RA-1706_10508_CA_LAB_20200213

02/13/20
Technical Report for
ATC Group Services LLC
Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
SLP1050804
SGS Job Number: LA61492
Sampling Date: 02/05/20
Report to:
ATC Group Services LLC.
2725 East Millbrook Road Suite 121
Raleigh, NC 27604
[e-mail]; [e-mail]
ATTN: Gabe Araos
Total number of pages in report:
Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), AZ(AZ0805), FL(E87657), IL(200082), KY(#31),
NC(487), SC(73004001), NJ(LA007), TX(T104704186-18-16), WV(257)
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 500 Ambassador Caffery • Scott, LA 70583 • tel: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Amy Jackson 337-237-4775
Ron Benjamin
Lab Director
Scott, LA 02/13/20
e-Hardcopy 2.0
Automated Report
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SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
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1 of 59
LA61492
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: LA61492-1: MW1 ........................................................................................................7
3.2: LA61492-2: MW2 ........................................................................................................10
3.3: LA61492-3: MW3 ........................................................................................................13
3.4: LA61492-4: MW6 ........................................................................................................16
3.5: LA61492-5: MW9 ........................................................................................................19
3.6: LA61492-6: MW13 ......................................................................................................22
3.7: LA61492-7: MW16D ...................................................................................................25
3.8: LA61492-8: PW1 ..........................................................................................................28
3.9: LA61492-9: PW2 ..........................................................................................................31
3.10: LA61492-10: FIELD BLANK ....................................................................................34
Section 4: Misc. Forms ............................................................................................................37
4.1: Chain of Custody ...........................................................................................................38
Section 5: MS Volatiles - QC Data Summaries .....................................................................41
5.1: Method Blank Summary ................................................................................................42
5.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................48
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................54 123452 of 59
LA61492
SGS North America Inc.
Sample Summary
ATC Group Services LLC
Job No:LA61492
Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Project No: SLP1050804
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the RL
LA61492-1 02/05/20 14:30 TJ 02/07/20 AQ Ground Water MW1
LA61492-2 02/05/20 12:15 TJ 02/07/20 AQ Ground Water MW2
LA61492-3 02/05/20 13:55 TJ 02/07/20 AQ Ground Water MW3
LA61492-4 02/05/20 12:45 TJ 02/07/20 AQ Ground Water MW6
LA61492-5 02/05/20 13:15 TJ 02/07/20 AQ Ground Water MW9
LA61492-6 02/05/20 10:40 TJ 02/07/20 AQ Ground Water MW13
LA61492-7 02/05/20 11:40 TJ 02/07/20 AQ Ground Water MW16D
LA61492-8 02/05/20 10:05 TJ 02/07/20 AQ Ground Water PW1
LA61492-9 02/05/20 14:50 TJ 02/07/20 AQ Ground Water PW2
LA61492-10 02/05/20 13:20 TJ 02/07/20 AQ Field Blank Water FIELD BLANK
3 of 59
LA614921
Summary of Hits Page 1 of 2
Job Number:LA61492
Account:ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Collected:02/05/20
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA61492-1 MW1
Benzene 30.2 10 ug/l SM 6200B
n-Butylbenzene 13.6 10 ug/l SM 6200B
Carbon Tetrachloride 102 4.0 ug/l SM 6200B
Chloroform 24.5 10 ug/l SM 6200B
1,2-Dichloroethane 57.4 4.0 ug/l SM 6200B
Ethylbenzene 590 10 ug/l SM 6200B
Isopropylbenzene 45.5 10 ug/l SM 6200B
Naphthalene 275 10 ug/l SM 6200B
n-Propylbenzene 113 10 ug/l SM 6200B
Toluene 49.6 10 ug/l SM 6200B
1,1,2-Trichloroethane 30.4 6.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 221 10 ug/l SM 6200B
1,3,5-Trimethylbenzene 105 10 ug/l SM 6200B
m,p-Xylene 1400 20 ug/l SM 6200B
o-Xylene 42.2 10 ug/l SM 6200B
Xylene (total)1450 10 ug/l SM 6200B
LA61492-2 MW2
Naphthalene 1.6 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.99 0.50 ug/l SM 6200B
LA61492-3 MW3
Benzene 905 10 ug/l SM 6200B
Carbon Tetrachloride 110 4.0 ug/l SM 6200B
Chloroform 27.2 10 ug/l SM 6200B
1,2-Dichloroethane 63.4 4.0 ug/l SM 6200B
Ethylbenzene 588 10 ug/l SM 6200B
Isopropylbenzene 30.5 10 ug/l SM 6200B
Methyl Chloride 18.6 10 ug/l SM 6200B
Methylene Chloride 11.4 10 ug/l SM 6200B
Naphthalene 155 10 ug/l SM 6200B
n-Propylbenzene 87.9 10 ug/l SM 6200B
Toluene 122 10 ug/l SM 6200B
1,1,2-Trichloroethane 32.5 6.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 488 10 ug/l SM 6200B
1,3,5-Trimethylbenzene 109 10 ug/l SM 6200B
m,p-Xylene 544 20 ug/l SM 6200B
o-Xylene 112 10 ug/l SM 6200B
Xylene (total)656 10 ug/l SM 6200B
4 of 59
LA614922
Summary of Hits Page 2 of 2
Job Number:LA61492
Account:ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Collected:02/05/20
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA61492-4 MW6
No hits reported in this sample.
LA61492-5 MW9
Methyl Tert Butyl Ether 0.78 0.50 ug/l SM 6200B
LA61492-6 MW13
Methyl Tert Butyl Ether 1.1 0.50 ug/l SM 6200B
LA61492-7 MW16D
n-Butylbenzene 0.65 0.50 ug/l SM 6200B
sec-Butylbenzene 1.8 0.50 ug/l SM 6200B
Di-Isopropyl Ether 4.2 0.50 ug/l SM 6200B
Isopropylbenzene 1.0 0.50 ug/l SM 6200B
Methyl Chloride 2.5 0.50 ug/l SM 6200B
Methyl Tert Butyl Ether 6.2 0.50 ug/l SM 6200B
n-Propylbenzene 1.2 0.50 ug/l SM 6200B
Vinyl Acetate 3.4 0.50 ug/l SM 6200B
m,p-Xylene 1.7 1.0 ug/l SM 6200B
Xylene (total)1.9 0.50 ug/l SM 6200B
LA61492-8 PW1
Di-Isopropyl Ether 2.0 0.50 ug/l SM 6200B
Methyl Tert Butyl Ether 9.4 0.50 ug/l SM 6200B
LA61492-9 PW2
Di-Isopropyl Ether 3.8 0.50 ug/l SM 6200B
Methyl Tert Butyl Ether 13.3 0.50 ug/l SM 6200B
LA61492-10 FIELD BLANK
Toluene 0.50 0.50 ug/l SM 6200B
5 of 59
LA614922
SGS North America Inc.
