23018_Corey Transmission_BrownfieldsAssessmentReport_09.11.2019

Brownfields Assessment Report
Brownfields Project ID: 23018-19-060
ECS Project No. 49-8458-B
Page 1

September 10, 2019

Mr. Cody Cannon
NCDEQ, DWM, NC Brownfields Program
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115

Reference: Brownfields Assessment Report
Corey Transmission Service
511 & 527 West Tremont Avenue
Charlotte, Mecklenburg County, North Carolina
Brownfields Project ID: 23018-19-060
ECS Project No. 49-8458-B

Dear Mr. Cannon:

ECS Southeast, LLP (ECS) prepared the attached Brownfields Assessment Report on behalf of TAC
Tremont, LLC. As part of the assessment, ECS constructed and sampled groundwater monitoring
wells and soil gas points, advanced soil borings and collected soil samples, and performed a
Brownfields receptor survey. Groundwater and soil samples were analyzed for volatile organic
compounds (VOCs), semi-volatile organic compounds (SVOCs), metals, and hexavalent
chromium. Soil gas samples were analyzed for VOCs. Soil gas was also screened for methane.
Because of a detection of mercury (a volatile metal) at concentrations above vapor intrusion
screening levels (VISLs) in a groundwater sample from monitoring well MW-5, a soil gas sample
was collected and analyzed for mercury vapor from a soil gas point (SG-7) located adjacent to
monitoring well MW-5. Monitoring well MW-5 was also resampled for mercury.

As indicated in the report, neither VOCs nor SVOCs were detected in groundwater samples at
concentrations above North Carolina Groundwater Quality Standards. Arsenic was detected in
one monitoring well (MW-4) at concentrations above North Carolina Groundwater Quality
Standards and the extent of arsenic appears limited based upon arsenic not being detected in
other monitoring wells. Monitoring well MW-4 is located near the southwest corner of the
smaller building located in the northeast portion of the site in Subsection C (as designated in work
plan and report). Mercury was detected in one monitoring well (MW-5) at concentrations above
North Carolina Groundwater Quality Standards and the extent of mercury appears limited based
upon mercury not being detected in other monitoring wells. Monitoring well MW-5 is located
northwest of the larger building located in the northwest portion of the site in Subsection D.

Brownfields Assessment Report
Brownfields Project ID: 23018-19-060
ECS Project No. 49-8458-B
Page 2

VOCs were not detected in soil samples at concentrations above preliminary soil remediation
goals (PSRGs). The SVOC, benzo(a)pyrene, was in one composite sample (B) at a concentration
above its respective residential PSRG. No other SVOCs were detected at concentrations above
PSRGs. Sample B is a composite sample collected from Subsection B which is located in the
southeastern portion of the site. Although the concentration of total chromium exceeded PSRGs
for the three different exposure scenarios in each of the five composite samples collected at the
site, ECS believes that trivalent chromium comprises the vast majority of the total chromium
detected based upon analyses for hexavalent chromium in these same samples. Hexavalent
chromium was detected in two of the five composite samples at concentrations above residential
PSRGs. The hexavalent detections are associated with composite samples D and E and are
associated with Subsections D and E which are located in the northwestern and western portions
of the site, respectively.

The concentrations of VOCs in soil gas samples did not exceed residential VISLs with the exception
of the soil gas sample SG-5. Soil gas sample SG-5 is located near the southwest corner of the
smaller building located in the northeast portion of the site in Subsection C. The extent of VOCs
in soil gas which exceeds residential VISLs appears limited based upon VOCs not being detected
above VISLs in other soil gas sample points.

Although mercury was detected in groundwater samples from monitoring well MW-5 at
concentrations above residential VISLs, mercury vapor was not detected in soil gas samples
collected near this same monitoring well.

Methane was detected at a maximum concentration of 12 percent of the lower explosive limit
(LEL). ECS understands that 20 percent of the LEL is typically used as a screening criteria for
methane and the results indicate methane concentrations were below this threshold.

Based upon the finding of this report which indicates isolated impacts in the various media and
the detected concentrations thereof, ECS opines that these media may be managed during
construction of proposed townhomes in a manner which is protective of construction workers,
future resident, persons visiting the site and surrounding areas, and persons working and residing
in surrounding areas.

REPORT OF ENVIRONMENTAL BROWNFIELD ASSESSMENT
COREY TRANSMISSION SERVICE
511 & 527 WEST TREMONT STREET
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT 49:8458-B
NCDEQ BROWNFIELDS ID NO. 23018-19-060

PREPARED FOR:
TAC TREMONT, LLC
2100 POWER FERRY ROAD SE
ATLANTA, GEORGIA, 30339

SEPTEMBER 10, 2019
September 10, 2019 Mr. Tyson Reilly
TAC Tremont, LLC
2100 Power Ferry Road SE
Atlanta, Georgia, 30339
Reference: Report of Environmental Brownfield Assessment Corey Transmission Service 511 & 527 West Tremont Avenue Charlotte, Mecklenburg County, North Carolina NCDEQ Brownfields ID No. 23018-19-060 ECS Project No. 49:8458-B Dear Mr. Reilly: ECS Southeast, LLP (ECS) is pleased to present TAC Tremont, LLC with the results of our Environmental Assessment for the above-referenced site. ECS’s services were provided in accordance with ECS proposals No. 49:15130P dated July 18, 2019 and authorized on July 19, 2019 and No.49:15420P dated August 9, 2019 and authorized on August 12, 2019. ECS appreciates the opportunity to provide our services to you. If there are questions regarding this report, or a need for further information, please contact us. Respectfully submitted, ECS SOUTHEAST, LLP Joseph P. Nestor, P.G, P.E. Lauren Zysling
Environmental Senior Project Manager Environmental Project Manager
[e-mail] [e-mail]
704-280-7422 803-250-3368

Matthew H. McDuffie, P.G.
Principal Geologist
[e-mail]
704-378-9003
Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
1
TABLE OF CONTENTS
1.0 PROJECT INFORMATION ...........................................................................................................1
2.0 SCOPE OF SERVICES ..................................................................................................................2
3.0 RESULTS ..................................................................................................................................8
4.0 CONCLUSIONS ....................................................................................................................... 11
5.0 RECOMMENDATIONS ............................................................................................................. 12
6.0 QUALIFICATIONS OF REPORT .................................................................................................. 12
FIGURES Figure 1 Site Topographic Map Figure 2 Site Location Map Figure 3 Groundwater Sample Location Map Figure 4 Soil Sample Location Map Figure 5 Soil Gas Sample Location Map Figure 6 Groundwater Potentiometric Map – August 19, 2019 TABLES Table 1 Summary of Well Construction and Groundwater Elevation Data – August 2019 Table 2 Summary of Groundwater Analytical Results Table 3 Summary of SVOCs and Metals in Soil (Composite Samples) Table 4 Summary of VOCs in Soil (Grab Samples) Table 5 Summary of Soil Gas Analytical Results Table 6 Summary of Methane in Soil Gas APPENDICES Appendix A Photograph Log Appendix B Monitoring Well Permits Appendix C Well Construction Records Appendix D Survey Data Table Appendix E Groundwater Sampling Field Parameters Data Appendix F Laboratory Analytical Data and Chain of Custody Records Appendix G Weather Information for August 21, 2019 Appendix H Brownfields Survey Form
Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
1
1.0 PROJECT INFORMATION

The site is currently comprised of one approximate 5.58-acre parcel identified as Mecklenburg Parcel ID
No. 11906101 located at 511 & 527 West Tremont Avenue in Charlotte, Mecklenburg County, North
Carolina and owned by Gene & Greg LLC (Figure 1 & 2). The site is currently developed with an
approximate 17,500-square foot building constructed in 1981 and an approximate 3,600-square foot
building that was constructed in 1988. Previous assessment activities include Phase I and II Environmental
Site Assessments (ESAs) completed by Salem Environmental in June and July of 2006, a Phase I ESA
completed by Enviro Scan in October 2014, a Phase I ESA completed by Summit Engineering, Inc. in
November 2015, and an Environmental Assessment and Phase I ESAs completed by ECS in October 2017
and January, 2019. The following recognized environmental conditions (RECs) were identified in the
previous Phase I ESAs:

• ECS considered the current and historical use of the subject property as an automotive repair
facility to be a REC of the subject property. The results from the previous environmental reports
completed at the subject property in 2006 and 2017, which identified soil, groundwater, and soil
gas impacts at concentrations that exceed the applicable standards is considered to be a REC of
the subject property.
• Based on the documented contamination and distance from the subject property and inferred
groundwater flow direction, the following facilities were considered to be RECs of the subject
property: Steve Lit, Inc., Powers Site, Beach Property, and Adams Property.
o Steve Lit, Inc., 421 West Tremont Avenue - Located on the east adjacent property and
topographically upgradient from the site. According to a 1998 Limited Site Assessment,
this facility had 2,000-gallon gasoline underground storage tank (UST) that was removed
in September 1997. Soil samples and one groundwater sample were collected in the
vicinity of the former UST. Groundwater was encountered at a depth of 10 feet below
grade. Soil sample concentrations were below detectable limits. The petroleum
hydrocarbons associated with gasoline and diesel were also below the detectable limit.
Tetrachloroethene (which is also known as perchloroethylene or PCE) was detected at 1
micrograms per liter (ug/L) and naphthalene at 600 ug/L, which exceeds their respective
NCDEQ 2L Groundwater Quality Standards. This incident received a letter of No Further
Action (NFA) with a Notice of Residual Petroleum in September 1998 for the UST Section
of the Division of Waste Management (DWM). The NFA indicates that PCE was detected
in monitoring well MW-1 and will be assessed by the Division of Water Quality.
o Adams Property, 510 West Tremont Avenue - Located on the north adjacent property
and topographically upgradient from the site. According to the online North Carolina
Department of Environmental Quality (NCDEQ) Brownfields Map Viewer, this facility is
listed as "active-eligible" brownfields property. According to the 2017
brownfield application submittal, known contaminants in the groundwater/surface water
at this facility include naphthalene, lead, and manganese. It was noted that chlorinated
solvents are possible due to trace levels for nearby properties.
o Powers Site, 436 West Tremont Avenue - Located on the north adjacent property and
topographically upgradient from the site. According to NCDEQ, this facility is listed as
active eligible North Carolina Brownfields Project as of July 6, 2017. No additional
information was available for this listing.
Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
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o Beacham Property, 420 West Tremont Avenue - Located approximately 200 feet
northeast and topographically upgradient from the site. According to the database and
information provided by the EDR report, naphthalene and low levels of PCE were
discovered in two temporary monitoring wells during a UST investigation involving one
6,000-gallon and one 1,000-gallon gasoline UST that were removed prior to 1980. The
petroleum release received a NFA with a Notice of Residual Petroleum, which disallows
the use of groundwater at this facility. Naphthalene detections in groundwater samples
collected were above the North Carolina DWM Non-Residential Vapor Intrusion Screening
Levels.
ECS performed environmental assessment in October 2017 including the collection of soil, groundwater, and soil gas samples at the site. The findings and results of the October 2017 assessment activities are summarized in a Draft Report of Environmental Assessment dated October 24, 2017.

On March 15, 2019, TAC Tremont, LLC submitted a Brownfields Property Application to the NCDEQ. On
June 12, 2019 NCDEQ issued a Letter of Eligibility (LOE) to TAC Tremont, LLC indicating that the subject
property was eligible for the North Carolina Brownfields Program (NCBP). The Brownfields Identification
Number assigned to this site is 23018-19-060. On July 17, 2019, representatives from ECS, NCBP and TAC
Tremont, LLC met on site to discuss data gaps and possible additional assessment activities required
before the Brownfields Agreement is finalized. On July 18, 2019, the NCBP forwarded a Request for
Additional Assessment (RAA) to TAC Tremont, LLC on July 22, 2019. ECS submitted a work plan to the
NCBP in response to its Request for Additional Assessment. The July 22, 2019 work plan was prepared to
address groundwater assessment and no other media. On July 23, 2019, NCBP approved the July 22, 2019
work plan. On August 1, 2019, ECS submitted another work plan to address soil and soil gas. On August
2, 2019, NCBP commented on the August 1, 2019 work plan and requested revised work plan be
submitted. ECS submitted a revised work plan on August 2, 2019, which was accepted by the NCBP on
August 5, 2019. The client plans to develop the property with approximately 100 townhome units,
including small private yards and shared open space consistent with the approved zoning of the property. The approved work plans were implemented. This report summarizes the findings from the assessment
activities which were performed as outlined in the approved work plans.

2.0 SCOPE OF SERVICES

The environmental assessment consisted of the collection of soil, groundwater samples, and soil gas
samples. Drilling activities were conducted using a Geoprobe® drill rig capable of both DPT and air
rotary/percussion drilling. The drilling subcontractors used for this project were Geologic Exploration
Company (GEX) of Statesville, North Carolina and 3D Environmental Investigations, LCC of Statesville,
North Carolina. Monitoring wells were constructed on July 29 and 30, 2019. Soil sampling activities were
conducted on August 19, 2019 and August 20, 2019. Groundwater sampling was performed on August 2,
2019, August 5, 2019, August 6, 2019 and August 26, 2019. Soil gas monitoring points were installed on
August 19, 2019 and August 20, 2019. Soil gas sampling was performed on August 21, 2019 and August
26, 2019. A photographic log documenting the field activities is provided in Appendix A.

Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
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2.1 Public Utility Locate

Prior to implementing the field activities, ECS contacted North Carolina public utility locate service (811)
to locate/mark public utilities at the site.

2.2 Monitoring Well Permit

Prior to commencing with field activities, ECS obtained a monitoring well permit from the North Carolina
Department of Environmental Quality (NCDEQ). A copy of the permit is included in Appendix B. In
accordance with the NCDEQ permit, a well construction record for each permanent monitoring well is to
be submitted to the NCDEQ on its Form GW-1. The forms were completed by the North Carolina licensed
well driller and are included as Appendix C. Additionally, a Mecklenburg County Subsurface Investigation
Permit (SIP) was procured. The Mecklenburg County SIP is included as Appendix B.

2.3 Monitoring Well Installation Activities

The monitoring wells were designated as MW-1, MW-2, MW-3, MW-4 and MW-5 respectively. The
monitoring well locations are depicted on Figure 3.

On July 29, 2019 and July 30, 2019, each monitoring well was installed by advancing a six inch diameter air
percussion bit. At monitoring well locations MW-1, MW-2 and MW-3, a 20-foot section of 2-inch diameter
well screen was connected to an 18-foot, 2-inch diameter section of well casing and placed into the boring.
At monitoring well location MW-4, a 10-foot section of 2-inch diameter well screen was connected to a 5-
foot, 2-inch diameter section of well casing and placed into the boring. At monitoring well location MW-5, a
15-foot section of 2-inch diameter well screen was connected to a 10-foot, 2-inch diameter section of well
casing and placed into the boring. The material of construction of the well screen and casing was schedule
40, polyvinyl chloride (PVC) pipe. The well screen contained 0.010-inch slots which were machine cut. After
the well screen and casing was set, fine silica sand was placed around and approximately 2 feet above the top
of the well screen at each monitoring well location. A 3-foot (approximate) bentonite seal was placed above
the filter sand and the remaining annular space was grouted nearly to grade at each monitoring well location.
Each monitoring well was completed flush to grade inside an 8-inch diameter, bolt-down manhole set in a 2-
foot by 2-foot concrete pad. Each monitoring well was provided with a locking expansion plug. Refer to Table
1 for well construction details.

Following completion of the well construction, the driller developed each monitoring well by over pumping
with an electric submersible pump. Water was extracted from each well until it appeared relatively free of
sediments and discharged to the ground surface. Approximately 15, 28, 45, 60, and 30 gallons of water
were removed from monitoring wells MW-1, MW-2, MW-3, MW-4 and MW-5, respectively.

On August 22, 2019, Summit of the Carolinas, PC surveyed the horizontal locations and ground surface
and top of casing elevations of the monitoring wells. Appendix D contains a table which summarizes this
survey data.

Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
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2.4 Groundwater Sample Collection

ECS visited the subject site on August 2, 2019, August 5, 2019, August 6, 2019 and August 26, 2019 for the
purpose of conducting groundwater monitoring activities. Monitoring well MW-1 was sampled on August
2, 2019 and monitoring wells MW-2, MW-3, and MW-5 were sampled on August 5, 2019 and monitoring
well MW-4 was sampled on August 6, 2019. Monitoring well MW-5 was resampled on August 26, 2019
for mercury.

Prior to collection of groundwater samples, ECS measured the depth to water in each monitoring well
using an electronic water level meter (Heron Model Dipper T). ECS opened each monitoring well and
allowed each well to equilibrate with atmospheric pressure prior to collecting depth to water
measurements. ECS cleaned the water level indicator prior to use at each monitoring well.
Measurements were recorded to the nearest one-hundredth of a foot. Measurements of the depth to
water for the August 2019 monitoring events, surveyed elevations of the tops of well casings, and
calculated groundwater elevations are included in Table 1.

The five monitoring wells were sampled using low-flow sampling techniques in general conformance with
the procedures outlined in the July 22, 2019 work plan. Groundwater was extracted from each monitoring
well at low flow rates using an electric submersible variable speed sampling pump (Proactive
Environmental Products Stainless Steel 12 volt Monsoon Model with Power Booster II LCD Controller).
ECS cleaned the pump prior to use at each monitoring well. A new length of polyethylene tubing was
connected to the pump and the pump was lowered to the approximate midpoint between the measured
water level and bottom of the screen in each monitoring well. The polyethylene tubing was connected to
a flow cell into which the probe of a multi-parameter water quality meter (Horiba model U-52 or Hanna
model 9829) was inserted. Field water quality measurements were collected as water was extracted from
each well and passed though the flow cell. Appendix E includes groundwater sampling field parameters
data. Groundwater was pumped from each monitoring well using the submersible electric pump directly
into laboratory provided containers at each of the sampling locations.

The groundwater sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into a cooler with ice to
maintain the samples at approximately 4° Celsius (C°). The soil and groundwater samples were submitted
to Pace Analytical Services, LLC in Huntersville, North Carolina.

Groundwater samples from monitoring wells MW-1, MW-2, MW-3, MW-4, MW-5 and a duplicate sample
from monitoring well MW-1 (sample designated DUP) were analyzed for VOCs by EPA Method 8260B;
SVOCs by EPA Method 8270D; total RCRA metals by EPA Methods 6020B/7470A. In addition a trip blank
sample (designated sample TB) was analyzed for VOCs, SVOCs and RCRA Metals. Monitoring well MW-5
was resampled on August 26, 2019 for mercury only by EPA Method 7470A. ECS maintained chain-of-
custody (COC) procedures throughout the sample collection and transportation process. Copies of the COCs
are included in Appendix E.

Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
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2.5 Soil Boring Activities

On August 19 and 20, 2019, five soil borings were advanced in each of the five distinct subsections at the
site (identified as A through E), yielding a total of twenty-five soil borings. The soil boring designations
were A-1 through A-5, B-1 through B-5, C-1 through C-5, D-1 through D-5, and E-1 through E-5. The soil
boring locations are depicted on Figure 4.

The soil borings were advanced by hydraulically driving a five-foot long, 1.5-inch diameter soil sampling
probe into the soil to a depth of 2-feet below the ground surface (bgs). Prior to advancing each boring,
the down-hole equipment was decontaminated utilizing a pressure washer and municipal water. The
down-hole equipment was decontaminated to prevent cross-contamination between boring locations.

Soil samples were collected from each of the soil boring locations using a soil sampling probe lined with a
dedicated disposable clear plastic tube. After the soil sampling probe was driven, the clear plastic tube
filled with soil was removed from the probe and cut open to expose the soil. ECS visually classified the soil
collected from each boring and screened the soil samples for relative levels of volatile organic vapors using
a photoionization detector (PID) and soil samples were collected from an interval between 0 and 2 feet
bgs.

On August 22, 2019, Summit of the Carolinas, PC surveyed the horizontal locations and ground surface
elevations of the soil boings. Appendix D contains a table which summarizes this survey data.

2.6 Soil Sample Collection

On August 19 and 20, 2019, soil samples were collected by a sampler wearing a new pair of disposable
nitrile gloves from the clear plastic tubes retrieved from the soil sample probe. The soil samples were
placed directly into laboratory provided containers.

Soil samples from the 0 to 2-foot interval from each boring, in each subsection (A through E), were
composited into a single sample, identified as A, B, C, D, E and duplicate sample, DUP-2 from the B
subsection, for analyses for semi-volatile organic compounds (SVOCs) by EPA Method 8270 and metals
regulated under the Resource Conservation and Recovery Act (RCRA metals) by EPA Method 6010D. In
addition, an aliquot of each composite sample was held pending results of the analyses for RCRA metals.
These aliquots may be analyzed for hexavalent chromium by EPA Method 7199 at a later time if deemed
appropriate by NCBP. Two grab samples were collected from two soil borings in each subsection and
where identified as A-2, A-3, B-1, B-2, C-2, C-3, D-1, D-4 E-3, E-5 and duplicated sample, DUP-1 from the
A-2 location, were analyzed for volatile organic compounds (VOCs) by EPA Method 8260. The grab
samples were selected on the basis of highest evidence of apparent impacts based upon field screening
with photoionization detector (PID) and/or visual and olfactory observations.

The soil sample containers were labeled with ECS project number, sample identification, sample date and
time, and requested analytical analysis. The containers were placed into a cooler with ice to maintain the
samples at approximately 4° Celsius (C°). The soil and groundwater samples were submitted to Pace
Analytical Services, LLC in Huntersville, North Carolina.

Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
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ECS maintained proper chain-of-custody (COC) procedures throughout the sample collection and
transportation process. Copies of the COCs are included in Appendix F.

2.7 Soil Gas Sample Point Installation Activities

On August 19, 2019 and August 20, 2019, ECS installed eight permanent exterior sub-slab soil gas
sample points and were identified as SG-1 through SG-8. The locations of the sample points are
shown in Figure 5. Each soil gas sample was constructed by excavating a 1.5-inch diameter boring using
a Geoprobe® drill rig to a depth of 5 feet bgs. A 6-inch long stainless-steel vapor implant was placed in
the bottom of each boring. Polyethylene tubing was then connected to vapor implant and routed above
grade at each sample point. Clean quartz filter sand was placed around and approximately 6 inches above
the vapor implant at each sample point, with a 1-foot bentonite seal was placed above the filter sand and
hydrated. The remaining annular space was grouted to near-grade at each sample point and capped with
a bolt-down manhole.

2.8 Soil Gas Sample Collection

On August 21, 2019 ECS collected soil gas samples from each of the eight sample points (SG-1 through SG-
8 and a duplicate sample [designated DUP-1] was collected from sampling point SG-1). Sampling activities
were performed between approximately 1235 and 1600 on this date. ECS noted that the barometric
pressure fell during the time when sampling was conducted. ECS noted at 1253 and 1552 on this date
that the barometric pressure was 30.04 and 30.00 inches of mercury (in-Hg), respectively. The
temperature during this same period increased from 87 to 90 degrees Fahrenheit. Winds velocities during
the time sampling was performed ranged from 7 to 1 miles per hour. A printout from the webpage
https://www.timeanddate.com/weather/usa/charlotte/historic showing weather observations on
August 21, 2019 is included as Appendix G.

The seal was leaked tested using helium gas, a gas shroud, and a helium detector as recommended in
NCDEQ-DWM Vapor Intrusion Guidance (Alexander, March 2018). Helium was released into the shroud
and the helium concentration was monitored. When the helium concentration reached 20 percent, a soil
gas sample was collected and measured with a helium detector.
After leak testing, the sample train was purged of approximately 3 tubing volumes at a rate of 200
milliliters per minute. The tubing was then connected to a pre-evacuated and pre-cleaned Summa
canister for sampling. ECS utilized 1-liter Summa canisters which were individually certified by laboratory.
The Summa canisters were submitted to a Pace laboratory for analyses for VOCs by EPA Method TO-15.
North Carolina does not certify laboratories for analyses of air/soil gas samples. ECS will requested that
the laboratory analyze the samples for the most current and applicable standards from the National
Environmental Laboratory Accreditation Conference (NELAC) Program. One duplicate soil gas sample of
SG-1 was collected and submitted for laboratory analysis by EPA Method TO-15.

ECS maintained chain-of-custody (COC) procedures throughout the sample collection and transportation
process. Copies of the COCs are included in Appendix F.

Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
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2.9 Assessment of Methane in Soil Gas

On August 21, 2019, ECS extracted and measured methane gas concentration from each of the soil gas
sampling points utilizing a Landtec GEM™ 2000 Landfill Gas Analyzer and Extraction Monitor. Calibration
of the meter was performed in accordance with the GEM™ 2000 Operation Manual prior to use. In
addition, a bump test was performed at the beginning of sampling to verify meter calibration and
accuracy. The bump test was performed by briefly exposing the unit to a known concentration of
methane gas (50 percent). Bump test reading was 50%, within a range of ±3% of the actual test gas
concentration is considered acceptable.

ECS connected the gas analyzer to the tubing at each sample point and purged and measure extracted
methane gas. ECS observed the readings and recorded the highest percent methane and percent of lower
explosive limit reading.

2.10 Assessment of Mercury in Soil Gas

Following detection of mercury in the initial groundwater sample from monitoring well MW-5, at the
suggestion of NCDEQ, ECS made arrangements to perform soil gas sampling for mercury vapor at the
nearest soil gas sample point to monitoring well MW-5 which is sample point SG-7.

On August 21, 2019, ECS extracted soil gas from sample point SG-7 using an industrial hygiene air sampling
pump set at a flow rate of 200 milliliters per minute (mL/min). Soil gas was run through a carulite sorbent
tube to collect mercury vapor. Soil gas was collected over a period of 150 minutes (2.5 hours) for a total
volume of 30 liters (L). In addition, ECS collected a field blank sample on another carulite sorbent tube.
The samples tubes were submitted to EMSL Analytical, Inc. in Pineville, North Carolina for analyses for
mercury vapor by NIOSH Method 6009.

ECS maintained chain-of-custody (COC) procedures throughout the sample collection and transportation
process. Copies of the COCs are included in Appendix F.

2.11 Surveying of Sample Points

ECS engaged the services of Summit to survey the horizontal locations and ground surface elevations of
the various sample collection points. In addition, Summit determined the top of casing elevations of each
of the monitoring wells. Appendix D contains a table which summarizes this survey data.

2.12 Brownfields Receptor Survey

ECS performed a Brownfields receptor survey. This survey was performed by researching various data
sources through the internet and a windshield survey of the area.

Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
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3.0 RESULTS

3.1 Groundwater Elevation and Inferred Flow Direction

Table 1 summarizes water level measurement collected on August 2, 2019 and August 19, 2019 as well as the
calculated groundwater elevation. The groundwater elevation data was calculated by subtracting the
measured depth to water from the survey elevation of the top of casing for each monitoring well. Figure 6 is
a groundwater potentiometric map for the shallow groundwater at the subject property based upon the
calculated groundwater elevation data for August 19, 2019. As shown in this figure, the inferred groundwater
flow direction on August 19, 2019 is to the northwest.

3.2 Groundwater Sample Results

A summary of the groundwater analytical results are provided on Table 2. As shown in this table, the
analytical results for groundwater samples were compared to the NC2LGWQS and the vapor intrusion
screening levels (VISLs) for residential and non-residential exposure scenarios. VISLs were established by
the IHSB. The VISLs were last updated by the IHSB in February 2018.

Several total RCRA metals were detected in samples MW-1, MW-2, MW-3, MW-4, MW-5 and DUP
(duplicate of sample MW-1) above their respective minimal detection limits (MDL). Arsenic (170 µg/l) in
monitoring well MW-4 and mercury (1.3 µg/l), in monitoring well MW-5, were detected at a
concentrations of exceeding their NC2LGWQS of 10 µg/l and 1 µg/l, respectively. The remainder of the
detected metals did not exceeded the NC2LGWQS. In addition, mercury (1.3 µg/l) exceeded the
residential and non-residential VISLs of 0.18 µg/l and 0.75 µg/l, respectively. VISL have not been
established for the remainder of the RCRA metals because the metals are not volatile and do not pose a
vapor intrusion risk. Of the 12 positive detections for metals, 5 were detected at concentration above
their respective MDL, but below their respective reporting limit (RL) and were J-flagged by the laboratory.

Due to the exceedance of mercury in samples from monitoring well MW-5, at the suggestion of NCDEQ,
that well was re-sampled for mercury on August 26, 2019. The results indicated that mercury was detected
at a lower level than the previous sampling, at a concentration of 0.70 µg/l, exceeding the residential of
0.18 µg/l, but below the NC2LGWQS of 1 µg/l and the non-residential VISLs of 0.70 µg/l.

Laboratory results indicated that SVOC were not detected at concentrations in samples MW-1, MW-2,
MW-3, MW-4, MW-5 and DUP (duplicate of sample MW-1) above their respective MDLs and below their
respective NC2LGWQS.

Laboratory results for sample MW-3, MW-4 and MW-5 indicate that the VOC compound methyl tertiary-
butyl ether (MTBE) were detected at concentrations below the NC2LGWQS of 20 µg/L and did not exceed
the VISL. The remainder of the VOC were not detected at concentrations above their respective MDLs
and are below their respective NC2LGWQS.

Laboratory results for the Trip Blank (TB) indicated that metals, SVOC and VOCs were not detected above
their respective MDLs and are below their respective NC2LGWQS.

Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
9
3.3 Soil Sample Results

COMPOSITE SAMPLES
Laboratory analysis indicates that SVOCs, and RCRA metals were detected in several soil samples soil
samples collected on August 19, 2019 and August 20, 2019. ECS compared detected concentrations for
SVOCs, and RCRA metals to preliminary soil remediation goals (PSRGs) for residential or
industrial/commercial exposure scenarios and the leaching from soil to groundwater exposure scenario.
The laboratory data and comparison data are shown in Table 3.

Several SVOCs were detected in composite soil samples A, B, and E at concentrations below their
respective PSRGs, with the exception of benzo(a)pyrene in sample B. Benzo(a)pyrene was detected in
sample B at a concentration of 0.322 mg/Kg, which exceeds the residential PSRG (0.11 mg/Kg) and the
groundwater PSRG (0.12mg/Kg), however, the detected concentrations is below the
industrial/commercial PSRG (2.1 mg/Kg).

RCRA metals were detected in each of the five composite soil samples. With the exception of total
chromium, none of the detected concentrations of RCRA metals exceeded industrial/commercial PSRGs.
The detected concentrations of total chromium ranged from 17.7 mg/kg for sample DUP-2 to 104 mg/kg
for sample D. The concentrations of total chromium associated with samples A, B, C, D, E, and DUP-2
(duplicate of MP-1S) exceeded the industrial/commercial PSRG for total chromium (6.5 mg/kg).
Hexavalent chromium was detected at an estimated concentration of 0.509 mg/kg in sample D and 0.316
mg/Kg in sample E. These results were J-flagged by the laboratory indicating that the estimated
concentration was above the adjusted method detection limit and below the adjusted reporting limit.
Hexavalent chromium was not detected in the remaining three soil samples or the duplicate sample. The
calculated concentrations of trivalent chromium for the soil samples collected on April 29, 2019 did not
exceed PSRGs. ECS calculated the concentration of trivalent chromium in soil samples by subtracting the
detected concentration of hexavalent chromium from the detected concentration of total chromium. In
cases in which hexavalent chromium was reported as not detected by laboratory, ECS assumed the
concentration of hexavalent chromium was at the laboratory method detection limit (MDL) and
subtracted this value from the concentration for total chromium.

Arsenic was detected in soil samples C (1.0 mg/Kg) and E (1.5 mg/Kg) at concentration exceeding the
residential use PSRG (0.68 mg/Kg), but below the industrial/commercial PSEG (3.0 mg/Kg) and protection
of groundwater PSEG (5.8 mg/Kg). The concentrations of arsenic in soil detected during this assessment
are consistent with expected concentrations of naturally occurring arsenic in this region and is not
necessarily indicative of a release of hazardous substances.

The remainder of the RCRA metals were not detected at concentrations exceeding their respective PSRGs
for residential or industrial/commercial exposure scenarios and the leaching from soil to groundwater
exposure scenario.

GRAB SAMPLES
Laboratory analysis indicates that VOCs were detected in several soil samples soil samples collected on
August 19, 2019 and August 20, 2019. ECS compared detected concentrations for VOCs PSRGs for
residential or industrial/commercial exposure scenarios and the leaching from soil to groundwater
exposure scenario. The laboratory data and comparison data are shown in Table 4.
Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
10

Acetone was detected in samples C-3, D-1, and DUP-1 (duplicate of A-2) at concentrations below PSRGs.
Acetone is a common laboratory contaminant.

The compound, benzene, was detected in samples C-3 at a concentration below the PSRGs for residential
or industrial/commercial exposure scenarios and the leaching from soil to groundwater exposure
scenario.

3.4 Soil Gas Sample Results

Laboratory analysis indicates that VOCs were detected in several soil gas samples soil collected on August
21, 2019. ECS compared detected concentrations for VOCs to sub-slab and exterior vapor intrusion
screening level (VISL) for residential and non-residential scenarios. The laboratory data and comparison
data are shown in Table 5.

Laboratory results for sample SG-1, SG-2, SG-3, SG-4, SG-7, SG-8 and DUP-1 indicate detections of several
VOCS above their respective method detection limits. Of these detections, the concentrations of the VOCs
did not exceed their respective residential or non-residential soil gas VISLs.

Laboratory results for sample SG-5 indicate detections of several VOCS above their respective method
detection limits. Of these detections, the concentration of ethylbenzene (15,400 ug/m3) exceeded both
the residential and non-residential soil gas VISLs (370 and 4,900 ug/m3, respectively) and the
concentrations of n-heptane (13,600 ug/m3), n-hexane (5,000 ug/m3), 1,3,5-trimethylbenzene (461
ug/m3), and m,p-xylene (4,150 ug/m3) exceeded their respective residential soil gas VISLs of 2,800 ug/m3,
4,900 ug/m3, 420 ug/m3, and 700 ug/m3, but below their respective non-residential soil gas VISLs.

Laboratory results for sample SG-6 indicate the detection of trichhloroethene (TCE) at 15.2 ug/m3 which
is above its residential VISL (14 ug/m3) but below its non-residential VISL (180 ug/m3). Laboratory results
for sample SG-6 indicate the concentrations of n-heptane (13,600 ug/m3), n-hexane (5,000 ug/m3), 1,3,5-
trimethylbenzene (461 ug/m3), and m,p-xylene (4,150 ug/m3) exceeded their respective residential soil
gas VISLs of 2,800 ug/m3, 4,900 ug/m3, 420 ug/m3, and 700 ug/m3, but below their respective non-
residential soil gas VISLs.

3.5 Mercury in Soil Gas

Laboratory results for sample SG-7 indicated the mercury was not detected at concentration exceeding
its respective RL and below the residential sub-slab and exterior soil gas VISL. The laboratory data and
comparison data are shown in Table 5.

Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
11
3.6 Methane in Soil Gas

Table 6 summarizes methane gas readings. Methane was detected in soil gas extracted from sample
points SG-1, SG-2, SG-3 or SG-8 on August 21, 2019. Methane was detected in soil gas extracted from
sample points SG-4, SG-5, SG-6, and SG-7. The measured methane concentrations associated with sample
point SG-4, SG-5, SG-6, and SG-7 were 0.6, 0.4, 0.6, and 0.3 percent on August 21, 2019, respectively.
Lower explosion limits (LEL) reading were recorded between 0.0 % and 12.0 %.

3.7 Brownfields Survey

ECS completed the Brownfields receptor survey on a form provided by the NCBP. This form is included as
Appendix H.

4.0 CONCLUSIONS

Based on the results of the field activities and laboratory analysis, ECS concludes the following:

• VOCs, specifically acetone and benzene, were detected in the grab soil samples at concentrations
below PSRGs for the three exposure scenarios during this assessment. Acetone is common laboratory
contaminant and its detection is soil samples may be unrelated to site conditions.
• Benzo(a)pyrene was detected in composite soil sample B at a concentration above the PSRG for
residential exposure and protection of groundwater, but below the PSRG for commercial/industrial
exposure. Benzo(a)pyrene was not detected in groundwater samples above the NC2LGWQS.
• Arsenic was detected in composite soil samples C and D at concentrations above PSRGs for residential
and below industrial/commercial exposure scenarios during this assessment. The concentrations of
arsenic detected in soil during this assessment are consistent with expected concentrations of
naturally occurring arsenic in this region and is not necessarily indicative of a release of hazardous
substances.
• Total chromium in soil was detected in each of the five composite soil samples at concentrations
above PSRGs for protection of groundwater and residential and industrial/commercial exposure
scenarios during this assessment. It appears that the vast majority of total chromium is comprised of
trivalent chromium and not the more toxic hexavalent chromium. Hexavalent chromium was
detected in two composite samples (Samples D and E) at concentrations above the PSRG for
residential exposure.
• With the exception of arsenic and chromium; no RCRA metal was detected in soil samples collected
in concentrations above PSRGs for the three exposure scenarios during this assessment.
• Arsenic was detected at a concentration above the NC2LGWQS in monitoring well MW-4.
• The initial groundwater sample collected on August 5, 2019, from monitoring well MW-5 indicated
that mercury was detected at a concentration above the NC2LGWQS and residential and non-
residential VISL. Monitoring well MW-5 was re-sampled on August 26, 2019 and the results indicated
that the concentration of mercury is below the NC2LGWQS and non-residential VISL, however above
the residential VISL. Additional soil gas sampling for mercury was conducted at point SG-7 (adjacent
to MW-5). The results indicated that mercury was not detected in SG-7 at a concentration above the
non-residential and residential VISLs.
Report of Environmental Assessment
Corey Transmission
ECS Project No. 49:8458-B
September 10, 2019
12
• No other RCRA metals were detected in groundwater samples collected at concentrations above the
NC2LGWQS during this assessment.
• Concentrations of methane gas did not exceed 12 % of LEL.
• Ethylbenzene was detected in a single soil gas sample, SG-5, at concentrations above non-residential
and residential VISLs.
• The compounds n-heptane, n-hexane, 1,3,5-trimethylbenzene, and m,p-xylene were detected in soil
gas samples at concentrations above residential VISLs in one soil gas sample (SG-5).

5.0 RECOMMENDATIONS

Based on the results of this Brownfields assessment, ECS recommends that the NCBP approve this report,
and a Brownfields agreement be prepared for the subject property authorizing the development of the
townhomes with private yards, subject to restrictions consistent with the goals of the Brownfields
program.

