RA-631_3887_CA_LAB_20191203. Shealy Lab Rpt Church POE

SHEALY ENVIRONMENTAL SERVICES,INC.
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This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Report of Analysis
NCDEQ-DWM-UST Section
1646 Mail Service Ctr.
Raleigh,NC 27699
Attention:Linda Blalock
Project Name:Saint's Delight Baptist Church
Project Number:NC0207 TF 3887
Lot Number:UK27041
Date Completed:12/03/2019
12/09/2019 10:29 AM
Approved and released by:
Project Manager:Nisreen Saikaly
Page 1 of 16
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Case Narrative
NCDEQ-DWM-UST Section
Lot Number:UK27041
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved NELAC standards,the Shealy Environmental Services,Inc.("Shealy")Quality
Assurance Management Plan (QAMP),standard operating procedures (SOPs),and Shealy policies.Any
exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Page 2 of 16
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
NCDEQ-DWM-UST Section
Lot Number: UK27041

Project Name: Saint's Delight Baptist Church
Project Number: NC0207 TF 3887
Sample Number Sample ID Matrix Date Sampled Date Received
001 11/21/2019 1250D1Aqueous 11/27/2019
002 11/21/2019 1255D3Aqueous 11/27/2019
(2 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 3 of 16
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
NCDEQ-DWM-UST Section
Lot Number: UK27041

Project Name: Saint's Delight Baptist Church
Project Number: NC0207 TF 3887
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 D1 Aqueous Benzene SM 6200B-31 ug/L 5
001 D1 Aqueous 1,2-Dichloroethane SM 6200B-3.4 ug/L 5
001 D1 Aqueous Diisopropyl ether (IPE)SM 6200B-4.4 ug/L 5
001 D1 Aqueous Isopropylbenzene SM 6200B-1.1 ug/L 5
001 D1 Aqueous Naphthalene SM 6200B-7.5 ug/L 5
(5 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 4 of 16
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDEQ-DWM-UST Section
D1
UK27041-001
11/21/2019 1250
11/27/2019
Aqueous
Project Name: Saint's Delight Baptist Church
Project Number: NC0207 TF 3887
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/29/2019 1315 JJG 37425
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzene 71-43-2 SM 6200B-31 1ug/L0.400.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.400.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.400.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.400.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.400.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.400.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.400.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.400.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.400.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.400.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.400.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.400.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.400.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.400.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.400.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.400.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 SM 6200B-3.4 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.400.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.400.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.400.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-4.4 1ug/L0.400.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.400.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.400.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-1.1 1ug/L0.400.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.400.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.400.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.400.50
Naphthalene 91-20-3 SM 6200B-7.5 1ug/L0.400.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.400.50
Styrene 100-42-5 SM 6200B-ND 1ug/L0.400.50
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 5 of 16
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDEQ-DWM-UST Section
D1
UK27041-001
11/21/2019 1250
11/27/2019
Aqueous
Project Name: Saint's Delight Baptist Church
Project Number: NC0207 TF 3887
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/29/2019 1315 JJG 37425
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.400.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.400.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.400.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.400.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.400.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.400.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.400.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.400.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.400.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.400.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.400.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.400.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 86 70-130
Bromofluorobenzene 94 70-130
Toluene-d8 97 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 6 of 16
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDEQ-DWM-UST Section
D3
UK27041-002
11/21/2019 1255
11/27/2019
Aqueous
Project Name: Saint's Delight Baptist Church
Project Number: NC0207 TF 3887
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/29/2019 1337 JJG 37425
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzene 71-43-2 SM 6200B-ND 1ug/L0.400.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.400.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.400.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.400.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.400.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.400.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.400.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.400.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.400.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.400.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.400.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.400.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.400.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.400.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.400.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.400.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.400.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.400.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.400.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.400.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-ND 1ug/L0.400.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.400.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.400.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.400.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.400.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.400.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.400.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.400.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.400.50
Styrene 100-42-5 SM 6200B-ND 1ug/L0.400.50
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 7 of 16
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
NCDEQ-DWM-UST Section
D3
UK27041-002
11/21/2019 1255
11/27/2019
Aqueous
Project Name: Saint's Delight Baptist Church
Project Number: NC0207 TF 3887
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/29/2019 1337 JJG 37425
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.400.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.400.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.400.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.400.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.400.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.400.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.400.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.400.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.400.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.400.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.400.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.400.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 89 70-130
Bromofluorobenzene 95 70-130
Toluene-d8 98 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 8 of 16
QC Summary
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Shealy Environmental Services, Inc.

