RA-2071_12611_CA_MRP_20100920_Terraine Groundwater Monitoring Letter Report

September 20, 2010
Mark Petermann, Hydrogeologist
Underground Storage Tank Section Division of Waste Management -- NCDENR
1637 Mail Service Center Raleigh, North Carolina 27699-1637

Reference: Ferrell Residence 5379 Wiggins Mill Road
Lucama, NC 27851 Wilson County
Incident # 12611
Subject: Groundwater Monitoring Results
Dear Mr. Petermann:
Terraine, Inc. (Terraine) has prepared this letter report to summarize the results of groundwater
monitoring activities at the Ferrell Residence located at 5379 Wiggins Mill Road, Lucama, Wilson County, North Carolina.
On August 31, 2010, Terraine personnel mobilized to the site to collect groundwater samples from
monitoring wells MW-1, MW-3, and MW-5R using new disposable bailers, and from water supply wells WSW-2 and WSW-3 to evaluate current groundwater quality conditions. Groundwater elevation data is
presented in Table 1. The groundwater samples were submitted under proper chain of custody control to the Pace Analytical laboratory in Huntersville, North Carolina, for chemical analysis. Groundwater
analytical data are summarized in Table 2. A complete laboratory report and chain of custody form for the groundwater samples obtained are attached.
Immediately following sampling, a Universal Remediation, Inc. PRP® Well Boom was installed in
monitoring well MW-1. Well Booms contain powdered beeswax and stimulate rapid biodegradation of dissolved petroleum contaminants. The incident manager was notified of contamination in water supply
well WSW-3 immediately following receipt of the analytical results.
Should you have any questions regarding any of this information, please contact me at 1-800-531-1242 ext. 710 or [e-mail].
Sincerely,

Jad Bean Project Manager
Terraine, Inc.
Groundwater Monitoring Results – 9/20/2010 Incident # 12611 Ferrell Residence Page 2 Lucama, NC Wilson County
Attachments: Table 1: Summary of Groundwater Elevation Data Table 2: Summary of Groundwater Analytical Results
Chain of Custody Record
Cooler Receipt Form Laboratory Certificates of Analysis
Quality Control Certificate
cc: File
MW-1 10/26/2009 94.03 Unknown 2 30 08/31/2010 11.01 83.02
MW-3 10/26/2009 93.83 Unknown 2 20 08/31/2010 10.53 83.30
MW-5R 12/14/2009 93.49 15-25 2 25 08/31/2010 9.97 83.52
Wilson County
Table 1
Summary of Groundwater Elevation Data
Ferrell Residence
5379 Wiggins Mill Road
Lucama, NC
Units measured in feet unless otherwise noted.
Groundwater elevation measurements based on an unknown benchmark.
GW - Groundwater
TOC - Top of Casing
NCDENR Incident No. 12611
WELL ID INSTALL
DATE
TOC
ELEVATION
SCREEN
INTERVAL
WELL
DIAMETER
(INCHES)
TOTAL
DEPTH
WELL
GAUGE
DATE
DEPTH TO
WATER
FROM TOC
GW
ELEVATION
Table 2 Summary of Groundwater Analytical Results Ferrell Residence 5379 Wiggins Mill Road Lucama, NC Wilson County NCDENR Incident No. 12611MADEP VPH & EPHBenzeneToluene Ethylbenzene XylenesEDBNaphthalene 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene BromodichloromethaneChloroformDibromochloromethaneIsopropylbenzeneMethylene chloride n-Propylbenzene StyreneAliphatic (C05-C08)Aliphatic (C09-C12)Aliphatic (C09-18)Aliphatic (C09-C18) TOTALAliphatic (C19-C36)Aromatic (C09-C10)Aromatic (C11-C22)Aromatic (C09-C22) TOTALLead2-MethylnaphthaleneWell ID Sample DateAAMW-1 8/31/2010106450 5192,010ND250 554192 ND ND ND 38.916.7 72.87.52,82013,400 16713,567ND 1,840 2282,068 15.913.6MW-3 8/31/2010 ND ND ND ND ND ND ND ND ND 0.82 ND ND ND ND ND ND ND ND ND ND ND ND ND 8.2 NDMW-5R 8/31/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND144WSW-2 8/31/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NDWSW-3 8/31/2010 ND ND ND ND ND ND ND ND 1.3 1.31.4ND ND ND ND ND ND ND ND ND ND ND ND ND ND1 600 600 500 0.02 6 400 400 NE 70 0.4 70 5 70 70 420 NE NE 4,200 42,000 NE NE 210 15 3015A NCAC 2L.0202 (2L) Standard,,5,000 260,000 84,500 85,500 50 6,000 28,500 25,000 NE 70,000 400 25,000 5,000 30,000 70,000 NE NE NE NE NE NE NE NE 15,000 12,500()Gross Contamination Level (GCL)All results expressed in µg/L (ppb)ND - None Detected (below method detection limit)Values shown in bold, italicized, yellow highlighted font indicate concentrations that exceed the 2L standardsEPH - Extractable Petroleum HydrocarbonsNA - Not AnalyzedMTBE - Methyl tert-butyl etherIPE - Diisopropyl etherEDB - 1,2-DibromoethaneMADEP - Massachusetts Department of Environmental ProtectionVPH - Volatile Petroleum HydrocarbonsNE - No Standard EstablishedEPH - Extractable Petroleum Hydrocarbons
I I
/~eAnalytica/"
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CHAIN-OF-CUSTODY I Analytical Request Document
The Chain-ol-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C Page: ( of
Required Client Information: Required Project Information: Invoice Information: 1352221 Company: ...-~V /I, LoA tJ l",e.. Attention:
Address: II "{ S ' PuS tV\. sf, Company Name: Nl'E~fl:. REGULATORY AGENCY
Address: r NPDES r GROUND WATER r' DRINKING WATER
EntV~ ~~ e~t.i.c.t.CtJM.. urchase Order No.: t·t.J..R t \
lJIfytt:q tlI.ot¥t~ IFax: Project Name: ~vvt..lt .~ l ~(...LJ
Requested Due DatelT AT: Project Number: .13 -tJCSLtJ'1-D 11--1-
Pace Quote
Reference:
Pace Project
Manager:
Pace Profile #:
. ~ST r RCRA
Site Location tJCt STATE:
~equested Analysis Filtered (YIN) -Section D
Required Client Information
Matrix Codes ~ Ii:" Z
MATRIX I CODE :;: COLLECTED Preservatives ): g 0 Drinking Waler OW !8 () z ~. Water WT "8 " 0 () COMPOSITE COMPOSITE >= WasteWater WW "0 III END/GRAB () .~ Product P ~ ~ START UJ ...I
Soil/Solid SL ...I 1 (!) 0 en .. Oil OL " () t= Q. IX: 'lil to Wipe WP I-W W « z ~ :l Air AR C UJ n. ~ "0 ~ Tissue TS 0 n. :;: CD III i other OT 0 ~ I!:! z 2: -i ~ I~ 1 X UJ UJ 0 CD 0 g
ex: ...I ...I 0 Ul ... n. n. l!10 0 J: J) III lii lfi ~ LL .s::: :;: :;: 0 a.cn U ~ dl' a;= « « c: N Z ~ ::!E CI) DATE TIME DATE TIME en 'It ::JJ: J: J: Z z ::20 .. ,..l
SAMPLE 10
(A-Z,O-9/,-)
Sample IDs MUST BE UNIQUE
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ADDITIONAL COMMENTS RELINQUIS""D BY I AFFIL"TION DATE TIME Aq E TED)l11t AF.!!}IA TION DATE TIME
... V I I ( '--___ J
ORIGINAL SAMPLER NAME AND SIGNATURE
PRINT Name of SAMPLER: I I1LtflL. 7J?ifii.l'1s~ •
*Important Note. By signing thiS form you are accepting Pace s NET 30 day payment terms and agreein to late charges of 1.5% er monYtorLn invoices not aid ~in 30 days.
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CD c: "§ :;:
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Pace Project No.1 Lab 1.0.
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SAMPLE CONDITIONS
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F-ALL-Q-020rev.07,15-May-2007
Sample Condition Upon Receipt ~ ....... ,.
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.. PaceAnalyticat Client Name:.T_L...-L=f\~4.~~""=<"-:....-___ __ Project # tty? {o161j!
Where Received: ~ Huntersville 0 Asheville o Eden
Courier: 0 Fed Ex 0 UPS 0 USPS 0 Client 0 Commercial ~ Pace Other __ _ .Qolional .... " .'
Custody Seal on Cooler!Box Present: 0 yes ~ no Seals intact: 0 yes o no 'p;roj. DUEl[)ate:
Proj. Name:
Packing Material: 0 Bubble Wrap ~Bubble Bags 0 None DOther ___ _
Thermometer Used: IR Gun: T809 Type of Ice: ~ Blue None fSJ. Samples on ice, cooling process has begun
Temp Correction Factor: Add! Subtract 0 C
Corrected Cooler Temp.: 2, } C Biological Tissue is Frozen: Yes C?v Date an~ns of p..~/txamining
content jt;;IJ-cA () I b
Temp should be above freezing to 6°C Comments: ,
Chain of Custody Present: '/JYes DNo DN/A 1. "
Chain of Custody Filled Out: \Zhes DNo DN/A 2.
Chain of Custody Relinquished: ' . 'rtJYes DNo DN/A 3, .
"
¢Yes
"",'
Sampler Name & Signature on COC: DNo DN/A 4 . "
. ¢Yes
.,
Samples Arrived within Hold Time: DNo DN/A 5. '.
Short Hold Time Analysis «72hr): '~Yes DNo DN/A 6.
DYes !fiNo
.'
Rush Turn Around Time Requested: DN/A 7.
Sufficient Volume: ¢Yes DNo DN/A 8. ,
Correct Containers Used: ~Yes DNo DN/A 9.
-"--~--
r/JYes dNo
.. .. I
-Pace Containers Used: DN/A
Containers Intact: rfJyes DNo DN/A 10,
Filtered volume received for Dissolved tests DYes DNo '/JN/A 11.
Sample Labels match COC: )t!yes DNo DN/A 12.
-Includes date/timeliD/Analysis Matrix: ~'\l
~II containers needing preservation have been checked.
rYes DNo DN/A 13. ..
1\11 containers needing preservation are found to be in
;ompliance with EPA recommendation. rYes DNo DN/A -lxceptions: VOA, coliform, TOe, O&G, WI,DRO (water) DYes DNo Initial when completed
Samples checked for dechlorination: rjjYes DNo DN/A 14.
;eadspace in VOA Vials ( >6mm): DYes ¢:lNO DN/A 15.
rrip Blank Present: DYes DNo ~N/A 16.
rrip Blank Custody Seals Present DYes DNo r{JN/A
:>ace Trip Blank Lot # (if purchased):
:;Iient Notification! Resolution: Field Data Required? YIN
Person Contacted: DatelTime: ---------------------------Comments! Resolution: ________________________________________________________________________ _
Project Manager Review:
~ote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the
~ertification Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers)
F-CHR-CS-003-rev.OO
September 13, 2010
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 9276754
9276754
Project:
Pace Project No.:
RE:
Ms. Linda BlalockNCDENR - UST Section1637 Mail Service CenterRaleigh, NC 276991637
12611 FERRELL RESIDENCE
Dear Ms. Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on September 01, 2010.
