20005_Highland Park Mill_2018 Summary Redevelopment Report (Alpha Block)

2017 SUMMARY REDEVELOPMENT
REPORT

Highland Park Mill Brownfields Site
NCBP #20005-16-060
East 16th Street at Parkwood Avenue
Charlotte, Mecklenburg County, North Carolina
January 24, 2018
Terracon Project No. 71177702

Prepared for:
White Point Paces Partners, LLC
Charlotte, North Carolina

Prepared by:
Terracon Consultants, Inc.
Charlotte, North Carolina

TABLE OF CONTENTS
Responsive ■ Resourceful ■ Reliable i

1.0 PROJECT INFORMATION ............................................................................................. 1
2.0 OVERVIEW ..................................................................................................................... 2
3.0 SOIL GRADING AND CUT AND FILL ACTIONS ........................................................... 2
3.1 Soil Import Activities ............................................................................................. 2
4.0 METHODOLOGIES USED FOR FIELD SCREENING, SAMPLING, AND LABORATORY
ANALYSIS OF ENVIRONMENTAL MEDIA ................................................................................ 3
4.1 Sump Water Sample ............................................................................................ 3
4.2 Asbestos Sampling .............................................................................................. 3
5.0 AST REMOVAL PLAN .................................................................................................... 3

FIGURES
Figure 1 – Site Location Map
Figure 2 – Preliminary Future Site Layout Map

APPENDIX A – Sump Sample Analytical Table
APPENDIX B – Approvals and Correspondence
APPENDIX C – Laboratory Analytical Reports

Responsive ■ Resourceful ■ Reliable 1

2017 SUMMARY REDEVELOPMENT REPORT
HIGHLAND PARK MILL BROWNFIELDS SITE
NCBP #20005-16-060
EAST 16TH STREET AT PARKWOOD AVENUE
CHARLOTTE, NORTH CAROLINA

Terracon Project No. 71177702
January 24, 2018

1.0 PROJECT INFORMATION
The Highland Park Mill Brownfields project is divided into two primary areas, identified as the
Alpha Block (red outline on Figure 1) and the Bravo Block (blue outline on Figure 1). The site
also includes (i) a portion of N. Brevard Street that was abandoned by the City of Charlotte to the
Prospective Developer (green outline on Figure 1); and (ii) a portion of E. 16th Street that the
City is planning to abandon to the Prospective Developer. The Prospective Developer anticipates
adding the E. 16th Street abandonment area to the existing Brownfields Agreement by
amendment. Consisting of approximately 8.67 acres, the former Highland Park textile mill property
(Mecklenburg County Tax Parcel No. 08104202) is the largest parcel within the project site. The
remaining parcels are predominantly residential or undeveloped land; however, a notable
exception is the 0.51-acre property identified as Parcel No. 08104201 which is located
immediately southwest of the textile mill. This parcel was formerly occupied by Gay Laundry and
Cleaners, a dry cleaning facility with a documented release of chlorinated compounds (DSCA Site
No. 060-0044). The former Gay Laundry and Cleaners building was renovated and converted into
offices prior to the Prospective Developer (PD) acquiring the Brownfields Property.

The Highland Park Mill site is generally bound to the south by N. Caldwell Street, to the east by
Parkwood Avenue, to the north and northwest by Norfolk-Southern railroad tracks and to the west
by an unnamed tributary of Little Sugar Creek and commercial businesses. The tributary also
traverses a portion of the Alpha Block.

The Environmental Management Plan (EMP) for the site was approved by the NC Brownfields
Program on August 2, 2017. The initial redevelopment of the property included limited demolition
of portions of the non-historical additions to the main mill building. The PD has hired Barnhill
Contracting Company (Barnhill) as the General Contractor for the project. EHG, LLC (EHG) was
subcontracted to conduct interior renovations and asbestos abatement activities. Interior
renovations of the mill building commenced in 2017. Redevelopment activities also include
parking areas in the southern portion of the site, bordered by Parkwood Avenue, Belmont Avenue,
and N. Brevard Street, and in the northern portion of the site, bordered by the CATs Blue Line
Extension (light rail line) and E. 16th Street. Various pedestrian plazas and open-air terraces are
planned for redevelopment along the perimeter of the mill building. A future site layout map is
included as Figure 2.

2017 Summary Redevelopment Report
Highland Park Mill (NCBP #20005-16-060) ■ Charlotte, North Carolina
January 24, 2018 ■ Terracon Project No. 71177702

Responsive ■ Resourceful ■ Reliable 2

This summary redevelopment report only addresses the Prospective Developer’s redevelopment
activities that have occurred on the Alpha Block and the N. Brevard Street abandonment area.
The Prospective Developer is cooperating with the City of Charlotte regarding its stream,
stormwater, and utility improvements and its construction of the CATS Light Rail pursuant to
easements granted by prior property owners. The Bravo Block was sold to and is being
redeveloped by an unrelated developer (DRI/Maple Tomkins Mill, L.L.C.). The Prospective
Developer has not conducted any redevelopment activities on the Bravo Block.

2.0 OVERVIEW
A summary of Brownfields-related environmental assessment activities, if applicable, is provided
in the following sections of the report. The following activities were completed pursuant to Land
Use Restriction 8:

 Actions taken on the Brownfield Property in accordance with Section V of the Brownfields
Agreement;
 Soil grading and cut and fill actions;
 Methodologies employed for field screening, sampling and laboratory analysis of
environmental media;
 Stockpiling, containerizing, decontaminating, treating, handling, laboratory analysis and
ultimate disposition of any soil, groundwater or other materials suspected or confirmed to
be contaminated with regulated substances; and
 Removal of any contaminated soil, water or other contaminated materials from the
Brownfields Property.
 Removal of any contaminated soil, water, or other contaminated materials (for example,
concrete, demolition debris).

3.0 SOIL GRADING AND CUT AND FILL ACTIONS
Grading activities at the site were conducted according to the initial grading plan included with the
EMP.
3.1 Soil Import Activities
The redevelopment project at the Highland Park Mill Brownfields Site requires soils to be imported
to the site. The soils that have been imported to the site were obtained from the Bravo Block
portion of the Brownfields Property. In accordance with the EMP, additional sampling of the
imported materials from the Bravo Block was not required prior to transport to the Alpha Block.
Any excavated materials created from grading activities on the site were used in fill areas
elsewhere on the property.
2017 Summary Redevelopment Report
Highland Park Mill (NCBP #20005-16-060) ■ Charlotte, North Carolina
January 24, 2018 ■ Terracon Project No. 71177702

Responsive ■ Resourceful ■ Reliable 3

In accordance with the EMP, fill soils obtained from somewhere other than the Brownfields
Property will be characterized, and the information will be submitted to the NCDEQ for review and
approval prior to importing the off-site soils.

4.0 METHODOLOGIES USED FOR FIELD SCREENING, SAMPLING,
AND LABORATORY ANALYSIS OF ENVIRONMENTAL MEDIA
Terracon conducted field screening at the Brownfields Property during site work. Details about
the sampling and laboratory analysis are described below. Laboratory reports are provided in
Appendix C.
4.1 Sump Water Sample
In April 2017, Terracon collected a water sample from a sump (Sump-1) located within the eastern
portion of the mill building (Figure 1). Constituents detected in the sump sample did not exceed
NCAC Title 15 Subchapter 2L Groundwater Standards or NCAC 2B Surface Water Quality
Standards (SWQS). A summary table (Table 1) of the constituents detected in the sump sample
is included in Appendix A.
4.2 Asbestos Sampling
In September 2017, Terracon collected 21 bulk samples from suspect asbestos-containing
materials within the mill building to supplement prior asbestos-containing materials assessments
conducted by others. Based on the laboratory analytical results, asbestos was detected in
samples collected from the roofing materials. EHG was subcontracted to conduct the asbestos
abatement services at the mill building.