6.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those normally employed in environmental assessment projects of this type. Our evaluation of site conditions has been based on our understanding of the site project information and the data obtained during our field activities. This report was prepared for the express use of Portman Holdings. Use of this report by other individuals or companies implies their acceptance of the General Conditions of Service of the original contract.
FIGURES
FIGURE 1SITE TOPOGRAPHIC MAP
511 and 527 West Tremont AvenueCharlotte, Mecklenburg County, North Carolina
ECS Project Number 49:8458-B
SOURCE:USGS Topographic MapCharlotte East & West North Carolina Quadrangle2016
Scale
1-inch = 2,000 feet
SITE
1’2,000’1,000’
FIGURE 2SITE LOCATION MAP
511 and 527 West Tremont AvenueCharlotte, Mecklenburg County, North Carolina
ECS Project Number 49:8458-B
SOURCE:
MECKLENBURG COUNTY POLARIS GEOGRAPHIC
INFORMATION SYSTEM
SEPTEMBER 3, 2019
SCALE NOT INDICATED
Gas-Fired
Products, Inc.
Residential
Residential
Inner Peaks
Climbing
Center
Vacant Land
FIGURE 3GROUNDWATER SAMPLE LOCATION MAP
511 and 527 West Tremont AvenueCharlotte, Mecklenburg County, North Carolina
ECS Project Number 49:8458-B
SOURCE:
GOOGLE EARTH, DATED 2017
SCALE:
AS SHOWN
GROUNDWATER SAMPLE LOCATION
APPROXIMATE SITE BOUNDARY
LEGEND
MW-5
MW-4
MW-3
MW-2
MW-1
FIGURE 4SOIL SAMPLE LOCATION MAP
511 and 527 West Tremont AvenueCharlotte, Mecklenburg County, North Carolina
ECS Project Number 49:8458-AB
SOURCE:
GOOGLE EARTH, DATED 2017
SCALE:
AS SHOWN
SOIL SAMPLE LOCATION
APPROXIMATE SITE BOUNDARY
LEGEND
SUBSECTION A
SUBSECTION D
SUBSECTION C
SUBSECTION B
SUBSECTION E
D-1
D-2
D-3
D-4
E-5 E-4
E-2
E-1
E-3
A-5
A-4
A-3
A-1
B-3
B-1
B-4
B-2
B-5A-2
D-5 C-2
C-1
C-5
C-4
C-3
FIGURE 5SOIL GAS SAMPLE LOCATION MAP
511 and 527 West Tremont AvenueCharlotte, Mecklenburg County, North Carolina
ECS Project Number 49:8458-B
SOURCE:
GOOGLE EARTH, DATED 2017
SCALE:
AS SHOWN
SOIL GAS SAMPLE LOCATION
APPROXIMATE SITE BOUNDARY
LEGEND
SG-1
SG-8
SG-7
SG-6
SG-5
SG-4
SG-3
SG-2
FIGURE 6GROUNDWATER POTENTIOMETIC MAP AUGUST 19, 2019511 and 527 West Tremont AvenueCharlotte, Mecklenburg County, North Carolina
ECS Project Number 49:8458-B
SOURCE:
GOOGLE EARTH, DATED 2017
SCALE:
AS SHOWN
GROUNDWATER MONITORINGWELL LOCATION
APPROXIMATE SITE BOUNDARY
LEGEND
MW-1
MW-5
MW-3
MW-4
MW-2(697.76)(702.36)
(699.77)
(695.68)
(680.98)
(697.76)GROUNDWATER ELEVATION
GROUNDWATER POTENTIOMETRIC CONTOUR
INFERRED GROUNDWATER FLOW DIRECTION
TABLES
APPENDIX A
PHOTOGRAPHIC LOG
COREY TRANSMISSION
511 W TREMONT AVENUE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-8458-B
Photograph 1: General view of well development at MW-3.
Photograph 2: General view of drilling for MW-4 installation.
PHOTOGRAPHIC LOG
COREY TRANSMISSION
511 W TREMONT AVENUE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-8458-B
Photograph 3: General view of soil gas installation at SG-4.
Photograph 4: General view of soil gas sampling activities.
APPENDIX B

July 19, 2019

Mr. Todd Terwilliger, V.P. (via email)
The Ardent Companies
1200 Powers Ferry Road SE
Atlanta, GA 30339

RE: Monitoring Well Construction Permit
Permit #WM0301025
W. Tremont Avenue Facility
511 W. Tremont Av., Charlotte
Mecklenburg County

Dear Mr. Terwilliger,

In accordance with your completed application received on July 19, 2019, we are forwarding
herewith Monitoring Well Construction Permit Numbered WM0301025 and issued for the
construction of five monitoring wells located near the subject site in Charlotte, Mecklenburg County.

This Permit will be effective for one year from the date of issuance and shall be subject to the
conditions and limitations as specified therein.

Should you have any questions, please contact Edward Watson at [phone] ext. 2198,
or by email at [e-mail].

Sincerely,

Andrew H. Pitner, P.G., Assistant Regional Supervisor
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources

CC: WQROS, Central Office (via Laserfiche)
Chris Orrell, ECS Limited (via email)
Geologic Exploration (via email)

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES
PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL
In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws,
Rules and Regulations.
PERMISSION IS HEREBY GRANTED TO
The Ardent Companies (ECS Limited as Agent)

FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of five monitoring wells owned by The Ardent
Companies at the subject site, Charlotte, Mecklenburg County. This Permit is issued in accordance with the application
received on July 19, 2019, in conformity with specifications and supporting data, all of which are filed with the Department
of Environmental Quality and are considered integral parts of this Permit.
This Permit is for well construction only, and does not waive any provision or requirement of any other applicable law or
regulation. Construction of any well under this Permit shall be in strict compliance with the North Carolina Well Construction
Regulations and Standards (15A NCAC 02C .0100), and other State and Local Laws and regulations pertaining to well
construction.

If any requirements or limitations specified in this Permit are unacceptable, you have a right to an adjudicatory hearing upon
written request within 30 days of receipt of this Permit. The request must be in the form of a written petition conforming to
Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service
Center, Raleigh, North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding.
This Permit will be effective for one year from the date of its issuance and shall be subject to other specified conditions,
limitations, or exceptions as follows:

1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these wells are being installed as
part of an investigation for contamination from an underground storage tank or dry cleaner incident.
2. Issuance of this Permit does not supersede any other agreement, permit, or requirement issued by another agency.
3. The well(s) shall be located and constructed as shown on the attachments submitted as part of the Permit application.
4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC 02C .0108(o).
5. Well construction records (GW-1) for each well shall be submitted to the Division of Water Resources’ Information
Processing Unit within 30 days of the well completion.
6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A NCAC 02C .0113 and a
well abandonment record (GW-30) shall be submitted to the Division of Water Resources’ Information Processing
Unit within 30 days of the well abandonment.
7. Adequate permits shall be obtained from Mecklenburg County Groundwater and Wastewater Services.

Permit issued the 19th day of July, 2019
FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION

_______________________________________________
Andrew H. Pitner, P.G., Assistant Regional Supervisor
Division of Water Resources
By Authority of the Environmental Management Commission
Permit No. # WM0301025
SIP Form – revised 2/15/11
Mecklenburg County Health Department Groundwater & Wastewater Services 700 N. Tryon St., Suite 211 Charlotte, NC 28202
Phone: [phone] Fax: [phone] http://groundwater.charmeck.org
Permit Issuance Date: _______________
Permit Number: ____________________ 
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
II. Agent Information (if applicable)

Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
III. Site Information

Site Name; ________________________________
Parcel ID Number: _____________________
Address: ________________________________
City: __________________________ State: _______ Zip: _____________

General Conditions of This Permit:
• This permit shall be VALID for a period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified aboveDQGmust be on-site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VIof the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.

28208
3205 Freedom Dr.
[phone]
Owner
7/26/2019
70002649
The Ardent Companies
Tyson Reilly
803-548-4656
2100 Powers Ferry Road SE
Suite 350
Atlanta GA 30339
ECS Southeast, LLP
Scott Young
7043789016
1812 Center Park Drive
Suite D
Charlotte NC 28217
Corey Transmission
11906101
527 W TREMONT AVE
CHARLOTTE NC 28203
APPENDIX C
List all applicable well construction permits (i.e. County, State, Variance, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.

ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ
ÖÑ ØÒÒÇ ÞËÎÎ
ß óíðçè
GEOLOGIC EXPLORATION, INC
É Ó ðíðïðîë
ì
ðéñíðñïç Ó É óï
ÝÑ ÎÛÇÍ ÌÎßÒÍÓ ×ÍÍ×ÑÒ
ëîé É ÛÍÌ ÌÎÛÓ ÑÒÌ ßÊÛÒËÛ ÝØßÎÔÑÌÌÛ îèîðí
Ó ÛÝÕÔÛÒÞËÎÙ
íëpïîùíèòêðþ èðpëîùïðòéîþ
ì
ì
ï
íèòð
îéòð
êòð
ß×Î ÎÑÌßÎÇñÐÛÎÝËÍÍ×ÑÒ
ðòð îíòð 2.0 ÍÝØ ìð ÐÊÝ
îíòð íèòð 2.0 òðïð ÐÊÝ
ðòð ïîòð ÐÑÎÌÔßÒÜ ÞÛÒÌÑÒ×ÌÛ ÍÔËÎÎÇ
îïòð íèòð îðóìð Ú×ÒÛ Í×Ô×Ýß ÍßÒÜ
ðòð íòð ÑÎßÒÙÛ Í×ÔÌÇ ÝÔßÇ
íòð ïîòð ÌßÒ Ó ËÜÍÌÑÒÛ
ïîòð íèòð ÙÎßÇ ÎÑÝÕ
ÞÛÒÌÑÒ×ÌÛ ÍÛßÔ ÚÎÑÓ ïîòð ÌÑ îïòð ÚÛÛÌ
ðèñðèñïç
List all applicable well construction permits (i.e. County, State, Variance, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.

ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ
ÖÑ ØÒÒÇ ÞËÎÎ
ß óíðçè
GEOLOGIC EXPLORATION, INC
É Ó ðíðïðîë
ì
ðéñíðñïç Ó É óî
ÝÑ ÎÛÇÍ ÌÎßÒÍÓ ×ÍÍ×ÑÒ
ëîé É ÛÍÌ ÌÎÛÓ ÑÒÌ ßÊÛÒËÛ ÝØßÎÔÑÌÌÛ îèîðí
Ó ÛÝÕÔÛÒÞËÎÙ
íëpïîùíèòêðþ èðpëîùïðòéîþ
ì
ì
ï
íèòð
îìòð
êòð
ß×Î ÎÑÌßÎÇñÐÛÎÝËÍÍ×ÑÒ
ðòð ïèòð 2.0 ÍÝØ ìð ÐÊÝ
ïèòð íèòð 2.0 òðïð ÐÊÝ
ðòð ïîòð ÐÑÎÌÔßÒÜ ÞÛÒÌÑÒ×ÌÛ ÍÔËÎÎÇ
ïêòð íèòð îðóìð Ú×ÒÛ Í×Ô×Ýß ÍßÒÜ
ðòð íòð ÑÎßÒÙÛ Í×ÔÌÇ ÝÔßÇ
íòð ïîòð ÌßÒ Ó ËÜÍÌÑÒÛ
ïîòð íèòð ÙÎßÇ ÎÑÝÕ
ÞÛÒÌÑÒ×ÌÛ ÍÛßÔ ÚÎÑÓ ïîòð ÌÑ ïêòð ÚÛÛÌ
ðèñðèñïç
List all applicable well construction permits (i.e. County, State, Variance, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.

ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ
ÖÑ ØÒÒÇ ÞËÎÎ
ß óíðçè
GEOLOGIC EXPLORATION, INC
É Ó ðíðïðîë
ì
ðéñíðñïç Ó É óí
ÝÑ ÎÛÇÍ ÌÎßÒÍÓ ×ÍÍ×ÑÒ
ëîé É ÛÍÌ ÌÎÛÓ ÑÒÌ ßÊÛÒËÛ ÝØßÎÔÑÌÌÛ îèîðí
Ó ÛÝÕÔÛÒÞËÎÙ
íëpïîùíèòêðþ èðpëîùïðòéîþ
ì
ì
ï
íèòð
ïðòð
êòð
ß×Î ÎÑÌßÎÇñÐÛÎÝËÍÍ×ÑÒ
ðòð ïèòð 2.0 ÍÝØ ìð ÐÊÝ
ïèòð íèòð 2.0 òðïð ÐÊÝ
ðòð ïîòð ÐÑÎÌÔßÒÜ ÞÛÒÌÑÒ×ÌÛ ÍÔËÎÎÇ
ïêòð íèòð îðóìð Ú×ÒÛ Í×Ô×Ýß ÍßÒÜ
ðòð íòð ÑÎßÒÙÛ Í×ÔÌÇ ÝÔßÇ
íòð ïîòð ÌßÒ Ó ËÜÍÌÑÒÛ
ïîòð íèòð ÙÎßÇ ÎÑÝÕ
ÞÛÒÌÑÒ×ÌÛ ÍÛßÔ ÚÎÑÓ ïîòð ÌÑ ïêòð ÚÛÛÌ
ðèñðèñïç
List all applicable well construction permits (i.e. County, State, Variance, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.

ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ
ÖÑ ØÒÒÇ ÞËÎÎ
ß óíðçè
GEOLOGIC EXPLORATION, INC
É Ó ðíðïðîë
ì
ðéñíðñïç Ó É óì
ÝÑ ÎÛÇÍ ÌÎßÒÍÓ ×ÍÍ×ÑÒ
ëîé É ÛÍÌ ÌÎÛÓ ÑÒÌ ßÊÛÒËÛ ÝØßÎÔÑÌÌÛ îèîðí
Ó ÛÝÕÔÛÒÞËÎÙ
íëpïîùíèòêðþ èðpëîùïðòéîþ
ì
ì
ï
ïëòð
êòð
êòð
ß×Î ÎÑÌßÎÇñÐÛÎÝËÍÍ×ÑÒ
ðòð ëòð 2.0 ÍÝØ ìð ÐÊÝ
ëòð ïëòð 2.0 òðïð ÐÊÝ
ðòð íòð ÐÑÎÌÔßÒÜ ÞÛÒÌÑÒ×ÌÛ ÍÔËÎÎÇ
ìòð ïëòð îðóìð Ú×ÒÛ Í×Ô×Ýß ÍßÒÜ
ðòð ðòë ÝÑÒÝÎÛÌÛ
ðòë ïòð ÙÎßÊÛÔ
ïòð ëòð ÑÎßÒÙÛ Í×ÔÌÇ ÝÔßÇ
ëòð ïëòð ÞÔßÝÕ ÝÔßÇ
ÞÛÒÌÑÒ×ÌÛ ÍÛßÔ ÚÎÑÓ íòð ÌÑ ìòð ÚÛÛÌ
ðèñðèñïç
List all applicable well construction permits (i.e. County, State, Variance, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.

ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ
ÖÑ ØÒÒÇ ÞËÎÎ
ß óíðçè
GEOLOGIC EXPLORATION, INC
É Ó ðíðïðîë
ì
ðéñíðñïç Ó É óë
ÝÑ ÎÛÇÍ ÌÎßÒÍÓ ×ÍÍ×ÑÒ
ëîé É ÛÍÌ ÌÎÛÓ ÑÒÌ ßÊÛÒËÛ ÝØßÎÔÑÌÌÛ îèîðí
Ó ÛÝÕÔÛÒÞËÎÙ
íëpïîùíèòêðþ èðpëîùïðòéîþ
ì
ì
ï
îëòð
ïîòð
êòð
ß×Î ÎÑÌßÎÇñÐÛÎÝËÍÍ×ÑÒ
ðòð ïðòð 2.0 ÍÝØ ìð ÐÊÝ
ïðòð îëòð 2.0 òðïð ÐÊÝ
ðòð ìòð ÐÑÎÌÔßÒÜ ÞÛÒÌÑÒ×ÌÛ ÍÔËÎÎÇ
èòð îëòð îðóìð Ú×ÒÛ Í×Ô×Ýß ÍßÒÜ
ðòð ðòë ÝÑÒÝÎÛÌÛ
ðòë ïòð ÙÎßÊÛÔ
ïòð êòð ÑÎßÒÙÛ Í×ÔÌÇ ÝÔßÇ
êòð îëòð ÙÎßÇ ÎÑÝÕ
ÞÛÒÌÑÒ×ÌÛ ÍÛßÔ ÚÎÑÓ ìòð ÌÑ èòð ÚÛÛÌ
ðèñðèñïç
APPENDIX D
APPENDIX E
APPENDIX F
#=CL#
August 13, 2019
LIMS USE: FR - JOE NESTOR
LIMS OBJECT ID: 92440149
92440149
Project:
Pace Project No.:
RE:
Joe Nestor
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
COREY'S TRANSMISSION
Dear Joe Nestor:
Enclosed are the analytical results for sample(s) received by the laboratory on August 06, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 48
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 48
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Lab ID Sample ID Matrix Date Collected Date Received
92440149001 MW-1 (MS/MSD)Water 08/02/19 12:55 08/06/19 13:40
92440149002 MW-2 Water 08/05/19 12:20 08/06/19 13:40
92440149003 MW-3 Water 08/05/19 17:00 08/06/19 13:40
92440149004 MW-4 Water 08/06/19 10:20 08/06/19 13:40
92440149005 MW-5 Water 08/05/19 15:30 08/06/19 13:40
92440149006 DUPLICATE Water 08/02/19 00:00 08/06/19 13:40
92440149007 TRIP BLANK Water 08/02/19 00:00 08/06/19 13:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 48
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92440149001 MW-1 (MS/MSD)EPA 6010D 7 PASI-ADS
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92440149002 MW-2 EPA 6010D 7 PASI-ADS
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92440149003 MW-3 EPA 6010D 7 PASI-ADS
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92440149004 MW-4 EPA 6010D 7 PASI-ADS
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92440149005 MW-5 EPA 6010D 7 PASI-ADS
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92440149006 DUPLICATE EPA 6010D 7 PASI-ADS
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92440149007 TRIP BLANK EPA 8260D 63 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 48
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92440149001 MW-1 (MS/MSD)
Barium 83.5 ug/L 08/12/19 00:315.0EPA 6010D
92440149002 MW-2
Barium 182 ug/L 08/12/19 00:435.0EPA 6010D
Chromium 2.2J ug/L 08/12/19 00:435.0EPA 6010D
92440149003 MW-3
Barium 123 ug/L 08/12/19 00:475.0EPA 6010D
Chromium 5.0J ug/L 08/12/19 00:475.0EPA 6010D
Methyl-tert-butyl ether 3.1 ug/L 08/09/19 14:091.0EPA 8260D
92440149004 MW-4
Arsenic 170 ug/L 08/12/19 00:5010.0EPA 6010D
Barium 103 ug/L 08/12/19 00:505.0EPA 6010D
Cadmium 0.95J ug/L 08/12/19 00:501.0EPA 6010D
Lead 4.1J ug/L 08/12/19 00:505.0EPA 6010D
Methyl-tert-butyl ether 6.4 ug/L 08/09/19 14:261.0EPA 8260D
92440149005 MW-5
Barium 35.7 ug/L 08/12/19 00:535.0EPA 6010D
Chromium 1.9J ug/L 08/12/19 00:535.0EPA 6010D
Mercury 1.3 ug/L 08/09/19 15:020.20EPA 7470A
Methyl-tert-butyl ether 1.8 ug/L 08/09/19 14:441.0EPA 8260D
92440149006 DUPLICATE
Barium 85.3 ug/L 08/12/19 01:085.0EPA 6010D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-1 (MS/MSD)Lab ID: 92440149001 Collected: 08/02/19 12:55 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/12/19 00:31 7440-38-208/11/19 10:0110.0 4.7 1
Barium 83.5 ug/L 08/12/19 00:31 7440-39-308/11/19 10:015.0 1.0 1
Cadmium ND ug/L 08/12/19 00:31 7440-43-908/11/19 10:011.0 0.40 1
Chromium ND ug/L 08/12/19 00:31 7440-47-308/11/19 10:015.0 1.0 1
Lead ND ug/L 08/12/19 00:31 7439-92-108/11/19 10:015.0 1.6 1
Selenium ND ug/L 08/12/19 00:31 7782-49-208/11/19 10:0110.0 4.7 1
Silver ND ug/L 08/12/19 00:31 7440-22-408/11/19 10:015.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/09/19 14:43 7439-97-608/07/19 14:460.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/11/19 13:01 83-32-908/08/19 18:0410.0 1.6 1
Acenaphthylene ND ug/L 08/11/19 13:01 208-96-808/08/19 18:0410.0 1.6 1
Aniline ND ug/L 08/11/19 13:01 62-53-308/08/19 18:0410.0 1.9 1
Anthracene ND ug/L 08/11/19 13:01 120-12-708/08/19 18:0410.0 1.7 1
Benzo(a)anthracene ND ug/L 08/11/19 13:01 56-55-308/08/19 18:0410.0 1.8 1
Benzo(a)pyrene ND ug/L 08/11/19 13:01 50-32-808/08/19 18:0410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 08/11/19 13:01 205-99-208/08/19 18:0410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 08/11/19 13:01 191-24-208/08/19 18:0410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 08/11/19 13:01 207-08-908/08/19 18:0410.0 1.9 1
Benzoic Acid ND ug/L 08/11/19 13:01 65-85-0 M1,v108/08/19 18:0450.0 43.0 1
Benzyl alcohol ND ug/L 08/11/19 13:01 100-51-608/08/19 18:0420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 08/11/19 13:01 101-55-308/08/19 18:0410.0 1.6 1
Butylbenzylphthalate ND ug/L 08/11/19 13:01 85-68-708/08/19 18:0410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 08/11/19 13:01 59-50-708/08/19 18:0420.0 2.8 1
4-Chloroaniline ND ug/L 08/11/19 13:01 106-47-808/08/19 18:0420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 08/11/19 13:01 111-91-108/08/19 18:0410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 08/11/19 13:01 111-44-408/08/19 18:0410.0 1.8 1
2-Chloronaphthalene ND ug/L 08/11/19 13:01 91-58-708/08/19 18:0410.0 1.5 1
2-Chlorophenol ND ug/L 08/11/19 13:01 95-57-808/08/19 18:0410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 08/11/19 13:01 7005-72-308/08/19 18:0410.0 1.6 1
Chrysene ND ug/L 08/11/19 13:01 218-01-908/08/19 18:0410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 08/11/19 13:01 53-70-308/08/19 18:0410.0 1.6 1
Dibenzofuran ND ug/L 08/11/19 13:01 132-64-908/08/19 18:0410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 08/11/19 13:01 95-50-108/08/19 18:0410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 08/11/19 13:01 541-73-108/08/19 18:0410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 08/11/19 13:01 106-46-708/08/19 18:0410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 08/11/19 13:01 91-94-108/08/19 18:0420.0 3.0 1
2,4-Dichlorophenol ND ug/L 08/11/19 13:01 120-83-208/08/19 18:0410.0 1.4 1
Diethylphthalate ND ug/L 08/11/19 13:01 84-66-208/08/19 18:0410.0 2.4 1
2,4-Dimethylphenol ND ug/L 08/11/19 13:01 105-67-908/08/19 18:0410.0 1.4 1
Dimethylphthalate ND ug/L 08/11/19 13:01 131-11-308/08/19 18:0410.0 1.6 1
Di-n-butylphthalate ND ug/L 08/11/19 13:01 84-74-208/08/19 18:0410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 08/11/19 13:01 534-52-1 v108/08/19 18:0420.0 15.2 1
2,4-Dinitrophenol ND ug/L 08/11/19 13:01 51-28-5 R1,v108/08/19 18:0450.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-1 (MS/MSD)Lab ID: 92440149001 Collected: 08/02/19 12:55 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 08/11/19 13:01 121-14-208/08/19 18:0410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 08/11/19 13:01 606-20-208/08/19 18:0410.0 1.4 1
Di-n-octylphthalate ND ug/L 08/11/19 13:01 117-84-008/08/19 18:0410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/11/19 13:01 117-81-708/08/19 18:046.0 2.1 1
Fluoranthene ND ug/L 08/11/19 13:01 206-44-008/08/19 18:0410.0 1.7 1
Fluorene ND ug/L 08/11/19 13:01 86-73-708/08/19 18:0410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 08/11/19 13:01 87-68-308/08/19 18:0410.0 2.0 1
Hexachlorobenzene ND ug/L 08/11/19 13:01 118-74-108/08/19 18:0410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 08/11/19 13:01 77-47-408/08/19 18:0410.0 1.7 1
Hexachloroethane ND ug/L 08/11/19 13:01 67-72-108/08/19 18:0410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/11/19 13:01 193-39-508/08/19 18:0410.0 1.6 1
Isophorone ND ug/L 08/11/19 13:01 78-59-108/08/19 18:0410.0 1.6 1
1-Methylnaphthalene ND ug/L 08/11/19 13:01 90-12-008/08/19 18:0410.0 1.4 1
2-Methylnaphthalene ND ug/L 08/11/19 13:01 91-57-608/08/19 18:0410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 08/11/19 13:01 95-48-708/08/19 18:0410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/11/19 13:01 15831-10-408/08/19 18:0410.0 1.2 1
Naphthalene ND ug/L 08/11/19 13:01 91-20-308/08/19 18:0410.0 1.4 1
2-Nitroaniline ND ug/L 08/11/19 13:01 88-74-408/08/19 18:0420.0 4.2 1
3-Nitroaniline ND ug/L 08/11/19 13:01 99-09-208/08/19 18:0420.0 2.3 1
4-Nitroaniline ND ug/L 08/11/19 13:01 100-01-608/08/19 18:0420.0 2.2 1
Nitrobenzene ND ug/L 08/11/19 13:01 98-95-308/08/19 18:0410.0 2.1 1
2-Nitrophenol ND ug/L 08/11/19 13:01 88-75-508/08/19 18:0410.0 1.4 1
4-Nitrophenol ND ug/L 08/11/19 13:01 100-02-708/08/19 18:0450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 08/11/19 13:01 62-75-908/08/19 18:0410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 08/11/19 13:01 621-64-708/08/19 18:0410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 08/11/19 13:01 86-30-608/08/19 18:0410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/11/19 13:01 108-60-108/08/19 18:0410.0 2.8 1
Pentachlorophenol ND ug/L 08/11/19 13:01 87-86-5 R1,v108/08/19 18:0425.0 2.2 1
Phenanthrene ND ug/L 08/11/19 13:01 85-01-808/08/19 18:0410.0 1.7 1
Phenol ND ug/L 08/11/19 13:01 108-95-208/08/19 18:0410.0 0.92 1
Pyrene ND ug/L 08/11/19 13:01 129-00-008/08/19 18:0410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 08/11/19 13:01 120-82-108/08/19 18:0410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 08/11/19 13:01 95-95-408/08/19 18:0410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 08/11/19 13:01 88-06-208/08/19 18:0410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)87 %08/11/19 13:01 4165-60-008/08/19 18:0413-130 1
2-Fluorobiphenyl (S)88 %08/11/19 13:01 321-60-808/08/19 18:0413-130 1
Terphenyl-d14 (S)111 %08/11/19 13:01 1718-51-008/08/19 18:0425-130 1
Phenol-d6 (S)49 %08/11/19 13:01 13127-88-308/08/19 18:0410-130 1
2-Fluorophenol (S)68 %08/11/19 13:01 367-12-408/08/19 18:0410-130 1
2,4,6-Tribromophenol (S)110 %08/11/19 13:01 118-79-608/08/19 18:0410-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/09/19 13:51 67-64-125.0 6.2 1
Benzene ND ug/L 08/09/19 13:51 71-43-21.0 0.15 1
Bromobenzene ND ug/L 08/09/19 13:51 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-1 (MS/MSD)Lab ID: 92440149001 Collected: 08/02/19 12:55 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 08/09/19 13:51 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 08/09/19 13:51 75-27-41.0 0.26 1
Bromoform ND ug/L 08/09/19 13:51 75-25-21.0 0.62 1
Bromomethane ND ug/L 08/09/19 13:51 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 08/09/19 13:51 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 08/09/19 13:51 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 08/09/19 13:51 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/09/19 13:51 75-00-31.0 0.49 1
Chloroform ND ug/L 08/09/19 13:51 67-66-35.0 2.3 1
Chloromethane ND ug/L 08/09/19 13:51 74-87-3 M1,v11.0 0.39 1
2-Chlorotoluene ND ug/L 08/09/19 13:51 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 08/09/19 13:51 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/19 13:51 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 08/09/19 13:51 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/19 13:51 106-93-41.0 0.26 1
Dibromomethane ND ug/L 08/09/19 13:51 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 08/09/19 13:51 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 08/09/19 13:51 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 08/09/19 13:51 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 08/09/19 13:51 75-71-8 v11.0 0.23 1
1,1-Dichloroethane ND ug/L 08/09/19 13:51 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 08/09/19 13:51 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 08/09/19 13:51 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 08/09/19 13:51 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 08/09/19 13:51 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 08/09/19 13:51 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 08/09/19 13:51 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 08/09/19 13:51 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 08/09/19 13:51 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 08/09/19 13:51 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 08/09/19 13:51 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 08/09/19 13:51 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 08/09/19 13:51 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 08/09/19 13:51 87-68-31.0 0.44 1
2-Hexanone ND ug/L 08/09/19 13:51 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 08/09/19 13:51 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 08/09/19 13:51 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/19 13:51 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 08/09/19 13:51 1634-04-41.0 0.28 1
Naphthalene ND ug/L 08/09/19 13:51 91-20-31.0 0.35 1
Styrene ND ug/L 08/09/19 13:51 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/19 13:51 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/19 13:51 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/09/19 13:51 127-18-41.0 0.16 1
Toluene ND ug/L 08/09/19 13:51 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 08/09/19 13:51 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
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Page 8 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-1 (MS/MSD)Lab ID: 92440149001 Collected: 08/02/19 12:55 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 08/09/19 13:51 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 08/09/19 13:51 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 08/09/19 13:51 79-00-51.0 0.24 1
Trichloroethene ND ug/L 08/09/19 13:51 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 08/09/19 13:51 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 08/09/19 13:51 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 08/09/19 13:51 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 08/09/19 13:51 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 08/09/19 13:51 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 08/09/19 13:51 179601-23-12.0 0.41 1
o-Xylene ND ug/L 08/09/19 13:51 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)108 %08/09/19 13:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %08/09/19 13:51 17060-07-070-130 1
Toluene-d8 (S)101 %08/09/19 13:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
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Page 9 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-2 Lab ID: 92440149002 Collected: 08/05/19 12:20 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/12/19 00:43 7440-38-208/11/19 10:0110.0 4.7 1
Barium 182 ug/L 08/12/19 00:43 7440-39-308/11/19 10:015.0 1.0 1
Cadmium ND ug/L 08/12/19 00:43 7440-43-908/11/19 10:011.0 0.40 1
Chromium 2.2J ug/L 08/12/19 00:43 7440-47-308/11/19 10:015.0 1.0 1
Lead ND ug/L 08/12/19 00:43 7439-92-108/11/19 10:015.0 1.6 1
Selenium ND ug/L 08/12/19 00:43 7782-49-208/11/19 10:0110.0 4.7 1
Silver ND ug/L 08/12/19 00:43 7440-22-408/11/19 10:015.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/09/19 14:55 7439-97-608/07/19 14:460.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/11/19 14:16 83-32-908/08/19 18:0410.0 1.6 1
Acenaphthylene ND ug/L 08/11/19 14:16 208-96-808/08/19 18:0410.0 1.6 1
Aniline ND ug/L 08/11/19 14:16 62-53-308/08/19 18:0410.0 1.9 1
Anthracene ND ug/L 08/11/19 14:16 120-12-708/08/19 18:0410.0 1.7 1
Benzo(a)anthracene ND ug/L 08/11/19 14:16 56-55-308/08/19 18:0410.0 1.8 1
Benzo(a)pyrene ND ug/L 08/11/19 14:16 50-32-808/08/19 18:0410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 08/11/19 14:16 205-99-208/08/19 18:0410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 08/11/19 14:16 191-24-208/08/19 18:0410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 08/11/19 14:16 207-08-908/08/19 18:0410.0 1.9 1
Benzoic Acid ND ug/L 08/11/19 14:16 65-85-0 v108/08/19 18:0450.0 43.0 1
Benzyl alcohol ND ug/L 08/11/19 14:16 100-51-608/08/19 18:0420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 08/11/19 14:16 101-55-308/08/19 18:0410.0 1.6 1
Butylbenzylphthalate ND ug/L 08/11/19 14:16 85-68-708/08/19 18:0410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 08/11/19 14:16 59-50-708/08/19 18:0420.0 2.8 1
4-Chloroaniline ND ug/L 08/11/19 14:16 106-47-808/08/19 18:0420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 08/11/19 14:16 111-91-108/08/19 18:0410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 08/11/19 14:16 111-44-408/08/19 18:0410.0 1.8 1
2-Chloronaphthalene ND ug/L 08/11/19 14:16 91-58-708/08/19 18:0410.0 1.5 1
2-Chlorophenol ND ug/L 08/11/19 14:16 95-57-808/08/19 18:0410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 08/11/19 14:16 7005-72-308/08/19 18:0410.0 1.6 1
Chrysene ND ug/L 08/11/19 14:16 218-01-908/08/19 18:0410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 08/11/19 14:16 53-70-308/08/19 18:0410.0 1.6 1
Dibenzofuran ND ug/L 08/11/19 14:16 132-64-908/08/19 18:0410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 08/11/19 14:16 95-50-108/08/19 18:0410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 08/11/19 14:16 541-73-108/08/19 18:0410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 08/11/19 14:16 106-46-708/08/19 18:0410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 08/11/19 14:16 91-94-108/08/19 18:0420.0 3.0 1
2,4-Dichlorophenol ND ug/L 08/11/19 14:16 120-83-208/08/19 18:0410.0 1.4 1
Diethylphthalate ND ug/L 08/11/19 14:16 84-66-208/08/19 18:0410.0 2.4 1
2,4-Dimethylphenol ND ug/L 08/11/19 14:16 105-67-908/08/19 18:0410.0 1.4 1
Dimethylphthalate ND ug/L 08/11/19 14:16 131-11-308/08/19 18:0410.0 1.6 1
Di-n-butylphthalate ND ug/L 08/11/19 14:16 84-74-208/08/19 18:0410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 08/11/19 14:16 534-52-1 v108/08/19 18:0420.0 15.2 1
2,4-Dinitrophenol ND ug/L 08/11/19 14:16 51-28-5 v108/08/19 18:0450.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
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Page 10 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-2 Lab ID: 92440149002 Collected: 08/05/19 12:20 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 08/11/19 14:16 121-14-208/08/19 18:0410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 08/11/19 14:16 606-20-208/08/19 18:0410.0 1.4 1
Di-n-octylphthalate ND ug/L 08/11/19 14:16 117-84-008/08/19 18:0410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/11/19 14:16 117-81-708/08/19 18:046.0 2.1 1
Fluoranthene ND ug/L 08/11/19 14:16 206-44-008/08/19 18:0410.0 1.7 1
Fluorene ND ug/L 08/11/19 14:16 86-73-708/08/19 18:0410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 08/11/19 14:16 87-68-308/08/19 18:0410.0 2.0 1
Hexachlorobenzene ND ug/L 08/11/19 14:16 118-74-108/08/19 18:0410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 08/11/19 14:16 77-47-408/08/19 18:0410.0 1.7 1
Hexachloroethane ND ug/L 08/11/19 14:16 67-72-108/08/19 18:0410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/11/19 14:16 193-39-508/08/19 18:0410.0 1.6 1
Isophorone ND ug/L 08/11/19 14:16 78-59-108/08/19 18:0410.0 1.6 1
1-Methylnaphthalene ND ug/L 08/11/19 14:16 90-12-008/08/19 18:0410.0 1.4 1
2-Methylnaphthalene ND ug/L 08/11/19 14:16 91-57-608/08/19 18:0410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 08/11/19 14:16 95-48-708/08/19 18:0410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/11/19 14:16 15831-10-408/08/19 18:0410.0 1.2 1
Naphthalene ND ug/L 08/11/19 14:16 91-20-308/08/19 18:0410.0 1.4 1
2-Nitroaniline ND ug/L 08/11/19 14:16 88-74-408/08/19 18:0420.0 4.2 1
3-Nitroaniline ND ug/L 08/11/19 14:16 99-09-208/08/19 18:0420.0 2.3 1
4-Nitroaniline ND ug/L 08/11/19 14:16 100-01-608/08/19 18:0420.0 2.2 1
Nitrobenzene ND ug/L 08/11/19 14:16 98-95-308/08/19 18:0410.0 2.1 1
2-Nitrophenol ND ug/L 08/11/19 14:16 88-75-508/08/19 18:0410.0 1.4 1
4-Nitrophenol ND ug/L 08/11/19 14:16 100-02-708/08/19 18:0450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 08/11/19 14:16 62-75-908/08/19 18:0410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 08/11/19 14:16 621-64-708/08/19 18:0410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 08/11/19 14:16 86-30-608/08/19 18:0410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/11/19 14:16 108-60-108/08/19 18:0410.0 2.8 1
Pentachlorophenol ND ug/L 08/11/19 14:16 87-86-5 v108/08/19 18:0425.0 2.2 1
Phenanthrene ND ug/L 08/11/19 14:16 85-01-808/08/19 18:0410.0 1.7 1
Phenol ND ug/L 08/11/19 14:16 108-95-208/08/19 18:0410.0 0.92 1
Pyrene ND ug/L 08/11/19 14:16 129-00-008/08/19 18:0410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 08/11/19 14:16 120-82-108/08/19 18:0410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 08/11/19 14:16 95-95-408/08/19 18:0410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 08/11/19 14:16 88-06-208/08/19 18:0410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)60 %08/11/19 14:16 4165-60-008/08/19 18:0413-130 1
2-Fluorobiphenyl (S)61 %08/11/19 14:16 321-60-808/08/19 18:0413-130 1
Terphenyl-d14 (S)88 %08/11/19 14:16 1718-51-008/08/19 18:0425-130 1
Phenol-d6 (S)32 %08/11/19 14:16 13127-88-308/08/19 18:0410-130 1
2-Fluorophenol (S)42 %08/11/19 14:16 367-12-408/08/19 18:0410-130 1
2,4,6-Tribromophenol (S)93 %08/11/19 14:16 118-79-608/08/19 18:0410-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/09/19 15:18 67-64-125.0 6.2 1
Benzene ND ug/L 08/09/19 15:18 71-43-21.0 0.15 1
Bromobenzene ND ug/L 08/09/19 15:18 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-2 Lab ID: 92440149002 Collected: 08/05/19 12:20 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 08/09/19 15:18 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 08/09/19 15:18 75-27-41.0 0.26 1
Bromoform ND ug/L 08/09/19 15:18 75-25-21.0 0.62 1
Bromomethane ND ug/L 08/09/19 15:18 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 08/09/19 15:18 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 08/09/19 15:18 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 08/09/19 15:18 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/09/19 15:18 75-00-31.0 0.49 1
Chloroform ND ug/L 08/09/19 15:18 67-66-35.0 2.3 1
Chloromethane ND ug/L 08/09/19 15:18 74-87-3 v11.0 0.39 1
2-Chlorotoluene ND ug/L 08/09/19 15:18 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 08/09/19 15:18 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/19 15:18 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 08/09/19 15:18 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/19 15:18 106-93-41.0 0.26 1
Dibromomethane ND ug/L 08/09/19 15:18 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 08/09/19 15:18 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 08/09/19 15:18 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 08/09/19 15:18 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 08/09/19 15:18 75-71-8 v11.0 0.23 1
1,1-Dichloroethane ND ug/L 08/09/19 15:18 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 08/09/19 15:18 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 08/09/19 15:18 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 08/09/19 15:18 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 08/09/19 15:18 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 08/09/19 15:18 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 08/09/19 15:18 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 08/09/19 15:18 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 08/09/19 15:18 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 08/09/19 15:18 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 08/09/19 15:18 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 08/09/19 15:18 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 08/09/19 15:18 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 08/09/19 15:18 87-68-31.0 0.44 1
2-Hexanone ND ug/L 08/09/19 15:18 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 08/09/19 15:18 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 08/09/19 15:18 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/19 15:18 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 08/09/19 15:18 1634-04-41.0 0.28 1
Naphthalene ND ug/L 08/09/19 15:18 91-20-31.0 0.35 1
Styrene ND ug/L 08/09/19 15:18 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/19 15:18 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/19 15:18 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/09/19 15:18 127-18-41.0 0.16 1
Toluene ND ug/L 08/09/19 15:18 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 08/09/19 15:18 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 12 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-2 Lab ID: 92440149002 Collected: 08/05/19 12:20 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 08/09/19 15:18 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 08/09/19 15:18 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 08/09/19 15:18 79-00-51.0 0.24 1
Trichloroethene ND ug/L 08/09/19 15:18 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 08/09/19 15:18 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 08/09/19 15:18 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 08/09/19 15:18 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 08/09/19 15:18 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 08/09/19 15:18 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 08/09/19 15:18 179601-23-12.0 0.41 1
o-Xylene ND ug/L 08/09/19 15:18 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)108 %08/09/19 15:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %08/09/19 15:18 17060-07-070-130 1
Toluene-d8 (S)101 %08/09/19 15:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 13 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-3 Lab ID: 92440149003 Collected: 08/05/19 17:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/12/19 00:47 7440-38-208/11/19 10:0110.0 4.7 1
Barium 123 ug/L 08/12/19 00:47 7440-39-308/11/19 10:015.0 1.0 1
Cadmium ND ug/L 08/12/19 00:47 7440-43-908/11/19 10:011.0 0.40 1
Chromium 5.0J ug/L 08/12/19 00:47 7440-47-308/11/19 10:015.0 1.0 1
Lead ND ug/L 08/12/19 00:47 7439-92-108/11/19 10:015.0 1.6 1
Selenium ND ug/L 08/12/19 00:47 7782-49-208/11/19 10:0110.0 4.7 1
Silver ND ug/L 08/12/19 00:47 7440-22-408/11/19 10:015.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/09/19 14:57 7439-97-608/07/19 14:460.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/11/19 14:41 83-32-908/08/19 18:0410.0 1.6 1
Acenaphthylene ND ug/L 08/11/19 14:41 208-96-808/08/19 18:0410.0 1.6 1
Aniline ND ug/L 08/11/19 14:41 62-53-308/08/19 18:0410.0 1.9 1
Anthracene ND ug/L 08/11/19 14:41 120-12-708/08/19 18:0410.0 1.7 1
Benzo(a)anthracene ND ug/L 08/11/19 14:41 56-55-308/08/19 18:0410.0 1.8 1
Benzo(a)pyrene ND ug/L 08/11/19 14:41 50-32-808/08/19 18:0410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 08/11/19 14:41 205-99-208/08/19 18:0410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 08/11/19 14:41 191-24-208/08/19 18:0410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 08/11/19 14:41 207-08-908/08/19 18:0410.0 1.9 1
Benzoic Acid ND ug/L 08/11/19 14:41 65-85-0 v108/08/19 18:0450.0 43.0 1
Benzyl alcohol ND ug/L 08/11/19 14:41 100-51-608/08/19 18:0420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 08/11/19 14:41 101-55-308/08/19 18:0410.0 1.6 1
Butylbenzylphthalate ND ug/L 08/11/19 14:41 85-68-708/08/19 18:0410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 08/11/19 14:41 59-50-708/08/19 18:0420.0 2.8 1
4-Chloroaniline ND ug/L 08/11/19 14:41 106-47-808/08/19 18:0420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 08/11/19 14:41 111-91-108/08/19 18:0410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 08/11/19 14:41 111-44-408/08/19 18:0410.0 1.8 1
2-Chloronaphthalene ND ug/L 08/11/19 14:41 91-58-708/08/19 18:0410.0 1.5 1
2-Chlorophenol ND ug/L 08/11/19 14:41 95-57-808/08/19 18:0410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 08/11/19 14:41 7005-72-308/08/19 18:0410.0 1.6 1
Chrysene ND ug/L 08/11/19 14:41 218-01-908/08/19 18:0410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 08/11/19 14:41 53-70-308/08/19 18:0410.0 1.6 1
Dibenzofuran ND ug/L 08/11/19 14:41 132-64-908/08/19 18:0410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 08/11/19 14:41 95-50-108/08/19 18:0410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 08/11/19 14:41 541-73-108/08/19 18:0410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 08/11/19 14:41 106-46-708/08/19 18:0410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 08/11/19 14:41 91-94-108/08/19 18:0420.0 3.0 1
2,4-Dichlorophenol ND ug/L 08/11/19 14:41 120-83-208/08/19 18:0410.0 1.4 1
Diethylphthalate ND ug/L 08/11/19 14:41 84-66-208/08/19 18:0410.0 2.4 1
2,4-Dimethylphenol ND ug/L 08/11/19 14:41 105-67-908/08/19 18:0410.0 1.4 1
Dimethylphthalate ND ug/L 08/11/19 14:41 131-11-308/08/19 18:0410.0 1.6 1
Di-n-butylphthalate ND ug/L 08/11/19 14:41 84-74-208/08/19 18:0410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 08/11/19 14:41 534-52-1 v108/08/19 18:0420.0 15.2 1
2,4-Dinitrophenol ND ug/L 08/11/19 14:41 51-28-5 v108/08/19 18:0450.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
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Page 14 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-3 Lab ID: 92440149003 Collected: 08/05/19 17:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 08/11/19 14:41 121-14-208/08/19 18:0410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 08/11/19 14:41 606-20-208/08/19 18:0410.0 1.4 1
Di-n-octylphthalate ND ug/L 08/11/19 14:41 117-84-008/08/19 18:0410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/11/19 14:41 117-81-708/08/19 18:046.0 2.1 1
Fluoranthene ND ug/L 08/11/19 14:41 206-44-008/08/19 18:0410.0 1.7 1
Fluorene ND ug/L 08/11/19 14:41 86-73-708/08/19 18:0410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 08/11/19 14:41 87-68-308/08/19 18:0410.0 2.0 1
Hexachlorobenzene ND ug/L 08/11/19 14:41 118-74-108/08/19 18:0410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 08/11/19 14:41 77-47-408/08/19 18:0410.0 1.7 1
Hexachloroethane ND ug/L 08/11/19 14:41 67-72-108/08/19 18:0410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/11/19 14:41 193-39-508/08/19 18:0410.0 1.6 1
Isophorone ND ug/L 08/11/19 14:41 78-59-108/08/19 18:0410.0 1.6 1
1-Methylnaphthalene ND ug/L 08/11/19 14:41 90-12-008/08/19 18:0410.0 1.4 1
2-Methylnaphthalene ND ug/L 08/11/19 14:41 91-57-608/08/19 18:0410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 08/11/19 14:41 95-48-708/08/19 18:0410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/11/19 14:41 15831-10-408/08/19 18:0410.0 1.2 1
Naphthalene ND ug/L 08/11/19 14:41 91-20-308/08/19 18:0410.0 1.4 1
2-Nitroaniline ND ug/L 08/11/19 14:41 88-74-408/08/19 18:0420.0 4.2 1
3-Nitroaniline ND ug/L 08/11/19 14:41 99-09-208/08/19 18:0420.0 2.3 1
4-Nitroaniline ND ug/L 08/11/19 14:41 100-01-608/08/19 18:0420.0 2.2 1
Nitrobenzene ND ug/L 08/11/19 14:41 98-95-308/08/19 18:0410.0 2.1 1
2-Nitrophenol ND ug/L 08/11/19 14:41 88-75-508/08/19 18:0410.0 1.4 1
4-Nitrophenol ND ug/L 08/11/19 14:41 100-02-708/08/19 18:0450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 08/11/19 14:41 62-75-908/08/19 18:0410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 08/11/19 14:41 621-64-708/08/19 18:0410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 08/11/19 14:41 86-30-608/08/19 18:0410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/11/19 14:41 108-60-108/08/19 18:0410.0 2.8 1
Pentachlorophenol ND ug/L 08/11/19 14:41 87-86-5 v108/08/19 18:0425.0 2.2 1
Phenanthrene ND ug/L 08/11/19 14:41 85-01-808/08/19 18:0410.0 1.7 1
Phenol ND ug/L 08/11/19 14:41 108-95-208/08/19 18:0410.0 0.92 1
Pyrene ND ug/L 08/11/19 14:41 129-00-008/08/19 18:0410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 08/11/19 14:41 120-82-108/08/19 18:0410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 08/11/19 14:41 95-95-408/08/19 18:0410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 08/11/19 14:41 88-06-208/08/19 18:0410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)75 %08/11/19 14:41 4165-60-008/08/19 18:0413-130 1
2-Fluorobiphenyl (S)73 %08/11/19 14:41 321-60-808/08/19 18:0413-130 1
Terphenyl-d14 (S)86 %08/11/19 14:41 1718-51-008/08/19 18:0425-130 1
Phenol-d6 (S)42 %08/11/19 14:41 13127-88-308/08/19 18:0410-130 1
2-Fluorophenol (S)58 %08/11/19 14:41 367-12-408/08/19 18:0410-130 1
2,4,6-Tribromophenol (S)91 %08/11/19 14:41 118-79-608/08/19 18:0410-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/09/19 14:09 67-64-125.0 6.2 1
Benzene ND ug/L 08/09/19 14:09 71-43-21.0 0.15 1
Bromobenzene ND ug/L 08/09/19 14:09 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
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Huntersville, NC 28078
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Page 15 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-3 Lab ID: 92440149003 Collected: 08/05/19 17:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 08/09/19 14:09 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 08/09/19 14:09 75-27-41.0 0.26 1
Bromoform ND ug/L 08/09/19 14:09 75-25-21.0 0.62 1
Bromomethane ND ug/L 08/09/19 14:09 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 08/09/19 14:09 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 08/09/19 14:09 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 08/09/19 14:09 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/09/19 14:09 75-00-31.0 0.49 1
Chloroform ND ug/L 08/09/19 14:09 67-66-35.0 2.3 1
Chloromethane ND ug/L 08/09/19 14:09 74-87-3 v11.0 0.39 1
2-Chlorotoluene ND ug/L 08/09/19 14:09 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 08/09/19 14:09 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/19 14:09 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 08/09/19 14:09 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/19 14:09 106-93-41.0 0.26 1
Dibromomethane ND ug/L 08/09/19 14:09 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 08/09/19 14:09 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 08/09/19 14:09 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 08/09/19 14:09 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 08/09/19 14:09 75-71-8 v11.0 0.23 1
1,1-Dichloroethane ND ug/L 08/09/19 14:09 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 08/09/19 14:09 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 08/09/19 14:09 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 08/09/19 14:09 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 08/09/19 14:09 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 08/09/19 14:09 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 08/09/19 14:09 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 08/09/19 14:09 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 08/09/19 14:09 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 08/09/19 14:09 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 08/09/19 14:09 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 08/09/19 14:09 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 08/09/19 14:09 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 08/09/19 14:09 87-68-31.0 0.44 1
2-Hexanone ND ug/L 08/09/19 14:09 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 08/09/19 14:09 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 08/09/19 14:09 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/19 14:09 108-10-15.0 4.5 1
Methyl-tert-butyl ether 3.1 ug/L 08/09/19 14:09 1634-04-41.0 0.28 1
Naphthalene ND ug/L 08/09/19 14:09 91-20-31.0 0.35 1
Styrene ND ug/L 08/09/19 14:09 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/19 14:09 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/19 14:09 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/09/19 14:09 127-18-41.0 0.16 1
Toluene ND ug/L 08/09/19 14:09 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 08/09/19 14:09 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-3 Lab ID: 92440149003 Collected: 08/05/19 17:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 08/09/19 14:09 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 08/09/19 14:09 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 08/09/19 14:09 79-00-51.0 0.24 1
