethene [127-18-4]^
ND
mg/kg
dry
1
0.00039
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Toluene [108-88-3]^
ND
mg/kg
dry
1
0.00033
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
mg/kg
dry
1
0.00051
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
mg/kg
dry
1
0.00054
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Trichloroethene [79-01-6]^
ND
mg/kg
dry
1
0.00044
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF
Trichlorofluoromethane [75-69-4]^
ND
mg/kg
dry
1
0.00036
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF QV-01
Vinyl chloride [75-01-4]^
ND
mg/kg
dry
1
0.00033
0.0014
9302035
EPA 8260D
10/02/19
19:21
REF QV-01
Xylenes (Total) [1330-20-7]^
ND
mg/kg
dry
1
0.00078
0.0042
9302035
EPA 8260D
10/02/19
19:21
REF
surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Anaivzed
" Notes
4-Bromofluorobenzene
38
1
50.0
76 %
50-127
9JO2035
EPA 8260D
10/02/19 19:21
REF
Dibromofluoromethane
42
1
50.0
84 %
52-128
9JO2035
EPA 8260D
10/02/1919:21
REF
Toluene-d8
33
1
50.0
66 %
57-124
9JO2035
EPA 8260D
10/02/19 19:21
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
4
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
ND
mg/kg dry
5
0.18
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
1,2-Dichlorobenzene [95-50-1]^
ND
mg/kg dry
5
0.16
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
1,3-Dichlorobenzene [541-73-1]^
ND
mg/kg dry
5
0.14
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
1,4-Dichlorobenzene [106-46-7]^
ND
mg/kg dry
5
0.15
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
1-Methylnaphthalene [90-12-0]^
ND
mg/kg dry
5
0.19
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2,4,5-Trichlorophenol[95-95-4]^
ND
mg/kg dry
5
0.19
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2,4,6-Trichlorophenol[88-06-2]^
ND
mg/kg dry
5
0.19
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2,4-Dichlorophenol[120-83-2]^
ND
mg/kg dry
5
0.17
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2,4-Dimethylphenol [105-67-9]^
ND
mg/kg dry
5
0.30
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2,4-Dinitrophenol[51-28-5]^
ND
mg/kg dry
5
0.30
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2,4-Dinitrotoluene [121-14-2]^
ND
mg/kg dry
5
0.19
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2,6-Dinitrotoluene [606-20-2]^
ND
mg/kg dry
5
0.22
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2-Chloronaphthalene [91-58-7]^
ND
mg/kg dry
5
0.19
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2-Chlorophenol [95-57-8]^
ND
mg/kg dry
5
0.17
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
ND
mg/kg dry
5
0.23
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2-Methylnaphthalene [91-57-6]^
ND
mg/kg dry
5
0.19
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2-Methylphenol [95-48-7]^
ND
mg/kg dry
5
0.17
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
2-Nitroaniline [88-74-4]^
ND
mg/kg dry
5
0.21
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 15 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: ACC-1 SED Lab Sample ID:CC16129-03 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 11:00 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 71.92
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
I'Q
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
ND
mg/kg
dry
5
0.22
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
ND
mg/kg
dry
5
0.18
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
3,3'-Dichlorobenzidine [91-94-1]^
ND
mg/kg
dry
5
0.68
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
3-Nitroaniline [99-09-2]^
ND
mg/kg
dry
5
0.25
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
4-Bromophenyl-phenylether [101-55-3]^
ND
mg/kg
dry
5
0.19
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
4-Chloro-3-methylphenol[59-50-7]^
ND
mg/kg
dry
5
0.23
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
4-Chloroaniline [106-47-8]^
ND
mg/kg
dry
5
0.65
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
4-Chlorophenyl-phenylether [7005-72-3]^
ND
mg/kg
dry
5
0.18
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
4-Nitroaniline [100-01-6]^
ND
mg/kg
dry
5
0.37
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
4-Nitrophenol [100-02-7]^
ND
mg/kg
dry
5
0.22
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Acenaphthene [83-32-9]^
ND
mg/kg
dry
5
0.19
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Acenaphthylene [208-96-8]^
ND
mg/kg
dry
5
0.19
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Anthracene [120-12-7]^
ND
mg/kg
dry
5
0.26
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Benzidine [92-87-5]^
ND
mg/kg
dry
5
0.76
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Senzo(a)anthracene [56-55-3]^
0.40
JD
mg/kg
dry
5
0.19
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Senzo(a)pyrene [50-32-8]^
0.33
JD
mg/kg
dry
5
0.23
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Senzo(b)fluoranthene [205-99-2]^
0.53
JD
mg/kg
dry
5
0.13
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Benzo(g,h,i)perylene [191-24-2]^
ND
mg/kg
dry
5
0.33
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Benzo(k)fluoranthene [207-08-9]^
ND
mg/kg
dry
5
0.23
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Benzoic acid [65-85-0]^
ND
mg/kg
dry
5
1.0
12
9I23028
EPA
8270E
09/25/19
14:41
DFM
Benzyl alcohol [100-51-6]^
ND
mg/kg
dry
5
0.16
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
ND
mg/kg
dry
5
0.17
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Bis(2-chloroethyl)ether [111-44-4]^
ND
mg/kg
dry
5
0.30
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Bis(2-chloroisopropyl)ether [108-60-1]^
ND
mg/kg
dry
5
0.17
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM QV-01
Bis(2-ethylhexyl)phthalate [117-81-7]^
ND
mg/kg
dry
5
0.24
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Butylbenzylphthalate [85-68-7]^
ND
mg/kg
dry
5
0.28
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Chrysene [218-01-9]^
0.38
JD
mg/kg
dry
5
0.21
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Dibenzo(a,h)anthracene [53-70-3]^
ND
mg/kg
dry
5
0.35
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM QV-01
Dibenzofuran [132-64-9]^
ND
mg/kg
dry
5
0.19
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Diethylphthalate [84-66-2]^
ND
mg/kg
dry
5
0.19
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Dimethylphthalate [131-11-3]^
ND
mg/kg
dry
5
0.23
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Di-n-butylphthalate [84-74-2]^
0.46
JD
mg/kg
dry
5
0.29
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Di-n-octylphthalate [117-84-0]^
ND
mg/kg
dry
5
0.23
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Fluoranthene [206-44-0]^
0.91
JD
mg/kg
dry
5
0.25
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Fluorene [86-73-7]^
ND
mg/kg
dry
5
0.20
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Hexachlorobenzene [118-74-1]^
ND
mg/kg
dry
5
0.18
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Hexachlorobutadiene [87-68-3]^
ND
mg/kg
dry
5
0.18
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Hexachlorocyclopentadiene [77-47-4]^
ND
mg/kg
dry
5
0.27
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Hexachloroethane [67-72-1]^
ND
mg/kg
dry
5
0.15
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
ND
mg/kg
dry
5
0.33
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM QV-01
Isophorone [78-59-1]^
ND
mg/kg
dry
5
0.21
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Naphthalene [91-20-3]^
ND
mg/kg
dry
5
0.19
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
Nitrobenzene [98-95-3]^
ND
mg/kg
dry
5
0.18
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
N-Nitrosodimethylamine [62-75-9]^
ND
mg/kg
dry
5
0.15
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
ND
mg/kg
dry
5
0.56
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
N-nitrosodiphenylamine/Diphenylamine
ND
mg/kg
dry
5
0.38
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
ND
mg/kg
dry
5
0.23
2.3
9I23028
EPA
8270E
09/25/19
14:41
DFM
FINAL
This report relates only to the sample as
received
by the
laboratory,
and may only
be reproduced in full.
I Page 16 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-1 SED Lab Sample ID:CC16129-03 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 11:00 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 71.92
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Phenanthrene [85-01-8]A 0.60 ]D
mg/kg dry
5
0.19
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
Phenol[108-95-2]A ND
mg/kg dry
5
0.15
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
Pyrene [129-00-0]A 0.72 ]D
mg/kg dry
5
0.26
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
Pyridine [110-86-1]A ND
mg/kg dry
5
0.57
2.3
9I23028
EPA 8270E
09/25/19 14:41
DFM
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
1y Notes
2,4,6-Tribromophenol
4.0
5
4.63
86 %
26-130
9123026
EPA 8270E
0912511914:41
DFM
2-Fluorobiphenyl
2.0
5
2.32
87 %
56-120
9123026
EPA 8270E
0912511914:41
DFM
2-Fluorophenol
3.9
5
4.63
84 %
49-126
9123026
EPA 8270E
09125119 14:41
DFM
Nitrobenzene-d5
2.0
5
2.32
88 %
50-117
9123026
EPA 8270E
09/25/1914:41
DFM
Phenol-d5
3.9
5
4.63
85 %
56-120
9123026
EPA 8270E
0912511914:41
DFM
Terphenyl-d14
2.1
5
2.32
90 %
36-151
9123026
EPA 8270E
0912511914:41
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 Of 65

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 UP SW Lab Sample ID:CC16129-04 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 11:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,1,1-Trichloroethane [71-55-6]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,1,2-Trichloroethane [79-00-5]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,1-Dichloroethane [75-34-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,1-Dichloroethene [75-35-4]^
1.1
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,1-Dichloropropene [563-58-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
ug/L
1
0.012
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,2,3-Trichloropropane [96-18-4]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,2-Dibromoethane [106-93-4]^
ND
ug/L
1
0.66
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,2-Dichloroethane [107-06-2]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,2-Dichloropropane [78-87-5]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
ug/L
1
0.30
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,3-Dichloropropane [142-28-9]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
2,2-Dichloropropane [594-20-7]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
2-Butanone [78-93-3]^
ND
ug/L
1
1.3
5.0
9I26038
EPA 8260D
09/27/19
08:56
REF
2-Chloroethyl Vinyl Ether[110-75-8]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
08:56
REF
2-Chlorotoluene [95-49-8]^
ND
ug/L
1
0.081
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
2-Hexanone [591-78-6]^
ND
ug/L
1
0.88
5.0
9I26038
EPA 8260D
09/27/19
08:56
REF
4-Chlorotoluene [106-43-4]^
ND
ug/L
1
0.068
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
4-Isopropyltoluene [99-87-6]^
ND
ug/L
1
0.085
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
4-Methyl-2-pentanone [108-10-1]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Acetone [67-64-1]^
ND
ug/L
1
10
20
9I26038
EPA 8260D
09/27/19
08:56
REF
Benzene[71-43-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Bromobenzene [108-86-1]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Bromochloromethane [74-97-5]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Bromodichloromethane [75-27-4]^
0.87 1
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Bromoform [75-25-2]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Bromomethane [74-83-9]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Carbon disulfide [75-15-0]^
ND
ug/L
1
1.5
5.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Carbon tetrachloride [56-23-5]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Chlorobenzene [108-90-7]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Chloroethane [75-00-3]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Chloroform [67-66-3]^
2.9
ug/L
1
0.18
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Chloromethane [74-87-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Dibromochloromethane [124-48-1]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Dibromomethane [74-95-3]^
ND
ug/L
1
0.27
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Dichlorodifluoromethane [75-71-8]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Ethylbenzene [100-41-4]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 18 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 UP SW Lab Sample ID:CC16129-04 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 11:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flao
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Isopropyl Ether[108-20-3]^
ND
ug/L
1
0.36
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Isopropylbenzene [98-82-8]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
m,p-Xylenes [108-38-3/106-42-3]^
ND
ug/L
1
0.17
2.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Methylene chloride [75-09-2]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Methyl-tert-Butyl Ether [1634-04-4]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Naphthalene [91-20-3]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
n-Butyl Benzene [104-51-8]^
ND
ug/L
1
0.058
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
n-Propyl Benzene [103-65-1]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
o-Xylene [95-47-6]^
ND
ug/L
1
0.065
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
sec-Butylbenzene [135-98-8]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Styrene [100-42-5]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
tert-Butyl benzene [98-06-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Tetrachloroethene [127-18-4]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Toluene [108-88-3]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Trichloroethene [79-01-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Trichlorofluoromethane [75-69-4]^
ND
ug/L
1
0.24
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Vinyl chloride [75-01-4]^
ND
ug/L
1
0.32
1.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Xylenes (Total) [1330-20-7]^
ND
ug/L
1
0.45
3.0
9I26038
EPA 8260D
09/27/19
08:56
REF
Surrogates
Results DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analvzed
" Notes
4-Bromofluorobenzene
44 1
50.0
87 %
53-136
9126038
EPA 8260D
09127119 08:56
REF
Dibromofluoromethane
45 1
50.0
89 %
67-129
9126038
EPA 8260D
09127119 08:56
REF
Toluene-d8
37 1
50.0
75 %
59-134
9126038
EPA 8260D
09127119 08:56
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flaa
Units
DF
MDL
Q
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
2.4
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
1-Methylnaphthalene [90-12-0]^
ND
ug/L
1
2.7
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2,4,5-Trichlorophenol[95-95-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2,4,6-Trichlorophenol[88-06-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2,4-Dichlorophenol [120-83-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2,4-Dimethylphenol [105-67-9]^
ND
ug/L
1
2.3
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2,4-Dinitrophenol [51-28-5]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2,4-Dinitrotoluene [121-14-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2,6-Dinitrotoluene [606-20-2]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2-Chloronaphthalene [91-58-7]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2-Chlorophenol[95-57-8]^
ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]^
ND
ug/L
1
3.3
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2-Methylnaphthalene [91-57-6]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2-Methylphenol[95-48-7]^
ND
ug/L
1
2.0
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
2-Nitroaniline [88-74-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
FINAL
This report relates only to the
sample as received by the laboratory,
and may only be reproduced in full.
I Page 19 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 UP SW Lab Sample ID:CC16129-04 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 11:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl
Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
ND
ug/L
1
1.1
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
ND
ug/L
1
2.1
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
3,3'-Dichlorobenzidine [91-94-1]^
ND
ug/L
1
3.5
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
3-Nitroaniline [99-09-2]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
4-Bromophenyl-phenylether[101-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
4-Chloro-3-methylphenol[59-50-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
4-Chloroaniline [106-47-8]^
ND
ug/L
1
2.0
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
4-Nitroaniline [100-01-6]^
ND
ug/L
1
3.2
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
4-Nitrophenol[100-02-7]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Acenaphthene [83-32-9]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Acenaphthylene[208-96-8]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Anthracene [120-12-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Benzidine [92-87-5]^
ND
ug/L
1
1.6
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Benzo(a)anthracene [56-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Benzo(a)pyrene [50-32-8]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Benzo(b)fluoranthene [205-99-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Benzo(g,h,i)perylene [191-24-2]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Benzo(k)fluoranthene [207-08-9]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Benzoic acid [65-85-0]^
ND
ug/L
1
1.0
50
9I20004
EPA
8270E
09/23/19
22:08
DFM
Benzylalcohol [100-51-6]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Bis(2-chloroethyl)ether[111-44-4]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:08
DFM QV-01
Bis(2-ethylhexyl)phthalate [117-81-7]^
ND
ug/L
1
1.9
5.0
9I20004
EPA
8270E
09/23/19
22:08
DFM
Butyl benzylphtha late [85-68-7]^
ND
ug/L
1
3.8
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Chrysene [218-01-9]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Dibenzo(a,h)anthracene [53-70-3]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Dibenzofuran [132-64-9]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Diethylphtha late [84-66-2]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Dimethylphthalate [131-11-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Di-n-butylphthalate [84-74-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Di-n-octylphthalate [117-84-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Fluoranthene [206-44-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Fluorene [86-73-7]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Hexachlorobenzene [118-74-1]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Hexachlorocyclopentadiene [77-47-4]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Hexachloroethane [67-72-1]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Isophorone [78-59-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Naphthalene[91-20-3]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
Nitrobenzene [98-95-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
N-Nitrosodimethylamine [62-75-9]^
ND
ug/L
1
1.9
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
N-nitrosodiphenylamine/Diphenylamine
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
ND
ug/L
1
2.1
10
9I20004
EPA
8270E
09/23/19
22:08
DFM
FINAL
This report relates only to the sample as received
by the
laboratory,
and may only
be reproduced in full.
I Page 20 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 UP SW Lab Sample ID:CC16129-04 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 11:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Phenanthrene[85-01-8]A ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
Phenol[108-95-2]A ND
ug/L
1
1.7
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
Pyrene [129-00-0]A ND
ug/L
1
3.5
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
Pyridine [110-86-1]A ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 22:08
DFM
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
2,4,6-Tribromophenol
84
1
100
84 %
10-179
9120004
EPA 8270E
09123119 22:08
DFM
2-Fluorobiphenyl
39
1
50.0
77 %
10-149
9120004
EPA 8270E
09123119 22:08
DFM
2-Fluorophenol
53
1
100
53 %
10-110
9120004
EPA 8270E
09123119 22:08
DFM
Nitrobenzene-d5
34
1
50.0
67 %
10-149
9120004
EPA 8270E
09123119 22:08
DFM
Phenol-d5
49
1
100
49 %
10-88
9120004
EPA 8270E
09123119 22:08
DFM
Terphenyl-d14
52
1
50.0
103 %
10-166
9120004
EPA 8270E
09123119 22:08
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 21 of 65