The results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Renee Spencer
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784
South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031
Asheville Certification IDs2225 Riverside Dr., Asheville, NC 28804Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030New Jersey Certification #: NC011North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002South Carolina Certification #: 99030001Virginia Certification #: 00072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Lab ID Sample ID Matrix Date Collected Date Received
9276754001 MW-5 Water 08/31/10 10:30 09/01/10 15:50
9276754002 MW-1 Water 08/31/10 11:30 09/01/10 15:50
9276754003 WSW-2 Water 08/31/10 11:40 09/01/10 15:50
9276754004 WSW-3 Water 08/31/10 12:10 09/01/10 15:50
9276754005 MW-3 Water 08/31/10 12:45 09/01/10 15:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9276754001 MW-5 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CTLS
9276754002 MW-1 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CTLS
9276754003 WSW-2 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CTLS
9276754004 WSW-3 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CTLS
9276754005 MW-3 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CTLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-5 Lab ID:9276754001 Collected:08/31/10 10:30 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 09/04/10 11:5409/03/10 08:00125125
Aliphatic (C19-C36)ND ug/L 1 09/04/10 11:5409/03/10 08:00125125
Aromatic (C11-C22)ND ug/L 1 09/04/10 11:5409/03/10 08:00125125
Nonatriacontane (S)112 %1 09/04/10 11:54 7194-86-709/03/10 08:0040-140
o-Terphenyl (S)92 %1 09/04/10 11:54 84-15-109/03/10 08:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/02/10 18:23100100
Aliphatic (C09-C12)ND ug/L 1 09/02/10 18:23100100
Aromatic (C09-C10)ND ug/L 1 09/02/10 18:23100100
2,5-Dibromotoluene (PID)(S)95 %1 09/02/10 18:2370-130
2,5-Dibromotoluene (FID)(S)95 %1 09/02/10 18:2370-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 144 ug/L 1 09/08/10 00:42 7439-92-1 B09/02/10 10:355.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/08/10 21:26 83-32-909/07/10 17:306.2 3.5
Acenaphthylene ND ug/L 1 09/08/10 21:26 208-96-809/07/10 17:306.2 3.5
Anthracene ND ug/L 1 09/08/10 21:26 120-12-709/07/10 17:306.2 3.6
Benzo(a)anthracene ND ug/L 1 09/08/10 21:26 56-55-309/07/10 17:306.2 3.5
Benzo(a)pyrene ND ug/L 1 09/08/10 21:26 50-32-809/07/10 17:306.2 3.9
Benzo(b)fluoranthene ND ug/L 1 09/08/10 21:26 205-99-209/07/10 17:306.2 4.5
Benzo(g,h,i)perylene ND ug/L 1 09/08/10 21:26 191-24-209/07/10 17:306.2 3.9
Benzo(k)fluoranthene ND ug/L 1 09/08/10 21:26 207-08-909/07/10 17:306.2 3.8
4-Bromophenylphenyl ether ND ug/L 1 09/08/10 21:26 101-55-309/07/10 17:306.2 3.0
Butylbenzylphthalate ND ug/L 1 09/08/10 21:26 85-68-709/07/10 17:306.2 3.6
4-Chloro-3-methylphenol ND ug/L 1 09/08/10 21:26 59-50-709/07/10 17:306.2 3.5
bis(2-Chloroethoxy)methane ND ug/L 1 09/08/10 21:26 111-91-109/07/10 17:3012.5 7.2
bis(2-Chloroethyl) ether ND ug/L 1 09/08/10 21:26 111-44-409/07/10 17:306.2 6.0
bis(2-Chloroisopropyl) ether ND ug/L 1 09/08/10 21:26 108-60-109/07/10 17:306.2 5.0
2-Chloronaphthalene ND ug/L 1 09/08/10 21:26 91-58-709/07/10 17:306.2 4.5
2-Chlorophenol ND ug/L 1 09/08/10 21:26 95-57-809/07/10 17:306.2 5.5
4-Chlorophenylphenyl ether ND ug/L 1 09/08/10 21:26 7005-72-309/07/10 17:306.2 3.4
Chrysene ND ug/L 1 09/08/10 21:26 218-01-909/07/10 17:306.2 3.4
Dibenz(a,h)anthracene ND ug/L 1 09/08/10 21:26 53-70-309/07/10 17:306.2 3.6
3,3'-Dichlorobenzidine ND ug/L 1 09/08/10 21:26 91-94-109/07/10 17:3031.2 4.2
2,4-Dichlorophenol ND ug/L 1 09/08/10 21:26 120-83-209/07/10 17:306.2 5.1
Diethylphthalate ND ug/L 1 09/08/10 21:26 84-66-209/07/10 17:306.2 3.4
2,4-Dimethylphenol ND ug/L 1 09/08/10 21:26 105-67-909/07/10 17:3012.5 7.0
Dimethylphthalate ND ug/L 1 09/08/10 21:26 131-11-309/07/10 17:306.2 3.0
Di-n-butylphthalate ND ug/L 1 09/08/10 21:26 84-74-209/07/10 17:306.2 3.6
4,6-Dinitro-2-methylphenol ND ug/L 1 09/08/10 21:26 534-52-109/07/10 17:3025.0 9.8
2,4-Dinitrophenol ND ug/L 1 09/08/10 21:26 51-28-509/07/10 17:3062.5 12.5
2,4-Dinitrotoluene ND ug/L 1 09/08/10 21:26 121-14-209/07/10 17:306.2 3.2
2,6-Dinitrotoluene ND ug/L 1 09/08/10 21:26 606-20-209/07/10 17:306.2 3.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 5 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-5 Lab ID:9276754001 Collected:08/31/10 10:30 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 09/08/10 21:26 117-84-009/07/10 17:306.2 3.6
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/08/10 21:26 117-81-709/07/10 17:306.2 2.6
Fluoranthene ND ug/L 1 09/08/10 21:26 206-44-009/07/10 17:306.2 3.6
Fluorene ND ug/L 1 09/08/10 21:26 86-73-709/07/10 17:306.2 3.2
Hexachloro-1,3-butadiene ND ug/L 1 09/08/10 21:26 87-68-309/07/10 17:306.2 4.1
Hexachlorobenzene ND ug/L 1 09/08/10 21:26 118-74-109/07/10 17:306.2 3.2
Hexachlorocyclopentadiene ND ug/L 1 09/08/10 21:26 77-47-409/07/10 17:3012.5 4.6
Hexachloroethane ND ug/L 1 09/08/10 21:26 67-72-109/07/10 17:306.2 4.1
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/08/10 21:26 193-39-509/07/10 17:306.2 3.8
Isophorone ND ug/L 1 09/08/10 21:26 78-59-109/07/10 17:3012.5 8.1
2-Methylnaphthalene ND ug/L 1 09/08/10 21:26 91-57-609/07/10 17:306.2 4.2
Naphthalene ND ug/L 1 09/08/10 21:26 91-20-309/07/10 17:306.2 4.8
Nitrobenzene ND ug/L 1 09/08/10 21:26 98-95-309/07/10 17:306.2 5.5
2-Nitrophenol ND ug/L 1 09/08/10 21:26 88-75-509/07/10 17:306.2 5.8
4-Nitrophenol ND ug/L 1 09/08/10 21:26 100-02-709/07/10 17:3062.5 2.5
N-Nitrosodimethylamine ND ug/L 1 09/08/10 21:26 62-75-909/07/10 17:306.2 3.9
N-Nitroso-di-n-propylamine ND ug/L 1 09/08/10 21:26 621-64-709/07/10 17:306.2 4.6
N-Nitrosodiphenylamine ND ug/L 1 09/08/10 21:26 86-30-609/07/10 17:3012.5 8.2
Pentachlorophenol ND ug/L 1 09/08/10 21:26 87-86-509/07/10 17:3031.2 2.0
Phenanthrene ND ug/L 1 09/08/10 21:26 85-01-809/07/10 17:306.2 3.4
Phenol ND ug/L 1 09/08/10 21:26 108-95-209/07/10 17:306.2 2.2
Pyrene ND ug/L 1 09/08/10 21:26 129-00-009/07/10 17:306.2 3.6
1,2,4-Trichlorobenzene ND ug/L 1 09/08/10 21:26 120-82-109/07/10 17:306.2 4.2
2,4,6-Trichlorophenol ND ug/L 1 09/08/10 21:26 88-06-209/07/10 17:3012.5 7.6
Nitrobenzene-d5 (S)46 %1 09/08/10 21:26 4165-60-009/07/10 17:3010-120
2-Fluorobiphenyl (S)50 %1 09/08/10 21:26 321-60-809/07/10 17:3015-120
Terphenyl-d14 (S)61 %1 09/08/10 21:26 1718-51-009/07/10 17:3011-131
Phenol-d6 (S)19 %1 09/08/10 21:26 13127-88-309/07/10 17:3010-120
2-Fluorophenol (S)28 %1 09/08/10 21:26 367-12-409/07/10 17:3010-120
2,4,6-Tribromophenol (S)59 %1 09/08/10 21:26 118-79-609/07/10 17:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/07/10 20:28 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/07/10 20:28 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/07/10 20:28 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/07/10 20:28 75-27-40.50 0.50
Bromoform ND ug/L 1 09/07/10 20:28 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/07/10 20:28 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/07/10 20:28 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/07/10 20:28 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/07/10 20:28 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/07/10 20:28 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/07/10 20:28 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/07/10 20:28 75-00-31.0 1.0
Chloroform ND ug/L 1 09/07/10 20:28 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/07/10 20:28 74-87-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 6 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-5 Lab ID:9276754001 Collected:08/31/10 10:30 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 09/07/10 20:28 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/07/10 20:28 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/07/10 20:28 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/07/10 20:28 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/07/10 20:28 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/07/10 20:28 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/07/10 20:28 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/07/10 20:28 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/07/10 20:28 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/07/10 20:28 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/07/10 20:28 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/07/10 20:28 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/07/10 20:28 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/07/10 20:28 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/07/10 20:28 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/07/10 20:28 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/07/10 20:28 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/07/10 20:28 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/07/10 20:28 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/07/10 20:28 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/07/10 20:28 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/07/10 20:28 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/07/10 20:28 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/07/10 20:28 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/07/10 20:28 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/07/10 20:28 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/07/10 20:28 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/07/10 20:28 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/07/10 20:28 103-65-10.50 0.50
Styrene ND ug/L 1 09/07/10 20:28 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/07/10 20:28 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/07/10 20:28 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/07/10 20:28 127-18-40.50 0.50
Toluene ND ug/L 1 09/07/10 20:28 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/07/10 20:28 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/07/10 20:28 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/07/10 20:28 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/07/10 20:28 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/07/10 20:28 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/07/10 20:28 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/07/10 20:28 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/07/10 20:28 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/07/10 20:28 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/07/10 20:28 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/07/10 20:28 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/07/10 20:28 95-47-60.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 7 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-5 Lab ID:9276754001 Collected:08/31/10 10:30 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,2-Dichloroethane-d4 (S)107 %1 09/07/10 20:28 17060-07-070-130
Dibromofluoromethane (S)105 %1 09/07/10 20:28 1868-53-770-130
4-Bromofluorobenzene (S)96 %1 09/07/10 20:28 460-00-470-130
Toluene-d8 (S)102 %1 09/07/10 20:28 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 8 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-1 Lab ID:9276754002 Collected:08/31/10 11:30 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)167 ug/L 1 09/08/10 22:5009/03/10 08:00118118
Aliphatic (C19-C36)ND ug/L 1 09/08/10 22:5009/03/10 08:00118118
Aromatic (C11-C22)228 ug/L 1 09/08/10 22:5009/03/10 08:00118118
Nonatriacontane (S)82 %1 09/08/10 22:50 7194-86-709/03/10 08:0040-140
o-Terphenyl (S)72 %1 09/08/10 22:50 84-15-109/03/10 08:0040-140
2-Fluorobiphenyl (S)85 %1 09/08/10 22:50 321-60-809/03/10 08:0040-140
2-Bromonaphthalene (S)96 %1 09/08/10 22:50 580-13-209/03/10 08:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)2820 ug/L 10 09/02/10 18:4810001000
Aliphatic (C09-C12)13400 ug/L 10 09/02/10 18:48 1g10001000
Aromatic (C09-C10)1840 ug/L 10 09/02/10 18:4810001000
2,5-Dibromotoluene (PID)(S)101 %10 09/02/10 18:4870-130
2,5-Dibromotoluene (FID)(S)112 %10 09/02/10 18:4870-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 15.9 ug/L 1 09/08/10 00:52 7439-92-1 B09/02/10 10:355.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/08/10 21:53 83-32-909/07/10 17:305.9 3.3
Acenaphthylene ND ug/L 1 09/08/10 21:53 208-96-809/07/10 17:305.9 3.3
Anthracene ND ug/L 1 09/08/10 21:53 120-12-709/07/10 17:305.9 3.4
Benzo(a)anthracene ND ug/L 1 09/08/10 21:53 56-55-309/07/10 17:305.9 3.3
Benzo(a)pyrene ND ug/L 1 09/08/10 21:53 50-32-809/07/10 17:305.9 3.6
Benzo(b)fluoranthene ND ug/L 1 09/08/10 21:53 205-99-209/07/10 17:305.9 4.2
Benzo(g,h,i)perylene ND ug/L 1 09/08/10 21:53 191-24-209/07/10 17:305.9 3.6
