23053 Cotton Seed Oil Mill Brownfields Assessment Report 20200110

Via E-Mail
January 10, 2020
NC Brownfields Program Mail Service Center 1646 Raleigh, NC 27699-1646

Attn: Mr. Bill Schmithorst
Re: Brownfields Assessment Report and Environmental Management Plan Former Cotton Seed Oil Mill (BF #23053-19-060)
300 Rampart Street Charlotte, NC H&H Project No. JMC.009
Dear Bill:
On behalf of 300 Rampart Owner, LLC, Hart & Hickman, PC (H&H) has prepared the attached Brownfields Assessment Report in PDF format for the above-referenced site. Also attached for your review is the completed Environmental Management Plan. Should you have any questions
or need any additional information, please feel free to contact me.
Sincerely, Hart & Hickman, PC
Matt Bramblett Principal Attachments: Brownfields Assessment Report Environmental Management Plan
Cc: Mr. Christopher Deppoliti, JMC (via email) Mr. Jason Oriol, Colliers (via email) Ms. Mary Katherine Stukes, Parker Poe (via email) Mr. Robert Sorgel, H&H (via email)

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DRAFT Brownfields Assessment Report Former Cotton Seed Oil Mill
300 Rampart Street Charlotte, North Carolina Brownfields Project No. 23053-19-060 H&H Job No. JMC-009
Table of Contents

1.0 Introduction and Background .................................................................................................... 1
2.0 Brownfields Assessment Activities .............................................................................................. 3
3.0 Sub-Slab Vapor Assessment Activities ....................................................................................... 4
3.1 Sub-Slab Vapor Sampling Methodology ............................................................................. 4
3.2 Sub-Slab Vapor Analytical Results ...................................................................................... 5
4.0 Receptor Survey Activities .......................................................................................................... 7
5.0 Conclusions and Recommendations ......................................................................................... 10

List of Tables
Table 1 Summary of Sub-Slab Vapor and Soil Gas Analytical Results

List of Figures
Figure 1 Site Location Map
Figure 2 Sample Location Map
Figure 3 Receptor Survey Map
List of Appendices
Appendix A Sub-Slab Vapor QA/QC Field Form
Appendix B Laboratory Analytical Report
Appendix C DEQ Worst Case Risk Calculator Output
Appendix D Brownfields Property Receptor Survey Form

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DRAFT Brownfields Assessment Report Former Cotton Seed Oil Mill
300 Rampart Street Charlotte, North Carolina Brownfields Project No. 23053-19-060 H&H Job No. JMC-009
1.0 Introduction and Background
Hart & Hickman, PC (H&H) has prepared this Brownfields Assessment Report on behalf of 300
Rampart Owner, LLC (Prospective Developer or PD) for the former Cotton Seed Oil Mill facility
(Brownfields Project No. 23053-19-060) located at 300 Rampart Street in Charlotte, Mecklenburg
County, North Carolina (Site). A Site location map is provided as Figure 1.

The Site consists of an approximate 2.4-acre parcel of land (Parcel Identification Number
12103209) that is developed with an approximate 65,136-square foot (sq ft) industrial warehouse
building that is currently vacant. The central and eastern portions of the building were constructed
in 1958, and the western portion of the building was constructed in the late 1970s. A Site map is
included as Figure 2.

The subject Site was historically occupied by portions of a Cotton Seed Oil Mill (late 1800s to early
1900s), portions of the Virginia Carolina Chemical (VCC) fertilizer company (early 1900s to mid-
1900s), a lumber milling operation in the 1960s, and a steel pail painting operation in the 1980s.
The Site was then occupied by the Charlotte Salvage Company from the 1980s to the late 2010s.

H&H performed Phase II Environmental Site Assessment (ESA) activities at the Site in August
2019 to evaluate potential areas of environmental concern associated with historical activities
conducted at the Site and on nearby upgradient properties. The results of the Phase II ESA
indicated the presence of arsenic in Site soils at concentrations exceeding North Carolina
Department of Environmental Quality (NC DEQ) Protection of Groundwater (PoG), Residential,
and Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs). Additionally, potentially
elevated levels of chromium and hexavalent chromium were detected in soil samples.

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Groundwater analytical results did not indicate the presence of VOCs, SVOCs, or metals at
concentrations exceeding regulatory standards. Additionally, sub-slab vapor and soil gas analytical
results did not indicate the presence of VOCs at concentrations exceeding regulatory screening
levels.

The PD will perform interior and exterior renovations of the existing Site structure for commercial
use. Future redevelopment at the Site may include demolition of the current Site structure for
construction of a multi-story structure. The Site received a letter of eligibility for entry into the
DEQ Brownfields Program (Brownfields Project No. 23053-19-060) on October 8, 2019.

On October 23, 2019, a kick-off/data gap meeting was held at the Site with the PD, DEQ
Brownfields Program personnel, and H&H to discuss Site history, previous environmental
assessment activities at the Site, proposed redevelopment plans, data gaps, and the proposed
schedule for completing the Brownfields Agreement. DEQ followed-up in an email dated
November 5, 2019 requesting that five sub-slab vapor samples be collected to further assess
potential risks for future use of the Site building. H&H previously sampled sub-slab vapor and soil
gas concentrations during warm weather in August 2019. Results did not indicate a vapor intrusion
condition above NC DEQ Residential or Non-Residential Soil Gas Screening Levels (SGSLs) or
DEQ risk-based target levels.

H&H also conducted a sensitive receptor survey in the vicinity of the Site. Information regarding
the recent assessment activities is provided in the following sections.

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2.0 Brownfields Assessment Activities
In accordance with the DEQ Brownfields Program approved Proposed Scope of Work dated
November 14, 2019, H&H conducted further assessment activities at the Site in December 2019.
The assessment included the collection of sub-slab vapor samples and a receptor survey to further
evaluate Site impacts and their potential associated risks for redevelopment and future Site use.

The assessment activities were conducted in general accordance with the DEQ Inactive Hazardous
Sites Branch (IHSB) Guidelines for Assessment and Cleanup dated October 2015, DEQ’s Division
of Waste Management (DWM) Vapor Intrusion Guidance dated March 2018, the most recent
versions of the U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem
Support (SESD) Field Branches Quality System and Technical Procedures guidance, and the DEQ
approved Proposed Scope of Work. The results of the sub-slab vapor assessment activities are
provided in Section 3.0 and the receptor survey results are provided in Section 4.0. Conclusions and
recommendations based on the results of the assessment activities are provided in Section 5.0.

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3.0 Sub-Slab Vapor Assessment Activities
On December 3, 2019, H&H installed and sampled five sub-slab vapor monitoring points (SSV-1
through SSV-5) within the Site building. Temperatures during the sampling event were between 37
and 46 degrees Fahrenheit. SSV-1 through SSV-3 were installed near the three prior vapor sample
locations. SSV-4 and SSV-5 were installed in the northern and southern portions of the eastern
warehouse building, respectively. Sub-slab vapor sample locations are shown on Figure 2.

3.1 Sub-Slab Vapor Sampling Methodology

H&H drilled through the concrete floor at the five sub-slab vapor monitoring point locations using a
rotary hammer drill and 1½-inch diameter drill bit to advance a pilot hole into the concrete slab to a
depth of approximately 1¾ inches below the surface. A drill guide was then placed in the pilot hole,
and a 5/8-inch diameter drill bit was utilized to advance the boring through the concrete slab.
Following concrete borehole advancement, loose concrete cuttings were removed from the borings,
and a Cox-Colvin Vapor Pin™ (vapor pin) assembly (brass sampling point and silicone sleeve) was
seated in the borehole using an installation/extraction tool and hammer to form an air-tight seal.

After installation and prior to collection of the sub-slab samples, a leak check was conducted by
constructing a shroud around each sub-slab vapor sampling point and Summa sample canister
flooding the air within the shroud with helium gas. Helium concentrations inside the shroud were
measured using a helium gas detector. Using a syringe and three-way valve, the vapor point, Teflon
tubing, and surrounding sand pack was purged of approximately three volumes of air. Following
purging, a sample was collected from the sample tubing outside the shroud and analyzed using the
helium gas detector to ensure that helium concentrations were less than 10% of the helium
concentrations in the shroud.

Following a successful leak check, a laboratory-supplied 1-liter stainless steel Summa sample
canister was connected to an in-line flow controller with attached vacuum gauge. The flow
controller was then connected to the sample tubing using a brass nut and ferrule assembly to form
an air-tight seal. The flow regulator was pre-set by the laboratory to regulate the vapor intake rate to

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approximately 100 milliliters per minute. Once the sample train was assembled, the intake valve on
the canister was fully opened to begin collection of the sub-slab vapor sample. Vacuum readings on
the Summa canister were recorded prior to and following the sampling period to ensure adequate
sample volume was collected. As a quality control measure, negative pressure was maintained
within the canisters at the conclusion of the sampling event.

After sample collection, the Summa canister’s valves were closed prior to the regulator being
disconnected from the canister. The Summa canisters were then placed in laboratory supplied
shipping containers, properly labeled, and shipped under standard chain-of-custody protocols to
Pace Analytical Laboratory (Pace) for analysis of VOCs by EPA Method TO-15. For quality
assurance/quality control purposes, one duplicate sub-slab vapor sample was collected from SSV-4
using a “T”-fitting for simultaneous sample collection into two Summa canisters. The duplicate
sample was also analyzed for VOCs by EPA Method TO-15.

Upon completion of sampling activities, the vapor pins were removed and the concrete surface was
patched with concrete to match the surrounding area. Each sample location was estimated by
measuring from known benchmarks (doorways, walls, etc.).

3.2 Sub-Slab Vapor Analytical Results

The vapor samples were collected during cold weather conditions in December 2019. The sub-slab
vapor analytical results are summarized in Table 1. The laboratory analytical report and chain of
custody record are provided in Appendix B. Sub-slab vapor analytical results were compared to the
February 2018 DEQ DWM Residential and Non-Residential SGSLs.

Laboratory analytical results indicated the presence of low levels of several VOCs at concentrations
above laboratory method detection limits in the sub-slab vapor samples. However, no compounds
were detected in the sub-slab vapor samples at concentrations exceeding the Residential or Non-
Residential SGSLs. Trichloroethene (TCE), a common vapor intrusion compound of concern, was
not detected during the December 2019 sampling event.

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The DEQ DWM SGSLs are conservative and based upon a lifetime incremental cancer risk
(LICR) of 1 x 10-5 for potential carcinogenic effects and a hazard quotient (HQ) of 0.2 for
potential non-carcinogenic effects. The DEQ acceptable cumulative LICR for potential
carcinogenic risks is 1 x 10-4, and the acceptable cumulative risk level for non-carcinogenic risks
is a hazard index (HI) less than 1.

To further evaluate potential risks for structural vapor intrusion into the Site building, H&H used
DEQ’s risk calculator (May 2019) to calculate potential cumulative risks for both residential and
non-residential land use scenarios using the December 2019 cold weather data. H&H calculated the
cumulative risks under a worst-case scenario, using the highest concentration of compounds
detected in the December 2019 sub-slab vapor samples regardless of sample location. The results
of the risk calculations are summarized below and are included in Appendix C.

Land Use Scenario Calculated Cumulative LICR Calculated Cumulative HI
Calculated LICR or HI Exceeds Acceptable Risk Levels?
Residential 2.2 x 10-6 0.065 No
Non-Residential
Worker 1.7 x 10-7 0.0052 No

As shown on the table above, the results of risk calculations using sub-sab vapor data under a worst-
case scenario indicate a calculated LICR and HI below DEQ acceptable risk levels (LICR of 10-6
and HI of 1) for residential or non-residential land use scenarios. These results are consistent with
the August 2019 warm weather vapor data in which there were also no exceedances of SGSLs or
DEQ acceptable risk levels. As such, a vapor intrusion concern does not exist for the Site building.

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4.0 Receptor Survey Activities
On December 31, 2019, H&H conducted receptor survey activities at the Site and nearby area.
Receptor survey activities included an intensive pedestrian and vehicular survey for possible potable
water supply wells, springs, and surface water intakes used as a source of water within a 1,500 ft
radius of the Site. H&H also utilized the online geographic information systems, Mecklenburg
County Well Information System 3.0 and DEQ Source Water Assessment Program (SWAP), to
identify potential potable water sources for properties located within a 1,500 ft radius of the Site. In
addition, H&H identified the locations of main underground and aboveground utilities, and land use
and zoning adjacent to the Site using available Mecklenburg County online resources. A copy of the
completed DEQ Brownfields Property Receptor Survey form is provided as Appendix D, and a
receptor survey map is provided as Figure 3. The results of the receptor survey are summarized
below.

Site and Surrounding Properties
As previously mentioned, the Site consists of an approximately 2.4-acre parcel of land that is
developed with an approximate 65,136 sq ft industrial warehouse building. The central and eastern
portions of the building were constructed in 1958, and the western portion of the building was
constructed in the late 1970s. The Site buildings are currently vacant. The Site is located in a
mixed-use area of Charlotte, North Carolina. Surrounding properties currently consist of the
Penrose Apartments to the north, a multi-occupant commercial property to the northeast, a medical
imaging equipment manufacturing facility to the east, Rampart Street, followed by an automotive
repair facility and a mixed-use property under development (Hub South End) to the southwest, a
dog boarding facility to the west, and commercial properties to the northwest.