5.0 AST REMOVAL PLAN
During a 2016 site visit, Terracon confirmed the presence of a fuel oil AST, located in the
northwestern portion of the property, and a second AST located near the southern exterior corner
of the mill building (Figure 1). The contents or historical contents of the second tank were not
identified; however, according to mill employees, the contents of the AST were likely cotton seed
oil which was used exclusively at the mill for dyeing purposes. Soil samples collected in
September 2016, indicate soils near the fuel oil AST contain petroleum constituents above PSRG
industrial standards. According to Paragraph 14 of the Brownfields Agreement (BFA), a written
plan to remove the two on-site ASTs must be submitted to the NCDEQ for review and approval
within 90 days after the recordation of the Notice of a Brownfields Property and prior to
implementation of the Plan.
2017 Summary Redevelopment Report
Highland Park Mill (NCBP #20005-16-060) ■ Charlotte, North Carolina
January 24, 2018 ■ Terracon Project No. 71177702

Responsive ■ Resourceful ■ Reliable 4

In September 2017, an Aboveground Storage Tank Removal Plan was submitted to the NCDEQ
for approval. After revisions were submitted in October 2017, the NCDEQ approved the AST
removal plan on October 23, 2017. As of the issuance of this report, the ASTs have not been
removed from the site. A copy of the NCDEQ approval for the AST Removal Plan is included in
Appendix B.

FIGURES

08104202
08301125
08104201
Sources: Esri, HERE, DeLorme, Intermap, increment P Corp., GEBCO, USGS, FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, Esri Japan,METI, Esri China (Hong Kong), swisstopo, MapmyIndia, © OpenStreetMap contributors, and the GIS User Community
PH. [phone] terracon.com
2701 WESTPORT ROAD CHARLOTTE, NC
FIGURE
1
SITE LOCATION MAP71177702
CZ/HEH HIGHLAND PARK MILL BROWNFIELDS SITEEAST 16th ST. AT PARKWOOD AVE.CLC CHARLOTTE, NC
Project No.:
Drawn By:
Checked By:
Date: N:\71 Environmental\Bus Dev\Proposals\2016 Proposals\71167E100 Highland Park Mill BF - Soil LSI\GIS\MXD\Assessment Report\Fig 1-Overview.mxd³
0 150 30075Feet1 inch = 150 feet
Legend
Brownfields Boundary (Alpha Block)
Brownfields Boundary (Bravo Block)
Brevard Street Abandonment
Notes:- Locations of building footprints and site features are approximate.- The 8-Digit Number in each parcel represents the Mecklenburg County Tax Parcel ID.- Parcel data obtained from Mecklenburg County GIS website.
FORMER HIGHLAND PARK MILL
FORMERALPHAMILLS
Location of Sump-1
PH. [phone] terracon.com
2701 WESTPORT ROAD CHARLOTTE, NC
FIGURE
2
71177702
CZ/HEH
PRELIMINARY FUTURESITE LAYOUT MAP
HIGHLAND PARK MILL BROWNFIELDS SITEEAST 16th ST. AT PARKWOOD AVE.CLC CHARLOTTE, NC
Jan. 2018
Project No.:
Drawn By:
Checked By:
Date: N:\71 Environmental\Bus Dev\Proposals\2016 Proposals\71167E100 Highland Park Mill BF - Soil LSI\GIS\MXD\Assessment Report\Fig 8 - Prelim Future Site Layout.mxd³
0 100 20050Feet1 inch = 100 feet
Legend
Brownfields Boundary (Alpha Block)
Brownfields Boundary (Bravo Block)
Brevard Street Abandonment
Unnamed Tributary
Notes:- Preliminary future construction details provided by White Point Paces Partners, LLC.- Parcel data obtained from Mecklenburg County GIS website.- 2015 aerial imagery obtained from NC Onemap.- Construction details provided by White Point Paces Partners, LLC.

APPENDIX A
SUMP SAMPLE ANALYTICAL TABLE

Table 1
Sump Water Sample Analytical Results
Highland Park Mill Brownfields Site
E. 16th Street at Parkwood Avenue
Charlotte, Mecklenburg County, NC
Sample ID: Sump-1
Sample Date: 04/10/17
RCRA Metals by EPA Method 6010
Barium 700 200,0001 34.6
Chromium 10 111 5.6
Notes:
Concentrations are reported in micrograms per liter ( µg/L).
Only detected compounds are shown.
NCAC 2L GWQS - North Carolina Administrative Code Subchapter 2L Groundwater Quality Standards (April 1, 2013).
NCAC 2B SWQS - NCAC Subchapter 2B Surface Water Quality Standards for Class C Waters (June 30, 2016).
1 - 2B Standard is based on the most stringent Freshwater or Human Health standard for barium and chromium.
Not detected above laboratory method detection limits.
Not detected above laboratory method detection limits.
Analyte NCAC 2L GWQS
Volatile Organic Compounds by EPA Method 8260
Semi-Volatile Organic Compounds by EPA Method 8270
NCAC 2B SWQS

APPENDIX B
APPROVALS AND CORRESPONDENCE

1
Hindes, Haley E
From:Rudder, James <[e-mail]>
Sent:Monday, October 23, 2017 1:11 PM
To:Lins, Brittany N.
Cc:Jay Levell ([e-mail]); Erik Johnson ([e-mail]);
Corbitt, Chris L.; Hindes, Haley E; Eckard, Sharon; Nicholson, Bruce; Walker, Chris
Subject:RE: [External] RE: Highland Park Mill (NCBP#20005-16-060) - AST Removal Work Plan
Ms. Lins,
The Brownfields Program has received the “Revised Above Ground Storage Tank Removal Plan, Highland Park Mill
Brownfields Site (NCBP #20005-16-060)” as an email attachment to an email received this same day (10/23/2017 at
11:58 am). Please consider this email the Brownfields Program’s written approval of the Revised Plan dated October 20,
2017.
The Brownfields Program requests that the laboratory test results for the samples collected beneath the fuel oil AST be
forwarded to the Brownfields Program when Terracon first receives the laboratory analytical reports(s). Please include a
figure (can be draft until written report received) showing the sampling locations.
We look forward to receiving the written closure report as soon as it becomes available.
Regards,
Jim
James Rudder
Project Manager
Division of Waste Management - Brownfields
NC Department of Environmental Quality
1646 Mail Service Center
Raleigh, NC 27699-1646
{919} 707-8381 - Direct Line & Fax
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.
From: Lins, Brittany N. [mailto:[e-mail]]
Sent: Monday, October 23, 2017 11:58 AM
2
To: Rudder, James <[e-mail]>
Cc: Jay Levell ([e-mail]) <[e-mail]>; Erik Johnson
([e-mail]) <[e-mail]>; Corbitt, Chris L. ([e-mail])
<[e-mail]>; Hindes, Haley E ([e-mail]) <[e-mail]>; Eckard,
Sharon <[e-mail]>; Nicholson, Bruce <[e-mail]>; Walker, Chris
<[e-mail]>
Subject: [External] RE: Highland Park Mill (NCBP#20005-16-060) - AST Removal Work Plan
CAUTION: This email originated from outside of the organization. Do not click links or open attachments unless you verify that the
attachment and content are safe. Send all suspicious email as an attachment to [e-mail].
Jim,
For your review, please see attached the revised AST Removal Work Plan for the Highland Park Mill Brownfields Site,
addressing your comments below. Please let us know if you have any questions.
Regards,
Brittany
Brittany N. Lins
Attorney
K&L Gates LLP
Hearst Tower
214 North Tryon Street, 47th Floor
Charlotte, NC 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com
From: Rudder, James [mailto:[e-mail]]
Sent: Thursday, October 19, 2017 12:13 PMTo: Walker, Chris
Cc: Jay Levell ([e-mail]); Erik Johnson ([e-mail]); Corbitt, Chris L.
([e-mail]); Hindes, Haley E ([e-mail]); Eckard, Sharon; Lins, Brittany N.;
Nicholson, Bruce
Subject: RE: Highland Park Mill (NCBP#20005-16-060) - AST Removal Work Plan
Chris,
The Brownfields Program has reviewed the “above Ground Storage Tank Removal Plan, Highland Park Mills Brownfields
Site (NCBP #20005-16-060), East 16th Street at Parkwood Avenue” prepared by Terracon Consultants, Inc. and dated
September 27, 2017.
Based on this review we are providing the following comments:
1.The Plan excludes sampling soil beneath the fuel oil AST and references previous sampling completed in
2016. The referenced previous sampling location is shown on the “Brownfields Assessment Report, Highland
Park Mill Brownfields Site, NCBP #20005-16-060, East 16th Street at Parkwood Avenue” prepared by Terrcon and
3
dated October 27, 2016. This sampling location was designated SB-04 and the soil sample was collected across
the 0 – 5 ft depth interval. SB-04 was not collected beneath the fuel oil AST. Using the scale on Figure 5 (of the
assessment report, attached) SB-04 was collected about 15 to 18 feet east of the fuel oil AST.
Because of these facts and observations one to two soil samples must be collected beneath the former fuel oil
UST location. These soil samples should be collected as “grab” samples from a depth of 2 feet below the ground
surface. The samples should be collected below the invert of the fuel oil AST and be laboratory analyzed using
the laboratory methods for VOCs and SVOCs referenced at the bottom of paragraph 1 on page 2 of the Plan (EPA
Methods 8260, 8270 – metals analyses not necessary). These samples are to be collected so that the highest
magnitude contaminant concentrations (which should occur beneath the AST) will be characterized. From this
contaminant characterization risk management decisions can be made. Even though the fuel oil AST location is
expected to be covered with two feet of clean fill, as shown in the cut/fill diagram (Figure 2 of the Plan),
accurate characterization of the maximum residual concentrations remaining in soil is required.
2.The location of the AST believed to have historically contained cottonseed oil is not shown on Figure 1 of the
Plan. Please identify the location of this AST on Figure 1 of the Plan.
3.Because of ongoing redevelopment schedules and plans it will be important to review the AST closure data as
soon as it becomes available. Please provide the laboratory analytical reports and a draft sampling location map
to the Brownfields Program as soon as the laboratory report(s) is made available to Terracon.
We look forward to receiving a revised AST closure Plan at your earliest convenience.
Regards,
Jim
James Rudder
Project Manager
Division of Waste Management - Brownfields
NC Department of Environmental Quality
1646 Mail Service Center
Raleigh, NC 27699-1646
{919} 707-8381 - Direct Line & Fax
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.
From: Walker, Chris [mailto:[e-mail]]
Sent: Friday, September 29, 2017 12:39 PM
To: Rudder, James <[e-mail]>
4
Cc: Jay Levell ([e-mail]) <[e-mail]>; Erik Johnson
([e-mail]) <[e-mail]>; Corbitt, Chris L. ([e-mail])
<[e-mail]>; Hindes, Haley E ([e-mail]) <[e-mail]>; Lins,
Brittany N. <[e-mail]>
Subject: Highland Park Mill (NCBP#20005-16-060) - AST Removal Work Plan
Jim:
Paragraph 14 of the Brownfields Agreement for Highland Park Mill requires the submittal of a work plan for the removal
of the fuel oil AST and cottonseed oil AST within 90 days of the recordation of the Brownfields Agreement and before
implementation of the work plan. I’ve attached our proposed Aboveground Storage Tank Removal Plan for your review
and approval. We look forward to hearing back from you. In the meantime, please contact me with any questions.
Thanks,
Chris
Chris S. Walker
K&L Gates LLP
214 North Tryon Street
Charlotte, North Carolina 28202
Phone: [phone]
Fax: [phone]
[e-mail]
www.klgates.com
This electronic message contains information from the law firm of K&L Gates LLP. The contents may be privileged and confidential and are intended for
the use of the intended addressee(s) only. If you are not an intended addressee, note that any disclosure, copying, distribution, or use of the contents of
this message is prohibited. If you have received this e-mail in error, please contact me at [e-mail].-4
This electronic message contains information from the law firm of K&L Gates LLP. The contents may be privileged and confidential and are intended for
the use of the intended addressee(s) only. If you are not an intended addressee, note that any disclosure, copying, distribution, or use of the contents of
this message is prohibited. If you have received this e-mail in error, please contact me at [e-mail].-4

