22002_Overture Cary_SoilRemRpt_20200428

a�
Mid Atlantic
Engineering & Environmental Solutions
April 28, 2020
Ms. Kathleen Markey
North Carolina Department of Environmental Quality
Division of Waste Management — Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699
Subject: REPORT OF ENVIRONMENTAL SERVICES
SOIL EXCAVATION AND DISPOSAL
3612 & 3624 DAVIS DRIVE
MORRISVILLE & CARY, NORTH CAROLINA
MID -ATLANTIC JOB NO. 00OR3021.01
Dear Ms. Markey:
409 Rogers View Court
Raleigh, NC 2 76 10
office 919.250.9918
facsimile 919.250.9950
MAAONLiNE.COM
On behalf of Greystar GP II, LLC (Greystar), Mid -Atlantic Associates, Inc. (Mid -Atlantic)
submits this report of environmental services for a release from a residential heating oil
aboveground storage tank located at 3612 Davis Drive in Morrisville and Cary, North
Carolina.
This report presents background information; a summary of the contaminated soil
excavation activities; the soil analytical results; and our findings, conclusions and
recommendations. The opinions included herein are based on our experience, the
information obtained during the study. This report is based on limited observations made
on the dates noted using the procedures described herein. If additional information
becomes available, we request the opportunity to review the information, reassess the
potential environmental concerns and modify our conclusions and recommendations, if
appropriate.
BACKGROUND INFORMATION
The subject site is located at 3612 Davis Drive in Morrisville and Cary, North
Carolina (Drawing 1 in Attachment A) and is currently owned by CRP-GREP
Overture Cary Owner, L.L.C. (CRP-GREP). CRP-GREP recently purchased the property,
which had formerly included a residence, and has developed this
EXPERIENCED CUSTOMER FOCUSED INNOVATIVE

Report of Environmental Services April 28, 2020
3612 & 3624 Davis Drive Page 2
Cary, North Carolina
land into multifamily residential apartments. The aboveground storage tank (AST) was
removed approximately 15 years ago according to interview information obtained from a
Phase I Environmental Site Assessment conducted in December 2017. Staining from the
residential heating oil AST was visible on the house (3612 Davis Drive) and levels of Total
Petroleum Hydrocarbons (TPH) in excess of UST action levels were observed in soil were
beneath the tank supports. The approximate location of the former AST is provided in
Attachment A. although the AST had already been removed, soil contamination
was evident, and CRP-GREP contracted Mid -Atlantic to oversee the excavation of
impacted soil and collect post -excavation soil samples. The soil cleanup activities are
documented in this report.
SUMMARY OF SOIL EXCAVATION ACTIVITIES
Excavation Procedures
Gaines and Company provided a trackhoe, two 12-ton dump trucks, and operators to
perform the excavation with oversight from Mid -Atlantic personnel. On July 9, 2019,
representatives of CRP-GREP, Gaines and Company, and Mid -Atlantic mobilized to the
site to perform the excavation of soils in the vicinity of the former AST. Operators from
Gaines and Company used a trackhoe to excavate the soil until Mid -Atlantic was able to
identify the petroleum -impacted soils with a Toxic Vapor Analyzer (TVA) which
provides photoionization and flame ionization detection of vapors from organic
compounds. Contaminated soils were separated, direct -loaded in dump trucks or
loaded onto polyethethylene plastic sheeting, and hauled off site for disposal at Earthtec
of NC, Inc (Earthtec). in Bear Creek, North Carolina. Earthtec's soil disposal
documentation is provided in Attachment C. Excavation activities occurred from July
9, through July 12, 2019.
Soil Sampling Procedures
Mid -Atlantic personnel provided oversight of the excavation activities and screened soils
for analysis using a TVA to record the concentration of of volatilized vapors. Soil was
collected using nitrile gloves directly from the excavation or from the bucket of the
trackhoe, such that the soil collected had not contacted the bucket. Soils were screened as
the excavation proceeded and analyzed by the TVA to qualitatively document soil
contaminant concentrations and monitor the progress of cleanup. Soils were excavated
and analyzed until the results indicated TVA concentrations below 10 ppm (parts per
million) had been achieved. Mid -Atlantic personnel collected ten confirmatory soil samples
from the final extent of the excavation into prepared glassware provided by PRISM
laboratories. The locations of the soil samples collected from the final excavation limits are
shown on Drawing 2 in Attachment A. Sample depths are described in the Sample
flo ® " Atlantic

Report of Environmental Services April 28, 2020
3612 & 3624 Davis Drive Page 3
Cary, North Carolina
Location Table (Table 1) in Attachment B. Evidence of groundwater was not observed in
the excavation.
Backfilling Procedures
Personnel from Gaines and Company backfilled the excavation with surrounding soil.
The final grade level of the surrounding area was below the existing grade, in order to
prevent the hazard of a large hole Gaines and Company backfilled with surrounding
soils.
SOIL SAMPLING RESULTS
The soil sampling results are provided in Prism's report included as Attachment D. As
shown in the results, contaminated soils were removed from the approximate AST
location. Samples did not exhibit Volatile Organic Compounds (VOCs) or Semi -volatile
Organic Compounds (SVOCs) exceeding the Preliminary Soil Remediation Goals
(PSRGs). No SVOCs were detected above Method Detection Limits (MDLs), although
some MDLs of SVOCs exceed the PSRGs. These SVOCs and MDLs are listed in the
Summary of Chemical Constituents Detected in Excavation Samples Table (Table 2).
All samples were tested for the eight RCRA metals. Arsenic was detected above the
Unrestricted Health Based PSRGs in seven of these samples. The arsenic industrial
PSRG was exceeded in five samples. Arsenic is a metal that is found naturally
occurring in North Carolina soils. According to the North Carolina Department of
Agriculture and Consumer Services (NCDA), an average concentration of 4.5 mg/Kg of
arsenic was detected in laboratory testing of 3,286 soil samples collected across North
Carolina between 2005 and 2007 (NCDA, 2008). Furthermore, the EPA notes that
arsenic concentrations typically range from 4 to 9 mg/Kg in most soils (EPA, 2003).
According to the laboratory analysis, the arsenic concentrations detected in the soil
samples collected from the subject site fall within levels believed to be found naturally in
North Carolina soils. Arsenic was also detected with similar concentrations during the
Phase II Analysis background soil testing Mid -Atlantic conducted in April of 2019.
Chromium was detected in each soil sample tested at a concentration below the PSRG
for chromium III but above the PSRG for chromium VI. Chromium III is commonly
naturally occurring while the presence of chromium VI is typically associated with
industrial activities (metal fabrication/cutting, plating, etc.). The subject site has no
history of industrial use and therefore the chromium detected in the soil on the site is
likely chromium III. Sample SS-7, the soil sample with the greatest total chromium
value, was tested for chromium VI using method 7199 and exhibited a value of 0.45 J
mg/kg (J values indicate an estimated value less than the reporting limit and greater
than the method detection limit) This value exceeds the chromium IV unrestricted health
based PSRG of 0.31 mg/kg, but does not exceed the protection of groundwater or
Atlantic

Report of Environmental Services
3612 & 3624 Davis Drive
Cary, North Carolina
April28, 2020
Page 4
industrial PSRGs. Similar levels of chromium IV were detected in background samples
collected during Phase II Analysis conducted in April 2019.
Other RCRA metals were detected at concentrations above laboratory method detection
limits but below the PSRGs.The sampling was conducting in accordance with the
approved work plan as described in the Environmental Management Plan.
CLOSURE
The information provided herein demonstrates that petroleum -impacted soils have been
addressed in accordance with the Brownfield Program approved EMP. If you have any
questions, please call us at [phone].
MI AT ANTIC,ASS,OCIATES, INC.
D niel H _ Nielsen, PE
Principal'Engineer
Attachments:` A.- Drawings
B -' Tales
C — Earthtec Disposal Documentation
D — PRISM Lab Report - Analysis Results
Ruth Tull
Staff Scientist
Pc: Mr. Andy Bell and Chris Hustek, Construction Project Director, Greystar
Mid Atlantic

ATTACHMENT
DRAWINGS
M Mid Atlantic

a
REFERENCES:
1. CARY, NC DIGITAL RASTER GRAPHICS,
USGS. SCANNED FROM1:24,000-SCALE CARY, NC
TOPOGRAPHIC MAPS, PUBLISHED 2013, USGS.
2. INSET MAP DIGITAL DATA FROM 2002 NATIONAL TRANSPORTATION ATLAS
BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, D.C.
3. PROPERTY BOUNDARY DATA FROM WAKE COUNTY GIS.
Mid Atlantic
Engineering & Environmental Solutions
TOPOGRAPHIC SITE MAP
CARY OVERTURE
3624 & 3612 DAVIS DRIVE
CARY & MORRISVILLE,
NORTH CAROLINA
SCALE: 1:12,000
Feet
0 1,000 2,000
DRAWN
DATE:
BY: EBA
FEBRUARY 2019
DRAFT
JOB NO:
CHECK:
OOOR3021.01
ENG.
GIS NO:
CHECK:
1 G-R3021.01-1
APPROVAL:
DWG NO: 1

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LEGEND
SS-1 & 2 SOIL SAMPLE LOCATION
L r -1 J EXTENT OF EXCAVATION
---
NOTE:
SOIL SAMPLE LOCATIONS 1-8 ARE COMPRISED OF A PAIR, TAKEN FROM TWO SAMPLE DEPTHS,
ONE AT 4' DEEP AND ONE AT 10' DEEP
38'
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ATTACHMENT B
TABLES
M Mid Atlantic

TABLE 1
SOIL SAMPLE EXCAVATION LOCATIONS
CARY OVERTURE
3612 DAVIS DRIVE
CARY, NORTH CAROLINA
MID -ATLANTIC JOB NO. R3021.01
Sample ID
Sample Depth
Sample Location
SS-1
10
SW -East
SS-2
4
SW -East
SS-3
10
SW -North
SS-4
4
SW -North
SS-5
4
SW -South
SS-6
10
SW -South
SS-7
8
SW -West
SS-8
4
SW -West
SS-9
12
Bottom
Dup
12
Bottom
SS-10
12
Bottom
Notes:
Bottom = Bottom of excavation
SW= Side Wall

TABLE 2
SUMMARY OF CHEMICAL CONSTITUENTS DETECTED IN EXCAVATION SAMPLES
OVERTURE CARY
CARY AND MORRISVILLE, NORTH CAROLINA
BROWNFIELDS PROJECT NUMBER 22002-18-092
MID -ATLANTIC JOB NO.: R3021.01
CHEMICAL CONSTITUENT
SAMPLE ID
UNRESTRICTED
HEALTH BASED
PSRG (mg/Kg)
PROTECTION OF
GROUNDWATER
PSRG (mg/Kg)
INDUSTRIAL
PSRG (mg/kg)
55-1
55-2
SS-3
55-4
Ss-5
55-6
SS-7
55-8
SS-9
55-10
SS
Duplicate
VOLATILE ORGANIC COMPOUNDS (METHOD 8260 B) Sampled July 12, 2019
Acetone
<0.0015
0.014J
0.015J
<0.0016
0.017J
0.013J
0.016J
0.019J
<0.0015
<0.0017
<0.0015
12000
25
140000
1,2-Dibromoethane (FIDE)<0.00054
<0.00063
<0.00054
<0.00055
<0.00058
<0.00048
<0.00067
<0.00052
<0.00053
<0.00059
<0.00053
0.038
0.00011
0.17
Methylene Chloride
<0.00098
0.0058J
0.0035J
<0.00099
<0.0010
0.0034J
<0.0012
<0.00093
<0.00095
0.00371
<0.00095
58
0.025
650
1,2,4- Trimethylbenzene
<0.00064
<0.00074
<0.00064
<0.00065
<0.00069
<0.00056
<0.00079
<0.00061
<0.00062
0.0031J
0.00291
63
12
370
Vinyl chloride
<0.0012
<0.0014
<0.0011
<0.0012
<0.0013
<0.0011
<0.0015
<0.0011
<0.0011
<0.0013
<0.0011
0.061
0.00021
1.7
m,p-Xylenes
<0.0015
<0.0018
<0.0016
<0.0016
<0.0017
<0.0014
<0.0019
<0.0015
<0.0015
0.0032J
0.00311
120
9.8
Soo
Xylenes total
< 0.0022
< 0.0025
< 0.0022
< 0.0022
< 0.0023
< 0.0019
< 0.0027
< 0.0021
< 0.0021
0.0032 J
0.0031 J
120
9.9
530
Naphthalene
< 0.00061
< 0.00071
< 0.00061
< 0.00062
< 0.00065
< 0.00054
< 0.00075
< 0.00058
< 0.00059
< 0,00066
0.0029 J
4.1
0.39
18
CHEMICAL CONSTITUENT
SAMPLE ID
UNRESTRICTED
HEALTH BASED
PSRG (mg/Kg)
PROTECTION OF
GROUNDWATER
PSRG (mg/Kg)
INDUSTRIAL
PSRG (mg/kg)
SS-1
55-2
SS-3
55-4
SS-5
55-6
SS-7
55-8
SS-9
55-10
Ss
Duplicate I
SEMI -VOLATILE ORGANIC COMPOUNDS (METHOD 8270D) Sampled July 12, 2019
---
No constituents of concern were detected above the laboratory Method Detection Limit (MDL).
---
---
---
Azobenzene
<0.20
<0.21
<0.19
<0.21
<a20
<0.19
<0.23
<0.18
<0.17
<0.21
<a16
5.6
0.049
26
Benzo(a)pyrene
<0.21
<0.22
<0.19
<0.22
<0.21
<0.20
<0.24
<0.19
<0.17
<0.22
<0.17
0.11
0.12
2.1
4-Chloroaniline
<0.11
<0.12
<0.11
<0.12
<0.11
<0.11
<0.13
<0.10
<0.094
<0.12
<0.091
2.7
0.0015
11
Bis(2-chloroethoxy)methane
<0.18
<0.19
<a17
<0.18
<am
<0.17
<a21
<0.16
<0.15
<0.18
<a14
38
0.096
490
Bis(2-chloroethyl)ether
<0.15
<0.16
<0.14
<0.16
<0.15
<0.14
<0.17
<0.14
<0.13
<0.16
<0.12
0.24
0.00016
1.1
2-Chlorophenol
<0.18
<0.19
<0.17
<0.18
<0.18
<0.17
<0.21
<0.16
<0.15
<0.18
<0.14
78
0.0078
1200
Dibenz(a,h)anthracene
<0.27
<0.28
<0.25
<0.28
<0.27
<0.25
<0.31
<0.25
<0.22
<0.28
<0.22
0.11
0.38
2.1
3,3'-Dichlorobenzidine
<0.18
<0.19
<0.17
<0.19
<0.19
<0.18
<0.21
<0.17
<0.15
<0.19
<0.15
1.2
0.01
5.1
2,4-Dichlorophenol
<0.18
<0.19
<0.17
<0.19
<0.18
<0.17
<0.21
<0.17
<0.15
<0.19
<0.15
38
0.0097
490
2,4-Dinitrophenol
<0.54
<0.57
<O.SI
<0.57
<O.SS
<0.51
<0.63
<0.50
<0.46
<0.57
<0.44
25
0.31
330
2,4-Dinitrotoluene
<0.25
<0.26
<0.23
<0.26
<0.25
<0.23
<0.29
<0.23
<0.21
<0.26
<0.20
1.7
0.0027
7.4
2,6-Dinitrotoluene
<0.24
<0.15
<0.23
<0.25
<0.24
<0.23
<0.28
<0.21
<0.20
<0.25
<0.20
0.36
0.00064
1.5
Hexachloro-1,3-butadiene
<0.21
<0.22
<0.20
<0.22
<0.21
<0.20
<0.24
<0.19
<0.18
<0.22
<0.17
1.3
0.015
5.6
Hexachlorobenzene
<0.20
<0.21
<0.19
<0.21
<0.21
<0.19
<0.24
<0.19
<0.17
<0.21
<0.17
0.22
0.005
0.99
Hexachloroethane
<0.15
<0.15
<0.14
<0.15
<0.15
<0.14
<0.17
<0.14
<0.12
<0.15
<0.12
1.9
0.011
8.5
1-Methylnaphthalene
<0.20
<0.21
<0.18
<0.21
<0.20
<0.19
<0.23
<0.18
<0.17
<0.20
<0.16
18
0.11
73
Nitrobenzene
<0.20
<0.21
<0.18
<0.21
<0.20
<0.19
<0.23
<0.18
<0.17
<0.20
<0.16
5.5
0.18
24
N-Nitroso-di-n-propylamine
<0.21
<0.22
<0.20
<0.22
<0.22
<0.20
<0.25
<0.20
<0.18
<0.22
<0.17
0.078
0.000075
0.33
Pentachlorophenol
<0.59
<0.62
<0.55
<0.62
<0.60
<0.56
<0.69
<0.55
<0.50
<0.62
<0.48
1
0.0083
4
Pyridine
<0.089
<0.093
<0.083
<0.092
<0.090
<0.084
<0.10
<0.082
<0.074
<0.092
<0.072
16
0.048
230
2,4,6-Trichlorophenol
<0.23
<0.24
<0.21
<0.23
<0.23
<0.21
<0.26
<0.21
<0. 19
<0.23
<0. 18
13
0.077
160
Hexavalent Chromium (METHOD 7199) Sampled July 12, 2019
Chromium (VI) NT NT NT I NT I NT I NT 1 0.451 I NT I NT NT NT 0.31 3.8 6.5
RCRA METALS (METHODS 7471A & 60108) Sampled July 12, 2019
Mercury
< 0.024
< 0.025
< 0.023
< 0.025
< 0.025
< 0.023
< 0.028
< 0.023
< 0.020
< 0.025
< 0.020
2.3
1
9.7
Arsenic
<0.19
2.2
<0.17
<0.19
2.9
7.5
13
<0.17
4.3
3.2
4.6
0.68
5.8
3
Barium
40
20
24
24
24
96
440
25
620
92
620
3100
580
47000
Cadmium
<0.048
<0.050
<0.045
<0.050
<0.048
<0.045
<0.056
<0.044
<0.040
<0.050
<0.039
14
3
200
Total Chromium (III / VI)
2.4
9.3
6.0
7.5
IS
17
23
6.5
18
17
18
2300/0.31
36000/3.8
35000/6.5
Lead
13
11
7.1
7.9
8.3
60
50
5.1
15
38
15
400
270
800
Selenium
<0.39
<0.40
<0.36
<0.40
<0.39
<0.37
<0.45
<0.36
<0.33
<0.40
<0.31
78
2.1
1200
Silver
<0.043
<0.045
<0.041
<0.045
<0.044
<0.041
<0.050
<0.040
<0.036
<0.045
<0.035
78
3.4
1200
Notes: All concentrations reported in mg/Kg
mg/Kg= Milligrams per kilogram
PSRG = Preliminary Soil Remediation Goals (February 2018)
Italics = Value exceed protection of groundwater PSRG
Bold = Value exceeds Unrestricted Health based PSRG
<0.0012 = Sample not detected above laboratory method detection limit.
1= The identification of the analyze is acceptable; the reported value is an estimate
Yellow highlighted values exceed the Industrial PSRG
The established North Carolina wide background value for Arsenic -4.5 mg/kg
NT = Sample not tested

ATTACHMENT C
EARTHTEC DISPOSAL DOCUMENTATION
0 Mid Atlantic

Earthtec of NC, Inc.
3145 Rosser Road
Bear Creek, NC 27207
Certificate of Acceptance and Disposal
Earthtec of NC received 773.28 tons of contaminated soil from 09 JUL 2019 to 15 JUL 2019, which was
delivered by Gaines and Company, 526 Three Sisters Road, Knightdale, NC 27545. Earthtec guarantees
that this soil will be treated beyond State of North Carolina requirements for clean soil.
Johnny Boone,F --�—
Plant Manager
Scott Keller.
Owner

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ATTACHMENT D
PRISM REPORT
ANLYSIS RESULTS
0 Mid Atlantic

Case Narrative
PRISM Full -Service Analytical &
Environmental Solutions
`,. LABORATORIES, INC.
Mid -Atlantic Associates, Inc. - Raleigh
Darin McClure
409 Rogers View Court
Raleigh, NC 27610
NC Certification No. 402
NC Drinking Water Cent No. 37735
SC Certification No. 99012
Project: 3021.01
Lab Submittal Date: 07/16/2019
Prism Work Order: 9070214
8/21/19 9:50
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Method 7199 analysis was subcontracted to AILS Global. Laboratory report is attached.
Prism Summary of Detections does not include subcontracted data.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a ---I
Angela D. Overcash
VP Laboratory Services
Reviewed By Angela D. Overcash
VP Laboratory Services
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Data Qualifiers Key Reference:
BL MB greater than one half of the RL, but the sample concentrations are less than the RL.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
M Matrix spike outside of the control limits.
P Recovery outside of the QC limits due to inconsistency during extraction and chromatographic performance of this
compound.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PRISMSample
LABORATORIES INC.
Full -Service Analytical R
Environmental Solutions
Receipt Summary
08/21/2019
Prism Work Order: 9070214
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
SS-1
9070214-01
Solid
07/12/19
14:20
07/16/19 10:05
SS-2
9070214-02
Solid
07/12/19
14:30
07/16/19 10:05
SS-3
9070214-03
Solid
07/12/19
14:40
07/16/19 10:05
SS-4
9070214-04
Solid
07/12/19
14:50
07/16/19 10:05
SS-5
9070214-05
Solid
07/12/19
15:15
07/16/19 10:05
SS-6
9070214-06
Solid
07/12/19
15:25
07/16/19 10:05
SS-7
9070214-07
Solid
07/12/19
15:30
07/16/19 10:05
SS-8
9070214-08
Solid
07/12/19
15:40
07/16/19 10:05
SS-9
9070214-09
Solid
07/12/19
15:50
07/16/19 10:05
SS-10
9070214-10
Solid
07/12/19
16:00
07/16/19 10:05
Duplicate
9070214-11
Solid
07/12/19
15:55
07/16/19 10:05
Samples were received in good condition at 0.5 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I S M Full Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Summary of Detections
08/21 /2019
Prism Work Order: 9070214
Prism ID
Client ID
Parameter
Method
Result
Units
9070214-01
SS-1
Barium
`6010D
40
mg/kg dry
9070214-01
SS-1
Chromium
'6010D
2.4
mg/kg dry
9070214-01
SS-1
Lead
'6010D
13
mg/kg dry
9070214-02
SS-2
Arsenic
`6010D
2.2
mg/kg dry
9070214-02
SS-2
Barium
'6010D
20
mg/kg dry
9070214-02
SS-2
Chromium
"6010D
9.3
mg/kg dry
9070214-02
SS-2
Lead
'6010D
11
mg/kg dry
9070214-02
SS-2
Acetone
8260D
0.014
J
mg/kg dry
9070214-02
SS-2
Methylene Chloride
8260D
0.0058
J
mg/kg dry
9070214-03
SS-3
Barium
'6010D
24
mg/kg dry
9070214-03
SS-3
Chromium
`6010D
6.0
mg/kg dry
9070214-03
SS-3
Lead
'6010D
7.1
mg/kg dry
9070214-03
SS-3
Acetone
8260D
0.015
J
mg/kg dry
9070214-03
SS-3
Methylene Chloride
8260D
0.0035
J
mg/kg dry
9070214-04
SS-4
Barium
`6010D
24
mg/kg dry
9070214-04
SS-4
Chromium
"6010D
7.5
mg/kg dry
9070214-04
SS-4
Lead
'6010D
7.9
mg/kg dry
9070214-05
SS-5
Arsenic
`6010D
2.9
mg/kg dry
9070214-05
SS-5
Barium
'6010D
24
mg/kg dry
9070214-05
SS-5
Chromium
"6010D
15
mg/kg dry
9070214-05
SS-5
Lead
'6010D
8.3
mg/kg dry
9070214-05
SS-5
Acetone
8260D
0.017
J
mg/kg dry
9070214-06
SS-6
Arsenic
"6010D
7.5
mg/kg dry
9070214-06
SS-6
Barium
'6010D
96
mg/kg dry
9070214-06
SS-6
Chromium
`6010D
17
mg/kg dry
9070214-06
SS-6
Lead
'6010D
60
mg/kg dry
9070214-06
SS-6
Acetone
8260D
0.013
J
mg/kg dry
9070214-06
SS-6
Methylene Chloride
8260D
0.0034
J
mg/kg dry
9070214-07
SS-7
Arsenic
'6010D
13
mg/kg dry
9070214-07
SS-7
Barium
"6010D
440
mg/kg dry
9070214-07
SS-7
Chromium
'6010D
23
mg/kg dry
9070214-07
SS-7
Lead
`6010D
50
mg/kg dry
9070214-07
SS-7
Acetone
8260D
0.016
J
mg/kg dry
9070214-08
SS-8
Barium
'6010D
25
mg/kg dry
9070214-08
SS-8
Chromium
`6010D
6.5
mg/kg dry
9070214-08
SS-8
Lead
'6010D
5.1
mg/kg dry
9070214-08
SS-8
Acetone
8260D
0.019
J
mg/kg dry
9070214-09
SS-9
Arsenic
'6010D
4.3
mg/kg dry
9070214-09
SS-9
Barium
`6010D
620
mg/kg dry
9070214-09
SS-9
Chromium
"6010D
18
mg/kg dry
9070214-09
SS-9
Lead
'6010D
15
mg/kg dry
9070214-10
SS-10
Arsenic
`6010D
3.2
mg/kg dry
9070214-10
SS-10
Barium
'6010D
92
mg/kg dry
9070214-10
SS-10
Chromium
"6010D
17
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

