22002_Overture Cary_PIIR_2019425

Mid Atlantic
Engineering & Environmental Solutions
April 25, 2019
Mr. Kelly Johnson, LG
NC Brownfields Program
NC Department of Environmental Quality
Division of Waste Management
Mail Service Center 1646
Raleigh, NC 27699-1646
Reference: PHASE II ENVIRONMENTAL SITE ASSESSMENT
CARY OVERTURE SITE
3612 & 3624 DAVIS DRIVE
CARY / MORRISVILLE, WAKE COUNTY, NORTH CAROLINA
BROWNFIELD PROJECT NO.: 22002-18-092
MID -ATLANTIC PROJECT NO.: OOOR3021.01
Dear Mr. Johnson:
409 Rogers View Court
Raleigh. NC 27610
office 919.250.9918
facsimile 919.250.9950
MAAONLINE.COM
On behalf of CRP-GREP AA Overture Cary, LLC, we are pleased to present this Phase
II Environmental Site Assessment for the above -referenced site. Please contact me at
919-250-9918 if any questions arise.
Sincerely,
MID -ATLANTIC ASSOCIATES, INC.
Daniel H. Nielsen, PE
Principal Engineer
Enclosure
EXPERIENCED CUSTOMER FOCUSED INNOVATIVE

PHASE II ENVIRONMENTAL SITE ASSESSMENT
CARY OVERTURE SITE
3612 & 3624 DAVIS DRIVE
CARY / MORRISVILLE, WAKE COUNTY, NORTH CAROLINA
BROWNFIELD PROJECT NO.: 22002-18-092
Prepared For:
Mr. Robert Morgan
CRP-GREP AA Overture Cary, LLC
465 Meeting Street
Charleston, SC 29403
Prepared By:
Mid -Atlantic Associates, Inc.
409 Rogers View Court
Raleigh, North Carolina 27610
Mid -Atlantic Job No. OOOR3021.01
April 25, 2019
Mid Atlantic
�� Engineering & EnvwonMental SoiuLlOnS

Mid Atlantic
Engineering & Environmental Solutions
409 Rogers View Court
Raleigh, NC 27610
office 919.250.9918
facsimile 919.250.9950
MAAONLINE.COM
PHASE II ENVIRONMENTAL SITE ASSESSMENT
CARY OVERTURE SITE
3612 & 3624 DAVIS DRIVE
CARY / MORRISVILLE, WAKE COUNTY, NORTH CAROLINA
BROWNFIELD PROJECT NO.: 22002-18-092
Mid -Atlantic Associates Job No. OOOR3021.01
Prepared For:
CRP-GREP AA Overture Cary, LLC
465 Meeting Street,
Charleston, South Carolina 29403
April 25, 2019
Prepared By:
MID -ATLANTIC ASSOCIATES, INC.
Ruth Tull
Staff Scientist
UAL
Daniel H. iel n, 9
Principal E
EXPERIENCED CUSTOMER FOCUSED INNOVATIVE

TABLE OF CONTENTS
1.0 INTRODUCTION.....................................................................................................1
2.0 SUMMARY OF FIELD ACTIVITIES........................................................................ 2
2.1 Sampling Location Siting...................................................................................... 2
2.2 Soil Boring and Sampling..................................................................................... 2
2.3 Monitoring Well Installation and Sampling............................................................ 3
3.0 SUMMARY OF LABORATORY ANALYTICAL RESULTS....................................3
3.1 Soil Analytical Data...............................................................................................4
3.2 Groundwater Analytical Data................................................................................ 5
4.0 CONCLUSIONS AND RECOMMENDATIONS....................................................... 5
DRAWINGS
Drawing 1.1
Topographic Site Map
Drawing 2.1
Sample Location Map
Drawing 2.2
Former AST Area Sample Location Map
TABLE
Table 3.1 Summary of Chemical Constituents Detected in Soil
APPENDICES
Appendix A Boring Logs
Appendix B Laboratory Report and Chain of Custody Record for Soil &
Groundwater Samples
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1.0 INTRODUCTION
The subject site is comprised of two parcels totaling 7.19 acres (Drawing 1.1) located in
a generally residential and commercial/retail area in Morrisville/Cary, Wake County, North
Carolina. The site was formerly used as a residence and is currently developed with one
vacant residential structure and one cellular tower with supporting infrastructure.
Land use at the subject site has been confirmed by aerial photographs back to 1949,
when the northern portion of the site was used for agricultural purposes. The remainder
of the subject site has been largely agricultural or undeveloped until a residential structure
was added in 1957 and a cell tower was constructed by approximately 2002. This
telecommunications tower is located near the eastern property boundary within a fenced,
restricted facility that is subject to a long-term lease with the property owner.
Mid -Atlantic completed a Phase I Environmental Site Assessment (PESA) for the subject
site in December 2017 and during this assessment Mid -Atlantic noted evidence of a
former above ground storage tank (AST) at the rear of the vacant house on the subject
site which had likely contained heating oil. The former property owner, Mr. Wong,
confirmed the former presence of a heating oil AST. Staining on the support structures
for the AST and on the rear wall of the house suggested the possibility of a release. Mid -
Atlantic collected and tested three soil samples behind the house in the vicinity of the
former heating oil AST, and produced the Letter Report of Soil Sampling Results, 3612
Davis Drive. The report, produced in November 2017 confirmed the release of petroleum
contaminants but did not define the extent of impact.
As part of the purchase and re -purposing of the site, CRP-GREP AA Overture Cary, LLC
intends to obtain a Brownfields Agreement (BFA) under the North Carolina Brownfields
Program. CRP-GREP AA Overture Cary, LLC contracted with Mid -Atlantic to perform
additional assessment at the subject site. Mid -Atlantic developed a Phase 11 Work Plan
outlining soil and groundwater sampling activities designed to address the data gaps
identified by the Brownfield Program. This Work Plan was submitted to the Brownfields
Program on February 18, 2019 and approved by the Program on February 27, 2019. The
Phase II Work Plan proposed assessment of soil and groundwater in the vicinity of the
former heating oil AST, the assessment of soil in the vicinity of two observed debris piles,
and the assessment of soil and groundwater in the vicinity of the cellular tower and
associated emergency generators.
The opinions included herein are based on our experience and the information obtained
during the study. This report is based on limited observations made on the dates noted
using the procedures described herein. If additional information becomes available, we
request the opportunity to review the information, reassess the potential environmental
concerns and modify our conclusions and recommendations, if appropriate.
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Phase 11 Environmental Site Assessment Report April 25, 2019
Cary Overture Page 2
3612 & 3624 Davis Drive
Cary/Morrisville, North Carolina
2.0 SUMMARY OF FIELD ACTIVITIES
2.1 Sampling Location Siting
Mid -Atlantic identified five sampling locations as discussed in the Work Plan: the former
location of heating oil AST on the back wall of the vacant house to assess petroleum release
impacts; vicinity of the cellular tower to evaluate for the presence of contamination
associated with facility operations; the locations of two debris piles to evaluate for potential
release(s) of contaminates to the environment; and a background sample to evaluate
naturally occurring metals concentrations in the local soil.
On April 8, 2019 Mid -Atlantic marked the proposed soil boring and temporary monitoring
well locations at the subject site. Additionally, as specified in the Work Plan, soil boring
locations SB-1 through SB-3 and temporary monitoring well TMW-1 were chosen in the field
around the former heating oil AST area using visual observation of the surrounding ground
conditions. Boring SB-4 and TMW-2 had intended to be downgradient of the cellular tower
emergency generators, as specified by the Work Plan; however, despite three relocation
attempts, TMW-2 could not be installed due to auger refusal before reaching groundwater.
Borings SB-5 and SB-6 were placed in areas of observed household debris piles. Boring
BG-1 was placed in an undeveloped wooded area in order to analyze a representative
background soil sample. Sample locations are shown on Drawing 2.1.
On April 15, 2019, private utilities were located and marked by KCI Associates of North
Carolina (KCI) in the areas of the proposed sampling locations. Several of the original site
locations were not accessible with the Geoprobe and were either collected with a hand
auger or relocated. The final locations of the soil borings and monitoring wells were placed
to avoid the marked utilities and to be situated as close to the proposed sampling locations
as could safely be managed. Mid -Atlantic does not anticipate that the relocation of these soil
borings impacts the findings of this report.
2.2 Soil Boring and Sampling
On April 15, 2019, under the supervision of Mid -Atlantic, Quantex Inc. (Quantex) used a
Geoprobe 7822DT to advance seven soil borings at the designated locations (Drawing
2.1). Each boring was advanced using decontaminated equipment. Soil samples were
collected via 5-foot macrocores for soil characterization and laboratory analysis. Soil was
screened for the presence of volatile organic compounds (VOCs) using a Toxic Vapor
Analyzer (TVA) 1000 photo ionization detector and flame ionization detector (PID/FID) in
accordance with the procedures described in the Work Plan. Boring logs are provided in
Appendix A.
Mid Atlantic
Engineering & Environmental Solutions

Phase 11 Environmental Site Assessment Report
Cary Overture
3612 & 3624 Davis Drive
Cary/Morrisville, North Carolina
April 25, 2019
Page 3
Seven soil samples from various depths were collected for laboratory analysis of VOCs,
semi-VOCs (SVOCs), and RCRA Metals. Soil samples were shipped to Prism Laboratories,
Inc. (Prism) in Charlotte, North Carolina for laboratory analysis as shown on the chain of
custody record provided in Appendix B.
2.3 Monitoring Well Installation and Sampling
On April 15, 2019, Quantex installed one temporary monitoring well, TWM-1, using 5-inch
solid stem augers, at the location proposed in the Work Plan. The work was conducted
under the supervision of a Mid -Atlantic field technician. The temporary well was constructed
to 40 feet below ground surface with 2-inch diameter Schedule 40 PVC and 20 feet of well
screen (as shown on the boring log provided in Appendix A). The well was developed
upon completion using dedicated disposable bailers to remove particulates from the water
column and improve the hydraulic connection between the aquifer and the well.
Mid -Atlantic's technician sampled the temporary well and collected a water level
measurement of 33.20 feet below land surface. The groundwater sample was shipped to
Prism for laboratory analysis of VOCs, SVOCs, and metals as shown on the chain of custody
record provided in Appendix B. Following sampling activities, the temporary well was
abandoned by Quantex on April 15, 2019.
A second temporary monitoring well, TMW-2, was specified in the Work Plan. However,
the well boring for TMW-2 was relocated three times with auger refusal occurring from 4.5
to 7 feet below land surface on each event. These depths did not extend to below the
estimated depth to groundwater and prevented the installation of temporary monitoring well
TMW-2.
K��=•'i�1Jil►vi/_1:YK912 W_1 1167:7_%1101 X/_1, /_1 WA 1 [07_1 N:1=[ 91 N &'
Depths of grab and composite soil samples collected for the assessment of soil are shown
on Table 3.1. The laboratory analytical report and chain of custody record for the soil
samples and groundwater samples are provided in Appendix B. The test results for soil
samples were compared to the Unrestricted Health Based Preliminary Soil Remediation
Goals (PSRGs), the Protection of Groundwater PSRGs, and the Industrial PSRGs.
Groundwater samples were compared to the North Carolina Groundwater Quality
Standards (NCGQS).
Mid Atlantic
Engineering & Environmental Solubons

Phase 11 Environmental Site Assessment Report April 25, 2019
Cary Overture Page 4
3612 & 3624 Davis Drive
Cary/Morrisville, North Carolina
3.1 Soil Analytical Data
As summarized in Table 3.1, two VOCs were detected in five of the seven soil samples
tested. These compounds were detected at estimated concentrations below the PSRGs.
Acetone, one of the two compounds detected, is a common laboratory artifact.
Of the six soil samples tested for the presence of SVOCs, one sample (SB-6) exhibited
detectable concentrations. This sample, collected near a debris pile, exhibited six
polynuclear aromatic hydrocarbons at estimated concentration below the PSRGs.
Seven soil samples, including the background sample, were tested for the eight RCRA
metals. Arsenic was detected above the Unrestricted Health Based PSRG in five of these
samples.
The Industrial PSRG was exceeded in two samples including the background sample.
Arsenic is a metal that is found naturally occurring in North Carolina soils. According to
the North Carolina Department of Agriculture and Consumer Services (NCDA), an
average concentration of 4.5 mg/Kg of arsenic was detected in laboratory testing of 3,286
soil samples collected across North Carolina between 2005 and 2007 (NCDA, 2008).
Furthermore, the EPA notes that arsenic concentrations typically range from 4 to 9 mg/Kg
in most soils (EPA, 2003). According to the laboratory analysis, the arsenic
concentrations detected in the soil samples collected from the subject site fall within levels
believed to be found naturally in North Carolina soils.
Chromium was detected in each soil sample tested at a concentration below the PSRG
for chromium 111 but above the PSRG for chromium VI. Chromium III is commonly naturally
occurring while the presence of chromium VI is typically associated with industrial
activities (metal fabrication/cutting, plating, etc.). The subject site has no history of
industrial use and therefore the chromium detected in the soil on the site is likely
chromium III. Other RCRA metals were detected at concentrations above laboratory
method detection limits but below the PSRGs.
Included in Table 3.1 are the results from hand auger soil samples collected in November
2017, which contained Total Petroleum Hydrocarbons DRO and GRO in concentrations
above Action Levels. Petroleum compounds (VOCs and SVOCs) were not identified in
soil samples collected from SB-1, SB-2 or SB-3. These borings were located
approximately 5 to 10 feet further from the source area hand auger samples previously
collected. These test results indicate the impacted soils are confined to the immediate
proximity of the former AST location. The sample locations in proximity to the former AST
location are provided in Drawing 2.2.
Mid Atlantic
Engineering & Environmental Solubons

Phase 11 Environmental Site Assessment Report April 25, 2019
Cary Overture Page 5
3612 & 3624 Davis Drive
Cary/Morrisville, North Carolina
3.2 Groundwater Analytical Data
No SVOCs were detected in groundwater sampled from TWM-1. Chloroform, the only VOC
detected above laboratory method detection limits, was detected in groundwater sampled
from TMW-1 at a concentration of 1.2 ug/L, below its NCGQS of 70 ug/L. Three metals were
detected in the sample collected from TMW-1. These metals included barium (0.38 ug/L),
chromium (0.079 ug/L), and lead (0.015 ug/L). The detected concentrations were all below
the NCGQS of 700 ug/L, 10 ug/L and 15 ug/L, respectively.
4.0 CONCLUSIONS AND RECOMMENDATIONS
The objective of this assessment was to address the data gaps defined by the Brownfield
Program. In November 2017 Mid -Atlantic conducted an assessment of soil in vicinity of a
former AST. The results of this November 2017 assessment confirmed that a release
form the AST had occurred. The soil samples collected during the April 2019 assessment
described herein did not identify the presence petroleum compounds in soil. The original
soil samples were collected in closer proximity to the former AST than samples SB-1, SB-
2 and SB-3 (as shown on Drawing 2.2). This suggests the radius of impact is within 10
feet of the former AST.
Several soil samples exhibited chromium and arsenic above the chromium VI and arsenic
PSRGs. The site does not have a history of industrial use, therefore it is Mid -Atlantic's
opinion that the chromium detected in the samples is naturally occurring chromium III.
According to the laboratory analysis, the arsenic concentrations detected in the soil
samples collected from the subject site fall within levels found naturally in North Carolina
soils. The background sample also exhibits the concentrations of arsenic and chromium,
which supports that these compounds are naturally occurring and not likely a result of a
contaminant release.
Based on review of the data collected during this and the November 2017 assessment,
Mid -Atlantic concludes:
A petroleum release has occurred at the subject site. The extent of soil
contamination is limited to the immediate vicinity of the former AST. The release
has not impacted groundwater.
There is no evidence of environmental impact associated with the cell tower or the
two household debris piles located on the subject site.
Mid -Atlantic recommends submittal of this report to the NCDEQ Brownfields Program for
review and comment.
Mid Atlantic
Engineering & Environmental Solutions

DRAWINGS
Mid Atlantic
Engineering & Environmental Solubons

a
REFERENCES:
1. CARY, NC DIGITAL RASTER GRAPHICS,
USGS. SCANNED FROM1:24,000-SCALE CARY, NC
TOPOGRAPHIC MAPS, PUBLISHED 2013, USGS.
2. INSET MAP DIGITAL DATA FROM 2002 NATIONAL TRANSPORTATION ATLAS
BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, D.C.
3. PROPERTY BOUNDARY DATA FROM WAKE COUNTY GIS.
Mid Atlantic
Engineering & Environmental Solutions
TOPOGRAPHIC SITE MAP
CARY OVERTURE
3624 & 3612 DAVIS DRIVE
CARY & MORRISVILLE,
NORTH CAROLINA
SCALE: 1:12,000
Feet
0 1,000 2,000
DRAWN DATE:
BY: EBA APRIL 2019
DRAFT JOB NO:
CHECK: OOOR3021.01
ENG. GIS NO:
CHECK: 1 G-R3021.01-1
APPROVAL: DWG NO: 1

10
FORMER AST
- -
�LG
DRO (ppm)
GRO (ppm)
1
39.8
5.1
2
1,255
209.7
3
515.9
115.2
G
8260
827Q
ND
ND
ND
ND
ND
ND
I.,. . ... 0 13L%
M
yG LEGEND
(n HANDAUGER
O SOIL BORING
i
■ SOIL BORING AND TEMPORARY WELL
O SUBJECT SITE
O PARCEL BOUNDARY
0 30 60 —
Feet
DRAWN BY: RDC DATE: APRIL 2019
FORMER AST AREA SAMPLE LOCATION MAP DRAFT CHECK
MidAtlantic OVERTURE CARY BY JOB NO.: 00OR3021.01 T35000
Engineering& Environmental Solutions 3612 & 3624 DAVIS DRIVE ENGINEER CHECK GIs NO.: 01G-R3021.01-4
MORRISVILLE, NORTH CAROLINA APPROVED DRAWING NO.: 2.2
REFERENCE: DATA FROM WAKE COUNTY COUNTY GIS. MID -ATLANTIC FIELD NOTES.

TABLE
Mid Atlantic
Engineering & Environmental Solubons

TABLE 3.1
SUMMARY OF CHEMICAL CONSTITUENTS DETECTED IN SOIL
OVERTURE CARY
CARY AND MORRISVILLE, NORTH CAROLINA
BROWNFIELDS PROJECT NUMBER 22002-18-092
MID -ATLANTIC JOB NO.: R3021.01
CHEMICAL CONSTITUENT
SAMPLE ID
Action
Level
(mg/kg)
UNRESTRICTED
HEALTH BASED
PSRG (mg/Kg)
PROTECTION OF
GROUNDWATER
PSRG (mg/Kg)
INDUSTRIAL
PSRG (mg/kg)
SB-1
(4.0'-5.0')
SB-2
(0.0'-2.5')
SB-3
(2.5'-5.0')
SB-4
(3.0'-3.5')
SB-5
(2.5'-5.0')
SB-5
(Dupe)
SB-6
(0.0'-2.5')
BG-1
(0.0'-2.5')
HA-1
(2.5')
HA-2
(3.5')
HA-3
(3.5')
TOTAL PETROLEUM HYDROCARBONS (DIESEL AND GASOLINE RANGE ORGANICS) Sampled November 21, 2018
Diesel Range Organics
NA
NA
NA
NA
NA
NA
NA
NA
39.8
1,255
515.9
100
Gasoline Range Organics
NA
NA
NA
NA
NA
NA
NA
NA
5.1
209.7
115.2
50
VOLATILE ORGANIC COMPOUNDS (METHOD 8260 B) Sampled April 15, 2019
Acetone
<0.0018
0.022J
<0.0012
0.019J
0.0043J
0.0075J
0.018J
NA
NA
NA
NA
12000
25
140000
2-Butanone (MEK)
<0.0017
<0.0017
<0.0011
0.0026J
<0.0010
<0.00093
<0.0013
NA
NA
NA
NA
5500
17
40000
SEMI -VOLATILE ORGANIC COMPOUNDS (METHOD 8270D) Sampled April 15, 2019
Benzo(a)anthracene
<0.055
<0.066
<0.051
<0.052
<0.050
NA
0.077J
NA
NA
NA
NA
1.1
0.35
21
Benzo(b)fluoranthene
<0.049
<0.059
<0.045
<0.046
<0.044
NA
0.17.1
NA
NA
NA
NA
1.1
1.2
21
Benzo(a)pyrene
<0.045
<0.055
<0.042
<0.043
<0.041
NA
0.0541
NA
NA
NA
NA
0.11
0.12
2.1
Chrysene
<0.053
<0.064
<0.049
<0.050
<0.048
NA
0.11J
NA
NA
NA
NA
110
36
2100
Fluoranthene
<0.053
<0.064
<0.049
<0.051
<0.049
NA
0.14J
NA
NA
NA
NA
480
670
6000
Pyrene
<0.055
<0.067
<0.051
<0.053
<0.050
NA
0.24J
I NA
NA
NA
NA
360
440
4500
RCRA METALS (METHODS 7471A & 6010B) Sampled April 15, 2019
Mercury
<0.022
<0.027
<0.020
<0.021
<0.020
NA
<0.020
<0.021
NA
NA
NA
2.3
1
9.7
Arsenic
<0.17
5.5
1.9
1.6
<0.15
NA
2.6
3.1
NA
NA
NA
0.68
5.8
3
Barium
15
41
35
37
26
NA
59
250
NA
NA
NA
3100
580
47000
Cadmium
<0.043
<0.052
<0.089
<0.041
<0.039
NA
<0.039
<0.40
NA
NA
NA
14
3
200
Chromium III/Chromium VI
4.5
26
14
8.6
4.8
NA
26
21
NA
NA
NA
2300/0.31
36000/3.8
35000/6.5
Lead
8
10
20
8.8
5.4
NA
9.7
15
NA
NA
NA
400
270
800
Selenium
<0.35
<0.42
<0.32
<0.33
<0.32
NA
<0.32
<0.33
NA
NA
NA
78
2.1
1200
Silver
<0.039
<0.047
<0.036
<0.037
<0.036
NA
<0.36
<0.036
NA
NA
NA
78
3.4
1200
Notes: All concentrations reported in mg/Kg
mg/Kg = Milligrams per kilogram
PSRG = Preliminary Soil Remediation Goals (February 2018)
J = The identification of the analyte is acceptable; the reported value is an estimate
B = The same analyte is found in the associated blank
J4 = The associated batch QC was outside the established quality control range for accuracy
J6 = The sample matrix interfered with the ability to make any accurate determination; spike value is low
NE = Not established
NA = Not analyzed
Bold = Concentration exceeds Action Level or
Protection of Groundwater PSRG
Highlighted = Concentration exceeds Unrestricted Health Based PSRG
Border = Concentration exceeds Industrial PSRG
(1.5'-25) = Sample Depth, feet
Dupe = Duplicate Sample
= Not applicable

APPENDIX A
SOIL BORING LOGS
Mid Atlantic
Engineering & Environmental Solutions

409
LOG OF BORING: SB-1
Rogers View Ct.
Ift Mid Atlantic Raleigh, NC 27610
Engineering e. Environmental solutions Ph: [phone]
Page: 1 1
Site Name: Cary Overture Drilling/Boring Method: Geoprobe 7822DT Total Boring Depth (ft): 5 feet
Project Number: R3021.01 Sampling Method: Macrocore Well Depth (ft): NA
Location: Cary/Morrisville, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 4/15/2019 Driller : Michael Allen Jr. DTW: NA
Date Completed: 4/15/2019 Monitoring Equipment: TVA 1000 MAA Field Staff: R. Tull
o
Sampling
°�
a
A
=
Interval,
a+
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction
Odors
a
Details
w
E~
C°
�
1.58
Dark brown Clay/Topsoil
1
1
2
2
25.92
Orange and Tan Clay with Sand
3
3
4
4
28.20
*
Tan silty Clay with streak of Dark Grey
5
5
*Boring terminated by technician at 5 feet BLS
6
6
7
7
8
8
9
9
10
10
11
11
12
12
COMMENTS:
in - indicates inches ppm - indicates parts per million B - Bentonite
ft - indicates depth in feet ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling
DTW - Depth to Water N/R - Not recorded N/A - Not Appicable

409
LOG OF BORING: SB-2
Rogers View Ct.
Ift M i d Atlantic Raleigh, NC 27610
Engineering i& EnAronmenni solutions Ph: [phone]
Page: 1 1
Site Name: Cary Overture Drilling/Boring Method: Geoprobe 7822DT Total Boring Depth (ft): 5 feet
Project Number: R3021.01 Sampling Method: Macrocore Well Depth (ft): NA
Location: Cary/Morrisville, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 4/15/2019 Driller : Michael Allen Jr. DTW: NA
Date Completed: 4/15/2019 Monitoring Equipment: TVA 1000 MAA Field Staff: R. Tull
a
�
Sampling
°�
o.
A
=
Interval,
a?
SOIL DESCRIPTION (color, texture, moisture, etc.
Construction
Odors
Details
w
E~
C°
�
Dark brown Clay/Topsoil
1
1
24.40
2
2
*
Orange and Tan Clay with Sand
3
3
12.20
4
4
Tan silty Clay
5
5
*Boring terminated by technician at 5 feet BLS
6
6
7
7
8
8
9
9
10
10
11
11
12
12
COMMENTS:
in - indicates inches ppm - indicates parts per million B - Bentonite
ft - indicates depth in feet ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling
DTW - Depth to Water N/R - Not recorded N/A - Not Appicable

LOG OF BORING: SB-3/TMW-1
Mid Atlantic �RAB9)"�C`
Raleigh, NC 27610
Engl neerl nil& Envlronm a-1 501 Uc10 n$ 2h: [phone]
Page: 1 of 1
Site Name: Cary Overture Drilling/Boring Method: Geoprobe 7822DT Total Boring Depth (ft): 40 feet
ProjectNumber R3021.01 Sampling Method: Macrocore Well Depth (ft): NA
Location: Cary/Morrisville, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 4/15/2019 Driller: Michael Allen Jr. DTW: NA
Date Completed: 4/15/2019 Monitoring Equipment: TVA 1000 MAA Field Staff: R. Tull
n
Sampling
�R
a
A
Interval,
SOIL DESCRIPTION (color, texture, moisture, etc.(
Construction Details
a
Odors
C°
�
F
Dark brown and Orange Topsoil with wood
6.4
Orange hard Clay
18.01
*
4
4
Odor
Dark Burgundy and Tan Silt with Clay
Screen: 20-40'
8
8
12
12
16
16
20
20
24
24
28
28
32
32
36
36
40
40
44
44
48
48
*Probe refusal encountered at 24 feet
52
Temporary well installed to 40 feet using 5" solid stem auger
52
COMMENTS: in - indicates inches
ft - indicates depth in feet ppm - indicates parts per million
TD - Total Depth of Boring for Sampling ft-bgs - indicates feet below ground surface B - Bentonite
�DTW
- Depth to Water N/R - Not recorded N/A - Not Appicable

409
LOG OF BORING: SB-4
Rogers View Ct.
Ift M i d Atlantic Raleigh, NC 27610
Engineering i& EnAronmenni solutions Ph: [phone]
Page: 1 1
Site Name: Cary Overture Drilling/Boring Method: Hand Auger Total Boring Depth (ft): 5 feet
Project Number: R3021.01 Sampling Method: Hand Auger Well Depth (ft): NA
Location: Cary/Morrisville, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 4/15/2019 Driller : Michael Allen Jr. DTW: NA
Date Completed: 4/15/2019 Monitoring Equipment: TVA 1000 MAA Field Staff: R. Tull
a
�
Sampling
°�
o.
A
=
Interval,
a?
SOIL DESCRIPTION (color, texture, moisture, etc.
Construction
Odors
Details
w
E~
C°
�
Tan hard Clay
Tan hard Clay with Orange and Red streaks
1
0.63
1
Tan and Grey hard Clay
2
2
2.18
*
Tan Orange Clay with Silt and Sand
3
3
2.15
Red and Grey Silt with Sand
4
4
*Boring terminated by technician at 4.5 feet BLS
5
5
6
6
7
7
8
8
9
9
10
10
11
11
12
12
COMMENTS:
in - indicates inches ppm - indicates parts per million B - Bentonite
ft - indicates depth in feet ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling
DTW - Depth to Water N/R - Not recorded N/A - Not Appicable

409
LOG OF BORING: SB-5
Rogers View Ct.
Ift M i d Atlantic Raleigh, NC 27610
Engineering i& EnAronmenni solutions Ph: [phone]
Page: 1 1
Site Name: Cary Overture Drilling/Boring Method: Geoprobe 7822DT Total Boring Depth (ft): 5 feet
Project Number: R3021.01 Sampling Method: Macrocore Well Depth (ft): NA
Location: Cary/Morrisville, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 4/15/2019 Driller : Michael Allen Jr. DTW: NA
Date Completed: 4/15/2019 Monitoring Equipment: TVA 1000 MAA Field Staff: R. Tull
a
�
Sampling
°�
o.
A
=
Interval,
a?
SOIL DESCRIPTION (color, texture, moisture, etc.
Construction
Odors
Details
w
E~
C°
�
1
brown and grey Clay with very fine Sand
1
0.46
2
2
3
3
tan and orange Clay with very fine Sand
1.01
4
4
5
5
*Boring terminated by technician at 5 feet BLS
6
6
7
7
8
8
9
9
10
10
11
11
12
12
COMMENTS:
in - indicates inches ppm - indicates parts per million B - Bentonite
ft - indicates depth in feet ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling
DTW - Depth to Water N/R - Not recorded N/A - Not Appicable

409
LOG OF BORING: SB-6
Rogers View Ct.
Ift M i d Atlantic Raleigh, NC 27610
Engineering i& EnAronmenni solutions Ph: [phone]
Page: 1 1
Site Name: Cary Overture Drilling/Boring Method: Geoprobe 7822DT Total Boring Depth (ft): 5 feet
Project Number: R3021.01 Sampling Method: Macrocore Well Depth (ft): NA
Location: Cary/Morrisville, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 4/15/2019 Driller : Michael Allen Jr. DTW: NA
Date Completed: 4/15/2019 Monitoring Equipment: TVA 1000 MAA Field Staff: R. Tull
a
�
Sampling
°�
o.
A
=
Interval,
a?
SOIL DESCRIPTION (color, texture, moisture, etc.
Construction
Odors
Details
w
E~
C°
�
Topsoil
Orange and Grey Silt with Clay
1
1
0.40
2
2
Orange and Red Clay with Grey and Black streaks
3
3
0.65
4
4
Red Silt with Clay
5
5
*Boring terminated by technician at 5 feet BLS
6
6
7
7
8
8
9
9
10
10
11
11
12
12
COMMENTS:
in - indicates inches ppm - indicates parts per million B - Bentonite
ft - indicates depth in feet ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling
DTW - Depth to Water N/R - Not recorded N/A - Not Appicable

409
LOG OF BORING: BG-1
Rogers View Ct.
Ift M i d Atlantic Raleigh, NC 27610
Engineering i& EnAronmenni solutions Ph: [phone]
Page: 1 1
Site Name: Cary Overture Drilling/Boring Method: Geoprobe 7822DT Total Boring Depth (ft): 5 feet
Project Number: R3021.01 Sampling Method: Macrocore Well Depth (ft): NA
Location: Cary/Morrisville, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 4/15/2019 Driller : Michael Allen Jr. DTW: NA
Date Completed: 4/15/2019 Monitoring Equipment: TVA 1000 MAA Field Staff: R. Tull
a
�
Sampling
°�
o.
A
=
Interval,
a?
SOIL DESCRIPTION (color, texture, moisture, etc.
Construction
Odors
Details
w
E~
C°
�
Topsoil
1
1
2.40
Orange hard Clay
2
2
3
3
light Orange and Tan hard Silt and Clay
0.63
4
4
Red Silt with Clay
5
5
*Boring terminated by technician at 5 feet BLS
6
6
7
7
8
8
9
9
10
10
11
11
12
12
COMMENTS:
in - indicates inches ppm - indicates parts per million B - Bentonite
ft - indicates depth in feet ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling
DTW - Depth to Water N/R - Not recorded N/A - Not Appicable

APPENDIX B
LABORATORY ANALYTICAL REPORT
AND CHAIN OF CUSTODY RECORD
FOR SOIL & GROUNDWATER SAMPLES
Ift Mid Atlantic
Engineering & Environmental Solutions