APPENDIX C
LABORATORY ANALYTICAL RESULTS

#=CL#
April 13, 2017
LIMS USE: FR - CHRIS CORBITT
LIMS OBJECT ID: 92336532
92336532
Project:
Pace Project No.:
RE:
Mr. Chris Corbitt
Terracon
2020 E-Starita Road
Charlotte, NC 28206
HIGHLAND PARK MILL 71167505
Dear Mr. Corbitt:
Enclosed are the analytical results for sample(s) received by the laboratory on April 10, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:McKhenzy Welch, Terracon
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 25
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 25
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Lab ID Sample ID Matrix Date Collected Date Received
92336532001 SUMP-1 Water 04/10/17 11:15 04/10/17 14:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 25
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92336532001 SUMP-1 EPA 6010 7 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Sample:SUMP-1 Lab ID:92336532001 Collected:04/10/17 11:15 Received:04/10/17 14:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 04/12/17 13:32 7440-38-204/11/17 19:0010.0 5.0 1
Barium 34.6 ug/L 04/12/17 13:32 7440-39-304/11/17 19:005.0 2.5 1
Cadmium ND ug/L 04/12/17 13:32 7440-43-904/11/17 19:001.0 0.50 1
Chromium 5.6 ug/L 04/12/17 13:32 7440-47-304/11/17 19:005.0 2.5 1
Lead ND ug/L 04/12/17 13:32 7439-92-104/11/17 19:005.0 2.5 1
Selenium ND ug/L 04/12/17 13:32 7782-49-204/11/17 19:0010.0 5.0 1
Silver ND ug/L 04/12/17 13:32 7440-22-404/11/17 19:005.0 2.5 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 04/12/17 18:31 7439-97-604/12/17 07:100.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 04/11/17 15:37 83-32-904/11/17 08:3910.0 0.25 1
Acenaphthylene ND ug/L 04/11/17 15:37 208-96-804/11/17 08:3910.0 0.21 1
Aniline ND ug/L 04/11/17 15:37 62-53-304/11/17 08:3910.0 1.3 1
Anthracene ND ug/L 04/11/17 15:37 120-12-704/11/17 08:3910.0 0.14 1
Benzo(a)anthracene ND ug/L 04/11/17 15:37 56-55-304/11/17 08:3910.0 0.33 1
Benzo(a)pyrene ND ug/L 04/11/17 15:37 50-32-804/11/17 08:3910.0 0.30 1
Benzo(b)fluoranthene ND ug/L 04/11/17 15:37 205-99-204/11/17 08:3910.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 04/11/17 15:37 191-24-204/11/17 08:3910.0 0.38 1
Benzo(k)fluoranthene ND ug/L 04/11/17 15:37 207-08-904/11/17 08:3910.0 0.43 1
Benzoic Acid ND ug/L 04/11/17 15:37 65-85-004/11/17 08:3950.0 11.1 1
Benzyl alcohol ND ug/L 04/11/17 15:37 100-51-604/11/17 08:3920.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 04/11/17 15:37 101-55-304/11/17 08:3910.0 1.3 1
Butylbenzylphthalate ND ug/L 04/11/17 15:37 85-68-704/11/17 08:3910.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 04/11/17 15:37 59-50-704/11/17 08:3920.0 4.2 1
4-Chloroaniline ND ug/L 04/11/17 15:37 106-47-804/11/17 08:3920.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 04/11/17 15:37 111-91-104/11/17 08:3910.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 04/11/17 15:37 111-44-404/11/17 08:3910.0 1.5 1
2-Chloronaphthalene ND ug/L 04/11/17 15:37 91-58-704/11/17 08:3910.0 2.2 1
2-Chlorophenol ND ug/L 04/11/17 15:37 95-57-804/11/17 08:3910.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 04/11/17 15:37 7005-72-304/11/17 08:3910.0 2.1 1
Chrysene ND ug/L 04/11/17 15:37 218-01-904/11/17 08:3910.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 04/11/17 15:37 53-70-304/11/17 08:3910.0 0.55 1
Dibenzofuran ND ug/L 04/11/17 15:37 132-64-904/11/17 08:3910.0 1.8 1
1,2-Dichlorobenzene ND ug/L 04/11/17 15:37 95-50-104/11/17 08:3910.0 1.2 1
1,3-Dichlorobenzene ND ug/L 04/11/17 15:37 541-73-104/11/17 08:3910.0 1.1 1
1,4-Dichlorobenzene ND ug/L 04/11/17 15:37 106-46-704/11/17 08:3910.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 04/11/17 15:37 91-94-104/11/17 08:3920.0 1.4 1
2,4-Dichlorophenol ND ug/L 04/11/17 15:37 120-83-204/11/17 08:3910.0 1.7 1
Diethylphthalate ND ug/L 04/11/17 15:37 84-66-204/11/17 08:3910.0 1.3 1
2,4-Dimethylphenol ND ug/L 04/11/17 15:37 105-67-904/11/17 08:3910.0 2.2 1
Dimethylphthalate ND ug/L 04/11/17 15:37 131-11-304/11/17 08:3910.0 1.5 1
Di-n-butylphthalate ND ug/L 04/11/17 15:37 84-74-204/11/17 08:3910.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 04/11/17 15:37 534-52-104/11/17 08:3920.0 1.7 1
2,4-Dinitrophenol ND ug/L 04/11/17 15:37 51-28-504/11/17 08:3950.0 6.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
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Page 5 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Sample:SUMP-1 Lab ID:92336532001 Collected:04/10/17 11:15 Received:04/10/17 14:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dinitrotoluene ND ug/L 04/11/17 15:37 121-14-204/11/17 08:3910.0 1.2 1
2,6-Dinitrotoluene ND ug/L 04/11/17 15:37 606-20-204/11/17 08:3910.0 1.7 1
Di-n-octylphthalate ND ug/L 04/11/17 15:37 117-84-004/11/17 08:3910.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/11/17 15:37 117-81-704/11/17 08:396.0 0.85 1
Fluoranthene ND ug/L 04/11/17 15:37 206-44-004/11/17 08:3910.0 0.21 1
Fluorene ND ug/L 04/11/17 15:37 86-73-704/11/17 08:3910.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 04/11/17 15:37 87-68-304/11/17 08:3910.0 1.8 1
Hexachlorobenzene ND ug/L 04/11/17 15:37 118-74-104/11/17 08:3910.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 04/11/17 15:37 77-47-404/11/17 08:3910.0 1.8 1
Hexachloroethane ND ug/L 04/11/17 15:37 67-72-104/11/17 08:3910.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/11/17 15:37 193-39-504/11/17 08:3910.0 0.29 1
Isophorone ND ug/L 04/11/17 15:37 78-59-104/11/17 08:3910.0 1.8 1
1-Methylnaphthalene ND ug/L 04/11/17 15:37 90-12-004/11/17 08:3910.0 0.32 1
2-Methylnaphthalene ND ug/L 04/11/17 15:37 91-57-604/11/17 08:3910.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 04/11/17 15:37 95-48-704/11/17 08:3910.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/11/17 15:37 L104/11/17 08:3910.0 1.7 1
Naphthalene ND ug/L 04/11/17 15:37 91-20-304/11/17 08:3910.0 0.34 1
2-Nitroaniline ND ug/L 04/11/17 15:37 88-74-404/11/17 08:3950.0 2.8 1
3-Nitroaniline ND ug/L 04/11/17 15:37 99-09-204/11/17 08:3950.0 2.4 1
4-Nitroaniline ND ug/L 04/11/17 15:37 100-01-604/11/17 08:3920.0 2.5 1
Nitrobenzene ND ug/L 04/11/17 15:37 98-95-304/11/17 08:3910.0 1.7 1
2-Nitrophenol ND ug/L 04/11/17 15:37 88-75-504/11/17 08:3910.0 1.7 1
4-Nitrophenol ND ug/L 04/11/17 15:37 100-02-704/11/17 08:3950.0 5.8 1