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 UP SED Lab Sample ID:CC16129-05 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 11:20 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 81.45
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
mg/kg
dry
0.762
0.00015
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,1,1-Trichloroethane [71-55-6]^
ND
mg/kg
dry
0.762
0.00023
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
mg/kg
dry
0.762
0.00019
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,1,2-Trichloroethane [79-00-5]^
ND
mg/kg
dry
0.762
0.00023
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,1-Dichloroethane [75-34-3]^
ND
mg/kg
dry
0.762
0.00023
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,1-Dichloroethene [75-35-4]^
ND
mg/kg
dry
0.762
0.00028
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,1-Dichloropropene [563-58-6]^
ND
mg/kg
dry
0.762
0.00015
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
mg/kg
dry
0.762
0.00026
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,2,3-Trichloropropane [96-18-4]^
ND
mg/kg
dry
0.762
0.00060
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
mg/kg
dry
0.762
0.00025
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
mg/kg
dry
0.762
0.00016
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
mg/kg
dry
0.762
0.00074
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,2-Dibromoethane [106-93-4]^
ND
mg/kg
dry
0.762
0.00043
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,2-Dichlorobenzene [95-50-1]^
ND
mg/kg
dry
0.762
0.00025
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,2-Dichloroethane [107-06-2]^
ND
mg/kg
dry
0.762
0.00038
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,2-Dichloropropane [78-87-5]^
ND
mg/kg
dry
0.762
0.00024
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
mg/kg
dry
0.762
0.00019
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,3-Dichlorobenzene [541-73-1]^
ND
mg/kg
dry
0.762
0.00021
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,3-Dichloropropane [142-28-9]^
ND
mg/kg
dry
0.762
0.00027
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
1,4-Dichlorobenzene [106-46-7]^
ND
mg/kg
dry
0.762
0.00019
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
2,2-Dichloropropane [594-20-7]^
ND
mg/kg
dry
0.762
0.00022
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
2-Butanone [78-93-3]^
ND
mg/kg
dry
0.762
0.00073
0.0047
9302035
EPA
8260D
10/02/19
19:52
REF
2-Chloroethyl Vinyl Ether [110-75-8]^
ND
mg/kg
dry
0.762
0.00015
0.0047
9302035
EPA
8260D
10/02/19
19:52
REF
2-Chlorotoluene [95-49-8]^
ND
mg/kg
dry
0.762
0.00017
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
2-Hexanone [591-78-6]^
ND
mg/kg
dry
0.762
0.00070
0.0047
9302035
EPA
8260D
10/02/19
19:52
REF
4-Chlorotoluene [106-43-4]^
ND
mg/kg
dry
0.762
0.00024
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
4-Isopropyltoluene [99-87-6]^
ND
mg/kg
dry
0.762
0.00015
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
4-Methyl-2-pentanone [108-10-1]^
ND
mg/kg
dry
0.762
0.00053
0.0047
9302035
EPA
8260D
10/02/19
19:52
REF
Acetone [67-64-1]^
ND
mg/kg
dry
0.762
0.013
0.019
9302035
EPA
8260D
10/02/19
19:52
REF
Benzene [71-43-2]^
ND
mg/kg
dry
0.762
0.00016
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Bromobenzene [108-86-1]^
ND
mg/kg
dry
0.762
0.00021
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Bromochloromethane [74-97-5]^
ND
mg/kg
dry
0.762
0.00038
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Bromodichloromethane [75-27-4]^
ND
mg/kg
dry
0.762
0.00022
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Bromoform [75-25-2]^
ND
mg/kg
dry
0.762
0.00042
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Bromomethane [74-83-9]^
ND
mg/kg
dry
0.762
0.00030
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Carbon disulfide [75-15-0]^
0.00054 J
mg/kg
dry
0.762
0.00036
0.0047
9102035
EPA
8260D
10/02/19
19:52
REF
Carbon Tetrachloride [56-23-5]^
ND
mg/kg
dry
0.762
0.00021
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Chlorobenzene [108-90-7]^
ND
mg/kg
dry
0.762
0.00016
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Chloroethane [75-00-3]^
ND
mg/kg
dry
0.762
0.00023
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF QV-01
Chloroform [67-66-3]^
ND
mg/kg
dry
0.762
0.00017
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Chloromethane [74-87-3]^
ND
mg/kg
dry
0.762
0.00020
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
mg/kg
dry
0.762
0.00022
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
mg/kg
dry
0.762
0.00016
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Dibromochloromethane [124-48-1]^
ND
mg/kg
dry
0.762
0.00033
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Dibromomethane [74-95-3]^
ND
mg/kg
dry
0.762
0.00031
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
Dichlorodifluoromethane [75-71-8]^
ND
mg/kg
dry
0.762
0.00042
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF QV-01
Ethylbenzene [100-41-4]^
ND
mg/kg
dry
0.762
0.00019
0.00094
9302035
EPA
8260D
10/02/19
19:52
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 Of 65

00�
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ANALYTICAL RESULTS
Description: AOC-2 UP SED Lab Sample ID:CC16129-05 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 11:20 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 81.45
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flag
Units
DF
MDL POL
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]^
ND
mg/kg dry
0.762
0.00033 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
Isopropyl Ether [108-20-3]^
ND
mg/kg dry
0.762
0.00017 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
Isopropylbenzene [98-82-8]^
ND
mg/kg dry
0.762
0.00014 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
m,p-Xylenes [108-38-3/106-42-3]^
ND
mg/kg dry
0.762
0.00035 0.0019
9302035
EPA 8260D
10/02/19 19:52
REF
Methylene Chloride [75-09-2]^
ND
mg/kg dry
0.762
0.00068 0.0019
9302035
EPA 8260D
10/02/19 19:52
REF
Methyl-tert-Butyl Ether [1634-04-4]^
ND
mg/kg dry
0.762
0.00028 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
Naphthalene [91-20-3]^
ND
mg/kg dry
0.762
0.00025 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
n-Butyl Benzene [104-51-8]^
ND
mg/kg dry
0.762
0.00012 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
n-Propyl Benzene [103-65-1]^
ND
mg/kg dry
0.762
0.00017 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
o-Xylene [95-47-6]^
ND
mg/kg dry
0.762
0.00021 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
sec-Butylbenzene [135-98-8]^
ND
mg/kg dry
0.762
0.00089 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
Styrene [100-42-5]^
ND
mg/kg dry
0.762
0.00092 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
tert-Butyl benzene [98-06-6]^
ND
mg/kg dry
0.762
0.00016 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
Tetrachloroethene [127-18-4]^
ND
mg/kg dry
0.762
0.00026 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
Toluene [108-88-3]^
ND
mg/kg dry
0.762
0.00022 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
mg/kg dry
0.762
0.00035 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
mg/kg dry
0.762
0.00036 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
Trichloroethene [79-01-6]^
ND
mg/kg dry
0.762
0.00030 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF
Trichlorofluoromethane [75-69-4]^
ND
mg/kg dry
0.762
0.00024 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF QV-01
Vinyl chloride [75-01-4]^
ND
mg/kg dry
0.762
0.00022 0.00094
9302035
EPA 8260D
10/02/19 19:52
REF QV-01
Xylenes (Total) [1330-20-7]^
ND
mg/kg dry
0.762
0.00052 0.0028
9302035
EPA 8260D
10/02/19 19:52
REF
surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
" Notes
4-Bromofluorobenzene
38
0.762
50.0
76 %
50-127
9JO2035
EPA 8260D
1010211919:52
REF
Dibromofluoromethane
42
0.762
50.0
84 %
52-128
9JO2035
EPA 8260D
10102119 19:52
REF
Toluene-d8
33
0.762
50.0
65 %
57-124
9JO2035
EPA 8260D
10102119 19:52
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
4
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
ND
mg/kg dry
5
0.16
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
1,2-Dichlorobenzene [95-50-1]^
ND
mg/kg dry
5
0.14
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
1,3-Dichlorobenzene [541-73-1]^
ND
mg/kg dry
5
0.12
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
1,4-Dichlorobenzene [106-46-7]^
ND
mg/kg dry
5
0.13
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
1-Methylnaphthalene [90-12-0]^
ND
mg/kg dry
5
0.17
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2,4,5-Trichlorophenol[95-95-4]^
ND
mg/kg dry
5
0.17
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2,4,6-Trichlorophenol[88-06-2]^
ND
mg/kg dry
5
0.17
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2,4-Dichlorophenol[120-83-2]^
ND
mg/kg dry
5
0.15
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2,4-Dimethylphenol[105-67-9]^
ND
mg/kg dry
5
0.26
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2,4-Dinitrophenol[51-28-5]^
ND
mg/kg dry
5
0.26
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2,4-Dinitrotoluene [121-14-2]^
ND
mg/kg dry
5
0.17
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2,6-Dinitrotoluene [606-20-2]^
ND
mg/kg dry
5
0.19
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2-Chloronaphthalene [91-58-7]^
ND
mg/kg dry
5
0.17
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2-Chlorophenol [95-57-8]^
ND
mg/kg dry
5
0.15
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
ND
mg/kg dry
5
0.20
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2-Methylnaphthalene [91-57-6]^
ND
mg/kg dry
5
0.17
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2-Methylphenol[95-48-7]^
ND
mg/kg dry
5
0.15
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
2-Nitroaniline [88-74-4]^
ND
mg/kg dry
5
0.18
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 23 Of 65

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www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 UP SED Lab Sample ID:CC16129-05 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 11:20 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 81.45
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
ND
mg/kg
dry
5
0.19
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
ND
mg/kg
dry
5
0.16
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
3,3'-Dichlorobenzidine [91-94-1]^
ND
mg/kg
dry
5
0.60
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
3-Nitroaniline [99-09-2]^
ND
mg/kg
dry
5
0.22
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
4-Bromophenyl-phenylether [101-55-3]^
ND
mg/kg
dry
5
0.17
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
4-Chloro-3-methylphenol[59-50-7]^
ND
mg/kg
dry
5
0.20
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
4-Chloroaniline [106-47-8]^
ND
mg/kg
dry
5
0.57
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
4-Chlorophenyl-phenylether [7005-72-3]^
ND
mg/kg
dry
5
0.16
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
4-Nitroaniline [100-01-6]^
ND
mg/kg
dry
5
0.33
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
4-Nitrophenol [100-02-7]^
ND
mg/kg
dry
5
0.19
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Acenaphthene [83-32-9]^
ND
mg/kg
dry
5
0.17
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Acenaphthylene [208-96-8]^
ND
mg/kg
dry
5
0.17
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Anthracene [120-12-7]^
ND
mg/kg
dry
5
0.23
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Benzidine [92-87-5]^
ND
mg/kg
dry
5
0.68
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Benzo(a)anthracene [56-55-3]^
0.33
JD
mg/kg
dry
5
0.17
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Benzo(a)pyrene [50-32-8]^
0.34
JD
mg/kg
dry
5
0.20
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Benzo(b)fluoranthene [205-99-2]^
0.47
JD
mg/kg
dry
5
0.11
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Benzo(g,h,i)perylene [191-24-2]^
0.36
JD
mg/kg
dry
5
0.29
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Benzo(k)fluoranthene [207-08-9]^
0.21
JD
mg/kg
dry
5
0.20
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Benzoic acid [65-85-0]^
ND
mg/kg
dry
5
0.92
10
9I23028
EPA
8270E
09/25/19
17:14
DFM
Benzyl alcohol [100-51-6]^
ND
mg/kg
dry
5
0.14
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
ND
mg/kg
dry
5
0.15
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Bis(2-chloroethyl)ether [111-44-4]^
ND
mg/kg
dry
5
0.26
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Bis(2-chloroisopropyl)ether [108-60-1]^
ND
mg/kg
dry
5
0.15
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM QV-01
Bis(2-ethylhexyl)phthalate [117-81-7]^
ND
mg/kg
dry
5
0.21
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Butylbenzylphthalate [85-68-7]^
ND
mg/kg
dry
5
0.25
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Chrysene [218-01-9]^
0.43
JD
mg/kg
dry
5
0.18
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Dibenzo(a,h)anthracene [53-70-3]^
ND
mg/kg
dry
5
0.31
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM QV-01
Dibenzofuran [132-64-9]^
ND
mg/kg
dry
5
0.17
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Diethylphthalate [84-66-2]^
ND
mg/kg
dry
5
0.17
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Dimethylphthalate [131-11-3]^
ND
mg/kg
dry
5
0.20
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Di-n-butylphthalate [84-74-2]^
ND
mg/kg
dry
5
0.25
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Di-n-octylphthalate [117-84-0]^
ND
mg/kg
dry
5
0.20
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Fluoranthene [206-44-0]^
0.78
JD
mg/kg
dry
5
0.22
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Fluorene [86-73-7]^
ND
mg/kg
dry
5
0.18
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Hexachlorobenzene [118-74-1]^
ND
mg/kg
dry
5
0.16
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Hexachlorobutadiene [87-68-3]^
ND
mg/kg
dry
5
0.16
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Hexachlorocyclopentadiene [77-47-4]^
ND
mg/kg
dry
5
0.24
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Hexachloroethane [67-72-1]^
ND
mg/kg
dry
5
0.13
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
0.30
JD
mg/kg
dry
5
0.29
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM QV-01
Isophorone [78-59-1]^
ND
mg/kg
dry
5
0.18
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Naphthalene [91-20-3]^
ND
mg/kg
dry
5
0.17
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
Nitrobenzene [98-95-3]^
ND
mg/kg
dry
5
0.16
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
N-Nitrosodimethylamine [62-75-9]^
ND
mg/kg
dry
5
0.13
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
ND
mg/kg
dry
5
0.50
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
N-nitrosodiphenylamine/Diphenylamine
ND
mg/kg
dry
5
0.33
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
ND
mg/kg
dry
5
0.20
2.0
9I23028
EPA
8270E
09/25/19
17:14
DFM
FINAL
This report relates only to the sample as
received
by the
laboratory,
and may only
be reproduced in full.
I Page 24 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 UP SED Lab Sample ID:CC16129-05 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 11:20 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 81.45
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Phenanthrene [85-01-8]A 0.47 ]D
mg/kg dry
5
0.17
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
Phenol[108-95-2]A ND
mg/kg dry
5
0.14
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
Pyrene [129-00-0]A 0.58 ]D
mg/kg dry
5
0.23
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
Pyridine [110-86-1]A ND
mg/kg dry
5
0.50
2.0
9I23028
EPA 8270E
09/25/19 17:14
DFM
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
1y Notes
2,4,6-Tribromophenol
2.9
5
4.09
70 %
26-130
9123026
EPA 8270E
0912511917:14
DFM
2-Fluorobiphenyl
1.4
5
2.05
70 %
56-120
9123026
EPA 8270E
0912511917:14
DFM
2-Fluorophenol
2.3
5
4.09
56 %
49-126
9123026
EPA 8270E
09125119 17:14
DFM
Nitrobenzene-d5
1.3
5
2.05
64 %
50-117
9123026
EPA 8270E
09/25/1917:14
DFM
Phenol-d5
2.6
5
4.09
68 %
56-120
9123026
EPA 8270E
09/25/1917:14
DFM
Terphenyl-d14
1.4
5
2.05
67 %
36-151
9123026
EPA 8270E
0912511917:14
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 25 Of 65