Zoning
The Site is zoned as Transit-Oriented Development (TOD-UC). Adjacent properties to the south
and east are also zoned as Transit-Oriented Development (TOD-UC). Adjacent properties to the
north are zoned as Transit-Oriented Development (TOD-MO), while adjacent properties to the west
and southwest are zoned as Transit-Oriented Development (TOD-NC).

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Municipal Water Availability
Municipal water supplied by Charlotte Water is available to the Site and surrounding area. H&H
did not identify sources of public drinking water within 1,500 ft of the Site based on the DEQ
SWAP’s and Mecklenburg County Well Information System 3.0 geographic information system
maps. Based on the Annual Water Quality Report published by the City of Charlotte, the City of
Charlotte obtains raw water from Lake Norman and Mountain Island Lake which are located
approximately 15 miles north and 11 miles northwest of the Site, respectively. H&H observed the
service area map published by Mecklenburg County which indicated that municipal water is
available to the Site and the surrounding area within a 1,500 ft radius of the Site. Additionally,
H&H observed municipal water meters for the Site and surrounding properties during receptor
survey reconnaissance activities.

Water Supply Wells
H&H conducted a pedestrian and vehicular survey of properties within a 1,500 ft radius of the Site
to identify potential water supply wells. H&H also utilized the DEQ SWAP’s geographic
information system map to identify potential potable water supply wells located within a 1,500 ft
radius of the Site. H&H did not identify private water supply wells within 1,500 ft of the Site. A
water supply well was historically located at the subject Site, but it was abandoned by a NC-
licensed well driller in December 2019.

Surface Water Bodies
Surface water bodies are not located at the subject Site. The closest water body is an unnamed
tributary of Irwin Creek, located approximately 1,400 ft north of the Site. Based on the NC DEQ
classification system, Irwin Creek is a Class C surface water body. A Class C surface water body is
defined as “waters protected for uses such as secondary recreation, fishing, wildlife, fish
consumption, aquatic life including propagation, survival and maintenance of biological integrity,
and agriculture. Secondary recreation includes wading, boating, and other uses involving human
body contact with water where such activities take place in an infrequent, unorganized, or incidental
manner.” Irwin Creek flows south through Mecklenburg County and discharges into Sugar Creek
approximately three miles south of the Site.

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Subsurface Structures
H&H conducted a visual reconnaissance in the Site area to identify potential subsurface structures
within 1,000 ft of the subject Site. H&H observed evidence of subsurface utilities including
sanitary sewer, storm sewer, municipal water, natural gas, and/or communications utilities within or
adjacent to Rampart Street (immediately south of the Site). The Site is serviced by natural gas.
Electric service is primarily via overhead lines along Rampart Street. H&H did not observe
structures with crawlspaces and/or basements within a 1,500 ft radius of the Site during visual
reconnaissance.

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5.0 Conclusions and Recommendations
H&H has completed Brownfields assessment activities on the Former Cotton Seed Oil Mill
Brownfields Property (Brownfields Project No. 23053-19-060) located at 300 Rampart Street in
Charlotte, Mecklenburg County, North Carolina. The assessment activities were conducted in
accordance with the DEQ-approved Work Plan and included a receptor survey and sub-slab
vapor sampling to evaluate potential environmental risks associated with redevelopment of the
Site. A summary of the assessment results is provided below.

Receptor Survey
H&H conducted a Brownfields receptor survey for the Site and nearby area. The results of the
receptor survey indicate that municipal water is available to the Site and area within a 1,500-ft
radius of the Site. No sources of public drinking water were identified within 1,500 ft of the Site.
An unnamed tributary of Irwin Creek is located approximately 400 ft east of the Site. H&H
observed evidence of subsurface utilities, including sanitary sewer, storm sewer, municipal
water, and natural gas on the Site and nearby adjacent properties. H&H did not identify obvious
evidence of basements within a 1,000-ft radius of the Site.

Sub-Slab Vapor
H&H collected five sub-slab vapor samples (SSV-1 through SSV-5) within the Site building in cold
weather conditions to further evaluate the potential for vapor intrusion. Laboratory analytical
results did not indicate the presence of VOCs in the sub-slab vapor samples at concentrations
exceeding Residential or Non-Residential SGSLs.

H&H utilized DEQ’s risk calculator (May 2019) to calculate potential cumulative risks under a
worst-case scenario at the Site using the cold weather condition data. The results of the risk
calculations indicate that a vapor intrusion concern does not exist under residential or non-
residential land use scenarios.

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Recommendations
Based on the recent sub-slab vapor sampling results and the results of risk calculations, a vapor
intrusion concern does not exist for the Site building under residential or non-residential use
scenarios. As such, vapor mitigation is not warranted for the Site building, and no vapor mitigation
plan is needed.

H&H recommends completing an Environmental Management Plan (EMP) and obtaining DEQ
approval for the EMP prior to subsurface disturbance. Previously-identified soil impacts can be
managed in accordance with a DEQ Brownfields approved EMP during redevelopment.
Table 1Summary of Sub-Slab Vapor and Soil Gas Analytical ResultsFormer Cotton Seed Oil MillCharlotte, North CarolinaH&H Job No. JMC-009Sample IDSample LocationSlab Thickness (in)Screen Depth (ft bgs)Sample DateAnalytical MethodAcetoneBenzeneBromomethane2-Butanone (MEK)Carbon DisulfideChloroformChloromethaneCyclohexane1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane (Freon 12)1,1-Dichloroethane1,1-Dichloroethylenecis-1,2-DichloroethyleneEthyl AcetateEthylbenzene4-EthyltolueneHeptaneHexane8/29/2019 114 1.1<0.4430.4 5.5<0.38 <0.301.9J 4.1<1.92.2<0.44 <0.53 <0.422.0 2.7 1.9J 2.9 4.212/3/2019 57.2 0.41 J<0.445.0 J 1.2 J<0.38 <0.300.72 J<1.1 <1.93.2<0.44 <0.53 <0.42 <0.37 <0.59 <1.1 <0.749.58/29/2019 100 0.84<0.4613.6 1.5<0.40 <0.32 <0.716.0<2.02.2<0.45 <0.55 <0.44 <0.383.4 2.7J<0.774.112/3/2019 64.5 1.9<0.444.1 J 0.74 J<0.380.38 J 1.7 J<1.1 <1.93.3<0.44 <0.53 <0.421.3 J<0.59 <1.1 <0.747.88/29/2019 158 1.2<0.4619.9 7.4<0.402.1<0.713.9<2.02.3 9.0<0.5514.1<0.383.0 1.9J<0.774.612/3/2019 136 0.66<0.449.9<0.42 <0.380.73 J 1.4 J<1.13.1 J 3.6<0.44 <0.53 <0.42 <0.37 <0.59 <1.11.5 J 5.9SSV-467.6<0.30 <0.445.9 0.63 J<0.380.45 J<0.68 <1.1 <1.92.4<0.44 <0.53 <0.421.1 J<0.59 <1.10.90 J 4.1SSV-DUP71.5<0.30 <0.445.0 J<0.42 <0.38 <0.30 <0.68 <1.1 <1.92.2<0.44 <0.53 <0.42 <0.37 <0.59 <1.1 <0.744.1SSV-5Southern portion of eastern warehouse4.0 -- 12/3/2019 116<0.310.50 J 8.3<0.440.44 J 1.1<0.71 <1.2 <2.02.7<0.45 <0.55 <0.44 <0.38 <0.62 <1.20.92 J 8.7SG-1Northeastern (upgradient) portion of Site4.0 10.0 8/30/2019 57.9 36.9<0.46 <0.7555.5 11.0 10.6 34.3 45.3<2.02.2<0.456.5<0.44 <0.389.0 3.4J 24.8 53.8220,000 120 35 35,000 4,900 41 630 42,000 NS 85 700 580 1,400 NS 490 370 NS 2,8004,9002,700,000 1,600 440 440,000 61,000 530 7,900 530,000 NS 1,100 8,800 7,700 18,000 NS 6,100 4,900 NS 35,000 61,000Notes:1) North Carolina Department of Environment Quality (DEQ) Division of Waste Management (DWM) Residential Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) (February 2018)2) North Carolina DWM Non-Residential SGSLs (February 2018)Only constituents detected in at least one sample are shownCompound concentrations and SGSLs are reported in micrograms per cubic meter (µg/m3)Compound concentrations are reported to the laboratory detection limitsBold indicates concentration exceeds Residential SGSLBold and Underlined indicates concentration exceeds Non-Residential SGSLGray and underlined values are method detection limits that exceed Residential SGSL or both the Residential SGSL and Non-Residential SGSL.ft bgs = feet below ground surface; NS = Not Specified; -- = Not ApplicableJ = estimated value between the laboratory method detection limit and the laboratory reporting limit------ 12/3/2019DWM Non-Residential SGSL (2)DWM Residential SGSL (1)TO-15Central portion of western warehouseSSV-1Western portion of eastern warehouseSSV-2Eastern portion of eastern warehouseSSV-3Northern portion of eastern warehouse4.0 --4.04.04.0S:\AAA-Master Projects\JMC Holdings\JMC.009 300 Rampart Brownfields\Brownfields Assessment\Tables\JMC-007 Data Tables1/7/2020Table 1 (Page 1 of 2)Hart & Hickman, PC
Table 1Summary of Sub-Slab Vapor and Soil Gas Analytical ResultsFormer Cotton Seed Oil MillCharlotte, North CarolinaH&H Job No. JMC-009Sample IDSample LocationSlab Thickness (in)Screen Depth (ft bgs)Sample DateAnalytical Method8/29/201912/3/20198/29/201912/3/20198/29/201912/3/2019SSV-4SSV-DUPSSV-5Southern portion of eastern warehouse4.0 -- 12/3/2019SG-1Northeastern (upgradient) portion of Site4.0 10.0 8/30/2019------ 12/3/2019DWM Non-Residential SGSL (2)DWM Residential SGSL (1)TO-15Central portion of western warehouseSSV-1Western portion of eastern warehouseSSV-2Eastern portion of eastern warehouseSSV-3Northern portion of eastern warehouse4.0 --4.04.04.02-Hexanone (MBK)Methylene Chloride4-Methyl-2-pentanone (MIBK)NaphthalenePropeneStyreneTetrachloroethyleneTetrahydrofuranToluene1,1,1-TrichloroethaneTrichloroethyleneTrichlorofluoromethane (Freon 11)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneVinyl AcetateVinyl Chloridem&p-Xyleneo-Xylene1.7J 6.8J<1.05.1J 4.4 1.5J<0.613.2 8.2<0.602.5<0.718.8 1.9J<0.52 <0.2410.5 5.02.1 J 96.5<1.04.2 J 3.6 1.6 J 1.2 J 0.60 J 1.8<0.60 <0.491.8 J<0.88 <0.773.2<0.24 <1.4 <0.671.6J 11.7<1.05.5 0.91 1.6J 1.7 3.7 8.2<0.62 <0.52 <0.7412.2 2.6<0.55 <0.2513.4 6.6<1.481.7<1.0 <2.53.8<0.670.63 J<0.512.6<0.60 <0.492.8<0.88 <0.77 <0.52 <0.24 <1.40.76 J2.4J 13.5 3.5J 4.3J 2.1 1.4J 9.5 3.7 11.4 0.80J 3.6<0.749.3 2.1<0.55 <0.2511.6 5.34.6 J 37.2 1.1 J 2.9 J 5.4<0.6713.9<0.512.1 0.64 J<0.495.9 0.89 J<0.77 <0.52 <0.24 <1.40.69 J<1.431.7<1.0 <2.5 <0.271.1 J 1.6<0.512.3<0.60 <0.492.0 J<0.88 <0.77 <0.52 <0.24 <1.4 <0.67<1.431.5<1.0 <2.5 <0.271.1 J 0.70 J<0.510.89 J<0.60 <0.492.0 J<0.88 <0.77 <0.52 <0.24 <1.4 <0.67<1.582.1 1.4 J<2.6 <0.28 <0.693.2<0.531.4 J 8.2<0.513.3<0.91 <0.81 <0.55 <0.25 <1.4 <0.69<1.57.4 4.6J 6.0 439 11.0 1.4<0.5326.0<0.62 <0.523.7 12.4 3.5<0.553.4 16.7 6.7210 4,200 21,000 21 21,000 7,000 280 14,000 35,000 35,000 14 NS 420 420 1,40056 700 7002,600 53,000 260,000 260 260,000 88,000 3,500 180,000 440,000 440,000 180NS 5,300 5,300 18,000 2,800 8,800 8,800Notes:1) North Carolina Department of Environment Quality (DEQ) Division of Waste Management (DWM) Residential Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) (February 2018)2) North Carolina DWM Non-Residential SGSLs (February 2018)Only constituents detected in at least one sample are shown.Compound concentrations and SGSLs are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory detection limits.Bold indicates concentration exceeds Residential SGSLBold and Underlined indicates concentration exceeds Non-Residential SGSLGray and underlined values are method detection limits that exceed Residential SGSL or both the Residential SGSL and Non-Residential SGSL.ft bgs = feet below ground surface; NS = Not Specified; -- = Not Applicable; NM = Not MeasuredJ = estimated value between the laboratory method detection limit and the laboratory reporting limitS:\AAA-Master Projects\JMC Holdings\JMC.009 300 Rampart Brownfields\Brownfields Assessment\Tables\JMC-007 Data Tables1/7/2020Table 1 (Page 2 of 2)Hart & Hickman, PC
Copyright:© 2013 National Geographic Society, i-cubed
SITE LOCATION MAP
FORMER COTTON SEED OIL MILL 300 RAMPART STREET CHARLOTTE, NORTH CAROLINA
DATE: 11-12-19
JOB NO: JMC-009
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: \\HHFS01\Redirectedfolders\Sperry\My Documents\ArcGIS\PROJECTS\JMC-009\Figure 1 - Site Location Map.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA 2013
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
REVISION NO. 0
JOB NO. JMC-009
DATE: 12-10-19
FIGURE NO. 2
CHARLOTTE SALVAGE COMPANY
300 RAMPART STREET
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
SUB-SLAB VAPOR SAMPLE LOCATION
SOIL GAS SAMPLE LOCATION
FLOOR DRAIN
DUMPSTER
POLE-MOUNTED TRANSFORMER
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
RAMPART ST
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RAMPART S
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HAW
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HAW
KI
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S
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TS. TRYON STREETS. TRYON STREETTHE PENROSE APARTMENTS / FORMER
VCC CHARLOTTE (349 W. TREMONT AVENUE)
THE PENROSE APARTMENTS / FORMER
VCC CHARLOTTE (349 W. TREMONT AVENUE)
VACANT
(2129 S. TRYON STREET)
VACANT
(2129 S. TRYON STREET)
K9 PLAYLAND
(2139 S. TRYON STREET)
K9 PLAYLAND
(2139 S. TRYON STREET)
MUTLI-TENANT COMMERCIAL BUILDINGS
(2204-2228 HAWKINS STREET)
MUTLI-TENANT COMMERCIAL BUILDINGS
(2204-2228 HAWKINS STREET)
KEG N CUE
(2131 S. TRYON STREET)
KEG N CUE
(2131 S. TRYON STREET)
MAACO FLEET SOLUTIONS
(2217 S. TRYON STREET)
MAACO FLEET SOLUTIONS
(2217 S. TRYON STREET)
NOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2019).
GMI
(222 RAMPART STREET)
GMI
(222 RAMPART STREET)
SGP-1
SSV-3
SSV-2
SSV-1
SSV-5
SSV-4
S:\AAA-Master Projects\JMC Holdings\JMC.009 300 Rampart Brownfields\Brownfields Assessment\Figures\Site Map.dwg, FIG 2, 1/6/2020 10:31:45 PM, sperry
REVISION NO. 0
JOB NO. JMC-007
DATE: 1-3-19
FIGURE NO. 3
CHARLOTTE SALVAGE COMPANY
300 RAMPART STREET
CHARLOTTE, NORTH CAROLINA
RECEPTOR SURVEY MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
GAS UTILITY LINE
WATER UTILITY LINE
SEWER UTILITY LINE
CABLE LINE
STORM WATER INLET
STORM WATER OUTFALL
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 GeologyHAWKINS STREETHAWKINS STREET
NOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2019).
2.UTILITY LINES ONLY SHOWN ADJACENT TO SITE.
D
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A
V
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S
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D
U
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A
V
A
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S
T
R
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T
WEST TREM
O
N
T