Benzo(k)fluoranthene ND ug/L 1 09/08/10 21:53 207-08-909/07/10 17:305.9 3.5
4-Bromophenylphenyl ether ND ug/L 1 09/08/10 21:53 101-55-309/07/10 17:305.9 2.8
Butylbenzylphthalate ND ug/L 1 09/08/10 21:53 85-68-709/07/10 17:305.9 3.4
4-Chloro-3-methylphenol ND ug/L 1 09/08/10 21:53 59-50-709/07/10 17:305.9 3.3
bis(2-Chloroethoxy)methane ND ug/L 1 09/08/10 21:53 111-91-109/07/10 17:3011.8 6.8
bis(2-Chloroethyl) ether ND ug/L 1 09/08/10 21:53 111-44-409/07/10 17:305.9 5.6
bis(2-Chloroisopropyl) ether ND ug/L 1 09/08/10 21:53 108-60-109/07/10 17:305.9 4.7
2-Chloronaphthalene ND ug/L 1 09/08/10 21:53 91-58-709/07/10 17:305.9 4.2
2-Chlorophenol ND ug/L 1 09/08/10 21:53 95-57-809/07/10 17:305.9 5.2
4-Chlorophenylphenyl ether ND ug/L 1 09/08/10 21:53 7005-72-309/07/10 17:305.9 3.2
Chrysene ND ug/L 1 09/08/10 21:53 218-01-909/07/10 17:305.9 3.2
Dibenz(a,h)anthracene ND ug/L 1 09/08/10 21:53 53-70-309/07/10 17:305.9 3.4
3,3'-Dichlorobenzidine ND ug/L 1 09/08/10 21:53 91-94-109/07/10 17:3029.4 4.0
2,4-Dichlorophenol ND ug/L 1 09/08/10 21:53 120-83-209/07/10 17:305.9 4.8
Diethylphthalate ND ug/L 1 09/08/10 21:53 84-66-209/07/10 17:305.9 3.2
2,4-Dimethylphenol ND ug/L 1 09/08/10 21:53 105-67-909/07/10 17:3011.8 6.6
Dimethylphthalate ND ug/L 1 09/08/10 21:53 131-11-309/07/10 17:305.9 2.8
Di-n-butylphthalate ND ug/L 1 09/08/10 21:53 84-74-209/07/10 17:305.9 3.4
4,6-Dinitro-2-methylphenol ND ug/L 1 09/08/10 21:53 534-52-109/07/10 17:3023.5 9.2
2,4-Dinitrophenol ND ug/L 1 09/08/10 21:53 51-28-509/07/10 17:3058.8 11.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 9 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-1 Lab ID:9276754002 Collected:08/31/10 11:30 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 09/08/10 21:53 121-14-209/07/10 17:305.9 3.1
2,6-Dinitrotoluene ND ug/L 1 09/08/10 21:53 606-20-209/07/10 17:305.9 3.3
Di-n-octylphthalate ND ug/L 1 09/08/10 21:53 117-84-009/07/10 17:305.9 3.4
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/08/10 21:53 117-81-709/07/10 17:305.9 2.5
Fluoranthene ND ug/L 1 09/08/10 21:53 206-44-009/07/10 17:305.9 3.4
Fluorene ND ug/L 1 09/08/10 21:53 86-73-709/07/10 17:305.9 3.1
Hexachloro-1,3-butadiene ND ug/L 1 09/08/10 21:53 87-68-309/07/10 17:305.9 3.9
Hexachlorobenzene ND ug/L 1 09/08/10 21:53 118-74-109/07/10 17:305.9 3.1
Hexachlorocyclopentadiene ND ug/L 1 09/08/10 21:53 77-47-409/07/10 17:3011.8 4.4
Hexachloroethane ND ug/L 1 09/08/10 21:53 67-72-109/07/10 17:305.9 3.9
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/08/10 21:53 193-39-509/07/10 17:305.9 3.5
Isophorone ND ug/L 1 09/08/10 21:53 78-59-109/07/10 17:3011.8 7.6
2-Methylnaphthalene 13.6 ug/L 1 09/08/10 21:53 91-57-609/07/10 17:305.9 4.0
Naphthalene 86.3 ug/L 1 09/08/10 21:53 91-20-309/07/10 17:305.9 4.5
Nitrobenzene ND ug/L 1 09/08/10 21:53 98-95-309/07/10 17:305.9 5.2
2-Nitrophenol ND ug/L 1 09/08/10 21:53 88-75-509/07/10 17:305.9 5.4
4-Nitrophenol ND ug/L 1 09/08/10 21:53 100-02-709/07/10 17:3058.8 2.4
N-Nitrosodimethylamine ND ug/L 1 09/08/10 21:53 62-75-909/07/10 17:305.9 3.6
N-Nitroso-di-n-propylamine ND ug/L 1 09/08/10 21:53 621-64-709/07/10 17:305.9 4.4
N-Nitrosodiphenylamine ND ug/L 1 09/08/10 21:53 86-30-609/07/10 17:3011.8 7.8
Pentachlorophenol ND ug/L 1 09/08/10 21:53 87-86-509/07/10 17:3029.4 1.9
Phenanthrene ND ug/L 1 09/08/10 21:53 85-01-809/07/10 17:305.9 3.2
Phenol ND ug/L 1 09/08/10 21:53 108-95-209/07/10 17:305.9 2.1
Pyrene ND ug/L 1 09/08/10 21:53 129-00-009/07/10 17:305.9 3.4
1,2,4-Trichlorobenzene ND ug/L 1 09/08/10 21:53 120-82-109/07/10 17:305.9 4.0
2,4,6-Trichlorophenol ND ug/L 1 09/08/10 21:53 88-06-209/07/10 17:3011.8 7.2
Nitrobenzene-d5 (S)63 %1 09/08/10 21:53 4165-60-009/07/10 17:3010-120
2-Fluorobiphenyl (S)66 %1 09/08/10 21:53 321-60-809/07/10 17:3015-120
Terphenyl-d14 (S)67 %1 09/08/10 21:53 1718-51-009/07/10 17:3011-131
Phenol-d6 (S)28 %1 09/08/10 21:53 13127-88-309/07/10 17:3010-120
2-Fluorophenol (S)39 %1 09/08/10 21:53 367-12-409/07/10 17:3010-120
2,4,6-Tribromophenol (S)71 %1 09/08/10 21:53 118-79-609/07/10 17:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene 106 ug/L 5 09/08/10 05:37 71-43-22.5 2.5
Bromobenzene ND ug/L 5 09/08/10 05:37 108-86-12.5 2.5
Bromochloromethane ND ug/L 5 09/08/10 05:37 74-97-52.5 2.5
Bromodichloromethane ND ug/L 5 09/08/10 05:37 75-27-42.5 2.5
Bromoform ND ug/L 5 09/08/10 05:37 75-25-22.5 2.5
Bromomethane ND ug/L 5 09/08/10 05:37 74-83-925.0 5.0
n-Butylbenzene ND ug/L 5 09/08/10 05:37 104-51-82.5 2.5
sec-Butylbenzene ND ug/L 5 09/08/10 05:37 135-98-82.5 2.5
tert-Butylbenzene ND ug/L 5 09/08/10 05:37 98-06-62.5 2.5
Carbon tetrachloride ND ug/L 5 09/08/10 05:37 56-23-52.5 2.5
Chlorobenzene ND ug/L 5 09/08/10 05:37 108-90-72.5 2.5
Chloroethane ND ug/L 5 09/08/10 05:37 75-00-35.0 5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 10 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-1 Lab ID:9276754002 Collected:08/31/10 11:30 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 5 09/08/10 05:37 67-66-32.5 2.5
Chloromethane ND ug/L 5 09/08/10 05:37 74-87-35.0 5.0
2-Chlorotoluene ND ug/L 5 09/08/10 05:37 95-49-82.5 2.5
4-Chlorotoluene ND ug/L 5 09/08/10 05:37 106-43-42.5 2.5
1,2-Dibromo-3-chloropropane ND ug/L 5 09/08/10 05:37 96-12-85.0 5.0
Dibromochloromethane ND ug/L 5 09/08/10 05:37 124-48-12.5 2.5
1,2-Dibromoethane (EDB)ND ug/L 5 09/08/10 05:37 106-93-42.5 2.5
Dibromomethane ND ug/L 5 09/08/10 05:37 74-95-32.5 2.5
1,2-Dichlorobenzene ND ug/L 5 09/08/10 05:37 95-50-12.5 2.5
1,3-Dichlorobenzene ND ug/L 5 09/08/10 05:37 541-73-12.5 2.5
1,4-Dichlorobenzene ND ug/L 5 09/08/10 05:37 106-46-72.5 2.5
Dichlorodifluoromethane ND ug/L 5 09/08/10 05:37 75-71-82.5 2.5
1,1-Dichloroethane ND ug/L 5 09/08/10 05:37 75-34-32.5 2.5
1,2-Dichloroethane ND ug/L 5 09/08/10 05:37 107-06-22.5 2.5
1,1-Dichloroethene ND ug/L 5 09/08/10 05:37 75-35-42.5 2.5
cis-1,2-Dichloroethene ND ug/L 5 09/08/10 05:37 156-59-22.5 2.5
trans-1,2-Dichloroethene ND ug/L 5 09/08/10 05:37 156-60-52.5 2.5
1,2-Dichloropropane ND ug/L 5 09/08/10 05:37 78-87-52.5 2.5
1,3-Dichloropropane ND ug/L 5 09/08/10 05:37 142-28-92.5 2.5
2,2-Dichloropropane ND ug/L 5 09/08/10 05:37 594-20-72.5 2.5
1,1-Dichloropropene ND ug/L 5 09/08/10 05:37 563-58-62.5 2.5
cis-1,3-Dichloropropene ND ug/L 5 09/08/10 05:37 10061-01-52.5 2.5
trans-1,3-Dichloropropene ND ug/L 5 09/08/10 05:37 10061-02-62.5 2.5
Diisopropyl ether ND ug/L 5 09/08/10 05:37 108-20-32.5 2.5
Ethylbenzene 519 ug/L 5 09/08/10 05:37 100-41-42.5 2.5
Hexachloro-1,3-butadiene ND ug/L 5 09/08/10 05:37 87-68-310.0 10.0
Isopropylbenzene (Cumene)38.9 ug/L 5 09/08/10 05:37 98-82-82.5 2.5
Methylene Chloride 16.7 ug/L 5 09/08/10 05:37 75-09-210.0 10.0
Methyl-tert-butyl ether ND ug/L 5 09/08/10 05:37 1634-04-42.5 2.5
Naphthalene 250 ug/L 5 09/08/10 05:37 91-20-310.0 10.0
n-Propylbenzene 72.8 ug/L 5 09/08/10 05:37 103-65-12.5 2.5
Styrene 7.5 ug/L 5 09/08/10 05:37 100-42-52.5 2.5
1,1,1,2-Tetrachloroethane ND ug/L 5 09/08/10 05:37 630-20-62.5 2.5
1,1,2,2-Tetrachloroethane ND ug/L 5 09/08/10 05:37 79-34-52.5 2.5
Tetrachloroethene ND ug/L 5 09/08/10 05:37 127-18-42.5 2.5
Toluene 450 ug/L 5 09/08/10 05:37 108-88-32.5 2.5
1,2,3-Trichlorobenzene ND ug/L 5 09/08/10 05:37 87-61-610.0 10.0
1,2,4-Trichlorobenzene ND ug/L 5 09/08/10 05:37 120-82-110.0 10.0
1,1,1-Trichloroethane ND ug/L 5 09/08/10 05:37 71-55-62.5 2.5
1,1,2-Trichloroethane ND ug/L 5 09/08/10 05:37 79-00-52.5 2.5
Trichloroethene ND ug/L 5 09/08/10 05:37 79-01-62.5 2.5
Trichlorofluoromethane ND ug/L 5 09/08/10 05:37 75-69-45.0 5.0
1,2,3-Trichloropropane ND ug/L 5 09/08/10 05:37 96-18-42.5 2.5
1,2,4-Trimethylbenzene 554 ug/L 5 09/08/10 05:37 95-63-62.5 2.5
1,3,5-Trimethylbenzene 192 ug/L 5 09/08/10 05:37 108-67-82.5 2.5
Vinyl chloride ND ug/L 5 09/08/10 05:37 75-01-45.0 5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 11 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-1 Lab ID:9276754002 Collected:08/31/10 11:30 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene 1380 ug/L 5 09/08/10 05:37 179601-23-15.0 5.0
o-Xylene 630 ug/L 5 09/08/10 05:37 95-47-62.5 2.5
1,2-Dichloroethane-d4 (S)99 %5 09/08/10 05:37 17060-07-070-130
Dibromofluoromethane (S)94 %5 09/08/10 05:37 1868-53-770-130
4-Bromofluorobenzene (S)104 %5 09/08/10 05:37 460-00-470-130
Toluene-d8 (S)104 %5 09/08/10 05:37 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 12 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:WSW-2 Lab ID:9276754003 Collected:08/31/10 11:40 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 09/04/10 13:0609/03/10 08:00118118
Aliphatic (C19-C36)ND ug/L 1 09/04/10 13:0609/03/10 08:00118118
Aromatic (C11-C22)ND ug/L 1 09/04/10 13:0609/03/10 08:00118118
Nonatriacontane (S)102 %1 09/04/10 13:06 7194-86-709/03/10 08:0040-140
o-Terphenyl (S)94 %1 09/04/10 13:06 84-15-109/03/10 08:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/02/10 19:14100100
Aliphatic (C09-C12)ND ug/L 1 09/02/10 19:14100100
Aromatic (C09-C10)ND ug/L 1 09/02/10 19:14100100
2,5-Dibromotoluene (PID)(S)98 %1 09/02/10 19:1470-130
2,5-Dibromotoluene (FID)(S)97 %1 09/02/10 19:1470-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 09/08/10 00:55 7439-92-109/02/10 10:355.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/08/10 22:21 83-32-909/07/10 17:305.0 2.8
Acenaphthylene ND ug/L 1 09/08/10 22:21 208-96-809/07/10 17:305.0 2.8
Anthracene ND ug/L 1 09/08/10 22:21 120-12-709/07/10 17:305.0 2.9
Benzo(a)anthracene ND ug/L 1 09/08/10 22:21 56-55-309/07/10 17:305.0 2.8
Benzo(a)pyrene ND ug/L 1 09/08/10 22:21 50-32-809/07/10 17:305.0 3.1
Benzo(b)fluoranthene ND ug/L 1 09/08/10 22:21 205-99-209/07/10 17:305.0 3.6
Benzo(g,h,i)perylene ND ug/L 1 09/08/10 22:21 191-24-209/07/10 17:305.0 3.1
Benzo(k)fluoranthene ND ug/L 1 09/08/10 22:21 207-08-909/07/10 17:305.0 3.0
4-Bromophenylphenyl ether ND ug/L 1 09/08/10 22:21 101-55-309/07/10 17:305.0 2.4
Butylbenzylphthalate ND ug/L 1 09/08/10 22:21 85-68-709/07/10 17:305.0 2.9
4-Chloro-3-methylphenol ND ug/L 1 09/08/10 22:21 59-50-709/07/10 17:305.0 2.8
bis(2-Chloroethoxy)methane ND ug/L 1 09/08/10 22:21 111-91-109/07/10 17:3010.0 5.8
bis(2-Chloroethyl) ether ND ug/L 1 09/08/10 22:21 111-44-409/07/10 17:305.0 4.8
bis(2-Chloroisopropyl) ether ND ug/L 1 09/08/10 22:21 108-60-109/07/10 17:305.0 4.0
2-Chloronaphthalene ND ug/L 1 09/08/10 22:21 91-58-709/07/10 17:305.0 3.6
2-Chlorophenol ND ug/L 1 09/08/10 22:21 95-57-809/07/10 17:305.0 4.4
4-Chlorophenylphenyl ether ND ug/L 1 09/08/10 22:21 7005-72-309/07/10 17:305.0 2.7
Chrysene ND ug/L 1 09/08/10 22:21 218-01-909/07/10 17:305.0 2.7
Dibenz(a,h)anthracene ND ug/L 1 09/08/10 22:21 53-70-309/07/10 17:305.0 2.9
3,3'-Dichlorobenzidine ND ug/L 1 09/08/10 22:21 91-94-109/07/10 17:3025.0 3.4
2,4-Dichlorophenol ND ug/L 1 09/08/10 22:21 120-83-209/07/10 17:305.0 4.1
Diethylphthalate ND ug/L 1 09/08/10 22:21 84-66-209/07/10 17:305.0 2.7
2,4-Dimethylphenol ND ug/L 1 09/08/10 22:21 105-67-909/07/10 17:3010.0 5.6
Dimethylphthalate ND ug/L 1 09/08/10 22:21 131-11-309/07/10 17:305.0 2.4
Di-n-butylphthalate ND ug/L 1 09/08/10 22:21 84-74-209/07/10 17:305.0 2.9
4,6-Dinitro-2-methylphenol ND ug/L 1 09/08/10 22:21 534-52-109/07/10 17:3020.0 7.8
2,4-Dinitrophenol ND ug/L 1 09/08/10 22:21 51-28-509/07/10 17:3050.0 10.0
2,4-Dinitrotoluene ND ug/L 1 09/08/10 22:21 121-14-209/07/10 17:305.0 2.6
2,6-Dinitrotoluene ND ug/L 1 09/08/10 22:21 606-20-209/07/10 17:305.0 2.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 13 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:WSW-2 Lab ID:9276754003 Collected:08/31/10 11:40 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 09/08/10 22:21 117-84-009/07/10 17:305.0 2.9
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/08/10 22:21 117-81-709/07/10 17:305.0 2.1
Fluoranthene ND ug/L 1 09/08/10 22:21 206-44-009/07/10 17:305.0 2.9
Fluorene ND ug/L 1 09/08/10 22:21 86-73-709/07/10 17:305.0 2.6
Hexachloro-1,3-butadiene ND ug/L 1 09/08/10 22:21 87-68-309/07/10 17:305.0 3.3
Hexachlorobenzene ND ug/L 1 09/08/10 22:21 118-74-109/07/10 17:305.0 2.6
Hexachlorocyclopentadiene ND ug/L 1 09/08/10 22:21 77-47-409/07/10 17:3010.0 3.7
Hexachloroethane ND ug/L 1 09/08/10 22:21 67-72-109/07/10 17:305.0 3.3
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/08/10 22:21 193-39-509/07/10 17:305.0 3.0
Isophorone ND ug/L 1 09/08/10 22:21 78-59-109/07/10 17:3010.0 6.5
2-Methylnaphthalene ND ug/L 1 09/08/10 22:21 91-57-609/07/10 17:305.0 3.4
Naphthalene ND ug/L 1 09/08/10 22:21 91-20-309/07/10 17:305.0 3.8
Nitrobenzene ND ug/L 1 09/08/10 22:21 98-95-309/07/10 17:305.0 4.4
2-Nitrophenol ND ug/L 1 09/08/10 22:21 88-75-509/07/10 17:305.0 4.6
4-Nitrophenol ND ug/L 1 09/08/10 22:21 100-02-709/07/10 17:3050.0 2.0
N-Nitrosodimethylamine ND ug/L 1 09/08/10 22:21 62-75-909/07/10 17:305.0 3.1