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 DOWN SW Lab Sample ID:CC16129-06 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 11:50 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,1,1-Trichloroethane [71-55-6]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,1,2-Trichloroethane [79-00-5]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,1-Dichloroethane [75-34-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,1-Dichloroethene [75-35-4]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,1-Dichloropropene [563-58-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
ug/L
1
0.012
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,2,3-Trichloropropane [96-18-4]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,2-Dibromoethane [106-93-4]^
ND
ug/L
1
0.66
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,2-Dichloroethane [107-06-2]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,2-Dichloropropane [78-87-5]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
ug/L
1
0.30
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,3-Dichloropropane [142-28-9]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
2,2-Dichloropropane [594-20-7]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
2-Butanone [78-93-3]^
ND
ug/L
1
1.3
5.0
9I26038
EPA 8260D
09/27/19
09:27
REF
2-Chloroethyl Vinyl Ether[110-75-8]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
09:27
REF
2-Chlorotoluene [95-49-8]^
ND
ug/L
1
0.081
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
2-Hexanone [591-78-6]^
ND
ug/L
1
0.88
5.0
9I26038
EPA 8260D
09/27/19
09:27
REF
4-Chlorotoluene [106-43-4]^
ND
ug/L
1
0.068
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
4-Isopropyltoluene [99-87-6]^
ND
ug/L
1
0.085
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
4-Methyl-2-pentanone [108-10-1]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Acetone [67-64-1]^
ND
ug/L
1
10
20
9I26038
EPA 8260D
09/27/19
09:27
REF
Benzene[71-43-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Bromobenzene [108-86-1]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Bromochloromethane [74-97-5]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Bromodichloromethane [75-27-4]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Bromoform [75-25-2]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Bromomethane [74-83-9]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Carbon disulfide [75-15-0]^
ND
ug/L
1
1.5
5.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Carbon tetrachloride [56-23-5]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Chlorobenzene [108-90-7]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Chloroethane [75-00-3]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Chloroform [67-66-3]^
ND
ug/L
1
0.18
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Chloromethane [74-87-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Dibromochloromethane [124-48-1]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Dibromomethane [74-95-3]^
ND
ug/L
1
0.27
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Dichlorodifluoromethane [75-71-8]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Ethylbenzene [100-41-4]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 26 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 DOWN SW Lab Sample ID:CC16129-06 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 11:50 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flao
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Isopropyl Ether[108-20-3]^
ND
ug/L
1
0.36
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Isopropylbenzene [98-82-8]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
m,p-Xylenes [108-38-3/106-42-3]^
ND
ug/L
1
0.17
2.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Methylene chloride [75-09-2]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Methyl-tert-Butyl Ether [1634-04-4]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Naphthalene [91-20-3]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
n-Butyl Benzene [104-51-8]^
ND
ug/L
1
0.058
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
n-Propyl Benzene [103-65-1]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
o-Xylene [95-47-6]^
ND
ug/L
1
0.065
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
sec-Butylbenzene [135-98-8]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Styrene [100-42-5]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
tert-Butyl benzene [98-06-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Tetrachloroethene [127-18-4]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Toluene [108-88-3]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Trichloroethene [79-01-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Trichlorofluoromethane [75-69-4]^
ND
ug/L
1
0.24
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Vinyl chloride [75-01-4]^
ND
ug/L
1
0.32
1.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Xylenes (Total) [1330-20-7]^
ND
ug/L
1
0.45
3.0
9I26038
EPA 8260D
09/27/19
09:27
REF
Surrogates
Results DF
Spike L v/
% Reg
% Rec Limits
Batch
Method
Analvzed
" Notes
4-Bromofluorobenzene
44 1
50.0
88 %
53-136
9126038
EPA 8260D
09127119 09:27
REF
Dibromofluoromethane
46 1
50.0
92 %
67-129
9126038
EPA 8260D
09127119 09:27
REF
Toluene-d8
37 1
50.0
74 %
59-134
9126038
EPA 8260D
09127119 09:27
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flaa
Units
DF
MDL
Q
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
2.4
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
1-Methylnaphthalene [90-12-0]^
ND
ug/L
1
2.7
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2,4,5-Trichlorophenol[95-95-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2,4,6-Trichlorophenol[88-06-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2,4-Dichlorophenol [120-83-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2,4-Dimethylphenol [105-67-9]^
ND
ug/L
1
2.3
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2,4-Dinitrophenol [51-28-5]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2,4-Dinitrotoluene [121-14-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2,6-Dinitrotoluene [606-20-2]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2-Chloronaphthalene [91-58-7]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2-Chlorophenol[95-57-8]^
ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]^
ND
ug/L
1
3.3
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2-Methylnaphthalene [91-57-6]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2-Methylphenol[95-48-7]^
ND
ug/L
1
2.0
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
2-Nitroaniline [88-74-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
FINAL
This report relates only to the
sample as received by the laboratory,
and may only be reproduced in full.
I Page 27 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 DOWN SW Lab Sample ID:CC16129-06 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 11:50 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
ND
ug/L
1
1.1
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
ND
ug/L
1
2.1
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
3,3'-Dichlorobenzidine [91-94-1]^
ND
ug/L
1
3.5
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
3-Nitroaniline [99-09-2]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
4-Bromophenyl-phenylether[101-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
4-Chloro-3-methylphenol[59-50-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
4-Chloroaniline [106-47-8]^
ND
ug/L
1
2.0
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
4-Nitroaniline [100-01-6]^
ND
ug/L
1
3.2
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
4-Nitrophenol[100-02-7]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Acenaphthene [83-32-9]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Acenaphthylene[208-96-8]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Anthracene [120-12-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Benzidine [92-87-5]^
ND
ug/L
1
1.6
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Benzo(a)anthracene [56-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Benzo(a)pyrene [50-32-8]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Benzo(b)fluoranthene [205-99-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Benzo(g,h,i)perylene [191-24-2]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Benzo(k)fluoranthene [207-08-9]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Benzoic acid [65-85-0]^
ND
ug/L
1
1.0
50
9I20004
EPA
8270E
09/23/19
22:38
DFM
Benzylalcohol [100-51-6]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Bis(2-chloroethyl)ether[111-44-4]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:38
DFM QV-01
Bis(2-ethylhexyl)phthalate [117-81-7]^
ND
ug/L
1
1.9
5.0
9I20004
EPA
8270E
09/23/19
22:38
DFM
Butyl benzylphtha late [85-68-7]^
ND
ug/L
1
3.8
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Chrysene [218-01-9]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Dibenzo(a,h)anthracene [53-70-3]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Dibenzofuran [132-64-9]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Diethylphtha late [84-66-2]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Dimethylphthalate [131-11-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Di-n-butylphthalate [84-74-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Di-n-octylphthalate [117-84-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Fluoranthene [206-44-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Fluorene [86-73-7]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Hexachlorobenzene [118-74-1]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Hexachlorocyclopentadiene [77-47-4]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Hexachloroethane [67-72-1]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Isophorone [78-59-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
Naphthalene [91-20-3]^
3.6 J
ug/L
1
2.8
10
9120004
EPA
8270E
09/23/19
22:38
DFM
Nitrobenzene [98-95-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
N-Nitrosodimethylamine [62-75-9]^
ND
ug/L
1
1.9
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
N-nitrosodiphenylamine/Diphenylamine
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
22:38
DFM
[86-30-6/122-39-4]^
Pentachlorophenol[87-86-S]^
6.9 J
ug/L
1
2.1
10
9120004
EPA
8270E
09/23/19
22:38
DFM
FINAL
This report relates only to the sample as received
by the
laboratory,
and may only
be reproduced in full.
I Page 28 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 DOWN SW Lab Sample ID:CC16129-06 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 11:50 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Phenanthrene[85-01-8]A ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
Phenol[108-95-2]A ND
ug/L
1
1.7
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
Pyrene [129-00-0]A ND
ug/L
1
3.5
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
Pyridine [110-86-1]A ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 22:38
DFM
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
2,4,6-Tribromophenol
90
1
100
90 %
10-179
9120004
EPA 8270E
0912311922:38
DFM
2-Fluorobiphenyl
45
1
50.0
90 %
10-149
9120004
EPA 8270E
09123119 22:38
DFM
2-Fluorophenol
53
1
100
53 %
10-110
9120004
EPA 8270E
09123119 22:38
DFM
Nitrobenzene-d5
40
1
50.0
80 %
10-149
9120004
EPA 8270E
09123119 22:38
DFM
Phenol-d5
40
1
100
40 %
10-88
9120004
EPA 8270E
09123119 22:38
DFM
Terphenyl-d14
51
1
50.0
102 %
10-166
9120004
EPA 8270E
09123119 22:38
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 29 Of 65

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 DOWN SED Lab Sample ID:CC16129-07 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 12:00 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 77.62
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
mg/kg
dry
1
0.00019
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,1,1-Trichloroethane [71-55-6]^
ND
mg/kg
dry
1
0.00029
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
mg/kg
dry
1
0.00023
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,1,2-Trichloroethane [79-00-5]^
ND
mg/kg
dry
1
0.00029
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,1-Dichloroethane [75-34-3]^
ND
mg/kg
dry
1
0.00029
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,1-Dichloroethene [75-35-4]^
ND
mg/kg
dry
1
0.00035
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,1-Dichloropropene [563-58-6]^
ND
mg/kg
dry
1
0.00019
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
mg/kg
dry
1
0.00033
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,2,3-Trichloropropane [96-18-4]^
ND
mg/kg
dry
1
0.00075
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
mg/kg
dry
1
0.00032
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
mg/kg
dry
1
0.00020
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
mg/kg
dry
1
0.00092
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,2-Dibromoethane [106-93-4]^
ND
mg/kg
dry
1
0.00054
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,2-Dichlorobenzene [95-50-1]^
ND
mg/kg
dry
1
0.00032
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,2-Dichloroethane [107-06-2]^
ND
mg/kg
dry
1
0.00048
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,2-Dichloropropane [78-87-5]^
ND
mg/kg
dry
1
0.00030
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
mg/kg
dry
1
0.00023
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,3-Dichlorobenzene [541-73-1]^
ND
mg/kg
dry
1
0.00026
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,3-Dichloropropane [142-28-9]^
ND
mg/kg
dry
1
0.00034
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
1,4-Dichlorobenzene [106-46-7]^
ND
mg/kg
dry
1
0.00023
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
2,2-Dichloropropane [594-20-7]^
ND
mg/kg
dry
1
0.00027
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
2-Butanone [78-93-3]^
0.0038 J
mg/kg
dry
1
0.00091
0.0058
9102035
EPA
8260D
10/02/19
20:23
REF
2-Chloroethyl Vinyl Ether [110-75-8]^
ND
mg/kg
dry
1
0.00019
0.0058
9302035
EPA
8260D
10/02/19
20:23
REF
2-Chlorotoluene [95-49-8]^
ND
mg/kg
dry
1
0.00021
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
2-Hexanone [591-78-6]^
ND
mg/kg
dry
1
0.00088
0.0058
9302035
EPA
8260D
10/02/19
20:23
REF
4-Chlorotoluene [106-43-4]^
ND
mg/kg
dry
1
0.00030
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
4-Isopropyltoluene [99-87-6]^
ND
mg/kg
dry
1
0.00019
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
4-Methyl-2-pentanone [108-10-1]^
ND
mg/kg
dry
1
0.00067
0.0058
9302035
EPA
8260D
10/02/19
20:23
REF
Acetone [67-64-1]^
0.036
mg/kg
dry
1
0.016
0.023
9102035
EPA
8260D
10/02/19
20:23
REF
Benzene [71-43-2]^
ND
mg/kg
dry
1
0.00020
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Bromobenzene [108-86-1]^
ND
mg/kg
dry
1
0.00026
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Bromochloromethane [74-97-5]^
ND
mg/kg
dry
1
0.00048
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Bromodichloromethane [75-27-4]^
ND
mg/kg
dry
1
0.00028
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Bromoform [75-25-2]^
ND
mg/kg
dry
1
0.00053
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Bromomethane [74-83-9]^
ND
mg/kg
dry
1
0.00037
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Carbon disulfide [75-15-0]^
0.00060 J
mg/kg
dry
1
0.00046
0.0058
9102035
EPA
8260D
10/02/19
20:23
REF
Carbon Tetrachloride [56-23-5]^
ND
mg/kg
dry
1
0.00026
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Chlorobenzene [108-90-7]^
ND
mg/kg
dry
1
0.00020
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Chloroethane [75-00-3]^
ND
mg/kg
dry
1
0.00029
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF QV-01
Chloroform [67-66-3]^
ND
mg/kg
dry
1
0.00021
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Chloromethane [74-87-3]^
ND
mg/kg
dry
1
0.00025
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
mg/kg
dry
1
0.00027
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
mg/kg
dry
1
0.00020
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Dibromochloromethane [124-48-1]^
ND
mg/kg
dry
1
0.00041
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Dibromomethane [74-95-3]^
ND
mg/kg
dry
1
0.00039
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
Dichlorodifluoromethane [75-71-8]^
ND
mg/kg
dry
1
0.00053
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF QV-01
Ethylbenzene [100-41-4]^
ND
mg/kg
dry
1
0.00023
0.0012
9302035
EPA
8260D
10/02/19
20:23
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 30 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 DOWN SED Lab Sample ID:CC16129-07 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 12:00 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 77.62
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]^
ND
mg/kg
dry
1
0.00041
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
Isopropyl Ether [108-20-3]^
ND
mg/kg
dry
1
0.00021
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
Isopropylbenzene [98-82-8]^
ND
mg/kg
dry
1
0.00018
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
m,p-Xylenes [108-38-3/106-42-3]^
ND
mg/kg
dry
1
0.00043
0.0023
9302035
EPA 8260D
10/02/19
20:23
REF
Methylene Chloride [75-09-2]^
ND
mg/kg
dry
1
0.00085
0.0023
9302035
EPA 8260D
10/02/19
20:23
REF
Methyl-tert-Butyl Ether [1634-04-4]^
ND
mg/kg
dry
1
0.00035
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
Naphthalene [91-20-3]^
ND
mg/kg
dry
1
0.00032
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
n-Butyl Benzene [104-51-8]^
ND
mg/kg
dry
1
0.00015
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
n-Propyl Benzene [103-65-1]^
ND
mg/kg
dry
1
0.00021
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
o-Xylene [95-47-6]^
ND
mg/kg
dry
1
0.00026
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
sec-Butylbenzene [135-98-8]^
ND
mg/kg
dry
1
0.0011
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
Styrene [100-42-5]^
ND
mg/kg
dry
1
0.0011
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
tert-Butyl benzene [98-06-6]^
ND
mg/kg
dry
1
0.00020
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
Tetrachloroethene [127-18-4]^
ND
mg/kg
dry
1
0.00033
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
Toluene [108-88-3]^
ND
mg/kg
dry
1
0.00028
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
mg/kg
dry
1
0.00043
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
mg/kg
dry
1
0.00046
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
Trichloroethene [79-01-6]^
ND
mg/kg
dry
1
0.00037
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF
Trichlorofluoromethane [75-69-4]^
ND
mg/kg
dry
1
0.00030
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF QV-01
Vinyl chloride [75-01-4]^
ND
mg/kg
dry
1
0.00028
0.0012
9302035
EPA 8260D
10/02/19
20:23
REF QV-01
Xylenes (Total) [1330-20-7]^
ND
mg/kg
dry
1
0.00065
0.0035
9302035
EPA 8260D
10/02/19
20:23
REF
surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Anaivzed
" Notes
4-Bromofluorobenzene
38
1
50.0
76 %
50-127
9JO2035
EPA 8260D
10102119 20:23
REF
Dibromofluoromethane
41
1
50.0
82 %
52-128
9JO2035
EPA 8260D
10102119 20:23
REF
Toluene-d8
33
1
50.0
65 %
57-124
9JO2035
EPA 8260D
10102119 20:23
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
4
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
ND
mg/kg dry
5
0.17
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
1,2-Dichlorobenzene [95-50-1]^
ND
mg/kg dry
5
0.15
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
1,3-Dichlorobenzene [541-73-1]^
ND
mg/kg dry
5
0.13
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
1,4-Dichlorobenzene [106-46-7]^
ND
mg/kg dry
5
0.14
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
1-Methylnaphthalene [90-12-0]^
ND
mg/kg dry
5
0.17
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2,4,5-Trichlorophenol[95-95-4]^
ND
mg/kg dry
5
0.17
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2,4,6-Trichlorophenol[88-06-2]^
ND
mg/kg dry
5
0.17
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2,4-Dichlorophenol[120-83-2]^
ND
mg/kg dry
5
0.15
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2,4-Dimethylphenol [105-67-9]^
ND
mg/kg dry
5
0.28
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2,4-Dinitrophenol[51-28-5]^
ND
mg/kg dry
5
0.28
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2,4-Dinitrotoluene [121-14-2]^
ND
mg/kg dry
5
0.18
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2,6-Dinitrotoluene [606-20-2]^
ND
mg/kg dry
5
0.20
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2-Chloronaphthalene [91-58-7]^
ND
mg/kg dry
5
0.18
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2-Chlorophenol [95-57-8]^
ND
mg/kg dry
5
0.16
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
ND
mg/kg dry
5
0.21
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2-Methylnaphthalene [91-57-6]^
ND
mg/kg dry
5
0.18
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2-Methylphenol[95-48-7]^
ND
mg/kg dry
5
0.16
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
2-Nitroaniline [88-74-4]^
ND
mg/kg dry
5
0.19
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 31 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 DOWN SED Lab Sample ID:CC16129-07 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 12:00 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 77.62
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
ND
mg/kg
dry
5
0.20
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
ND
mg/kg
dry
5
0.17
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
3,3'-Dichlorobenzidine [91-94-1]^
ND
mg/kg
dry
5
0.63
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
3-Nitroaniline [99-09-2]^
ND
mg/kg
dry
5
0.23
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
4-Bromophenyl-phenylether [101-55-3]^
ND
mg/kg
dry
5
0.17
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
4-Chloro-3-methylphenol[59-50-7]^
ND
mg/kg
dry
5
0.21
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
4-Chloroaniline [106-47-8]^
ND
mg/kg
dry
5
0.60
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
4-Chlorophenyl-phenylether [7005-72-3]^
ND
mg/kg
dry
5
0.17
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
4-Nitroaniline [100-01-6]^
ND
mg/kg
dry
5
0.34
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
4-Nitrophenol [100-02-7]^
ND
mg/kg
dry
5
0.20
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Acenaphthene [83-32-9]^
ND
mg/kg
dry
5
0.18
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Acenaphthylene [208-96-8]^
ND
mg/kg
dry
5
0.18
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Anthracene [120-12-7]^
ND
mg/kg
dry
5
0.24
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Benzidine [92-87-5]^
ND
mg/kg
dry
5
0.71
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Benzo(a)anthracene [56-55-3]^
ND
mg/kg
dry
5
0.18
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Benzo(a)pyrene [50-32-8]^
ND
mg/kg
dry
5
0.21
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Benzo(b)fluoranthene [205-99-2]^
ND
mg/kg
dry
5
0.12
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Benzo(g,h,i)perylene [191-24-2]^
ND
mg/kg
dry
5
0.30
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Benzo(k)fluoranthene [207-08-9]^
ND
mg/kg
dry
5
0.21
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Benzoic acid [65-85-0]^
ND
mg/kg
dry
5
0.97
11
9I23028
EPA
8270E
09/25/19
15:11
DFM
Benzyl alcohol [100-51-6]^
ND
mg/kg
dry
5
0.15
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
ND
mg/kg
dry
5
0.16
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Bis(2-chloroethyl)ether [111-44-4]^
ND
mg/kg
dry
5
0.28
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Bis(2-chloroisopropyl)ether [108-60-1]^
ND
mg/kg
dry
5
0.15
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM QV-01
Bis(2-ethylhexyl)phthalate [117-81-7]^
ND
mg/kg
dry
5
0.23
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Butylbenzylphthalate [85-68-7]^
ND
mg/kg
dry
5
0.26
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Chrysene [218-01-9]^
ND
mg/kg
dry
5
0.19
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Dibenzo(a,h)anthracene [53-70-3]^
ND
mg/kg
dry
5
0.33
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM QV-01
Dibenzofuran [132-64-9]^
ND
mg/kg
dry
5
0.17
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Diethylphthalate [84-66-2]^
ND
mg/kg
dry
5
0.18
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Dimethylphthalate [131-11-3]^
ND
mg/kg
dry
5
0.21
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Di-n-butylphthalate [84-74-2]^
ND
mg/kg
dry
5
0.26
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Di-n-octylphthalate [117-84-0]^
ND
mg/kg
dry
5
0.21
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Fluoranthene [206-44-0]^
0.28 ID
mg/kg
dry
5
0.23
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Fluorene [86-73-7]^
ND
mg/kg
dry
5
0.19
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Hexachlorobenzene [118-74-1]^
ND
mg/kg
dry
5
0.17
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Hexachlorobutadiene [87-68-3]^
ND
mg/kg
dry
5
0.17
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Hexachlorocyclopentadiene [77-47-4]^
ND
mg/kg
dry
5
0.25
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Hexachloroethane [67-72-1]^
ND
mg/kg
dry
5
0.14
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
ND
mg/kg
dry
5
0.30
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM QV-01
Isophorone [78-59-1]^
ND
mg/kg
dry
5
0.19
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Naphthalene [91-20-3]^
ND
mg/kg
dry
5
0.18
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
Nitrobenzene [98-95-3]^
ND
mg/kg
dry
5
0.17
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
N-Nitrosodimethylamine [62-75-9]^
ND
mg/kg
dry
5
0.14
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
ND
mg/kg
dry
5
0.52
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
N-nitrosodiphenylamine/Diphenylamine
ND
mg/kg
dry
5
0.35
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
ND
mg/kg
dry
5
0.21
2.1
9I23028
EPA
8270E
09/25/19
15:11
DFM
FINAL
This report relates only to the sample as
received
by the
laboratory,
and may only
be reproduced in full.
I Page 32 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-2 DOWN SED Lab Sample ID:CC16129-07 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 12:00 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 77.62
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Phenanthrene [85-01-8]A ND
mg/kg dry
5
0.17
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
Phenol[108-95-2]A ND
mg/kg dry
5
0.14
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
Pyrene [129-00-0]A ND
mg/kg dry
5
0.24
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
Pyridine [110-86-1]A ND
mg/kg dry
5
0.53
2.1
9I23028
EPA 8270E
09/25/19 15:11
DFM
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
3.1
5
4.29
71 %
26-130
9123026
EPA 8270E
0912511915:11
DFM
2-Fluorobiphenyl
1.7
5
2.15
78 %
56-120
9123026
EPA 8270E
0912511915:11
DFM
2-Fluorophenol
3.0
5
4.29
69 %
49-126
9123026
EPA 8270E
09125119 15:11
DFM
Nitrobenzene-d5
1.6
5
2.15
74 %
50-117
9123026
EPA 8270E
09/25/1915:11
DFM
Phenol-d5
3.3
5
4.29
76 %
56-120
9123026
EPA 8270E
09/25/1915:11
DFM
Terphenyl-d14
1.7
5
2.15
79 %
36-151
9123026
EPA 8270E
0912511915:11
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 33 Of 65