A
V
E
N
U
E
WEST TRE
M
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N
T

A
V
E
N
U
E
SOU
T
H
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Y
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S
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SOU
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DOGGETT S
T
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E
E
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DOGGETT
S
T
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T
SOUTH BOULEVARD
SOUTH BOULEVARD
B
R
O
O
K
H
I
L
L

R
O
A
D
B
R
O
O
K
H
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A
D
R
EM
O
UN
T

R
O
A
D
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R
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A
D
DISTRIBUTION STREETDISTRIBUTION STREETB
A
S
I
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S
T
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B
A
S
I
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S
T
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MAINLINE BOULEVARDMAINLINE BOULEVARD1,500 FT
SPECTRUM SOUTH END APARTMENTS
2225 HAWKINS STREET
JUNCTION 1504 APARTMENTS
1504 MAINLINE BOULEVARD
CAMDEN SOUTHLINE APARTMENTS
2300 SOUTH BOULEVARD
THE HUB
2250 HAWKINS STREET
BROOKHILL VILLAGE
409 BASIN STREET
PRIMROSE APARTMENTS
327 WEST TREMONT AVENUE
THREE30FIVE APARTMENTS
335 DOGGETT STREET
ASHTON SOUTH END
APARTMENTS
125 WEST TREMONT AVENUE
S:\AAA-Master Projects\JMC Holdings\JMC.009 300 Rampart Brownfields\Brownfields Assessment\Figures\Site Map.dwg, RECEPTOR.SURVEY, 1/7/2020 8:49:39 AM, sperry