Sample Results
Report of Analysis
Scott, LA
Section 3
6 of 59
LA614923
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW1
Lab Sample ID:LA61492-1 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122641.D 20 02/11/20 17:05 CP n/a n/a V2K2289
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 200 ug/l
71-43-2 Benzene 30.2 10 ug/l
108-86-1 Bromobenzene ND 10 ug/l
74-97-5 Bromochloromethane ND 10 ug/l
75-27-4 Bromodichloromethane ND 10 ug/l
75-25-2 Bromoform ND 10 ug/l
104-51-8 n-Butylbenzene 13.6 10 ug/l
135-98-8 sec-Butylbenzene ND 10 ug/l
98-06-6 tert-Butylbenzene ND 10 ug/l
56-23-5 Carbon Tetrachloride 102 4.0 ug/l
108-90-7 Chlorobenzene ND 10 ug/l
75-00-3 Chloroethane ND 10 ug/l
67-66-3 Chloroform 24.5 10 ug/l
95-49-8 o-Chlorotoluene ND 10 ug/l
106-43-4 p-Chlorotoluene ND 10 ug/l
124-48-1 Dibromochloromethane ND 4.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 10 ug/l
106-93-4 1,2-Dibromoethane ND 10 ug/l
75-71-8 Dichlorodifluoromethane ND 10 ug/l
541-73-1 m-Dichlorobenzene ND 10 ug/l
95-50-1 o-Dichlorobenzene ND 10 ug/l
106-46-7 p-Dichlorobenzene ND 10 ug/l
75-34-3 1,1-Dichloroethane ND 10 ug/l
107-06-2 1,2-Dichloroethane 57.4 4.0 ug/l
75-35-4 1,1-Dichloroethylene ND 10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 ug/l
78-87-5 1,2-Dichloropropane ND 6.0 ug/l
142-28-9 1,3-Dichloropropane ND 10 ug/l
594-20-7 2,2-Dichloropropane ND 10 ug/l
563-58-6 1,1-Dichloropropene ND 10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 4.0 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 59
LA6149233.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW1
Lab Sample ID:LA61492-1 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.0 ug/l
108-20-3 Di-Isopropyl Ether ND 10 ug/l
64-17-5 Ethyl Alcohol ND 1000 ug/l
100-41-4 Ethylbenzene 590 10 ug/l
591-78-6 2-Hexanone ND 20 ug/l
87-68-3 Hexachlorobutadiene ND 4.0 ug/l
98-82-8 Isopropylbenzene 45.5 10 ug/l
99-87-6 p-Isopropyltoluene ND 10 ug/l
74-83-9 Methyl Bromide ND 10 ug/l
74-87-3 Methyl Chloride ND 10 ug/l
74-95-3 Methylene Bromide ND 10 ug/l
75-09-2 Methylene Chloride ND 10 ug/l
78-93-3 Methyl Ethyl Ketone ND 500 ug/l
108-10-1 4-Methyl-2-pentanone ND 10 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 10 ug/l
91-20-3 Naphthalene 275 10 ug/l
103-65-1 n-Propylbenzene 113 10 ug/l
100-42-5 Styrene ND 10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 4.0 ug/l
127-18-4 Tetrachloroethylene ND 10 ug/l
108-88-3 Toluene 49.6 10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 ug/l
79-00-5 1,1,2-Trichloroethane 30.4 6.0 ug/l
79-01-6 Trichloroethylene ND 10 ug/l
75-69-4 Trichlorofluoromethane ND 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 ug/l
95-63-6 1,2,4-Trimethylbenzene 221 10 ug/l
108-67-8 1,3,5-Trimethylbenzene 105 10 ug/l
108-05-4 Vinyl Acetate ND 10 ug/l
75-01-4 Vinyl Chloride ND 2.0 ug/l
m,p-Xylene 1400 20 ug/l
95-47-6 o-Xylene 42.2 10 ug/l
1330-20-7 Xylene (total)1450 10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 59
LA6149233.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW1
Lab Sample ID:LA61492-1 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 59
LA6149233.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW2
Lab Sample ID:LA61492-2 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122652.D 1 02/11/20 22:42 CP n/a n/a V2K2289
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 59
LA6149233.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW2
Lab Sample ID:LA61492-2 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene 1.6 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.99 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 59
LA6149233.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW2
Lab Sample ID:LA61492-2 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 59
LA6149233.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW3
Lab Sample ID:LA61492-3 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122642.D 20 02/11/20 17:35 CP n/a n/a V2K2289
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 200 ug/l
71-43-2 Benzene 905 10 ug/l
108-86-1 Bromobenzene ND 10 ug/l
74-97-5 Bromochloromethane ND 10 ug/l
75-27-4 Bromodichloromethane ND 10 ug/l
75-25-2 Bromoform ND 10 ug/l
104-51-8 n-Butylbenzene ND 10 ug/l
135-98-8 sec-Butylbenzene ND 10 ug/l
98-06-6 tert-Butylbenzene ND 10 ug/l
56-23-5 Carbon Tetrachloride 110 4.0 ug/l
108-90-7 Chlorobenzene ND 10 ug/l
75-00-3 Chloroethane ND 10 ug/l
67-66-3 Chloroform 27.2 10 ug/l
95-49-8 o-Chlorotoluene ND 10 ug/l
106-43-4 p-Chlorotoluene ND 10 ug/l
124-48-1 Dibromochloromethane ND 4.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 10 ug/l
106-93-4 1,2-Dibromoethane ND 10 ug/l
75-71-8 Dichlorodifluoromethane ND 10 ug/l
541-73-1 m-Dichlorobenzene ND 10 ug/l
95-50-1 o-Dichlorobenzene ND 10 ug/l
106-46-7 p-Dichlorobenzene ND 10 ug/l
75-34-3 1,1-Dichloroethane ND 10 ug/l
107-06-2 1,2-Dichloroethane 63.4 4.0 ug/l
75-35-4 1,1-Dichloroethylene ND 10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 ug/l
78-87-5 1,2-Dichloropropane ND 6.0 ug/l
142-28-9 1,3-Dichloropropane ND 10 ug/l
594-20-7 2,2-Dichloropropane ND 10 ug/l
563-58-6 1,1-Dichloropropene ND 10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 4.0 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 59
LA6149233.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW3
Lab Sample ID:LA61492-3 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.0 ug/l
108-20-3 Di-Isopropyl Ether ND 10 ug/l
64-17-5 Ethyl Alcohol ND 1000 ug/l
100-41-4 Ethylbenzene 588 10 ug/l
591-78-6 2-Hexanone ND 20 ug/l
87-68-3 Hexachlorobutadiene ND 4.0 ug/l
98-82-8 Isopropylbenzene 30.5 10 ug/l
99-87-6 p-Isopropyltoluene ND 10 ug/l
74-83-9 Methyl Bromide ND 10 ug/l
74-87-3 Methyl Chloride 18.6 10 ug/l
74-95-3 Methylene Bromide ND 10 ug/l
75-09-2 Methylene Chloride 11.4 10 ug/l
78-93-3 Methyl Ethyl Ketone ND 500 ug/l
108-10-1 4-Methyl-2-pentanone ND 10 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 10 ug/l
91-20-3 Naphthalene 155 10 ug/l
103-65-1 n-Propylbenzene 87.9 10 ug/l
100-42-5 Styrene ND 10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 4.0 ug/l
127-18-4 Tetrachloroethylene ND 10 ug/l
108-88-3 Toluene 122 10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 ug/l
79-00-5 1,1,2-Trichloroethane 32.5 6.0 ug/l
79-01-6 Trichloroethylene ND 10 ug/l