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-4 SW Lab Sample ID:CC16129-08 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 13:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,1,1-Trichloroethane [71-55-6]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,1,2-Trichloroethane [79-00-5]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,1-Dichloroethane [75-34-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,1-Dichloroethene [75-35-4]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,1-Dichloropropene [563-58-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
ug/L
1
0.012
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,2,3-Trichloropropane [96-18-4]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,2-Dibromoethane [106-93-4]^
ND
ug/L
1
0.66
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,2-Dichloroethane [107-06-2]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,2-Dichloropropane [78-87-5]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
ug/L
1
0.30
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,3-Dichloropropane [142-28-9]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
0.19
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
2,2-Dichloropropane [594-20-7]^
ND
ug/L
1
0.28
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
2-Butanone [78-93-3]^
4.0 J
ug/L
1
1.3
5.0
9I26038
EPA 8260D
09/27/19
09:58
REF
2-Chloroethyl Vinyl Ether[110-75-8]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
09:58
REF
2-Chlorotoluene [95-49-8]^
ND
ug/L
1
0.081
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
2-Hexanone [591-78-6]^
ND
ug/L
1
0.88
5.0
9I26038
EPA 8260D
09/27/19
09:58
REF
4-Chlorotoluene [106-43-4]^
ND
ug/L
1
0.068
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
4-Isopropyltoluene [99-87-6]^
ND
ug/L
1
0.085
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
4-Methyl-2-pentanone [108-10-1]^
ND
ug/L
1
1.1
5.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Acetone [67-64-1]^
21
ug/L
1
10
20
9I26038
EPA 8260D
09/27/19
09:58
REF
Benzene[71-43-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Bromobenzene [108-86-1]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Bromochloromethane [74-97-5]^
ND
ug/L
1
0.48
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Bromodichloromethane [75-27-4]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Bromoform [75-25-2]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Bromomethane [74-83-9]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Carbon disulfide [75-15-0]^
ND
ug/L
1
1.5
5.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Carbon tetrachloride [56-23-5]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Chlorobenzene [108-90-7]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Chloroethane [75-00-3]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Chloroform [67-66-3]^
ND
ug/L
1
0.18
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Chloromethane [74-87-3]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Dibromochloromethane [124-48-1]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Dibromomethane [74-95-3]^
ND
ug/L
1
0.27
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Dichlorodifluoromethane [75-71-8]^
ND
ug/L
1
0.20
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Ethylbenzene [100-41-4]^
ND
ug/L
1
0.13
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 34 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-4 SW Lab Sample ID:CC16129-08 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 13:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flao
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
0.22
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Isopropyl Ether[108-20-3]^
ND
ug/L
1
0.36
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Isopropylbenzene [98-82-8]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
m,p-Xylenes [108-38-3/106-42-3]^
ND
ug/L
1
0.17
2.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Methylene chloride [75-09-2]^
ND
ug/L
1
0.23
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Methyl-tert-Butyl Ether [1634-04-4]^
ND
ug/L
1
0.16
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Naphthalene [91-20-3]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
n-Butyl Benzene [104-51-8]^
ND
ug/L
1
0.058
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
n-Propyl Benzene [103-65-1]^
ND
ug/L
1
0.12
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
o-Xylene [95-47-6]^
ND
ug/L
1
0.065
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
sec-Butylbenzene [135-98-8]^
ND
ug/L
1
0.10
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Styrene [100-42-5]^
ND
ug/L
1
0.11
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
tert-Butyl benzene [98-06-6]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Tetrachloroethene [127-18-4]^
ND
ug/L
1
0.17
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Toluene [108-88-3]^
ND
ug/L
1
0.14
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
ug/L
1
0.21
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Trichloroethene [79-01-6]^
ND
ug/L
1
0.15
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Trichlorofluoromethane [75-69-4]^
ND
ug/L
1
0.24
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Vinyl chloride [75-01-4]^
ND
ug/L
1
0.32
1.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Xylenes (Total) [1330-20-7]^
ND
ug/L
1
0.45
3.0
9I26038
EPA 8260D
09/27/19
09:58
REF
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
" Notes
4-Bromofluorobenzene
43
1
50.0
86 %
53-136
9126038
EPA 8260D
09127119 09:58
REF
Dibromofluoromethane
45
1
50.0
90 %
67-129
9126038
EPA 8260D
09127119 09:58
REF
Toluene-d8
38
1
50.0
75 %
59-134
9126038
EPA 8260D
09127119 09:58
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
Q
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
2.4
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
1-Methylnaphthalene [90-12-0]^
ND
ug/L
1
2.7
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2,4,5-Trichlorophenol[95-95-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2,4,6-Trichlorophenol[88-06-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2,4-Dichlorophenol [120-83-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2,4-Dimethylphenol [105-67-9]^
ND
ug/L
1
2.3
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2,4-Dinitrophenol [51-28-5]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2,4-Dinitrotoluene [121-14-2]^
ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2,6-Dinitrotoluene [606-20-2]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2-Chloronaphthalene [91-58-7]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2-Chlorophenol[95-57-8]^
ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]^
ND
ug/L
1
3.3
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2-Methylnaphthalene [91-57-6]^
ND
ug/L
1
2.8
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2-Methylphenol[95-48-7]^
ND
ug/L
1
2.0
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
2-Nitroaniline [88-74-4]^
ND
ug/L
1
2.5
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 35 Of 65

(� �Eo
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ANALYTICAL RESULTS
Description: AOC-4 SW Lab Sample ID:CC16129-08 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 13:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl
Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
ND
ug/L
1
1.1
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
ND
ug/L
1
2.1
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
3,3'-Dichlorobenzidine [91-94-1]^
ND
ug/L
1
3.5
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
3-Nitroaniline [99-09-2]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
4-Bromophenyl-phenylether[101-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
4-Chloro-3-methylphenol[59-50-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
4-Chloroaniline [106-47-8]^
ND
ug/L
1
2.0
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
4-Chlorophenyl-phenylether[7005-72-3]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
4-Nitroaniline [100-01-6]^
ND
ug/L
1
3.2
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
4-Nitrophenol[100-02-7]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Acenaphthene [83-32-9]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Acenaphthylene[208-96-8]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Anthracene [120-12-7]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Benzidine [92-87-5]^
ND
ug/L
1
1.6
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Benzo(a)anthracene [56-55-3]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Benzo(a)pyrene [50-32-8]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Benzo(b)fluoranthene [205-99-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Benzo(g,h,i)perylene [191-24-2]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Benzo(k)fluoranthene [207-08-9]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Benzoic acid [65-85-0]^
ND
ug/L
1
1.0
50
9I20004
EPA
8270E
09/23/19
23:08
DFM
Benzylalcohol [100-51-6]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Bis(2-chloroethyl)ether[111-44-4]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
23:08
DFM QV-01
Bis(2-ethylhexyl)phthalate [117-81-7]^
ND
ug/L
1
1.9
5.0
9I20004
EPA
8270E
09/23/19
23:08
DFM
Butyl benzylphtha late [85-68-7]^
ND
ug/L
1
3.8
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Chrysene [218-01-9]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Dibenzo(a,h)anthracene [53-70-3]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Dibenzofuran [132-64-9]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Diethylphtha late [84-66-2]^
ND
ug/L
1
2.4
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Dimethylphthalate [131-11-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Di-n-butylphthalate [84-74-2]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Di-n-octylphthalate [117-84-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Fluoranthene [206-44-0]^
ND
ug/L
1
3.1
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Fluorene [86-73-7]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Hexachlorobenzene [118-74-1]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Hexachlorobutadiene [87-68-3]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Hexachlorocyclopentadiene [77-47-4]^
ND
ug/L
1
2.7
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Hexachloroethane [67-72-1]^
ND
ug/L
1
2.6
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
ND
ug/L
1
2.2
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Isophorone [78-59-1]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Naphthalene[91-20-3]^
ND
ug/L
1
2.8
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
Nitrobenzene [98-95-3]^
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
N-Nitrosodimethylamine [62-75-9]^
ND
ug/L
1
1.9
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
ND
ug/L
1
2.3
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
N-nitrosodiphenylamine/Diphenylamine
ND
ug/L
1
2.5
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
ND
ug/L
1
2.1
10
9I20004
EPA
8270E
09/23/19
23:08
DFM
FINAL
This report relates only to the sample as received
by the
laboratory,
and may only
be reproduced in full.
I Page 36 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-4 SW Lab Sample ID:CC16129-08 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 13:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Phenanthrene[85-01-8]A ND
ug/L
1
2.6
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
Phenol[108-95-2]A ND
ug/L
1
1.7
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
Pyrene [129-00-0]A ND
ug/L
1
3.5
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
Pyridine [110-86-1]A ND
ug/L
1
2.2
10
9I20004
EPA 8270E
09/23/19 23:08
DFM
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
2,4,6-Tribromophenol
80
1
100
80 %
10-179
9120004
EPA 8270E
09123119 23:08
DFM
2-Fluorobiphenyl
41
1
50.0
82 %
10-149
9120004
EPA 8270E
09123119 23:08
DFM
2-Fluorophenol
43
1
100
43 %
10-110
9120004
EPA 8270E
09123119 23:08
DFM
Nitrobenzene-d5
36
1
50.0
73 %
10-149
9120004
EPA 8270E
09123119 23:08
DFM
Phenol-d5
36
1
100
36 %
10-88
9120004
EPA 8270E
09123119 23:08
DFM
Terphenyl-d14
35
1
50.0
70 %
10-166
9120004
EPA 8270E
09123119 23:08
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 37 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-4 SED Lab Sample ID:CC16129-09 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 13:25 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 85.29
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl
Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
mg/kg
dry
0.567
0.00011
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,1,1-Trichloroethane [71-55-6]^
ND
mg/kg
dry
0.567
0.00017
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
mg/kg
dry
0.567
0.00013
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,1,2-Trichloroethane [79-00-5]^
ND
mg/kg
dry
0.567
0.00017
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,1-Dichloroethane [75-34-3]1
ND
mg/kg
dry
0.567
0.00017
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,1-Dichloroethene [75-35-4]1
ND
mg/kg
dry
0.567
0.00020
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,1-Dichloropropene [563-58-6]^
ND
mg/kg
dry
0.567
0.00011
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,2,3-Trichlorobenzene [87-61-6]1
ND
mg/kg
dry
0.567
0.00019
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,2,3-Trichloropropane [96-18-4]1
ND
mg/kg
dry
0.567
0.00043
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
mg/kg
dry
0.567
0.00018
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,2,4-Trimethylbenzene [95-63-6]1
ND
mg/kg
dry
0.567
0.00011
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,2-Dibromo-3-chloropropane [96-12-8]1
ND
mg/kg
dry
0.567
0.00053
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,2-Dibromoethane [106-93-4]1
ND
mg/kg
dry
0.567
0.00031
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,2-Dichlorobenzene [95-50-1]^
ND
mg/kg
dry
0.567
0.00018
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,2-Dichloroethane [107-06-2]1
ND
mg/kg
dry
0.567
0.00027
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,2-Dichloropropane [78-87-5]1
ND
mg/kg
dry
0.567
0.00017
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,3,5-Trimethylbenzene [108-67-8]1
ND
mg/kg
dry
0.567
0.00013
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,3-Dichlorobenzene [541-73-1]^
ND
mg/kg
dry
0.567
0.00015
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,3-Dichloropropane [142-28-9]1
ND
mg/kg
dry
0.567
0.00019
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
1,4-Dichlorobenzene [106-46-7]^
ND
mg/kg
dry
0.567
0.00013
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
2,2-Dichloropropane [594-20-7]^
ND
mg/kg
dry
0.567
0.00015
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
2-Butanone [78-93-3]^
0.00090 J
mg/kg
dry
0.567
0.00052
0.0033
9303011
EPA 8260D
10/03/19 15:21
REF
2-ChloroethylVinyl Ether [110-75-8]^
ND
mg/kg
dry
0.567
0.00011
0.0033
9303011
EPA 8260D
10/03/19 15:21
REF
2-Chlorotoluene [95-49-8]^
ND
mg/kg
dry
0.567
0.00012
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
2-Hexanone [591-78-6]^
ND
mg/kg
dry
0.567
0.00050
0.0033
9303011
EPA 8260D
10/03/19 15:21
REF
4-Chlorotoluene [106-43-4]^
ND
mg/kg
dry
0.567
0.00017
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
4-Isopropyltoluene [99-87-6]^
ND
mg/kg
dry
0.567
0.00011
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
4-Methyl-2-pentanone [108-10-1]^
ND
mg/kg
dry
0.567
0.00038
0.0033
9303011
EPA 8260D
10/03/19 15:21
REF
Acetone [67-64-1]^
ND
mg/kg
dry
0.567
0.0093
0.013
9303011
EPA 8260D
10/03/19 15:21
REF
Benzene [71-43-2]^
ND
mg/kg
dry
0.567
0.00011
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Bromobenzene [108-86-1]^
ND
mg/kg
dry
0.567
0.00015
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Bromochloromethane [74-97-5]^
ND
mg/kg
dry
0.567
0.00027
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Bromodichloromethane [75-27-4]^
ND
mg/kg
dry
0.567
0.00016
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Bromoform [75-25-2]^
ND
mg/kg
dry
0.567
0.00030
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Bromomethane [74-83-9]^
ND
mg/kg
dry
0.567
0.00021
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Carbon disulfide [75-15-0]^
ND
mg/kg
dry
0.567
0.00026
0.0033
9303011
EPA 8260D
10/03/19 15:21
REF
Carbon Tetrachloride [56-23-5]^
ND
mg/kg
dry
0.567
0.00015
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Chlorobenzene [108-90-7]^
ND
mg/kg
dry
0.567
0.00011
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Chloroethane [75-00-3]^
ND
mg/kg
dry
0.567
0.00017
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF QV-01
Chloroform [67-66-3]^
ND
mg/kg
dry
0.567
0.00012
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Chloromethane [74-87-3]^
ND
mg/kg
dry
0.567
0.00014
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
cis- 1,2-Dichloroethene [156-59-2]^
ND
mg/kg
dry
0.567
0.00015
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
cis- 1,3-Dichloropropene [10061-01-5]^
ND
mg/kg
dry
0.567
0.00011
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Dibromochloromethane [124-48-1]^
ND
mg/kg
dry
0.567
0.00023
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Dibromomethane [74-95-3]^
ND
mg/kg
dry
0.567
0.00022
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Dichlorodifluoromethane [75-71-8]^
ND
mg/kg
dry
0.567
0.00030
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF QV-01
Ethylbenzene [100-41-4]^
ND
mg/kg
dry
0.567
0.00013
0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 38 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-4 SED Lab Sample ID:CC16129-09 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 13:25 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 85.29
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]^
ND
mg/kg dry
0.567
0.00023 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Isopropyl Ether [108-20-3]^
ND
mg/kg dry
0.567
0.00012 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Isopropylbenzene [98-82-8]^
ND
mg/kg dry
0.567
0.00010 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
m,p-Xylenes [108-38-3/106-42-3]^
ND
mg/kg dry
0.567
0.00025 0.0013
9303011
EPA 8260D
10/03/19 15:21
REF
Methylene Chloride [75-09-2]^
ND
mg/kg dry
0.567
0.00049 0.0013
9303011
EPA 8260D
10/03/19 15:21
REF
Methyl-tert-Butyl Ether [1634-04-4]^
ND
mg/kg dry
0.567
0.00020 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Naphthalene [91-20-3]^
ND
mg/kg dry
0.567
0.00018 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
n-Butyl Benzene [104-51-8]^
ND
mg/kg dry
0.567
0.00009 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
n-Propyl Benzene [103-65-1]^
ND
mg/kg dry
0.567
0.00012 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
o-Xylene [95-47-6]^
ND
mg/kg dry
0.567
0.00015 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
sec-Butylbenzene [135-98-8]^
ND
mg/kg dry
0.567
0.00063 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Styrene [100-42-5]^
ND
mg/kg dry
0.567
0.00065 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
tert-Butyl benzene [98-06-6]^
ND
mg/kg dry
0.567
0.00011 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Tetrachloroethene [127-18-4]^
ND
mg/kg dry
0.567
0.00019 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Toluene [108-88-3]^
ND
mg/kg dry
0.567
0.00016 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
mg/kg dry
0.567
0.00025 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
mg/kg dry
0.567
0.00026 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Trichloroethene [79-01-6]^
ND
mg/kg dry
0.567
0.00021 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF
Trichlorofluoromethane [75-69-4]^
ND
mg/kg dry
0.567
0.00017 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF QV-01
Vinyl chloride [75-01-4]^
ND
mg/kg dry
0.567
0.00016 0.00066
9303011
EPA 8260D
10/03/19 15:21
REF QV-01
Xylenes (Total) [1330-20-7]^
ND
mg/kg dry
0.567
0.00037 0.0020
9303011
EPA 8260D
10/03/19 15:21
REF
surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
" Notes
4-Bromofluorobenzene
37
0.567
50.0
73 %
50-127
9JO3011
EPA 8260D
1010311915:21
REF
Dibromofluoromethane
41
0.567
50.0
82 %
52-128
9JO3011
EPA 8260D
1010311915:21
REF
Toluene-d8
33
0.567
50.0
67 %
57-124
9JO3011
EPA 8260D
1010311915:21
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
4
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
ND
mg/kg dry
5
0.15
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
1,2-Dichlorobenzene [95-50-1]^
ND
mg/kg dry
5
0.13
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
1,3-Dichlorobenzene [541-73-1]^
ND
mg/kg dry
5
0.12
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
1,4-Dichlorobenzene [106-46-7]^
ND
mg/kg dry
5
0.12
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
1-Methylnaphthalene [90-12-0]^
ND
mg/kg dry
5
0.16
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2,4,5-Trichlorophenol[95-95-4]^
ND
mg/kg dry
5
0.16
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2,4,6-Trichlorophenol[88-06-2]^
ND
mg/kg dry
5
0.16
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2,4-Dichlorophenol [120-83-2]^
ND
mg/kg dry
5
0.14
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2,4-Dimethylphenol [105-67-9]^
ND
mg/kg dry
5
0.25
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2,4-Dinitrophenol [51-28-5]^
ND
mg/kg dry
5
0.25
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2,4-Dinitrotoluene [121-14-2]^
ND
mg/kg dry
5
0.16
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2,6-Dinitrotoluene [606-20-2]^
ND
mg/kg dry
5
0.18
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2-Chloronaphthalene [91-58-7]^
ND
mg/kg dry
5
0.16
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2-Chlorophenol [95-57-8]^
ND
mg/kg dry
5
0.15
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
ND
mg/kg dry
5
0.19
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2-Methylnaphthalene [91-57-6]^
ND
mg/kg dry
5
0.16
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2-Methylphenol [95-48-7]^
ND
mg/kg dry
5
0.15
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
2-Nitroaniline [88-74-4]^
ND
mg/kg dry
5
0.18
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 39 Of 65