Trichloroethene ND ug/L 08/09/19 14:09 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 08/09/19 14:09 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 08/09/19 14:09 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 08/09/19 14:09 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 08/09/19 14:09 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 08/09/19 14:09 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 08/09/19 14:09 179601-23-12.0 0.41 1
o-Xylene ND ug/L 08/09/19 14:09 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)108 %08/09/19 14:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %08/09/19 14:09 17060-07-070-130 1
Toluene-d8 (S)101 %08/09/19 14:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-4 Lab ID: 92440149004 Collected: 08/06/19 10:20 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic 170 ug/L 08/12/19 00:50 7440-38-208/11/19 10:0110.0 4.7 1
Barium 103 ug/L 08/12/19 00:50 7440-39-308/11/19 10:015.0 1.0 1
Cadmium 0.95J ug/L 08/12/19 00:50 7440-43-908/11/19 10:011.0 0.40 1
Chromium ND ug/L 08/12/19 00:50 7440-47-308/11/19 10:015.0 1.0 1
Lead 4.1J ug/L 08/12/19 00:50 7439-92-108/11/19 10:015.0 1.6 1
Selenium ND ug/L 08/12/19 00:50 7782-49-208/11/19 10:0110.0 4.7 1
Silver ND ug/L 08/12/19 00:50 7440-22-408/11/19 10:015.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/09/19 15:00 7439-97-608/07/19 14:460.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/11/19 15:07 83-32-908/08/19 18:0410.0 1.6 1
Acenaphthylene ND ug/L 08/11/19 15:07 208-96-808/08/19 18:0410.0 1.6 1
Aniline ND ug/L 08/11/19 15:07 62-53-308/08/19 18:0410.0 1.9 1
Anthracene ND ug/L 08/11/19 15:07 120-12-708/08/19 18:0410.0 1.7 1
Benzo(a)anthracene ND ug/L 08/11/19 15:07 56-55-308/08/19 18:0410.0 1.8 1
Benzo(a)pyrene ND ug/L 08/11/19 15:07 50-32-808/08/19 18:0410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 08/11/19 15:07 205-99-208/08/19 18:0410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 08/11/19 15:07 191-24-208/08/19 18:0410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 08/11/19 15:07 207-08-908/08/19 18:0410.0 1.9 1
Benzoic Acid ND ug/L 08/11/19 15:07 65-85-0 v108/08/19 18:0450.0 43.0 1
Benzyl alcohol ND ug/L 08/11/19 15:07 100-51-608/08/19 18:0420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 08/11/19 15:07 101-55-308/08/19 18:0410.0 1.6 1
Butylbenzylphthalate ND ug/L 08/11/19 15:07 85-68-708/08/19 18:0410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 08/11/19 15:07 59-50-708/08/19 18:0420.0 2.8 1
4-Chloroaniline ND ug/L 08/11/19 15:07 106-47-808/08/19 18:0420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 08/11/19 15:07 111-91-108/08/19 18:0410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 08/11/19 15:07 111-44-408/08/19 18:0410.0 1.8 1
2-Chloronaphthalene ND ug/L 08/11/19 15:07 91-58-708/08/19 18:0410.0 1.5 1
2-Chlorophenol ND ug/L 08/11/19 15:07 95-57-808/08/19 18:0410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 08/11/19 15:07 7005-72-308/08/19 18:0410.0 1.6 1
Chrysene ND ug/L 08/11/19 15:07 218-01-908/08/19 18:0410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 08/11/19 15:07 53-70-308/08/19 18:0410.0 1.6 1
Dibenzofuran ND ug/L 08/11/19 15:07 132-64-908/08/19 18:0410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 08/11/19 15:07 95-50-108/08/19 18:0410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 08/11/19 15:07 541-73-108/08/19 18:0410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 08/11/19 15:07 106-46-708/08/19 18:0410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 08/11/19 15:07 91-94-108/08/19 18:0420.0 3.0 1
2,4-Dichlorophenol ND ug/L 08/11/19 15:07 120-83-208/08/19 18:0410.0 1.4 1
Diethylphthalate ND ug/L 08/11/19 15:07 84-66-208/08/19 18:0410.0 2.4 1
2,4-Dimethylphenol ND ug/L 08/11/19 15:07 105-67-908/08/19 18:0410.0 1.4 1
Dimethylphthalate ND ug/L 08/11/19 15:07 131-11-308/08/19 18:0410.0 1.6 1
Di-n-butylphthalate ND ug/L 08/11/19 15:07 84-74-208/08/19 18:0410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 08/11/19 15:07 534-52-1 v108/08/19 18:0420.0 15.2 1
2,4-Dinitrophenol ND ug/L 08/11/19 15:07 51-28-5 v108/08/19 18:0450.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-4 Lab ID: 92440149004 Collected: 08/06/19 10:20 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 08/11/19 15:07 121-14-208/08/19 18:0410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 08/11/19 15:07 606-20-208/08/19 18:0410.0 1.4 1
Di-n-octylphthalate ND ug/L 08/11/19 15:07 117-84-008/08/19 18:0410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/11/19 15:07 117-81-708/08/19 18:046.0 2.1 1
Fluoranthene ND ug/L 08/11/19 15:07 206-44-008/08/19 18:0410.0 1.7 1
Fluorene ND ug/L 08/11/19 15:07 86-73-708/08/19 18:0410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 08/11/19 15:07 87-68-308/08/19 18:0410.0 2.0 1
Hexachlorobenzene ND ug/L 08/11/19 15:07 118-74-108/08/19 18:0410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 08/11/19 15:07 77-47-408/08/19 18:0410.0 1.7 1
Hexachloroethane ND ug/L 08/11/19 15:07 67-72-108/08/19 18:0410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/11/19 15:07 193-39-508/08/19 18:0410.0 1.6 1
Isophorone ND ug/L 08/11/19 15:07 78-59-108/08/19 18:0410.0 1.6 1
1-Methylnaphthalene ND ug/L 08/11/19 15:07 90-12-008/08/19 18:0410.0 1.4 1
2-Methylnaphthalene ND ug/L 08/11/19 15:07 91-57-608/08/19 18:0410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 08/11/19 15:07 95-48-708/08/19 18:0410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/11/19 15:07 15831-10-408/08/19 18:0410.0 1.2 1
Naphthalene ND ug/L 08/11/19 15:07 91-20-308/08/19 18:0410.0 1.4 1
2-Nitroaniline ND ug/L 08/11/19 15:07 88-74-408/08/19 18:0420.0 4.2 1
3-Nitroaniline ND ug/L 08/11/19 15:07 99-09-208/08/19 18:0420.0 2.3 1
4-Nitroaniline ND ug/L 08/11/19 15:07 100-01-608/08/19 18:0420.0 2.2 1
Nitrobenzene ND ug/L 08/11/19 15:07 98-95-308/08/19 18:0410.0 2.1 1
2-Nitrophenol ND ug/L 08/11/19 15:07 88-75-508/08/19 18:0410.0 1.4 1
4-Nitrophenol ND ug/L 08/11/19 15:07 100-02-708/08/19 18:0450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 08/11/19 15:07 62-75-908/08/19 18:0410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 08/11/19 15:07 621-64-708/08/19 18:0410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 08/11/19 15:07 86-30-608/08/19 18:0410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/11/19 15:07 108-60-108/08/19 18:0410.0 2.8 1
Pentachlorophenol ND ug/L 08/11/19 15:07 87-86-5 v108/08/19 18:0425.0 2.2 1
Phenanthrene ND ug/L 08/11/19 15:07 85-01-808/08/19 18:0410.0 1.7 1
Phenol ND ug/L 08/11/19 15:07 108-95-208/08/19 18:0410.0 0.92 1
Pyrene ND ug/L 08/11/19 15:07 129-00-008/08/19 18:0410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 08/11/19 15:07 120-82-108/08/19 18:0410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 08/11/19 15:07 95-95-408/08/19 18:0410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 08/11/19 15:07 88-06-208/08/19 18:0410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)67 %08/11/19 15:07 4165-60-008/08/19 18:0413-130 1
2-Fluorobiphenyl (S)68 %08/11/19 15:07 321-60-808/08/19 18:0413-130 1
Terphenyl-d14 (S)82 %08/11/19 15:07 1718-51-008/08/19 18:0425-130 1
Phenol-d6 (S)37 %08/11/19 15:07 13127-88-308/08/19 18:0410-130 1
2-Fluorophenol (S)53 %08/11/19 15:07 367-12-408/08/19 18:0410-130 1
2,4,6-Tribromophenol (S)81 %08/11/19 15:07 118-79-608/08/19 18:0410-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/09/19 14:26 67-64-125.0 6.2 1
Benzene ND ug/L 08/09/19 14:26 71-43-21.0 0.15 1
Bromobenzene ND ug/L 08/09/19 14:26 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
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Page 19 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-4 Lab ID: 92440149004 Collected: 08/06/19 10:20 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 08/09/19 14:26 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 08/09/19 14:26 75-27-41.0 0.26 1
Bromoform ND ug/L 08/09/19 14:26 75-25-21.0 0.62 1
Bromomethane ND ug/L 08/09/19 14:26 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 08/09/19 14:26 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 08/09/19 14:26 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 08/09/19 14:26 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/09/19 14:26 75-00-31.0 0.49 1
Chloroform ND ug/L 08/09/19 14:26 67-66-35.0 2.3 1
Chloromethane ND ug/L 08/09/19 14:26 74-87-3 v11.0 0.39 1
2-Chlorotoluene ND ug/L 08/09/19 14:26 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 08/09/19 14:26 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/19 14:26 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 08/09/19 14:26 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/19 14:26 106-93-41.0 0.26 1
Dibromomethane ND ug/L 08/09/19 14:26 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 08/09/19 14:26 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 08/09/19 14:26 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 08/09/19 14:26 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 08/09/19 14:26 75-71-8 v11.0 0.23 1
1,1-Dichloroethane ND ug/L 08/09/19 14:26 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 08/09/19 14:26 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 08/09/19 14:26 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 08/09/19 14:26 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 08/09/19 14:26 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 08/09/19 14:26 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 08/09/19 14:26 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 08/09/19 14:26 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 08/09/19 14:26 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 08/09/19 14:26 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 08/09/19 14:26 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 08/09/19 14:26 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 08/09/19 14:26 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 08/09/19 14:26 87-68-31.0 0.44 1
2-Hexanone ND ug/L 08/09/19 14:26 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 08/09/19 14:26 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 08/09/19 14:26 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/19 14:26 108-10-15.0 4.5 1
Methyl-tert-butyl ether 6.4 ug/L 08/09/19 14:26 1634-04-41.0 0.28 1
Naphthalene ND ug/L 08/09/19 14:26 91-20-31.0 0.35 1
Styrene ND ug/L 08/09/19 14:26 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/19 14:26 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/19 14:26 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/09/19 14:26 127-18-41.0 0.16 1
Toluene ND ug/L 08/09/19 14:26 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 08/09/19 14:26 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 20 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-4 Lab ID: 92440149004 Collected: 08/06/19 10:20 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 08/09/19 14:26 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 08/09/19 14:26 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 08/09/19 14:26 79-00-51.0 0.24 1
Trichloroethene ND ug/L 08/09/19 14:26 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 08/09/19 14:26 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 08/09/19 14:26 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 08/09/19 14:26 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 08/09/19 14:26 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 08/09/19 14:26 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 08/09/19 14:26 179601-23-12.0 0.41 1
o-Xylene ND ug/L 08/09/19 14:26 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)109 %08/09/19 14:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %08/09/19 14:26 17060-07-070-130 1
Toluene-d8 (S)102 %08/09/19 14:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 21 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-5 Lab ID: 92440149005 Collected: 08/05/19 15:30 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/12/19 00:53 7440-38-208/11/19 10:0110.0 4.7 1
Barium 35.7 ug/L 08/12/19 00:53 7440-39-308/11/19 10:015.0 1.0 1
Cadmium ND ug/L 08/12/19 00:53 7440-43-908/11/19 10:011.0 0.40 1
Chromium 1.9J ug/L 08/12/19 00:53 7440-47-308/11/19 10:015.0 1.0 1
Lead ND ug/L 08/12/19 00:53 7439-92-108/11/19 10:015.0 1.6 1
Selenium ND ug/L 08/12/19 00:53 7782-49-208/11/19 10:0110.0 4.7 1
Silver ND ug/L 08/12/19 00:53 7440-22-408/11/19 10:015.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury 1.3 ug/L 08/09/19 15:02 7439-97-608/07/19 14:460.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/11/19 15:32 83-32-908/08/19 18:0410.0 1.6 1
Acenaphthylene ND ug/L 08/11/19 15:32 208-96-808/08/19 18:0410.0 1.6 1
Aniline ND ug/L 08/11/19 15:32 62-53-308/08/19 18:0410.0 1.9 1
Anthracene ND ug/L 08/11/19 15:32 120-12-708/08/19 18:0410.0 1.7 1
Benzo(a)anthracene ND ug/L 08/11/19 15:32 56-55-308/08/19 18:0410.0 1.8 1
Benzo(a)pyrene ND ug/L 08/11/19 15:32 50-32-808/08/19 18:0410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 08/11/19 15:32 205-99-208/08/19 18:0410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 08/11/19 15:32 191-24-208/08/19 18:0410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 08/11/19 15:32 207-08-908/08/19 18:0410.0 1.9 1
Benzoic Acid ND ug/L 08/11/19 15:32 65-85-0 v108/08/19 18:0450.0 43.0 1
Benzyl alcohol ND ug/L 08/11/19 15:32 100-51-608/08/19 18:0420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 08/11/19 15:32 101-55-308/08/19 18:0410.0 1.6 1
Butylbenzylphthalate ND ug/L 08/11/19 15:32 85-68-708/08/19 18:0410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 08/11/19 15:32 59-50-708/08/19 18:0420.0 2.8 1
4-Chloroaniline ND ug/L 08/11/19 15:32 106-47-808/08/19 18:0420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 08/11/19 15:32 111-91-108/08/19 18:0410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 08/11/19 15:32 111-44-408/08/19 18:0410.0 1.8 1
2-Chloronaphthalene ND ug/L 08/11/19 15:32 91-58-708/08/19 18:0410.0 1.5 1
2-Chlorophenol ND ug/L 08/11/19 15:32 95-57-808/08/19 18:0410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 08/11/19 15:32 7005-72-308/08/19 18:0410.0 1.6 1
Chrysene ND ug/L 08/11/19 15:32 218-01-908/08/19 18:0410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 08/11/19 15:32 53-70-308/08/19 18:0410.0 1.6 1
Dibenzofuran ND ug/L 08/11/19 15:32 132-64-908/08/19 18:0410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 08/11/19 15:32 95-50-108/08/19 18:0410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 08/11/19 15:32 541-73-108/08/19 18:0410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 08/11/19 15:32 106-46-708/08/19 18:0410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 08/11/19 15:32 91-94-108/08/19 18:0420.0 3.0 1
2,4-Dichlorophenol ND ug/L 08/11/19 15:32 120-83-208/08/19 18:0410.0 1.4 1
Diethylphthalate ND ug/L 08/11/19 15:32 84-66-208/08/19 18:0410.0 2.4 1
2,4-Dimethylphenol ND ug/L 08/11/19 15:32 105-67-908/08/19 18:0410.0 1.4 1
Dimethylphthalate ND ug/L 08/11/19 15:32 131-11-308/08/19 18:0410.0 1.6 1
Di-n-butylphthalate ND ug/L 08/11/19 15:32 84-74-208/08/19 18:0410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 08/11/19 15:32 534-52-1 v108/08/19 18:0420.0 15.2 1
2,4-Dinitrophenol ND ug/L 08/11/19 15:32 51-28-5 v108/08/19 18:0450.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-5 Lab ID: 92440149005 Collected: 08/05/19 15:30 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 08/11/19 15:32 121-14-208/08/19 18:0410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 08/11/19 15:32 606-20-208/08/19 18:0410.0 1.4 1
Di-n-octylphthalate ND ug/L 08/11/19 15:32 117-84-008/08/19 18:0410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/11/19 15:32 117-81-708/08/19 18:046.0 2.1 1
Fluoranthene ND ug/L 08/11/19 15:32 206-44-008/08/19 18:0410.0 1.7 1
Fluorene ND ug/L 08/11/19 15:32 86-73-708/08/19 18:0410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 08/11/19 15:32 87-68-308/08/19 18:0410.0 2.0 1
Hexachlorobenzene ND ug/L 08/11/19 15:32 118-74-108/08/19 18:0410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 08/11/19 15:32 77-47-408/08/19 18:0410.0 1.7 1
Hexachloroethane ND ug/L 08/11/19 15:32 67-72-108/08/19 18:0410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/11/19 15:32 193-39-508/08/19 18:0410.0 1.6 1
Isophorone ND ug/L 08/11/19 15:32 78-59-108/08/19 18:0410.0 1.6 1
1-Methylnaphthalene ND ug/L 08/11/19 15:32 90-12-008/08/19 18:0410.0 1.4 1
2-Methylnaphthalene ND ug/L 08/11/19 15:32 91-57-608/08/19 18:0410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 08/11/19 15:32 95-48-708/08/19 18:0410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/11/19 15:32 15831-10-408/08/19 18:0410.0 1.2 1
Naphthalene ND ug/L 08/11/19 15:32 91-20-308/08/19 18:0410.0 1.4 1
2-Nitroaniline ND ug/L 08/11/19 15:32 88-74-408/08/19 18:0420.0 4.2 1
3-Nitroaniline ND ug/L 08/11/19 15:32 99-09-208/08/19 18:0420.0 2.3 1
4-Nitroaniline ND ug/L 08/11/19 15:32 100-01-608/08/19 18:0420.0 2.2 1
Nitrobenzene ND ug/L 08/11/19 15:32 98-95-308/08/19 18:0410.0 2.1 1
2-Nitrophenol ND ug/L 08/11/19 15:32 88-75-508/08/19 18:0410.0 1.4 1
4-Nitrophenol ND ug/L 08/11/19 15:32 100-02-708/08/19 18:0450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 08/11/19 15:32 62-75-908/08/19 18:0410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 08/11/19 15:32 621-64-708/08/19 18:0410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 08/11/19 15:32 86-30-608/08/19 18:0410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/11/19 15:32 108-60-108/08/19 18:0410.0 2.8 1
Pentachlorophenol ND ug/L 08/11/19 15:32 87-86-5 v108/08/19 18:0425.0 2.2 1
Phenanthrene ND ug/L 08/11/19 15:32 85-01-808/08/19 18:0410.0 1.7 1
Phenol ND ug/L 08/11/19 15:32 108-95-208/08/19 18:0410.0 0.92 1
Pyrene ND ug/L 08/11/19 15:32 129-00-008/08/19 18:0410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 08/11/19 15:32 120-82-108/08/19 18:0410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 08/11/19 15:32 95-95-408/08/19 18:0410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 08/11/19 15:32 88-06-208/08/19 18:0410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)67 %08/11/19 15:32 4165-60-008/08/19 18:0413-130 1
2-Fluorobiphenyl (S)66 %08/11/19 15:32 321-60-808/08/19 18:0413-130 1
Terphenyl-d14 (S)88 %08/11/19 15:32 1718-51-008/08/19 18:0425-130 1
Phenol-d6 (S)34 %08/11/19 15:32 13127-88-308/08/19 18:0410-130 1
2-Fluorophenol (S)48 %08/11/19 15:32 367-12-408/08/19 18:0410-130 1
2,4,6-Tribromophenol (S)78 %08/11/19 15:32 118-79-608/08/19 18:0410-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/09/19 14:44 67-64-125.0 6.2 1
Benzene ND ug/L 08/09/19 14:44 71-43-21.0 0.15 1
Bromobenzene ND ug/L 08/09/19 14:44 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-5 Lab ID: 92440149005 Collected: 08/05/19 15:30 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 08/09/19 14:44 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 08/09/19 14:44 75-27-41.0 0.26 1
Bromoform ND ug/L 08/09/19 14:44 75-25-21.0 0.62 1
Bromomethane ND ug/L 08/09/19 14:44 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 08/09/19 14:44 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 08/09/19 14:44 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 08/09/19 14:44 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/09/19 14:44 75-00-31.0 0.49 1
Chloroform ND ug/L 08/09/19 14:44 67-66-35.0 2.3 1
Chloromethane ND ug/L 08/09/19 14:44 74-87-3 v11.0 0.39 1
2-Chlorotoluene ND ug/L 08/09/19 14:44 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 08/09/19 14:44 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/19 14:44 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 08/09/19 14:44 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/19 14:44 106-93-41.0 0.26 1
Dibromomethane ND ug/L 08/09/19 14:44 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 08/09/19 14:44 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 08/09/19 14:44 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 08/09/19 14:44 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 08/09/19 14:44 75-71-8 v11.0 0.23 1
1,1-Dichloroethane ND ug/L 08/09/19 14:44 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 08/09/19 14:44 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 08/09/19 14:44 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 08/09/19 14:44 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 08/09/19 14:44 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 08/09/19 14:44 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 08/09/19 14:44 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 08/09/19 14:44 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 08/09/19 14:44 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 08/09/19 14:44 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 08/09/19 14:44 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 08/09/19 14:44 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 08/09/19 14:44 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 08/09/19 14:44 87-68-31.0 0.44 1
2-Hexanone ND ug/L 08/09/19 14:44 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 08/09/19 14:44 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 08/09/19 14:44 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/19 14:44 108-10-15.0 4.5 1
Methyl-tert-butyl ether 1.8 ug/L 08/09/19 14:44 1634-04-41.0 0.28 1
Naphthalene ND ug/L 08/09/19 14:44 91-20-31.0 0.35 1
Styrene ND ug/L 08/09/19 14:44 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/19 14:44 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/19 14:44 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/09/19 14:44 127-18-41.0 0.16 1
Toluene ND ug/L 08/09/19 14:44 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 08/09/19 14:44 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 24 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: MW-5 Lab ID: 92440149005 Collected: 08/05/19 15:30 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 08/09/19 14:44 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 08/09/19 14:44 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 08/09/19 14:44 79-00-51.0 0.24 1
Trichloroethene ND ug/L 08/09/19 14:44 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 08/09/19 14:44 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 08/09/19 14:44 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 08/09/19 14:44 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 08/09/19 14:44 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 08/09/19 14:44 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 08/09/19 14:44 179601-23-12.0 0.41 1
o-Xylene ND ug/L 08/09/19 14:44 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)108 %08/09/19 14:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %08/09/19 14:44 17060-07-070-130 1
Toluene-d8 (S)102 %08/09/19 14:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: DUPLICATE Lab ID: 92440149006 Collected: 08/02/19 00:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/12/19 01:08 7440-38-208/11/19 10:0110.0 4.7 1
Barium 85.3 ug/L 08/12/19 01:08 7440-39-308/11/19 10:015.0 1.0 1
Cadmium ND ug/L 08/12/19 01:08 7440-43-908/11/19 10:011.0 0.40 1
Chromium ND ug/L 08/12/19 01:08 7440-47-308/11/19 10:015.0 1.0 1
Lead ND ug/L 08/12/19 01:08 7439-92-108/11/19 10:015.0 1.6 1
Selenium ND ug/L 08/12/19 01:08 7782-49-208/11/19 10:0110.0 4.7 1
Silver ND ug/L 08/12/19 01:08 7440-22-408/11/19 10:015.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/09/19 15:05 7439-97-608/07/19 14:460.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/11/19 15:57 83-32-908/08/19 18:0410.0 1.6 1
Acenaphthylene ND ug/L 08/11/19 15:57 208-96-808/08/19 18:0410.0 1.6 1
Aniline ND ug/L 08/11/19 15:57 62-53-308/08/19 18:0410.0 1.9 1
Anthracene ND ug/L 08/11/19 15:57 120-12-708/08/19 18:0410.0 1.7 1
Benzo(a)anthracene ND ug/L 08/11/19 15:57 56-55-308/08/19 18:0410.0 1.8 1
Benzo(a)pyrene ND ug/L 08/11/19 15:57 50-32-808/08/19 18:0410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 08/11/19 15:57 205-99-208/08/19 18:0410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 08/11/19 15:57 191-24-208/08/19 18:0410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 08/11/19 15:57 207-08-908/08/19 18:0410.0 1.9 1
Benzoic Acid ND ug/L 08/11/19 15:57 65-85-0 v108/08/19 18:0450.0 43.0 1
Benzyl alcohol ND ug/L 08/11/19 15:57 100-51-608/08/19 18:0420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 08/11/19 15:57 101-55-308/08/19 18:0410.0 1.6 1
Butylbenzylphthalate ND ug/L 08/11/19 15:57 85-68-708/08/19 18:0410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 08/11/19 15:57 59-50-708/08/19 18:0420.0 2.8 1
4-Chloroaniline ND ug/L 08/11/19 15:57 106-47-808/08/19 18:0420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 08/11/19 15:57 111-91-108/08/19 18:0410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 08/11/19 15:57 111-44-408/08/19 18:0410.0 1.8 1
2-Chloronaphthalene ND ug/L 08/11/19 15:57 91-58-708/08/19 18:0410.0 1.5 1
2-Chlorophenol ND ug/L 08/11/19 15:57 95-57-808/08/19 18:0410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 08/11/19 15:57 7005-72-308/08/19 18:0410.0 1.6 1
Chrysene ND ug/L 08/11/19 15:57 218-01-908/08/19 18:0410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 08/11/19 15:57 53-70-308/08/19 18:0410.0 1.6 1
Dibenzofuran ND ug/L 08/11/19 15:57 132-64-908/08/19 18:0410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 08/11/19 15:57 95-50-108/08/19 18:0410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 08/11/19 15:57 541-73-108/08/19 18:0410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 08/11/19 15:57 106-46-708/08/19 18:0410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 08/11/19 15:57 91-94-108/08/19 18:0420.0 3.0 1
2,4-Dichlorophenol ND ug/L 08/11/19 15:57 120-83-208/08/19 18:0410.0 1.4 1
Diethylphthalate ND ug/L 08/11/19 15:57 84-66-208/08/19 18:0410.0 2.4 1
2,4-Dimethylphenol ND ug/L 08/11/19 15:57 105-67-908/08/19 18:0410.0 1.4 1
Dimethylphthalate ND ug/L 08/11/19 15:57 131-11-308/08/19 18:0410.0 1.6 1
Di-n-butylphthalate ND ug/L 08/11/19 15:57 84-74-208/08/19 18:0410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 08/11/19 15:57 534-52-1 v108/08/19 18:0420.0 15.2 1
2,4-Dinitrophenol ND ug/L 08/11/19 15:57 51-28-5 v108/08/19 18:0450.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: DUPLICATE Lab ID: 92440149006 Collected: 08/02/19 00:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 08/11/19 15:57 121-14-208/08/19 18:0410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 08/11/19 15:57 606-20-208/08/19 18:0410.0 1.4 1
Di-n-octylphthalate ND ug/L 08/11/19 15:57 117-84-008/08/19 18:0410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/11/19 15:57 117-81-708/08/19 18:046.0 2.1 1
Fluoranthene ND ug/L 08/11/19 15:57 206-44-008/08/19 18:0410.0 1.7 1
Fluorene ND ug/L 08/11/19 15:57 86-73-708/08/19 18:0410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 08/11/19 15:57 87-68-308/08/19 18:0410.0 2.0 1
Hexachlorobenzene ND ug/L 08/11/19 15:57 118-74-108/08/19 18:0410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 08/11/19 15:57 77-47-408/08/19 18:0410.0 1.7 1
Hexachloroethane ND ug/L 08/11/19 15:57 67-72-108/08/19 18:0410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/11/19 15:57 193-39-508/08/19 18:0410.0 1.6 1
Isophorone ND ug/L 08/11/19 15:57 78-59-108/08/19 18:0410.0 1.6 1
1-Methylnaphthalene ND ug/L 08/11/19 15:57 90-12-008/08/19 18:0410.0 1.4 1
2-Methylnaphthalene ND ug/L 08/11/19 15:57 91-57-608/08/19 18:0410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 08/11/19 15:57 95-48-708/08/19 18:0410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/11/19 15:57 15831-10-408/08/19 18:0410.0 1.2 1
Naphthalene ND ug/L 08/11/19 15:57 91-20-308/08/19 18:0410.0 1.4 1
2-Nitroaniline ND ug/L 08/11/19 15:57 88-74-408/08/19 18:0420.0 4.2 1
3-Nitroaniline ND ug/L 08/11/19 15:57 99-09-208/08/19 18:0420.0 2.3 1
4-Nitroaniline ND ug/L 08/11/19 15:57 100-01-608/08/19 18:0420.0 2.2 1
Nitrobenzene ND ug/L 08/11/19 15:57 98-95-308/08/19 18:0410.0 2.1 1
2-Nitrophenol ND ug/L 08/11/19 15:57 88-75-508/08/19 18:0410.0 1.4 1
4-Nitrophenol ND ug/L 08/11/19 15:57 100-02-708/08/19 18:0450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 08/11/19 15:57 62-75-908/08/19 18:0410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 08/11/19 15:57 621-64-708/08/19 18:0410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 08/11/19 15:57 86-30-608/08/19 18:0410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/11/19 15:57 108-60-108/08/19 18:0410.0 2.8 1
Pentachlorophenol ND ug/L 08/11/19 15:57 87-86-5 v108/08/19 18:0425.0 2.2 1
Phenanthrene ND ug/L 08/11/19 15:57 85-01-808/08/19 18:0410.0 1.7 1
Phenol ND ug/L 08/11/19 15:57 108-95-208/08/19 18:0410.0 0.92 1
Pyrene ND ug/L 08/11/19 15:57 129-00-008/08/19 18:0410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 08/11/19 15:57 120-82-108/08/19 18:0410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 08/11/19 15:57 95-95-408/08/19 18:0410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 08/11/19 15:57 88-06-208/08/19 18:0410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)84 %08/11/19 15:57 4165-60-008/08/19 18:0413-130 1
2-Fluorobiphenyl (S)83 %08/11/19 15:57 321-60-808/08/19 18:0413-130 1
Terphenyl-d14 (S)107 %08/11/19 15:57 1718-51-008/08/19 18:0425-130 1
Phenol-d6 (S)46 %08/11/19 15:57 13127-88-308/08/19 18:0410-130 1
2-Fluorophenol (S)65 %08/11/19 15:57 367-12-408/08/19 18:0410-130 1
2,4,6-Tribromophenol (S)103 %08/11/19 15:57 118-79-608/08/19 18:0410-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/09/19 15:01 67-64-125.0 6.2 1
Benzene ND ug/L 08/09/19 15:01 71-43-21.0 0.15 1
Bromobenzene ND ug/L 08/09/19 15:01 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: DUPLICATE Lab ID: 92440149006 Collected: 08/02/19 00:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 08/09/19 15:01 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 08/09/19 15:01 75-27-41.0 0.26 1
Bromoform ND ug/L 08/09/19 15:01 75-25-21.0 0.62 1
Bromomethane ND ug/L 08/09/19 15:01 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 08/09/19 15:01 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 08/09/19 15:01 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 08/09/19 15:01 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/09/19 15:01 75-00-31.0 0.49 1
Chloroform ND ug/L 08/09/19 15:01 67-66-35.0 2.3 1
Chloromethane ND ug/L 08/09/19 15:01 74-87-3 v11.0 0.39 1
2-Chlorotoluene ND ug/L 08/09/19 15:01 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 08/09/19 15:01 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/19 15:01 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 08/09/19 15:01 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/19 15:01 106-93-41.0 0.26 1
Dibromomethane ND ug/L 08/09/19 15:01 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 08/09/19 15:01 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 08/09/19 15:01 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 08/09/19 15:01 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 08/09/19 15:01 75-71-8 v11.0 0.23 1
1,1-Dichloroethane ND ug/L 08/09/19 15:01 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 08/09/19 15:01 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 08/09/19 15:01 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 08/09/19 15:01 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 08/09/19 15:01 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 08/09/19 15:01 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 08/09/19 15:01 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 08/09/19 15:01 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 08/09/19 15:01 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 08/09/19 15:01 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 08/09/19 15:01 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 08/09/19 15:01 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 08/09/19 15:01 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 08/09/19 15:01 87-68-31.0 0.44 1
2-Hexanone ND ug/L 08/09/19 15:01 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 08/09/19 15:01 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 08/09/19 15:01 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/19 15:01 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 08/09/19 15:01 1634-04-41.0 0.28 1
Naphthalene ND ug/L 08/09/19 15:01 91-20-31.0 0.35 1
Styrene ND ug/L 08/09/19 15:01 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/19 15:01 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/19 15:01 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 08/09/19 15:01 127-18-41.0 0.16 1
Toluene ND ug/L 08/09/19 15:01 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 08/09/19 15:01 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: DUPLICATE Lab ID: 92440149006 Collected: 08/02/19 00:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 08/09/19 15:01 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 08/09/19 15:01 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 08/09/19 15:01 79-00-51.0 0.24 1
Trichloroethene ND ug/L 08/09/19 15:01 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 08/09/19 15:01 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 08/09/19 15:01 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 08/09/19 15:01 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 08/09/19 15:01 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 08/09/19 15:01 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 08/09/19 15:01 179601-23-12.0 0.41 1
o-Xylene ND ug/L 08/09/19 15:01 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)107 %08/09/19 15:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %08/09/19 15:01 17060-07-070-130 1
Toluene-d8 (S)101 %08/09/19 15:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 29 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: TRIP BLANK Lab ID: 92440149007 Collected: 08/02/19 00:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/09/19 12:42 67-64-125.0 6.2 1
Benzene ND ug/L 08/09/19 12:42 71-43-21.0 0.15 1
Bromobenzene ND ug/L 08/09/19 12:42 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 08/09/19 12:42 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 08/09/19 12:42 75-27-41.0 0.26 1
Bromoform ND ug/L 08/09/19 12:42 75-25-21.0 0.62 1
Bromomethane ND ug/L 08/09/19 12:42 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 08/09/19 12:42 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 08/09/19 12:42 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 08/09/19 12:42 108-90-71.0 0.23 1
Chloroethane ND ug/L 08/09/19 12:42 75-00-31.0 0.49 1
Chloroform ND ug/L 08/09/19 12:42 67-66-35.0 2.3 1
Chloromethane ND ug/L 08/09/19 12:42 74-87-3 v11.0 0.39 1
2-Chlorotoluene ND ug/L 08/09/19 12:42 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 08/09/19 12:42 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/19 12:42 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 08/09/19 12:42 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/19 12:42 106-93-41.0 0.26 1
Dibromomethane ND ug/L 08/09/19 12:42 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 08/09/19 12:42 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 08/09/19 12:42 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 08/09/19 12:42 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 08/09/19 12:42 75-71-8 v11.0 0.23 1
1,1-Dichloroethane ND ug/L 08/09/19 12:42 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 08/09/19 12:42 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 08/09/19 12:42 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 08/09/19 12:42 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 08/09/19 12:42 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 08/09/19 12:42 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 08/09/19 12:42 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 08/09/19 12:42 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 08/09/19 12:42 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 08/09/19 12:42 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 08/09/19 12:42 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 08/09/19 12:42 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 08/09/19 12:42 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 08/09/19 12:42 87-68-31.0 0.44 1