/GAIER I S M Fun -Service Analytical Environmental Solutions
LABORATORIES, ING
Summary of Detections
08/21 /2019
Prism Work Order: 9070214
Prism ID
Client ID
Parameter
Method
Result
Units
9070214-10
SS-10
Lead
'6010D
38
mg/kg dry
9070214-10
SS-10
1,2,4-Trimethylbenzene
8260D
0.0031
J
mg/kg dry
9070214-10
SS-10
m,p-Xylenes
8260D
0.0032
.1
mg/kg dry
9070214-10
SS-10
Methylene Chloride
8260D
0.0037
J
mg/kg dry
9070214-10
SS-10
Xylenes, total
8260D
0.0032
J
mg/kg dry
9070214-11
Duplicate
Arsenic
'6010D
4.6
mg/kg dry
9070214-11
Duplicate
Barium
'6010D
620
mg/kg dry
9070214-11
Duplicate
Chromium
"6010D
18
mg/kg dry
9070214-11
Duplicate
Lead
'6010D
15
mg/kg dry
9070214-11
Duplicate
1,2,4-Trimethylbenzene
8260D
0.0029
.1
mg/kg dry
9070214-11
Duplicate
m,p-Xylenes
8260D
0.0031
J
mg/kg dry
9070214-11
Duplicate
Naphthalene
8260D
0.0029
J
mg/kg dry
9070214-11
Duplicate
Xylenes, total
8260D
0.0031
J
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
08/21/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3021.01
Client
Sample ID:
SS-1
Attn: Darin McClure
Prism
Sample ID:
9070214-01
409 Rogers View Court
Prism
Work Order: 9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected: 07/12/19
14:20
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
71.1
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.93
0.16
1
8270E
7/22/19 14:17
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.93
0.15
1
8270E
7/22/19 14:17
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.93
0.14
1
8270E
7/22/19 14:17
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.46
0.15
1
8270E
7/22/19 14:17
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.93
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.93
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.93
0.23
1
8270E
7/22/19 14:17
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.93
0.18
1
8270E
7/22/19 14:17
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.46
0.19
1
8270E
7/22/19 14:17
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
2.1
0.54
1
8270E
7/22/19 14:17
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.93
0.25
1
8270E
7/22/19 14:17
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.93
0.24
1
8270E
7/22/19 14:17
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.93
0.23
1
8270E
7/22/19 14:17
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.93
0.18
1
8270E
7/22/19 14:17
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.93
0.18
1
8270E
7/22/19 14:17
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.93
0.18
1
8270E
7/22/19 14:17
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.93
0.15
1
8270E
7/22/19 14:17
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.93
0.18
1
8270E
7/22/19 14:17
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.93
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.1
0.51
1
8270E
7/22/19 14:17
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.93
0.22
1
8270E
7/22/19 14:17
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.93
0.18
1
8270E
7/22/19 14:17
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.46
0.11
1
8270E
7/22/19 14:17
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.4
0.28
1
8270E
7/22/19 14:17
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.93
0.23
1
8270E
7/22/19 14:17
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.93
0.22
1
8270E
7/22/19 14:17
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.93
0.25
1
8270E
7/22/19 14:17
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.93
0.25
1
8270E
7/22/19 14:17
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.93
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.93
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.93
0.21
1
8270E
7/22/19 14:17
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.93
0.22
1
8270E
7/22/19 14:17
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.93
0.18
1
8270E
7/22/19 14:17
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.93
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.8
0.77
1
8270E
7/22/19 14:17
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.93
0.17
1
8270E
7/22/19 14:17
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.93
0.18
1
8270E
7/22/19 14:17
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.93
0.15
1
8270E
7/22/19 14:17
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.46
0.17
1
8270E
7/22/19 14:17
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
P R S M
/ Environmental Solutions
LABORATORIES INC.
08/21/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3021.01
Client Sample ID: SS-1
Attn: Darin McClure
Prism Sample ID: 9070214-01
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 14:20
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.93
0.21
1
8270E
7/22/19 14:17
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.46
0.16
1
8270E
7/22/19 14:17
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.93
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.93
0.27
1
8270E
7/22/19 14:17
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.93
0.25
1
8270E
7/22/19 14:17
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.93
0.24
1
8270E
7/22/19 14:17
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.93
0.22
1
8270E
7/22/19 14:17
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.93
0.23
1
8270E
7/22/19 14:17
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.46
0.24
1
8270E
7/22/19 14:17
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.93
0.23
1
8270E
7/22/19 14:17
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.93
0.28
1
8270E
7/22/19 14:17
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.93
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.93
0.21
1
8270E
7/22/19 14:17
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.93
0.32
1
8270E
7/22/19 14:17
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.93
0.15
1
8270E
7/22/19 14:17
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.93
0.17
1
8270E
7/22/19 14:17
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.93
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.93
0.18
1
8270E
7/22/19 14:17
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.46
0.20
1
8270E
7/22/19 14:17
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.93
0.21
1
8270E
7/22/19 14:17
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.93
0.25
1
8270E
7/22/19 14:17
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.4
0.59
1
8270E
7/22/19 14:17
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.93
0.24
1
8270E
7/22/19 14:17
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.93
0.15
1
8270E
7/22/19 14:17
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.93
0.21
1
8270E
7/22/19 14:17
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.46
0.089
1
8270E
7/22/19 14:17
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
90 %
39-132
2-Fluorobiphenyl
81 %
44-115
2-Fluorophenol
82 %
35-115
Nitrobenzene-d5
67 %
37-122
Phenol-d5
81 %
34-121
Terphenyl-d14
85 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.070
0.024
1
*7471B
7/31/19 12:52
MMR
P9G0500
Arsenic
BRL
mg/kg dry
1.4
0.19
1
*6010D
8/1/19 12:27
JAB
P9G0507
Barium
40
mg/kg dry
14
4.2
1
*6010D
8/1119 12:27
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.70
0.048
1
*6010D
8/1/19 12:27
JAB
P9G0507
Chromium
2.4
mg/kg dry
1.4
0.11
1
*60101)
8/1/19 12:27
JAB
P9G0507
Lead
13
mg/kg dry
1.4
0.23
1
*60101)
8/1/19 12:27
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.4
0.39
1
*6010D
8/1/19 12:27
JAB
P9G0507
Silver
BRL
mg/kg dry
0.70
0.043
1
*6010D
8/1/19 12:27
JAB
P9G0507
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01
Sample Matrix: Solid
Laboratory Report
08/21/2019
Client Sample ID: SS-1
Prism Sample ID: 9070214-01
Prism Work Order: 9070214
Time Collected: 07/12/19 14:20
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0060
0.00074
1
8260D
7/19/19 15:22
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0060
0.00089
1
8260D
7/19/19 15:22
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0060
0.00044
1
8260D
7/19/19 15:22
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0060
0.00065
1
8260D
7/19/19 15:22
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0060
0.0011
1
8260D
7/19/19 15:22
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0060
0.0011
1
8260D
7/19/19 15:22
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00093
1
8260D
7/19/19 15:22
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00087
1
8260D
7/19/19 15:22
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0060
0.00069
1
8260D
7/19/19 15:22
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00058
1
8260D
7/19/19 15:22
JLB
P9G0319
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0060
0.00064
1
8260D
7/19/19 15:22
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0060
0.00054
1
8260D
7/19/19 15:22
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00067
1
8260D
7/19/19 15:22
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0060
0.00072
1
8260D
7/19/19 15:22
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0060
0.00091
1
8260D
7/19/19 15:22
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0060
0.00076
1
8260D
7/19/19 15:22
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00075
1
8260D
7/19/19 15:22
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0060
0.00051
1
8260D
7/19/19 15:22
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00077
1
8260D
7/19/19 15:22
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0060
0.00075
1
8260D
7/19/19 15:22
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0060
0.00081
1
8260D
7/19/19 15:22
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0060
0.00069
1
8260D
7/19/19 15:22
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0060
0.0015
1
8260D
7/19/19 15:22
JLB
P9G0319
Acetone
BRL
mg/kg dry
0.024
0.0015
1
8260D
7/19/19 15:22
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0060
0.00094
1
8260D
7/19/19 15:22
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0060
0.00084
1
8260D
7/19/19 15:22
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0060
0.00099
1
8260D
7/19/19 15:22
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0060
0.00057
1
8260D
7/19/19 15:22
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0060
0.00047
1
8260D
7/19/19 15:22
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.012
0.0030
1
8260D
7/19/19 15:22
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0060
0.0012
1
8260D
7/19/19 15:22
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0060
0.00094
1
8260D
7/19/19 15:22
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.012
0.0012
1
8260D
7/19/19 15:22
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0060
0.00074
1
8260D
7/19/19 15:22
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
8260D
7/19/19 15:22
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0060
0.00095
1
8260D
7/19/19 15:22
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00060
1
8260D
7/19/19 15:22
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0060
0.00040
1
8260D
7/19/19 15:22
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
7/19/19 15:22
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0060
0.00091
1
8260D
7/19/19 15:22
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0060
0.00089
1
8260D
7/19/19 15:22
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0060
0.00070
1
8260D
7/19/19 15:22
JLB
P9G0319
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0015
1
8260D
7/19/19 15:22
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-1
Attn: Darin McClure Prism Sample ID: 9070214-01
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 14:20
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.024
0.00042
1
8260D
7/19/19 15:22
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.024
0.0014
1
8260D
7/19/19 15:22
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.024
0.00049
1
8260D
7/19/19 15:22
JLB
P9G0319
Methylene Chloride
BRL
mg/kg dry
0.0060
0.00098
1
8260D
7/19/19 15:22
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0060
0.00085
1
8260D
7/19/19 15:22
JLB
P9G0319
Naphthalene
BRL
mg/kg dry
0.012
0.00061
1
8260D
7/19/19 15:22
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0060
0.00057
1
8260D
7/19/19 15:22
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0060
0.00088
1
8260D
7/19/19 15:22
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0060
0.00064
1
8260D
7/19/19 15:22
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0060
0.00065
1
8260D
7/19/19 15:22
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0060
0.00059
1
8260D
7/19/19 15:22
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0060
0.00072
1
8260D
7/19/19 15:22
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0060
0.0011
1
8260D
7/19/19 15:22
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0060
0.00096
1
8260D
7/19/19 15:22
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0060
0.0012
1
8260D
7/19/19 15:22
JLB
P9G0319
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00052
1
8260D
7/19/19 15:22
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0060
0.0012
1
8260D
7/19/19 15:22
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
7/19/19 15:22
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.012
0.00065
1
8260D
7/19/19 15:22
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
7/19/19 15:22
JLB
P9G0319
Xylenes, total
BRL
mg/kg dry
0.018
0.0022
1
8260D
7/19/19 15:22
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
103 %
70-130
Dibromofluoromethane
101 %
84-123
Toluene-d8
92 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-2
Attn: Darin McClure Prism Sample ID: 9070214-02
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 14:30
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
67.9
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.97
0.17
1
8270E
7/22/19 14:39
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 14:39
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.97
0.14
1
8270E
7/22/19 14:39
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.49
0.15
1
8270E
7/22/19 14:39
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 14:39
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 14:39
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.49
0.20
1
8270E
7/22/19 14:39
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
2.2
0.57
1
8270E
7/22/19 14:39
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 14:39
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.97
0.25
1
8270E
7/22/19 14:39
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 14:39
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 14:39
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 14:39
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 14:39
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 14:39
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 14:39
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.2
0.54
1
8270E
7/22/19 14:39
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 14:39
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 14:39
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.49
0.12
1
8270E
7/22/19 14:39
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.5
0.30
1
8270E
7/22/19 14:39
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 14:39
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 14:39
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 14:39
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 14:39
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 14:39
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 14:39
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 14:39
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.9
0.81
1
8270E
7/22/19 14:39
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 14:39
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 14:39
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 14:39
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.49
0.17
1
8270E
7/22/19 14:39
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
08/21/2019
Mid -Atlantic Associates,
Inc. - Raleigh
Project: 3021.01
Client Sample ID: SS-2
Attn: Darin McClure
Prism Sample ID: 9070214-02
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 14:30
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 14:39
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.49
0.17
1
8270E
7/22/19 14:39
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.97
0.28
1
8270E
7/22/19 14:39
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 14:39
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.97
0.25
1
8270E
7/22/19 14:39
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 14:39
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 14:39
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.49
0.25
1
8270E
7/22/19 14:39
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 14:39
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.97
0.29
1
8270E
7/22/19 14:39
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 14:39
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.97
0.33
1
8270E
7/22/19 14:39
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.97
0.15
1
8270E
7/22/19 14:39
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 14:39
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 14:39
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.49
0.21
1
8270E
7/22/19 14:39
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 14:39
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.97
0.27
1
8270E
7/22/19 14:39
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.5
0.62
1
8270E
7/22/19 14:39
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.97
0.25
1
8270E
7/22/19 14:39
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 14:39
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 14:39
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.49
0.093
1
8270E
7/22/19 14:39
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
89 %
39-132
2-Fluorobiphenyl
86 %
44-115
2-Fluorophenol
86 %
35-115
Nitrobenzene-d5
71 %
37-122
Phenol-d5
83 %
34-121
Terphenyl-d14
84 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.074
0.025
1
*7471B
7/31/19 12:01
MMR
P9G0500
Arsenic
2.2
mg/kg dry
1.5
0.19
1
*6010D
8/1/19 12:51
JAB
P9G0507
Barium
20
mg/kg dry
15
4.4
1
*60101)
8/1/19 12:51
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.74
0.050
1
*6010D
8/1/19 12:51
JAB
P9G0507
Chromium
9.3
mg/kg dry
1.5
0.11
1
*6010D
8/1/19 12:51
JAB
P9G0507
Lead
11
mg/kg dry
1.5
0.25
1
*6010D
8/1/19 12:51
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.5
0.40
1
*6010D
8/1/19 12:51
JAB
P9G0507
Silver
BRL
mg/kg dry
0.74
0.045
1
*6010D
8/1/19 12:51
JAB
P9G0507
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
08/21 /2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01 Client Sample ID: SS-2
Prism Sample ID: 9070214-02
Prism Work Order: 9070214
Sample Matrix: Solid Time Collected: 07/12/19 14:30
Time Submitted: 07/16/19 10:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0070
0.00086
1
8260D
7/19/19 15:51
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0070
0.0010
1
8260D
7/19/19 15:51
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0070
0.00051
1
8260D
7/19/19 15:51
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0070
0.00076
1
8260D
7/19/19 15:51
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0070
0.0013
1
8260D
7/19/19 15:51
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0070
0.0013
1
8260D
7/19/19 15:51
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0070
0.0011
1
8260D
7/19/19 15:51
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.014
0.0010
1
8260D
7/19/19 15:51
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0070
0.00080
1
8260D
7/19/19 15:51
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.014
0.00067
1
8260D
7/19/19 15:51
JLB
P9G0319
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0070
0.00074
1
8260D
7/19/19 15:51
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0070
0.00063
1
8260D
7/19/19 15:51
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0070
0.00078
1
8260D
7/19/19 15:51
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0070
0.00084
1
8260D
7/19/19 15:51
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0070
0.0011
1
8260D
7/19/19 15:51
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0070
0.00088
1
8260D
7/19/19 15:51
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0070
0.00087
1
8260D
7/19/19 15:51
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0070
0.00059
1
8260D
7/19/19 15:51
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0070
0.00089
1
8260D
7/19/19 15:51
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0070
0.00088
1
8260D
7/19/19 15:51
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0070
0.00094
1
8260D
7/19/19 15:51
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0070
0.00080
1
8260D
7/19/19 15:51
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0070
0.0018
1
8260D
7/19/19 15:51
JLB
P9G0319
Acetone
0.014 J
mg/kg dry
0.028
0.0018
1
8260D
7/19/19 15:51
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0070
0.0011
1
8260D
7/19/19 15:51
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0070
0.00098
1
8260D
7/19/19 15:51
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0070
0.0012
1
8260D
7/19/19 15:51
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0070
0.00067
1
8260D
7/19/19 15:51
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0070
0.00054
1
8260D
7/19/19 15:51
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.014
0.0034
1
8260D
7/19/19 15:51
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0070
0.0014
1
8260D
7/19/19 15:51
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0070
0.0011
1
8260D
7/19/19 15:51
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.014
0.0013
1
8260D
7/19/19 15:51
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0070
0.00086
1
8260D
7/19/19 15:51
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.014
0.0021
1
8260D
7/19/19 15:51
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0070
0.0011
1
8260D
7/19/19 15:51
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0070
0.00069
1
8260D
7/19/19 15:51
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0070
0.00047
1
8260D
7/19/19 15:51
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.014
0.0020
1
8260D
7/19/19 15:51
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0070
0.0011
1
8260D
7/19/19 15:51
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0070
0.0010
1
8260D
7/19/19 15:51
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0070
0.00082
1
8260D
7/19/19 15:51
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-2
Attn: Darin McClure Prism Sample ID: 9070214-02
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 14:30
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.014
0.0018
1
8260D
7/19/19 15:51
JLB
P9G0319
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.028
0.00049
1
8260D
7/19/19 15:51
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.028
0.0016
1
8260D
7/19/19 15:51
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.028
0.00057
1
8260D
7/19/19 15:51
JLB
P9G0319
Methylene Chloride
0.0058 J
mg/kg dry
0.0070
0.0011
1
8260D
7/19/19 15:51
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0070
0.00098
1
8260D
7/19/19 15:51
JLB
P9G0319
Naphthalene
BRL
mg/kg dry
0.014
0.00071
1
8260D
7/19/19 15:51
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0070
0.00066
1
8260D
7/19/19 15:51
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0070
0.0010
1
8260D
7/19/19 15:51
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0070
0.00075
1
8260D
7/19/19 15:51
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0070
0.00076
1
8260D
7/19/19 15:51
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0070
0.00068
1
8260D
7/19/19 15:51
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0070
0.00083
1
8260D
7/19/19 15:51
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0070
0.0013
1
8260D
7/19/19 15:51
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0070
0.0011
1
8260D
7/19/19 15:51
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0070
0.0013
1
8260D
7/19/19 15:51
JLB
P9G0319
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0070
0.00060
1
8260D
7/19/19 15:51
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0070
0.0014
1
8260D
7/19/19 15:51
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.014
0.0019
1
8260D
7/19/19 15:51
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.014
0.00076
1
8260D
7/19/19 15:51
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.014
0.0014
1
8260D
7/19/19 15:51
JLB
P9G0319
Xylenes, total
BRL
mg/kg dry
0.021
0.0025
1
8260D
7/19/19 15:51
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101 %
70-130
Dibromofluoromethane
101 %
84-123
Toluene-d8
92 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-3
Attn: Darin McClure Prism Sample ID: 9070214-03
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 14:40
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
75.6
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.87
0.15
1
8270E
7/22/19 15:01
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.87
0.14
1
8270E
7/22/19 15:01
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.87
0.13
1
8270E
7/22/19 15:01
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.44
0.14
1
8270E
7/22/19 15:01
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.87
0.18
1
8270E
7/22/19 15:01
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.87
0.18
1
8270E
7/22/19 15:01
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.87
0.21
1
8270E
7/22/19 15:01
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.87
0.17
1
8270E
7/22/19 15:01
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.44
0.18
1
8270E
7/22/19 15:01
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
2.0
0.51
1
8270E
7/22/19 15:01
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.87
0.23
1
8270E
7/22/19 15:01
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.87
0.23
1
8270E
7/22/19 15:01
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.87
0.21
1
8270E
7/22/19 15:01
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.87
0.17
1
8270E
7/22/19 15:01
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.87
0.17
1
8270E
7/22/19 15:01
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.87
0.17
1
8270E
7/22/19 15:01
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.87
0.15
1
8270E
7/22/19 15:01
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.87
0.17
1
8270E
7/22/19 15:01
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.87
0.19
1
8270E
7/22/19 15:01
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.0
0.48
1
8270E
7/22/19 15:01
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.87
0.20
1
8270E
7/22/19 15:01
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.87
0.17
1
8270E
7/22/19 15:01
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.44
0.11
1
8270E
7/22/19 15:01
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.27
1
8270E
7/22/19 15:01
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.87
0.21
1
8270E
7/22/19 15:01
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.87
0.21
1
8270E
7/22/19 15:01
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.87
0.23
1
8270E
7/22/19 15:01
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.87
0.24
1
8270E
7/22/19 15:01
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.87
0.19
1
8270E
7/22/19 15:01
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.87
0.19
1
8270E
7/22/19 15:01
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.87
0.19
1
8270E
7/22/19 15:01
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.87
0.20
1
8270E
7/22/19 15:01
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.87
0.17
1
8270E
7/22/19 15:01
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.87
0.19
1
8270E
7/22/19 15:01
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.6
0.72
1
8270E
7/22/19 15:01
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.87
0.16
1
8270E
7/22/19 15:01
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.87
0.17
1
8270E
7/22/19 15:01
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.87
0.14
1
8270E
7/22/19 15:01
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.44
0.16
1
8270E
7/22/19 15:01
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
P R S M
/ Environmental Solutions
LABORATORIES INC.
08/21/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3021.01
Client Sample ID: SS-3
Attn: Darin McClure
Prism Sample ID: 9070214-03
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 14:40
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.87
0.20
1
8270E
7/22/19 15:01
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.44
0.15
1
8270E
7/22/19 15:01
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.87
0.19
1
8270E
7/22/19 15:01
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.87
0.25
1
8270E
7/22/19 15:01
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.87
0.23
1
8270E
7/22/19 15:01
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.87
0.22
1
8270E
7/22/19 15:01
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.87
0.21
1
8270E
7/22/19 15:01
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.87
0.22
1
8270E
7/22/19 15:01
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.44
0.23
1
8270E
7/22/19 15:01
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.87
0.22
1
8270E
7/22/19 15:01
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.87
0.26
1
8270E
7/22/19 15:01
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.87
0.19
1
8270E
7/22/19 15:01
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.87
0.20
1
8270E
7/22/19 15:01
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.87
0.30
1
8270E
7/22/19 15:01
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.87
0.14
1
8270E
7/22/19 15:01
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.87
0.16
1
8270E
7/22/19 15:01
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.87
0.19
1
8270E
7/22/19 15:01
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.87
0.17
1
8270E
7/22/19 15:01
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.44
0.18
1
8270E
7/22/19 15:01
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.87
0.20
1
8270E
7/22/19 15:01
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.87
0.24
1
8270E
7/22/19 15:01
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.3
0.56
1
8270E
7/22/19 15:01
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.87
0.23
1
8270E
7/22/19 15:01
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.87
0.14
1
8270E
7/22/19 15:01
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.87
0.20
1
8270E
7/22/19 15:01
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.44
0.083
1
8270E
7/22/19 15:01
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
81 %
39-132
2-Fluorobiphenyl
80 %
44-115
2-Fluorophenol
80 %
35-115
Nitrobenzene-d5
65 %
37-122
Phenol-d5
78 %
34-121
Terphenyl-d14
79 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.066
0.023
1
*7471B
7/31/19 12:06
MMR
P9G0500
Arsenic
BRL
mg/kg dry
1.3
0.17
1
*6010D
8/1/19 12:58
JAB
P9G0507
Barium
24
mg/kg dry
13
4.0
1
*6010D
8/1119 12:58
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.66
0.045
1
*6010D
8/1/19 12:58
JAB
P9G0507
Chromium
6.0
mg/kg dry
1.3
0.10
1
*60101)
8/1/19 12:58
JAB
P9G0507
Lead
7.1
mg/kg dry
1.3
0.22
1
*60101)
8/1/19 12:58
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.3
0.36
1
*6010D
8/1/19 12:58
JAB
P9G0507
Silver
BRL
mg/kg dry
0.66
0.041
1
*6010D
8/1/19 12:58
JAB
P9G0507
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01
Sample Matrix: Solid
Laboratory Report
08/21/2019
Client Sample ID: SS-3
Prism Sample ID: 9070214-03
Prism Work Order: 9070214
Time Collected: 07/12/19 14:40
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0061
0.00074
1
8260D
7/22/19 15:21
JLB
P9G0345
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0061
0.00089
1
8260D
7/22/19 15:21
JLB
P9G0345
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0061
0.00044
1
8260D
7/22/19 15:21
JLB
P9G0345
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0061
0.00066
1
8260D
7/22/19 15:21
JLB
P9G0345
1,1-Dichloroethane
BRL
mg/kg dry
0.0061
0.0011
1
8260D
7/22/19 15:21
JLB
P9G0345
1,1-Dichloroethylene
BRL
mg/kg dry
0.0061
0.0011
1
8260D
7/22/19 15:21
JLB
P9G0345
1,1-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00094
1
8260D
7/22/19 15:21
JLB
P9G0345
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00087
1
8260D
7/22/19 15:21
JLB
P9G0345
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0061
0.00069
1
8260D
7/22/19 15:21
JLB
P9G0345
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00058
1
8260D
7/22/19 15:21
JLB
P9G0345
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0061
0.00064
1
8260D
7/22/19 15:21
JLB
P9G0345
1,2-Dibromoethane
BRL
mg/kg dry
0.0061
0.00054
1
8260D
7/22/19 15:21
JLB
P9G0345
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00068
1
8260D
7/22/19 15:21
JLB
P9G0345
1,2-Dichloroethane
BRL
mg/kg dry
0.0061
0.00072
1
8260D
7/22/19 15:21
JLB
P9G0345
1,2-Dichloropropane
BRL
mg/kg dry
0.0061
0.00091
1
8260D
7/22/19 15:21
JLB
P9G0345
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0061
0.00076
1
8260D
7/22/19 15:21
JLB
P9G0345
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00076
1
8260D
7/22/19 15:21
JLB
P9G0345
1,3-Dichloropropane
BRL
mg/kg dry
0.0061
0.00051
1
8260D
7/22/19 15:21
JLB
P9G0345
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00077
1
8260D
7/22/19 15:21
JLB
P9G0345
2,2-Dichloropropane
BRL
mg/kg dry
0.0061
0.00076
1
8260D
7/22/19 15:21
JLB
P9G0345
2-Chlorotoluene
BRL
mg/kg dry
0.0061
0.00081
1
8260D
7/22/19 15:21
JLB
P9G0345
4-Chlorotoluene
BRL
mg/kg dry
0.0061
0.00069
1
8260D
7/22/19 15:21
JLB
P9G0345
4-Isopropyltoluene
BRL
mg/kg dry
0.0061
0.0015
1
8260D
7/22/19 15:21
JLB
P9G0345
Acetone
0.015
J mg/kg dry
0.024
0.0016
1
8260D
7/22/19 15:21
JLB
P9G0345
Benzene
BRL
mg/kg dry
0.0061
0.00095
1
8260D
7/22/19 15:21
JLB
P9G0345
Bromobenzene
BRL
mg/kg dry
0.0061
0.00084
1
8260D
7/22/19 15:21
JLB
P9G0345
Bromochloromethane
BRL
mg/kg dry
0.0061
0.0010
1
8260D
7/22/19 15:21
JLB
P9G0345
Bromodichloromethane
BRL
mg/kg dry
0.0061
0.00058
1
8260D
7/22/19 15:21
JLB
P9G0345
Bromoform
BRL
mg/kg dry
0.0061
0.00047
1
8260D
7/22/19 15:21
JLB
P9G0345
Bromomethane
BRL
mg/kg dry
0.012
0.0030
1
8260D
7/22/19 15:21
JLB
P9G0345
Carbon Tetrachloride
BRL
mg/kg dry
0.0061
0.0012
1
8260D
7/22/19 15:21
JLB
P9G0345
Chlorobenzene
BRL
mg/kg dry
0.0061
0.00095
1
8260D
7/22/19 15:21
JLB
P9G0345
Chloroethane
BRL
mg/kg dry
0.012
0.0012
1
8260D
7/22/19 15:21
JLB
P9G0345
Chloroform
BRL
mg/kg dry
0.0061
0.00074
1
8260D
7/22/19 15:21
JLB
P9G0345
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
8260D
7/22/19 15:21
JLB
P9G0345
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0061
0.00096
1
8260D
7/22/19 15:21
JLB
P9G0345
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00060
1
8260D
7/22/19 15:21
JLB
P9G0345
Dibromochloromethane
BRL
mg/kg dry
0.0061
0.00041
1
8260D
7/22/19 15:21
JLB
P9G0345
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
7/22/19 15:21
JLB
P9G0345
Ethylbenzene
BRL
mg/kg dry
0.0061
0.00091
1
8260D
7/22/19 15:21
JLB
P9G0345
Isopropyl Ether
BRL
mg/kg dry
0.0061
0.00089
1
8260D
7/22/19 15:21
JLB
P9G0345
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0061
0.00071
1
8260D
7/22/19 15:21
JLB
P9G0345
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0016
1
8260D
7/22/19 15:21
JLB
P9G0345
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-3
Attn: Darin McClure Prism Sample ID: 9070214-03
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 14:40
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.024
0.00042
1
8260D
7/22/19 15:21
JLB
P9G0345
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.024
0.0014
1
8260D
7/22/19 15:21
JLB
P9G0345
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.024
0.00050
1
8260D
7/22/19 15:21
JLB
P9G0345
Methylene Chloride
0.0035 J
mg/kg dry
0.0061
0.00098
1
8260D
7/22/19 15:21
JLB
P9G0345
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0061
0.00085
1
8260D
7/22/19 15:21
JLB
P9G0345
Naphthalene
BRL
mg/kg dry
0.012
0.00061
1
8260D
7/22/19 15:21
JLB
P9G0345
n-Butylbenzene
BRL
mg/kg dry
0.0061
0.00057
1
8260D
7/22/19 15:21
JLB
P9G0345
n-Propylbenzene
BRL
mg/kg dry
0.0061
0.00088
1
8260D
7/22/19 15:21
JLB
P9G0345
o-Xylene
BRL
mg/kg dry
0.0061
0.00065
1
8260D
7/22/19 15:21
JLB
P9G0345
sec-Butylbenzene
BRL
mg/kg dry
0.0061
0.00066
1
8260D
7/22/19 15:21
JLB
P9G0345
Styrene
BRL
mg/kg dry
0.0061
0.00059
1
8260D
7/22/19 15:21
JLB
P9G0345
tert-Butylbenzene
BRL
mg/kg dry
0.0061
0.00072
1
8260D
7/22/19 15:21
JLB
P9G0345
Tetrachloroethylene
BRL
mg/kg dry
0.0061
0.0011
1
8260D
7/22/19 15:21
JLB
P9G0345
Toluene
BRL
mg/kg dry
0.0061
0.00097
1
8260D
7/22/19 15:21
JLB
P9G0345
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0061
0.0012
1
8260D
7/22/19 15:21
JLB
P9G0345
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00052
1
8260D
7/22/19 15:21
JLB
P9G0345
Trichloroethylene
BRL
mg/kg dry
0.0061
0.0012
1
8260D
7/22/19 15:21
JLB
P9G0345
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
7/22/19 15:21
JLB
P9G0345
Vinyl acetate
BRL
mg/kg dry
0.012
0.00066
1
8260D
7/22/19 15:21
JLB
P9G0345
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
7/22/19 15:21
JLB
P9G0345
Xylenes, total
BRL
mg/kg dry
0.018
0.0022
1
8260D
7/22/19 15:21
JLB
P9G0345
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
103 %
70-130
Dibromofluoromethane
109 %
84-123
Toluene-d8
91 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-4
Attn: Darin McClure Prism Sample ID: 9070214-04
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 14:50
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
68.0
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.97
0.17
1
8270E
7/22/19 15:24
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 15:24
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.97
0.14
1
8270E
7/22/19 15:24
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.48
0.15
1
8270E
7/22/19 15:24
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 15:24
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 15:24
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.48
0.20
1
8270E
7/22/19 15:24
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
2.2
0.57
1
8270E
7/22/19 15:24
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 15:24
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.97
0.25
1
8270E
7/22/19 15:24
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 15:24
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 15:24
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 15:24
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 15:24
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 15:24
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 15:24
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.2
0.53
1
8270E
7/22/19 15:24
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 15:24
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 15:24
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.48
0.12
1
8270E
7/22/19 15:24
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.5
0.30
1
8270E
7/22/19 15:24
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 15:24
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 15:24
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 15:24
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 15:24
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 15:24
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 15:24
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 15:24
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.9
0.80
1
8270E
7/22/19 15:24
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 15:24
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 15:24
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 15:24
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.48
0.17
1
8270E
7/22/19 15:24
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
P R S M
/ Environmental Solutions
LABORATORIES INC.
08/21/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3021.01
Client Sample ID: SS-4
Attn: Darin McClure
Prism Sample ID: 9070214-04
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 14:50
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 15:24
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.48
0.17
1
8270E
7/22/19 15:24
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.97
0.28
1
8270E
7/22/19 15:24
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 15:24
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.97
0.25
1
8270E
7/22/19 15:24
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 15:24
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 15:24
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.48
0.25
1
8270E
7/22/19 15:24
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 15:24
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.97
0.29
1
8270E
7/22/19 15:24
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 15:24
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.97
0.33
1
8270E
7/22/19 15:24
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.97
0.15
1
8270E
7/22/19 15:24
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 15:24
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 15:24
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.48
0.21
1
8270E
7/22/19 15:24
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 15:24
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.97
0.27
1
8270E
7/22/19 15:24
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.5
0.62
1
8270E
7/22/19 15:24
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.97
0.25
1
8270E
7/22/19 15:24
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 15:24
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 15:24
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.48
0.092
1
8270E
7/22/19 15:24
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
82 %
39-132
2-Fluorobiphenyl
81 %
44-115
2-Fluorophenol
81 %
35-115
Nitrobenzene-d5
67 %
37-122
Phenol-d5
78 %
34-121
Terphenyl-d14
81 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.073
0.025
1
*7471B
7/31/19 12:10
MMR
P9G0500
Arsenic
BRL
mg/kg dry
1.5
0.19
1
*6010D
8/1/19 13:06
JAB
P9G0507
Barium
24
mg/kg dry
15
4.4
1
*6010D
8/1119 13:06
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.73
0.050
1
*6010D
8/1/19 13:06
JAB
P9G0507
Chromium
7.5
mg/kg dry
1.5
0.11
1
*60101)
8/1/19 13:06
JAB
P9G0507
Lead
7.9
mg/kg dry
1.5
0.25
1
*60101)
8/1/19 13:06
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.5
0.40
1
*6010D
8/1/19 13:06
JAB
P9G0507
Silver
BRL
mg/kg dry
0.73
0.045
1
*6010D
8/1/19 13:06
JAB
P9G0507
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01
Sample Matrix: Solid
Laboratory Report
08/21/2019
Client Sample ID: SS-4
Prism Sample ID: 9070214-04
Prism Work Order: 9070214
Time Collected: 07/12/19 14:50
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0061
0.00075
1
8260D
7/19/19 16:51
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0061
0.00090
1
8260D
7/19/19 16:51
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0061
0.00045
1
8260D
7/19/19 16:51
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0061
0.00066
1
8260D
7/19/19 16:51
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0061
0.0011
1
8260D
7/19/19 16:51
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0061
0.0011
1
8260D
7/19/19 16:51
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00094
1
8260D
7/19/19 16:51
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00088
1
8260D
7/19/19 16:51
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0061
0.00069
1
8260D
7/19/19 16:51
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00058
1
8260D
7/19/19 16:51
JLB
P9G0319
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0061
0.00065
1
8260D
7/19/19 16:51
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0061
0.00055
1
8260D
7/19/19 16:51
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00068
1
8260D
7/19/19 16:51
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0061
0.00073
1
8260D
7/19/19 16:51
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0061
0.00092
1
8260D
7/19/19 16:51
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0061
0.00077
1
8260D
7/19/19 16:51
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00076
1
8260D
7/19/19 16:51
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0061
0.00051
1
8260D
7/19/19 16:51
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00078
1
8260D
7/19/19 16:51
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0061
0.00076
1
8260D
7/19/19 16:51
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0061
0.00082
1
8260D
7/19/19 16:51
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0061
0.00070
1
8260D
7/19/19 16:51
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0061
0.0015
1
8260D
7/19/19 16:51
JLB
P9G0319
Acetone
BRL
mg/kg dry
0.024
0.0016
1
8260D
7/19/19 16:51
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0061
0.00095
1
8260D
7/19/19 16:51
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0061
0.00085
1
8260D
7/19/19 16:51
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0061
0.0010
1
8260D
7/19/19 16:51
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0061
0.00058
1
8260D
7/19/19 16:51
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0061
0.00047
1
8260D
7/19/19 16:51
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.012
0.0030
1
8260D
7/19/19 16:51
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0061
0.0012
1
8260D
7/19/19 16:51
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0061
0.00096
1
8260D
7/19/19 16:51
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.012
0.0012
1
8260D
7/19/19 16:51
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0061
0.00075
1
8260D
7/19/19 16:51
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.012
0.0019
1
8260D
7/19/19 16:51
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0061
0.00096
1
8260D
7/19/19 16:51
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00060
1
8260D
7/19/19 16:51
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0061
0.00041
1
8260D
7/19/19 16:51
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
7/19/19 16:51
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0061
0.00092
1
8260D
7/19/19 16:51
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0061
0.00090
1
8260D
7/19/19 16:51
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0061
0.00071
1
8260D
7/19/19 16:51
JLB
P9G0319
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0016
1
8260D
7/19/19 16:51
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-4
Attn: Darin McClure Prism Sample ID: 9070214-04