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-4 SED Lab Sample ID:CC16129-09 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 13:25 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 85.29
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
ND
mg/kg
dry
5
0.18
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]^
ND
mg/kg
dry
5
0.15
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
3,3'-Dichlorobenzidine [91-94-1]^
ND
mg/kg
dry
5
0.57
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
3-Nitroaniline [99-09-2]^
ND
mg/kg
dry
5
0.21
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
4-Bromophenyl-phenylether [101-55-3]^
ND
mg/kg
dry
5
0.16
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
4-Chloro-3-methylphenol[59-50-7]^
ND
mg/kg
dry
5
0.19
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
4-Chloroaniline [106-47-8]^
ND
mg/kg
dry
5
0.55
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
4-Chlorophenyl-phenylether [7005-72-3]^
ND
mg/kg
dry
5
0.15
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
4-Nitroaniline [100-01-6]^
ND
mg/kg
dry
5
0.31
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
4-Nitrophenol [100-02-7]^
ND
mg/kg
dry
5
0.18
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Acenaphthene [83-32-9]^
ND
mg/kg
dry
5
0.16
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Acenaphthylene [208-96-8]^
ND
mg/kg
dry
5
0.16
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Anthracene [120-12-7]^
ND
mg/kg
dry
5
0.22
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Benzidine [92-87-5]^
ND
mg/kg
dry
5
0.64
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Benzo(a)anthracene [56-55-3]^
ND
mg/kg
dry
5
0.16
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Benzo(a)pyrene [50-32-8]^
ND
mg/kg
dry
5
0.19
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Benzo(b)fluoranthene [205-99-2]^
ND
mg/kg
dry
5
0.11
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Benzo(g,h,i)perylene [191-24-2]^
ND
mg/kg
dry
5
0.28
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Benzo(k)fluoranthene [207-08-9]^
ND
mg/kg
dry
5
0.19
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Benzoic acid [65-85-0]^
ND
mg/kg
dry
5
0.88
10
9I23028
EPA
8270E
09/25/19
15:42
DFM
Benzyl alcohol [100-51-6]^
ND
mg/kg
dry
5
0.13
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
ND
mg/kg
dry
5
0.15
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Bis(2-chloroethyl)ether [111-44-4]^
ND
mg/kg
dry
5
0.25
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Bis(2-chloroisopropyl)ether [108-60-1]^
ND
mg/kg
dry
5
0.14
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM QV-01
Bis(2-ethylhexyl)phthalate [117-81-7]^
ND
mg/kg
dry
5
0.21
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Butylbenzylphthalate [85-68-7]^
ND
mg/kg
dry
5
0.23
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Chrysene [218-01-9]^
ND
mg/kg
dry
5
0.18
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Dibenzo(a,h)anthracene [53-70-3]^
ND
mg/kg
dry
5
0.30
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM QV-01
Dibenzofuran [132-64-9]^
ND
mg/kg
dry
5
0.16
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Diethylphthalate [84-66-2]^
ND
mg/kg
dry
5
0.16
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Dimethylphthalate [131-11-3]^
ND
mg/kg
dry
5
0.19
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Di-n-butylphthalate [84-74-2]^
ND
mg/kg
dry
5
0.24
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Di-n-octylphthalate [117-84-0]^
ND
mg/kg
dry
5
0.19
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Fluoranthene [206-44-0]^
ND
mg/kg
dry
5
0.21
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Fluorene [86-73-7]^
ND
mg/kg
dry
5
0.17
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Hexachlorobenzene [118-74-1]^
ND
mg/kg
dry
5
0.15
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Hexachlorobutadiene [87-68-3]^
ND
mg/kg
dry
5
0.15
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Hexachlorocyclopentadiene [77-47-4]^
ND
mg/kg
dry
5
0.23
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Hexachloroethane [67-72-1]^
ND
mg/kg
dry
5
0.12
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
ND
mg/kg
dry
5
0.28
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM QV-01
Isophorone [78-59-1]^
ND
mg/kg
dry
5
0.18
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Naphthalene [91-20-3]^
ND
mg/kg
dry
5
0.16
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
Nitrobenzene [98-95-3]^
ND
mg/kg
dry
5
0.15
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
N-Nitrosodimethylamine [62-75-9]^
ND
mg/kg
dry
5
0.12
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
ND
mg/kg
dry
5
0.47
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
N-nitrosodiphenylamine/Diphenylamine
ND
mg/kg
dry
5
0.32
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
ND
mg/kg
dry
5
0.19
1.9
9I23028
EPA
8270E
09/25/19
15:42
DFM
FINAL
This report relates only to the sample as
received
by the
laboratory,
and may only
be reproduced in full.
I Page 40 Of 65

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www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-4 SED Lab Sample ID:CC16129-09 Received: 09/20/19 11:05
Matrix: Soil Sampled:09/19/19 13:25 Work Order: CC16129
Project: Smith Property FSA Sampled By: PHIL Rahn % Solids: 85.29
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Phenanthrene [85-01-8]A ND
mg/kg dry
5
0.16
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
Phenol[108-95-2]A ND
mg/kg dry
5
0.13
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
Pyrene [129-00-0]A ND
mg/kg dry
5
0.22
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
Pyridine [110-86-1]A ND
mg/kg dry
5
0.48
1.9
9I23028
EPA 8270E
09/25/19 15:42
DFM
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
2.9
5
3.91
74 %
26-130
9123026
EPA 8270E
0912511915:42
DFM
2-Fluorobiphenyl
1.7
5
1.95
89 %
56-120
9123026
EPA 8270E
0912511915:42
DFM
2-Fluorophenol
2.6
5
3.91
71 %
49-126
9123026
EPA 8270E
09125119 15:42
DFM
Nitrobenzene-d5
1.7
5
1.95
85 %
50-117
9123026
EPA 8270E
0912511915:42
DFM
Phenol-d5
3.1
5
3.91
60 %
56-120
9123026
EPA 8270E
0912511915:42
DFM
Terphenyl-d14
1.8
5
1.95
91 %
36-151
9123026
EPA 8270E
0912511915:42
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 41 of 65

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-5 -SPRING #2 Lab Sample ID:CC16129-10 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 13:50 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
ug/L
1
0.17
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,1,1-Trichloroethane [71-55-6]^
ND
ug/L
1
0.12
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
ug/L
1
0.28
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,1,2-Trichloroethane [79-00-5]^
ND
ug/L
1
0.14
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,1-Dichloroethane [75-34-3]^
ND
ug/L
1
0.13
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,1-Dichloroethene [75-35-4]^
ND
ug/L
1
0.21
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,1-Dichloropropene [563-58-6]^
ND
ug/L
1
0.15
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
ug/L
1
0.012
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,2,3-Trichloropropane [96-18-4]^
ND
ug/L
1
0.23
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
0.14
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
ug/L
1
0.10
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
ug/L
1
0.48
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,2-Dibromoethane [106-93-4]^
ND
ug/L
1
0.66
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
0.19
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,2-Dichloroethane [107-06-2]^
ND
ug/L
1
0.21
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,2-Dichloropropane [78-87-5]^
ND
ug/L
1
0.10
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
ug/L
1
0.30
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
0.15
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,3-Dichloropropane [142-28-9]^
ND
ug/L
1
0.16
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
0.19
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
2,2-Dichloropropane [594-20-7]^
ND
ug/L
1
0.28
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
2-Butanone [78-93-3]^
ND
ug/L
1
1.3
5.0
9I30034
EPA 8260D
10/01/19 11:20
REF
2-Chloroethyl Vinyl Ether[110-75-8]^
ND
ug/L
1
1.1
5.0
9I30034
EPA 8260D
10/01/19 11:20
REF
2-Chlorotoluene [95-49-8]^
ND
ug/L
1
0.081
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
2-Hexanone [591-78-6]^
ND
ug/L
1
0.88
5.0
9I30034
EPA 8260D
10/01/19 11:20
REF
4-Chlorotoluene [106-43-4]^
ND
ug/L
1
0.068
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
4-Isopropyltoluene [99-87-6]^
ND
ug/L
1
0.085
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
4-Methyl-2-pentanone [108-10-1]^
ND
ug/L
1
1.1
5.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Acetone [67-64-1]^
13 1
ug/L
1
10
20
9I30034
EPA 8260D
10/01/19 11:20
REF
Benzene[71-43-2]^
ND
ug/L
1
0.15
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Bromobenzene [108-86-1]^
ND
ug/L
1
0.16
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Bromochloromethane [74-97-5]^
ND
ug/L
1
0.48
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Bromodichloromethane [75-27-4]^
ND
ug/L
1
0.17
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Bromoform [75-25-2]^
ND
ug/L
1
0.22
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Bromomethane [74-83-9]^
ND
ug/L
1
0.14
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Carbon disulfide [75-15-0]^
ND
ug/L
1
1.5
5.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Carbon tetrachloride [56-23-5]^
ND
ug/L
1
0.17
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Chlorobenzene [108-90-7]^
ND
ug/L
1
0.17
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Chloroethane [75-00-3]^
ND
ug/L
1
0.23
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Chloroform [67-66-3]^
ND
ug/L
1
0.18
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Chloromethane [74-87-3]^
ND
ug/L
1
0.13
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
ug/L
1
0.15
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
ug/L
1
0.20
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Dibromochloromethane [124-48-1]^
ND
ug/L
1
0.17
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Dibromomethane [74-95-3]^
ND
ug/L
1
0.27
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Dichlorodifluoromethane [75-71-8]^
ND
ug/L
1
0.20
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Ethylbenzene [100-41-4]^
ND
ug/L
1
0.13
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 42 Of 65

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-5 -SPRING #2 Lab Sample ID:CC16129-10 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 13:50 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]1
ND
ug/L
1
0.22
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Isopropyl Ether[108-20-3]^
ND
ug/L
1
0.36
1.0
9I26038
EPA 8260D
09/27/19 10:29
REF
Isopropyl benzene [98-82-8]1
ND
ug/L
1
0.14
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
m,p-Xylenes [108-38-3/106-42-3]1
ND
ug/L
1
0.17
2.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Methylene chloride [75-09-2]^
ND
ug/L
1
0.23
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Methyl-tert-Butyl Ether [1634-04-4]^
ND
ug/L
1
0.16
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Naphthalene [91-20-3]^
ND
ug/L
1
0.11
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
n-Butyl Benzene [104-51-8]^
ND
ug/L
1
0.058
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
n-Propyl Benzene [103-65-1]^
ND
ug/L
1
0.12
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
o-Xylene [95-47-6]^
ND
ug/L
1
0.065
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
sec-Burylbenzene [135-98-8]^
ND
ug/L
1
0.10
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Styrene [100-42-5]^
ND
ug/L
1
0.11
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
tert-Butylbenzene [98-06-6]^
ND
ug/L
1
0.17
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Tetrachloroethene [127-18-4]^
ND
ug/L
1
0.17
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Toluene [308-88-3]^
0.35 J
ug/L
1
0.14
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
trans-1,2-Dichloroethene [156-60-5]^
ND
ug/L
1
0.21
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
trans-1,3-Dichloropropene [10061-02-6]^
ND
ug/L
1
0.15
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Trichloroethene [79-01-6]^
ND
ug/L
1
0.15
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Trichlorofluoromethane [75-69-4]^
ND
ug/L
1
0.24
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Vinyl chloride [75-01-4]^
ND
ug/L
1
0.32
1.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Xylenes(Total)[1330-20-7]^
ND
ug/L
1
0.45
3.0
9I30034
EPA 8260D
10/01/19 11:20
REF
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
45
1
50.0
89 %
53-136
9130034
EPA 8260D
10101119 11:20
REF
Dlbromofluoromethane
47
1
50.0
93 %
67-129
9130034
EPA 6260D
1010111911:20
REF
Toluene-&
37
1
50.0
74 %
59-134
9130034
EPA 6260D
1010111911:20
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 43 Of 65

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: AOC-5 -SPRING #3 Lab Sample ID:CC16129-11 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 14:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
ND
ug/L
1
0.17
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,1,1-Trichloroethane [71-55-6]^
ND
ug/L
1
0.12
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
ND
ug/L
1
0.28
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,1,2-Trichloroethane [79-00-5]^
ND
ug/L
1
0.14
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,1-Dichloroethane [75-34-3]^
ND
ug/L
1
0.13
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,1-Dichloroethene [75-35-4]^
ND
ug/L
1
0.21
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,1-Dichloropropene [563-58-6]^
ND
ug/L
1
0.15
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,2,3-Trichlorobenzene [87-61-6]^
ND
ug/L
1
0.012
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,2,3-Trichloropropane [96-18-4]^
ND
ug/L
1
0.23
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,2,4-Trichlorobenzene [120-82-1]^
ND
ug/L
1
0.14
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,2,4-Trimethylbenzene [95-63-6]^
ND
ug/L
1
0.10
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
ND
ug/L
1
0.48
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,2-Dibromoethane [106-93-4]^
ND
ug/L
1
0.66
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,2-Dichlorobenzene [95-50-1]^
ND
ug/L
1
0.19
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,2-Dichloroethane [107-06-2]^
ND
ug/L
1
0.21
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,2-Dichloropropane [78-87-5]^
ND
ug/L
1
0.10
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,3,5-Trimethylbenzene [108-67-8]^
ND
ug/L
1
0.30
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,3-Dichlorobenzene [541-73-1]^
ND
ug/L
1
0.15
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,3-Dichloropropane [142-28-9]^
ND
ug/L
1
0.16
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
1,4-Dichlorobenzene [106-46-7]^
ND
ug/L
1
0.19
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
2,2-Dichloropropane [594-20-7]^
ND
ug/L
1
0.28
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF QV-01
2-Butanone [78-93-3]^
ND
ug/L
1
1.3
5.0
9I27013
EPA 8260D
09/28/19
00:38
REF
2-Chloroethyl Vinyl Ether[110-75-8]^
ND
ug/L
1
1.1
5.0
9I27013
EPA 8260D
09/28/19
00:38
REF
2-Chlorotoluene [95-49-8]^
ND
ug/L
1
0.081
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
2-Hexanone [591-78-6]^
ND
ug/L
1
0.88
5.0
9I27013
EPA 8260D
09/28/19
00:38
REF
4-Chlorotoluene [106-43-4]^
ND
ug/L
1
0.068
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
4-Isopropyltoluene [99-87-6]^
ND
ug/L
1
0.085
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
4-Methyl-2-pentanone [108-10-1]^
ND
ug/L
1
1.1
5.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Acetone [67-64-1]^
ND
ug/L
1
10
20
9I27013
EPA 8260D
09/28/19
00:38
REF
Benzene[71-43-2]^
ND
ug/L
1
0.15
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Bromobenzene [108-86-1]^
ND
ug/L
1
0.16
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Bromochloromethane [74-97-5]^
ND
ug/L
1
0.48
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Bromodichloromethane [75-27-4]^
ND
ug/L
1
0.17
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Bromoform [75-25-2]^
ND
ug/L
1
0.22
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Bromomethane [74-83-9]^
ND
ug/L
1
0.14
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Carbon disulfide [75-15-0]^
ND
ug/L
1
1.5
5.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Carbon tetrachloride [56-23-5]^
ND
ug/L
1
0.17
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Chlorobenzene [108-90-7]^
ND
ug/L
1
0.17
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Chloroethane [75-00-3]^
ND
ug/L
1
0.23
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Chloroform [67-66-3]^
ND
ug/L
1
0.18
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Chloromethane [74-87-3]^
ND
ug/L
1
0.13
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
cis-1,2-Dichloroethene [156-59-2]^
ND
ug/L
1
0.15
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
cis-1,3-Dichloropropene [10061-01-5]^
ND
ug/L
1
0.20
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Dibromochloromethane [124-48-1]^
ND
ug/L
1
0.17
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Dibromomethane [74-95-3]^
ND
ug/L
1
0.27
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Dichlorodifluoromethane [75-71-8]^
ND
ug/L
1
0.20
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Ethylbenzene [100-41-4]^
ND
ug/L
1
0.13
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 44 Of 65

