RA-1929_11818_CA_MRP_20200212

Groundwater Monitoring Report

Mayo’s Grocery
Incident #11818
416 US Highway 301
Garysburg, Northampton County, North Carolina
ATC Project No. SLP1181805

February 12, 2020

TABLE OF CONTENTS

1.0 SITE IDENTIFICATION .......................................................................................1
2.0 EXECUTIVE SUMMARY .....................................................................................2
3.0 SITE DESCRIPTION .............................................................................................3
3.1 Site Characterization ................................................................................3
3.2 Site Background .......................................................................................3
4.0 GROUNDWATER CHARACTERIZATION.......................................................6
4.1 Groundwater Levels .................................................................................6
4.2 Groundwater Quality ...............................................................................6
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................8

TABLES
Table 1 Water Supply Well Information
Table 2 Well Construction and Groundwater Elevation Data
Table 3 Groundwater Analytical Results
Table 4 Historical Groundwater Analytical Results
Table 5 Natural Attenuation Parameters

FIGURES
Figure 1 Site Topographic Map
Figure 2 Site Map
Figure 3 Potential Receptor Map
Figure 4 Groundwater Elevation Contour Map
Figure 5 Dissolved Benzene Isoconcentration Contour Map
Figure 6 Additional Chemicals of Concern

APPENDICES
Appendix A Field Notes
Appendix B Laboratory Analytical Results
Appendix C Mann-Kendall Analyses

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2.0 EXECUTIVE SUMMARY

ATC Associates of North Carolina, P.C. (ATC) has completed a Groundwater Monitoring Report
for the former Mayo’s Grocery. This report documents the groundwater sampling event conducted
at the site in November 2019. The activities were performed based on a October 24, 2019, Task
Authorization (TA-05) by the Trust Fund Branch of the Underground Storage Tank (UST) Section,
Division of Waste Management, North Carolina Department of Environmental Quality (NCDEQ).
The work is being performed as part of State Lead Contract #N17004 between NCDEQ and ATC.

The former Mayo’s Grocery is located at 416 US Highway 301 in Garysburg, Northampton
County, North Carolina. The site consists of one vacant single-story building. Ten monitoring
wells (MW-2 through MW-11) are located at the site. Twenty-eight water supply wells are
identified within 1,000 feet of the site. One water supply well is abandoned (on-site well), eight
wells are inactive, and 19 wells have an unknown use. Of the 19 properties with water supply wells
with unknown use, 17 of those properties are connected to a municipal water supply. Municipal
water is available to the site and vicinity.

On November 11, 2019 and November 20, 2019, ATC personnel mobilized to the site to collect
groundwater samples and measure groundwater elevations for monitoring wells MW-2, MW-3,
MW-4, MW-5, MW-6, MW-7, MW-8, MW-9, MW-10, and MW-11. Laboratory analytical results
of the November 2019 sampling event indicated petroleum hydrocarbon compounds at
concentrations exceeding North Carolina Groundwater Quality Standards (2L Standards) in
monitoring well MW-2, MW-4, MW-5, MW-9, and MW-10. Compounds exceeding 2L Standards
include benzene, naphthalene, 1,2-dichloroethane, n-propylbenzene, hexachlorobutadiene, and
1,2,3-trichloropropane. With the exception of hexachlorobutadiene and 1,2,3-trichloropropane,
these compounds have historically been detected above the 2L Standards.

ATC recommends sampling monitoring wells MW-2, MW-7, MW-9, and MW-10 in May 2020
to monitor the concentrations trends in these wells. In addition, ATC recommends replacing the
ORS sleeves since they appear to be effective. ATC also recommends confirming the usage of
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water supply wells WSW-11 and WSW-27, the two water supply wells where the properties are
not connected to the municipal water supply.

3.0 SITE DESCRIPTION

3.1 Site Characterization
The former Mayo’s Grocery is located at 416 US Highway 301 in Garysburg, North Carolina.
Currently, one vacant single-story building exists on-site. The vacant building was a former
automobile service station and repair facility that operated four USTs. The former UST system
consisted of one 5,000-gallon gasoline UST, one 4,000-gallon gasoline UST, one 2,000-gallon
gasoline UST, and one 1,000-gallon kerosene UST. The UST system was removed from the site in
March 1996. The site is bound by US 301 Highway to the west, NC 186 Highway to the east, and
by a vacant lot to the north. Surrounding properties are characterized by residential and agricultural
use. A site topographic map is included as Figure 1 and a site map with pertinent site features is
included as Figure 2.

3.2 Site Background
A potable water supply well (Well #1) located approximately 450 feet north of the site, which
provided water to approximately 600 residences, was sampled on October 21, 1993. The
groundwater sample contained detections above standards causing the well to be shut-down. On
December 21, 1993, the Mayo’s Grocery UST owner submitted a letter to North Carolina
Department of Environment, Health, and Natural Resources (NCDEHNR) asking for assistance
in removing the tanks from Mayo’s Grocery Property. Due to the contaminated water-supply
well, the site was ranked “High” priority and was accepted into the Federal Trust Fund (FTF)
program on March 4, 1994.

Investigative activities were first conducted at the site by Geophex, Ltd. (Geophex) in August
1995. Geophex advanced two borings adjacent to the two previously identified USTs. In October
1995, Geophex conducted a geophysical survey to locate and determine the size of existing
USTs. Between November 1995 and April 1996, Geophex performed soil and groundwater
delineation by advancing eighteen soil borings to depths ranging from 15 to 23 feet, and installed
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eight monitoring wells (MW-1 through MW-8). Analytical results of the groundwater samples
collected identified the largest concentration of benzene, toluene, ethylbenzene, and total xylenes
(BTEX) in monitoring well MW-4 (approximately 20 feet northwest of the kerosene tank [Tank
4]). The UST system was permanently removed from the site on March 26-27, 1996. Soil
samples collected during the closure activities indicated the UST basins of Tanks 1 and 4 were
impacted with petroleum products above the Soil-to-Groundwater Maximum Soil Contaminant
Concentrations (MSCCs). The UST closure activities are documented in a UST Closure Report
dated May 23, 1996. In association with the UST system removal, approximately 40 cubic yards
of impacted soil was removed from the site.

In March 1999, Geophex collected groundwater samples from six of the eight monitoring wells
and found similar detections of BTEX in comparison to their previous sampling event in 1996.
The greatest concentration of BTEX was identified in monitoring wells MW-2 and MW-4.

In 2007, the property was leased out to a small construction company for equipment storage. In
November 2007 Groundwater Management Associates, Inc. (GMA) installed a temporary
monitoring well (TMW-1) and sampled monitoring wells MW-2 and MW-3. Note that
monitoring well MW-1 could not be located and was assumed to be destroyed. Laboratory
analytical results determined that all wells had petroleum-related compounds exceeding the 2L
Standards.

On December 18, 2014, a Groundwater Monitoring Report was submitted for the site
documenting an updated receptor survey and monitoring event. The receptor survey indicated up
to three drinking water supply wells within 1,000 feet of the site. Water supply well information
and locations are included on Table 1 and Figure 3, respectively. Results from the groundwater
monitoring event indicated petroleum impact in monitoring wells MW-2, MW-4, and MW-7
above the 2L Standards. Based on the findings, ATC recommended connecting properties
located within 1,000 feet of the site with potable wells to a municipal water supply. In addition,
ATC recommended delineating the groundwater plume.

On November 9, 2015, a Groundwater Monitoring Report was submitted for the site
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documenting the installation of three monitoring wells and subsequent monitoring event.
Results from the groundwater monitoring event indicated impact in monitoring wells MW-2,
MW-9, and MW-10 above the 2L Standards.

On December 19, 2017, ATC submitted a Groundwater Monitoring Report documenting a
groundwater sampling event conducted for monitoring wells MW-2, MW-3, MW-4, MW-7, MW-
8, MW-9, MW-10, and MW-11 which was conducted in September 2017. Monitoring well MW-5
was dry and MW-6 could not be located at the time of sampling. Results from the groundwater
monitoring event indicated impact in monitoring wells MW-2, MW-7, MW-9, and MW-10
above the 2L Standards. ATC recommended installing ORS sleeves in monitoring wells MW-2,
MW-7, MW-9, and MW-10 to aide in natural attenuation at the site. ATC also recommended a
groundwater sampling event be performed six months following sleeve installation.

On January 11, 2018, ATC installed ORS sleeves in monitoring wells MW-2, MW-7, MW-9,
and MW-10.

On August 30, 2018, ATC submitted a Groundwater Monitoring Report documenting a
groundwater sampling event conducted for monitoring wells MW-2, MW-7, MW-9, and MW-10
which was conducted in July 2018. Results from the groundwater monitoring event indicated
impact in monitoring wells MW-2, MW-7, and MW-9 above the 2L Standards. ATC
recommended replacing the ORS sleeves in monitoring wells MW-2, MW-7, and MW-9. ATC
also recommended a groundwater sampling event be performed six months following sleeve
installation.

On June 4, 2019, ATC submitted a Groundwater Monitoring Report documenting a groundwater
sampling event conducted for monitoring wells MW-2, MW-4, MW-7, MW-8, MW-9, and MW-
10 which was conducted in May 2019. Results from the groundwater monitoring event indicated
impact in monitoring wells MW-2, MW-4, MW-7, MW-9, and MW-10 above the 2L Standards.
Following the completion of the sampling event, new ORS sleeves were installed into MW-2,
MW-7, and MW-9.

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This report documents the results of the November 2019 groundwater monitoring event.

4.0 GROUNDWATER CHARACTERIZATION

4.1 Groundwater Levels
Groundwater level measurements were collected from monitoring wells MW-2, MW-3, MW-4,
MW-5, MW-6, MW-7, MW-8, MW-9, MW-10, and MW-11 on November 11, 2019. Monitoring
well construction details and current and historical groundwater elevation data are summarized in
Table 2. Light non-aqueous phase liquid (LNAPL) was not observed in any of the monitoring wells
that were gauged. Depth to groundwater measurements ranged from 6.61 feet below ground surface
(bgs) in MW-6 to 12.19 feet bgs in MW-3. A groundwater elevation contour map generated using
the November 2019 groundwater elevation data is included as Figure 4. This figure indicates that
the direction of groundwater flow at the site is to the northwest which is generally consistent with
historical data. Field notes from the November 11, 2019 and November 20, 2019, site visit are
included in Appendix A.

4.2 Groundwater Quality
On November 11, 2019, groundwater samples were collected from monitoring wells MW-2, MW-3,
MW-4, MW-5, MW-6, MW-7, MW-8, MW-9, MW-10, and MW-11. The laboratory containers
for monitoring well MW-5 were damaged upon receipt by the laboratory; therefore, MW-5 was
re-sampled on November 20, 2019. Samples were collected in laboratory-approved containers,
packed in ice and delivered under chain-of-custody protocol to SGS North America Inc., in
Scott, Louisiana for analyses. Groundwater samples were analyzed for volatile organic
compounds (VOCs) by Environmental Protection Agency (EPA) Method 6200B. Following the
completion of the sampling event, the ORS sleeves were placed back into MW-2, MW-7, and
MW-9.

The laboratory analytical results indicated the presence of petroleum hydrocarbon compounds at
concentrations above 2L Standards as follows:

 Benzene – MW-2, MW-9, and MW-10
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 Naphthalene – MW-10
 1,2-Dichloroethane – MW-2
 n-Propylbenzene –MW-4
 Hexachlorobutadiene – MW-5
 1,2,3-Trichloropropane – MW-10

Concentrations did not exceed the respective Gross Contaminant Levels (GCLs). Current
groundwater analytical data are summarized in Table 3 and historical groundwater analytical
data is summarized in Table 4. An isoconcentration contour map for benzene is included as
Figure 5. An additional chemicals of concern in groundwater map is included as Figure 6. The
laboratory analytical report and chain-of-custody forms are included in Appendix B. Natural
attenuation parameters collected during the sampling event are summarized in Table 5.

Since installation of the ORS sleeves, concentrations of key compounds have decreased in MW-
2. Concentration trends in MW-7 varied as benzene had decreased while naphthalene exhibits no
trend; however, the naphthalene concentration was below the 2L Standard during the November
2019 sampling event. Concentration trends in MW-9 indicates benzene exhibits no trend while
total xylenes and naphthalene concentrations are decreasing and below the 2L Standard during
the November 2019 sampling event. No concentration trends were identified for MW-10.
Concentration versus time graphs are included in Appendix C. Overall, the ORS sleeves appear
effective at the site.

As part of ATC’s quality assurance and quality control (QA and QC) measures, a data review of
the laboratory report was conducted. During the review, it was concluded that samples were
received by the laboratory in acceptable condition and properly preserved. The samples were
analyzed within the correct holding times, and the chain of custody was properly completed by
all parties. The laboratory QC report shows an internal blank was analyzed for each method that
was used for the original samples. The laboratory fortified blank (LFB) and laboratory control
sample (LCS) data results were also provided for each analytical method. Refer to the laboratory
report in Appendix B for details regarding QA results for the laboratory samples and any noted
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exceptions. Overall, ATC concludes that the laboratory results are usable and any exceptions do
not significantly impact the conclusions presented in this report.