Case Narrative
PRISM Full -Service Analytical &
Environmental Solutions
`,. LABORATORIES, INC.
Mid -Atlantic Associates, Inc. - Raleigh
Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
NC Certification No. 402
NC Drinking Water Cent No. 37735
SC Certification No. 99012
Project: 3612 & 3624 Davis Drive
Lab Submittal Date: 04/16/2019
Prism Work Order: 9040256
4/22/19 14:21
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a,j
Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
Reviewed By Angela D. Overcash
VP Laboratory Services
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLIP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
M Matrix spike outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PRISMSample
LABORATORIES INC.
Full -Service Analytical R
Environmental Solutions
Receipt Summary
04/22/2019
Prism Work Order: 9040256
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
S13-1
9040256-01
Solid
04/15/19
9:40
04/16/19
9:45
S13-2
9040256-02
Solid
04/15/19
10:05
04/16/19
9:45
S13-3
9040256-03
Solid
04/15/19
10:45
04/16/19
9:45
S13-4
9040256-04
Solid
04/15/19
14:25
04/16/19
9:45
S13-5
9040256-05
Solid
04/15/19
12:00
04/16/19
9:45
S13-6
9040256-06
Solid
04/15/19
14:05
04/16/19
9:45
BG-1
9040256-07
Solid
04/15/19
12:40
04/16/19
9:45
Duplicate
9040256-08
Solid
04/15/19
12:20
04/16/19
9:45
TMW-1
9040256-09
Water
04/15/19
14:25
04/16/19
9:45
Duplicate - water
9040256-10
Water
04/15/19
14:30
04/16/19
9:45
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I S M Full Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Summary of Detections
04/22/2019
Prism Work Order: 9040256
Prism ID
Client ID
Parameter
Method
Result
Units
9040256-01
SB-1
Barium
`6010D
15
mg/kg dry
9040256-01
SB-1
Chromium
'6010D
4.5
mg/kg dry
9040256-01
SB-1
Lead
'6010D
8.0
mg/kg dry
9040256-02
SB-2
Arsenic
`6010D
5.5
mg/kg dry
9040256-02
SB-2
Barium
'6010D
41
mg/kg dry
9040256-02
SB-2
Chromium
"6010D
26
mg/kg dry
9040256-02
SB-2
Lead
'6010D
10
mg/kg dry
9040256-02
SB-2
Acetone
8260E
0.022
1
mg/kg dry
9040256-03
SB-3
Arsenic
'6010D
1.9
mg/kg dry
9040256-03
SB-3
Barium
'6010D
35
mg/kg dry
9040256-03
SB-3
Chromium
`6010D
14
mg/kg dry
9040256-03
SB-3
Lead
'6010D
20
mg/kg dry
9040256-04
SB-4
Arsenic
"6010D
1.6
mg/kg dry
9040256-04
SB-4
Barium
'6010D
37
mg/kg dry
9040256-04
SB-4
Chromium
`6010D
8.6
mg/kg dry
9040256-04
SB-4
Lead
"6010D
8.8
mg/kg dry
9040256-04
SB-4
Acetone
8260B
0.019
1
mg/kg dry
9040256-05
SB-5
Barium
`6010D
26
mg/kg dry
9040256-05
SB-5
Chromium
'6010D
4.8
mg/kg dry
9040256-05
SB-5
Lead
"6010D
5.4
mg/kg dry
9040256-06
SB-6
Benzo(a)anthracene
8270D
0.077
J
mg/kg dry
9040256-06
SB-6
Benzo(a)pyrene
8270D
0.054
1
mg/kg dry
9040256-06
SB-6
Benzo(b)fluoranthene
8270D
0.17
1
mg/kg dry
9040256-06
SB-6
Chrysene
8270D
0.11
1
mg/kg dry
9040256-06
SB-6
Fluoranthene
8270D
0.14
1
mg/kg dry
9040256-06
SB-6
Pyrene
8270D
0.24
1
mg/kg dry
9040256-06
SB-6
Arsenic
'6010D
2.6
mg/kg dry
9040256-06
SB-6
Barium
`6010D
59
mg/kg dry
9040256-06
SB-6
Chromium
'6010D
26
mg/kg dry
9040256-06
SB-6
Lead
"6010D
9.7
mg/kg dry
9040256-06
SB-6
Acetone
8260B
0.018
1
mg/kg dry
9040256-07
BG-1
Arsenic
`6010D
3.1
mg/kg dry
9040256-07
BG-1
Barium
'6010D
250
mg/kg dry
9040256-07
BG-1
Chromium
'6010D
21
mg/kg dry
9040256-07
BG-1
Lead
`6010D
15
mg/kg dry
9040256-09
TMW-1
Barium
'6010D
0.38
mg/L
9040256-09
TMW-1
Chromium
"6010D
0.079
mg/L
9040256-09
TMW-1
Lead
'6010D
0.015
mg/L
9040256-09
TMW-1
Chloroform
8260E
1.2
ug/L
9040256-10
Duplicate - water
Acetone
8260E
5.6
ug/L
9040256-10
Duplicate - water
Chloroform
8260B
0.89
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3612 & 3624 Davis Drive
Client
Sample ID:
SB-1
Attn: Dan Nielsen
Prism
Sample ID:
9040256-01
409 Rogers View Court
Prism
Work Order: 9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected: 04/15/19 09:40
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
78.7
% by
0.100
0.100
1
*SM2540 G
4/18/19 9:30
KBS
P9D0322
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.42
0.065
1
8270D
4/17/19 18:53
JMV
P9D0300
1,2-Dichlorobenzene
BRL
mg/kg dry
0.42
0.064
1
8270D
4/17/19 18:53
JMV
P9D0300
1,3-Dichlorobenzene
BRL
mg/kg dry
0.42
0.059
1
8270D
4/17/19 18:53
JMV
P9D0300
1,4-Dichlorobenzene
BRL
mg/kg dry
0.42
0.061
1
8270D
4/17/19 18:53
JMV
P9D0300
1-Methyl naphthalene
BRL
mg/kg dry
0.42
0.081
1
8270D
4/17/19 18:53
JMV
P9D0300
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.42
0.068
1
8270D
4/17/19 18:53
JMV
P9D0300
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.42
0.079
1
8270D
4/17/19 18:53
JMV
P9D0300
2,4-Dichlorophenol
BRL
mg/kg dry
0.42
0.081
1
8270D
4/17/19 18:53
JMV
P9D0300
2,4-Dimethylphenol
BRL
mg/kg dry
0.42
0.064
1
8270D
4/17/19 18:53
JMV
P9D0300
2,4-Dinitrophenol
BRL
mg/kg dry
0.42
0.058
1
8270D
4/17/19 18:53
JMV
P9D0300
2,4-Dinitrotoluene
BRL
mg/kg dry
0.42
0.051
1
8270D
4/17/19 18:53
JMV
P9D0300
2,6-Dinitrotoluene
BRL
mg/kg dry
0.42
0.056
1
8270D
4/17/19 18:53
JMV
P9D0300
2-Chloronaphthalene
BRL
mg/kg dry
0.42
0.061
1
8270D
4/17/19 18:53
JMV
P9D0300
2-Chlorophenol
BRL
mg/kg dry
0.42
0.059
1
8270D
4/17/19 18:53
JMV
P9D0300
2-Methyl naphthalene
BRL
mg/kg dry
0.42
0.067
1
8270D
4/17/19 18:53
JMV
P9D0300
2-Methylphenol
BRL
mg/kg dry
0.42
0.054
1
8270D
4/17/19 18:53
JMV
P9D0300
2-Nitrophenol
BRL
mg/kg dry
0.42
0.076
1
8270D
4/17/19 18:53
JMV
P9D0300
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.42
0.083
1
8270D
4/17/19 18:53
JMV
P9D0300
3/4-Methyl phenol
BRL
mg/kg dry
0.42
0.052
1
8270D
4/17/19 18:53
JMV
P9D0300
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.42
0.063
1
8270D
4/17/19 18:53
JMV
P9D0300
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.42
0.072
1
8270D
4/17/19 18:53
JMV
P9D0300
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.42
0.059
1
8270D
4/17/19 18:53
JMV
P9D0300
4-Chloroaniline
BRL
mg/kg dry
0.42
0.050
1
8270D
4/17/19 18:53
JMV
P9D0300
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.42
0.054
1
8270D
4/17/19 18:53
JMV
P9D0300
4-Nitrophenol
BRL
mg/kg dry
0.42
0.065
1
8270D
4/17/19 18:53
JMV
P9D0300
Acenaphthene
BRL
mg/kg dry
0.42
0.057
1
8270D
4/17/19 18:53
JMV
P9D0300
Acenaphthylene
BRL
mg/kg dry
0.42
0.061
1
8270D
4/17/19 18:53
JMV
P9D0300
Anthracene
BRL
mg/kg dry
0.42
0.067
1
8270D
4/17/19 18:53
JMV
P9D0300
Azobenzene
BRL
mg/kg dry
0.42
0.055
1
8270D
4/17/19 18:53
JMV
P9D0300
Benzo(a)anthracene
BRL
mg/kg dry
0.42
0.055
1
8270D
4/17/19 18:53
JMV
P9D0300
Benzo(a)pyrene
BRL
mg/kg dry
0.42
0.045
1
8270D
4/17/19 18:53
JMV
P9D0300
Benzo(b)fluoranthene
BRL
mg/kg dry
0.42
0.049
1
8270D
4/17/19 18:53
JMV
P9D0300
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.42
0.046
1
8270D
4/17/19 18:53
JMV
P9D0300
Benzo(k)fluoranthene
BRL
mg/kg dry
0.42
0.055
1
8270D
4/17/19 18:53
JMV
P9D0300
Benzoic Acid
BRL
mg/kg dry
0.42
0.035
1
8270D
4/17/19 18:53
JMV
P9D0300
Benzyl alcohol
BRL
mg/kg dry
0.42
0.055
1
8270D
4/17/19 18:53
JMV
P9D0300
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.42
0.073
1
8270D
4/17/19 18:53
JMV
P9D0300
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.42
0.059
1
8270D
4/17/19 18:53
JMV
P9D0300
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.42
0.072
1
8270D
4/17/19 18:53
JMV
P9D0300
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
P R S M
/ Environmental Solutions
LABORATORIES INC.
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3612 & 3624
Davis Drive
Client Sample ID: SB-1
Attn: Dan Nielsen
Prism Sample ID: 9040256-01
409 Rogers View Court
Prism Work Order:
9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
04/15/19 09:40
Time Submitted:
04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.42
0.062
1
8270D
4/17/19 18:53
JMV
P9D0300
Butyl benzyl phthalate
BRL
mg/kg dry
0.42
0.060
1
8270D
4/17/19 18:53
JMV
P9D0300
Chrysene
BRL
mg/kg dry
0.42
0.053
1
8270D
4/17/19 18:53
JMV
P9D0300
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.42
0.051
1
8270D
4/17/19 18:53
JMV
P9D0300
Dibenzofuran
BRL
mg/kg dry
0.42
0.064
1
8270D
4/17/19 18:53
JMV
P9D0300
Diethyl phthalate
BRL
mg/kg dry
0.42
0.058
1
8270D
4/17/19 18:53
JMV
P9D0300
Dimethyl phthalate
BRL
mg/kg dry
0.42
0.055
1
8270D
4/17/19 18:53
JMV
P9D0300
Di-n-butyl phthalate
BRL
mg/kg dry
0.42
0.059
1
8270D
4/17/19 18:53
JMV
P9D0300
Di-n-octyl phthalate
BRL
mg/kg dry
0.42
0.051
1
8270D
4/17/19 18:53
JMV
P9D0300
Fluoranthene
BRL
mg/kg dry
0.42
0.053
1
8270D
4/17/19 18:53
JMV
P9D0300
Fluorene
BRL
mg/kg dry
0.42
0.060
1
8270D
4/17/19 18:53
JMV
P9D0300
Hexachlorobenzene
BRL
mg/kg dry
0.42
0.066
1
8270D
4/17/19 18:53
JMV
P9D0300
Hexachlorobutadiene
BRL
mg/kg dry
0.42
0.075
1
8270D
4/17/19 18:53
JMV
P9D0300
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.42
0.075
1
8270D
4/17/19 18:53
JMV
P9D0300
Hexachloroethane
BRL
mg/kg dry
0.42
0.070
1
8270D
4/17/19 18:53
JMV
P9D0300
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.42
0.048
1
8270D
4/17/19 18:53
JMV
P9D0300
Isophorone
BRL
mg/kg dry
0.42
0.057
1
8270D
4/17/19 18:53
JMV
P9D0300
Naphthalene
BRL
mg/kg dry
0.42
0.067
1
8270D
4/17/19 18:53
JMV
P9D0300
Nitrobenzene
BRL
mg/kg dry
0.42
0.059
1
8270D
4/17/19 18:53
JMV
P9D0300
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.42
0.066
1
8270D
4/17/19 18:53
JMV
P9D0300
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.42
0.064
1
8270D
4/17/19 18:53
JMV
P9D0300
Pentachlorophenol
BRL
mg/kg dry
0.42
0.049
1
8270D
4/17/19 18:53
JMV
P9D0300
Phenanthrene
BRL
mg/kg dry
0.42
0.054
1
8270D
4/17/19 18:53
JMV
P9D0300
Phenol
BRL
mg/kg dry
0.42
0.062
1
8270D
4/17/19 18:53
JMV
P9D0300
Pyrene
BRL
mg/kg dry
0.42
0.055
1
8270D
4/17/19 18:53
JMV
P9D0300
Pyridine
BRL
mg/kg dry
0.42
0.073
1
8270D
4/17/19 18:53
JMV
P9D0300
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
100 %
39-132
2-Fluorobiphenyl
95 %
44-115
2-Fluorophenol
90 %
35-115
Nitrobenzene-d5
84 %
37-122
Phenol-d5
88 %
34-121
Terphenyl-d14
97 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.064
0.022
1
*7471B
4/18/19 11:32
MMR
P9D0323
Arsenic
BRL
mg/kg dry
1.3
0.17
1
*6010D
4/18/19 10:43
JAB
P9D0297
Barium
15
mg/kg dry
13
3.8
1
*6010D
4/18/19 10:43
JAB
P9D0297
Cadmium
BRL
mg/kg dry
0.64
0.043
1
*6010D
4/18/19 10:43
JAB
P9D0297
Chromium
4.5
mg/kg dry
1.3
0.096
1
*6010D
4/18/19 10:43
JAB
P9D0297
Lead
8.0
mg/kg dry
1.3
0.21
1
*60101)
4/18/19 10:43
JAB
P9D0297
Selenium
BRL
mg/kg dry
1.3
0.35
1
*6010D
4/18/19 10:43
JAB
P9D0297
Silver
BRL
mg/kg dry
0.64
0.039
1
*6010D
4/18/19 10:43
JAB
P9D0297
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Solid
Laboratory Report
04/22/2019
Client Sample ID: SB-1
Prism Sample ID: 9040256-01
Prism Work Order: 9040256
Time Collected: 04/15/19 09:40
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0071
0.00086
1
8260B
4/16/19 14:31
JLB
P9D0298
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0071
0.0010
1
8260B
4/16/19 14:31
JLB
P9D0298
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0071
0.00052
1
8260B
4/16/19 14:31
JLB
P9D0298
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0071
0.00076
1
8260B
4/16/19 14:31
JLB
P9D0298
1,1-Dichloroethane
BRL
mg/kg dry
0.0071
0.0013
1
8260B
4/16/19 14:31
JLB
P9D0298
1,1-Dichloroethylene
BRL
mg/kg dry
0.0071
0.0013
1
8260B
4/16/19 14:31
JLB
P9D0298
1,1-Dichloropropylene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 14:31
JLB
P9D0298
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.014
0.0010
1
8260B
4/16/19 14:31
JLB
P9D0298
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0071
0.00080
1
8260B
4/16/19 14:31
JLB
P9D0298
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.014
0.00068
1
8260B
4/16/19 14:31
JLB
P9D0298
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0071
0.00075
1
8260B
4/16/19 14:31
JLB
P9D0298
1,2-Dibromoethane
BRL
mg/kg dry
0.0071
0.00063
1
8260B
4/16/19 14:31
JLB
P9D0298
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0071
0.00079
1
8260B
4/16/19 14:31
JLB
P9D0298
1,2-Dichloroethane
BRL
mg/kg dry
0.0071
0.00084
1
8260B
4/16/19 14:31
JLB
P9D0298
1,2-Dichloropropane
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 14:31
JLB
P9D0298
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0071
0.00089
1
8260B
4/16/19 14:31
JLB
P9D0298
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0071
0.00088
1
8260B
4/16/19 14:31
JLB
P9D0298
1,3-Dichloropropane
BRL
mg/kg dry
0.0071
0.00059
1
8260B
4/16/19 14:31
JLB
P9D0298
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0071
0.00090
1
8260B
4/16/19 14:31
JLB
P9D0298
2,2-Dichloropropane
BRL
mg/kg dry
0.0071
0.00088
1
8260B
4/16/19 14:31
JLB
P9D0298
2-Chlorotoluene
BRL
mg/kg dry
0.0071
0.00095
1
8260B
4/16/19 14:31
JLB
P9D0298
4-Chlorotoluene
BRL
mg/kg dry
0.0071
0.00081
1
8260B
4/16/19 14:31
JLB
P9D0298
4-Isopropyltoluene
BRL
mg/kg dry
0.0071
0.0018
1
8260B
4/16/19 14:31
JLB
P9D0298
Acetone
BRL
mg/kg dry
0.028
0.0018
1
8260B
4/16/19 14:31
JLB
P9D0298
Benzene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 14:31
JLB
P9D0298
Bromobenzene
BRL
mg/kg dry
0.0071
0.00098
1
8260B
4/16/19 14:31
JLB
P9D0298
Bromochloromethane
BRL
mg/kg dry
0.0071
0.0012
1
8260B
4/16/19 14:31
JLB
P9D0298
Bromodichloromethane
BRL
mg/kg dry
0.0071
0.00067
1
8260B
4/16/19 14:31
JLB
P9D0298
Bromoform
BRL
mg/kg dry
0.0071
0.00055
1
8260B
4/16/19 14:31
JLB
P9D0298
Bromomethane
BRL
mg/kg dry
0.014
0.0035
1
8260B
4/16/19 14:31
JLB
P9D0298
Carbon Tetrachloride
BRL
mg/kg dry
0.0071
0.0014
1
8260B
4/16/19 14:31
JLB
P9D0298
Chlorobenzene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 14:31
JLB
P9D0298
Chloroethane
BRL
mg/kg dry
0.014
0.0013
1
8260B
4/16/19 14:31
JLB
P9D0298
Chloroform
BRL
mg/kg dry
0.0071
0.00087
1
8260B
4/16/19 14:31
JLB
P9D0298
Chloromethane
BRL
mg/kg dry
0.014
0.0022
1
8260B
4/16/19 14:31
JLB
P9D0298
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 14:31
JLB
P9D0298
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0071
0.00070
1
8260B
4/16/19 14:31
JLB
P9D0298
Dibromochloromethane
BRL
mg/kg dry
0.0071
0.00047
1
8260B
4/16/19 14:31
JLB
P9D0298
Dichlorodifluoromethane
BRL
mg/kg dry
0.014
0.0020
1
8260B
4/16/19 14:31
JLB
P9D0298
Ethylbenzene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 14:31
JLB
P9D0298
Isopropyl Ether
BRL
mg/kg dry
0.0071
0.0010
1
8260B
4/16/19 14:31
JLB
P9D0298
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0071
0.00082
1
8260B
4/16/19 14:31
JLB
P9D0298
m,p-Xylenes
BRL
mg/kg dry
0.014
0.0018
1
8260B
4/16/19 14:31
JLB
P9D0298
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: SB-1
Attn: Dan Nielsen Prism Sample ID: 9040256-01
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 04/15/19 09:40
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.028
0.00049
1
8260B
4/16/19 14:31
JLB
P9D0298
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.028
0.0017
1
8260B
4/16/19 14:31
JLB
P9D0298
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.028
0.00058
1
8260B
4/16/19 14:31
JLB
P9D0298
Methylene Chloride
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 14:31
JLB
P9D0298
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0071
0.00099
1
8260B
4/16/19 14:31
JLB
P9D0298
Naphthalene
BRL
mg/kg dry
0.014
0.00071
1
8260B
4/16/19 14:31
JLB
P9D0298
n-Butylbenzene
BRL
mg/kg dry
0.0071
0.00066
1
8260B
4/16/19 14:31
JLB
P9D0298
n-Propylbenzene
BRL
mg/kg dry
0.0071
0.0010
1
8260B
4/16/19 14:31
JLB
P9D0298
o-Xylene
BRL
mg/kg dry
0.0071
0.00075
1
8260B
4/16/19 14:31
JLB
P9D0298
sec-Butylbenzene
BRL
mg/kg dry
0.0071
0.00076
1
8260B
4/16/19 14:31
JLB
P9D0298
Styrene
BRL
mg/kg dry
0.0071
0.00069
1
8260B
4/16/19 14:31
JLB
P9D0298
tert-Butylbenzene
BRL
mg/kg dry
0.0071
0.00084
1
8260B
4/16/19 14:31
JLB
P9D0298
Tetrachloroethylene
BRL
mg/kg dry
0.0071
0.0013
1
8260B
4/16/19 14:31
JLB
P9D0298
Toluene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 14:31
JLB
P9D0298
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0071
0.0014
1
8260B
4/16/19 14:31
JLB
P9D0298
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0071
0.00061
1
8260B
4/16/19 14:31
JLB
P9D0298
Trichloroethylene
BRL
mg/kg dry
0.0071
0.0014
1
8260B
4/16/19 14:31
JLB
P9D0298
Trichlorofluoromethane
BRL
mg/kg dry
0.014
0.0019
1
8260B
4/16/19 14:31
JLB
P9D0298
Vinyl acetate
BRL
mg/kg dry
0.014
0.00077
1
8260B
4/16/19 14:31
JLB
P9D0298
Vinyl chloride
BRL
mg/kg dry
0.014
0.0014
1
8260B
4/16/19 14:31
JLB
P9D0298
Xylenes, total
BRL
mg/kg dry
0.021
0.0025
1
8260B
4/16/19 14:31
JLB
P9D0298
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
97 %
70-130
Dibromofluoromethane
101 %
84-123
Toluene-d8
94 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3612 & 3624 Davis Drive
Client
Sample ID:
SB-2
Attn: Dan Nielsen
Prism
Sample ID:
9040256-02
409 Rogers View Court
Prism
Work Order: 9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected: 04/15/19 10:05
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
65.2
% by
0.100
0.100
1
*SM2540 G
4/18/19 9:30
KBS
P9D0322
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.50
0.079
1
8270D
4/17/19 19:15
JMV
P9D0300
1,2-Dichlorobenzene
BRL
mg/kg dry
0.50
0.077
1
8270D
4/17/19 19:15
JMV
P9D0300
1,3-Dichlorobenzene
BRL
mg/kg dry
0.50
0.071
1
8270D
4/17/19 19:15
JMV
P9D0300
1,4-Dichlorobenzene
BRL
mg/kg dry
0.50
0.074
1
8270D
4/17/19 19:15
JMV
P9D0300
1-Methyl naphthalene
BRL
mg/kg dry
0.50
0.097
1
8270D
4/17/19 19:15
JMV
P9D0300
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.50
0.082
1
8270D
4/17/19 19:15
JMV
P9D0300
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.50
0.095
1
8270D
4/17/19 19:15
JMV
P9D0300
2,4-Dichlorophenol
BRL
mg/kg dry
0.50
0.098
1
8270D
4/17/19 19:15
JMV
P9D0300
2,4-Dimethylphenol
BRL
mg/kg dry
0.50
0.077
1
8270D
4/17/19 19:15
JMV
P9D0300
2,4-Dinitrophenol
BRL
mg/kg dry
0.50
0.070
1
8270D
4/17/19 19:15
JMV
P9D0300
2,4-Dinitrotoluene
BRL
mg/kg dry
0.50
0.061
1
8270D
4/17/19 19:15
JMV
P9D0300
2,6-Dinitrotoluene
BRL
mg/kg dry
0.50
0.067
1
8270D
4/17/19 19:15
JMV
P9D0300
2-Chloronaphthalene
BRL
mg/kg dry
0.50
0.073
1
8270D
4/17/19 19:15
JMV
P9D0300
2-Chlorophenol
BRL
mg/kg dry
0.50
0.072
1
8270D
4/17/19 19:15
JMV
P9D0300
2-Methyl naphthalene
BRL
mg/kg dry
0.50
0.081
1
8270D
4/17/19 19:15
JMV
P9D0300
2-Methylphenol
BRL
mg/kg dry
0.50
0.065
1
8270D
4/17/19 19:15
JMV
P9D0300
2-Nitrophenol
BRL
mg/kg dry
0.50
0.092
1
8270D
4/17/19 19:15
JMV
P9D0300
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.50
0.10
1
8270D
4/17/19 19:15
JMV
P9D0300
3/4-Methyl phenol
BRL
mg/kg dry
0.50
0.062
1
8270D
4/17/19 19:15
JMV
P9D0300
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.50
0.076
1
8270D
4/17/19 19:15
JMV
P9D0300
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.50
0.087
1
8270D
4/17/19 19:15
JMV
P9D0300
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.50
0.071
1
8270D
4/17/19 19:15
JMV
P9D0300
4-Chloroaniline
BRL
mg/kg dry
0.50
0.061
1
8270D
4/17/19 19:15
JMV
P9D0300
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.50
0.066
1
8270D
4/17/19 19:15
JMV
P9D0300
4-Nitrophenol
BRL
mg/kg dry
0.50
0.078
1
8270D
4/17/19 19:15
JMV
P9D0300
Acenaphthene
BRL
mg/kg dry
0.50
0.069
1
8270D
4/17/19 19:15
JMV
P9D0300
Acenaphthylene
BRL
mg/kg dry
0.50
0.073
1
8270D
4/17/19 19:15
JMV
P9D0300
Anthracene
BRL
mg/kg dry
0.50
0.081
1
8270D
4/17/19 19:15
JMV
P9D0300
Azobenzene
BRL
mg/kg dry
0.50
0.067
1
8270D
4/17/19 19:15
JMV
P9D0300
Benzo(a)anthracene
BRL
mg/kg dry
0.50
0.066
1
8270D
4/17/19 19:15
JMV
P9D0300
Benzo(a)pyrene
BRL
mg/kg dry
0.50
0.055
1
8270D
4/17/19 19:15
JMV
P9D0300
Benzo(b)fluoranthene
BRL
mg/kg dry
0.50
0.059
1
8270D
4/17/19 19:15
JMV
P9D0300
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.50
0.055
1
8270D
4/17/19 19:15
JMV
P9D0300
Benzo(k)fluoranthene
BRL
mg/kg dry
0.50
0.066
1
8270D
4/17/19 19:15
JMV
P9D0300
Benzoic Acid
BRL
mg/kg dry
0.50
0.043
1
8270D
4/17/19 19:15
JMV
P9D0300
Benzyl alcohol
BRL
mg/kg dry
0.50
0.067
1
8270D
4/17/19 19:15
JMV
P9D0300
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.50
0.088
1
8270D
4/17/19 19:15
JMV
P9D0300
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.50
0.071
1
8270D
4/17/19 19:15
JMV
P9D0300
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.50
0.086
1
8270D
4/17/19 19:15
JMV
P9D0300
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
04/22/2019
Mid -Atlantic Associates,
Inc. - Raleigh
Project: 3612 & 3624
Davis Drive
Client Sample ID: SB-2
Attn: Dan Nielsen
Prism Sample ID: 9040256-02
409 Rogers View Court
Prism Work Order:
9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
04/15/19 10:05
Time Submitted:
04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.50
0.075
1
8270D
4/17/19 19:15
JMV
P9D0300
Butyl benzyl phthalate
BRL
mg/kg dry
0.50
0.072
1
8270D
4/17/19 19:15
JMV
P9D0300
Chrysene
BRL
mg/kg dry
0.50
0.064
1
8270D
4/17/19 19:15
JMV
P9D0300
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.50
0.061
1
8270D
4/17/19 19:15
JMV
P9D0300
Dibenzofuran
BRL
mg/kg dry
0.50
0.077
1
8270D
4/17/19 19:15
JMV
P9D0300
Diethyl phthalate
BRL
mg/kg dry
0.50
0.070
1
8270D
4/17/19 19:15
JMV
P9D0300
Dimethyl phthalate
BRL
mg/kg dry
0.50
0.067
1
8270D
4/17/19 19:15
JMV
P9D0300
Di-n-butyl phthalate
BRL
mg/kg dry
0.50
0.072
1
8270D
4/17/19 19:15
JMV
P9D0300
Di-n-octyl phthalate
BRL
mg/kg dry
0.50
0.062
1
8270D
4/17/19 19:15
JMV
P9D0300
Fluoranthene
BRL
mg/kg dry
0.50
0.064
1
8270D
4/17/19 19:15
JMV
P9D0300
Fluorene
BRL
mg/kg dry
0.50
0.072
1
8270D
4/17/19 19:15
JMV
P9D0300
Hexachlorobenzene
BRL
mg/kg dry
0.50
0.080
1
8270D
4/17/19 19:15
JMV
P9D0300
Hexachlorobutadiene
BRL
mg/kg dry
0.50
0.091
1
8270D
4/17/19 19:15
JMV
P9D0300
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.50
0.090
1
8270D
4/17/19 19:15
JMV
P9D0300
Hexachloroethane
BRL
mg/kg dry
0.50
0.085
1
8270D
4/17/19 19:15
JMV
P9D0300
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.50
0.058
1
8270D
4/17/19 19:15
JMV
P9D0300
Isophorone
BRL
mg/kg dry
0.50
0.068
1
8270D
4/17/19 19:15
JMV
P9D0300
Naphthalene
BRL
mg/kg dry
0.50
0.081
1
8270D
4/17/19 19:15
JMV
P9D0300
Nitrobenzene
BRL
mg/kg dry
0.50
0.072
1
8270D
4/17/19 19:15
JMV
P9D0300
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.50
0.080
1
8270D
4/17/19 19:15
JMV
P9D0300
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.50
0.077
1
8270D
4/17/19 19:15
JMV
P9D0300
Pentachlorophenol
BRL
mg/kg dry
0.50
0.060
1
8270D
4/17/19 19:15
JMV
P9D0300
Phenanthrene
BRL
mg/kg dry
0.50
0.066
1
8270D
4/17/19 19:15
JMV
P9D0300
Phenol
BRL
mg/kg dry
0.50
0.074
1
8270D
4/17/19 19:15
JMV
P9D0300
Pyrene
BRL
mg/kg dry
0.50
0.067
1
8270D
4/17/19 19:15
JMV
P9D0300
Pyridine
BRL
mg/kg dry
0.50
0.088
1
8270D
4/17/19 19:15
JMV
P9D0300
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
98 %
39-132
2-Fluorobiphenyl
90 %
44-115
2-Fluorophenol
88 %
35-115
Nitrobenzene-d5
81 %
37-122
Phenol-d5
86 %
34-121
Terphenyl-d14
92 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.077
0.027
1
*7471B
4/18/19 11:37
MMR
P9D0323
Arsenic
5.5
mg/kg dry
1.5
0.20
1
*6010D
4/18/19 11:09
JAB
P91010297
Barium
41
mg/kg dry
15
4.6
1
*6010D
4/18/19 11:09
JAB
P9D0297
Cadmium
BRL
mg/kg dry
0.77
0.052
1
*6010D
4/18/19 11:09
JAB
P9D0297
Chromium
26
mg/kg dry
1.5
0.12
1
*6010D
4/18/19 11:09
JAB
P9D0297
Lead
10
mg/kg dry
1.5
0.26
1
*6010D
4/18/19 11:09
JAB
P9D0297
Selenium
BRL
mg/kg dry
1.5
0.42
1
*6010D
4/18/19 11:09
JAB
P9D0297
Silver
BRL
mg/kg dry
0.77
0.047
1
*6010D
4/18/19 11:09
JAB
P9D0297
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Solid
Client Sample ID: SB-2
Prism Sample ID: 9040256-02
Prism Work Order: 9040256
Time Collected: 04/15/19 10:05
Time Submitted: 04/16/19 09:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0071
0.00087
1
8260B
4/16/19 18:01
JLB
P9D0298
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0071
0.0010
1
8260B
4/16/19 18:01
JLB
P9D0298
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0071
0.00052
1
8260B
4/16/19 18:01
JLB
P9D0298
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0071
0.00077
1
8260B
4/16/19 18:01
JLB
P9D0298
1,1-Dichloroethane
BRL
mg/kg dry
0.0071
0.0013
1
8260B
4/16/19 18:01
JLB
P9D0298
1,1-Dichloroethylene
BRL
mg/kg dry
0.0071
0.0013
1
8260B
4/16/19 18:01
JLB
P9D0298
1,1-Dichloropropylene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 18:01
JLB
P9D0298
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.014
0.0010
1
8260B
4/16/19 18:01
JLB
P9D0298
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0071
0.00081
1
8260B
4/16/19 18:01
JLB
P9D0298
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.014
0.00068
1
8260B
4/16/19 18:01
JLB
P9D0298
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0071
0.00075
1
8260B
4/16/19 18:01
JLB
P9D0298
1,2-Dibromoethane
BRL
mg/kg dry
0.0071
0.00064
1
8260B
4/16/19 18:01
JLB
P9D0298
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0071
0.00079
1
8260B
4/16/19 18:01
JLB
P9D0298
1,2-Dichloroethane
BRL
mg/kg dry
0.0071
0.00085
1
8260B
4/16/19 18:01
JLB
P9D0298
1,2-Dichloropropane
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 18:01
JLB
P9D0298
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0071
0.00089
1
8260B
4/16/19 18:01
JLB
P9D0298
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0071
0.00089
1
8260B
4/16/19 18:01
JLB
P9D0298
1,3-Dichloropropane
BRL
mg/kg dry
0.0071
0.00059
1
8260B
4/16/19 18:01
JLB
P9D0298
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0071
0.00090
1
8260B
4/16/19 18:01
JLB
P9D0298
2,2-Dichloropropane
BRL
mg/kg dry
0.0071
0.00089
1
8260B
4/16/19 18:01
JLB
P9D0298
2-Chlorotoluene
BRL
mg/kg dry
0.0071
0.00095
1
8260B
4/16/19 18:01
JLB
P9D0298
4-Chlorotoluene
BRL
mg/kg dry
0.0071
0.00081
1
8260B
4/16/19 18:01
JLB
P9D0298
4-Isopropyltoluene
BRL
mg/kg dry
0.0071
0.0018
1
8260B
4/16/19 18:01
JLB
P9D0298
Acetone
0.022 J
mg/kg dry
0.028
0.0018
1
8260B
4/16/19 18:01
JLB
P900298
Benzene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 18:01
JLB
P9D0298
Bromobenzene
BRL
mg/kg dry
0.0071
0.00099
1
8260B
4/16/19 18:01
JLB
P9D0298
Bromochloromethane
BRL
mg/kg dry
0.0071
0.0012
1
8260B
4/16/19 18:01
JLB
P9D0298
Bromodichloromethane
BRL
mg/kg dry
0.0071
0.00068
1
8260B
4/16/19 18:01
JLB
P9D0298
Bromoform
BRL
mg/kg dry
0.0071
0.00055
1
8260B
4/16/19 18:01
JLB
P9D0298
Bromomethane
BRL
mg/kg dry
0.014
0.0035
1
8260B
4/16/19 18:01
JLB
P9D0298
Carbon Tetrachloride
BRL
mg/kg dry
0.0071
0.0014
1
8260B
4/16/19 18:01
JLB
P9D0298
Chlorobenzene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 18:01
JLB
P9D0298
Chloroethane
BRL
mg/kg dry
0.014
0.0014
1
8260B
4/16/19 18:01
JLB
P9D0298
Chloroform