00�
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ANALYTICAL RESULTS
Description: AOC-5 -SPRING #3 Lab Sample ID:CC16129-11 Received: 09/20/19 11:05
Matrix: Water Sampled:09/19/19 14:15 Work Order: CC16129
Project: Smith Property FSA Sampled By: Phil Rahn
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl
Results Flag
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
Hexachlorobutadiene [87-68-3]A
ND
ug/L
1
0.22
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Isopropyl Ether[108-20-3]A
ND
ug/L
1
0.36
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Isopropylbenzene [98-82-8]A
ND
ug/L
1
0.14
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
m,p-Xylenes [108-38-3/106-42-3]A
ND
ug/L
1
0.17
2.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Methylene chloride [75-09-2]A
ND
ug/L
1
0.23
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Methyl-tert-Butyl Ether [1634-04-4]A
ND
ug/L
1
0.16
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Naphthalene [91-20-3]A
ND
ug/L
1
0.11
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
n-Butyl Benzene [104-51-8]A
ND
ug/L
1
0.058
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
n-Propyl Benzene [103-65-1]A
ND
ug/L
1
0.12
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
o-Xylene [95-47-6]A
ND
ug/L
1
0.065
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
sec-Butylbenzene [135-98-8]A
ND
ug/L
1
0.10
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Styrene [100-42-5]A
ND
ug/L
1
0.11
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
tert-Butyl benzene [98-06-6]A
ND
ug/L
1
0.17
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Tetrachloroethene [127-18-4]A
ND
ug/L
1
0.17
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Toluene [108-88-3]A
ND
ug/L
1
0.14
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
trans-1,2-Dichloroethene [156-60-5]A
ND
ug/L
1
0.21
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
trans-1,3-Dichloropropene [10061-02-6]A
ND
ug/L
1
0.15
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Trichloroethene [79-01-6]A
ND
ug/L
1
0.15
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Trichlorofluoromethane [75-69-4]A
ND
ug/L
1
0.24
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Vinyl chloride [75-01-4]A
ND
ug/L
1
0.32
1.0
9I27013
EPA 8260D
09/28/19
00:38
REF
Xylenes (Total) [1330-20-7]A
ND
ug/L
1
0.45
3.0
9I27013
EPA 8260D
09/28/19
00:38
REF
surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
" Notes
4-Bromofluorobenzene
43
1
50.0
86 %
53-136
9127013
EPA 8260D
09128119 00338
REF
Dibromofluoromethane
46
1
50.0
91 %
67-129
9127013
EPA 8260D
09128119 00338
REF
Toluene-d8
38
1
50.0
76 %
59-134
9127013
EPA 8260D
09128119 00338
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 45 Of 65

0Nk"q09
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9126038 - EPA 5030B MS
Blank (9I26038-BLKI) Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 02:11
Spike
Analvte
Result
Flag
POL
Units Level
1, 1, 1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,1-Dichloropropene
0.15
U
1.0
ug/L
1,2,3-Trichlorobenzene
0.012
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2,4-Trichlorobenzene
0.14
U
1.0
ug/L
1,2,4-Trimethylbenzene
0.10
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,3,5-Trimethylbenzene
0.30
U
1.0
ug/L
1,3-Dichlorobenzene
0.15
U
1.0
ug/L
1,3-Dichloropropane
0.16
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2,2-Dichloropropane
0.28
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Chloroethyl Vinyl Ether
1.1
U
5.0
ug/L
2-Chlorotoluene
0.081
U
1.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Chlorotoluene
0.068
U
1.0
ug/L
4-Isopropyltoluene
0.085
U
1.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Benzene
0.15
U
1.0
ug/L
Bromobenzene
0.16
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis-1,2-Dichloroethene
0.15
U
1.0
ug/L
cis-1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Dichlorodifluoromethane
0.20
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Hexachlorobutadiene
0.22
U
1.0
ug/L
Isopropyl Ether
0.36
U
1.0
ug/L
Source %REC
Result %REC Limits
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 46 Of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9126038 - EPA 5030E MS - Continued
Blank (9I26038-BLKI) Continued Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 02:11
Spike
Source
%REC
RPD
Analvte
Result
Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Isopropylbenzene
0.14
U
1.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
Methyl-tert-Butyl Ether
0.16
U
1.0
ug/L
Naphthalene
0.11
U
1.0
ug/L
n-Butyl Benzene
0.058
U
1.0
ug/L
n-Propyl Benzene
0.12
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
sec-Butylbenzene
0.10
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
tert-Butylbenzene
0.17
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
4-Bromofluorobenzene
43
u9/L
50.0
86
53-136
Dibromofluoromethane
44
u9/L
50.0
88
67-129
Toluene-&
37
u9/L
50.0
74
59-134
LCS (9I26038-BS1)
Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 00:06
Spike
Source
%REC
RPD
Analvte
Result
Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
17
1.0
ug/L
20.0
86
75-133
Benzene
19
1.0
ug/L
20.0
96
80-134
Chlorobenzene
19
1.0
ug/L
20.0
93
80-120
Toluene
19
1.0
ug/L
20.0
96
71-120
Trichloroethene
18
1.0
ug/L
20.0
91
74-120
4-9romofluorobenzene
45
u9/L
50.0
89
53-136
Dibromofluoromethane
43
u9/L
50.0
86
67-129
Toluene-d8
36
u9/L
50.0
72
59-134
Matrix Spike (9I26038-MS1)
Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 00:37
Source: CC16420-05
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Lim! RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
0.21 U
91
75-133
Benzene
20
1.0
ug/L
20.0
0.15 U
98
80-134
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
93
80-120
Toluene
18
1.0
ug/L
20.0
0.14 U
92
71-120
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
93
74-120
4-Bromofluorobenzene
45
u9/L
50.0
91
53-136
Dibromofluoromethane
43
u9/L
50.0
86
67-129
Toluene-&
36
u9/L
50.0
75
59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 47 Of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9I26038 - EPA 50308 MS - Continued
Matrix Spike Dup (9I26038-MSD3)
Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 01:08
Source: CC16420-05
Spike
Source
%REC
RPD
Analvte Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene 17
1.0
ug/L
20.0
0.21 U
84
75-133
8
20
Benzene 19
1.0
ug/L
20.0
0.15 U
94
80-134
5
17
Chlorobenzene 18
1.0
ug/L
20.0
0.17 U
88
80-120
6
16
Toluene 18
1.0
ug/L
20.0
0.14 U
88
71-120
4
17
Trichloroethene 17
1.0
ug/L
20.0
0.15 U
87
74-120
6
22
4-Bromofluorobenzene 44 ug/L 50.0 86 53-136
Dibromofluoromethane 43 ug/L 50.0 86 67-129
Toluene-d8 37 ug/L 50.0 75 59-134
Batch 9I27013 - EPA 50308 MS
Blank (9I27013-BLK1) Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 15:47
Spike
Analvte
Result
Flaq
POL
Units Level
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,1-Dichloropropene
0.15
U
1.0
ug/L
1,2,3-Trichlorobenzene
0.012
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2,4-Trichlorobenzene
0.14
U
1.0
ug/L
1,2,4-Trimethylbenzene
0.10
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,3,5-Trimethylbenzene
0.30
U
1.0
ug/L
1,3-Dichlorobenzene
0.15
U
1.0
ug/L
1,3-Dichloropropane
0.16
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2,2-Dichloropropane
0.28
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Chloroethyl Vinyl Ether
1.1
U
5.0
ug/L
2-Chlorotoluene
0.081
U
1.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Chlorotoluene
0.068
U
1.0
ug/L
4-Isopropyltoluene
0.085
U
1.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Benzene
0.15
U
1.0
ug/L
Bromobenzene
0.16
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Source %REC
Result %REC Limits
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 48 Of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9I27013 - EPA 50308 MS - Continued
Blank (9I27013-BLKi) Continued Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 15:47
Spike
Analvte
Result
Flaq
POL
Units Level
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Dichlorodifluoromethane
0.20
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Hexachlorobutadiene
0.22
U
1.0
ug/L
Isopropyl Ether
0.36
U
1.0
ug/L
Isopropyl benzene
0.14
U
1.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
Methyl-tert-Butyl Ether
0.16
U
1.0
ug/L
Naphthalene
0.11
U
1.0
ug/L
n-Butyl Benzene
0.058
U
1.0
ug/L
n-Propyl Benzene
0.12
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
sec-Butylbenzene
0.10
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
tert-Butyl benzene
0.17
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Source %REC RPD
Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene
43
u91L
50.0
87
53-136
Dibromofluoromethane
45
u91L
50.0
89
67-129
Toluene-d8
38
u91L
50.0
75
59-134
LCS (9I27013-BS1)
Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 13:42
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
17
1.0
ug/L
20.0
86
75-133
Benzene
19
1.0
ug/L
20.0
96
80-134
Chlorobenzene
18
1.0
ug/L
20.0
90
80-120
Toluene
18
1.0
ug/L
20.0
92
71-120
Trichloroethene
17
1.0
ug/L
20.0
86
74-120
4-Bromofluorobenzene
43
u91L
50.0
87
53-136
Dibromofluoromethane
43
u91L
50.0
66
67-129
Toluene-d8
37
u91L
50.0
75
59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 49 Of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9I27013 - EPA 50308 MS - Continued
Matrix Spike (9I27013-MSI) Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 14:13
Source: CC16420-06
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
17
1.0
ug/L
20.0
0.21 U
85
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
94
80-134
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
90
80-120
Toluene
17
1.0
ug/L
20.0
0.14 U
87
71-120
Trichloroethene
16
1.0
ug/L
20.0
0.15 U
82
74-120
4-Bromofluorobenzene
44
ug/L
50.0
89
53-136
Dibromofluoromethane
44
ug/L
50.0
88
67-129
Toluene-d8
37
ug/L
50.0
75
59-134
Matrix Spike Dup (9I27013-MSD1)
Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 14:45
Source: CC16420-06
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
0.21 U
91
75-133
7
20
Benzene
21
1.0
ug/L
20.0
0.15 U
104
80-134
10
17
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
96
80-120
7
16
Toluene
19
1.0
ug/L
20.0
0.14 U
97
71-120
11
17
Trichloroethene
18
1.0
ug/L
20.0
0.15 U
91
74-120
10
22
4-Bromofluorobenzene 43 ug/L 50.0 86 53-136
Dibromofluoromethane 43 ug/L 50.0 87 67-129
Toluene-d8 38 ug/L 50.0 76 59-134
Batch 9I30034 - EPA 50308 MS
Blank (9I30034-BLK3) Prepared: 09/30/2019 14:34 Analyzed: 10/01/2019 03:32
Spike
Analvte
Result
Flaq
POL
Units Level
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,1-Dichloropropene
0.15
U
1.0
ug/L
1,2,3-Trichlorobenzene
0.012
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2,4-Trichlorobenzene
0.14
U
1.0
ug/L
1,2,4-Trimethylbenzene
0.10
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,3,5-Trimethylbenzene
0.30
U
1.0
ug/L
1,3-Dichlorobenzene
0.15
U
1.0
ug/L
1,3-Dichloropropane
0.16
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2,2-Dichloropropane
0.28
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
Source %REC
Result %REC Limits
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5O Of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9130034 - EPA 50308 MS - Continued
Blank (9I30034-BLKi) Continued Prepared: 09/30/2019 14:34 Analyzed: 10/01/2019 03:32
Spike
Analvte
Result
Flaa
POL
Units Level
2-Chloroethyl Vinyl Ether
1.1
U
5.0
ug/L
2-Chlorotoluene
0.081
U
1.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Chlorotoluene
0.068
U
1.0
ug/L
4-Isopropyltoluene
0.085
U
1.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Benzene
0.15
U
1.0
ug/L
Bromobenzene
0.16
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Dichlorodifluoromethane
0.20
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Hexachlorobutadiene
0.22
U
1.0
ug/L
Isopropyl benzene
0.14
U
1.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
Methyl-tert-Butyl Ether
0.16
U
1.0
ug/L
Naphthalene
0.11
U
1.0
ug/L
n-Butyl Benzene
0.058
U
1.0
ug/L
n-Propyl Benzene
0.12
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
sec-Butylbenzene
0.10
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
tert-Butyl benzene
0.17
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Source %REC RPD
Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 44 u9/L 50.0 89 53-136
Dibromof/uoromethane 46 u9/L 50.0 92 67-129
Toluene-d8 37 u9/L 50.0 75 59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 51 of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9I30034 - EPA 50308 MS - Continued
LCS (9I30034-BS3) Prepared: 09/30/2019 14:34 Analyzed: 10/01/2019 00:25
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
91
75-133
Benzene
21
1.0
ug/L
20.0
103
80-134
Chlorobenzene
19
1.0
ug/L
20.0
95
80-120
Toluene
20
1.0
ug/L
20.0
98
71-120
Trichloroethene
19
1.0
ug/L
20.0
95
74-120
4-Bromofluorobenzene
44
ug/L
50.0
89
53-136
Dibromofluoromethane
44
ug/L
50.0
88
67-129
Toluene-d8
37
ug/L
50.0
74
59-134
Matrix Spike (9I30034-MS1)
Prepared: 09/30/2019 14:34 Analyzed: 10/01/2019 00:56
Source: CC13964-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
0.21 U
92
75-133
Benzene
20
1.0
ug/L
20.0
0.15 U
101
80-134
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
92
80-120
Toluene
19
1.0
ug/L
20.0
0.24
94
71-120
Trichloroethene
17
1.0
ug/L
20.0
0.15 U
87
74-120
4-Bromofluorobenzene
46
ug/L
50.0
92
53-136
Dibromofluoromethane
45
ug/L
50.0
90
67-129
Toluene-d8
37
ug/L
50.0
73
59-134
Matrix Spike Dup (9I30034-MSD1)
Prepared: 09/30/2019 14:34 Analyzed: 10/01/2019 01:27
Source: CC13964-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
0.21 U
89
75-133
4
20
Benzene
20
1.0
ug/L
20.0
0.15 U
100
80-134
1
17
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
91
80-120
2
16
Toluene
18
1.0
ug/L
20.0
0.24
88
71-120
7
17
Trichloroethene
17
1.0
ug/L
20.0
0.15 U
84
74-120
3
22
4-Bromofluorobenzene 45 ug/L 50.0 90 53-136
Dibromofluoromethane 44 ug/L 50.0 69 67-129
Toluene-d8 37 ug/L 50.0 74 59-134
Batch W02035 - EPA 5030E MS
Blank (9302035-BLK3) Prepared: 10/02/2019 12:41 Analyzed: 10/02/2019 18:18
Analvte
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dich loroethane
1,1-Dichloroethene
1,1-Dich loropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
FINAL
Spike Source %REC
Result
Flaq
POL
Units Level Result %REC Limits
0.00016
U
0.0010
mg/kg wet
0.00025
U
0.0010
mg/kg wet
0.00020
U
0.0010
mg/kg wet
0.00025
U
0.0010
mg/kg wet
0.00025
U
0.0010
mg/kg wet
0.00030
U
0.0010
mg/kg wet
0.00016
U
0.0010
mg/kg wet
0.00028
U
0.0010
mg/kg wet
0.00064
U
0.0010
mg/kg wet
0.00027
U
0.0010
mg/kg wet
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD Limit Notes
Page 52 of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9JO2035 - EPA 5030E MS - Continued
Blank (9102035-BLK3) Continued Prepared: 10/02/2019 12:41 Analyzed: 10/02/2019 18:18
Spike
Analvte
Result
Flaa
POL
Units Level
1,2,4-Trimethylbenzene
0.00017
U
0.0010
mg/kg wet
1,2-Dibromo-3-chloropropane
0.00079
U
0.0010
mg/kg wet
1,2-Dibromoethane
0.00046
U
0.0010
mg/kg wet
1,2-Dichlorobenzene
0.00027
U
0.0010
mg/kg wet
1,2-Dichloroethane
0.00041
U
0.0010
mg/kg wet
1,2-Dichloropropane
0.00026
U
0.0010
mg/kg wet
1,3,5-Trimethylbenzene
0.00020
U
0.0010
mg/kg wet
1,3-Dichlorobenzene
0.00022
U
0.0010
mg/kg wet
1,3-Dichloropropane
0.00029
U
0.0010
mg/kg wet
1,4-Dichlorobenzene
0.00020
U
0.0010
mg/kg wet
2,2-Dichloropropane
0.00023
U
0.0010
mg/kg wet
2-Butanone
0.00078
U
0.0050
mg/kg wet
2-Chloroethyl Vinyl Ether
0.00016
U
0.0050
mg/kg wet
2-Chlorotoluene
0.00018
U
0.0010
mg/kg wet
2-Hexanone
0.00075
U
0.0050
mg/kg wet
4-Chlorotoluene
0.00026
U
0.0010
mg/kg wet
4-Isopropyltoluene
0.00016
U
0.0010
mg/kg wet
4-Methyl-2-pentanone
0.00057
U
0.0050
mg/kg wet
Acetone
0.014
U
0.020
mg/kg wet
Benzene
0.00017
U
0.0010
mg/kg wet
Bromobenzene
0.00022
U
0.0010
mg/kg wet
Bromochloromethane
0.00041
U
0.0010
mg/kg wet
Bromodichloromethane
0.00024
U
0.0010
mg/kg wet
Bromoform
0.00045
U
0.0010
mg/kg wet
Bromomethane
0.00032
U
0.0010
mg/kg wet
Carbon disulfide
0.00039
U
0.0050
mg/kg wet
Carbon Tetrachloride
0.00022
U
0.0010
mg/kg wet
Chlorobenzene
0.00017
U
0.0010
mg/kg wet
Chloroethane
0.00025
U
0.0010
mg/kg wet
Chloroform
0.00018
U
0.0010
mg/kg wet
Chloromethane
0.00021
U
0.0010
mg/kg wet
cis- 1,2-Dichloroethene
0.00023
U
0.0010
mg/kg wet
cis- 1,3-Dichloropropene
0.00017
U
0.0010
mg/kg wet
Dibromochloromethane
0.00035
U
0.0010
mg/kg wet
Dibromomethane
0.00033
U
0.0010
mg/kg wet
Dichlorodifluoromethane
0.00045
U
0.0010
mg/kg wet
Ethylbenzene
0.00020
U
0.0010
mg/kg wet
Hexachlorobutadiene
0.00035
U
0.0010
mg/kg wet
Isopropyl Ether
0.00018
U
0.0010
mg/kg wet
Isopropyl benzene
0.00015
U
0.0010
mg/kg wet
m,p-Xylenes
0.00037
U
0.0020
mg/kg wet
Methylene Chloride
0.00073
U
0.0020
mg/kg wet
Methyl-tert-Butyl Ether
0.00030
U
0.0010
mg/kg wet
Naphthalene
0.00027
U
0.0010
mg/kg wet
n-Butyl Benzene
0.00013
U
0.0010
mg/kg wet
n-Propyl Benzene
0.00018
U
0.0010
mg/kg wet
o-Xylene
0.00022
U
0.0010
mg/kg wet
sec-Butylbenzene
0.00095
U
0.0010
mg/kg wet
Styrene
0.00098
U
0.0010
mg/kg wet
Source %REC
Result %REC Limits
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 53 Of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9JO2035 - EPA 5030B MS - Continued
Blank (9302035-BLK3) Continued Prepared: 10/02/2019 12:41 Analyzed: 10/02/2019 18:18
Spike
Source
%REC RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
tert-Butylbenzene
0.00017
U
0.0010
mg/kg wet
Tetrachloroethene
0.00028
U
0.0010
mg/kg wet
Toluene
0.00024
U
0.0010
mg/kg wet
trans-1,2-Dichloroethene
0.00037
U
0.0010
mg/kg wet
trans-1,3-Dichloropropene
0.00039
U
0.0010
mg/kg wet
Trichloroethene
0.00032
U
0.0010
mg/kg wet
Trichlorofluoromethane
0.00026
U
0.0010
mg/kg wet
Vinyl chloride
0.00024
U
0.0010
mg/kg wet
Xylenes(Total)
0.00056
U
0.0030
mg/kg wet
4-8romofluorobenzene
38
u91L
50.0
75
50-127
Dibromofluoromethane
41
u91L
50.0
83
52-128
Toluene-&
33
u91L
50.0
66
57-124
LCS (9302035-BS1)
Prepared: 10/02/2019 12:41 Analyzed: 10/02/2019 16:12
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
0.019
0.0010
mg/kg wet
0.0200
96
64-133
Benzene
0.020
0.0010
mg/kg wet
0.0200
101
79-129
Chlorobenzene
0.018
0.0010
mg/kg wet
0.0200
91
79-121
Toluene
0.019
0.0010
mg/kg wet
0.0200
94
77-120
Trichloroethene
0.020
0.0010
mg/kg wet
0.0200
98
78-120
4-8romofluorobenzene
39
u91L
50.0
77
50-127
Dibromofluoromethane
40
u91L
50.0
80
52-128
Toluene-d8
34
u91L
50.0
68
57-124
Matrix Spike (9302035-MS1)
Prepared: 10/02/2019 12:41 Analyzed: 10/02/2019 16:43
Source: CC16420-10
Spike
Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
0.020
0.0010
mg/kg wet
0.0200
0.00030 U
102
64-133
Benzene
0.021
0.0010
mg/kg wet
0.0200
0.00017 U
105
79-129
Chlorobenzene
0.019
0.0010
mg/kg wet
0.0200
0.00017 U
95
79-121
Toluene
0.019
0.0010
mg/kg wet
0.0200
0.00024 U
95
77-120
Trichloroethene
0.020
0.0010
mg/kg wet
0.0200
0.00032 U
100
78-120
4-8romofluorobenzene
40
u91L
50.0
79
50-127
Dibromofluoromethane
40
u91L
50.0
79
52-128
Toluene-d8
33
u91L
50.0
66
57-124
Matrix Spike Dup (9302035-MSD1)
Prepared: 10/02/2019 12:41 Analyzed: 10/02/2019 17:15
Source: CC16420-10
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
0.020
0.0010
mg/kg wet
0.0200
0.00030 U
98
64-133
5
23
Benzene
0.021
0.0010
mg/kg wet
0.0200
0.00017 U
105
79-129
0.1
23
Chlorobenzene
0.019
0.0010
mg/kg wet
0.0200
0.00017 U
97
79-121
2
25
Toluene
0.020
0.0010
mg/kg wet
0.0200
0.00024 U
100
77-120
5
23
Trichloroethene
0.020
0.0010
mg/kg wet
0.0200
0.00032 U
102
78-120
1
24
4-8romofluorobenzene 39 u91L 50.0 77 50-127
Dibromofluoromethane 40 u91L 50.0 80 52-128
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 54 Of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9J02035 - EPA 5030E MS - Continued
Matrix Spike Dup (9302035-MSD3) Continued Prepared: 10/02/2019 12:41 Analyzed: 10/02/2019 17:15
Source: CC16420-10
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Toluene-d8 33 ug/L 50.0 66 57-124
Batch 9J03011 - EPA 5030E MS
Blank (9303011-BLK3) Prepared: 10/03/2019 09:45 Analyzed: 10/03/2019 14:49
Spike
Analvte
Result
Flaq
POL
Units Level
1, 1, 1,2-Tetrachloroethane
0.00016
U
0.0010
mg/kg wet
1,1,1-Trichloroethane
0.00025
U
0.0010
mg/kg wet
1,1,2,2-Tetrachloroethane
0.00020
U
0.0010
mg/kg wet
1,1,2-Trichloroethane
0.00025
U
0.0010
mg/kg wet
1,1-Dichloroethane
0.00025
U
0.0010
mg/kg wet
1,1-Dichloroethene
0.00030
U
0.0010
mg/kg wet
1,1-Dichloropropene
0.00016
U
0.0010
mg/kg wet
1,2,3-Trichlorobenzene
0.00028
U
0.0010
mg/kg wet
1,2,3-Trichloropropane
0.00064
U
0.0010
mg/kg wet
1,2,4-Trichlorobenzene
0.00027
U
0.0010
mg/kg wet
1,2,4-Trimethylbenzene
0.00017
U
0.0010
mg/kg wet
1,2-Dibromo-3-chloropropane
0.00079
U
0.0010
mg/kg wet
1,2-Dibromoethane
0.00046
U
0.0010
mg/kg wet
1,2-Dichlorobenzene
0.00027
U
0.0010
mg/kg wet
1,2-Dichloroethane
0.00041
U
0.0010
mg/kg wet
1,2-Dichloropropane
0.00026
U
0.0010
mg/kg wet
1,3,5-Trimethylbenzene
0.00020
U
0.0010
mg/kg wet
1,3-Dichlorobenzene
0.00022
U
0.0010
mg/kg wet
1,3-Dichloropropane
0.00029
U
0.0010
mg/kg wet
1,4-Dichlorobenzene
0.00020
U
0.0010
mg/kg wet
2,2-Dichloropropane
0.00023
U
0.0010
mg/kg wet
2-Butanone
0.00078
U
0.0050
mg/kg wet
2-Chloroethyl Vinyl Ether
0.00016
U
0.0050
mg/kg wet
2-Chlorotoluene
0.00018
U
0.0010
mg/kg wet
2-Hexanone
0.00075
U
0.0050
mg/kg wet
4-Chlorotoluene
0.00026
U
0.0010
mg/kg wet
4-Isopropyltoluene
0.00016
U
0.0010
mg/kg wet
4-Methyl-2-pentanone
0.00057
U
0.0050
mg/kg wet
Acetone
0.014
U
0.020
mg/kg wet
Benzene
0.00017
U
0.0010
mg/kg wet
Bromobenzene
0.00022
U
0.0010
mg/kg wet
Bromochloromethane
0.00041
U
0.0010
mg/kg wet
Bromodichloromethane
0.00024
U
0.0010
mg/kg wet
Bromoform
0.00045
U
0.0010
mg/kg wet
Bromomethane
0.00032
U
0.0010
mg/kg wet
Carbon disulfide
0.00039
U
0.0050
mg/kg wet
Carbon Tetrachloride
0.00022
U
0.0010
mg/kg wet
Chlorobenzene
0.00017
U
0.0010
mg/kg wet
Chloroethane
0.00025
U
0.0010
mg/kg wet
Chloroform
0.00018
U
0.0010
mg/kg wet
Chloromethane
0.00021
U
0.0010
mg/kg wet
cis- 1,2-Dichloroethene
0.00023
U
0.0010
mg/kg wet
Source %REC
Result %REC Limits
RPD
RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 55 Of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9JO3011 - EPA 5030E MS - Continued
Blank (9103011-BLK3) Continued Prepared: 10/03/2019 09:45 Analyzed: 10/03/2019 14:49
Spike
Analvte
Result
Flaq
POL
Units Level
cis- 1,3-Dichloropropene
0.00017
U
0.0010
mg/kg wet
Dibromochloromethane
0.00035
U
0.0010
mg/kg wet
Dibromomethane
0.00033
U
0.0010
mg/kg wet
Dichlorodifluoromethane
0.00045
U
0.0010
mg/kg wet
Ethylbenzene
0.00020
U
0.0010
mg/kg wet
Hexachlorobutadiene
0.00035
U
0.0010
mg/kg wet
Isopropyl Ether
0.00018
U
0.0010
mg/kg wet
Isopropyl benzene
0.00015
U
0.0010
mg/kg wet
m,p-Xylenes
0.00037
U
0.0020
mg/kg wet
Methylene Chloride
0.00073
U
0.0020
mg/kg wet
Methyl-tert-Butyl Ether
0.00030
U
0.0010
mg/kg wet
Naphthalene
0.00027
U
0.0010
mg/kg wet
n-Butyl Benzene
0.00013
U
0.0010
mg/kg wet
n-Propyl Benzene
0.00018
U
0.0010
mg/kg wet
o-Xylene
0.00022
U
0.0010
mg/kg wet
sec-Butylbenzene
0.00095
U
0.0010
mg/kg wet
Styrene
0.00098
U
0.0010
mg/kg wet
tert-Butyl benzene
0.00017
U
0.0010
mg/kg wet
Tetrachloroethene
0.00028
U
0.0010
mg/kg wet
Toluene
0.00024
U
0.0010
mg/kg wet
trans-1,2-Dichloroethene
0.00037
U
0.0010
mg/kg wet
trans-1,3-Dichloropropene
0.00039
U
0.0010
mg/kg wet
Trichloroethene
0.00032
U
0.0010
mg/kg wet
Trichlorofluoromethane
0.00026
U
0.0010
mg/kg wet
Vinyl chloride
0.00024
U
0.0010
mg/kg wet
Xylenes (Total)
0.00056
U
0.0030
mg/kg wet
Source %REC RPD
Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 39
ug/L
50.0 77 50-127
Dibromofluoromethane 40
u9/L
50.0 80 52-128
Toluene-d8 33
u91L
50.0 66 57-124
LCS (9303011-BS1)
Prepared: 10/03/2019 09:45 Analyzed: 10/03/2019 12:43
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.020
0.0010
mg/kg wet
0.0200
98
64-133
Benzene
0.022
0.0010
mg/kg wet
0.0200
108
79-129
Chlorobenzene
0.020
0.0010
mg/kg wet
0.0200
98
79-121
Toluene
0.021
0.0010
mg/kg wet
0.0200
103
77-120
Trichloroethene
0.021
0.0010
mg/kg wet
0.0200
107
78-120
4-Bromofluorobenzene
38
u91L
50.0
75
50-127
Dibromofluoromethane
39
u91L
50.0
78
52-128
Toluene-d8
33
u9/L
50.0
67
57-124
Matrix Spike (9703011-MS3)
Prepared: 10/03/2019 09:45 Analyzed: 10/03/2019 13:15
Source: CC16S89-07
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
0.020
0.0010
mg/kg wet
0.0200
0.00030 U
99
64-133
Benzene
0.021
0.0010
mg/kg wet
0.0200
0.00017 U
106
79-129
Chlorobenzene
0.019
0.0010
mg/kg wet
0.0200
0.00017 U
97
79-121
FINAL
This report relates only to the sample as received by the
laboratory, and
may only be reproduced
in
full.
Page 56 Of 65