5.0 CONCLUSIONS AND RECOMMENDATIONS

On behalf of the Trust Fund Branch of the UST Section, ATC has completed a Groundwater
Monitoring Report documenting the November 2019 groundwater sampling activities at the
Mayo’s Grocery Property, located at 416 US Highway 301 in Garysburg, Northampton County,
North Carolina. Results from the groundwater monitoring event indicate impact in monitoring
wells MW-2, MW-4, MW-5, MW-9, and MW-10 above the 2L Standards. Based on the results,
the groundwater plume is not delineated to the west of monitoring well MW-9 and the north of
monitoring well MW-10.

ATC recommends sampling monitoring wells MW-2, MW-7, MW-9, and MW-10 in May 2020
to monitor the concentrations trends in these wells. In addition, ATC recommends replacing the
ORS sleeves since they appear to be effective. ATC also recommends confirming the usage of
water supply wells WSW-11 and WSW-27, the two water supply wells where the properties are
not connected to the municipal water supply.

TABLES
TABLE 1
WATER SUPPLY WELL INFORMATION
Mayo's Grocery
416 U.S. Highway 301
Garysburg, North Carolina
Incident #11818
Water Supply Well ID Well Map ID for Figure 3 Property Owner(s)Property Address Distance from Source
and Direction
Connected to
Municipal Water Usage
2824 1
W A Buffalo Heirs
PO Box 43
Garysburg, NC 27831
252-529-3292
416 US 301 Highway 73 feet Northeast No-
Site is vacant Abandoned
4197 2
Northampton County Utilties
PO Box 68
Jackson, NC 27845
Jason Morris - 252-534-6314 ext 307
NC 186 Highway 530 feet Northeast
No-
No structure on
property
Inactive
0154 3
Viola Boone
PO Box 154
Garysburg, NC 27831
B.J. (Daughter) - 363-536-4334
501 US 301 Highway 429 feet Northwest Yes Inactive
9136 4
Lonnie and Pattie Grant
2021 Valley Court
Clayton, NC 27520
100 Maple Street 530 feet Northwest Yes Unknown
7129 5
Joyce and Edward Davis
PO Box 742
Garysburg, NC 27831
106 Maple Street 680 feet Northwest Yes Unknown
5222 6
Inez Faison Heirs
202 Maple Street
Garysburg, NC 27831
202 Maple Street 825 feet Northwest Yes Unknown
5867 7
John and Jerry Edmonds
321 Eastern Parkway
Neward, New Jersy 07106
200 Elm Street 635 feet West Yes Unknown
7825 8
Theodore Bynum Heirs
PO Box 434
Halifax, NC 27839
104 Elm Street
(Parcel ID 4928-36-7825)480 feet West Yes Unknown
8979 9
William and Sarah Vassor
PO Box 187
Garysburg, NC 27831
101 Maple Street 410 feet Northwest Yes Unknown
0929 10
James Boone
3514 Wylie Meadow Lane
Charlotte, NC 28269
B.J. (Sister) - 363-536-4334
419 US 301 Highway 330 feet Northwest Yes Inactive
9654 11
David and Annie Belle
PO Box 1375
Knightdale, NC 27545
409 US 301 Highway 270 feet West No Unknown
8626 12
James Garner
Po Box 2097
Hempstead, NY 11551
101 Elm Street 360 feet West Yes Inactive
3753 13
Cynthia Fenner
PO Box 424
Enfield, NC 27823
252-308-3158
207 Elm Street 815 feet West Yes Inactive
3658 14
Lann't Juan Clanton
PO Box 893
Garysburg, NC 27831
202 Bush Street 845 feet West Yes Unknown
8392 15
Pattie Kee
PO Box 19
Garysburg, NC 27831
315 US 301 Highway 530 feet Southwest Yes Unknown
5386 16
W.W. and Annie Harding
PO Box 214
Garysburg, NC 27831
109 Bush Street 635 feet Southwest Yes Unknown
7187 17
Curtis and Mertice Smith
PO Box 98
Garysburg, NC 27831
100 Pine Street 620 feet Southwest Yes Unknown
4263 18
Dorothy Johnson
305 Holmes Drive
Weldon, NC 27890
110 Pine Street 900 feet Southwest Yes Inactive
3255 19
Brittany and Denae Rogers
13211 Longwood Drive
Culpeper, VA 22701
200 Pine Street 930 feet Southwest Yes Unknown
2285 20
C.W. Counseling Services
608-B Jackson Street
Roanoke Rapids, NC 27870
202 Pine Street 1,000 feet Southwest Yes Unknown
Notes:
1. * = Property address not supplied by Northampton County NC GIS, therefore unable to determine if there is an active water account.
Page 1 of 2
TABLE 1
WATER SUPPLY WELL INFORMATION
Mayo's Grocery
416 U.S. Highway 301
Garysburg, North Carolina
Incident #11818
Water Supply Well ID Well Map ID for Figure 3 Property Owner(s)Property Address Distance from Source
and Direction
Connected to
Municipal Water Usage
8010 21
Lester and Lillie Greenwood
PO Box 173
Garysburg, NC 27831
252-536-4307
207 US 301 Highway 800 feet Southwest Yes
Inactive - owner
claims no well on
property
7001 22
Eula Robinson
1553 Abbotston Street
Baltimore, MD 21218
101 Pine Street 905 feet Southwest Yes Unknown
5083 23
Evelyn Moody
1496 Carolina Rest Home Road
Roanoke Rapids, NC 27870
105 Pine Street 900 feet Southwest Yes Unknown
4065 24
Lenora Vick
109 Pine Street
Garysburg, NC 27831
109 Pine Street 935 feet Southwest Yes Unknown
4014 25
Jamiann Bazemore
PO Box 923
Seaboard, NC 27876
111 Pine Street 970 feet Southwest Yes Unknown
6573 26
Julia Boone
PO Box 685
Garysburg, NC 27831
252-536-2647
108 Bush Street 530 feet Southwest Yes Inactive
9884 27
Mack and Robin Bennett
Street Address Not Provided
Drumor, PA 17518
415 US 301 Highway 220 feet West No Unknown
9504 28
William Rice
PO Box 195
Garysburg, NC 27831
403 US Highway 301 380 feet Southwest Yes Unknown
Notes:
1. * = Property address not supplied by Northampton County NC GIS, therefore unable to determine if there is an active water account.
Page 2 of 2
TABLE 2
WELL CONSTRUCTION AND
GROUNDWATER ELEVATION DATA
Mayo's Grocery
416 U.S. Highway 301
Garysburg, North Carolina
Incident #11818
2/13/1996 3.96 96.14
2/28/1996 4.17 95.93
TMW-1
11/29/07
(abandoned
11/30/07)
6.5 6.5-21.5 21.5 103.39 TMW-1 16.45 86.94
2/13/1996 3.76 95.26
2/28/1996 3.87 95.15
4/26/1996 5.34 93.68
5/6/1996 4.56 94.46
3/8/1999 6.16 92.86
11/30/2007 12.65 86.37
12/18/2014 5.54 93.48
9/10/2015 11.31 87.71
9/20/2017 9.46 89.56
7/9/2018 8.36 90.66
5/10/2019 6.58 92.44
11/11/2019 12.11 86.91
2/13/1996 7.30 91.88
2/28/1996 6.93 92.25
4/26/1996 7.77 91.41
5/6/1996 7.97 91.21
3/8/1999 8.82 90.36
11/30/2007 14.63 84.55
12/18/2014
9/20/2017 11.90 87.28
5/10/2019
11/11/2019 12.19 86.99
4/26/1996 3.61 95.81
5/6/1996 3.45 95.97
3/8/1999 3.55 95.87
11/30/2007 Dry Dry
12/18/2014 4.13 95.29
9/10/2015 Dry Dry
9/20/2017 7.96 91.46
5/10/2019 5.22 94.20
11/11/2019 7.88 91.54
4/26/1996 4.25 95.16
5/6/1996 4.40 95.01
3/8/1999 4.45 94.96
11/30/2007 Dry Dry
12/18/2014
9/20/2017 Dry Dry
5/10/2019
11/11/2019 6.90 92.51
4/26/1996 3.59 94.34
5/6/1996 3.80 94.13
3/8/1999 3.90 94.03
11/30/2007 7.58 90.35
12/18/2014
9/20/2017
5/10/2019
11/11/2019 6.61 91.32
Notes:
3. NM = Not Measured
Screened
Interval
Bottom
of Well
171/23/1996
Well
Casing
Depth
3-8
22 100.1017-22
Top of Casing
Elevation (feet)
19-24 24
Assumed Destroyed
Groundwater
Elevation
(feet)
Well ID Date Installed
MW-1
Date
Measured
Depth to
Water
(feet)
MW-6
99.18
MW-2 1/23/1996
Could Not Locate
MW-3 1/23/1996 19
3.5-8.5
3-10
4/3/1996
Could Not Locate
8 97.93
10
Could Not Locate
Could Not Locate
4/3/1996 3
Could Not Locate
Could Not Locate
8.5 99.41
2. TOC Elevations for monitoring well MW-1 was surveyed by Geophex in 1996; MW-2, MW-3, MW-4, MW-5, MW-6, MW-7, and MW-8 was surveyed by GMA in 2007;
MW-9, MW-10, and MW-11 were surveyed on 9/10/15.
15 15-22 22 99.02
99.42
4/3/1996MW-5
MW-4
3
1. TOC = Top of casing
3.5
Could Not Locate
TABLE 2
WELL CONSTRUCTION AND
GROUNDWATER ELEVATION DATA
Mayo's Grocery
416 U.S. Highway 301
Garysburg, North Carolina
Incident #11818
Screened
Interval
Bottom
of Well
Well
Casing
Depth
Top of Casing
Elevation (feet)
Groundwater
Elevation
(feet)
Well ID Date Installed Date
Measured
Depth to
Water
(feet)
4/26/1996 4.17 95.18
5/6/1996 4.22 95.13
3/8/1999 4.20 95.15
11/30/2007 Dry Dry
12/18/2014 4.60 94.75
9/10/2015 Dry Dry
9/20/2017 8.50 90.85
7/9/2018 6.12 93.23
5/10/2019 5.53 93.82
11/11/2019 7.70 91.65
5/6/1996 3.40 96.60
3/8/1999 NM NM
11/30/2007 8.24 91.76
12/18/2014 4.14 95.86
9/10/2015 Dry Dry
9/20/2017 6.89 93.11
5/10/2019 4.14 95.86
11/11/2019 7.08 92.92
9/10/2015 10.57 88.51
9/20/2017 9.57 89.51
7/9/2018 6.90 92.18
5/10/2019 6.55 92.53
11/11/2019 8.88 90.20
9/10/2015 10.66 88.11
9/20/2017 8.66 90.11
7/9/2018 6.50 92.27
5/10/2019 5.93 92.84
11/11/2019 8.05 90.72
9/10/2015 13.71 86.08
9/20/2017 11.78 88.01
5/10/2019
11/11/2019 11.85 87.94
Notes:
3. NM = Not Measured
MW-8
4/3/1996 3.5
MW-10 5-15 15
4/3/1996 3
59/4/2015
1. TOC = Top of casing
MW-7
MW-11 9/4/2015 5 5-15
2. TOC Elevations for monitoring well MW-1 was surveyed by Geophex in 1996; MW-2, MW-3, MW-4, MW-5, MW-6, MW-7, and MW-8 was surveyed by GMA in 2007;
MW-9, MW-10, and MW-11 were surveyed on 9/10/15.
9/4/2015 5 5-15 15 99.08MW-9
Could Not Locate
99.35
100.008.33-8
3.5-8.5
99.79
98.77
8.5
15
TABLE 3
GROUNDWATER ANALYTICAL RESULTS
Mayo's Grocery
416 U.S. Highway 301
Garysburg, North Carolina
Incident #11818