N-Nitroso-di-n-propylamine ND ug/L 1 09/08/10 22:21 621-64-709/07/10 17:305.0 3.7
N-Nitrosodiphenylamine ND ug/L 1 09/08/10 22:21 86-30-609/07/10 17:3010.0 6.6
Pentachlorophenol ND ug/L 1 09/08/10 22:21 87-86-509/07/10 17:3025.0 1.6
Phenanthrene ND ug/L 1 09/08/10 22:21 85-01-809/07/10 17:305.0 2.7
Phenol ND ug/L 1 09/08/10 22:21 108-95-209/07/10 17:305.0 1.8
Pyrene ND ug/L 1 09/08/10 22:21 129-00-009/07/10 17:305.0 2.9
1,2,4-Trichlorobenzene ND ug/L 1 09/08/10 22:21 120-82-109/07/10 17:305.0 3.4
2,4,6-Trichlorophenol ND ug/L 1 09/08/10 22:21 88-06-209/07/10 17:3010.0 6.1
Nitrobenzene-d5 (S)37 %1 09/08/10 22:21 4165-60-009/07/10 17:3010-120
2-Fluorobiphenyl (S)41 %1 09/08/10 22:21 321-60-809/07/10 17:3015-120
Terphenyl-d14 (S)65 %1 09/08/10 22:21 1718-51-009/07/10 17:3011-131
Phenol-d6 (S)15 %1 09/08/10 22:21 13127-88-309/07/10 17:3010-120
2-Fluorophenol (S)20 %1 09/08/10 22:21 367-12-409/07/10 17:3010-120
2,4,6-Tribromophenol (S)57 %1 09/08/10 22:21 118-79-609/07/10 17:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/07/10 20:51 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/07/10 20:51 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/07/10 20:51 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/07/10 20:51 75-27-40.50 0.50
Bromoform ND ug/L 1 09/07/10 20:51 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/07/10 20:51 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/07/10 20:51 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/07/10 20:51 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/07/10 20:51 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/07/10 20:51 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/07/10 20:51 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/07/10 20:51 75-00-31.0 1.0
Chloroform ND ug/L 1 09/07/10 20:51 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/07/10 20:51 74-87-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 14 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:WSW-2 Lab ID:9276754003 Collected:08/31/10 11:40 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 09/07/10 20:51 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/07/10 20:51 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/07/10 20:51 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/07/10 20:51 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/07/10 20:51 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/07/10 20:51 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/07/10 20:51 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/07/10 20:51 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/07/10 20:51 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/07/10 20:51 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/07/10 20:51 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/07/10 20:51 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/07/10 20:51 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/07/10 20:51 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/07/10 20:51 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/07/10 20:51 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/07/10 20:51 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/07/10 20:51 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/07/10 20:51 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/07/10 20:51 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/07/10 20:51 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/07/10 20:51 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/07/10 20:51 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/07/10 20:51 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/07/10 20:51 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/07/10 20:51 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/07/10 20:51 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/07/10 20:51 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/07/10 20:51 103-65-10.50 0.50
Styrene ND ug/L 1 09/07/10 20:51 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/07/10 20:51 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/07/10 20:51 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/07/10 20:51 127-18-40.50 0.50
Toluene ND ug/L 1 09/07/10 20:51 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/07/10 20:51 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/07/10 20:51 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/07/10 20:51 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/07/10 20:51 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/07/10 20:51 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/07/10 20:51 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/07/10 20:51 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/07/10 20:51 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/07/10 20:51 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/07/10 20:51 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/07/10 20:51 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/07/10 20:51 95-47-60.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 15 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:WSW-2 Lab ID:9276754003 Collected:08/31/10 11:40 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,2-Dichloroethane-d4 (S)105 %1 09/07/10 20:51 17060-07-070-130
Dibromofluoromethane (S)106 %1 09/07/10 20:51 1868-53-770-130
4-Bromofluorobenzene (S)99 %1 09/07/10 20:51 460-00-470-130
Toluene-d8 (S)101 %1 09/07/10 20:51 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 16 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:WSW-3 Lab ID:9276754004 Collected:08/31/10 12:10 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 09/04/10 13:4209/03/10 08:00102102
Aliphatic (C19-C36)ND ug/L 1 09/04/10 13:4209/03/10 08:00102102
Aromatic (C11-C22)ND ug/L 1 09/04/10 13:4209/03/10 08:00102102
Nonatriacontane (S)116 %1 09/04/10 13:42 7194-86-709/03/10 08:0040-140
o-Terphenyl (S)95 %1 09/04/10 13:42 84-15-109/03/10 08:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/02/10 19:39100100
Aliphatic (C09-C12)ND ug/L 1 09/02/10 19:39100100
Aromatic (C09-C10)ND ug/L 1 09/02/10 19:39100100
2,5-Dibromotoluene (PID)(S)90 %1 09/02/10 19:3970-130
2,5-Dibromotoluene (FID)(S)91 %1 09/02/10 19:3970-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 09/08/10 00:59 7439-92-109/02/10 10:355.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/08/10 22:48 83-32-909/07/10 17:305.0 2.8
Acenaphthylene ND ug/L 1 09/08/10 22:48 208-96-809/07/10 17:305.0 2.8
Anthracene ND ug/L 1 09/08/10 22:48 120-12-709/07/10 17:305.0 2.9
Benzo(a)anthracene ND ug/L 1 09/08/10 22:48 56-55-309/07/10 17:305.0 2.8
Benzo(a)pyrene ND ug/L 1 09/08/10 22:48 50-32-809/07/10 17:305.0 3.1
Benzo(b)fluoranthene ND ug/L 1 09/08/10 22:48 205-99-209/07/10 17:305.0 3.6
Benzo(g,h,i)perylene ND ug/L 1 09/08/10 22:48 191-24-209/07/10 17:305.0 3.1
Benzo(k)fluoranthene ND ug/L 1 09/08/10 22:48 207-08-909/07/10 17:305.0 3.0
4-Bromophenylphenyl ether ND ug/L 1 09/08/10 22:48 101-55-309/07/10 17:305.0 2.4
Butylbenzylphthalate ND ug/L 1 09/08/10 22:48 85-68-709/07/10 17:305.0 2.9
4-Chloro-3-methylphenol ND ug/L 1 09/08/10 22:48 59-50-709/07/10 17:305.0 2.8
bis(2-Chloroethoxy)methane ND ug/L 1 09/08/10 22:48 111-91-109/07/10 17:3010.0 5.8
bis(2-Chloroethyl) ether ND ug/L 1 09/08/10 22:48 111-44-409/07/10 17:305.0 4.8
bis(2-Chloroisopropyl) ether ND ug/L 1 09/08/10 22:48 108-60-109/07/10 17:305.0 4.0
2-Chloronaphthalene ND ug/L 1 09/08/10 22:48 91-58-709/07/10 17:305.0 3.6
2-Chlorophenol ND ug/L 1 09/08/10 22:48 95-57-809/07/10 17:305.0 4.4
4-Chlorophenylphenyl ether ND ug/L 1 09/08/10 22:48 7005-72-309/07/10 17:305.0 2.7
Chrysene ND ug/L 1 09/08/10 22:48 218-01-909/07/10 17:305.0 2.7
Dibenz(a,h)anthracene ND ug/L 1 09/08/10 22:48 53-70-309/07/10 17:305.0 2.9
3,3'-Dichlorobenzidine ND ug/L 1 09/08/10 22:48 91-94-109/07/10 17:3025.0 3.4
2,4-Dichlorophenol ND ug/L 1 09/08/10 22:48 120-83-209/07/10 17:305.0 4.1
Diethylphthalate ND ug/L 1 09/08/10 22:48 84-66-209/07/10 17:305.0 2.7
2,4-Dimethylphenol ND ug/L 1 09/08/10 22:48 105-67-909/07/10 17:3010.0 5.6
Dimethylphthalate ND ug/L 1 09/08/10 22:48 131-11-309/07/10 17:305.0 2.4
Di-n-butylphthalate ND ug/L 1 09/08/10 22:48 84-74-209/07/10 17:305.0 2.9
4,6-Dinitro-2-methylphenol ND ug/L 1 09/08/10 22:48 534-52-109/07/10 17:3020.0 7.8
2,4-Dinitrophenol ND ug/L 1 09/08/10 22:48 51-28-509/07/10 17:3050.0 10.0
2,4-Dinitrotoluene ND ug/L 1 09/08/10 22:48 121-14-209/07/10 17:305.0 2.6
2,6-Dinitrotoluene ND ug/L 1 09/08/10 22:48 606-20-209/07/10 17:305.0 2.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 17 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:WSW-3 Lab ID:9276754004 Collected:08/31/10 12:10 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 09/08/10 22:48 117-84-009/07/10 17:305.0 2.9
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/08/10 22:48 117-81-709/07/10 17:305.0 2.1
Fluoranthene ND ug/L 1 09/08/10 22:48 206-44-009/07/10 17:305.0 2.9
Fluorene ND ug/L 1 09/08/10 22:48 86-73-709/07/10 17:305.0 2.6
Hexachloro-1,3-butadiene ND ug/L 1 09/08/10 22:48 87-68-309/07/10 17:305.0 3.3
Hexachlorobenzene ND ug/L 1 09/08/10 22:48 118-74-109/07/10 17:305.0 2.6
Hexachlorocyclopentadiene ND ug/L 1 09/08/10 22:48 77-47-409/07/10 17:3010.0 3.7
Hexachloroethane ND ug/L 1 09/08/10 22:48 67-72-109/07/10 17:305.0 3.3
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/08/10 22:48 193-39-509/07/10 17:305.0 3.0
Isophorone ND ug/L 1 09/08/10 22:48 78-59-109/07/10 17:3010.0 6.5
2-Methylnaphthalene ND ug/L 1 09/08/10 22:48 91-57-609/07/10 17:305.0 3.4
Naphthalene ND ug/L 1 09/08/10 22:48 91-20-309/07/10 17:305.0 3.8
Nitrobenzene ND ug/L 1 09/08/10 22:48 98-95-309/07/10 17:305.0 4.4
2-Nitrophenol ND ug/L 1 09/08/10 22:48 88-75-509/07/10 17:305.0 4.6
4-Nitrophenol ND ug/L 1 09/08/10 22:48 100-02-709/07/10 17:3050.0 2.0
N-Nitrosodimethylamine ND ug/L 1 09/08/10 22:48 62-75-909/07/10 17:305.0 3.1
N-Nitroso-di-n-propylamine ND ug/L 1 09/08/10 22:48 621-64-709/07/10 17:305.0 3.7
N-Nitrosodiphenylamine ND ug/L 1 09/08/10 22:48 86-30-609/07/10 17:3010.0 6.6
Pentachlorophenol ND ug/L 1 09/08/10 22:48 87-86-509/07/10 17:3025.0 1.6
Phenanthrene ND ug/L 1 09/08/10 22:48 85-01-809/07/10 17:305.0 2.7
Phenol ND ug/L 1 09/08/10 22:48 108-95-209/07/10 17:305.0 1.8
Pyrene ND ug/L 1 09/08/10 22:48 129-00-009/07/10 17:305.0 2.9
1,2,4-Trichlorobenzene ND ug/L 1 09/08/10 22:48 120-82-109/07/10 17:305.0 3.4
2,4,6-Trichlorophenol ND ug/L 1 09/08/10 22:48 88-06-209/07/10 17:3010.0 6.1
Nitrobenzene-d5 (S)88 %1 09/08/10 22:48 4165-60-009/07/10 17:3010-120
2-Fluorobiphenyl (S)92 %1 09/08/10 22:48 321-60-809/07/10 17:3015-120
Terphenyl-d14 (S)119 %1 09/08/10 22:48 1718-51-009/07/10 17:3011-131
Phenol-d6 (S)12 %1 09/08/10 22:48 13127-88-309/07/10 17:3010-120
2-Fluorophenol (S)47 %1 09/08/10 22:48 367-12-409/07/10 17:3010-120
2,4,6-Tribromophenol (S)111 %1 09/08/10 22:48 118-79-609/07/10 17:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/08/10 02:34 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/08/10 02:34 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/08/10 02:34 74-97-50.50 0.50
Bromodichloromethane 1.3 ug/L 1 09/08/10 02:34 75-27-4 CC0.50 0.50
Bromoform ND ug/L 1 09/08/10 02:34 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/08/10 02:34 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/08/10 02:34 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/08/10 02:34 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/08/10 02:34 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/08/10 02:34 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/08/10 02:34 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/08/10 02:34 75-00-31.0 1.0
Chloroform 1.3 ug/L 1 09/08/10 02:34 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/08/10 02:34 74-87-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 18 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:WSW-3 Lab ID:9276754004 Collected:08/31/10 12:10 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 09/08/10 02:34 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/08/10 02:34 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/08/10 02:34 96-12-81.0 1.0