BRL
mg/kg dry
0.0071
0.00087
1
8260B
4/16/19 18:01
JLB
P9D0298
Chloromethane
BRL
mg/kg dry
0.014
0.0022
1
8260B
4/16/19 18:01
JLB
P9D0298
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 18:01
JLB
P9D0298
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0071
0.00070
1
8260B
4/16/19 18:01
JLB
P9D0298
Dibromochloromethane
BRL
mg/kg dry
0.0071
0.00048
1
8260B
4/16/19 18:01
JLB
P9D0298
Dichlorodifluoromethane
BRL
mg/kg dry
0.014
0.0020
1
8260B
4/16/19 18:01
JLB
P9D0298
Ethylbenzene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 18:01
JLB
P9D0298
Isopropyl Ether
BRL
mg/kg dry
0.0071
0.0010
1
8260B
4/16/19 18:01
JLB
P9D0298
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0071
0.00083
1
8260B
4/16/19 18:01
JLB
P9D0298
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: SB-2
Attn: Dan Nielsen Prism Sample ID: 9040256-02
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 04/15/19 10:05
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.014
0.0018
1
8260B
4/16/19 18:01
JLB
P9D0298
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.028
0.00049
1
8260B
4/16/19 18:01
JLB
P9D0298
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.028
0.0017
1
8260B
4/16/19 18:01
JLB
P9D0298
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.028
0.00058
1
8260B
4/16/19 18:01
JLB
P9D0298
Methylene Chloride
BRL
mg/kg dry
0.0071
0.0012
1
8260B
4/16/19 18:01
JLB
P9D0298
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0071
0.0010
1
8260B
4/16/19 18:01
JLB
P9D0298
Naphthalene
BRL
mg/kg dry
0.014
0.00072
1
8260B
4/16/19 18:01
JLB
P9D0298
n-Butylbenzene
BRL
mg/kg dry
0.0071
0.00067
1
8260B
4/16/19 18:01
JLB
P9D0298
n-Propylbenzene
BRL
mg/kg dry
0.0071
0.0010
1
8260B
4/16/19 18:01
JLB
P9D0298
o-Xylene
BRL
mg/kg dry
0.0071
0.00076
1
8260B
4/16/19 18:01
JLB
P9D0298
sec-Butylbenzene
BRL
mg/kg dry
0.0071
0.00077
1
8260B
4/16/19 18:01
JLB
P9D0298
Styrene
BRL
mg/kg dry
0.0071
0.00069
1
8260B
4/16/19 18:01
JLB
P9D0298
tert-Butylbenzene
BRL
mg/kg dry
0.0071
0.00085
1
8260B
4/16/19 18:01
JLB
P9D0298
Tetrachloroethylene
BRL
mg/kg dry
0.0071
0.0013
1
8260B
4/16/19 18:01
JLB
P9D0298
Toluene
BRL
mg/kg dry
0.0071
0.0011
1
8260B
4/16/19 18:01
JLB
P9D0298
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0071
0.0014
1
8260B
4/16/19 18:01
JLB
P9D0298
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0071
0.00061
1
8260B
4/16/19 18:01
JLB
P9D0298
Trichloroethylene
BRL
mg/kg dry
0.0071
0.0014
1
8260B
4/16/19 18:01
JLB
P9D0298
Trichlorofluoromethane
BRL
mg/kg dry
0.014
0.0019
1
8260B
4/16/19 18:01
JLB
P9D0298
Vinyl acetate
BRL
mg/kg dry
0.014
0.00077
1
8260B
4/16/19 18:01
JLB
P9D0298
Vinyl chloride
BRL
mg/kg dry
0.014
0.0014
1
8260B
4/16/19 18:01
JLB
P9D0298
Xylenes, total
BRL
mg/kg dry
0.021
0.0026
1
8260B
4/16/19 18:01
JLB
P9D0298
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
99 %
70-130
Dibromofluoromethane
100 %
84-123
Toluene-d8
94 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3612 & 3624 Davis Drive
Client
Sample ID:
SB-3
Attn: Dan Nielsen
Prism
Sample ID:
9040256-03
409 Rogers View Court
Prism
Work Order: 9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected: 04/15/19 10:45
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
85.2
% by
0.100
0.100
1
*SM2540 G
4/18/19 9:30
KBS
P9D0322
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.39
0.060
1
8270D
4/17/19 19:37
JMV
P9D0300
1,2-Dichlorobenzene
BRL
mg/kg dry
0.39
0.059
1
8270D
4/17/19 19:37
JMV
P9D0300
1,3-Dichlorobenzene
BRL
mg/kg dry
0.39
0.054
1
8270D
4/17/19 19:37
JMV
P9D0300
1,4-Dichlorobenzene
BRL
mg/kg dry
0.39
0.057
1
8270D
4/17/19 19:37
JMV
P9D0300
1-Methyl naphthalene
BRL
mg/kg dry
0.39
0.075
1
8270D
4/17/19 19:37
JMV
P9D0300
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.39
0.062
1
8270D
4/17/19 19:37
JMV
P9D0300
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.39
0.073
1
8270D
4/17/19 19:37
JMV
P9D0300
2,4-Dichlorophenol
BRL
mg/kg dry
0.39
0.075
1
8270D
4/17/19 19:37
JMV
P9D0300
2,4-Dimethylphenol
BRL
mg/kg dry
0.39
0.059
1
8270D
4/17/19 19:37
JMV
P9D0300
2,4-Dinitrophenol
BRL
mg/kg dry
0.39
0.054
1
8270D
4/17/19 19:37
JMV
P9D0300
2,4-Dinitrotoluene
BRL
mg/kg dry
0.39
0.047
1
8270D
4/17/19 19:37
JMV
P9D0300
2,6-Dinitrotoluene
BRL
mg/kg dry
0.39
0.051
1
8270D
4/17/19 19:37
JMV
P9D0300
2-Chloronaphthalene
BRL
mg/kg dry
0.39
0.056
1
8270D
4/17/19 19:37
JMV
P9D0300
2-Chlorophenol
BRL
mg/kg dry
0.39
0.055
1
8270D
4/17/19 19:37
JMV
P9D0300
2-Methyl naphthalene
BRL
mg/kg dry
0.39
0.062
1
8270D
4/17/19 19:37
JMV
P9D0300
2-Methylphenol
BRL
mg/kg dry
0.39
0.050
1
8270D
4/17/19 19:37
JMV
P9D0300
2-Nitrophenol
BRL
mg/kg dry
0.39
0.070
1
8270D
4/17/19 19:37
JMV
P9D0300
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.39
0.076
1
8270D
4/17/19 19:37
JMV
P9D0300
3/4-Methyl phenol
BRL
mg/kg dry
0.39
0.048
1
8270D
4/17/19 19:37
JMV
P9D0300
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.39
0.058
1
8270D
4/17/19 19:37
JMV
P9D0300
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.39
0.066
1
8270D
4/17/19 19:37
JMV
P9D0300
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.39
0.054
1
8270D
4/17/19 19:37
JMV
P9D0300
4-Chloroaniline
BRL
mg/kg dry
0.39
0.047
1
8270D
4/17/19 19:37
JMV
P9D0300
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.39
0.050
1
8270D
4/17/19 19:37
JMV
P9D0300
4-Nitrophenol
BRL
mg/kg dry
0.39
0.060
1
8270D
4/17/19 19:37
JMV
P9D0300
Acenaphthene
BRL
mg/kg dry
0.39
0.053
1
8270D
4/17/19 19:37
JMV
P9D0300
Acenaphthylene
BRL
mg/kg dry
0.39
0.056
1
8270D
4/17/19 19:37
JMV
P9D0300
Anthracene
BRL
mg/kg dry
0.39
0.062
1
8270D
4/17/19 19:37
JMV
P9D0300
Azobenzene
BRL
mg/kg dry
0.39
0.051
1
8270D
4/17/19 19:37
JMV
P9D0300
Benzo(a)anthracene
BRL
mg/kg dry
0.39
0.051
1
8270D
4/17/19 19:37
JMV
P9D0300
Benzo(a)pyrene
BRL
mg/kg dry
0.39
0.042
1
8270D
4/17/19 19:37
JMV
P9D0300
Benzo(b)fluoranthene
BRL
mg/kg dry
0.39
0.045
1
8270D
4/17/19 19:37
JMV
P9D0300
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.39
0.042
1
8270D
4/17/19 19:37
JMV
P9D0300
Benzo(k)fluoranthene
BRL
mg/kg dry
0.39
0.051
1
8270D
4/17/19 19:37
JMV
P9D0300
Benzoic Acid
BRL
mg/kg dry
0.39
0.033
1
8270D
4/17/19 19:37
JMV
P9D0300
Benzyl alcohol
BRL
mg/kg dry
0.39
0.051
1
8270D
4/17/19 19:37
JMV
P9D0300
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.39
0.067
1
8270D
4/17/19 19:37
JMV
P9D0300
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.39
0.055
1
8270D
4/17/19 19:37
JMV
P9D0300
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.39
0.066
1
8270D
4/17/19 19:37
JMV
P9D0300
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
04/22/2019
Mid -Atlantic Associates,
Inc. - Raleigh
Project: 3612 & 3624
Davis Drive
Client Sample ID: SB-3
Attn: Dan Nielsen
Prism Sample ID: 9040256-03
409 Rogers View Court
Prism Work Order:
9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
04/15/19 10:45
Time Submitted:
04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.39
0.057
1
8270D
4/17/19 19:37
JMV
P9D0300
Butyl benzyl phthalate
BRL
mg/kg dry
0.39
0.055
1
8270D
4/17/19 19:37
JMV
P9D0300
Chrysene
BRL
mg/kg dry
0.39
0.049
1
8270D
4/17/19 19:37
JMV
P9D0300
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.39
0.047
1
8270D
4/17/19 19:37
JMV
P9D0300
Dibenzofuran
BRL
mg/kg dry
0.39
0.059
1
8270D
4/17/19 19:37
JMV
P9D0300
Diethyl phthalate
BRL
mg/kg dry
0.39
0.053
1
8270D
4/17/19 19:37
JMV
P9D0300
Dimethyl phthalate
BRL
mg/kg dry
0.39
0.051
1
8270D
4/17/19 19:37
JMV
P9D0300
Di-n-butyl phthalate
BRL
mg/kg dry
0.39
0.055
1
8270D
4/17/19 19:37
JMV
P9D0300
Di-n-octyl phthalate
BRL
mg/kg dry
0.39
0.048
1
8270D
4/17/19 19:37
JMV
P9D0300
Fluoranthene
BRL
mg/kg dry
0.39
0.049
1
8270D
4/17/19 19:37
JMV
P9D0300
Fluorene
BRL
mg/kg dry
0.39
0.056
1
8270D
4/17/19 19:37
JMV
P9D0300
Hexachlorobenzene
BRL
mg/kg dry
0.39
0.061
1
8270D
4/17/19 19:37
JMV
P9D0300
Hexachlorobutadiene
BRL
mg/kg dry
0.39
0.069
1
8270D
4/17/19 19:37
JMV
P9D0300
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.39
0.069
1
8270D
4/17/19 19:37
JMV
P9D0300
Hexachloroethane
BRL
mg/kg dry
0.39
0.065
1
8270D
4/17/19 19:37
JMV
P9D0300
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.39
0.044
1
8270D
4/17/19 19:37
JMV
P9D0300
Isophorone
BRL
mg/kg dry
0.39
0.052
1
8270D
4/17/19 19:37
JMV
P9D0300
Naphthalene
BRL
mg/kg dry
0.39
0.062
1
8270D
4/17/19 19:37
JMV
P9D0300
Nitrobenzene
BRL
mg/kg dry
0.39
0.055
1
8270D
4/17/19 19:37
JMV
P9D0300
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.39
0.061
1
8270D
4/17/19 19:37
JMV
P9D0300
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.39
0.059
1
8270D
4/17/19 19:37
JMV
P9D0300
Pentachlorophenol
BRL
mg/kg dry
0.39
0.046
1
8270D
4/17/19 19:37
JMV
P9D0300
Phenanthrene
BRL
mg/kg dry
0.39
0.050
1
8270D
4/17/19 19:37
JMV
P9D0300
Phenol
BRL
mg/kg dry
0.39
0.057
1
8270D
4/17/19 19:37
JMV
P9D0300
Pyrene
BRL
mg/kg dry
0.39
0.051
1
8270D
4/17/19 19:37
JMV
P9D0300
Pyridine
BRL
mg/kg dry
0.39
0.067
1
8270D
4/17/19 19:37
JMV
P9D0300
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
93 %
39-132
2-Fluorobiphenyl
86 %
44-115
2-Fluorophenol
83 %
35-115
Nitrobenzene-d5
78 %
37-122
Phenol-d5
80 %
34-121
Terphenyl-d14
90 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.059
0.020
1
*7471B
4/18/19 11:41
MMR
P9D0323
Arsenic
1.9
mg/kg dry
1.2
0.15
1
*6010D
4/18/19 11:17
JAB
P91010297
Barium
35
mg/kg dry
12
3.5
1
*6010D
4/18/19 11:17
JAB
P9D0297
Cadmium
BRL
mg/kg dry
0.59
0.040
1
*6010D
4/18/19 11:17
JAB
P9D0297
Chromium
14
mg/kg dry
1.2
0.089
1
*6010D
4/18/19 11:17
JAB
P9D0297
Lead
20
mg/kg dry
1.2
0.20
1
*6010D
4/18/19 11:17
JAB
P9D0297
Selenium
BRL
mg/kg dry
1.2
0.32
1
*6010D
4/18/19 11:17
JAB
P9D0297
Silver
BRL
mg/kg dry
0.59
0.036
1
*6010D
4/18/19 11:17
JAB
P9D0297
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Solid
Client Sample ID: SB-3
Prism Sample ID: 9040256-03
Prism Work Order: 9040256
Time Collected: 04/15/19 10:45
Time Submitted: 04/16/19 09:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0047
0.00058
1
8260B
4/16/19 18:31
JLB
P9D0298
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0047
0.00069
1
8260B
4/16/19 18:31
JLB
P9D0298
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0047
0.00034
1
8260B
4/16/19 18:31
JLB
P9D0298
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0047
0.00051
1
8260B
4/16/19 18:31
JLB
P9D0298
1,1-Dichloroethane
BRL
mg/kg dry
0.0047
0.00085
1
8260B
4/16/19 18:31
JLB
P9D0298
1,1-Dichloroethylene
BRL
mg/kg dry
0.0047
0.00086
1
8260B
4/16/19 18:31
JLB
P9D0298
1,1-Dichloropropylene
BRL
mg/kg dry
0.0047
0.00073
1
8260B
4/16/19 18:31
JLB
P9D0298
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0094
0.00067
1
8260B
4/16/19 18:31
JLB
P9D0298
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0047
0.00054
1
8260B
4/16/19 18:31
JLB
P9D0298
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0094
0.00045
1
8260B
4/16/19 18:31
JLB
P9D0298
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0047
0.00050
1
8260B
4/16/19 18:31
JLB
P9D0298
1,2-Dibromoethane
BRL
mg/kg dry
0.0047
0.00042
1
8260B
4/16/19 18:31
JLB
P9D0298
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0047
0.00053
1
8260B
4/16/19 18:31
JLB
P9D0298
1,2-Dichloroethane
BRL
mg/kg dry
0.0047
0.00056
1
8260B
4/16/19 18:31
JLB
P9D0298
1,2-Dichloropropane
BRL
mg/kg dry
0.0047
0.00071
1
8260B
4/16/19 18:31
JLB
P9D0298
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0047
0.00059
1
8260B
4/16/19 18:31
JLB
P9D0298
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0047
0.00059
1
8260B
4/16/19 18:31
JLB
P9D0298
1,3-Dichloropropane
BRL
mg/kg dry
0.0047
0.00039
1
8260B
4/16/19 18:31
JLB
P9D0298
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0047
0.00060
1
8260B
4/16/19 18:31
JLB
P9D0298
2,2-Dichloropropane
BRL
mg/kg dry
0.0047
0.00059
1
8260B
4/16/19 18:31
JLB
P9D0298
2-Chlorotoluene
BRL
mg/kg dry
0.0047
0.00063
1
8260B
4/16/19 18:31
JLB
P9D0298
4-Chlorotoluene
BRL
mg/kg dry
0.0047
0.00054
1
8260B
4/16/19 18:31
JLB
P9D0298
4-Isopropyltoluene
BRL
mg/kg dry
0.0047
0.0012
1
8260B
4/16/19 18:31
JLB
P9D0298
Acetone
BRL
mg/kg dry
0.019
0.0012
1
8260B
4/16/19 18:31
JLB
P9D0298
Benzene
BRL
mg/kg dry
0.0047
0.00073
1
8260B
4/16/19 18:31
JLB
P9D0298
Bromobenzene
BRL
mg/kg dry
0.0047
0.00065
1
8260B
4/16/19 18:31
JLB
P9D0298
Bromochloromethane
BRL
mg/kg dry
0.0047
0.00077
1
8260B
4/16/19 18:31
JLB
P9D0298
Bromodichloromethane
BRL
mg/kg dry
0.0047
0.00045
1
8260B
4/16/19 18:31
JLB
P9D0298
Bromoform
BRL
mg/kg dry
0.0047
0.00036
1
8260B
4/16/19 18:31
JLB
P9D0298
Bromomethane
BRL
mg/kg dry
0.0094
0.0023
1
8260B
4/16/19 18:31
JLB
P9D0298
Carbon Tetrachloride
BRL
mg/kg dry
0.0047
0.00093
1
8260B
4/16/19 18:31
JLB
P9D0298
Chlorobenzene
BRL
mg/kg dry
0.0047
0.00074
1
8260B
4/16/19 18:31
JLB
P9D0298
Chloroethane
BRL
mg/kg dry
0.0094
0.00090
1
8260B
4/16/19 18:31
JLB
P9D0298
Chloroform
BRL
mg/kg dry
0.0047
0.00058
1
8260B
4/16/19 18:31
JLB
P9D0298
Chloromethane
BRL
mg/kg dry
0.0094
0.0014
1
8260B
4/16/19 18:31
JLB
P9D0298
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0047
0.00074
1
8260B
4/16/19 18:31
JLB
P9D0298
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0047
0.00046
1
8260B
4/16/19 18:31
JLB
P9D0298
Dibromochloromethane
BRL
mg/kg dry
0.0047
0.00032
1
8260B
4/16/19 18:31
JLB
P9D0298
Dichlorodifluoromethane
BRL
mg/kg dry
0.0094
0.0013
1
8260B
4/16/19 18:31
JLB
P9D0298
Ethylbenzene
BRL
mg/kg dry
0.0047
0.00071
1
8260B
4/16/19 18:31
JLB
P9D0298
Isopropyl Ether
BRL
mg/kg dry
0.0047
0.00069
1
8260B
4/16/19 18:31
JLB
P9D0298
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0047
0.00055
1
8260B
4/16/19 18:31
JLB
P9D0298
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: SB-3
Attn: Dan Nielsen Prism Sample ID: 9040256-03
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 04/15/19 10:45
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.0094
0.0012
1
8260B
4/16/19 18:31
JLB
P9D0298
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.019
0.00033
1
8260B
4/16/19 18:31
JLB
P9D0298
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.019
0.0011
1
8260B
4/16/19 18:31
JLB
P9D0298
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.019
0.00038
1
8260B
4/16/19 18:31
JLB
P9D0298
Methylene Chloride
BRL
mg/kg dry
0.0047
0.00076
1
8260B
4/16/19 18:31
JLB
P9D0298
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0047
0.00066
1
8260B
4/16/19 18:31
JLB
P9D0298
Naphthalene
BRL
mg/kg dry
0.0094
0.00048
1
8260B
4/16/19 18:31
JLB
P9D0298
n-Butylbenzene
BRL
mg/kg dry
0.0047
0.00044
1
8260B
4/16/19 18:31
JLB
P9D0298
n-Propylbenzene
BRL
mg/kg dry
0.0047
0.00068
1
8260B
4/16/19 18:31
JLB
P9D0298
o-Xylene
BRL
mg/kg dry
0.0047
0.00050
1
8260B
4/16/19 18:31
JLB
P9D0298
sec-Butylbenzene
BRL
mg/kg dry
0.0047
0.00051
1
8260B
4/16/19 18:31
JLB
P9D0298
Styrene
BRL
mg/kg dry
0.0047
0.00046
1
8260B
4/16/19 18:31
JLB
P9D0298
tert-Butylbenzene
BRL
mg/kg dry
0.0047
0.00056
1
8260B
4/16/19 18:31
JLB
P9D0298
Tetrachloroethylene
BRL
mg/kg dry
0.0047
0.00085
1
8260B
4/16/19 18:31
JLB
P9D0298
Toluene
BRL
mg/kg dry
0.0047
0.00075
1
8260B
4/16/19 18:31
JLB
P9D0298
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0047
0.00090
1
8260B
4/16/19 18:31
JLB
P9D0298
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0047
0.00040
1
8260B
4/16/19 18:31
JLB
P9D0298
Trichloroethylene
BRL
mg/kg dry
0.0047
0.00091
1
8260B
4/16/19 18:31
JLB
P9D0298
Trichlorofluoromethane
BRL
mg/kg dry
0.0094
0.0013
1
8260B
4/16/19 18:31
JLB
P9D0298
Vinyl acetate
BRL
mg/kg dry
0.0094
0.00051
1
8260B
4/16/19 18:31
JLB
P9D0298
Vinyl chloride
BRL
mg/kg dry
0.0094
0.00093
1
8260B
4/16/19 18:31
JLB
P9D0298
Xylenes, total
BRL
mg/kg dry
0.014
0.0017
1
8260B
4/16/19 18:31
JLB
P9D0298
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
97 %
70-130
Dibromofluoromethane
100 %
84-123
Toluene-d8
91 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3612 & 3624 Davis Drive
Client
Sample ID:
SB-4
Attn: Dan Nielsen
Prism
Sample ID:
9040256-04
409 Rogers View Court
Prism
Work Order: 9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected: 04/15/19 14:25
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
82.4
% by
0.100
0.100
1
*SM2540 G
4/18/19 9:30
KBS
P9D0322
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.40
0.062
1
8270D
4/17/19 19:59
JMV
P9D0300
1,2-Dichlorobenzene
BRL
mg/kg dry
0.40
0.061
1
8270D
4/17/19 19:59
JMV
P9D0300
1,3-Dichlorobenzene
BRL
mg/kg dry
0.40
0.056
1
8270D
4/17/19 19:59
JMV
P9D0300
1,4-Dichlorobenzene
BRL
mg/kg dry
0.40
0.059
1
8270D
4/17/19 19:59
JMV
P9D0300
1-Methyl naphthalene
BRL
mg/kg dry
0.40
0.077
1
8270D
4/17/19 19:59
JMV
P9D0300
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.40
0.065
1
8270D
4/17/19 19:59
JMV
P9D0300
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.40
0.075
1
8270D
4/17/19 19:59
JMV
P9D0300
2,4-Dichlorophenol
BRL
mg/kg dry
0.40
0.077
1
8270D
4/17/19 19:59
JMV
P9D0300
2,4-Dimethylphenol
BRL
mg/kg dry
0.40
0.061
1
8270D
4/17/19 19:59
JMV
P9D0300
2,4-Dinitrophenol
BRL
mg/kg dry
0.40
0.056
1
8270D
4/17/19 19:59
JMV
P9D0300
2,4-Dinitrotoluene
BRL
mg/kg dry
0.40
0.049
1
8270D
4/17/19 19:59
JMV
P9D0300
2,6-Dinitrotoluene
BRL
mg/kg dry
0.40
0.053
1
8270D
4/17/19 19:59
JMV
P9D0300
2-Chloronaphthalene
BRL
mg/kg dry
0.40
0.058
1
8270D
4/17/19 19:59
JMV
P9D0300
2-Chlorophenol
BRL
mg/kg dry
0.40
0.057
1
8270D
4/17/19 19:59
JMV
P9D0300
2-Methyl naphthalene
BRL
mg/kg dry
0.40
0.064
1
8270D
4/17/19 19:59
JMV
P9D0300
2-Methylphenol
BRL
mg/kg dry
0.40
0.051
1
8270D
4/17/19 19:59
JMV
P9D0300
2-Nitrophenol
BRL
mg/kg dry
0.40
0.073
1
8270D
4/17/19 19:59
JMV
P9D0300
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.40
0.079
1
8270D
4/17/19 19:59
JMV
P9D0300
3/4-Methyl phenol
BRL
mg/kg dry
0.40
0.049
1
8270D
4/17/19 19:59
JMV
P9D0300
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.40
0.060
1
8270D
4/17/19 19:59
JMV
P9D0300
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.40
0.069
1
8270D
4/17/19 19:59
JMV
P9D0300
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.40
0.056
1
8270D
4/17/19 19:59
JMV
P9D0300
4-Chloroaniline
BRL
mg/kg dry
0.40
0.048
1
8270D
4/17/19 19:59
JMV
P9D0300
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.40
0.052
1
8270D
4/17/19 19:59
JMV
P9D0300
4-Nitrophenol
BRL
mg/kg dry
0.40
0.062
1
8270D
4/17/19 19:59
JMV
P9D0300
Acenaphthene
BRL
mg/kg dry
0.40
0.054
1
8270D
4/17/19 19:59
JMV
P9D0300
Acenaphthylene
BRL
mg/kg dry
0.40
0.058
1
8270D
4/17/19 19:59
JMV
P9D0300
Anthracene
BRL
mg/kg dry
0.40
0.065
1
8270D
4/17/19 19:59
JMV
P9D0300
Azobenzene
BRL
mg/kg dry
0.40
0.053
1
8270D
4/17/19 19:59
JMV
P9D0300
Benzo(a)anthracene
BRL
mg/kg dry
0.40
0.052
1
8270D
4/17/19 19:59
JMV
P9D0300
Benzo(a)pyrene
BRL
mg/kg dry
0.40
0.043
1
8270D
4/17/19 19:59
JMV
P9D0300
Benzo(b)fluoranthene
BRL
mg/kg dry
0.40
0.046
1
8270D
4/17/19 19:59
JMV
P9D0300
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.40
0.044
1
8270D
4/17/19 19:59
JMV
P9D0300
Benzo(k)fluoranthene
BRL
mg/kg dry
0.40
0.053
1
8270D
4/17/19 19:59
JMV
P9D0300
Benzoic Acid
BRL
mg/kg dry
0.40
0.034
1
8270D
4/17/19 19:59
JMV
P9D0300
Benzyl alcohol
BRL
mg/kg dry
0.40
0.053
1
8270D
4/17/19 19:59
JMV
P9D0300
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.40
0.069
1
8270D
4/17/19 19:59
JMV
P9D0300
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.40
0.057
1
8270D
4/17/19 19:59
JMV
P9D0300
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.40
0.068
1
8270D
4/17/19 19:59
JMV
P9D0300
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
04/22/2019
Mid -Atlantic Associates,
Inc. - Raleigh
Project: 3612 & 3624
Davis Drive
Client Sample ID: SB-4
Attn: Dan Nielsen
Prism Sample ID: 9040256-04
409 Rogers View Court
Prism Work Order: 9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
04/15/19 14:25
Time Submitted:
04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.40
0.059
1
8270D
4/17/19 19:59
JMV
P9D0300
Butyl benzyl phthalate
BRL
mg/kg dry
0.40
0.057
1
8270D
4/17/19 19:59
JMV
P9D0300
Chrysene
BRL
mg/kg dry
0.40
0.050
1
8270D
4/17/19 19:59
JMV
P9D0300
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.40
0.049
1
8270D
4/17/19 19:59
JMV
P9D0300
Dibenzofuran
BRL
mg/kg dry
0.40
0.061
1
8270D
4/17/19 19:59
JMV
P9D0300
Diethyl phthalate
BRL
mg/kg dry
0.40
0.055
1
8270D
4/17/19 19:59
JMV
P9D0300
Dimethyl phthalate
BRL
mg/kg dry
0.40
0.053
1
8270D
4/17/19 19:59
JMV
P9D0300
Di-n-butyl phthalate
BRL
mg/kg dry
0.40
0.057
1
8270D
4/17/19 19:59
JMV
P9D0300
Di-n-octyl phthalate
BRL
mg/kg dry
0.40
0.049
1
8270D
4/17/19 19:59
JMV
P9D0300
Fluoranthene
BRL
mg/kg dry
0.40
0.051
1
8270D
4/17/19 19:59
JMV
P9D0300
Fluorene
BRL
mg/kg dry
0.40
0.057
1
8270D
4/17/19 19:59
JMV
P9D0300
Hexachlorobenzene
BRL
mg/kg dry
0.40
0.064
1
8270D
4/17/19 19:59
JMV
P9D0300
Hexachlorobutadiene
BRL
mg/kg dry
0.40
0.072
1
8270D
4/17/19 19:59
JMV
P9D0300
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.40
0.071
1
8270D
4/17/19 19:59
JMV
P9D0300
Hexachloroethane
BRL
mg/kg dry
0.40
0.067
1
8270D
4/17/19 19:59
JMV
P9D0300
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.40
0.046
1
8270D
4/17/19 19:59
JMV
P9D0300
Isophorone
BRL
mg/kg dry
0.40
0.054
1
8270D
4/17/19 19:59
JMV
P9D0300
Naphthalene
BRL
mg/kg dry
0.40
0.064
1
8270D
4/17/19 19:59
JMV
P9D0300
Nitrobenzene
BRL
mg/kg dry
0.40
0.057
1
8270D
4/17/19 19:59
JMV
P9D0300
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.40
0.063
1
8270D
4/17/19 19:59
JMV
P9D0300
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.40
0.061
1
8270D
4/17/19 19:59
JMV
P9D0300
Pentachlorophenol
BRL
mg/kg dry
0.40
0.047
1
8270D
4/17/19 19:59
JMV
P9D0300
Phenanthrene
BRL
mg/kg dry
0.40
0.052
1
8270D
4/17/19 19:59
JMV
P9D0300
Phenol
BRL
mg/kg dry
0.40
0.059
1
8270D
4/17/19 19:59
JMV
P9D0300
Pyrene
BRL
mg/kg dry
0.40
0.053
1
8270D
4/17/19 19:59
JMV
P9D0300
Pyridine
BRL
mg/kg dry
0.40
0.070
1
8270D
4/17/19 19:59
JMV
P9D0300
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
101 %
39-132
2-Fluorobiphenyl
92 %
44-115
2-Fluorophenol
89 %
35-115
Nitrobenzene-d5
82 %
37-122
Phenol-d5
85 %
34-121
Terphenyl-d14
94 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.061
0.021
1
*7471B
4/18/19 11:46
MMR
P9D0323
Arsenic
1.6
mg/kg dry
1.2
0.16
1
*6010D
4/18/19 11:26
JAB
P91010297
Barium
37
mg/kg dry
12
3.6
1
*6010D
4/18/19 11:26
JAB
P9D0297
Cadmium
BRL
mg/kg dry
0.61
0.041
1
*6010D
4/18/19 11:26
JAB
P9D0297
Chromium
8.6
mg/kg dry
1.2
0.092
1
*6010D
4/18/19 11:26
JAB
P9D0297
Lead
8.8
mg/kg dry
1.2
0.20
1
*6010D
4/18/19 11:26
JAB
P9D0297
Selenium
BRL
mg/kg dry
1.2
0.33
1
*6010D
4/18/19 11:26
JAB
P9D0297
Silver
BRL
mg/kg dry
0.61
0.037
1
*6010D
4/18/19 11:26
JAB
P9D0297
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Solid
Client Sample ID: SB-4
Prism Sample ID: 9040256-04
Prism Work Order: 9040256
Time Collected: 04/15/19 14:25
Time Submitted: 04/16/19 09:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0050
0.00061
1
8260B
4/16/19 19:01
JLB
P9D0298
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0050
0.00073
1
8260B
4/16/19 19:01
JLB
P9D0298
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0050
0.00036
1
8260B
4/16/19 19:01
JLB
P9D0298
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0050
0.00054
1
8260B
4/16/19 19:01
JLB
P9D0298
1,1-Dichloroethane
BRL
mg/kg dry
0.0050
0.00090
1
8260B
4/16/19 19:01
JLB
P9D0298
1,1-Dichloroethylene
BRL
mg/kg dry
0.0050
0.00092
1
8260B
4/16/19 19:01
JLB
P9D0298
1,1-Dichloropropylene
BRL
mg/kg dry
0.0050
0.00077
1
8260B
4/16/19 19:01
JLB
P9D0298
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.010
0.00072
1
8260B
4/16/19 19:01
JLB
P9D0298
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0050
0.00057
1
8260B
4/16/19 19:01
JLB
P9D0298
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.010
0.00048
1
8260B
4/16/19 19:01
JLB
P9D0298
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0050
0.00053
1
8260B
4/16/19 19:01
JLB
P9D0298
1,2-Dibromoethane
BRL
mg/kg dry
0.0050
0.00045
1
8260B
4/16/19 19:01
JLB
P9D0298
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0050
0.00056
1
8260B
4/16/19 19:01
JLB
P9D0298
1,2-Dichloroethane
BRL
mg/kg dry
0.0050
0.00059
1
8260B
4/16/19 19:01
JLB
P9D0298
1,2-Dichloropropane
BRL
mg/kg dry
0.0050
0.00075
1
8260B
4/16/19 19:01
JLB
P9D0298
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0050
0.00063
1
8260B
4/16/19 19:01
JLB
P9D0298
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0050
0.00062
1
8260B
4/16/19 19:01
JLB
P9D0298
1,3-Dichloropropane
BRL
mg/kg dry
0.0050
0.00042
1
8260B
4/16/19 19:01
JLB
P9D0298
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0050
0.00063
1
8260B
4/16/19 19:01
JLB
P9D0298
2,2-Dichloropropane
BRL
mg/kg dry
0.0050
0.00062
1
8260B
4/16/19 19:01
JLB
P9D0298
2-Chlorotoluene
BRL
mg/kg dry
0.0050
0.00067
1
8260B
4/16/19 19:01
JLB
P9D0298
4-Chlorotoluene
BRL
mg/kg dry
0.0050
0.00057
1
8260B
4/16/19 19:01
JLB
P9D0298
4-Isopropyltoluene
BRL
mg/kg dry
0.0050
0.0013
1
8260B
4/16/19 19:01
JLB
P9D0298
Acetone
0.019 J
mg/kg dry
0.020
0.0013
1
8260B
4/16/19 19:01
JLB
P900298
Benzene
BRL
mg/kg dry
0.0050
0.00078
1
8260B
4/16/19 19:01
JLB
P9D0298
Bromobenzene
BRL
mg/kg dry
0.0050
0.00069
1
8260B
4/16/19 19:01
JLB
P9D0298
Bromochloromethane
BRL
mg/kg dry
0.0050
0.00082
1
8260B
4/16/19 19:01
JLB
P9D0298
Bromodichloromethane
BRL
mg/kg dry
0.0050
0.00047
1
8260B
4/16/19 19:01
JLB
P9D0298
Bromoform
BRL
mg/kg dry
0.0050
0.00039
1
8260B
4/16/19 19:01
JLB
P9D0298
Bromomethane
BRL
mg/kg dry
0.010
0.0024
1
8260B
4/16/19 19:01
JLB
P9D0298
Carbon Tetrachloride
BRL
mg/kg dry
0.0050
0.00098
1
8260B
4/16/19 19:01
JLB
P9D0298
Chlorobenzene
BRL
mg/kg dry
0.0050
0.00078
1
8260B
4/16/19 19:01
JLB
P9D0298
Chloroethane
BRL
mg/kg dry
0.010
0.00095
1
8260B
4/16/19 19:01
JLB
P9D0298
Chloroform
BRL
mg/kg dry
0.0050
0.00061
1
8260B
4/16/19 19:01
JLB
P9D0298
Chloromethane
BRL
mg/kg dry
0.010
0.0015
1
8260B
4/16/19 19:01
JLB
P9D0298
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0050
0.00079
1
8260B
4/16/19 19:01
JLB
P9D0298
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0050
0.00049
1
8260B
4/16/19 19:01
JLB
P9D0298
Dibromochloromethane
BRL
mg/kg dry
0.0050
0.00033
1
8260B
4/16/19 19:01
JLB
P9D0298
Dichlorodifluoromethane
BRL
mg/kg dry
0.010
0.0014
1
8260B
4/16/19 19:01
JLB
P9D0298
Ethylbenzene
BRL
mg/kg dry
0.0050
0.00075
1
8260B
4/16/19 19:01
JLB
P9D0298
Isopropyl Ether
BRL
mg/kg dry
0.0050
0.00073
1
8260B
4/16/19 19:01
JLB
P9D0298
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0050