Appendix A
Sub-Slab Soil Vapor QA/QC Field Form

Appendix B Laboratory Analytical Report
#=CL#
December 11, 2019
LIMS USE: FR - ROBERT SORGEL
LIMS OBJECT ID: 92456012
92456012
Project:
Pace Project No.:
RE:
Robert Sorgel
Hart & Hickman
2923 S Tryon Street
Suite 100
Charlotte, NC 28203
JMC-009
Dear Robert Sorgel:
Enclosed are the analytical results for sample(s) received by the laboratory on December 04, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92456012
JMC-009
Pace Analytical Services Minneapolis
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
CNMI Saipan Certification #: MP0003
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8+Wyoming DW Certification #: via MN 027-
053-137
Florida Certification #: E87605
Georgia Certification #: 959
Guam EPA Certification #: MN00064
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: 03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Massachusetts Certification #: M-MN064
Massachusetts DWP Certification #: via MN 027-053-137
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Minnesota Dept of Ag Certifcation #: via MN 027-053-137
Minnesota Petrofund Certification #: 1240
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Vermont Certification #: VT-027053137
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92456012
JMC-009
Lab ID Sample ID Matrix Date Collected Date Received
92456012001 SSV-1 CAN #2408 Air 12/03/19 12:20 12/04/19 07:49
92456012002 SSV-2 CAN #3638 Air 12/03/19 11:48 12/04/19 07:49
92456012003 SSV-3 CAN #2983 Air 12/03/19 10:16 12/04/19 07:49
92456012004 SSV-4 CAN #2255 Air 12/03/19 11:08 12/04/19 07:49
92456012005 SSV-5 CAN #1023 Air 12/03/19 09:24 12/04/19 07:49
92456012006 DUP CAN #1775 Air 12/03/19 00:00 12/04/19 07:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92456012
JMC-009
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92456012001 SSV-1 CAN #2408 TO-15 58 PASI-MNCK
92456012002 SSV-2 CAN #3638 TO-15 58 PASI-MNCK
92456012003 SSV-3 CAN #2983 TO-15 58 PASI-MNCK
92456012004 SSV-4 CAN #2255 TO-15 58 PASI-MMJL
92456012005 SSV-5 CAN #1023 TO-15 58 PASI-MMJL
92456012006 DUP CAN #1775 TO-15 58 PASI-MMJL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-1 CAN #2408 Lab ID:92456012001 Collected:12/03/19 12:20 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 57.2 ug/m3 12/09/19 20:48 67-64-14.7 2.3 1.94
Benzene 0.41J ug/m3 12/09/19 20:48 71-43-20.63 0.30 1.94
Bromodichloromethane ND ug/m3 12/09/19 20:48 75-27-42.6 0.71 1.94
Bromoform ND ug/m3 12/09/19 20:48 75-25-210.2 2.8 1.94
Bromomethane ND ug/m3 12/09/19 20:48 74-83-91.5 0.44 1.94
1,3-Butadiene ND ug/m3 12/09/19 20:48 106-99-00.87 0.25 1.94
2-Butanone (MEK)5.0J ug/m3 12/09/19 20:48 78-93-35.8 0.72 1.94
Carbon disulfide 1.2J ug/m3 12/09/19 20:48 75-15-01.2 0.42 1.94
Carbon tetrachloride ND ug/m3 12/09/19 20:48 56-23-52.5 0.83 1.94
Chlorobenzene ND ug/m3 12/09/19 20:48 108-90-71.8 0.53 1.94
Chloroethane ND ug/m3 12/09/19 20:48 75-00-31.0 0.50 1.94
Chloroform ND ug/m3 12/09/19 20:48 67-66-30.96 0.38 1.94
Chloromethane ND ug/m3 12/09/19 20:48 74-87-30.81 0.30 1.94
Cyclohexane 0.72J ug/m3 12/09/19 20:48 110-82-73.4 0.68 1.94
Dibromochloromethane ND ug/m3 12/09/19 20:48 124-48-13.4 1.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 12/09/19 20:48 106-93-41.5 0.71 1.94
1,2-Dichlorobenzene ND ug/m3 12/09/19 20:48 95-50-12.4 0.97 1.94
1,3-Dichlorobenzene ND ug/m3 12/09/19 20:48 541-73-12.4 1.1 1.94
1,4-Dichlorobenzene ND ug/m3 12/09/19 20:48 106-46-75.9 1.9 1.94
Dichlorodifluoromethane 3.2 ug/m3 12/09/19 20:48 75-71-82.0 0.57 1.94
1,1-Dichloroethane ND ug/m3 12/09/19 20:48 75-34-31.6 0.44 1.94
1,2-Dichloroethane ND ug/m3 12/09/19 20:48 107-06-20.80 0.29 1.94
1,1-Dichloroethene ND ug/m3 12/09/19 20:48 75-35-41.6 0.53 1.94
cis-1,2-Dichloroethene ND ug/m3 12/09/19 20:48 156-59-21.6 0.42 1.94
trans-1,2-Dichloroethene ND ug/m3 12/09/19 20:48 156-60-51.6 0.55 1.94
1,2-Dichloropropane ND ug/m3 12/09/19 20:48 78-87-51.8 0.45 1.94
cis-1,3-Dichloropropene ND ug/m3 12/09/19 20:48 10061-01-51.8 0.59 1.94
trans-1,3-Dichloropropene ND ug/m3 12/09/19 20:48 10061-02-61.8 0.85 1.94
Dichlorotetrafluoroethane ND ug/m3 12/09/19 20:48 76-14-22.8 0.85 1.94
Ethyl acetate ND ug/m3 12/09/19 20:48 141-78-61.4 0.37 1.94
Ethylbenzene ND ug/m3 12/09/19 20:48 100-41-41.7 0.59 1.94
4-Ethyltoluene ND ug/m3 12/09/19 20:48 622-96-84.8 1.1 1.94
n-Heptane ND ug/m3 12/09/19 20:48 142-82-51.6 0.74 1.94
Hexachloro-1,3-butadiene ND ug/m3 12/09/19 20:48 87-68-310.5 3.8 1.94
n-Hexane 9.5 ug/m3 12/09/19 20:48 110-54-31.4 0.60 1.94
2-Hexanone 2.1J ug/m3 12/09/19 20:48 591-78-6 CH8.1 1.4 1.94
Methylene Chloride 96.5 ug/m3 12/09/19 20:48 75-09-26.8 2.3 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 12/09/19 20:48 108-10-18.1 1.0 1.94
Methyl-tert-butyl ether ND ug/m3 12/09/19 20:48 1634-04-47.1 1.3 1.94
Naphthalene 4.2J ug/m3 12/09/19 20:48 91-20-35.2 2.5 1.94
Propylene 3.6 ug/m3 12/09/19 20:48 115-07-10.68 0.27 1.94
Styrene 1.6J ug/m3 12/09/19 20:48 100-42-51.7 0.67 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 12/09/19 20:48 79-34-51.4 0.60 1.94
Tetrachloroethene 1.2J ug/m3 12/09/19 20:48 127-18-41.3 0.61 1.94
Tetrahydrofuran 0.60J ug/m3 12/09/19 20:48 109-99-91.2 0.51 1.94
Toluene 1.8 ug/m3 12/09/19 20:48 108-88-31.5 0.68 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-1 CAN #2408 Lab ID:92456012001 Collected:12/03/19 12:20 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 12/09/19 20:48 120-82-114.6 7.2 1.94
1,1,1-Trichloroethane ND ug/m3 12/09/19 20:48 71-55-62.2 0.60 1.94
1,1,2-Trichloroethane ND ug/m3 12/09/19 20:48 79-00-51.1 0.47 1.94
Trichloroethene ND ug/m3 12/09/19 20:48 79-01-61.1 0.49 1.94
Trichlorofluoromethane 1.8J ug/m3 12/09/19 20:48 75-69-42.2 0.71 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 12/09/19 20:48 76-13-13.0 1.1 1.94
1,2,4-Trimethylbenzene ND ug/m3 12/09/19 20:48 95-63-61.9 0.88 1.94
1,3,5-Trimethylbenzene ND ug/m3 12/09/19 20:48 108-67-81.9 0.77 1.94
Vinyl acetate 3.2 ug/m3 12/09/19 20:48 108-05-41.4 0.52 1.94
Vinyl chloride ND ug/m3 12/09/19 20:48 75-01-40.50 0.24 1.94
m&p-Xylene ND ug/m3 12/09/19 20:48 179601-23-13.4 1.4 1.94
o-Xylene ND ug/m3 12/09/19 20:48 95-47-61.7 0.67 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-2 CAN #3638 Lab ID:92456012002 Collected:12/03/19 11:48 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 64.5 ug/m3 12/09/19 21:17 67-64-14.7 2.3 1.94
Benzene 1.9 ug/m3 12/09/19 21:17 71-43-20.63 0.30 1.94
Bromodichloromethane ND ug/m3 12/09/19 21:17 75-27-42.6 0.71 1.94
Bromoform ND ug/m3 12/09/19 21:17 75-25-210.2 2.8 1.94
Bromomethane ND ug/m3 12/09/19 21:17 74-83-91.5 0.44 1.94
1,3-Butadiene ND ug/m3 12/09/19 21:17 106-99-00.87 0.25 1.94
2-Butanone (MEK)4.1J ug/m3 12/09/19 21:17 78-93-35.8 0.72 1.94
Carbon disulfide 0.74J ug/m3 12/09/19 21:17 75-15-01.2 0.42 1.94
Carbon tetrachloride ND ug/m3 12/09/19 21:17 56-23-52.5 0.83 1.94
Chlorobenzene ND ug/m3 12/09/19 21:17 108-90-71.8 0.53 1.94
Chloroethane ND ug/m3 12/09/19 21:17 75-00-31.0 0.50 1.94
Chloroform ND ug/m3 12/09/19 21:17 67-66-30.96 0.38 1.94
Chloromethane 0.38J ug/m3 12/09/19 21:17 74-87-30.81 0.30 1.94
Cyclohexane 1.7J ug/m3 12/09/19 21:17 110-82-73.4 0.68 1.94
Dibromochloromethane ND ug/m3 12/09/19 21:17 124-48-13.4 1.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 12/09/19 21:17 106-93-41.5 0.71 1.94
1,2-Dichlorobenzene ND ug/m3 12/09/19 21:17 95-50-12.4 0.97 1.94
1,3-Dichlorobenzene ND ug/m3 12/09/19 21:17 541-73-12.4 1.1 1.94
1,4-Dichlorobenzene ND ug/m3 12/09/19 21:17 106-46-75.9 1.9 1.94
Dichlorodifluoromethane 3.3 ug/m3 12/09/19 21:17 75-71-82.0 0.57 1.94
1,1-Dichloroethane ND ug/m3 12/09/19 21:17 75-34-31.6 0.44 1.94
1,2-Dichloroethane ND ug/m3 12/09/19 21:17 107-06-20.80 0.29 1.94
1,1-Dichloroethene ND ug/m3 12/09/19 21:17 75-35-41.6 0.53 1.94
cis-1,2-Dichloroethene ND ug/m3 12/09/19 21:17 156-59-21.6 0.42 1.94
trans-1,2-Dichloroethene ND ug/m3 12/09/19 21:17 156-60-51.6 0.55 1.94
1,2-Dichloropropane ND ug/m3 12/09/19 21:17 78-87-51.8 0.45 1.94
cis-1,3-Dichloropropene ND ug/m3 12/09/19 21:17 10061-01-51.8 0.59 1.94
trans-1,3-Dichloropropene ND ug/m3 12/09/19 21:17 10061-02-61.8 0.85 1.94
Dichlorotetrafluoroethane ND ug/m3 12/09/19 21:17 76-14-22.8 0.85 1.94
Ethyl acetate 1.3J ug/m3 12/09/19 21:17 141-78-61.4 0.37 1.94
Ethylbenzene ND ug/m3 12/09/19 21:17 100-41-41.7 0.59 1.94
4-Ethyltoluene ND ug/m3 12/09/19 21:17 622-96-84.8 1.1 1.94
n-Heptane ND ug/m3 12/09/19 21:17 142-82-51.6 0.74 1.94
Hexachloro-1,3-butadiene ND ug/m3 12/09/19 21:17 87-68-310.5 3.8 1.94
n-Hexane 7.8 ug/m3 12/09/19 21:17 110-54-31.4 0.60 1.94
2-Hexanone ND ug/m3 12/09/19 21:17 591-78-68.1 1.4 1.94
Methylene Chloride 81.7 ug/m3 12/09/19 21:17 75-09-26.8 2.3 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 12/09/19 21:17 108-10-18.1 1.0 1.94
Methyl-tert-butyl ether ND ug/m3 12/09/19 21:17 1634-04-47.1 1.3 1.94
Naphthalene ND ug/m3 12/09/19 21:17 91-20-35.2 2.5 1.94
Propylene 3.8 ug/m3 12/09/19 21:17 115-07-10.68 0.27 1.94
Styrene ND ug/m3 12/09/19 21:17 100-42-51.7 0.67 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 12/09/19 21:17 79-34-51.4 0.60 1.94
Tetrachloroethene 0.63J ug/m3 12/09/19 21:17 127-18-41.3 0.61 1.94
Tetrahydrofuran ND ug/m3 12/09/19 21:17 109-99-91.2 0.51 1.94
Toluene 2.6 ug/m3 12/09/19 21:17 108-88-31.5 0.68 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-2 CAN #3638 Lab ID:92456012002 Collected:12/03/19 11:48 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 12/09/19 21:17 120-82-114.6 7.2 1.94
1,1,1-Trichloroethane ND ug/m3 12/09/19 21:17 71-55-62.2 0.60 1.94
1,1,2-Trichloroethane ND ug/m3 12/09/19 21:17 79-00-51.1 0.47 1.94
Trichloroethene ND ug/m3 12/09/19 21:17 79-01-61.1 0.49 1.94
Trichlorofluoromethane 2.8 ug/m3 12/09/19 21:17 75-69-42.2 0.71 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 12/09/19 21:17 76-13-13.0 1.1 1.94
1,2,4-Trimethylbenzene ND ug/m3 12/09/19 21:17 95-63-61.9 0.88 1.94
1,3,5-Trimethylbenzene ND ug/m3 12/09/19 21:17 108-67-81.9 0.77 1.94
Vinyl acetate ND ug/m3 12/09/19 21:17 108-05-41.4 0.52 1.94
Vinyl chloride ND ug/m3 12/09/19 21:17 75-01-40.50 0.24 1.94
m&p-Xylene ND ug/m3 12/09/19 21:17 179601-23-13.4 1.4 1.94
o-Xylene 0.76J ug/m3 12/09/19 21:17 95-47-61.7 0.67 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-3 CAN #2983 Lab ID:92456012003 Collected:12/03/19 10:16 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 136 ug/m3 12/09/19 21:46 67-64-14.7 2.3 1.94
Benzene 0.66 ug/m3 12/09/19 21:46 71-43-20.63 0.30 1.94
Bromodichloromethane ND ug/m3 12/09/19 21:46 75-27-42.6 0.71 1.94
Bromoform ND ug/m3 12/09/19 21:46 75-25-210.2 2.8 1.94
Bromomethane ND ug/m3 12/09/19 21:46 74-83-91.5 0.44 1.94
1,3-Butadiene ND ug/m3 12/09/19 21:46 106-99-00.87 0.25 1.94
2-Butanone (MEK)9.9 ug/m3 12/09/19 21:46 78-93-35.8 0.72 1.94
Carbon disulfide ND ug/m3 12/09/19 21:46 75-15-01.2 0.42 1.94
Carbon tetrachloride ND ug/m3 12/09/19 21:46 56-23-52.5 0.83 1.94
Chlorobenzene ND ug/m3 12/09/19 21:46 108-90-71.8 0.53 1.94
Chloroethane ND ug/m3 12/09/19 21:46 75-00-31.0 0.50 1.94
Chloroform ND ug/m3 12/09/19 21:46 67-66-30.96 0.38 1.94
Chloromethane 0.73J ug/m3 12/09/19 21:46 74-87-30.81 0.30 1.94
Cyclohexane 1.4J ug/m3 12/09/19 21:46 110-82-73.4 0.68 1.94
Dibromochloromethane ND ug/m3 12/09/19 21:46 124-48-13.4 1.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 12/09/19 21:46 106-93-41.5 0.71 1.94
1,2-Dichlorobenzene ND ug/m3 12/09/19 21:46 95-50-12.4 0.97 1.94
1,3-Dichlorobenzene ND ug/m3 12/09/19 21:46 541-73-12.4 1.1 1.94
1,4-Dichlorobenzene 3.1J ug/m3 12/09/19 21:46 106-46-75.9 1.9 1.94
Dichlorodifluoromethane 3.6 ug/m3 12/09/19 21:46 75-71-82.0 0.57 1.94
1,1-Dichloroethane ND ug/m3 12/09/19 21:46 75-34-31.6 0.44 1.94
1,2-Dichloroethane ND ug/m3 12/09/19 21:46 107-06-20.80 0.29 1.94
1,1-Dichloroethene ND ug/m3 12/09/19 21:46 75-35-41.6 0.53 1.94
cis-1,2-Dichloroethene ND ug/m3 12/09/19 21:46 156-59-21.6 0.42 1.94
trans-1,2-Dichloroethene ND ug/m3 12/09/19 21:46 156-60-51.6 0.55 1.94
1,2-Dichloropropane ND ug/m3 12/09/19 21:46 78-87-51.8 0.45 1.94
cis-1,3-Dichloropropene ND ug/m3 12/09/19 21:46 10061-01-51.8 0.59 1.94
trans-1,3-Dichloropropene ND ug/m3 12/09/19 21:46 10061-02-61.8 0.85 1.94
Dichlorotetrafluoroethane ND ug/m3 12/09/19 21:46 76-14-22.8 0.85 1.94
Ethyl acetate ND ug/m3 12/09/19 21:46 141-78-61.4 0.37 1.94
Ethylbenzene ND ug/m3 12/09/19 21:46 100-41-41.7 0.59 1.94
4-Ethyltoluene ND ug/m3 12/09/19 21:46 622-96-84.8 1.1 1.94
n-Heptane 1.5J ug/m3 12/09/19 21:46 142-82-51.6 0.74 1.94
Hexachloro-1,3-butadiene ND ug/m3 12/09/19 21:46 87-68-310.5 3.8 1.94
n-Hexane 5.9 ug/m3 12/09/19 21:46 110-54-31.4 0.60 1.94
2-Hexanone 4.6J ug/m3 12/09/19 21:46 591-78-6 CH8.1 1.4 1.94
Methylene Chloride 37.2 ug/m3 12/09/19 21:46 75-09-26.8 2.3 1.94
4-Methyl-2-pentanone (MIBK)1.1J ug/m3 12/09/19 21:46 108-10-18.1 1.0 1.94
Methyl-tert-butyl ether ND ug/m3 12/09/19 21:46 1634-04-47.1 1.3 1.94
Naphthalene 2.9J ug/m3 12/09/19 21:46 91-20-35.2 2.5 1.94
Propylene 5.4 ug/m3 12/09/19 21:46 115-07-10.68 0.27 1.94
Styrene ND ug/m3 12/09/19 21:46 100-42-51.7 0.67 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 12/09/19 21:46 79-34-51.4 0.60 1.94
Tetrachloroethene 13.9 ug/m3 12/09/19 21:46 127-18-41.3 0.61 1.94
Tetrahydrofuran ND ug/m3 12/09/19 21:46 109-99-91.2 0.51 1.94
Toluene 2.1 ug/m3 12/09/19 21:46 108-88-31.5 0.68 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-3 CAN #2983 Lab ID:92456012003 Collected:12/03/19 10:16 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 12/09/19 21:46 120-82-114.6 7.2 1.94
1,1,1-Trichloroethane 0.64J ug/m3 12/09/19 21:46 71-55-62.2 0.60 1.94
1,1,2-Trichloroethane ND ug/m3 12/09/19 21:46 79-00-51.1 0.47 1.94
Trichloroethene ND ug/m3 12/09/19 21:46 79-01-61.1 0.49 1.94
Trichlorofluoromethane 5.9 ug/m3 12/09/19 21:46 75-69-42.2 0.71 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 12/09/19 21:46 76-13-13.0 1.1 1.94
1,2,4-Trimethylbenzene 0.89J ug/m3 12/09/19 21:46 95-63-61.9 0.88 1.94
1,3,5-Trimethylbenzene ND ug/m3 12/09/19 21:46 108-67-81.9 0.77 1.94
Vinyl acetate ND ug/m3 12/09/19 21:46 108-05-41.4 0.52 1.94
Vinyl chloride ND ug/m3 12/09/19 21:46 75-01-40.50 0.24 1.94
m&p-Xylene ND ug/m3 12/09/19 21:46 179601-23-13.4 1.4 1.94
o-Xylene 0.69J ug/m3 12/09/19 21:46 95-47-61.7 0.67 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-4 CAN #2255 Lab ID:92456012004 Collected:12/03/19 11:08 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 67.6 ug/m3 12/11/19 00:18 67-64-14.7 2.3 1.94
Benzene ND ug/m3 12/11/19 00:18 71-43-20.63 0.30 1.94
Bromodichloromethane ND ug/m3 12/11/19 00:18 75-27-42.6 0.71 1.94
Bromoform ND ug/m3 12/11/19 00:18 75-25-210.2 2.8 1.94
Bromomethane ND ug/m3 12/11/19 00:18 74-83-91.5 0.44 1.94
1,3-Butadiene ND ug/m3 12/11/19 00:18 106-99-00.87 0.25 1.94
2-Butanone (MEK)5.9 ug/m3 12/11/19 00:18 78-93-35.8 0.72 1.94
Carbon disulfide 0.63J ug/m3 12/11/19 00:18 75-15-01.2 0.42 1.94
Carbon tetrachloride ND ug/m3 12/11/19 00:18 56-23-52.5 0.83 1.94
Chlorobenzene ND ug/m3 12/11/19 00:18 108-90-71.8 0.53 1.94