Dibromochloromethane 1.4 ug/L 1 09/08/10 02:34 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/08/10 02:34 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/08/10 02:34 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/08/10 02:34 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/08/10 02:34 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/08/10 02:34 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/08/10 02:34 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/08/10 02:34 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/08/10 02:34 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/08/10 02:34 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/08/10 02:34 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/08/10 02:34 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/08/10 02:34 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/08/10 02:34 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/08/10 02:34 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/08/10 02:34 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/08/10 02:34 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/08/10 02:34 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/08/10 02:34 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/08/10 02:34 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/08/10 02:34 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/08/10 02:34 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/08/10 02:34 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/08/10 02:34 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/08/10 02:34 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/08/10 02:34 103-65-10.50 0.50
Styrene ND ug/L 1 09/08/10 02:34 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/08/10 02:34 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/08/10 02:34 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/08/10 02:34 127-18-40.50 0.50
Toluene ND ug/L 1 09/08/10 02:34 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/08/10 02:34 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/08/10 02:34 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/08/10 02:34 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/08/10 02:34 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/08/10 02:34 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/08/10 02:34 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/08/10 02:34 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/08/10 02:34 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/08/10 02:34 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/08/10 02:34 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/08/10 02:34 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/08/10 02:34 95-47-60.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 19 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:WSW-3 Lab ID:9276754004 Collected:08/31/10 12:10 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,2-Dichloroethane-d4 (S)102 %1 09/08/10 02:34 17060-07-070-130
Dibromofluoromethane (S)100 %1 09/08/10 02:34 1868-53-770-130
4-Bromofluorobenzene (S)100 %1 09/08/10 02:34 460-00-470-130
Toluene-d8 (S)100 %1 09/08/10 02:34 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 20 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-3 Lab ID:9276754005 Collected:08/31/10 12:45 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 09/04/10 14:1809/03/10 08:00118118
Aliphatic (C19-C36)ND ug/L 1 09/04/10 14:1809/03/10 08:00118118
Aromatic (C11-C22)ND ug/L 1 09/04/10 14:1809/03/10 08:00118118
Nonatriacontane (S)102 %1 09/04/10 14:18 7194-86-709/03/10 08:0040-140
o-Terphenyl (S)88 %1 09/04/10 14:18 84-15-109/03/10 08:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/02/10 20:04100100
Aliphatic (C09-C12)ND ug/L 1 09/02/10 20:04100100
Aromatic (C09-C10)ND ug/L 1 09/02/10 20:04100100
2,5-Dibromotoluene (PID)(S)90 %1 09/02/10 20:0470-130
2,5-Dibromotoluene (FID)(S)93 %1 09/02/10 20:0470-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 8.2 ug/L 1 09/08/10 01:02 7439-92-1 B09/02/10 10:355.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/08/10 23:15 83-32-909/07/10 17:305.9 3.3
Acenaphthylene ND ug/L 1 09/08/10 23:15 208-96-809/07/10 17:305.9 3.3
Anthracene ND ug/L 1 09/08/10 23:15 120-12-709/07/10 17:305.9 3.4
Benzo(a)anthracene ND ug/L 1 09/08/10 23:15 56-55-309/07/10 17:305.9 3.3
Benzo(a)pyrene ND ug/L 1 09/08/10 23:15 50-32-809/07/10 17:305.9 3.6
Benzo(b)fluoranthene ND ug/L 1 09/08/10 23:15 205-99-209/07/10 17:305.9 4.2
Benzo(g,h,i)perylene ND ug/L 1 09/08/10 23:15 191-24-209/07/10 17:305.9 3.6
Benzo(k)fluoranthene ND ug/L 1 09/08/10 23:15 207-08-909/07/10 17:305.9 3.5
4-Bromophenylphenyl ether ND ug/L 1 09/08/10 23:15 101-55-309/07/10 17:305.9 2.8
Butylbenzylphthalate ND ug/L 1 09/08/10 23:15 85-68-709/07/10 17:305.9 3.4
4-Chloro-3-methylphenol ND ug/L 1 09/08/10 23:15 59-50-709/07/10 17:305.9 3.3
bis(2-Chloroethoxy)methane ND ug/L 1 09/08/10 23:15 111-91-109/07/10 17:3011.8 6.8
bis(2-Chloroethyl) ether ND ug/L 1 09/08/10 23:15 111-44-409/07/10 17:305.9 5.6
bis(2-Chloroisopropyl) ether ND ug/L 1 09/08/10 23:15 108-60-109/07/10 17:305.9 4.7
2-Chloronaphthalene ND ug/L 1 09/08/10 23:15 91-58-709/07/10 17:305.9 4.2
2-Chlorophenol ND ug/L 1 09/08/10 23:15 95-57-809/07/10 17:305.9 5.2
4-Chlorophenylphenyl ether ND ug/L 1 09/08/10 23:15 7005-72-309/07/10 17:305.9 3.2
Chrysene ND ug/L 1 09/08/10 23:15 218-01-909/07/10 17:305.9 3.2
Dibenz(a,h)anthracene ND ug/L 1 09/08/10 23:15 53-70-309/07/10 17:305.9 3.4
3,3'-Dichlorobenzidine ND ug/L 1 09/08/10 23:15 91-94-109/07/10 17:3029.4 4.0
2,4-Dichlorophenol ND ug/L 1 09/08/10 23:15 120-83-209/07/10 17:305.9 4.8
Diethylphthalate ND ug/L 1 09/08/10 23:15 84-66-209/07/10 17:305.9 3.2
2,4-Dimethylphenol ND ug/L 1 09/08/10 23:15 105-67-909/07/10 17:3011.8 6.6
Dimethylphthalate ND ug/L 1 09/08/10 23:15 131-11-309/07/10 17:305.9 2.8
Di-n-butylphthalate ND ug/L 1 09/08/10 23:15 84-74-209/07/10 17:305.9 3.4
4,6-Dinitro-2-methylphenol ND ug/L 1 09/08/10 23:15 534-52-109/07/10 17:3023.5 9.2
2,4-Dinitrophenol ND ug/L 1 09/08/10 23:15 51-28-509/07/10 17:3058.8 11.8
2,4-Dinitrotoluene ND ug/L 1 09/08/10 23:15 121-14-209/07/10 17:305.9 3.1
2,6-Dinitrotoluene ND ug/L 1 09/08/10 23:15 606-20-209/07/10 17:305.9 3.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 21 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-3 Lab ID:9276754005 Collected:08/31/10 12:45 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 09/08/10 23:15 117-84-009/07/10 17:305.9 3.4
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/08/10 23:15 117-81-709/07/10 17:305.9 2.5
Fluoranthene ND ug/L 1 09/08/10 23:15 206-44-009/07/10 17:305.9 3.4
Fluorene ND ug/L 1 09/08/10 23:15 86-73-709/07/10 17:305.9 3.1
Hexachloro-1,3-butadiene ND ug/L 1 09/08/10 23:15 87-68-309/07/10 17:305.9 3.9
Hexachlorobenzene ND ug/L 1 09/08/10 23:15 118-74-109/07/10 17:305.9 3.1
Hexachlorocyclopentadiene ND ug/L 1 09/08/10 23:15 77-47-409/07/10 17:3011.8 4.4
Hexachloroethane ND ug/L 1 09/08/10 23:15 67-72-109/07/10 17:305.9 3.9
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/08/10 23:15 193-39-509/07/10 17:305.9 3.5
Isophorone ND ug/L 1 09/08/10 23:15 78-59-109/07/10 17:3011.8 7.6
2-Methylnaphthalene ND ug/L 1 09/08/10 23:15 91-57-609/07/10 17:305.9 4.0
Naphthalene ND ug/L 1 09/08/10 23:15 91-20-309/07/10 17:305.9 4.5
Nitrobenzene ND ug/L 1 09/08/10 23:15 98-95-309/07/10 17:305.9 5.2
2-Nitrophenol ND ug/L 1 09/08/10 23:15 88-75-509/07/10 17:305.9 5.4
4-Nitrophenol ND ug/L 1 09/08/10 23:15 100-02-709/07/10 17:3058.8 2.4
N-Nitrosodimethylamine ND ug/L 1 09/08/10 23:15 62-75-909/07/10 17:305.9 3.6
N-Nitroso-di-n-propylamine ND ug/L 1 09/08/10 23:15 621-64-709/07/10 17:305.9 4.4
N-Nitrosodiphenylamine ND ug/L 1 09/08/10 23:15 86-30-609/07/10 17:3011.8 7.8
Pentachlorophenol ND ug/L 1 09/08/10 23:15 87-86-509/07/10 17:3029.4 1.9
Phenanthrene ND ug/L 1 09/08/10 23:15 85-01-809/07/10 17:305.9 3.2
Phenol ND ug/L 1 09/08/10 23:15 108-95-209/07/10 17:305.9 2.1
Pyrene ND ug/L 1 09/08/10 23:15 129-00-009/07/10 17:305.9 3.4
1,2,4-Trichlorobenzene ND ug/L 1 09/08/10 23:15 120-82-109/07/10 17:305.9 4.0
2,4,6-Trichlorophenol ND ug/L 1 09/08/10 23:15 88-06-209/07/10 17:3011.8 7.2
Nitrobenzene-d5 (S)26 %1 09/08/10 23:15 4165-60-009/07/10 17:3010-120
2-Fluorobiphenyl (S)28 %1 09/08/10 23:15 321-60-809/07/10 17:3015-120
Terphenyl-d14 (S)51 %1 09/08/10 23:15 1718-51-009/07/10 17:3011-131
Phenol-d6 (S)13 %1 09/08/10 23:15 13127-88-309/07/10 17:3010-120
2-Fluorophenol (S)17 %1 09/08/10 23:15 367-12-409/07/10 17:3010-120
2,4,6-Tribromophenol (S)40 %1 09/08/10 23:15 118-79-609/07/10 17:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/08/10 02:57 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/08/10 02:57 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/08/10 02:57 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/08/10 02:57 75-27-40.50 0.50
Bromoform ND ug/L 1 09/08/10 02:57 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/08/10 02:57 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/08/10 02:57 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/08/10 02:57 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/08/10 02:57 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/08/10 02:57 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/08/10 02:57 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/08/10 02:57 75-00-31.0 1.0
Chloroform 0.82 ug/L 1 09/08/10 02:57 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/08/10 02:57 74-87-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 22 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-3 Lab ID:9276754005 Collected:08/31/10 12:45 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 09/08/10 02:57 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/08/10 02:57 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/08/10 02:57 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/08/10 02:57 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/08/10 02:57 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/08/10 02:57 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/08/10 02:57 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/08/10 02:57 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/08/10 02:57 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/08/10 02:57 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/08/10 02:57 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/08/10 02:57 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/08/10 02:57 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/08/10 02:57 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/08/10 02:57 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/08/10 02:57 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/08/10 02:57 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/08/10 02:57 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/08/10 02:57 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/08/10 02:57 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/08/10 02:57 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/08/10 02:57 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/08/10 02:57 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/08/10 02:57 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/08/10 02:57 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/08/10 02:57 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/08/10 02:57 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/08/10 02:57 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/08/10 02:57 103-65-10.50 0.50
Styrene ND ug/L 1 09/08/10 02:57 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/08/10 02:57 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/08/10 02:57 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/08/10 02:57 127-18-40.50 0.50
Toluene ND ug/L 1 09/08/10 02:57 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/08/10 02:57 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/08/10 02:57 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/08/10 02:57 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/08/10 02:57 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/08/10 02:57 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/08/10 02:57 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/08/10 02:57 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/08/10 02:57 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/08/10 02:57 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/08/10 02:57 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/08/10 02:57 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/08/10 02:57 95-47-60.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 23 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Sample:MW-3 Lab ID:9276754005 Collected:08/31/10 12:45 Received:09/01/10 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,2-Dichloroethane-d4 (S)103 %1 09/08/10 02:57 17060-07-070-130
Dibromofluoromethane (S)100 %1 09/08/10 02:57 1868-53-770-130
4-Bromofluorobenzene (S)94 %1 09/08/10 02:57 460-00-470-130
Toluene-d8 (S)100 %1 09/08/10 02:57 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 24 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/11065