2-Hexanone ND ug/L 08/09/19 12:42 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 08/09/19 12:42 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 08/09/19 12:42 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/19 12:42 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 08/09/19 12:42 1634-04-41.0 0.28 1
Naphthalene ND ug/L 08/09/19 12:42 91-20-31.0 0.35 1
Styrene ND ug/L 08/09/19 12:42 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/19 12:42 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/19 12:42 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
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Page 30 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Sample: TRIP BLANK Lab ID: 92440149007 Collected: 08/02/19 00:00 Received: 08/06/19 13:40 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 08/09/19 12:42 127-18-41.0 0.16 1
Toluene ND ug/L 08/09/19 12:42 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 08/09/19 12:42 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 08/09/19 12:42 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 08/09/19 12:42 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 08/09/19 12:42 79-00-51.0 0.24 1
Trichloroethene ND ug/L 08/09/19 12:42 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 08/09/19 12:42 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 08/09/19 12:42 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 08/09/19 12:42 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 08/09/19 12:42 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 08/09/19 12:42 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 08/09/19 12:42 179601-23-12.0 0.41 1
o-Xylene ND ug/L 08/09/19 12:42 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)107 %08/09/19 12:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %08/09/19 12:42 17060-07-070-130 1
Toluene-d8 (S)102 %08/09/19 12:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
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Huntersville, NC 28078
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Page 31 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
490841
EPA 7470A
EPA 7470A
7470 Mercury
Associated Lab Samples: 92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2647503
Associated Lab Samples:92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 08/09/19 13:530.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2647504LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.32.5 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2647505MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92440149001
2647506
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 100 75-12597 3 252.5ND 2.5 2.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
491593
EPA 3010A
EPA 6010D
6010 MET
Associated Lab Samples: 92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2651232
Associated Lab Samples:92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006
Matrix: Water
AnalyzedMDL
Arsenic ug/L ND 10.0 08/11/19 23:184.7
Barium ug/L ND 5.0 08/11/19 23:181.0
Cadmium ug/L ND 1.0 08/11/19 23:180.40
Chromium ug/L ND 5.0 08/11/19 23:181.0
Lead ug/L ND 5.0 08/11/19 23:181.6
Selenium ug/L ND 10.0 08/11/19 23:184.7
Silver ug/L ND 5.0 08/11/19 23:182.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2651233LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 474500 95 80-120
Barium ug/L 489500 98 80-120
Cadmium ug/L 488500 98 80-120
Chromium ug/L 486500 97 80-120
Lead ug/L 490500 98 80-120
Selenium ug/L 488500 98 80-120
Silver ug/L 246250 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2651234MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92440149001
2651235
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 103 75-125103 0 20500ND514 516
Barium ug/L 500 104 75-125104 0 2050083.5 603 603
Cadmium ug/L 500 105 75-125105 0 20500ND527 527
Chromium ug/L 500 103 75-125104 1 20500ND517 522
Lead ug/L 500 103 75-125103 0 20500ND515 514
Selenium ug/L 500 109 75-125110 1 20500ND544 548
Silver ug/L 250 104 75-125104 0 20250ND261 261
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
491275
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples: 92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006, 92440149007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2649859
Associated Lab Samples:92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006, 92440149007
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/09/19 12:250.34
1,1,1-Trichloroethane ug/L ND 1.0 08/09/19 12:250.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/09/19 12:250.22
1,1,2-Trichloroethane ug/L ND 1.0 08/09/19 12:250.24
1,1-Dichloroethane ug/L ND 1.0 08/09/19 12:250.27
1,1-Dichloroethene ug/L ND 1.0 08/09/19 12:250.24
1,1-Dichloropropene ug/L ND 1.0 08/09/19 12:250.21
1,2,3-Trichlorobenzene ug/L ND 1.0 08/09/19 12:250.34
1,2,3-Trichloropropane ug/L ND 1.0 08/09/19 12:250.35
1,2,4-Trichlorobenzene ug/L ND 1.0 08/09/19 12:250.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 08/09/19 12:250.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/09/19 12:250.26
1,2-Dichlorobenzene ug/L ND 1.0 08/09/19 12:250.29
1,2-Dichloroethane ug/L ND 1.0 08/09/19 12:250.34
1,2-Dichloropropane ug/L ND 1.0 08/09/19 12:250.19
1,3-Dichlorobenzene ug/L ND 1.0 08/09/19 12:250.22
1,3-Dichloropropane ug/L ND 1.0 08/09/19 12:250.16
1,4-Dichlorobenzene ug/L ND 1.0 08/09/19 12:250.26
2,2-Dichloropropane ug/L ND 1.0 08/09/19 12:250.27
2-Butanone (MEK)ug/L ND 5.0 08/09/19 12:253.3
2-Chlorotoluene ug/L ND 1.0 08/09/19 12:250.20
2-Hexanone ug/L ND 5.0 08/09/19 12:250.57
4-Chlorotoluene ug/L ND 1.0 08/09/19 12:250.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/09/19 12:254.5
Acetone ug/L ND 25.0 08/09/19 12:256.2
Benzene ug/L ND 1.0 08/09/19 12:250.15
Bromobenzene ug/L ND 1.0 08/09/19 12:250.22
Bromochloromethane ug/L ND 1.0 08/09/19 12:250.34
Bromodichloromethane ug/L ND 1.0 08/09/19 12:250.26
Bromoform ug/L ND 1.0 08/09/19 12:250.62
Bromomethane ug/L ND 2.0 08/09/19 12:250.62
Carbon tetrachloride ug/L ND 1.0 08/09/19 12:250.22
Chlorobenzene ug/L ND 1.0 08/09/19 12:250.23
Chloroethane ug/L ND 1.0 08/09/19 12:250.49
Chloroform ug/L ND 5.0 08/09/19 12:252.3
Chloromethane ug/L ND 1.0 v108/09/19 12:250.39
cis-1,2-Dichloroethene ug/L ND 1.0 08/09/19 12:250.29
cis-1,3-Dichloropropene ug/L ND 1.0 08/09/19 12:250.30
Dibromochloromethane ug/L ND 1.0 08/09/19 12:250.41
Dibromomethane ug/L ND 1.0 08/09/19 12:250.46
Dichlorodifluoromethane ug/L ND 1.0 v108/09/19 12:250.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2649859
Associated Lab Samples:92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006, 92440149007
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 08/09/19 12:250.22
Ethylbenzene ug/L ND 1.0 08/09/19 12:250.26
Hexachloro-1,3-butadiene ug/L ND 1.0 08/09/19 12:250.44
m&p-Xylene ug/L ND 2.0 08/09/19 12:250.41
Methyl-tert-butyl ether ug/L ND 1.0 08/09/19 12:250.28
Methylene Chloride ug/L ND 5.0 08/09/19 12:253.7
Naphthalene ug/L ND 1.0 08/09/19 12:250.35
o-Xylene ug/L ND 1.0 08/09/19 12:250.22
p-Isopropyltoluene ug/L ND 1.0 08/09/19 12:250.21
Styrene ug/L ND 1.0 08/09/19 12:250.27
Tetrachloroethene ug/L ND 1.0 08/09/19 12:250.16
Toluene ug/L ND 1.0 08/09/19 12:250.24
trans-1,2-Dichloroethene ug/L ND 1.0 08/09/19 12:250.25
trans-1,3-Dichloropropene ug/L ND 1.0 08/09/19 12:250.31
Trichloroethene ug/L ND 1.0 08/09/19 12:250.22
Trichlorofluoromethane ug/L ND 1.0 08/09/19 12:250.31
Vinyl acetate ug/L ND 2.0 08/09/19 12:251.4
Vinyl chloride ug/L ND 1.0 08/09/19 12:250.24
Xylene (Total)ug/L ND 1.0 08/09/19 12:250.63
1,2-Dichloroethane-d4 (S)%101 70-130 08/09/19 12:25
4-Bromofluorobenzene (S)%108 70-130 08/09/19 12:25
Toluene-d8 (S)%102 70-130 08/09/19 12:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2649860LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.550 107 70-130
1,1,1-Trichloroethane ug/L 57.850 116 70-130
1,1,2,2-Tetrachloroethane ug/L 53.850 108 70-130
1,1,2-Trichloroethane ug/L 56.250 112 70-130
1,1-Dichloroethane ug/L 58.050 116 70-130
1,1-Dichloroethene ug/L 61.750 123 70-130
1,1-Dichloropropene ug/L 56.350 113 70-130
1,2,3-Trichlorobenzene ug/L 51.450 103 70-130
1,2,3-Trichloropropane ug/L 54.650 109 70-130
1,2,4-Trichlorobenzene ug/L 51.150 102 70-130
1,2-Dibromo-3-chloropropane ug/L 50.150 100 70-130
1,2-Dibromoethane (EDB)ug/L 53.350 107 70-130
1,2-Dichlorobenzene ug/L 49.650 99 70-130
1,2-Dichloroethane ug/L 53.550 107 70-130
1,2-Dichloropropane ug/L 55.750 111 70-130
1,3-Dichlorobenzene ug/L 49.250 98 70-130
1,3-Dichloropropane ug/L 53.250 106 70-131
1,4-Dichlorobenzene ug/L 48.850 98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2649860LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 61.450 123 69-130
2-Butanone (MEK)ug/L 121100 121 64-135
2-Chlorotoluene ug/L 48.150 96 70-130
2-Hexanone ug/L 111100 111 66-135
4-Chlorotoluene ug/L 49.050 98 70-130
4-Methyl-2-pentanone (MIBK)ug/L 113100 113 70-130
Acetone ug/L 122100 122 61-157
Benzene ug/L 55.450 111 70-130
Bromobenzene ug/L 49.150 98 70-130
Bromochloromethane ug/L 58.550 117 70-130
Bromodichloromethane ug/L 57.250 114 70-130
Bromoform ug/L 56.950 114 70-130
Bromomethane ug/L 45.150 90 38-130
Carbon tetrachloride ug/L 55.050 110 70-130
Chlorobenzene ug/L 50.050 100 70-130
Chloroethane ug/L 27.7 F3,IK5055 37-142
Chloroform ug/L 55.250 110 70-130
Chloromethane ug/L 64.2 v150128 48-130
cis-1,2-Dichloroethene ug/L 56.850 114 70-130
cis-1,3-Dichloropropene ug/L 61.650 123 70-130
Dibromochloromethane ug/L 54.850 110 70-130
Dibromomethane ug/L 56.350 113 70-130
Dichlorodifluoromethane ug/L 63.5 v150127 53-134
Diisopropyl ether ug/L 59.950 120 70-135
Ethylbenzene ug/L 50.950 102 70-130
Hexachloro-1,3-butadiene ug/L 52.550 105 68-132
m&p-Xylene ug/L 104100 104 70-130
Methyl-tert-butyl ether ug/L 59.350 119 70-130
Methylene Chloride ug/L 54.750 109 67-132
Naphthalene ug/L 50.250 100 70-130
o-Xylene ug/L 52.650 105 70-131
p-Isopropyltoluene ug/L 52.150 104 70-130
Styrene ug/L 53.650 107 70-130
Tetrachloroethene ug/L 51.950 104 69-130
Toluene ug/L 53.050 106 70-130
trans-1,2-Dichloroethene ug/L 59.550 119 70-130
trans-1,3-Dichloropropene ug/L 61.050 122 70-130
Trichloroethene ug/L 54.550 109 70-130
Trichlorofluoromethane ug/L 51.150 102 63-130
Vinyl acetate ug/L 128100 128 55-143
Vinyl chloride ug/L 61.050 122 70-131
Xylene (Total)ug/L 156150 104 70-130
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2649861MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92440149001
2649862
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 102 73-134101 1 3020ND20.5 20.3
1,1,1-Trichloroethane ug/L 20 117 82-143116 1 3020ND23.3 23.2
1,1,2,2-Tetrachloroethane ug/L 20 108 70-136109 0 3020ND21.7 21.7
1,1,2-Trichloroethane ug/L 20 110 70-135110 1 3020ND22.1 21.9
1,1-Dichloroethane ug/L 20 118 70-139117 1 3020ND23.5 23.4
1,1-Dichloroethene ug/L 20 123 70-154124 1 3020ND24.7 24.8
1,1-Dichloropropene ug/L 20 116 70-149115 1 3020ND23.2 22.9
1,2,3-Trichlorobenzene ug/L 20 94 70-13598 4 3020ND18.9 19.6
1,2,3-Trichloropropane ug/L 20 115 71-137110 5 3020ND23.1 22.0
1,2,4-Trichlorobenzene ug/L 20 96 73-14097 2 3020ND19.2 19.5
1,2-Dibromo-3-
chloropropane ug/L 20 102 65-134106 4 3020ND20.5 21.3
1,2-Dibromoethane (EDB) ug/L 20 104 70-137103 1 3020ND20.7 20.6
1,2-Dichlorobenzene ug/L 20 101 70-133100 0 3020ND20.1 20.0
1,2-Dichloroethane ug/L 20 107 70-137107 0 3020ND21.4 21.3
1,2-Dichloropropane ug/L 20 114 70-140112 1 3020ND22.7 22.4
1,3-Dichlorobenzene ug/L 20 99 70-13599 0 3020ND19.9 19.8
1,3-Dichloropropane ug/L 20 104 70-143104 1 3020ND20.9 20.7
1,4-Dichlorobenzene ug/L 20 98 70-13398 0 3020ND19.7 19.7
2,2-Dichloropropane ug/L 20 122 61-148121 0 3020ND24.3 24.2
2-Butanone (MEK)ug/L 40 126 60-139120 5 3040ND50.5 47.9
2-Chlorotoluene ug/L 20 96 70-14496 1 3020ND19.3 19.1
2-Hexanone ug/L 40 114 65-138110 4 3040ND45.5 43.9
4-Chlorotoluene ug/L 20 97 70-13795 2 3020ND19.4 19.1
4-Methyl-2-pentanone
(MIBK)ug/L 40 114 65-135110 3 3040ND45.5 44.0
Acetone ug/L 40 124 60-148118 5 3040ND49.8 47.2
Benzene ug/L 20 120 70-151115 4 3020ND24.0 23.0
Bromobenzene ug/L 20 97 70-13695 2 3020ND19.4 19.0
Bromochloromethane ug/L 20 124 70-141119 4 3020ND24.7 23.8
Bromodichloromethane ug/L 20 111 70-138110 1 3020ND22.2 22.0
Bromoform ug/L 20 102 63-130102 0 3020ND20.4 20.5
Bromomethane ug/L 20 100 15-15297 3 3020ND19.9 19.3
Carbon tetrachloride ug/L 20 109 70-143108 1 3020ND21.9 21.6
Chlorobenzene ug/L 20 103 70-138101 2 3020ND20.7 20.3
Chloroethane ug/L 20 95 52-16392 3 3020ND19.0 18.4
Chloroform ug/L 20 112 70-139110 2 3020ND22.4 21.9
Chloromethane ug/L M1,v12014041-139143 2 3020ND27.9 28.5
cis-1,2-Dichloroethene ug/L 20 114 70-141113 1 3020ND22.9 22.7
cis-1,3-Dichloropropene ug/L 20 119 70-137118 1 3020ND23.7 23.5
Dibromochloromethane ug/L 20 100 70-134100 0 3020ND20.0 19.9
Dibromomethane ug/L 20 114 70-138112 2 3020ND22.9 22.4
Dichlorodifluoromethane ug/L v12013247-155130 1 3020ND26.3 26.0
Diisopropyl ether ug/L 20 117 63-144116 1 3020ND23.4 23.2
Ethylbenzene ug/L 20 108 66-153106 2 3020ND21.6 21.2
Hexachloro-1,3-butadiene ug/L 20 101 65-149105 4 3020ND20.2 21.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2649861MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92440149001
2649862
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 111 69-152107 4 3040ND44.6 43.0
Methyl-tert-butyl ether ug/L 20 143 54-156119 18 3020ND28.5 23.7
Methylene Chloride ug/L 20 112 42-159113 1 3020ND22.4 22.7
Naphthalene ug/L 20 120 61-148100 19 3020ND24.1 20.0
o-Xylene ug/L 20 116 70-148110 6 3020ND23.2 21.9
p-Isopropyltoluene ug/L 20 103 70-146102 2 3020ND20.7 20.4
Styrene ug/L 20 108 70-135109 1 3020ND21.6 21.7
Tetrachloroethene ug/L 20 107 59-143105 2 3020ND21.5 21.1
Toluene ug/L 20 134 59-148115 16 3020ND26.9 23.0
trans-1,2-Dichloroethene ug/L 20 120 70-146117 3 3020ND24.0 23.4
trans-1,3-Dichloropropene ug/L 20 115 70-135114 1 3020ND22.9 22.8
Trichloroethene ug/L 20 116 70-147113 2 3020ND23.1 22.6
Trichlorofluoromethane ug/L 20 113 70-148112 1 3020ND22.6 22.4
Vinyl acetate ug/L 40 122 49-151120 2 3040ND48.6 47.9
Vinyl chloride ug/L 20 131 70-156131 0 3020ND26.3 26.2
Xylene (Total)ug/L 60 113 63-158108 4 3060ND67.8 64.9
1,2-Dichloroethane-d4 (S) %102 70-130103
4-Bromofluorobenzene (S) %106 70-130107
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
491346
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Associated Lab Samples: 92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2650031
Associated Lab Samples:92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 08/09/19 13:361.5
1,2-Dichlorobenzene ug/L ND 10.0 08/09/19 13:361.3
1,3-Dichlorobenzene ug/L ND 10.0 08/09/19 13:361.5
1,4-Dichlorobenzene ug/L ND 10.0 08/09/19 13:362.1
1-Methylnaphthalene ug/L ND 10.0 08/09/19 13:361.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 08/09/19 13:362.8
2,4,5-Trichlorophenol ug/L ND 10.0 08/09/19 13:361.4
2,4,6-Trichlorophenol ug/L ND 10.0 08/09/19 13:361.5
2,4-Dichlorophenol ug/L ND 10.0 08/09/19 13:361.4
2,4-Dimethylphenol ug/L ND 10.0 08/09/19 13:361.4
2,4-Dinitrophenol ug/L ND 50.0 08/09/19 13:3640.5
2,4-Dinitrotoluene ug/L ND 10.0 08/09/19 13:361.2
2,6-Dinitrotoluene ug/L ND 10.0 08/09/19 13:361.4
2-Chloronaphthalene ug/L ND 10.0 08/09/19 13:361.5
2-Chlorophenol ug/L ND 10.0 08/09/19 13:361.2
2-Methylnaphthalene ug/L ND 10.0 08/09/19 13:361.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 08/09/19 13:361.2
2-Nitroaniline ug/L ND 20.0 08/09/19 13:364.2
2-Nitrophenol ug/L ND 10.0 08/09/19 13:361.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 08/09/19 13:361.2
3,3'-Dichlorobenzidine ug/L ND 20.0 08/09/19 13:363.0
3-Nitroaniline ug/L ND 20.0 08/09/19 13:362.3
4,6-Dinitro-2-methylphenol ug/L ND 20.0 08/09/19 13:3615.2
4-Bromophenylphenyl ether ug/L ND 10.0 08/09/19 13:361.6
4-Chloro-3-methylphenol ug/L ND 20.0 08/09/19 13:362.8
4-Chloroaniline ug/L ND 20.0 08/09/19 13:362.8
4-Chlorophenylphenyl ether ug/L ND 10.0 08/09/19 13:361.6
4-Nitroaniline ug/L ND 20.0 08/09/19 13:362.2
4-Nitrophenol ug/L ND 50.0 08/09/19 13:363.5
Acenaphthene ug/L ND 10.0 08/09/19 13:361.6
Acenaphthylene ug/L ND 10.0 08/09/19 13:361.6
Aniline ug/L ND 10.0 08/09/19 13:361.9
Anthracene ug/L ND 10.0 08/09/19 13:361.7
Benzo(a)anthracene ug/L ND 10.0 08/09/19 13:361.8
Benzo(a)pyrene ug/L ND 10.0 08/09/19 13:362.1
Benzo(b)fluoranthene ug/L ND 10.0 08/09/19 13:361.9
Benzo(g,h,i)perylene ug/L ND 10.0 08/09/19 13:361.4
Benzo(k)fluoranthene ug/L ND 10.0 08/09/19 13:361.9
Benzoic Acid ug/L ND 50.0 08/09/19 13:3643.0
Benzyl alcohol ug/L ND 20.0 08/09/19 13:362.6
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/09/19 13:361.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2650031
Associated Lab Samples:92440149001, 92440149002, 92440149003, 92440149004, 92440149005, 92440149006
Matrix: Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 08/09/19 13:361.8
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 08/09/19 13:362.1
Butylbenzylphthalate ug/L ND 10.0 08/09/19 13:361.6
Chrysene ug/L ND 10.0 08/09/19 13:361.7
Di-n-butylphthalate ug/L ND 10.0 08/09/19 13:361.8
Di-n-octylphthalate ug/L ND 10.0 08/09/19 13:361.8
Dibenz(a,h)anthracene ug/L ND 10.0 08/09/19 13:361.6
Dibenzofuran ug/L ND 10.0 08/09/19 13:361.5
Diethylphthalate ug/L ND 10.0 08/09/19 13:362.4
Dimethylphthalate ug/L ND 10.0 08/09/19 13:361.6
Fluoranthene ug/L ND 10.0 08/09/19 13:361.7
Fluorene ug/L ND 10.0 08/09/19 13:361.6
Hexachloro-1,3-butadiene ug/L ND 10.0 08/09/19 13:362.0
Hexachlorobenzene ug/L ND 10.0 08/09/19 13:361.7
Hexachlorocyclopentadiene ug/L ND 10.0 08/09/19 13:361.7
Hexachloroethane ug/L ND 10.0 08/09/19 13:362.0
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 08/09/19 13:361.6
Isophorone ug/L ND 10.0 08/09/19 13:361.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 08/09/19 13:362.2
N-Nitrosodimethylamine ug/L ND 10.0 08/09/19 13:361.2
N-Nitrosodiphenylamine ug/L ND 10.0 08/09/19 13:361.7
Naphthalene ug/L ND 10.0 08/09/19 13:361.4
Nitrobenzene ug/L ND 10.0 08/09/19 13:362.1
Pentachlorophenol ug/L ND 25.0 08/09/19 13:362.2
Phenanthrene ug/L ND 10.0 08/09/19 13:361.7
Phenol ug/L ND 10.0 08/09/19 13:360.92
Pyrene ug/L ND 10.0 08/09/19 13:362.1
2,4,6-Tribromophenol (S)%79 10-137 08/09/19 13:36
2-Fluorobiphenyl (S)%68 13-130 08/09/19 13:36
2-Fluorophenol (S)%62 10-130 08/09/19 13:36
Nitrobenzene-d5 (S)%73 13-130 08/09/19 13:36
Phenol-d6 (S)%44 10-130 08/09/19 13:36
Terphenyl-d14 (S)%100 25-130 08/09/19 13:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2650032LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2650033
1,2,4-Trichlorobenzene ug/L 36.350 73 30-1307537.4 3 30
1,2-Dichlorobenzene ug/L 36.250 72 30-1307336.6 1 30
1,3-Dichlorobenzene ug/L 36.650 73 20-1307336.5 0 30
1,4-Dichlorobenzene ug/L 37.050 74 30-1307437.1 0 30
1-Methylnaphthalene ug/L 41.150 82 30-1308442.1 2 30
2,2'-Oxybis(1-chloropropane)ug/L 41.050 82 20-1308542.5 3 30
2,4,5-Trichlorophenol ug/L 38.150 76 40-1308140.4 6 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2650032LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2650033
2,4,6-Trichlorophenol ug/L 38.750 77 40-1308241.1 6 30
2,4-Dichlorophenol ug/L 38.450 77 31-1308241.1 7 30
2,4-Dimethylphenol ug/L 37.450 75 30-1307839.0 4 30
2,4-Dinitrophenol ug/L 233250 93 30-13095237 2 30
2,4-Dinitrotoluene ug/L 42.050 84 49-1308441.9 0 30
2,6-Dinitrotoluene ug/L 40.750 81 50-1308542.4 4 30
2-Chloronaphthalene ug/L 34.350 69 30-1307135.4 3 30
2-Chlorophenol ug/L 37.550 75 30-1308039.9 6 30
2-Methylnaphthalene ug/L 43.350 87 30-1308944.3 2 30
2-Methylphenol(o-Cresol)ug/L 35.450 71 30-1307537.5 6 30
2-Nitroaniline ug/L 89.9100 90 40-1309292.3 3 30
2-Nitrophenol ug/L 39.150 78 20-1308441.8 7 30
3&4-Methylphenol(m&p Cresol)ug/L 35.050 70 20-1307336.6 4 30
3,3'-Dichlorobenzidine ug/L 87.9100 88 10-1509392.6 5 30
3-Nitroaniline ug/L 93.4100 93 40-1309393.1 0 30
4,6-Dinitro-2-methylphenol ug/L 97.8100 98 40-130103103 6 30
4-Bromophenylphenyl ether ug/L 44.150 88 30-1309447.1 7 30
4-Chloro-3-methylphenol ug/L 81.8100 82 30-1308585.4 4 30
4-Chloroaniline ug/L 83.0100 83 20-1308584.7 2 30
4-Chlorophenylphenyl ether ug/L 41.350 83 20-1308542.7 3 30
4-Nitroaniline ug/L 98.2100 98 40-1309797.0 1 30
4-Nitrophenol ug/L 162250 65 10-13064161 1 30
Acenaphthene ug/L 39.650 79 30-1308241.0 4 30
Acenaphthylene ug/L 40.350 81 30-1308442.2 5 30
Aniline ug/L 34.250 68 20-1307336.5 6 30
Anthracene ug/L 47.150 94 50-1309949.4 5 30
Benzo(a)anthracene ug/L 49.350 99 50-13010753.3 8 30
Benzo(a)pyrene ug/L 49.250 98 50-13010552.3 6 30
Benzo(b)fluoranthene ug/L 48.650 97 50-13010552.3 7 30
Benzo(g,h,i)perylene ug/L 48.750 97 50-13010251.0 5 30
Benzo(k)fluoranthene ug/L 48.950 98 50-13010652.9 8 30
Benzoic Acid ug/L 109250 44 10-1303381.8 28 30
Benzyl alcohol ug/L 72.8100 73 20-1307676.4 5 30
bis(2-Chloroethoxy)methane ug/L 39.650 79 30-1308442.0 6 30
bis(2-Chloroethyl) ether ug/L 39.150 78 30-1308542.6 8 30
bis(2-Ethylhexyl)phthalate ug/L 51.450 103 50-13010954.6 6 30
Butylbenzylphthalate ug/L 49.250 98 50-15010853.9 9 30
Chrysene ug/L 50.150 100 50-13010854.2 8 30
Di-n-butylphthalate ug/L 51.150 102 50-13010251.2 0 30
Di-n-octylphthalate ug/L 52.450 105 50-13011055.2 5 30
Dibenz(a,h)anthracene ug/L 49.450 99 40-13010351.5 4 30
Dibenzofuran ug/L 39.750 79 40-1308140.7 3 30
Diethylphthalate ug/L 43.150 86 40-1308944.5 3 30
Dimethylphthalate ug/L 42.650 85 40-1308843.8 3 30
Fluoranthene ug/L 50.350 101 30-13010351.7 3 30
Fluorene ug/L 42.150 84 20-1308643.0 2 30
Hexachloro-1,3-butadiene ug/L 36.550 73 10-1307336.7 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2650032LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2650033
Hexachlorobenzene ug/L 39.350 79 30-1308241.2 5 30
Hexachlorocyclopentadiene ug/L 34.850 70 10-1507135.6 2 30
Hexachloroethane ug/L 36.050 72 10-1307135.4 2 30
Indeno(1,2,3-cd)pyrene ug/L 49.250 98 40-13010351.7 5 30
Isophorone ug/L 36.250 72 30-1307738.6 6 30
N-Nitroso-di-n-propylamine ug/L 40.350 81 30-1308743.5 8 30
N-Nitrosodimethylamine ug/L 35.550 71 10-1307738.4 8 30
N-Nitrosodiphenylamine ug/L 45.750 91 30-1309447.1 3 30
Naphthalene ug/L 42.050 84 20-1308743.5 4 30
Nitrobenzene ug/L 36.250 72 20-1307738.4 6 30
Pentachlorophenol ug/L 99.5100 100 10-140101101 1 30
Phenanthrene ug/L 46.350 93 50-1309648.1 4 30
Phenol ug/L 26.350 53 10-1305527.6 5 30
Pyrene ug/L 48.350 97 50-13010652.9 9 30
2,4,6-Tribromophenol (S)%102 10-13793
2-Fluorobiphenyl (S)%79 13-13073
2-Fluorophenol (S)%69 10-13065
Nitrobenzene-d5 (S)%80 13-13077
Phenol-d6 (S)%54 10-13050
Terphenyl-d14 (S)%97 25-13095
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2651585MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92440149001
2651586
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 69 30-13069 1 3050ND34.5 34.7
1,2-Dichlorobenzene ug/L 50 68 30-13067 3 3050ND34.2 33.4
1,3-Dichlorobenzene ug/L 50 66 20-13067 1 3050ND33.1 33.3
1,4-Dichlorobenzene ug/L 50 66 30-13066 1 3050ND34.1 33.8
1-Methylnaphthalene ug/L 50 82 30-13077 7 3050ND41.1 38.3
2,2'-Oxybis(1-
chloropropane)ug/L 50 81 20-13074 9 3050ND40.6 37.2
2,4,5-Trichlorophenol ug/L 50 82 40-13076 8 3050ND40.8 37.9
2,4,6-Trichlorophenol ug/L 50 86 40-13079 9 3050ND42.9 39.4
2,4-Dichlorophenol ug/L 50 82 31-13075 9 3050ND40.9 37.4
2,4-Dimethylphenol ug/L 50 77 30-13070 9 3050ND38.6 35.1
2,4-Dinitrophenol ug/L R1,v125011430-13035 106 30250ND284 87.5
2,4-Dinitrotoluene ug/L 50 90 49-13081 10 3050ND44.9 40.4
2,6-Dinitrotoluene ug/L 50 86 50-13079 9 3050ND42.9 39.3
2-Chloronaphthalene ug/L 50 68 30-13066 3 3050ND34.2 33.1
2-Chlorophenol ug/L 50 78 30-13072 9 3050ND39.2 36.0
2-Methylnaphthalene ug/L 50 86 30-13082 5 3050ND43.0 41.0
2-Methylphenol(o-Cresol) ug/L 50 71 30-13065 8 3050ND35.5 32.6
2-Nitroaniline ug/L 100 87 40-13085 3 30100ND86.8 84.5
2-Nitrophenol ug/L 50 87 20-13082 6 3050ND43.4 40.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/13/2019 03:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2651585MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92440149001
2651586
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/L 50 70 20-13064 9 3050ND34.8 31.9
3,3'-Dichlorobenzidine ug/L 100 82 10-15082 0 30100ND82.5 82.4
3-Nitroaniline ug/L 100 94 40-13087 7 30100ND94.1 87.5
4,6-Dinitro-2-methylphenol ug/L v110011340-13086 27 30100ND113 86.5
4-Bromophenylphenyl ether ug/L 50 95 30-13086 10 3050ND47.6 43.1
4-Chloro-3-methylphenol ug/L 100 86 30-13077 11 30100ND86.3 77.1
4-Chloroaniline ug/L 100 86 20-13079 9 30100ND86.2 78.6
4-Chlorophenylphenyl ether ug/L 50 89 20-13081 9 3050ND44.3 40.6
4-Nitroaniline ug/L 100 99 40-13092 8 30100ND99.2 91.6
4-Nitrophenol ug/L 250 60 10-13045 28 30250ND150 113
Acenaphthene ug/L 50 82 30-13077 6 3050ND40.9 38.5
Acenaphthylene ug/L 50 83 30-13078 6 3050ND41.4 39.1
Aniline ug/L 50 55 20-13067 19 3050ND27.5 33.3
Anthracene ug/L 50 99 50-13089 11 3050ND49.6 44.5
Benzo(a)anthracene ug/L 50 102 50-13096 6 3050ND51.2 48.2
Benzo(a)pyrene ug/L 50 99 50-13093 6 3050ND49.3 46.7
Benzo(b)fluoranthene ug/L 50 98 50-13094 4 3050ND49.2 47.2
Benzo(g,h,i)perylene ug/L 50 102 50-13095 7 3050ND51.0 47.4
Benzo(k)fluoranthene ug/L 50 101 50-13093 8 3050ND50.5 46.4
Benzoic Acid ug/L M1,v12505910-1305 30250ND146 ND
Benzyl alcohol ug/L 100 76 20-13067 12 30100ND75.7 67.4
bis(2-
Chloroethoxy)methane ug/L 50 83 30-13077 8 3050ND41.5 38.3
bis(2-Chloroethyl) ether ug/L 50 84 30-13076 10 3050ND42.0 38.0
bis(2-Ethylhexyl)phthalate ug/L 50 105 50-13098 7 3050ND52.5 48.8
Butylbenzylphthalate ug/L 50 103 50-15096 7 3050ND51.5 48.0
Chrysene ug/L 50 104 50-13097 7 3050ND52.0 48.7
Di-n-butylphthalate ug/L 50 101 50-13092 9 3050ND50.4 46.2
Di-n-octylphthalate ug/L 50 106 50-13097 9 3050ND52.9 48.6
Dibenz(a,h)anthracene ug/L 50 102 40-13094 8 3050ND51.2 47.2
Dibenzofuran ug/L 50 83 40-13077 8 3050ND41.6 38.3
Diethylphthalate ug/L 50 92 40-13083 10 3050ND46.0 41.7
Dimethylphthalate ug/L 50 89 40-13082 9 3050ND44.6 40.9
Fluoranthene ug/L 50 104 30-13095 9 3050ND52.2 47.5
Fluorene ug/L 50 89 20-13081 9 3050ND44.3 40.4
Hexachloro-1,3-butadiene ug/L 50 65 10-13067 3 3050ND32.6 33.4
Hexachlorobenzene ug/L 50 85 30-13077 9 3050ND42.3 38.7
Hexachlorocyclopentadiene ug/L 50 64 10-15063 1 3050ND31.9 31.4
Hexachloroethane ug/L 50 65 10-13065 0 3050ND32.6 32.4
Indeno(1,2,3-cd)pyrene ug/L 50 102 40-13095 7 3050ND50.9 47.6
Isophorone ug/L 50 77 30-13069 11 3050ND38.5 34.6
N-Nitroso-di-n-propylamine ug/L 50 85 30-13076 10 3050ND42.3 38.2
N-Nitrosodimethylamine ug/L 50 68 10-13064 6 3050ND33.9 31.8
N-Nitrosodiphenylamine ug/L 50 88 30-13084 5 3050ND44.1 42.1
Naphthalene ug/L 50 82 20-13080 2 3050ND40.9 39.9
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2651585MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92440149001
2651586
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrobenzene ug/L 50 76 20-13071 7 3050ND38.1 35.5
Pentachlorophenol ug/L R1,v110011810-14079 39 30100ND118 79.2
Phenanthrene ug/L 50 98 50-13088 11 3050ND48.8 43.9
Phenol ug/L 50 48 10-13043 11 3050ND24.1 21.6
Pyrene ug/L 50 102 50-13095 6 3050ND50.8 47.7
2,4,6-Tribromophenol (S) %118 10-137102
2-Fluorobiphenyl (S)%80 13-13075
2-Fluorophenol (S)%67 10-13061
Nitrobenzene-d5 (S)%84 13-13077
Phenol-d6 (S)%49 10-13044
Terphenyl-d14 (S)%101 25-13093
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92440149
COREY'S TRANSMISSION
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92440149001 491593 491649MW-1 (MS/MSD)EPA 3010A EPA 6010D
92440149002 491593 491649MW-2 EPA 3010A EPA 6010D
92440149003 491593 491649MW-3 EPA 3010A EPA 6010D
92440149004 491593 491649MW-4 EPA 3010A EPA 6010D
92440149005 491593 491649MW-5 EPA 3010A EPA 6010D
92440149006 491593 491649DUPLICATEEPA 3010A EPA 6010D
92440149001 490841 490902MW-1 (MS/MSD)EPA 7470A EPA 7470A
92440149002 490841 490902MW-2 EPA 7470A EPA 7470A
92440149003 490841 490902MW-3 EPA 7470A EPA 7470A
92440149004 490841 490902MW-4 EPA 7470A EPA 7470A
92440149005 490841 490902MW-5 EPA 7470A EPA 7470A
92440149006 490841 490902DUPLICATEEPA 7470A EPA 7470A
92440149001 491346 491442MW-1 (MS/MSD)EPA 3510C EPA 8270E
92440149002 491346 491442MW-2 EPA 3510C EPA 8270E
92440149003 491346 491442MW-3 EPA 3510C EPA 8270E
92440149004 491346 491442MW-4 EPA 3510C EPA 8270E
92440149005 491346 491442MW-5 EPA 3510C EPA 8270E
92440149006 491346 491442DUPLICATEEPA 3510C EPA 8270E
92440149001 491275MW-1 (MS/MSD)EPA 8260D
92440149002 491275MW-2 EPA 8260D
92440149003 491275MW-3 EPA 8260D
92440149004 491275MW-4 EPA 8260D
92440149005 491275MW-5 EPA 8260D
92440149006 491275DUPLICATEEPA 8260D
92440149007 491275TRIP BLANK EPA 8260D
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Page 46 of 48
Page 47 of 48
Page 48 of 48
#=CL#
August 30, 2019
LIMS USE: FR - JOE NESTOR
LIMS OBJECT ID: 92442364
92442364
Project:
Pace Project No.:
RE:
Joe Nestor
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
Corey's
Dear Joe Nestor:
Enclosed are the analytical results for sample(s) received by the laboratory on August 21, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
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Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92442364
Corey's
Pace Analytical National Certification IDs
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92442364
Corey's
Lab ID Sample ID Matrix Date Collected Date Received
92442364001 A Solid 08/20/19 16:05 08/21/19 14:31
92442364002 B Solid 08/19/19 16:15 08/21/19 14:31
92442364003 C Solid 08/19/19 16:25 08/21/19 14:31
92442364004 D Solid 08/20/19 16:35 08/21/19 14:31
92442364005 E Solid 08/20/19 16:45 08/21/19 14:31
92442364006 DUP2 Solid 08/20/19 00:00 08/21/19 14:31
REPORT OF LABORATORY ANALYSIS
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Page 3 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92442364
Corey's
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92442364001 A SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92442364002 B SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92442364003 C SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92442364004 D SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92442364005 E SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92442364006 DUP2 SM 2540G 1 PANKDW
EPA 7199 1 PANGB
REPORT OF LABORATORY ANALYSIS
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#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442364
Corey's
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442364001 A
Total Solids 86.5 %08/29/19 13:48SM 2540G
92442364002 B
Total Solids 85.2 %08/29/19 13:48SM 2540G
92442364003 C
Total Solids 81.8 %08/29/19 13:48SM 2540G
92442364004 D
Total Solids 85.3 %08/29/19 13:48SM 2540G
Chromium, Hexavalent 0.509J mg/kg 08/29/19 16:20 J1.17EPA 7199
92442364005 E
Total Solids 87.9 %08/29/19 13:48SM 2540G
92442364006 DUP2
Total Solids 89.8 %08/29/19 13:48SM 2540G
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442364
Corey's
Sample: A Lab ID: 92442364001 Collected: 08/20/19 16:05 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 86.5 %08/29/19 13:4808/29/19 13:411
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/29/19 16:05 18540-29-908/28/19 20:191.16 0.295 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442364
Corey's
Sample: B Lab ID: 92442364002 Collected: 08/19/19 16:15 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 85.2 %08/29/19 13:4808/29/19 13:411
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/29/19 16:10 18540-29-908/28/19 20:191.17 0.299 1
REPORT OF LABORATORY ANALYSIS
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Page 7 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442364
Corey's
Sample: C Lab ID: 92442364003 Collected: 08/19/19 16:25 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 81.8 %08/29/19 13:4808/29/19 13:411
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/29/19 16:15 18540-29-908/28/19 20:191.22 0.312 1
REPORT OF LABORATORY ANALYSIS
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Page 8 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442364
Corey's
Sample: D Lab ID: 92442364004 Collected: 08/20/19 16:35 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 85.3 %08/29/19 13:4808/29/19 13:411
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.509J mg/kg 08/29/19 16:20 18540-29-9 J08/28/19 20:191.17 0.299 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442364
Corey's
Sample: E Lab ID: 92442364005 Collected: 08/20/19 16:45 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 87.9 %08/29/19 13:4808/29/19 13:411
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.316J mg/kg 08/29/19 16:25 18540-29-9 J08/28/19 20:191.14 0.290 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442364
Corey's
Sample: DUP2 Lab ID: 92442364006 Collected: 08/20/19 00:00 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 89.8 %08/29/19 13:4808/29/19 13:411
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/29/19 16:30 18540-29-908/28/19 20:191.11 0.284 1
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442364
Corey's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1336504
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples: 92442364001, 92442364002, 92442364003, 92442364004, 92442364005, 92442364006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3446085-1
Associated Lab Samples:92442364001, 92442364002, 92442364003, 92442364004, 92442364005, 92442364006
Matrix: Solid
AnalyzedMDL
Total Solids %ND 08/29/19 13:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3446085-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1132135-01
R3446085-3SAMPLE DUPLICATE:
Total Solids %87.2 2.38 1089.3
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442364
Corey's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1335649
3060A
EPA 7199
Wet Chemistry 7199
Associated Lab Samples: 92442364001, 92442364002, 92442364003, 92442364004, 92442364005, 92442364006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3445659-1
Associated Lab Samples:92442364001, 92442364002, 92442364003, 92442364004, 92442364005, 92442364006
Matrix: Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 08/29/19 13:590.255
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3445659-3
Associated Lab Samples:92442364001, 92442364002, 92442364003, 92442364004, 92442364005, 92442364006
Matrix: Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 08/29/19 14:590.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3445659-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.8910.0 98.9 80.0-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3445659-4LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.110.0 101 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3445659-6MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1131786-04
R3445659-7
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 27.8 99.2 75.0-12596.0 3.18 2027.8ND 28.0 27.1
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3445659-8MATRIX SPIKE SAMPLE:
MSSpike
Result
L1131786-04
Chromium, Hexavalent mg/kg 11401160 98.6 75.0-125ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/30/2019 05:07 PM
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Page 13 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442364
Corey's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1131786-03
R3445659-5SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1132220-11
R3445659-10SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.556J J18.9 200.672
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/30/2019 05:07 PM
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92442364
Corey's
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
ANALYTE QUALIFIERS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92442364
Corey's
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92442364001 1336504 1336504ASM 2540 G SM 2540G
92442364002 1336504 1336504BSM 2540 G SM 2540G
92442364003 1336504 1336504CSM 2540 G SM 2540G
92442364004 1336504 1336504DSM 2540 G SM 2540G
92442364005 1336504 1336504ESM 2540 G SM 2540G
92442364006 1336504 1336504DUP2SM 2540 G SM 2540G
92442364001 1335649 1335649A3060AEPA 7199
92442364002 1335649 1335649B3060AEPA 7199
92442364003 1335649 1335649C3060AEPA 7199
92442364004 1335649 1335649D3060AEPA 7199
92442364005 1335649 1335649E3060AEPA 7199