N-Nitrosodimethylamine ND ug/L 04/11/17 15:37 62-75-904/11/17 08:3910.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 04/11/17 15:37 621-64-704/11/17 08:3910.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 04/11/17 15:37 86-30-604/11/17 08:3910.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/11/17 15:37 108-60-104/11/17 08:3910.0 1.6 1
Pentachlorophenol ND ug/L 04/11/17 15:37 87-86-504/11/17 08:3925.0 2.3 1
Phenanthrene ND ug/L 04/11/17 15:37 85-01-804/11/17 08:3910.0 0.22 1
Phenol ND ug/L 04/11/17 15:3704/11/17 08:3910.0 1.7 1
Pyrene ND ug/L 04/11/17 15:37 129-00-004/11/17 08:3910.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 04/11/17 15:37 120-82-104/11/17 08:3910.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 04/11/17 15:37 95-95-404/11/17 08:3910.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 04/11/17 15:37 88-06-204/11/17 08:3910.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)61 %04/11/17 15:37 4165-60-004/11/17 08:3921-110 1
2-Fluorobiphenyl (S)74 %04/11/17 15:37 321-60-804/11/17 08:3927-110 1
Terphenyl-d14 (S)76 %04/11/17 15:37 1718-51-004/11/17 08:3931-107 1
Phenol-d6 (S)22 %04/11/17 15:37 13127-88-304/11/17 08:3910-110 1
2-Fluorophenol (S)36 %04/11/17 15:37 367-12-404/11/17 08:3912-110 1
2,4,6-Tribromophenol (S)96 %04/11/17 15:37 118-79-604/11/17 08:3927-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 04/11/17 14:50 67-64-125.0 10.0 1
Benzene ND ug/L 04/11/17 14:50 71-43-21.0 0.25 1
Bromobenzene ND ug/L 04/11/17 14:50 108-86-11.0 0.30 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Sample:SUMP-1 Lab ID:92336532001 Collected:04/10/17 11:15 Received:04/10/17 14:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Bromochloromethane ND ug/L 04/11/17 14:50 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 04/11/17 14:50 75-27-41.0 0.18 1
Bromoform ND ug/L 04/11/17 14:50 75-25-21.0 0.26 1
Bromomethane ND ug/L 04/11/17 14:50 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 04/11/17 14:50 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 04/11/17 14:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 04/11/17 14:50 108-90-71.0 0.23 1
Chloroethane ND ug/L 04/11/17 14:50 75-00-31.0 0.54 1
Chloroform ND ug/L 04/11/17 14:50 67-66-31.0 0.14 1
Chloromethane ND ug/L 04/11/17 14:50 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 04/11/17 14:50 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 04/11/17 14:50 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 04/11/17 14:50 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 04/11/17 14:50 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 04/11/17 14:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/11/17 14:50 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 04/11/17 14:50 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 04/11/17 14:50 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 04/11/17 14:50 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/11/17 14:50 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 04/11/17 14:50 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 04/11/17 14:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 04/11/17 14:50 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 04/11/17 14:50 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 04/11/17 14:50 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 04/11/17 14:50 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 04/11/17 14:50 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/11/17 14:50 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 04/11/17 14:50 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 04/11/17 14:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 04/11/17 14:50 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 04/11/17 14:50 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 04/11/17 14:50 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/11/17 14:50 87-68-31.0 0.71 1
2-Hexanone ND ug/L 04/11/17 14:50 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 04/11/17 14:50 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 04/11/17 14:50 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/11/17 14:50 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 04/11/17 14:50 1634-04-41.0 0.21 1
Naphthalene ND ug/L 04/11/17 14:50 91-20-31.0 0.24 1
Styrene ND ug/L 04/11/17 14:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 04/11/17 14:50 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 04/11/17 14:50 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 04/11/17 14:50 127-18-41.0 0.46 1
Toluene ND ug/L 04/11/17 14:50 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 04/11/17 14:50 87-61-61.0 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Sample:SUMP-1 Lab ID:92336532001 Collected:04/10/17 11:15 Received:04/10/17 14:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 04/11/17 14:50 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 04/11/17 14:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 04/11/17 14:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 04/11/17 14:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 04/11/17 14:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 04/11/17 14:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 04/11/17 14:50 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 04/11/17 14:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 04/11/17 14:50 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 04/11/17 14:50 179601-23-12.0 0.66 1
o-Xylene ND ug/L 04/11/17 14:50 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %04/11/17 14:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %04/11/17 14:50 17060-07-070-130 1
Toluene-d8 (S)108 %04/11/17 14:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
356246
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92336532001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1976334
Associated Lab Samples:92336532001
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 04/12/17 18:000.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1976335LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1976336MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92336263001
1976337
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 97 75-12598 1 252.5ND 2.5 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
356085