Well ID Sample Date
BenzeneTolueneEthylbenzeneTotal XylenesMTBENaphthaleneDiisopropyl Ethern-Butylbenzenesec-Butylbenzenetert-ButylbenzeneIsopropylbenzenep-Isopropyltoluene1,2-DichloroethaneHexachlorobutdienen-Propylbenzene1,2,3-Trichloropropane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene2-HexanoneMW-2 11/11/2019 176 <2.5 8.1 <5.0 <2.5 2.7 2.6 <2.5 3.3 <2.5 18.4 <2.5 20.9 <1.0 30.0 <2.5 <2.5 <2.5 <5.0
MW-3 11/11/2019 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 0.29 <0.50 <0.50 <0.50 <0.50 <1.0
MW-4 11/11/2019 <0.50 <0.50 26.8 1.2 <0.50 3.6 <0.50 1.7 7.8 0.95 24.7 3.2 <0.20 0.20 71.0 <0.50 21.5 7.3 <1.0
MW-5 11/20/2019 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 0.43 <0.50 <0.50 <0.50 <0.50 <1.0
MW-6 11/11/2019 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.20 0.53 <0.50 <0.50 <0.50 <1.0
MW-7 11/11/2019 <0.50 <0.50 <0.50 0.56 <0.50 4.4 <0.50 <0.50 <0.50 <0.50 1.9 <0.50 <0.20 0.20 <0.50 <0.50 5.6 2.2 <1.0
MW-8 11/11/2019 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 0.87 <0.50 1.1 <0.50 <0.20 <0.20 <0.50 <0.50 0.75 <0.50 <1.0
MW-9 11/11/2019 2.1 <0.50 14.1 <1.0 <0.50 1.7 <0.50 <0.50 <0.50 <0.50 3.1 <0.50 <0.20 <0.20 7.8 <0.50 <0.50 <0.50 1.5
MW-10 11/11/2019 2.2 <0.50 70.3 14.6 <0.50 45.1 <0.50 <0.50 3.5 <0.50 19.6 2.1 0.20 <0.20 39.4 0.99 65.5 19.2 <1.0
MW-11 11/11/2019 <0.50 <0.50 <0.50 <0.50 <0.50 1.7 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.20 <0.50 <0.50 0.54 <0.50 <1.0
1 600 600 500 20 6 70 70 70 70 70 25 0.4 0.4 70 0.0005 400 400 40
5,000 260,000 84,500 85,500 20,000 6,000 70,000 6,900 8,500 15,000 25,000 11,700 400 400 30,000 NS 28,500 25,000 40,000
Notes:
2. IPE = Isopropyl Ether.
2. "<" = Not detected at or above the laboratory dectection limit.
3. Concentrations are reported in micrograms per liter (ug/l) = parts per billion (ppb).
4. Concentrations in bold equal or exceed the corresponding NCDEQ Groundwater Quality Standard (2L Standard).
5. GCL = Gross Contamination Limit.
6. NS = No Standard
2L Standard (ug/l)
GCL (ug/l)
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
Mayo's Grocery
416 U.S. Highway 301
Garysburg, North Carolina
Incident #11818

WELL ID
MW-1 1/23/1996 3.4 7.8 8.3 40 <1.0 NA NA NA NA NA NA <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA
TMW-1 11/30/2007 45 <0.50 <0.50 50 <0.50 14 25 1 1.2 5.8 0.99 12.5 0.63 <20 <0.50 <0.50 NA 10 15 <0.02 317 168 NA <100
1/23/1996 3,800 50 J <50 833 <50 NA NA NA NA NA NA 225 <50 NA NA NA NA NA NA NA NA NA NA NA
4/26/1996 5,070 143 54 1,516 <10 714 NA 28 7.6 41 <5.0 337 <5.0 NA <5.0 14 NA 233 31 <5.0 NA NA NA NA
3/8/1999 3,660 <100 189 1,320 <100 NA NA NA NA NA NA 243 <100 NA NA NA NA NA NA NA NA NA NA NA
11/30/2007 4,170 16 197 1,061 <1.0 222 23 6.9 4.9 53 2 <1.0 6.8 22,000 3.1 25 NA 126 34 2 6,730 3,380 <100 232
12/18/2014 500 1.4 220 130 <0.09 150 1.8 8.0 9.4 62 3.6 <0.19 <0.32 NA 1.6 85 NA 140 41 <0.089 NA NA NA NA
9/10/2015 1.2 0.6 29 7 <0.09 7.4 <0.18 5 9.8 36 2.4 <0.19 <0.32 NA 1 100 NA 18 4.6 <0.089 NA NA NA NA
9/20/2017 72 0.98J 130 56.6 <1.0 96 0.80J 23 9.1 64 4.5 <1.0 <1.2 NA 0.84J 120 NA 110 12 <1.0 NA NA NA NA
7/9/2018 44.7 <0.50 14.3 3.6 <0.50 22.9 3.7 0.69 4.1 22.4 0.60 25.4 <0.50 NA 0.58 21.7 NA 9.6 2.2 <0.50 NA NA NA NA
5/10/2019 52.8 <0.50 54.6 3.4 <0.50 31.0 0.65 5.5 18.5 71.9 10.8 4.9 <0.50 NA 1.8 133 NA 18.7 2.8 <0.50 NA NA NA NA
11/11/2019 176 <2.5 8.1 <5.0 <2.5 2.7 2.6 <2.5 3.3 18.4 <2.5 20.9 NA NA <2.5 30.0 <2.5 <2.5 <2.5 <2.5 NA NA NA NA
1/23/1996 357 0.8 J <1.0 95 0.8 NA NA NA NA NA NA 9.7 <1.0 NA NA NA NA NA NA NA NA NA NA NA
4/26/1996 274 <2.5 <2.5 73 <5.0 28 NA <2.5 <2.5 5.6 <2.5 7.4 <2.5 NA <2.5 1.9 J NA 12 <2.5 <2.5 NA NA NA NA
3/8/1999 604 <10 <10 128 <10 NA NA NA NA NA NA 13 <10 NA NA NA NA NA NA NA NA NA NA NA
11/30/2007 1,380 <0.50 <0.50 63 1.1 127 4.1 4.9 3.8 19 2.9 <0.50 3.2 <20 <0.50 0.9 NA 1.6 <0.50 8.2 2,640 <386 NA <346
12/18/2014
9/20/2017 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.60 NA <0.50 <0.50 NA <0.50 <0.50 <0.50 NA NA NA NA
5/10/2019
11/11/2019 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
4/26/1996 431 1,680 1,630 7,210 <100 429 NA 186 45 J 116 <50 <50 <50 NA <50 290 NA 1,820 520 <50 NA NA NA NA
3/8/1999 197 312 1,340 3,110 <100 NA NA NA NA NA NA <100 <100 NA NA NA NA NA NA NA NA NA NA NA
11/30/2007
12/18/2014 <0.4 <0.45 69 <0.9 <0.45 75 <0.9 14 14 40 11 <0.97 <1.6 NA <0.48 140 NA 15 2.4 J <0.44 NA NA NA NA
9/10/2015
9/20/2017 0.31J <0.50 7.7 0.72J <0.50 0.89 <0.50 2.6 7.0 17 1.9 <0.50 <0.60 NA 0.65 47 NA 1.9 0.22J <0.50 NA NA NA NA
5/10/2019 <0.50 <0.50 17.5 0.55 <0.50 2.8 <0.50 2.4 10.5 27.2 2.9 <0.20 <0.50 NA 1.1 72.2 NA 6.3 1.2 <0.50 NA NA NA NA
11/11/2019 <0.50 <0.50 26.8 1.2 <0.50 3.6 <0.50 1.7 7.8 24.7 3.2 <0.20 NA NA 0.95 71.0 <0.50 21.5 7.3 <0.50 NA NA NA NA
4/26/1996 <0.5 <0.5 <0.5 <1.0 <1.0 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA <0.5 <0.5 <0.5 NA NA NA NA
3/8/1999 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA
11/30/2007
12/18/2014
9/20/2017
5/10/2019
11/20/2019 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
4/26/1996 <0.5 <0.5 <0.5 <1.0 <1.0 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA <0.5 <0.5 <0.5 NA NA NA NA
3/8/1999 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA <1.0 <1.0 NA NA NA NA NA NA <1.0 NA NA NA NA
11/30/2007
12/18/2014
9/20/2017
5/10/2019
11/11/2019 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 NA NA <0.50 0.53 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
1 600 600 500 20 6 70 70 70 70 25 0.4 3 10 40 70 0.005 400 400 0.02 400 700 700 700
5,000 260,000 84,500 85,500 20,000 6,000 70,000 6,900 8,500 25,000 11,700 400 3,000 10,000 40,000 30,000 NE 28,500 25,000 50 NE NE NE NE
Notes:
1. MTBE = Methyl Tertiary Butyl Ether
2. "<" = Not detected at or above the laboratory detection limit
3. GCL = Gross Contamination Limit
4. NE = Not established
5. J = Indicates constituent was detected above laboratory detection limit but below laboratory reporting limit
6. Concentrations are reported in ug/L (micrograms per liter = parts per billion (ppb).
7. Concentrations in bold equal or exceed the corresponding NCDEQ Groundwater Quality Standard (2L Standard).tert-ButylbenzeneC9-C18 AliphaticsC9-C22 AromaticsToluene1,2,4-Trimethylbenzenen-Propylbenzene1,2,3-TrichloropropaneUNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
INADEQUATE VOLUME OF WATER TO SAMPLE WELL
UNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
UNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
MW-3
2L Standard (ug/l)
GCL (ug/l)ChloromethaneBenzeneEthylbenzene1,3,5-TrimethylbenzeneDiisopropyl Ether (DIPE)1,2-Dibromoethane (EDB)MW-2
MW-4
UNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
UNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
UNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
WELL WAS DRY, UNABLE TO SAMPLE
INADEQUATE VOLUME OF WATER TO SAMPLE WELL
UNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
Date Collected
Naphthalenetert-butyl alcoholC19-C36 Aliphatics1,2-DichloroethaneMTBEn-ButlybenzeneC5-C8 AliphaticsUNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
MW-6 Isopropylbenzenep-IsopropyltolueneWELL WAS DRY, UNABLE TO SAMPLEsec-ButylbenzeneMW-5 Total XylenesPage 1 of 2
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
Mayo's Grocery
416 U.S. Highway 301
Garysburg, North Carolina
Incident #11818