Chloroethane ND ug/m3 12/11/19 00:18 75-00-31.0 0.50 1.94
Chloroform ND ug/m3 12/11/19 00:18 67-66-30.96 0.38 1.94
Chloromethane 0.45J ug/m3 12/11/19 00:18 74-87-30.81 0.30 1.94
Cyclohexane ND ug/m3 12/11/19 00:18 110-82-73.4 0.68 1.94
Dibromochloromethane ND ug/m3 12/11/19 00:18 124-48-13.4 1.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 12/11/19 00:18 106-93-41.5 0.71 1.94
1,2-Dichlorobenzene ND ug/m3 12/11/19 00:18 95-50-12.4 0.97 1.94
1,3-Dichlorobenzene ND ug/m3 12/11/19 00:18 541-73-12.4 1.1 1.94
1,4-Dichlorobenzene ND ug/m3 12/11/19 00:18 106-46-75.9 1.9 1.94
Dichlorodifluoromethane 2.4 ug/m3 12/11/19 00:18 75-71-82.0 0.57 1.94
1,1-Dichloroethane ND ug/m3 12/11/19 00:18 75-34-31.6 0.44 1.94
1,2-Dichloroethane ND ug/m3 12/11/19 00:18 107-06-20.80 0.29 1.94
1,1-Dichloroethene ND ug/m3 12/11/19 00:18 75-35-41.6 0.53 1.94
cis-1,2-Dichloroethene ND ug/m3 12/11/19 00:18 156-59-21.6 0.42 1.94
trans-1,2-Dichloroethene ND ug/m3 12/11/19 00:18 156-60-51.6 0.55 1.94
1,2-Dichloropropane ND ug/m3 12/11/19 00:18 78-87-51.8 0.45 1.94
cis-1,3-Dichloropropene ND ug/m3 12/11/19 00:18 10061-01-51.8 0.59 1.94
trans-1,3-Dichloropropene ND ug/m3 12/11/19 00:18 10061-02-61.8 0.85 1.94
Dichlorotetrafluoroethane ND ug/m3 12/11/19 00:18 76-14-22.8 0.85 1.94
Ethyl acetate 1.1J ug/m3 12/11/19 00:18 141-78-61.4 0.37 1.94
Ethylbenzene ND ug/m3 12/11/19 00:18 100-41-41.7 0.59 1.94
4-Ethyltoluene ND ug/m3 12/11/19 00:18 622-96-84.8 1.1 1.94
n-Heptane 0.90J ug/m3 12/11/19 00:18 142-82-51.6 0.74 1.94
Hexachloro-1,3-butadiene ND ug/m3 12/11/19 00:18 87-68-310.5 3.8 1.94
n-Hexane 4.1 ug/m3 12/11/19 00:18 110-54-31.4 0.60 1.94
2-Hexanone ND ug/m3 12/11/19 00:18 591-78-68.1 1.4 1.94
Methylene Chloride 31.7 ug/m3 12/11/19 00:18 75-09-26.8 2.3 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 12/11/19 00:18 108-10-18.1 1.0 1.94
Methyl-tert-butyl ether ND ug/m3 12/11/19 00:18 1634-04-47.1 1.3 1.94
Naphthalene ND ug/m3 12/11/19 00:18 91-20-35.2 2.5 1.94
Propylene ND ug/m3 12/11/19 00:18 115-07-10.68 0.27 1.94
Styrene 1.1J ug/m3 12/11/19 00:18 100-42-51.7 0.67 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 12/11/19 00:18 79-34-51.4 0.60 1.94
Tetrachloroethene 1.6 ug/m3 12/11/19 00:18 127-18-41.3 0.61 1.94
Tetrahydrofuran ND ug/m3 12/11/19 00:18 109-99-91.2 0.51 1.94
Toluene 2.3 ug/m3 12/11/19 00:18 108-88-31.5 0.68 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-4 CAN #2255 Lab ID:92456012004 Collected:12/03/19 11:08 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 12/11/19 00:18 120-82-114.6 7.2 1.94
1,1,1-Trichloroethane ND ug/m3 12/11/19 00:18 71-55-62.2 0.60 1.94
1,1,2-Trichloroethane ND ug/m3 12/11/19 00:18 79-00-51.1 0.47 1.94
Trichloroethene ND ug/m3 12/11/19 00:18 79-01-61.1 0.49 1.94
Trichlorofluoromethane 2.0J ug/m3 12/11/19 00:18 75-69-42.2 0.71 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 12/11/19 00:18 76-13-13.0 1.1 1.94
1,2,4-Trimethylbenzene ND ug/m3 12/11/19 00:18 95-63-61.9 0.88 1.94
1,3,5-Trimethylbenzene ND ug/m3 12/11/19 00:18 108-67-81.9 0.77 1.94
Vinyl acetate ND ug/m3 12/11/19 00:18 108-05-41.4 0.52 1.94
Vinyl chloride ND ug/m3 12/11/19 00:18 75-01-40.50 0.24 1.94
m&p-Xylene ND ug/m3 12/11/19 00:18 179601-23-13.4 1.4 1.94
o-Xylene ND ug/m3 12/11/19 00:18 95-47-61.7 0.67 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-5 CAN #1023 Lab ID:92456012005 Collected:12/03/19 09:24 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 116 ug/m3 12/11/19 01:18 67-64-14.9 2.4 2.02
Benzene ND ug/m3 12/11/19 01:18 71-43-20.66 0.31 2.02
Bromodichloromethane ND ug/m3 12/11/19 01:18 75-27-42.7 0.74 2.02
Bromoform ND ug/m3 12/11/19 01:18 75-25-210.6 2.9 2.02
Bromomethane 0.50J ug/m3 12/11/19 01:18 74-83-91.6 0.46 2.02
1,3-Butadiene ND ug/m3 12/11/19 01:18 106-99-00.91 0.26 2.02
2-Butanone (MEK)8.3 ug/m3 12/11/19 01:18 78-93-36.1 0.75 2.02
Carbon disulfide ND ug/m3 12/11/19 01:18 75-15-01.3 0.44 2.02
Carbon tetrachloride ND ug/m3 12/11/19 01:18 56-23-52.6 0.87 2.02
Chlorobenzene ND ug/m3 12/11/19 01:18 108-90-71.9 0.56 2.02
Chloroethane ND ug/m3 12/11/19 01:18 75-00-31.1 0.53 2.02
Chloroform 0.44J ug/m3 12/11/19 01:18 67-66-31.0 0.40 2.02
Chloromethane 1.1 ug/m3 12/11/19 01:18 74-87-30.85 0.32 2.02
Cyclohexane ND ug/m3 12/11/19 01:18 110-82-73.5 0.71 2.02
Dibromochloromethane ND ug/m3 12/11/19 01:18 124-48-13.5 1.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 12/11/19 01:18 106-93-41.6 0.74 2.02
1,2-Dichlorobenzene ND ug/m3 12/11/19 01:18 95-50-12.5 1.0 2.02
1,3-Dichlorobenzene ND ug/m3 12/11/19 01:18 541-73-12.5 1.2 2.02
1,4-Dichlorobenzene ND ug/m3 12/11/19 01:18 106-46-76.2 2.0 2.02
Dichlorodifluoromethane 2.7 ug/m3 12/11/19 01:18 75-71-82.0 0.59 2.02
1,1-Dichloroethane ND ug/m3 12/11/19 01:18 75-34-31.7 0.45 2.02
1,2-Dichloroethane ND ug/m3 12/11/19 01:18 107-06-20.83 0.30 2.02
1,1-Dichloroethene ND ug/m3 12/11/19 01:18 75-35-41.6 0.55 2.02
cis-1,2-Dichloroethene ND ug/m3 12/11/19 01:18 156-59-21.6 0.44 2.02
trans-1,2-Dichloroethene ND ug/m3 12/11/19 01:18 156-60-51.6 0.58 2.02
1,2-Dichloropropane ND ug/m3 12/11/19 01:18 78-87-51.9 0.46 2.02
cis-1,3-Dichloropropene ND ug/m3 12/11/19 01:18 10061-01-51.9 0.61 2.02
trans-1,3-Dichloropropene ND ug/m3 12/11/19 01:18 10061-02-61.9 0.89 2.02
Dichlorotetrafluoroethane ND ug/m3 12/11/19 01:18 76-14-22.9 0.88 2.02
Ethyl acetate ND ug/m3 12/11/19 01:18 141-78-61.5 0.38 2.02
Ethylbenzene ND ug/m3 12/11/19 01:18 100-41-41.8 0.62 2.02
4-Ethyltoluene ND ug/m3 12/11/19 01:18 622-96-85.0 1.2 2.02
n-Heptane 0.92J ug/m3 12/11/19 01:18 142-82-51.7 0.77 2.02
Hexachloro-1,3-butadiene ND ug/m3 12/11/19 01:18 87-68-310.9 4.0 2.02
n-Hexane 8.7 ug/m3 12/11/19 01:18 110-54-31.4 0.63 2.02
2-Hexanone ND ug/m3 12/11/19 01:18 591-78-68.4 1.5 2.02
Methylene Chloride 82.1 ug/m3 12/11/19 01:18 75-09-27.1 2.4 2.02
4-Methyl-2-pentanone (MIBK)1.4J ug/m3 12/11/19 01:18 108-10-18.4 1.0 2.02
Methyl-tert-butyl ether ND ug/m3 12/11/19 01:18 1634-04-47.4 1.3 2.02
Naphthalene ND ug/m3 12/11/19 01:18 91-20-35.4 2.6 2.02
Propylene ND ug/m3 12/11/19 01:18 115-07-10.71 0.28 2.02
Styrene ND ug/m3 12/11/19 01:18 100-42-51.7 0.69 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 12/11/19 01:18 79-34-51.4 0.62 2.02
Tetrachloroethene 3.2 ug/m3 12/11/19 01:18 127-18-41.4 0.63 2.02
Tetrahydrofuran ND ug/m3 12/11/19 01:18 109-99-91.2 0.53 2.02
Toluene 1.4J ug/m3 12/11/19 01:18 108-88-31.5 0.71 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:SSV-5 CAN #1023 Lab ID:92456012005 Collected:12/03/19 09:24 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 12/11/19 01:18 120-82-115.2 7.5 2.02
1,1,1-Trichloroethane 8.2 ug/m3 12/11/19 01:18 71-55-62.2 0.62 2.02
1,1,2-Trichloroethane ND ug/m3 12/11/19 01:18 79-00-51.1 0.49 2.02
Trichloroethene ND ug/m3 12/11/19 01:18 79-01-61.1 0.51 2.02
Trichlorofluoromethane 3.3 ug/m3 12/11/19 01:18 75-69-42.3 0.74 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 12/11/19 01:18 76-13-13.2 1.1 2.02
1,2,4-Trimethylbenzene ND ug/m3 12/11/19 01:18 95-63-62.0 0.91 2.02
1,3,5-Trimethylbenzene ND ug/m3 12/11/19 01:18 108-67-82.0 0.81 2.02
Vinyl acetate ND ug/m3 12/11/19 01:18 108-05-41.4 0.55 2.02
Vinyl chloride ND ug/m3 12/11/19 01:18 75-01-40.53 0.25 2.02
m&p-Xylene ND ug/m3 12/11/19 01:18 179601-23-13.6 1.4 2.02
o-Xylene ND ug/m3 12/11/19 01:18 95-47-61.8 0.69 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:DUP CAN #1775 Lab ID:92456012006 Collected:12/03/19 00:00 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 71.5 ug/m3 12/11/19 02:17 67-64-14.7 2.3 1.94
Benzene ND ug/m3 12/11/19 02:17 71-43-20.63 0.30 1.94
Bromodichloromethane ND ug/m3 12/11/19 02:17 75-27-42.6 0.71 1.94
Bromoform ND ug/m3 12/11/19 02:17 75-25-210.2 2.8 1.94
Bromomethane ND ug/m3 12/11/19 02:17 74-83-91.5 0.44 1.94
1,3-Butadiene ND ug/m3 12/11/19 02:17 106-99-00.87 0.25 1.94
2-Butanone (MEK)5.0J ug/m3 12/11/19 02:17 78-93-35.8 0.72 1.94
Carbon disulfide ND ug/m3 12/11/19 02:17 75-15-01.2 0.42 1.94
Carbon tetrachloride ND ug/m3 12/11/19 02:17 56-23-52.5 0.83 1.94
Chlorobenzene ND ug/m3 12/11/19 02:17 108-90-71.8 0.53 1.94
Chloroethane ND ug/m3 12/11/19 02:17 75-00-31.0 0.50 1.94
Chloroform ND ug/m3 12/11/19 02:17 67-66-30.96 0.38 1.94
Chloromethane ND ug/m3 12/11/19 02:17 74-87-30.81 0.30 1.94
Cyclohexane ND ug/m3 12/11/19 02:17 110-82-73.4 0.68 1.94
Dibromochloromethane ND ug/m3 12/11/19 02:17 124-48-13.4 1.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 12/11/19 02:17 106-93-41.5 0.71 1.94
1,2-Dichlorobenzene ND ug/m3 12/11/19 02:17 95-50-12.4 0.97 1.94
1,3-Dichlorobenzene ND ug/m3 12/11/19 02:17 541-73-12.4 1.1 1.94
1,4-Dichlorobenzene ND ug/m3 12/11/19 02:17 106-46-75.9 1.9 1.94
Dichlorodifluoromethane 2.2 ug/m3 12/11/19 02:17 75-71-82.0 0.57 1.94
1,1-Dichloroethane ND ug/m3 12/11/19 02:17 75-34-31.6 0.44 1.94
1,2-Dichloroethane ND ug/m3 12/11/19 02:17 107-06-20.80 0.29 1.94
1,1-Dichloroethene ND ug/m3 12/11/19 02:17 75-35-41.6 0.53 1.94
cis-1,2-Dichloroethene ND ug/m3 12/11/19 02:17 156-59-21.6 0.42 1.94
trans-1,2-Dichloroethene ND ug/m3 12/11/19 02:17 156-60-51.6 0.55 1.94
1,2-Dichloropropane ND ug/m3 12/11/19 02:17 78-87-51.8 0.45 1.94
cis-1,3-Dichloropropene ND ug/m3 12/11/19 02:17 10061-01-51.8 0.59 1.94
trans-1,3-Dichloropropene ND ug/m3 12/11/19 02:17 10061-02-61.8 0.85 1.94
Dichlorotetrafluoroethane ND ug/m3 12/11/19 02:17 76-14-22.8 0.85 1.94
Ethyl acetate ND ug/m3 12/11/19 02:17 141-78-61.4 0.37 1.94
Ethylbenzene ND ug/m3 12/11/19 02:17 100-41-41.7 0.59 1.94
4-Ethyltoluene ND ug/m3 12/11/19 02:17 622-96-84.8 1.1 1.94
n-Heptane ND ug/m3 12/11/19 02:17 142-82-51.6 0.74 1.94
Hexachloro-1,3-butadiene ND ug/m3 12/11/19 02:17 87-68-310.5 3.8 1.94
n-Hexane 4.1 ug/m3 12/11/19 02:17 110-54-31.4 0.60 1.94
2-Hexanone ND ug/m3 12/11/19 02:17 591-78-68.1 1.4 1.94
Methylene Chloride 31.5 ug/m3 12/11/19 02:17 75-09-26.8 2.3 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 12/11/19 02:17 108-10-18.1 1.0 1.94
Methyl-tert-butyl ether ND ug/m3 12/11/19 02:17 1634-04-47.1 1.3 1.94
Naphthalene ND ug/m3 12/11/19 02:17 91-20-35.2 2.5 1.94
Propylene ND ug/m3 12/11/19 02:17 115-07-10.68 0.27 1.94
Styrene 1.1J ug/m3 12/11/19 02:17 100-42-51.7 0.67 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 12/11/19 02:17 79-34-51.4 0.60 1.94
Tetrachloroethene 0.70J ug/m3 12/11/19 02:17 127-18-41.3 0.61 1.94
Tetrahydrofuran ND ug/m3 12/11/19 02:17 109-99-91.2 0.51 1.94
Toluene 0.89J ug/m3 12/11/19 02:17 108-88-31.5 0.68 1.94
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
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Page 15 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92456012
JMC-009
Sample:DUP CAN #1775 Lab ID:92456012006 Collected:12/03/19 00:00 Received:12/04/19 07:49 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 12/11/19 02:17 120-82-114.6 7.2 1.94
1,1,1-Trichloroethane ND ug/m3 12/11/19 02:17 71-55-62.2 0.60 1.94
1,1,2-Trichloroethane ND ug/m3 12/11/19 02:17 79-00-51.1 0.47 1.94
Trichloroethene ND ug/m3 12/11/19 02:17 79-01-61.1 0.49 1.94
Trichlorofluoromethane 2.0J ug/m3 12/11/19 02:17 75-69-42.2 0.71 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 12/11/19 02:17 76-13-13.0 1.1 1.94
1,2,4-Trimethylbenzene ND ug/m3 12/11/19 02:17 95-63-61.9 0.88 1.94
1,3,5-Trimethylbenzene ND ug/m3 12/11/19 02:17 108-67-81.9 0.77 1.94
Vinyl acetate ND ug/m3 12/11/19 02:17 108-05-41.4 0.52 1.94
Vinyl chloride ND ug/m3 12/11/19 02:17 75-01-40.50 0.24 1.94
m&p-Xylene ND ug/m3 12/11/19 02:17 179601-23-13.4 1.4 1.94
o-Xylene ND ug/m3 12/11/19 02:17 95-47-61.7 0.67 1.94
REPORT OF LABORATORY ANALYSIS
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Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92456012
JMC-009
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
648929
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92456012001, 92456012002, 92456012003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3490712
Associated Lab Samples:92456012001, 92456012002, 92456012003
Matrix:Air
AnalyzedMDL
1,1,1-Trichloroethane ug/m3 ND 0.56 12/09/19 11:370.15
1,1,2,2-Tetrachloroethane ug/m3 ND 0.35 12/09/19 11:370.15
1,1,2-Trichloroethane ug/m3 ND 0.28 12/09/19 11:370.12
1,1,2-Trichlorotrifluoroethane ug/m3 ND 0.78 12/09/19 11:370.28
1,1-Dichloroethane ug/m3 ND 0.41 12/09/19 11:370.11
1,1-Dichloroethene ug/m3 ND 0.40 12/09/19 11:370.14
1,2,4-Trichlorobenzene ug/m3 ND 3.8 12/09/19 11:371.9
1,2,4-Trimethylbenzene ug/m3 ND 0.50 12/09/19 11:370.23
1,2-Dibromoethane (EDB)ug/m3 ND 0.39 12/09/19 11:370.18
1,2-Dichlorobenzene ug/m3 ND 0.61 12/09/19 11:370.25
1,2-Dichloroethane ug/m3 ND 0.21 12/09/19 11:370.075
1,2-Dichloropropane ug/m3 ND 0.47 12/09/19 11:370.12
1,3,5-Trimethylbenzene ug/m3 ND 0.50 12/09/19 11:370.20
1,3-Butadiene ug/m3 ND 0.22 12/09/19 11:370.064
1,3-Dichlorobenzene ug/m3 ND 0.61 12/09/19 11:370.29
1,4-Dichlorobenzene ug/m3 ND 1.5 12/09/19 11:370.50
2-Butanone (MEK)ug/m3 ND 1.5 12/09/19 11:370.18
2-Hexanone ug/m3 ND 2.1 12/09/19 11:370.37
4-Ethyltoluene ug/m3 ND 1.2 12/09/19 11:370.28
4-Methyl-2-pentanone (MIBK)ug/m3 ND 2.1 12/09/19 11:370.26
Acetone ug/m3 ND 1.2 12/09/19 11:370.60
Benzene ug/m3 ND 0.16 12/09/19 11:370.076
Bromodichloromethane ug/m3 ND 0.68 12/09/19 11:370.18
Bromoform ug/m3 ND 2.6 12/09/19 11:370.71
Bromomethane ug/m3 ND 0.39 12/09/19 11:370.11
Carbon disulfide ug/m3 ND 0.32 12/09/19 11:370.11
Carbon tetrachloride ug/m3 ND 0.64 12/09/19 11:370.21
Chlorobenzene ug/m3 ND 0.47 12/09/19 11:370.14
Chloroethane ug/m3 ND 0.27 12/09/19 11:370.13
Chloroform ug/m3 ND 0.25 12/09/19 11:370.098
Chloromethane ug/m3 ND 0.21 12/09/19 11:370.078
cis-1,2-Dichloroethene ug/m3 ND 0.40 12/09/19 11:370.11
cis-1,3-Dichloropropene ug/m3 ND 0.46 12/09/19 11:370.15
Cyclohexane ug/m3 ND 0.88 12/09/19 11:370.18
Dibromochloromethane ug/m3 ND 0.86 12/09/19 11:370.36
Dichlorodifluoromethane ug/m3 ND 0.50 12/09/19 11:370.15
Dichlorotetrafluoroethane ug/m3 ND 0.71 12/09/19 11:370.22
Ethyl acetate ug/m3 ND 0.37 12/09/19 11:370.095
Ethylbenzene ug/m3 ND 0.44 12/09/19 11:370.15
Hexachloro-1,3-butadiene ug/m3 ND 2.7 12/09/19 11:370.98
m&p-Xylene ug/m3 ND 0.88 12/09/19 11:370.35
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
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Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92456012
JMC-009
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3490712
Associated Lab Samples:92456012001, 92456012002, 92456012003
Matrix:Air
AnalyzedMDL
Methyl-tert-butyl ether ug/m3 ND 1.8 12/09/19 11:370.33
Methylene Chloride ug/m3 ND 1.8 12/09/19 11:370.60
n-Heptane ug/m3 ND 0.42 12/09/19 11:370.19
n-Hexane ug/m3 ND 0.36 12/09/19 11:370.16
Naphthalene ug/m3 ND 1.3 12/09/19 11:370.66
o-Xylene ug/m3 ND 0.44 12/09/19 11:370.17
Propylene ug/m3 ND 0.18 12/09/19 11:370.070
Styrene ug/m3 ND 0.43 12/09/19 11:370.17
Tetrachloroethene ug/m3 ND 0.34 12/09/19 11:370.16
Tetrahydrofuran ug/m3 ND 0.30 12/09/19 11:370.13
Toluene ug/m3 ND 0.38 12/09/19 11:370.18
trans-1,2-Dichloroethene ug/m3 ND 0.40 12/09/19 11:370.14
trans-1,3-Dichloropropene ug/m3 ND 0.46 12/09/19 11:370.22
Trichloroethene ug/m3 ND 0.27 12/09/19 11:370.13