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92336532001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1975250
Associated Lab Samples:92336532001
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 10.0 04/12/17 13:145.0
Barium ug/L ND 5.0 04/12/17 13:142.5
Cadmium ug/L ND 1.0 04/12/17 13:140.50
Chromium ug/L ND 5.0 04/12/17 13:142.5
Lead ug/L ND 5.0 04/12/17 13:142.5
Selenium ug/L ND 10.0 04/12/17 13:145.0
Silver ug/L ND 5.0 04/12/17 13:142.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1975251LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 466500 93 80-120
Barium ug/L 473500 95 80-120
Cadmium ug/L 480500 96 80-120
Chromium ug/L 470500 94 80-120
Lead ug/L 478500 96 80-120
Selenium ug/L 485500 97 80-120
Silver ug/L 242250 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1975252MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92336549001
1975253
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L H35008275-12583 1 20500ND414419
Barium ug/L H35008575-12589 2 20500423850870
Cadmium ug/L H35008775-12588 2 20500ND435442
Chromium ug/L H35008875-12588 0 2050081.3 520 522
Lead ug/L H35008475-12585 2 2050030.2 449 456
Selenium ug/L H35008575-12587 2 20500ND429436
Silver ug/L H32509075-12591 2 20250ND224228
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
355922
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92336532001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1974350
Associated Lab Samples:92336532001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 04/11/17 13:060.33
1,1,1-Trichloroethane ug/L ND 1.0 04/11/17 13:060.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 04/11/17 13:060.40
1,1,2-Trichloroethane ug/L ND 1.0 04/11/17 13:060.29
1,1-Dichloroethane ug/L ND 1.0 04/11/17 13:060.32
1,1-Dichloroethene ug/L ND 1.0 04/11/17 13:060.56
1,1-Dichloropropene ug/L ND 1.0 04/11/17 13:060.49
1,2,3-Trichlorobenzene ug/L ND 1.0 04/11/17 13:060.33
1,2,3-Trichloropropane ug/L ND 1.0 04/11/17 13:060.41
1,2,4-Trichlorobenzene ug/L ND 1.0 04/11/17 13:060.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 04/11/17 13:062.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/11/17 13:060.27
1,2-Dichlorobenzene ug/L ND 1.0 04/11/17 13:060.30
1,2-Dichloroethane ug/L ND 1.0 04/11/17 13:060.24
1,2-Dichloropropane ug/L ND 1.0 04/11/17 13:060.27
1,3-Dichlorobenzene ug/L ND 1.0 04/11/17 13:060.24
1,3-Dichloropropane ug/L ND 1.0 04/11/17 13:060.28
1,4-Dichlorobenzene ug/L ND 1.0 04/11/17 13:060.33
2,2-Dichloropropane ug/L ND 1.0 04/11/17 13:060.13
2-Butanone (MEK)ug/L ND 5.0 04/11/17 13:060.96
2-Chlorotoluene ug/L ND 1.0 04/11/17 13:060.35
2-Hexanone ug/L ND 5.0 04/11/17 13:060.46
4-Chlorotoluene ug/L ND 1.0 04/11/17 13:060.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 04/11/17 13:060.33
Acetone ug/L ND 25.0 04/11/17 13:0610.0
Benzene ug/L ND 1.0 04/11/17 13:060.25
Bromobenzene ug/L ND 1.0 04/11/17 13:060.30
Bromochloromethane ug/L ND 1.0 04/11/17 13:060.17
Bromodichloromethane ug/L ND 1.0 04/11/17 13:060.18
Bromoform ug/L ND 1.0 04/11/17 13:060.26
Bromomethane ug/L ND 2.0 04/11/17 13:060.29
Carbon tetrachloride ug/L ND 1.0 04/11/17 13:060.25
Chlorobenzene ug/L ND 1.0 04/11/17 13:060.23
Chloroethane ug/L ND 1.0 04/11/17 13:060.54
Chloroform ug/L ND 1.0 04/11/17 13:060.14
Chloromethane ug/L ND 1.0 04/11/17 13:060.11
cis-1,2-Dichloroethene ug/L ND 1.0 04/11/17 13:060.19
cis-1,3-Dichloropropene ug/L ND 1.0 04/11/17 13:060.13
Dibromochloromethane ug/L ND 1.0 04/11/17 13:060.21
Dibromomethane ug/L ND 1.0 04/11/17 13:060.21
Dichlorodifluoromethane ug/L ND 1.0 04/11/17 13:060.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1974350
Associated Lab Samples:92336532001
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 04/11/17 13:060.12
Ethylbenzene ug/L ND 1.0 04/11/17 13:060.30
Hexachloro-1,3-butadiene ug/L ND 1.0 04/11/17 13:060.71
m&p-Xylene ug/L ND 2.0 04/11/17 13:060.66
Methyl-tert-butyl ether ug/L ND 1.0 04/11/17 13:060.21
Methylene Chloride ug/L ND 2.0 04/11/17 13:060.97
Naphthalene ug/L ND 1.0 04/11/17 13:060.24
o-Xylene ug/L ND 1.0 04/11/17 13:060.23
p-Isopropyltoluene ug/L ND 1.0 04/11/17 13:060.31
Styrene ug/L ND 1.0 04/11/17 13:060.26
Tetrachloroethene ug/L ND 1.0 04/11/17 13:060.46
Toluene ug/L ND 1.0 04/11/17 13:060.26
trans-1,2-Dichloroethene ug/L ND 1.0 04/11/17 13:060.49
trans-1,3-Dichloropropene ug/L ND 1.0 04/11/17 13:060.26
Trichloroethene ug/L ND 1.0 04/11/17 13:060.47
Trichlorofluoromethane ug/L ND 1.0 04/11/17 13:060.20
Vinyl acetate ug/L ND 2.0 04/11/17 13:060.35
Vinyl chloride ug/L ND 1.0 04/11/17 13:060.62
Xylene (Total)ug/L ND 1.0 04/11/17 13:060.66
1,2-Dichloroethane-d4 (S)%95 70-130 04/11/17 13:06
4-Bromofluorobenzene (S)%98 70-130 04/11/17 13:06
Toluene-d8 (S)%104 70-130 04/11/17 13:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1974351LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.750 103 70-130
1,1,1-Trichloroethane ug/L 50.850 102 70-130
1,1,2,2-Tetrachloroethane ug/L 48.650 97 70-130
1,1,2-Trichloroethane ug/L 49.950 100 70-130
1,1-Dichloroethane ug/L 49.150 98 70-130
1,1-Dichloroethene ug/L 53.050 106 70-132
1,1-Dichloropropene ug/L 52.250 104 70-130
1,2,3-Trichlorobenzene ug/L 47.750 95 70-135
1,2,3-Trichloropropane ug/L 48.350 97 70-130
1,2,4-Trichlorobenzene ug/L 49.450 99 70-134
1,2-Dibromo-3-chloropropane ug/L 49.150 98 70-130
1,2-Dibromoethane (EDB)ug/L 50.650 101 70-130
1,2-Dichlorobenzene ug/L 47.650 95 70-130
1,2-Dichloroethane ug/L 46.950 94 70-130
1,2-Dichloropropane ug/L 47.750 95 70-130
1,3-Dichlorobenzene ug/L 47.450 95 70-130
1,3-Dichloropropane ug/L 51.050 102 70-130
1,4-Dichlorobenzene ug/L 48.350 97 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
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Page 12 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1974351LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 54.150 108 58-145
2-Butanone (MEK)ug/L 95.8100 96 70-145
2-Chlorotoluene ug/L 47.650 95 70-130
2-Hexanone ug/L 99.9100 100 70-144
4-Chlorotoluene ug/L 47.850 96 70-130
4-Methyl-2-pentanone (MIBK)ug/L 96.5100 96 70-140
Acetone ug/L 99.6100 100 50-175
Benzene ug/L 50.950 102 70-130
Bromobenzene ug/L 48.750 97 70-130
Bromochloromethane ug/L 51.050 102 70-130
Bromodichloromethane ug/L 52.150 104 70-130
Bromoform ug/L 48.650 97 70-130
Bromomethane ug/L 35.450 71 54-130
Carbon tetrachloride ug/L 53.250 106 70-132
Chlorobenzene ug/L 49.450 99 70-130