0.00058
1
8260B
4/16/19 19:01
JLB
P9D0298
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: SB-4
Attn: Dan Nielsen Prism Sample ID: 9040256-04
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 04/15/19 14:25
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.010
0.0013
1
8260B
4/16/19 19:01
JLB
P9D0298
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.020
0.00035
1
8260B
4/16/19 19:01
JLB
P9D0298
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.020
0.0012
1
8260B
4/16/19 19:01
JLB
P9D0298
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.020
0.00041
1
8260B
4/16/19 19:01
JLB
P9D0298
Methylene Chloride
BRL
mg/kg dry
0.0050
0.00081
1
8260B
4/16/19 19:01
JLB
P9D0298
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0050
0.00070
1
8260B
4/16/19 19:01
JLB
P9D0298
Naphthalene
BRL
mg/kg dry
0.010
0.00050
1
8260B
4/16/19 19:01
JLB
P9D0298
n-Butylbenzene
BRL
mg/kg dry
0.0050
0.00047
1
8260B
4/16/19 19:01
JLB
P9D0298
n-Propylbenzene
BRL
mg/kg dry
0.0050
0.00072
1
8260B
4/16/19 19:01
JLB
P9D0298
o-Xylene
BRL
mg/kg dry
0.0050
0.00053
1
8260B
4/16/19 19:01
JLB
P9D0298
sec-Butylbenzene
BRL
mg/kg dry
0.0050
0.00054
1
8260B
4/16/19 19:01
JLB
P9D0298
Styrene
BRL
mg/kg dry
0.0050
0.00048
1
8260B
4/16/19 19:01
JLB
P9D0298
tert-Butylbenzene
BRL
mg/kg dry
0.0050
0.00059
1
8260B
4/16/19 19:01
JLB
P9D0298
Tetrachloroethylene
BRL
mg/kg dry
0.0050
0.00090
1
8260B
4/16/19 19:01
JLB
P9D0298
Toluene
BRL
mg/kg dry
0.0050
0.00080
1
8260B
4/16/19 19:01
JLB
P9D0298
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0050
0.00096
1
8260B
4/16/19 19:01
JLB
P9D0298
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0050
0.00043
1
8260B
4/16/19 19:01
JLB
P9D0298
Trichloroethylene
BRL
mg/kg dry
0.0050
0.00097
1
8260B
4/16/19 19:01
JLB
P9D0298
Trichlorofluoromethane
BRL
mg/kg dry
0.010
0.0013
1
8260B
4/16/19 19:01
JLB
P9D0298
Vinyl acetate
BRL
mg/kg dry
0.010
0.00054
1
8260B
4/16/19 19:01
JLB
P9D0298
Vinyl chloride
BRL
mg/kg dry
0.010
0.00099
1
8260B
4/16/19 19:01
JLB
P9D0298
Xylenes, total
BRL
mg/kg dry
0.015
0.0018
1
8260B
4/16/19 19:01
JLB
P9D0298
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
99 %
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
93 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3612 & 3624 Davis Drive
Client
Sample ID:
SB-5
Attn: Dan Nielsen
Prism
Sample ID:
9040256-05
409 Rogers View Court
Prism
Work Order: 9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected: 04/15/19 12:00
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
86.3
% by
0.100
0.100
1
*SM2540 G
4/18/19 9:30
KBS
P9D0322
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.38
0.059
1
8270D
4/17/19 20:21
JMV
P9D0300
1,2-Dichlorobenzene
BRL
mg/kg dry
0.38
0.058
1
8270D
4/17/19 20:21
JMV
P9D0300
1,3-Dichlorobenzene
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:21
JMV
P9D0300
1,4-Dichlorobenzene
BRL
mg/kg dry
0.38
0.056
1
8270D
4/17/19 20:21
JMV
P9D0300
1-Methyl naphthalene
BRL
mg/kg dry
0.38
0.073
1
8270D
4/17/19 20:21
JMV
P9D0300
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.38
0.061
1
8270D
4/17/19 20:21
JMV
P9D0300
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.38
0.071
1
8270D
4/17/19 20:21
JMV
P9D0300
2,4-Dichlorophenol
BRL
mg/kg dry
0.38
0.074
1
8270D
4/17/19 20:21
JMV
P9D0300
2,4-Dimethylphenol
BRL
mg/kg dry
0.38
0.058
1
8270D
4/17/19 20:21
JMV
P9D0300
2,4-Dinitrophenol
BRL
mg/kg dry
0.38
0.053
1
8270D
4/17/19 20:21
JMV
P9D0300
2,4-Dinitrotoluene
BRL
mg/kg dry
0.38
0.046
1
8270D
4/17/19 20:21
JMV
P9D0300
2,6-Dinitrotoluene
BRL
mg/kg dry
0.38
0.051
1
8270D
4/17/19 20:21
JMV
P9D0300
2-Chloronaphthalene
BRL
mg/kg dry
0.38
0.055
1
8270D
4/17/19 20:21
JMV
P9D0300
2-Chlorophenol
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:21
JMV
P9D0300
2-Methyl naphthalene
BRL
mg/kg dry
0.38
0.061
1
8270D
4/17/19 20:21
JMV
P9D0300
2-Methylphenol
BRL
mg/kg dry
0.38
0.049
1
8270D
4/17/19 20:21
JMV
P9D0300
2-Nitrophenol
BRL
mg/kg dry
0.38
0.069
1
8270D
4/17/19 20:21
JMV
P9D0300
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.38
0.075
1
8270D
4/17/19 20:21
JMV
P9D0300
3/4-Methyl phenol
BRL
mg/kg dry
0.38
0.047
1
8270D
4/17/19 20:21
JMV
P9D0300
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.38
0.057
1
8270D
4/17/19 20:21
JMV
P9D0300
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.38
0.065
1
8270D
4/17/19 20:21
JMV
P9D0300
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.38
0.053
1
8270D
4/17/19 20:21
JMV
P9D0300
4-Chloroaniline
BRL
mg/kg dry
0.38
0.046
1
8270D
4/17/19 20:21
JMV
P9D0300
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.38
0.049
1
8270D
4/17/19 20:21
JMV
P9D0300
4-Nitrophenol
BRL
mg/kg dry
0.38
0.059
1
8270D
4/17/19 20:21
JMV
P9D0300
Acenaphthene
BRL
mg/kg dry
0.38
0.052
1
8270D
4/17/19 20:21
JMV
P9D0300
Acenaphthylene
BRL
mg/kg dry
0.38
0.055
1
8270D
4/17/19 20:21
JMV
P9D0300
Anthracene
BRL
mg/kg dry
0.38
0.061
1
8270D
4/17/19 20:21
JMV
P9D0300
Azobenzene
BRL
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:21
JMV
P9D0300
Benzo(a)anthracene
BRL
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:21
JMV
P9D0300
Benzo(a)pyrene
BRL
mg/kg dry
0.38
0.041
1
8270D
4/17/19 20:21
JMV
P9D0300
Benzo(b)fluoranthene
BRL
mg/kg dry
0.38
0.044
1
8270D
4/17/19 20:21
JMV
P9D0300
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.38
0.042
1
8270D
4/17/19 20:21
JMV
P9D0300
Benzo(k)fluoranthene
BRL
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:21
JMV
P9D0300
Benzoic Acid
BRL
mg/kg dry
0.38
0.032
1
8270D
4/17/19 20:21
JMV
P9D0300
Benzyl alcohol
BRL
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:21
JMV
P9D0300
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.38
0.066
1
8270D
4/17/19 20:21
JMV
P9D0300
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:21
JMV
P9D0300
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.38
0.065
1
8270D
4/17/19 20:21
JMV
P9D0300
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
P R S M
/ Environmental Solutions
LABORATORIES INC.
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3612 & 3624
Davis Drive
Client Sample ID: SB-5
Attn: Dan Nielsen
Prism Sample ID: 9040256-05
409 Rogers View Court
Prism Work Order:
9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
04/15/19 12:00
Time Submitted:
04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.38
0.057
1
8270D
4/17/19 20:21
JMV
P9D0300
Butyl benzyl phthalate
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:21
JMV
P9D0300
Chrysene
BRL
mg/kg dry
0.38
0.048
1
8270D
4/17/19 20:21
JMV
P9D0300
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.38
0.046
1
8270D
4/17/19 20:21
JMV
P9D0300
Dibenzofuran
BRL
mg/kg dry
0.38
0.058
1
8270D
4/17/19 20:21
JMV
P9D0300
Diethyl phthalate
BRL
mg/kg dry
0.38
0.052
1
8270D
4/17/19 20:21
JMV
P9D0300
Dimethyl phthalate
BRL
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:21
JMV
P9D0300
Di-n-butyl phthalate
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:21
JMV
P9D0300
Di-n-octyl phthalate
BRL
mg/kg dry
0.38
0.047
1
8270D
4/17/19 20:21
JMV
P9D0300
Fluoranthene
BRL
mg/kg dry
0.38
0.049
1
8270D
4/17/19 20:21
JMV
P9D0300
Fluorene
BRL
mg/kg dry
0.38
0.055
1
8270D
4/17/19 20:21
JMV
P9D0300
Hexachlorobenzene
BRL
mg/kg dry
0.38
0.060
1
8270D
4/17/19 20:21
JMV
P9D0300
Hexachlorobutadiene
BRL
mg/kg dry
0.38
0.068
1
8270D
4/17/19 20:21
JMV
P9D0300
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.38
0.068
1
8270D
4/17/19 20:21
JMV
P9D0300
Hexachloroethane
BRL
mg/kg dry
0.38
0.064
1
8270D
4/17/19 20:21
JMV
P9D0300
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.38
0.044
1
8270D
4/17/19 20:21
JMV
P9D0300
Isophorone
BRL
mg/kg dry
0.38
0.052
1
8270D
4/17/19 20:21
JMV
P9D0300
Naphthalene
BRL
mg/kg dry
0.38
0.061
1
8270D
4/17/19 20:21
JMV
P9D0300
Nitrobenzene
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:21
JMV
P9D0300
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.38
0.060
1
8270D
4/17/19 20:21
JMV
P9D0300
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.38
0.058
1
8270D
4/17/19 20:21
JMV
P9D0300
Pentachlorophenol
BRL
mg/kg dry
0.38
0.045
1
8270D
4/17/19 20:21
JMV
P9D0300
Phenanthrene
BRL
mg/kg dry
0.38
0.049
1
8270D
4/17/19 20:21
JMV
P9D0300
Phenol
BRL
mg/kg dry
0.38
0.056
1
8270D
4/17/19 20:21
JMV
P9D0300
Pyrene
BRL
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:21
JMV
P9D0300
Pyridine
BRL
mg/kg dry
0.38
0.066
1
8270D
4/17/19 20:21
JMV
P9D0300
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
99 %
39-132
2-Fluorobiphenyl
91 %
44-115
2-Fluorophenol
88 %
35-115
Nitrobenzene-d5
81 %
37-122
Phenol-d5
86 %
34-121
Terphenyl-d14
95 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.058
0.020
1
*7471B
4/18/19 11:51
MMR
P9D0323
Arsenic
BRL
mg/kg dry
1.2
0.15
1
*6010D
4/18/19 11:34
JAB
P9D0297
Barium
26
mg/kg dry
12
3.5
1
*6010D
4/18/19 11:34
JAB
P9D0297
Cadmium
BRL
mg/kg dry
0.58
0.039
1
*6010D
4/18/19 11:34
JAB
P9D0297
Chromium
4.8
mg/kg dry
1.2
0.088
1
*6010D
4/18/19 11:34
JAB
P9D0297
Lead
5.4
mg/kg dry
1.2
0.19
1
*60101)
4/18/19 11:34
JAB
P9D0297
Selenium
BRL
mg/kg dry
1.2
0.32
1
*6010D
4/18/19 11:34
JAB
P9D0297
Silver
BRL
mg/kg dry
0.58
0.036
1
*6010D
4/18/19 11:34
JAB
P9D0297
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Solid
Laboratory Report
04/22/2019
Client Sample ID: SB-5
Prism Sample ID: 9040256-05
Prism Work Order: 9040256
Time Collected: 04/15/19 12:00
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0045
0.00055
1
8260B
4/16/19 15:01
JLB
P9D0298
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0045
0.00066
1
8260B
4/16/19 15:01
JLB
P9D0298
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0045
0.00033
1
8260B
4/16/19 15:01
JLB
P9D0298
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0045
0.00048
1
8260B
4/16/19 15:01
JLB
P9D0298
1,1-Dichloroethane
BRL
mg/kg dry
0.0045
0.00081
1
8260B
4/16/19 15:01
JLB
P9D0298
1,1-Dichloroethylene
BRL
mg/kg dry
0.0045
0.00082
1
8260B
4/16/19 15:01
JLB
P9D0298
1,1-Dichloropropylene
BRL
mg/kg dry
0.0045
0.00069
1
8260B
4/16/19 15:01
JLB
P9D0298
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0090
0.00064
1
8260B
4/16/19 15:01
JLB
P9D0298
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0045
0.00051
1
8260B
4/16/19 15:01
JLB
P9D0298
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0090
0.00043
1
8260B
4/16/19 15:01
JLB
P9D0298
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0045
0.00048
1
8260B
4/16/19 15:01
JLB
P9D0298
1,2-Dibromoethane
BRL
mg/kg dry
0.0045
0.00040
1
8260B
4/16/19 15:01
JLB
P9D0298
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0045
0.00050
1
8260B
4/16/19 15:01
JLB
P9D0298
1,2-Dichloroethane
BRL
mg/kg dry
0.0045
0.00053
1
8260B
4/16/19 15:01
JLB
P9D0298
1,2-Dichloropropane
BRL
mg/kg dry
0.0045
0.00067
1
8260B
4/16/19 15:01
JLB
P9D0298
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0045
0.00056
1
8260B
4/16/19 15:01
JLB
P9D0298
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0045
0.00056
1
8260B
4/16/19 15:01
JLB
P9D0298
1,3-Dichloropropane
BRL
mg/kg dry
0.0045
0.00038
1
8260B
4/16/19 15:01
JLB
P9D0298
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0045
0.00057
1
8260B
4/16/19 15:01
JLB
P9D0298
2,2-Dichloropropane
BRL
mg/kg dry
0.0045
0.00056
1
8260B
4/16/19 15:01
JLB
P9D0298
2-Chlorotoluene
BRL
mg/kg dry
0.0045
0.00060
1
8260B
4/16/19 15:01
JLB
P9D0298
4-Chlorotoluene
BRL
mg/kg dry
0.0045
0.00051
1
8260B
4/16/19 15:01
JLB
P9D0298
4-Isopropyltoluene
BRL
mg/kg dry
0.0045
0.0011
1
8260B
4/16/19 15:01
JLB
P9D0298
Acetone
BRL
mg/kg dry
0.018
0.0011
1
8260B
4/16/19 15:01
JLB
P9D0298
Benzene
BRL
mg/kg dry
0.0045
0.00070
1
8260B
4/16/19 15:01
JLB
P9D0298
Bromobenzene
BRL
mg/kg dry
0.0045
0.00062
1
8260B
4/16/19 15:01
JLB
P9D0298
Bromochloromethane
BRL
mg/kg dry
0.0045
0.00074
1
8260B
4/16/19 15:01
JLB
P9D0298
Bromodichloromethane
BRL
mg/kg dry
0.0045
0.00043
1
8260B
4/16/19 15:01
JLB
P9D0298
Bromoform
BRL
mg/kg dry
0.0045
0.00035
1
8260B
4/16/19 15:01
JLB
P9D0298
Bromomethane
BRL
mg/kg dry
0.0090
0.0022
1
8260B
4/16/19 15:01
JLB
P9D0298
Carbon Tetrachloride
BRL
mg/kg dry
0.0045
0.00088
1
8260B
4/16/19 15:01
JLB
P9D0298
Chlorobenzene
BRL
mg/kg dry
0.0045
0.00070
1
8260B
4/16/19 15:01
JLB
P9D0298
Chloroethane
BRL
mg/kg dry
0.0090
0.00085
1
8260B
4/16/19 15:01
JLB
P9D0298
Chloroform
BRL
mg/kg dry
0.0045
0.00055
1
8260B
4/16/19 15:01
JLB
P9D0298
Chloromethane
BRL
mg/kg dry
0.0090
0.0014
1
8260B
4/16/19 15:01
JLB
P9D0298
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0045
0.00071
1
8260B
4/16/19 15:01
JLB
P9D0298
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0045
0.00044
1
8260B
4/16/19 15:01
JLB
P9D0298
Dibromochloromethane
BRL
mg/kg dry
0.0045
0.00030
1
8260B
4/16/19 15:01
JLB
P9D0298
Dichlorodifluoromethane
BRL
mg/kg dry
0.0090
0.0013
1
8260B
4/16/19 15:01
JLB
P9D0298
Ethylbenzene
BRL
mg/kg dry
0.0045
0.00067
1
8260B
4/16/19 15:01
JLB
P9D0298
Isopropyl Ether
BRL
mg/kg dry
0.0045
0.00066
1
8260B
4/16/19 15:01
JLB
P9D0298
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0045
0.00052
1
8260B
4/16/19 15:01
JLB
P9D0298
m,p-Xylenes
BRL
mg/kg dry
0.0090
0.0011
1
8260B
4/16/19 15:01
JLB
P9D0298
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: SB-5
Attn: Dan Nielsen Prism Sample ID: 9040256-05
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 04/15/19 12:00
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.018
0.00031
1
8260B
4/16/19 15:01
JLB
P9D0298
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.018
0.0010
1
8260B
4/16/19 15:01
JLB
P9D0298
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.018
0.00037
1
8260B
4/16/19 15:01
JLB
P9D0298
Methylene Chloride
BRL
mg/kg dry
0.0045
0.00073
1
8260B
4/16/19 15:01
JLB
P9D0298
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0045
0.00063
1
8260B
4/16/19 15:01
JLB
P9D0298
Naphthalene
BRL
mg/kg dry
0.0090
0.00045
1
8260B
4/16/19 15:01
JLB
P9D0298
n-Butylbenzene
BRL
mg/kg dry
0.0045
0.00042
1
8260B
4/16/19 15:01
JLB
P9D0298
n-Propylbenzene
BRL
mg/kg dry
0.0045
0.00065
1
8260B
4/16/19 15:01
JLB
P9D0298
o-Xylene
BRL
mg/kg dry
0.0045
0.00048
1
8260B
4/16/19 15:01
JLB
P9D0298
sec-Butylbenzene
BRL
mg/kg dry
0.0045
0.00048
1
8260B
4/16/19 15:01
JLB
P9D0298
Styrene
BRL
mg/kg dry
0.0045
0.00044
1
8260B
4/16/19 15:01
JLB
P9D0298
tert-Butylbenzene
BRL
mg/kg dry
0.0045
0.00053
1
8260B
4/16/19 15:01
JLB
P9D0298
Tetrachloroethylene
BRL
mg/kg dry
0.0045
0.00081
1
8260B
4/16/19 15:01
JLB
P9D0298
Toluene
BRL
mg/kg dry
0.0045
0.00071
1
8260B
4/16/19 15:01
JLB
P9D0298
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0045
0.00086
1
8260B
4/16/19 15:01
JLB
P9D0298
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0045
0.00038
1
8260B
4/16/19 15:01
JLB
P9D0298
Trichloroethylene
BRL
mg/kg dry
0.0045
0.00087
1
8260B
4/16/19 15:01
JLB
P9D0298
Trichlorofluoromethane
BRL
mg/kg dry
0.0090
0.0012
1
8260B
4/16/19 15:01
JLB
P9D0298
Vinyl acetate
BRL
mg/kg dry
0.0090
0.00049
1
8260B
4/16/19 15:01
JLB
P9D0298
Vinyl chloride
BRL
mg/kg dry
0.0090
0.00089
1
8260B
4/16/19 15:01
JLB
P9D0298
Xylenes, total
BRL
mg/kg dry
0.013
0.0016
1
8260B
4/16/19 15:01
JLB
P9D0298
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
98 %
70-130
Dibromofluoromethane
98 %
84-123
Toluene-d8
94 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical
&
/ Environmental Solutions
P R S M
LABORATORIES INC.
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3612 & 3624 Davis Drive
Client
Sample ID:
SB-6
Attn: Dan Nielsen
Prism
Sample ID:
9040256-06
409 Rogers View Court
Prism
Work Order: 9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected: 04/15/19 14:05
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
85.7
% by
0.100
0.100
1
*SM2540 G
4/18/19 9:30
KBS
P9D0322
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.38
0.060
1
8270D
4/17/19 20:43
JMV
P9D0300
1,2-Dichlorobenzene
BRL
mg/kg dry
0.38
0.058
1
8270D
4/17/19 20:43
JMV
P9D0300
1,3-Dichlorobenzene
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:43
JMV
P9D0300
1,4-Dichlorobenzene
BRL
mg/kg dry
0.38
0.056
1
8270D
4/17/19 20:43
JMV
P9D0300
1-Methyl naphthalene
BRL
mg/kg dry
0.38
0.074
1
8270D
4/17/19 20:43
JMV
P9D0300
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.38
0.062
1
8270D
4/17/19 20:43
JMV
P9D0300
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.38
0.072
1
8270D
4/17/19 20:43
JMV
P9D0300
2,4-Dichlorophenol
BRL
mg/kg dry
0.38
0.074
1
8270D
4/17/19 20:43
JMV
P9D0300
2,4-Dimethylphenol
BRL
mg/kg dry
0.38
0.059
1
8270D
4/17/19 20:43
JMV
P9D0300
2,4-Dinitrophenol
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:43
JMV
P9D0300
2,4-Dinitrotoluene
BRL
mg/kg dry
0.38
0.047
1
8270D
4/17/19 20:43
JMV
P9D0300
2,6-Dinitrotoluene
BRL
mg/kg dry
0.38
0.051
1
8270D
4/17/19 20:43
JMV
P9D0300
2-Chloronaphthalene
BRL
mg/kg dry
0.38
0.056
1
8270D
4/17/19 20:43
JMV
P9D0300
2-Chlorophenol
BRL
mg/kg dry
0.38
0.055
1
8270D
4/17/19 20:43
JMV
P9D0300
2-Methyl naphthalene
BRL
mg/kg dry
0.38
0.062
1
8270D
4/17/19 20:43
JMV
P9D0300
2-Methylphenol
BRL
mg/kg dry
0.38
0.049
1
8270D
4/17/19 20:43
JMV
P9D0300
2-Nitrophenol
BRL
mg/kg dry
0.38
0.070
1
8270D
4/17/19 20:43
JMV
P9D0300
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.38
0.076
1
8270D
4/17/19 20:43
JMV
P9D0300
3/4-Methyl phenol
BRL
mg/kg dry
0.38
0.047
1
8270D
4/17/19 20:43
JMV
P9D0300
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.38
0.058
1
8270D
4/17/19 20:43
JMV
P9D0300
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.38
0.066
1
8270D
4/17/19 20:43
JMV
P9D0300
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:43
JMV
P9D0300
4-Chloroaniline
BRL
mg/kg dry
0.38
0.046
1
8270D
4/17/19 20:43
JMV
P9D0300
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:43
JMV
P9D0300
4-Nitrophenol
BRL
mg/kg dry
0.38
0.059
1
8270D
4/17/19 20:43
JMV
P9D0300
Acenaphthene
BRL
mg/kg dry
0.38
0.052
1
8270D
4/17/19 20:43
JMV
P9D0300
Acenaphthylene
BRL
mg/kg dry
0.38
0.056
1
8270D
4/17/19 20:43
JMV
P9D0300
Anthracene
BRL
mg/kg dry
0.38
0.062
1
8270D
4/17/19 20:43
JMV
P9D0300
Azobenzene
BRL
mg/kg dry
0.38
0.051
1
8270D
4/17/19 20:43
JMV
P9D0300
Benzo(a)anthrace ne
0.077 J
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:43
JMV
P9D0300
Benzo(a)pyrene
0.054 J
mg/kg dry
0.38
0.042
1
8270D
4/17/19 20:43
JMV
P9D0300
Benzo(b)fluoranthene
0.17 J
mg/kg dry
0.38
0.045
1
8270D
4/17/19 20:43
JMV
P900300
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.38
0.042
1
8270D
4/17/19 20:43
JMV
P9D0300
Benzo(k)fluoranthene
BRL
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:43
JMV
P9D0300
Benzoic Acid
BRL
mg/kg dry
0.38
0.032
1
8270D
4/17/19 20:43
JMV
P9D0300
Benzyl alcohol
BRL
mg/kg dry
0.38
0.051
1
8270D
4/17/19 20:43
JMV
P9D0300
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.38
0.067
1
8270D
4/17/19 20:43
JMV
P9D0300
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.38
0.054
1
8270D
4/17/19 20:43
JMV
P9D0300
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.38
0.066
1
8270D
4/17/19 20:43
JMV
P9D0300
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
04/22/2019
Mid -Atlantic Associates,
Inc. - Raleigh Project: 3612 & 3624
Davis Drive
Client Sample ID: SB-6
Attn: Dan Nielsen
Prism Sample ID: 9040256-06
409 Rogers View Court
Prism Work Order: 9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
04/15/19 14:05
Time Submitted:
04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.38
0.057
1
8270D
4/17/19 20:43
JMV
P9D0300
Butyl benzyl phthalate
BRL
mg/kg dry
0.38
0.055
1
8270D
4/17/19 20:43
JMV
P9D0300
Chrysene
0.11 J
mg/kg dry
0.38
0.048
1
8270D
4/17/19 20:43
JMV
P9D0300
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.38
0.047
1
8270D
4/17/19 20:43
JMV
P9D0300
Dibenzofuran
BRL
mg/kg dry
0.38
0.059
1
8270D
4/17/19 20:43
JMV
P9D0300
Diethyl phthalate
BRL
mg/kg dry
0.38
0.053
1
8270D
4/17/19 20:43
JMV
P9D0300
Dimethyl phthalate
BRL
mg/kg dry
0.38
0.051
1
8270D
4/17/19 20:43
JMV
P9D0300
Di-n-butyl phthalate
BRL
mg/kg dry
0.38
0.055
1
8270D
4/17/19 20:43
JMV
P9D0300
Di-n-octyl phthalate
BRL
mg/kg dry
0.38
0.047
1
8270D
4/17/19 20:43
JMV
P9D0300
Fluoranthene
0.14 J
mg/kg dry
0.38
0.049
1
8270D
4/17/19 20:43
JMV
P9D0300
Fluorene
BRL
mg/kg dry
0.38
0.055
1
8270D
4/17/19 20:43
JMV
P9D0300
Hexachlorobenzene
BRL
mg/kg dry
0.38
0.061
1
8270D
4/17/19 20:43
JMV
P9D0300
Hexachlorobutadiene
BRL
mg/kg dry
0.38
0.069
1
8270D
4/17/19 20:43
JMV
P9D0300
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.38
0.069
1
8270D
4/17/19 20:43
JMV
P9D0300
Hexachloroethane
BRL
mg/kg dry
0.38
0.064
1
8270D
4/17/19 20:43
JMV
P9D0300
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.38
0.044
1
8270D
4/17/19 20:43
JMV
P9D0300
Isophorone
BRL
mg/kg dry
0.38
0.052
1
8270D
4/17/19 20:43
JMV
P9D0300
Naphthalene
BRL
mg/kg dry
0.38
0.062
1
8270D
4/17/19 20:43
JMV
P9D0300
Nitrobenzene
BRL
mg/kg dry
0.38
0.055
1
8270D
4/17/19 20:43
JMV
P9D0300
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.38
0.061
1
8270D
4/17/19 20:43
JMV
P9D0300
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.38
0.059
1
8270D
4/17/19 20:43
JMV
P9D0300
Pentachlorophenol
BRL
mg/kg dry
0.38
0.045
1
8270D
4/17/19 20:43
JMV
P9D0300
Phenanthrene
BRL
mg/kg dry
0.38
0.050
1
8270D
4/17/19 20:43
JMV
P9D0300
Phenol
BRL
mg/kg dry
0.38
0.057
1
8270D
4/17/19 20:43
JMV
P9D0300
Pyrene
0.24 J
mg/kg dry
0.38
0.051
1
8270D
4/17/19 20:43
JMV
P9D0300
Pyridine
BRL
mg/kg dry
0.38
0.067
1
8270D
4/17/19 20:43
JMV
P9D0300
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
100 %
39-132
2-Fluorobiphenyl
91 %
44-115
2-Fluorophenol
86 %
35-115
Nitrobenzene-d5
81 %
37-122
Phenol-d5
85 %
34-121
Terphenyl-d14
95 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.058
0.020
1
*7471B
4/18/19 11:55
MMR
P9D0323
Arsenic
2.6
mg/kg dry
1.2
0.15
1
*6010D
4/18/19 11:43
JAB
P91010297
Barium
59
mg/kg dry
12
3.5
1
*6010D
4/18/19 11:43
JAB
P9D0297
Cadmium
BRL
mg/kg dry
0.58
0.039
1
*6010D
4/18/19 11:43
JAB
P9D0297
Chromium
26
mg/kg dry
1.2
0.088
1
*6010D
4/18/19 11:43
JAB
P9D0297
Lead
9.7
mg/kg dry
1.2
0.19
1
*6010D
4/18/19 11:43
JAB
P9D0297
Selenium
BRL
mg/kg dry
1.2
0.32
1
*6010D
4/18/19 11:43
JAB
P9D0297
Silver
BRL
mg/kg dry
0.58
0.036
1
*6010D
4/18/19 11:43
JAB
P9D0297
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Solid
Client Sample ID: SB-6
Prism Sample ID: 9040256-06
Prism Work Order: 9040256
Time Collected: 04/15/19 14:05
Time Submitted: 04/16/19 09:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0055
0.00067
1
8260B
4/16/19 15:31
JLB
P9D0298
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0055
0.00080
1
8260B
4/16/19 15:31
JLB
P9D0298
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0055
0.00040
1
8260B
4/16/19 15:31
JLB
P9D0298
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0055
0.00059
1
8260B
4/16/19 15:31
JLB
P9D0298
1,1-Dichloroethane
BRL
mg/kg dry
0.0055
0.00099
1
8260B
4/16/19 15:31
JLB
P9D0298
1,1-Dichloroethylene
BRL
mg/kg dry
0.0055
0.0010
1
8260B
4/16/19 15:31
JLB
P9D0298
1,1-Dichloropropylene
BRL
mg/kg dry
0.0055
0.00084
1
8260B
4/16/19 15:31
JLB
P9D0298
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00078
1
8260B
4/16/19 15:31
JLB
P9D0298
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0055
0.00062
1
8260B
4/16/19 15:31
JLB
P9D0298
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00052
1
8260B
4/16/19 15:31
JLB
P9D0298
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0055
0.00058
1
8260B
4/16/19 15:31
JLB
P9D0298
1,2-Dibromoethane
BRL
mg/kg dry
0.0055
0.00049
1
8260B
4/16/19 15:31
JLB
P9D0298
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0055
0.00061
1
8260B
4/16/19 15:31
JLB
P9D0298
1,2-Dichloroethane
BRL
mg/kg dry
0.0055
0.00065
1
8260B
4/16/19 15:31
JLB
P9D0298
1,2-Dichloropropane
BRL
mg/kg dry
0.0055
0.00082
1
8260B
4/16/19 15:31
JLB
P9D0298
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0055
0.00069
1
8260B
4/16/19 15:31
JLB
P9D0298
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0055
0.00068
1
8260B
4/16/19 15:31
JLB
P9D0298
1,3-Dichloropropane
BRL
mg/kg dry
0.0055
0.00046
1
8260B
4/16/19 15:31
JLB
P9D0298
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0055
0.00069
1
8260B
4/16/19 15:31
JLB
P9D0298
2,2-Dichloropropane
BRL
mg/kg dry
0.0055
0.00068
1
8260B
4/16/19 15:31
JLB
P9D0298
2-Chlorotoluene
BRL
mg/kg dry
0.0055
0.00073
1
8260B
4/16/19 15:31
JLB
P9D0298
4-Chlorotoluene
BRL
mg/kg dry
0.0055
0.00062
1
8260B
4/16/19 15:31
JLB
P9D0298
4-Isopropyltoluene
BRL
mg/kg dry
0.0055
0.0014
1
8260B
4/16/19 15:31
JLB
P9D0298
Acetone
0.018 J
mg/kg dry
0.022
0.0014
1
8260B
4/16/19 15:31
JLB
P900298
Benzene
BRL
mg/kg dry
0.0055
0.00085
1
8260B
4/16/19 15:31
JLB
P9D0298
Bromobenzene
BRL
mg/kg dry
0.0055
0.00076
1
8260B
4/16/19 15:31
JLB
P9D0298
Bromochloromethane
BRL
mg/kg dry
0.0055
0.00090
1
8260B
4/16/19 15:31
JLB
P9D0298
Bromodichloromethane
BRL
mg/kg dry
0.0055
0.00052
1
8260B
4/16/19 15:31
JLB
P9D0298
Bromoform
BRL
mg/kg dry
0.0055
0.00042
1
8260B
4/16/19 15:31
JLB
P9D0298
Bromomethane
BRL
mg/kg dry
0.011
0.0027
1
8260B
4/16/19 15:31
JLB
P9D0298
Carbon Tetrachloride
BRL
mg/kg dry
0.0055
0.0011
1
8260B
4/16/19 15:31
JLB
P9D0298
Chlorobenzene
BRL
mg/kg dry
0.0055
0.00085
1
8260B
4/16/19 15:31
JLB
P9D0298
Chloroethane
BRL
mg/kg dry
0.011
0.0010
1
8260B
4/16/19 15:31
JLB
P9D0298
Chloroform
BRL
mg/kg dry
0.0055
0.00067
1
8260B
4/16/19 15:31
JLB
P9D0298
Chloromethane
BRL
mg/kg dry
0.011
0.0017
1
8260B
4/16/19 15:31
JLB
P9D0298
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0055
0.00086
1
8260B
4/16/19 15:31
JLB
P9D0298
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0055
0.00054
1
8260B
4/16/19 15:31
JLB
P9D0298
Dibromochloromethane
BRL
mg/kg dry
0.0055
0.00037
1
8260B
4/16/19 15:31
JLB
P9D0298
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260B
4/16/19 15:31
JLB
P9D0298
Ethylbenzene
BRL
mg/kg dry
0.0055
0.00082
1
8260B
4/16/19 15:31
JLB
P9D0298
Isopropyl Ether
BRL
mg/kg dry
0.0055
0.00080
1
8260B
4/16/19 15:31
JLB
P9D0298
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0055
0.00064
1
8260B
4/16/19 15:31
JLB
P9D0298
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: SB-6
Attn: Dan Nielsen Prism Sample ID: 9040256-06
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 04/15/19 14:05
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.011
0.0014
1
8260B
4/16/19 15:31
JLB
P9D0298
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.022
0.00038
1
8260B
4/16/19 15:31
JLB
P9D0298