WELL ID
tert-ButylbenzeneC9-C18 AliphaticsC9-C22 AromaticsToluene1,2,4-Trimethylbenzenen-Propylbenzene1,2,3-TrichloropropaneChloromethaneBenzeneEthylbenzene1,3,5-TrimethylbenzeneDiisopropyl Ether (DIPE)1,2-Dibromoethane (EDB)Date Collected
Naphthalenetert-butyl alcoholC19-C36 Aliphatics1,2-DichloroethaneMTBEn-ButlybenzeneC5-C8 AliphaticsIsopropylbenzenep-Isopropyltoluenesec-ButylbenzeneTotal Xylenes4/26/1996 605 855 1,200 4,070 <100 151 NA 162 <50 80 <50 <50 <50 NA <50 201 NA 1,380 389 <50 NA NA NA NA
3/8/1999 220 103 827 1,700 <50 NA NA NA NA NA NA <50 <50 NA NA NA NA NA NA NA NA NA NA NA
11/30/2007
12/18/2014 4 <0.09 11 0.62 <0.09 24 <0.18 3.2 2.7 5 1.8 <0.19 <0.32 NA 1.4 11 NA 6.1 0.54 <0.089 NA NA NA NA
9/10/2015
9/20/2017 4.3 0.20J 1.0 1.0J <0.50 0.35J <0.50 0.85 1.4 1.7 <0.50 <0.50 <0.60 NA 0.37J 0.25J NA 0.50 <0.50 <0.50 NA NA NA NA
7/9/2018 1.1 <0.50 9.7 0.74 <0.50 6.6 <0.50 <0.50 1.1 2.5 0.82 <0.20 <0.50 NA <0.50 5.0 NA 4.6 0.64 <0.50 NA NA NA NA
5/10/2019 0.57 <0.50 8.8 0.67 <0.50 6.2 <0.50 <0.50 1.1 2.9 0.59 <0.20 <0.50 NA <0.50 5.0 NA 6.0 <0.50 <0.50 NA NA NA NA
11/11/2019 <0.50 <0.50 <0.50 0.56 <0.50 4.4 <0.50 <0.50 <0.50 1.9 <0.50 <0.20 NA NA <0.50 <0.50 <0.50 5.6 2.2 <0.50 NA NA NA NA
5/6/1996 30 7.1 25 893 <1.0 54 NA 145 12 37 8.7 <0.5 <0.5 NA <0.5 62 NA 747 188 <0.5 NA NA NA NA
3/8/1999
11/30/2007
12/18/2014 <0.079 <0.092 <0.09 <0.18 <0.09 <0.12 <0.18 <0.054 <0.084 <0.11 <0.12 <0.19 <0.32 NA <0.096 <0.094 NA <0.18 <0.1 <0.089 NA NA NA NA
9/10/2015
9/20/2017 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <0.50 0.79 0.69 <0.50 <0.50 <0.60 NA <0.50 0.63 NA <0.50 <0.50 <0.50 NA NA NA NA
5/10/2019 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 <0.50 NA <0.50 <0.50 NA <0.50 <0.50 <0.50 NA NA NA NA
11/11/2019 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 0.87 1.1 <0.50 <0.20 NA NA <0.50 <0.50 <0.50 0.75 <0.50 <0.50 NA NA NA NA
9/10/2015 310 11 20 1,350 6.2J 120 <3.6 10 8.6J 57 4.8J <3.9 <6.5 NA <0.096 27 NA 760 34 <1.8 NA NA NA NA
9/20/2017 5.4 <5.0 160 44.8 <5.0 90 <5.0 12 5.8 37 3.8J <5.0 <6.0 NA <5.0 96 NA 340 42 <5.0 NA NA NA NA
7/9/2018 1.2 <0.50 19.8 1.5 <0.50 8.2 <0.50 <0.50 2.0 8.6 1.2 <0.20 <0.50 NA <0.50 25.8 NA 35.3 23.3 <0.50 NA NA NA NA
5/10/2019 16.1 <0.50 187 35.6 <0.50 89.0 <0.50 8.3 10.0 67.2 6.2 0.22 <0.50 NA <0.50 123 NA 323 11.5 <0.50 NA NA NA NA
11/11/2019 2.1 <0.50 14.1 <1.0 <0.50 1.7 <0.50 <0.50 <0.50 3.1 <0.50 <0.20 NA NA <0.50 7.8 <0.50 <0.50 <0.50 <0.50 NA NA NA NA
9/10/2015 110 190 770 2,900 <2.2 190 <4.5 5.2J 5J 42 3.5J <4.8 <8.1 NA <2.4 81 NA 730 190 <2.2 NA NA NA NA
9/20/2017 9.2 <2.5 300 15.3J <2.5 150 <2.5 5.6 6.4 49 3.6 <2.5 <3.0 NA <2.5 110 NA 26 2.2J <2.5 NA NA NA NA
7/9/2018 <0.50 <0.50 2.8 <0.50 <0.50 2.0 <0.50 <0.50 <0.50 1.1 <0.50 <0.20 <0.50 NA <0.50 2.1 NA 0.76 <0.50 <0.50 NA NA NA NA
5/10/2019 5.5 <0.50 64.2 <0.50 <0.50 8.1 <0.50 0.54 5.9 22.2 2.0 0.32 <0.50 NA 0.64 39.4 NA 1.5 <0.50 <0.50 NA NA NA NA
11/11/2019 2.2 <0.50 70.3 14.6 <0.50 45.1 <0.50 <0.50 3.5 19.6 2.1 0.20 NA NA <0.50 39.4 0.99 65.5 19.2 <0.50 NA NA NA NA
9/10/2015 <0.079 <0.09 <0.092 <0.18 <0.09 <0.12 <0.18 <0.054 <0.084 <0.11 <0.12 <0.19 <0.32 NA <0.096 <0.094 NA <0.18 <0.1 <0.089 NA NA NA NA
9/20/2017 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.60 NA <0.50 <0.50 NA <0.50 <0.50 <0.50 NA NA NA NA
5/10/2019
11/11/2019 <0.50 <0.50 <0.50 <0.50 <0.50 1.7 <0.50 <0.50 <0.50 <0.50 <0.50 <0.20 NA NA <0.50 <0.50 <0.50 0.54 <0.50 <0.50 NA NA NA NA
1 600 600 500 20 6 70 70 70 70 25 0.4 3 10 40 70 0.0005 400 400 0.02 400 700 700 700
5,000 260,000 84,500 85,500 20,000 6,000 70,000 6,900 8,500 25,000 11,700 400 3,000 10,000 40,000 30,000 NS 28,500 25,000 50 NE NE NE NE
Notes:
1. MTBE = Methyl Tertiary Butyl Ether
2. "<" = Not detected at or above the laboratory detection limit
3. GCL = Gross Contamination Limit
4. NE = Not established
5. J = Indicates constituent was detected above laboratory detection limit but below laboratory reporting limit
6. Concentrations are reported in ug/L (micrograms per liter = parts per billion (ppb).
7. Concentrations in bold equal or exceed the corresponding NCDEQ Groundwater Quality Standard (2L Standard).
GCL (ug/l)
2L Standard (ug/l)
INADEQUATE VOLUME OF WATER TO SAMPLE WELL
MW-9
MW-10
UNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
UNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
UNABLE TO LOCATE WELL, MONITORING WELL NOT SAMPLED
WELL WAS DRY, UNABLE TO SAMPLE
INADEQUATE VOLUME OF WATER TO SAMPLE WELL
MW-11
MW-7
MW-8
Page 2 of 2
TABLE 5
NATURAL ATTENUATION PARAMETERS
Mayo's Grocery
416 U.S. Highway 301
Garysburg, North Carolina
Incident #11818
MW-2 11/11/2019 18.6 13.05 253.6 11.05 -108.6
MW-3 11/11/2019 19.1 4.43 152.4 4.46 -16.0
MW-4 11/11/2019 20.2 2.49 256.6 2.03 121.0
MW-5 11/11/2019 18.8 2.51 87.6 1.52 -55.6
MW-6 11/11/2019 20.2 3.51 215.1 4.44 138.2
MW-7 11/11/2019 20.4 12.70 467.2 10.82 26.4
MW-8 11/11/2019 22.0 0.91 149.3 5.59 42.0
MW-9 11/11/2019 21.5 9.71 329.5 8.79 135.4
MW-10 11/11/2019 20.5 1.83 100.5 4.62 69.0
MW-11 11/11/2019 19.0 5.49 96.8 4.48 17.2
Notes:
1. oC = Degrees Celsius.
2. mg/L = milligrams per liter.
3. µs/cm = micro Siemens per centimeter.
4. SU = Standard Units.
5. ORP = Oxidation Reduction Potential
6. mV = Millivolts Conductivity (ms/cm)pH (SU)ORP (mV)WELL ID Date
Collected
Temperature (oC)Dissolved Oxygen (mg/L)Page 1 of 1

FIGURES
.

2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
[phone]
PROJECT NO: SLP1181805
DATE: 8/2018 REVIEWED BY: GA
Mayo’s Grocery –Incident #11818
416 U.S. Highway 301
Garysburg, Northampton County, North Carolina
SOURCE: MyTopoMap.com
SCALE: 1” = 1,780’
FIGURE 1: SITE TOPOGRAPHIC MAP
SITE
N
MAYO'SGROCERYMW-6MW-10MW-7MW-5MW-3MW-11MW-2MW-4MW-8TANK 4SEPTICTANKTANK 2TANK 3TANK 1MW-9APPROXIMATE LOCATIONOF BURIED TRAIN
2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
[phone]
PROJECT NO: SLP1181805
DATE: 8/2018 REVIEWED BY: GA
Mayo’s Grocery –Incident #11818
401 U.S. Highway 301
Garysburg, Northampton County, North Carolina
SOURCE: Northampton County NC GIS
SCALE: 1” = 370’
FIGURE 3: POTENTIAL RECEPTOR MAP
Abandoned Water Supply Well
Inactive Water Supply Well
Water Supply Well With Unknown Use –Connected to a
Municipal Water Supply
Water Supply Well With Unknown Use –Not Connected to a
Municipal Water Supply
500 Foot Radius
1,000 Foot Radius
Map ID –Reference Table 1
1
11
10
97
6 5
4
2
21
20
18 17
16
28
27
26
25
24
N
SITE
3
8
12
15
23
19
14
22
13
21
MAYO'SGROCERYMW-6MW-10MW-7MW-5MW-3MW-11MW-2MW-4MW-8TANK 4SEPTICTANKTANK 2TANK 3TANK 1MW-9APPROXIMATE LOCATIONOF BURIED TRAIN
MAYO'SGROCERYMW-6MW-10MW-7MW-5MW-3MW-11MW-2MW-4MW-8TANK 4SEPTICTANKTANK 2TANK 3TANK 1MW-9APPROXIMATE LOCATIONOF BURIED TRAIN
MAYO'SGROCERYMW-6MW-10MW-7MW-5MW-3MW-11MW-2MW-4MW-8TANK 4SEPTICTANKTANK 2TANK 3TANK 1MW-9APPROXIMATE LOCATIONOF BURIED TRAIN