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:9276754001, 9276754002, 9276754003, 9276754004, 9276754005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:492855
Associated Lab Samples:9276754001, 9276754002, 9276754003, 9276754004, 9276754005
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 09/07/10 21:26
Aliphatic (C19-C36)ug/L ND 100 09/07/10 21:26
Aromatic (C11-C22)ug/L ND 100 09/07/10 21:26
2-Bromonaphthalene (S)%97 40-140 09/07/10 21:26
2-Fluorobiphenyl (S)%82 40-140 09/07/10 21:26
Nonatriacontane (S)%70 40-140 09/07/10 21:26
o-Terphenyl (S)%71 40-140 09/07/10 21:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
492856LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
492857
Aliphatic (C09-C18)ug/L 148300 49 40-14061184 21 50
Aliphatic (C19-C36)ug/L 287400 72 40-14079318 10 50
Aromatic (C11-C22)ug/L 622850 73 40-14074633 2 50
2-Bromonaphthalene (S)%102 40-14089
2-Fluorobiphenyl (S)%88 40-14087
Nonatriacontane (S)%82 40-14087
o-Terphenyl (S)%70 40-14067
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 25 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/4302
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:9276754001, 9276754002, 9276754003, 9276754004, 9276754005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:492456
Associated Lab Samples:9276754001, 9276754002, 9276754003, 9276754004, 9276754005
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 100 09/02/10 15:28
Aliphatic (C09-C12)ug/L ND 100 09/02/10 15:28
Aromatic (C09-C10)ug/L ND 100 09/02/10 15:28
2,5-Dibromotoluene (FID)(S)%97 70-130 09/02/10 15:28
2,5-Dibromotoluene (PID)(S)%95 70-130 09/02/10 15:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
492457LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
492458
Aliphatic (C05-C08)ug/L 294300 98 70-13092275 7 25
Aliphatic (C09-C12)ug/L 356300 119 30-130115346 3 25
Aromatic (C09-C10)ug/L 103100 103 70-130100ND 25
2,5-Dibromotoluene (FID)(S)%94 70-13091
2,5-Dibromotoluene (PID)(S)%95 70-13090
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 26 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/6997
SM 3030C
EPA 200.7
200.7 MET 3030C
Associated Lab Samples:9276754001, 9276754002, 9276754003, 9276754004, 9276754005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:492113
Associated Lab Samples:9276754001, 9276754002, 9276754003, 9276754004, 9276754005
Matrix:Water
Analyzed
Lead ug/L 43.9 5.0 B09/08/10 00:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
492114LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 515500 103 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
492115MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9276754001
492116
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 500 90 70-13090 0 20500144594592
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 27 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/11088
EPA 625
EPA 625
625 MSS
Associated Lab Samples:9276754001, 9276754002, 9276754003, 9276754004, 9276754005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:494095
Associated Lab Samples:9276754001, 9276754002, 9276754003, 9276754004, 9276754005
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 09/08/10 19:09
2,4,6-Trichlorophenol ug/L ND 10.0 09/08/10 19:09
2,4-Dichlorophenol ug/L ND 5.0 09/08/10 19:09
2,4-Dimethylphenol ug/L ND 10.0 09/08/10 19:09
2,4-Dinitrophenol ug/L ND 50.0 09/08/10 19:09
2,4-Dinitrotoluene ug/L ND 5.0 09/08/10 19:09
2,6-Dinitrotoluene ug/L ND 5.0 09/08/10 19:09
2-Chloronaphthalene ug/L ND 5.0 09/08/10 19:09
2-Chlorophenol ug/L ND 5.0 09/08/10 19:09
2-Methylnaphthalene ug/L ND 5.0 09/08/10 19:09
2-Nitrophenol ug/L ND 5.0 09/08/10 19:09
3,3'-Dichlorobenzidine ug/L ND 25.0 09/08/10 19:09
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/08/10 19:09
4-Bromophenylphenyl ether ug/L ND 5.0 09/08/10 19:09
4-Chloro-3-methylphenol ug/L ND 5.0 09/08/10 19:09
4-Chlorophenylphenyl ether ug/L ND 5.0 09/08/10 19:09
4-Nitrophenol ug/L ND 50.0 09/08/10 19:09
Acenaphthene ug/L ND 5.0 09/08/10 19:09
Acenaphthylene ug/L ND 5.0 09/08/10 19:09
Anthracene ug/L ND 5.0 09/08/10 19:09
Benzo(a)anthracene ug/L ND 5.0 09/08/10 19:09
Benzo(a)pyrene ug/L ND 5.0 09/08/10 19:09
Benzo(b)fluoranthene ug/L ND 5.0 09/08/10 19:09
Benzo(g,h,i)perylene ug/L ND 5.0 09/08/10 19:09
Benzo(k)fluoranthene ug/L ND 5.0 09/08/10 19:09
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/08/10 19:09
bis(2-Chloroethyl) ether ug/L ND 5.0 09/08/10 19:09
bis(2-Chloroisopropyl) ether ug/L ND 5.0 09/08/10 19:09
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 09/08/10 19:09
Butylbenzylphthalate ug/L ND 5.0 09/08/10 19:09
Chrysene ug/L ND 5.0 09/08/10 19:09
Di-n-butylphthalate ug/L ND 5.0 09/08/10 19:09
Di-n-octylphthalate ug/L ND 5.0 09/08/10 19:09
Dibenz(a,h)anthracene ug/L ND 5.0 09/08/10 19:09
Diethylphthalate ug/L ND 5.0 09/08/10 19:09
Dimethylphthalate ug/L ND 5.0 09/08/10 19:09
Fluoranthene ug/L ND 5.0 09/08/10 19:09
Fluorene ug/L ND 5.0 09/08/10 19:09
Hexachloro-1,3-butadiene ug/L ND 5.0 09/08/10 19:09
Hexachlorobenzene ug/L ND 5.0 09/08/10 19:09
Hexachlorocyclopentadiene ug/L ND 10.0 09/08/10 19:09
Hexachloroethane ug/L ND 5.0 09/08/10 19:09
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 09/08/10 19:09
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 28 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:494095
Associated Lab Samples:9276754001, 9276754002, 9276754003, 9276754004, 9276754005
Matrix:Water
Analyzed
Isophorone ug/L ND 10.0 09/08/10 19:09
N-Nitroso-di-n-propylamine ug/L ND 5.0 09/08/10 19:09
N-Nitrosodimethylamine ug/L ND 5.0 09/08/10 19:09
N-Nitrosodiphenylamine ug/L ND 10.0 09/08/10 19:09
Naphthalene ug/L ND 5.0 09/08/10 19:09
Nitrobenzene ug/L ND 5.0 09/08/10 19:09
Pentachlorophenol ug/L ND 25.0 09/08/10 19:09
Phenanthrene ug/L ND 5.0 09/08/10 19:09
Phenol ug/L ND 5.0 09/08/10 19:09
Pyrene ug/L ND 5.0 09/08/10 19:09
2,4,6-Tribromophenol (S)%74 10-137 09/08/10 19:09
2-Fluorobiphenyl (S)%64 15-120 09/08/10 19:09
2-Fluorophenol (S)%36 10-120 09/08/10 19:09
Nitrobenzene-d5 (S)%60 10-120 09/08/10 19:09
Phenol-d6 (S)%24 10-120 09/08/10 19:09
Terphenyl-d14 (S)%69 11-131 09/08/10 19:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
494096LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 20.6 L2504144-142
2,4,6-Trichlorophenol ug/L 40.650 81 37-144
2,4-Dichlorophenol ug/L 31.950 64 1-191
2,4-Dimethylphenol ug/L 31.950 64 32-119
2,4-Dinitrophenol ug/L 127250 51 1-181
2,4-Dinitrotoluene ug/L 41.350 83 39-139
2,6-Dinitrotoluene ug/L 43.350 87 50-158
2-Chloronaphthalene ug/L 40.150 80 60-118
2-Chlorophenol ug/L 31.950 64 23-134
2-Methylnaphthalene ug/L 26.850 54 25-150
2-Nitrophenol ug/L 29.250 58 29-182
3,3'-Dichlorobenzidine ug/L 69.9100 70 1-262
4,6-Dinitro-2-methylphenol ug/L 81.0100 81 1-181
4-Bromophenylphenyl ether ug/L 38.250 76 53-127
4-Chloro-3-methylphenol ug/L 67.7100 68 22-147
4-Chlorophenylphenyl ether ug/L 39.750 79 25-158
4-Nitrophenol ug/L 88.3250 35 1-132
Acenaphthene ug/L 38.450 77 47-145
Acenaphthylene ug/L 38.550 77 33-145
Anthracene ug/L 39.050 78 1-166
Benzo(a)anthracene ug/L 35.150 70 33-143
Benzo(a)pyrene ug/L 33.950 68 17-163
Benzo(b)fluoranthene ug/L 34.750 69 24-159
Benzo(g,h,i)perylene ug/L 35.950 72 1-219
Benzo(k)fluoranthene ug/L 35.150 70 11-162
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 29 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
494096LABORATORY CONTROL SAMPLE:
LCSSpike
bis(2-Chloroethoxy)methane ug/L 36.450 73 33-184
bis(2-Chloroethyl) ether ug/L 34.950 70 12-158
bis(2-Chloroisopropyl) ether ug/L 32.550 65 36-166
bis(2-Ethylhexyl)phthalate ug/L 35.850 72 8-158
Butylbenzylphthalate ug/L 35.750 71 1-152
Chrysene ug/L 34.150 68 17-168
Di-n-butylphthalate ug/L 40.050 80 1-118
Di-n-octylphthalate ug/L 38.050 76 4-146
Dibenz(a,h)anthracene ug/L 36.950 74 1-227
Diethylphthalate ug/L 41.050 82 1-114
Dimethylphthalate ug/L 39.950 80 1-112
Fluoranthene ug/L 41.250 82 26-137
Fluorene ug/L 40.050 80 59-121
Hexachloro-1,3-butadiene ug/L 16.050 32 24-116
Hexachlorobenzene ug/L 37.350 75 1-152
Hexachlorocyclopentadiene ug/L 27.750 55 25-150
Hexachloroethane ug/L 21.750 43 40-113
Indeno(1,2,3-cd)pyrene ug/L 36.750 73 1-171
Isophorone ug/L 32.750 65 21-196
N-Nitroso-di-n-propylamine ug/L 40.650 81 1-230
N-Nitrosodimethylamine ug/L 21.150 42 25-150
N-Nitrosodiphenylamine ug/L 38.350 77 25-150
Naphthalene ug/L 26.350 53 21-133
Nitrobenzene ug/L 29.850 60 35-180
Pentachlorophenol ug/L 83.0100 83 14-176
Phenanthrene ug/L 38.050 76 54-120
Phenol ug/L 16.050 32 5-112
Pyrene ug/L 35.950 72 52-115
2,4,6-Tribromophenol (S)%82 10-137
2-Fluorobiphenyl (S)%73 15-120
2-Fluorophenol (S)%37 10-120
Nitrobenzene-d5 (S)%56 10-120
Phenol-d6 (S)%27 10-120
Terphenyl-d14 (S)%70 11-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 30 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/12117
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9276754001, 9276754003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:492645
Associated Lab Samples:9276754001, 9276754003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/07/10 14:23
1,1,1-Trichloroethane ug/L ND 0.50 09/07/10 14:23
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/07/10 14:23
1,1,2-Trichloroethane ug/L ND 0.50 09/07/10 14:23
1,1-Dichloroethane ug/L ND 0.50 09/07/10 14:23
1,1-Dichloroethene ug/L ND 0.50 09/07/10 14:23
1,1-Dichloropropene ug/L ND 0.50 09/07/10 14:23
1,2,3-Trichlorobenzene ug/L ND 2.0 09/07/10 14:23
1,2,3-Trichloropropane ug/L ND 0.50 09/07/10 14:23
1,2,4-Trichlorobenzene ug/L ND 2.0 09/07/10 14:23
1,2,4-Trimethylbenzene ug/L ND 0.50 09/07/10 14:23
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/07/10 14:23
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/07/10 14:23
1,2-Dichlorobenzene ug/L ND 0.50 09/07/10 14:23
1,2-Dichloroethane ug/L ND 0.50 09/07/10 14:23
1,2-Dichloropropane ug/L ND 0.50 09/07/10 14:23
1,3,5-Trimethylbenzene ug/L ND 0.50 09/07/10 14:23
1,3-Dichlorobenzene ug/L ND 0.50 09/07/10 14:23
1,3-Dichloropropane ug/L ND 0.50 09/07/10 14:23
1,4-Dichlorobenzene ug/L ND 0.50 09/07/10 14:23
2,2-Dichloropropane ug/L ND 0.50 09/07/10 14:23
2-Chlorotoluene ug/L ND 0.50 09/07/10 14:23
4-Chlorotoluene ug/L ND 0.50 09/07/10 14:23
Benzene ug/L ND 0.50 09/07/10 14:23
Bromobenzene ug/L ND 0.50 09/07/10 14:23
Bromochloromethane ug/L ND 0.50 09/07/10 14:23
Bromodichloromethane ug/L ND 0.50 09/07/10 14:23
Bromoform ug/L ND 0.50 09/07/10 14:23
Bromomethane ug/L ND 5.0 09/07/10 14:23
Carbon tetrachloride ug/L ND 0.50 09/07/10 14:23
Chlorobenzene ug/L ND 0.50 09/07/10 14:23
Chloroethane ug/L ND 1.0 09/07/10 14:23
Chloroform ug/L ND 0.50 09/07/10 14:23
Chloromethane ug/L ND 1.0 09/07/10 14:23
cis-1,2-Dichloroethene ug/L ND 0.50 09/07/10 14:23
cis-1,3-Dichloropropene ug/L ND 0.50 09/07/10 14:23
Dibromochloromethane ug/L ND 0.50 09/07/10 14:23
Dibromomethane ug/L ND 0.50 09/07/10 14:23
Dichlorodifluoromethane ug/L ND 0.50 09/07/10 14:23
Diisopropyl ether ug/L ND 0.50 09/07/10 14:23
Ethylbenzene ug/L ND 0.50 09/07/10 14:23
Hexachloro-1,3-butadiene ug/L ND 2.0 09/07/10 14:23
Isopropylbenzene (Cumene)ug/L ND 0.50 09/07/10 14:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 31 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:492645
Associated Lab Samples:9276754001, 9276754003
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 09/07/10 14:23
Methyl-tert-butyl ether ug/L ND 0.50 09/07/10 14:23
Methylene Chloride ug/L ND 2.0 09/07/10 14:23
n-Butylbenzene ug/L ND 0.50 09/07/10 14:23
n-Propylbenzene ug/L ND 0.50 09/07/10 14:23
Naphthalene ug/L ND 2.0 09/07/10 14:23
o-Xylene ug/L ND 0.50 09/07/10 14:23
sec-Butylbenzene ug/L ND 0.50 09/07/10 14:23
Styrene ug/L ND 0.50 09/07/10 14:23
tert-Butylbenzene ug/L ND 0.50 09/07/10 14:23
Tetrachloroethene ug/L ND 0.50 09/07/10 14:23
Toluene ug/L ND 0.50 09/07/10 14:23
trans-1,2-Dichloroethene ug/L ND 0.50 09/07/10 14:23
trans-1,3-Dichloropropene ug/L ND 0.50 09/07/10 14:23
Trichloroethene ug/L ND 0.50 09/07/10 14:23
Trichlorofluoromethane ug/L ND 1.0 09/07/10 14:23
Vinyl chloride ug/L ND 1.0 09/07/10 14:23
1,2-Dichloroethane-d4 (S)%102 70-130 09/07/10 14:23
4-Bromofluorobenzene (S)%99 70-130 09/07/10 14:23
Dibromofluoromethane (S)%105 70-130 09/07/10 14:23
Toluene-d8 (S)%99 70-130 09/07/10 14:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
492646LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.850 104 60-140
1,1,1-Trichloroethane ug/L 49.650 99 60-140
1,1,2,2-Tetrachloroethane ug/L 46.450 93 60-140
1,1,2-Trichloroethane ug/L 48.750 97 60-140
1,1-Dichloroethane ug/L 50.250 100 60-140
1,1-Dichloroethene ug/L 50.350 101 60-140
1,1-Dichloropropene ug/L 44.950 90 60-140
1,2,3-Trichlorobenzene ug/L 49.350 99 60-140
1,2,3-Trichloropropane ug/L 45.350 91 60-140
1,2,4-Trichlorobenzene ug/L 49.850 100 60-140