Trichlorofluoromethane ug/m3 ND 0.57 12/09/19 11:370.18
Vinyl acetate ug/m3 ND 0.36 12/09/19 11:370.14
Vinyl chloride ug/m3 ND 0.13 12/09/19 11:370.063
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3490713LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 66.555.5 120 70-130
1,1,2,2-Tetrachloroethane ug/m3 82.369.8 118 70-132
1,1,2-Trichloroethane ug/m3 64.455.5 116 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 91.377.9 117 70-130
1,1-Dichloroethane ug/m3 51.841.1 126 70-130
1,1-Dichloroethene ug/m3 48.340.3 120 70-130
1,2,4-Trichlorobenzene ug/m3 81.375.4 108 56-130
1,2,4-Trimethylbenzene ug/m3 59.950 120 70-134
1,2-Dibromoethane (EDB)ug/m3 94.778.1 121 70-130
1,2-Dichlorobenzene ug/m3 73.961.1 121 70-132
1,2-Dichloroethane ug/m3 49.941.1 121 70-130
1,2-Dichloropropane ug/m3 54.547 116 70-130
1,3,5-Trimethylbenzene ug/m3 56.750 114 70-132
1,3-Butadiene ug/m3 26.722.5 119 65-130
1,3-Dichlorobenzene ug/m3 76.161.1 125 70-137
1,4-Dichlorobenzene ug/m3 61.361.1 100 70-134
2-Butanone (MEK)ug/m3 28.730 96 70-130
2-Hexanone ug/m3 54.1 CH41.6 130 70-135
4-Ethyltoluene ug/m3 59.850 120 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 51.041.6 122 70-131
Acetone ug/m3 134121 111 67-130
Benzene ug/m3 37.132.5 114 70-130
Bromodichloromethane ug/m3 82.768.1 121 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
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Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92456012
JMC-009
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3490713LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 119105 114 70-132
Bromomethane ug/m3 46.839.5 119 69-130
Carbon disulfide ug/m3 37.131.6 117 56-137
Carbon tetrachloride ug/m3 75.064 117 66-131
Chlorobenzene ug/m3 54.246.8 116 70-130
Chloroethane ug/m3 30.526.8 114 70-130
Chloroform ug/m3 58.449.6 118 70-130
Chloromethane ug/m3 25.021 119 66-130
cis-1,2-Dichloroethene ug/m3 46.240.3 115 70-130
cis-1,3-Dichloropropene ug/m3 56.046.1 121 70-133
Cyclohexane ug/m3 41.235 118 68-132
Dibromochloromethane ug/m3 10586.6 122 70-130
Dichlorodifluoromethane ug/m3 57.150.3 114 70-130
Dichlorotetrafluoroethane ug/m3 83.371 117 70-130
Ethyl acetate ug/m3 43.836.6 120 69-130
Ethylbenzene ug/m3 51.544.1 117 67-131
Hexachloro-1,3-butadiene ug/m3 114108 105 66-137
m&p-Xylene ug/m3 10488.3 117 70-132
Methyl-tert-butyl ether ug/m3 58.2 CH,L336.6 159 70-130
Methylene Chloride ug/m3 188177 106 65-130
n-Heptane ug/m3 48.441.7 116 65-130
n-Hexane ug/m3 40.235.8 112 66-130
Naphthalene ug/m3 57.653.3 108 56-130
o-Xylene ug/m3 50.244.1 114 70-130
Propylene ug/m3 19.417.5 111 67-130
Styrene ug/m3 51.643.3 119 69-136
Tetrachloroethene ug/m3 77.368.9 112 70-130
Tetrahydrofuran ug/m3 35.830 119 68-131
Toluene ug/m3 42.738.3 111 70-130
trans-1,2-Dichloroethene ug/m3 72.4 CH,L3,SS40.3 180 70-130
trans-1,3-Dichloropropene ug/m3 51.946.1 113 70-134
Trichloroethene ug/m3 62.354.6 114 70-130
Trichlorofluoromethane ug/m3 68.057.1 119 65-130
Vinyl acetate ug/m3 39.835.8 111 61-133
Vinyl chloride ug/m3 31.026 119 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
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Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92456012
JMC-009
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
649157
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92456012004, 92456012005, 92456012006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3491670
Associated Lab Samples:92456012004, 92456012005, 92456012006
Matrix:Air
AnalyzedMDL
1,1,1-Trichloroethane ug/m3 ND 1.1 12/10/19 15:170.31
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 12/10/19 15:170.31
1,1,2-Trichloroethane ug/m3 ND 0.56 12/10/19 15:170.24
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 12/10/19 15:170.56
1,1-Dichloroethane ug/m3 ND 0.82 12/10/19 15:170.22
1,1-Dichloroethene ug/m3 ND 0.81 12/10/19 15:170.27
1,2,4-Trichlorobenzene ug/m3 ND 7.5 12/10/19 15:173.7
1,2,4-Trimethylbenzene ug/m3 ND 1.0 12/10/19 15:170.45
1,2-Dibromoethane (EDB)ug/m3 ND 0.78 12/10/19 15:170.37
1,2-Dichlorobenzene ug/m3 ND 1.2 12/10/19 15:170.50
1,2-Dichloroethane ug/m3 ND 0.41 12/10/19 15:170.15
1,2-Dichloropropane ug/m3 ND 0.94 12/10/19 15:170.23
1,3,5-Trimethylbenzene ug/m3 ND 1.0 12/10/19 15:170.40
1,3-Butadiene ug/m3 ND 0.45 12/10/19 15:170.13
1,3-Dichlorobenzene ug/m3 ND 1.2 12/10/19 15:170.58
1,4-Dichlorobenzene ug/m3 ND 3.1 12/10/19 15:171.0
2-Butanone (MEK)ug/m3 ND 3.0 12/10/19 15:170.37
2-Hexanone ug/m3 ND 4.2 12/10/19 15:170.74
4-Ethyltoluene ug/m3 ND 2.5 12/10/19 15:170.57
4-Methyl-2-pentanone (MIBK)ug/m3 ND 4.2 12/10/19 15:170.52
Acetone ug/m3 ND 2.4 12/10/19 15:171.2
Benzene ug/m3 ND 0.32 12/10/19 15:170.15
Bromodichloromethane ug/m3 ND 1.4 12/10/19 15:170.37
Bromoform ug/m3 ND 5.2 12/10/19 15:171.4
Bromomethane ug/m3 ND 0.79 12/10/19 15:170.23
Carbon disulfide ug/m3 ND 0.63 12/10/19 15:170.22
Carbon tetrachloride ug/m3 ND 1.3 12/10/19 15:170.43
Chlorobenzene ug/m3 ND 0.94 12/10/19 15:170.28
Chloroethane ug/m3 ND 0.54 12/10/19 15:170.26
Chloroform ug/m3 ND 0.50 12/10/19 15:170.20
Chloromethane ug/m3 ND 0.42 12/10/19 15:170.16
cis-1,2-Dichloroethene ug/m3 ND 0.81 12/10/19 15:170.22
cis-1,3-Dichloropropene ug/m3 ND 0.92 12/10/19 15:170.30
Cyclohexane ug/m3 ND 1.8 12/10/19 15:170.35
Dibromochloromethane ug/m3 ND 1.7 12/10/19 15:170.72
Dichlorodifluoromethane ug/m3 ND 1.0 12/10/19 15:170.29
Dichlorotetrafluoroethane ug/m3 ND 1.4 12/10/19 15:170.44
Ethyl acetate ug/m3 ND 0.73 12/10/19 15:170.19
Ethylbenzene ug/m3 ND 0.88 12/10/19 15:170.30
Hexachloro-1,3-butadiene ug/m3 ND 5.4 12/10/19 15:172.0
m&p-Xylene ug/m3 ND 1.8 12/10/19 15:170.70
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/11/2019 03:38 PM
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Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92456012
JMC-009
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3491670
Associated Lab Samples:92456012004, 92456012005, 92456012006
Matrix:Air
AnalyzedMDL
Methyl-tert-butyl ether ug/m3 ND 3.7 12/10/19 15:170.66
Methylene Chloride ug/m3 ND 3.5 12/10/19 15:171.2
n-Heptane ug/m3 ND 0.83 12/10/19 15:170.38
n-Hexane ug/m3 ND 0.72 12/10/19 15:170.31
Naphthalene ug/m3 ND 2.7 12/10/19 15:171.3
o-Xylene ug/m3 ND 0.88 12/10/19 15:170.34
Propylene ug/m3 ND 0.35 12/10/19 15:170.14
Styrene ug/m3 ND 0.87 12/10/19 15:170.34
Tetrachloroethene ug/m3 ND 0.69 12/10/19 15:170.31
Tetrahydrofuran ug/m3 ND 0.60 12/10/19 15:170.26
Toluene ug/m3 ND 0.77 12/10/19 15:170.35
trans-1,2-Dichloroethene ug/m3 ND 0.81 12/10/19 15:170.28
trans-1,3-Dichloropropene ug/m3 ND 0.92 12/10/19 15:170.44
Trichloroethene ug/m3 ND 0.55 12/10/19 15:170.25
Trichlorofluoromethane ug/m3 ND 1.1 12/10/19 15:170.37
Vinyl acetate ug/m3 ND 0.72 12/10/19 15:170.27
Vinyl chloride ug/m3 ND 0.26 12/10/19 15:170.13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3491671LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 54.156.6 96 70-130
1,1,2,2-Tetrachloroethane ug/m3 74.269.8 106 70-132
1,1,2-Trichloroethane ug/m3 54.658.2 94 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 75.984.9 89 70-130
1,1-Dichloroethane ug/m3 40.342.4 95 70-130
1,1-Dichloroethene ug/m3 37.443.5 86 70-130
1,2,4-Trichlorobenzene ug/m3 83.574.7 112 56-130
1,2,4-Trimethylbenzene ug/m3 53.953 102 70-134
1,2-Dibromoethane (EDB)ug/m3 80.583.6 96 70-130
1,2-Dichlorobenzene ug/m3 66.159.9 110 70-132
1,2-Dichloroethane ug/m3 39.842.8 93 70-130
1,2-Dichloropropane ug/m3 45.448.4 94 70-130
1,3,5-Trimethylbenzene ug/m3 52.453.5 98 70-132
1,3-Butadiene ug/m3 22.022.5 98 65-130
1,3-Dichlorobenzene ug/m3 66.365.4 101 70-137
1,4-Dichlorobenzene ug/m3 66.165.4 101 70-134
2-Butanone (MEK)ug/m3 24.232.4 75 70-130
2-Hexanone ug/m3 42.642.9 99 70-135
4-Ethyltoluene ug/m3 53.652 103 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 41.742 99 70-131
Acetone ug/m3 25.626.6 96 67-130
Benzene ug/m3 30.834.4 90 70-130
Bromodichloromethane ug/m3 66.569.5 96 70-130
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92456012
JMC-009
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3491671LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 73.297.7 75 70-132
Bromomethane ug/m3 36.940.6 91 69-130
Carbon disulfide ug/m3 31.032.9 94 56-137
Carbon tetrachloride ug/m3 70.565.9 107 66-131
Chlorobenzene ug/m3 45.349.6 91 70-130
Chloroethane ug/m3 27.126.8 101 70-130
Chloroform ug/m3 48.552.6 92 70-130
Chloromethane ug/m3 21.222.2 95 66-130
cis-1,2-Dichloroethene ug/m3 37.241.9 89 70-130
cis-1,3-Dichloropropene ug/m3 43.048 90 70-133
Cyclohexane ug/m3 31.635.3 90 68-132
Dibromochloromethane ug/m3 80.990 90 70-130
Dichlorodifluoromethane ug/m3 48.852.8 92 70-130
Dichlorotetrafluoroethane ug/m3 71.474.6 96 70-130
Ethyl acetate ug/m3 33.638.8 87 69-130
Ethylbenzene ug/m3 42.445.5 93 67-131
Hexachloro-1,3-butadiene ug/m3 125108 115 66-137
m&p-Xylene ug/m3 55.645.9 121 70-132
Methyl-tert-butyl ether ug/m3 34.837.4 93 70-130
Methylene Chloride ug/m3 37.938.1 100 65-130
n-Heptane ug/m3 39.043.7 89 65-130
n-Hexane ug/m3 31.737.6 84 66-130
Naphthalene ug/m3 58.852.7 112 56-130
o-Xylene ug/m3 42.144.1 95 70-130
Propylene ug/m3 17.919.2 93 67-130
Styrene ug/m3 45.744.2 103 69-136
Tetrachloroethene ug/m3 66.270.3 94 70-130
Tetrahydrofuran ug/m3 31.330.3 103 68-131
Toluene ug/m3 36.539.4 93 70-130
trans-1,2-Dichloroethene ug/m3 37.941.5 91 70-130
trans-1,3-Dichloropropene ug/m3 48.244.8 108 70-134
Trichloroethene ug/m3 51.456.3 91 70-130
Trichlorofluoromethane ug/m3 54.158.8 92 65-130
Vinyl acetate ug/m3 40.435.1 115 61-133
Vinyl chloride ug/m3 26.328.1 94 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92456012004
3492350SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 ND 25ND
1,1,2,2-Tetrachloroethane ug/m3 ND 25ND
1,1,2-Trichloroethane ug/m3 ND 25ND
1,1,2-Trichlorotrifluoroethane ug/m3 ND 25ND
1,1-Dichloroethane ug/m3 ND 25ND
1,1-Dichloroethene ug/m3 ND 25ND
REPORT OF LABORATORY ANALYSIS
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Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92456012
JMC-009
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92456012004
3492350SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/m3 ND 25ND
1,2,4-Trimethylbenzene ug/m3 ND 25ND
1,2-Dibromoethane (EDB)ug/m3 ND 25ND
1,2-Dichlorobenzene ug/m3 ND 25ND
1,2-Dichloroethane ug/m3 ND 25ND
1,2-Dichloropropane ug/m3 ND 25ND
1,3,5-Trimethylbenzene ug/m3 ND 25ND
1,3-Butadiene ug/m3 ND 25ND
1,3-Dichlorobenzene ug/m3 ND 25ND
1,4-Dichlorobenzene ug/m3 ND 25ND
2-Butanone (MEK)ug/m3 6.4 8 255.9
2-Hexanone ug/m3 ND 25ND
4-Ethyltoluene ug/m3 ND 25ND
4-Methyl-2-pentanone (MIBK)ug/m3 ND 25ND
Acetone ug/m3 75.0 10 2567.6
Benzene ug/m3 0.34J 25ND
Bromodichloromethane ug/m3 ND 25ND
Bromoform ug/m3 ND 25ND
Bromomethane ug/m3 ND 25ND
Carbon disulfide ug/m3 0.71J 250.63J
Carbon tetrachloride ug/m3 ND 25ND
Chlorobenzene ug/m3 ND 25ND
Chloroethane ug/m3 ND 25ND
Chloroform ug/m3 ND 25ND
Chloromethane ug/m3 0.43J 250.45J
cis-1,2-Dichloroethene ug/m3 ND 25ND
cis-1,3-Dichloropropene ug/m3 ND 25ND
Cyclohexane ug/m3 ND 25ND
Dibromochloromethane ug/m3 ND 25ND
Dichlorodifluoromethane ug/m3 2.9 19 252.4
Dichlorotetrafluoroethane ug/m3 ND 25ND
Ethyl acetate ug/m3 ND 251.1J
Ethylbenzene ug/m3 ND 25ND
Hexachloro-1,3-butadiene ug/m3 ND 25ND
m&p-Xylene ug/m3 ND 25ND
Methyl-tert-butyl ether ug/m3 ND 25ND
Methylene Chloride ug/m3 36.8 15 2531.7
n-Heptane ug/m3 1.1J 250.90J
n-Hexane ug/m3 4.9 18 254.1
Naphthalene ug/m3 ND 25ND
o-Xylene ug/m3 ND 25ND
Propylene ug/m3 ND 25ND
Styrene ug/m3 1.3J 251.1J
Tetrachloroethene ug/m3 1.7 3 251.6
Tetrahydrofuran ug/m3 ND 25ND
Toluene ug/m3 2.5 9 252.3
trans-1,2-Dichloroethene ug/m3 ND 25ND
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92456012
JMC-009
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92456012004
3492350SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/m3 ND 25ND
Trichloroethene ug/m3 ND 25ND
Trichlorofluoromethane ug/m3 2.4 252.0J
Vinyl acetate ug/m3 ND 25ND
Vinyl chloride ug/m3 ND 25ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92456012005
3492351SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 8.8 7 258.2
1,1,2,2-Tetrachloroethane ug/m3 ND 25ND
1,1,2-Trichloroethane ug/m3 ND 25ND
1,1,2-Trichlorotrifluoroethane ug/m3 ND 25ND
1,1-Dichloroethane ug/m3 ND 25ND
1,1-Dichloroethene ug/m3 ND 25ND
1,2,4-Trichlorobenzene ug/m3 ND 25ND
1,2,4-Trimethylbenzene ug/m3 ND 25ND
1,2-Dibromoethane (EDB)ug/m3 ND 25ND
1,2-Dichlorobenzene ug/m3 ND 25ND
1,2-Dichloroethane ug/m3 ND 25ND
1,2-Dichloropropane ug/m3 ND 25ND
1,3,5-Trimethylbenzene ug/m3 ND 25ND
1,3-Butadiene ug/m3 ND 25ND
1,3-Dichlorobenzene ug/m3 ND 25ND
1,4-Dichlorobenzene ug/m3 ND 25ND
2-Butanone (MEK)ug/m3 9.6 14 258.3
2-Hexanone ug/m3 ND 25ND
4-Ethyltoluene ug/m3 ND 25ND
4-Methyl-2-pentanone (MIBK)ug/m3 ND 251.4J
Acetone ug/m3 122 5 25116
Benzene ug/m3 0.35J 25ND
Bromodichloromethane ug/m3 ND 25ND
Bromoform ug/m3 ND 25ND
Bromomethane ug/m3 0.49J 250.50J
Carbon disulfide ug/m3 ND 25ND
Carbon tetrachloride ug/m3 ND 25ND
Chlorobenzene ug/m3 ND 25ND
Chloroethane ug/m3 ND 25ND
Chloroform ug/m3 0.44J 250.44J
Chloromethane ug/m3 1.3 18 251.1
cis-1,2-Dichloroethene ug/m3 ND 25ND
cis-1,3-Dichloropropene ug/m3 ND 25ND
Cyclohexane ug/m3 ND 25ND
Dibromochloromethane ug/m3 ND 25ND
Dichlorodifluoromethane ug/m3 3.1 14 252.7
REPORT OF LABORATORY ANALYSIS
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92456012
JMC-009
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92456012005
3492351SAMPLE DUPLICATE:
Dichlorotetrafluoroethane ug/m3 ND 25ND
Ethyl acetate ug/m3 ND 25ND
Ethylbenzene ug/m3 ND 25ND
Hexachloro-1,3-butadiene ug/m3 ND 25ND
m&p-Xylene ug/m3 ND 25ND
Methyl-tert-butyl ether ug/m3 ND 25ND
Methylene Chloride ug/m3 92.7 12 2582.1
n-Heptane ug/m3 ND 250.92J
n-Hexane ug/m3 9.1 5 258.7
Naphthalene ug/m3 ND 25ND
o-Xylene ug/m3 ND 25ND
Propylene ug/m3 ND 25ND
Styrene ug/m3 ND 25ND
Tetrachloroethene ug/m3 3.8 17 253.2
Tetrahydrofuran ug/m3 ND 25ND
Toluene ug/m3 1.6 251.4J
trans-1,2-Dichloroethene ug/m3 ND 25ND
trans-1,3-Dichloropropene ug/m3 ND 25ND
Trichloroethene ug/m3 ND 25ND
Trichlorofluoromethane ug/m3 3.8 15 253.3
Vinyl acetate ug/m3 ND 25ND
Vinyl chloride ug/m3 ND 25ND
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Page 25 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92456012
JMC-009
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.CH
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples.L3
This analyte did not meet the secondary source verification criteria for the initial calibration. The reported result should be
considered an estimated value.SS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92456012
JMC-009
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92456012001 648929SSV-1 CAN #2408 TO-15
92456012002 648929SSV-2 CAN #3638 TO-15
92456012003 648929SSV-3 CAN #2983 TO-15
92456012004 649157SSV-4 CAN #2255 TO-15
92456012005 649157SSV-5 CAN #1023 TO-15
92456012006 649157DUP CAN #1775 TO-15
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Page 27 of 28
Page 28 of 28