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 14:50
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.024
0.00042
1
8260D
7/19/19 16:51
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.024
0.0014
1
8260D
7/19/19 16:51
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.024
0.00050
1
8260D
7/19/19 16:51
JLB
P9G0319
Methylene Chloride
BRL
mg/kg dry
0.0061
0.00099
1
8260D
7/19/19 16:51
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0061
0.00086
1
8260D
7/19/19 16:51
JLB
P9G0319
Naphthalene
BRL
mg/kg dry
0.012
0.00062
1
8260D
7/19/19 16:51
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0061
0.00057
1
8260D
7/19/19 16:51
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0061
0.00089
1
8260D
7/19/19 16:51
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0061
0.00065
1
8260D
7/19/19 16:51
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0061
0.00066
1
8260D
7/19/19 16:51
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0061
0.00059
1
8260D
7/19/19 16:51
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0061
0.00073
1
8260D
7/19/19 16:51
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0061
0.0011
1
8260D
7/19/19 16:51
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0061
0.00097
1
8260D
7/19/19 16:51
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0061
0.0012
1
8260D
7/19/19 16:51
JLB
P9G0319
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00052
1
8260D
7/19/19 16:51
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0061
0.0012
1
8260D
7/19/19 16:51
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
7/19/19 16:51
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.012
0.00066
1
8260D
7/19/19 16:51
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
7/19/19 16:51
JLB
P9G0319
Xylenes, total
BRL
mg/kg dry
0.018
0.0022
1
8260D
7/19/19 16:51
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
103 %
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
93 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-5
Attn: Darin McClure Prism Sample ID: 9070214-05
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:15
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
69.8
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.94
0.17
1
8270E
7/22/19 15:46
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.94
0.15
1
8270E
7/22/19 15:46
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.94
0.14
1
8270E
7/22/19 15:46
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.47
0.15
1
8270E
7/22/19 15:46
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.94
0.20
1
8270E
7/22/19 15:46
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.94
0.20
1
8270E
7/22/19 15:46
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.94
0.23
1
8270E
7/22/19 15:46
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.94
0.18
1
8270E
7/22/19 15:46
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.47
0.20
1
8270E
7/22/19 15:46
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
2.1
0.55
1
8270E
7/22/19 15:46
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.94
0.25
1
8270E
7/22/19 15:46
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.94
0.24
1
8270E
7/22/19 15:46
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.94
0.23
1
8270E
7/22/19 15:46
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.94
0.18
1
8270E
7/22/19 15:46
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.94
0.18
1
8270E
7/22/19 15:46
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.94
0.18
1
8270E
7/22/19 15:46
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.94
0.16
1
8270E
7/22/19 15:46
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.94
0.19
1
8270E
7/22/19 15:46
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.94
0.20
1
8270E
7/22/19 15:46
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.1
0.52
1
8270E
7/22/19 15:46
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.94
0.22
1
8270E
7/22/19 15:46
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.94
0.18
1
8270E
7/22/19 15:46
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.47
0.11
1
8270E
7/22/19 15:46
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.4
0.29
1
8270E
7/22/19 15:46
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.94
0.23
1
8270E
7/22/19 15:46
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.94
0.23
1
8270E
7/22/19 15:46
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.94
0.25
1
8270E
7/22/19 15:46
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.94
0.26
1
8270E
7/22/19 15:46
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.94
0.20
1
8270E
7/22/19 15:46
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.94
0.20
1
8270E
7/22/19 15:46
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.94
0.21
1
8270E
7/22/19 15:46
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.94
0.22
1
8270E
7/22/19 15:46
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.94
0.18
1
8270E
7/22/19 15:46
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.94
0.21
1
8270E
7/22/19 15:46
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.9
0.78
1
8270E
7/22/19 15:46
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.94
0.18
1
8270E
7/22/19 15:46
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.94
0.18
1
8270E
7/22/19 15:46
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.94
0.15
1
8270E
7/22/19 15:46
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.47
0.17
1
8270E
7/22/19 15:46
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
08/21/2019
Mid -Atlantic Associates,
Inc. - Raleigh
Project: 3021.01
Client Sample ID: SS-5
Attn: Darin McClure
Prism Sample ID: 9070214-05
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 15:15
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.94
0.21
1
8270E
7/22/19 15:46
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.47
0.16
1
8270E
7/22/19 15:46
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.94
0.21
1
8270E
7/22/19 15:46
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.94
0.27
1
8270E
7/22/19 15:46
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.94
0.25
1
8270E
7/22/19 15:46
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.94
0.24
1
8270E
7/22/19 15:46
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.94
0.23
1
8270E
7/22/19 15:46
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.94
0.23
1
8270E
7/22/19 15:46
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.47
0.24
1
8270E
7/22/19 15:46
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.94
0.24
1
8270E
7/22/19 15:46
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.94
0.28
1
8270E
7/22/19 15:46
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.94
0.21
1
8270E
7/22/19 15:46
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.94
0.21
1
8270E
7/22/19 15:46
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.94
0.32
1
8270E
7/22/19 15:46
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.94
0.15
1
8270E
7/22/19 15:46
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.94
0.17
1
8270E
7/22/19 15:46
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.94
0.20
1
8270E
7/22/19 15:46
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.94
0.19
1
8270E
7/22/19 15:46
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.47
0.20
1
8270E
7/22/19 15:46
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.94
0.22
1
8270E
7/22/19 15:46
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.94
0.26
1
8270E
7/22/19 15:46
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.4
0.60
1
8270E
7/22/19 15:46
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.94
0.24
1
8270E
7/22/19 15:46
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.94
0.15
1
8270E
7/22/19 15:46
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.94
0.22
1
8270E
7/22/19 15:46
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.47
0.090
1
8270E
7/22/19 15:46
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
76 %
39-132
2-Fluorobiphenyl
74 %
44-115
2-Fluorophenol
74 %
35-115
Nitrobenzene-d5
62 %
37-122
Phenol-d5
72 %
34-121
Terphenyl-d14
73 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.072
0.025
1
*7471B
7/31/19 12:15
MMR
P9G0500
Arsenic
2.9
mg/kg dry
1.4
0.19
1
*6010D
8/1/19 13:15
JAB
P9G0507
Barium
24
mg/kg dry
14
4.3
1
*60101)
8/1/19 13:15
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.72
0.048
1
*6010D
8/1/19 13:15
JAB
P9G0507
Chromium
15
mg/kg dry
1.4
0.11
1
*6010D
8/1/19 13:15
JAB
P9G0507
Lead
8.3
mg/kg dry
1.4
0.24
1
*6010D
8/1/19 13:15
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.4
0.39
1
*6010D
8/1/19 13:15
JAB
P9G0507
Silver
BRL
mg/kg dry
0.72
0.044
1
*6010D
8/1/19 13:15
JAB
P9G0507
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
08/21 /2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01 Client Sample ID: SS-5
Prism Sample ID: 9070214-05
Prism Work Order: 9070214
Sample Matrix: Solid Time Collected: 07/12/19 15:15
Time Submitted: 07/16/19 10:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0065
0.00079
1
8260D
7/19/19 17:21
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0065
0.00095
1
8260D
7/19/19 17:21
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0065
0.00047
1
8260D
7/19/19 17:21
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0065
0.00070
1
8260D
7/19/19 17:21
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0065
0.0012
1
8260D
7/19/19 17:21
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0065
0.0012
1
8260D
7/19/19 17:21
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0065
0.0010
1
8260D
7/19/19 17:21
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00093
1
8260D
7/19/19 17:21
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0065
0.00074
1
8260D
7/19/19 17:21
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00062
1
8260D
7/19/19 17:21
JLB
P9G0319
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0065
0.00069
1
8260D
7/19/19 17:21
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0065
0.00058
1
8260D
7/19/19 17:21
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0065
0.00072
1
8260D
7/19/19 17:21
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0065
0.00077
1
8260D
7/19/19 17:21
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0065
0.00097
1
8260D
7/19/19 17:21
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0065
0.00081
1
8260D
7/19/19 17:21
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0065
0.00081
1
8260D
7/19/19 17:21
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0065
0.00054
1
8260D
7/19/19 17:21
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0065
0.00082
1
8260D
7/19/19 17:21
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0065
0.00081
1
8260D
7/19/19 17:21
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0065
0.00087
1
8260D
7/19/19 17:21
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0065
0.00074
1
8260D
7/19/19 17:21
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0065
0.0016
1
8260D
7/19/19 17:21
JLB
P9G0319
Acetone
0.017 J
mg/kg dry
0.026
0.0017
1
8260D
7/19/19 17:21
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0065
0.0010
1
8260D
7/19/19 17:21
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0065
0.00090
1
8260D
7/19/19 17:21
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0065
0.0011
1
8260D
7/19/19 17:21
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0065
0.00062
1
8260D
7/19/19 17:21
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0065
0.00050
1
8260D
7/19/19 17:21
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.013
0.0032
1
8260D
7/19/19 17:21
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0065
0.0013
1
8260D
7/19/19 17:21
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0065
0.0010
1
8260D
7/19/19 17:21
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.013
0.0012
1
8260D
7/19/19 17:21
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0065
0.00079
1
8260D
7/19/19 17:21
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.013
0.0020
1
8260D
7/19/19 17:21
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0065
0.0010
1
8260D
7/19/19 17:21
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0065
0.00064
1
8260D
7/19/19 17:21
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0065
0.00043
1
8260D
7/19/19 17:21
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.013
0.0018
1
8260D
7/19/19 17:21
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0065
0.00097
1
8260D
7/19/19 17:21
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0065
0.00095
1
8260D
7/19/19 17:21
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0065
0.00075
1
8260D
7/19/19 17:21
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-5
Attn: Darin McClure Prism Sample ID: 9070214-05
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:15
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.013
0.0017
1
8260D
7/19/19 17:21
JLB
P9G0319
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.026
0.00045
1
8260D
7/19/19 17:21
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.026
0.0015
1
8260D
7/19/19 17:21
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.026
0.00053
1
8260D
7/19/19 17:21
JLB
P9G0319
Methylene Chloride
BRL
mg/kg dry
0.0065
0.0010
1
8260D
7/19/19 17:21
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0065
0.00091
1
8260D
7/19/19 17:21
JLB
P9G0319
Naphthalene
BRL
mg/kg dry
0.013
0.00065
1
8260D
7/19/19 17:21
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0065
0.00061
1
8260D
7/19/19 17:21
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0065
0.00094
1
8260D
7/19/19 17:21
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0065
0.00069
1
8260D
7/19/19 17:21
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0065
0.00070
1
8260D
7/19/19 17:21
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0065
0.00063
1
8260D
7/19/19 17:21
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0065
0.00077
1
8260D
7/19/19 17:21
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0065
0.0012
1
8260D
7/19/19 17:21
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0065
0.0010
1
8260D
7/19/19 17:21
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0065
0.0012
1
8260D
7/19/19 17:21
JLB
P9G0319
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0065
0.00055
1
8260D
7/19/19 17:21
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0065
0.0013
1
8260D
7/19/19 17:21
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.013
0.0017
1
8260D
7/19/19 17:21
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.013
0.00070
1
8260D
7/19/19 17:21
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.013
0.0013
1
8260D
7/19/19 17:21
JLB
P9G0319
Xylenes, total
BRL
mg/kg dry
0.019
0.0023
1
8260D
7/19/19 17:21
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
100 %
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
93 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-6
Attn: Darin McClure Prism Sample ID: 9070214-06
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:25
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
74.3
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.89
0.16
1
8270E
7/22/19 16:08
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.89
0.14
1
8270E
7/22/19 16:08
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.89
0.13
1
8270E
7/22/19 16:08
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.44
0.14
1
8270E
7/22/19 16:08
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.89
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.89
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.89
0.21
1
8270E
7/22/19 16:08
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.89
0.17
1
8270E
7/22/19 16:08
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.44
0.18
1
8270E
7/22/19 16:08
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
2.0
0.52
1
8270E
7/22/19 16:08
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.89
0.23
1
8270E
7/22/19 16:08
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.89
0.23
1
8270E
7/22/19 16:08
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.89
0.22
1
8270E
7/22/19 16:08
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.89
0.17
1
8270E
7/22/19 16:08
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.89
0.17
1
8270E
7/22/19 16:08
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.89
0.17
1
8270E
7/22/19 16:08
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.89
0.15
1
8270E
7/22/19 16:08
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.89
0.18
1
8270E
7/22/19 16:08
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.89
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.0
0.49
1
8270E
7/22/19 16:08
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.89
0.21
1
8270E
7/22/19 16:08
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.89
0.17
1
8270E
7/22/19 16:08
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.44
0.11
1
8270E
7/22/19 16:08
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.27
1
8270E
7/22/19 16:08
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.89
0.22
1
8270E
7/22/19 16:08
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.89
0.21
1
8270E
7/22/19 16:08
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.89
0.24
1
8270E
7/22/19 16:08
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.89
0.24
1
8270E
7/22/19 16:08
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.89
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.89
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.89
0.20
1
8270E
7/22/19 16:08
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.89
0.21
1
8270E
7/22/19 16:08
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.89
0.17
1
8270E
7/22/19 16:08
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.89
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.7
0.74
1
8270E
7/22/19 16:08
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.89
0.17
1
8270E
7/22/19 16:08
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.89
0.17
1
8270E
7/22/19 16:08
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.89
0.14
1
8270E
7/22/19 16:08
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.44
0.16
1
8270E
7/22/19 16:08
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
08/21/2019
Mid -Atlantic Associates,
Inc. - Raleigh
Project: 3021.01
Client Sample ID: SS-6
Attn: Darin McClure
Prism Sample ID: 9070214-06
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 15:25
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.89
0.20
1
8270E
7/22/19 16:08
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.44
0.15
1
8270E
7/22/19 16:08
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.89
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.89
0.25
1
8270E
7/22/19 16:08
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.89
0.24
1
8270E
7/22/19 16:08
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.89
0.23
1
8270E
7/22/19 16:08
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.89
0.21
1
8270E
7/22/19 16:08
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.89
0.22
1
8270E
7/22/19 16:08
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.44
0.23
1
8270E
7/22/19 16:08
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.89
0.22
1
8270E
7/22/19 16:08
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.89
0.27
1
8270E
7/22/19 16:08
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.89
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.89
0.20
1
8270E
7/22/19 16:08
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.89
0.30
1
8270E
7/22/19 16:08
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.89
0.14
1
8270E
7/22/19 16:08
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.89
0.16
1
8270E
7/22/19 16:08
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.89
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.89
0.18
1
8270E
7/22/19 16:08
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.44
0.19
1
8270E
7/22/19 16:08
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.89
0.20
1
8270E
7/22/19 16:08
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.89
0.24
1
8270E
7/22/19 16:08
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.3
0.56
1
8270E
7/22/19 16:08
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.89
0.23
1
8270E
7/22/19 16:08
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.89
0.14
1
8270E
7/22/19 16:08
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.89
0.20
1
8270E
7/22/19 16:08
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.44
0.084
1
8270E
7/22/19 16:08
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
77 %
39-132
2-Fluorobiphenyl
75 %
44-115
2-Fluorophenol
75 %
35-115
Nitrobenzene-d5
62 %
37-122
Phenol-d5
72 %
34-121
Terphenyl-d14
76 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.067
0.023
1
*7471B
7/31/19 12:20
MMR
P9G0500
Arsenic
7.5
mg/kg dry
1.3
0.18
1
*6010D
8/1/19 13:22
JAB
P9G0507
Barium
96
mg/kg dry
13
4.0
1
*60101)
8/1/19 13:22
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.67
0.045
1
*6010D
8/1/19 13:22
JAB
P9G0507
Chromium
17
mg/kg dry
1.3
0.10
1
*6010D
8/1/19 13:22
JAB
P9G0507
Lead
60
mg/kg dry
1.3
0.22
1
*6010D
8/1/19 13:22
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.3
0.37
1
*6010D
8/1/19 13:22
JAB
P9G0507
Silver
BRL
mg/kg dry
0.67
0.041
1
*6010D
8/1/19 13:22
JAB
P9G0507
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
08/21 /2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01 Client Sample ID: SS-6
Prism Sample ID: 9070214-06
Prism Work Order: 9070214
Sample Matrix: Solid Time Collected: 07/12/19 15:25
Time Submitted: 07/16/19 10:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0053
0.00065
1
8260D
7/19/19 17:51
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0053
0.00078
1
8260D
7/19/19 17:51
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0053
0.00039
1
8260D
7/19/19 17:51
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0053
0.00057
1
8260D
7/19/19 17:51
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0053
0.00096
1
8260D
7/19/19 17:51
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0053
0.00097
1
8260D
7/19/19 17:51
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0053
0.00082
1
8260D
7/19/19 17:51
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00076
1
8260D
7/19/19 17:51
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0053
0.00060
1
8260D
7/19/19 17:51
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00051
1
8260D
7/19/19 17:51
JLB
P9G0319
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0053
0.00056
1
8260D
7/19/19 17:51
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0053
0.00048
1
8260D
7/19/19 17:51
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0053
0.00059
1
8260D
7/19/19 17:51
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0053
0.00063
1
8260D
7/19/19 17:51
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0053
0.00080
1
8260D
7/19/19 17:51
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0053
0.00067
1
8260D
7/19/19 17:51
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0053
0.00066
1
8260D
7/19/19 17:51
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0053
0.00044
1
8260D
7/19/19 17:51
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0053
0.00067
1
8260D
7/19/19 17:51
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0053
0.00066
1
8260D
7/19/19 17:51
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0053
0.00071
1
8260D
7/19/19 17:51
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0053
0.00061
1
8260D
7/19/19 17:51
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0053
0.0013
1
8260D
7/19/19 17:51
JLB
P9G0319
Acetone
0.013 J
mg/kg dry
0.021
0.0014
1
8260D
7/19/19 17:51
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0053
0.00083
1
8260D
7/19/19 17:51
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0053
0.00074
1
8260D
7/19/19 17:51
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0053
0.00087
1
8260D
7/19/19 17:51
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0053
0.00050
1
8260D
7/19/19 17:51
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0053
0.00041
1
8260D
7/19/19 17:51
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.011
0.0026
1
8260D
7/19/19 17:51
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0053
0.0010
1
8260D
7/19/19 17:51
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0053
0.00083
1
8260D
7/19/19 17:51
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.011
0.0010
1
8260D
7/19/19 17:51
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0053
0.00065
1
8260D
7/19/19 17:51
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.011
0.0016
1
8260D
7/19/19 17:51
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0053
0.00084
1
8260D
7/19/19 17:51
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0053
0.00052
1
8260D
7/19/19 17:51
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0053
0.00036
1
8260D
7/19/19 17:51
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
7/19/19 17:51
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0053
0.00080
1
8260D
7/19/19 17:51
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0053
0.00078
1
8260D
7/19/19 17:51
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0053
0.00062
1
8260D
7/19/19 17:51
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-6
Attn: Darin McClure Prism Sample ID: 9070214-06
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:25
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.011
0.0014
1
8260D
7/19/19 17:51
JLB
P9G0319
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.021
0.00037
1
8260D
7/19/19 17:51
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.021
0.0012
1
8260D
7/19/19 17:51
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.021
0.00043
1
8260D
7/19/19 17:51
JLB
P9G0319
Methylene Chloride
0.0034 J
mg/kg dry
0.0053
0.00086
1
8260D
7/19/19 17:51
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0053
0.00075
1
8260D
7/19/19 17:51
JLB
P9G0319
Naphthalene
BRL
mg/kg dry
0.011
0.00054
1
8260D
7/19/19 17:51
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0053
0.00050
1
8260D
7/19/19 17:51
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0053
0.00077
1
8260D
7/19/19 17:51
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0053
0.00057
1
8260D
7/19/19 17:51
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0053
0.00057
1
8260D
7/19/19 17:51
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0053
0.00052
1
8260D
7/19/19 17:51
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0053
0.00063
1
8260D
7/19/19 17:51
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0053
0.00096
1
8260D
7/19/19 17:51
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0053
0.00085
1
8260D
7/19/19 17:51
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0053
0.0010
1
8260D
7/19/19 17:51
JLB
P9G0319
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0053
0.00045
1
8260D
7/19/19 17:51
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0053
0.0010
1
8260D
7/19/19 17:51
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0014
1
8260D
7/19/19 17:51
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.011
0.00058
1
8260D
7/19/19 17:51
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260D
7/19/19 17:51
JLB
P9G0319
Xylenes, total
BRL
mg/kg dry
0.016
0.0019
1
8260D
7/19/19 17:51
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
92 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-7
Attn: Darin McClure Prism Sample ID: 9070214-07
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:30
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
60.8
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
1.1
0.19
1
8270E
7/22/19 16:30
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
1.1
0.17
1
8270E
7/22/19 16:30
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
1.1
0.16
1
8270E
7/22/19 16:30
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.54
0.17
1
8270E
7/22/19 16:30
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
1.1
0.23
1
8270E
7/22/19 16:30
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
1.1
0.23
1
8270E
7/22/19 16:30
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
1.1
0.26
1
8270E
7/22/19 16:30
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
1.1
0.21
1
8270E
7/22/19 16:30
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.54
0.22
1
8270E
7/22/19 16:30
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
2.5
0.63
1
8270E
7/22/19 16:30
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
1.1
0.29
1
8270E
7/22/19 16:30
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
1.1
0.28
1
8270E
7/22/19 16:30
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
1.1
0.26
1
8270E
7/22/19 16:30
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
1.1
0.21
1
8270E
7/22/19 16:30
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
1.1
0.21
1
8270E
7/22/19 16:30
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
1.1
0.21
1
8270E
7/22/19 16:30
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
1.1
0.18
1
8270E
7/22/19 16:30
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
1.1
0.21
1
8270E
7/22/19 16:30
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
1.1
0.23
1
8270E
7/22/19 16:30
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.5
0.60
1
8270E
7/22/19 16:30
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
1.1
0.25
1
8270E
7/22/19 16:30
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
1.1
0.21
1
8270E
7/22/19 16:30
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.54
0.13
1
8270E
7/22/19 16:30
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.6
0.33
1
8270E
7/22/19 16:30
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
1.1
0.27
1
8270E
7/22/19 16:30
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
1.1
0.26
1
8270E
7/22/19 16:30
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
1.1
0.29
1
8270E
7/22/19 16:30
JMV
P9G0316
Anthracene
BRL
mg/kg dry
1.1
0.29
1
8270E
7/22/19 16:30
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
1.1
0.23
1
8270E
7/22/19 16:30
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
1.1
0.23
1
8270E
7/22/19 16:30
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
1.1
0.24
1
8270E
7/22/19 16:30
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
1.1
0.25
1
8270E
7/22/19 16:30
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
1.1
0.21
1
8270E
7/22/19 16:30
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
1.1
0.24
1
8270E
7/22/19 16:30
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
3.3
0.90
1
8270E
7/22/19 16:30
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
1.1
0.20
1
8270E
7/22/19 16:30
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
1.1
0.21
1
8270E
7/22/19 16:30
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
1.1
0.17
1
8270E
7/22/19 16:30
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.54
0.19
1
8270E
7/22/19 16:30
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-7
Attn: Darin McClure Prism Sample ID: 9070214-07
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:30
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
1.1
0.24
1
8270E
7/22/19 16:30
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.54
0.19
1
8270E
7/22/19 16:30
JMV
P9G0316
Chrysene
BRL
mg/kg dry
1.1
0.24
1
8270E
7/22/19 16:30
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
1.1
0.31
1
8270E
7/22/19 16:30
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
1.1
0.29
1
8270E
7/22/19 16:30
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
1.1
0.28
1
8270E
7/22/19 16:30
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
1.1
0.26
1
8270E
7/22/19 16:30
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
1.1
0.27
1
8270E
7/22/19 16:30
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.54
0.28
1
8270E
7/22/19 16:30
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
1.1
0.27
1
8270E
7/22/19 16:30
JMV
P9G0316
Fluorene
BRL
mg/kg dry
1.1
0.32
1
8270E
7/22/19 16:30
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
1.1
0.24
1
8270E
7/22/19 16:30
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
1.1
0.24
1
8270E
7/22/19 16:30
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
1.1
0.37
1
8270E
7/22/19 16:30
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
1.1
0.17
1
8270E
7/22/19 16:30
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
1.1
0.20
1
8270E
7/22/19 16:30
JMV
P9G0316
Isophorone
BRL
mg/kg dry
1.1
0.23
1
8270E
7/22/19 16:30
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
1.1
0.21
1
8270E
7/22/19 16:30
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.54
0.23
1
8270E
7/22/19 16:30
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
1.1
0.25
1
8270E
7/22/19 16:30
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
1.1
0.30
1
8270E
7/22/19 16:30
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.6
0.69
1
8270E
7/22/19 16:30
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
1.1
0.28
1
8270E
7/22/19 16:30
JMV
P9G0316
Phenol
BRL
mg/kg dry
1.1
0.18
1
8270E
7/22/19 16:30
JMV
P9G0316
Pyrene
BRL
mg/kg dry
1.1
0.25
1
8270E
7/22/19 16:30
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.54
0.10
1
8270E
7/22/19 16:30
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
74 %
39-132
2-Fluorobiphenyl
71 %
44-115
2-Fluorophenol
68 %
35-115
Nitrobenzene-d5
57 %
37-122
Phenol-d5
66 %
34-121
Terphenyl-d14
73 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.082
0.028
1
*7471B
7/31/19 12:24
MMR
P9G0500
Arsenic
13
mg/kg dry
1.6
0.22
1
*6010D
8/1/19 13:38
JAB
P9G0507
Barium
440
mg/kg dry
160
49
10
*60101)
8/1/19 13:30
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.82
0.056
1
*6010D
8/1/19 13:38
JAB
P9G0507
Chromium
23
mg/kg dry
1.6
0.12
1
*6010D
8/1/19 13:38
JAB
P9G0507
Lead
50
mg/kg dry
1.6
0.27
1
*6010D
8/1/19 13:38
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.6
0.45
1
*6010D
8/1/19 13:38
JAB
P9G0507
Silver
BRL
mg/kg dry
0.82
0.050
1
*6010D
8/1/19 13:38
JAB
P9G0507
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
08/21 /2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01 Client Sample ID: SS-7
Prism Sample ID: 9070214-07
Prism Work Order: 9070214
Sample Matrix: Solid Time Collected: 07/12/19 15:30
Time Submitted: 07/16/19 10:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0074
0.00091
1
8260D
7/19/19 18:21
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0074
0.0011
1
8260D
7/19/19 18:21
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0074
0.00054
1
8260D
7/19/19 18:21
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0074
0.00080
1
8260D
7/19/19 18:21
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0074
0.0013
1
8260D
7/19/19 18:21
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0074
0.0014
1
8260D
7/19/19 18:21
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0074
0.0011
1
8260D
7/19/19 18:21
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.015
0.0011
1
8260D
7/19/19 18:21
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0074
0.00084
1
8260D
7/19/19 18:21
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.015
0.00071
1
8260D
7/19/19 18:21
JLB
P9G0319
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0074
0.00079
1
8260D
7/19/19 18:21
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0074
0.00067
1
8260D
7/19/19 18:21
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0074
0.00083
1
8260D
7/19/19 18:21
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0074
0.00088
1
8260D
7/19/19 18:21
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0074
0.0011
1
8260D
7/19/19 18:21
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0074
0.00093
1
8260D
7/19/19 18:21
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0074
0.00092
1
8260D
7/19/19 18:21
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0074
0.00062
1
8260D
7/19/19 18:21
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0074
0.00094
1
8260D
7/19/19 18:21
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0074
0.00093
1
8260D
7/19/19 18:21
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0074
0.0010
1
8260D
7/19/19 18:21
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0074
0.00085
1
8260D
7/19/19 18:21
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0074
0.0019
1
8260D
7/19/19 18:21
JLB
P9G0319
Acetone
0.016 J
mg/kg dry
0.030
0.0019
1
8260D
7/19/19 18:21
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0074
0.0012
1
8260D
7/19/19 18:21
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0074
0.0010
1
8260D
7/19/19 18:21
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0074
0.0012
1
8260D
7/19/19 18:21
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0074
0.00071
1
8260D
7/19/19 18:21
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0074
0.00058
1
8260D
7/19/19 18:21
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.015
0.0036
1
8260D
7/19/19 18:21
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0074
0.0015
1
8260D
7/19/19 18:21
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0074
0.0012
1
8260D
7/19/19 18:21
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.015
0.0014
1
8260D
7/19/19 18:21
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0074
0.00091
1
8260D
7/19/19 18:21
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.015
0.0023
1
8260D
7/19/19 18:21
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0074
0.0012
1
8260D
7/19/19 18:21
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0074
0.00073
1
8260D
7/19/19 18:21
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0074
0.00050
1
8260D
7/19/19 18:21
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.015
0.0021
1
8260D
7/19/19 18:21
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0074
0.0011
1
8260D
7/19/19 18:21
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0074
0.0011
1
8260D
7/19/19 18:21
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0074
0.00087
1
8260D
7/19/19 18:21
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-7
Attn: Darin McClure Prism Sample ID: 9070214-07
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:30
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.015
0.0019
1
8260D
7/19/19 18:21
JLB
P9G0319
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.030
0.00051
1
8260D
7/19/19 18:21
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.030
0.0017
1
8260D
7/19/19 18:21
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.030
0.00061
1
8260D
7/19/19 18:21
JLB
P9G0319
Methylene Chloride
BRL
mg/kg dry
0.0074
0.0012
1
8260D
7/19/19 18:21
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0074
0.0010
1
8260D
7/19/19 18:21
JLB
P9G0319
Naphthalene
BRL
mg/kg dry
0.015
0.00075
1
8260D
7/19/19 18:21
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0074
0.00070
1
8260D
7/19/19 18:21
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0074
0.0011
1
8260D
7/19/19 18:21
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0074
0.00079
1
8260D
7/19/19 18:21
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0074
0.00080
1
8260D
7/19/19 18:21
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0074
0.00072
1
8260D
7/19/19 18:21
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0074
0.00088
1
8260D
7/19/19 18:21
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0074
0.0013
1
8260D
7/19/19 18:21
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0074
0.0012
1
8260D
7/19/19 18:21
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0074
0.0014
1
8260D
7/19/19 18:21
JLB
P9G0319
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0074
0.00064
1
8260D
7/19/19 18:21
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0074
0.0014
1
8260D
7/19/19 18:21
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.015
0.0020
1
8260D
7/19/19 18:21
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.015
0.00081
1
8260D
7/19/19 18:21
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.015
0.0015
1
8260D
7/19/19 18:21
JLB
P9G0319
Xylenes, total
BRL
mg/kg dry
0.022
0.0027
1
8260D
7/19/19 18:21
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
105 %
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
93 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-8
Attn: Darin McClure Prism Sample ID: 9070214-08
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:40
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
76.5
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.86
0.15
1
8270E
7/22/19 16:53
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.86
0.14
1
8270E
7/22/19 16:53
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.86
0.13
1
8270E
7/22/19 16:53
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.14
1
8270E
7/22/19 16:53
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.86
0.18
1
8270E
7/22/19 16:53
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.86
0.18
1
8270E
7/22/19 16:53
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.86
0.21
1
8270E
7/22/19 16:53
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.86
0.17
1
8270E
7/22/19 16:53
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.43
0.18
1
8270E
7/22/19 16:53
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
2.0
0.50
1
8270E
7/22/19 16:53
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.86
0.23
1
8270E
7/22/19 16:53
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.86
0.22
1
8270E
7/22/19 16:53
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.86
0.21
1
8270E
7/22/19 16:53
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.86
0.16
1
8270E
7/22/19 16:53
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.86
0.17
1
8270E
7/22/19 16:53
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.86
0.16
1
8270E
7/22/19 16:53
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.86
0.14
1
8270E
7/22/19 16:53
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.86
0.17
1
8270E
7/22/19 16:53
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.86
0.19
1
8270E
7/22/19 16:53
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.0
0.47
1
8270E
7/22/19 16:53
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.86
0.20
1
8270E
7/22/19 16:53
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.86
0.16
1
8270E
7/22/19 16:53
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
8270E
7/22/19 16:53
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
8270E
7/22/19 16:53
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.86
0.21
1
8270E
7/22/19 16:53
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.86
0.21
1
8270E
7/22/19 16:53
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.86
0.23
1
8270E
7/22/19 16:53
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.86
0.23
1
8270E
7/22/19 16:53
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.86
0.18
1
8270E
7/22/19 16:53
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.86
0.18
1
8270E
7/22/19 16:53
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.86
0.19
1
8270E
7/22/19 16:53
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.86
0.20
1
8270E
7/22/19 16:53
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.86
0.17
1
8270E
7/22/19 16:53
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.86
0.19
1
8270E
7/22/19 16:53
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.6
0.71
1
8270E
7/22/19 16:53
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.86
0.16
1
8270E
7/22/19 16:53
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.86
0.16
1
8270E
7/22/19 16:53
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.86
0.14
1
8270E
7/22/19 16:53
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
8270E
7/22/19 16:53
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
` Full -Service Analytical &
P R S M
/ Environmental Solutions
LABORATORIES INC.
08/21/2019
Mid -Atlantic Associates, Inc. - Raleigh
Project: 3021.01
Client Sample ID: SS-8
Attn: Darin McClure
Prism Sample ID: 9070214-08
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 15:40
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.86
0.19
1
8270E
7/22/19 16:53
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
8270E
7/22/19 16:53
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.86
0.19
1
8270E
7/22/19 16:53
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.86
0.25
1
8270E
7/22/19 16:53
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.86
0.23
1
8270E
7/22/19 16:53
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.86
0.22
1
8270E
7/22/19 16:53
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.86
0.21
1
8270E
7/22/19 16:53
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.86
0.21
1
8270E
7/22/19 16:53
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
8270E
7/22/19 16:53
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.86
0.22
1
8270E
7/22/19 16:53
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.86
0.26
1
8270E
7/22/19 16:53
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.86
0.19
1
8270E
7/22/19 16:53
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.86
0.19
1
8270E
7/22/19 16:53
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.86
0.30
1
8270E
7/22/19 16:53
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.86
0.14
1
8270E
7/22/19 16:53
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.86
0.16
1
8270E
7/22/19 16:53
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.86
0.19
1
8270E
7/22/19 16:53
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.86
0.17
1
8270E
7/22/19 16:53
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
8270E
7/22/19 16:53
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.86
0.20
1
8270E
7/22/19 16:53
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.86
0.24
1
8270E
7/22/19 16:53
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.3
0.55
1
8270E
7/22/19 16:53
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.86
0.22
1
8270E
7/22/19 16:53
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.86
0.14
1
8270E
7/22/19 16:53
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.86
0.20
1
8270E
7/22/19 16:53
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.43
0.082
1
8270E
7/22/19 16:53
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
65 %
39-132
2-Fluorobiphenyl
65 %
44-115
2-Fluorophenol
66 %
35-115
Nitrobenzene-d5
54 %
37-122
Phenol-d5
64 %
34-121
Terphenyl-d14
66 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.065
0.023
1
*7471B
7/31/19 12:29
MMR
P9G0500
Arsenic
BRL
mg/kg dry
1.3
0.17
1
*6010D
8/1/19 13:46
JAB
P9G0507
Barium
25
mg/kg dry
13
3.9
1
*6010D
8/1119 13:46
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.65
0.044
1
*6010D
8/1/19 13:46
JAB
P9G0507
Chromium
6.5
mg/kg dry
1.3
0.099
1
*60101)
8/1/19 13:46
JAB
P9G0507
Lead
5.1
mg/kg dry
1.3
0.22
1
*60101)
8/1/19 13:46
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.3
0.36
1
*6010D
8/1/19 13:46
JAB
P9G0507
Silver
BRL
mg/kg dry
0.65
0.040
1
*6010D
8/1/19 13:46
JAB
P9G0507
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