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9JO3011 - EPA 5030E MS - Continued
Matrix Spike (9303011-MS3) Continued
Prepared: 10/03/2019 09:45 Analyzed: 10/03/2019 13:15
Source: CC16589-07
Spike
Source
%REC RPD
Analvte Result Flaq
POL Units
Level
Result %REC
Limits RPD Limit Notes
Toluene 0.021
0.0010 mg/kg wet
0.0200
0.00024 U 103
77-120
Trichloroethene 0.021
0.0010 mg/kg wet
0.0200
0.00032 U 103
78-120
4-Bromofluorobenzene
39
u91L
50.0
78
50-127
Dibromofluoromethane
39
u91L
50.0
79
52-128
Toluene-d8
33
u91L
50.0
66
57-124
Matrix Spike Dup (9303011-MSD1)
Prepared: 10/03/2019 09:45 Analyzed: 10/03/2019 13:46
Source: CC16589-07
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
0.022
0.0010
mg/kg wet
0.0200
0.00030 U
108
64-133
9
23
Benzene
0.023
0.0010
mg/kg wet
0.0200
0.00017 U
116
79-129
10
23
Chlorobenzene
0.021
0.0010
mg/kg wet
0.0200
0.00017 U
104
79-121
7
25
Toluene
0.023
0.0010
mg/kg wet
0.0200
0.00024 U
113
77-120
9
23
Trichloroethene
0.023
0.0010
mg/kg wet
0.0200
0.00032 U
115
78-120
11
24
4-Bromofluorobenzene 38 u91L 50.0 76 50-127
Dibromofluoromethane 40 u91L 50.0 79 52-128
Toluene-d8 34 u91L 50.0 67 57-124
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9120004 - EPA 3510C MS
Blank (9I20004-BLK1) Prepared: 09/20/2019 08:54 Analyzed: 09/23/2019 17:34
Spike Source %REC
Analvte
Result
Flaq
POL
Units Level Result %REC Limits
1,2,4-Trichlorobenzene
2.5
U
10
ug/L
1,2-Dichlorobenzene
2.5
U
10
ug/L
1,3-Dichlorobenzene
2.5
U
10
ug/L
1,4-Dichlorobenzene
2.4
U
10
ug/L
1- Methyl naphthalene
2.7
U
10
ug/L
2,4,5-Trichlorophenol
2.5
U
10
ug/L
2,4,6-Trichlorophenol
2.6
U
10
ug/L
2,4-Dichlorophenol
2.6
U
10
ug/L
2,4-Di methyl phenol
2.3
U
10
ug/L
2,4-Dinitrophenol
2.6
U
10
ug/L
2,4-Dinitrotoluene
2.6
U
10
ug/L
2,6-Dinitrotoluene
2.5
U
10
ug/L
2-Chloronaphthalene
2.8
U
10
ug/L
2-Chlorophenol
2.2
U
10
ug/L
2-Methyl-4,6-dinitrophenol
3.3
U
10
ug/L
2- Methyl naphthalene
2.8
U
10
ug/L
2-Methylphenol
2.0
U
10
ug/L
2-Nitroaniline
2.5
U
10
ug/L
2-Nitrophenol
1.1
U
10
ug/L
3 & 4-Methylphenol
2.1
U
10
ug/L
3,3'-Dichlorobenzidine
3.5
U
10
ug/L
3-Nitroaniline
2.6
U
10
ug/L
4-Bromophenyl-phenylether
2.4
U
10
ug/L
4-Chloro-3-methylphenol
2.4
U
10
ug/L
FINAL
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full.
RPD
RPD Limit Notes
Page 57 of 65

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9120004 - EPA 3510C MS - Continued
Blank (9I20004-BLKI) Continued Prepared: 09/20/2019 08:54 Analyzed: 09/23/2019 17:34
Spike
Analvte
Result
Flag
POL
Units Level
4-Chloroaniline
2.0
U
10
ug/L
4-Chlorophenyl-phenylether
2.6
U
10
ug/L
4-Nitroaniline
3.2
U
10
ug/L
4-Nitrophenol
2.8
U
10
ug/L
Acenaphthene
2.7
U
10
ug/L
Acenaphthylene
2.6
U
10
ug/L
Anthracene
2.4
U
10
ug/L
Benzidine
1.6
U
10
ug/L
Benzo(a)anthracene
2.4
U
10
ug/L
Benzo(a)pyrene
2.2
U
10
ug/L
Benzo(b)fluoranthene
2.8
U
10
ug/L
Benzo(g,h,i)perylene
2.4
U
10
ug/L
Benzo(k)fluoranthene
2.4
U
10
ug/L
Benzoic acid
1.0
U
50
ug/L
Benzyl alcohol
2.4
U
10
ug/L
Bis(2-chloroethoxy)methane
2.4
U
10
ug/L
Bis(2-chloroethyl)ether
2.6
U
10
ug/L
Bis(2-chloroisopropyl)ether
2.5
U
10
ug/L
Bis(2-ethylhexyl)phthalate
1.9
U
5.0
ug/L
Butylbenzylphthalate
3.8
U
10
ug/L
Chrysene
2.2
U
10
ug/L
Dibenzo(a,h)anthracene
2.3
U
10
ug/L
Dibenzofuran
2.6
U
10
ug/L
Diethylphthalate
2.4
U
10
ug/L
Dimethylphthalate
2.5
U
10
ug/L
Di-n-butylphthalate
2.8
U
10
ug/L
Di-n-octylphthalate
3.1
U
10
ug/L
Fluoranthene
3.1
U
10
ug/L
Fluorene
2.5
U
10
ug/L
Hexachlorobenzene
2.3
U
10
ug/L
Hexachlorobutadiene
2.8
U
10
ug/L
Hexachlorocyclopentadiene
2.7
U
10
ug/L
Hexachloroethane
2.6
U
10
ug/L
Indeno(1,2,3-cd)pyrene
2.2
U
10
ug/L
Isophorone
2.5
U
10
ug/L
Naphthalene
2.8
U
10
ug/L
Nitrobenzene
2.5
U
10
ug/L
N-Nitrosodimethylamine
1.9
U
10
ug/L
N-Nitroso-di-n-propylamine
2.3
U
10
ug/L
N-nitrosodiphenylamine/Diphenylamine
2.5
U
10
ug/L
Pentachlorophenol
2.1
U
10
ug/L
Phenanthrene
2.6
U
10
ug/L
Phenol
1.7
U
10
ug/L
Pyrene
3.5
U
10
ug/L
Pyridine
2.2
U
10
ug/L
Source %REC RPD
Result %REC Limits RPD Limit Notes
24,6-Thbromophenol
93
u9/L
100
93
10-179
2-Fluorobiphenyl
43
u9/L
50.0
86
10-149
2-Fluorophenol
58
u9/L
100
58
10-110
Nitrobenzene-d5
40
u9/L
50.0
81
10-149
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 58 Of 65