92442364006 1335649 1335649DUP23060AEPA 7199
REPORT OF LABORATORY ANALYSIS
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Page 16 of 17
Page 17 of 17
#=CL#
August 26, 2019
LIMS USE: FR - JOE NESTOR
LIMS OBJECT ID: 92442356
92442356
Project:
Pace Project No.:
RE:
Joe Nestor
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
Corey's Transmission
Dear Joe Nestor:
Enclosed are the analytical results for sample(s) received by the laboratory on August 21, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 77
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92442356
Corey's Transmission
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 77
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92442356
Corey's Transmission
Lab ID Sample ID Matrix Date Collected Date Received
92442356001 A-2 Solid 08/20/19 15:20 08/21/19 14:31
92442356002 A-3 Solid 08/20/19 15:30 08/21/19 14:31
92442356003 B-1 Solid 08/20/19 15:40 08/21/19 14:31
92442356004 B-2 Solid 08/20/19 15:45 08/21/19 14:31
92442356005 C-2 Solid 08/19/19 16:20 08/21/19 14:31
92442356006 C-3 Solid 08/19/19 16:00 08/21/19 14:31
92442356007 D-1 Solid 08/19/19 16:30 08/21/19 14:31
92442356008 D-4 Solid 08/19/19 16:40 08/21/19 14:31
92442356009 E-3 Solid 08/20/19 15:50 08/21/19 14:31
92442356010 E-5 Solid 08/20/19 16:00 08/21/19 14:31
92442356011 A Solid 08/20/19 16:05 08/21/19 14:31
92442356012 B Solid 08/20/19 16:15 08/21/19 14:31
92442356013 C Solid 08/20/19 16:25 08/21/19 14:31
92442356014 D Solid 08/20/19 16:35 08/21/19 14:31
92442356015 E Solid 08/20/19 16:45 08/21/19 14:31
92442356016 DUP1 Solid 08/20/19 00:00 08/21/19 14:31
92442356017 DUP2 Solid 08/20/19 00:00 08/21/19 14:31
REPORT OF LABORATORY ANALYSIS
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Page 3 of 77
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92442356
Corey's Transmission
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92442356001 A-2 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356002 A-3 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356003 B-1 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356004 B-2 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356005 C-2 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356006 C-3 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356007 D-1 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356008 D-4 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356009 E-3 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356010 E-5 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356011 A EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-AJMW1
EPA 8270E 74 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
92442356012 B EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-AJMW1
EPA 8270E 74 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
92442356013 C EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-AJMW1
EPA 8270E 74 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
92442356014 D EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-AJMW1
EPA 8270E 74 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
92442356015 E EPA 6010D 7 PASI-ASH1
REPORT OF LABORATORY ANALYSIS
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Page 4 of 77
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92442356
Corey's Transmission
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7471B 1 PASI-AJMW1
EPA 8270E 74 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
92442356016 DUP1 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92442356017 DUP2 EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-AJMW1
EPA 8270E 74 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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Page 5 of 77
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442356
Corey's Transmission
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442356001 A-2
Percent Moisture 14.2 %08/23/19 12:500.10ASTM D2974-87
92442356002 A-3
Percent Moisture 14.7 %08/23/19 12:500.10ASTM D2974-87
92442356003 B-1
Percent Moisture 14.6 %08/23/19 12:510.10ASTM D2974-87
92442356004 B-2
Percent Moisture 16.7 %08/23/19 12:510.10ASTM D2974-87
92442356005 C-2
Percent Moisture 23.3 %08/23/19 12:510.10ASTM D2974-87
92442356006 C-3
Acetone 72.7J ug/kg 08/23/19 13:32 B,v190.1EPA 8260D
Benzene 1.3J ug/kg 08/23/19 13:324.5EPA 8260D
Percent Moisture 15.0 %08/23/19 12:510.10ASTM D2974-87
92442356007 D-1
Acetone 17.7J ug/kg 08/23/19 13:57 B,v194.9EPA 8260D
Percent Moisture 13.1 %08/23/19 12:510.10ASTM D2974-87
92442356008 D-4
Percent Moisture 15.1 %08/22/19 16:530.10ASTM D2974-87
92442356009 E-3
Percent Moisture 15.6 %08/22/19 16:580.10ASTM D2974-87
92442356010 E-5
Percent Moisture 16.8 %08/22/19 16:580.10ASTM D2974-87
92442356011 A
Arsenic 0.45J mg/kg 08/23/19 10:22 M10.67EPA 6010D
Barium 91.7 mg/kg 08/23/19 10:220.33EPA 6010D
Cadmium 0.042J mg/kg 08/23/19 10:220.067EPA 6010D
Chromium 30.8 mg/kg 08/23/19 10:220.33EPA 6010D
Lead 3.6 mg/kg 08/23/19 10:22 M10.33EPA 6010D
Selenium 0.63J mg/kg 08/23/19 10:22 M10.67EPA 6010D
Mercury 0.023 mg/kg 08/26/19 14:020.0051EPA 7471B
Benzo(a)anthracene 116J ug/kg 08/22/19 14:45360EPA 8270E
Benzo(b)fluoranthene 177J ug/kg 08/22/19 14:45360EPA 8270E
Chrysene 127J ug/kg 08/22/19 14:45360EPA 8270E
Fluoranthene 258J ug/kg 08/22/19 14:45360EPA 8270E
Phenanthrene 155J ug/kg 08/22/19 14:45360EPA 8270E
Pyrene 228J ug/kg 08/22/19 14:45360EPA 8270E
Percent Moisture 8.7 %08/22/19 13:210.10ASTM D2974-87
92442356012 B
Barium 258 mg/kg 08/23/19 10:340.34EPA 6010D
Cadmium 0.039J mg/kg 08/23/19 10:340.068EPA 6010D
REPORT OF LABORATORY ANALYSIS
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Page 6 of 77
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442356
Corey's Transmission
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442356012 B
Chromium 60.3 mg/kg 08/23/19 10:340.34EPA 6010D
Lead 1.1 mg/kg 08/23/19 10:34 B0.34EPA 6010D
Selenium 0.62J mg/kg 08/23/19 10:340.68EPA 6010D
Mercury 0.010 mg/kg 08/26/19 14:050.0060EPA 7471B
Benzo(a)anthracene 326J ug/kg 08/22/19 15:52391EPA 8270E
Benzo(a)pyrene 322J ug/kg 08/22/19 15:52391EPA 8270E
Benzo(b)fluoranthene 509 ug/kg 08/22/19 15:52391EPA 8270E
Benzo(g,h,i)perylene 247J ug/kg 08/22/19 15:52391EPA 8270E
Benzo(k)fluoranthene 203J ug/kg 08/22/19 15:52391EPA 8270E
Chrysene 373J ug/kg 08/22/19 15:52391EPA 8270E
Fluoranthene 797 ug/kg 08/22/19 15:52391EPA 8270E
Indeno(1,2,3-cd)pyrene 202J ug/kg 08/22/19 15:52391EPA 8270E
Phenanthrene 541 ug/kg 08/22/19 15:52391EPA 8270E
Pyrene 672 ug/kg 08/22/19 15:52391EPA 8270E
Percent Moisture 15.0 %08/22/19 13:210.10ASTM D2974-87
92442356013 C
Arsenic 1.0 mg/kg 08/23/19 10:370.85EPA 6010D
Barium 74.0 mg/kg 08/23/19 10:370.42EPA 6010D
Cadmium 0.090 mg/kg 08/23/19 10:370.085EPA 6010D
Chromium 54.9 mg/kg 08/23/19 10:370.42EPA 6010D
Lead 3.6 mg/kg 08/23/19 10:370.42EPA 6010D
Selenium 0.73J mg/kg 08/23/19 10:370.85EPA 6010D
Mercury 0.011 mg/kg 08/26/19 14:070.0043EPA 7471B
Percent Moisture 22.6 %08/22/19 13:210.10ASTM D2974-87
92442356014 D
Barium 75.1 mg/kg 08/23/19 10:460.33EPA 6010D
Cadmium 0.059J mg/kg 08/23/19 10:460.067EPA 6010D
Chromium 104 mg/kg 08/23/19 10:460.33EPA 6010D
Lead 2.1 mg/kg 08/23/19 10:460.33EPA 6010D
Selenium 0.51J mg/kg 08/23/19 10:460.67EPA 6010D
Mercury 0.010 mg/kg 08/26/19 14:140.0041EPA 7471B
Percent Moisture 15.1 %08/22/19 13:210.10ASTM D2974-87
92442356015 E
Arsenic 1.5 mg/kg 08/23/19 10:490.78EPA 6010D
Barium 67.2 mg/kg 08/23/19 10:490.39EPA 6010D
Cadmium 0.13 mg/kg 08/23/19 10:490.078EPA 6010D
Chromium 23.6 mg/kg 08/23/19 10:490.39EPA 6010D
Lead 33.3 mg/kg 08/23/19 10:490.39EPA 6010D
Selenium 0.69J mg/kg 08/23/19 10:490.78EPA 6010D
Mercury 0.018 mg/kg 08/26/19 14:160.0032EPA 7471B
Chrysene 126J ug/kg 08/22/19 17:01383EPA 8270E
Fluoranthene 270J ug/kg 08/22/19 17:01383EPA 8270E
Phenanthrene 173J ug/kg 08/22/19 17:01383EPA 8270E
Pyrene 207J ug/kg 08/22/19 17:01383EPA 8270E
Percent Moisture 13.6 %08/22/19 13:220.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 7 of 77
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442356
Corey's Transmission
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442356016 DUP1
Acetone 25.9J ug/kg 08/23/19 13:0479.9EPA 8260D
Percent Moisture 14.8 %08/22/19 16:580.10ASTM D2974-87
92442356017 DUP2
Arsenic 0.72 mg/kg 08/23/19 10:520.71EPA 6010D
Barium 55.5 mg/kg 08/23/19 10:520.36EPA 6010D
Cadmium 0.068J mg/kg 08/23/19 10:520.071EPA 6010D
Chromium 17.7 mg/kg 08/23/19 10:520.36EPA 6010D
Lead 6.2 mg/kg 08/23/19 10:520.36EPA 6010D
Selenium 1.2 mg/kg 08/23/19 10:520.71EPA 6010D
Mercury 0.073 mg/kg 08/26/19 15:380.0063EPA 7471B
Percent Moisture 12.4 %08/22/19 13:220.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 8 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: A-2 Lab ID: 92442356001 Collected: 08/20/19 15:20 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 08/22/19 17:47 67-64-108/22/19 13:5983.6 7.9 1
Benzene ND ug/kg 08/22/19 17:47 71-43-208/22/19 13:594.2 0.75 1
Bromobenzene ND ug/kg 08/22/19 17:47 108-86-108/22/19 13:594.2 1.1 1
Bromochloromethane ND ug/kg 08/22/19 17:47 74-97-508/22/19 13:594.2 1.0 1
Bromodichloromethane ND ug/kg 08/22/19 17:47 75-27-408/22/19 13:594.2 0.82 1
Bromoform ND ug/kg 08/22/19 17:47 75-25-208/22/19 13:594.2 2.0 1
Bromomethane ND ug/kg 08/22/19 17:47 74-83-908/22/19 13:598.4 2.0 1
2-Butanone (MEK)ND ug/kg 08/22/19 17:47 78-93-308/22/19 13:5983.6 9.9 1
n-Butylbenzene ND ug/kg 08/22/19 17:47 104-51-808/22/19 13:594.2 2.4 1
sec-Butylbenzene ND ug/kg 08/22/19 17:47 135-98-808/22/19 13:594.2 1.8 1
tert-Butylbenzene ND ug/kg 08/22/19 17:47 98-06-608/22/19 13:594.2 1.4 1
Carbon tetrachloride ND ug/kg 08/22/19 17:47 56-23-508/22/19 13:594.2 0.80 1
Chlorobenzene ND ug/kg 08/22/19 17:47 108-90-708/22/19 13:594.2 0.81 1
Chloroethane ND ug/kg 08/22/19 17:47 75-00-308/22/19 13:598.4 1.7 1
Chloroform ND ug/kg 08/22/19 17:47 67-66-308/22/19 13:594.2 0.89 1
Chloromethane ND ug/kg 08/22/19 17:47 74-87-308/22/19 13:598.4 2.7 1
2-Chlorotoluene ND ug/kg 08/22/19 17:47 95-49-808/22/19 13:594.2 1.3 1
4-Chlorotoluene ND ug/kg 08/22/19 17:47 106-43-408/22/19 13:594.2 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/22/19 17:47 96-12-808/22/19 13:594.2 2.1 1
Dibromochloromethane ND ug/kg 08/22/19 17:47 124-48-108/22/19 13:594.2 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 08/22/19 17:47 106-93-408/22/19 13:594.2 0.94 1
Dibromomethane ND ug/kg 08/22/19 17:47 74-95-308/22/19 13:594.2 1.2 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 17:47 95-50-108/22/19 13:594.2 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 17:47 541-73-108/22/19 13:594.2 1.5 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 17:47 106-46-708/22/19 13:594.2 1.4 1
Dichlorodifluoromethane ND ug/kg 08/22/19 17:47 75-71-808/22/19 13:598.4 3.4 1
1,1-Dichloroethane ND ug/kg 08/22/19 17:47 75-34-308/22/19 13:594.2 0.61 1
1,2-Dichloroethane ND ug/kg 08/22/19 17:47 107-06-208/22/19 13:594.2 0.84 1
1,1-Dichloroethene ND ug/kg 08/22/19 17:47 75-35-408/22/19 13:594.2 0.97 1
cis-1,2-Dichloroethene ND ug/kg 08/22/19 17:47 156-59-208/22/19 13:594.2 0.73 1
trans-1,2-Dichloroethene ND ug/kg 08/22/19 17:47 156-60-508/22/19 13:594.2 0.82 1
1,2-Dichloropropane ND ug/kg 08/22/19 17:47 78-87-508/22/19 13:594.2 1.6 1
1,3-Dichloropropane ND ug/kg 08/22/19 17:47 142-28-908/22/19 13:594.2 1.6 1
2,2-Dichloropropane ND ug/kg 08/22/19 17:47 594-20-708/22/19 13:594.2 0.41 1
1,1-Dichloropropene ND ug/kg 08/22/19 17:47 563-58-608/22/19 13:594.2 1.8 1
cis-1,3-Dichloropropene ND ug/kg 08/22/19 17:47 10061-01-508/22/19 13:594.2 1.9 1
trans-1,3-Dichloropropene ND ug/kg 08/22/19 17:47 10061-02-608/22/19 13:594.2 0.73 1
Diisopropyl ether ND ug/kg 08/22/19 17:47 108-20-308/22/19 13:594.2 2.4 1
Ethylbenzene ND ug/kg 08/22/19 17:47 100-41-408/22/19 13:594.2 0.89 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 17:47 87-68-308/22/19 13:594.2 2.1 1
2-Hexanone ND ug/kg 08/22/19 17:47 591-78-608/22/19 13:5941.8 4.3 1
Isopropylbenzene (Cumene)ND ug/kg 08/22/19 17:47 98-82-808/22/19 13:594.2 1.2 1
p-Isopropyltoluene ND ug/kg 08/22/19 17:47 99-87-608/22/19 13:594.2 2.0 1
Methylene Chloride ND ug/kg 08/22/19 17:47 75-09-208/22/19 13:5916.7 4.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/22/19 17:47 108-10-108/22/19 13:5941.8 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: A-2 Lab ID: 92442356001 Collected: 08/20/19 15:20 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/22/19 17:47 1634-04-408/22/19 13:594.2 2.4 1
Naphthalene ND ug/kg 08/22/19 17:47 91-20-308/22/19 13:594.2 3.6 1
n-Propylbenzene ND ug/kg 08/22/19 17:47 103-65-108/22/19 13:594.2 1.4 1
Styrene ND ug/kg 08/22/19 17:47 100-42-508/22/19 13:594.2 1.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/22/19 17:47 630-20-608/22/19 13:594.2 1.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/22/19 17:47 79-34-508/22/19 13:594.2 1.4 1
Tetrachloroethene ND ug/kg 08/22/19 17:47 127-18-408/22/19 13:594.2 1.3 1
Toluene ND ug/kg 08/22/19 17:47 108-88-308/22/19 13:594.2 1.4 1
1,2,3-Trichlorobenzene ND ug/kg 08/22/19 17:47 87-61-608/22/19 13:594.2 3.0 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 17:47 120-82-108/22/19 13:594.2 2.2 1
1,1,1-Trichloroethane ND ug/kg 08/22/19 17:47 71-55-608/22/19 13:594.2 0.73 1
1,1,2-Trichloroethane ND ug/kg 08/22/19 17:47 79-00-508/22/19 13:594.2 0.94 1
Trichloroethene ND ug/kg 08/22/19 17:47 79-01-608/22/19 13:594.2 1.1 1
Trichlorofluoromethane ND ug/kg 08/22/19 17:47 75-69-408/22/19 13:594.2 0.99 1
1,2,3-Trichloropropane ND ug/kg 08/22/19 17:47 96-18-408/22/19 13:594.2 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 08/22/19 17:47 95-63-608/22/19 13:594.2 1.6 1
1,3,5-Trimethylbenzene ND ug/kg 08/22/19 17:47 108-67-808/22/19 13:594.2 1.4 1
Vinyl acetate ND ug/kg 08/22/19 17:47 108-05-408/22/19 13:5941.8 13.6 1
Vinyl chloride ND ug/kg 08/22/19 17:47 75-01-408/22/19 13:598.4 1.6 1
Xylene (Total)ND ug/kg 08/22/19 17:47 1330-20-708/22/19 13:598.4 2.9 1
m&p-Xylene ND ug/kg 08/22/19 17:47 179601-23-108/22/19 13:598.4 2.0 1
o-Xylene ND ug/kg 08/22/19 17:47 95-47-608/22/19 13:594.2 0.98 1
Surrogates
Toluene-d8 (S)108 %08/22/19 17:47 2037-26-5 1g08/22/19 13:5970-130 1
4-Bromofluorobenzene (S)107 %08/22/19 17:47 460-00-408/22/19 13:5970-130 1
1,2-Dichloroethane-d4 (S)142 %08/22/19 17:47 17060-07-0 S308/22/19 13:5970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.2 %08/23/19 12:500.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: A-3 Lab ID: 92442356002 Collected: 08/20/19 15:30 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 08/22/19 18:12 67-64-108/22/19 13:59101 9.5 1
Benzene ND ug/kg 08/22/19 18:12 71-43-208/22/19 13:595.0 0.90 1
Bromobenzene ND ug/kg 08/22/19 18:12 108-86-108/22/19 13:595.0 1.4 1
Bromochloromethane ND ug/kg 08/22/19 18:12 74-97-508/22/19 13:595.0 1.2 1
Bromodichloromethane ND ug/kg 08/22/19 18:12 75-27-408/22/19 13:595.0 0.98 1
Bromoform ND ug/kg 08/22/19 18:12 75-25-208/22/19 13:595.0 2.5 1
Bromomethane ND ug/kg 08/22/19 18:12 74-83-908/22/19 13:5910.1 2.4 1
2-Butanone (MEK)ND ug/kg 08/22/19 18:12 78-93-308/22/19 13:59101 12.0 1
n-Butylbenzene ND ug/kg 08/22/19 18:12 104-51-808/22/19 13:595.0 2.8 1
sec-Butylbenzene ND ug/kg 08/22/19 18:12 135-98-808/22/19 13:595.0 2.1 1
tert-Butylbenzene ND ug/kg 08/22/19 18:12 98-06-608/22/19 13:595.0 1.7 1
Carbon tetrachloride ND ug/kg 08/22/19 18:12 56-23-508/22/19 13:595.0 0.96 1
Chlorobenzene ND ug/kg 08/22/19 18:12 108-90-708/22/19 13:595.0 0.97 1
Chloroethane ND ug/kg 08/22/19 18:12 75-00-308/22/19 13:5910.1 2.1 1
Chloroform ND ug/kg 08/22/19 18:12 67-66-308/22/19 13:595.0 1.1 1
Chloromethane ND ug/kg 08/22/19 18:12 74-87-308/22/19 13:5910.1 3.3 1
2-Chlorotoluene ND ug/kg 08/22/19 18:12 95-49-808/22/19 13:595.0 1.5 1
4-Chlorotoluene ND ug/kg 08/22/19 18:12 106-43-408/22/19 13:595.0 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/22/19 18:12 96-12-808/22/19 13:595.0 2.6 1
Dibromochloromethane ND ug/kg 08/22/19 18:12 124-48-108/22/19 13:595.0 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 08/22/19 18:12 106-93-408/22/19 13:595.0 1.1 1
Dibromomethane ND ug/kg 08/22/19 18:12 74-95-308/22/19 13:595.0 1.5 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 18:12 95-50-108/22/19 13:595.0 1.8 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 18:12 541-73-108/22/19 13:595.0 1.8 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 18:12 106-46-708/22/19 13:595.0 1.7 1
Dichlorodifluoromethane ND ug/kg 08/22/19 18:12 75-71-808/22/19 13:5910.1 4.1 1
1,1-Dichloroethane ND ug/kg 08/22/19 18:12 75-34-308/22/19 13:595.0 0.74 1
1,2-Dichloroethane ND ug/kg 08/22/19 18:12 107-06-208/22/19 13:595.0 1.0 1
1,1-Dichloroethene ND ug/kg 08/22/19 18:12 75-35-408/22/19 13:595.0 1.2 1
cis-1,2-Dichloroethene ND ug/kg 08/22/19 18:12 156-59-208/22/19 13:595.0 0.87 1
trans-1,2-Dichloroethene ND ug/kg 08/22/19 18:12 156-60-508/22/19 13:595.0 0.99 1
1,2-Dichloropropane ND ug/kg 08/22/19 18:12 78-87-508/22/19 13:595.0 1.9 1
1,3-Dichloropropane ND ug/kg 08/22/19 18:12 142-28-908/22/19 13:595.0 1.9 1
2,2-Dichloropropane ND ug/kg 08/22/19 18:12 594-20-708/22/19 13:595.0 0.50 1
1,1-Dichloropropene ND ug/kg 08/22/19 18:12 563-58-608/22/19 13:595.0 2.1 1
cis-1,3-Dichloropropene ND ug/kg 08/22/19 18:12 10061-01-508/22/19 13:595.0 2.3 1
trans-1,3-Dichloropropene ND ug/kg 08/22/19 18:12 10061-02-608/22/19 13:595.0 0.88 1
Diisopropyl ether ND ug/kg 08/22/19 18:12 108-20-308/22/19 13:595.0 2.9 1
Ethylbenzene ND ug/kg 08/22/19 18:12 100-41-408/22/19 13:595.0 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 18:12 87-68-308/22/19 13:595.0 2.5 1
2-Hexanone ND ug/kg 08/22/19 18:12 591-78-608/22/19 13:5950.3 5.2 1
Isopropylbenzene (Cumene)ND ug/kg 08/22/19 18:12 98-82-808/22/19 13:595.0 1.5 1
p-Isopropyltoluene ND ug/kg 08/22/19 18:12 99-87-608/22/19 13:595.0 2.4 1
Methylene Chloride ND ug/kg 08/22/19 18:12 75-09-208/22/19 13:5920.1 5.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/22/19 18:12 108-10-108/22/19 13:5950.3 3.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: A-3 Lab ID: 92442356002 Collected: 08/20/19 15:30 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/22/19 18:12 1634-04-408/22/19 13:595.0 2.9 1
Naphthalene ND ug/kg 08/22/19 18:12 91-20-308/22/19 13:595.0 4.3 1
n-Propylbenzene ND ug/kg 08/22/19 18:12 103-65-108/22/19 13:595.0 1.7 1
Styrene ND ug/kg 08/22/19 18:12 100-42-508/22/19 13:595.0 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/22/19 18:12 630-20-608/22/19 13:595.0 1.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/22/19 18:12 79-34-508/22/19 13:595.0 1.7 1
Tetrachloroethene ND ug/kg 08/22/19 18:12 127-18-408/22/19 13:595.0 1.6 1
Toluene ND ug/kg 08/22/19 18:12 108-88-308/22/19 13:595.0 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 08/22/19 18:12 87-61-608/22/19 13:595.0 3.6 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 18:12 120-82-108/22/19 13:595.0 2.7 1
1,1,1-Trichloroethane ND ug/kg 08/22/19 18:12 71-55-608/22/19 13:595.0 0.88 1
1,1,2-Trichloroethane ND ug/kg 08/22/19 18:12 79-00-508/22/19 13:595.0 1.1 1
Trichloroethene ND ug/kg 08/22/19 18:12 79-01-608/22/19 13:595.0 1.3 1
Trichlorofluoromethane ND ug/kg 08/22/19 18:12 75-69-408/22/19 13:595.0 1.2 1
1,2,3-Trichloropropane ND ug/kg 08/22/19 18:12 96-18-408/22/19 13:595.0 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 08/22/19 18:12 95-63-608/22/19 13:595.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 08/22/19 18:12 108-67-808/22/19 13:595.0 1.7 1
Vinyl acetate ND ug/kg 08/22/19 18:12 108-05-408/22/19 13:5950.3 16.4 1
Vinyl chloride ND ug/kg 08/22/19 18:12 75-01-408/22/19 13:5910.1 1.9 1
Xylene (Total)ND ug/kg 08/22/19 18:12 1330-20-708/22/19 13:5910.1 3.5 1
m&p-Xylene ND ug/kg 08/22/19 18:12 179601-23-108/22/19 13:5910.1 2.4 1
o-Xylene ND ug/kg 08/22/19 18:12 95-47-608/22/19 13:595.0 1.2 1
Surrogates
Toluene-d8 (S)108 %08/22/19 18:12 2037-26-508/22/19 13:5970-130 1
4-Bromofluorobenzene (S)101 %08/22/19 18:12 460-00-408/22/19 13:5970-130 1
1,2-Dichloroethane-d4 (S)94 %08/22/19 18:12 17060-07-008/22/19 13:5970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.7 %08/23/19 12:500.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: B-1 Lab ID: 92442356003 Collected: 08/20/19 15:40 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 08/22/19 18:36 67-64-108/22/19 13:5985.3 8.1 1
Benzene ND ug/kg 08/22/19 18:36 71-43-208/22/19 13:594.3 0.77 1
Bromobenzene ND ug/kg 08/22/19 18:36 108-86-108/22/19 13:594.3 1.2 1
Bromochloromethane ND ug/kg 08/22/19 18:36 74-97-508/22/19 13:594.3 1.0 1
Bromodichloromethane ND ug/kg 08/22/19 18:36 75-27-408/22/19 13:594.3 0.83 1
Bromoform ND ug/kg 08/22/19 18:36 75-25-208/22/19 13:594.3 2.1 1
Bromomethane ND ug/kg 08/22/19 18:36 74-83-908/22/19 13:598.5 2.0 1
2-Butanone (MEK)ND ug/kg 08/22/19 18:36 78-93-308/22/19 13:5985.3 10.2 1
n-Butylbenzene ND ug/kg 08/22/19 18:36 104-51-808/22/19 13:594.3 2.4 1
sec-Butylbenzene ND ug/kg 08/22/19 18:36 135-98-808/22/19 13:594.3 1.8 1
tert-Butylbenzene ND ug/kg 08/22/19 18:36 98-06-608/22/19 13:594.3 1.4 1
Carbon tetrachloride ND ug/kg 08/22/19 18:36 56-23-508/22/19 13:594.3 0.82 1
Chlorobenzene ND ug/kg 08/22/19 18:36 108-90-708/22/19 13:594.3 0.83 1
Chloroethane ND ug/kg 08/22/19 18:36 75-00-308/22/19 13:598.5 1.8 1
Chloroform ND ug/kg 08/22/19 18:36 67-66-308/22/19 13:594.3 0.90 1
Chloromethane ND ug/kg 08/22/19 18:36 74-87-308/22/19 13:598.5 2.8 1
2-Chlorotoluene ND ug/kg 08/22/19 18:36 95-49-808/22/19 13:594.3 1.3 1
4-Chlorotoluene ND ug/kg 08/22/19 18:36 106-43-408/22/19 13:594.3 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/22/19 18:36 96-12-808/22/19 13:594.3 2.2 1
Dibromochloromethane ND ug/kg 08/22/19 18:36 124-48-108/22/19 13:594.3 2.1 1
1,2-Dibromoethane (EDB)ND ug/kg 08/22/19 18:36 106-93-408/22/19 13:594.3 0.96 1
Dibromomethane ND ug/kg 08/22/19 18:36 74-95-308/22/19 13:594.3 1.3 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 18:36 95-50-108/22/19 13:594.3 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 18:36 541-73-108/22/19 13:594.3 1.5 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 18:36 106-46-708/22/19 13:594.3 1.5 1
Dichlorodifluoromethane ND ug/kg 08/22/19 18:36 75-71-808/22/19 13:598.5 3.5 1
1,1-Dichloroethane ND ug/kg 08/22/19 18:36 75-34-308/22/19 13:594.3 0.63 1
1,2-Dichloroethane ND ug/kg 08/22/19 18:36 107-06-208/22/19 13:594.3 0.85 1
1,1-Dichloroethene ND ug/kg 08/22/19 18:36 75-35-408/22/19 13:594.3 0.99 1
cis-1,2-Dichloroethene ND ug/kg 08/22/19 18:36 156-59-208/22/19 13:594.3 0.74 1
trans-1,2-Dichloroethene ND ug/kg 08/22/19 18:36 156-60-508/22/19 13:594.3 0.84 1
1,2-Dichloropropane ND ug/kg 08/22/19 18:36 78-87-508/22/19 13:594.3 1.6 1
1,3-Dichloropropane ND ug/kg 08/22/19 18:36 142-28-908/22/19 13:594.3 1.6 1
2,2-Dichloropropane ND ug/kg 08/22/19 18:36 594-20-708/22/19 13:594.3 0.42 1
1,1-Dichloropropene ND ug/kg 08/22/19 18:36 563-58-608/22/19 13:594.3 1.8 1
cis-1,3-Dichloropropene ND ug/kg 08/22/19 18:36 10061-01-508/22/19 13:594.3 1.9 1
trans-1,3-Dichloropropene ND ug/kg 08/22/19 18:36 10061-02-608/22/19 13:594.3 0.75 1
Diisopropyl ether ND ug/kg 08/22/19 18:36 108-20-308/22/19 13:594.3 2.4 1
Ethylbenzene ND ug/kg 08/22/19 18:36 100-41-408/22/19 13:594.3 0.90 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 18:36 87-68-308/22/19 13:594.3 2.1 1
2-Hexanone ND ug/kg 08/22/19 18:36 591-78-608/22/19 13:5942.7 4.4 1
Isopropylbenzene (Cumene)ND ug/kg 08/22/19 18:36 98-82-808/22/19 13:594.3 1.2 1
p-Isopropyltoluene ND ug/kg 08/22/19 18:36 99-87-608/22/19 13:594.3 2.1 1
Methylene Chloride ND ug/kg 08/22/19 18:36 75-09-208/22/19 13:5917.1 5.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/22/19 18:36 108-10-108/22/19 13:5942.7 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: B-1 Lab ID: 92442356003 Collected: 08/20/19 15:40 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/22/19 18:36 1634-04-408/22/19 13:594.3 2.4 1
Naphthalene ND ug/kg 08/22/19 18:36 91-20-308/22/19 13:594.3 3.6 1
n-Propylbenzene ND ug/kg 08/22/19 18:36 103-65-108/22/19 13:594.3 1.4 1
Styrene ND ug/kg 08/22/19 18:36 100-42-508/22/19 13:594.3 1.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/22/19 18:36 630-20-608/22/19 13:594.3 1.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/22/19 18:36 79-34-508/22/19 13:594.3 1.5 1
Tetrachloroethene ND ug/kg 08/22/19 18:36 127-18-408/22/19 13:594.3 1.3 1
Toluene ND ug/kg 08/22/19 18:36 108-88-308/22/19 13:594.3 1.4 1
1,2,3-Trichlorobenzene ND ug/kg 08/22/19 18:36 87-61-608/22/19 13:594.3 3.0 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 18:36 120-82-108/22/19 13:594.3 2.3 1
1,1,1-Trichloroethane ND ug/kg 08/22/19 18:36 71-55-608/22/19 13:594.3 0.74 1
1,1,2-Trichloroethane ND ug/kg 08/22/19 18:36 79-00-508/22/19 13:594.3 0.96 1
Trichloroethene ND ug/kg 08/22/19 18:36 79-01-608/22/19 13:594.3 1.1 1
Trichlorofluoromethane ND ug/kg 08/22/19 18:36 75-69-408/22/19 13:594.3 1.0 1
1,2,3-Trichloropropane ND ug/kg 08/22/19 18:36 96-18-408/22/19 13:594.3 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 08/22/19 18:36 95-63-608/22/19 13:594.3 1.7 1
1,3,5-Trimethylbenzene ND ug/kg 08/22/19 18:36 108-67-808/22/19 13:594.3 1.4 1
Vinyl acetate ND ug/kg 08/22/19 18:36 108-05-408/22/19 13:5942.7 13.9 1
Vinyl chloride ND ug/kg 08/22/19 18:36 75-01-408/22/19 13:598.5 1.6 1
Xylene (Total)ND ug/kg 08/22/19 18:36 1330-20-708/22/19 13:598.5 3.0 1
m&p-Xylene ND ug/kg 08/22/19 18:36 179601-23-108/22/19 13:598.5 2.0 1
o-Xylene ND ug/kg 08/22/19 18:36 95-47-608/22/19 13:594.3 1.0 1
Surrogates
Toluene-d8 (S)104 %08/22/19 18:36 2037-26-508/22/19 13:5970-130 1
4-Bromofluorobenzene (S)105 %08/22/19 18:36 460-00-408/22/19 13:5970-130 1
1,2-Dichloroethane-d4 (S)126 %08/22/19 18:36 17060-07-008/22/19 13:5970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.6 %08/23/19 12:510.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: B-2 Lab ID: 92442356004 Collected: 08/20/19 15:45 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 08/22/19 19:01 67-64-108/22/19 13:59107 10.1 1
Benzene ND ug/kg 08/22/19 19:01 71-43-208/22/19 13:595.3 0.96 1
Bromobenzene ND ug/kg 08/22/19 19:01 108-86-108/22/19 13:595.3 1.5 1
Bromochloromethane ND ug/kg 08/22/19 19:01 74-97-508/22/19 13:595.3 1.3 1
Bromodichloromethane ND ug/kg 08/22/19 19:01 75-27-408/22/19 13:595.3 1.0 1
Bromoform ND ug/kg 08/22/19 19:01 75-25-208/22/19 13:595.3 2.6 1
Bromomethane ND ug/kg 08/22/19 19:01 74-83-908/22/19 13:5910.7 2.5 1
2-Butanone (MEK)ND ug/kg 08/22/19 19:01 78-93-308/22/19 13:59107 12.7 1
n-Butylbenzene ND ug/kg 08/22/19 19:01 104-51-808/22/19 13:595.3 3.0 1
sec-Butylbenzene ND ug/kg 08/22/19 19:01 135-98-808/22/19 13:595.3 2.3 1
tert-Butylbenzene ND ug/kg 08/22/19 19:01 98-06-608/22/19 13:595.3 1.8 1
Carbon tetrachloride ND ug/kg 08/22/19 19:01 56-23-508/22/19 13:595.3 1.0 1
Chlorobenzene ND ug/kg 08/22/19 19:01 108-90-708/22/19 13:595.3 1.0 1
Chloroethane ND ug/kg 08/22/19 19:01 75-00-308/22/19 13:5910.7 2.2 1
Chloroform ND ug/kg 08/22/19 19:01 67-66-308/22/19 13:595.3 1.1 1
Chloromethane ND ug/kg 08/22/19 19:01 74-87-308/22/19 13:5910.7 3.5 1
2-Chlorotoluene ND ug/kg 08/22/19 19:01 95-49-808/22/19 13:595.3 1.6 1
4-Chlorotoluene ND ug/kg 08/22/19 19:01 106-43-408/22/19 13:595.3 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/22/19 19:01 96-12-808/22/19 13:595.3 2.7 1
Dibromochloromethane ND ug/kg 08/22/19 19:01 124-48-108/22/19 13:595.3 2.7 1
1,2-Dibromoethane (EDB)ND ug/kg 08/22/19 19:01 106-93-408/22/19 13:595.3 1.2 1
Dibromomethane ND ug/kg 08/22/19 19:01 74-95-308/22/19 13:595.3 1.6 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 19:01 95-50-108/22/19 13:595.3 1.9 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 19:01 541-73-108/22/19 13:595.3 1.9 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 19:01 106-46-708/22/19 13:595.3 1.8 1
Dichlorodifluoromethane ND ug/kg 08/22/19 19:01 75-71-808/22/19 13:5910.7 4.4 1
1,1-Dichloroethane ND ug/kg 08/22/19 19:01 75-34-308/22/19 13:595.3 0.79 1
1,2-Dichloroethane ND ug/kg 08/22/19 19:01 107-06-208/22/19 13:595.3 1.1 1
1,1-Dichloroethene ND ug/kg 08/22/19 19:01 75-35-408/22/19 13:595.3 1.2 1
cis-1,2-Dichloroethene ND ug/kg 08/22/19 19:01 156-59-208/22/19 13:595.3 0.93 1
trans-1,2-Dichloroethene ND ug/kg 08/22/19 19:01 156-60-508/22/19 13:595.3 1.0 1
1,2-Dichloropropane ND ug/kg 08/22/19 19:01 78-87-508/22/19 13:595.3 2.0 1
1,3-Dichloropropane ND ug/kg 08/22/19 19:01 142-28-908/22/19 13:595.3 2.0 1
2,2-Dichloropropane ND ug/kg 08/22/19 19:01 594-20-708/22/19 13:595.3 0.53 1
1,1-Dichloropropene ND ug/kg 08/22/19 19:01 563-58-608/22/19 13:595.3 2.3 1
cis-1,3-Dichloropropene ND ug/kg 08/22/19 19:01 10061-01-508/22/19 13:595.3 2.4 1
trans-1,3-Dichloropropene ND ug/kg 08/22/19 19:01 10061-02-608/22/19 13:595.3 0.93 1
Diisopropyl ether ND ug/kg 08/22/19 19:01 108-20-308/22/19 13:595.3 3.1 1
Ethylbenzene ND ug/kg 08/22/19 19:01 100-41-408/22/19 13:595.3 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 19:01 87-68-308/22/19 13:595.3 2.6 1
2-Hexanone ND ug/kg 08/22/19 19:01 591-78-608/22/19 13:5953.4 5.5 1
Isopropylbenzene (Cumene)ND ug/kg 08/22/19 19:01 98-82-808/22/19 13:595.3 1.5 1
p-Isopropyltoluene ND ug/kg 08/22/19 19:01 99-87-608/22/19 13:595.3 2.6 1
Methylene Chloride ND ug/kg 08/22/19 19:01 75-09-208/22/19 13:5921.4 6.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/22/19 19:01 108-10-108/22/19 13:5953.4 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: B-2 Lab ID: 92442356004 Collected: 08/20/19 15:45 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/22/19 19:01 1634-04-408/22/19 13:595.3 3.1 1
Naphthalene ND ug/kg 08/22/19 19:01 91-20-308/22/19 13:595.3 4.5 1
n-Propylbenzene ND ug/kg 08/22/19 19:01 103-65-108/22/19 13:595.3 1.8 1
Styrene ND ug/kg 08/22/19 19:01 100-42-508/22/19 13:595.3 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/22/19 19:01 630-20-608/22/19 13:595.3 1.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/22/19 19:01 79-34-508/22/19 13:595.3 1.8 1
Tetrachloroethene ND ug/kg 08/22/19 19:01 127-18-408/22/19 13:595.3 1.7 1
Toluene ND ug/kg 08/22/19 19:01 108-88-308/22/19 13:595.3 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 08/22/19 19:01 87-61-608/22/19 13:595.3 3.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 19:01 120-82-108/22/19 13:595.3 2.8 1
1,1,1-Trichloroethane ND ug/kg 08/22/19 19:01 71-55-608/22/19 13:595.3 0.93 1
1,1,2-Trichloroethane ND ug/kg 08/22/19 19:01 79-00-508/22/19 13:595.3 1.2 1
Trichloroethene ND ug/kg 08/22/19 19:01 79-01-608/22/19 13:595.3 1.4 1
Trichlorofluoromethane ND ug/kg 08/22/19 19:01 75-69-408/22/19 13:595.3 1.3 1
1,2,3-Trichloropropane ND ug/kg 08/22/19 19:01 96-18-408/22/19 13:595.3 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 08/22/19 19:01 95-63-608/22/19 13:595.3 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 08/22/19 19:01 108-67-808/22/19 13:595.3 1.8 1
Vinyl acetate ND ug/kg 08/22/19 19:01 108-05-408/22/19 13:5953.4 17.4 1
Vinyl chloride ND ug/kg 08/22/19 19:01 75-01-408/22/19 13:5910.7 2.0 1
Xylene (Total)ND ug/kg 08/22/19 19:01 1330-20-708/22/19 13:5910.7 3.7 1
m&p-Xylene ND ug/kg 08/22/19 19:01 179601-23-108/22/19 13:5910.7 2.5 1
o-Xylene ND ug/kg 08/22/19 19:01 95-47-608/22/19 13:595.3 1.2 1
Surrogates
Toluene-d8 (S)108 %08/22/19 19:01 2037-26-508/22/19 13:5970-130 1
4-Bromofluorobenzene (S)103 %08/22/19 19:01 460-00-408/22/19 13:5970-130 1
1,2-Dichloroethane-d4 (S)94 %08/22/19 19:01 17060-07-008/22/19 13:5970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.7 %08/23/19 12:510.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: C-2 Lab ID: 92442356005 Collected: 08/19/19 16:20 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 08/22/19 19:26 67-64-108/22/19 13:59100 9.5 1
Benzene ND ug/kg 08/22/19 19:26 71-43-208/22/19 13:595.0 0.90 1
Bromobenzene ND ug/kg 08/22/19 19:26 108-86-108/22/19 13:595.0 1.4 1
Bromochloromethane ND ug/kg 08/22/19 19:26 74-97-508/22/19 13:595.0 1.2 1
Bromodichloromethane ND ug/kg 08/22/19 19:26 75-27-408/22/19 13:595.0 0.98 1
Bromoform ND ug/kg 08/22/19 19:26 75-25-208/22/19 13:595.0 2.4 1
Bromomethane ND ug/kg 08/22/19 19:26 74-83-908/22/19 13:5910.0 2.4 1
2-Butanone (MEK)ND ug/kg 08/22/19 19:26 78-93-308/22/19 13:59100 11.9 1
n-Butylbenzene ND ug/kg 08/22/19 19:26 104-51-808/22/19 13:595.0 2.8 1
sec-Butylbenzene ND ug/kg 08/22/19 19:26 135-98-808/22/19 13:595.0 2.1 1
tert-Butylbenzene ND ug/kg 08/22/19 19:26 98-06-608/22/19 13:595.0 1.7 1
Carbon tetrachloride ND ug/kg 08/22/19 19:26 56-23-508/22/19 13:595.0 0.96 1
Chlorobenzene ND ug/kg 08/22/19 19:26 108-90-708/22/19 13:595.0 0.97 1
Chloroethane ND ug/kg 08/22/19 19:26 75-00-308/22/19 13:5910.0 2.1 1
Chloroform ND ug/kg 08/22/19 19:26 67-66-308/22/19 13:595.0 1.1 1
Chloromethane ND ug/kg 08/22/19 19:26 74-87-308/22/19 13:5910.0 3.3 1
2-Chlorotoluene ND ug/kg 08/22/19 19:26 95-49-808/22/19 13:595.0 1.5 1
4-Chlorotoluene ND ug/kg 08/22/19 19:26 106-43-408/22/19 13:595.0 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/22/19 19:26 96-12-808/22/19 13:595.0 2.5 1
Dibromochloromethane ND ug/kg 08/22/19 19:26 124-48-108/22/19 13:595.0 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 08/22/19 19:26 106-93-408/22/19 13:595.0 1.1 1
Dibromomethane ND ug/kg 08/22/19 19:26 74-95-308/22/19 13:595.0 1.5 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 19:26 95-50-108/22/19 13:595.0 1.8 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 19:26 541-73-108/22/19 13:595.0 1.8 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 19:26 106-46-708/22/19 13:595.0 1.7 1
Dichlorodifluoromethane ND ug/kg 08/22/19 19:26 75-71-808/22/19 13:5910.0 4.1 1
1,1-Dichloroethane ND ug/kg 08/22/19 19:26 75-34-308/22/19 13:595.0 0.74 1
1,2-Dichloroethane ND ug/kg 08/22/19 19:26 107-06-208/22/19 13:595.0 1.0 1
1,1-Dichloroethene ND ug/kg 08/22/19 19:26 75-35-408/22/19 13:595.0 1.2 1
cis-1,2-Dichloroethene ND ug/kg 08/22/19 19:26 156-59-208/22/19 13:595.0 0.87 1
trans-1,2-Dichloroethene ND ug/kg 08/22/19 19:26 156-60-508/22/19 13:595.0 0.98 1
1,2-Dichloropropane ND ug/kg 08/22/19 19:26 78-87-508/22/19 13:595.0 1.9 1
1,3-Dichloropropane ND ug/kg 08/22/19 19:26 142-28-908/22/19 13:595.0 1.9 1
2,2-Dichloropropane ND ug/kg 08/22/19 19:26 594-20-708/22/19 13:595.0 0.50 1
1,1-Dichloropropene ND ug/kg 08/22/19 19:26 563-58-608/22/19 13:595.0 2.1 1
cis-1,3-Dichloropropene ND ug/kg 08/22/19 19:26 10061-01-508/22/19 13:595.0 2.3 1
trans-1,3-Dichloropropene ND ug/kg 08/22/19 19:26 10061-02-608/22/19 13:595.0 0.88 1
Diisopropyl ether ND ug/kg 08/22/19 19:26 108-20-308/22/19 13:595.0 2.9 1
Ethylbenzene ND ug/kg 08/22/19 19:26 100-41-408/22/19 13:595.0 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 19:26 87-68-308/22/19 13:595.0 2.5 1
2-Hexanone ND ug/kg 08/22/19 19:26 591-78-608/22/19 13:5950.1 5.2 1
Isopropylbenzene (Cumene)ND ug/kg 08/22/19 19:26 98-82-808/22/19 13:595.0 1.5 1
p-Isopropyltoluene ND ug/kg 08/22/19 19:26 99-87-608/22/19 13:595.0 2.4 1
Methylene Chloride ND ug/kg 08/22/19 19:26 75-09-208/22/19 13:5920.1 5.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/22/19 19:26 108-10-108/22/19 13:5950.1 3.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: C-2 Lab ID: 92442356005 Collected: 08/19/19 16:20 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/22/19 19:26 1634-04-408/22/19 13:595.0 2.9 1
Naphthalene ND ug/kg 08/22/19 19:26 91-20-308/22/19 13:595.0 4.3 1
n-Propylbenzene ND ug/kg 08/22/19 19:26 103-65-108/22/19 13:595.0 1.7 1
Styrene ND ug/kg 08/22/19 19:26 100-42-508/22/19 13:595.0 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/22/19 19:26 630-20-608/22/19 13:595.0 1.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/22/19 19:26 79-34-508/22/19 13:595.0 1.7 1
Tetrachloroethene ND ug/kg 08/22/19 19:26 127-18-408/22/19 13:595.0 1.6 1
Toluene ND ug/kg 08/22/19 19:26 108-88-308/22/19 13:595.0 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 08/22/19 19:26 87-61-608/22/19 13:595.0 3.6 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 19:26 120-82-108/22/19 13:595.0 2.7 1
1,1,1-Trichloroethane ND ug/kg 08/22/19 19:26 71-55-608/22/19 13:595.0 0.87 1
1,1,2-Trichloroethane ND ug/kg 08/22/19 19:26 79-00-508/22/19 13:595.0 1.1 1
Trichloroethene ND ug/kg 08/22/19 19:26 79-01-608/22/19 13:595.0 1.3 1
Trichlorofluoromethane ND ug/kg 08/22/19 19:26 75-69-408/22/19 13:595.0 1.2 1