` Full -Service Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01
Sample Matrix: Solid
Laboratory Report
08/21/2019
Client Sample ID: SS-8
Prism Sample ID: 9070214-08
Prism Work Order: 9070214
Time Collected: 07/12/19 15:40
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0058
0.00070
1
8260D
7/19/19 18:51
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0058
0.00085
1
8260D
7/19/19 18:51
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0058
0.00042
1
8260D
7/19/19 18:51
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0058
0.00062
1
8260D
7/19/19 18:51
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0058
0.0010
1
8260D
7/19/19 18:51
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260D
7/19/19 18:51
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0058
0.00089
1
8260D
7/19/19 18:51
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00083
1
8260D
7/19/19 18:51
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0058
0.00065
1
8260D
7/19/19 18:51
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00055
1
8260D
7/19/19 18:51
JLB
P9G0319
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0058
0.00061
1
8260D
7/19/19 18:51
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0058
0.00052
1
8260D
7/19/19 18:51
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0058
0.00064
1
8260D
7/19/19 18:51
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0058
0.00069
1
8260D
7/19/19 18:51
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0058
0.00087
1
8260D
7/19/19 18:51
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0058
0.00072
1
8260D
7/19/19 18:51
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0058
0.00072
1
8260D
7/19/19 18:51
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0058
0.00048
1
8260D
7/19/19 18:51
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0058
0.00073
1
8260D
7/19/19 18:51
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0058
0.00072
1
8260D
7/19/19 18:51
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0058
0.00077
1
8260D
7/19/19 18:51
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0058
0.00066
1
8260D
7/19/19 18:51
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0058
0.0015
1
8260D
7/19/19 18:51
JLB
P9G0319
Acetone
0.019
J mg/kg dry
0.023
0.0015
1
8260D
7/19/19 18:51
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0058
0.00090
1
8260D
7/19/19 18:51
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0058
0.00080
1
8260D
7/19/19 18:51
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0058
0.00095
1
8260D
7/19/19 18:51
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0058
0.00055
1
8260D
7/19/19 18:51
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0058
0.00045
1
8260D
7/19/19 18:51
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.012
0.0028
1
8260D
7/19/19 18:51
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0058
0.0011
1
8260D
7/19/19 18:51
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0058
0.00090
1
8260D
7/19/19 18:51
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.012
0.0011
1
8260D
7/19/19 18:51
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0058
0.00071
1
8260D
7/19/19 18:51
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
8260D
7/19/19 18:51
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0058
0.00091
1
8260D
7/19/19 18:51
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0058
0.00057
1
8260D
7/19/19 18:51
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0058
0.00039
1
8260D
7/19/19 18:51
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
7/19/19 18:51
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0058
0.00087
1
8260D
7/19/19 18:51
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0058
0.00085
1
8260D
7/19/19 18:51
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0058
0.00067
1
8260D
7/19/19 18:51
JLB
P9G0319
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0015
1
8260D
7/19/19 18:51
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-8
Attn: Darin McClure Prism Sample ID: 9070214-08
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:40
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.023
0.00040
1
8260D
7/19/19 18:51
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.023
0.0013
1
8260D
7/19/19 18:51
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.023
0.00047
1
8260D
7/19/19 18:51
JLB
P9G0319
Methylene Chloride
BRL
mg/kg dry
0.0058
0.00093
1
8260D
7/19/19 18:51
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0058
0.00081
1
8260D
7/19/19 18:51
JLB
P9G0319
Naphthalene
BRL
mg/kg dry
0.012
0.00058
1
8260D
7/19/19 18:51
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0058
0.00054
1
8260D
7/19/19 18:51
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0058
0.00084
1
8260D
7/19/19 18:51
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0058
0.00061
1
8260D
7/19/19 18:51
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0058
0.00062
1
8260D
7/19/19 18:51
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0058
0.00056
1
8260D
7/19/19 18:51
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0058
0.00068
1
8260D
7/19/19 18:51
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0058
0.0010
1
8260D
7/19/19 18:51
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0058
0.00092
1
8260D
7/19/19 18:51
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260D
7/19/19 18:51
JLB
P9G0319
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0058
0.00049
1
8260D
7/19/19 18:51
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260D
7/19/19 18:51
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
7/19/19 18:51
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.012
0.00062
1
8260D
7/19/19 18:51
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.012
0.0011
1
8260D
7/19/19 18:51
JLB
P9G0319
Xylenes, total
BRL
mg/kg dry
0.017
0.0021
1
8260D
7/19/19 18:51
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
103 %
70-130
Dibromofluoromethane
107 %
84-123
Toluene-d8
91 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-9
Attn: Darin McClure Prism Sample ID: 9070214-09
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:50
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
84.5
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.78
0.14
1
8270E
7/22/19 17:15
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.78
0.13
1
8270E
7/22/19 17:15
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.78
0.11
1
8270E
7/22/19 17:15
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.39
0.12
1
8270E
7/22/19 17:15
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.78
0.19
1
8270E
7/22/19 17:15
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.39
0.16
1
8270E
7/22/19 17:15
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
1.8
0.46
1
8270E
7/22/19 17:15
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.78
0.21
1
8270E
7/22/19 17:15
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.78
0.20
1
8270E
7/22/19 17:15
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.78
0.19
1
8270E
7/22/19 17:15
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.78
0.13
1
8270E
7/22/19 17:15
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.8
0.43
1
8270E
7/22/19 17:15
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.78
0.18
1
8270E
7/22/19 17:15
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.39
0.094
1
8270E
7/22/19 17:15
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.24
1
8270E
7/22/19 17:15
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.78
0.19
1
8270E
7/22/19 17:15
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.78
0.19
1
8270E
7/22/19 17:15
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.78
0.21
1
8270E
7/22/19 17:15
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.78
0.21
1
8270E
7/22/19 17:15
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.78
0.18
1
8270E
7/22/19 17:15
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.4
0.65
1
8270E
7/22/19 17:15
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.78
0.13
1
8270E
7/22/19 17:15
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.39
0.14
1
8270E
7/22/19 17:15
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
08/21/2019
Mid -Atlantic Associates,
Inc. - Raleigh
Project: 3021.01
Client Sample ID: SS-9
Attn: Darin McClure
Prism Sample ID: 9070214-09
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 15:50
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.78
0.18
1
8270E
7/22/19 17:15
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.39
0.13
1
8270E
7/22/19 17:15
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.78
0.22
1
8270E
7/22/19 17:15
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.78
0.21
1
8270E
7/22/19 17:15
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.78
0.20
1
8270E
7/22/19 17:15
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.78
0.19
1
8270E
7/22/19 17:15
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.78
0.19
1
8270E
7/22/19 17:15
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.39
0.20
1
8270E
7/22/19 17:15
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.78
0.20
1
8270E
7/22/19 17:15
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.78
0.23
1
8270E
7/22/19 17:15
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.78
0.18
1
8270E
7/22/19 17:15
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.78
0.27
1
8270E
7/22/19 17:15
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.78
0.12
1
8270E
7/22/19 17:15
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.78
0.14
1
8270E
7/22/19 17:15
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.78
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.78
0.15
1
8270E
7/22/19 17:15
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.39
0.17
1
8270E
7/22/19 17:15
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.78
0.18
1
8270E
7/22/19 17:15
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.78
0.21
1
8270E
7/22/19 17:15
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.2
0.50
1
8270E
7/22/19 17:15
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.78
0.20
1
8270E
7/22/19 17:15
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.78
0.13
1
8270E
7/22/19 17:15
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.78
0.18
1
8270E
7/22/19 17:15
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.39
0.074
1
8270E
7/22/19 17:15
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
84 %
39-132
2-Fluorobiphenyl
79 %
44-115
2-Fluorophenol
79 %
35-115
Nitrobenzene-d5
66 %
37-122
Phenol-d5
77 %
34-121
Terphenyl-d14
84 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.059
0.020
1
*7471B
7/31/19 12:33
MMR
P9G0500
Arsenic
4.3
mg/kg dry
1.2
0.16
1
*6010D
8/1/19 14:16
JAB
P9G0507
Barium
620
mg/kg dry
120
35
10
*60101)
8/1/19 14:08
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.59
0.040
1
*6010D
8/1/19 14:16
JAB
P9G0507
Chromium
18
mg/kg dry
1.2
0.090
1
*6010D
8/1/19 14:16
JAB
P9G0507
Lead
15
mg/kg dry
1.2
0.20
1
*6010D
8/1/19 14:16
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.2
0.33
1
*6010D
8/1/19 14:16
JAB
P9G0507
Silver
BRL
mg/kg dry
0.59
0.036
1
*6010D
8/1/19 14:16
JAB
P9G0507
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
08/21 /2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01 Client Sample ID: SS-9
Prism Sample ID: 9070214-09
Prism Work Order: 9070214
Sample Matrix: Solid Time Collected: 07/12/19 15:50
Time Submitted: 07/16/19 10:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0059
0.00072
1
8260D
7/19/19 19:20
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0059
0.00086
1
8260D
7/19/19 19:20
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0059
0.00043
1
8260D
7/19/19 19:20
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0059
0.00063
1
8260D
7/19/19 19:20
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 19:20
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 19:20
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0059
0.00090
1
8260D
7/19/19 19:20
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00084
1
8260D
7/19/19 19:20
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0059
0.00067
1
8260D
7/19/19 19:20
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00056
1
8260D
7/19/19 19:20
JLB
P9G0319
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0059
0.00062
1
8260D
7/19/19 19:20
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0059
0.00053
1
8260D
7/19/19 19:20
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0059
0.00065
1
8260D
7/19/19 19:20
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0059
0.00070
1
8260D
7/19/19 19:20
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0059
0.00088
1
8260D
7/19/19 19:20
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0059
0.00074
1
8260D
7/19/19 19:20
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0059
0.00073
1
8260D
7/19/19 19:20
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0059
0.00049
1
8260D
7/19/19 19:20
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0059
0.00074
1
8260D
7/19/19 19:20
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0059
0.00073
1
8260D
7/19/19 19:20
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0059
0.00079
1
8260D
7/19/19 19:20
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0059
0.00067
1
8260D
7/19/19 19:20
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0059
0.0015
1
8260D
7/19/19 19:20
JLB
P9G0319
Acetone
BRL
mg/kg dry
0.023
0.0015
1
8260D
7/19/19 19:20
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0059
0.00092
1
8260D
7/19/19 19:20
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0059
0.00081
1
8260D
7/19/19 19:20
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0059
0.00096
1
8260D
7/19/19 19:20
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0059
0.00056
1
8260D
7/19/19 19:20
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0059
0.00045
1
8260D
7/19/19 19:20
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.012
0.0029
1
8260D
7/19/19 19:20
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0059
0.0012
1
8260D
7/19/19 19:20
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0059
0.00092
1
8260D
7/19/19 19:20
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.012
0.0011
1
8260D
7/19/19 19:20
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0059
0.00072
1
8260D
7/19/19 19:20
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
8260D
7/19/19 19:20
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0059
0.00092
1
8260D
7/19/19 19:20
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0059
0.00058
1
8260D
7/19/19 19:20
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0059
0.00039
1
8260D
7/19/19 19:20
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
7/19/19 19:20
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0059
0.00088
1
8260D
7/19/19 19:20
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0059
0.00086
1
8260D
7/19/19 19:20
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0059
0.00068
1
8260D
7/19/19 19:20
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-9
Attn: Darin McClure Prism Sample ID: 9070214-09
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:50
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0015
1
8260D
7/19/19 19:20
JLB
P9G0319
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.023
0.00041
1
8260D
7/19/19 19:20
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.023
0.0014
1
8260D
7/19/19 19:20
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.023
0.00048
1
8260D
7/19/19 19:20
JLB
P9G0319
Methylene Chloride
BRL
mg/kg dry
0.0059
0.00095
1
8260D
7/19/19 19:20
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0059
0.00082
1
8260D
7/19/19 19:20
JLB
P9G0319
Naphthalene
BRL
mg/kg dry
0.012
0.00059
1
8260D
7/19/19 19:20
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0059
0.00055
1
8260D
7/19/19 19:20
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0059
0.00085
1
8260D
7/19/19 19:20
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0059
0.00062
1
8260D
7/19/19 19:20
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0059
0.00063
1
8260D
7/19/19 19:20
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0059
0.00057
1
8260D
7/19/19 19:20
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0059
0.00070
1
8260D
7/19/19 19:20
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 19:20
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0059
0.00093
1
8260D
7/19/19 19:20
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 19:20
JLB
P9G0319
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0059
0.00050
1
8260D
7/19/19 19:20
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 19:20
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
7/19/19 19:20
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.012
0.00064
1
8260D
7/19/19 19:20
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
7/19/19 19:20
JLB
P9G0319
Xylenes, total
BRL
mg/kg dry
0.018
0.0021
1
8260D
7/19/19 19:20
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
100 %
70-130
Dibromofluoromethane
107 %
84-123
Toluene-d8
92 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-10
Attn: Darin McClure Prism Sample ID: 9070214-10
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 16:00
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
68.2
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.97
0.17
1
8270E
7/22/19 17:37
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 17:37
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.97
0.14
1
8270E
7/22/19 17:37
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.48
0.15
1
8270E
7/22/19 17:37
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.97
0.20
1
8270E
7/22/19 17:37
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.97
0.20
1
8270E
7/22/19 17:37
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 17:37
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 17:37
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.48
0.20
1
8270E
7/22/19 17:37
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
2.2
0.57
1
8270E
7/22/19 17:37
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 17:37
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.97
0.25
1
8270E
7/22/19 17:37
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 17:37
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 17:37
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 17:37
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 17:37
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 17:37
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 17:37
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 17:37
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.2
0.53
1
8270E
7/22/19 17:37
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 17:37
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 17:37
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.48
0.12
1
8270E
7/22/19 17:37
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.5
0.30
1
8270E
7/22/19 17:37
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 17:37
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 17:37
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 17:37
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 17:37
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 17:37
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 17:37
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 17:37
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 17:37
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 17:37
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 17:37
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.9
0.80
1
8270E
7/22/19 17:37
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 17:37
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 17:37
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 17:37
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.48
0.17
1
8270E
7/22/19 17:37
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
08/21/2019
Mid -Atlantic Associates,
Inc. - Raleigh
Project: 3021.01
Client Sample ID: SS-10
Attn: Darin McClure
Prism Sample ID: 9070214-10
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 16:00
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 17:37
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.48
0.17
1
8270E
7/22/19 17:37
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 17:37
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.97
0.28
1
8270E
7/22/19 17:37
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 17:37
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.97
0.25
1
8270E
7/22/19 17:37
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.97
0.23
1
8270E
7/22/19 17:37
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 17:37
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.48
0.25
1
8270E
7/22/19 17:37
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.97
0.24
1
8270E
7/22/19 17:37
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.97
0.29
1
8270E
7/22/19 17:37
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 17:37
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 17:37
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.97
0.33
1
8270E
7/22/19 17:37
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.97
0.15
1
8270E
7/22/19 17:37
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.97
0.18
1
8270E
7/22/19 17:37
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.97
0.21
1
8270E
7/22/19 17:37
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.97
0.19
1
8270E
7/22/19 17:37
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.48
0.20
1
8270E
7/22/19 17:37
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 17:37
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.97
0.26
1
8270E
7/22/19 17:37
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.5
0.62
1
8270E
7/22/19 17:37
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.97
0.25
1
8270E
7/22/19 17:37
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.97
0.16
1
8270E
7/22/19 17:37
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.97
0.22
1
8270E
7/22/19 17:37
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.48
0.092
1
8270E
7/22/19 17:37
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
80 %
39-132
2-Fluorobiphenyl
74 %
44-115
2-Fluorophenol
76 %
35-115
Nitrobenzene-d5
60 %
37-122
Phenol-d5
73 %
34-121
Terphenyl-d14
78 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.073
0.025
1
*7471B
7/31/19 12:47
MMR
P9G0500
Arsenic
3.2
mg/kg dry
1.5
0.19
1
*6010D
8/1/19 14:25
JAB
P9G0507
Barium
92
mg/kg dry
15
4.4
1
*60101)
8/1/19 14:25
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.73
0.050
1
*6010D
8/1/19 14:25
JAB
P9G0507
Chromium
17
mg/kg dry
1.5
0.11
1
*6010D
8/1/19 14:25
JAB
P9G0507
Lead
38
mg/kg dry
1.5
0.24
1
*6010D
8/1/19 14:25
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.5
0.40
1
*6010D
8/1/19 14:25
JAB
P9G0507
Silver
BRL
mg/kg dry
0.73
0.045
1
*6010D
8/1/19 14:25
JAB
P9G0507
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
08/21 /2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01 Client Sample ID: SS-10
Prism Sample ID: 9070214-10
Prism Work Order: 9070214
Sample Matrix: Solid Time Collected: 07/12/19 16:00
Time Submitted: 07/16/19 10:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0066
0.00080
1
8260D
7/19/19 19:51
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0066
0.00097
1
8260D
7/19/19 19:51
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0066
0.00048
1
8260D
7/19/19 19:51
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0066
0.00071
1
8260D
7/19/19 19:51
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0066
0.0012
1
8260D
7/19/19 19:51
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0066
0.0012
1
8260D
7/19/19 19:51
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0066
0.0010
1
8260D
7/19/19 19:51
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00094
1
8260D
7/19/19 19:51
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0066
0.00075
1
8260D
7/19/19 19:51
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00063
1
8260D
7/19/19 19:51
JLB
P9G0319
1,2,4-Trimethyl benzene 0.0031
J
mg/kg dry
0.0066
0.00070
1
8260D
7/19/19 19:51
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0066
0.00059
1
8260D
7/19/19 19:51
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0066
0.00073
1
8260D
7/19/19 19:51
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0066
0.00078
1
8260D
7/19/19 19:51
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0066
0.00099
1
8260D
7/19/19 19:51
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0066
0.00082
1
8260D
7/19/19 19:51
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0066
0.00082
1
8260D
7/19/19 19:51
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0066
0.00055
1
8260D
7/19/19 19:51
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0066
0.00083
1
8260D
7/19/19 19:51
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0066
0.00082
1
8260D
7/19/19 19:51
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0066
0.00088
1
8260D
7/19/19 19:51
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0066
0.00075
1
8260D
7/19/19 19:51
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0066
0.0017
1
8260D
7/19/19 19:51
JLB
P9G0319
Acetone
BRL
mg/kg dry
0.026
0.0017
1
8260D
7/19/19 19:51
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0066
0.0010
1
8260D
7/19/19 19:51
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0066
0.00091
1
8260D
7/19/19 19:51
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0066
0.0011
1
8260D
7/19/19 19:51
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0066
0.00062
1
8260D
7/19/19 19:51
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0066
0.00051
1
8260D
7/19/19 19:51
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.013
0.0032
1
8260D
7/19/19 19:51
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0066
0.0013
1
8260D
7/19/19 19:51
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0066
0.0010
1
8260D
7/19/19 19:51
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.013
0.0013
1
8260D
7/19/19 19:51
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0066
0.00080
1
8260D
7/19/19 19:51
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.013
0.0020
1
8260D
7/19/19 19:51
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0066
0.0010
1
8260D
7/19/19 19:51
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0066
0.00065
1
8260D
7/19/19 19:51
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0066
0.00044
1
8260D
7/19/19 19:51
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.013
0.0019
1
8260D
7/19/19 19:51
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0066
0.00099
1
8260D
7/19/19 19:51
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0066
0.00096
1
8260D
7/19/19 19:51
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0066
0.00076
1
8260D
7/19/19 19:51
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: SS-10
Attn: Darin McClure Prism Sample ID: 9070214-10
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 16:00
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
0.0032 J
mg/kg dry
0.013
0.0017
1
8260D
7/19/19 19:51
JLB
P9G0319
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.026
0.00045
1
8260D
7/19/19 19:51
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.026
0.0015
1
8260D
7/19/19 19:51
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.026
0.00054
1
8260D
7/19/19 19:51
JLB
P9G0319
Methylene Chloride
0.0037 J
mg/kg dry
0.0066
0.0011
1
8260D
7119/19 19:51
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0066
0.00092
1
8260D
7/19/19 19:51
JLB
P9G0319
Naphthalene
BRL
mg/kg dry
0.013
0.00066
1
8260D
7/19/19 19:51
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0066
0.00061
1
8260D
7/19/19 19:51
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0066
0.00095
1
8260D
7/19/19 19:51
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0066
0.00070
1
8260D
7/19/19 19:51
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0066
0.00071
1
8260D
7/19/19 19:51
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0066
0.00064
1
8260D
7/19/19 19:51
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0066
0.00078
1
8260D
7/19/19 19:51
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0066
0.0012
1
8260D
7/19/19 19:51
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0066
0.0010
1
8260D
7/19/19 19:51
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0066
0.0013
1
8260D
7/19/19 19:51
JLB
P9G0319
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0066
0.00056
1
8260D
7/19/19 19:51
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0066
0.0013
1
8260D
7/19/19 19:51
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.013
0.0018
1
8260D
7/19/19 19:51
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.013
0.00071
1
8260D
7/19/19 19:51
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.013
0.0013
1
8260D
7/19/19 19:51
JLB
P9G0319
Xylenes, total
0.0032 J
mg/kg dry
0.020
0.0024
1
8260D
7/19/19 19:51
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
103 %
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
91 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: Duplicate
Attn: Darin McClure Prism Sample ID: 9070214-11
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:55
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
87.6
% by
0.100
0.100
1
*SM2540 G
7/25/19 9:49
KBS
P9G0396
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.75
0.13
1
8270E
7/22/19 17:59
JMV
P9G0316
1,2-Dichlorobenzene
BRL
mg/kg dry
0.75
0.12
1
8270E
7/22/19 17:59
JMV
P9G0316
1,3-Dichlorobenzene
BRL
mg/kg dry
0.75
0.11
1
8270E
7/22/19 17:59
JMV
P9G0316
1,4-Dichlorobenzene
BRL
mg/kg dry
0.38
0.12
1
8270E
7/22/19 17:59
JMV
P9G0316
1-Methyl naphthalene
BRL
mg/kg dry
0.75
0.16
1
8270E
7/22/19 17:59
JMV
P9G0316
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.75
0.16
1
8270E
7/22/19 17:59
JMV
P9G0316
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.75
0.18
1
8270E
7/22/19 17:59
JMV
P9G0316
2,4-Dichlorophenol
BRL
mg/kg dry
0.75
0.15
1
8270E
7/22/19 17:59
JMV
P9G0316
2,4-Dimethyl phenol
BRL
mg/kg dry
0.38
0.16
1
8270E
7/22/19 17:59
JMV
P9G0316
2,4-Dinitrophenol
BRL
mg/kg dry
1.7
0.44
1
8270E
7/22/19 17:59
JMV
P9G0316
2,4-Dinitrotoluene
BRL
mg/kg dry
0.75
0.20
1
8270E
7/22/19 17:59
JMV
P9G0316
2,6-Dinitrotoluene
BRL
mg/kg dry
0.75
0.20
1
8270E
7/22/19 17:59
JMV
P9G0316
2-Chloronaphthalene
BRL
mg/kg dry
0.75
0.18
1
8270E
7/22/19 17:59
JMV
P9G0316
2-Chlorophenol
BRL
mg/kg dry
0.75
0.14
1
8270E
7/22/19 17:59
JMV
P9G0316
2-Methyl naphthalene
BRL
mg/kg dry
0.75
0.15
1
8270E
7/22/19 17:59
JMV
P9G0316
2-Methylphenol
BRL
mg/kg dry
0.75
0.14
1
8270E
7/22/19 17:59
JMV
P9G0316
2-Nitrophenol
BRL
mg/kg dry
0.75
0.13
1
8270E
7/22/19 17:59
JMV
P9G0316
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.75
0.15
1
8270E
7/22/19 17:59
JMV
P9G0316
3/4-Methyl phenol
BRL
mg/kg dry
0.75
0.16
1
8270E
7/22/19 17:59
JMV
P9G0316
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.7
0.42
1
8270E
7/22/19 17:59
JMV
P9G0316
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.75
0.18
1
8270E
7/22/19 17:59
JMV
P9G0316
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.75
0.14
1
8270E
7/22/19 17:59
JMV
P9G0316
4-Chloroaniline
BRL
mg/kg dry
0.38
0.091
1
8270E
7/22/19 17:59
JMV
P9G0316
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.1
0.23
1
8270E
7/22/19 17:59
JMV
P9G0316
4-Nitrophenol
BRL
mg/kg dry
0.75
0.19
1
8270E
7/22/19 17:59
JMV
P9G0316
Acenaphthene
BRL
mg/kg dry
0.75
0.18
1
8270E
7/22/19 17:59
JMV
P9G0316
Acenaphthylene
BRL
mg/kg dry
0.75
0.20
1
8270E
7/22/19 17:59
JMV
P9G0316
Anthracene
BRL
mg/kg dry
0.75
0.20
1
8270E
7/22/19 17:59
JMV
P9G0316
Azobenzene
BRL
mg/kg dry
0.75
0.16
1
8270E
7/22/19 17:59
JMV
P9G0316
Benzo(a)anthracene
BRL
mg/kg dry
0.75
0.16
1
8270E
7/22/19 17:59
JMV
P9G0316
Benzo(a)pyrene
BRL
mg/kg dry
0.75
0.17
1
8270E
7/22/19 17:59
JMV
P9G0316
Benzo(b)fluoranthene
BRL
mg/kg dry
0.75
0.18
1
8270E
7/22/19 17:59
JMV
P9G0316
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.75
0.15
1
8270E
7/22/19 17:59
JMV
P9G0316
Benzo(k)fluoranthene
BRL
mg/kg dry
0.75
0.16
1
8270E
7/22/19 17:59
JMV
P9G0316
Benzoic Acid
BRL
mg/kg dry
2.3
0.63
1
8270E
7/22/19 17:59
JMV
P9G0316
Benzyl alcohol
BRL
mg/kg dry
0.75
0.14
1
8270E
7/22/19 17:59
JMV
P9G0316
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.75
0.14
1
8270E
7/22/19 17:59
JMV
P9G0316
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.75
0.12
1
8270E
7/22/19 17:59
JMV
P9G0316
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.38
0.13
1
8270E
7/22/19 17:59
JMV
P9G0316
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
`
P R S M
Full -Service Analytical &
/ LABORATORIES INC.
Environmental Solutions
08/21/2019
Mid -Atlantic Associates,
Inc. - Raleigh
Project: 3021.01
Client Sample ID: Duplicate
Attn: Darin McClure
Prism Sample ID: 9070214-11
409 Rogers View Court
Prism Work Order:
9070214
Raleigh, NC 27610
Sample Matrix: Solid
Time Collected:
07/12/19 15:55
Time Submitted:
07/16/19 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.75
0.17
1
8270E
7/22/19 17:59
JMV
P9G0316
Butyl benzyl phthalate
BRL
mg/kg dry
0.38
0.13
1
8270E
7/22/19 17:59
JMV
P9G0316
Chrysene
BRL
mg/kg dry
0.75
0.17
1
8270E
7/22/19 17:59
JMV
P9G0316
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.75
0.22
1
8270E
7/22/19 17:59
JMV
P9G0316
Dibenzofuran
BRL
mg/kg dry
0.75
0.20
1
8270E
7/22/19 17:59
JMV
P9G0316
Diethyl phthalate
BRL
mg/kg dry
0.75
0.19
1
8270E
7/22/19 17:59
JMV
P9G0316
Dimethyl phthalate
BRL
mg/kg dry
0.75
0.18
1
8270E
7/22/19 17:59
JMV
P9G0316
Di-n-butyl phthalate
BRL
mg/kg dry
0.75
0.19
1
8270E
7/22/19 17:59
JMV
P9G0316
Di-n-octyl phthalate
BRL
mg/kg dry
0.38
0.20
1
8270E
7/22/19 17:59
JMV
P9G0316
Fluoranthene
BRL
mg/kg dry
0.75
0.19
1
8270E
7/22/19 17:59
JMV
P9G0316
Fluorene
BRL
mg/kg dry
0.75
0.23
1
8270E
7/22/19 17:59
JMV
P9G0316
Hexachlorobenzene
BRL
mg/kg dry
0.75
0.17
1
8270E
7/22/19 17:59
JMV
P9G0316
Hexachlorobutadiene
BRL
mg/kg dry
0.75
0.17
1
8270E
7/22/19 17:59
JMV
P9G0316
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.75
0.26
1
8270E
7/22/19 17:59
JMV
P9G0316
Hexachloroethane
BRL
mg/kg dry
0.75
0.12
1
8270E
7/22/19 17:59
JMV
P9G0316
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.75
0.14
1
8270E
7/22/19 17:59
JMV
P9G0316
Isophorone
BRL
mg/kg dry
0.75
0.16
1
8270E
7/22/19 17:59
JMV
P9G0316
Naphthalene
BRL
mg/kg dry
0.75
0.15
1
8270E
7/22/19 17:59
JMV
P9G0316
Nitrobenzene
BRL
mg/kg dry
0.38
0.16
1
8270E
7/22/19 17:59
JMV
P9G0316
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.75
0.17
1
8270E
7/22/19 17:59
JMV
P9G0316
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.75
0.21
1
8270E
7/22/19 17:59
JMV
P9G0316
Pentachlorophenol
BRL
mg/kg dry
1.1
0.48
1
8270E
7/22/19 17:59
JMV
P9G0316
Phenanthrene
BRL
mg/kg dry
0.75
0.20
1
8270E
7/22/19 17:59
JMV
P9G0316
Phenol
BRL
mg/kg dry
0.75
0.12
1
8270E
7/22/19 17:59
JMV
P9G0316
Pyrene
BRL
mg/kg dry
0.75
0.17
1
8270E
7/22/19 17:59
JMV
P9G0316
Pyridine
BRL
mg/kg dry
0.38
0.072
1
8270E
7/22/19 17:59
JMV
P9G0316
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
80 %
39-132
2-Fluorobiphenyl
76 %
44-115
2-Fluorophenol
73 %
35-115
Nitrobenzene-d5
61 %
37-122
Phenol-d5
72 %
34-121
Terphenyl-d14
82 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.057
0.020
1
*7471B
7/31/19 11:47
MMR
P9G0500
Arsenic
4.6
mg/kg dry
1.1
0.15
1
*6010D
8/1/19 14:41
JAB
P9G0507
Barium
620
mg/kg dry
110
34
10
*60101)
8/1/19 14:33
JAB
P9G0507
Cadmium
BRL
mg/kg dry
0.57
0.039
1
*6010D
8/1/19 14:41
JAB
P9G0507
Chromium
18
mg/kg dry
1.1
0.087
1
*6010D
8/1/19 14:41
JAB
P9G0507
Lead
15
mg/kg dry
1.1
0.19
1
*6010D
8/1/19 14:41
JAB
P9G0507
Selenium
BRL
mg/kg dry
1.1
0.31
1
*6010D
8/1/19 14:41
JAB
P9G0507
Silver
BRL
mg/kg dry
0.57
0.035
1
*6010D
8/1/19 14:41
JAB
P9G0507
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
08/21 /2019
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Project: 3021.01 Client Sample ID: Duplicate
Prism Sample ID: 9070214-11
Prism Work Order: 9070214
Sample Matrix: Solid Time Collected: 07/12/19 15:55
Time Submitted: 07/16/19 10:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0059
0.00072
1
8260D
7/19/19 20:21
JLB
P9G0319
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0059
0.00086
1
8260D
7/19/19 20:21
JLB
P9G0319
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0059
0.00043
1
8260D
7/19/19 20:21
JLB
P9G0319
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0059
0.00063
1
8260D
7/19/19 20:21
JLB
P9G0319
1,1-Dichloroethane
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 20:21
JLB
P9G0319
1,1-Dichloroethylene
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 20:21
JLB
P9G0319
1,1-Dichloropropylene
BRL
mg/kg dry
0.0059
0.00091
1
8260D
7/19/19 20:21
JLB
P9G0319
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00084
1
8260D
7/19/19 20:21
JLB
P9G0319
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0059
0.00067
1
8260D
7/19/19 20:21
JLB
P9G0319
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00056
1
8260D
7/19/19 20:21
JLB
P9G0319
1,2,4-Trimethyl benzene 0.0029
J
mg/kg dry
0.0059
0.00062
1
8260D
7/19/19 20:21
JLB
P9G0319
1,2-Dibromoethane
BRL
mg/kg dry
0.0059
0.00053
1
8260D
7/19/19 20:21
JLB
P9G0319
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0059
0.00066
1
8260D
7/19/19 20:21
JLB
P9G0319
1,2-Dichloroethane
BRL
mg/kg dry
0.0059
0.00070
1
8260D
7/19/19 20:21
JLB
P9G0319
1,2-Dichloropropane
BRL
mg/kg dry
0.0059
0.00088
1
8260D
7/19/19 20:21
JLB
P9G0319
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0059
0.00074
1
8260D
7/19/19 20:21
JLB
P9G0319
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0059
0.00073
1
8260D
7/19/19 20:21
JLB
P9G0319
1,3-Dichloropropane
BRL
mg/kg dry
0.0059
0.00049
1
8260D
7/19/19 20:21
JLB
P9G0319
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0059
0.00074
1
8260D
7/19/19 20:21
JLB
P9G0319
2,2-Dichloropropane
BRL
mg/kg dry
0.0059
0.00073
1
8260D
7/19/19 20:21
JLB
P9G0319
2-Chlorotoluene
BRL
mg/kg dry
0.0059
0.00079
1
8260D
7/19/19 20:21
JLB
P9G0319
4-Chlorotoluene
BRL
mg/kg dry
0.0059
0.00067
1
8260D
7/19/19 20:21
JLB
P9G0319
4-Isopropyltoluene
BRL
mg/kg dry
0.0059
0.0015
1
8260D
7/19/19 20:21
JLB
P9G0319
Acetone
BRL
mg/kg dry
0.023
0.0015
1
8260D
7/19/19 20:21
JLB
P9G0319
Benzene
BRL
mg/kg dry
0.0059
0.00092
1
8260D
7/19/19 20:21
JLB
P9G0319
Bromobenzene
BRL
mg/kg dry
0.0059
0.00082
1
8260D
7/19/19 20:21
JLB
P9G0319
Bromochloromethane
BRL
mg/kg dry
0.0059
0.00097
1
8260D
7/19/19 20:21
JLB
P9G0319
Bromodichloromethane
BRL
mg/kg dry
0.0059
0.00056
1
8260D
7/19/19 20:21
JLB
P9G0319
Bromoform
BRL
mg/kg dry
0.0059
0.00045
1
8260D
7/19/19 20:21
JLB
P9G0319
Bromomethane
BRL
mg/kg dry
0.012
0.0029
1
8260D
7/19/19 20:21
JLB
P9G0319
Carbon Tetrachloride
BRL
mg/kg dry
0.0059
0.0012
1
8260D
7/19/19 20:21
JLB
P9G0319
Chlorobenzene
BRL
mg/kg dry
0.0059
0.00092
1
8260D
7/19/19 20:21
JLB
P9G0319
Chloroethane
BRL
mg/kg dry
0.012
0.0011
1
8260D
7/19/19 20:21
JLB
P9G0319
Chloroform
BRL
mg/kg dry
0.0059
0.00072
1
8260D
7/19/19 20:21
JLB
P9G0319
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
8260D
7/19/19 20:21
JLB
P9G0319
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0059
0.00092
1
8260D
7/19/19 20:21
JLB
P9G0319
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0059
0.00058
1
8260D
7/19/19 20:21
JLB
P9G0319
Dibromochloromethane
BRL
mg/kg dry
0.0059
0.00039
1
8260D
7/19/19 20:21
JLB
P9G0319
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
7/19/19 20:21
JLB
P9G0319
Ethylbenzene
BRL
mg/kg dry
0.0059
0.00088
1
8260D
7/19/19 20:21
JLB
P9G0319
Isopropyl Ether
BRL
mg/kg dry
0.0059
0.00086
1
8260D
7/19/19 20:21
JLB
P9G0319
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0059
0.00068
1
8260D
7/19/19 20:21
JLB
P9G0319
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 08/21/2019
LABORATORIES INC.
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Client Sample ID: Duplicate
Attn: Darin McClure Prism Sample ID: 9070214-11
409 Rogers View Court Prism Work Order: 9070214
Raleigh, NC 27610 Sample Matrix: Solid Time Collected: 07/12/19 15:55
Time Submitted: 07/16/19 10:05
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
0.0031 J
mg/kg dry
0.012
0.0015
1
8260D
7/19/19 20:21
JLB
P9G0319
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.023
0.00041
1
8260D
7/19/19 20:21
JLB
P9G0319
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.023
0.0014
1
8260D
7/19/19 20:21
JLB
P9G0319
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.023
0.00048
1
8260D
7/19/19 20:21
JLB
P9G0319
Methylene Chloride
BRL
mg/kg dry
0.0059
0.00095
1
8260D
7/19/19 20:21
JLB
P9G0319
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0059
0.00082
1
8260D
7/19/19 20:21
JLB
P9G0319
Naphthalene
0.0029 J
mg/kg dry
0.012
0.00059
1
8260D
7/19/19 20:21
JLB
P9G0319
n-Butylbenzene
BRL
mg/kg dry
0.0059
0.00055
1
8260D
7/19/19 20:21
JLB
P9G0319
n-Propylbenzene
BRL
mg/kg dry
0.0059
0.00085
1
8260D
7/19/19 20:21
JLB
P9G0319
o-Xylene
BRL
mg/kg dry
0.0059
0.00062
1
8260D
7/19/19 20:21
JLB
P9G0319
sec-Butylbenzene
BRL
mg/kg dry
0.0059
0.00063
1
8260D
7/19/19 20:21
JLB
P9G0319
Styrene
BRL
mg/kg dry
0.0059
0.00057
1
8260D
7/19/19 20:21
JLB
P9G0319
tert-Butylbenzene
BRL
mg/kg dry
0.0059
0.00070
1
8260D
7/19/19 20:21
JLB
P9G0319
Tetrachloroethylene
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 20:21
JLB
P9G0319
Toluene
BRL
mg/kg dry
0.0059
0.00093
1
8260D
7/19/19 20:21
JLB
P9G0319
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 20:21
JLB
P9G0319
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0059
0.00050
1
8260D
7/19/19 20:21
JLB
P9G0319
Trichloroethylene
BRL
mg/kg dry
0.0059
0.0011
1
8260D
7/19/19 20:21
JLB
P9G0319
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
7/19/19 20:21
JLB
P9G0319
Vinyl acetate
BRL
mg/kg dry
0.012
0.00064
1
8260D
7/19/19 20:21
JLB
P9G0319
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
7/19/19 20:21
JLB
P9G0319
Xylenes, total
0.0031 J
mg/kg dry
0.018
0.0021
1
8260D
7/19/19 20:21
JLB
P9G0319
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
100 %
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
92 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