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.022
0.0013
1
8260B
4/16/19 15:31
JLB
P9D0298
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.022
0.00045
1
8260B
4/16/19 15:31
JLB
P9D0298
Methylene Chloride
BRL
mg/kg dry
0.0055
0.00088
1
8260B
4/16/19 15:31
JLB
P9D0298
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0055
0.00077
1
8260B
4/16/19 15:31
JLB
P9D0298
Naphthalene
BRL
mg/kg dry
0.011
0.00055
1
8260B
4/16/19 15:31
JLB
P9D0298
n-Butylbenzene
BRL
mg/kg dry
0.0055
0.00051
1
8260B
4/16/19 15:31
JLB
P9D0298
n-Propylbenzene
BRL
mg/kg dry
0.0055
0.00079
1
8260B
4/16/19 15:31
JLB
P9D0298
o-Xylene
BRL
mg/kg dry
0.0055
0.00058
1
8260B
4/16/19 15:31
JLB
P9D0298
sec-Butylbenzene
BRL
mg/kg dry
0.0055
0.00059
1
8260B
4/16/19 15:31
JLB
P9D0298
Styrene
BRL
mg/kg dry
0.0055
0.00053
1
8260B
4/16/19 15:31
JLB
P9D0298
tert-Butylbenzene
BRL
mg/kg dry
0.0055
0.00065
1
8260B
4/16/19 15:31
JLB
P9D0298
Tetrachloroethylene
BRL
mg/kg dry
0.0055
0.00099
1
8260B
4/16/19 15:31
JLB
P9D0298
Toluene
BRL
mg/kg dry
0.0055
0.00087
1
8260B
4/16/19 15:31
JLB
P9D0298
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0055
0.0010
1
8260B
4/16/19 15:31
JLB
P9D0298
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0055
0.00047
1
8260B
4/16/19 15:31
JLB
P9D0298
Trichloroethylene
BRL
mg/kg dry
0.0055
0.0011
1
8260B
4/16/19 15:31
JLB
P9D0298
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260B
4/16/19 15:31
JLB
P9D0298
Vinyl acetate
BRL
mg/kg dry
0.011
0.00059
1
8260B
4/16/19 15:31
JLB
P9D0298
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260B
4/16/19 15:31
JLB
P9D0298
Xylenes, total
BRL
mg/kg dry
0.016
0.0020
1
8260B
4/16/19 15:31
JLB
P9D0298
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
99 %
70-130
Dibromofluoromethane
100 %
84-123
Toluene-d8
95 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Solid
Laboratory Report
04/22/2019
Client Sample ID: BG-1
Prism Sample ID: 9040256-07
Prism Work Order: 9040256
Time Collected: 04/15/19 12:40
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
84.2
% by
0.100
0.100
1
*SM2540 G
4/18/19 9:30
KBS
P91010322
Weight
Total Metals
Mercury
BRL
mg/kg dry
0.059
0.021
1
*7471B
4/18/19 12:00
MMR
P9D0323
Arsenic
3.1
mg/kg dry
1.2
0.16
1
*6010D
4118/19 11:52
JAB
P9D0297
Barium
250
mg/kg dry
120
36
10
*6010D
4/18/19 15:03
JAB
P91010297
Cadmium
BRL
mg/kg dry
0.59
0.040
1
*6010D
4/18/19 11:52
JAB
P9D0297
Chromium
21
mg/kg dry
1.2
0.090
1
*60101)
4/18/19 11:52
JAB
P9D0297
Lead
15
mg/kg dry
1.2
0.20
1
*6010D
4/18/19 11:52
JAB
P9D0297
Selenium
BRL
mg/kg dry
1.2
0.33
1
*6010D
4/18/19 11:52
JAB
P9D0297
Silver
BRL
mg/kg dry
0.59
0.036
1
*6010D
4/18/19 11:52
JAB
P9D0297
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3612 & 3624 Davis Drive
Client
Sample ID:
Duplicate
Attn: Dan Nielsen
Prism
Sample ID:
9040256-08
409 Rogers View Court
Prism
Work Order: 9040256
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected: 04/15/19 12:20
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
68.6
% by
0.100
0.100
1
*SM2540 G
4118/19 14:33
KBS
P9D0331
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0058
0.00071
1
8260B
4/16/19 16:01
JLB
P9D0298
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0058
0.00086
1
8260B
4/16/19 16:01
JLB
P9D0298
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0058
0.00042
1
8260B
4/16/19 16:01
JLB
P9D0298
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0058
0.00063
1
8260B
4/16/19 16:01
JLB
P9D0298
1,1-Dichloroethane
BRL
mg/kg dry
0.0058
0.0011
1
8260B
4/16/19 16:01
JLB
P9D0298
1,1-Dichloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260B
4/16/19 16:01
JLB
P9D0298
1,1-Dichloropropylene
BRL
mg/kg dry
0.0058
0.00090
1
8260B
4/16/19 16:01
JLB
P9D0298
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00083
1
8260B
4/16/19 16:01
JLB
P9D0298
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0058
0.00066
1
8260B
4/16/19 16:01
JLB
P9D0298
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00056
1
8260B
4/16/19 16:01
JLB
P9D0298
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0058
0.00062
1
8260B
4/16/19 16:01
JLB
P9D0298
1,2-Dibromoethane
BRL
mg/kg dry
0.0058
0.00052
1
8260B
4/16/19 16:01
JLB
P9D0298
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0058
0.00065
1
8260B
4/16/19 16:01
JLB
P9D0298
1,2-Dichloroethane
BRL
mg/kg dry
0.0058
0.00069
1
8260B
4/16/19 16:01
JLB
P9D0298
1,2-Dichloropropane
BRL
mg/kg dry
0.0058
0.00088
1
8260B
4/16/19 16:01
JLB
P9D0298
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0058
0.00073
1
8260B
4/16/19 16:01
JLB
P9D0298
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0058
0.00072
1
8260B
4/16/19 16:01
JLB
P9D0298
1,3-Dichloropropane
BRL
mg/kg dry
0.0058
0.00049
1
8260B
4/16/19 16:01
JLB
P9D0298
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0058
0.00074
1
8260B
4/16/19 16:01
JLB
P9D0298
2,2-Dichloropropane
BRL
mg/kg dry
0.0058
0.00073
1
8260B
4/16/19 16:01
JLB
P9D0298
2-Chlorotoluene
BRL
mg/kg dry
0.0058
0.00078
1
8260B
4/16/19 16:01
JLB
P9D0298
4-Chlorotoluene
BRL
mg/kg dry
0.0058
0.00066
1
8260B
4/16/19 16:01
JLB
P9D0298
4-Isopropyltoluene
BRL
mg/kg dry
0.0058
0.0015
1
8260B
4/16/19 16:01
JLB
P9D0298
Acetone
BRL
mg/kg dry
0.023
0.0015
1
8260B
4/16/19 16:01
JLB
P9D0298
Benzene
BRL
mg/kg dry
0.0058
0.00091
1
8260B
4/16/19 16:01
JLB
P9D0298
Bromobenzene
BRL
mg/kg dry
0.0058
0.00081
1
8260B
4/16/19 16:01
JLB
P9D0298
Bromochloromethane
BRL
mg/kg dry
0.0058
0.00096
1
8260B
4/16/19 16:01
JLB
P9D0298
Bromodichloromethane
BRL
mg/kg dry
0.0058
0.00055
1
8260B
4/16/19 16:01
JLB
P9D0298
Bromoform
BRL
mg/kg dry
0.0058
0.00045
1
8260B
4/16/19 16:01
JLB
P9D0298
Bromomethane
BRL
mg/kg dry
0.012
0.0029
1
8260B
4/16/19 16:01
JLB
P9D0298
Carbon Tetrachloride
BRL
mg/kg dry
0.0058
0.0011
1
8260B
4/16/19 16:01
JLB
P9D0298
Chlorobenzene
BRL
mg/kg dry
0.0058
0.00091
1
8260B
4/16/19 16:01
JLB
P9D0298
Chloroethane
BRL
mg/kg dry
0.012
0.0011
1
8260B
4/16/19 16:01
JLB
P9D0298
Chloroform
BRL
mg/kg dry
0.0058
0.00071
1
8260B
4/16/19 16:01
JLB
P9D0298
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
8260B
4/16/19 16:01
JLB
P9D0298
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0058
0.00092
1
8260B
4/16/19 16:01
JLB
P9D0298
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0058
0.00057
1
8260B
4/16/19 16:01
JLB
P9D0298
Dibromochloromethane
BRL
mg/kg dry
0.0058
0.00039
1
8260B
4/16/19 16:01
JLB
P9D0298
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260B
4/16/19 16:01
JLB
P9D0298
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: Duplicate
Attn: Dan Nielsen Prism Sample ID: 9040256-08
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 04/15/19 12:20
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Ethylbenzene
BRL
mg/kg dry
0.0058
0.00088
1
8260B
4/16/19 16:01
JLB
P9D0298
Isopropyl Ether
BRL
mg/kg dry
0.0058
0.00085
1
8260B
4/16/19 16:01
JLB
P9D0298
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0058
0.00068
1
8260B
4/16/19 16:01
JLB
P9D0298
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0015
1
8260B
4/16/19 16:01
JLB
P9D0298
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.023
0.00040
1
8260B
4/16/19 16:01
JLB
P9D0298
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.023
0.0014
1
8260B
4/16/19 16:01
JLB
P9D0298
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.023
0.00048
1
8260B
4/16/19 16:01
JLB
P9D0298
Methylene Chloride
BRL
mg/kg dry
0.0058
0.00094
1
8260B
4/16/19 16:01
JLB
P9D0298
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0058
0.00082
1
8260B
4/16/19 16:01
JLB
P9D0298
Naphthalene
BRL
mg/kg dry
0.012
0.00059
1
8260B
4/16/19 16:01
JLB
P9D0298
n-Butylbenzene
BRL
mg/kg dry
0.0058
0.00055
1
8260B
4/16/19 16:01
JLB
P9D0298
n-Propylbenzene
BRL
mg/kg dry
0.0058
0.00084
1
8260B
4/16/19 16:01
JLB
P9D0298
o-Xylene
BRL
mg/kg dry
0.0058
0.00062
1
8260B
4/16/19 16:01
JLB
P9D0298
sec-Butylbenzene
BRL
mg/kg dry
0.0058
0.00063
1
8260B
4/16/19 16:01
JLB
P9D0298
Styrene
BRL
mg/kg dry
0.0058
0.00056
1
8260B
4/16/19 16:01
JLB
P9D0298
tert-Butylbenzene
BRL
mg/kg dry
0.0058
0.00069
1
8260B
4/16/19 16:01
JLB
P9D0298
Tetrachloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260B
4/16/19 16:01
JLB
P9D0298
Toluene
BRL
mg/kg dry
0.0058
0.00093
1
8260B
4/16/19 16:01
JLB
P9D0298
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260B
4/16/19 16:01
JLB
P9D0298
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0058
0.00050
1
8260B
4/16/19 16:01
JLB
P9D0298
Trichloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260B
4/16/19 16:01
JLB
P9D0298
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260B
4/16/19 16:01
JLB
P9D0298
Vinyl acetate
BRL
mg/kg dry
0.012
0.00063
1
8260B
4/16/19 16:01
JLB
P9D0298
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260B
4/16/19 16:01
JLB
P9D0298
Xylenes, total
BRL
mg/kg dry
0.017
0.0021
1
8260B
4/16/19 16:01
JLB
P9D0298
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
97 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
92 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Water
Client Sample ID: TMW-1
Prism Sample ID: 9040256-09
Prism Work Order: 9040256
Time Collected: 04/15/19 14:25
Time Submitted: 04/16/19 09:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
ug/L
10
3.2
1
8270D
4/18/19
1:31
JMV
P9D0284
1,2-Dichlorobenzene
BRL
ug/L
10
2.5
1
8270D
4/18/19
1:31
JMV
P9D0284
1,3-Dichlorobenzene
BRL
ug/L
10
2.7
1
8270D
4/18/19
1:31
JMV
P9D0284
1,4-Dichlorobenzene
BRL
ug/L
10
2.6
1
8270D
4/18/19
1:31
JMV
P9D0284
1-Methyl naphthalene
BRL
ug/L
10
3.8
1
8270D
4/18/19
1:31
JMV
P9D0284
2,4,5-Trichlorophenol
BRL
ug/L
21
4.2
1
8270D
4/18/19
1:31
JMV
P9D0284
2,4,6-Trichlorophenol
BRL
ug/L
21
4.6
1
8270D
4/18/19
1:31
JMV
P9D0284
2,4-Dichlorophenol
BRL
ug/L
10
3.0
1
8270D
4/18/19
1:31
JMV
P9D0284
2,4-Dimethylphenol
BRL
ug/L
10
2.2
1
8270D
4/18/19
1:31
JMV
P9D0284
2,4-Dinitrophenol
BRL
ug/L
52
13
1
8270D
4/18/19
1:31
JMV
P9D0284
2,4-Dinitrotoluene
BRL
ug/L
10
3.3
1
8270D
4/18/19
1:31
JMV
P9D0284
2,6-Dinitrotoluene
BRL
ug/L
21
4.1
1
8270D
4/18/19
1:31
JMV
P9D0284
2-Chloronaphthalene
BRL
ug/L
21
4.0
1
8270D
4/18/19
1:31
JMV
P9D0284
2-Chlorophenol
BRL
ug/L
10
2.9
1
8270D
4/18/19
1:31
JMV
P9D0284
2-Methyl naphthalene
BRL
ug/L
10
3.5
1
8270D
4/18/19
1:31
JMV
P9D0284
2-Methylphenol
BRL
ug/L
10
2.0
1
8270D
4/18/19
1:31
JMV
P9D0284
2-Nitroaniline
BRL
ug/L
10
3.2
1
8270D
4/18/19
1:31
JMV
P9D0284
2-Nitrophenol
BRL
ug/L
10
2.8
1
8270D
4/18/19
1:31
JMV
P9D0284
3,3'-Dichlorobenzidine
BRL
ug/L
10
2.5
1
8270D
4/18/19
1:31
JMV
P9D0284
3/4-Methyl phenol
BRL
ug/L
10
2.6
1
8270D
4/18/19
1:31
JMV
P9D0284
3-Nitroaniline
BRL
ug/L
10
2.3
1
8270D
4/18/19
1:31
JMV
P9D0284
4,6-Dinitro-2-methylphenol
BRL
ug/L
52
16
1
8270D
4/18/19
1:31
JMV
P9D0284
4-Bromophenyl phenyl ether
BRL
ug/L
21
3.7
1
8270D
4/18/19
1:31
JMV
P9D0284
4-Chloro-3-methylphenol
BRL
ug/L
10
2.8
1
8270D
4/18/19
1:31
JMV
P9D0284
4-Chloroaniline
BRL
ug/L
10
1.6
1
8270D
4/18/19
1:31
JMV
P9D0284
4-Chlorophenyl phenyl ether
BRL
ug/L
21
5.1
1
8270D
4/18/19
1:31
JMV
P9D0284
4-Nitroaniline
BRL
ug/L
10
1.5
1
8270D
4/18/19
1:31
JMV
P9D0284
4-Nitrophenol
BRL
ug/L
10
2.3
1
8270D
4/18/19
1:31
JMV
P9D0284
Acenaphthene
BRL
ug/L
21
4.0
1
8270D
4/18/19
1:31
JMV
P9D0284
Acenaphthylene
BRL
ug/L
21
4.3
1
8270D
4/18/19
1:31
JMV
P9D0284
Aniline
BRL
ug/L
21
6.4
1
8270D
4/18/19
1:31
JMV
P9D0284
Anthracene
BRL
ug/L
21
5.1
1
8270D
4/18/19
1:31
JMV
P9D0284
Azobenzene
BRL
ug/L
10
3.3
1
8270D
4/18/19
1:31
JMV
P9D0284
Benzo(a)anthracene
BRL
ug/L
10
3.4
1
8270D
4/18/19
1:31
JMV
P9D0284
Benzo(a)pyrene
BRL
ug/L
10
2.5
1
8270D
4/18/19
1:31
JMV
P9D0284
Benzo(b)fluoranthene
BRL
ug/L
10
2.6
1
8270D
4/18/19
1:31
JMV
P9D0284
Benzo(g,h,i)perylene
BRL
ug/L
10
2.8
1
8270D
4/18/19
1:31
JMV
P9D0284
Benzo(k)fluoranthene
BRL
ug/L
10
2.8
1
8270D
4/18/19
1:31
JMV
P9D0284
Benzoic Acid
BRL
ug/L
100
24
1
8270D
4/18/19
1:31
JMV
P9D0284
Benzyl alcohol
BRL
ug/L
10
1.9
1
8270D
4/18/19
1:31
JMV
P9D0284
bis(2-Chloroethoxy)methane
BRL
ug/L
10
2.9
1
8270D
4/18/19
1:31
JMV
P9D0284
Bis(2-Chloroethyl)ether
BRL
ug/L
10
2.6
1
8270D
4/18/19
1:31
JMV
P9D0284
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: TMW-1
Attn: Dan Nielsen Prism Sample ID: 9040256-09
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Water Time Collected: 04/15/19 14:25
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-chloroisopropyl)ether
BRL
ug/L
10
2.2
1
8270D
4/18/19 1:31
JMV
P9D0284
Bis(2-Ethylhexyl)phthaIate
BRL
ug/L
10
3.6
1
8270D
4/18/19 1:31
JMV
P9D0284
Butyl benzyl phthalate
BRL
ug/L
10
1.8
1
8270D
4/18/19 1:31
JMV
P9D0284
Chrysene
BRL
ug/L
10
3.1
1
8270D
4/18/19 1:31
JMV
P9D0284
Dibenzo(a,h)anthracene
BRL
ug/L
10
1.5
1
8270D
4/18/19 1:31
JMV
P9D0284
Dibenzofuran
BRL
ug/L
21
4.4
1
8270D
4/18/19 1:31
JMV
P9D0284
Diethyl phthalate
BRL
ug/L
21
3.8
1
8270D
4/18/19 1:31
JMV
P9D0284
Dimethyl phthalate
BRL
ug/L
21
3.8
1
8270D
4/18/19 1:31
JMV
P9D0284
Di-n-butyl phthalate
BRL
ug/L
21
4.0
1
8270D
4/18/19 1:31
JMV
P9D0284
Di-n-octyl phthalate
BRL
ug/L
10
2.1
1
8270D
4/18/19 1:31
JMV
P9D0284
Fluoranthene
BRL
ug/L
21
4.9
1
8270D
4/18/19 1:31
JMV
P9D0284
Fluorene
BRL
ug/L
21
5.3
1
8270D
4/18/19 1:31
JMV
P9D0284
Hexachlorobenzene
BRL
ug/L
21
4.2
1
8270D
4/18/19 1:31
JMV
P9D0284
Hexachlorobutadiene
BRL
ug/L
10
2.9
1
8270D
4/18/19 1:31
JMV
P9D0284
Hexachlorocyclopentadiene
BRL
ug/L
10
2.2
1
8270D
4/18/19 1:31
JMV
P9D0284
Hexachloroethane
BRL
ug/L
10
2.4
1
8270D
4/18/19 1:31
JMV
P9D0284
Indeno(1,2,3-cd)pyrene
BRL
ug/L
10
2.9
1
8270D
4/18/19 1:31
JMV
P9D0284
Isophorone
BRL
ug/L
10
2.5
1
8270D
4/18/19 1:31
JMV
P9D0284
Naphthalene
BRL
ug/L
10
3.3
1
8270D
4/18/19 1:31
JMV
P9D0284
Nitrobenzene
BRL
ug/L
10
2.5
1
8270D
4/18/19 1:31
JMV
P9D0284
N-Nitroso-di-n-propylamine
BRL
ug/L
21
3.9
1
8270D
4/18/19 1:31
JMV
P9D0284
N-Nitrosodiphenylamine
BRL
ug/L
21
5.0
1
8270D
4/18/19 1:31
JMV
P9D0284
Pentachlorophenol
BRL
ug/L
10
3.5
1
8270D
4/18/19 1:31
JMV
P9D0284
Phenanthrene
BRL
ug/L
21
4.7
1
8270D
4/18/19 1:31
JMV
P9D0284
Phenol
BRL
ug/L
10
0.74
1
8270D
4/18/19 1:31
JMV
P9D0284
Pyrene
BRL
ug/L
10
3.4
1
8270D
4/18/19 1:31
JMV
P9D0284
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
77 %
43-140
2-Fluorobiphenyl
75 %
44-119
2-Fluorophenol
50 %
19-119
Nitrobenzene-d5
71 %
44-120
Phenol-d5
35 %
11-52
Terphenyl-d14
79 %
50-134
Total Metals
Mercury
BRL
mg/L
0.00050
0.00016
1
*7470A
4/17/19 12:57
MMR
P9D0290
Arsenic
BRL
mg/L
0.020
0.0060
1
*6010D
4/18/19 14:16
JAB
P9D0292
Barium
0.38
mg/L
0.010
0.0020
1
*6010D
4/18/19 14:16
JAB
P9D0292
Cadmium
BRL
mg/L
0.0020
0.00040
1
*6010D
4/18/19 14:16
JAB
P9D0292
Chromium
0.079
mg/L
0.010
0.0030
1
*60101)
4/18/19 14:16
JAB
P91010292
Lead
0.015
mg/L
0.0050
0.0039
1
*60101)
4/18/19 14:16
JAB
P9D0292
Selenium
BRL
mg/L
0.030
0.013
1
*6010D
4/18/19 14:16
JAB
P9D0292
Silver
BRL
mg/L
0.0050
0.00090
1
*6010D
4/18/19 14:16
JAB
P9D0292
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Water
Laboratory Report
04/22/2019
Client Sample ID: TMW-1
Prism Sample ID: 9040256-09
Prism Work Order: 9040256
Time Collected: 04/15/19 14:25
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
ug/L
0.50
0.11
1
8260B
4/18/19
2:31
KDM
P9D0320
1,1,1-Trichloroethane
BRL
ug/L
0.50
0.061
1
8260B
4/18/19
2:31
KDM
P9D0320
1,1,2,2-Tetrachloroethane
BRL
ug/L
0.50
0.036
1
8260B
4/18/19
2:31
KDM
P9D0320
1,1,2-Trichloroethane
BRL
ug/L
0.50
0.066
1
8260B
4/18/19
2:31
KDM
P9D0320
1,1-Dichloroethane
BRL
ug/L
0.50
0.083
1
8260B
4/18/19
2:31
KDM
P9D0320
1,1-Dichloroethylene
BRL
ug/L
0.50
0.083
1
8260B
4/18/19
2:31
KDM
P9D0320
1,1-Dichloropropylene
BRL
ug/L
0.50
0.051
1
8260B
4/18/19
2:31
KDM
P9D0320
1,2,3-Trichlorobenzene
BRL
ug/L
2.0
0.40
1
8260B
4/18/19
2:31
KDM
P9D0320
1,2,3-Trichloropropane
BRL
ug/L
1.0
0.14
1
8260B
4/18/19
2:31
KDM
P9D0320
1,2,4-Trichlorobenzene
BRL
ug/L
1.0
0.13
1
8260B
4/18/19
2:31
KDM
P9D0320
1,2,4-Trimethyl benzene
BRL
ug/L
0.50
0.054
1
8260B
4/18/19
2:31
KDM
P9D0320
1,2-Dibromo-3-chloropropane
BRL
ug/L
2.0
0.17
1
8260B
4/18/19
2:31
KDM
P9D0320
1,2-Dibromoethane
BRL
ug/L
0.50
0.051
1
8260B
4/18/19
2:31
KDM
P9D0320
1,2-Dichlorobenzene
BRL
ug/L
0.50
0.076
1
8260B
4/18/19
2:31
KDM
P9D0320
1,2-Dichloroethane
BRL
ug/L
0.50
0.066
1
8260B
4/18/19
2:31
KDM
P9D0320
1,2-Dichloropropane
BRL
ug/L
0.50
0.11
1
8260B
4/18/19
2:31
KDM
P9D0320
1,3,5-Trimethyl benzene
BRL
ug/L
0.50
0.076
1
8260B
4/18/19
2:31
KDM
P9D0320
1,3-Dichlorobenzene
BRL
ug/L
0.50
0.054
1
8260B
4/18/19
2:31
KDM
P9D0320
1,3-Dichloropropane
BRL
ug/L
0.50
0.043
1
8260B
4/18/19
2:31
KDM
P9D0320
1,4-Dichlorobenzene
BRL
ug/L
0.50
0.050
1
8260B
4/18/19
2:31
KDM
P9D0320
2,2-Dichloropropane
BRL
ug/L
2.0
0.11
1
8260B
4/18/19
2:31
KDM
P9D0320
2-Chlorotoluene
BRL
ug/L
0.50
0.066
1
8260B
4/18/19
2:31
KDM
P9D0320
4-Chlorotoluene
BRL
ug/L
0.50
0.050
1
8260B
4/18/19
2:31
KDM
P9D0320
4-Isopropyltoluene
BRL
ug/L
0.50
0.089
1
8260B
4/18/19
2:31
KDM
P9D0320
Acetone
BRL
ug/L
5.0
0.31
1
8260B
4/18/19
2:31
KDM
P9D0320
Acrolein
BRL
ug/L
20
0.20
1
8260B
4/18/19
2:31
KDM
P9D0320
Acrylonitrile
BRL
ug/L
20
0.20
1
8260B
4/18/19
2:31
KDM
P9D0320
Benzene
BRL
ug/L
0.50
0.048
1
8260B
4/18/19
2:31
KDM
P9D0320
Bromobenzene
BRL
ug/L
0.50
0.057
1
8260B
4/18/19
2:31
KDM
P9D0320
Bromochloromethane
BRL
ug/L
0.50
0.14
1
8260B
4/18/19
2:31
KDM
P9D0320
Bromodichloromethane
BRL
ug/L
0.50
0.062
1
8260B
4/18/19
2:31
KDM
P9D0320
Bromoform
BRL
ug/L
1.0
0.040
1
8260B
4/18/19
2:31
KDM
P9D0320
Bromomethane
BRL
ug/L
1.0
0.18
1
8260B
4/18/19
2:31
KDM
P9D0320
Carbon disulfide
BRL
ug/L
5.0
0.075
1
8260B
4/18/19
2:31
KDM
P9D0320
Carbon Tetrachloride
BRL
ug/L
0.50
0.11
1
8260B
4/18/19
2:31
KDM
P9D0320
Chlorobenzene
BRL
ug/L
0.50
0.062
1
8260B
4/18/19
2:31
KDM
P9D0320
Chloroethane
BRL
ug/L
0.50
0.22
1
8260B
4/18/19
2:31
KDM
P9D0320
Chloroform
1.2
ug/L
0.50
0.076
1
8260B
4/18/19
2:31
KDM
P9D0320
Chloromethane
BRL
ug/L
0.50
0.079
1
8260B
4/18/19
2:31
KDM
P9D0320
cis-1,2-Dichloroethylene
BRL
ug/L
0.50
0.056
1
8260B
4/18/19
2:31
KDM
P9D0320
cis-1,3-Dichloropropylene
BRL
ug/L
0.50
0.079
1
8260B
4/18/19
2:31
KDM
P9D0320
Dibromochloromethane
BRL
ug/L
0.50
0.081
1
8260B
4/18/19
2:31
KDM
P9D0320
Dibromomethane
BRL
ug/L
0.50
0.065
1
8260B
4/18/19
2:31
KDM
P9D0320
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: TMW-1
Attn: Dan Nielsen Prism Sample ID: 9040256-09
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Water Time Collected: 04/15/19 14:25
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Dichlorodifluoromethane
BRL
ug/L
1.0
0.11
1
8260B
4/18/19
2:31
KDM
P9D0320
Ethylbenzene
BRL
ug/L
0.50
0.061
1
8260B
4/18/19
2:31
KDM
P9D0320
Hexachlorobutadiene
BRL
ug/L
2.0
0.16
1
8260B
4/18/19
2:31
KDM
P9D0320
Isopropyl Ether
BRL
ug/L
0.50
0.050
1
8260B
4/18/19
2:31
KDM
P9D0320
Isopropylbenzene (Cumene)
BRL
ug/L
0.50
0.054
1
8260B
4/18/19
2:31
KDM
P9D0320
m,p-Xylenes
BRL
ug/L
1.0
0.12
1
8260B
4/18/19
2:31
KDM
P9D0320
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/L
5.0
0.065
1
8260B
4/18/19
2:31
KDM
P9D0320
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
5.0
0.24
1
8260B
4/18/19
2:31
KDM
P9D0320
Methyl Isobutyl Ketone
BRL
ug/L
5.0
0.078
1
8260B
4/18/19
2:31
KDM
P9D0320
Methylene Chloride
BRL
ug/L
1.0
0.083
1
8260B
4/18/19
2:31
KDM
P9D0320
Methyl-tert-Butyl Ether
BRL
ug/L
0.50
0.042
1
8260B
4/18/19
2:31
KDM
P9D0320
Naphthalene
BRL
ug/L
1.0
0.19
1
8260B
4/18/19
2:31
KDM
P9D0320
n-Butylbenzene
BRL
ug/L
1.0
0.076
1
8260B
4/18/19
2:31
KDM
P9D0320
n-Propylbenzene
BRL
ug/L
0.50
0.087
1
8260B
4/18/19
2:31
KDM
P9D0320
o-Xylene
BRL
ug/L
0.50
0.044
1
8260B
4/18/19
2:31
KDM
P9D0320
sec-Butylbenzene
BRL
ug/L
0.50
0.076
1
8260B
4/18/19
2:31
KDM
P9D0320
Styrene
BRL
ug/L
0.50
0.047
1
8260B
4/18/19
2:31
KDM
P9D0320
tert-Butylbenzene
BRL
ug/L
0.50
0.088
1
8260B
4/18/19
2:31
KDM
P9D0320
Tetrachloroethylene
BRL
ug/L
0.50
0.098
1
8260B
4/18/19
2:31
KDM
P9D0320
Toluene
BRL
ug/L
0.50
0.044
1
8260B
4/18/19
2:31
KDM
P9D0320
trans-1,2-Dichloroethylene
BRL
ug/L
0.50
0.094
1
8260B
4/18/19
2:31
KDM
P9D0320
trans- 1,3-Dichloropropylene
BRL
ug/L
0.50
0.070
1
8260B
4/18/19
2:31
KDM
P9D0320
Trichloroethylene
BRL
ug/L
0.50
0.078
1
8260B
4/18/19
2:31
KDM
P9D0320
Trichlorofluoromethane
BRL
ug/L
0.50
0.062
1
8260B
4/18/19
2:31
KDM
P9D0320
Vinyl acetate
BRL
ug/L
2.0
0.060
1
8260B
4/18/19
2:31
KDM
P9D0320
Vinyl chloride
BRL
ug/L
0.50
0.097
1
8260B
4/18/19
2:31
KDM
P9D0320
Xylenes, total
BRL
ug/L
1.5
0.15
1
8260B
4/18/19
2:31
KDM
P9D0320
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
104 %
80-124
Dibromofluoromethane
98 %
75-129
Toluene-d8
97 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
04/22/2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Sample Matrix: Water
Client Sample ID: Duplicate - water
Prism Sample ID: 9040256-10
Prism Work Order: 9040256
Time Collected: 04/15/19 14:30
Time Submitted: 04/16/19 09:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/L
0.50
0.11
1
8260B
4/18/19
2:57
KDM
P9D0320
1,1,1-Trichloroethane
BRL
ug/L
0.50
0.061
1
8260B
4/18/19
2:57
KDM
P9D0320
1,1,2,2-Tetrachloroethane
BRL
ug/L
0.50
0.036
1
8260B
4/18/19
2:57
KDM
P9D0320
1,1,2-Trichloroethane
BRL
ug/L
0.50
0.066
1
8260B
4/18/19
2:57
KDM
P9D0320
1,1-Dichloroethane
BRL
ug/L
0.50
0.083
1
8260B
4/18/19
2:57
KDM
P9D0320
1,1-Dichloroethylene
BRL
ug/L
0.50
0.083
1
8260B
4/18/19
2:57
KDM
P9D0320
1,1-Dichloropropylene
BRL
ug/L
0.50
0.051
1
8260B
4/18/19
2:57
KDM
P9D0320
1,2,3-Trichlorobenzene
BRL
ug/L
2.0
0.40
1
8260B
4/18/19
2:57
KDM
P9D0320
1,2,3-Trichloropropane
BRL
ug/L
1.0
0.14
1
8260B
4/18/19
2:57
KDM
P9D0320
1,2,4-Trichlorobenzene
BRL
ug/L
1.0
0.13
1
8260B
4/18/19
2:57
KDM
P9D0320
1,2,4-Trimethyl benzene
BRL
ug/L
0.50
0.054
1
8260B
4/18/19
2:57
KDM
P9D0320
1,2-Dibromo-3-chloropropane
BRL
ug/L
2.0
0.17
1
8260B
4/18/19
2:57
KDM
P9D0320
1,2-Dibromoethane
BRL
ug/L
0.50
0.051
1
8260B
4/18/19
2:57
KDM
P9D0320
1,2-Dichlorobenzene
BRL
ug/L
0.50
0.076
1
8260B
4/18/19
2:57
KDM
P9D0320
1,2-Dichloroethane
BRL
ug/L
0.50
0.066
1
8260B
4/18/19
2:57
KDM
P9D0320
1,2-Dichloropropane
BRL
ug/L
0.50
0.11
1
8260B
4/18/19
2:57
KDM
P9D0320
1,3,5-Trimethyl benzene
BRL
ug/L
0.50
0.076
1
8260B
4/18/19
2:57
KDM
P9D0320
1,3-Dichlorobenzene
BRL
ug/L
0.50
0.054
1
8260B
4/18/19
2:57
KDM
P9D0320
1,3-Dichloropropane
BRL
ug/L
0.50
0.043
1
8260B
4/18/19
2:57
KDM
P9D0320
1,4-Dichlorobenzene
BRL
ug/L
0.50
0.050
1
8260B
4/18/19
2:57
KDM
P9D0320
2,2-Dichloropropane
BRL
ug/L
2.0
0.11
1
8260B
4/18/19
2:57
KDM
P9D0320
2-Chlorotoluene
BRL
ug/L
0.50
0.066
1
8260B
4/18/19
2:57
KDM
P9D0320
4-Chlorotoluene
BRL
ug/L
0.50
0.050
1
8260B
4/18/19
2:57
KDM
P9D0320
4-Isopropyltoluene
BRL
ug/L
0.50
0.089
1
8260B
4/18/19
2:57
KDM
P9D0320
Acetone
5.6
ug/L
5.0
0.31
1
8260B
4/18/19
2:57
KDM
P91010320
Acrolein
BRL
ug/L
20
0.20
1
8260B
4/18/19
2:57
KDM
P9D0320
Acrylonitrile
BRL
ug/L
20
0.20
1
8260B
4/18/19
2:57
KDM
P9D0320
Benzene
BRL
ug/L
0.50
0.048
1
8260B
4/18/19
2:57
KDM
P9D0320
Bromobenzene
BRL
ug/L
0.50
0.057
1
8260B
4/18/19
2:57
KDM
P9D0320
Bromochloromethane
BRL
ug/L
0.50
0.14
1
8260B
4/18/19
2:57
KDM
P9D0320
Bromodichloromethane
BRL
ug/L
0.50
0.062
1
8260B
4/18/19
2:57
KDM
P9D0320
Bromoform
BRL
ug/L
1.0
0.040
1
8260B
4/18/19
2:57
KDM
P9D0320
Bromomethane
BRL
ug/L
1.0
0.18
1
8260B
4/18/19
2:57
KDM
P9D0320
Carbon disulfide
BRL
ug/L
5.0
0.075
1
8260B
4/18/19
2:57
KDM
P9D0320
Carbon Tetrachloride
BRL
ug/L
0.50
0.11
1
8260B
4/18/19
2:57
KDM
P9D0320
Chlorobenzene
BRL
ug/L
0.50
0.062
1
8260B
4/18/19
2:57
KDM
P9D0320
Chloroethane
BRL
ug/L
0.50
0.22
1
8260B
4/18/19
2:57
KDM
P9D0320
Chloroform
0.89
ug/L
0.50
0.076
1
8260B
4/18/19
2:57
KDM
P9D0320
Chloromethane
BRL
ug/L
0.50
0.079
1
8260B
4/18/19
2:57
KDM
P9D0320
cis-1,2-Dichloroethylene
BRL
ug/L
0.50
0.056
1
8260B
4/18/19
2:57
KDM
P9D0320
cis-1,3-Dichloropropylene
BRL
ug/L
0.50
0.079
1
8260B
4/18/19
2:57
KDM
P9D0320
Dibromochloromethane
BRL
ug/L
0.50
0.081
1
8260B
4/18/19
2:57
KDM
P9D0320
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 04/22/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Client Sample ID: Duplicate - water
Attn: Dan Nielsen Prism Sample ID: 9040256-10
409 Rogers View Court Prism Work Order: 9040256
Raleigh, NC 27610 Sample Matrix: Water Time Collected: 04/15/19 14:30
Time Submitted: 04/16/19 09:45
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Dibromomethane
BRL
ug/L
0.50
0.065
1
8260B
4/18/19
2:57
KDM
P9D0320
Dichlorodifluoromethane
BRL
ug/L
1.0
0.11
1
8260B
4/18/19
2:57
KDM
P9D0320
Ethylbenzene
BRL
ug/L
0.50
0.061
1
8260B
4/18/19
2:57
KDM
P9D0320
Hexachlorobutadiene
BRL
ug/L
2.0
0.16
1
8260B
4/18/19
2:57
KDM
P9D0320
Isopropyl Ether
BRL
ug/L
0.50
0.050
1
8260B
4/18/19
2:57
KDM
P9D0320
Isopropylbenzene (Cumene)
BRL
ug/L
0.50
0.054
1
8260B
4/18/19
2:57
KDM
P9D0320
m,p-Xylenes
BRL
ug/L
1.0
0.12
1
8260B
4/18/19
2:57
KDM
P9D0320
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/L
5.0
0.065
1
8260B
4/18/19
2:57
KDM
P9D0320
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
5.0
0.24
1
8260B
4/18/19
2:57
KDM
P9D0320
Methyl Isobutyl Ketone
BRL
ug/L
5.0
0.078
1
8260B
4/18/19
2:57
KDM
P9D0320
Methylene Chloride
BRL
ug/L
1.0
0.083
1
8260B
4/18/19
2:57
KDM
P9D0320
Methyl-tert-Butyl Ether
BRL
ug/L
0.50
0.042
1
8260B
4/18/19
2:57
KDM
P9D0320
Naphthalene
BRL
ug/L
1.0
0.19
1
8260B
4/18/19
2:57
KDM
P9D0320
n-Butylbenzene
BRL
ug/L
1.0
0.076
1
8260B
4/18/19
2:57
KDM
P9D0320
n-Propylbenzene
BRL
ug/L
0.50
0.087
1
8260B
4/18/19
2:57
KDM
P9D0320
o-Xylene
BRL
ug/L
0.50
0.044
1
8260B
4/18/19
2:57
KDM
P9D0320
sec-Butylbenzene
BRL
ug/L
0.50
0.076
1
8260B
4/18/19
2:57
KDM
P9D0320
Styrene
BRL
ug/L
0.50
0.047
1
8260B
4/18/19
2:57
KDM
P9D0320
tert-Butylbenzene
BRL
ug/L
0.50
0.088
1
8260B
4/18/19
2:57
KDM
P9D0320
Tetrachloroethylene
BRL
ug/L
0.50
0.098
1
8260B
4/18/19
2:57
KDM
P9D0320
Toluene
BRL
ug/L
0.50
0.044
1
8260B
4/18/19
2:57
KDM
P9D0320
trans-1,2-Dichloroethylene
BRL
ug/L
0.50
0.094
1
8260B
4/18/19
2:57
KDM
P9D0320
trans-1,3-Dichloropropylene
BRL
ug/L
0.50
0.070
1
8260B
4/18/19
2:57
KDM
P9D0320
Trichloroethylene
BRL
ug/L
0.50
0.078
1
8260B
4/18/19
2:57
KDM
P9D0320
Trichlorofluoromethane
BRL
ug/L
0.50
0.062
1
8260B
4/18/19
2:57
KDM
P9D0320
Vinyl acetate
BRL
ug/L
2.0
0.060
1
8260B
4/18/19
2:57
KDM
P9D0320
Vinyl chloride
BRL
ug/L
0.50
0.097
1
8260B
4/18/19
2:57
KDM
P9D0320
Xylenes, total
BRL
ug/L
1.5
0.15
1
8260B
4/18/19
2:57
KDM
P9D0320
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
80-124
Dibromofluoromethane
99 %
75-129
Toluene-d8
98 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