1,2,3-Trichloropropane ND ug/kg 08/22/19 19:26 96-18-408/22/19 13:595.0 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 08/22/19 19:26 95-63-608/22/19 13:595.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 08/22/19 19:26 108-67-808/22/19 13:595.0 1.7 1
Vinyl acetate ND ug/kg 08/22/19 19:26 108-05-408/22/19 13:5950.1 16.3 1
Vinyl chloride ND ug/kg 08/22/19 19:26 75-01-408/22/19 13:5910.0 1.9 1
Xylene (Total)ND ug/kg 08/22/19 19:26 1330-20-708/22/19 13:5910.0 3.5 1
m&p-Xylene ND ug/kg 08/22/19 19:26 179601-23-108/22/19 13:5910.0 2.4 1
o-Xylene ND ug/kg 08/22/19 19:26 95-47-608/22/19 13:595.0 1.2 1
Surrogates
Toluene-d8 (S)107 %08/22/19 19:26 2037-26-508/22/19 13:5970-130 1
4-Bromofluorobenzene (S)105 %08/22/19 19:26 460-00-408/22/19 13:5970-130 1
1,2-Dichloroethane-d4 (S)105 %08/22/19 19:26 17060-07-008/22/19 13:5970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.3 %08/23/19 12:510.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: C-3 Lab ID: 92442356006 Collected: 08/19/19 16:00 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 72.7J ug/kg 08/23/19 13:32 67-64-1 B,v108/23/19 12:4990.1 8.5 1
Benzene 1.3J ug/kg 08/23/19 13:32 71-43-208/23/19 12:494.5 0.81 1
Bromobenzene ND ug/kg 08/23/19 13:32 108-86-108/23/19 12:494.5 1.2 1
Bromochloromethane ND ug/kg 08/23/19 13:32 74-97-508/23/19 12:494.5 1.1 1
Bromodichloromethane ND ug/kg 08/23/19 13:32 75-27-408/23/19 12:494.5 0.88 1
Bromoform ND ug/kg 08/23/19 13:32 75-25-208/23/19 12:494.5 2.2 1
Bromomethane ND ug/kg 08/23/19 13:32 74-83-9 v108/23/19 12:499.0 2.1 1
2-Butanone (MEK)ND ug/kg 08/23/19 13:32 78-93-308/23/19 12:4990.1 10.7 1
n-Butylbenzene ND ug/kg 08/23/19 13:32 104-51-808/23/19 12:494.5 2.5 1
sec-Butylbenzene ND ug/kg 08/23/19 13:32 135-98-808/23/19 12:494.5 1.9 1
tert-Butylbenzene ND ug/kg 08/23/19 13:32 98-06-608/23/19 12:494.5 1.5 1
Carbon tetrachloride ND ug/kg 08/23/19 13:32 56-23-508/23/19 12:494.5 0.86 1
Chlorobenzene ND ug/kg 08/23/19 13:32 108-90-708/23/19 12:494.5 0.87 1
Chloroethane ND ug/kg 08/23/19 13:32 75-00-308/23/19 12:499.0 1.9 1
Chloroform ND ug/kg 08/23/19 13:32 67-66-308/23/19 12:494.5 0.96 1
Chloromethane ND ug/kg 08/23/19 13:32 74-87-3 v108/23/19 12:499.0 3.0 1
2-Chlorotoluene ND ug/kg 08/23/19 13:32 95-49-808/23/19 12:494.5 1.4 1
4-Chlorotoluene ND ug/kg 08/23/19 13:32 106-43-408/23/19 12:494.5 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/23/19 13:32 96-12-808/23/19 12:494.5 2.3 1
Dibromochloromethane ND ug/kg 08/23/19 13:32 124-48-108/23/19 12:494.5 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 08/23/19 13:32 106-93-408/23/19 12:494.5 1.0 1
Dibromomethane ND ug/kg 08/23/19 13:32 74-95-308/23/19 12:494.5 1.3 1
1,2-Dichlorobenzene ND ug/kg 08/23/19 13:32 95-50-108/23/19 12:494.5 1.6 1
1,3-Dichlorobenzene ND ug/kg 08/23/19 13:32 541-73-108/23/19 12:494.5 1.6 1
1,4-Dichlorobenzene ND ug/kg 08/23/19 13:32 106-46-708/23/19 12:494.5 1.6 1
Dichlorodifluoromethane ND ug/kg 08/23/19 13:32 75-71-808/23/19 12:499.0 3.7 1
1,1-Dichloroethane ND ug/kg 08/23/19 13:32 75-34-308/23/19 12:494.5 0.66 1
1,2-Dichloroethane ND ug/kg 08/23/19 13:32 107-06-208/23/19 12:494.5 0.90 1
1,1-Dichloroethene ND ug/kg 08/23/19 13:32 75-35-408/23/19 12:494.5 1.0 1
cis-1,2-Dichloroethene ND ug/kg 08/23/19 13:32 156-59-208/23/19 12:494.5 0.78 1
trans-1,2-Dichloroethene ND ug/kg 08/23/19 13:32 156-60-508/23/19 12:494.5 0.88 1
1,2-Dichloropropane ND ug/kg 08/23/19 13:32 78-87-508/23/19 12:494.5 1.7 1
1,3-Dichloropropane ND ug/kg 08/23/19 13:32 142-28-908/23/19 12:494.5 1.7 1
2,2-Dichloropropane ND ug/kg 08/23/19 13:32 594-20-708/23/19 12:494.5 0.45 1
1,1-Dichloropropene ND ug/kg 08/23/19 13:32 563-58-608/23/19 12:494.5 1.9 1
cis-1,3-Dichloropropene ND ug/kg 08/23/19 13:32 10061-01-508/23/19 12:494.5 2.0 1
trans-1,3-Dichloropropene ND ug/kg 08/23/19 13:32 10061-02-608/23/19 12:494.5 0.79 1
Diisopropyl ether ND ug/kg 08/23/19 13:32 108-20-308/23/19 12:494.5 2.6 1
Ethylbenzene ND ug/kg 08/23/19 13:32 100-41-408/23/19 12:494.5 0.96 1
Hexachloro-1,3-butadiene ND ug/kg 08/23/19 13:32 87-68-308/23/19 12:494.5 2.2 1
2-Hexanone ND ug/kg 08/23/19 13:32 591-78-6 v108/23/19 12:4945.1 4.7 1
Isopropylbenzene (Cumene)ND ug/kg 08/23/19 13:32 98-82-808/23/19 12:494.5 1.3 1
p-Isopropyltoluene ND ug/kg 08/23/19 13:32 99-87-608/23/19 12:494.5 2.2 1
Methylene Chloride ND ug/kg 08/23/19 13:32 75-09-208/23/19 12:4918.0 5.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/23/19 13:32 108-10-108/23/19 12:4945.1 3.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: C-3 Lab ID: 92442356006 Collected: 08/19/19 16:00 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/23/19 13:32 1634-04-408/23/19 12:494.5 2.6 1
Naphthalene ND ug/kg 08/23/19 13:32 91-20-308/23/19 12:494.5 3.8 1
n-Propylbenzene ND ug/kg 08/23/19 13:32 103-65-108/23/19 12:494.5 1.5 1
Styrene ND ug/kg 08/23/19 13:32 100-42-508/23/19 12:494.5 1.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/23/19 13:32 630-20-608/23/19 12:494.5 1.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/23/19 13:32 79-34-508/23/19 12:494.5 1.6 1
Tetrachloroethene ND ug/kg 08/23/19 13:32 127-18-408/23/19 12:494.5 1.4 1
Toluene ND ug/kg 08/23/19 13:32 108-88-308/23/19 12:494.5 1.5 1
1,2,3-Trichlorobenzene ND ug/kg 08/23/19 13:32 87-61-608/23/19 12:494.5 3.2 1
1,2,4-Trichlorobenzene ND ug/kg 08/23/19 13:32 120-82-108/23/19 12:494.5 2.4 1
1,1,1-Trichloroethane ND ug/kg 08/23/19 13:32 71-55-608/23/19 12:494.5 0.78 1
1,1,2-Trichloroethane ND ug/kg 08/23/19 13:32 79-00-508/23/19 12:494.5 1.0 1
Trichloroethene ND ug/kg 08/23/19 13:32 79-01-608/23/19 12:494.5 1.2 1
Trichlorofluoromethane ND ug/kg 08/23/19 13:32 75-69-408/23/19 12:494.5 1.1 1
1,2,3-Trichloropropane ND ug/kg 08/23/19 13:32 96-18-408/23/19 12:494.5 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 08/23/19 13:32 95-63-608/23/19 12:494.5 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/23/19 13:32 108-67-808/23/19 12:494.5 1.5 1
Vinyl acetate ND ug/kg 08/23/19 13:32 108-05-4 v108/23/19 12:4945.1 14.7 1
Vinyl chloride ND ug/kg 08/23/19 13:32 75-01-408/23/19 12:499.0 1.7 1
Xylene (Total)ND ug/kg 08/23/19 13:32 1330-20-708/23/19 12:499.0 3.2 1
m&p-Xylene ND ug/kg 08/23/19 13:32 179601-23-108/23/19 12:499.0 2.1 1
o-Xylene ND ug/kg 08/23/19 13:32 95-47-608/23/19 12:494.5 1.1 1
Surrogates
Toluene-d8 (S)101 %08/23/19 13:32 2037-26-508/23/19 12:4970-130 1
4-Bromofluorobenzene (S)106 %08/23/19 13:32 460-00-408/23/19 12:4970-130 1
1,2-Dichloroethane-d4 (S)103 %08/23/19 13:32 17060-07-008/23/19 12:4970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.0 %08/23/19 12:510.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: D-1 Lab ID: 92442356007 Collected: 08/19/19 16:30 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 17.7J ug/kg 08/23/19 13:57 67-64-1 B,v108/23/19 12:4994.9 9.0 1
Benzene ND ug/kg 08/23/19 13:57 71-43-208/23/19 12:494.7 0.85 1
Bromobenzene ND ug/kg 08/23/19 13:57 108-86-108/23/19 12:494.7 1.3 1
Bromochloromethane ND ug/kg 08/23/19 13:57 74-97-508/23/19 12:494.7 1.2 1
Bromodichloromethane ND ug/kg 08/23/19 13:57 75-27-408/23/19 12:494.7 0.93 1
Bromoform ND ug/kg 08/23/19 13:57 75-25-208/23/19 12:494.7 2.3 1
Bromomethane ND ug/kg 08/23/19 13:57 74-83-9 v108/23/19 12:499.5 2.2 1
2-Butanone (MEK)ND ug/kg 08/23/19 13:57 78-93-308/23/19 12:4994.9 11.3 1
n-Butylbenzene ND ug/kg 08/23/19 13:57 104-51-808/23/19 12:494.7 2.7 1
sec-Butylbenzene ND ug/kg 08/23/19 13:57 135-98-808/23/19 12:494.7 2.0 1
tert-Butylbenzene ND ug/kg 08/23/19 13:57 98-06-608/23/19 12:494.7 1.6 1
Carbon tetrachloride ND ug/kg 08/23/19 13:57 56-23-508/23/19 12:494.7 0.91 1
Chlorobenzene ND ug/kg 08/23/19 13:57 108-90-708/23/19 12:494.7 0.92 1
Chloroethane ND ug/kg 08/23/19 13:57 75-00-308/23/19 12:499.5 2.0 1
Chloroform ND ug/kg 08/23/19 13:57 67-66-308/23/19 12:494.7 1.0 1
Chloromethane ND ug/kg 08/23/19 13:57 74-87-3 v108/23/19 12:499.5 3.1 1
2-Chlorotoluene ND ug/kg 08/23/19 13:57 95-49-808/23/19 12:494.7 1.4 1
4-Chlorotoluene ND ug/kg 08/23/19 13:57 106-43-408/23/19 12:494.7 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/23/19 13:57 96-12-808/23/19 12:494.7 2.4 1
Dibromochloromethane ND ug/kg 08/23/19 13:57 124-48-108/23/19 12:494.7 2.4 1
1,2-Dibromoethane (EDB)ND ug/kg 08/23/19 13:57 106-93-408/23/19 12:494.7 1.1 1
Dibromomethane ND ug/kg 08/23/19 13:57 74-95-308/23/19 12:494.7 1.4 1
1,2-Dichlorobenzene ND ug/kg 08/23/19 13:57 95-50-108/23/19 12:494.7 1.7 1
1,3-Dichlorobenzene ND ug/kg 08/23/19 13:57 541-73-108/23/19 12:494.7 1.7 1
1,4-Dichlorobenzene ND ug/kg 08/23/19 13:57 106-46-708/23/19 12:494.7 1.6 1
Dichlorodifluoromethane ND ug/kg 08/23/19 13:57 75-71-808/23/19 12:499.5 3.9 1
1,1-Dichloroethane ND ug/kg 08/23/19 13:57 75-34-308/23/19 12:494.7 0.70 1
1,2-Dichloroethane ND ug/kg 08/23/19 13:57 107-06-208/23/19 12:494.7 0.95 1
1,1-Dichloroethene ND ug/kg 08/23/19 13:57 75-35-408/23/19 12:494.7 1.1 1
cis-1,2-Dichloroethene ND ug/kg 08/23/19 13:57 156-59-208/23/19 12:494.7 0.82 1
trans-1,2-Dichloroethene ND ug/kg 08/23/19 13:57 156-60-508/23/19 12:494.7 0.93 1
1,2-Dichloropropane ND ug/kg 08/23/19 13:57 78-87-508/23/19 12:494.7 1.8 1
1,3-Dichloropropane ND ug/kg 08/23/19 13:57 142-28-908/23/19 12:494.7 1.8 1
2,2-Dichloropropane ND ug/kg 08/23/19 13:57 594-20-708/23/19 12:494.7 0.47 1
1,1-Dichloropropene ND ug/kg 08/23/19 13:57 563-58-608/23/19 12:494.7 2.0 1
cis-1,3-Dichloropropene ND ug/kg 08/23/19 13:57 10061-01-508/23/19 12:494.7 2.2 1
trans-1,3-Dichloropropene ND ug/kg 08/23/19 13:57 10061-02-608/23/19 12:494.7 0.83 1
Diisopropyl ether ND ug/kg 08/23/19 13:57 108-20-308/23/19 12:494.7 2.7 1
Ethylbenzene ND ug/kg 08/23/19 13:57 100-41-408/23/19 12:494.7 1.0 1
Hexachloro-1,3-butadiene ND ug/kg 08/23/19 13:57 87-68-308/23/19 12:494.7 2.3 1
2-Hexanone ND ug/kg 08/23/19 13:57 591-78-6 v108/23/19 12:4947.5 4.9 1
Isopropylbenzene (Cumene)ND ug/kg 08/23/19 13:57 98-82-808/23/19 12:494.7 1.4 1
p-Isopropyltoluene ND ug/kg 08/23/19 13:57 99-87-608/23/19 12:494.7 2.3 1
Methylene Chloride ND ug/kg 08/23/19 13:57 75-09-208/23/19 12:4919.0 5.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/23/19 13:57 108-10-108/23/19 12:4947.5 3.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: D-1 Lab ID: 92442356007 Collected: 08/19/19 16:30 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/23/19 13:57 1634-04-408/23/19 12:494.7 2.7 1
Naphthalene ND ug/kg 08/23/19 13:57 91-20-308/23/19 12:494.7 4.0 1
n-Propylbenzene ND ug/kg 08/23/19 13:57 103-65-108/23/19 12:494.7 1.6 1
Styrene ND ug/kg 08/23/19 13:57 100-42-508/23/19 12:494.7 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/23/19 13:57 630-20-608/23/19 12:494.7 1.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/23/19 13:57 79-34-508/23/19 12:494.7 1.6 1
Tetrachloroethene ND ug/kg 08/23/19 13:57 127-18-408/23/19 12:494.7 1.5 1
Toluene ND ug/kg 08/23/19 13:57 108-88-308/23/19 12:494.7 1.5 1
1,2,3-Trichlorobenzene ND ug/kg 08/23/19 13:57 87-61-608/23/19 12:494.7 3.4 1
1,2,4-Trichlorobenzene ND ug/kg 08/23/19 13:57 120-82-108/23/19 12:494.7 2.5 1
1,1,1-Trichloroethane ND ug/kg 08/23/19 13:57 71-55-608/23/19 12:494.7 0.83 1
1,1,2-Trichloroethane ND ug/kg 08/23/19 13:57 79-00-508/23/19 12:494.7 1.1 1
Trichloroethene ND ug/kg 08/23/19 13:57 79-01-608/23/19 12:494.7 1.2 1
Trichlorofluoromethane ND ug/kg 08/23/19 13:57 75-69-408/23/19 12:494.7 1.1 1
1,2,3-Trichloropropane ND ug/kg 08/23/19 13:57 96-18-408/23/19 12:494.7 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 08/23/19 13:57 95-63-608/23/19 12:494.7 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 08/23/19 13:57 108-67-808/23/19 12:494.7 1.6 1
Vinyl acetate ND ug/kg 08/23/19 13:57 108-05-4 v108/23/19 12:4947.5 15.5 1
Vinyl chloride ND ug/kg 08/23/19 13:57 75-01-408/23/19 12:499.5 1.8 1
Xylene (Total)ND ug/kg 08/23/19 13:57 1330-20-708/23/19 12:499.5 3.3 1
m&p-Xylene ND ug/kg 08/23/19 13:57 179601-23-108/23/19 12:499.5 2.2 1
o-Xylene ND ug/kg 08/23/19 13:57 95-47-608/23/19 12:494.7 1.1 1
Surrogates
Toluene-d8 (S)99 %08/23/19 13:57 2037-26-508/23/19 12:4970-130 1
4-Bromofluorobenzene (S)108 %08/23/19 13:57 460-00-408/23/19 12:4970-130 1
1,2-Dichloroethane-d4 (S)101 %08/23/19 13:57 17060-07-008/23/19 12:4970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.1 %08/23/19 12:510.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: D-4 Lab ID: 92442356008 Collected: 08/19/19 16:40 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 08/23/19 14:22 67-64-1 v108/23/19 12:4993.2 8.8 1
Benzene ND ug/kg 08/23/19 14:22 71-43-208/23/19 12:494.7 0.84 1
Bromobenzene ND ug/kg 08/23/19 14:22 108-86-108/23/19 12:494.7 1.3 1
Bromochloromethane ND ug/kg 08/23/19 14:22 74-97-508/23/19 12:494.7 1.1 1
Bromodichloromethane ND ug/kg 08/23/19 14:22 75-27-408/23/19 12:494.7 0.91 1
Bromoform ND ug/kg 08/23/19 14:22 75-25-208/23/19 12:494.7 2.3 1
Bromomethane ND ug/kg 08/23/19 14:22 74-83-9 v108/23/19 12:499.3 2.2 1
2-Butanone (MEK)ND ug/kg 08/23/19 14:22 78-93-308/23/19 12:4993.2 11.1 1
n-Butylbenzene ND ug/kg 08/23/19 14:22 104-51-808/23/19 12:494.7 2.6 1
sec-Butylbenzene ND ug/kg 08/23/19 14:22 135-98-808/23/19 12:494.7 2.0 1
tert-Butylbenzene ND ug/kg 08/23/19 14:22 98-06-608/23/19 12:494.7 1.6 1
Carbon tetrachloride ND ug/kg 08/23/19 14:22 56-23-508/23/19 12:494.7 0.89 1
Chlorobenzene ND ug/kg 08/23/19 14:22 108-90-708/23/19 12:494.7 0.90 1
Chloroethane ND ug/kg 08/23/19 14:22 75-00-308/23/19 12:499.3 1.9 1
Chloroform ND ug/kg 08/23/19 14:22 67-66-308/23/19 12:494.7 0.99 1
Chloromethane ND ug/kg 08/23/19 14:22 74-87-3 v108/23/19 12:499.3 3.1 1
2-Chlorotoluene ND ug/kg 08/23/19 14:22 95-49-808/23/19 12:494.7 1.4 1
4-Chlorotoluene ND ug/kg 08/23/19 14:22 106-43-408/23/19 12:494.7 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/23/19 14:22 96-12-808/23/19 12:494.7 2.4 1
Dibromochloromethane ND ug/kg 08/23/19 14:22 124-48-108/23/19 12:494.7 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 08/23/19 14:22 106-93-408/23/19 12:494.7 1.0 1
Dibromomethane ND ug/kg 08/23/19 14:22 74-95-308/23/19 12:494.7 1.4 1
1,2-Dichlorobenzene ND ug/kg 08/23/19 14:22 95-50-108/23/19 12:494.7 1.6 1
1,3-Dichlorobenzene ND ug/kg 08/23/19 14:22 541-73-108/23/19 12:494.7 1.7 1
1,4-Dichlorobenzene ND ug/kg 08/23/19 14:22 106-46-708/23/19 12:494.7 1.6 1
Dichlorodifluoromethane ND ug/kg 08/23/19 14:22 75-71-808/23/19 12:499.3 3.8 1
1,1-Dichloroethane ND ug/kg 08/23/19 14:22 75-34-308/23/19 12:494.7 0.68 1
1,2-Dichloroethane ND ug/kg 08/23/19 14:22 107-06-208/23/19 12:494.7 0.93 1
1,1-Dichloroethene ND ug/kg 08/23/19 14:22 75-35-408/23/19 12:494.7 1.1 1
cis-1,2-Dichloroethene ND ug/kg 08/23/19 14:22 156-59-208/23/19 12:494.7 0.81 1
trans-1,2-Dichloroethene ND ug/kg 08/23/19 14:22 156-60-508/23/19 12:494.7 0.91 1
1,2-Dichloropropane ND ug/kg 08/23/19 14:22 78-87-508/23/19 12:494.7 1.8 1
1,3-Dichloropropane ND ug/kg 08/23/19 14:22 142-28-908/23/19 12:494.7 1.8 1
2,2-Dichloropropane ND ug/kg 08/23/19 14:22 594-20-708/23/19 12:494.7 0.46 1
1,1-Dichloropropene ND ug/kg 08/23/19 14:22 563-58-608/23/19 12:494.7 2.0 1
cis-1,3-Dichloropropene ND ug/kg 08/23/19 14:22 10061-01-508/23/19 12:494.7 2.1 1
trans-1,3-Dichloropropene ND ug/kg 08/23/19 14:22 10061-02-608/23/19 12:494.7 0.82 1
Diisopropyl ether ND ug/kg 08/23/19 14:22 108-20-308/23/19 12:494.7 2.7 1
Ethylbenzene ND ug/kg 08/23/19 14:22 100-41-408/23/19 12:494.7 0.99 1
Hexachloro-1,3-butadiene ND ug/kg 08/23/19 14:22 87-68-308/23/19 12:494.7 2.3 1
2-Hexanone ND ug/kg 08/23/19 14:22 591-78-6 v108/23/19 12:4946.6 4.8 1
Isopropylbenzene (Cumene)ND ug/kg 08/23/19 14:22 98-82-808/23/19 12:494.7 1.4 1
p-Isopropyltoluene ND ug/kg 08/23/19 14:22 99-87-608/23/19 12:494.7 2.2 1
Methylene Chloride ND ug/kg 08/23/19 14:22 75-09-208/23/19 12:4918.6 5.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/23/19 14:22 108-10-108/23/19 12:4946.6 3.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: D-4 Lab ID: 92442356008 Collected: 08/19/19 16:40 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/23/19 14:22 1634-04-408/23/19 12:494.7 2.7 1
Naphthalene ND ug/kg 08/23/19 14:22 91-20-308/23/19 12:494.7 4.0 1
n-Propylbenzene ND ug/kg 08/23/19 14:22 103-65-108/23/19 12:494.7 1.6 1
Styrene ND ug/kg 08/23/19 14:22 100-42-508/23/19 12:494.7 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/23/19 14:22 630-20-608/23/19 12:494.7 1.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/23/19 14:22 79-34-508/23/19 12:494.7 1.6 1
Tetrachloroethene ND ug/kg 08/23/19 14:22 127-18-408/23/19 12:494.7 1.5 1
Toluene ND ug/kg 08/23/19 14:22 108-88-308/23/19 12:494.7 1.5 1
1,2,3-Trichlorobenzene ND ug/kg 08/23/19 14:22 87-61-608/23/19 12:494.7 3.3 1
1,2,4-Trichlorobenzene ND ug/kg 08/23/19 14:22 120-82-108/23/19 12:494.7 2.5 1
1,1,1-Trichloroethane ND ug/kg 08/23/19 14:22 71-55-608/23/19 12:494.7 0.81 1
1,1,2-Trichloroethane ND ug/kg 08/23/19 14:22 79-00-508/23/19 12:494.7 1.1 1
Trichloroethene ND ug/kg 08/23/19 14:22 79-01-608/23/19 12:494.7 1.2 1
Trichlorofluoromethane ND ug/kg 08/23/19 14:22 75-69-408/23/19 12:494.7 1.1 1
1,2,3-Trichloropropane ND ug/kg 08/23/19 14:22 96-18-408/23/19 12:494.7 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 08/23/19 14:22 95-63-608/23/19 12:494.7 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 08/23/19 14:22 108-67-808/23/19 12:494.7 1.6 1
Vinyl acetate ND ug/kg 08/23/19 14:22 108-05-4 v108/23/19 12:4946.6 15.2 1
Vinyl chloride ND ug/kg 08/23/19 14:22 75-01-408/23/19 12:499.3 1.8 1
Xylene (Total)ND ug/kg 08/23/19 14:22 1330-20-708/23/19 12:499.3 3.3 1
m&p-Xylene ND ug/kg 08/23/19 14:22 179601-23-108/23/19 12:499.3 2.2 1
o-Xylene ND ug/kg 08/23/19 14:22 95-47-608/23/19 12:494.7 1.1 1
Surrogates
Toluene-d8 (S)100 %08/23/19 14:22 2037-26-508/23/19 12:4970-130 1
4-Bromofluorobenzene (S)105 %08/23/19 14:22 460-00-408/23/19 12:4970-130 1
1,2-Dichloroethane-d4 (S)100 %08/23/19 14:22 17060-07-008/23/19 12:4970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.1 %08/22/19 16:530.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: E-3 Lab ID: 92442356009 Collected: 08/20/19 15:50 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 08/22/19 19:50 67-64-108/22/19 13:5987.1 8.2 1
Benzene ND ug/kg 08/22/19 19:50 71-43-208/22/19 13:594.4 0.78 1
Bromobenzene ND ug/kg 08/22/19 19:50 108-86-108/22/19 13:594.4 1.2 1
Bromochloromethane ND ug/kg 08/22/19 19:50 74-97-508/22/19 13:594.4 1.1 1
Bromodichloromethane ND ug/kg 08/22/19 19:50 75-27-408/22/19 13:594.4 0.85 1
Bromoform ND ug/kg 08/22/19 19:50 75-25-208/22/19 13:594.4 2.1 1
Bromomethane ND ug/kg 08/22/19 19:50 74-83-908/22/19 13:598.7 2.1 1
2-Butanone (MEK)ND ug/kg 08/22/19 19:50 78-93-308/22/19 13:5987.1 10.4 1
n-Butylbenzene ND ug/kg 08/22/19 19:50 104-51-808/22/19 13:594.4 2.5 1
sec-Butylbenzene ND ug/kg 08/22/19 19:50 135-98-808/22/19 13:594.4 1.8 1
tert-Butylbenzene ND ug/kg 08/22/19 19:50 98-06-608/22/19 13:594.4 1.5 1
Carbon tetrachloride ND ug/kg 08/22/19 19:50 56-23-508/22/19 13:594.4 0.83 1
Chlorobenzene ND ug/kg 08/22/19 19:50 108-90-708/22/19 13:594.4 0.84 1
Chloroethane ND ug/kg 08/22/19 19:50 75-00-308/22/19 13:598.7 1.8 1
Chloroform ND ug/kg 08/22/19 19:50 67-66-308/22/19 13:594.4 0.92 1
Chloromethane ND ug/kg 08/22/19 19:50 74-87-308/22/19 13:598.7 2.9 1
2-Chlorotoluene ND ug/kg 08/22/19 19:50 95-49-808/22/19 13:594.4 1.3 1
4-Chlorotoluene ND ug/kg 08/22/19 19:50 106-43-408/22/19 13:594.4 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/22/19 19:50 96-12-808/22/19 13:594.4 2.2 1
Dibromochloromethane ND ug/kg 08/22/19 19:50 124-48-108/22/19 13:594.4 2.2 1
1,2-Dibromoethane (EDB)ND ug/kg 08/22/19 19:50 106-93-408/22/19 13:594.4 0.98 1
Dibromomethane ND ug/kg 08/22/19 19:50 74-95-308/22/19 13:594.4 1.3 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 19:50 95-50-108/22/19 13:594.4 1.5 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 19:50 541-73-108/22/19 13:594.4 1.6 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 19:50 106-46-708/22/19 13:594.4 1.5 1
Dichlorodifluoromethane ND ug/kg 08/22/19 19:50 75-71-808/22/19 13:598.7 3.6 1
1,1-Dichloroethane ND ug/kg 08/22/19 19:50 75-34-308/22/19 13:594.4 0.64 1
1,2-Dichloroethane ND ug/kg 08/22/19 19:50 107-06-208/22/19 13:594.4 0.87 1
1,1-Dichloroethene ND ug/kg 08/22/19 19:50 75-35-408/22/19 13:594.4 1.0 1
cis-1,2-Dichloroethene ND ug/kg 08/22/19 19:50 156-59-208/22/19 13:594.4 0.76 1
trans-1,2-Dichloroethene ND ug/kg 08/22/19 19:50 156-60-508/22/19 13:594.4 0.85 1
1,2-Dichloropropane ND ug/kg 08/22/19 19:50 78-87-508/22/19 13:594.4 1.6 1
1,3-Dichloropropane ND ug/kg 08/22/19 19:50 142-28-908/22/19 13:594.4 1.6 1
2,2-Dichloropropane ND ug/kg 08/22/19 19:50 594-20-708/22/19 13:594.4 0.43 1
1,1-Dichloropropene ND ug/kg 08/22/19 19:50 563-58-608/22/19 13:594.4 1.8 1
cis-1,3-Dichloropropene ND ug/kg 08/22/19 19:50 10061-01-508/22/19 13:594.4 2.0 1
trans-1,3-Dichloropropene ND ug/kg 08/22/19 19:50 10061-02-608/22/19 13:594.4 0.76 1
Diisopropyl ether ND ug/kg 08/22/19 19:50 108-20-308/22/19 13:594.4 2.5 1
Ethylbenzene ND ug/kg 08/22/19 19:50 100-41-408/22/19 13:594.4 0.92 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 19:50 87-68-308/22/19 13:594.4 2.2 1
2-Hexanone ND ug/kg 08/22/19 19:50 591-78-608/22/19 13:5943.6 4.5 1
Isopropylbenzene (Cumene)ND ug/kg 08/22/19 19:50 98-82-808/22/19 13:594.4 1.3 1
p-Isopropyltoluene ND ug/kg 08/22/19 19:50 99-87-608/22/19 13:594.4 2.1 1
Methylene Chloride ND ug/kg 08/22/19 19:50 75-09-208/22/19 13:5917.4 5.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/22/19 19:50 108-10-108/22/19 13:5943.6 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: E-3 Lab ID: 92442356009 Collected: 08/20/19 15:50 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/22/19 19:50 1634-04-408/22/19 13:594.4 2.5 1
Naphthalene ND ug/kg 08/22/19 19:50 91-20-308/22/19 13:594.4 3.7 1
n-Propylbenzene ND ug/kg 08/22/19 19:50 103-65-108/22/19 13:594.4 1.5 1
Styrene ND ug/kg 08/22/19 19:50 100-42-508/22/19 13:594.4 1.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/22/19 19:50 630-20-608/22/19 13:594.4 1.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/22/19 19:50 79-34-508/22/19 13:594.4 1.5 1
Tetrachloroethene ND ug/kg 08/22/19 19:50 127-18-408/22/19 13:594.4 1.4 1
Toluene ND ug/kg 08/22/19 19:50 108-88-308/22/19 13:594.4 1.4 1
1,2,3-Trichlorobenzene ND ug/kg 08/22/19 19:50 87-61-608/22/19 13:594.4 3.1 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 19:50 120-82-108/22/19 13:594.4 2.3 1
1,1,1-Trichloroethane ND ug/kg 08/22/19 19:50 71-55-608/22/19 13:594.4 0.76 1
1,1,2-Trichloroethane ND ug/kg 08/22/19 19:50 79-00-508/22/19 13:594.4 0.98 1
Trichloroethene ND ug/kg 08/22/19 19:50 79-01-608/22/19 13:594.4 1.1 1
Trichlorofluoromethane ND ug/kg 08/22/19 19:50 75-69-408/22/19 13:594.4 1.0 1
1,2,3-Trichloropropane ND ug/kg 08/22/19 19:50 96-18-408/22/19 13:594.4 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 08/22/19 19:50 95-63-608/22/19 13:594.4 1.7 1
1,3,5-Trimethylbenzene ND ug/kg 08/22/19 19:50 108-67-808/22/19 13:594.4 1.5 1
Vinyl acetate ND ug/kg 08/22/19 19:50 108-05-408/22/19 13:5943.6 14.2 1
Vinyl chloride ND ug/kg 08/22/19 19:50 75-01-408/22/19 13:598.7 1.7 1
Xylene (Total)ND ug/kg 08/22/19 19:50 1330-20-708/22/19 13:598.7 3.0 1
m&p-Xylene ND ug/kg 08/22/19 19:50 179601-23-108/22/19 13:598.7 2.1 1
o-Xylene ND ug/kg 08/22/19 19:50 95-47-608/22/19 13:594.4 1.0 1
Surrogates
Toluene-d8 (S)102 %08/22/19 19:50 2037-26-508/22/19 13:5970-130 1
4-Bromofluorobenzene (S)103 %08/22/19 19:50 460-00-408/22/19 13:5970-130 1
1,2-Dichloroethane-d4 (S)123 %08/22/19 19:50 17060-07-008/22/19 13:5970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.6 %08/22/19 16:580.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: E-5 Lab ID: 92442356010 Collected: 08/20/19 16:00 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 08/22/19 20:15 67-64-108/22/19 13:59106 10 1
Benzene ND ug/kg 08/22/19 20:15 71-43-208/22/19 13:595.3 0.95 1
Bromobenzene ND ug/kg 08/22/19 20:15 108-86-108/22/19 13:595.3 1.4 1
Bromochloromethane ND ug/kg 08/22/19 20:15 74-97-508/22/19 13:595.3 1.3 1
Bromodichloromethane ND ug/kg 08/22/19 20:15 75-27-408/22/19 13:595.3 1.0 1
Bromoform ND ug/kg 08/22/19 20:15 75-25-208/22/19 13:595.3 2.6 1
Bromomethane ND ug/kg 08/22/19 20:15 74-83-908/22/19 13:5910.6 2.5 1
2-Butanone (MEK)ND ug/kg 08/22/19 20:15 78-93-308/22/19 13:59106 12.6 1
n-Butylbenzene ND ug/kg 08/22/19 20:15 104-51-808/22/19 13:595.3 3.0 1
sec-Butylbenzene ND ug/kg 08/22/19 20:15 135-98-808/22/19 13:595.3 2.2 1
tert-Butylbenzene ND ug/kg 08/22/19 20:15 98-06-608/22/19 13:595.3 1.8 1
Carbon tetrachloride ND ug/kg 08/22/19 20:15 56-23-508/22/19 13:595.3 1.0 1
Chlorobenzene ND ug/kg 08/22/19 20:15 108-90-708/22/19 13:595.3 1.0 1
Chloroethane ND ug/kg 08/22/19 20:15 75-00-308/22/19 13:5910.6 2.2 1
Chloroform ND ug/kg 08/22/19 20:15 67-66-308/22/19 13:595.3 1.1 1
Chloromethane ND ug/kg 08/22/19 20:15 74-87-308/22/19 13:5910.6 3.5 1
2-Chlorotoluene ND ug/kg 08/22/19 20:15 95-49-808/22/19 13:595.3 1.6 1
4-Chlorotoluene ND ug/kg 08/22/19 20:15 106-43-408/22/19 13:595.3 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/22/19 20:15 96-12-808/22/19 13:595.3 2.7 1
Dibromochloromethane ND ug/kg 08/22/19 20:15 124-48-108/22/19 13:595.3 2.6 1
1,2-Dibromoethane (EDB)ND ug/kg 08/22/19 20:15 106-93-408/22/19 13:595.3 1.2 1
Dibromomethane ND ug/kg 08/22/19 20:15 74-95-308/22/19 13:595.3 1.6 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 20:15 95-50-108/22/19 13:595.3 1.9 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 20:15 541-73-108/22/19 13:595.3 1.9 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 20:15 106-46-708/22/19 13:595.3 1.8 1
Dichlorodifluoromethane ND ug/kg 08/22/19 20:15 75-71-808/22/19 13:5910.6 4.3 1
1,1-Dichloroethane ND ug/kg 08/22/19 20:15 75-34-308/22/19 13:595.3 0.78 1
1,2-Dichloroethane ND ug/kg 08/22/19 20:15 107-06-208/22/19 13:595.3 1.1 1
1,1-Dichloroethene ND ug/kg 08/22/19 20:15 75-35-408/22/19 13:595.3 1.2 1
cis-1,2-Dichloroethene ND ug/kg 08/22/19 20:15 156-59-208/22/19 13:595.3 0.92 1
trans-1,2-Dichloroethene ND ug/kg 08/22/19 20:15 156-60-508/22/19 13:595.3 1.0 1
1,2-Dichloropropane ND ug/kg 08/22/19 20:15 78-87-508/22/19 13:595.3 2.0 1
1,3-Dichloropropane ND ug/kg 08/22/19 20:15 142-28-908/22/19 13:595.3 2.0 1
2,2-Dichloropropane ND ug/kg 08/22/19 20:15 594-20-708/22/19 13:595.3 0.52 1
1,1-Dichloropropene ND ug/kg 08/22/19 20:15 563-58-608/22/19 13:595.3 2.2 1
cis-1,3-Dichloropropene ND ug/kg 08/22/19 20:15 10061-01-508/22/19 13:595.3 2.4 1
trans-1,3-Dichloropropene ND ug/kg 08/22/19 20:15 10061-02-608/22/19 13:595.3 0.93 1
Diisopropyl ether ND ug/kg 08/22/19 20:15 108-20-308/22/19 13:595.3 3.0 1
Ethylbenzene ND ug/kg 08/22/19 20:15 100-41-408/22/19 13:595.3 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 20:15 87-68-308/22/19 13:595.3 2.6 1
2-Hexanone ND ug/kg 08/22/19 20:15 591-78-608/22/19 13:5952.9 5.5 1
Isopropylbenzene (Cumene)ND ug/kg 08/22/19 20:15 98-82-808/22/19 13:595.3 1.5 1
p-Isopropyltoluene ND ug/kg 08/22/19 20:15 99-87-608/22/19 13:595.3 2.5 1
Methylene Chloride ND ug/kg 08/22/19 20:15 75-09-208/22/19 13:5921.2 6.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/22/19 20:15 108-10-108/22/19 13:5952.9 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: E-5 Lab ID: 92442356010 Collected: 08/20/19 16:00 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/22/19 20:15 1634-04-408/22/19 13:595.3 3.0 1
Naphthalene ND ug/kg 08/22/19 20:15 91-20-308/22/19 13:595.3 4.5 1
n-Propylbenzene ND ug/kg 08/22/19 20:15 103-65-108/22/19 13:595.3 1.8 1
Styrene ND ug/kg 08/22/19 20:15 100-42-508/22/19 13:595.3 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/22/19 20:15 630-20-608/22/19 13:595.3 1.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/22/19 20:15 79-34-508/22/19 13:595.3 1.8 1
Tetrachloroethene ND ug/kg 08/22/19 20:15 127-18-408/22/19 13:595.3 1.7 1
Toluene ND ug/kg 08/22/19 20:15 108-88-308/22/19 13:595.3 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 08/22/19 20:15 87-61-608/22/19 13:595.3 3.8 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 20:15 120-82-108/22/19 13:595.3 2.8 1
1,1,1-Trichloroethane ND ug/kg 08/22/19 20:15 71-55-608/22/19 13:595.3 0.92 1
1,1,2-Trichloroethane ND ug/kg 08/22/19 20:15 79-00-508/22/19 13:595.3 1.2 1
Trichloroethene ND ug/kg 08/22/19 20:15 79-01-608/22/19 13:595.3 1.4 1
Trichlorofluoromethane ND ug/kg 08/22/19 20:15 75-69-408/22/19 13:595.3 1.2 1
1,2,3-Trichloropropane ND ug/kg 08/22/19 20:15 96-18-408/22/19 13:595.3 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 08/22/19 20:15 95-63-608/22/19 13:595.3 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 08/22/19 20:15 108-67-808/22/19 13:595.3 1.8 1
Vinyl acetate ND ug/kg 08/22/19 20:15 108-05-408/22/19 13:5952.9 17.2 1
Vinyl chloride ND ug/kg 08/22/19 20:15 75-01-408/22/19 13:5910.6 2.0 1
Xylene (Total)ND ug/kg 08/22/19 20:15 1330-20-708/22/19 13:5910.6 3.7 1
m&p-Xylene ND ug/kg 08/22/19 20:15 179601-23-108/22/19 13:5910.6 2.5 1
o-Xylene ND ug/kg 08/22/19 20:15 95-47-608/22/19 13:595.3 1.2 1
Surrogates
Toluene-d8 (S)106 %08/22/19 20:15 2037-26-508/22/19 13:5970-130 1
4-Bromofluorobenzene (S)103 %08/22/19 20:15 460-00-408/22/19 13:5970-130 1
1,2-Dichloroethane-d4 (S)107 %08/22/19 20:15 17060-07-008/22/19 13:5970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.8 %08/22/19 16:580.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: A Lab ID: 92442356011 Collected: 08/20/19 16:05 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 0.45J mg/kg 08/23/19 10:22 7440-38-2 M108/22/19 11:480.67 0.33 1
Barium 91.7 mg/kg 08/23/19 10:22 7440-39-308/22/19 11:480.33 0.17 1
Cadmium 0.042J mg/kg 08/23/19 10:22 7440-43-908/22/19 11:480.067 0.033 1
Chromium 30.8 mg/kg 08/23/19 10:22 7440-47-308/22/19 11:480.33 0.17 1
Lead 3.6 mg/kg 08/23/19 10:22 7439-92-1 M108/22/19 11:480.33 0.17 1
Selenium 0.63J mg/kg 08/23/19 10:22 7782-49-2 M108/22/19 11:480.67 0.33 1
Silver ND mg/kg 08/23/19 10:22 7440-22-4 M108/22/19 11:480.33 0.17 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.023 mg/kg 08/26/19 14:02 7439-97-608/22/19 14:530.0051 0.0025 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 08/22/19 14:45 83-32-908/22/19 10:08360 92.7 1
Acenaphthylene ND ug/kg 08/22/19 14:45 208-96-808/22/19 10:08360 85.3 1
Aniline ND ug/kg 08/22/19 14:45 62-53-308/22/19 10:08360 80.9 1
Anthracene ND ug/kg 08/22/19 14:45 120-12-708/22/19 10:08360 93.5 1
Benzo(a)anthracene 116J ug/kg 08/22/19 14:45 56-55-308/22/19 10:08360 115 1
Benzo(a)pyrene ND ug/kg 08/22/19 14:45 50-32-808/22/19 10:08360 156 1
Benzo(b)fluoranthene 177J ug/kg 08/22/19 14:45 205-99-208/22/19 10:08360 145 1
Benzo(g,h,i)perylene ND ug/kg 08/22/19 14:45 191-24-208/22/19 10:08360 141 1
Benzo(k)fluoranthene ND ug/kg 08/22/19 14:45 207-08-908/22/19 10:08360 152 1
Benzoic Acid ND ug/kg 08/22/19 14:45 65-85-008/22/19 10:081800 389 1
Benzyl alcohol ND ug/kg 08/22/19 14:45 100-51-608/22/19 10:08721 191 1
4-Bromophenylphenyl ether ND ug/kg 08/22/19 14:45 101-55-308/22/19 10:08360 94.5 1
Butylbenzylphthalate ND ug/kg 08/22/19 14:45 85-68-708/22/19 10:08360 96.0 1
4-Chloro-3-methylphenol ND ug/kg 08/22/19 14:45 59-50-708/22/19 10:08721 219 1
4-Chloroaniline ND ug/kg 08/22/19 14:45 106-47-808/22/19 10:081800 221 1
bis(2-Chloroethoxy)methane ND ug/kg 08/22/19 14:45 111-91-108/22/19 10:08360 96.2 1
bis(2-Chloroethyl) ether ND ug/kg 08/22/19 14:45 111-44-408/22/19 10:08360 76.5 1
2-Chloronaphthalene ND ug/kg 08/22/19 14:45 91-58-708/22/19 10:08360 80.2 1
2-Chlorophenol ND ug/kg 08/22/19 14:45 95-57-808/22/19 10:08360 83.8 1
4-Chlorophenylphenyl ether ND ug/kg 08/22/19 14:45 7005-72-308/22/19 10:08360 93.6 1
Chrysene 127J ug/kg 08/22/19 14:45 218-01-908/22/19 10:08360 105 1
Dibenz(a,h)anthracene ND ug/kg 08/22/19 14:45 53-70-308/22/19 10:08360 144 1
Dibenzofuran ND ug/kg 08/22/19 14:45 132-64-908/22/19 10:08360 90.1 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 14:45 95-50-108/22/19 10:08360 77.9 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 14:45 541-73-108/22/19 10:08360 81.1 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 14:45 106-46-708/22/19 10:08360 79.3 1
3,3'-Dichlorobenzidine ND ug/kg 08/22/19 14:45 91-94-108/22/19 10:081800 251 1
2,4-Dichlorophenol ND ug/kg 08/22/19 14:45 120-83-208/22/19 10:08360 119 1
Diethylphthalate ND ug/kg 08/22/19 14:45 84-66-208/22/19 10:08360 78.2 1
2,4-Dimethylphenol ND ug/kg 08/22/19 14:45 105-67-908/22/19 10:08360 89.7 1
Dimethylphthalate ND ug/kg 08/22/19 14:45 131-11-308/22/19 10:08360 81.4 1
Di-n-butylphthalate ND ug/kg 08/22/19 14:45 84-74-208/22/19 10:08360 88.9 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/22/19 14:45 534-52-108/22/19 10:08721 581 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: A Lab ID: 92442356011 Collected: 08/20/19 16:05 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 08/22/19 14:45 51-28-508/22/19 10:081800 1150 1
2,4-Dinitrotoluene ND ug/kg 08/22/19 14:45 121-14-208/22/19 10:08360 95.4 1
2,6-Dinitrotoluene ND ug/kg 08/22/19 14:45 606-20-208/22/19 10:08360 94.2 1
Di-n-octylphthalate ND ug/kg 08/22/19 14:45 117-84-008/22/19 10:08360 205 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/22/19 14:45 117-81-708/22/19 10:08360 118 1
Fluoranthene 258J ug/kg 08/22/19 14:45 206-44-008/22/19 10:08360 109 1
Fluorene ND ug/kg 08/22/19 14:45 86-73-708/22/19 10:08360 96.4 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 14:45 87-68-308/22/19 10:08360 87.6 1
Hexachlorobenzene ND ug/kg 08/22/19 14:45 118-74-108/22/19 10:08360 91.5 1
Hexachlorocyclopentadiene ND ug/kg 08/22/19 14:45 77-47-408/22/19 10:08360 144 1
Hexachloroethane ND ug/kg 08/22/19 14:45 67-72-108/22/19 10:08360 82.1 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/22/19 14:45 193-39-508/22/19 10:08360 165 1
Isophorone ND ug/kg 08/22/19 14:45 78-59-108/22/19 10:08360 78.3 1
1-Methylnaphthalene ND ug/kg 08/22/19 14:45 90-12-008/22/19 10:08360 96.0 1
2-Methylnaphthalene ND ug/kg 08/22/19 14:45 91-57-608/22/19 10:08360 91.7 1
2-Methylphenol(o-Cresol)ND ug/kg 08/22/19 14:45 95-48-708/22/19 10:08360 79.8 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/22/19 14:45 15831-10-408/22/19 10:08360 90.6 1
Naphthalene ND ug/kg 08/22/19 14:45 91-20-308/22/19 10:08360 86.2 1
2-Nitroaniline ND ug/kg 08/22/19 14:45 88-74-408/22/19 10:081800 181 1
3-Nitroaniline ND ug/kg 08/22/19 14:45 99-09-208/22/19 10:081800 191 1
4-Nitroaniline ND ug/kg 08/22/19 14:45 100-01-608/22/19 10:08721 178 1
Nitrobenzene ND ug/kg 08/22/19 14:45 98-95-308/22/19 10:08360 86.0 1
2-Nitrophenol ND ug/kg 08/22/19 14:45 88-75-508/22/19 10:08360 111 1
4-Nitrophenol ND ug/kg 08/22/19 14:45 100-02-708/22/19 10:081800 574 1
N-Nitrosodimethylamine ND ug/kg 08/22/19 14:45 62-75-908/22/19 10:08360 101 1
N-Nitroso-di-n-propylamine ND ug/kg 08/22/19 14:45 621-64-708/22/19 10:08360 101 1
N-Nitrosodiphenylamine ND ug/kg 08/22/19 14:45 86-30-608/22/19 10:08360 91.9 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 08/22/19 14:45 108-60-108/22/19 10:08360 100 1
Pentachlorophenol ND ug/kg 08/22/19 14:45 87-86-508/22/19 10:081800 165 1
Phenanthrene 155J ug/kg 08/22/19 14:45 85-01-808/22/19 10:08360 90.7 1
Phenol ND ug/kg 08/22/19 14:45 108-95-208/22/19 10:08360 86.0 1
Pyrene 228J ug/kg 08/22/19 14:45 129-00-008/22/19 10:08360 99.1 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 14:45 120-82-108/22/19 10:08360 82.5 1
2,4,5-Trichlorophenol ND ug/kg 08/22/19 14:45 95-95-408/22/19 10:08360 93.6 1
2,4,6-Trichlorophenol ND ug/kg 08/22/19 14:45 88-06-208/22/19 10:08360 90.5 1
Surrogates
Nitrobenzene-d5 (S)52 %08/22/19 14:45 4165-60-008/22/19 10:0823-110 1
2-Fluorobiphenyl (S)55 %08/22/19 14:45 321-60-808/22/19 10:0830-110 1
Terphenyl-d14 (S)78 %08/22/19 14:45 1718-51-008/22/19 10:0828-110 1
Phenol-d6 (S)53 %08/22/19 14:45 13127-88-308/22/19 10:0822-110 1
2-Fluorophenol (S)52 %08/22/19 14:45 367-12-408/22/19 10:0813-110 1
2,4,6-Tribromophenol (S)82 %08/22/19 14:45 118-79-608/22/19 10:0827-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 8.7 %08/22/19 13:210.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: B Lab ID: 92442356012 Collected: 08/20/19 16:15 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic ND mg/kg 08/23/19 10:34 7440-38-208/22/19 11:480.68 0.34 1
Barium 258 mg/kg 08/23/19 10:34 7440-39-308/22/19 11:480.34 0.17 1
Cadmium 0.039J mg/kg 08/23/19 10:34 7440-43-908/22/19 11:480.068 0.034 1
Chromium 60.3 mg/kg 08/23/19 10:34 7440-47-308/22/19 11:480.34 0.17 1
Lead 1.1 mg/kg 08/23/19 10:34 7439-92-1 B08/22/19 11:480.34 0.17 1