/r E
P R I IS M Service Analytical
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21 /19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Prism Work Order: 9070214
Attn: Darin McClure Time Submitted: 7/16/2019 10:05:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9GO319 - 5035
Blank (P9130319-131-K1)
Prepared & Analyzed: 07/19/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130319 - 5035
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9G0319-BLK1)
Prepared & Analyzed: 07/19/19
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
50.6
ug/L
50.00 101 70-130
Surrogate: Dibromofluoromethane
50.7
ug/L
50.00 101 84-123
Surrogate: Toluene-d8
46.9
ug/L
50.00 94 76-129
LCS (P9G0319-BS1)
Prepared
& Analyzed: 07/19/19
1,1,1,2-Tetrachloroethane
0.0415
0.0050
mg/kg wet
0.05000
83
72-115
1, 1,1 -Trichloroethane
0.0402
0.0050
mg/kg wet
0.05000
80
67-131
1,1,2,2-Tetrachloroethane
0.0423
0.0050
mg/kg wet
0.05000
85
56-126
1,1,2-Trichloroethane
0.0436
0.0050
mg/kg wet
0.05000
87
70-133
1,1-Dichloroethane
0.0412
0.0050
mg/kg wet
0.05000
82
74-127
1,1-Dichloroethylene
0.0395
0.0050
mg/kg wet
0.05000
79
67-149
1, 1 -Dichloropropylene
0.0433
0.0050
mg/kg wet
0.05000
87
71-130
1,2,3-Trichlorobenzene
0.0408
0.010
mg/kg wet
0.05000
82
68-130
1,2,3-Trichloropropane
0.0424
0.0050
mg/kg wet
0.05000
85
60-137
1,2,4-Trichlorobenzene
0.0418
0.010
mg/kg wet
0.05000
84
66-125
1,2,4-Trimethylbenzene
0.0400
0.0050
mg/kg wet
0.05000
80
69-129
1,2-Dibromoethane
0.0431
0.0050
mg/kg wet
0.05000
86
70-132
1,2-Dichlorobenzene
0.0398
0.0050
mg/kg wet
0.05000
80
72-123
1,2-Dichloroethane
0.0413
0.0050
mg/kg wet
0.05000
83
68-128
1,2-Dichloropropane
0.0443
0.0050
mg/kg wet
0.05000
89
73-130
1,3,5-Trimethylbenzene
0.0400
0.0050
mg/kg wet
0.05000
80
69-128
1,3-Dichlorobenzene
0.0395
0.0050
mg/kg wet
0.05000
79
71-120
1,3-Dichloropropane
0.0430
0.0050
mg/kg wet
0.05000
86
75-124
1,4-Dichlorobenzene
0.0397
0.0050
mg/kg wet
0.05000
79
71-123
2,2-Dichloropropane
0.0411
0.0050
mg/kg wet
0.05000
82
50-142
2-Chlorotoluene
0.0395
0.0050
mg/kg wet
0.05000
79
67-124
4-Chlorotoluene
0.0399
0.0050
mg/kg wet
0.05000
80
71-126
4-Isopropyltoluene
0.0407
0.0050
mg/kg wet
0.05000
81
68-129
Acetone
0.0845
0.020
mg/kg wet
0.1000
85
29-198
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130319 - 5035
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P91130319-113SI)
Prepared & Analyzed: 07/19/19
Benzene
0.0433
0.0050
mg/kg wet
0.05000
87
74-127
Bromobenzene
0.0387
0.0050
mg/kg wet
0.05000
77
73-125
Bromochloromethane
0.0431
0.0050
mg/kg wet
0.05000
86
72-134
Bromodichloromethane
0.0419
0.0050
mg/kg wet
0.05000
84
75-122
Bromoform
0.0442
0.0050
mg/kg wet
0.05000
88
66-135
Bromomethane
0.0507
0.010
mg/kg wet
0.05000
101
20-180
Carbon Tetrachloride
0.0410
0.0050
mg/kg wet
0.05000
82
64-143
Chlorobenzene
0.0415
0.0050
mg/kg wet
0.05000
83
74-118
Chloroethane
0.0404
0.010
mg/kg wet
0.05000
81
33-149
Chloroform
0.0418
0.0050
mg/kg wet
0.05000
84
73-127
Chloromethane
0.0445
0.010
mg/kg wet
0.05000
89
45-143
cis-1,2-Dichloroethylene
0.0425
0.0050
mg/kg wet
0.05000
85
76-134
cis-1,3-Dichloropropylene
0.0455
0.0050
mg/kg wet
0.05000
91
71-125
Dibromochloromethane
0.0422
0.0050
mg/kg wet
0.05000
84
73-122
Dichlorodifluoromethane
0.0457
0.010
mg/kg wet
0.05000
91
26-146
Ethylbenzene
0.0411
0.0050
mg/kg wet
0.05000
82
74-128
Isopropyl Ether
0.0440
0.0050
mg/kg wet
0.05000
88
59-159
Isopropylbenzene (Cumene)
0.0411
0.0050
mg/kg wet
0.05000
82
68-126
m,p-Xylenes
0.0839
0.010
mg/kg wet
0.1000
84
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0504
0.020
mg/kg wet
0.05000
101
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0466
0.020
mg/kg wet
0.05000
93
63-149
Methyl Isobutyl Ketone
0.0490
0.020
mg/kg wet
0.05000
98
57-162
Methylene Chloride
0.0410
0.0050
mg/kg wet
0.05000
82
74-129
Methyl-tert-Butyl Ether
0.0444
0.0050
mg/kg wet
0.05000
89
70-130
Naphthalene
0.0445
0.010
mg/kg wet
0.05000
89
57-157
n-Butylbenzene
0.0403
0.0050
mg/kg wet
0.05000
81
65-135
n-Propylbenzene
0.0397
0.0050
mg/kg wet
0.05000
79
67-130
o-Xylene
0.0414
0.0050
mg/kg wet
0.05000
83
74-126
sec-Butylbenzene
0.0396
0.0050
mg/kg wet
0.05000
79
66-131
Styrene
0.0442
0.0050
mg/kg wet
0.05000
88
77-121
tert-Butyl benzene
0.0400
0.0050
mg/kg wet
0.05000
80
67-132
Tetrachloroethylene
0.0432
0.0050
mg/kg wet
0.05000
86
68-130
Toluene
0.0430
0.0050
mg/kg wet
0.05000
86
71-129
trans- 1,2-Dichloroethylene
0.0407
0.0050
mg/kg wet
0.05000
81
73-132
trans- 1,3-Dichloropropylene
0.0450
0.0050
mg/kg wet
0.05000
90
68-123
Trichloroethylene
0.0438
0.0050
mg/kg wet
0.05000
88
75-133
Trichlorofluoromethane
0.0390
0.010
mg/kg wet
0.05000
78
44-146
Vinyl acetate
0.0482
0.010
mg/kg wet
0.05000
96
85-161
Vinyl chloride
0.0439
0.010
mg/kg wet
0.05000
88
48-147
Xylenes, total
0.125
0.015
mg/kg wet
0.1500
84
74-126
Surrogate:4-Bromofluorobenzene
49.4
ug/L
50.00
99
70-130
Surrogate: Dibromofluoromethane
48.3
ug/L
50.00
97
84-123
Surrogate: Toluene-d8
47.5
ug/L
50.00
95
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130319 - 5035
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P9G0319-BSD1)
Prepared & Analyzed: 07/19/19
1,1,1,2-Tetrachloroethane
0.0419
0.0050
mg/kg wet
0.05000
84
72-115
1
20
1, 1,1 -Trichloroethane
0.0399
0.0050
mg/kg wet
0.05000
80
67-131
0.8
20
1,1,2,2-Tetrachloroethane
0.0457
0.0050
mg/kg wet
0.05000
91
56-126
8
20
1,1,2-Trichloroethane
0.0447
0.0050
mg/kg wet
0.05000
89
70-133
3
20
1,1-Dichloroethane
0.0420
0.0050
mg/kg wet
0.05000
84
74-127
2
20
1,1-Dichloroethylene
0.0383
0.0050
mg/kg wet
0.05000
77
67-149
3
20
1, 1 -Dichloropropylene
0.0426
0.0050
mg/kg wet
0.05000
85
71-130
2
20
1,2,3-Trichlorobenzene
0.0438
0.010
mg/kg wet
0.05000
88
68-130
7
20
1,2,3-Trichloropropane
0.0451
0.0050
mg/kg wet
0.05000
90
60-137
6
20
1,2,4-Trichlorobenzene
0.0444
0.010
mg/kg wet
0.05000
89
66-125
6
20
1,2,4-Trimethylbenzene
0.0415
0.0050
mg/kg wet
0.05000
83
69-129
4
20
1,2-Dibromoethane
0.0451
0.0050
mg/kg wet
0.05000
90
70-132
5
20
1,2-Dichlorobenzene
0.0420
0.0050
mg/kg wet
0.05000
84
72-123
6
20
1,2-Dichloroethane
0.0425
0.0050
mg/kg wet
0.05000
85
68-128
3
20
1,2-Dichloropropane
0.0463
0.0050
mg/kg wet
0.05000
93
73-130
4
20
1,3,5-Trimethylbenzene
0.0415
0.0050
mg/kg wet
0.05000
83
69-128
4
20
1,3-Dichlorobenzene
0.0415
0.0050
mg/kg wet
0.05000
83
71-120
5
20
1,3-Dichloropropane
0.0445
0.0050
mg/kg wet
0.05000
89
75-124
3
20
1,4-Dichlorobenzene
0.0419
0.0050
mg/kg wet
0.05000
84
71-123
5
20
2,2-Dichloropropane
0.0408
0.0050
mg/kg wet
0.05000
82
50-142
0.9
20
2-Chlorotoluene
0.0409
0.0050
mg/kg wet
0.05000
82
67-124
4
20
4-Chlorotoluene
0.0411
0.0050
mg/kg wet
0.05000
82
71-126
3
20
4-Isopropyltoluene
0.0415
0.0050
mg/kg wet
0.05000
83
68-129
2
20
Acetone
0.0878
0.020
mg/kg wet
0.1000
88
29-198
4
20
Benzene
0.0437
0.0050
mg/kg wet
0.05000
87
74-127
1
20
Bromobenzene
0.0409
0.0050
mg/kg wet
0.05000
82
73-125
5
20
Bromochloromethane
0.0450
0.0050
mg/kg wet
0.05000
90
72-134
4
20
Bromodichloromethane
0.0427
0.0050
mg/kg wet
0.05000
85
75-122
2
20
Bromoform
0.0454
0.0050
mg/kg wet
0.05000
91
66-135
3
20
Bromomethane
0.0482
0.010
mg/kg wet
0.05000
96
20-180
5
20
Carbon Tetrachloride
0.0393
0.0050
mg/kg wet
0.05000
79
64-143
4
20
Chlorobenzene
0.0422
0.0050
mg/kg wet
0.05000
84
74-118
2
20
Chloroethane
0.0398
0.010
mg/kg wet
0.05000
80
33-149
2
20
Chloroform
0.0426
0.0050
mg/kg wet
0.05000
85
73-127
2
20
Chloromethane
0.0432
0.010
mg/kg wet
0.05000
86
45-143
3
20
cis-1,2-Dichloroethylene
0.0430
0.0050
mg/kg wet
0.05000
86
76-134
1
20
cis-1,3-Dichloropropylene
0.0464
0.0050
mg/kg wet
0.05000
93
71-125
2
20
Dibromochloromethane
0.0436
0.0050
mg/kg wet
0.05000
87
73-122
3
20
Dichlorodifluoromethane
0.0437
0.010
mg/kg wet
0.05000
87
26-146
5
20
Ethylbenzene
0.0414
0.0050
mg/kg wet
0.05000
83
74-128
0.6
20
Isopropyl Ether
0.0454
0.0050
mg/kg wet
0.05000
91
59-159
3
20
Isopropylbenzene (Cumene)
0.0420
0.0050
mg/kg wet
0.05000
84
68-126
2
20
m,p-Xylenes
0.0838
0.010
mg/kg wet
0.1000
84
75-124
0.2
20
Methyl Butyl Ketone (2-Hexanone)
0.0517
0.020
mg/kg wet
0.05000
103
61-157
3
20
Methyl Ethyl Ketone (2-Butanone)
0.0481
0.020
mg/kg wet
0.05000
96
63-149
3
20
Methyl Isobutyl Ketone
0.0514
0.020
mg/kg wet
0.05000
103
57-162
5
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130319 - 5035
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P9G0319-BSD1)
Prepared & Analyzed: 07/19/19
Methylene Chloride
0.0422
0.0050
mg/kg wet
0.05000
84
74-129
3
20
Methyl-tert-Butyl Ether
0.0458
0.0050
mg/kg wet
0.05000
92
70-130
3
20
Naphthalene
0.0481
0.010
mg/kg wet
0.05000
96
57-157
8
20
n-Butylbenzene
0.0414
0.0050
mg/kg wet
0.05000
83
65-135
3
20
n-Propylbenzene
0.0406
0.0050
mg/kg wet
0.05000
81
67-130
2
20
o-Xylene
0.0422
0.0050
mg/kg wet
0.05000
84
74-126
2
20
sec-Butylbenzene
0.0407
0.0050
mg/kg wet
0.05000
81
66-131
3
20
Styrene
0.0452
0.0050
mg/kg wet
0.05000
90
77-121
2
20
tert-Butyl benzene
0.0405
0.0050
mg/kg wet
0.05000
81
67-132
1
20
Tetrachloroethylene
0.0432
0.0050
mg/kg wet
0.05000
86
68-130
0
20
Toluene
0.0433
0.0050
mg/kg wet
0.05000
87
71-129
0.7
20
trans- 1,2-Dichloroethylene
0.0409
0.0050
mg/kg wet
0.05000
82
73-132
0.4
20
trans- 1,3-Dichloropropylene
0.0465
0.0050
mg/kg wet
0.05000
93
68-123
3
20
Trichloroethylene
0.0437
0.0050
mg/kg wet
0.05000
87
75-133
0.2
20
Trichlorofluoromethane
0.0383
0.010
mg/kg wet
0.05000
77
44-146
2
20
Vinyl acetate
0.0507
0.010
mg/kg wet
0.05000
101
85-161
5
20
Vinyl chloride
0.0425
0.010
mg/kg wet
0.05000
85
48-147
3
20
Xylenes, total
0.126
0.015
mg/kg wet
0.1500
84
74-126
0.5
20
Surrogate:4-Bromofluorobenzene
49.7
ug/L
50.00
99
70-130
Surrogate: Dibromofluoromethane
48.1
ug/L
50.00
96
84-123
Surrogate: Toluene-d8
47.3
ug/L
50.00
95
76-129
Batch P91130345 - 5035
Blank (P9GO345-BLK1)
Prepared & Analyzed: 07/22/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1, 1,1 -Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1, 1 -Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethylbenzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethylbenzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
8/21 /19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Prism Work Order: 9070214
Attn: Darin McClure Time Submitted: 7/16/2019 10:05:OOAM
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9GO345 - 5035
Blank (P9G0345-BLK1)
Prepared & Analyzed: 07/22/19
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butylbenzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
51.4
ug/L
50.00 103 70-130
Surrogate: Dibromofluoromethane
52.4
ug/L
50.00 105 84-123
Surrogate: Toluene-d8
46.2
ug/L
50.00 92 76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130345 - 5035
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9G0345-BS1)
Prepared & Analyzed: 07/22/19
1,1,1,2-Tetrachloroethane
0.0479
0.0050
mg/kg wet
0.05000
96
72-115
1, 1,1 -Trichloroethane
0.0497
0.0050
mg/kg wet
0.05000
99
67-131
1,1,2,2-Tetrachloroethane
0.0419
0.0050
mg/kg wet
0.05000
84
56-126
1,1,2-Trichloroethane
0.0431
0.0050
mg/kg wet
0.05000
86
70-133
1,1-Dichloroethane
0.0464
0.0050
mg/kg wet
0.05000
93
74-127
1,1-Dichloroethylene
0.0460
0.0050
mg/kg wet
0.05000
92
67-149
1, 1 -Dichloropropylene
0.0495
0.0050
mg/kg wet
0.05000
99
71-130
1,2,3-Trichlorobenzene
0.0431
0.010
mg/kg wet
0.05000
86
68-130
1,2,3-Trichloropropane
0.0445
0.0050
mg/kg wet
0.05000
89
60-137
1,2,4-Trichlorobenzene
0.0426
0.010
mg/kg wet
0.05000
85
66-125
1,2,4-Trimethylbenzene
0.0436
0.0050
mg/kg wet
0.05000
87
69-129
1,2-Dibromoethane
0.0430
0.0050
mg/kg wet
0.05000
86
70-132
1,2-Dichlorobenzene
0.0409
0.0050
mg/kg wet
0.05000
82
72-123
1,2-Dichloroethane
0.0495
0.0050
mg/kg wet
0.05000
99
68-128
1,2-Dichloropropane
0.0454
0.0050
mg/kg wet
0.05000
91
73-130
1,3,5-Trimethylbenzene
0.0435
0.0050
mg/kg wet
0.05000
87
69-128
1,3-Dichlorobenzene
0.0407
0.0050
mg/kg wet
0.05000
81
71-120
1,3-Dichloropropane
0.0438
0.0050
mg/kg wet
0.05000
88
75-124
1,4-Dichlorobenzene
0.0410
0.0050
mg/kg wet
0.05000
82
71-123
2,2-Dichloropropane
0.0511
0.0050
mg/kg wet
0.05000
102
50-142
2-Chlorotoluene
0.0418
0.0050
mg/kg wet
0.05000
84
67-124
4-Chlorotoluene
0.0420
0.0050
mg/kg wet
0.05000
84
71-126
4-Isopropyltoluene
0.0439
0.0050
mg/kg wet
0.05000
88
68-129
Acetone
0.0931
0.020
mg/kg wet
0.1000
93
29-198
Benzene
0.0456
0.0050
mg/kg wet
0.05000
91
74-127
Bromobenzene
0.0412
0.0050
mg/kg wet
0.05000
82
73-125
Bromochloromethane
0.0455
0.0050
mg/kg wet
0.05000
91
72-134
Bromodichloromethane
0.0477
0.0050
mg/kg wet
0.05000
95
75-122
Bromoform
0.0458
0.0050
mg/kg wet
0.05000
92
66-135
Bromomethane
0.0479
0.010
mg/kg wet
0.05000
96
20-180
Carbon Tetrachloride
0.0519
0.0050
mg/kg wet
0.05000
104
64-143
Chlorobenzene
0.0421
0.0050
mg/kg wet
0.05000
84
74-118
Chloroethane
0.0397
0.010
mg/kg wet
0.05000
79
33-149
Chloroform
0.0482
0.0050
mg/kg wet
0.05000
96
73-127
Chloromethane
0.0448
0.010
mg/kg wet
0.05000
90
45-143
cis-1,2-Dichloroethylene
0.0458
0.0050
mg/kg wet
0.05000
92
76-134
cis-1,3-Dichloropropylene
0.0481
0.0050
mg/kg wet
0.05000
96
71-125
Dibromochloromethane
0.0446
0.0050
mg/kg wet
0.05000
89
73-122
Dichlorodifluoromethane
0.0566
0.010
mg/kg wet
0.05000
113
26-146
Ethylbenzene
0.0449
0.0050
mg/kg wet
0.05000
90
74-128
Isopropyl Ether
0.0421
0.0050
mg/kg wet
0.05000
84
59-159
Isopropylbenzene (Cumene)
0.0438
0.0050
mg/kg wet
0.05000
88
68-126
m,p-Xylenes
0.0921
0.010
mg/kg wet
0.1000
92
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0464
0.020
mg/kg wet
0.05000
93
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0480
0.020
mg/kg wet
0.05000
96
63-149
Methyl Isobutyl Ketone
0.0470
0.020
mg/kg wet
0.05000
94
57-162
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130345 - 5035
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9G0345-BS1)
Prepared & Analyzed: 07/22/19
Methylene Chloride
0.0446
0.0050
mg/kg wet
0.05000
89
74-129
Methyl-tert-Butyl Ether
0.0458
0.0050
mg/kg wet
0.05000
92
70-130
Naphthalene
0.0441
0.010
mg/kg wet
0.05000
88
57-157
n-Butylbenzene
0.0439
0.0050
mg/kg wet
0.05000
88
65-135
n-Propylbenzene
0.0425
0.0050
mg/kg wet
0.05000
85
67-130
o-Xylene
0.0449
0.0050
mg/kg wet
0.05000
90
74-126
sec-Butylbenzene
0.0438
0.0050
mg/kg wet
0.05000
88
66-131
Styrene
0.0447
0.0050
mg/kg wet
0.05000
89
77-121
tert-Butyl benzene
0.0434
0.0050
mg/kg wet
0.05000
87
67-132
Tetrachloroethylene
0.0473
0.0050
mg/kg wet
0.05000
95
68-130
Toluene
0.0460
0.0050
mg/kg wet
0.05000
92
71-129
trans- 1,2-Dichloroethylene
0.0460
0.0050
mg/kg wet
0.05000
92
73-132
trans- 1,3-Dichloropropylene
0.0498
0.0050
mg/kg wet
0.05000
100
68-123
Trichloroethylene
0.0461
0.0050
mg/kg wet
0.05000
92
75-133
Trichlorofluoromethane
0.0539
0.010
mg/kg wet
0.05000
108
44-146
Vinyl acetate
0.0517
0.010
mg/kg wet
0.05000
103
85-161
Vinyl chloride
0.0469
0.010
mg/kg wet
0.05000
94
48-147
Xylenes, total
0.137
0.015
mg/kg wet
0.1500
91
74-126
Surrogate:4-Bromofluorobenzene
49.3
ug/L
50.00
99
70-130
Surrogate: Dibromofluoromethane
50.2
ug/L
50.00
100
84-123
Surrogate: Toluene-d8
46.4
ug/L
50.00
93
76-129
LCS Dup (P9G0345-BSD1)
Prepared & Analyzed: 07/22/19
1,1,1,2-Tetrachloroethane
0.0490
0.0050
mg/kg wet
0.05000
98
72-115
2
20
1, 1,1 -Trichloroethane
0.0511
0.0050
mg/kg wet
0.05000
102
67-131
3
20
1,1,2,2-Tetrachloroethane
0.0453
0.0050
mg/kg wet
0.05000
91
56-126
8
20
1,1,2-Trichloroethane
0.0457
0.0050
mg/kg wet
0.05000
91
70-133
6
20
1,1-Dichloroethane
0.0480
0.0050
mg/kg wet
0.05000
96
74-127
4
20
1,1-Dichloroethylene
0.0467
0.0050
mg/kg wet
0.05000
93
67-149
2
20
1, 1 -Dichloropropylene
0.0499
0.0050
mg/kg wet
0.05000
100
71-130
0.9
20
1,2,3-Trichlorobenzene
0.0456
0.010
mg/kg wet
0.05000
91
68-130
6
20
1,2,3-Trichloropropane
0.0488
0.0050
mg/kg wet
0.05000
98
60-137
9
20
1,2,4-Trichlorobenzene
0.0448
0.010
mg/kg wet
0.05000
90
66-125
5
20
1,2,4-Trimethylbenzene
0.0454
0.0050
mg/kg wet
0.05000
91
69-129
4
20
1,2-Dibromoethane
0.0464
0.0050
mg/kg wet
0.05000
93
70-132
7
20
1,2-Dichlorobenzene
0.0433
0.0050
mg/kg wet
0.05000
87
72-123
6
20
1,2-Dichloroethane
0.0521
0.0050
mg/kg wet
0.05000
104
68-128
5
20
1,2-Dichloropropane
0.0489
0.0050
mg/kg wet
0.05000
98
73-130
8
20
1,3,5-Trimethylbenzene
0.0444
0.0050
mg/kg wet
0.05000
89
69-128
2
20
1,3-Dichlorobenzene
0.0427
0.0050
mg/kg wet
0.05000
85
71-120
5
20
1,3-Dichloropropane
0.0466
0.0050
mg/kg wet
0.05000
93
75-124
6
20
1,4-Dichlorobenzene
0.0430
0.0050
mg/kg wet
0.05000
86
71-123
5
20
2,2-Dichloropropane
0.0512
0.0050
mg/kg wet
0.05000
102
50-142
0.2
20
2-Chlorotoluene
0.0434
0.0050
mg/kg wet
0.05000
87
67-124
4
20
4-Chlorotoluene
0.0437
0.0050
mg/kg wet
0.05000
87
71-126
4
20
4-Isopropyltoluene
0.0449
0.0050
mg/kg wet
0.05000
90
68-129
2
20
Acetone
0.0972
0.020
mg/kg wet
0.1000
97
29-198
4
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130345 - 5035
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P9G0345-BSD1)
Prepared & Analyzed: 07/22/19
Benzene
0.0471
0.0050
mg/kg wet
0.05000
94
74-127
3
20
Bromobenzene
0.0434
0.0050
mg/kg wet
0.05000
87
73-125
5
20
Bromochloromethane
0.0476
0.0050
mg/kg wet
0.05000
95
72-134
5
20
Bromodichloromethane
0.0509
0.0050
mg/kg wet
0.05000
102
75-122
6
20
Bromoform
0.0485
0.0050
mg/kg wet
0.05000
97
66-135
6
20
Bromomethane
0.0522
0.010
mg/kg wet
0.05000
104
20-180
8
20
Carbon Tetrachloride
0.0522
0.0050
mg/kg wet
0.05000
104
64-143
0.6
20
Chlorobenzene
0.0442
0.0050
mg/kg wet
0.05000
88
74-118
5
20
Chloroethane
0.0406
0.010
mg/kg wet
0.05000
81
33-149
2
20
Chloroform
0.0501
0.0050
mg/kg wet
0.05000
100
73-127
4
20
Chloromethane
0.0445
0.010
mg/kg wet
0.05000
89
45-143
0.6
20
cis-1,2-Dichloroethylene
0.0485
0.0050
mg/kg wet
0.05000
97
76-134
6
20
cis-1,3-Dichloropropylene
0.0511
0.0050
mg/kg wet
0.05000
102
71-125
6
20
Dibromochloromethane
0.0470
0.0050
mg/kg wet
0.05000
94
73-122
5
20
Dichlorodifluoromethane
0.0566
0.010
mg/kg wet
0.05000
113
26-146
0
20
Ethylbenzene
0.0463
0.0050
mg/kg wet
0.05000
93
74-128
3
20
Isopropyl Ether
0.0453
0.0050
mg/kg wet
0.05000
91
59-159
7
20
Isopropylbenzene (Cumene)
0.0448
0.0050
mg/kg wet
0.05000
90
68-126
2
20
m,p-Xylenes
0.0943
0.010
mg/kg wet
0.1000
94
75-124
2
20
Methyl Butyl Ketone (2-Hexanone)
0.0500
0.020
mg/kg wet
0.05000
100
61-157
7
20
Methyl Ethyl Ketone (2-Butanone)
0.0503
0.020
mg/kg wet
0.05000
101
63-149
5
20
Methyl Isobutyl Ketone
0.0509
0.020
mg/kg wet
0.05000
102
57-162
8
20
Methylene Chloride
0.0461
0.0050
mg/kg wet
0.05000
92
74-129
3
20
Methyl-tert-Butyl Ether
0.0515
0.0050
mg/kg wet
0.05000
103
70-130
12
20
Naphthalene
0.0477
0.010
mg/kg wet
0.05000
95
57-157
8
20
n-Butylbenzene
0.0455
0.0050
mg/kg wet
0.05000
91
65-135
3
20
n-Propylbenzene
0.0436
0.0050
mg/kg wet
0.05000
87
67-130
3
20
o-Xylene
0.0462
0.0050
mg/kg wet
0.05000
92
74-126
3
20
sec-Butylbenzene
0.0449
0.0050
mg/kg wet
0.05000
90
66-131
3
20
Styrene
0.0466
0.0050
mg/kg wet
0.05000
93
77-121
4
20
tert-Butyl benzene
0.0443
0.0050
mg/kg wet
0.05000
89
67-132
2
20
Tetrachloroethylene
0.0491
0.0050
mg/kg wet
0.05000
98
68-130
4
20
Toluene
0.0479
0.0050
mg/kg wet
0.05000
96
71-129
4
20
trans- 1,2-Dichloroethylene
0.0462
0.0050
mg/kg wet
0.05000
92
73-132
0.4
20
trans- 1,3-Dichloropropylene
0.0531
0.0050
mg/kg wet
0.05000
106
68-123
6
20
Trichloroethylene
0.0475
0.0050
mg/kg wet
0.05000
95
75-133
3
20
Trichlorofluoromethane
0.0525
0.010
mg/kg wet
0.05000
105
44-146
3
20
Vinyl acetate
0.0545
0.010
mg/kg wet
0.05000
109
85-161
5
20
Vinyl chloride
0.0468
0.010
mg/kg wet
0.05000
94
48-147
0.2
20
Xylenes, total
0.141
0.015
mg/kg wet
0.1500
94
74-126
3
20
Surrogate:4-Bromofluorobenzene
50.3
ug/L
50.00
101
70-130
Surrogate: Dibromofluoromethane
50.5
ug/L
50.00
101
84-123
Surrogate: Toluene-d8
45.8
ug/L
50.00
92
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
8/21 /19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Prism Work Order: 9070214
Attn: Darin McClure Time Submitted: 7/16/2019 10:05:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9GO316 - 3546
Blank (P9G0316-BLK1)
Prepared: 07/19/19 Analyzed: 07/22/19
1,2,4-Trichlorobenzene
BRL
0.66
mg/kg wet
1,2-Dichlorobenzene
BRL
0.66
mg/kg wet
1,3-Dichlorobenzene
BRL
0.66
mg/kg wet
1,4-Dichlorobenzene
BRL
0.33
mg/kg wet
1-Methyl naphthalene
BRL
0.66
mg/kg wet
2,4,5-Trichlorophenol
BRL
0.66
mg/kg wet
2,4,6-Trichlorophenol
BRL
0.66
mg/kg wet
2,4-Dichlorophenol
BRL
0.66
mg/kg wet
2,4-Dimethylphenol
BRL
0.33
mg/kg wet
2,4-Dinitrophenol
BRL
1.5
mg/kg wet
2,4-Dinitrotoluene
BRL
0.66
mg/kg wet
2,6-Dinitrotoluene
BRL
0.66
mg/kg wet
2-Chloronaphthalene
BRL
0.66
mg/kg wet
2-Chlorophenol
BRL
0.66
mg/kg wet
2-Methyl naphthalene
BRL
0.66
mg/kg wet
2-Methylphenol
BRL
0.66
mg/kg wet
2-Nitrophenol
BRL
0.66
mg/kg wet
3,3'-Dichlorobenzidine
BRL
0.66
mg/kg wet
3/4-Methyl phenol
BRL
0.66
mg/kg wet
4,6-Dinitro-2-methylphenol
BRL
1.5
mg/kg wet
4-Bromophenyl phenyl ether
BRL
0.66
mg/kg wet
4-Chloro-3-methylphenol
BRL
0.66
mg/kg wet
4-Chloroaniline
BRL
0.33
mg/kg wet
4-Chlorophenyl phenyl ether
BRL
1.0
mg/kg wet
4-Nitrophenol
BRL
0.66
mg/kg wet
Acenaphthene
BRL
0.66
mg/kg wet
Acenaphthylene
BRL
0.66
mg/kg wet
Anthracene
BRL
0.66
mg/kg wet
Azobenzene
BRL
0.66
mg/kg wet
Benzo(a)anthracene
BRL
0.66
mg/kg wet
Benzo(a)pyrene
BRL
0.66
mg/kg wet
Benzo(b)fluoranthene
BRL
0.66
mg/kg wet
Benzo(g,h,i)perylene
BRL
0.66
mg/kg wet
Benzo(k)fluoranthene
BRL
0.66
mg/kg wet
Benzoic Acid
BRL
2.0
mg/kg wet
Benzyl alcohol
BRL
0.66
mg/kg wet
bis(2-Chloroethoxy)methane
BRL
0.66
mg/kg wet
Bis(2-Chloroethyl)ether
BRL
0.66
mg/kg wet
Bis(2-chloroisopropyl)ether
BRL
0.33
mg/kg wet
Bis(2-Ethylhexyl)phthalate
BRL
0.66
mg/kg wet
Butyl benzyl phthalate
BRL
0.33
mg/kg wet
Chrysene
BRL
0.66
mg/kg wet
Dibenzo(a,h)anthracene
BRL
0.66
mg/kg wet
Dibenzofuran
BRL
0.66
mg/kg wet
Diethyl phthalate
BRL
0.66
mg/kg wet
Dimethyl phthalate
BRL
0.66
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
8/21 /19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9GO316 - 3546
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9G0316-BLK1)
Prepared: 07/19/19 Analyzed: 07/22/19
Di-n-butyl phthalate
BRL
0.66
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.66
mg/kg wet
Fluorene
BRL
0.66
mg/kg wet
Hexachlorobenzene
BRL
0.66
mg/kg wet
Hexachlorobutadiene
BRL
0.66
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.66
mg/kg wet
Hexachloroethane
BRL
0.66
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.66
mg/kg wet
Isophorone
BRL
0.66
mg/kg wet
Naphthalene
BRL
0.66
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.66
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.66
mg/kg wet
Pentachlorophenol
BRL
1.0
mg/kg wet
Phenanthrene
BRL
0.66
mg/kg wet
Phenol
BRL
0.66
mg/kg wet
Pyrene
BRL
0.66
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
2.75
mg/kg wet
3.333
83
39-132
Surrogate: 2-Fluorobiphenyl
1.44
mg/kg wet
1.667
86
44-115
Surrogate: 2-Fluorophenol
2.94
mg/kg wet
3.333
88
35-115
Surrogate: Nitrobenzene-d5
1.21
mg/kg wet
1.667
73
37-122
Surrogate: Phenol-d5
2.81
mg/kg wet
3.333
84
34-121
Surrogate: Terphenyl-d14
1.49
mg/kg wet
1.667
90
54-127
LCS (P9G0316-113SI)
Prepared: 07/19/19 Analyzed: 07/22/19
1,2,4-Trichlorobenzene
0.963
0.66
mg/kg wet
1.667
58
34-118
1,2-Dichlorobenzene
0.901
0.66
mg/kg wet
1.667
54
33-117
1,3-Dichlorobenzene
0.837
0.66
mg/kg wet
1.667
50
30-115
1,4-Dichlorobenzene
0.854
0.33
mg/kg wet
1.667
51
31-115
1-Methyl naphthalene
1.14
0.66
mg/kg wet
1.667
68
40-119
2,4,5-Trichlorophenol
1.37
0.66
mg/kg wet
1.667
82
62-124
2,4,6-Trichlorophenol
1.30
0.66
mg/kg wet
1.667
78
39-126
2,4-Dichlorophenol
1.14
0.66
mg/kg wet
1.667
68
40-122
2,4-Dimethylphenol
1.32
0.33
mg/kg wet
1.667
79
30-127
2,4-Dinitrophenol
0.505
1.5
mg/kg wet
1.667
30
27-129 J
2,4-Dinitrotoluene
1.44
0.66
mg/kg wet
1.667
87
48-126
2,6-Dinitrotoluene
1.50
0.66
mg/kg wet
1.667
90
46-124
2-Chloronaphthalene
1.26
0.66
mg/kg wet
1.667
76
41-114
2-Chlorophenol
1.08
0.66
mg/kg wet
1.667
65
34-121
2-Methyl naphthalene
1.10
0.66
mg/kg wet
1.667
66
38-122
2-Methylphenol
1.14
0.66
mg/kg wet
1.667
69
32-122
2-Nitrophenol
0.999
0.66
mg/kg wet
1.667
60
36-123
3,3'-Dichlorobenzidine
1.47
0.66
mg/kg wet
1.667
88
22-121
3/4-Methyl phenol
1.10
0.66
mg/kg wet
1.667
66
34-119
4,6-Dinitro-2-methylphenol
1.06
1.5
mg/kg wet