75-69-4 Trichlorofluoromethane ND 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 ug/l
95-63-6 1,2,4-Trimethylbenzene 488 10 ug/l
108-67-8 1,3,5-Trimethylbenzene 109 10 ug/l
108-05-4 Vinyl Acetate ND 10 ug/l
75-01-4 Vinyl Chloride ND 2.0 ug/l
m,p-Xylene 544 20 ug/l
95-47-6 o-Xylene 112 10 ug/l
1330-20-7 Xylene (total)656 10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 59
LA6149233.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW3
Lab Sample ID:LA61492-3 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 59
LA6149233.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW6
Lab Sample ID:LA61492-4 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122653.D 1 02/11/20 23:12 CP n/a n/a V2K2289
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 59
LA6149233.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW6
Lab Sample ID:LA61492-4 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 59
LA6149233.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW6
Lab Sample ID:LA61492-4 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 59
LA6149233.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW9
Lab Sample ID:LA61492-5 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122711.D 1 02/13/20 03:48 PJ n/a n/a V2K2292
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 59
LA6149233.5
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW9
Lab Sample ID:LA61492-5 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.78 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 59
LA6149233.5
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW9
Lab Sample ID:LA61492-5 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 59
LA6149233.5
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW13
Lab Sample ID:LA61492-6 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122712.D 1 02/13/20 04:19 PJ n/a n/a V2K2292
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 59
LA6149233.6
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW13
Lab Sample ID:LA61492-6 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.1 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 59
LA6149233.6
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW13
Lab Sample ID:LA61492-6 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 59
LA6149233.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW16D
Lab Sample ID:LA61492-7 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122647.D 1 02/11/20 20:08 CP n/a n/a V2K2289
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene 0.65 0.50 ug/l
135-98-8 sec-Butylbenzene 1.8 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 59
LA6149233.7
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW16D
Lab Sample ID:LA61492-7 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether 4.2 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene 1.0 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride 2.5 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether 6.2 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene 1.2 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate 3.4 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene 1.7 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)1.9 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 59
LA6149233.7
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW16D
Lab Sample ID:LA61492-7 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 59
LA6149233.7
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:PW1
Lab Sample ID:LA61492-8 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122648.D 1 02/11/20 20:39 CP n/a n/a V2K2289
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 59
LA6149233.8
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:PW1
Lab Sample ID:LA61492-8 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether 2.0 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether 9.4 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 59
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SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:PW1
Lab Sample ID:LA61492-8 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 59
LA6149233.8
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:PW2
Lab Sample ID:LA61492-9 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122649.D 1 02/11/20 21:10 CP n/a n/a V2K2289
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:PW2
Lab Sample ID:LA61492-9 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether 3.8 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether 13.3 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 59
LA6149233.9
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:PW2
Lab Sample ID:LA61492-9 Date Sampled:02/05/20
Matrix:AQ - Ground Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 59
LA6149233.9
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:FIELD BLANK
Lab Sample ID:LA61492-10 Date Sampled:02/05/20
Matrix:AQ - Field Blank Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2K0122639.D 1 02/11/20 16:04 CP n/a n/a V2K2289
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 59
LA6149233.10
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:FIELD BLANK
Lab Sample ID:LA61492-10 Date Sampled:02/05/20
Matrix:AQ - Field Blank Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene 0.50 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 59
LA6149233.10
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:FIELD BLANK
Lab Sample ID:LA61492-10 Date Sampled:02/05/20
Matrix:AQ - Field Blank Water Date Received:02/07/20
Method:SM 6200B Percent Solids:n/a
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 59
LA6149233.10
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Scott, LA
Section 4
37 of 59
LA614924
LA61492: Chain of Custody
Page 1 of 3
38 of 59
LA6149244.1
LA61492: Chain of Custody
Page 2 of 3
39 of 59
LA6149244.1
SGS Sample Receipt Summary
Job Number:LA61492 Client:ATC
Date / Time Received:2/7/2020 9:25:00 AM Delivery Method:FedEx
Project:STRAYHORN
4. No. Coolers:1
Airbill #'s:4913 8691 2020
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR Gun
Ice (direct contact)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Broken / Leaking
Y or N
Comments
Received 1 of 4 vials broken in cooler for mw-2.
Received 2 of 4 vials broken in cooler for mw-6.