Chloroethane ug/L 54.850 110 64-134
Chloroform ug/L 48.050 96 70-130
Chloromethane ug/L 47.450 95 64-130
cis-1,2-Dichloroethene ug/L 47.950 96 70-131
cis-1,3-Dichloropropene ug/L 53.550 107 70-130
Dibromochloromethane ug/L 56.250 112 70-130
Dibromomethane ug/L 47.350 95 70-131
Dichlorodifluoromethane ug/L 57.650 115 56-130
Diisopropyl ether ug/L 50.150 100 70-130
Ethylbenzene ug/L 48.050 96 70-130
Hexachloro-1,3-butadiene ug/L 50.350 101 70-130
m&p-Xylene ug/L 96.8100 97 70-130
Methyl-tert-butyl ether ug/L 52.050 104 70-130
Methylene Chloride ug/L 49.750 99 63-130
Naphthalene ug/L 51.150 102 70-138
o-Xylene ug/L 47.750 95 70-130
p-Isopropyltoluene ug/L 47.350 95 70-130
Styrene ug/L 48.850 98 70-130
Tetrachloroethene ug/L 47.950 96 70-130
Toluene ug/L 48.550 97 70-130
trans-1,2-Dichloroethene ug/L 50.150 100 70-130
trans-1,3-Dichloropropene ug/L 55.550 111 70-132
Trichloroethene ug/L 49.550 99 70-130
Trichlorofluoromethane ug/L 58.850 118 62-133
Vinyl acetate ug/L 101100 101 66-157
Vinyl chloride ug/L 47.050 94 50-150
Xylene (Total)ug/L 145150 96 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 13 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1975426MATRIX SPIKE SAMPLE:
MSSpike
Result
92336366001
1,1,1,2-Tetrachloroethane ug/L 6.2 M1203170-130ND
1,1,1-Trichloroethane ug/L 8.9 M1204570-130ND
1,1,2,2-Tetrachloroethane ug/L ND M120070-130ND
1,1,2-Trichloroethane ug/L 14.920 75 70-130ND
1,1-Dichloroethane ug/L 18.720 93 70-130ND
1,1-Dichloroethene ug/L 15.220 76 70-166ND
1,1-Dichloropropene ug/L 7.3 M1203670-130ND
1,2,3-Trichlorobenzene ug/L ND M120070-130ND
1,2,3-Trichloropropane ug/L 16.620 83 70-130ND
1,2,4-Trichlorobenzene ug/L ND M120070-130ND
1,2-Dibromo-3-chloropropane ug/L ND M120070-130ND
1,2-Dibromoethane (EDB)ug/L 13.1 M1206670-130ND
1,2-Dichlorobenzene ug/L 2.2 M1201170-130ND
1,2-Dichloroethane ug/L 18.220 91 70-130ND
1,2-Dichloropropane ug/L 14.020 70 70-130ND
1,3-Dichlorobenzene ug/L 1.8 M120970-130ND
1,3-Dichloropropane ug/L 14.720 73 70-130ND
1,4-Dichlorobenzene ug/L 1.9 M120970-130ND
2,2-Dichloropropane ug/L 8.4 M1204270-130ND
2-Butanone (MEK)ug/L 48.040 114 70-130ND
2-Chlorotoluene ug/L 2.9 M1201470-130ND
2-Hexanone ug/L 42.440 106 70-130ND
4-Chlorotoluene ug/L ND M120070-130ND
4-Methyl-2-pentanone (MIBK)ug/L 46.940 117 70-130ND
Acetone ug/L 24340 119 70-130195
Benzene ug/L 17.0 M1206670-1483.8
Bromobenzene ug/L 4.6 M1202370-130ND
Bromochloromethane ug/L 21.720 109 70-130ND
Bromodichloromethane ug/L 13.6 M1206870-130ND
Bromoform ug/L 9.6 M1204870-130ND
Bromomethane ug/L 8.1 M1204170-130ND
Carbon tetrachloride ug/L 5.7 M1202870-130ND
Chlorobenzene ug/L 5.7 M1202870-146ND
Chloroethane ug/L 27.9 M12014070-130ND
Chloroform ug/L 16.720 84 70-130ND
Chloromethane ug/L 22.820 113 70-130ND
cis-1,2-Dichloroethene ug/L 18.120 91 70-130ND
cis-1,3-Dichloropropene ug/L 12.7 M1206470-130ND
Dibromochloromethane ug/L 11.0 M1205570-130ND
Dibromomethane ug/L 18.220 91 70-130ND
Dichlorodifluoromethane ug/L 16.020 80 70-130ND
Diisopropyl ether ug/L 17.820 89 70-130ND
Ethylbenzene ug/L 6.1 M1201270-1303.7
Hexachloro-1,3-butadiene ug/L 1.3 M120670-130ND
m&p-Xylene ug/L 6.7 M1401370-130ND
Methyl-tert-butyl ether ug/L 21.220 106 70-130ND
Methylene Chloride ug/L 21.120 105 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
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Huntersville, NC 28078
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Page 14 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1975426MATRIX SPIKE SAMPLE:
MSSpike
Result
92336366001
Naphthalene ug/L 25.420 -17 70-13028.7
o-Xylene ug/L 4.5 M1201170-1302.2
p-Isopropyltoluene ug/L 9.7 M1204870-130ND
Styrene ug/L 4.2 M1202170-130ND
Tetrachloroethene ug/L 2.3 M1201270-130ND
Toluene ug/L 7.3 M1203570-155ND
trans-1,2-Dichloroethene ug/L 16.020 80 70-130ND
trans-1,3-Dichloropropene ug/L 12.3 M1206270-130ND
Trichloroethene ug/L 8.2 M1204169-151ND
Trichlorofluoromethane ug/L 11.7 M1205870-130ND
Vinyl acetate ug/L 16.3 M1404170-130ND
Vinyl chloride ug/L 20.520 102 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92336255009
1975474SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 15 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92336255009
1975474SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L 0.37J 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%99 1100
4-Bromofluorobenzene (S)%95 095
Toluene-d8 (S)%114 8105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
356113
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92336532001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1975346
Associated Lab Samples:92336532001
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 04/11/17 09:591.9
1,2-Dichlorobenzene ug/L ND 10.0 04/11/17 09:591.2
1,3-Dichlorobenzene ug/L ND 10.0 04/11/17 09:591.1
1,4-Dichlorobenzene ug/L ND 10.0 04/11/17 09:591.2
1-Methylnaphthalene ug/L ND 10.0 04/11/17 09:590.32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 04/11/17 09:591.6
2,4,5-Trichlorophenol ug/L ND 10.0 04/11/17 09:592.2
2,4,6-Trichlorophenol ug/L ND 10.0 04/11/17 09:591.9
2,4-Dichlorophenol ug/L ND 10.0 04/11/17 09:591.7
2,4-Dimethylphenol ug/L ND 10.0 04/11/17 09:592.2
2,4-Dinitrophenol ug/L ND 50.0 04/11/17 09:596.5
2,4-Dinitrotoluene ug/L ND 10.0 04/11/17 09:591.2
2,6-Dinitrotoluene ug/L ND 10.0 04/11/17 09:591.7
2-Chloronaphthalene ug/L ND 10.0 04/11/17 09:592.2
2-Chlorophenol ug/L ND 10.0 04/11/17 09:591.5
2-Methylnaphthalene ug/L ND 10.0 04/11/17 09:590.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 04/11/17 09:591.7
2-Nitroaniline ug/L ND 50.0 04/11/17 09:592.8
2-Nitrophenol ug/L ND 10.0 04/11/17 09:591.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 04/11/17 09:591.7
3,3'-Dichlorobenzidine ug/L ND 20.0 04/11/17 09:591.4
3-Nitroaniline ug/L ND 50.0 04/11/17 09:592.4
4,6-Dinitro-2-methylphenol ug/L ND 20.0 04/11/17 09:591.7
4-Bromophenylphenyl ether ug/L ND 10.0 04/11/17 09:591.3
4-Chloro-3-methylphenol ug/L ND 20.0 04/11/17 09:594.2
4-Chloroaniline ug/L ND 20.0 04/11/17 09:593.4
4-Chlorophenylphenyl ether ug/L ND 10.0 04/11/17 09:592.1
4-Nitroaniline ug/L ND 20.0 04/11/17 09:592.5
4-Nitrophenol ug/L ND 50.0 04/11/17 09:595.8
Acenaphthene ug/L ND 10.0 04/11/17 09:590.25
Acenaphthylene ug/L ND 10.0 04/11/17 09:590.21
Aniline ug/L ND 10.0 04/11/17 09:591.3
Anthracene ug/L ND 10.0 04/11/17 09:590.14