/r E
P R I IS M Service Analytical
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO298 - 5035
Blank (P9D0298-BLK1)
Prepared & Analyzed: 04/16/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO298 - 5035
Blank (P9D0298-BLK1)
Prepared & Analyzed: 04/16/19
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
49.4
ug/L
50.00
99
70-130
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
84-123
Surrogate: Toluene-d8
47.7
ug/L
50.00
95
76-129
LCS (P9DO298-BS1)
Prepared & Analyzed:
04/16/19
1,1,1,2-Tetrachloroethane
0.0403
0.0050
mg/kg wet
0.05000
81
72-115
1, 1,1 -Trichloroethane
0.0415
0.0050
mg/kg wet
0.05000
83
67-131
1,1,2,2-Tetrachloroethane
0.0391
0.0050
mg/kg wet
0.05000
78
56-126
1,1,2-Trichloroethane
0.0398
0.0050
mg/kg wet
0.05000
80
70-133
1,1-Dichloroethane
0.0416
0.0050
mg/kg wet
0.05000
83
74-127
1,1-Dichloroethylene
0.0425
0.0050
mg/kg wet
0.05000
85
67-149
1, 1 -Dichloropropylene
0.0433
0.0050
mg/kg wet
0.05000
87
71-130
1,2,3-Trichlorobenzene
0.0394
0.010
mg/kg wet
0.05000
79
68-130
1,2,3-Trichloropropane
0.0389
0.0050
mg/kg wet
0.05000
78
60-137
1,2,4-Trichlorobenzene
0.0396
0.010
mg/kg wet
0.05000
79
66-125
1,2,4-Trimethylbenzene
0.0385
0.0050
mg/kg wet
0.05000
77
69-129
1,2-Dibromoethane
0.0405
0.0050
mg/kg wet
0.05000
81
70-132
1,2-Dichlorobenzene
0.0387
0.0050
mg/kg wet
0.05000
77
72-123
1,2-Dichloroethane
0.0406
0.0050
mg/kg wet
0.05000
81
68-128
1,2-Dichloropropane
0.0422
0.0050
mg/kg wet
0.05000
84
73-130
1,3,5-Trimethylbenzene
0.0400
0.0050
mg/kg wet
0.05000
80
69-128
1,3-Dichlorobenzene
0.0390
0.0050
mg/kg wet
0.05000
78
71-120
1,3-Dichloropropane
0.0400
0.0050
mg/kg wet
0.05000
80
75-124
1,4-Dichlorobenzene
0.0389
0.0050
mg/kg wet
0.05000
78
71-123
2,2-Dichloropropane
0.0430
0.0050
mg/kg wet
0.05000
86
50-142
2-Chlorotoluene
0.0393
0.0050
mg/kg wet
0.05000
79
67-124
4-Chlorotoluene
0.0393
0.0050
mg/kg wet
0.05000
79
71-126
4-Isopropyltoluene
0.0404
0.0050
mg/kg wet
0.05000
81
68-129
Acetone
0.0830
0.020
mg/kg wet
0.1000
83
29-198
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO298 - 5035
LCS (P9D0298-BSI)
Prepared & Analyzed: 04/16/19
Benzene
0.0418
0.0050
mg/kg wet
0.05000
84
74-127
Bromobenzene
0.0385
0.0050
mg/kg wet
0.05000
77
73-125
Bromochloromethane
0.0404
0.0050
mg/kg wet
0.05000
81
72-134
Bromodichloromethane
0.0414
0.0050
mg/kg wet
0.05000
83
75-122
Bromoform
0.0406
0.0050
mg/kg wet
0.05000
81
66-135
Bromomethane
0.0412
0.010
mg/kg wet
0.05000
82
20-180
Carbon Tetrachloride
0.0426
0.0050
mg/kg wet
0.05000
85
64-143
Chlorobenzene
0.0404
0.0050
mg/kg wet
0.05000
81
74-118
Chloroethane
0.0479
0.010
mg/kg wet
0.05000
96
33-149
Chloroform
0.0414
0.0050
mg/kg wet
0.05000
83
73-127
Chloromethane
0.0468
0.010
mg/kg wet
0.05000
94
45-143
cis-1,2-Dichloroethylene
0.0415
0.0050
mg/kg wet
0.05000
83
76-134
cis-1,3-Dichloropropylene
0.0422
0.0050
mg/kg wet
0.05000
84
71-125
Dibromochloromethane
0.0406
0.0050
mg/kg wet
0.05000
81
73-122
Dichlorodifluoromethane
0.0452
0.010
mg/kg wet
0.05000
90
26-146
Ethylbenzene
0.0406
0.0050
mg/kg wet
0.05000
81
74-128
Isopropyl Ether
0.0416
0.0050
mg/kg wet
0.05000
83
59-159
Isopropylbenzene (Cumene)
0.0400
0.0050
mg/kg wet
0.05000
80
68-126
m,p-Xylenes
0.0821
0.010
mg/kg wet
0.1000
82
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0428
0.020
mg/kg wet
0.05000
86
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0404
0.020
mg/kg wet
0.05000
81
63-149
Methyl Isobutyl Ketone
0.0425
0.020
mg/kg wet
0.05000
85
57-162
Methylene Chloride
0.0376
0.0050
mg/kg wet
0.05000
75
74-129
Methyl-tert-Butyl Ether
0.0416
0.0050
mg/kg wet
0.05000
83
70-130
Naphthalene
0.0366
0.010
mg/kg wet
0.05000
73
57-157
n-Butylbenzene
0.0411
0.0050
mg/kg wet
0.05000
82
65-135
n-Propylbenzene
0.0398
0.0050
mg/kg wet
0.05000
80
67-130
o-Xylene
0.0407
0.0050
mg/kg wet
0.05000
81
74-126
sec-Butylbenzene
0.0405
0.0050
mg/kg wet
0.05000
81
66-131
Styrene
0.0417
0.0050
mg/kg wet
0.05000
83
77-121
tert-Butyl benzene
0.0401
0.0050
mg/kg wet
0.05000
80
67-132
Tetrachloroethylene
0.0429
0.0050
mg/kg wet
0.05000
86
68-130
Toluene
0.0413
0.0050
mg/kg wet
0.05000
83
71-129
trans- 1,2-Dichloroethylene
0.0419
0.0050
mg/kg wet
0.05000
84
73-132
trans- 1,3-Dichloropropylene
0.0422
0.0050
mg/kg wet
0.05000
84
68-123
Trichloroethylene
0.0432
0.0050
mg/kg wet
0.05000
86
75-133
Trichlorofluoromethane
0.0469
0.010
mg/kg wet
0.05000
94
44-146
Vinyl acetate
0.0424
0.010
mg/kg wet
0.05000
85
85-161
Vinyl chloride
0.0431
0.010
mg/kg wet
0.05000
86
48-147
Xylenes, total
0.123
0.015
mg/kg wet
0.1500
82
74-126
Surrogate:4-Bromofluorobenzene
49.2
ug/L
50.00
98
70-130
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
84-123
Surrogate: Toluene-d8
48.6
ug/L
50.00
97
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO298 - 5035
LCS Dup (P9DO298-BSD1)
Prepared & Analyzed: 04/16/19
1,1,1,2-Tetrachloroethane
0.0409
0.0050
mg/kg wet
0.05000
82
72-115
1 20
1, 1,1 -Trichloroethane
0.0401
0.0050
mg/kg wet
0.05000
80
67-131
3 20
1,1,2,2-Tetrachloroethane
0.0405
0.0050
mg/kg wet
0.05000
81
56-126
3 20
1,1,2-Trichloroethane
0.0411
0.0050
mg/kg wet
0.05000
82
70-133
3 20
1,1-Dichloroethane
0.0407
0.0050
mg/kg wet
0.05000
81
74-127
2 20
1,1-Dichloroethylene
0.0393
0.0050
mg/kg wet
0.05000
79
67-149
8 20
1, 1 -Dichloropropylene
0.0414
0.0050
mg/kg wet
0.05000
83
71-130
5 20
1,2,3-Trichlorobenzene
0.0401
0.010
mg/kg wet
0.05000
80
68-130
2 20
1,2,3-Trichloropropane
0.0397
0.0050
mg/kg wet
0.05000
79
60-137
2 20
1,2,4-Trichlorobenzene
0.0405
0.010
mg/kg wet
0.05000
81
66-125
2 20
1,2,4-Trimethylbenzene
0.0383
0.0050
mg/kg wet
0.05000
77
69-129
0.4 20
1,2-Dibromoethane
0.0415
0.0050
mg/kg wet
0.05000
83
70-132
2 20
1,2-Dichlorobenzene
0.0394
0.0050
mg/kg wet
0.05000
79
72-123
2 20
1,2-Dichloroethane
0.0412
0.0050
mg/kg wet
0.05000
82
68-128
1 20
1,2-Dichloropropane
0.0420
0.0050
mg/kg wet
0.05000
84
73-130
0.5 20
1,3,5-Trimethylbenzene
0.0395
0.0050
mg/kg wet
0.05000
79
69-128
1 20
1,3-Dichlorobenzene
0.0394
0.0050
mg/kg wet
0.05000
79
71-120
1 20
1,3-Dichloropropane
0.0412
0.0050
mg/kg wet
0.05000
82
75-124
3 20
1,4-Dichlorobenzene
0.0393
0.0050
mg/kg wet
0.05000
79
71-123
0.9 20
2,2-Dichloropropane
0.0412
0.0050
mg/kg wet
0.05000
82
50-142
4 20
2-Chlorotoluene
0.0389
0.0050
mg/kg wet
0.05000
78
67-124
0.9 20
4-Chlorotoluene
0.0391
0.0050
mg/kg wet
0.05000
78
71-126
0.5 20
4-Isopropyltoluene
0.0398
0.0050
mg/kg wet
0.05000
80
68-129
2 20
Acetone
0.0825
0.020
mg/kg wet
0.1000
82
29-198
0.6 20
Benzene
0.0410
0.0050
mg/kg wet
0.05000
82
74-127
2 20
Bromobenzene
0.0390
0.0050
mg/kg wet
0.05000
78
73-125
1 20
Bromochloromethane
0.0409
0.0050
mg/kg wet
0.05000
82
72-134
1 20
Bromodichloromethane
0.0418
0.0050
mg/kg wet
0.05000
84
75-122
0.9 20
Bromoform
0.0417
0.0050
mg/kg wet
0.05000
83
66-135
3 20
Bromomethane
0.0409
0.010
mg/kg wet
0.05000
82
20-180
0.7 20
Carbon Tetrachloride
0.0413
0.0050
mg/kg wet
0.05000
83
64-143
3 20
Chlorobenzene
0.0401
0.0050
mg/kg wet
0.05000
80
74-118
0.7 20
Chloroethane
0.0466
0.010
mg/kg wet
0.05000
93
33-149
3 20
Chloroform
0.0405
0.0050
mg/kg wet
0.05000
81
73-127
2 20
Chloromethane
0.0453
0.010
mg/kg wet
0.05000
91
45-143
3 20
cis-1,2-Dichloroethylene
0.0411
0.0050
mg/kg wet
0.05000
82
76-134
1 20
cis-1,3-Dichloropropylene
0.0424
0.0050
mg/kg wet
0.05000
85
71-125
0.7 20
Dibromochloromethane
0.0412
0.0050
mg/kg wet
0.05000
82
73-122
1 20
Dichlorodifluoromethane
0.0420
0.010
mg/kg wet
0.05000
84
26-146
7 20
Ethylbenzene
0.0400
0.0050
mg/kg wet
0.05000
80
74-128
1 20
Isopropyl Ether
0.0417
0.0050
mg/kg wet
0.05000
83
59-159
0.3 20
Isopropylbenzene (Cumene)
0.0393
0.0050
mg/kg wet
0.05000
79
68-126
2 20
m,p-Xylenes
0.0817
0.010
mg/kg wet
0.1000
82
75-124
0.5 20
Methyl Butyl Ketone (2-Hexanone)
0.0434
0.020
mg/kg wet
0.05000
87
61-157
2 20
Methyl Ethyl Ketone (2-Butanone)
0.0409
0.020
mg/kg wet
0.05000
82
63-149
1 20
Methyl Isobutyl Ketone
0.0436
0.020
mg/kg wet
0.05000
87
57-162
3 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO298 - 5035
LCS Dup (P9D0298-BSD1)
Prepared & Analyzed: 04/16/19
Methylene Chloride
0.0375
0.0050
mg/kg wet
0.05000
75
74-129
0.05 20
Methyl-tert-Butyl Ether
0.0417
0.0050
mg/kg wet
0.05000
83
70-130
0.1 20
Naphthalene
0.0376
0.010
mg/kg wet
0.05000
75
57-157
3 20
n-Butylbenzene
0.0404
0.0050
mg/kg wet
0.05000
81
65-135
2 20
n-Propylbenzene
0.0391
0.0050
mg/kg wet
0.05000
78
67-130
2 20
o-Xylene
0.0402
0.0050
mg/kg wet
0.05000
80
74-126
1 20
sec-Butylbenzene
0.0396
0.0050
mg/kg wet
0.05000
79
66-131
2 20
Styrene
0.0416
0.0050
mg/kg wet
0.05000
83
77-121
0.1 20
tert-Butyl benzene
0.0393
0.0050
mg/kg wet
0.05000
79
67-132
2 20
Tetrachloroethylene
0.0415
0.0050
mg/kg wet
0.05000
83
68-130
3 20
Toluene
0.0404
0.0050
mg/kg wet
0.05000
81
71-129
2 20
trans- 1,2-Dichloroethylene
0.0404
0.0050
mg/kg wet
0.05000
81
73-132
4 20
trans- 1,3-Dichloropropylene
0.0425
0.0050
mg/kg wet
0.05000
85
68-123
0.6 20
Trichloroethylene
0.0416
0.0050
mg/kg wet
0.05000
83
75-133
4 20
Trichlorofluoromethane
0.0446
0.010
mg/kg wet
0.05000
89
44-146
5 20
Vinyl acetate
0.0441
0.010
mg/kg wet
0.05000
88
85-161
4 20
Vinyl chloride
0.0413
0.010
mg/kg wet
0.05000
83
48-147
4 20
Xylenes, total
0.122
0.015
mg/kg wet
0.1500
81
74-126
0.7 20
Surrogate:4-Bromofluorobenzene
49.2
ug/L
50.00
98
70-130
Surrogate: Dibromofluoromethane
48.4
ug/L
50.00
97
84-123
Surrogate: Toluene-d8
48.2
ug/L
50.00
96
76-129
Matrix Spike (P9DO298-MS1)
Source: 9040256-01
Prepared & Analyzed: 04/16/19
1,1,1,2-Tetrachloroethane
0.0345
0.0064
mg/kg dry
0.06354
BRL
54
60-120 M
1,1,1-Trichloroethane
0.0421
0.0064
mg/kg dry
0.06354
BRL
66
52-139
1,1,2,2-Tetrachloroethane
0.0281
0.0064
mg/kg dry
0.06354
BRL
44
39-135
1,1,2-Trichloroethane
0.0314
0.0064
mg/kg dry
0.06354
BRL
49
44-140
1,1-Dichloroethane
0.0400
0.0064
mg/kg dry
0.06354
BRL
63
59-137
1,1-Dichloroethylene
0.0438
0.0064
mg/kg dry
0.06354
BRL
69
54-162
1, 1 -Dichloropropylene
0.0434
0.0064
mg/kg dry
0.06354
BRL
68
55-137
1,2,3-Trichlorobenzene
0.0279
0.013
mg/kg dry
0.06354
BRL
44
34-120
1,2,3-Trichloropropane
0.0276
0.0064
mg/kg dry
0.06354
BRL
43
45-139 M
1,2,4-Trichlorobenzene
0.0279
0.013
mg/kg dry
0.06354
BRL
44
35-116
1,2,4-Trimethylbenzene
0.0328
0.0064
mg/kg dry
0.06354
BRL
52
38-142
1,2-Dibromoethane
0.0311
0.0064
mg/kg dry
0.06354
BRL
49
49-132
1,2-Dichlorobenzene
0.0300
0.0064
mg/kg dry
0.06354
BRL
47
42-130
1,2-Dichloroethane
0.0341
0.0064
mg/kg dry
0.06354
BRL
54
51-131
1,2-Dichloropropane
0.0368
0.0064
mg/kg dry
0.06354
BRL
58
55-138
1,3,5-Trimethylbenzene
0.0350
0.0064
mg/kg dry
0.06354
BRL
55
44-140
1,3-Dichlorobenzene
0.0314
0.0064
mg/kg dry
0.06354
BRL
49
41-129
1,3-Dichloropropane
0.0312
0.0064
mg/kg dry
0.06354
BRL
49
53-129 M
1,4-Dichlorobenzene
0.0306
0.0064
mg/kg dry
0.06354
BRL
48
44-134
2,2-Dichloropropane
0.0424
0.0064
mg/kg dry
0.06354
BRL
67
30-147
2-Chlorotoluene
0.0335
0.0064
mg/kg dry
0.06354
BRL
53
46-132
4-Chlorotoluene
0.0326
0.0064
mg/kg dry
0.06354
BRL
51
44-135
4-Isopropyltoluene
0.0357
0.0064
mg/kg dry
0.06354
BRL
56
32-144
Acetone
0.0643
0.025
mg/kg dry
0.1271
BRL
51
34-143
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO298 - 5035
Matrix Spike (P9D0298-MS1)
Source: 9040256-01
Prepared & Analyzed: 04/16/19
Benzene
0.0400
0.0064
mg/kg dry
0.06354
BRL
63
60-135
Bromobenzene
0.0313
0.0064
mg/kg dry
0.06354
BRL
49
45-135
Bromochloromethane
0.0345
0.0064
mg/kg dry
0.06354
BRL
54
55-136 M
Bromodichloromethane
0.0355
0.0064
mg/kg dry
0.06354
BRL
56
55-127
Bromoform
0.0302
0.0064
mg/kg dry
0.06354
BRL
48
40-136
Bromomethane
0.0334
0.013
mg/kg dry
0.06354
BRL
53
30-137
Carbon Tetrachloride
0.0442
0.0064
mg/kg dry
0.06354
BRL
70
48-153
Chlorobenzene
0.0350
0.0064
mg/kg dry
0.06354
BRL
55
57-125 M
Chloroethane
0.0443
0.013
mg/kg dry
0.06354
BRL
70
16-177
Chloroform
0.0388
0.0064
mg/kg dry
0.06354
BRL
61
56-137
Chloromethane
0.0434
0.013
mg/kg dry
0.06354
BRL
68
40-145
cis-1,2-Dichloroethylene
0.0384
0.0064
mg/kg dry
0.06354
BRL
60
58-140
cis-1,3-Dichloropropylene
0.0350
0.0064
mg/kg dry
0.06354
BRL
55
42-135
Dibromochloromethane
0.0320
0.0064
mg/kg dry
0.06354
BRL
50
49-127
Dichlorodifluoromethane
0.0455
0.013
mg/kg dry
0.06354
BRL
72
25-151
Ethylbenzene
0.0372
0.0064
mg/kg dry
0.06354
BRL
58
44-144
Isopropyl Ether
0.0357
0.0064
mg/kg dry
0.06354
BRL
56
51-155
Isopropylbenzene (Cumene)
0.0364
0.0064
mg/kg dry
0.06354
BRL
57
41-140
m,p-Xylenes
0.0751
0.013
mg/kg dry
0.1271
BRL
59
36-148
Methyl Butyl Ketone (2-Hexanone)
0.0286
0.025
mg/kg dry
0.06354
BRL
45
30-147
Methyl Ethyl Ketone (2-Butanone)
0.0289
0.025
mg/kg dry
0.06354
BRL
45
24-160
Methyl Isobutyl Ketone
0.0301
0.025
mg/kg dry
0.06354
BRL
47
25-163
Methylene Chloride
0.0347
0.0064
mg/kg dry
0.06354
BRL
55
53-144
Methyl-tert-Butyl Ether
0.0327
0.0064
mg/kg dry
0.06354
BRL
51
49-135
Naphthalene
0.0245
0.013
mg/kg dry
0.06354
BRL
38
32-127
n-Butylbenzene
0.0356
0.0064
mg/kg dry
0.06354
BRL
56
23-148
n-Propylbenzene
0.0360
0.0064
mg/kg dry
0.06354
BRL
57
35-144
o-Xylene
0.0356
0.0064
mg/kg dry
0.06354
BRL
56
43-143
sec-Butylbenzene
0.0367
0.0064
mg/kg dry
0.06354
BRL
58
34-144
Styrene
0.0349
0.0064
mg/kg dry
0.06354
BRL
55
42-132
tert-Butyl benzene
0.0363
0.0064
mg/kg dry
0.06354
BRL
57
36-150
Tetrachloroethylene
0.0419
0.0064
mg/kg dry
0.06354
BRL
66
47-142
Toluene
0.0388
0.0064
mg/kg dry
0.06354
BRL
61
57-135
trans- 1,2-Dichloroethylene
0.0413
0.0064
mg/kg dry
0.06354
BRL
65
58-141
trans- 1,3-Dichloropropylene
0.0339
0.0064
mg/kg dry
0.06354
BRL
53
41-124
Trichloroethylene
0.0412
0.0064
mg/kg dry
0.06354
BRL
65
38-164
Trichlorofluoromethane
0.0471
0.013
mg/kg dry
0.06354
BRL
74
30-157
Vinyl acetate
0.0134
0.013
mg/kg dry
0.06354
BRL
21
61-154 M
Vinyl chloride
0.0434
0.013
mg/kg dry
0.06354
BRL
68
40-156
Xylenes, total
0.111
0.019
mg/kg dry
0.1906
BRL
58
36-148
Surrogate:4-Bromofluorobenzene
49.0
ug/L
50.00
98
70-130
Surrogate: Dibromofluoromethane
50.7
ug/L
50.00
101
84-123
Surrogate: Toluene-d8
47.2
ug/L
50.00
94
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO298 - 5035
Matrix Spike Dup (P9D0298-MSD1)
Source: 9040256-01
Prepared & Analyzed: 04/16/19
1,1,1,2-Tetrachloroethane
0.0341
0.0064
mg/kg dry
0.06354
BRL
54
60-120
1
15
1,1,1-Trichloroethane
0.0424
0.0064
mg/kg dry
0.06354
BRL
67
52-139
0.6
21
1,1,2,2-Tetrachloroethane
0.0284
0.0064
mg/kg dry
0.06354
BRL
45
39-135
0.8
22
1,1,2-Trichloroethane
0.0315
0.0064
mg/kg dry
0.06354
BRL
50
44-140
0.4
21
1,1-Dichloroethane
0.0401
0.0064
mg/kg dry
0.06354
BRL
63
59-137
0.3
21
1,1-Dichloroethylene
0.0439
0.0064
mg/kg dry
0.06354
BRL
69
54-162
0.2
22
1, 1 -Dichloropropylene
0.0440
0.0064
mg/kg dry
0.06354
BRL
69
55-137
1
19
1,2,3-Trichlorobenzene
0.0288
0.013
mg/kg dry
0.06354
BRL
45
34-120
3
41
1,2,3-Trichloropropane
0.0277
0.0064
mg/kg dry
0.06354
BRL
44
45-139
0.4
25
1,2,4-Trichlorobenzene
0.0287
0.013
mg/kg dry
0.06354
BRL
45
35-116
3
62
1,2,4-Trimethylbenzene
0.0333
0.0064
mg/kg dry
0.06354
BRL
52
38-142
2
24
1,2-Dibromoethane
0.0315
0.0064
mg/kg dry
0.06354
BRL
49
49-132
1
15
1,2-Dichlorobenzene
0.0310
0.0064
mg/kg dry
0.06354
BRL
49
42-130
3
21
1,2-Dichloroethane
0.0343
0.0064
mg/kg dry
0.06354
BRL
54
51-131
0.6
13
1,2-Dichloropropane
0.0370
0.0064
mg/kg dry
0.06354
BRL
58
55-138
0.3
16
1,3,5-Trimethylbenzene
0.0353
0.0064
mg/kg dry
0.06354
BRL
56
44-140
0.7
29
1,3-Dichlorobenzene
0.0319
0.0064
mg/kg dry
0.06354
BRL
50
41-129
2
24
1,3-Dichloropropane
0.0316
0.0064
mg/kg dry
0.06354
BRL
50
53-129
1
15
1,4-Dichlorobenzene
0.0311
0.0064
mg/kg dry
0.06354
BRL
49
44-134
2
21
2,2-Dichloropropane
0.0430
0.0064
mg/kg dry
0.06354
BRL
68
30-147
1
20
2-Chlorotoluene
0.0342
0.0064
mg/kg dry
0.06354
BRL
54
46-132
2
29
4-Chlorotoluene
0.0332
0.0064
mg/kg dry
0.06354
BRL
52
44-135
2
23
4-Isopropyltoluene
0.0362
0.0064
mg/kg dry
0.06354
BRL
57
32-144
1
22
Acetone
0.0632
0.025
mg/kg dry
0.1271
BRL
50
34-143
2
49
Benzene
0.0396
0.0064
mg/kg dry
0.06354
BRL
62
60-135
0.9
20
Bromobenzene
0.0318
0.0064
mg/kg dry
0.06354
BRL
50
45-135
2
25
Bromochloromethane
0.0349
0.0064
mg/kg dry
0.06354
BRL
55
55-136
1
18
Bromodichloromethane
0.0364
0.0064
mg/kg dry
0.06354
BRL
57
55-127
2
17
Bromoform
0.0306
0.0064
mg/kg dry
0.06354
BRL
48
40-136
1
35
Bromomethane
0.0372
0.013
mg/kg dry
0.06354
BRL
59
30-137
11
30
Carbon Tetrachloride
0.0444
0.0064
mg/kg dry
0.06354
BRL
70
48-153
0.4
23
Chlorobenzene
0.0350
0.0064
mg/kg dry
0.06354
BRL
55
57-125
0.1
14
Chloroethane
0.0451
0.013
mg/kg dry
0.06354
BRL
71
16-177
2
47
Chloroform
0.0390
0.0064
mg/kg dry
0.06354
BRL
61
56-137
0.7
18
Chloromethane
0.0453
0.013
mg/kg dry
0.06354
BRL
71
40-145
4
26
cis-1,2-Dichloroethylene
0.0383
0.0064
mg/kg dry
0.06354
BRL
60
58-140
0.3
28
cis-1,3-Dichloropropylene
0.0355
0.0064
mg/kg dry
0.06354
BRL
56
42-135
1
32
Dibromochloromethane
0.0322
0.0064
mg/kg dry
0.06354
BRL
51
49-127
0.5
24
Dichlorodifluoromethane
0.0447
0.013
mg/kg dry
0.06354
BRL
70
25-151
2
37
Ethylbenzene
0.0371
0.0064
mg/kg dry
0.06354
BRL
58
44-144
0.03
19
Isopropyl Ether
0.0361
0.0064
mg/kg dry
0.06354
BRL
57
51-155
1
13
Isopropylbenzene (Cumene)
0.0364
0.0064
mg/kg dry
0.06354
BRL
57
41-140
0.2
27
m,p-Xylenes
0.0752
0.013
mg/kg dry
0.1271
BRL
59
36-148
0.2
20
Methyl Butyl Ketone (2-Hexanone)
0.0276
0.025
mg/kg dry
0.06354
BRL
43
30-147
4
42
Methyl Ethyl Ketone (2-Butanone)
0.0285
0.025
mg/kg dry
0.06354
BRL
45
24-160
1
42
Methyl Isobutyl Ketone
0.0297
0.025
mg/kg dry
0.06354
BRL
47
25-163
1
44
M
M
M
J&
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO298 - 5035
Matrix Spike Dup (P9D0298-MSD1)
Source: 9040256-01
Prepared & Analyzed: 04/16/19
Methylene Chloride
0.0346
0.0064
mg/kg dry
0.06354
BRL
55
53-144
0.04
14
Methyl-tert-Butyl Ether
0.0327
0.0064
mg/kg dry
0.06354
BRL
51
49-135
0.2
22
Naphthalene
0.0253
0.013
mg/kg dry
0.06354
BRL
40
32-127
3
44
n-Butylbenzene
0.0365
0.0064
mg/kg dry
0.06354
BRL
57
23-148
2
39
n-Propylbenzene
0.0361
0.0064
mg/kg dry
0.06354
BRL
57
35-144
0.4
27
o-Xylene
0.0359
0.0064
mg/kg dry
0.06354
BRL
56
43-143
0.6
17
sec-Butylbenzene
0.0373
0.0064
mg/kg dry
0.06354
BRL
59
34-144
2
28
Styrene
0.0352
0.0064
mg/kg dry
0.06354
BRL
55
42-132
0.7
28
tert-Butylbenzene
0.0371
0.0064
mg/kg dry
0.06354
BRL
58
36-150
2
29
Tetrachloroethylene
0.0421
0.0064
mg/kg dry
0.06354
BRL
66
47-142
0.4
26
Toluene
0.0389
0.0064
mg/kg dry
0.06354
BRL
61
57-135
0.2
22
trans-1,2-Dichloroethylene
0.0417
0.0064
mg/kg dry
0.06354
BRL
66
58-141
1
18
trans- 1,3-Dichloropropylene
0.0342
0.0064
mg/kg dry
0.06354
BRL
54
41-124
0.9
20
Trichloroethylene
0.0414
0.0064
mg/kg dry
0.06354
BRL
65
38-164
0.5
18
Trichlorofluoromethane
0.0468
0.013
mg/kg dry
0.06354
BRL
74
30-157
0.7
27
Vinyl acetate
0.0155
0.013
mg/kg dry
0.06354
BRL
24
61-154
15
35 M
Vinyl chloride
0.0429
0.013
mg/kg dry
0.06354
BRL
68
40-156
1
35
Xylenes, total
0.111
0.019
mg/kg dry
0.1906
BRL
58
36-148
0.3
20
Surrogate:4-Bromofluorobenzene
49.9
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
50.7
ug/L
50.00
101
84-123
Surrogate: Toluene-d8
47.4
ug/L
50.00
95
76-129
Batch P9DO320 - 5030B
Blank (P9D0320-BLK1)
Prepared & Analyzed: 04/17/19
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1,1-Dichloropropylene
BRL
0.50
ug/L
1,2,3-Trichlorobenzene
BRL
2.0
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
BRL
1.0
ug/L
1,2,4-Trimethyl benzene
BRL
0.50
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,3,5-Trimethyl benzene
BRL
0.50
ug/L
1,3-Dichlorobenzene
BRL
0.50
ug/L
1,3-Dichloropropane
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