Y or N N/A
Cooler Temps (Initial/Adjusted):#1: (0.8/0.8); DV439
LA61492: Chain of Custody
Page 3 of 3
40 of 59
LA6149244.1
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Scott, LA
Section 5
41 of 59
LA614925
Method Blank Summary Page 1 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2289-MB1 2K0122638.D 1 02/11/20 CP n/a n/a V2K2289
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-1, LA61492-2, LA61492-3, LA61492-4, LA61492-7, LA61492-8, LA61492-9, LA61492-10
CAS No.Compound Result RL Units Q
67-64-1 Acetone 1.3 10 ug/l J
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene ND 0.50 ug/l
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
42 of 59
LA6149255.1.1
Method Blank Summary Page 2 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2289-MB1 2K0122638.D 1 02/11/20 CP n/a n/a V2K2289
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-1, LA61492-2, LA61492-3, LA61492-4, LA61492-7, LA61492-8, LA61492-9, LA61492-10
CAS No.Compound Result RL Units Q
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene 0.35 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene 0.32 0.50 ug/l J
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.49 0.50 ug/l J
120-82-1 1,2,4-Trichlorobenzene 0.37 0.50 ug/l J
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
43 of 59
LA6149255.1.1
Method Blank Summary Page 3 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2289-MB1 2K0122638.D 1 02/11/20 CP n/a n/a V2K2289
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-1, LA61492-2, LA61492-3, LA61492-4, LA61492-7, LA61492-8, LA61492-9, LA61492-10
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
44 of 59
LA6149255.1.1
Method Blank Summary Page 1 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2292-MB1 2K0122706.D 1 02/13/20 PJ n/a n/a V2K2292
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-5, LA61492-6
CAS No.Compound Result RL Units Q
67-64-1 Acetone 2.5 10 ug/l J
71-43-2 Benzene ND 0.50 ug/l
108-86-1 Bromobenzene ND 0.50 ug/l
74-97-5 Bromochloromethane ND 0.50 ug/l
75-27-4 Bromodichloromethane ND 0.50 ug/l
75-25-2 Bromoform ND 0.50 ug/l
104-51-8 n-Butylbenzene 0.15 0.50 ug/l J
135-98-8 sec-Butylbenzene ND 0.50 ug/l
98-06-6 tert-Butylbenzene ND 0.50 ug/l
56-23-5 Carbon Tetrachloride ND 0.20 ug/l
108-90-7 Chlorobenzene ND 0.50 ug/l
75-00-3 Chloroethane ND 0.50 ug/l
67-66-3 Chloroform ND 0.50 ug/l
95-49-8 o-Chlorotoluene ND 0.50 ug/l
106-43-4 p-Chlorotoluene ND 0.50 ug/l
124-48-1 Dibromochloromethane ND 0.20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 ug/l
541-73-1 m-Dichlorobenzene 0.12 0.50 ug/l J
95-50-1 o-Dichlorobenzene ND 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 0.30 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.50 ug/l
45 of 59
LA6149255.1.2
Method Blank Summary Page 2 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2292-MB1 2K0122706.D 1 02/13/20 PJ n/a n/a V2K2292
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-5, LA61492-6
CAS No.Compound Result RL Units Q
591-78-6 2-Hexanone ND 1.0 ug/l
87-68-3 Hexachlorobutadiene a 0.42 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.50 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 ug/l
75-09-2 Methylene Chloride 0.11 0.50 ug/l J
78-93-3 Methyl Ethyl Ketone ND 25 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 ug/l
91-20-3 Naphthalene b 0.33 0.50 ug/l J
103-65-1 n-Propylbenzene ND 0.50 ug/l
100-42-5 Styrene ND 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 ug/l
127-18-4 Tetrachloroethylene ND 0.50 ug/l
108-88-3 Toluene ND 0.50 ug/l
87-61-6 1,2,3-Trichlorobenzene a 0.53 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene a 0.41 0.50 ug/l J
71-55-6 1,1,1-Trichloroethane ND 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.30 ug/l
79-01-6 Trichloroethylene ND 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 ug/l
108-05-4 Vinyl Acetate ND 0.50 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 1.0 ug/l
95-47-6 o-Xylene ND 0.50 ug/l
1330-20-7 Xylene (total)ND 0.50 ug/l
46 of 59
LA6149255.1.2
Method Blank Summary Page 3 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2292-MB1 2K0122706.D 1 02/13/20 PJ n/a n/a V2K2292
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-5, LA61492-6
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Compound not detected in samples at less than 10 times the hit in the blank.
(b) Concentration > 1/2 RL.
47 of 59
LA6149255.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2289-BS2 2K0122635.D 1 02/11/20 CP n/a n/a V2K2289
V2K2289-BSD2 2K0122636.D 1 02/11/20 CP n/a n/a V2K2289
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-1, LA61492-2, LA61492-3, LA61492-4, LA61492-7, LA61492-8, LA61492-9, LA61492-10
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
67-64-1 Acetone 50 41.0 82 35.1 70 16 70-130/30
71-43-2 Benzene 20 22.9 115 20.9 105 9 70-130/30
108-86-1 Bromobenzene 20 19.7 99 20.7 104 5 70-130/30
74-97-5 Bromochloromethane 20 26.0 130 23.4 117 11 70-130/30
75-27-4 Bromodichloromethane 20 24.7 124 22.4 112 10 70-130/30
75-25-2 Bromoform 20 15.8 79 16.9 85 7 70-130/30
104-51-8 n-Butylbenzene 20 22.6 113 21.6 108 5 70-130/30
135-98-8 sec-Butylbenzene 20 24.0 120 19.0 95 23 70-130/30
98-06-6 tert-Butylbenzene 20 23.9 120 18.4 92 26 70-130/30
56-23-5 Carbon Tetrachloride 20 27.7 139*23.1 116 18 70-130/30
108-90-7 Chlorobenzene 20 21.2 106 19.0 95 11 70-130/30
75-00-3 Chloroethane 20 23.7 119 20.1 101 16 60-140/30
67-66-3 Chloroform 20 23.8 119 20.7 104 14 70-130/30
95-49-8 o-Chlorotoluene 20 24.2 121 17.8 89 30 70-130/30
106-43-4 p-Chlorotoluene 20 24.5 123 18.2 91 30 70-130/30
124-48-1 Dibromochloromethane 20 18.4 92 16.1 81 13 70-130/30
96-12-8 1,2-Dibromo-3-chloropropane 20 10.6 53*25.1 126 81*70-130/30
106-93-4 1,2-Dibromoethane 20 21.6 108 19.5 98 10 70-130/30
75-71-8 Dichlorodifluoromethane 20 21.2 106 19.9 100 6 60-140/30
541-73-1 m-Dichlorobenzene 20 21.8 109 19.4 97 12 70-130/30
95-50-1 o-Dichlorobenzene 20 18.6 93 19.9 100 7 70-130/30
106-46-7 p-Dichlorobenzene 20 21.6 108 19.3 97 11 70-130/30
75-34-3 1,1-Dichloroethane 20 26.6 133*22.9 115 15 70-130/30
107-06-2 1,2-Dichloroethane 20 21.9 110 20.4 102 7 70-130/30
75-35-4 1,1-Dichloroethylene 20 27.2 136*23.8 119 13 70-130/30
156-59-2 cis-1,2-Dichloroethylene 20 26.5 133*23.2 116 13 70-130/30
156-60-5 trans-1,2-Dichloroethylene 20 27.3 137*23.6 118 15 70-130/30
78-87-5 1,2-Dichloropropane 20 22.7 114 20.7 104 9 70-130/30
142-28-9 1,3-Dichloropropane 20 21.2 106 18.2 91 15 70-130/30
594-20-7 2,2-Dichloropropane 20 32.6 163*25.6 128 24 70-130/30
563-58-6 1,1-Dichloropropene 20 28.1 141*24.6 123 13 70-130/30
10061-01-5 cis-1,3-Dichloropropene 20 23.6 118 21.8 109 8 70-130/30
10061-02-6 trans-1,3-Dichloropropene 20 23.0 115 19.2 96 18 70-130/30
108-20-3 Di-Isopropyl Ether 20 27.5 138*24.2 121 13 70-130/30
64-17-5 Ethyl Alcohol 400 436 109 887 222*68*70-130/30
100-41-4 Ethylbenzene 20 21.8 109 19.1 96 13 70-130/30
* = Outside of Control Limits.