APPENDIX A

FIELD NOTES

APPENDIX B

LABORATORY ANALYTICAL RESULTS
11/19/19
Technical Report for
ATC Group Services LLC
Mayo's Grocery 416 US Hwy 301, Garysboro, NC
SLP1181805
SGS Job Number: LA59326
Sampling Date: 11/11/19
Report to:
ATC Group Services LLC.
2725 East Millbrook Road Suite 121
Raleigh, NC 27604
[e-mail]; [e-mail]
ATTN: liz Allyn
Total number of pages in report:
Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), AZ(AZ0805), FL(E87657), IL(200082), KY(#31),
NC(487), SC(73004001), NJ(LA007), TX(T104704186-18-16), WV(257)
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 500 Ambassador Caffery • Scott, LA 70583 • tel: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Amy Jackson 337-237-4775
Ron Benjamin
Lab Director
Scott, LA 11/19/19
e-Hardcopy 2.0
Automated Report
48
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 48
LA59326
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: LA59326-1: MW2 ........................................................................................................7
3.2: LA59326-2: MW3 ........................................................................................................10
3.3: LA59326-3: MW4 ........................................................................................................13
3.4: LA59326-5: MW6 ........................................................................................................16
3.5: LA59326-6: MW7 ........................................................................................................19
3.6: LA59326-7: MW8 ........................................................................................................22
3.7: LA59326-8: MW9 ........................................................................................................25
3.8: LA59326-9: MW10 ......................................................................................................28
3.9: LA59326-10: MW11 ....................................................................................................31
Section 4: Misc. Forms ............................................................................................................34
4.1: Chain of Custody ...........................................................................................................35
Section 5: MS Volatiles - QC Data Summaries .....................................................................39
5.1: Method Blank Summary ................................................................................................40
5.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................43
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................46 123452 of 48
LA59326
SGS North America Inc.
Sample Summary
ATC Group Services LLC
Job No:LA59326
Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Project No: SLP1181805
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the RL
LA59326-1 11/11/19 15:30 TJ 11/13/19 AQ Ground Water MW2
LA59326-2 11/11/19 14:10 TJ 11/13/19 AQ Ground Water MW3
LA59326-3 11/11/19 15:00 TJ 11/13/19 AQ Ground Water MW4
LA59326-4 11/11/19 13:30 TJ 11/13/19 AQ Ground Water MW5
LA59326-5 11/11/19 11:00 TJ 11/13/19 AQ Ground Water MW6
LA59326-6 11/11/19 14:30 TJ 11/13/19 AQ Ground Water MW7
LA59326-7 11/11/19 12:30 TJ 11/13/19 AQ Ground Water MW8
LA59326-8 11/11/19 12:00 TJ 11/13/19 AQ Ground Water MW9
LA59326-9 11/11/19 11:30 TJ 11/13/19 AQ Ground Water MW10
LA59326-10 11/11/19 13:00 TJ 11/13/19 AQ Ground Water MW11
3 of 48
LA593261
Summary of Hits Page 1 of 2
Job Number:LA59326
Account:ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Collected:11/11/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA59326-1 MW2
Benzene 176 2.5 ug/l SM 6200B
sec-Butylbenzene 3.3 2.5 ug/l SM 6200B
1,2-Dichloroethane 20.9 1.0 ug/l SM 6200B
Di-Isopropyl Ether 2.6 2.5 ug/l SM 6200B
Ethylbenzene 8.1 2.5 ug/l SM 6200B
Isopropylbenzene 18.4 2.5 ug/l SM 6200B
Naphthalene 2.7 2.5 ug/l SM 6200B
n-Propylbenzene 30.0 2.5 ug/l SM 6200B
LA59326-2 MW3
Hexachlorobutadiene 0.29 0.20 ug/l SM 6200B
LA59326-3 MW4
n-Butylbenzene 1.7 0.50 ug/l SM 6200B
sec-Butylbenzene 7.8 0.50 ug/l SM 6200B
tert-Butylbenzene 0.95 0.50 ug/l SM 6200B
Ethylbenzene 26.8 0.50 ug/l SM 6200B
Hexachlorobutadiene 0.20 0.20 ug/l SM 6200B
Isopropylbenzene 24.7 0.50 ug/l SM 6200B
p-Isopropyltoluene 3.2 0.50 ug/l SM 6200B
Naphthalene 3.6 0.50 ug/l SM 6200B
n-Propylbenzene 71.0 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 21.5 0.50 ug/l SM 6200B
1,3,5-Trimethylbenzene 7.3 0.50 ug/l SM 6200B
Xylene (total)1.2 0.50 ug/l SM 6200B
LA59326-5 MW6
n-Propylbenzene 0.53 0.50 ug/l SM 6200B
LA59326-6 MW7
Isopropylbenzene 1.9 0.50 ug/l SM 6200B
Naphthalene 4.4 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 5.6 0.50 ug/l SM 6200B
1,3,5-Trimethylbenzene 2.2 0.50 ug/l SM 6200B
Xylene (total)0.56 0.50 ug/l SM 6200B
LA59326-7 MW8
sec-Butylbenzene 0.87 0.50 ug/l SM 6200B
4 of 48
LA593262
Summary of Hits Page 2 of 2
Job Number:LA59326
Account:ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Collected:11/11/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Isopropylbenzene 1.1 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.75 0.50 ug/l SM 6200B
LA59326-8 MW9
Benzene 2.1 0.50 ug/l SM 6200B
Ethylbenzene 14.1 0.50 ug/l SM 6200B
2-Hexanone 1.5 1.0 ug/l SM 6200B
Isopropylbenzene 3.1 0.50 ug/l SM 6200B
Naphthalene 1.7 0.50 ug/l SM 6200B
n-Propylbenzene 7.8 0.50 ug/l SM 6200B
LA59326-9 MW10
Benzene 2.2 0.50 ug/l SM 6200B
sec-Butylbenzene 3.5 0.50 ug/l SM 6200B
1,2-Dichloroethane 0.20 0.20 ug/l SM 6200B
Ethylbenzene 70.3 0.50 ug/l SM 6200B
Isopropylbenzene 19.6 0.50 ug/l SM 6200B
p-Isopropyltoluene 2.1 0.50 ug/l SM 6200B
Naphthalene 45.1 0.50 ug/l SM 6200B
n-Propylbenzene 39.4 0.50 ug/l SM 6200B
1,2,3-Trichloropropane 0.99 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 65.5 0.50 ug/l SM 6200B
1,3,5-Trimethylbenzene 19.2 0.50 ug/l SM 6200B
m,p-Xylene 10.1 1.0 ug/l SM 6200B
o-Xylene 4.5 0.50 ug/l SM 6200B
Xylene (total)14.6 0.50 ug/l SM 6200B
LA59326-10 MW11
Naphthalene 1.7 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.54 0.50 ug/l SM 6200B
5 of 48
LA593262
SGS North America Inc.
Sample Results
Report of Analysis
Scott, LA
Section 3
6 of 48
LA593263
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW2
Lab Sample ID:LA59326-1 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0119724.D 5 11/16/19 14:41 CP n/a n/a V2K2165
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 50 ug/l
71-43-2 Benzene 176 2.5 ug/l
108-86-1 Bromobenzene ND 2.5 ug/l
74-97-5 Bromochloromethane ND 2.5 ug/l
75-27-4 Bromodichloromethane ND 2.5 ug/l
75-25-2 Bromoform ND 2.5 ug/l
104-51-8 n-Butylbenzene ND 2.5 ug/l
135-98-8 sec-Butylbenzene 3.3 2.5 ug/l
98-06-6 tert-Butylbenzene ND 2.5 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 ug/l
108-90-7 Chlorobenzene ND 2.5 ug/l
75-00-3 Chloroethane ND 2.5 ug/l
67-66-3 Chloroform ND 2.5 ug/l
95-49-8 o-Chlorotoluene ND 2.5 ug/l
106-43-4 p-Chlorotoluene ND 2.5 ug/l
124-48-1 Dibromochloromethane ND 1.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 ug/l
541-73-1 m-Dichlorobenzene ND 2.5 ug/l
95-50-1 o-Dichlorobenzene ND 2.5 ug/l
106-46-7 p-Dichlorobenzene ND 2.5 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 ug/l
107-06-2 1,2-Dichloroethane 20.9 1.0 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 ug/l
78-87-5 1,2-Dichloropropane ND 1.5 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 48
LA5932633.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW2
Lab Sample ID:LA59326-1 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 ug/l
108-20-3 Di-Isopropyl Ether 2.6 2.5 ug/l
64-17-5 Ethyl Alcohol ND 250 ug/l
100-41-4 Ethylbenzene 8.1 2.5 ug/l
591-78-6 2-Hexanone ND 5.0 ug/l
87-68-3 Hexachlorobutadiene ND 1.0 ug/l
98-82-8 Isopropylbenzene 18.4 2.5 ug/l
99-87-6 p-Isopropyltoluene ND 2.5 ug/l
74-83-9 Methyl Bromide ND 2.5 ug/l
74-87-3 Methyl Chloride ND 2.5 ug/l
74-95-3 Methylene Bromide ND 2.5 ug/l
75-09-2 Methylene Chloride ND 2.5 ug/l
78-93-3 Methyl Ethyl Ketone ND 130 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.5 ug/l
91-20-3 Naphthalene 2.7 2.5 ug/l
103-65-1 n-Propylbenzene 30.0 2.5 ug/l
100-42-5 Styrene ND 2.5 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 ug/l
127-18-4 Tetrachloroethylene ND 2.5 ug/l
108-88-3 Toluene ND 2.5 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.5 ug/l
79-01-6 Trichloroethylene ND 2.5 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 2.5 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 2.5 ug/l
108-05-4 Vinyl Acetate ND 2.5 ug/l
75-01-4 Vinyl Chloride ND 0.50 ug/l
m,p-Xylene ND 5.0 ug/l
95-47-6 o-Xylene ND 2.5 ug/l
1330-20-7 Xylene (total)ND 2.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 48
LA5932633.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW2
Lab Sample ID:LA59326-1 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 48
LA5932633.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW3
Lab Sample ID:LA59326-2 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0119716.D 1 11/16/19 10:37 CP n/a n/a V2K2165
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 48
LA5932633.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW3
Lab Sample ID:LA59326-2 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene 0.29 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 48
LA5932633.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW3
Lab Sample ID:LA59326-2 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 94%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 48
LA5932633.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW4
Lab Sample ID:LA59326-3 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0119717.D 1 11/16/19 11:07 CP n/a n/a V2K2165
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene 1.7 0.50 ug/l
135-98-8 sec-Butylbenzene 7.8 0.50 ug/l
98-06-6 tert-Butylbenzene 0.95 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 48
LA5932633.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW4
Lab Sample ID:LA59326-3 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene 26.8 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene 0.20 0.20 ug/l
98-82-8 Isopropylbenzene 24.7 0.50 ug/l
99-87-6 p-Isopropyltoluene 3.2 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene 3.6 0.50 ug/l
103-65-1 n-Propylbenzene 71.0 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene 21.5 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene 7.3 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)1.2 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 95%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 48
LA5932633.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW4
Lab Sample ID:LA59326-3 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 48
LA5932633.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW6
Lab Sample ID:LA59326-5 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0119718.D 1 11/16/19 11:38 CP n/a n/a V2K2165
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 48
LA5932633.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW6
Lab Sample ID:LA59326-5 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene 0.53 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 93%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 48
LA5932633.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW6
Lab Sample ID:LA59326-5 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 93%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 48
LA5932633.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW7
Lab Sample ID:LA59326-6 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0119719.D 1 11/16/19 12:08 CP n/a n/a V2K2165
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 48
LA5932633.5
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW7
Lab Sample ID:LA59326-6 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene 1.9 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene 4.4 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene 5.6 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene 2.2 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)0.56 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 48
LA5932633.5
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW7
Lab Sample ID:LA59326-6 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 48
LA5932633.5
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW8
Lab Sample ID:LA59326-7 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0119720.D 1 11/16/19 12:38 CP n/a n/a V2K2165
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene 0.87 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 48
LA5932633.6
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW8
Lab Sample ID:LA59326-7 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene 1.1 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.75 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 48
LA5932633.6
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW8
Lab Sample ID:LA59326-7 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 48
LA5932633.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW9
Lab Sample ID:LA59326-8 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0119721.D 1 11/16/19 13:08 CP n/a n/a V2K2165
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene 2.1 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 48
LA5932633.7
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW9
Lab Sample ID:LA59326-8 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene 14.1 0.50 ug/l
591-78-6 2-Hexanone 1.5 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene 3.1 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene 1.7 0.50 ug/l
103-65-1 n-Propylbenzene 7.8 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 48
LA5932633.7
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW9
Lab Sample ID:LA59326-8 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 48
LA5932633.7
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW10
Lab Sample ID:LA59326-9 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0119722.D 1 11/16/19 13:39 CP n/a n/a V2K2165
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene 2.2 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene 3.5 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane 0.20 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 48
LA5932633.8
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW10
Lab Sample ID:LA59326-9 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene 70.3 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene 19.6 0.50 ug/l
99-87-6 p-Isopropyltoluene 2.1 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene 45.1 0.50 ug/l
103-65-1 n-Propylbenzene 39.4 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane 0.99 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene 65.5 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene 19.2 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene 10.1 1.0 ug/l
95-47-6 o-Xylene 4.5 0.50 ug/l
1330-20-7 Xylene (total)14.6 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 48
LA5932633.8
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW10
Lab Sample ID:LA59326-9 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 48
LA5932633.8
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW11
Lab Sample ID:LA59326-10 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0119723.D 1 11/16/19 14:10 CP n/a n/a V2K2165
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 48
LA5932633.9
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW11
Lab Sample ID:LA59326-10 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene 1.7 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.54 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 48
LA5932633.9
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW11
Lab Sample ID:LA59326-10 Date Sampled:11/11/19
Matrix:AQ - Ground Water Date Received:11/13/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 94%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 48
LA5932633.9
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Scott, LA
Section 4
34 of 48
LA593264
LA59326: Chain of Custody