Page 9 of 16
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:UQ37425-001
37425 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Benzene ND 11/29/2019 11040.50 0.40 ug/L1
Bromobenzene ND 11/29/2019 11040.50 0.40 ug/L1
Bromochloromethane ND 11/29/2019 11040.50 0.40 ug/L1
Bromodichloromethane ND 11/29/2019 11040.50 0.40 ug/L1
Bromoform ND 11/29/2019 11040.50 0.40 ug/L1
Bromomethane (Methyl bromide)ND 11/29/2019 11040.50 0.40 ug/L1
n-Butylbenzene ND 11/29/2019 11040.50 0.40 ug/L1
sec-Butylbenzene ND 11/29/2019 11040.50 0.40 ug/L1
tert-Butylbenzene ND 11/29/2019 11040.50 0.40 ug/L1
Carbon tetrachloride ND 11/29/2019 11040.50 0.40 ug/L1
Chlorobenzene ND 11/29/2019 11040.50 0.40 ug/L1
Chloroethane ND 11/29/2019 11040.50 0.40 ug/L1
Chloroform ND 11/29/2019 11040.50 0.40 ug/L1
Chloromethane (Methyl chloride)ND 11/29/2019 11040.50 0.40 ug/L1
2-Chlorotoluene ND 11/29/2019 11040.50 0.40 ug/L1
4-Chlorotoluene ND 11/29/2019 11040.50 0.40 ug/L1
Dibromochloromethane ND 11/29/2019 11040.50 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 11/29/2019 11040.50 0.40 ug/L1
Dibromomethane (Methylene bromide)ND 11/29/2019 11040.50 0.40 ug/L1
1,2-Dichlorobenzene ND 11/29/2019 11040.50 0.40 ug/L1
1,3-Dichlorobenzene ND 11/29/2019 11040.50 0.40 ug/L1
1,4-Dichlorobenzene ND 11/29/2019 11040.50 0.40 ug/L1
Dichlorodifluoromethane ND 11/29/2019 11040.50 0.40 ug/L1
1,1-Dichloroethane ND 11/29/2019 11040.50 0.40 ug/L1
1,2-Dichloroethane ND 11/29/2019 11040.50 0.40 ug/L1
1,1-Dichloroethene ND 11/29/2019 11040.50 0.40 ug/L1
cis-1,2-Dichloroethene ND 11/29/2019 11040.50 0.40 ug/L1
trans-1,2-Dichloroethene ND 11/29/2019 11040.50 0.40 ug/L1
1,2-Dichloropropane ND 11/29/2019 11040.50 0.40 ug/L1
1,3-Dichloropropane ND 11/29/2019 11040.50 0.40 ug/L1
2,2-Dichloropropane ND 11/29/2019 11040.50 0.40 ug/L1
1,1-Dichloropropene ND 11/29/2019 11040.50 0.40 ug/L1
cis-1,3-Dichloropropene ND 11/29/2019 11040.50 0.40 ug/L1
trans-1,3-Dichloropropene ND 11/29/2019 11040.50 0.40 ug/L1
Diisopropyl ether (IPE)ND 11/29/2019 11040.50 0.40 ug/L1
Ethylbenzene ND 11/29/2019 11040.50 0.40 ug/L1
Hexachlorobutadiene ND 11/29/2019 11040.50 0.40 ug/L1
Isopropylbenzene (Cumene)ND 11/29/2019 11040.50 0.40 ug/L1
p-Isopropyltoluene (p-Cymene)ND 11/29/2019 11040.50 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 11/29/2019 11040.50 0.40 ug/L1
Methylene chloride ND 11/29/2019 11040.50 0.40 ug/L1
Naphthalene ND 11/29/2019 11040.50 0.40 ug/L1
n-Propylbenzene ND 11/29/2019 11040.50 0.40 ug/L1
Styrene ND 11/29/2019 11040.50 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 10 of 16
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:UQ37425-001
37425 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
1,1,1,2-Tetrachloroethane ND 11/29/2019 11040.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 11/29/2019 11040.50 0.40 ug/L1
Tetrachloroethene ND 11/29/2019 11040.50 0.40 ug/L1
Toluene ND 11/29/2019 11040.50 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 11/29/2019 11040.50 0.40 ug/L1
1,2,3-Trichlorobenzene ND 11/29/2019 11040.50 0.40 ug/L1
1,2,4-Trichlorobenzene ND 11/29/2019 11040.50 0.40 ug/L1
1,1,1-Trichloroethane ND 11/29/2019 11040.50 0.40 ug/L1
1,1,2-Trichloroethane ND 11/29/2019 11040.50 0.40 ug/L1
Trichloroethene ND 11/29/2019 11040.50 0.40 ug/L1
Trichlorofluoromethane ND 11/29/2019 11040.50 0.40 ug/L1
1,2,3-Trichloropropane ND 11/29/2019 11040.50 0.40 ug/L1
1,3,5-Trimethylbenzene (Mesitylene)ND 11/29/2019 11040.50 0.40 ug/L1
1,2,4-Trimethylbenzene ND 11/29/2019 11040.50 0.40 ug/L1
Vinyl chloride ND 11/29/2019 11040.50 0.40 ug/L1
m+p - Xylenes ND 11/29/2019 11040.50 0.40 ug/L1
o - Xylenes ND 11/29/2019 11040.50 0.40 ug/L1
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 84 70-130
Bromofluorobenzene 93 70-130