Appendix C DEQ Worst Case Risk Calculator Output
Risk for Individual Pathways Output Form 1A
Version Date: May 2019
Basis: May 2019 EPA RSL Table
Site ID:
Exposure Unit ID: Worst Case Vapor Levels - Cold Weather
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use* NC NC NC
Soil NC NC NC
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.2E-06 6.5E-02 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.7E-07 5.2E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: May 2019
Basis: May 2019 EPA RSL Table
Site ID:
Exposure Unit ID: Worst Case Vapor Levels - Cold Weather
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 136 1.36 - 2.7E+04 1.0E-05
71-43-2 Benzene 1.9 0.019 1.6E+00 2.6E+01 1.2E-08 1.4E-04
75-15-0 Carbon Disulfide 1.2 0.012 - 6.1E+02 3.9E-06
67-66-3 Chloroform 0.44 0.0044 5.3E-01 8.6E+01 8.3E-09 1.0E-05
74-87-3 Chloromethane 1.1 0.011 - 7.9E+01 2.8E-05
110-82-7 Cyclohexane 1.7 0.017 - 5.3E+03 6.5E-07
106-46-7 Dichlorobenzene, 1,4- 3.1 0.031 1.1E+00 7.0E+02 2.8E-08 8.8E-06
75-71-8 Dichlorodifluoromethane 3.6 0.036 - 8.8E+01 8.2E-05
141-78-6 Ethyl Acetate 1.3 0.013 - 6.1E+01 4.2E-05
109-99-9 ~Tetrahydrofuran 1.2 0.012 - 1.8E+03 1.4E-06
142-82-5 Heptane, N- 1.5 0.015 - 3.5E+02 8.6E-06
110-54-3 Hexane, N- 9.5 0.095 - 6.1E+02 3.1E-05
591-78-6 Hexanone, 2- 4.6 0.046 - 2.6E+01 3.5E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone) 9.9 0.099 - 4.4E+03 4.5E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 1.4 0.014 - 2.6E+03 1.1E-06
75-09-2 Methylene Chloride 96.5 0.965 1.2E+03 5.3E+02 7.9E-10 3.7E-04
91-20-3 ~Naphthalene 4.2 0.042 3.6E-01 2.6E+00 1.2E-07 3.2E-03
115-07-1 Propylene 5.4 0.054 - 2.6E+03 4.1E-06
100-42-5 Styrene 1.6 0.016 - 8.8E+02 3.7E-06
127-18-4 Tetrachloroethylene 13.9 0.139 4.7E+01 3.5E+01 2.9E-09 7.9E-04
108-88-3 Toluene 2.6 0.026 - 4.4E+03 1.2E-06
71-55-6 Trichloroethane, 1,1,1- 8.2 0.082 - 4.4E+03 3.7E-06
75-69-4 Trichlorofluoromethane 5.9 0.059 - -
95-63-6 Trimethylbenzene, 1,2,4- 0.89 0.0089 - 5.3E+01 3.4E-05
108-05-4 Vinyl Acetate 3.2 0.032 - 1.8E+02 3.7E-05
108-38-3 Xylene, m- 0.76 0.0076 - 8.8E+01 1.7E-05
Cumulative: 1.7E-07 5.2E-03
All concentrations are in ug/m3
Output Form
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: May 2019
Basis: May 2019 EPA RSL Table
Site ID:
Exposure Unit ID: Worst Case Vapor Levels - Cold Weather
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 136 4.08 - 6.5E+03 1.3E-04
71-43-2 Benzene 1.9 0.057 3.6E-01 6.3E+00 1.6E-07 1.8E-03
75-15-0 Carbon Disulfide 1.2 0.036 - 1.5E+02 4.9E-05
67-66-3 Chloroform 0.44 0.0132 1.2E-01 2.0E+01 1.1E-07 1.3E-04
74-87-3 Chloromethane 1.1 0.033 - 1.9E+01 3.5E-04
110-82-7 Cyclohexane 1.7 0.051 - 1.3E+03 8.2E-06
106-46-7 Dichlorobenzene, 1,4- 3.1 0.093 2.6E-01 1.7E+02 3.6E-07 1.1E-04
75-71-8 Dichlorodifluoromethane 3.6 0.108 - 2.1E+01 1.0E-03
141-78-6 Ethyl Acetate 1.3 0.039 - 1.5E+01 5.3E-04
109-99-9 ~Tetrahydrofuran 1.2 0.036 - 4.2E+02 1.7E-05
142-82-5 Heptane, N- 1.5 0.045 - 8.3E+01 1.1E-04
110-54-3 Hexane, N- 9.5 0.285 - 1.5E+02 3.9E-04
591-78-6 Hexanone, 2- 4.6 0.138 - 6.3E+00 4.4E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone) 9.9 0.297 - 1.0E+03 5.7E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 1.4 0.042 - 6.3E+02 1.3E-05
75-09-2 Methylene Chloride 96.5 2.895 1.0E+02 1.3E+02 2.9E-08 4.6E-03
91-20-3 ~Naphthalene 4.2 0.126 8.3E-02 6.3E-01 1.5E-06 4.0E-02
115-07-1 Propylene 5.4 0.162 - 6.3E+02 5.2E-05
100-42-5 Styrene 1.6 0.048 - 2.1E+02 4.6E-05
127-18-4 Tetrachloroethylene 13.9 0.417 1.1E+01 8.3E+00 3.9E-08 1.0E-02
108-88-3 Toluene 2.6 0.078 - 1.0E+03 1.5E-05
71-55-6 Trichloroethane, 1,1,1- 8.2 0.246 - 1.0E+03 4.7E-05
75-69-4 Trichlorofluoromethane 5.9 0.177 - -
95-63-6 Trimethylbenzene, 1,2,4- 0.89 0.0267 - 1.3E+01 4.3E-04
108-05-4 Vinyl Acetate 3.2 0.096 - 4.2E+01 4.6E-04
108-38-3 Xylene, m- 0.76 0.0228 - 2.1E+01 2.2E-04
Cumulative: 2.2E-06 6.5E-02
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator

Appendix D Brownfields Property Receptor Survey Form
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site: Former Cotton Seed Oil Mill
Address: 300 Rampart Street
City: Charlotte
County: Mecklenburg
Brownfields Project Number: 23053-19-060
Property and Building Characteristics
a. Provide occupancy and use information.
The Site consists of one parcel of land (Parcel ID: 12103209) that total approximately 2.4 acres.
The Site is currently developed with an approximately 65,136-square foot industrial warehouse building that is currently vacant
The Site was historically occupied by portions of a Cotton Seed Oil Mill (late 1800s to early 1900s), portions of the Virginia
Carolina Chemical fertilizer company (early 1900s to mid-1900s), a lumber milling operation in the 1960s, and a steel pail
painting operation in the 1980s. The Site was then occupied by the Charlotte Salage Company until the late 2010s.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
The Site building is constructed with a slab on-grade foundation.
The building is heated by electric and natural gas-powered heaters. Cooling is not currently provided within the building.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
The presence of subslab moisture barriers within the Site property building is unknown, but unlikely.
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design
considerations (e.g. positive pressure?).
0
65
% of property that is grassed areas (unpaved)
% of property that is agricultural crops
% of property that is paved
The warehouse building is a single-story, brick and concrete block framed, slab on-grade building. Bay doors are located along
the northern, eastern, and southern edges of the building.
Current Usage Proposed UsageSurface Conditions
% of property that is wooded/brush
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed. If numerous
buildings are on-site, consult with your PM as only information on specific buildings may be needed.
b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of openings (e.g. windows, bay
doors), and height (number of stories).
% of property that is covered by buildings
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information requested
below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ Brownfield’s Project Manager
(PM).
NA
Commercial
2.4
0
5
30
Size of Property (acres)
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North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
West
N----
Y* Adjacent N, S
N----
Utilities
Is there a septic system on-site? (Y or N) N
Please provide the utility providers for the subject property
a. Natural Gas: Piedmont Natural Gas (underground)
b. Sewer: Charlotte Water (underground)
c. Electricity: Duke Energy (above ground)
d. Other: Communication (underground)
For surrounding properties, please complete the following table with available information.
Y <5 On-Site, S
Y <5 On-Site, NE, SW
UNK -- --
Y<5 S
Y30 S
Y<5 S
N-- --
Is there a residence within 1,000 ft of the Property?
Y/N * DirectionUtility/Potential Receptor
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses.
Distance
(ft)
Is a sanitary sewer within 100 ft of the Property boundary?
For the subject property, please provide a map of known buried utilites. If available, include depth to top, construction material, and
diameter of the utilities. In addition, please provide the following information on utilty providers. If additional assessment is required, the
public utility locators should be contacted. This information can then be added to a site map.
Transit-Oriented (TOD-MO)
Transit-Oriented (TOD-UC)
Transit-Oriented (TOD-UC)
Transit-Oriented (TOD-NC)
NA
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If specific
receptors are present, please provide addresses of the facilities.
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject property.
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is there a basement within 1,000 ft of the Property
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
--
Zoning/Land Use
See Figure 3
--
Proposed Usage Current Use/Occupant
Is a school or daycare center within 1,000 ft of the Property?
NA
NA
NA
DirectionDistance
(ft)Address
Rev. 09/2015 Page 2 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public X Private ______
Charlotte Water
N -- -- --
N -- -- --
N -- -- --
Surface Water & Wetlands
b. List the uses of the water body.
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property boundary?
Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
a. Is the water body naturally developed or man-made?
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield survey
within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation wells may be present.
Information from applicable databases can and should be utilized; however, should not be utilized in lieu of the windshield survey. If
multiple wells are present within the requested radius, please provide a map of the well locations. If needed, please attach a separate table
to list all wells. Please note, the PM may opt for a more extensive water supply well survey if needed.
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the
Property.
No
Are there surface water features on the property? (If yes,
please complete a. to d.)
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the water
providers name.
Distance
(ft)Direction
Provide Information regarding Surface Water and Wetlands
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
Address
Rev. 09/2015 Page 3 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
No
c. What is the source of the water for the water body?
d. What is the nature of the bottom of the water body
(e.g., rocky or concrete bottom, drainage ways or
impoundments)
If no on-site surface water features, what is the nearest
surface water body?
Are there any wetlands present on the property? If no
wetlands on-site, are wetlands suspected on adjoining
properties?
Unnamed tribuatry of Irwin Creek, located approximately 1,400 ft north of the Site
Rev. 09/2015 Page 4 of 4