48 of 59
LA6149255.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2289-BS2 2K0122635.D 1 02/11/20 CP n/a n/a V2K2289
V2K2289-BSD2 2K0122636.D 1 02/11/20 CP n/a n/a V2K2289
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-1, LA61492-2, LA61492-3, LA61492-4, LA61492-7, LA61492-8, LA61492-9, LA61492-10
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
591-78-6 2-Hexanone 50 39.3 79 39.8 80 1 70-130/30
87-68-3 Hexachlorobutadiene 20 13.2 66*25.0 125 62*70-130/30
98-82-8 Isopropylbenzene 20 21.7 109 20.6 103 5 70-130/30
99-87-6 p-Isopropyltoluene 20 23.8 119 19.9 100 18 70-130/30
74-83-9 Methyl Bromide 20 23.0 115 28.6 143*22 60-140/30
74-87-3 Methyl Chloride 20 18.9 95 20.1 101 6 60-140/30
74-95-3 Methylene Bromide 20 21.8 109 20.3 102 7 70-130/30
75-09-2 Methylene Chloride 20 24.3 122 21.1 106 14 70-130/30
78-93-3 Methyl Ethyl Ketone 50 46.9 94 45.2 90 4 70-130/30
108-10-1 4-Methyl-2-pentanone 50 51.3 103 56.1 112 9 70-130/30
1634-04-4 Methyl Tert Butyl Ether 20 25.0 125 21.9 110 13 70-130/30
91-20-3 Naphthalene 20 4.6 23*27.3 137*142*70-130/30
103-65-1 n-Propylbenzene 20 25.2 126 17.7 89 35*70-130/30
100-42-5 Styrene 20 21.8 109 20.6 103 6 70-130/30
630-20-6 1,1,1,2-Tetrachloroethane 20 22.6 113 20.2 101 11 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 20 21.7 109 18.6 93 15 70-130/30
127-18-4 Tetrachloroethylene 20 22.7 114 18.8 94 19 70-130/30
108-88-3 Toluene 20 22.0 110 18.1 91 19 70-130/30
87-61-6 1,2,3-Trichlorobenzene 20 4.8 24*31.7 159*147*70-130/30
120-82-1 1,2,4-Trichlorobenzene 20 9.0 45*29.1 146*106*70-130/30
71-55-6 1,1,1-Trichloroethane 20 28.1 141*23.9 120 16 70-130/30
79-00-5 1,1,2-Trichloroethane 20 20.9 105 18.1 91 14 70-130/30
79-01-6 Trichloroethylene 20 23.6 118 21.1 106 11 70-130/30
75-69-4 Trichlorofluoromethane 20 25.8 129 23.6 118 9 60-140/30
96-18-4 1,2,3-Trichloropropane 20 18.5 93 21.6 108 15 70-130/30
95-63-6 1,2,4-Trimethylbenzene 20 23.3 117 18.6 93 22 70-130/30
108-67-8 1,3,5-Trimethylbenzene 20 24.4 122 18.2 91 29 70-130/30
108-05-4 Vinyl Acetate 20 33.4 167*29.3 147*13 70-130/30
75-01-4 Vinyl Chloride 20 22.7 114 21.7 109 5 60-140/30
m,p-Xylene 40 43.7 109 39.8 100 9 70-130/30
95-47-6 o-Xylene 20 20.7 104 19.3 97 7 70-130/30
1330-20-7 Xylene (total)60 64.4 107 59.1 99 9 70-130/30
* = Outside of Control Limits.
49 of 59
LA6149255.2.1
Blank Spike/Blank Spike Duplicate Summary Page 3 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2289-BS2 2K0122635.D 1 02/11/20 CP n/a n/a V2K2289
V2K2289-BSD2 2K0122636.D 1 02/11/20 CP n/a n/a V2K2289
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-1, LA61492-2, LA61492-3, LA61492-4, LA61492-7, LA61492-8, LA61492-9, LA61492-10
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 104%106%70-130%
2037-26-5 Toluene-D8 98%104%70-130%
460-00-4 4-Bromofluorobenzene 93%107%70-130%
* = Outside of Control Limits.
50 of 59
LA6149255.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2292-BS1 2K0122703.D 1 02/12/20 PJ n/a n/a V2K2292
V2K2292-BSD1 2K0122704.D 1 02/13/20 PJ n/a n/a V2K2292
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-5, LA61492-6
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
67-64-1 Acetone 50 47.2 94 50.8 102 7 70-130/30
71-43-2 Benzene 20 20.5 103 20.0 100 2 70-130/30
108-86-1 Bromobenzene 20 20.5 103 20.3 102 1 70-130/30
74-97-5 Bromochloromethane 20 19.7 99 19.7 99 0 70-130/30
75-27-4 Bromodichloromethane 20 20.2 101 19.5 98 4 70-130/30
75-25-2 Bromoform 20 19.2 96 19.9 100 4 70-130/30
104-51-8 n-Butylbenzene 20 23.2 116 22.4 112 4 70-130/30
135-98-8 sec-Butylbenzene 20 22.4 112 21.5 108 4 70-130/30
98-06-6 tert-Butylbenzene 20 21.3 107 20.7 104 3 70-130/30
56-23-5 Carbon Tetrachloride 20 21.6 108 20.7 104 4 70-130/30
108-90-7 Chlorobenzene 20 21.1 106 20.9 105 1 70-130/30
75-00-3 Chloroethane 20 19.1 96 18.4 92 4 60-140/30
67-66-3 Chloroform 20 19.7 99 19.4 97 2 70-130/30
95-49-8 o-Chlorotoluene 20 21.0 105 20.4 102 3 70-130/30
106-43-4 p-Chlorotoluene 20 21.0 105 20.6 103 2 70-130/30
124-48-1 Dibromochloromethane 20 19.7 99 19.9 100 1 70-130/30
96-12-8 1,2-Dibromo-3-chloropropane 20 20.4 102 20.7 104 1 70-130/30
106-93-4 1,2-Dibromoethane 20 21.7 109 21.8 109 0 70-130/30
75-71-8 Dichlorodifluoromethane 20 21.9 110 21.0 105 4 60-140/30
541-73-1 m-Dichlorobenzene 20 20.1 101 19.6 98 3 70-130/30
95-50-1 o-Dichlorobenzene 20 20.5 103 20.4 102 0 70-130/30
106-46-7 p-Dichlorobenzene 20 20.2 101 19.8 99 2 70-130/30
75-34-3 1,1-Dichloroethane 20 20.6 103 20.0 100 3 70-130/30
107-06-2 1,2-Dichloroethane 20 19.6 98 19.4 97 1 70-130/30
75-35-4 1,1-Dichloroethylene 20 20.7 104 19.8 99 4 70-130/30
156-59-2 cis-1,2-Dichloroethylene 20 20.3 102 19.7 99 3 70-130/30
156-60-5 trans-1,2-Dichloroethylene 20 20.9 105 20.0 100 4 70-130/30
78-87-5 1,2-Dichloropropane 20 21.0 105 20.8 104 1 70-130/30
142-28-9 1,3-Dichloropropane 20 20.9 105 21.1 106 1 70-130/30
594-20-7 2,2-Dichloropropane 20 22.5 113 21.4 107 5 70-130/30
563-58-6 1,1-Dichloropropene 20 21.0 105 20.2 101 4 70-130/30
10061-01-5 cis-1,3-Dichloropropene 20 20.6 103 20.1 101 2 70-130/30
10061-02-6 trans-1,3-Dichloropropene 20 20.3 102 20.5 103 1 70-130/30
108-20-3 Di-Isopropyl Ether 20 21.2 106 20.9 105 1 70-130/30
64-17-5 Ethyl Alcohol 400 409 102 401 100 2 70-130/30
100-41-4 Ethylbenzene 20 21.8 109 21.3 107 2 70-130/30
* = Outside of Control Limits.