1,2,4-Trimethylbenzene ug/L 51.250 102 60-140
1,2-Dibromo-3-chloropropane ug/L 47.450 95 60-140
1,2-Dibromoethane (EDB)ug/L 47.150 94 60-140
1,2-Dichlorobenzene ug/L 49.150 98 60-140
1,2-Dichloroethane ug/L 48.250 96 60-140
1,2-Dichloropropane ug/L 46.950 94 60-140
1,3,5-Trimethylbenzene ug/L 51.150 102 60-140
1,3-Dichlorobenzene ug/L 49.350 99 60-140
1,3-Dichloropropane ug/L 47.050 94 60-140
1,4-Dichlorobenzene ug/L 46.550 93 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 32 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
492646LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 48.650 97 60-140
2-Chlorotoluene ug/L 49.250 98 60-140
4-Chlorotoluene ug/L 51.650 103 60-140
Benzene ug/L 49.550 99 60-140
Bromobenzene ug/L 47.950 96 60-140
Bromochloromethane ug/L 47.350 95 60-140
Bromodichloromethane ug/L 49.950 100 60-140
Bromoform ug/L 49.250 98 60-140
Bromomethane ug/L 50.950 102 60-140
Carbon tetrachloride ug/L 48.250 96 60-140
Chlorobenzene ug/L 47.550 95 60-140
Chloroethane ug/L 49.150 98 60-140
Chloroform ug/L 46.950 94 60-140
Chloromethane ug/L 51.250 102 60-140
cis-1,2-Dichloroethene ug/L 49.350 99 60-140
cis-1,3-Dichloropropene ug/L 49.650 99 60-140
Dibromochloromethane ug/L 48.250 96 60-140
Dibromomethane ug/L 49.750 99 60-140
Dichlorodifluoromethane ug/L 49.250 98 60-140
Diisopropyl ether ug/L 49.250 98 60-140
Ethylbenzene ug/L 49.950 100 60-140
Hexachloro-1,3-butadiene ug/L 46.150 92 60-140
Isopropylbenzene (Cumene)ug/L 55.350 111 60-140
m&p-Xylene ug/L 106100 106 60-140
Methyl-tert-butyl ether ug/L 46.450 93 60-140
Methylene Chloride ug/L 50.550 101 60-140
n-Butylbenzene ug/L 51.350 103 60-140
n-Propylbenzene ug/L 52.250 104 60-140
Naphthalene ug/L 52.550 105 60-140
o-Xylene ug/L 55.950 112 60-140
sec-Butylbenzene ug/L 53.250 106 60-140
Styrene ug/L 53.450 107 60-140
tert-Butylbenzene ug/L 53.950 108 60-140
Tetrachloroethene ug/L 49.750 99 60-140
Toluene ug/L 56.350 113 60-140
trans-1,2-Dichloroethene ug/L 48.650 97 60-140
trans-1,3-Dichloropropene ug/L 49.650 99 60-140
Trichloroethene ug/L 51.250 102 60-140
Trichlorofluoromethane ug/L 50.350 101 60-140
Vinyl chloride ug/L 52.450 105 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Dibromofluoromethane (S)%101 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 33 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
493731MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9276637005
493732
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 104 60-14086 20 3020ND20.8 17.1
1,1,1-Trichloroethane ug/L 20 112 60-14093 18 3020ND22.3 18.6
1,1,2,2-Tetrachloroethane ug/L 20 108 60-14091 17 3020ND21.6 18.1
1,1,2-Trichloroethane ug/L 20 111 60-14089 21 3020ND22.1 17.9
1,1-Dichloroethane ug/L 20 122 60-140102 18 3020ND24.5 20.5
1,1-Dichloroethene ug/L 20 124 60-140110 12 3020ND24.8 22.0
1,1-Dichloropropene ug/L 20 96 60-14085 13 3020ND19.3 16.9
1,2,3-Trichlorobenzene ug/L 20 94 60-14079 17 3020ND18.8 15.8
1,2,3-Trichloropropane ug/L 20 102 60-14080 23 3020ND20.3 16.1
1,2,4-Trichlorobenzene ug/L 20 90 60-14077 15 3020ND18.0 15.5
1,2,4-Trimethylbenzene ug/L 20 112 60-14093 18 3020ND22.3 18.6
1,2-Dibromo-3-chloropropane ug/L 20 96 60-14086 11 3020ND19.2 17.3
1,2-Dibromoethane (EDB)ug/L 20 103 60-14088 16 3020ND20.6 17.5
1,2-Dichlorobenzene ug/L 20 105 60-14088 18 3020ND21.0 17.5
1,2-Dichloroethane ug/L 20 107 60-14089 18 3020ND21.4 17.8
1,2-Dichloropropane ug/L 20 108 60-14086 22 3020ND21.6 17.3
1,3,5-Trimethylbenzene ug/L 20 108 60-14092 16 3020ND21.6 18.4
1,3-Dichlorobenzene ug/L 20 103 60-14089 15 3020ND20.6 17.7
1,3-Dichloropropane ug/L 20 106 60-14084 23 3020ND21.3 16.9
1,4-Dichlorobenzene ug/L 20 99 60-14084 16 3020ND19.7 16.9
2,2-Dichloropropane ug/L 20 106 60-14093 14 3020ND21.3 18.5
2-Chlorotoluene ug/L 20 105 60-14092 13 3020ND21.0 18.4
4-Chlorotoluene ug/L 20 110 60-14094 15 3020ND22.0 18.9
Benzene ug/L 20 112 60-14094 18 3020ND22.4 18.7
Bromobenzene ug/L 20 105 60-14090 15 3020ND21.0 18.0
Bromochloromethane ug/L M0,R12014960-140109 31 3020ND29.8 21.7
Bromodichloromethane ug/L 20 105 60-14085 20 3020ND20.9 17.0
Bromoform ug/L 20 94 60-14078 19 3020ND18.9 15.6
Bromomethane ug/L 20 116 60-140103 12 3020ND23.2 20.5
Carbon tetrachloride ug/L 20 114 60-14094 19 3020ND22.7 18.7
Chlorobenzene ug/L M02010660-14087 20 3020ND21.1 17.3
Chloroethane ug/L 20 141 60-140120 16 3020ND28.2 23.9
Chloroform ug/L 20 105 60-14090 15 3020ND21.0 18.1
Chloromethane ug/L 20 113 60-140104 9 3020ND22.7 20.8
cis-1,2-Dichloroethene ug/L 20 125 60-140109 14 3020ND24.9 21.8
cis-1,3-Dichloropropene ug/L 20 92 60-14075 20 3020ND18.4 15.0
Dibromochloromethane ug/L 20 95 60-14078 19 3020ND19.0 15.6
Dibromomethane ug/L 20 103 60-14086 18 3020ND20.6 17.1
Dichlorodifluoromethane ug/L 20 100 60-14087 13 3020ND19.9 17.4
Diisopropyl ether ug/L 20 118 60-140101 16 3020ND23.6 20.1
Ethylbenzene ug/L 20 107 60-14091 16 3020ND21.4 18.1
Hexachloro-1,3-butadiene ug/L 20 93 60-14084 10 3020ND18.6 16.8
Isopropylbenzene (Cumene)ug/L 20 114 60-14096 17 3020ND22.8 19.3
m&p-Xylene ug/L 40 111 60-14094 17 3040ND44.4 37.6
Methyl-tert-butyl ether ug/L 20 104 60-14088 16 3020ND20.7 17.6
Methylene Chloride ug/L 20 127 60-140104 15 30207.0 32.4 27.9
n-Butylbenzene ug/L 20 109 60-14092 17 3020ND21.9 18.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 34 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
493731MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9276637005
493732
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 114 60-14099 14 3020ND22.9 19.8
Naphthalene ug/L 20 102 60-14083 21 3020ND20.3 16.6
o-Xylene ug/L 20 115 60-14092 22 3020ND23.1 18.5
sec-Butylbenzene ug/L 20 114 60-14097 16 3020ND22.8 19.5
Styrene ug/L 20 113 60-14094 19 3020ND22.7 18.7
tert-Butylbenzene ug/L 20 114 60-14097 17 3020ND22.9 19.3
Tetrachloroethene ug/L 20 100 60-14084 17 3020ND19.9 16.8
Toluene ug/L 20 106 60-14090 17 3020ND21.3 18.0
trans-1,2-Dichloroethene ug/L 20 114 60-140101 12 3020ND22.8 20.2
trans-1,3-Dichloropropene ug/L 20 96 60-14076 24 3020ND19.3 15.2
Trichloroethene ug/L 20 108 60-14091 16 3020ND21.5 18.3
Trichlorofluoromethane ug/L 20 122 60-140107 13 3020ND24.4 21.4
Vinyl chloride ug/L 20 119 60-140104 13 3020ND23.8 20.8
1,2-Dichloroethane-d4 (S)%98 70-13098
4-Bromofluorobenzene (S)%99 70-13098
Dibromofluoromethane (S)%99 70-130101
Toluene-d8 (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 35 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/12143
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9276754002, 9276754004, 9276754005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:493785
Associated Lab Samples:9276754002, 9276754004, 9276754005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/08/10 01:48
1,1,1-Trichloroethane ug/L ND 0.50 09/08/10 01:48
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/08/10 01:48
1,1,2-Trichloroethane ug/L ND 0.50 09/08/10 01:48
1,1-Dichloroethane ug/L ND 0.50 09/08/10 01:48
1,1-Dichloroethene ug/L ND 0.50 09/08/10 01:48
1,1-Dichloropropene ug/L ND 0.50 09/08/10 01:48
1,2,3-Trichlorobenzene ug/L ND 2.0 09/08/10 01:48
1,2,3-Trichloropropane ug/L ND 0.50 09/08/10 01:48
1,2,4-Trichlorobenzene ug/L ND 2.0 09/08/10 01:48
1,2,4-Trimethylbenzene ug/L ND 0.50 09/08/10 01:48
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/08/10 01:48
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/08/10 01:48
1,2-Dichlorobenzene ug/L ND 0.50 09/08/10 01:48
1,2-Dichloroethane ug/L ND 0.50 09/08/10 01:48
1,2-Dichloropropane ug/L ND 0.50 09/08/10 01:48
1,3,5-Trimethylbenzene ug/L ND 0.50 09/08/10 01:48
1,3-Dichlorobenzene ug/L ND 0.50 09/08/10 01:48
1,3-Dichloropropane ug/L ND 0.50 09/08/10 01:48
1,4-Dichlorobenzene ug/L ND 0.50 09/08/10 01:48
2,2-Dichloropropane ug/L ND 0.50 09/08/10 01:48
2-Chlorotoluene ug/L ND 0.50 09/08/10 01:48
4-Chlorotoluene ug/L ND 0.50 09/08/10 01:48
Benzene ug/L ND 0.50 09/08/10 01:48
Bromobenzene ug/L ND 0.50 09/08/10 01:48
Bromochloromethane ug/L ND 0.50 09/08/10 01:48
Bromodichloromethane ug/L ND 0.50 09/08/10 01:48
Bromoform ug/L ND 0.50 09/08/10 01:48
Bromomethane ug/L ND 5.0 09/08/10 01:48
Carbon tetrachloride ug/L ND 0.50 09/08/10 01:48
Chlorobenzene ug/L ND 0.50 09/08/10 01:48
Chloroethane ug/L ND 1.0 09/08/10 01:48
Chloroform ug/L ND 0.50 09/08/10 01:48
Chloromethane ug/L ND 1.0 09/08/10 01:48
cis-1,2-Dichloroethene ug/L ND 0.50 09/08/10 01:48
cis-1,3-Dichloropropene ug/L ND 0.50 09/08/10 01:48
Dibromochloromethane ug/L ND 0.50 09/08/10 01:48
Dibromomethane ug/L ND 0.50 09/08/10 01:48
Dichlorodifluoromethane ug/L ND 0.50 09/08/10 01:48
Diisopropyl ether ug/L ND 0.50 09/08/10 01:48
Ethylbenzene ug/L ND 0.50 09/08/10 01:48
Hexachloro-1,3-butadiene ug/L ND 2.0 09/08/10 01:48
Isopropylbenzene (Cumene)ug/L ND 0.50 09/08/10 01:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 36 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:493785
Associated Lab Samples:9276754002, 9276754004, 9276754005
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 09/08/10 01:48
Methyl-tert-butyl ether ug/L ND 0.50 09/08/10 01:48
Methylene Chloride ug/L ND 2.0 09/08/10 01:48
n-Butylbenzene ug/L ND 0.50 09/08/10 01:48
n-Propylbenzene ug/L ND 0.50 09/08/10 01:48
Naphthalene ug/L ND 2.0 09/08/10 01:48
o-Xylene ug/L ND 0.50 09/08/10 01:48
sec-Butylbenzene ug/L ND 0.50 09/08/10 01:48
Styrene ug/L ND 0.50 09/08/10 01:48
tert-Butylbenzene ug/L ND 0.50 09/08/10 01:48
Tetrachloroethene ug/L ND 0.50 09/08/10 01:48
Toluene ug/L ND 0.50 09/08/10 01:48
trans-1,2-Dichloroethene ug/L ND 0.50 09/08/10 01:48
trans-1,3-Dichloropropene ug/L ND 0.50 09/08/10 01:48
Trichloroethene ug/L ND 0.50 09/08/10 01:48
Trichlorofluoromethane ug/L ND 1.0 09/08/10 01:48
Vinyl chloride ug/L ND 1.0 09/08/10 01:48
1,2-Dichloroethane-d4 (S)%103 70-130 09/08/10 01:48
4-Bromofluorobenzene (S)%96 70-130 09/08/10 01:48
Dibromofluoromethane (S)%100 70-130 09/08/10 01:48
Toluene-d8 (S)%102 70-130 09/08/10 01:48
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:494529
Associated Lab Samples:9276754002, 9276754004, 9276754005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/08/10 14:00
1,1,1-Trichloroethane ug/L ND 0.50 09/08/10 14:00
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/08/10 14:00
1,1,2-Trichloroethane ug/L ND 0.50 09/08/10 14:00
1,1-Dichloroethane ug/L ND 0.50 09/08/10 14:00
1,1-Dichloroethene ug/L ND 0.50 09/08/10 14:00
1,1-Dichloropropene ug/L ND 0.50 09/08/10 14:00
1,2,3-Trichlorobenzene ug/L ND 2.0 09/08/10 14:00
1,2,3-Trichloropropane ug/L ND 0.50 09/08/10 14:00
1,2,4-Trichlorobenzene ug/L ND 2.0 09/08/10 14:00
1,2,4-Trimethylbenzene ug/L ND 0.50 09/08/10 14:00
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/08/10 14:00
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/08/10 14:00
1,2-Dichlorobenzene ug/L ND 0.50 09/08/10 14:00
1,2-Dichloroethane ug/L ND 0.50 09/08/10 14:00
1,2-Dichloropropane ug/L ND 0.50 09/08/10 14:00
1,3,5-Trimethylbenzene ug/L ND 0.50 09/08/10 14:00
1,3-Dichlorobenzene ug/L ND 0.50 09/08/10 14:00
1,3-Dichloropropane ug/L ND 0.50 09/08/10 14:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 37 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:494529
Associated Lab Samples:9276754002, 9276754004, 9276754005
Matrix:Water
Analyzed
1,4-Dichlorobenzene ug/L ND 0.50 09/08/10 14:00
2,2-Dichloropropane ug/L ND 0.50 09/08/10 14:00
2-Chlorotoluene ug/L ND 0.50 09/08/10 14:00
4-Chlorotoluene ug/L ND 0.50 09/08/10 14:00
Benzene ug/L ND 0.50 09/08/10 14:00
Bromobenzene ug/L ND 0.50 09/08/10 14:00
Bromochloromethane ug/L ND 0.50 09/08/10 14:00
Bromodichloromethane ug/L ND 0.50 09/08/10 14:00
Bromoform ug/L ND 0.50 09/08/10 14:00
Bromomethane ug/L ND 5.0 09/08/10 14:00
Carbon tetrachloride ug/L ND 0.50 09/08/10 14:00
Chlorobenzene ug/L ND 0.50 09/08/10 14:00
Chloroethane ug/L ND 1.0 09/08/10 14:00
Chloroform ug/L ND 0.50 09/08/10 14:00
Chloromethane ug/L ND 1.0 09/08/10 14:00
cis-1,2-Dichloroethene ug/L ND 0.50 09/08/10 14:00
cis-1,3-Dichloropropene ug/L ND 0.50 09/08/10 14:00
Dibromochloromethane ug/L ND 0.50 09/08/10 14:00
Dibromomethane ug/L ND 0.50 09/08/10 14:00
Dichlorodifluoromethane ug/L ND 0.50 09/08/10 14:00
Diisopropyl ether ug/L ND 0.50 09/08/10 14:00
Ethylbenzene ug/L ND 0.50 09/08/10 14:00
Hexachloro-1,3-butadiene ug/L ND 2.0 09/08/10 14:00
Isopropylbenzene (Cumene)ug/L ND 0.50 09/08/10 14:00
m&p-Xylene ug/L ND 1.0 09/08/10 14:00
Methyl-tert-butyl ether ug/L ND 0.50 09/08/10 14:00
Methylene Chloride ug/L ND 2.0 09/08/10 14:00
n-Butylbenzene ug/L ND 0.50 09/08/10 14:00
n-Propylbenzene ug/L ND 0.50 09/08/10 14:00
Naphthalene ug/L ND 2.0 09/08/10 14:00
o-Xylene ug/L ND 0.50 09/08/10 14:00
sec-Butylbenzene ug/L ND 0.50 09/08/10 14:00
Styrene ug/L ND 0.50 09/08/10 14:00
tert-Butylbenzene ug/L ND 0.50 09/08/10 14:00
Tetrachloroethene ug/L ND 0.50 09/08/10 14:00