Page 1 of 4
35 of 48
LA5932644.1
LA59326: Chain of Custody
Page 2 of 4
36 of 48
LA5932644.1
Job Number:LA59326 Client:ATC
Date / Time Received:11/13/2019 8:15:00 AM Delivery Method:
Project:MAYA'S GROCERY
4. No. Coolers:1
Airbill #'s:4913 8690 9181
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR Gun
Ice (direct contact)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Broken / Leaking
Y or N
Comments Received 3 of 4 -40ml vilals broken in cooler for mw5. (frozen)
Y or N N/A
Cooler Temps:#1: (1.2/1.2); DV440
SGS Sample Receipt Summary
Proceed with analysis using remaining vial.
Amy Jackson 11/13/2019Responded to by:Response Date:
LA59326: Chain of Custody
Page 3 of 4
37 of 48
LA5932644.1
TAT (Days):7Received Date:11/13/2019Due Date:11/20/2019Project Description:Mayo's Grocery 416 US Hwy 301, Garysboro, NCAccount Name:ATC Group Services LLCDeliverable:COMMBCSR:AJRequested Date:11/13/2019Job Change Order:LA59326Sample #:LA59326-4MW5Change:Cancel V6200SL analysis. 3 of 4 vials received frozen and broken. Remaining vial broke during analysis.Dept:========================================================================================================================================================================================================================================TAT:7Above Changes Per:To Client: This Change Order is confirmation of the revisions, previously discussed with the a Client Service Representative.Date/Time:11/13/2019 12:35:56 PMPage 1 of 1Amy JacksonLA59326: Chain of Custody
Page 4 of 4
38 of 48
LA5932644.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Scott, LA
Section 5
39 of 48
LA593265
Method Blank Summary Page 1 of 3
Job Number:LA59326
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2165-MB2 2K0119707.D 1 11/16/19 CP n/a n/a V2K2165
The QC reported here applies to the following samples:Method: SM 6200B
LA59326-1, LA59326-2, LA59326-3, LA59326-5, LA59326-6, LA59326-7, LA59326-8, LA59326-9, LA59326-10
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene 0.21 0.50 ug/l J
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
40 of 48
LA5932655.1.1
Method Blank Summary Page 2 of 3
Job Number:LA59326
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2165-MB2 2K0119707.D 1 11/16/19 CP n/a n/a V2K2165
The QC reported here applies to the following samples:Method: SM 6200B
LA59326-1, LA59326-2, LA59326-3, LA59326-5, LA59326-6, LA59326-7, LA59326-8, LA59326-9, LA59326-10
CAS No.Compound Result RL Units Q
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene 0.45 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene 0.29 0.50 ug/l J
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.62 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene 0.48 0.50 ug/l J
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
41 of 48
LA5932655.1.1
Method Blank Summary Page 3 of 3
Job Number:LA59326
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2165-MB2 2K0119707.D 1 11/16/19 CP n/a n/a V2K2165
The QC reported here applies to the following samples:Method: SM 6200B
LA59326-1, LA59326-2, LA59326-3, LA59326-5, LA59326-6, LA59326-7, LA59326-8, LA59326-9, LA59326-10
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 92%70-130%
42 of 48
LA5932655.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 3
Job Number:LA59326
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2165-BS3 2K0119704.D 1 11/16/19 CP n/a n/a V2K2165
V2K2165-BSD3 2K0119705.D 1 11/16/19 CP n/a n/a V2K2165
The QC reported here applies to the following samples:Method: SM 6200B
LA59326-1, LA59326-2, LA59326-3, LA59326-5, LA59326-6, LA59326-7, LA59326-8, LA59326-9, LA59326-10
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
67-64-1 Acetone 50 58.4 117 52.5 105 11 70-130/30
71-43-2 Benzene 20 19.9 100 17.9 90 11 70-130/30
108-86-1 Bromobenzene 20 21.8 109 21.4 107 2 70-130/30
74-97-5 Bromochloromethane 20 20.5 103 18.9 95 8 70-130/30
75-27-4 Bromodichloromethane 20 23.6 118 22.9 115 3 70-130/30
75-25-2 Bromoform 20 20.4 102 19.3 97 6 70-130/30
104-51-8 n-Butylbenzene 20 24.6 123 25.4 127 3 70-130/30
135-98-8 sec-Butylbenzene 20 24.1 121 25.0 125 4 70-130/30
98-06-6 tert-Butylbenzene 20 24.1 121 25.1 126 4 70-130/30
56-23-5 Carbon Tetrachloride 20 22.9 115 21.9 110 4 70-130/30
108-90-7 Chlorobenzene 20 21.4 107 21.4 107 0 70-130/30
75-00-3 Chloroethane 20 21.5 108 21.2 106 1 60-140/30
67-66-3 Chloroform 20 21.1 106 20.3 102 4 70-130/30
95-49-8 o-Chlorotoluene 20 22.4 112 22.9 115 2 70-130/30
106-43-4 p-Chlorotoluene 20 23.2 116 23.6 118 2 70-130/30
124-48-1 Dibromochloromethane 20 20.6 103 19.8 99 4 70-130/30
96-12-8 1,2-Dibromo-3-chloropropane 20 20.7 104 19.9 100 4 70-130/30
106-93-4 1,2-Dibromoethane 20 22.8 114 21.9 110 4 70-130/30
75-71-8 Dichlorodifluoromethane 20 20.8 104 20.5 103 1 60-140/30
541-73-1 m-Dichlorobenzene 20 20.5 103 20.8 104 1 70-130/30
95-50-1 o-Dichlorobenzene 20 20.9 105 20.9 105 0 70-130/30
106-46-7 p-Dichlorobenzene 20 20.4 102 20.6 103 1 70-130/30
75-34-3 1,1-Dichloroethane 20 21.9 110 20.9 105 5 70-130/30
107-06-2 1,2-Dichloroethane 20 20.2 101 19.3 97 5 70-130/30
75-35-4 1,1-Dichloroethylene 20 22.1 111 21.3 107 4 70-130/30
156-59-2 cis-1,2-Dichloroethylene 20 21.1 106 20.2 101 4 70-130/30
156-60-5 trans-1,2-Dichloroethylene 20 21.9 110 21.1 106 4 70-130/30
78-87-5 1,2-Dichloropropane 20 22.5 113 21.8 109 3 70-130/30
142-28-9 1,3-Dichloropropane 20 22.5 113 21.5 108 5 70-130/30
594-20-7 2,2-Dichloropropane 20 21.0 105 19.7 99 6 70-130/30
563-58-6 1,1-Dichloropropene 20 22.3 112 21.4 107 4 70-130/30
10061-01-5 cis-1,3-Dichloropropene 20 20.7 104 20.1 101 3 70-130/30
10061-02-6 trans-1,3-Dichloropropene 20 20.6 103 20.1 101 2 70-130/30
108-20-3 Di-Isopropyl Ether 20 22.9 115 21.6 108 6 70-130/30
64-17-5 Ethyl Alcohol 400 481 120 424 106 13 70-130/30
100-41-4 Ethylbenzene 20 22.4 112 22.4 112 0 70-130/30
* = Outside of Control Limits.
43 of 48
LA5932655.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 3
Job Number:LA59326
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2165-BS3 2K0119704.D 1 11/16/19 CP n/a n/a V2K2165
V2K2165-BSD3 2K0119705.D 1 11/16/19 CP n/a n/a V2K2165
The QC reported here applies to the following samples:Method: SM 6200B
LA59326-1, LA59326-2, LA59326-3, LA59326-5, LA59326-6, LA59326-7, LA59326-8, LA59326-9, LA59326-10
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
591-78-6 2-Hexanone 50 55.5 111 51.9 104 7 70-130/30
87-68-3 Hexachlorobutadiene 20 21.6 108 22.1 111 2 70-130/30
98-82-8 Isopropylbenzene 20 21.2 106 21.3 107 0 70-130/30
99-87-6 p-Isopropyltoluene 20 23.8 119 24.6 123 3 70-130/30
74-83-9 Methyl Bromide 20 20.9 105 19.6 98 6 60-140/30
74-87-3 Methyl Chloride 20 21.9 110 21.4 107 2 60-140/30
74-95-3 Methylene Bromide 20 21.5 108 20.5 103 5 70-130/30
75-09-2 Methylene Chloride 20 19.5 98 18.4 92 6 70-130/30
78-93-3 Methyl Ethyl Ketone 50 46.4 93 43.3 87 7 70-130/30
108-10-1 4-Methyl-2-pentanone 50 51.2 102 48.1 96 6 70-130/30
1634-04-4 Methyl Tert Butyl Ether 20 22.9 115 21.1 106 8 70-130/30
91-20-3 Naphthalene 20 20.9 105 20.4 102 2 70-130/30
103-65-1 n-Propylbenzene 20 23.0 115 23.8 119 3 70-130/30
100-42-5 Styrene 20 21.3 107 21.0 105 1 70-130/30
630-20-6 1,1,1,2-Tetrachloroethane 20 23.6 118 23.2 116 2 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 20 19.8 99 18.9 95 5 70-130/30
127-18-4 Tetrachloroethylene 20 20.6 103 20.7 104 0 70-130/30
108-88-3 Toluene 20 21.1 106 21.1 106 0 70-130/30
87-61-6 1,2,3-Trichlorobenzene 20 24.5 123 24.3 122 1 70-130/30
120-82-1 1,2,4-Trichlorobenzene 20 24.5 123 24.5 123 0 70-130/30
71-55-6 1,1,1-Trichloroethane 20 22.7 114 21.8 109 4 70-130/30
79-00-5 1,1,2-Trichloroethane 20 21.6 108 20.5 103 5 70-130/30
79-01-6 Trichloroethylene 20 22.4 112 22.5 113 0 70-130/30
75-69-4 Trichlorofluoromethane 20 20.8 104 20.8 104 0 60-140/30
96-18-4 1,2,3-Trichloropropane 20 19.3 97 18.3 92 5 70-130/30
95-63-6 1,2,4-Trimethylbenzene 20 23.9 120 24.4 122 2 70-130/30
108-67-8 1,3,5-Trimethylbenzene 20 23.9 120 24.4 122 2 70-130/30
108-05-4 Vinyl Acetate 20 20.8 104 19.1 96 9 70-130/30
75-01-4 Vinyl Chloride 20 22.1 111 22.0 110 0 60-140/30
m,p-Xylene 40 46.3 116 46.4 116 0 70-130/30
95-47-6 o-Xylene 20 25.0 125 24.9 125 0 70-130/30
1330-20-7 Xylene (total)60 71.4 119 71.3 119 0 70-130/30
* = Outside of Control Limits.
44 of 48
LA5932655.2.1
Blank Spike/Blank Spike Duplicate Summary Page 3 of 3
Job Number:LA59326
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2165-BS3 2K0119704.D 1 11/16/19 CP n/a n/a V2K2165
V2K2165-BSD3 2K0119705.D 1 11/16/19 CP n/a n/a V2K2165
The QC reported here applies to the following samples:Method: SM 6200B
LA59326-1, LA59326-2, LA59326-3, LA59326-5, LA59326-6, LA59326-7, LA59326-8, LA59326-9, LA59326-10
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 99%91%70-130%
2037-26-5 Toluene-D8 102%103%70-130%
460-00-4 4-Bromofluorobenzene 104%103%70-130%
* = Outside of Control Limits.
45 of 48
LA5932655.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:LA59326
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA59290-9MS 2K0119713.D 100 11/16/19 CP n/a n/a V2K2165
LA59290-9MSD 2K0119714.D 100 11/16/19 CP n/a n/a V2K2165
LA59290-9 2K0119712.D 50 11/16/19 CP n/a n/a V2K2165
The QC reported here applies to the following samples:Method: SM 6200B
LA59326-1, LA59326-2, LA59326-3, LA59326-5, LA59326-6, LA59326-7, LA59326-8, LA59326-9, LA59326-10
LA59290-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 5000 3650 73 5000 3530 71 3 70-130/20
71-43-2 Benzene 3290 2000 4850 78 2000 4780 75 1 70-130/20
108-86-1 Bromobenzene ND 2000 2120 106 2000 2020 101 5 70-130/20
74-97-5 Bromochloromethane ND 2000 2030 102 2000 1960 98 4 70-130/20
75-27-4 Bromodichloromethane ND 2000 2320 116 2000 2230 112 4 70-130/20
75-25-2 Bromoform ND 2000 1970 99 2000 1920 96 3 70-130/20
104-51-8 n-Butylbenzene 12.1 2000 2150 107 2000 2070 103 4 70-130/20
135-98-8 sec-Butylbenzene ND 2000 2270 114 2000 2180 109 4 70-130/20
98-06-6 tert-Butylbenzene ND 2000 2340 117 2000 2250 113 4 70-130/20
56-23-5 Carbon Tetrachloride ND 2000 2200 110 2000 2080 104 6 70-130/20
108-90-7 Chlorobenzene ND 2000 2090 105 2000 1990 100 5 70-130/20
75-00-3 Chloroethane ND 2000 2050 103 2000 1970 99 4 60-140/20
67-66-3 Chloroform ND 2000 2050 103 2000 2000 100 2 70-130/20
95-49-8 o-Chlorotoluene ND 2000 2190 110 2000 2090 105 5 70-130/20
106-43-4 p-Chlorotoluene ND 2000 2200 110 2000 2120 106 4 70-130/20
124-48-1 Dibromochloromethane ND 2000 2030 102 2000 1940 97 5 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 2000 1960 98 2000 1970 99 1 70-130/20
106-93-4 1,2-Dibromoethane ND 2000 2260 113 2000 2170 109 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 2000 1740 87 2000 1600 80 8 60-140/20
541-73-1 m-Dichlorobenzene ND 2000 1960 98 2000 1870 94 5 70-130/20
95-50-1 o-Dichlorobenzene ND 2000 2050 103 2000 1950 98 5 70-130/20
106-46-7 p-Dichlorobenzene ND 2000 1930 97 2000 1840 92 5 70-130/20
75-34-3 1,1-Dichloroethane ND 2000 2130 107 2000 2060 103 3 70-130/20
107-06-2 1,2-Dichloroethane ND 2000 1950 98 2000 1900 95 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 2000 2070 104 2000 1970 99 5 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 2000 2060 103 2000 1980 99 4 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 2000 2030 102 2000 1950 98 4 70-130/20
78-87-5 1,2-Dichloropropane ND 2000 2180 109 2000 2100 105 4 70-130/20
142-28-9 1,3-Dichloropropane ND 2000 2170 109 2000 2120 106 2 70-130/20
594-20-7 2,2-Dichloropropane ND 2000 855 43*2000 821 41*4 70-130/20
563-58-6 1,1-Dichloropropene ND 2000 2070 104 2000 1990 100 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 2000 1750 88 2000 1690 85 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 2000 1740 87 2000 1700 85 2 70-130/20
108-20-3 Di-Isopropyl Ether ND 2000 2210 111 2000 2140 107 3 70-130/20
64-17-5 Ethyl Alcohol ND 40000 41600 104 40000 50400 126 19 70-130/20
100-41-4 Ethylbenzene 1030 2000 3090 103 2000 2960 97 4 70-130/20
* = Outside of Control Limits.
46 of 48
LA5932655.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:LA59326
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA59290-9MS 2K0119713.D 100 11/16/19 CP n/a n/a V2K2165
LA59290-9MSD 2K0119714.D 100 11/16/19 CP n/a n/a V2K2165
LA59290-9 2K0119712.D 50 11/16/19 CP n/a n/a V2K2165
The QC reported here applies to the following samples:Method: SM 6200B
LA59326-1, LA59326-2, LA59326-3, LA59326-5, LA59326-6, LA59326-7, LA59326-8, LA59326-9, LA59326-10
LA59290-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 5000 4670 93 5000 4690 94 0 70-130/20
87-68-3 Hexachlorobutadiene ND 2000 1700 85 2000 1680 84 1 70-130/20
98-82-8 Isopropylbenzene 44.5 2000 2070 101 2000 1980 97 4 70-130/20
99-87-6 p-Isopropyltoluene ND 2000 2200 110 2000 2100 105 5 70-130/20
74-83-9 Methyl Bromide ND 2000 1380 69 2000 1700 85 21*60-140/20
74-87-3 Methyl Chloride ND 2000 1910 96 2000 1950 98 2 60-140/20
74-95-3 Methylene Bromide ND 2000 2150 108 2000 2020 101 6 70-130/20
75-09-2 Methylene Chloride 19.8 2000 1930 96 2000 1870 93 3 70-130/20
78-93-3 Methyl Ethyl Ketone ND 5000 3760 75 5000 3630 73 4 70-130/20
108-10-1 4-Methyl-2-pentanone ND 5000 4940 99 5000 4790 96 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether 270 2000 2490 111 2000 2460 110 1 70-130/20
91-20-3 Naphthalene 217 2000 2250 102 2000 2260 102 0 70-130/20
103-65-1 n-Propylbenzene 105 2000 2290 109 2000 2190 104 4 70-130/20
100-42-5 Styrene ND 2000 2030 102 2000 1960 98 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 2000 2340 117 2000 2230 112 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 2000 2120 106 2000 2050 103 3 70-130/20
127-18-4 Tetrachloroethylene ND 2000 1920 96 2000 1800 90 6 70-130/20
108-88-3 Toluene 134 2000 2190 103 2000 2110 99 4 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 2000 2120 106 2000 2170 109 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 2000 2130 107 2000 2090 105 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 2000 2210 111 2000 2120 106 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 2000 2110 106 2000 2010 101 5 70-130/20
79-01-6 Trichloroethylene ND 2000 2040 102 2000 1960 98 4 70-130/20
75-69-4 Trichlorofluoromethane ND 2000 1970 99 2000 1890 95 4 60-140/20
96-18-4 1,2,3-Trichloropropane ND 2000 1930 97 2000 2040 102 6 70-130/20
95-63-6 1,2,4-Trimethylbenzene 726 2000 2980 113 2000 2860 107 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 231 2000 2520 114 2000 2410 109 4 70-130/20
108-05-4 Vinyl Acetate ND 2000 2550 128 2000 2530 127 1 70-130/20
75-01-4 Vinyl Chloride ND 2000 2020 101 2000 2000 100 1 60-140/20
m,p-Xylene 2150 4000 6330 105 4000 6110 99 4 70-130/20
95-47-6 o-Xylene 1010 2000 3350 117 2000 3240 112 3 70-130/20
1330-20-7 Xylene (total)3170 6000 9680 109 6000 9350 103 3 70-130/20
* = Outside of Control Limits.
47 of 48
LA5932655.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:LA59326
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA59290-9MS 2K0119713.D 100 11/16/19 CP n/a n/a V2K2165
LA59290-9MSD 2K0119714.D 100 11/16/19 CP n/a n/a V2K2165
LA59290-9 2K0119712.D 50 11/16/19 CP n/a n/a V2K2165
The QC reported here applies to the following samples:Method: SM 6200B
LA59326-1, LA59326-2, LA59326-3, LA59326-5, LA59326-6, LA59326-7, LA59326-8, LA59326-9, LA59326-10
CAS No.Surrogate Recoveries MS MSD LA59290-9 Limits
17060-07-0 1,2-Dichloroethane-D4 97%97%97%70-130%
2037-26-5 Toluene-D8 102%103%100%70-130%
460-00-4 4-Bromofluorobenzene 103%103%99%70-130%
* = Outside of Control Limits.
48 of 48
LA5932655.3.1
11/27/19
Technical Report for
ATC Group Services LLC
Mayo's Grocery 416 US Hwy 301, Garysboro, NC
SGS Job Number: LA59603
Sampling Date: 11/20/19
Report to:
ATC Group Services LLC.
2725 East Millbrook Road Suite 121
Raleigh, NC 27604
[e-mail]; [e-mail]
ATTN: liz Allyn
Total number of pages in report:
Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), AZ(AZ0805), FL(E87657), IL(200082), KY(#31),
NC(487), SC(73004001), NJ(LA007), TX(T104704186-18-16), WV(257)
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 500 Ambassador Caffery • Scott, LA 70583 • tel: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Amy Jackson 337-237-4775
Ron Benjamin
Lab Director