51 of 59
LA6149255.2.2
Blank Spike/Blank Spike Duplicate Summary Page 2 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2292-BS1 2K0122703.D 1 02/12/20 PJ n/a n/a V2K2292
V2K2292-BSD1 2K0122704.D 1 02/13/20 PJ n/a n/a V2K2292
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-5, LA61492-6
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
591-78-6 2-Hexanone 50 58.7 117 56.7 113 3 70-130/30
87-68-3 Hexachlorobutadiene 20 23.2 116 22.6 113 3 70-130/30
98-82-8 Isopropylbenzene 20 22.7 114 21.9 110 4 70-130/30
99-87-6 p-Isopropyltoluene 20 23.1 116 22.3 112 4 70-130/30
74-83-9 Methyl Bromide 20 19.3 97 18.7 94 3 60-140/30
74-87-3 Methyl Chloride 20 21.3 107 20.4 102 4 60-140/30
74-95-3 Methylene Bromide 20 21.1 106 21.3 107 1 70-130/30
75-09-2 Methylene Chloride 20 21.0 105 20.7 104 1 70-130/30
78-93-3 Methyl Ethyl Ketone 50 49.9 100 52.1 104 4 70-130/30
108-10-1 4-Methyl-2-pentanone 50 57.1 114 59.5 119 4 70-130/30
1634-04-4 Methyl Tert Butyl Ether 20 21.6 108 21.9 110 1 70-130/30
91-20-3 Naphthalene 20 20.5 103 21.1 106 3 70-130/30
103-65-1 n-Propylbenzene 20 21.7 109 20.8 104 4 70-130/30
100-42-5 Styrene 20 23.1 116 22.7 114 2 70-130/30
630-20-6 1,1,1,2-Tetrachloroethane 20 22.5 113 22.5 113 0 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 20 21.1 106 21.6 108 2 70-130/30
127-18-4 Tetrachloroethylene 20 20.5 103 19.7 99 4 70-130/30
108-88-3 Toluene 20 21.5 108 20.9 105 3 70-130/30
87-61-6 1,2,3-Trichlorobenzene 20 23.3 117 23.5 118 1 70-130/30
120-82-1 1,2,4-Trichlorobenzene 20 23.8 119 23.6 118 1 70-130/30
71-55-6 1,1,1-Trichloroethane 20 21.9 110 20.9 105 5 70-130/30
79-00-5 1,1,2-Trichloroethane 20 19.0 95 19.9 100 5 70-130/30
79-01-6 Trichloroethylene 20 20.7 104 19.7 99 5 70-130/30
75-69-4 Trichlorofluoromethane 20 22.0 110 20.9 105 5 60-140/30
96-18-4 1,2,3-Trichloropropane 20 21.4 107 21.9 110 2 70-130/30
95-63-6 1,2,4-Trimethylbenzene 20 21.7 109 21.1 106 3 70-130/30
108-67-8 1,3,5-Trimethylbenzene 20 22.1 111 21.4 107 3 70-130/30
108-05-4 Vinyl Acetate 20 23.6 118 23.9 120 1 70-130/30
75-01-4 Vinyl Chloride 20 20.5 103 19.3 97 6 60-140/30
m,p-Xylene 40 46.7 117 45.5 114 3 70-130/30
95-47-6 o-Xylene 20 22.4 112 21.9 110 2 70-130/30
1330-20-7 Xylene (total)60 69.2 115 67.4 112 3 70-130/30
* = Outside of Control Limits.
52 of 59
LA6149255.2.2
Blank Spike/Blank Spike Duplicate Summary Page 3 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2K2292-BS1 2K0122703.D 1 02/12/20 PJ n/a n/a V2K2292
V2K2292-BSD1 2K0122704.D 1 02/13/20 PJ n/a n/a V2K2292
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-5, LA61492-6
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 100%101%70-130%
2037-26-5 Toluene-D8 102%100%70-130%
460-00-4 4-Bromofluorobenzene 102%103%70-130%
* = Outside of Control Limits.
53 of 59
LA6149255.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA61492-1MS 2K0122643.D 50 02/11/20 CP n/a n/a V2K2289
LA61492-1MSD 2K0122644.D 50 02/11/20 CP n/a n/a V2K2289
LA61492-1 2K0122641.D 20 02/11/20 CP n/a n/a V2K2289
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-1, LA61492-2, LA61492-3, LA61492-4, LA61492-7, LA61492-8, LA61492-9, LA61492-10
LA61492-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 2500 1100 44*2500 1060 42*4 70-130/20
71-43-2 Benzene 30.2 1000 1060 103 1000 1110 108 5 70-130/20
108-86-1 Bromobenzene ND 1000 1000 100 1000 1040 104 4 70-130/20
74-97-5 Bromochloromethane ND 1000 1220 122 1000 1210 121 1 70-130/20
75-27-4 Bromodichloromethane ND 1000 1140 114 1000 1180 118 3 70-130/20
75-25-2 Bromoform ND 1000 746 75 1000 779 78 4 70-130/20
104-51-8 n-Butylbenzene 13.6 1000 1050 104 1000 1150 114 9 70-130/20
135-98-8 sec-Butylbenzene ND 1000 990 99 1000 1070 107 8 70-130/20
98-06-6 tert-Butylbenzene ND 1000 982 98 1000 1050 105 7 70-130/20
56-23-5 Carbon Tetrachloride 102 1000 1250 115 1000 1300 120 4 70-130/20
108-90-7 Chlorobenzene ND 1000 989 99 1000 1030 103 4 70-130/20
75-00-3 Chloroethane ND 1000 1130 113 1000 1140 114 1 60-140/20
67-66-3 Chloroform 24.5 1000 1130 111 1000 1140 112 1 70-130/20
95-49-8 o-Chlorotoluene ND 1000 1030 103 1000 1080 108 5 70-130/20
106-43-4 p-Chlorotoluene ND 1000 1010 101 1000 1060 106 5 70-130/20
124-48-1 Dibromochloromethane ND 1000 812 81 1000 841 84 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 935 94 1000 995 100 6 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 992 99 1000 1030 103 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 1030 103 1000 1080 108 5 60-140/20
541-73-1 m-Dichlorobenzene ND 1000 1000 100 1000 1060 106 6 70-130/20
95-50-1 o-Dichlorobenzene ND 1000 984 98 1000 1040 104 6 70-130/20
106-46-7 p-Dichlorobenzene ND 1000 1000 100 1000 1060 106 6 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 1240 124 1000 1250 125 1 70-130/20
107-06-2 1,2-Dichloroethane 57.4 1000 1050 99 1000 1080 102 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 1230 123 1000 1250 125 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 1250 125 1000 1250 125 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 1260 126 1000 1260 126 0 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 1050 105 1000 1090 109 4 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 956 96 1000 994 99 4 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 1220 122 1000 1230 123 1 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 1280 128 1000 1300 130 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 1040 104 1000 1080 108 4 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 964 96 1000 1010 101 5 70-130/20
108-20-3 Di-Isopropyl Ether ND 1000 1310 131*1000 1310 131*0 70-130/20
64-17-5 Ethyl Alcohol ND 20000 24800 124 20000 28500 143*14 70-130/20
100-41-4 Ethylbenzene 590 1000 1620 103 1000 1690 110 4 70-130/20
* = Outside of Control Limits.