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9120004 - EPA 3510C MS - Continued
Blank (9I20004-BLKI) Continued Prepared: 09/20/2019 08:54 Analyzed: 09/23/2019 17:34
Spike Source %REC RPD
Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes
Phenol-d5 48 u9/L 100 48 10-88
Terphenyl-d14 51 u9/L 50.0 101 10-188
LCS (9I20004-BS1) Prepared: 09/20/2019 08:54 Analyzed: 09/24/2019 15:01
Spike
Source
%REC RPD
Analvte
Result Flao
POL
Units
Level
Result %REC
Limi RPD Mma Notes
1,2,4-Trichlorobenzene
35
10
ug/L
50.0
71
27-90
1,4-Dichlorobenzene
34
10
ug/L
50.0
68
23-84
2,4-Dinitrotoluene
41
10
ug/L
50.0
82
67-132
2-Chlorophenol
34
10
ug/L
50.0
69
40-109
4-Chloro-3-methylphenol
40
10
ug/L
50.0
80
58-121
4-Nitrophenol
24
10
ug/L
50.0
48
33-105
Acenaphthene
44
10
ug/L
50.0
88
39-125
N-Nitroso-di-n-propylamine
37
10
ug/L
50.0
75
48-126
Pentachlorophenol
40
10
ug/L
50.0
80
51-135
Phenol
27
10
ug/L
50.0
53
19-78
Pyrene
48
10
ug/L
50.0
97
44-137
2,4,6-Tribromophenol
95
u9/L
100 95 10-179
2-Fluorobiphenyl
45
u9/L
50.0 89 10-149
2-Fluorophenol
60
u9/L
100 60 10-110
Nitrobenzene-d5
40
u9/L
50.0 79 10-149
Phenohd5
51
u9/L
100 51 10-88
Terphenyhd14
52
u9/L
50.0 103 10-I88
Matrix Spike (9I20004-MS1)
Prepared: 09/20/2019 08:54 Analyzed: 09/23/2019 18:36
Source: CC15675-10
Spike
Source
%REC RPD
Analvte
Result Flao
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
31
10
ug/L
50.0
2.5 U
63
27-90
1,4-Dichlorobenzene
33
10
ug/L
50.0
2.4 U
66
23-84
2,4-Dinitrotoluene
43
10
ug/L
50.0
2.6 U
86
67-132
2-Chlorophenol
35
10
ug/L
50.0
2.2 U
69
40-109
4-Chloro-3-methylphenol
39
10
ug/L
50.0
2.4 U
78
58-121
4-Nitrophenol
26
10
ug/L
50.0
2.8 U
53
33-105
Acenaphthene
45
10
ug/L
50.0
2.7 U
89
39-125
N-Nitroso-di-n-propylamine
37
10
ug/L
50.0
2.3 U
74
48-126
Pentachlorophenol
39
10
ug/L
50.0
2.1 U
78
51-135
Phenol
24
10
ug/L
50.0
1.7 U
49
19-78
Pyrene
51
10
ug/L
50.0
3.5 U
103
44-137
2,4,6-Tribromophenol
99
u9/L
100
99
10-179
2-Fluorobiphenyl
44
u9/L
50.0
87
10-149
2-Fluorophenol
55
u9/L
100
55
10-110
Nitrobenzene-d5
40
u9/L
50.0
80
10-149
Phenol-d5
51
u9/L
100
51
10-88
Terphenyl-d14
54
u9/L
50.0
109
10-188
Matrix Spike Dup (9I20004-MSD1)
Prepared: 09/20/2019 08:54 Analyzed: 09/24/2019 15:31
Source: CC15675-10
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 59 Of 65

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9120004 - EPA 3510C MS - Continued
Matrix Spike Dup (9I20004-MSD3) Continued Prepared: 09/20/2019 08:54 Analyzed: 09/24/2019 15:31
Source: CC15675-10
Spike
Source
%REC
RPD
Analvte
Result Flao
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,2,4-Trichlorobenzene
34
10
ug/L
50.0
2.5 U
67
27-90
7
43
1,4-Dichlorobenzene
32
10
ug/L
50.0
2.4 U
65
23-84
3
39
2,4-Dinitrotoluene
45
10
ug/L
50.0
2.6 U
91
67-132
5
17
2-Chlorophenol
29
10
ug/L
50.0
2.2 U
57
40-109
19
22
4-Chloro-3-methylphenol
42
10
ug/L
50.0
2.4 U
84
58-121
8
22
4-Nitrophenol
30
10
ug/L
50.0
2.8 U
61
33-105
14
27
Acenaphthene
41
10
ug/L
50.0
2.7 U
83
39-125
8
25
N-Nitroso-di-n-propylamine
40
10
ug/L
50.0
2.3 U
81
48-126
9
23
Pentachlorophenol
45
10
ug/L
50.0
2.1 U
91
51-135
15
11 QM-11
Phenol
22
10
ug/L
50.0
1.7 U
43
19-78
12
18
Pyrene
49
10
ug/L
50.0
3.5 U
99
44-137
4
24
2,4,6-Tribromophenol
110
u9/L
100
111
10-179
2-Fluorobiphenyl
51
u9/L
50.0
103
10-149
2-Fluorophenol
46
u9/L
100
46
10-110
Nitrobenzene-d5
41
u9/L
50.0
83
10-149
Phenol-d5
46
u9/L
100
46
10-88
Terphenyl-d14
52
u9/L
50.0
104
10-188
Batch 9123028 - SOP EXSV-33
Blank (9I23028-BLKI)
Prepared: 09/23/2019 14:03 Analyzed: 09/24/2019 16:32
Spike Source %REC RPD
Analvte
Result
Flag
POL
Units Level Result %REC Limi RPD Limit Notes
1,2,4-Trichlorobenzene
0.026
U
0.33
mg/kg wet
1,2-Dichlorobenzene
0.023
U
0.33
mg/kg wet
1,3-Dichlorobenzene
0.020
U
0.33
mg/kg wet
1,4-Dichlorobenzene
0.021
U
0.33
mg/kg wet
1-Methylnaphthalene
0.027
U
0.33
mg/kg wet
2,4,5-Trichlorophenol
0.027
U
0.33
mg/kg wet
2,4,6-Trichlorophenol
0.027
U
0.33
mg/kg wet
2,4-Dichlorophenol
0.024
U
0.33
mg/kg wet
2,4-Dimethylphenol
0.043
U
0.33
mg/kg wet
2,4-Dinitrophenol
0.043
U
0.33
mg/kg wet
2,4-Dinitrotoluene
0.028
U
0.33
mg/kg wet
2,6-Dinitrotoluene
0.031
U
0.33
mg/kg wet
2-Chloronaphthalene
0.028
U
0.33
mg/kg wet
2-Chlorophenol
0.025
U
0.33
mg/kg wet
2-Methyl-4,6-dinitrophenol
0.033
U
0.33
mg/kg wet
2-Methylnaphthalene
0.028
U
0.33
mg/kg wet
2-Methylphenol
0.025
U
0.33
mg/kg wet
2-Nitroaniline
0.030
U
0.33
mg/kg wet
2-Nitrophenol
0.031
U
0.33
mg/kg wet
3 & 4-Methylphenol
0.026
U
0.33
mg/kg wet
3,3'-Dichlorobenzidine
0.098
U
0.33
mg/kg wet
3-Nitroaniline
0.036
U
0.33
mg/kg wet
4-Bromophenyl-phenylether
0.027
U
0.33
mg/kg wet
4-Chloro-3-methylphenol
0.033
U
0.33
mg/kg wet
4-Chloroaniline
0.093
U
0.33
mg/kg wet
4-Chlorophenyl-phenylether
0.026
U
0.33
mg/kg wet
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 60 Of 65

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9123028 - SOP EXSV-33 - Continued
Blank (9I23028-BLKI) Continued Prepared: 09/23/2019 14:03 Analyzed: 09/24/2019 16:32
Spike
Analvte
Result
Flag
POL
Units Level
4-Nitroaniline
0.053
U
0.33
mg/kg wet
4-Nitrophenol
0.031
U
0.33
mg/kg wet
Acenaphthene
0.028
U
0.33
mg/kg wet
Acenaphthylene
0.028
U
0.33
mg/kg wet
Anthracene
0.038
U
0.33
mg/kg wet
Benzidine
0.11
U
0.33
mg/kg wet
Benzo(a)anthracene
0.028
U
0.33
mg/kg wet
Benzo(a)pyrene
0.033
U
0.33
mg/kg wet
Benzo(b)fluoranthene
0.018
U
0.33
mg/kg wet
Benzo(g,h,i)perylene
0.047
U
0.33
mg/kg wet
Benzo(k)fluoranthene
0.033
U
0.33
mg/kg wet
Benzoic acid
0.15
U
1.7
mg/kg wet
Benzyl alcohol
0.023
U
0.33
mg/kg wet
Bis(2-chloroethoxy)methane
0.025
U
0.33
mg/kg wet
Bis(2-chloroethyl)ether
0.043
U
0.33
mg/kg wet
Bis(2-chloroisopropyl)ether
0.024
U
0.33
mg/kg wet
Bis(2-ethylhexyl)phthalate
0.035
U
0.33
mg/kg wet
Butylbenzylphthalate
0.040
U
0.33
mg/kg wet
Chrysene
0.030
U
0.33
mg/kg wet
Dibenzo(a,h)anthracene
0.051
U
0.33
mg/kg wet
Dibenzofuran
0.027
U
0.33
mg/kg wet
Diethylphthalate
0.028
U
0.33
mg/kg wet
Dimethylphthalate
0.033
U
0.33
mg/kg wet
Di-n-butylphthalate
0.041
U
0.33
mg/kg wet
Di-n-octylphthalate
0.033
U
0.33
mg/kg wet
Fluoranthene
0.036
U
0.33
mg/kg wet
Fluorene
0.029
U
0.33
mg/kg wet
Hexachlorobenzene
0.026
U
0.33
mg/kg wet
Hexachlorobutadiene
0.026
U
0.33
mg/kg wet
Hexachlorocyclopentadiene
0.039
U
0.33
mg/kg wet
Hexachloroethane
0.021
U
0.33
mg/kg wet
Indeno(1,2,3-cd)pyrene
0.047
U
0.33
mg/kg wet
Isophorone
0.030
U
0.33
mg/kg wet
Naphthalene
0.028
U
0.33
mg/kg wet
Nitrobenzene
0.026
U
0.33
mg/kg wet
N-Nitrosodimethylamine
0.021
U
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
0.081
U
0.33
mg/kg wet
N-nitrosodiphenylamine/Diphenylamine
0.054
U
0.33
mg/kg wet
Pentachlorophenol
0.033
U
0.33
mg/kg wet
Phenanthrene
0.027
U
0.33
mg/kg wet
Phenol
0.022
U
0.33
mg/kg wet
Pyrene
0.038
U
0.33
mg/kg wet
Pyridine
0.082
U
0.33
mg/kg wet
Source %REC
Result %REC Limits
2,4,6-Tribromophenol
3.2
mg/kg wet
3.33
96
28-130
2-Fluorobiphenyl
1.6
mg/kg wet
1.67
98
56-120
2-Fluorophenol
2.9
mg/kg wet
3.33
87
49-126
Nitrobenzene-d5
1.5
mg/kg wet
1.67
91
50-117
Phenol-d5
3.1
mg/kg wet
3.33
94
56-120
TerphenyhdM
1.6
mg/kg wet
1.67
93
36-151
RPD
RPD Limit Notes
QV-01
QV-01
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 61 Of 65

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9123028 - SOP EXSV-33 - Continued
LCS (9I23028-BSI) Prepared: 09/23/2019 14:03 Analyzed:09/24/2019 17:03
Spike
Source
%REC RPD
Analvte
Result Flaa
POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
1.5
0.33
mg/kg wet
1.67
90
51-121
1,4-Dichlorobenzene
1.5
0.33
mg/kg wet
1.67
92
48-118
2,4-Dinitrotoluene
1.6
0.33
mg/kg wet
1.67
99
63-127
2-Chlorophenol
1.4
0.33
mg/kg wet
1.67
85
56-120
4-Chloro-3-methylphenol
1.6
0.33
mg/kg wet
1.67
93
59-121
4-Nitrophenol
1.4
0.33
mg/kg wet
1.67
86
73-147
Acenaphthene
1.7
0.33
mg/kg wet
1.67
100
64-131
N-Nitroso-di-n-propylamine
1.4
0.33
mg/kg wet
1.67
86
55-135
Pentachlorophenol
1.5
0.33
mg/kg wet
1.67
90
45-117
Phenol
1.6
0.33
mg/kg wet
1.67
98
54-121
Pyrene
1.7
0.33
mg/kg wet
1.67
103
65-146
2,4,6-Tribromophenol
3.7
mg/kg wet
3.33
111
28-130
2-Fluorobiphenyl
1.7
mg/kg wet
1.67
102
56-120
2-Fluorophenol
3.0
mg/kg wet
3.33
90
49-126
Nitrobenzene-d5
1.6
mg/kg wet
1.67
93
50-117
Phenol-d5
3.2
mg/kg wet
3.33
97
56-120
Terphenyl-d14
1.8
mg/kg wet
1.67
110
36-151
Matrix Spike (9I23028-MSI)
Prepared: 09/23/2019 14:03 Analyzed: 09/25/2019 16:13
Source: CC16129-09
Spike
Source
%REC RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
1.5
JD
1.9
mg/kg dry
1.95
0.15 U
75
51-121
1,4-Dichlorobenzene
1.5
JD
1.9
mg/kg dry
1.95
0.12 U
76
48-118
2,4-Dinitrotoluene
1.5
JD
1.9
mg/kg dry
1.95
0.16 U
76
63-127
2-Chlorophenol
1.3
JD
1.9
mg/kg dry
1.95
0.15 U
68
56-120
4-Chloro-3-methylphenol
1.3
JD
1.9
mg/kg dry
1.95
0.19 U
68
59-121
4-Nitrophenol
1.9
D
1.9
mg/kg dry
1.95
0.18 U
96
73-147
Acenaphthene
1.7
JD
1.9
mg/kg dry
1.95
0.16 U
87
64-131
N-Nitroso-di-n-propylamine
1.4
JD
1.9
mg/kg dry
1.95
0.47 U
74
55-135
Pentachlorophenol
2.2
D
1.9
mg/kg dry
1.95
0.19 U
113
45-117
Phenol
1.3
JD
1.9
mg/kg dry
1.95
0.13 U
68
54-121
Pyrene
1.8
JD
1.9
mg/kg dry
1.95
0.22 U
94
65-146
2,4,6-Tribromophenol
2.9
mg/kg dry
3.91
73
28-130
2-Fluorobiphenyl
1.5
mg/kg dry
1.95
79
56-120
2-Fluorophenol
2.6
mg/kg dry
3.91
67
49-126
Nitrobenzene-d5
1.5
mg/kg dry
1.95
75
50-117
Phenohd5
2.9
mg/kg dry
3.91
74
56-120
Terphenyhd14
1.6
mg/kg dry
1.95
82
36-151
Matrix Spike Dup (9I23028-MSD1)
Prepared: 09/23/2019 14:03 Analyzed: 09/25/2019 16:43
Source: CC16129-09
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,2,4-Trichlorobenzene
1.5
JD
1.9
mg/kg dry
1.95
0.15 U
79
51-121
5
10
1,4-Dichlorobenzene
1.6
JD
1.9
mg/kg dry
1.95
0.12 U
81
48-118
7
13
2,4-Dinitrotoluene
1.6
JD
1.9
mg/kg dry
1.95
0.16 U
81
63-127
6
10
2-Chlorophenol
1.4
JD
1.9
mg/kg dry
1.95
0.15 U
73
56-120
7
11
4-Chloro-3-methylphenol
1.3
JD
1.9
mg/kg dry
1.95
0.19 U
69
59-121
2
10
4-Nitrophenol
2.0
D
1.9
mg/kg dry
1.95
0.18 U
100
73-147
4
10
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be
reproduced in
full.
Page 62 Of 65

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 9123028 - SOP EXSV-33 - Continued
Matrix Spike Dup (9I23028-MSD3) Continued
Prepared: 09/23/2019 14:03 Analyzed: 09/25/2019 16:43
Source: CC16129-09
Spike
Source
%REC
RPD
Analvte Result Flaa
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Acenaphthene 1.8 JD
1.9
mg/kg dry
1.95
0.16 U
91
64-131
5
19
N-Nitroso-di-n-propylamine 1.5 JD
1.9
mg/kg dry
1.95
0.47 U
79
55-135
6
10
Pentachlorophenol 2.3 D
1.9
mg/kg dry
1.95
0.19 U
118
45-117
4
10 QM-07
Phenol 1.4 JD
1.9
mg/kg dry
1.95
0.13 U
71
54-121
5
13
Pyrene 1.9 D
1.9
mg/kg dry
1.95
0.22 U
97
65-146
3
50
2,4,6-Tribromophenol
3.0
mg/kg dry
3.91
76
28-130
2-Fluorobiphenyl
1.7
mg/kg dry
1.95
66
56-120
2-Fluorophenol
2.8
mg/kg dry
3.91
73
49-126
Nitrobenzene-d5
1.6
mg/kg dry
1.95
82
50-117
Phenol-d5
3.1
mg/kg dry
3.91
80
56-I20
Terphenyl-d14
1.7
mg/kg dry
1.95
89
36-151
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 63 Of 65

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
QV-02 The associated continuing calibration verification standard exhibited low bias; the reported result should
be considered to be a minimum estimate.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 64 of 65

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