Benzo(a)anthracene ug/L ND 10.0 04/11/17 09:590.33
Benzo(a)pyrene ug/L ND 10.0 04/11/17 09:590.30
Benzo(b)fluoranthene ug/L ND 10.0 04/11/17 09:590.28
Benzo(g,h,i)perylene ug/L ND 10.0 04/11/17 09:590.38
Benzo(k)fluoranthene ug/L ND 10.0 04/11/17 09:590.43
Benzoic Acid ug/L ND 50.0 04/11/17 09:5911.1
Benzyl alcohol ug/L ND 20.0 04/11/17 09:593.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/11/17 09:591.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 17 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1975346
Associated Lab Samples:92336532001
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 04/11/17 09:591.5
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 04/11/17 09:590.85
Butylbenzylphthalate ug/L ND 10.0 04/11/17 09:590.75
Chrysene ug/L ND 10.0 04/11/17 09:590.21
Di-n-butylphthalate ug/L ND 10.0 04/11/17 09:591.1
Di-n-octylphthalate ug/L ND 10.0 04/11/17 09:590.86
Dibenz(a,h)anthracene ug/L ND 10.0 04/11/17 09:590.55
Dibenzofuran ug/L ND 10.0 04/11/17 09:591.8
Diethylphthalate ug/L ND 10.0 04/11/17 09:591.3
Dimethylphthalate ug/L ND 10.0 04/11/17 09:591.5
Fluoranthene ug/L ND 10.0 04/11/17 09:590.21
Fluorene ug/L ND 10.0 04/11/17 09:590.21
Hexachloro-1,3-butadiene ug/L ND 10.0 04/11/17 09:591.8
Hexachlorobenzene ug/L ND 10.0 04/11/17 09:591.1
Hexachlorocyclopentadiene ug/L ND 10.0 04/11/17 09:591.8
Hexachloroethane ug/L ND 10.0 04/11/17 09:591.5
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 04/11/17 09:590.29
Isophorone ug/L ND 10.0 04/11/17 09:591.8
N-Nitroso-di-n-propylamine ug/L ND 10.0 04/11/17 09:592.1
N-Nitrosodimethylamine ug/L ND 10.0 04/11/17 09:591.3
N-Nitrosodiphenylamine ug/L ND 10.0 04/11/17 09:591.3
Naphthalene ug/L ND 10.0 04/11/17 09:590.34
Nitrobenzene ug/L ND 10.0 04/11/17 09:591.7
Pentachlorophenol ug/L ND 25.0 04/11/17 09:592.3
Phenanthrene ug/L ND 10.0 04/11/17 09:590.22
Phenol ug/L ND 10.0 04/11/17 09:591.7
Pyrene ug/L ND 10.0 04/11/17 09:590.19
2,4,6-Tribromophenol (S)%84 27-110 04/11/17 09:59
2-Fluorobiphenyl (S)%81 27-110 04/11/17 09:59
2-Fluorophenol (S)%38 12-110 04/11/17 09:59
Nitrobenzene-d5 (S)%76 21-110 04/11/17 09:59
Phenol-d6 (S)%25 10-110 04/11/17 09:59
Terphenyl-d14 (S)%99 31-107 04/11/17 09:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1975347LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 35.450 71 31-120
1,2-Dichlorobenzene ug/L 32.950 66 38-120
1,3-Dichlorobenzene ug/L 30.950 62 30-122
1,4-Dichlorobenzene ug/L 31.250 62 37-120
1-Methylnaphthalene ug/L 40.650 81 34-113
2,2'-Oxybis(1-chloropropane)ug/L 37.450 75 18-120
2,4,5-Trichlorophenol ug/L 39.650 79 43-113
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1975347LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 45.650 91 42-120
2,4-Dichlorophenol ug/L 45.050 90 30-120
2,4-Dimethylphenol ug/L 46.250 92 29-111
2,4-Dinitrophenol ug/L 221250 88 19-132
2,4-Dinitrotoluene ug/L 54.150 108 58-128
2,6-Dinitrotoluene ug/L 55.750 111 54-129
2-Chloronaphthalene ug/L 48.150 96 43-117
2-Chlorophenol ug/L 39.550 79 37-120
2-Methylnaphthalene ug/L 43.050 86 33-120
2-Methylphenol(o-Cresol)ug/L 32.950 66 31-120
2-Nitroaniline ug/L 79.3100 79 48-121
2-Nitrophenol ug/L 42.450 85 25-116
3&4-Methylphenol(m&p Cresol)ug/L 70.2 L15014023-120
3,3'-Dichlorobenzidine ug/L 86.3100 86 10-154
3-Nitroaniline ug/L 92.7100 93 43-115
4,6-Dinitro-2-methylphenol ug/L 85.6100 86 44-124
4-Bromophenylphenyl ether ug/L 42.650 85 34-113
4-Chloro-3-methylphenol ug/L 90.3100 90 31-110
4-Chloroaniline ug/L 86.3100 86 20-120
4-Chlorophenylphenyl ether ug/L 43.350 87 34-116
4-Nitroaniline ug/L 96.0100 96 46-128
4-Nitrophenol ug/L 101250 40 11-120
Acenaphthene ug/L 43.850 88 48-114
Acenaphthylene ug/L 42.750 85 48-112
Aniline ug/L 28.650 57 26-120
Anthracene ug/L 43.650 87 57-118
Benzo(a)anthracene ug/L 44.950 90 56-121
Benzo(a)pyrene ug/L 44.550 89 55-127
Benzo(b)fluoranthene ug/L 45.750 91 53-128
Benzo(g,h,i)perylene ug/L 45.950 92 54-125
Benzo(k)fluoranthene ug/L 46.050 92 51-123
Benzoic Acid ug/L 95.3250 38 10-120
Benzyl alcohol ug/L 74.1100 74 27-120
bis(2-Chloroethoxy)methane ug/L 42.350 85 32-120
bis(2-Chloroethyl) ether ug/L 40.450 81 33-111
bis(2-Ethylhexyl)phthalate ug/L 53.350 107 50-145
Butylbenzylphthalate ug/L 54.150 108 54-138
Chrysene ug/L 43.750 87 58-127
Di-n-butylphthalate ug/L 50.150 100 56-125
Di-n-octylphthalate ug/L 51.650 103 50-134
Dibenz(a,h)anthracene ug/L 45.050 90 53-129
Dibenzofuran ug/L 44.550 89 45-120
Diethylphthalate ug/L 48.250 96 53-120
Dimethylphthalate ug/L 47.750 95 55-116
Fluoranthene ug/L 44.950 90 57-125
Fluorene ug/L 44.650 89 53-118
Hexachloro-1,3-butadiene ug/L 32.150 64 23-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1975347LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 42.550 85 49-116
Hexachlorocyclopentadiene ug/L 32.250 64 26-158
Hexachloroethane ug/L 29.150 58 30-114
Indeno(1,2,3-cd)pyrene ug/L 46.250 92 55-128
Isophorone ug/L 49.950 100 31-118
N-Nitroso-di-n-propylamine ug/L 45.950 92 32-119
N-Nitrosodimethylamine ug/L 25.250 50 13-120
N-Nitrosodiphenylamine ug/L 43.350 87 43-120
Naphthalene ug/L 38.450 77 32-120
Nitrobenzene ug/L 43.550 87 33-110
Pentachlorophenol ug/L 87.1100 87 10-137
Phenanthrene ug/L 42.750 85 57-117
Phenol ug/L 19.150 38 10-120
Pyrene ug/L 44.950 90 55-122
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%80 27-110
2-Fluorophenol (S)%46 12-110
Nitrobenzene-d5 (S)%79 21-110
Phenol-d6 (S)%35 10-110
Terphenyl-d14 (S)%95 31-107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 25
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was received or analysis requested beyond the recognized method holding time.H3
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 25
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92336532
HIGHLAND PARK MILL 71167505
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92336532001 356085 356248SUMP-1 EPA 3010A EPA 6010
92336532001 356246 356286SUMP-1 EPA 7470 EPA 7470
92336532001 356113 356161SUMP-1 EPA 3510 EPA 8270
92336532001 355922SUMP-1 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/13/2017 04:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 25
Page 23 of 25
Page 24 of 25
Page 25 of 25
EMSL Analytical, Inc.
376 Crompton Street Charlotte, NC 28273
Tel/Fax: [phone]
http://www.EMSL.com / [e-mail]
411707500EMSL Order:
Customer ID:TITA52
Customer PO:
Project ID:
Attention:Phone:Alex Manzanarez [phone]