Toluene ug/L ND 0.50 09/08/10 14:00
trans-1,2-Dichloroethene ug/L ND 0.50 09/08/10 14:00
trans-1,3-Dichloropropene ug/L ND 0.50 09/08/10 14:00
Trichloroethene ug/L ND 0.50 09/08/10 14:00
Trichlorofluoromethane ug/L ND 1.0 09/08/10 14:00
Vinyl chloride ug/L ND 1.0 09/08/10 14:00
1,2-Dichloroethane-d4 (S)%102 70-130 09/08/10 14:00
4-Bromofluorobenzene (S)%96 70-130 09/08/10 14:00
Dibromofluoromethane (S)%106 70-130 09/08/10 14:00
Toluene-d8 (S)%102 70-130 09/08/10 14:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 38 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:495525
Associated Lab Samples:9276754002, 9276754004, 9276754005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/09/10 14:23
1,1,1-Trichloroethane ug/L ND 0.50 09/09/10 14:23
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/09/10 14:23
1,1,2-Trichloroethane ug/L ND 0.50 09/09/10 14:23
1,1-Dichloroethane ug/L ND 0.50 09/09/10 14:23
1,1-Dichloroethene ug/L ND 0.50 09/09/10 14:23
1,1-Dichloropropene ug/L ND 0.50 09/09/10 14:23
1,2,3-Trichlorobenzene ug/L ND 2.0 09/09/10 14:23
1,2,3-Trichloropropane ug/L ND 0.50 09/09/10 14:23
1,2,4-Trichlorobenzene ug/L ND 2.0 09/09/10 14:23
1,2,4-Trimethylbenzene ug/L ND 0.50 09/09/10 14:23
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/09/10 14:23
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/09/10 14:23
1,2-Dichlorobenzene ug/L ND 0.50 09/09/10 14:23
1,2-Dichloroethane ug/L ND 0.50 09/09/10 14:23
1,2-Dichloropropane ug/L ND 0.50 09/09/10 14:23
1,3,5-Trimethylbenzene ug/L ND 0.50 09/09/10 14:23
1,3-Dichlorobenzene ug/L ND 0.50 09/09/10 14:23
1,3-Dichloropropane ug/L ND 0.50 09/09/10 14:23
1,4-Dichlorobenzene ug/L ND 0.50 09/09/10 14:23
2,2-Dichloropropane ug/L ND 0.50 09/09/10 14:23
2-Chlorotoluene ug/L ND 0.50 09/09/10 14:23
4-Chlorotoluene ug/L ND 0.50 09/09/10 14:23
Benzene ug/L ND 0.50 09/09/10 14:23
Bromobenzene ug/L ND 0.50 09/09/10 14:23
Bromochloromethane ug/L ND 0.50 09/09/10 14:23
Bromodichloromethane ug/L ND 0.50 09/09/10 14:23
Bromoform ug/L ND 0.50 09/09/10 14:23
Bromomethane ug/L ND 5.0 09/09/10 14:23
Carbon tetrachloride ug/L ND 0.50 09/09/10 14:23
Chlorobenzene ug/L ND 0.50 09/09/10 14:23
Chloroethane ug/L ND 1.0 09/09/10 14:23
Chloroform ug/L ND 0.50 09/09/10 14:23
Chloromethane ug/L ND 1.0 09/09/10 14:23
cis-1,2-Dichloroethene ug/L ND 0.50 09/09/10 14:23
cis-1,3-Dichloropropene ug/L ND 0.50 09/09/10 14:23
Dibromochloromethane ug/L ND 0.50 09/09/10 14:23
Dibromomethane ug/L ND 0.50 09/09/10 14:23
Dichlorodifluoromethane ug/L ND 0.50 09/09/10 14:23
Diisopropyl ether ug/L ND 0.50 09/09/10 14:23
Ethylbenzene ug/L ND 0.50 09/09/10 14:23
Hexachloro-1,3-butadiene ug/L ND 2.0 09/09/10 14:23
Isopropylbenzene (Cumene)ug/L ND 0.50 09/09/10 14:23
m&p-Xylene ug/L ND 1.0 09/09/10 14:23
Methyl-tert-butyl ether ug/L ND 0.50 09/09/10 14:23
Methylene Chloride ug/L ND 2.0 09/09/10 14:23
n-Butylbenzene ug/L ND 0.50 09/09/10 14:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 39 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:495525
Associated Lab Samples:9276754002, 9276754004, 9276754005
Matrix:Water
Analyzed
n-Propylbenzene ug/L ND 0.50 09/09/10 14:23
Naphthalene ug/L ND 2.0 09/09/10 14:23
o-Xylene ug/L ND 0.50 09/09/10 14:23
sec-Butylbenzene ug/L ND 0.50 09/09/10 14:23
Styrene ug/L ND 0.50 09/09/10 14:23
tert-Butylbenzene ug/L ND 0.50 09/09/10 14:23
Tetrachloroethene ug/L ND 0.50 09/09/10 14:23
Toluene ug/L ND 0.50 09/09/10 14:23
trans-1,2-Dichloroethene ug/L ND 0.50 09/09/10 14:23
trans-1,3-Dichloropropene ug/L ND 0.50 09/09/10 14:23
Trichloroethene ug/L ND 0.50 09/09/10 14:23
Trichlorofluoromethane ug/L ND 1.0 09/09/10 14:23
Vinyl chloride ug/L ND 1.0 09/09/10 14:23
1,2-Dichloroethane-d4 (S)%99 70-130 09/09/10 14:23
4-Bromofluorobenzene (S)%99 70-130 09/09/10 14:23
Dibromofluoromethane (S)%105 70-130 09/09/10 14:23
Toluene-d8 (S)%99 70-130 09/09/10 14:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
493786LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.050 96 60-140
1,1,1-Trichloroethane ug/L 44.250 88 60-140
1,1,2,2-Tetrachloroethane ug/L 48.250 96 60-140
1,1,2-Trichloroethane ug/L 49.450 99 60-140
1,1-Dichloroethane ug/L 53.850 108 60-140
1,1-Dichloroethene ug/L 51.950 104 60-140
1,1-Dichloropropene ug/L 41.950 84 60-140
1,2,3-Trichlorobenzene ug/L 46.450 93 60-140
1,2,3-Trichloropropane ug/L 46.650 93 60-140
1,2,4-Trichlorobenzene ug/L 46.550 93 60-140
1,2,4-Trimethylbenzene ug/L 63.350 127 60-140
1,2-Dibromo-3-chloropropane ug/L 44.950 90 60-140
1,2-Dibromoethane (EDB)ug/L 46.350 93 60-140
1,2-Dichlorobenzene ug/L 47.450 95 60-140
1,2-Dichloroethane ug/L 46.950 94 60-140
1,2-Dichloropropane ug/L 46.750 93 60-140
1,3,5-Trimethylbenzene ug/L 49.650 99 60-140
1,3-Dichlorobenzene ug/L 47.150 94 60-140
1,3-Dichloropropane ug/L 46.350 93 60-140
1,4-Dichlorobenzene ug/L 45.450 91 60-140
2,2-Dichloropropane ug/L 49.150 98 60-140
2-Chlorotoluene ug/L 47.750 95 60-140
4-Chlorotoluene ug/L 49.550 99 60-140
Benzene ug/L 48.250 96 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 40 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
493786LABORATORY CONTROL SAMPLE:
LCSSpike
Bromobenzene ug/L 46.350 93 60-140
Bromochloromethane ug/L 45.750 91 60-140
Bromodichloromethane ug/L 47.450 95 60-140
Bromoform ug/L 46.650 93 60-140
Bromomethane ug/L 45.350 91 60-140
Carbon tetrachloride ug/L 44.250 88 60-140
Chlorobenzene ug/L 46.850 94 60-140
Chloroethane ug/L 56.950 114 60-140
Chloroform ug/L 45.050 90 60-140
Chloromethane ug/L 46.050 92 60-140
cis-1,2-Dichloroethene ug/L 55.950 112 60-140
cis-1,3-Dichloropropene ug/L 45.850 92 60-140
Dibromochloromethane ug/L 45.150 90 60-140
Dibromomethane ug/L 46.450 93 60-140
Dichlorodifluoromethane ug/L 38.850 78 60-140
Diisopropyl ether ug/L 52.250 104 60-140
Ethylbenzene ug/L 48.950 98 60-140
Hexachloro-1,3-butadiene ug/L 39.550 79 60-140
Isopropylbenzene (Cumene)ug/L 53.550 107 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 46.450 93 60-140
Methylene Chloride ug/L 56.850 114 60-140
n-Butylbenzene ug/L 50.150 100 60-140
n-Propylbenzene ug/L 51.250 102 60-140
Naphthalene ug/L 49.950 100 60-140
o-Xylene ug/L 53.550 107 60-140
sec-Butylbenzene ug/L 51.650 103 60-140
Styrene ug/L 52.050 104 60-140
tert-Butylbenzene ug/L 51.850 104 60-140
Tetrachloroethene ug/L 45.450 91 60-140
Toluene ug/L 47.950 96 60-140
trans-1,2-Dichloroethene ug/L 51.350 103 60-140
trans-1,3-Dichloropropene ug/L 47.050 94 60-140
Trichloroethene ug/L 47.950 96 60-140
Trichlorofluoromethane ug/L 54.650 109 60-140
Vinyl chloride ug/L 49.150 98 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%99 70-130
Dibromofluoromethane (S)%96 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
494915MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9276754005
494916
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 90 60-14097 8 3020ND17.9 19.5
1,1,1-Trichloroethane ug/L 20 86 60-14097 12 3020ND17.2 19.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 41 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
494915MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9276754005
494916
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,2,2-Tetrachloroethane ug/L 20 92 60-140101 10 3020ND18.3 20.2
1,1,2-Trichloroethane ug/L 20 90 60-140100 10 3020ND18.0 20.0
1,1-Dichloroethane ug/L 20 112 60-140120 7 3020ND22.4 24.0
1,1-Dichloroethene ug/L 20 117 60-140123 5 3020ND23.3 24.6
1,1-Dichloropropene ug/L 20 81 60-14087 7 3020ND16.2 17.3
1,2,3-Trichlorobenzene ug/L 20 79 60-14084 6 3020ND15.7 16.7
1,2,3-Trichloropropane ug/L 20 87 60-14096 10 3020ND17.3 19.1
1,2,4-Trichlorobenzene ug/L 20 75 60-14082 8 3020ND15.0 16.3
1,2,4-Trimethylbenzene ug/L 20 91 60-140100 9 3020ND18.3 20.0
1,2-Dibromo-3-chloropropane ug/L 20 75 60-14083 9 3020ND15.1 16.6
1,2-Dibromoethane (EDB)ug/L 20 86 60-14095 10 3020ND17.2 19.0
1,2-Dichlorobenzene ug/L 20 88 60-14096 8 3020ND17.6 19.1
1,2-Dichloroethane ug/L 20 88 60-14094 7 3020ND17.6 18.9
1,2-Dichloropropane ug/L 20 89 60-14098 9 3020ND17.9 19.6
1,3,5-Trimethylbenzene ug/L 20 93 60-140100 7 3020ND18.6 20.1
1,3-Dichlorobenzene ug/L 20 88 60-14095 8 3020ND17.5 19.0
1,3-Dichloropropane ug/L 20 86 60-14094 9 3020ND17.2 18.7
1,4-Dichlorobenzene ug/L 20 86 60-14089 3 3020ND17.3 17.9
2,2-Dichloropropane ug/L 20 112 60-140115 3 3020ND22.3 23.0
2-Chlorotoluene ug/L 20 89 60-14096 8 3020ND17.8 19.2
4-Chlorotoluene ug/L 20 94 60-14099 5 3020ND18.7 19.7
Benzene ug/L 20 90 60-14097 8 3020ND18.0 19.5
Bromobenzene ug/L 20 87 60-14096 9 3020ND17.5 19.2
Bromochloromethane ug/L M02014460-140111 26 3020ND28.8 22.2
Bromodichloromethane ug/L 20 86 60-14093 8 3020ND17.2 18.5
Bromoform ug/L 20 80 60-14087 9 3020ND16.0 17.4
Bromomethane ug/L 20 102 60-140109 7 3020ND20.3 21.7
Carbon tetrachloride ug/L 20 89 60-14096 8 3020ND17.7 19.2
Chlorobenzene ug/L 20 90 60-14098 8 3020ND18.0 19.6
Chloroethane ug/L M02013960-140151 8 3020ND27.8 30.2
Chloroform ug/L 20 90 60-14096 7 30200.82 18.7 20.0
Chloromethane ug/L 20 90 60-140103 13 3020ND18.1 20.5
cis-1,2-Dichloroethene ug/L 20 119 60-140125 5 3020ND23.8 24.9
cis-1,3-Dichloropropene ug/L 20 74 60-14080 8 3020ND14.8 16.1
Dibromochloromethane ug/L 20 79 60-14089 12 3020ND15.7 17.8
Dibromomethane ug/L 20 85 60-14097 13 3020ND17.0 19.3
Dichlorodifluoromethane ug/L 20 87 60-14094 8 3020ND17.3 18.8
Diisopropyl ether ug/L 20 104 60-140113 8 3020ND20.9 22.7
Ethylbenzene ug/L 20 94 60-140100 6 3020ND18.9 20.1
Hexachloro-1,3-butadiene ug/L 20 84 60-14089 6 3020ND16.7 17.7
Isopropylbenzene (Cumene)ug/L 20 98 60-140107 10 3020ND19.5 21.5
m&p-Xylene ug/L 40 96 60-140104 8 3040ND38.3 41.6
Methyl-tert-butyl ether ug/L 20 88 60-14094 7 3020ND17.5 18.8
Methylene Chloride ug/L 20 113 60-140121 7 3020ND22.5 24.1
n-Butylbenzene ug/L 20 91 60-14099 8 3020ND18.1 19.7
n-Propylbenzene ug/L 20 97 60-140106 9 3020ND19.4 21.2
Naphthalene ug/L 20 77 60-14084 9 3020ND15.5 16.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 42 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
494915MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9276754005
494916
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
o-Xylene ug/L 20 96 60-140104 8 3020ND19.3 20.8
sec-Butylbenzene ug/L 20 100 60-140104 4 3020ND20.0 20.9
Styrene ug/L 20 95 60-140103 9 3020ND18.9 20.7
tert-Butylbenzene ug/L 20 97 60-140102 5 3020ND19.5 20.4
Tetrachloroethene ug/L 20 85 60-14096 12 3020ND17.1 19.2
Toluene ug/L 20 91 60-14098 7 3020ND18.2 19.6
trans-1,2-Dichloroethene ug/L 20 104 60-140111 7 3020ND20.8 22.2
trans-1,3-Dichloropropene ug/L 20 80 60-14085 6 3020ND16.0 17.0
Trichloroethene ug/L 20 95 60-140103 8 3020ND19.0 20.6
Trichlorofluoromethane ug/L 20 116 60-140123 6 3020ND23.1 24.7
Vinyl chloride ug/L 20 103 60-140111 7 3020ND20.6 22.1
1,2-Dichloroethane-d4 (S)%95 70-13094
4-Bromofluorobenzene (S)%100 70-130103
Dibromofluoromethane (S)%96 70-13097
Toluene-d8 (S)%99 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 43 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Results acceptable because non target analyte peak heights do not exceed the maximum calibrated upper range of thesystem per Section 9.5.8 of the Madep VPH method.1g
Analyte was detected in the associated method blank.B
The continuing calibration for this compound is outside of method control limits. The result is estimated.CC
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 44 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9276754
12611 FERRELL RESIDENCE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9276754001 OEXT/11065 GCSV/8316MW-5 MADEP EPH MADEP EPH
9276754002 OEXT/11065 GCSV/8316MW-1 MADEP EPH MADEP EPH
9276754003 OEXT/11065 GCSV/8316WSW-2 MADEP EPH MADEP EPH
9276754004 OEXT/11065 GCSV/8316WSW-3 MADEP EPH MADEP EPH
9276754005 OEXT/11065 GCSV/8316MW-3 MADEP EPH MADEP EPH
9276754001 GCV/4302MW-5 MADEP VPH
9276754002 GCV/4302MW-1 MADEP VPH
9276754003 GCV/4302WSW-2 MADEP VPH
9276754004 GCV/4302WSW-3 MADEP VPH
9276754005 GCV/4302MW-3 MADEP VPH
9276754001 MPRP/6997 ICP/6452MW-5 SM 3030C EPA 200.7
9276754002 MPRP/6997 ICP/6452MW-1 SM 3030C EPA 200.7
9276754003 MPRP/6997 ICP/6452WSW-2 SM 3030C EPA 200.7
9276754004 MPRP/6997 ICP/6452WSW-3 SM 3030C EPA 200.7
9276754005 MPRP/6997 ICP/6452MW-3 SM 3030C EPA 200.7
9276754001 OEXT/11088 MSSV/3962MW-5 EPA 625 EPA 625
9276754002 OEXT/11088 MSSV/3962MW-1 EPA 625 EPA 625
9276754003 OEXT/11088 MSSV/3962WSW-2 EPA 625 EPA 625
9276754004 OEXT/11088 MSSV/3962WSW-3 EPA 625 EPA 625
9276754005 OEXT/11088 MSSV/3962MW-3 EPA 625 EPA 625
9276754001 MSV/12117MW-5 SM 6200B
9276754002 MSV/12143MW-1 SM 6200B
9276754003 MSV/12117WSW-2 SM 6200B
9276754004 MSV/12143WSW-3 SM 6200B
9276754005 MSV/12143MW-3 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 09/13/2010 03:13 PM Page 45 of 45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]