1.667
64
29-132 J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
8/21 /19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9GO316 - 3546
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9G0316-BS1)
Prepared: 07/19/19 Analyzed: 07/22/19
4-Bromophenyl phenyl ether
1.38
0.66
mg/kg wet
1.667
83
46-124
4-Chloro-3-methylphenol
1.22
0.66
mg/kg wet
1.667
73
45-122
4-Chloroaniline
1.05
0.33
mg/kg wet
1.667
63
17-106
4-Chlorophenyl phenyl ether
1.38
1.0
mg/kg wet
1.667
83
45-121
4-Nitrophenol
1.33
0.66
mg/kg wet
1.667
80
30-132
Acenaphthene
1.33
0.66
mg/kg wet
1.667
80
40-123
Acenaphthylene
1.43
0.66
mg/kg wet
1.667
86
32-132
Anthracene
1.51
0.66
mg/kg wet
1.667
91
47-123
Azobenzene
1.27
0.66
mg/kg wet
1.667
76
39-125
Benzo(a)anthracene
1.42
0.66
mg/kg wet
1.667
85
49-126
Benzo(a)pyrene
1.48
0.66
mg/kg wet
1.667
89
45-129
Benzo(b)fluoranthene
1.46
0.66
mg/kg wet
1.667
87
45-132
Benzo(g,h,i)perylene
1.51
0.66
mg/kg wet
1.667
91
43-134
Benzo(k)fluoranthene
1.54
0.66
mg/kg wet
1.667
92
47-132
Benzoic Acid
BRL
2.0
mg/kg wet
1.667
10-83
Benzyl alcohol
1.14
0.66
mg/kg wet
1.667
69
29-122
bis(2-Chloroethoxy)methane
1.07
0.66
mg/kg wet
1.667
64
36-121
Bis(2-Chloroethyl)ether
0.908
0.66
mg/kg wet
1.667
54
31-120
Bis(2-chloroisopropyl)ether
0.988
0.33
mg/kg wet
1.667
59
33-131
Bis(2-Ethylhexyl)phthalate
1.51
0.66
mg/kg wet
1.667
91
51-133
Butyl benzyl phthalate
1.41
0.33
mg/kg wet
1.667
85
48-132
Chrysene
1.42
0.66
mg/kg wet
1.667
85
50-124
Dibenzo(a,h)anthracene
1.12
0.66
mg/kg wet
1.667
67
45-134
Dibenzofuran
1.33
0.66
mg/kg wet
1.667
80
44-120
Diethyl phthalate
1.43
0.66
mg/kg wet
1.667
86
50-124
Dimethyl phthalate
1.40
0.66
mg/kg wet
1.667
84
48-124
Di-n-butyl phthalate
1.46
0.66
mg/kg wet
1.667
88
51-128
Di-n-octyl phthalate
1.39
0.33
mg/kg wet
1.667
84
45-140
Fluoranthene
1.45
0.66
mg/kg wet
1.667
87
50-127
Fluorene
1.44
0.66
mg/kg wet
1.667
87
43-125
Hexachlorobenzene
1.35
0.66
mg/kg wet
1.667
81
45-122
Hexachlorobutadiene
0.984
0.66
mg/kg wet
1.667
59
32-123
Hexachlorocyclopentadiene
1.04
0.66
mg/kg wet
1.667
62
32-117
Hexachloroethane
0.855
0.66
mg/kg wet
1.667
51
28-117
Indeno(1,2,3-cd)pyrene
1.62
0.66
mg/kg wet
1.667
97
45-133
Isophorone
1.15
0.66
mg/kg wet
1.667
69
30-122
Naphthalene
1.03
0.66
mg/kg wet
1.667
62
35-123
Nitrobenzene
0.999
0.33
mg/kg wet
1.667
60
34-122
N-Nitroso-di-n-propylamine
1.09
0.66
mg/kg wet
1.667
65
36-120
N-Nitrosodiphenylamine
1.66
0.66
mg/kg wet
1.667
99
38-127
Pentachlorophenol
1.58
1.0
mg/kg wet
1.667
95
25-133
Phenanthrene
1.46
0.66
mg/kg wet
1.667
87
50-121
Phenol
1.11
0.66
mg/kg wet
1.667
67
34-121
Pyrene
1.45
0.66
mg/kg wet
1.667
87
47-127
Pyridine
0.643
0.33
mg/kg wet
1.667
39
10-60
Surrogate: 2,4,6-Tribromophenol
2.80
mg/kg wet
3.333
84
39-132
L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130316 - 3546
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P91130316-113SI) Prepared: 07/19/19 Analyzed: 07/22/19
Surrogate: 2-Fluorobiphenyl
1.25
mg/kg wet
1.667
75
44-115
Surrogate: 2-Fluorophenol
2.16
mg/kg wet
3.333
65
35-115
Surrogate: Nitrobenzene-d5
0.931
mg/kg wet
1.667
56
37-122
Surrogate: Phenol-d5
2.18
mg/kg wet
3.333
65
34-121
Surrogate: Terphenyl-d14
1.25
mg/kg wet
1.667
75
54-127
LCS Dup (P9GO316-BSD1)
Prepared: 07/19/19 Analyzed: 07/22/19
1,2,4-Trichlorobenzene
0.789
0.66
mg/kg wet
1.667
47
34-118
20
20
1,2-Dichlorobenzene
0.717
0.66
mg/kg wet
1.667
43
33-117
23
20 D
1,3-Dichlorobenzene
0.673
0.66
mg/kg wet
1.667
40
30-115
22
20 D
1,4-Dichlorobenzene
0.687
0.33
mg/kg wet
1.667
41
31-115
22
20 D
1-Methyl naphthalene
0.949
0.66
mg/kg wet
1.667
57
40-119
18
20
2,4,5-Trichlorophenol
1.19
0.66
mg/kg wet
1.667
71
62-124
14
20
2,4,6-Trichlorophenol
1.14
0.66
mg/kg wet
1.667
68
39-126
13
20
2,4-Dichlorophenol
0.943
0.66
mg/kg wet
1.667
57
40-122
18
20
2,4-Dimethylphenol
1.10
0.33
mg/kg wet
1.667
66
30-127
18
20
2,4-Dinitrophenol
0.520
1.5
mg/kg wet
1.667
31
27-129
3
20 J
2,4-Dinitrotoluene
1.33
0.66
mg/kg wet
1.667
80
48-126
8
20
2,6-Dinitrotoluene
1.34
0.66
mg/kg wet
1.667
81
46-124
11
20
2-Chloronaphthalene
1.06
0.66
mg/kg wet
1.667
63
41-114
18
20
2-Chlorophenol
0.875
0.66
mg/kg wet
1.667
53
34-121
21
20 D
2-Methyl naphthalene
0.919
0.66
mg/kg wet
1.667
55
38-122
17
20
2-Methylphenol
0.952
0.66
mg/kg wet
1.667
57
32-122
18
20
2-Nitrophenol
0.843
0.66
mg/kg wet
1.667
51
36-123
17
20
3,3'-Dichlorobenzidine
1.37
0.66
mg/kg wet
1.667
82
22-121
7
20
3/4-Methyl phenol
0.889
0.66
mg/kg wet
1.667
53
34-119
21
20 D
4,6-Dinitro-2-methylphenol
1.06
1.5
mg/kg wet
1.667
63
29-132
0.3
20 J
4-Bromophenyl phenyl ether
1.23
0.66
mg/kg wet
1.667
74
46-124
11
20
4-Chloro-3-methylphenol
1.09
0.66
mg/kg wet
1.667
65
45-122
12
20
4-Chloroaniline
0.886
0.33
mg/kg wet
1.667
53
17-106
17
20
4-Chlorophenyl phenyl ether
1.21
1.0
mg/kg wet
1.667
72
45-121
13
20
4-Nitrophenol
1.25
0.66
mg/kg wet
1.667
75
30-132
7
20
Acenaphthene
1.15
0.66
mg/kg wet
1.667
69
40-123
14
20
Acenaphthylene
1.21
0.66
mg/kg wet
1.667
73
32-132
16
20
Anthracene
1.37
0.66
mg/kg wet
1.667
82
47-123
10
20
Azobenzene
1.12
0.66
mg/kg wet
1.667
67
39-125
13
20
Benzo(a)anthracene
1.32
0.66
mg/kg wet
1.667
79
49-126
8
20
Benzo(a)pyrene
1.36
0.66
mg/kg wet
1.667
82
45-129
8
20
Benzo(b)fluoranthene
1.33
0.66
mg/kg wet
1.667
80
45-132
9
20
Benzo(g,h,i)perylene
1.38
0.66
mg/kg wet
1.667
83
43-134
9
20
Benzo(k)fluoranthene
1.43
0.66
mg/kg wet
1.667
86
47-132
7
20
Benzoic Acid
BRL
2.0
mg/kg wet
1.667
10-83
20 L
Benzyl alcohol
0.931
0.66
mg/kg wet
1.667
56
29-122
20
20
bis(2-Chloroethoxy)methane
0.886
0.66
mg/kg wet
1.667
53
36-121
18
20
Bis(2-Chloroethyl)ether
0.761
0.66
mg/kg wet
1.667
46
31-120
18
20
Bis(2-chloroisopropyl)ether
0.794
0.33
mg/kg wet
1.667
48
33-131
22
20 D
Bis(2-Ethylhexyl)phthalate
1.38
0.66
mg/kg wet
1.667
83
51-133
9
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
8/21 /19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Prism Work Order: 9070214
Attn: Darin McClure Time Submitted: 7/16/2019 10:05:OOAM
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9GO316 - 3546
LCS Dup (P9G0316-BSD1)
Prepared: 07/19/19 Analyzed: 07/22/19
Butyl benzyl phthalate
1.33
0.33
mg/kg wet
1.667
80
48-132
6
20
Chrysene
1.30
0.66
mg/kg wet
1.667
78
50-124
9
20
Dibenzo(a,h)anthracene
1.04
0.66
mg/kg wet
1.667
63
45-134
8
20
Dibenzofuran
1.16
0.66
mg/kg wet
1.667
69
44-120
14
20
Diethyl phthalate
1.27
0.66
mg/kg wet
1.667
76
50-124
11
20
Dimethyl phthalate
1.24
0.66
mg/kg wet
1.667
74
48-124
12
20
Di-n-butyl phthalate
1.34
0.66
mg/kg wet
1.667
80
51-128
9
20
Di-n-octyl phthalate
1.31
0.33
mg/kg wet
1.667
79
45-140
6
20
Fluoranthene
1.32
0.66
mg/kg wet
1.667
79
50-127
9
20
Fluorene
1.27
0.66
mg/kg wet
1.667
76
43-125
12
20
Hexachlorobenzene
1.21
0.66
mg/kg wet
1.667
73
45-122
11
20
Hexachlorobutadiene
0.801
0.66
mg/kg wet
1.667
48
32-123
21
20 D
Hexachlorocyclopentadiene
0.844
0.66
mg/kg wet
1.667
51
32-117
21
20 D
Hexachloroethane
0.662
0.66
mg/kg wet
1.667
40
28-117
25
20 D
Indeno(1,2,3-cd)pyrene
1.50
0.66
mg/kg wet
1.667
90
45-133
8
20
Isophorone
0.969
0.66
mg/kg wet
1.667
58
30-122
17
20
Naphthalene
0.858
0.66
mg/kg wet
1.667
51
35-123
19
20
Nitrobenzene
0.816
0.33
mg/kg wet
1.667
49
34-122
20
20
N-Nitroso-di-n-propylamine
0.883
0.66
mg/kg wet
1.667
53
36-120
21
20 D
N-Nitrosodiphenylamine
1.48
0.66
mg/kg wet
1.667
89
38-127
12
20
Pentachlorophenol
1.42
1.0
mg/kg wet
1.667
85
25-133
10
20
Phenanthrene
1.31
0.66
mg/kg wet
1.667
79
50-121
11
20
Phenol
0.912
0.66
mg/kg wet
1.667
55
34-121
20
20
Pyrene
1.35
0.66
mg/kg wet
1.667
81
47-127
7
20
Pyridine
0.515
0.33
mg/kg wet
1.667
31
10-60
22
20 D
Surrogate: 2,4,6-Tribromophenol
2.48
mg/kg wet
3.333
74
39-132
Surrogate: 2-Fluorobiphenyl
1.02
mg/kg wet
1.667
61
44-115
Surrogate: 2-Fluorophenol
1.73
mg/kg wet
3.333
52
35-115
Surrogate: Nitrobenzene-d5
0.759
mg/kg wet
1.667
46
37-122
Surrogate: Phenol-d5
1.78
mg/kg wet
3.333
53
34-121
Surrogate: Terphenyl-d14
1.16
mg/kg wet
1.667
70
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130316 - 3546
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P9G0316-MS1)
Source: 9070214-03
Prepared: 07/19/19 Analyzed: 07/22/19
1,2,4-Trichlorobenzene
1.50
0.87
mg/kg dry
2.204
BRL
68
34-118
1,2-Dichlorobenzene
1.50
0.87
mg/kg dry
2.204
BRL
68
33-117
1,3-Dichlorobenzene
1.44
0.87
mg/kg dry
2.204
BRL
65
30-115
1,4-Dichlorobenzene
1.49
0.44
mg/kg dry
2.204
BRL
67
31-115
1-Methyl naphthalene
1.67
0.87
mg/kg dry
2.204
BRL
76
40-119
2,4,5-Trichlorophenol
1.89
0.87
mg/kg dry
2.204
BRL
86
45-121
2,4,6-Trichlorophenol
1.84
0.87
mg/kg dry
2.204
BRL
83
39-126
2,4-Dichlorophenol
1.69
0.87
mg/kg dry
2.204
BRL
77
40-122
2,4-Dimethylphenol
1.98
0.44
mg/kg dry
2.204
BRL
90
30-127
2,4-Dinitrophenol
1.60
2.0
mg/kg dry
2.204
BRL
73
27-129
2,4-Dinitrotoluene
1.99
0.87
mg/kg dry
2.204
BRL
90
48-126
2,6-Dinitrotoluene
2.09
0.87
mg/kg dry
2.204
BRL
95
46-124
2-Chloronaphthalene
1.82
0.87
mg/kg dry
2.204
BRL
82
41-114
2-Chlorophenol
1.80
0.87
mg/kg dry
2.204
BRL
82
34-121
2-Methyl naphthalene
1.63
0.87
mg/kg dry
2.204
BRL
74
38-122
2-Methylphenol
1.85
0.87
mg/kg dry
2.204
BRL
84
32-122
2-Nitrophenol
1.61
0.87
mg/kg dry
2.204
BRL
73
36-123
3,3'-Dichlorobenzidine
2.02
0.87
mg/kg dry
2.204
BRL
92
22-121
3/4-Methyl phenol
1.73
0.87
mg/kg dry
2.204
BRL
79
34-119
4,6-Dinitro-2-methylphenol
1.74
2.0
mg/kg dry
2.204
BRL
79
29-132
4-Bromophenyl phenyl ether
1.89
0.87
mg/kg dry
2.204
BRL
86
46-124
4-Chloro-3-methylphenol
1.75
0.87
mg/kg dry
2.204
BRL
79
45-122
4-Chloroaniline
1.54
0.44
mg/kg dry
2.204
BRL
70
17-106
4-Chlorophenyl phenyl ether
1.91
1.3
mg/kg dry
2.204
BRL
87
45-121
4-Nitrophenol
1.91
0.87
mg/kg dry
2.204
BRL
87
30-132
Acenaphthene
1.96
0.87
mg/kg dry
2.204
BRL
89
40-123
Acenaphthylene
2.00
0.87
mg/kg dry
2.204
BRL
91
32-132
Anthracene
2.01
0.87
mg/kg dry
2.204
BRL
91
47-123
Azobenzene
1.74
0.87
mg/kg dry
2.204
BRL
79
39-125
Benzo(a)anthracene
1.95
0.87
mg/kg dry
2.204
BRL
89
49-126
Benzo(a)pyrene
2.01
0.87
mg/kg dry
2.204
BRL
91
45-129
Benzo(b)fluoranthene
1.98
0.87
mg/kg dry
2.204
BRL
90
45-132
Benzo(g,h,i)perylene
2.07
0.87
mg/kg dry
2.204
BRL
94
43-134
Benzo(k)fluoranthene
2.07
0.87
mg/kg dry
2.204
BRL
94
47-132
Benzoic Acid
1.34
2.6
mg/kg dry
2.204
BRL
61
10-83
Benzyl alcohol
1.84
0.87
mg/kg dry
2.204
BRL
84
29-122
bis(2-Chloroethoxy)methane
1.63
0.87
mg/kg dry
2.204
BRL
74
36-121
Bis(2-Chloroethyl)ether
1.45
0.87
mg/kg dry
2.204
BRL
66
31-120
Bis(2-chloroisopropyl)ether
1.64
0.44
mg/kg dry
2.204
BRL
74
33-131
Bis(2-Ethylhexyl)phthalate
2.10
0.87
mg/kg dry
2.204
BRL
95
51-133
Butyl benzyl phthalate
1.99
0.44
mg/kg dry
2.204
BRL
90
48-132
Chrysene
1.93
0.87
mg/kg dry
2.204
BRL
88
50-124
Dibenzo(a,h)anthracene
1.56
0.87
mg/kg dry
2.204
BRL
71
45-134
Dibenzofuran
1.87
0.87
mg/kg dry
2.204
BRL
85
44-120
Diethyl phthalate
1.93
0.87
mg/kg dry
2.204
BRL
88
50-124
Dimethyl phthalate
1.93
0.87
mg/kg dry
2.204
BRL
88
48-124
J
J
J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91130316 - 3546
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P9G0316-MS1)
Source: 9070214-03
Prepared: 07/19/19 Analyzed: 07/22/19
Di-n-butyl phthalate
1.99
0.87
mg/kg dry
2.204
BRL
90
51-128
Di-n-octyl phthalate
1.95
0.44
mg/kg dry
2.204
BRL
88
45-140
Fluoranthene
1.95
0.87
mg/kg dry
2.204
BRL
88
50-127
Fluorene
2.00
0.87
mg/kg dry
2.204
BRL
91
43-125
Hexachlorobenzene
1.83
0.87
mg/kg dry
2.204
BRL
83
45-122
Hexachlorobutadiene
1.57
0.87
mg/kg dry
2.204
BRL
71
32-123
Hexachlorocyclopentadiene
1.51
0.87
mg/kg dry
2.204
BRL
69
32-117
Hexachloroethane
1.46
0.87
mg/kg dry
2.204
BRL
66
28-117
Indeno(1,2,3-cd)pyrene
2.19
0.87
mg/kg dry
2.204
BRL
99
45-133
Isophorone
1.72
0.87
mg/kg dry
2.204
BRL
78
30-122
Naphthalene
1.60
0.87
mg/kg dry
2.204
BRL
73
35-123
Nitrobenzene
1.59
0.44
mg/kg dry
2.204
BRL
72
34-122
N-Nitroso-di-n-propylamine
1.72
0.87
mg/kg dry
2.204
BRL
78
36-120
N-Nitrosodiphenylamine
2.26
0.87
mg/kg dry
2.204
BRL
102
38-127
Pentachlorophenol
2.18
1.3
mg/kg dry
2.204
BRL
99
25-133
Phenanthrene
1.99
0.87
mg/kg dry
2.204
BRL
90
50-121
Phenol
1.81
0.87
mg/kg dry
2.204
BRL
82
34-121
Pyrene
1.95
0.87
mg/kg dry
2.204
BRL
89
47-127
Pyridine
0.287
0.44
mg/kg dry
2.204
BRL
13
20-150
M, J
Surrogate: 2,4,6-Tribromophenol
3.81
mg/kg dry
4.409
87
39-132
Surrogate: 2-Fluorobiphenyl
1.78
mg/kg dry
2.204
81
44-115
Surrogate: 2-Fluorophenol
3.67
mg/kg dry
4.409
83
35-115
Surrogate: Nitrobenzene-d5
1.46
mg/kg dry
2.204
66
37-122
Surrogate: Phenol-d5
3.53
mg/kg dry
4.409
80
34-121
Surrogate: Terphenyl-d14
1.71
mg/kg dry
2.204
78
54-127
Matrix Spike Dup (P9GO316-MSD1)
Source: 9070214-03
Prepared:
07/19/19
Analyzed: 07/22/19
1,2,4-Trichlorobenzene
1.47
0.87
mg/kg dry
2.202
BRL
67
34-118
2
20
1,2-Dichlorobenzene
1.42
0.87
mg/kg dry
2.202
BRL
65
33-117
5
20
1,3-Dichlorobenzene
1.37
0.87
mg/kg dry
2.202
BRL
62
30-115
5
20
1,4-Dichlorobenzene
1.41
0.44
mg/kg dry
2.202
BRL
64
31-115
6
20
1-Methyl naphthalene
1.68
0.87
mg/kg dry
2.202
BRL
76
40-119
0.6
20
2,4,5-Trichlorophenol
1.92
0.87
mg/kg dry
2.202
BRL
87
45-121
2
35
2,4,6-Trichlorophenol
1.87
0.87
mg/kg dry
2.202
BRL
85
39-126
2
20
2,4-Dichlorophenol
1.69
0.87
mg/kg dry
2.202
BRL
77
40-122
0.06
20
2,4-Dimethylphenol
1.97
0.44
mg/kg dry
2.202
BRL
90
30-127
0.08
20
2,4-Dinitrophenol
1.65
2.0
mg/kg dry
2.202
BRL
75
27-129
3
20 J
2,4-Dinitrotoluene
2.08
0.87
mg/kg dry
2.202
BRL
94
48-126
4
20
2,6-Dinitrotoluene
2.18
0.87
mg/kg dry
2.202
BRL
99
46-124
4
20
2-Chloronaphthalene
1.82
0.87
mg/kg dry
2.202
BRL
83
41-114
0.3
20
2-Chlorophenol
1.72
0.87
mg/kg dry
2.202
BRL
78
34-121
5
20
2-Methyl naphthalene
1.63
0.87
mg/kg dry
2.202
BRL
74
38-122
0.07
20
2-Methylphenol
1.80
0.87
mg/kg dry
2.202
BRL
82
32-122
3
20
2-Nitrophenol
1.58
0.87
mg/kg dry
2.202
BRL
72
36-123
2
20
3,3'-Dichlorobenzidine
1.95
0.87
mg/kg dry
2.202
BRL
89
22-121
3
20
3/4-Methyl phenol
1.68
0.87
mg/kg dry
2.202
BRL
76
34-119
3
20
4,6-Dinitro-2-methylphenol
1.77
2.0
mg/kg dry
2.202
BRL
80
29-132
2
20 J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
8/21/19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Reporting
Result Limit Units
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P91130316 - 3546
Matrix Spike Dup (P9G0316-MSD1)
Source: 9070214-03
Prepared: 07/19/19 Analyzed: 07/22/19
4-Bromophenyl phenyl ether
1.93
0.87
mg/kg dry
2.202
BRL
88
46-124
2
20
4-Chloro-3-methyl phenol
1.84
0.87
mg/kg dry
2.202
BRL
84
45-122
5
20
4-Chloroaniline
1.55
0.44
mg/kg dry
2.202
BRL
71
17-106
1
20
4-Chlorophenyl phenyl ether
1.93
1.3
mg/kg dry
2.202
BRL
88
45-121
1
20
4-Nitrophenol
1.97
0.87
mg/kg dry
2.202
BRL
89
30-132
3
20
Acenaphthene
1.98
0.87
mg/kg dry
2.202
BRL
90
40-123
1
20
Acenaphthylene
2.03
0.87
mg/kg dry
2.202
BRL
92
32-132
1
20
Anthracene
2.11
0.87
mg/kg dry
2.202
BRL
96
47-123
5
20
Azobenzene
1.76
0.87
mg/kg dry
2.202
BRL
80
39-125
1
20
Benzo(a)anthracene
2.01
0.87
mg/kg dry
2.202
BRL
91
49-126
3
20
Benzo(a)pyrene
2.08
0.87
mg/kg dry
2.202
BRL
94
45-129
3
20
Benzo(b)fluoranthene
2.09
0.87
mg/kg dry
2.202
BRL
95
45-132
6
20
Benzo(g,h,i)perylene
2.08
0.87
mg/kg dry
2.202
BRL
94
43-134
0.2
20
Benzo(k)fluoranthene
2.12
0.87
mg/kg dry
2.202
BRL
96
47-132
2
20
Benzoic Acid
1.46
2.6
mg/kg dry
2.202
BRL
66
10-83
9
20 J
Benzyl alcohol
1.83
0.87
mg/kg dry
2.202
BRL
83
29-122
0.7
20
bis(2-Chloroethoxy)methane
1.62
0.87
mg/kg dry
2.202
BRL
74
36-121
0.3
20
Bis(2-Chloroethyl)ether
1.68
0.87
mg/kg dry
2.202
BRL
76
31-120
15
20
Bis(2-chloroisopropyl)ether
1.56
0.44
mg/kg dry
2.202
BRL
71
33-131
5
20
Bis(2-Ethylhexyl)phthalate
2.12
0.87
mg/kg dry
2.202
BRL
96
51-133
0.9
20
Butyl benzyl phthalate
2.03
0.44
mg/kg dry
2.202
BRL
92
48-132
2
20
Chrysene
1.97
0.87
mg/kg dry
2.202
BRL
89
50-124
2
20
Dibenzo(a,h)anthracene
1.57
0.87
mg/kg dry
2.202
BRL
71
45-134
0.9
20
Dibenzofuran
1.89
0.87
mg/kg dry
2.202
BRL
86
44-120
0.9
20
Diethyl phthalate
2.02
0.87
mg/kg dry
2.202
BRL
92
50-124
4
20
Dimethyl phthalate
2.00
0.87
mg/kg dry
2.202
BRL
91
48-124
3
20
Di-n-butyl phthalate
2.05
0.87
mg/kg dry
2.202
BRL
93
51-128
3
20
Di-n-octyl phthalate
2.04
0.44
mg/kg dry
2.202
BRL
93
45-140
4
20
Fluoranthene
1.99
0.87
mg/kg dry
2.202
BRL
90
50-127
2
20
Fluorene
2.04
0.87
mg/kg dry
2.202
BRL
93
43-125
2
20
Hexachlorobenzene
1.87
0.87
mg/kg dry
2.202
BRL
85
45-122
2
20
Hexachlorobutadiene
1.49
0.87
mg/kg dry
2.202
BRL
67
32-123
5
20
Hexachlorocyclopentadiene
1.53
0.87
mg/kg dry
2.202
BRL
69
32-117
1
20
Hexachloroethane
1.36
0.87
mg/kg dry
2.202
BRL
62
28-117
7
20
Indeno(1,2,3-cd)pyrene
2.28
0.87
mg/kg dry
2.202
BRL
104
45-133
4
20
Isophorone
1.72
0.87
mg/kg dry
2.202
BRL
78
30-122
0.3
20
Naphthalene
1.56
0.87
mg/kg dry
2.202
BRL
71
35-123
3
20
Nitrobenzene
1.56
0.44
mg/kg dry
2.202
BRL
71
34-122
2
20
N-Nitroso-di-n-propylamine
1.69
0.87
mg/kg dry
2.202
BRL
77
36-120
2
20
N-Nitrosodiphenylamine
2.30
0.87
mg/kg dry
2.202
BRL
104
38-127
2
20
Pentachlorophenol
2.32
1.3
mg/kg dry
2.202
BRL
105
25-133
6
20
Phenanthrene
2.01
0.87
mg/kg dry
2.202
BRL
91
50-121
1
20
Phenol
1.75
0.87
mg/kg dry
2.202
BRL
80
34-121
3
20
Pyrene
2.01
0.87
mg/kg dry
2.202
BRL
91
47-127
3
20
Pyridine
0.256
0.44
mg/kg dry
2.202
BRL
12
20-150
12
60 M, J
Surrogate: 2,4,6-Tribromophenol
3.88
mg/kg dry
4.404
88
39-132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
8/21 /19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01
Attn: Darin McClure
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting
Analyte Result Limit Units
Batch P9GO316 - 3546
Prism Work Order: 9070214
Time Submitted: 7/16/2019 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P9G0316-MSD1)
Source: 9070214-03
Prepared: 07/19/19 Analyzed: 07/22/19
Surrogate: 2-Fluorobiphenyl
1.75
mg/kg dry
2.202
80
44-115
Surrogate: 2-Fluorophenol
3.42
mg/kg dry
4.404
78
35-115
Surrogate: Nitrobenzene-d5
1.40
mg/kg dry
2.202
63
37-122
Surrogate: Phenol-d5
3.37
mg/kg dry
4.404
76
34-121
Surrogate: Terphenyl-d14
1.72
mg/kg dry
2.202
78
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
8/21 /19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Prism Work Order: 9070214
Attn: Darin McClure Time Submitted: 7/16/2019 10:05:OOAM
409 Rogers View Court
Raleigh, NC 27610
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9G0500 - 7471 B
Blank (P9G0500-BLK1)
Prepared & Analyzed: 07/31/19
Mercury
BRL
0.050
mg/kg wet
BL
LCS (P9G0500-BS1)
Prepared & Analyzed: 07/31/19
Mercury
0.446
0.050
mg/kg wet
0.4167 107
80-120
Matrix Spike (P9G0500-MS1)
Source: 9070214-11
Prepared & Analyzed: 07/31/19
Mercury
0.505
0.057
mg/kg dry
0.4756 BRL 106
80-120
Matrix Spike Dup (P9G0500-MSD1)
Source: 9070214-11
Prepared & Analyzed: 07/31/19
Mercury
0.491
0.057
mg/kg dry
0.4756 BRL 103
80-120 3 20
Batch P9G0507 - 3050B
Blank (P9G0507-BLK1)
Prepared: 07/31/19 Analyzed: 08/01/19
Arsenic
BRL
1.0
mg/kg wet
Barium
BRL
10
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Chromium
BRL
1.0
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Silver
BRL
0.50
mg/kg wet
LCS (P9G0507-BS1)
Prepared: 07/31/19 Analyzed: 08/01/19
Arsenic
13.9
1.0
mg/kg wet
12.50 111
80-120
Barium
14.3
10
mg/kg wet
12.50 114
80-120
Cadmium
13.8
0.50
mg/kg wet
12.50 110
80-120
Chromium
14.7
1.0
mg/kg wet
12.50 118
80-120
Lead
13.9
1.0
mg/kg wet
12.50 111
80-120
Selenium
13.6
1.0
mg/kg wet
12.50 109
80-120
Silver
5.44
0.50
mg/kg wet
5.000 109
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
8/21 /19
Mid -Atlantic Associates, Inc. - Raleigh Project: 3021.01 Prism Work Order: 9070214
Attn: Darin McClure Time Submitted: 7/16/2019 10:05:OOAM
409 Rogers View Court
Raleigh, NC 27610
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9G0507 - 3050B
Matrix Spike (P9G0507-MS1)
Source: 9070214-01
Prepared: 07/31/19 Analyzed: 08/01/19
Arsenic
19.6
1.4
mg/kg dry
17.58
0.829
106
75-125
Barium
50.3
14
mg/kg dry
17.58
39.7
60
75-125
M
Cadmium
18.9
0.70
mg/kg dry
17.58
BRL
107
75-125
Chromium
23.0
1.4
mg/kg dry
17.58
2.39
117
75-125
Lead
29.8
1.4
mg/kg dry
17.58
12.7
97
75-125
Selenium
18.5
1.4
mg/kg dry
17.57
BRL
105
75-125
Silver
7.75
0.70
mg/kg dry
7.031
BRL
110
75-125
Matrix Spike Dup (P9G0507-MSD1)
Source: 9070214-01
Prepared:
07/31/19 Analyzed: 08/01/19
Arsenic
19.6
1.4
mg/kg dry
17.58
0.829
107
75-125
0.2
20
Barium
46.4
14
mg/kg dry
17.58
39.7
38
75-125
8
20 M
Cadmium
19.0
0.70
mg/kg dry
17.58
BRL
108
75-125
0.5
20
Chromium
23.0
1.4
mg/kg dry
17.58
2.39
117
75-125
0.04
20
Lead
30.2
1.4
mg/kg dry
17.58
12.7
100
75-125
1
20
Selenium
18.5
1.4
mg/kg dry
17.57
BRL
105
75-125
0.03
20
Silver
7.84
0.70
mg/kg dry
7.031
BRL
112
75-125
1
20
Post Spike (P9G0507-PS1)
Source: 9070214-01
Prepared
& Analyzed:
07/31/19
Arsenic
0.485
mg/L
0.5001
0.0236
92
75-125
Barium
1.21
mg/L
0.5000
1.13
17
75-125
P
Cadmium
0.447
mg/L
0.5000
0.000816
89
75-125
Chromium
0.516
mg/L
0.5001
0.0679
90
75-125
Lead
0.701
mg/L
0.5001
0.362
68
75-125
P
Selenium
0.450
mg/L
0.4999
-0.00406
90
75-125
Silver
0.180
mg/L
0.2000
-0.00177
90
75-125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/Time
9070214-01
P9G0396
30
g 30 g
07/24/19
16:45
9070214-02
P9G0396
30
g 30 g
07/24/19
16:45
9070214-03
P9G0396
30
g 30 g
07/24/19
16:45
9070214-04
P9G0396
30
g 30 g
07/24/19
16:45
9070214-05
P9G0396
30
g 30 g
07/24/19
16:45
9070214-06
P9G0396
30
g 30 g
07/24/19
16:45
9070214-07
P9G0396
30
g 30 g
07/24/19
16:45
9070214-08
P9G0396
30
g 30 g
07/24/19
16:45
9070214-09
P9G0396
30
g 30 g
07/24/19
16:45
9070214-10
P9G0396
30
g 30 g
07/24/19
16:45
9070214-11
P9G0396
30
g 30 g
07/24/19
16:45
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
9070214-01
P9G0316
30
g 1 mL
07/19/19 13:10
9070214-02
P9G0316
30.05
g 1 mL
07/19/19 13:10
9070214-03
P9G0316
30.1
g 1 mL
07/19/19 13:10
9070214-04
P9G0316
30.09
g 1 mL
07/19/19 13:10
9070214-05
P9G0316
30.07
g 1 mL
07/19/19 13:10
9070214-06
P9G0316
30.1
g 1 mL
07/19/19 13:10
9070214-07
P9G0316
30.17
g 1 mL
07/19/19 13:10
9070214-08
P9G0316
30.08
g 1 mL
07/19/19 13:10
9070214-09
P9G0316
30.08
g 1 mL
07/19/19 13:10
9070214-10
P9G0316
30.06
g 1 mL
07/19/19 13:10
9070214-11
P9G0316
30.02
g 1 mL
07/19/19 13:10
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
9070214-01
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-02
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-03
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-04
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-05
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-06
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-07
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-07
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-08
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-09
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-09
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-10
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-11
P9G0507
2
g 50 mL
07/31/19
7:40
9070214-11
P9G0507
2
g 50 mL
07/31/19
7:40
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
9070214-01
P9G0500
0.6
g 50 mL
07/31/19
9:20
9070214-02
P9G0500
0.6
g 50 mL
07/31/19
9:20
9070214-03
P9G0500
0.6
g 50 mL
07/31/19
9:20
9070214-04
P9G0500
0.6
g 50 mL
07/31/19
9:20
9070214-05
P9G0500
0.6
g 50 mL
07/31/19
9:20
9070214-06
P9G0500
0.6
g 50 mL
07/31/19
9:20
9070214-07
P9G0500
0.6
g 50 mL
07/31/19
9:20
9070214-08
P9G0500
0.6
g 50 mL
07/31/19
9:20
9070214-09
P9G0500
0.6
g 50 mL
07/31/19
9:20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: 7471E
Lab Number Batch Initial Final Date/Time
9070214-10 P9G0500 0.6 g 50 mL 07/31/19 9:20
9070214-11 P9G0500 0.6 g 50 mL 07/31/19 9:20
Prep Method: 5035
Lab Number Batch Initial Final Date/Time
9070214-01
P9G0319
5.82
g
5 mL
07/19/19 14:28
9070214-02
P9G0319
5.24
g
5 mL
07/19/19 14:28
9070214-03
P9G0345
5.44
g
5 mL
07/22/19 10:00
9070214-04
P9G0319
6.01
g
5 mL
07/19/19 14:28
9070214-05
P9G0319
5.53
g
5 mL
07/19/19 14:28
9070214-06
P9G0319
6.33
g
5 mL
07/19/19 14:28
9070214-07
P9G0319
5.53
g
5 mL
07/19/19 14:28
9070214-08
P9G0319
5.67
g
5 mL
07/19/19 14:28
9070214-09
P9G0319
5.04
g
5 mL
07/19/19 14:28
9070214-10
P9G0319
5.58
g
5 mL
07/19/19 14:28
9070214-11
P9G0319
4.86
g
5 mL
07/19/19 14:28
Subcontracted Analyses
The following analyses were subcontracted to ALS -
Rochester, NY
Lab Number
Analysis
9070214-07 Hexavalent Chromium (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