Fax:Terracon Consultants, Inc.[phone]
Received Date:2020 Starita Road 09/28/2017 4:15 PM
Analysis Date:Suite E 09/29/2017
Collected Date:Charlotte, NC 28206 09/28/2017
Project:340 E. 16th Street
Test Report: Asbestos Analysis of Bulk Materials via EPA 600/R-93/116 Method using Polarized
Light Microscopy
Sample Description Appearance % Fibrous % Non-Fibrous
Non-Asbestos Asbestos
% Type
1-1
411707500-0001
2%ChrysotileNon-fibrous (Other)83%Cellulose15%Black
Fibrous
Heterogeneous
Roof 1 - Membrane
1-2
411707500-0002
5%ChrysotileNon-fibrous (Other)65%Cellulose30%Black
Fibrous
Heterogeneous
Roof 1 - Membrane
1-3
411707500-0003
None DetectedNon-fibrous (Other)92%Cellulose8%Black
Fibrous
Homogeneous
Roof 1 - Membrane
2-1
411707500-0004
None DetectedCa Carbonate
Non-fibrous (Other)
5%
95%
Black
Non-Fibrous
Homogeneous
Roof 2 - Rubber
2-2
411707500-0005
None DetectedCa Carbonate
Non-fibrous (Other)
5%
95%
Black
Non-Fibrous
Homogeneous
Roof 2 - Rubber
2-3
411707500-0006
None DetectedNon-fibrous (Other)100%Cellulose<1%Black
Fibrous
Homogeneous
Roof 2 - Rubber
3-1-Roofing
411707500-0007
None DetectedQuartz
Non-fibrous (Other)
15%
75%
Cellulose10%Black
Fibrous
Heterogeneous
Roof 3 - Membrane
3-1-Brown Layer
411707500-0007A
None DetectedNon-fibrous (Other)100%Cellulose<1%Brown
Non-Fibrous
Homogeneous
Roof 3 - Membrane
3-1-Insulation
411707500-0007B
None DetectedNon-fibrous (Other)1%Cellulose99%Brown
Non-Fibrous
Homogeneous
Roof 3 - Membrane
3-2-Roofing
411707500-0008
None DetectedQuartz
Non-fibrous (Other)
15%
75%
Cellulose10%Black
Non-Fibrous
Homogeneous
Roof 3 - Membrane
3-2-Brown Layer
411707500-0008A
None DetectedNon-fibrous (Other)99%Cellulose1%Brown
Non-Fibrous
Homogeneous
Roof 3 - Membrane
3-2-Insulation
411707500-0008B
None DetectedCellulose100%Brown
Non-Fibrous
Homogeneous
Roof 3 - Membrane
3-3-Roofing
411707500-0009
None DetectedNon-fibrous (Other)92%Cellulose8%Black
Fibrous
Homogeneous
Roof 3 - Membrane
3-3-Brown Layer
411707500-0009A
None DetectedNon-fibrous (Other)99%Cellulose1%Brown
Fibrous
Homogeneous
Roof 3 - Membrane
3-3-Insulation
411707500-0009B
None DetectedNon-fibrous (Other)1%Cellulose99%Brown
Fibrous
Homogeneous
Roof 3 - Membrane
4-1-Roofing
411707500-0010
None DetectedNon-fibrous (Other)93%Cellulose
Glass
2%
5%
Black
Non-Fibrous
Homogeneous
Roof 4 - Membrane
Initial report from: 09/29/2017 11:19:25
Page 1 of 3ASB_PLM_0008_0001 - 1.78 Printed: 9/29/2017 11:19 AM
EMSL Analytical, Inc.
376 Crompton Street Charlotte, NC 28273
Tel/Fax: [phone]
http://www.EMSL.com / [e-mail]
411707500EMSL Order:
Customer ID:TITA52
Customer PO:
Project ID:
Test Report: Asbestos Analysis of Bulk Materials via EPA 600/R-93/116 Method using Polarized
Light Microscopy
Sample Description Appearance % Fibrous % Non-Fibrous
Non-Asbestos Asbestos
% Type
4-1-Insulation
411707500-0010A
None DetectedNon-fibrous (Other)1%Cellulose99%Tan
Fibrous
Homogeneous
Roof 4 - Membrane
4-2-Roofing
411707500-0011
None DetectedNon-fibrous (Other)93%Cellulose
Glass
5%
2%
Black
Fibrous
Heterogeneous
Roof 4 - Membrane
4-2-Insulation
411707500-0011A
None DetectedNon-fibrous (Other)1%Cellulose99%Brown
Fibrous
Homogeneous
Roof 4 - Membrane
4-3-Roofing
411707500-0012
None DetectedNon-fibrous (Other)91%Cellulose
Glass
4%
5%
Black
Fibrous
Homogeneous
Roof 4 - Membrane
4-3-Insulation
411707500-0012A
None DetectedNon-fibrous (Other)1%Cellulose99%Tan
Fibrous
Homogeneous
Roof 4 - Membrane
5-1
411707500-0013
None DetectedCa Carbonate
Non-fibrous (Other)
5%
95%
Black
Non-Fibrous
Homogeneous
Roof 5 - Rubber
5-2
411707500-0014
None DetectedNon-fibrous (Other)100%Black
Non-Fibrous
Homogeneous
Roof 5 - Rubber
5-3
411707500-0015
None DetectedNon-fibrous (Other)100%Cellulose<1%Black
Fibrous
Homogeneous
Roof 5 - Rubber
6-1-Roofing
411707500-0016
None DetectedQuartz
Non-fibrous (Other)
10%
82%
Cellulose8%Gray/Black
Non-Fibrous
Homogeneous
Roof 6 - Membrane
6-1-Insulation
411707500-0016A
None DetectedNon-fibrous (Other)1%Cellulose99%Brown
Fibrous
Homogeneous
Roof 6 - Membrane
6-2-Roofing
411707500-0017
None DetectedQuartz
Non-fibrous (Other)
10%
79%
Cellulose
Glass
8%
3%
Black
Non-Fibrous
Homogeneous
Roof 6 - Membrane
6-2-Insulation
411707500-0017A
None DetectedNon-fibrous (Other)1%Cellulose99%Tan
Fibrous
Homogeneous
Roof 6 - Membrane
6-3-Roofing
411707500-0018
None DetectedQuartz
Non-fibrous (Other)
5%
91%
Cellulose4%Black
Fibrous
Homogeneous
Roof 6 - Membrane
6-3-Insulation
411707500-0018A
None DetectedNon-fibrous (Other)1%Cellulose99%Brown
Fibrous
Homogeneous
Roof 6 - Membrane
6-4
411707500-0019
3%ChrysotileNon-fibrous (Other)82%Cellulose15%Black
Fibrous
Homogeneous
Roof 6 - Silver
Flashing
6-5
411707500-0020
4%ChrysotileNon-fibrous (Other)85%Cellulose
Glass
3%
8%
Black
Non-Fibrous
Homogeneous
Roof 6 - Silver
Flashing
6-6
411707500-0021
4%ChrysotileNon-fibrous (Other)91%Cellulose
Glass
3%
2%
Black
Non-Fibrous
Homogeneous
Roof 6 - Silver
Flashing
Initial report from: 09/29/2017 11:19:25
Page 2 of 3ASB_PLM_0008_0001 - 1.78 Printed: 9/29/2017 11:19 AM
EMSL Analytical, Inc.
376 Crompton Street Charlotte, NC 28273
Tel/Fax: [phone]
http://www.EMSL.com / [e-mail]
411707500EMSL Order:
Customer ID:TITA52
Customer PO:
Project ID:
Analyst(s)
Eric Loomis (22)
Lacy Searcy (11)
Lee Plumley, Laboratory Manager
or Other Approved Signatory
EMSL maintains liability limited to cost of analysis. This report relates only to the samples reported and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no
responsibility for sample collection activities or analytical method limitations. Interpretation and use of test results are the responsibility of the client. This report must not be used by the client to claim
product certification, approval, or endorsement by NVLAP, NIST or any agency of the federal government. Non-friable organically bound materials present a problem matrix and therefore EMSL
recommends gravimetric reduction prior to analysis. Samples received in good condition unless otherwise noted. Estimated accuracy, precision and uncertainty data available upon request. Unless
requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample. Reporting limit is 1%
Samples analyzed by EMSL Analytical, Inc. Charlotte, NC NVLAP Lab Code 200841-0, VA 3333 00312
Initial report from: 09/29/2017 11:19:25
Page 3 of 3ASB_PLM_0008_0001 - 1.78 Printed: 9/29/2017 11:19 AM
OrderID: 411707500
Page 1 Of 2
OrderID: 411707500
Page 2 Of 2