Toluene-d8 95 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 11 of 16
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:UQ37425-002
37425 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 47 11/29/2019 0925935070-1301
Bromobenzene 49 11/29/2019 0925985070-1301
Bromochloromethane 44 11/29/2019 0925895070-1301
Bromodichloromethane 45 11/29/2019 0925905070-1301
Bromoform 53 11/29/2019 09251075070-1301
Bromomethane (Methyl bromide)50 11/29/2019 0925995060-1401
n-Butylbenzene 49 11/29/2019 0925985070-1301
sec-Butylbenzene 52 11/29/2019 09251035070-1301
tert-Butylbenzene 52 11/29/2019 09251055070-1301
Carbon tetrachloride 46 11/29/2019 0925925070-1301
Chlorobenzene 48 11/29/2019 0925965070-1301
Chloroethane 53 11/29/2019 09251075042-1631
Chloroform 43 11/29/2019 0925865070-1301
Chloromethane (Methyl chloride)53 11/29/2019 09251055020-1581
2-Chlorotoluene 45 11/29/2019 0925915070-1301
4-Chlorotoluene 47 11/29/2019 0925945070-1301
Dibromochloromethane 49 11/29/2019 0925985070-1301
1,2-Dibromoethane (EDB)47 11/29/2019 0925955070-1301
Dibromomethane (Methylene bromide)46 11/29/2019 0925915070-1301
1,2-Dichlorobenzene 48 11/29/2019 0925965070-1301
1,3-Dichlorobenzene 47 11/29/2019 0925945070-1301
1,4-Dichlorobenzene 46 11/29/2019 0925925070-1301
Dichlorodifluoromethane 56 11/29/2019 09251115060-1401
1,1-Dichloroethane 44 11/29/2019 0925885070-1301
1,2-Dichloroethane 44 11/29/2019 0925885070-1301
1,1-Dichloroethene 44 11/29/2019 0925875070-1301
cis-1,2-Dichloroethene 43 11/29/2019 0925875070-1301
trans-1,2-Dichloroethene 44 11/29/2019 0925875070-1301
1,2-Dichloropropane 46 11/29/2019 0925925070-1301
1,3-Dichloropropane 46 11/29/2019 0925915070-1301
2,2-Dichloropropane 50 11/29/2019 09251015070-1301
1,1-Dichloropropene 44 11/29/2019 0925885070-1301
cis-1,3-Dichloropropene 45 11/29/2019 0925915070-1301
trans-1,3-Dichloropropene 47 11/29/2019 0925945070-1301
Diisopropyl ether (IPE)43 11/29/2019 0925865070-1301
Ethylbenzene 48 11/29/2019 0925965070-1301
Hexachlorobutadiene 59 11/29/2019 09251195070-1301
Isopropylbenzene (Cumene)53 11/29/2019 09251065070-1301
p-Isopropyltoluene (p-Cymene)51 11/29/2019 09251015070-1301
Methyl tertiary butyl ether (MTBE)41 11/29/2019 0925825070-1301
Methylene chloride 42 11/29/2019 0925845070-1301
Naphthalene 51 11/29/2019 09251015050-1401
n-Propylbenzene 49 11/29/2019 0925985070-1301
Styrene 49 11/29/2019 0925975070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 12 of 16
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:UQ37425-002
37425 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,1,1,2-Tetrachloroethane 52 11/29/2019 09251045070-1301
1,1,2,2-Tetrachloroethane 50 11/29/2019 0925995070-1301
Tetrachloroethene 52 11/29/2019 09251035070-1301
Toluene 48 11/29/2019 0925955070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 48 11/29/2019 0925955070-1301
1,2,3-Trichlorobenzene 55 11/29/2019 09251105070-1301
1,2,4-Trichlorobenzene 53 11/29/2019 09251065070-1301
1,1,1-Trichloroethane 44 11/29/2019 0925875070-1301
1,1,2-Trichloroethane 48 11/29/2019 0925965070-1301
Trichloroethene 49 11/29/2019 0925975070-1301
Trichlorofluoromethane 50 11/29/2019 09251005060-1401
1,2,3-Trichloropropane 44 11/29/2019 0925875070-1301
1,3,5-Trimethylbenzene (Mesitylene)49 11/29/2019 0925985070-1301
1,2,4-Trimethylbenzene 48 11/29/2019 0925965070-1301
Vinyl chloride 53 11/29/2019 09251065060-1401
m+p - Xylenes 49 11/29/2019 0925995070-1301
o - Xylenes 49 11/29/2019 0925975070-1301
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 89 70-130
Bromofluorobenzene 98 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 13 of 16
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 14 of 16
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 15 of 16
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 16 of 16