Scott, LA 11/27/19
e-Hardcopy 2.0
Automated Report
22
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 22
LA59603
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: LA59603-1: MW5 ........................................................................................................6
Section 4: Misc. Forms ............................................................................................................9
4.1: Chain of Custody ...........................................................................................................10
Section 5: MS Volatiles - QC Data Summaries .....................................................................13
5.1: Method Blank Summary ................................................................................................14
5.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................17
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................20 123452 of 22
LA59603
SGS North America Inc.
Sample Summary
ATC Group Services LLC
Job No:LA59603
Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the RL
LA59603-1 11/20/19 13:00 CH 11/22/19 AQ Ground Water MW5
3 of 22
LA596031
Summary of Hits Page 1 of 1
Job Number:LA59603
Account:ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Collected:11/20/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA59603-1 MW5
Hexachlorobutadiene 0.43 0.20 ug/l SM 6200B
4 of 22
LA596032
SGS North America Inc.
Sample Results
Report of Analysis
Scott, LA
Section 3
5 of 22
LA596033
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW5
Lab Sample ID:LA59603-1 Date Sampled:11/20/19
Matrix:AQ - Ground Water Date Received:11/22/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0120073.D 1 11/26/19 15:06 CP n/a n/a V2K2179
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 22
LA5960333.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW5
Lab Sample ID:LA59603-1 Date Sampled:11/20/19
Matrix:AQ - Ground Water Date Received:11/22/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene 0.43 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 22
LA5960333.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW5
Lab Sample ID:LA59603-1 Date Sampled:11/20/19
Matrix:AQ - Ground Water Date Received:11/22/19
Method:SM 6200B Percent Solids:n/a
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 91%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 22
LA5960333.1
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Scott, LA
Section 4
9 of 22
LA596034
LA59603: Chain of Custody
Page 1 of 3
10 of 22
LA5960344.1
LA59603: Chain of Custody
Page 2 of 3
11 of 22
LA5960344.1
SGS Sample Receipt Summary
Job Number:LA59603 Client:ATC
Date / Time Received:11/22/2019 9:50:00 AM Delivery Method:FedEx
Project:MAYO GROCERY
4. No. Coolers:1
Airbill #'s:4913 8690 9788
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Thermometer ID:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
DV439;
Ice (direct contact)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Initial/Adjusted):#1: (1.6/1.6); DV439
LA59603: Chain of Custody
Page 3 of 3
12 of 22
LA5960344.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Scott, LA
Section 5
13 of 22
LA596035
Method Blank Summary Page 1 of 3
Job Number:LA59603
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2179-MB1 2K0120066.D 1 11/26/19 CP n/a n/a V2K2179
The QC reported here applies to the following samples:Method: SM 6200B
LA59603-1
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene 0.18 0.50 ug/l J
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol 16.4 50 ug/l J
100-41-4 Ethylbenzene ND 0.50 ug/l
14 of 22
LA5960355.1.1
Method Blank Summary Page 2 of 3
Job Number:LA59603
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2179-MB1 2K0120066.D 1 11/26/19 CP n/a n/a V2K2179
The QC reported here applies to the following samples:Method: SM 6200B
LA59603-1
CAS No.Compound Result RL Units Q
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene 0.41 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride 0.21 0.50 ug/l J
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene 0.20 0.50 ug/l J
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.45 0.50 ug/l J
120-82-1 1,2,4-Trichlorobenzene 0.34 0.50 ug/l J
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
15 of 22
LA5960355.1.1
Method Blank Summary Page 3 of 3
Job Number:LA59603
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2179-MB1 2K0120066.D 1 11/26/19 CP n/a n/a V2K2179
The QC reported here applies to the following samples:Method: SM 6200B
LA59603-1
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 92%70-130%
16 of 22
LA5960355.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 3
Job Number:LA59603
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2179-BS2 2K0120070.D 1 11/26/19 CP n/a n/a V2K2179
V2K2179-BSD2 2K0120071.D 1 11/26/19 CP n/a n/a V2K2179
The QC reported here applies to the following samples:Method: SM 6200B
LA59603-1
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
67-64-1 Acetone 50 67.4 135*64.8 130 4 70-130/30
71-43-2 Benzene 20 19.7 99 18.2 91 8 70-130/30
108-86-1 Bromobenzene 20 21.6 108 20.3 102 6 70-130/30
74-97-5 Bromochloromethane 20 25.1 126 23.6 118 6 70-130/30
75-27-4 Bromodichloromethane 20 24.7 124 23.0 115 7 70-130/30
75-25-2 Bromoform 20 19.2 96 18.2 91 5 70-130/30
104-51-8 n-Butylbenzene 20 25.8 129 24.4 122 6 70-130/30
135-98-8 sec-Butylbenzene 20 24.8 124 23.0 115 8 70-130/30
98-06-6 tert-Butylbenzene 20 24.3 122 22.5 113 8 70-130/30
56-23-5 Carbon Tetrachloride 20 27.9 140*25.4 127 9 70-130/30
108-90-7 Chlorobenzene 20 21.8 109 20.3 102 7 70-130/30
75-00-3 Chloroethane 20 26.0 130 24.2 121 7 60-140/30
67-66-3 Chloroform 20 25.9 130 23.8 119 8 70-130/30
95-49-8 o-Chlorotoluene 20 22.8 114 21.0 105 8 70-130/30
106-43-4 p-Chlorotoluene 20 23.8 119 21.7 109 9 70-130/30
124-48-1 Dibromochloromethane 20 20.2 101 18.9 95 7 70-130/30
96-12-8 1,2-Dibromo-3-chloropropane 20 19.2 96 18.9 95 2 70-130/30
106-93-4 1,2-Dibromoethane 20 23.0 115 21.4 107 7 70-130/30
75-71-8 Dichlorodifluoromethane 20 22.8 114 21.9 110 4 60-140/30
541-73-1 m-Dichlorobenzene 20 20.8 104 19.2 96 8 70-130/30
95-50-1 o-Dichlorobenzene 20 20.8 104 19.4 97 7 70-130/30
106-46-7 p-Dichlorobenzene 20 20.5 103 19.2 96 7 70-130/30
75-34-3 1,1-Dichloroethane 20 27.0 135*25.0 125 8 70-130/30
107-06-2 1,2-Dichloroethane 20 21.2 106 20.1 101 5 70-130/30
75-35-4 1,1-Dichloroethylene 20 28.0 140*25.2 126 11 70-130/30
156-59-2 cis-1,2-Dichloroethylene 20 26.5 133*24.2 121 9 70-130/30
156-60-5 trans-1,2-Dichloroethylene 20 27.8 139*25.6 128 8 70-130/30
78-87-5 1,2-Dichloropropane 20 23.8 119 22.4 112 6 70-130/30
142-28-9 1,3-Dichloropropane 20 22.2 111 21.2 106 5 70-130/30
594-20-7 2,2-Dichloropropane 20 37.5 188*33.6 168*11 70-130/30
563-58-6 1,1-Dichloropropene 20 28.1 141*25.9 130 8 70-130/30
10061-01-5 cis-1,3-Dichloropropene 20 22.6 113 21.0 105 7 70-130/30
10061-02-6 trans-1,3-Dichloropropene 20 21.8 109 20.6 103 6 70-130/30
108-20-3 Di-Isopropyl Ether 20 27.4 137*25.8 129 6 70-130/30
64-17-5 Ethyl Alcohol 400 552 138*544 136*1 70-130/30
100-41-4 Ethylbenzene 20 22.9 115 21.4 107 7 70-130/30
* = Outside of Control Limits.
17 of 22
LA5960355.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 3
Job Number:LA59603
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2179-BS2 2K0120070.D 1 11/26/19 CP n/a n/a V2K2179
V2K2179-BSD2 2K0120071.D 1 11/26/19 CP n/a n/a V2K2179
The QC reported here applies to the following samples:Method: SM 6200B
LA59603-1
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
591-78-6 2-Hexanone 50 57.5 115 56.1 112 2 70-130/30
87-68-3 Hexachlorobutadiene 20 21.8 109 21.3 107 2 70-130/30
98-82-8 Isopropylbenzene 20 21.4 107 19.9 100 7 70-130/30
99-87-6 p-Isopropyltoluene 20 24.3 122 22.7 114 7 70-130/30
74-83-9 Methyl Bromide 20 18.0 90 20.2 101 12 60-140/30
74-87-3 Methyl Chloride 20 23.0 115 22.3 112 3 60-140/30
74-95-3 Methylene Bromide 20 23.3 117 21.4 107 9 70-130/30
75-09-2 Methylene Chloride 20 24.3 122 22.4 112 8 70-130/30
78-93-3 Methyl Ethyl Ketone 50 60.1 120 56.4 113 6 70-130/30
108-10-1 4-Methyl-2-pentanone 50 54.4 109 51.6 103 5 70-130/30
1634-04-4 Methyl Tert Butyl Ether 20 26.0 130 24.8 124 5 70-130/30
91-20-3 Naphthalene 20 18.7 94 18.9 95 1 70-130/30
103-65-1 n-Propylbenzene 20 23.9 120 21.9 110 9 70-130/30
100-42-5 Styrene 20 21.3 107 19.9 100 7 70-130/30
630-20-6 1,1,1,2-Tetrachloroethane 20 23.6 118 22.0 110 7 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 20 21.4 107 19.8 99 8 70-130/30
127-18-4 Tetrachloroethylene 20 21.5 108 19.7 99 9 70-130/30
108-88-3 Toluene 20 21.5 108 20.2 101 6 70-130/30
87-61-6 1,2,3-Trichlorobenzene 20 22.0 110 22.2 111 1 70-130/30
120-82-1 1,2,4-Trichlorobenzene 20 22.9 115 22.4 112 2 70-130/30
71-55-6 1,1,1-Trichloroethane 20 27.7 139*25.3 127 9 70-130/30
79-00-5 1,1,2-Trichloroethane 20 21.4 107 20.1 101 6 70-130/30
79-01-6 Trichloroethylene 20 23.4 117 21.6 108 8 70-130/30
75-69-4 Trichlorofluoromethane 20 25.4 127 23.9 120 6 60-140/30
96-18-4 1,2,3-Trichloropropane 20 20.9 105 19.9 100 5 70-130/30
95-63-6 1,2,4-Trimethylbenzene 20 24.1 121 22.4 112 7 70-130/30
108-67-8 1,3,5-Trimethylbenzene 20 24.3 122 22.4 112 8 70-130/30
108-05-4 Vinyl Acetate 20 34.2 171*32.7 164*4 70-130/30
75-01-4 Vinyl Chloride 20 25.5 128 24.4 122 4 60-140/30
m,p-Xylene 40 47.6 119 44.5 111 7 70-130/30
95-47-6 o-Xylene 20 25.1 126 23.4 117 7 70-130/30
1330-20-7 Xylene (total)60 72.7 121 67.8 113 7 70-130/30
* = Outside of Control Limits.
18 of 22
LA5960355.2.1
Blank Spike/Blank Spike Duplicate Summary Page 3 of 3
Job Number:LA59603
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2179-BS2 2K0120070.D 1 11/26/19 CP n/a n/a V2K2179
V2K2179-BSD2 2K0120071.D 1 11/26/19 CP n/a n/a V2K2179
The QC reported here applies to the following samples:Method: SM 6200B
LA59603-1
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 104%106%70-130%
2037-26-5 Toluene-D8 102%103%70-130%
460-00-4 4-Bromofluorobenzene 103%104%70-130%
* = Outside of Control Limits.
19 of 22
LA5960355.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:LA59603
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA59603-1MS 2K0120082.D 5 11/26/19 CP n/a n/a V2K2179
LA59603-1MSD 2K0120083.D 5 11/26/19 CP n/a n/a V2K2179
LA59603-1 2K0120073.D 1 11/26/19 CP n/a n/a V2K2179
The QC reported here applies to the following samples:Method: SM 6200B
LA59603-1
LA59603-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 250 178 71 250 176 70 1 70-130/20
71-43-2 Benzene ND 100 95.2 95 100 94.7 95 1 70-130/20
108-86-1 Bromobenzene ND 100 105 105 100 103 103 2 70-130/20
74-97-5 Bromochloromethane ND 100 120 120 100 118 118 2 70-130/20
75-27-4 Bromodichloromethane ND 100 120 120 100 118 118 2 70-130/20
75-25-2 Bromoform ND 100 93.7 94 100 88.3 88 6 70-130/20
104-51-8 n-Butylbenzene ND 100 115 115 100 119 119 3 70-130/20
135-98-8 sec-Butylbenzene ND 100 116 116 100 119 119 3 70-130/20
98-06-6 tert-Butylbenzene ND 100 116 116 100 119 119 3 70-130/20
56-23-5 Carbon Tetrachloride ND 100 133 133*100 131 131*2 70-130/20
108-90-7 Chlorobenzene ND 100 105 105 100 102 102 3 70-130/20
75-00-3 Chloroethane ND 100 125 125 100 122 122 2 60-140/20
67-66-3 Chloroform ND 100 121 121 100 120 120 1 70-130/20
95-49-8 o-Chlorotoluene ND 100 109 109 100 110 110 1 70-130/20
106-43-4 p-Chlorotoluene ND 100 112 112 100 113 113 1 70-130/20
124-48-1 Dibromochloromethane ND 100 98.8 99 100 94.0 94 5 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 100 88.2 88 100 89.2 89 1 70-130/20
106-93-4 1,2-Dibromoethane ND 100 112 112 100 107 107 5 70-130/20
75-71-8 Dichlorodifluoromethane ND 100 110 110 100 107 107 3 60-140/20
541-73-1 m-Dichlorobenzene ND 100 98.5 99 100 99.9 100 1 70-130/20
95-50-1 o-Dichlorobenzene ND 100 99.1 99 100 100 100 1 70-130/20
106-46-7 p-Dichlorobenzene ND 100 97.6 98 100 98.8 99 1 70-130/20
75-34-3 1,1-Dichloroethane ND 100 128 128 100 128 128 0 70-130/20
107-06-2 1,2-Dichloroethane ND 100 107 107 100 102 102 5 70-130/20
75-35-4 1,1-Dichloroethylene ND 100 132 132*100 130 130 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 100 124 124 100 123 123 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 100 132 132*100 128 128 3 70-130/20
78-87-5 1,2-Dichloropropane ND 100 114 114 100 113 113 1 70-130/20
142-28-9 1,3-Dichloropropane ND 100 108 108 100 106 106 2 70-130/20
594-20-7 2,2-Dichloropropane ND 100 135 135*100 137 137*1 70-130/20
563-58-6 1,1-Dichloropropene ND 100 131 131*100 130 130 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 100 102 102 100 100 100 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 100 99.7 100 100 96.7 97 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 100 128 128 100 129 129 1 70-130/20
64-17-5 Ethyl Alcohol ND 2000 2430 122 2000 2600 130 7 70-130/20
100-41-4 Ethylbenzene ND 100 110 110 100 109 109 1 70-130/20
* = Outside of Control Limits.
20 of 22
LA5960355.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:LA59603
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA59603-1MS 2K0120082.D 5 11/26/19 CP n/a n/a V2K2179
LA59603-1MSD 2K0120083.D 5 11/26/19 CP n/a n/a V2K2179
LA59603-1 2K0120073.D 1 11/26/19 CP n/a n/a V2K2179
The QC reported here applies to the following samples:Method: SM 6200B
LA59603-1
LA59603-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 250 234 94 250 221 88 6 70-130/20
87-68-3 Hexachlorobutadiene 0.43 100 90.6 90 100 94.8 94 5 70-130/20
98-82-8 Isopropylbenzene ND 100 102 102 100 101 101 1 70-130/20
99-87-6 p-Isopropyltoluene ND 100 113 113 100 115 115 2 70-130/20
74-83-9 Methyl Bromide ND 100 87.8 88 100 107 107 20 60-140/20
74-87-3 Methyl Chloride ND 100 105 105 100 110 110 5 60-140/20
74-95-3 Methylene Bromide ND 100 113 113 100 110 110 3 70-130/20
75-09-2 Methylene Chloride ND 100 115 115 100 114 114 1 70-130/20
78-93-3 Methyl Ethyl Ketone ND 250 222 89 250 224 90 1 70-130/20
108-10-1 4-Methyl-2-pentanone ND 250 254 102 250 250 100 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 100 122 122 100 122 122 0 70-130/20
91-20-3 Naphthalene 0.17 100 86.4 86 100 91.0 91 5 70-130/20
103-65-1 n-Propylbenzene ND 100 112 112 100 114 114 2 70-130/20
100-42-5 Styrene ND 100 101 101 100 98.3 98 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 100 115 115 100 112 112 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 100 104 104 100 103 103 1 70-130/20
127-18-4 Tetrachloroethylene ND 100 103 103 100 99.0 99 4 70-130/20
108-88-3 Toluene ND 100 104 104 100 102 102 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene 0.43 100 101 101 100 107 107 6 70-130/20
120-82-1 1,2,4-Trichlorobenzene 0.31 100 104 104 100 109 109 5 70-130/20
71-55-6 1,1,1-Trichloroethane ND 100 132 132*100 132 132*0 70-130/20
79-00-5 1,1,2-Trichloroethane ND 100 105 105 100 102 102 3 70-130/20
79-01-6 Trichloroethylene ND 100 112 112 100 110 110 2 70-130/20
75-69-4 Trichlorofluoromethane ND 100 124 124 100 122 122 2 60-140/20
96-18-4 1,2,3-Trichloropropane ND 100 102 102 100 99.2 99 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 100 111 111 100 114 114 3 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 100 112 112 100 114 114 2 70-130/20
108-05-4 Vinyl Acetate ND 100 165 165*100 162 162*2 70-130/20
75-01-4 Vinyl Chloride ND 100 121 121 100 121 121 0 60-140/20
m,p-Xylene ND 200 229 115 200 223 112 3 70-130/20
95-47-6 o-Xylene ND 100 119 119 100 118 118 1 70-130/20
1330-20-7 Xylene (total)ND 300 348 116 300 341 114 2 70-130/20
* = Outside of Control Limits.
21 of 22
LA5960355.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:LA59603
Account:ATCNCR ATC Group Services LLC
Project:Mayo's Grocery 416 US Hwy 301, Garysboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA59603-1MS 2K0120082.D 5 11/26/19 CP n/a n/a V2K2179
LA59603-1MSD 2K0120083.D 5 11/26/19 CP n/a n/a V2K2179
LA59603-1 2K0120073.D 1 11/26/19 CP n/a n/a V2K2179
The QC reported here applies to the following samples:Method: SM 6200B
LA59603-1
CAS No.Surrogate Recoveries MS MSD LA59603-1 Limits
17060-07-0 1,2-Dichloroethane-D4 101%100%102%70-130%
2037-26-5 Toluene-D8 101%102%94%70-130%
460-00-4 4-Bromofluorobenzene 103%102%91%70-130%
* = Outside of Control Limits.
22 of 22
LA5960355.3.1