2-Chlorotoluene
BRL
0.50
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO320 - 5030B
Blank (P9D0320-BLK1)
Prepared & Analyzed: 04/17/19
4-Chlorotoluene
BRL
0.50
ug/L
4-Isopropyltoluene
BRL
0.50
ug/L
Acetone
BRL
5.0
ug/L
Acrolein
BRL
20
ug/L
Acrylonitrile
BRL
20
ug/L
Benzene
BRL
0.50
ug/L
Bromobenzene
BRL
0.50
ug/L
Bromochloromethane
BRL
0.50
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
1.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
0.50
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromomethane
BRL
0.50
ug/L
Dichlorodifluoromethane
BRL
1.0
ug/L
Ethylbenzene
BRL
0.50
ug/L
Hexachlorobutadiene
BRL
2.0
ug/L
Isopropyl Ether
BRL
0.50
ug/L
Isopropylbenzene (Cumene)
BRL
0.50
ug/L
m,p-Xylenes
BRL
1.0
ug/L
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methylene Chloride
BRL
1.0
ug/L
Methyl-tert-Butyl Ether
BRL
0.50
ug/L
Naphthalene
BRL
1.0
ug/L
n-Butylbenzene
BRL
1.0
ug/L
n-Propylbenzene
BRL
0.50
ug/L
o-Xylene
BRL
0.50
ug/L
sec-Butylbenzene
BRL
0.50
ug/L
Styrene
BRL
0.50
ug/L
tert-Butylbenzene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Toluene
BRL
0.50
ug/L
trans-1,2-Dichloroethylene
BRL
0.50
ug/L
trans-1,3-Dichloropropylene
BRL
0.50
ug/L
Trichloroethylene
BRL
0.50
ug/L
Trichlorofluoromethane
BRL
0.50
ug/L
Vinyl acetate
BRL
2.0
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO320 - 5030B
Blank (P9D0320-BLK1)
Prepared & Analyzed: 04/17/19
Vinyl chloride
BRL
0.50
ug/L
Xylenes, total
BRL
1.5
ug/L
Surrogate:4-Bromofluorobenzene
50.5
ug/L
50.00
101
80-124
Surrogate: Dibromofluoromethane
50.6
ug/L
50.00
101
75-129
Surrogate: Toluene-d8
49.7
ug/L
50.00
99
77-123
LCS (1139D0320-113SI)
Prepared & Analyzed: 04/17/19
1,1,1,2-Tetrachloroethane
17.1
0.50
ug/L
20.00
86
79-134
1,1,1-Trichloroethane
19.2
0.50
ug/L
20.00
96
75-136
1,1,2,2-Tetrachloroethane
18.5
0.50
ug/L
20.00
92
62-127
1,1,2-Trichloroethane
20.1
0.50
ug/L
20.00
100
70-140
1,1-Dichloroethane
20.1
0.50
ug/L
20.00
101
78-130
1,1-Dichloroethylene
18.3
0.50
ug/L
20.00
91
70-154
1, 1 -Dichloropropylene
18.8
0.50
ug/L
20.00
94
71-136
1,2,3-Trichlorobenzene
19.9
2.0
ug/L
20.00
100
58-144
1,2,3-Trichloropropane
19.2
1.0
ug/L
20.00
96
71-127
1,2,4-Trichlorobenzene
19.0
1.0
ug/L
20.00
95
66-139
1,2,4-Trimethylbenzene
17.2
0.50
ug/L
20.00
86
75-133
1,2-Dibromo-3-chloropropane
18.0
2.0
ug/L
20.00
90
63-134
1,2-Dibromoethane
19.5
0.50
ug/L
20.00
97
77-135
1,2-Dichlorobenzene
19.1
0.50
ug/L
20.00
96
78-128
1,2-Dichloroethane
20.5
0.50
ug/L
20.00
103
68-131
1,2-Dichloropropane
20.1
0.50
ug/L
20.00
101
77-130
1,3,5-Trimethylbenzene
17.4
0.50
ug/L
20.00
87
75-131
1,3-Dichlorobenzene
18.5
0.50
ug/L
20.00
92
77-125
1,3-Dichloropropane
19.1
0.50
ug/L
20.00
96
76-132
1,4-Dichlorobenzene
18.5
0.50
ug/L
20.00
92
75-126
2,2-Dichloropropane
18.1
2.0
ug/L
20.00
90
29-149
2-Chlorotoluene
19.5
0.50
ug/L
20.00
98
74-126
4-Chlorotoluene
18.5
0.50
ug/L
20.00
93
78-129
4-Isopropyltoluene
18.1
0.50
ug/L
20.00
91
69-132
Acetone
40.4
5.0
ug/L
40.00
101
40-166
Acrolein
38.5
20
ug/L
40.00
96
70-130
Acrylonitrile
40.9
20
ug/L
40.00
102
81-127
Benzene
19.1
0.50
ug/L
20.00
96
77-128
Bromobenzene
19.0
0.50
ug/L
20.00
95
78-129
Bromochloromethane
19.5
0.50
ug/L
20.00
98
78-135
Bromodichloromethane
20.2
0.50
ug/L
20.00
101
76-138
Bromoform
15.2
1.0
ug/L
20.00
76
71-135
Bromomethane
16.8
1.0
ug/L
20.00
84
41-168
Carbon disulfide
19.2
5.0
ug/L
20.00
96
59-135
Carbon Tetrachloride
17.8
0.50
ug/L
20.00
89
72-142
Chlorobenzene
18.2
0.50
ug/L
20.00
91
78-119
Chloroethane
24.0
0.50
ug/L
20.00
120
57-142
Chloroform
20.2
0.50
ug/L
20.00
101
77-130
Chloromethane
19.2
0.50
ug/L
20.00
96
47-145
cis-1,2-Dichloroethylene
20.0
0.50
ug/L
20.00
100
76-141
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO320 - 5030B
LCS (P9D0320-BS1)
Prepared & Analyzed: 04/17/19
cis-1,3-Dichloropropylene
17.8
0.50
ug/L
20.00
89
65-140
Dibromochloromethane
16.5
0.50
ug/L
20.00
82
75-134
Dibromomethane
19.1
0.50
ug/L
20.00
95
76-138
Dichlorodifluoromethane
19.5
1.0
ug/L
20.00
98
28-163
Ethylbenzene
18.1
0.50
ug/L
20.00
91
80-127
Hexachlorobutadiene
20.2
2.0
ug/L
20.00
101
61-134
Isopropyl Ether
20.8
0.50
ug/L
20.00
104
60-154
Isopropylbenzene (Cumene)
21.2
0.50
ug/L
20.00
106
70-130
m,p-Xylenes
32.6
1.0
ug/L
40.00
82
77-133
Methyl Butyl Ketone (2-Hexanone)
17.9
5.0
ug/L
20.00
90
64-137
Methyl Ethyl Ketone (2-Butanone)
18.0
5.0
ug/L
20.00
90
71-134
Methyl Isobutyl Ketone
18.4
5.0
ug/L
20.00
92
69-134
Methylene Chloride
19.6
1.0
ug/L
20.00
98
73-131
Methyl-tert-Butyl Ether
18.2
0.50
ug/L
20.00
91
68-135
Naphthalene
18.3
1.0
ug/L
20.00
91
64-136
n-Butylbenzene
19.4
1.0
ug/L
20.00
97
68-134
n-Propylbenzene
19.9
0.50
ug/L
20.00
100
72-132
o-Xylene
18.4
0.50
ug/L
20.00
92
78-128
sec-Butylbenzene
17.7
0.50
ug/L
20.00
88
71-131
Styrene
16.7
0.50
ug/L
20.00
83
78-129
tert-Butylbenzene
18.4
0.50
ug/L
20.00
92
70-132
Tetrachloroethylene
18.5
0.50
ug/L
20.00
92
80-129
Toluene
19.4
0.50
ug/L
20.00
97
76-131
trans-1,2-Dichloroethylene
20.4
0.50
ug/L
20.00
102
76-135
trans-1,3-Dichloropropylene
17.2
0.50
ug/L
20.00
86
67-140
Trichloroethylene
19.5
0.50
ug/L
20.00
98
77-133
Trichlorofluoromethane
14.2
0.50
ug/L
20.00
71
62-148
Vinyl acetate
17.5
2.0
ug/L
20.00
87
34-167
Vinyl chloride
20.6
0.50
ug/L
20.00
103
57-141
Xylenes, total
51.0
1.5
ug/L
60.00
85
77-133
Surrogate:4-Bromofluorobenzene
52.4
ug/L
50.00
105
80-124
Surrogate: Dibromofluoromethane
52.0
ug/L
50.00
104
75-129
Surrogate: Toluene-d8
48.9
ug/L
50.00
98
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO320 - 5030B
LCS Dup (P91130320-13SD1)
Prepared & Analyzed: 04/17/19
1,1,1,2-Tetrachloroethane
16.3
0.50
ug/L
20.00
82
79-134
5
20
1,1,1-Trichloroethane
18.4
0.50
ug/L
20.00
92
75-136
4
20
1,1,2,2-Tetrachloroethane
18.1
0.50
ug/L
20.00
90
62-127
2
20
1,1,2-Trichloroethane
19.7
0.50
ug/L
20.00
98
70-140
2
20
1,1-Dichloroethane
19.3
0.50
ug/L
20.00
97
78-130
4
20
1,1-Dichloroethylene
17.5
0.50
ug/L
20.00
87
70-154
5
20
1, 1 -Dichloropropylene
18.0
0.50
ug/L
20.00
90
71-136
4
20
1,2,3-Trichlorobenzene
19.3
2.0
ug/L
20.00
97
58-144
3
20
1,2,3-Trichloropropane
16.7
1.0
ug/L
20.00
83
71-127
14
20
1,2,4-Trichlorobenzene
19.2
1.0
ug/L
20.00
96
66-139
1
20
1,2,4-Trimethylbenzene
16.3
0.50
ug/L
20.00
81
75-133
6
20
1,2-Dibromo-3-chloropropane
18.6
2.0
ug/L
20.00
93
63-134
3
20
1,2-Dibromoethane
20.1
0.50
ug/L
20.00
100
77-135
3
20
1,2-Dichlorobenzene
18.7
0.50
ug/L
20.00
93
78-128
2
20
1,2-Dichloroethane
20.5
0.50
ug/L
20.00
103
68-131
0.05
20
1,2-Dichloropropane
19.5
0.50
ug/L
20.00
97
77-130
3
20
1,3,5-Trimethylbenzene
16.5
0.50
ug/L
20.00
83
75-131
5
20
1,3-Dichlorobenzene
17.9
0.50
ug/L
20.00
89
77-125
3
20
1,3-Dichloropropane
19.9
0.50
ug/L
20.00
100
76-132
4
20
1,4-Dichlorobenzene
18.3
0.50
ug/L
20.00
92
75-126
0.8
20
2,2-Dichloropropane
17.5
2.0
ug/L
20.00
88
29-149
3
20
2-Chlorotoluene
18.1
0.50
ug/L
20.00
90
74-126
8
20
4-Chlorotoluene
18.1
0.50
ug/L
20.00
90
78-129
2
20
4-Isopropyltoluene
17.2
0.50
ug/L
20.00
86
69-132
5
20
Acetone
41.9
5.0
ug/L
40.00
105
40-166
4
20
Acrolein
36.2
20
ug/L
40.00
91
70-130
6
20
Acrylonitrile
40.6
20
ug/L
40.00
102
81-127
0.7
20
Benzene
18.5
0.50
ug/L
20.00
92
77-128
3
20
Bromobenzene
18.5
0.50
ug/L
20.00
93
78-129
3
20
Bromochloromethane
18.4
0.50
ug/L
20.00
92
78-135
6
20
Bromodichloromethane
20.0
0.50
ug/L
20.00
100
76-138
1
20
Bromoform
15.7
1.0
ug/L
20.00
79
71-135
3
20
Bromomethane
17.1
1.0
ug/L
20.00
85
41-168
2
20
Carbon disulfide
18.1
5.0
ug/L
20.00
90
59-135
6
20
Carbon Tetrachloride
17.2
0.50
ug/L
20.00
86
72-142
3
20
Chlorobenzene
18.0
0.50
ug/L
20.00
90
78-119
0.8
20
Chloroethane
23.6
0.50
ug/L
20.00
118
57-142
1
20
Chloroform
19.4
0.50
ug/L
20.00
97
77-130
4
20
Chloromethane
17.0
0.50
ug/L
20.00
85
47-145
12
20
cis-1,2-Dichloroethylene
19.3
0.50
ug/L
20.00
97
76-141
4
20
cis-1,3-Dichloropropylene
17.1
0.50
ug/L
20.00
86
65-140
4
20
Dibromochloromethane
17.1
0.50
ug/L
20.00
86
75-134
4
20
Dibromomethane
18.6
0.50
ug/L
20.00
93
76-138
2
20
Dichlorodifluoromethane
18.4
1.0
ug/L
20.00
92
28-163
6
20
Ethylbenzene
18.0
0.50
ug/L
20.00
90
80-127
0.8
20
Hexachlorobutadiene
17.8
2.0
ug/L
20.00
89
61-134
12
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
4/22/19
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO320 - 5030B
LCS Dup (P9D0320-BSD1)
Prepared & Analyzed: 04/17/19
Isopropyl Ether
20.1
0.50
ug/L
20.00
100
60-154
4
20
Isopropylbenzene (Cumene)
19.5
0.50
ug/L
20.00
97
70-130
8
20
m,p-Xylenes
32.6
1.0
ug/L
40.00
81
77-133
0.2
20
Methyl Butyl Ketone (2-Hexanone)
19.0
5.0
ug/L
20.00
95
64-137
6
20
Methyl Ethyl Ketone (2-Butanone)
18.1
5.0
ug/L
20.00
90
71-134
0.7
20
Methyl Isobutyl Ketone
19.0
5.0
ug/L
20.00
95
69-134
4
20
Methylene Chloride
19.2
1.0
ug/L
20.00
96
73-131
2
20
Methyl-tert-Butyl Ether
18.9
0.50
ug/L
20.00
94
68-135
4
20
Naphthalene
18.6
1.0
ug/L
20.00
93
64-136
2
20
n-Butylbenzene
18.6
1.0
ug/L
20.00
93
68-134
4
20
n-Propylbenzene
18.6
0.50
ug/L
20.00
93
72-132
7
20
o-Xylene
18.2
0.50
ug/L
20.00
91
78-128
1
20
sec-Butylbenzene
17.1
0.50
ug/L
20.00
86
71-131
3
20
Styrene
17.0
0.50
ug/L
20.00
85
78-129
2
20
tert-Butylbenzene
18.0
0.50
ug/L
20.00
90
70-132
3
20
Tetrachloroethylene
18.1
0.50
ug/L
20.00
90
80-129
2
20
Toluene
18.7
0.50
ug/L
20.00
93
76-131
4
20
trans-1,2-Dichloroethylene
19.8
0.50
ug/L
20.00
99
76-135
3
20
trans- 1,3-Dichloropropylene
17.2
0.50
ug/L
20.00
86
67-140
0.1
20
Trichloroethylene
18.5
0.50
ug/L
20.00
92
77-133
5
20
Trichlorofluoromethane
14.6
0.50
ug/L
20.00
73
62-148
3
20
Vinyl acetate
17.9
2.0
ug/L
20.00
89
34-167
2
20
Vinyl chloride
19.3
0.50
ug/L
20.00
96
57-141
6
20
Xylenes, total
50.7
1.5
ug/L
60.00
85
77-133
0.6
20
Surrogate:4-Bromofluorobenzene
49.5
ug/L
50.00
99
80-124
Surrogate: Dibromofluoromethane
50.1
ug/L
50.00
100
75-129
Surrogate: Toluene-d8
49.7
ug/L
50.00
99
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO284 - 3510C MS
Blank (P9D0284-BLK1)
Prepared: 04/16/19 Analyzed: 04/17/19
1,2,4-Trichlorobenzene
BRL
10
ug/L
1,2-Dichlorobenzene
BRL
10
ug/L
1,3-Dichlorobenzene
BRL
10
ug/L
1,4-Dichlorobenzene
BRL
10
ug/L
1-Methyl naphthalene
BRL
10
ug/L
2,4,5-Trichlorophenol
BRL
20
ug/L
2,4,6-Trichlorophenol
BRL
20
ug/L
2,4-Dichlorophenol
BRL
10
ug/L
2,4-Dimethylphenol
BRL
10
ug/L
2,4-Dinitrophenol
BRL
50
ug/L
2,4-Dinitrotoluene
BRL
10
ug/L
2,6-Dinitrotoluene
BRL
20
ug/L
2-Chloronaphthalene
BRL
20
ug/L
2-Chlorophenol
BRL
10
ug/L
2-Methyl naphthalene
BRL
10
ug/L
2-Methylphenol
BRL
10
ug/L
2-Nitroaniline
BRL
10
ug/L
2-Nitrophenol
BRL
10
ug/L
3,3'-Dichlorobenzidine
BRL
10
ug/L
3/4-Methyl phenol
BRL
10
ug/L
3-Nitroaniline
BRL
10
ug/L
4,6-Dinitro-2-methylphenol
BRL
50
ug/L
4-Bromophenyl phenyl ether
BRL
20
ug/L
4-Chloro-3-methylphenol
BRL
10
ug/L
4-Chloroaniline
BRL
10
ug/L
4-Chlorophenyl phenyl ether
BRL
20
ug/L
4-Nitroaniline
BRL
10
ug/L
4-Nitrophenol
BRL
10
ug/L
Acenaphthene
BRL
20
ug/L
Acenaphthylene
BRL
20
ug/L
Aniline
BRL
20
ug/L
Anthracene
BRL
20
ug/L
Azobenzene
BRL
10
ug/L
Benzo(a)anthracene
BRL
10
ug/L
Benzo(a)pyrene
BRL
10
ug/L
Benzo(b)fluoranthene
BRL
10
ug/L
Benzo(g,h,i)perylene
BRL
10
ug/L
Benzo(k)fluoranthene
BRL
10
ug/L
Benzoic Acid
BRL
100
ug/L
Benzyl alcohol
BRL
10
ug/L
bis(2-Chloroethoxy)methane
BRL
10
ug/L
Bis(2-Chloroethyl)ether
BRL
10
ug/L
Bis(2-chloroisopropyl)ether
BRL
10
ug/L
Bis(2-Ethylhexyl)phthalate
BRL
10
ug/L
Butyl benzyl phthalate
BRL
10
ug/L
Chrysene
BRL
10
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO284 - 3510C MS
Blank (P9D0284-BLK1)
Prepared: 04/16/19 Analyzed: 04/17/19
Dibenzo(a,h)anthracene
BRL
10
ug/L
Dibenzofuran
BRL
20
ug/L
Diethyl phthalate
BRL
20
ug/L
Dimethyl phthalate
BRL
20
ug/L
Di-n-butyl phthalate
BRL
20
ug/L
Di-n-octyl phthalate
BRL
10
ug/L
Fluoranthene
BRL
20
ug/L
Fluorene
BRL
20
ug/L
Hexachlorobenzene
BRL
20
ug/L
Hexachlorobutadiene
BRL
10
ug/L
Hexachlorocyclopentadiene
BRL
10
ug/L
Hexachloroethane
BRL
10
ug/L
Indeno(1,2,3-cd)pyrene
BRL
10
ug/L
Isophorone
BRL
10
ug/L
Naphthalene
BRL
10
ug/L
Nitrobenzene
BRL
10
ug/L
N-Nitroso-di-n-propylamine
BRL
20
ug/L
N-Nitrosodiphenylamine
BRL
20
ug/L
Pentachlorophenol
BRL
10
ug/L
Phenanthrene
BRL
20
ug/L
Phenol
BRL
10
ug/L
Pyrene
BRL
10
ug/L
Surrogate: 2,4,6-Tribromophenol
116
ug/L
100.0
116
43-140
Surrogate:2-Fluorobiphenyl
53.9
ug/L
50.00
108
44-119
Surrogate:2-Fluorophenol
71.7
ug/L
100.0
72
19-119
Surrogate: Nitrobenzene-d5
51.7
ug/L
50.00
103
44-120
Surrogate: Phenol-d5
44.6
ug/L
100.0
45
11-52
Surrogate: Terphenyl-d14
56.4
ug/L
50.00
113
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO284 - 3510C MS
LCS (P9D0284-BS1)
Prepared: 04/16/19 Analyzed: 04/17/19
1,2,4-Trichlorobenzene
30.6
10
ug/L
50.00
61
29-126
1,2-Dichlorobenzene
29.0
10
ug/L
50.00
58
32-111
1,3-Dichlorobenzene
26.5
10
ug/L
50.00
53
28-110
1,4-Dichlorobenzene
27.8
10
ug/L
50.00
56
29-112
1-Methyl naphthalene
37.3
10
ug/L
50.00
75
41-119
2,4,5-Trichlorophenol
44.8
20
ug/L
50.00
90
53-123
2,4,6-Trichlorophenol
45.6
20
ug/L
50.00
91
50-125
2,4-Dichlorophenol
38.1
10
ug/L
50.00
76
47-121
2,4-Dimethylphenol
46.0
10
ug/L
50.00
92
31-124
2,4-Dinitrophenol
25.7
50
ug/L
50.00
51
23-143 J
2,4-Dinitrotoluene
47.9
10
ug/L
50.00
96
57-128
2,6-Dinitrotoluene
46.3
20
ug/L
50.00
93
57-124
2-Chloronaphthalene
43.3
20
ug/L
50.00
87
40-116
2-Chlorophenol
38.4
10
ug/L
50.00
77
38-117
2-Methyl naphthalene
36.1
10
ug/L
50.00
72
40-121
2-Methylphenol
37.3
10
ug/L
50.00
75
30-117
2-Nitroaniline
45.7
10
ug/L
50.00
91
55-127
2-Nitrophenol
36.1
10
ug/L
50.00
72
47-123
3,3'-Dichlorobenzidine
46.5
10
ug/L
50.00
93
27-129
3/4-Methyl phenol
31.0
10
ug/L
50.00
62
29-110
3-Nitroaniline
47.1
10
ug/L
50.00
94
41-128
4,6-Dinitro-2-methylphenol
39.9
50
ug/L
50.00
80
44-137 J
4-Bromophenyl phenyl ether
46.5
20
ug/L
50.00
93
55-124
4-Chloro-3-methylphenol
39.5
10
ug/L
50.00
79
52-119
4-Chloroaniline
39.8
10
ug/L
50.00
80
33-117
4-Chlorophenyl phenyl ether
46.8
20
ug/L
50.00
94
53-121
4-Nitroaniline
47.6
10
ug/L
50.00
95
45-135
4-Nitrophenol
19.8
10
ug/L
50.00
40
10-77
Acenaphthene
46.9
20
ug/L
50.00
94
47-122
Acenaphthylene
45.5
20
ug/L
50.00
91
41-130
Aniline
45.0
20
ug/L
50.00
90
12-197
Anthracene
50.4
20
ug/L
50.00
101
57-123
Azobenzene
46.2
10
ug/L
50.00
92
61-116
Benzo(a)anthracene
49.8
10
ug/L
50.00
100
58-125
Benzo(a)pyrene
49.1
10
ug/L
50.00
98
54-128
Benzo(b)fluoranthene
48.7
10
ug/L
50.00
97
53-131
Benzo(g,h,i)perylene
50.3
10
ug/L
50.00
101
50-134
Benzo(k)fluoranthene
50.3
10
ug/L
50.00
101
57-129
Benzoic Acid
BRL
100
ug/L
50.00
10-125 L
Benzyl alcohol
36.5
10
ug/L
50.00
73
31-112
bis(2-Chloroethoxy)methane
38.3
10
ug/L
50.00
77
48-120
Bis(2-Chloroethyl)ether
38.0
10
ug/L
50.00
76
43-118
Bis(2-chloroisopropyl)ether
38.4
10
ug/L
50.00
77
37-130
Bis(2-Ethylhexyl)phthalate
52.1
10
ug/L
50.00
104
55-135
Butyl benzyl phthalate
49.7
10
ug/L
50.00
99
53-134
Chrysene
50.1
10
ug/L
50.00
100
59-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO284 - 3510C MS
LCS (P9D0284-BSI)
Prepared: 04/16/19 Analyzed: 04/17/19
Dibenzo(a,h)anthracene
34.9
10
ug/L
50.00
70
51-134
Dibenzofuran
44.8
20
ug/L
50.00
90
53-118
Diethyl phthalate
49.5
20
ug/L
50.00
99
56-125
Dimethyl phthalate
47.0
20
ug/L
50.00
94
45-127
Di-n-butyl phthalate
49.6
20
ug/L
50.00
99
59-127
Di-n-octyl phthalate
50.2
10
ug/L
50.00
100
51-140
Fluoranthene
49.2
20
ug/L
50.00
98
57-128
Fluorene
48.7
20
ug/L
50.00
97
52-124
Hexachlorobenzene
45.4
20
ug/L
50.00
91
53-125
Hexachlorobutadiene
27.8
10
ug/L
50.00
56
22-124
Hexachlorocyclopentadiene
33.9
10
ug/L
50.00
68
32-117
Hexachloroethane
24.0
10
ug/L
50.00
48
21-115
Indeno(1,2,3-cd)pyrene
58.0
10
ug/L
50.00
116
52-134
Isophorone
38.3
10
ug/L
50.00
77
42-124
Naphthalene
34.2
10
ug/L
50.00
68
40-121
Nitrobenzene
35.5
10
ug/L
50.00
71
45-121
N-Nitroso-di-n-propylamine
41.1
20
ug/L
50.00
82
49-119
N-Nitrosodiphenylamine
51.3
20
ug/L
50.00
103
51-123
Pentachlorophenol
48.4
10
ug/L
50.00
97
35-138
Phenanthrene
49.2
20
ug/L
50.00
98
59-120
Phenol
17.5
10
ug/L
50.00
35
12-58
Pyrene
51.6
10
ug/L
50.00
103
57-126
Surrogate: 2,4,6-Tribromophenol
97.3
ug/L
100.0
97
43-140
Surrogate:2-Fluorobiphenyl
42.9
ug/L
50.00
86
44-119
Surrogate:2-Fluorophenol
49.0
ug/L
100.0
49
19-119
Surrogate: Nitrobenzene-d5
35.3
ug/L
50.00
71
44-120
Surrogate: Phenol-d5
32.5
ug/L
100.0
33
11-52
Surrogate: Terphenyl-d14
49.0
ug/L
50.00
98
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO284 - 3510C MS
LCS Dup (P9DO284-BSD1)
Prepared: 04/16/19 Analyzed: 04/17/19
1,2,4-Trichlorobenzene
30.8
10
ug/L
50.00
62
29-126
0.7
20
1,2-Dichlorobenzene
30.1
10
ug/L
50.00
60
32-111
4
20
1,3-Dichlorobenzene
27.4
10
ug/L
50.00
55
28-110
3
20
1,4-Dichlorobenzene
28.9
10
ug/L
50.00
58
29-112
4
20
1-Methyl naphthalene
38.7
10
ug/L
50.00
77
41-119
4
20
2,4,5-Trichlorophenol
33.8
20
ug/L
50.00
68
53-123
28
20
D
2,4,6-Trichlorophenol
26.2
20
ug/L
50.00
52
50-125
54
20
D
2,4-Dichlorophenol
36.4
10
ug/L
50.00
73
47-121
5
20
2,4-Dimethylphenol
51.4
10
ug/L
50.00
103
31-124
11
20
2,4-Dinitrophenol
BRL
50
ug/L
50.00
23-143
20
L
2,4-Dinitrotoluene
49.4
10
ug/L
50.00
99
57-128
3
20
2,6-Dinitrotoluene
49.9
20
ug/L
50.00
100
57-124
8
20
2-Chloronaphthalene
45.3
20
ug/L
50.00
91
40-116
5
20
2-Chlorophenol
42.4
10
ug/L
50.00
85
38-117
10
20
2-Methyl naphthalene
37.1
10
ug/L
50.00
74
40-121
3
20
2-Methylphenol
42.1
10
ug/L
50.00
84
30-117
12
20
2-Nitroaniline
48.6
10
ug/L
50.00
97
55-127
6
20
2-Nitrophenol
31.1
10
ug/L
50.00
62
47-123
15
20
3,3'-Dichlorobenzidine
55.4
10
ug/L
50.00
111
27-129
18
20
3/4-Methyl phenol
35.1
10
ug/L
50.00
70
29-110
12
20
3-Nitroaniline
50.1
10
ug/L
50.00
100
41-128
6
20
4,6-Dinitro-2-methylphenol
BRL
50
ug/L
50.00
44-137
20
L
4-Bromophenyl phenyl ether
49.1
20
ug/L
50.00
98
55-124
5
20
4-Chloro-3-methylphenol
41.7
10
ug/L
50.00
83
52-119
5
20
4-Chloroaniline
43.8
10
ug/L
50.00
88
33-117
9
20
4-Chlorophenyl phenyl ether
49.6
20
ug/L
50.00
99
53-121
6
20
4-Nitroaniline
48.2
10
ug/L
50.00
96
45-135
1
20
4-Nitrophenol
4.09
10
ug/L
50.00
8
10-77
131
20
D, L2, J
Acenaphthene
49.6
20
ug/L
50.00
99
47-122
6
20
Acenaphthylene
47.9
20
ug/L
50.00
96
41-130
5
20
Aniline
52.5
20
ug/L
50.00
105
12-197
15
20
Anthracene
53.1
20
ug/L
50.00
106
57-123
5
20
Azobenzene
49.1
10
ug/L
50.00
98
61-116
6
20
Benzo(a)anthracene
50.7
10
ug/L
50.00
101
58-125
2
20
Benzo(a)pyrene
49.4
10
ug/L
50.00
99
54-128
0.6
20
Benzo(b)fluoranthene
49.1
10
ug/L
50.00
98
53-131
0.9
20
Benzo(g,h,i)perylene
50.7
10
ug/L
50.00
101
50-134
0.8
20
Benzo(k)fluoranthene
51.5
10
ug/L
50.00
103
57-129
2
20
Benzoic Acid
BRL
100
ug/L
50.00
10-125
20
L
Benzyl alcohol
41.4
10
ug/L
50.00
83
31-112
13
20
bis(2-Chloroethoxy)methane
42.2
10
ug/L
50.00
84
48-120
10
20
Bis(2-Chloroethyl)ether
43.3
10
ug/L
50.00
87
43-118
13
20
Bis(2-chloroisopropyl)ether
43.0
10
ug/L
50.00
86
37-130
11
20
Bis(2-Ethylhexyl)phthalate
52.5
10
ug/L
50.00
105
55-135
0.8
20
Butyl benzyl phthalate
51.0
10
ug/L
50.00
102
53-134
3
20
Chrysene
51.6
10
ug/L
50.00
103
59-123
3
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO284 - 3510C MS
LCS Dup (P9D0284-BSD1)
Prepared: 04/16/19 Analyzed: 04/17/19
Dibenzo(a,h)anthracene
35.9
10
ug/L
50.00
72
51-134
3
20
Dibenzofuran
47.8
20
ug/L
50.00
96
53-118
6
20
Diethyl phthalate
51.2
20
ug/L
50.00
102
56-125
3
20
Dimethyl phthalate
50.2
20
ug/L
50.00
100
45-127
6
20
Di-n-butyl phthalate
51.8
20
ug/L
50.00
104
59-127
4
20
Di-n-octyl phthalate
50.5
10
ug/L
50.00
101
51-140
0.6
20
Fluoranthene
51.8
20
ug/L
50.00
104
57-128
5
20
Fluorene
51.7
20
ug/L
50.00
103
52-124
6
20
Hexachlorobenzene
46.7
20
ug/L
50.00
93
53-125
3
20