54 of 59
LA6149255.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA61492-1MS 2K0122643.D 50 02/11/20 CP n/a n/a V2K2289
LA61492-1MSD 2K0122644.D 50 02/11/20 CP n/a n/a V2K2289
LA61492-1 2K0122641.D 20 02/11/20 CP n/a n/a V2K2289
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-1, LA61492-2, LA61492-3, LA61492-4, LA61492-7, LA61492-8, LA61492-9, LA61492-10
LA61492-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 2500 1720 69*2500 1670 67*3 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 910 91 1000 1030 103 12 70-130/20
98-82-8 Isopropylbenzene 45.5 1000 1080 103 1000 1150 110 6 70-130/20
99-87-6 p-Isopropyltoluene ND 1000 1020 102 1000 1100 110 8 70-130/20
74-83-9 Methyl Bromide ND 1000 1020 102 1000 1240 124 19 60-140/20
74-87-3 Methyl Chloride ND 1000 984 98 1000 1000 100 2 60-140/20
74-95-3 Methylene Bromide ND 1000 1020 102 1000 1050 105 3 70-130/20
75-09-2 Methylene Chloride 4.9 1000 1140 114 1000 1140 114 0 70-130/20
78-93-3 Methyl Ethyl Ketone ND 2500 1850 74 2500 1770 71 4 70-130/20
108-10-1 4-Methyl-2-pentanone ND 2500 2500 100 2500 2560 102 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 4.2 1000 1160 116 1000 1150 115 1 70-130/20
91-20-3 Naphthalene 275 1000 1200 93 1000 1290 102 7 70-130/20
103-65-1 n-Propylbenzene 113 1000 1100 99 1000 1170 106 6 70-130/20
100-42-5 Styrene ND 1000 1040 104 1000 1080 108 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 1030 103 1000 1080 108 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 936 94 1000 984 98 5 70-130/20
127-18-4 Tetrachloroethylene 6.0 1000 995 99 1000 1040 103 4 70-130/20
108-88-3 Toluene 49.6 1000 1020 97 1000 1070 102 5 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 982 98 1000 1080 108 10 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 1020 102 1000 1120 112 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 1270 127 1000 1290 129 2 70-130/20
79-00-5 1,1,2-Trichloroethane 30.4 1000 957 93 1000 999 97 4 70-130/20
79-01-6 Trichloroethylene ND 1000 1090 109 1000 1130 113 4 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 1240 124 1000 1260 126 2 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 959 96 1000 1010 101 5 70-130/20
95-63-6 1,2,4-Trimethylbenzene 221 1000 1240 102 1000 1300 108 5 70-130/20
108-67-8 1,3,5-Trimethylbenzene 105 1000 1110 101 1000 1180 108 6 70-130/20
108-05-4 Vinyl Acetate ND 1000 1660 166*1000 1640 164*1 70-130/20
75-01-4 Vinyl Chloride ND 1000 1110 111 1000 1150 115 4 60-140/20
m,p-Xylene 1400 2000 3500 105 2000 3680 114 5 70-130/20
95-47-6 o-Xylene 42.2 1000 1000 96 1000 1060 102 6 70-130/20
1330-20-7 Xylene (total)1450 3000 4510 102 3000 4730 109 5 70-130/20
* = Outside of Control Limits.
55 of 59
LA6149255.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA61492-1MS 2K0122643.D 50 02/11/20 CP n/a n/a V2K2289
LA61492-1MSD 2K0122644.D 50 02/11/20 CP n/a n/a V2K2289
LA61492-1 2K0122641.D 20 02/11/20 CP n/a n/a V2K2289
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-1, LA61492-2, LA61492-3, LA61492-4, LA61492-7, LA61492-8, LA61492-9, LA61492-10
CAS No.Surrogate Recoveries MS MSD LA61492-1 Limits
17060-07-0 1,2-Dichloroethane-D4 107%103%102%70-130%
2037-26-5 Toluene-D8 102%102%98%70-130%
460-00-4 4-Bromofluorobenzene 101%100%99%70-130%
* = Outside of Control Limits.