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ALS
August 16, 2019
Angela Overcash
Prism Laboratories, Inc.
P.O. Box 240543
Charlotte, NC 28224-0543
Laboratory Results for: 9070214
Dear Angela,
Service Request No:R1907337
Enclosed are the results of the sample(s) submitted to our laboratory August 06, 2019
For your reference, these analyses have been assigned our service request number R1907337.
All testing was performed according to our laboratory's quality assurance program and met the
requirements of the TNI standards except as noted in the case narrative report. Any testing not
included in the lab's accreditation is identified on a Non -Certified Analytes report. All results are
intended to be considered in their entirety. ALS Environmental is not responsible for use of less than
the complete report. Results apply only to the individual samples submitted to the lab for analysis, as
listed in the report. The measurement uncertainty of the results included in this report is within that
expected when using the prescribed method(s), and represented by Laboratory Control Sample
control limits. Any events, such as QC failures or Holding Time exceedances, which may add to the
uncertainty are explained in the report narrative or are flagged with qualifiers. The flags are explained
in the Report Qualifiers and Definitions page of this report.
Please contact me if you have any questions. My extension is 7475. You may also contact me via
email at [e-mail].
Respectfully submitted,
ALS Group USA, Corp. dba ALS Environmental
n
Meghan Pedro
Project Manager
ADDRESS 1565 Jefferson Road, Building 300. Suite 360, Rochester, NY 14623
PHONE [phone] FP.X [phone]
A-S (41f:Ut' u=l,
dba ALS Environmental
1 of 24