APPENDIX C

MANN-KENDALL ANALYSES

Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:ug/L
Sampling Point ID:Benzene Xylenes Naphthalene
Sampling Sampling
Event Date
1 11/30/2007 4,170 1,061 222
2 12/18/2014 500 130 150
3 9/10/2015 1.2 7 7.4
4 9/20/2017 72 56.6 96
5 7/9/2018 44.7 3.6 22.9
6 5/10/2019 52.8 3.4 31.0
7 11/11/2019 176 2.50 2.7
8
9
10
11
12
13
14
15
16
17
18
19
20
Coefficient of Variation:2.14 2.17 1.10
Mann-Kendall Statistic (S):-5 -19 -13
Confidence Factor:71.9%99.9%96.5%
Concentration Trend:No Trend Decreasing Decreasing
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water, 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
MW-2 CONCENTRATION (ug/L)
GSI Environmental Inc., www.gsi-net.com
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
11-Nov-19 Incident #11818
Mayo's Grocery MW-2
ATC Associates of North Carolina, P.C.
1
10
100
1000
10000
10/06 02/08 07/09 11/10 04/12 08/13 12/14 05/16 09/17 02/19 06/20Concentration (ug/L)Sampling Date
Benzene
Xylenes
Naphthalene
Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:ug/L
Sampling Point ID:Benzene Naphthalene
Sampling Sampling
Event Date
1 12/18/2014 4 24
2 9/20/2017 4.3 0.35
3 7/9/2018 1.1 6.6
4 5/10/2019 0.57 6.2
5 11/11/2019 0.25 4.4
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Coefficient of Variation:0.95 1.10
Mann-Kendall Statistic (S):-8 -4
Confidence Factor:95.8%75.8%
Concentration Trend:Decreasing No Trend
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water, 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
MW-7 CONCENTRATION (ug/L)
GSI Environmental Inc., www.gsi-net.com
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
11-Nov-19 Incident #11818
Mayo's Grocery MW-7
ATC Associates of North Carolina, P.C.
0.1
1
10
100
06/14 12/14 07/15 01/16 08/16 03/17 09/17 04/18 10/18 05/19 12/19 06/20Concentration (ug/L)Sampling Date
Benzene
Naphthalene
Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:ug/L
Sampling Point ID:Benzene Xylenes Naphthalene
Sampling Sampling
Event Date
1 9/10/2015 310 1,350 120
2 9/20/2017 5.4 44.8 90
3 7/9/2018 1.2 1.5 8.2
4 5/10/2019 16.1 35.6 89.0
5 11/11/2019 2.1 0.5 1.7
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Coefficient of Variation:2.03 2.08 0.86
Mann-Kendall Statistic (S):-4 -8 -8
Confidence Factor:75.8%95.8%95.8%
Concentration Trend:No Trend Decreasing Decreasing
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water, 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
MW-9 CONCENTRATION (ug/L)
GSI Environmental Inc., www.gsi-net.com
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
11-Nov-19 Incident #11818
Mayo's Grocery MW-9
ATC Associates of North Carolina, P.C.
0.1
1
10
100
1000
10000
12/14 07/15 01/16 08/16 03/17 09/17 04/18 10/18 05/19 12/19 06/20Concentration (ug/L)Sampling Date
Benzene
Xylenes
Naphthalene
Evaluation Date:Job ID:
Facility Name:Constituent:
Conducted By:Concentration Units:ug/L
Sampling Point ID:Benzene Ethylbenzene Xylenes Naphthalene
Sampling Sampling
Event Date
1 9/10/2015 110 770 2,900 190
2 9/20/2017 9.2 300 15.3 150
3 7/9/2018 0.5 2.8 0.5 2.0
4 5/10/2019 5.5 64.2 0.5 8.1
5 11/11/2019 2.2 70.3 14.6 45.1
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Coefficient of Variation:1.86 1.31 2.21 1.09
Mann-Kendall Statistic (S):-6 -4 -5 -4
Confidence Factor:88.3%75.8%82.1%75.8%
Concentration Trend:No Trend No Trend No Trend No Trend
Notes:
1.At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2.Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
≥ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S≤0, and COV ≥ 1 = No Trend; < 90% and COV < 1 = Stable.
3.Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water, 41(3):355-367, 2003.
DISCLAIMER: The GSI Mann-Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
MW-10 CONCENTRATION (ug/L)
GSI Environmental Inc., www.gsi-net.com
GSI MANN-KENDALL TOOLKIT
for Constituent Trend Analysis
11-Nov-19 Incident #11818
Mayo's Grocery MW-10
ATC Associates of North Carolina, P.C.
0.1
1
10
100
1000
10000
12/14 07/15 01/16 08/16 03/17 09/17 04/18 10/18 05/19 12/19 06/20Concentration (ug/L)Sampling Date
Benzene
Ethylbenzene
Xylenes
Naphthalene