Hexachlorobutadiene
26.4
10
ug/L
50.00
53
22-124
5
20
Hexachlorocyclopentadiene
33.1
10
ug/L
50.00
66
32-117
3
20
Hexachloroethane
24.2
10
ug/L
50.00
48
21-115
1
20
Indeno(1,2,3-cd)pyrene
58.4
10
ug/L
50.00
117
52-134
0.6
20
Isophorone
40.6
10
ug/L
50.00
81
42-124
6
20
Naphthalene
35.9
10
ug/L
50.00
72
40-121
5
20
Nitrobenzene
39.8
10
ug/L
50.00
80
45-121
11
20
N-Nitroso-di-n-propylamine
44.4
20
ug/L
50.00
89
49-119
8
20
N-Nitrosodiphenylamine
58.9
20
ug/L
50.00
118
51-123
14
20
Pentachlorophenol
20.1
10
ug/L
50.00
40
35-138
83
20 D
Phenanthrene
51.9
20
ug/L
50.00
104
59-120
5
20
Phenol
20.1
10
ug/L
50.00
40
12-58
14
20
Pyrene
51.1
10
ug/L
50.00
102
57-126
0.9
20
Surrogate: 2,4,6-Tribromophenol
62.9
ug/L
100.0
63
43-140
Surrogate:2-Fluorobiphenyl
46.0
ug/L
50.00
92
44-119
Surrogate:2-Fluorophenol
51.0
ug/L
100.0
51
19-119
Surrogate: Nitrobenzene-d5
39.0
ug/L
50.00
78
44-120
Surrogate: Phenol-d5
37.8
ug/L
100.0
38
11-52
Surrogate: Terphenyl-d14
49.8
ug/L
50.00
100
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO300 - 3546
Blank (P9D0300-BLK1)
Prepared & Analyzed: 04/17/19
1,2,4-Trichlorobenzene
BRL
0.33
mg/kg wet
1,2-Dichlorobenzene
BRL
0.33
mg/kg wet
1,3-Dichlorobenzene
BRL
0.33
mg/kg wet
1,4-Dichlorobenzene
BRL
0.33
mg/kg wet
1-Methyl naphthalene
BRL
0.33
mg/kg wet
2,4,5-Trichlorophenol
BRL
0.33
mg/kg wet
2,4,6-Trichlorophenol
BRL
0.33
mg/kg wet
2,4-Dichlorophenol
BRL
0.33
mg/kg wet
2,4-Dimethylphenol
BRL
0.33
mg/kg wet
2,4-Dinitrophenol
BRL
0.33
mg/kg wet
2,4-Dinitrotoluene
BRL
0.33
mg/kg wet
2,6-Dinitrotoluene
BRL
0.33
mg/kg wet
2-Chloronaphthalene
BRL
0.33
mg/kg wet
2-Chlorophenol
BRL
0.33
mg/kg wet
2-Methyl naphthalene
BRL
0.33
mg/kg wet
2-Methylphenol
BRL
0.33
mg/kg wet
2-Nitrophenol
BRL
0.33
mg/kg wet
3,3'-Dichlorobenzidine
BRL
0.33
mg/kg wet
3/4-Methyl phenol
BRL
0.33
mg/kg wet
4,6-Dinitro-2-methylphenol
BRL
0.33
mg/kg wet
4-Bromophenyl phenyl ether
BRL
0.33
mg/kg wet
4-Chloro-3-methylphenol
BRL
0.33
mg/kg wet
4-Chloroaniline
BRL
0.33
mg/kg wet
4-Chlorophenyl phenyl ether
BRL
0.33
mg/kg wet
4-Nitrophenol
BRL
0.33
mg/kg wet
Acenaphthene
BRL
0.33
mg/kg wet
Acenaphthylene
BRL
0.33
mg/kg wet
Anthracene
BRL
0.33
mg/kg wet
Azobenzene
BRL
0.33
mg/kg wet
Benzo(a)anthracene
BRL
0.33
mg/kg wet
Benzo(a)pyrene
BRL
0.33
mg/kg wet
Benzo(b)fluoranthene
BRL
0.33
mg/kg wet
Benzo(g,h,i)perylene
BRL
0.33
mg/kg wet
Benzo(k)fluoranthene
BRL
0.33
mg/kg wet
Benzoic Acid
BRL
0.33
mg/kg wet
Benzyl alcohol
BRL
0.33
mg/kg wet
bis(2-Chloroethoxy)methane
BRL
0.33
mg/kg wet
Bis(2-Chloroethyl)ether
BRL
0.33
mg/kg wet
Bis(2-chloroisopropyl)ether
BRL
0.33
mg/kg wet
Bis(2-Ethylhexyl)phthalate
BRL
0.33
mg/kg wet
Butyl benzyl phthalate
BRL
0.33
mg/kg wet
Chrysene
BRL
0.33
mg/kg wet
Dibenzo(a,h)anthracene
BRL
0.33
mg/kg wet
Dibenzofuran
BRL
0.33
mg/kg wet
Diethyl phthalate
BRL
0.33
mg/kg wet
Dimethyl phthalate
BRL
0.33
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO300 - 3546
Blank (P9D0300-BLK1)
Prepared & Analyzed: 04/17/19
Di-n-butyl phthalate
BRL
0.33
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.33
mg/kg wet
Fluorene
BRL
0.33
mg/kg wet
Hexachlorobenzene
BRL
0.33
mg/kg wet
Hexachlorobutadiene
BRL
0.33
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.33
mg/kg wet
Hexachloroethane
BRL
0.33
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.33
mg/kg wet
Isophorone
BRL
0.33
mg/kg wet
Naphthalene
BRL
0.33
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.33
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.33
mg/kg wet
Pentachlorophenol
BRL
0.33
mg/kg wet
Phenanthrene
BRL
0.33
mg/kg wet
Phenol
BRL
0.33
mg/kg wet
Pyrene
BRL
0.33
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
3.56
mg/kg wet
3.333
107
39-132
Surrogate: 2-Fluorobiphenyl
1.80
mg/kg wet
1.667
108
44-115
Surrogate: 2-Fluorophenol
3.57
mg/kg wet
3.333
107
35-115
Surrogate: Nitrobenzene-d5
1.62
mg/kg wet
1.667
97
37-122
Surrogate: Phenol-d5
3.43
mg/kg wet
3.333
103
34-121
Surrogate: Terphenyl-d14
1.87
mg/kg wet
1.667
112
54-127
LCS (P9D0300-BSI)
Prepared & Analyzed: 04/17/19
1,2,4-Trichlorobenzene
1.29
0.33
mg/kg wet
1.667
77
34-118
1,2-Dichlorobenzene
1.34
0.33
mg/kg wet
1.667
80
33-117
1,3-Dichlorobenzene
1.29
0.33
mg/kg wet
1.667
77
30-115
1,4-Dichlorobenzene
1.30
0.33
mg/kg wet
1.667
78
31-115
1-Methyl naphthalene
1.38
0.33
mg/kg wet
1.667
83
40-119
2,4,5-Trichlorophenol
1.59
0.33
mg/kg wet
1.667
96
62-124
2,4,6-Trichlorophenol
1.64
0.33
mg/kg wet
1.667
98
39-126
2,4-Dichlorophenol
1.40
0.33
mg/kg wet
1.667
84
40-122
2,4-Dimethylphenol
1.73
0.33
mg/kg wet
1.667
104
30-127
2,4-Dinitrophenol
1.09
0.33
mg/kg wet
1.667
66
27-129
2,4-Dinitrotoluene
1.65
0.33
mg/kg wet
1.667
99
48-126
2,6-Dinitrotoluene
1.68
0.33
mg/kg wet
1.667
101
46-124
2-Chloronaphthalene
1.61
0.33
mg/kg wet
1.667
96
41-114
2-Chlorophenol
1.57
0.33
mg/kg wet
1.667
94
34-121
2-Methyl naphthalene
1.34
0.33
mg/kg wet
1.667
80
38-122
2-Methylphenol
1.62
0.33
mg/kg wet
1.667
97
32-122
2-Nitrophenol
1.30
0.33
mg/kg wet
1.667
78
36-123
3,3'-Dichlorobenzidine
1.67
0.33
mg/kg wet
1.667
100
22-121
3/4-Methyl phenol
1.45
0.33
mg/kg wet
1.667
87
34-119
4,6-Dinitro-2-methylphenol
1.39
0.33
mg/kg wet
1.667
83
29-132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9DO300 - 3546
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS (P9D0300-BSI)
Prepared & Analyzed: 04/17/19
4-Bromophenyl phenyl ether
1.59
0.33
mg/kg wet
1.667
95
46-124
4-Chloro-3-methylphenol
1.43
0.33
mg/kg wet
1.667
86
45-122
4-Chloroaniline
1.33
0.33
mg/kg wet
1.667
80
17-106
4-Chlorophenyl phenyl ether
1.65
0.33
mg/kg wet
1.667
99
45-121
4-Nitrophenol
1.71
0.33
mg/kg wet
1.667
102
30-132
Acenaphthene
1.67
0.33
mg/kg wet
1.667
100
40-123
Acenaphthylene
1.62
0.33
mg/kg wet
1.667
97
32-132
Anthracene
1.74
0.33
mg/kg wet
1.667
104
47-123
Azobenzene
1.62
0.33
mg/kg wet
1.667
97
39-125
Benzo(a)anthracene
1.67
0.33
mg/kg wet
1.667
100
49-126
Benzo(a)pyrene
1.62
0.33
mg/kg wet
1.667
97
45-129
Benzo(b)fluoranthene
1.62
0.33
mg/kg wet
1.667
97
45-132
Benzo(g,h,i)perylene
1.69
0.33
mg/kg wet
1.667
101
43-134
Benzo(k)fluoranthene
1.70
0.33
mg/kg wet
1.667
102
47-132
Benzoic Acid
0.611
0.33
mg/kg wet
1.667
37
10-83
Benzyl alcohol
1.50
0.33
mg/kg wet
1.667
90
29-122
bis(2-Chloroethoxy)methane
1.35
0.33
mg/kg wet
1.667
81
36-121
Bis(2-Chloroethyl)ether
1.28
0.33
mg/kg wet
1.667
77
31-120
Bis(2-chloroisopropyl)ether
1.42
0.33
mg/kg wet
1.667
85
33-131
Bis(2-Ethylhexyl)phthalate
1.70
0.33
mg/kg wet
1.667
102
51-133
Butyl benzyl phthalate
1.67
0.33
mg/kg wet
1.667
100
48-132
Chrysene
1.67
0.33
mg/kg wet
1.667
100
50-124
Dibenzo(a,h)anthracene
1.19
0.33
mg/kg wet
1.667
72
45-134
Dibenzofuran
1.60
0.33
mg/kg wet
1.667
96
44-120
Diethyl phthalate
1.68
0.33
mg/kg wet
1.667
101
50-124
Dimethyl phthalate
1.63
0.33
mg/kg wet
1.667
98
48-124
Di-n-butyl phthalate
1.67
0.33
mg/kg wet
1.667
100
51-128
Di-n-octyl phthalate
1.67
0.33
mg/kg wet
1.667
100
45-140
Fluoranthene
1.69
0.33
mg/kg wet
1.667
102
50-127
Fluorene
1.72
0.33
mg/kg wet
1.667
103
43-125
Hexachlorobenzene
1.55
0.33
mg/kg wet
1.667
93
45-122
Hexachlorobutadiene
1.35
0.33
mg/kg wet
1.667
81
32-123
Hexachlorocyclopentadiene
1.40
0.33
mg/kg wet
1.667
84
32-117
Hexachloroethane
1.29
0.33
mg/kg wet
1.667
77
28-117
Indeno(1,2,3-cd)pyrene
1.90
0.33
mg/kg wet
1.667
114
45-133
Isophorone
1.31
0.33
mg/kg wet
1.667
79
30-122
Naphthalene
1.32
0.33
mg/kg wet
1.667
79
35-123
Nitrobenzene
1.27
0.33
mg/kg wet
1.667
76
34-122
N-Nitroso-di-n-propylamine
1.44
0.33
mg/kg wet
1.667
87
36-120
N-Nitrosodiphenylamine
1.97
0.33
mg/kg wet
1.667
118
38-127
Pentachlorophenol
1.67
0.33
mg/kg wet
1.667
100
25-133
Phenanthrene
1.68
0.33
mg/kg wet
1.667
101
50-121
Phenol
1.55
0.33
mg/kg wet
1.667
93
34-121
Pyrene
1.70
0.33
mg/kg wet
1.667
102
47-127
Pyridine
0.951
0.33
mg/kg wet
1.667
57
10-60
Surrogate: 2,4,6-Tribromophenol
3.46
mg/kg wet
3.333
104
39-132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Project: 3612 & 3624 Davis Drive
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9DO300 - 3546
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS (P9D0300-BS1)
Prepared & Analyzed: 04/17/19
Surrogate: 2-Fluorobiphenyl
1.62
mg/kg wet
1.667
97
44-115
Surrogate: 2-Fluorophenol
3.19
mg/kg wet
3.333
96
35-115
Surrogate: Nitrobenzene-d5
1.29
mg/kg wet
1.667
78
37-122
Surrogate: Phenol-d5
3.07
mg/kg wet
3,333
92
34-121
Surrogate: Terphenyl-d14
1.72
mg/kg wet
1.667
103
54-127
LCS Dup (P9DO300-BSD1)
Prepared & Analyzed: 04/17/19
1,2,4-Trichlorobenzene
1.24
0.33
mg/kg wet
1.667
74
34-118
4
20
1,2-Dichlorobenzene
1.28
0.33
mg/kg wet
1.667
77
33-117
4
20
1,3-Dichlorobenzene
1.25
0.33
mg/kg wet
1.667
75
30-115
3
20
1,4-Dichlorobenzene
1.29
0.33
mg/kg wet
1.667
77
31-115
1
20
1-Methyl naphthalene
1.34
0.33
mg/kg wet
1.667
81
40-119
3
20
2,4,5-Trichlorophenol
1.54
0.33
mg/kg wet
1.667
92
62-124
3
20
2,4,6-Trichlorophenol
1.60
0.33
mg/kg wet
1.667
96
39-126
2
20
2,4-Dichlorophenol
1.36
0.33
mg/kg wet
1.667
82
40-122
3
20
2,4-Dimethylphenol
1.67
0.33
mg/kg wet
1.667
100
30-127
3
20
2,4-Dinitrophenol
0.987
0.33
mg/kg wet
1.667
59
27-129
10
20
2,4-Dinitrotoluene
1.65
0.33
mg/kg wet
1.667
99
48-126
0.02
20
2,6-Dinitrotoluene
1.64
0.33
mg/kg wet
1.667
98
46-124
3
20
2-Chloronaphthalene
1.54
0.33
mg/kg wet
1.667
92
41-114
4
20
2-Chlorophenol
1.50
0.33
mg/kg wet
1.667
90
34-121
4
20
2-Methyl naphthalene
1.30
0.33
mg/kg wet
1.667
78
38-122
3
20
2-Methylphenol
1.57
0.33
mg/kg wet
1.667
94
32-122
3
20
2-Nitrophenol
1.29
0.33
mg/kg wet
1.667
78
36-123
0.3
20
3,3'-Dichlorobenzidine
1.66
0.33
mg/kg wet
1.667
99
22-121
0.6
20
3/4-Methyl phenol
1.42
0.33
mg/kg wet
1.667
85
34-119
2
20
4,6-Dinitro-2-methylphenol
1.30
0.33
mg/kg wet
1.667
78
29-132
7
20
4-Bromophenyl phenyl ether
1.59
0.33
mg/kg wet
1.667
95
46-124
0.2
20
4-Chloro-3-methylphenol
1.42
0.33
mg/kg wet
1.667
85
45-122
0.8
20
4-Chloroaniline
1.32
0.33
mg/kg wet
1.667
79
17-106
0.4
20
4-Chlorophenyl phenyl ether
1.67
0.33
mg/kg wet
1.667
100
45-121
1
20
4-Nitrophenol
1.67
0.33
mg/kg wet
1.667
100
30-132
2
20
Acenaphthene
1.62
0.33
mg/kg wet
1.667
97
40-123
3
20
Acenaphthylene
1.57
0.33
mg/kg wet
1.667
94
32-132
3
20
Anthracene
1.74
0.33
mg/kg wet
1.667
104
47-123
0.3
20
Azobenzene
1.60
0.33
mg/kg wet
1.667
96
39-125
1
20
Benzo(a)anthracene
1.69
0.33
mg/kg wet
1.667
102
49-126
1
20
Benzo(a)pyrene
1.65
0.33
mg/kg wet
1.667
99
45-129
2
20
Benzo(b)fluoranthene
1.66
0.33
mg/kg wet
1.667
99
45-132
2
20
Benzo(g,h,i)perylene
1.70
0.33
mg/kg wet
1.667
102
43-134
0.8
20
Benzo(k)fluoranthene
1.70
0.33
mg/kg wet
1.667
102
47-132
0.06
20
Benzoic Acid
0.591
0.33
mg/kg wet
1.667
35
10-83
3
20
Benzyl alcohol
1.45
0.33
mg/kg wet
1.667
87
29-122
3
20
bis(2-Chloroethoxy)methane
1.34
0.33
mg/kg wet
1.667
81
36-121
0.7
20
Bis(2-Chloroethyl)ether
1.29
0.33
mg/kg wet
1.667
77
31-120
0.9
20
Bis(2-chloroisopropyl)ether
1.37
0.33
mg/kg wet
1.667
82
33-131
4
20
Bis(2-Ethylhexyl)phthalate
1.76
0.33
mg/kg wet
1.667
106
51-133
3
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9DO300 - 3546
LCS Dup (P9D0300-BSD1)
Prepared & Analyzed: 04/17/19
Butyl benzyl phthalate
1.68
0.33
mg/kg wet
1.667
101
48-132
1
20
Chrysene
1.71
0.33
mg/kg wet
1.667
102
50-124
2
20
Dibenzo(a,h)anthracene
1.23
0.33
mg/kg wet
1.667
74
45-134
3
20
Dibenzofuran
1.57
0.33
mg/kg wet
1.667
94
44-120
2
20
Diethyl phthalate
1.67
0.33
mg/kg wet
1.667
100
50-124
0.1
20
Dimethyl phthalate
1.63
0.33
mg/kg wet
1.667
98
48-124
0.02
20
Di-n-butyl phthalate
1.68
0.33
mg/kg wet
1.667
101
51-128
0.7
20
Di-n-octyl phthalate
1.72
0.33
mg/kg wet
1.667
103
45-140
3
20
Fluoranthene
1.71
0.33
mg/kg wet
1.667
103
50-127
1
20
Fluorene
1.69
0.33
mg/kg wet
1.667
101
43-125
2
20
Hexachlorobenzene
1.52
0.33
mg/kg wet
1.667
91
45-122
2
20
Hexachlorobutadiene
1.31
0.33
mg/kg wet
1.667
79
32-123
3
20
Hexachlorocyclopentadiene
1.32
0.33
mg/kg wet
1.667
79
32-117
6
20
Hexachloroethane
1.23
0.33
mg/kg wet
1.667
74
28-117
5
20
Indeno(1,2,3-cd)pyrene
1.93
0.33
mg/kg wet
1.667
116
45-133
1
20
Isophorone
1.31
0.33
mg/kg wet
1.667
78
30-122
0.6
20
Naphthalene
1.28
0.33
mg/kg wet
1.667
76
35-123
3
20
Nitrobenzene
1.23
0.33
mg/kg wet
1.667
74
34-122
3
20
N-Nitroso-di-n-propylamine
1.40
0.33
mg/kg wet
1.667
84
36-120
3
20
N-Nitrosodiphenylamine
1.94
0.33
mg/kg wet
1.667
116
38-127
1
20
Pentachlorophenol
1.63
0.33
mg/kg wet
1.667
98
25-133
3
20
Phenanthrene
1.71
0.33
mg/kg wet
1.667
102
50-121
1
20
Phenol
1.48
0.33
mg/kg wet
1.667
89
34-121
4
20
Pyrene
1.72
0.33
mg/kg wet
1.667
103
47-127
1
20
Pyridine
0.887
0.33
mg/kg wet
1.667
53
10-60
7
20
Surrogate: 2,4,6-Tribromophenol
3.33
mg/kg wet
3.333
100
39-132
Surrogate: 2-Fluorobiphenyl
1.54
mg/kg wet
1.667
92
44-115
Surrogate: 2-Fluorophenol
2.98
mg/kg wet
3.333
89
35-115
Surrogate: Nitrobenzene-d5
1.24
mg/kg wet
1.667
74
37-122
Surrogate: Phenol-d5
2.90
mg/kg wet
3.333
87
34-121
Surrogate: Terphenyl-d14
1.69
mg/kg wet
1.667
101
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Total Metals - Quality Control
Analyte
Batch P9DO290 - 7470A
Project: 3612 & 3624 Davis Drive
Level II QC Report
4/22/19
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9D0290-BLK1) Prepared & Analyzed: 04/17/19
Mercury BRL 0.00050 mg/L
LCS (P9D0290-BS1) Prepared & Analyzed: 04/17/19
Mercury 0.0101 0.00050 mg/L 0.009375 108 80-120
Batch P9D0292 - 3010A
Blank (P9D0292-BLK1)
Prepared: 04/17/19 Analyzed: 04/18/19
Arsenic
BRL
0.020
mg/L
Barium
BRL
0.010
mg/L
Cadmium
BRL
0.0020
mg/L
Chromium
BRL
0.010
mg/L
Lead
BRL
0.0050
mg/L
Selenium
BRL
0.030
mg/L
Silver
BRL
0.0050
mg/L
LCS (P9D0292-BSI)
Prepared: 04/17/19 Analyzed: 04/18/19
Arsenic
0.512
0.020
mg/L
0.5001 102 80-120
Barium
0.514
0.010
mg/L
0.5000 103 80-120
Cadmium
0.502
0.0020
mg/L
0.5000 100 80-120
Chromium
0.521
0.010
mg/L
0.5001 104 80-120
Lead
0.509
0.0050
mg/L
0.5001 102 80-120
Selenium
0.509
0.030
mg/L
0.4999 102 80-120
Silver
0.198
0.0050
mg/L
0.2000 99 80-120
Batch P9DO297 - 3050B
Blank (P9D0297-BLK1)
Prepared: 04/17/19 Analyzed: 04/18/19
Arsenic
BRL
1.0
mg/kg wet
Barium
BRL
10
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Chromium
BRL
1.0
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Silver
BRL
0.50
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive Prism Work Order: 9040256
Attn: Dan Nielsen Time Submitted: 4/16/2019 9:45:OOAM
409 Rogers View Court
Raleigh, NC 27610
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9D0297 - 3050B
LCS (P9D0297-BS1)
Prepared: 04/17/19 Analyzed: 04/18/19
Arsenic
12.4
1.0
mg/kg wet
12.50
99
80-120
Barium
12.2
10
mg/kg wet
12.50
98
80-120
Cadmium
12.1
0.50
mg/kg wet
12.50
97
80-120
Chromium
12.9
1.0
mg/kg wet
12.50
103
80-120
Lead
12.3
1.0
mg/kg wet
12.50
99
80-120
Selenium
12.2
1.0
mg/kg wet
12.50
97
80-120
Silver
4.78
0.50
mg/kg wet
5.000
96
80-120
Matrix Spike (P9D0297-MS1)
Source: 9040256-01
Prepared:
04/17/19 Analyzed: 04/18/19
Arsenic
15.1
1.3
mg/kg dry
15.89
0.819
90
75-125
Barium
33.0
13
mg/kg dry
15.89
15.5
110
75-125
Cadmium
14.4
0.64
mg/kg dry
15.89
BRL
91
75-125
Chromium
21.0
1.3
mg/kg dry
15.89
4.46
104
75-125
Lead
21.9
1.3
mg/kg dry
15.89
8.02
88
75-125
Selenium
14.4
1.3
mg/kg dry
15.88
BRL
91
75-125
Silver
5.92
0.64
mg/kg dry
6.354
BRL
93
75-125
Matrix Spike Dup (11129D0297-111,111SD1)
Source: 9040256-01
Prepared:
04/17/19 Analyzed: 04/18/19
Arsenic
15.7
1.3
mg/kg dry
15.89
0.819
94
75-125
4
20
Barium
34.1
13
mg/kg dry
15.89
15.5
118
75-125
3
20
Cadmium
15.0
0.64
mg/kg dry
15.89
BRL
95
75-125
4
20
Chromium
22.5
1.3
mg/kg dry
15.89
4.46
114
75-125
7
20
Lead
23.0
1.3
mg/kg dry
15.89
8.02
94
75-125
5
20
Selenium
14.9
1.3
mg/kg dry
15.88
BRL
94
75-125
3
20
Silver
6.24
0.64
mg/kg dry
6.354
BRL
98
75-125
5
20
Post Spike (P9D0297-PSI)
Source: 9040256-01
Prepared:
04/17/19 Analyzed: 04/18/19
Arsenic
0.508
mg/L
0.5001
0.0258
96
75-125
Barium
0.970
mg/L
0.5000
0.486
97
75-125
Cadmium
0.466
mg/L
0.5000
-0.000417
93
75-125
Chromium
0.626
mg/L
0.5001
0.140
97
75-125
Lead
0.699
mg/L
0.5001
0.252
89
75-125
Selenium
0.469
mg/L
0.4999
-0.00372
94
75-125
Silver
0.188
mg/L
0.2000
-0.00433
94
75-125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
Total Metals - Quality Control
Analyte
Batch P9D0323 - 7471B
Project: 3612 & 3624 Davis Drive
Level II QC Report
4/22/19
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9D0323-BLK1) Prepared & Analyzed: 04/18/19
Mercury BRL 0.050 mg/kg wet
LCS (P9D0323-BS1) Prepared & Analyzed: 04/18/19
Mercury 0.427 0.050 mg/kg wet 0.4167 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
4/22/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3612 & 3624 Davis Drive
Attn: Dan Nielsen
409 Rogers View Court
Raleigh, NC 27610
General Chemistry Parameters - Quality Control
Prism Work Order: 9040256
Time Submitted: 4/16/2019 9:45:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9D0322 - Solids, Dry Weight
Duplicate (P9D0322-DUP1) Source: 9040256-03 Prepared & Analyzed: 04/18/19
% Solids 83.2 0.100 % by Weight 85.2 2 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
9040256-01
P91D0322
30
g
30 g
04/18/19 8:33
9040256-02
P91D0322
30
g
30 g
04/18/19 8:33
9040256-03
P91D0322
30
g
30 g
04/18/19 8:33
9040256-04
P91D0322
30
g
30 g
04/18/19 8:33
9040256-05
P91D0322
30
g
30 g
04/18/19 8:33
9040256-06
P91D0322
30
g
30 g
04/18/19 8:33
9040256-07
P91D0322
30
g
30 g
04/18/19 8:33
9040256-08
P91D0331
30
g
30 g
04/18/19 9:56
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
Date/Time
9040256-09
P91D0284
960
mL
1 mL
04/17/19 9:53
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
9040256-01
P91D0300
30.06
g
1 mL
04/17/19 10:35
9040256-02
P91D0300
30.1
g
1 mL
04/17/19 10:35
9040256-03
P91D0300
30.06
g
1 mL
04/17/19 10:35
9040256-04
P91D0300
30.01
g
1 mL
04/17/19 10:35
9040256-05
P91D0300
30.15
g
1 mL
04/17/19 10:35
9040256-06
P91D0300
30.04
g
1 mL
04/17/19 10:35
Prep Method: 3010A
Lab Number
Batch
Initial
Final
DatelTime
9040256-09
P91D0292
50
mL
50 mL
04/17/19 7:20
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
9040256-01
P91D0297
2
g
50 mL
04/17/19 8:50
9040256-02
P91D0297
2
g
50 mL
04/17/19 8:50
9040256-03
P91D0297
2
g
50 mL
04/17/19 8:50
9040256-04
P91D0297
2
g
50 mL
04/17/19 8:50
9040256-05
P91D0297
2
g
50 mL
04/17/19 8:50
9040256-06
P9D0297
2
g
50 mL
04/17/19 8:50
9040256-07
P91D0297
2
g
50 mL
04/17/19 8:50
9040256-07
P91D0297
2
g
50 mL
04/17/19 8:50
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
9040256-09
P91D0290
20
mL
30 mL
04/17/19 8:40
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Date/Time
9040256-01
P91D0323
0.6
g
50 mL
04/18/19 9:00
9040256-02
P91D0323
0.6
g
50 mL
04/18/19 9:00
9040256-03
P91D0323
0.6
g
50 mL
04/18/19 9:00
9040256-04
P91D0323
0.6
g
50 mL
04/18/19 9:00
9040256-05
P91D0323
0.6
g
50 mL
04/18/19 9:00
9040256-06
P91D0323
0.6
g
50 mL
04/18/19 9:00
9040256-07
P91D0323
0.6
g
50 mL
04/18/19 9:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: 5030E
Lab Number Batch Initial Final Date/Time
9040256-09 P91D0320 10 mL 10 mL 04/17/19 16:12
9040256-10 P91D0320 10 mL 10 mL 04/17/19 16:12
Prep Method: 5035
Lab Number Batch Initial Final Date/Time
9040256-01
P91D0298
4.49
g 5 mL
04/16/19
9:37
9040256-02
P91D0298
5.39
g 5 mL
04/16/19
9:37
9040256-03
P91D0298
6.23
g 5 mL
04/16/19
9:37
9040256-04
P91D0298
6.07
g 5 mL
04/16/19
9:37
9040256-05
P91D0298
6.46
g 5 mL
04/16/19
9:37
9040256-06
P91D0298
5.34
g 5 mL
04/16/19
9:37
9040256-08
P91D0298
6.26
g 5 mL
04/16/19
9:37
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

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