56 of 59
LA6149255.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA61490-7MS 2K0122719.D 500 02/13/20 PJ n/a n/a V2K2292
LA61490-7MSD 2K0122720.D 500 02/13/20 PJ n/a n/a V2K2292
LA61490-7 2K0122716.D 200 02/13/20 PJ n/a n/a V2K2292
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-5, LA61492-6
LA61490-7 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 25000 36100 144* a 25000 33400 134* a 8 70-130/20
71-43-2 Benzene 1600 10000 12700 111 10000 12600 110 1 70-130/20
108-86-1 Bromobenzene ND 10000 10600 106 10000 10400 104 2 70-130/20
74-97-5 Bromochloromethane ND 10000 10300 103 10000 9890 99 4 70-130/20
75-27-4 Bromodichloromethane ND 10000 10400 104 10000 10400 104 0 70-130/20
75-25-2 Bromoform ND 10000 9720 97 10000 9550 96 2 70-130/20
104-51-8 n-Butylbenzene ND 10000 11200 112 10000 10800 108 4 70-130/20
135-98-8 sec-Butylbenzene ND 10000 11100 111 10000 10700 107 4 70-130/20
98-06-6 tert-Butylbenzene ND 10000 10800 108 10000 10500 105 3 70-130/20
56-23-5 Carbon Tetrachloride 74.2 10000 11100 110 10000 10900 108 2 70-130/20
108-90-7 Chlorobenzene ND 10000 11000 110 10000 10700 107 3 70-130/20
75-00-3 Chloroethane ND 10000 10400 104 10000 9720 97 7 60-140/20
67-66-3 Chloroform ND 10000 10200 102 10000 10200 102 0 70-130/20
95-49-8 o-Chlorotoluene ND 10000 11100 111 10000 10700 107 4 70-130/20
106-43-4 p-Chlorotoluene ND 10000 10800 108 10000 10500 105 3 70-130/20
124-48-1 Dibromochloromethane ND 10000 9810 98 10000 9520 95 3 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10000 10400 104 10000 9790 98 6 70-130/20
106-93-4 1,2-Dibromoethane ND 10000 11600 116 10000 10800 108 7 70-130/20
75-71-8 Dichlorodifluoromethane ND 10000 13900 139 10000 13200 132 5 60-140/20
541-73-1 m-Dichlorobenzene ND 10000 10500 105 10000 9970 100 5 70-130/20
95-50-1 o-Dichlorobenzene ND 10000 10900 109 10000 10300 103 6 70-130/20
106-46-7 p-Dichlorobenzene ND 10000 10400 104 10000 10100 101 3 70-130/20
75-34-3 1,1-Dichloroethane ND 10000 10400 104 10000 10200 102 2 70-130/20
107-06-2 1,2-Dichloroethane 30.4 10000 10400 104 10000 9910 99 5 70-130/20
75-35-4 1,1-Dichloroethylene ND 10000 10300 103 10000 9960 100 3 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10000 10400 104 10000 10000 100 4 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10000 10400 104 10000 9990 100 4 70-130/20
78-87-5 1,2-Dichloropropane ND 10000 10800 108 10000 10500 105 3 70-130/20
142-28-9 1,3-Dichloropropane ND 10000 11000 110 10000 10600 106 4 70-130/20
594-20-7 2,2-Dichloropropane ND 10000 3870 39* a 10000 4130 41* a 7 70-130/20
563-58-6 1,1-Dichloropropene ND 10000 10600 106 10000 10300 103 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10000 8700 87 10000 8540 85 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10000 8740 87 10000 8490 85 3 70-130/20
108-20-3 Di-Isopropyl Ether 95.9 10000 11200 111 10000 10900 108 3 70-130/20
64-17-5 Ethyl Alcohol ND 200000 91100 46* a 200000 84400 42* a 8 70-130/20
100-41-4 Ethylbenzene 765 10000 12300 115 10000 12000 112 2 70-130/20
* = Outside of Control Limits.
57 of 59
LA6149255.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA61490-7MS 2K0122719.D 500 02/13/20 PJ n/a n/a V2K2292
LA61490-7MSD 2K0122720.D 500 02/13/20 PJ n/a n/a V2K2292
LA61490-7 2K0122716.D 200 02/13/20 PJ n/a n/a V2K2292
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-5, LA61492-6
LA61490-7 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 25000 29000 116 25000 24400 98 17 70-130/20
87-68-3 Hexachlorobutadiene ND 10000 10900 109 10000 10700 107 2 70-130/20
98-82-8 Isopropylbenzene 29.7 10000 11500 115 10000 11200 112 3 70-130/20
99-87-6 p-Isopropyltoluene ND 10000 11600 116 10000 11200 112 4 70-130/20
74-83-9 Methyl Bromide ND 10000 8150 82 10000 9890 99 19 60-140/20
74-87-3 Methyl Chloride ND 10000 11400 114 10000 11200 112 2 60-140/20
74-95-3 Methylene Bromide ND 10000 10800 108 10000 10600 106 2 70-130/20
75-09-2 Methylene Chloride 22.7 10000 10900 109 10000 10400 104 5 70-130/20
78-93-3 Methyl Ethyl Ketone ND 25000 31000 124 25000 29500 118 5 70-130/20
108-10-1 4-Methyl-2-pentanone ND 25000 30000 120 25000 28600 114 5 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10000 11100 111 10000 10700 107 4 70-130/20
91-20-3 Naphthalene 439 10000 10600 102 10000 10200 98 4 70-130/20
103-65-1 n-Propylbenzene 80.4 10000 10700 106 10000 10300 102 4 70-130/20
100-42-5 Styrene 77.4 10000 12100 120 10000 11700 116 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10000 11700 117 10000 11300 113 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10000 11000 110 10000 10400 104 6 70-130/20
127-18-4 Tetrachloroethylene ND 10000 10600 106 10000 10300 103 3 70-130/20
108-88-3 Toluene 8290 10000 23600 153* a 10000 22900 146* a 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10000 11500 115 10000 11500 115 0 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10000 11600 116 10000 11400 114 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10000 10900 109 10000 10600 106 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10000 10400 104 10000 9990 100 4 70-130/20
79-01-6 Trichloroethylene ND 10000 10700 107 10000 10600 106 1 70-130/20
75-69-4 Trichlorofluoromethane ND 10000 11700 117 10000 11300 113 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10000 11500 115 10000 10700 107 7 70-130/20
95-63-6 1,2,4-Trimethylbenzene 616 10000 11800 112 10000 11400 108 3 70-130/20
108-67-8 1,3,5-Trimethylbenzene 142 10000 11300 112 10000 10900 108 4 70-130/20
108-05-4 Vinyl Acetate ND 10000 3510 35* a 10000 3340 33* a 5 70-130/20
75-01-4 Vinyl Chloride ND 10000 10500 105 10000 10300 103 2 60-140/20
m,p-Xylene 2630 20000 27500 124 20000 26700 120 3 70-130/20
95-47-6 o-Xylene 1630 10000 13600 120 10000 13300 117 2 70-130/20
1330-20-7 Xylene (total)4250 30000 41100 123 30000 40100 120 2 70-130/20
* = Outside of Control Limits.
58 of 59
LA6149255.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:LA61492
Account:ATCNCR ATC Group Services LLC
Project:Strayhorn Wrecker Service 1701 S. Miami Blvd, Durham, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA61490-7MS 2K0122719.D 500 02/13/20 PJ n/a n/a V2K2292
LA61490-7MSD 2K0122720.D 500 02/13/20 PJ n/a n/a V2K2292
LA61490-7 2K0122716.D 200 02/13/20 PJ n/a n/a V2K2292
The QC reported here applies to the following samples:Method: SM 6200B
LA61492-5, LA61492-6
CAS No.Surrogate Recoveries MS MSD LA61490-7 Limits
17060-07-0 1,2-Dichloroethane-D4 99%96%100%70-130%
2037-26-5 Toluene-D8 101%101%97%70-130%
460-00-4 4-Bromofluorobenzene 101%101%98%70-130%
(a) Outside control limits due to matrix interference. Blank Spike meets acceptance criteria.
* = Outside of Control Limits.
59 of 59
LA6149255.3.2