A^LS _'rule mmentaii
Narrative Documents
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsgiobal.com
2 of 24

1565 Jefferson Rd, Building 300, Rochester, NY 14623 1 585-288-5380 1 www.aisgiobal.com
ALSr
Client: Prism Laboratories, Inc. Service Request: R1907337
Project: 9070214 Date Received: 08/06/2019
Sample Matrix: Soil
CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains
analytical results for samples for the Tier 11 level requested by the client.
Sample Receipt:
One soil sample was received for analysis at ALS Environmental on 08/06/2019. Any discrepancies upon initial sample
inspection are annotated on the sample receipt and preservation form included within this report. The samples were stored at
minimum in accordance with the analytical method requirements.
General Chemistry:
No significant anomalies were noted with this analysis.
41V)A- 60
Approved by Date
08/16/2019
3 of 24

AALS nuir®nmentat
SAMPLE DETECTION SUMMARY
LIENS' ID: SS-7 Lab ID: R1907337-001
Analyte Results Flag MDL MRL Units Method
Chromium, Hexavalent 0.45
Chromium, Hexavalent 0.41
Total Solids 58.5
0.07 0.66 mg/Kg 7199
0.07 0.66 mg/Kg 7199
Percent ALS SOP
4 of 24

AAL S u �� r c;g n m e n t a q
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.aisglobal.com
5 of 24

Client: Prism Laboratories, Inc.
Project: 9070214
SAMPLE CROSS-REFERENCE
SAMPLE # CLIENT SAMPLE ID
R1907337-001 SS-7
Service Request:R1907337
DATE TIME
7/12/2019 1530
6 of 24
Printed 8/16/2019 12:09:01 PM Sample Summary

14
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R1r9O7337 5
ACooler Receipt and Preservation Check Form`'4itlgl�llgqlllqlqqllq�lqql>gtl�1i
Prujeif L t r_ }� FDUtrT Number
Coder received on fl /9 by: COURFER: ALL, UPS F.fSF . VFI OCITY CLIENT
I a'nt Ci;itlaly vials on .xU id: ofcunlr", Y
(:ustody palm pnllxxlr camplacd ilnk,,lprsvd.}? s.�
Utd all bbnlcs Misr in c�S cuadldan luatroktst}?�'ti
a 6ircir: eo a hry Ice Zell packs Pte7e111T
is
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Perehlwate salntnrS hnvorcq.lrrd head". Ce?
Did VOA vials. Alk,or Su18dc have sip' bubbles?
Y N : A
Y N
6
Miuedrd the Wit% W:guuh^ AIL-WOC ..€ ti
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Soli VpA rcaiscd as: IWIL kno aet 5Eid -A
1
S. Tanperatlue RodinL tkRr: !r Tbnc. Ji Ul IO IR iRN10 From: Tnnp Dank Ipk ott
Ohsrr,n! Temp faC1
1
Caredicm
Ca'redcd'I'cmp (`C)
A
Temp from: Fype of Mile .
Within 0.G°C?
N
Y N
Y N
Y N
Y N Y N
Y N
If <rCr "wes-01ci (re,=1'
N
Y N
Y N
Y N
Y N Y N
Y N
tfout of Tcmperature.note psckingiecroodlNon: Ice moiled Poorly AKkW(described below) sarne Day Rule
&Client Approval to Run Sampks:____ _ Sanding Approvl Clienn�t&&.are.% dropoff Cftrntnaifiedby:
All samples held in Mwagr twatiuw,. - _ by
SOTS samples placed in storage location: T by an _ at J
Coolcr 9rwkdownlPresenation Cbeek": Wle: _ TiMT by^ _
9, Were all bottle labels Complete (i C. analysis, Pf6scK%Um,
10. Did all bottle labels and L%g agree snlh euslah papers.' � NO
on I Wert ced owtainem wed rm she ILY[, irw imtrd? NO
1? Woe 503 5 vials acceptable(no extra label& not lcakinal? YES NO
I _ ... aT..'--t..,.. -� T.11.M M.— L.. 11-1 9Y,h
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I � T yr e6[rL rd t[er aepMnay]
Ddtle lot numbers:,/ _
Fxplain all Diserepane�l 1 cl),fia Cannowls:
CI.RES MILK
OU FLOT
WROD HUR
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PN SLIM
S03 MARRS
ALS REV
labels sccandary reviewed by—�
PC Secondary Review. - «significant air bubbles: VOA t 5.6 mm : WC%I in. diameter
P.11NFRANE-.(sAQC%r rCmrdlsa:Cmic, R-0 ri6AM ]11vtB
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A
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.aisglobal.com
9 of 24

AL5
REPORT QUALIFIERS AND DEFINITIONS
U Analyte was analyzed for but not detected.
The sample quantitation limit has been
corrected for dilution and for percent
moisture, unless otherwise noted in the case
narrative.
Estimated value due to either being a
Tentatively Identified Compound (TIC) or
that the concentration is between the MRL
and the MDL. Concentrations are not verified
within the linear range of the calibration. For
DoD: concentration >40% difference between
two GC columns (pesticides/Arclors).
B Analyte was also detected in the associated
method blank at a concentration that may
have contributed to the sample result.
E Inorganics- Concentration is estimated due to
the serial dilution was outside control limits.
E Organics- Concentration has exceeded the
calibration range for that specific analysis.
D Concentration is a result of a dilution,
typically a secondary analysis of the sample
due to exceeding the calibration range or that
a surrogate has been diluted out of the sample
and cannot be assessed.
* Indicates that a quality control parameter has
exceeded laboratory limits. Under the
"Notes" column of the Form I, this qualifier
denotes analysis was performed out of
Holding Time.
+ Correlation coefficient for MSA is <0.995.
N Inorganics- Matrix spike recovery was outside
laboratory limits.
N Organics- Presumptive evidence of a compound
(reported as a TIC) based on the MS library search.
S Concentration has been determined using Method
of Standard Additions (MSA).
W Post -Digestion Spike recovery is outside control
limits and the sample absorbance is <50% of the
spike absorbance.
P Concentration >40% difference between the two
GC columns.
C Confirmed by GC/MS
Q DoD reports: indicates a pesticide/Aroclor is not
confirmed (>100% Difference between two GC
columns).
X See Case Narrative for discussion.
MRL Method Reporting Limit. Also known as:
LOQ Limit of Quantitation (LOQ)
The lowest concentration at which the method
analyte may be reliably quantified under the
method conditions.
MDL Method Detection Limit. A statistical value
derived from a study designed to provide the lowest
concentration that will be detected 99% of the
time. Values between the MDL and MRL are
estimated (see J qualifier).
H Analysis was performed out of hold time for LOD Limit of Detection. A value at or above the MDL
tests that have an "immediate" hold time which has been verified to be detectable.
criteria. ND Non -Detect. Analyte was not detected at the
# Spike was diluted out. concentration listed. Same as U qualifier.
1� p N accogo4
tea*
�4 o,
U
¢ e • ' 2
Rochester Lab ID # for State Certifications'
Connecticut ID # PH0556
Maine ID #NY0032
Pennsylvania ID# 68-786
Delaware Approved
New Hampshire ID # 2941
Rhode Island ID # 158
DoD ELAP #65817
New York ID # 10145
Virginia #460167
Florida ID # E87674
North Carolina #676
Analyses were performed according to our laboratory's NELAP-approved quality assurance program and any applicable state or agency
requirements. The test results meet requirements of the current NELAP[fNI standards or state or agency requirements, where applicable, except as
noted in the case narrative. Since not all analyte/method/matrix combinations are offered for state/NELAC accreditation, this report may contain
results which are not accredited- For a specific list of accredited analytes, contact the laboratory or go to
ltittrs�•licsn�tir.slsr_fnhal comrloc�trnnrCamencas[norila-::merccalxrsalttiew-voritlruchester�m-Ironmental
10 of 24
P\INTRANETQAQC\Forms Connolled\QUALIF munne iev i,doc 0/28/I8

ALS Laboratory Group
Acronyms
ASTM
American Society for Testing and Materials
A2LA
American Association for Laboratory Accreditation
CARB
California Air Resources Board
CAS Number
Chemical Abstract Service registry Number
CFC
Chlorofluorocarbon
CFU
Colony -Forming Unit
DEC
Department of Environmental Conservation
DEQ
Department of Environmental Quality
DHS
Department of Health Services
DOE
Department of Ecology
DOH
Department of Health
EPA
U. S. Environmental Protection Agency
ELAP
Environmental Laboratory Accreditation Program
GC
Gas Chromatography
GC/MS
Gas Chromatography/Mass Spectrometry
LUFT
Leaking Underground Fuel Tank
M
Modified
MCL
Maximum Contaminant Level is the highest permissible concentration of a
substance allowed in drinking water as established by the USEPA.
MDL
Method Detection Limit
MPN
Most Probable Number
MRL
Method Reporting Limit
NA
Not Applicable
NC
Not Calculated
NCASI
National Council of the Paper Industry for Air and Stream Improvement
ND
Not Detected
NIOSH
National Institute for Occupational Safety and Health
PQL
Practical Quantitation Limit
RCRA
Resource Conservation and Recovery Act
SIM
Selected Ion Monitoring
TPH
Total Petroleum Hydrocarbons
tr
Trace level is the concentration of an analyte that is less than the PQL but
greater than or equal to the MDL.
11 of 24

ALS Group USA, Corp.
dba ALS Environmental
Analyst Summary report
Client: Prism Laboratories, Inc. Service Request: R1907337
Project: 9070214/
Sample Name: SS-7 Date Collected: 07/12/19
Lab Code: R1907337-001 Date Received: 08/6/19
Sample Matrix: Soil
Analysis Method Extracted/Digested By Analyzed By
7199 CWOODS CWOODS
ALS SOP GKNIGHT
Printed 8/16/2019 12:09:04 PM Superset Reference:19-0000518566 rev 00
12 of 24

INORGANIC PREPARATION METHODS
A L S
The preparation methods associated with this report are found in these tables unless discussed in the case narrative.
Water/Liquid Matrix
Analytical Method
Preparation Method
200.7
200.2
200.8
200.2
6010C
3005A/3010A
6020A
ILM05.3
9014 Cyanide Reactivity
SW846 Ch7, 7.3.4.2
9034 Sulfide Reactivity
SW846 Ch7 7.3.4.2
9034 Sulfide Acid
Soluble
9030B
9056A Bomb (Halogens)
5050A
9066 Manual Distillation
9065
SM 4500-CN-G
SM 4500-CN-E Residual
Cyanide
SM 4500-CN-E WAD
Cyanide
SM 4SOO-CN-1
Solid/Soil/Non-Aqueous Matrix
Analytical Method
Preparation
Method
6010C
3050B
6020A
3050B
601 OC TCLP (1 31 1)
extract
3005A/3010A
6010 SPLP (1 31 2) extract
3005A/3010A
7196A
3060A
7199
3060A
9056A Halogens/Halides
5050
300.0 Anions/ 350.1/
353.2/ SM 232013/ SM
521 OB 9056A Anions
DI extraction
For analytical methods not listed, the preparation
method is the same as the analytical method
reference.
P:\INTRANET\QAQC\Forms Controlled\Prep Methods Inorganic rev l.doc 1/19/15
13 of 24

ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
14❑f24

A
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsgiobal.com
15 of 24

ALS Group USA, Corp.
dba ALS Environmental
Client: Prism Laboratories, Inc.
Project: 9070214
Sample Matrix: Soil
Sample Name: SS-7
Lab Code: R1907337-001
Analytical Report
Inorganic Parameters
Service Request: R1907337
Date Collected: 07/12/19 15:30
Date Received: 08/06/19 09:50
Basis: Dry
Analysis
Date
Analyte Name
Method
Result Units MRL MDL
Dil. Date Analyzed Extracted Q
Chromium, Hexavalent
7199
0.45 J mg/Kg 0.66 0.07
1 08/14/19 15:11 08/09/19
Chromium, Hexavalent
7199
0.41 J mg/Kg 0.66 0.07
1 08/14/19 15:01 08/09/19
Printed 8/16/2019 12:09:05 PM Superset Reference:19-0000518566 rev 00
16 of 24

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client:
Prism Laboratories, Inc.
Service Request:
R1907337
Project:
9070214
Date Collected:
07/12/19 15:30
Sample Matrix:
Soil
Date Received:
08/06/19 09:50
Sample Name:
SS-7
Basis:
As Received
Lab Code:
R1907337-001
Inorganic Parameters
Analysis Date
Analyte Name Method Result Units MRL MDL Dil. Date Analyzed Extracted Q
Total Solids ALS SOP 58.5 Percent - - 1 08/12/19 08:30 NA
Printed 8/16/2019 12:09:05 PM Superset Reference: [9-0000518566 rev 00
17 of 24

A,AkLS
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.aisglobal.com
18of24

AALUS
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.aisgiobal.com
19 of 24

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: Prism Laboratories, Inc. Service Request: R1907337
Project: 9070214 Date Collected: NA
Sample Matrix: Soil Date Received: NA
Sample Name: Method Blank Basis: Dry
Lab Code: R1907337-MB
Inorganic Parameters
Analysis Date
Anal to Name Method Result Units MRL MDL Dil. Date Analyzed Extracted
Chromium, I lexavalent 7199 0.40 U mg/Kg 0.40 0.05 1 08/1 1/19 14:15 08/09/19
Chromium, Hexavalent 7199 0.40 U mg/Kg 0.40 0.05 1 08/14/19 14:06 08/09/19
Printed 8/16/2019 12:09:05 PM Superset Reference:19-0000518566 rev 00
20 of 24

ALS croup USA, Corp.
dba ALS Environmental
QA/QC Report
Client:
Prism Laboratories, Inc.
Service Request:
R1907337
Project:
9070214
Date Collected:
07/12/19
Sample Matrix:
Soil
Date Received:
08/06/19
Date Analyzed:
08/14/19
Date Extracted:
08/9/19
Matrix Spike Summary
Chromium, Hexavalent
Sample Name:
SS-7
Units:
Ing/Kg
Lab Code:
R1907337-001
Basis:
Dry
Analysis Method:
7199
Prep Method:
EPA 3060A
Matrix Spike
R1907337-001MS 1
Analyte Name
Sample Result Result Spike
Amount % Rec
% Rec Limits
Chromium, Hexavalent
0.45 J
66.5
67.3 98
75-125
Chromium, Hexavalent
0.41 J
67.4
67.3 100
75-125
Results flagged with an asterisk (") indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (PPD) are determined by the software using %aloes in the calculation which have not been rounded.
Printed 9/16/2019 12:09:05 PM 21 of 24 Superset Reference: 19-00005 18566 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: Prism Laboratories, Inc.
Service Request:
R1907337
Project: 9070214
Date Collected:
07/12/19
Sample Matrix: Soil
Date Received:
08/06/19
Date Analyzed:
08/14/19
Date Extracted:
08/9/19
Matrix Spike Summary
Chromium, Hexavalent
Sample Name: SS-7
Units:
mg/Kg
Lab Code: R1907337-001
Basis:
Dry
Analysis Method: 7199
Prep Method: EPA 3060A
Matrix Spike
R1907337-OO1MS2
Analvte Name Sample Result Result Spike
Amount % Rec
% Rec Limits
Chromium, Hexavalent 0.41 J
1020
1100 93
75-125
Chromium, Hexavalent 0.45 J
1070
1100 97
75-125
Results flagged with an asterisk (4) indicate values outside control criteria.
Results flagged with a pound (R) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded
Printed 8/16/2019 12:09:05 PM 22 of 24 Superset Reference: 19-0000518566 rev 00

ALS Group USA, Corp.
dba ALS Environmental
Client: Prism Laboratories, Inc.
Project 9070214
Sample Matrix: Soil
QA/QC Report
Replicate Sample Summary
General Chemistry Parameters
Service Request:
R1907337
Date Collected:
07/12/19
Date Received:
08/06/19
Date Analyzed:
08/14/19
Sample Name:
SS-7
Units: mg/Kg
Lab Code:
R1907337-001
Basis: Dry
Duplicate
Sample
R1907337-
Analysis
Sample
001DUP
Analyte Name
Method MRL
MDL Result
Result
Average RPD RPD Limit
Chromium, 1lexavalent
7199 0.67
0.08 0.45 J
0.42 J
0.433 7 20
Chromium, Hexavalent
7199 0.67
0.08 0.41 J
0.41 J
0.410 <1 20
Results flagged with an asterisk (") indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 8/16/2019 12:09:05 PM 23 of 24 Superset Reference:19-0000518566 rev 00

Client: Prism Laboratories, Inc.
Project: 9070214
Sample Matrix: Soil
ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Lab Control Sample Summary
General Chemistry Parameters
Lab Control Sample
R1907337-LCS
Service Request: R1907337
Date Analyzed: 08/14/19
Units:mg/Kg
Basis:Dry
Analyte Name Analytical Method Result Spike Amount % Rec % Rec Limits
Chromium, Hexavalent 7199 720 682 106 80-120
Chromium, Hexavalent 7199 634 682 93 80-I20
Printed 8/16/2019 12:09:05 PM Superset Reference:19-0000518566 rev 00
24 of 24