Selenium 0.62J mg/kg 08/23/19 10:34 7782-49-208/22/19 11:480.68 0.34 1
Silver ND mg/kg 08/23/19 10:34 7440-22-408/22/19 11:480.34 0.17 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.010 mg/kg 08/26/19 14:05 7439-97-608/22/19 14:530.0060 0.0030 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 08/22/19 15:52 83-32-908/22/19 10:08391 101 1
Acenaphthylene ND ug/kg 08/22/19 15:52 208-96-808/22/19 10:08391 92.5 1
Aniline ND ug/kg 08/22/19 15:52 62-53-308/22/19 10:08391 87.7 1
Anthracene ND ug/kg 08/22/19 15:52 120-12-708/22/19 10:08391 101 1
Benzo(a)anthracene 326J ug/kg 08/22/19 15:52 56-55-308/22/19 10:08391 124 1
Benzo(a)pyrene 322J ug/kg 08/22/19 15:52 50-32-808/22/19 10:08391 169 1
Benzo(b)fluoranthene 509 ug/kg 08/22/19 15:52 205-99-208/22/19 10:08391 157 1
Benzo(g,h,i)perylene 247J ug/kg 08/22/19 15:52 191-24-208/22/19 10:08391 153 1
Benzo(k)fluoranthene 203J ug/kg 08/22/19 15:52 207-08-908/22/19 10:08391 165 1
Benzoic Acid ND ug/kg 08/22/19 15:52 65-85-008/22/19 10:081950 421 1
Benzyl alcohol ND ug/kg 08/22/19 15:52 100-51-608/22/19 10:08781 207 1
4-Bromophenylphenyl ether ND ug/kg 08/22/19 15:52 101-55-308/22/19 10:08391 103 1
Butylbenzylphthalate ND ug/kg 08/22/19 15:52 85-68-708/22/19 10:08391 104 1
4-Chloro-3-methylphenol ND ug/kg 08/22/19 15:52 59-50-708/22/19 10:08781 238 1
4-Chloroaniline ND ug/kg 08/22/19 15:52 106-47-808/22/19 10:081950 239 1
bis(2-Chloroethoxy)methane ND ug/kg 08/22/19 15:52 111-91-108/22/19 10:08391 104 1
bis(2-Chloroethyl) ether ND ug/kg 08/22/19 15:52 111-44-408/22/19 10:08391 83.0 1
2-Chloronaphthalene ND ug/kg 08/22/19 15:52 91-58-708/22/19 10:08391 87.0 1
2-Chlorophenol ND ug/kg 08/22/19 15:52 95-57-808/22/19 10:08391 90.9 1
4-Chlorophenylphenyl ether ND ug/kg 08/22/19 15:52 7005-72-308/22/19 10:08391 101 1
Chrysene 373J ug/kg 08/22/19 15:52 218-01-908/22/19 10:08391 113 1
Dibenz(a,h)anthracene ND ug/kg 08/22/19 15:52 53-70-308/22/19 10:08391 156 1
Dibenzofuran ND ug/kg 08/22/19 15:52 132-64-908/22/19 10:08391 97.7 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 15:52 95-50-108/22/19 10:08391 84.5 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 15:52 541-73-108/22/19 10:08391 88.0 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 15:52 106-46-708/22/19 10:08391 86.0 1
3,3'-Dichlorobenzidine ND ug/kg 08/22/19 15:52 91-94-108/22/19 10:081950 272 1
2,4-Dichlorophenol ND ug/kg 08/22/19 15:52 120-83-208/22/19 10:08391 129 1
Diethylphthalate ND ug/kg 08/22/19 15:52 84-66-208/22/19 10:08391 84.8 1
2,4-Dimethylphenol ND ug/kg 08/22/19 15:52 105-67-908/22/19 10:08391 97.3 1
Dimethylphthalate ND ug/kg 08/22/19 15:52 131-11-308/22/19 10:08391 88.3 1
Di-n-butylphthalate ND ug/kg 08/22/19 15:52 84-74-208/22/19 10:08391 96.4 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/22/19 15:52 534-52-108/22/19 10:08781 630 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: B Lab ID: 92442356012 Collected: 08/20/19 16:15 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 08/22/19 15:52 51-28-508/22/19 10:081950 1250 1
2,4-Dinitrotoluene ND ug/kg 08/22/19 15:52 121-14-208/22/19 10:08391 103 1
2,6-Dinitrotoluene ND ug/kg 08/22/19 15:52 606-20-208/22/19 10:08391 102 1
Di-n-octylphthalate ND ug/kg 08/22/19 15:52 117-84-008/22/19 10:08391 223 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/22/19 15:52 117-81-708/22/19 10:08391 128 1
Fluoranthene 797 ug/kg 08/22/19 15:52 206-44-008/22/19 10:08391 118 1
Fluorene ND ug/kg 08/22/19 15:52 86-73-708/22/19 10:08391 105 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 15:52 87-68-308/22/19 10:08391 94.9 1
Hexachlorobenzene ND ug/kg 08/22/19 15:52 118-74-108/22/19 10:08391 99.2 1
Hexachlorocyclopentadiene ND ug/kg 08/22/19 15:52 77-47-408/22/19 10:08391 156 1
Hexachloroethane ND ug/kg 08/22/19 15:52 67-72-108/22/19 10:08391 89.0 1
Indeno(1,2,3-cd)pyrene 202J ug/kg 08/22/19 15:52 193-39-508/22/19 10:08391 179 1
Isophorone ND ug/kg 08/22/19 15:52 78-59-108/22/19 10:08391 84.9 1
1-Methylnaphthalene ND ug/kg 08/22/19 15:52 90-12-008/22/19 10:08391 104 1
2-Methylnaphthalene ND ug/kg 08/22/19 15:52 91-57-608/22/19 10:08391 99.4 1
2-Methylphenol(o-Cresol)ND ug/kg 08/22/19 15:52 95-48-708/22/19 10:08391 86.5 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/22/19 15:52 15831-10-408/22/19 10:08391 98.3 1
Naphthalene ND ug/kg 08/22/19 15:52 91-20-308/22/19 10:08391 93.5 1
2-Nitroaniline ND ug/kg 08/22/19 15:52 88-74-408/22/19 10:081950 197 1
3-Nitroaniline ND ug/kg 08/22/19 15:52 99-09-208/22/19 10:081950 207 1
4-Nitroaniline ND ug/kg 08/22/19 15:52 100-01-608/22/19 10:08781 193 1
Nitrobenzene ND ug/kg 08/22/19 15:52 98-95-308/22/19 10:08391 93.3 1
2-Nitrophenol ND ug/kg 08/22/19 15:52 88-75-508/22/19 10:08391 121 1
4-Nitrophenol ND ug/kg 08/22/19 15:52 100-02-708/22/19 10:081950 623 1
N-Nitrosodimethylamine ND ug/kg 08/22/19 15:52 62-75-908/22/19 10:08391 110 1
N-Nitroso-di-n-propylamine ND ug/kg 08/22/19 15:52 621-64-708/22/19 10:08391 109 1
N-Nitrosodiphenylamine ND ug/kg 08/22/19 15:52 86-30-608/22/19 10:08391 99.7 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 08/22/19 15:52 108-60-108/22/19 10:08391 109 1
Pentachlorophenol ND ug/kg 08/22/19 15:52 87-86-508/22/19 10:081950 179 1
Phenanthrene 541 ug/kg 08/22/19 15:52 85-01-808/22/19 10:08391 98.4 1
Phenol ND ug/kg 08/22/19 15:52 108-95-208/22/19 10:08391 93.3 1
Pyrene 672 ug/kg 08/22/19 15:52 129-00-008/22/19 10:08391 107 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 15:52 120-82-108/22/19 10:08391 89.5 1
2,4,5-Trichlorophenol ND ug/kg 08/22/19 15:52 95-95-408/22/19 10:08391 101 1
2,4,6-Trichlorophenol ND ug/kg 08/22/19 15:52 88-06-208/22/19 10:08391 98.1 1
Surrogates
Nitrobenzene-d5 (S)55 %08/22/19 15:52 4165-60-008/22/19 10:0823-110 1
2-Fluorobiphenyl (S)52 %08/22/19 15:52 321-60-808/22/19 10:0830-110 1
Terphenyl-d14 (S)73 %08/22/19 15:52 1718-51-008/22/19 10:0828-110 1
Phenol-d6 (S)54 %08/22/19 15:52 13127-88-308/22/19 10:0822-110 1
2-Fluorophenol (S)53 %08/22/19 15:52 367-12-408/22/19 10:0813-110 1
2,4,6-Tribromophenol (S)74 %08/22/19 15:52 118-79-608/22/19 10:0827-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.0 %08/22/19 13:210.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: C Lab ID: 92442356013 Collected: 08/20/19 16:25 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 1.0 mg/kg 08/23/19 10:37 7440-38-208/22/19 11:480.85 0.42 1
Barium 74.0 mg/kg 08/23/19 10:37 7440-39-308/22/19 11:480.42 0.21 1
Cadmium 0.090 mg/kg 08/23/19 10:37 7440-43-908/22/19 11:480.085 0.042 1
Chromium 54.9 mg/kg 08/23/19 10:37 7440-47-308/22/19 11:480.42 0.21 1
Lead 3.6 mg/kg 08/23/19 10:37 7439-92-108/22/19 11:480.42 0.21 1
Selenium 0.73J mg/kg 08/23/19 10:37 7782-49-208/22/19 11:480.85 0.42 1
Silver ND mg/kg 08/23/19 10:37 7440-22-408/22/19 11:480.42 0.21 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.011 mg/kg 08/26/19 14:07 7439-97-608/22/19 14:530.0043 0.0022 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 08/22/19 15:36 83-32-908/22/19 10:08432 111 1
Acenaphthylene ND ug/kg 08/22/19 15:36 208-96-808/22/19 10:08432 102 1
Aniline ND ug/kg 08/22/19 15:36 62-53-308/22/19 10:08432 97.0 1
Anthracene ND ug/kg 08/22/19 15:36 120-12-708/22/19 10:08432 112 1
Benzo(a)anthracene ND ug/kg 08/22/19 15:36 56-55-308/22/19 10:08432 137 1
Benzo(a)pyrene ND ug/kg 08/22/19 15:36 50-32-808/22/19 10:08432 187 1
Benzo(b)fluoranthene ND ug/kg 08/22/19 15:36 205-99-208/22/19 10:08432 174 1
Benzo(g,h,i)perylene ND ug/kg 08/22/19 15:36 191-24-208/22/19 10:08432 169 1
Benzo(k)fluoranthene ND ug/kg 08/22/19 15:36 207-08-908/22/19 10:08432 182 1
Benzoic Acid ND ug/kg 08/22/19 15:36 65-85-008/22/19 10:082160 466 1
Benzyl alcohol ND ug/kg 08/22/19 15:36 100-51-608/22/19 10:08864 229 1
4-Bromophenylphenyl ether ND ug/kg 08/22/19 15:36 101-55-308/22/19 10:08432 113 1
Butylbenzylphthalate ND ug/kg 08/22/19 15:36 85-68-708/22/19 10:08432 115 1
4-Chloro-3-methylphenol ND ug/kg 08/22/19 15:36 59-50-708/22/19 10:08864 263 1
4-Chloroaniline ND ug/kg 08/22/19 15:36 106-47-808/22/19 10:082160 264 1
bis(2-Chloroethoxy)methane ND ug/kg 08/22/19 15:36 111-91-108/22/19 10:08432 115 1
bis(2-Chloroethyl) ether ND ug/kg 08/22/19 15:36 111-44-408/22/19 10:08432 91.8 1
2-Chloronaphthalene ND ug/kg 08/22/19 15:36 91-58-708/22/19 10:08432 96.2 1
2-Chlorophenol ND ug/kg 08/22/19 15:36 95-57-808/22/19 10:08432 101 1
4-Chlorophenylphenyl ether ND ug/kg 08/22/19 15:36 7005-72-308/22/19 10:08432 112 1
Chrysene ND ug/kg 08/22/19 15:36 218-01-908/22/19 10:08432 125 1
Dibenz(a,h)anthracene ND ug/kg 08/22/19 15:36 53-70-308/22/19 10:08432 173 1
Dibenzofuran ND ug/kg 08/22/19 15:36 132-64-908/22/19 10:08432 108 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 15:36 95-50-108/22/19 10:08432 93.5 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 15:36 541-73-108/22/19 10:08432 97.3 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 15:36 106-46-708/22/19 10:08432 95.0 1
3,3'-Dichlorobenzidine ND ug/kg 08/22/19 15:36 91-94-108/22/19 10:082160 301 1
2,4-Dichlorophenol ND ug/kg 08/22/19 15:36 120-83-208/22/19 10:08432 143 1
Diethylphthalate ND ug/kg 08/22/19 15:36 84-66-208/22/19 10:08432 93.7 1
2,4-Dimethylphenol ND ug/kg 08/22/19 15:36 105-67-908/22/19 10:08432 108 1
Dimethylphthalate ND ug/kg 08/22/19 15:36 131-11-308/22/19 10:08432 97.7 1
Di-n-butylphthalate ND ug/kg 08/22/19 15:36 84-74-208/22/19 10:08432 107 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/22/19 15:36 534-52-108/22/19 10:08864 696 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: C Lab ID: 92442356013 Collected: 08/20/19 16:25 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 08/22/19 15:36 51-28-508/22/19 10:082160 1380 1
2,4-Dinitrotoluene ND ug/kg 08/22/19 15:36 121-14-208/22/19 10:08432 114 1
2,6-Dinitrotoluene ND ug/kg 08/22/19 15:36 606-20-208/22/19 10:08432 113 1
Di-n-octylphthalate ND ug/kg 08/22/19 15:36 117-84-008/22/19 10:08432 246 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/22/19 15:36 117-81-708/22/19 10:08432 141 1
Fluoranthene ND ug/kg 08/22/19 15:36 206-44-008/22/19 10:08432 131 1
Fluorene ND ug/kg 08/22/19 15:36 86-73-708/22/19 10:08432 116 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 15:36 87-68-308/22/19 10:08432 105 1
Hexachlorobenzene ND ug/kg 08/22/19 15:36 118-74-108/22/19 10:08432 110 1
Hexachlorocyclopentadiene ND ug/kg 08/22/19 15:36 77-47-408/22/19 10:08432 173 1
Hexachloroethane ND ug/kg 08/22/19 15:36 67-72-108/22/19 10:08432 98.4 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/22/19 15:36 193-39-508/22/19 10:08432 198 1
Isophorone ND ug/kg 08/22/19 15:36 78-59-108/22/19 10:08432 93.9 1
1-Methylnaphthalene ND ug/kg 08/22/19 15:36 90-12-008/22/19 10:08432 115 1
2-Methylnaphthalene ND ug/kg 08/22/19 15:36 91-57-608/22/19 10:08432 110 1
2-Methylphenol(o-Cresol)ND ug/kg 08/22/19 15:36 95-48-708/22/19 10:08432 95.7 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/22/19 15:36 15831-10-408/22/19 10:08432 109 1
Naphthalene ND ug/kg 08/22/19 15:36 91-20-308/22/19 10:08432 103 1
2-Nitroaniline ND ug/kg 08/22/19 15:36 88-74-408/22/19 10:082160 217 1
3-Nitroaniline ND ug/kg 08/22/19 15:36 99-09-208/22/19 10:082160 229 1
4-Nitroaniline ND ug/kg 08/22/19 15:36 100-01-608/22/19 10:08864 213 1
Nitrobenzene ND ug/kg 08/22/19 15:36 98-95-308/22/19 10:08432 103 1
2-Nitrophenol ND ug/kg 08/22/19 15:36 88-75-508/22/19 10:08432 134 1
4-Nitrophenol ND ug/kg 08/22/19 15:36 100-02-708/22/19 10:082160 689 1
N-Nitrosodimethylamine ND ug/kg 08/22/19 15:36 62-75-908/22/19 10:08432 121 1
N-Nitroso-di-n-propylamine ND ug/kg 08/22/19 15:36 621-64-708/22/19 10:08432 121 1
N-Nitrosodiphenylamine ND ug/kg 08/22/19 15:36 86-30-608/22/19 10:08432 110 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 08/22/19 15:36 108-60-108/22/19 10:08432 120 1
Pentachlorophenol ND ug/kg 08/22/19 15:36 87-86-508/22/19 10:082160 198 1
Phenanthrene ND ug/kg 08/22/19 15:36 85-01-808/22/19 10:08432 109 1
Phenol ND ug/kg 08/22/19 15:36 108-95-208/22/19 10:08432 103 1
Pyrene ND ug/kg 08/22/19 15:36 129-00-008/22/19 10:08432 119 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 15:36 120-82-108/22/19 10:08432 99.0 1
2,4,5-Trichlorophenol ND ug/kg 08/22/19 15:36 95-95-408/22/19 10:08432 112 1
2,4,6-Trichlorophenol ND ug/kg 08/22/19 15:36 88-06-208/22/19 10:08432 109 1
Surrogates
Nitrobenzene-d5 (S)57 %08/22/19 15:36 4165-60-008/22/19 10:0823-110 1
2-Fluorobiphenyl (S)48 %08/22/19 15:36 321-60-808/22/19 10:0830-110 1
Terphenyl-d14 (S)74 %08/22/19 15:36 1718-51-008/22/19 10:0828-110 1
Phenol-d6 (S)56 %08/22/19 15:36 13127-88-308/22/19 10:0822-110 1
2-Fluorophenol (S)57 %08/22/19 15:36 367-12-408/22/19 10:0813-110 1
2,4,6-Tribromophenol (S)64 %08/22/19 15:36 118-79-608/22/19 10:0827-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.6 %08/22/19 13:210.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: D Lab ID: 92442356014 Collected: 08/20/19 16:35 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic ND mg/kg 08/23/19 10:46 7440-38-208/22/19 11:480.67 0.33 1
Barium 75.1 mg/kg 08/23/19 10:46 7440-39-308/22/19 11:480.33 0.17 1
Cadmium 0.059J mg/kg 08/23/19 10:46 7440-43-908/22/19 11:480.067 0.033 1
Chromium 104 mg/kg 08/23/19 10:46 7440-47-308/22/19 11:480.33 0.17 1
Lead 2.1 mg/kg 08/23/19 10:46 7439-92-108/22/19 11:480.33 0.17 1
Selenium 0.51J mg/kg 08/23/19 10:46 7782-49-208/22/19 11:480.67 0.33 1
Silver ND mg/kg 08/23/19 10:46 7440-22-408/22/19 11:480.33 0.17 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.010 mg/kg 08/26/19 14:14 7439-97-608/22/19 14:530.0041 0.0020 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 08/22/19 16:05 83-32-908/22/19 10:08394 101 1
Acenaphthylene ND ug/kg 08/22/19 16:05 208-96-808/22/19 10:08394 93.2 1
Aniline ND ug/kg 08/22/19 16:05 62-53-308/22/19 10:08394 88.4 1
Anthracene ND ug/kg 08/22/19 16:05 120-12-708/22/19 10:08394 102 1
Benzo(a)anthracene ND ug/kg 08/22/19 16:05 56-55-308/22/19 10:08394 125 1
Benzo(a)pyrene ND ug/kg 08/22/19 16:05 50-32-808/22/19 10:08394 171 1
Benzo(b)fluoranthene ND ug/kg 08/22/19 16:05 205-99-208/22/19 10:08394 159 1
Benzo(g,h,i)perylene ND ug/kg 08/22/19 16:05 191-24-208/22/19 10:08394 154 1
Benzo(k)fluoranthene ND ug/kg 08/22/19 16:05 207-08-908/22/19 10:08394 166 1
Benzoic Acid ND ug/kg 08/22/19 16:05 65-85-008/22/19 10:081970 425 1
Benzyl alcohol ND ug/kg 08/22/19 16:05 100-51-608/22/19 10:08788 209 1
4-Bromophenylphenyl ether ND ug/kg 08/22/19 16:05 101-55-308/22/19 10:08394 103 1
Butylbenzylphthalate ND ug/kg 08/22/19 16:05 85-68-708/22/19 10:08394 105 1
4-Chloro-3-methylphenol ND ug/kg 08/22/19 16:05 59-50-708/22/19 10:08788 240 1
4-Chloroaniline ND ug/kg 08/22/19 16:05 106-47-808/22/19 10:081970 241 1
bis(2-Chloroethoxy)methane ND ug/kg 08/22/19 16:05 111-91-108/22/19 10:08394 105 1
bis(2-Chloroethyl) ether ND ug/kg 08/22/19 16:05 111-44-408/22/19 10:08394 83.7 1
2-Chloronaphthalene ND ug/kg 08/22/19 16:05 91-58-708/22/19 10:08394 87.7 1
2-Chlorophenol ND ug/kg 08/22/19 16:05 95-57-808/22/19 10:08394 91.7 1
4-Chlorophenylphenyl ether ND ug/kg 08/22/19 16:05 7005-72-308/22/19 10:08394 102 1
Chrysene ND ug/kg 08/22/19 16:05 218-01-908/22/19 10:08394 114 1
Dibenz(a,h)anthracene ND ug/kg 08/22/19 16:05 53-70-308/22/19 10:08394 158 1
Dibenzofuran ND ug/kg 08/22/19 16:05 132-64-908/22/19 10:08394 98.5 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 16:05 95-50-108/22/19 10:08394 85.2 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 16:05 541-73-108/22/19 10:08394 88.7 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 16:05 106-46-708/22/19 10:08394 86.7 1
3,3'-Dichlorobenzidine ND ug/kg 08/22/19 16:05 91-94-108/22/19 10:081970 275 1
2,4-Dichlorophenol ND ug/kg 08/22/19 16:05 120-83-208/22/19 10:08394 130 1
Diethylphthalate ND ug/kg 08/22/19 16:05 84-66-208/22/19 10:08394 85.5 1
2,4-Dimethylphenol ND ug/kg 08/22/19 16:05 105-67-908/22/19 10:08394 98.1 1
Dimethylphthalate ND ug/kg 08/22/19 16:05 131-11-308/22/19 10:08394 89.0 1
Di-n-butylphthalate ND ug/kg 08/22/19 16:05 84-74-208/22/19 10:08394 97.2 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/22/19 16:05 534-52-108/22/19 10:08788 635 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: D Lab ID: 92442356014 Collected: 08/20/19 16:35 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 08/22/19 16:05 51-28-508/22/19 10:081970 1260 1
2,4-Dinitrotoluene ND ug/kg 08/22/19 16:05 121-14-208/22/19 10:08394 104 1
2,6-Dinitrotoluene ND ug/kg 08/22/19 16:05 606-20-208/22/19 10:08394 103 1
Di-n-octylphthalate ND ug/kg 08/22/19 16:05 117-84-008/22/19 10:08394 224 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/22/19 16:05 117-81-708/22/19 10:08394 129 1
Fluoranthene ND ug/kg 08/22/19 16:05 206-44-008/22/19 10:08394 119 1
Fluorene ND ug/kg 08/22/19 16:05 86-73-708/22/19 10:08394 105 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 16:05 87-68-308/22/19 10:08394 95.7 1
Hexachlorobenzene ND ug/kg 08/22/19 16:05 118-74-108/22/19 10:08394 100 1
Hexachlorocyclopentadiene ND ug/kg 08/22/19 16:05 77-47-408/22/19 10:08394 158 1
Hexachloroethane ND ug/kg 08/22/19 16:05 67-72-108/22/19 10:08394 89.8 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/22/19 16:05 193-39-508/22/19 10:08394 180 1
Isophorone ND ug/kg 08/22/19 16:05 78-59-108/22/19 10:08394 85.6 1
1-Methylnaphthalene ND ug/kg 08/22/19 16:05 90-12-008/22/19 10:08394 105 1
2-Methylnaphthalene ND ug/kg 08/22/19 16:05 91-57-608/22/19 10:08394 100 1
2-Methylphenol(o-Cresol)ND ug/kg 08/22/19 16:05 95-48-708/22/19 10:08394 87.3 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/22/19 16:05 15831-10-408/22/19 10:08394 99.1 1
Naphthalene ND ug/kg 08/22/19 16:05 91-20-308/22/19 10:08394 94.3 1
2-Nitroaniline ND ug/kg 08/22/19 16:05 88-74-408/22/19 10:081970 198 1
3-Nitroaniline ND ug/kg 08/22/19 16:05 99-09-208/22/19 10:081970 209 1
4-Nitroaniline ND ug/kg 08/22/19 16:05 100-01-608/22/19 10:08788 195 1
Nitrobenzene ND ug/kg 08/22/19 16:05 98-95-308/22/19 10:08394 94.1 1
2-Nitrophenol ND ug/kg 08/22/19 16:05 88-75-508/22/19 10:08394 122 1
4-Nitrophenol ND ug/kg 08/22/19 16:05 100-02-708/22/19 10:081970 628 1
N-Nitrosodimethylamine ND ug/kg 08/22/19 16:05 62-75-908/22/19 10:08394 111 1
N-Nitroso-di-n-propylamine ND ug/kg 08/22/19 16:05 621-64-708/22/19 10:08394 110 1
N-Nitrosodiphenylamine ND ug/kg 08/22/19 16:05 86-30-608/22/19 10:08394 101 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 08/22/19 16:05 108-60-108/22/19 10:08394 109 1
Pentachlorophenol ND ug/kg 08/22/19 16:05 87-86-508/22/19 10:081970 180 1
Phenanthrene ND ug/kg 08/22/19 16:05 85-01-808/22/19 10:08394 99.2 1
Phenol ND ug/kg 08/22/19 16:05 108-95-208/22/19 10:08394 94.1 1
Pyrene ND ug/kg 08/22/19 16:05 129-00-008/22/19 10:08394 108 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 16:05 120-82-108/22/19 10:08394 90.2 1
2,4,5-Trichlorophenol ND ug/kg 08/22/19 16:05 95-95-408/22/19 10:08394 102 1
2,4,6-Trichlorophenol ND ug/kg 08/22/19 16:05 88-06-208/22/19 10:08394 99.0 1
Surrogates
Nitrobenzene-d5 (S)63 %08/22/19 16:05 4165-60-008/22/19 10:0823-110 1
2-Fluorobiphenyl (S)58 %08/22/19 16:05 321-60-808/22/19 10:0830-110 1
Terphenyl-d14 (S)73 %08/22/19 16:05 1718-51-008/22/19 10:0828-110 1
Phenol-d6 (S)62 %08/22/19 16:05 13127-88-308/22/19 10:0822-110 1
2-Fluorophenol (S)60 %08/22/19 16:05 367-12-408/22/19 10:0813-110 1
2,4,6-Tribromophenol (S)63 %08/22/19 16:05 118-79-608/22/19 10:0827-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.1 %08/22/19 13:210.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: E Lab ID: 92442356015 Collected: 08/20/19 16:45 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 1.5 mg/kg 08/23/19 10:49 7440-38-208/22/19 11:480.78 0.39 1
Barium 67.2 mg/kg 08/23/19 10:49 7440-39-308/22/19 11:480.39 0.20 1
Cadmium 0.13 mg/kg 08/23/19 10:49 7440-43-908/22/19 11:480.078 0.039 1
Chromium 23.6 mg/kg 08/23/19 10:49 7440-47-308/22/19 11:480.39 0.20 1
Lead 33.3 mg/kg 08/23/19 10:49 7439-92-108/22/19 11:480.39 0.20 1
Selenium 0.69J mg/kg 08/23/19 10:49 7782-49-208/22/19 11:480.78 0.39 1
Silver ND mg/kg 08/23/19 10:49 7440-22-408/22/19 11:480.39 0.20 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.018 mg/kg 08/26/19 14:16 7439-97-608/22/19 14:530.0032 0.0016 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 08/22/19 17:01 83-32-908/22/19 10:08383 98.6 1
Acenaphthylene ND ug/kg 08/22/19 17:01 208-96-808/22/19 10:08383 90.7 1
Aniline ND ug/kg 08/22/19 17:01 62-53-308/22/19 10:08383 86.1 1
Anthracene ND ug/kg 08/22/19 17:01 120-12-708/22/19 10:08383 99.4 1
Benzo(a)anthracene ND ug/kg 08/22/19 17:01 56-55-308/22/19 10:08383 122 1
Benzo(a)pyrene ND ug/kg 08/22/19 17:01 50-32-808/22/19 10:08383 166 1
Benzo(b)fluoranthene ND ug/kg 08/22/19 17:01 205-99-208/22/19 10:08383 154 1
Benzo(g,h,i)perylene ND ug/kg 08/22/19 17:01 191-24-208/22/19 10:08383 150 1
Benzo(k)fluoranthene ND ug/kg 08/22/19 17:01 207-08-908/22/19 10:08383 161 1
Benzoic Acid ND ug/kg 08/22/19 17:01 65-85-008/22/19 10:081920 413 1
Benzyl alcohol ND ug/kg 08/22/19 17:01 100-51-608/22/19 10:08767 203 1
4-Bromophenylphenyl ether ND ug/kg 08/22/19 17:01 101-55-308/22/19 10:08383 101 1
Butylbenzylphthalate ND ug/kg 08/22/19 17:01 85-68-708/22/19 10:08383 102 1
4-Chloro-3-methylphenol ND ug/kg 08/22/19 17:01 59-50-708/22/19 10:08767 233 1
4-Chloroaniline ND ug/kg 08/22/19 17:01 106-47-808/22/19 10:081920 235 1
bis(2-Chloroethoxy)methane ND ug/kg 08/22/19 17:01 111-91-108/22/19 10:08383 102 1
bis(2-Chloroethyl) ether ND ug/kg 08/22/19 17:01 111-44-408/22/19 10:08383 81.4 1
2-Chloronaphthalene ND ug/kg 08/22/19 17:01 91-58-708/22/19 10:08383 85.4 1
2-Chlorophenol ND ug/kg 08/22/19 17:01 95-57-808/22/19 10:08383 89.2 1
4-Chlorophenylphenyl ether ND ug/kg 08/22/19 17:01 7005-72-308/22/19 10:08383 99.5 1
Chrysene 126J ug/kg 08/22/19 17:01 218-01-908/22/19 10:08383 111 1
Dibenz(a,h)anthracene ND ug/kg 08/22/19 17:01 53-70-308/22/19 10:08383 153 1
Dibenzofuran ND ug/kg 08/22/19 17:01 132-64-908/22/19 10:08383 95.8 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 17:01 95-50-108/22/19 10:08383 82.9 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 17:01 541-73-108/22/19 10:08383 86.3 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 17:01 106-46-708/22/19 10:08383 84.3 1
3,3'-Dichlorobenzidine ND ug/kg 08/22/19 17:01 91-94-108/22/19 10:081920 267 1
2,4-Dichlorophenol ND ug/kg 08/22/19 17:01 120-83-208/22/19 10:08383 127 1
Diethylphthalate ND ug/kg 08/22/19 17:01 84-66-208/22/19 10:08383 83.2 1
2,4-Dimethylphenol ND ug/kg 08/22/19 17:01 105-67-908/22/19 10:08383 95.5 1
Dimethylphthalate ND ug/kg 08/22/19 17:01 131-11-308/22/19 10:08383 86.6 1
Di-n-butylphthalate ND ug/kg 08/22/19 17:01 84-74-208/22/19 10:08383 94.5 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/22/19 17:01 534-52-108/22/19 10:08767 618 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: E Lab ID: 92442356015 Collected: 08/20/19 16:45 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 08/22/19 17:01 51-28-508/22/19 10:081920 1220 1
2,4-Dinitrotoluene ND ug/kg 08/22/19 17:01 121-14-208/22/19 10:08383 102 1
2,6-Dinitrotoluene ND ug/kg 08/22/19 17:01 606-20-208/22/19 10:08383 100 1
Di-n-octylphthalate ND ug/kg 08/22/19 17:01 117-84-008/22/19 10:08383 218 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/22/19 17:01 117-81-708/22/19 10:08383 125 1
Fluoranthene 270J ug/kg 08/22/19 17:01 206-44-008/22/19 10:08383 116 1
Fluorene ND ug/kg 08/22/19 17:01 86-73-708/22/19 10:08383 103 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 17:01 87-68-308/22/19 10:08383 93.1 1
Hexachlorobenzene ND ug/kg 08/22/19 17:01 118-74-108/22/19 10:08383 97.3 1
Hexachlorocyclopentadiene ND ug/kg 08/22/19 17:01 77-47-408/22/19 10:08383 153 1
Hexachloroethane ND ug/kg 08/22/19 17:01 67-72-108/22/19 10:08383 87.3 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/22/19 17:01 193-39-508/22/19 10:08383 175 1
Isophorone ND ug/kg 08/22/19 17:01 78-59-108/22/19 10:08383 83.3 1
1-Methylnaphthalene ND ug/kg 08/22/19 17:01 90-12-008/22/19 10:08383 102 1
2-Methylnaphthalene ND ug/kg 08/22/19 17:01 91-57-608/22/19 10:08383 97.6 1
2-Methylphenol(o-Cresol)ND ug/kg 08/22/19 17:01 95-48-708/22/19 10:08383 84.9 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/22/19 17:01 15831-10-408/22/19 10:08383 96.4 1
Naphthalene ND ug/kg 08/22/19 17:01 91-20-308/22/19 10:08383 91.8 1
2-Nitroaniline ND ug/kg 08/22/19 17:01 88-74-408/22/19 10:081920 193 1
3-Nitroaniline ND ug/kg 08/22/19 17:01 99-09-208/22/19 10:081920 203 1
4-Nitroaniline ND ug/kg 08/22/19 17:01 100-01-608/22/19 10:08767 189 1
Nitrobenzene ND ug/kg 08/22/19 17:01 98-95-308/22/19 10:08383 91.5 1
2-Nitrophenol ND ug/kg 08/22/19 17:01 88-75-508/22/19 10:08383 118 1
4-Nitrophenol ND ug/kg 08/22/19 17:01 100-02-708/22/19 10:081920 611 1
N-Nitrosodimethylamine ND ug/kg 08/22/19 17:01 62-75-908/22/19 10:08383 108 1
N-Nitroso-di-n-propylamine ND ug/kg 08/22/19 17:01 621-64-708/22/19 10:08383 107 1
N-Nitrosodiphenylamine ND ug/kg 08/22/19 17:01 86-30-608/22/19 10:08383 97.8 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 08/22/19 17:01 108-60-108/22/19 10:08383 107 1
Pentachlorophenol ND ug/kg 08/22/19 17:01 87-86-508/22/19 10:081920 175 1
Phenanthrene 173J ug/kg 08/22/19 17:01 85-01-808/22/19 10:08383 96.5 1
Phenol ND ug/kg 08/22/19 17:01 108-95-208/22/19 10:08383 91.5 1
Pyrene 207J ug/kg 08/22/19 17:01 129-00-008/22/19 10:08383 105 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 17:01 120-82-108/22/19 10:08383 87.8 1
2,4,5-Trichlorophenol ND ug/kg 08/22/19 17:01 95-95-408/22/19 10:08383 99.5 1
2,4,6-Trichlorophenol ND ug/kg 08/22/19 17:01 88-06-208/22/19 10:08383 96.3 1
Surrogates
Nitrobenzene-d5 (S)62 %08/22/19 17:01 4165-60-008/22/19 10:0823-110 1
2-Fluorobiphenyl (S)60 %08/22/19 17:01 321-60-808/22/19 10:0830-110 1
Terphenyl-d14 (S)77 %08/22/19 17:01 1718-51-008/22/19 10:0828-110 1
Phenol-d6 (S)63 %08/22/19 17:01 13127-88-308/22/19 10:0822-110 1
2-Fluorophenol (S)62 %08/22/19 17:01 367-12-408/22/19 10:0813-110 1
2,4,6-Tribromophenol (S)69 %08/22/19 17:01 118-79-608/22/19 10:0827-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.6 %08/22/19 13:220.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: DUP1 Lab ID: 92442356016 Collected: 08/20/19 00:00 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 25.9J ug/kg 08/23/19 13:04 67-64-108/23/19 11:2879.9 7.5 1
Benzene ND ug/kg 08/23/19 13:04 71-43-208/23/19 11:284.0 0.72 1
Bromobenzene ND ug/kg 08/23/19 13:04 108-86-108/23/19 11:284.0 1.1 1
Bromochloromethane ND ug/kg 08/23/19 13:04 74-97-508/23/19 11:284.0 0.98 1
Bromodichloromethane ND ug/kg 08/23/19 13:04 75-27-408/23/19 11:284.0 0.78 1
Bromoform ND ug/kg 08/23/19 13:04 75-25-208/23/19 11:284.0 2.0 1
Bromomethane ND ug/kg 08/23/19 13:04 74-83-908/23/19 11:288.0 1.9 1
2-Butanone (MEK)ND ug/kg 08/23/19 13:04 78-93-308/23/19 11:2879.9 9.5 1
n-Butylbenzene ND ug/kg 08/23/19 13:04 104-51-808/23/19 11:284.0 2.3 1
sec-Butylbenzene ND ug/kg 08/23/19 13:04 135-98-808/23/19 11:284.0 1.7 1
tert-Butylbenzene ND ug/kg 08/23/19 13:04 98-06-608/23/19 11:284.0 1.4 1
Carbon tetrachloride ND ug/kg 08/23/19 13:04 56-23-508/23/19 11:284.0 0.77 1
Chlorobenzene ND ug/kg 08/23/19 13:04 108-90-708/23/19 11:284.0 0.77 1
Chloroethane ND ug/kg 08/23/19 13:04 75-00-308/23/19 11:288.0 1.7 1
Chloroform ND ug/kg 08/23/19 13:04 67-66-308/23/19 11:284.0 0.85 1
Chloromethane ND ug/kg 08/23/19 13:04 74-87-308/23/19 11:288.0 2.6 1
2-Chlorotoluene ND ug/kg 08/23/19 13:04 95-49-808/23/19 11:284.0 1.2 1
4-Chlorotoluene ND ug/kg 08/23/19 13:04 106-43-408/23/19 11:284.0 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/23/19 13:04 96-12-808/23/19 11:284.0 2.0 1
Dibromochloromethane ND ug/kg 08/23/19 13:04 124-48-108/23/19 11:284.0 2.0 1
1,2-Dibromoethane (EDB)ND ug/kg 08/23/19 13:04 106-93-408/23/19 11:284.0 0.90 1
Dibromomethane ND ug/kg 08/23/19 13:04 74-95-308/23/19 11:284.0 1.2 1
1,2-Dichlorobenzene ND ug/kg 08/23/19 13:04 95-50-108/23/19 11:284.0 1.4 1
1,3-Dichlorobenzene ND ug/kg 08/23/19 13:04 541-73-108/23/19 11:284.0 1.4 1
1,4-Dichlorobenzene ND ug/kg 08/23/19 13:04 106-46-708/23/19 11:284.0 1.4 1
Dichlorodifluoromethane ND ug/kg 08/23/19 13:04 75-71-808/23/19 11:288.0 3.3 1
1,1-Dichloroethane ND ug/kg 08/23/19 13:04 75-34-308/23/19 11:284.0 0.59 1
1,2-Dichloroethane ND ug/kg 08/23/19 13:04 107-06-208/23/19 11:284.0 0.80 1
1,1-Dichloroethene ND ug/kg 08/23/19 13:04 75-35-408/23/19 11:284.0 0.93 1
cis-1,2-Dichloroethene ND ug/kg 08/23/19 13:04 156-59-208/23/19 11:284.0 0.69 1
trans-1,2-Dichloroethene ND ug/kg 08/23/19 13:04 156-60-508/23/19 11:284.0 0.78 1
1,2-Dichloropropane ND ug/kg 08/23/19 13:04 78-87-508/23/19 11:284.0 1.5 1
1,3-Dichloropropane ND ug/kg 08/23/19 13:04 142-28-908/23/19 11:284.0 1.5 1
2,2-Dichloropropane ND ug/kg 08/23/19 13:04 594-20-708/23/19 11:284.0 0.39 1
1,1-Dichloropropene ND ug/kg 08/23/19 13:04 563-58-6 v108/23/19 11:284.0 1.7 1
cis-1,3-Dichloropropene ND ug/kg 08/23/19 13:04 10061-01-508/23/19 11:284.0 1.8 1
trans-1,3-Dichloropropene ND ug/kg 08/23/19 13:04 10061-02-608/23/19 11:284.0 0.70 1
Diisopropyl ether ND ug/kg 08/23/19 13:04 108-20-308/23/19 11:284.0 2.3 1
Ethylbenzene ND ug/kg 08/23/19 13:04 100-41-408/23/19 11:284.0 0.85 1
Hexachloro-1,3-butadiene ND ug/kg 08/23/19 13:04 87-68-308/23/19 11:284.0 2.0 1
2-Hexanone ND ug/kg 08/23/19 13:04 591-78-608/23/19 11:2840.0 4.1 1
Isopropylbenzene (Cumene)ND ug/kg 08/23/19 13:04 98-82-808/23/19 11:284.0 1.2 1
p-Isopropyltoluene ND ug/kg 08/23/19 13:04 99-87-608/23/19 11:284.0 1.9 1
Methylene Chloride ND ug/kg 08/23/19 13:04 75-09-208/23/19 11:2816.0 4.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/23/19 13:04 108-10-108/23/19 11:2840.0 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: DUP1 Lab ID: 92442356016 Collected: 08/20/19 00:00 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 08/23/19 13:04 1634-04-408/23/19 11:284.0 2.3 1
Naphthalene ND ug/kg 08/23/19 13:04 91-20-308/23/19 11:284.0 3.4 1
n-Propylbenzene ND ug/kg 08/23/19 13:04 103-65-108/23/19 11:284.0 1.3 1
Styrene ND ug/kg 08/23/19 13:04 100-42-508/23/19 11:284.0 1.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/23/19 13:04 630-20-608/23/19 11:284.0 0.98 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/23/19 13:04 79-34-508/23/19 11:284.0 1.4 1
Tetrachloroethene ND ug/kg 08/23/19 13:04 127-18-408/23/19 11:284.0 1.3 1
Toluene ND ug/kg 08/23/19 13:04 108-88-308/23/19 11:284.0 1.3 1
1,2,3-Trichlorobenzene ND ug/kg 08/23/19 13:04 87-61-608/23/19 11:284.0 2.9 1
1,2,4-Trichlorobenzene ND ug/kg 08/23/19 13:04 120-82-108/23/19 11:284.0 2.1 1
1,1,1-Trichloroethane ND ug/kg 08/23/19 13:04 71-55-608/23/19 11:284.0 0.70 1
1,1,2-Trichloroethane ND ug/kg 08/23/19 13:04 79-00-508/23/19 11:284.0 0.90 1
Trichloroethene ND ug/kg 08/23/19 13:04 79-01-608/23/19 11:284.0 1.0 1
Trichlorofluoromethane ND ug/kg 08/23/19 13:04 75-69-408/23/19 11:284.0 0.94 1
1,2,3-Trichloropropane ND ug/kg 08/23/19 13:04 96-18-408/23/19 11:284.0 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 08/23/19 13:04 95-63-608/23/19 11:284.0 1.6 1
1,3,5-Trimethylbenzene ND ug/kg 08/23/19 13:04 108-67-808/23/19 11:284.0 1.3 1
Vinyl acetate ND ug/kg 08/23/19 13:04 108-05-408/23/19 11:2840.0 13.0 1
Vinyl chloride ND ug/kg 08/23/19 13:04 75-01-408/23/19 11:288.0 1.5 1
Xylene (Total)ND ug/kg 08/23/19 13:04 1330-20-708/23/19 11:288.0 2.8 1
m&p-Xylene ND ug/kg 08/23/19 13:04 179601-23-108/23/19 11:288.0 1.9 1
o-Xylene ND ug/kg 08/23/19 13:04 95-47-608/23/19 11:284.0 0.94 1
Surrogates
Toluene-d8 (S)105 %08/23/19 13:04 2037-26-508/23/19 11:2870-130 1
4-Bromofluorobenzene (S)100 %08/23/19 13:04 460-00-408/23/19 11:2870-130 1
1,2-Dichloroethane-d4 (S)92 %08/23/19 13:04 17060-07-008/23/19 11:2870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.8 %08/22/19 16:580.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: DUP2 Lab ID: 92442356017 Collected: 08/20/19 00:00 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 0.72 mg/kg 08/23/19 10:52 7440-38-208/22/19 11:480.71 0.36 1
Barium 55.5 mg/kg 08/23/19 10:52 7440-39-308/22/19 11:480.36 0.18 1
Cadmium 0.068J mg/kg 08/23/19 10:52 7440-43-908/22/19 11:480.071 0.036 1
Chromium 17.7 mg/kg 08/23/19 10:52 7440-47-308/22/19 11:480.36 0.18 1
Lead 6.2 mg/kg 08/23/19 10:52 7439-92-108/22/19 11:480.36 0.18 1
Selenium 1.2 mg/kg 08/23/19 10:52 7782-49-208/22/19 11:480.71 0.36 1
Silver ND mg/kg 08/23/19 10:52 7440-22-408/22/19 11:480.36 0.18 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.073 mg/kg 08/26/19 15:38 7439-97-608/22/19 14:530.0063 0.0032 2
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 08/22/19 17:29 83-32-908/22/19 10:08376 96.6 1
Acenaphthylene ND ug/kg 08/22/19 17:29 208-96-808/22/19 10:08376 88.9 1
Aniline ND ug/kg 08/22/19 17:29 62-53-308/22/19 10:08376 84.3 1
Anthracene ND ug/kg 08/22/19 17:29 120-12-708/22/19 10:08376 97.4 1
Benzo(a)anthracene ND ug/kg 08/22/19 17:29 56-55-308/22/19 10:08376 120 1
Benzo(a)pyrene ND ug/kg 08/22/19 17:29 50-32-808/22/19 10:08376 163 1
Benzo(b)fluoranthene ND ug/kg 08/22/19 17:29 205-99-208/22/19 10:08376 151 1
Benzo(g,h,i)perylene ND ug/kg 08/22/19 17:29 191-24-208/22/19 10:08376 147 1
Benzo(k)fluoranthene ND ug/kg 08/22/19 17:29 207-08-908/22/19 10:08376 158 1
Benzoic Acid ND ug/kg 08/22/19 17:29 65-85-008/22/19 10:081880 405 1
Benzyl alcohol ND ug/kg 08/22/19 17:29 100-51-608/22/19 10:08751 199 1
4-Bromophenylphenyl ether ND ug/kg 08/22/19 17:29 101-55-308/22/19 10:08376 98.6 1
Butylbenzylphthalate ND ug/kg 08/22/19 17:29 85-68-708/22/19 10:08376 100 1
4-Chloro-3-methylphenol ND ug/kg 08/22/19 17:29 59-50-708/22/19 10:08751 229 1
4-Chloroaniline ND ug/kg 08/22/19 17:29 106-47-808/22/19 10:081880 230 1
bis(2-Chloroethoxy)methane ND ug/kg 08/22/19 17:29 111-91-108/22/19 10:08376 100 1
bis(2-Chloroethyl) ether ND ug/kg 08/22/19 17:29 111-44-408/22/19 10:08376 79.8 1
2-Chloronaphthalene ND ug/kg 08/22/19 17:29 91-58-708/22/19 10:08376 83.7 1
2-Chlorophenol ND ug/kg 08/22/19 17:29 95-57-808/22/19 10:08376 87.4 1
4-Chlorophenylphenyl ether ND ug/kg 08/22/19 17:29 7005-72-308/22/19 10:08376 97.5 1
Chrysene ND ug/kg 08/22/19 17:29 218-01-908/22/19 10:08376 109 1
Dibenz(a,h)anthracene ND ug/kg 08/22/19 17:29 53-70-308/22/19 10:08376 150 1
Dibenzofuran ND ug/kg 08/22/19 17:29 132-64-908/22/19 10:08376 93.9 1
1,2-Dichlorobenzene ND ug/kg 08/22/19 17:29 95-50-108/22/19 10:08376 81.3 1
1,3-Dichlorobenzene ND ug/kg 08/22/19 17:29 541-73-108/22/19 10:08376 84.6 1
1,4-Dichlorobenzene ND ug/kg 08/22/19 17:29 106-46-708/22/19 10:08376 82.6 1
3,3'-Dichlorobenzidine ND ug/kg 08/22/19 17:29 91-94-108/22/19 10:081880 262 1
2,4-Dichlorophenol ND ug/kg 08/22/19 17:29 120-83-208/22/19 10:08376 124 1
Diethylphthalate ND ug/kg 08/22/19 17:29 84-66-208/22/19 10:08376 81.5 1
2,4-Dimethylphenol ND ug/kg 08/22/19 17:29 105-67-908/22/19 10:08376 93.6 1
Dimethylphthalate ND ug/kg 08/22/19 17:29 131-11-308/22/19 10:08376 84.9 1
Di-n-butylphthalate ND ug/kg 08/22/19 17:29 84-74-208/22/19 10:08376 92.6 1
4,6-Dinitro-2-methylphenol ND ug/kg 08/22/19 17:29 534-52-108/22/19 10:08751 605 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442356
Corey's Transmission
Sample: DUP2 Lab ID: 92442356017 Collected: 08/20/19 00:00 Received: 08/21/19 14:31 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 08/22/19 17:29 51-28-508/22/19 10:081880 1200 1
2,4-Dinitrotoluene ND ug/kg 08/22/19 17:29 121-14-208/22/19 10:08376 99.5 1
2,6-Dinitrotoluene ND ug/kg 08/22/19 17:29 606-20-208/22/19 10:08376 98.2 1
Di-n-octylphthalate ND ug/kg 08/22/19 17:29 117-84-008/22/19 10:08376 214 1
bis(2-Ethylhexyl)phthalate ND ug/kg 08/22/19 17:29 117-81-708/22/19 10:08376 123 1
Fluoranthene ND ug/kg 08/22/19 17:29 206-44-008/22/19 10:08376 113 1
Fluorene ND ug/kg 08/22/19 17:29 86-73-708/22/19 10:08376 100 1
Hexachloro-1,3-butadiene ND ug/kg 08/22/19 17:29 87-68-308/22/19 10:08376 91.3 1
Hexachlorobenzene ND ug/kg 08/22/19 17:29 118-74-108/22/19 10:08376 95.4 1
Hexachlorocyclopentadiene ND ug/kg 08/22/19 17:29 77-47-408/22/19 10:08376 150 1
Hexachloroethane ND ug/kg 08/22/19 17:29 67-72-108/22/19 10:08376 85.6 1
Indeno(1,2,3-cd)pyrene ND ug/kg 08/22/19 17:29 193-39-508/22/19 10:08376 172 1
Isophorone ND ug/kg 08/22/19 17:29 78-59-108/22/19 10:08376 81.6 1
1-Methylnaphthalene ND ug/kg 08/22/19 17:29 90-12-008/22/19 10:08376 100 1
2-Methylnaphthalene ND ug/kg 08/22/19 17:29 91-57-608/22/19 10:08376 95.6 1
2-Methylphenol(o-Cresol)ND ug/kg 08/22/19 17:29 95-48-708/22/19 10:08376 83.2 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 08/22/19 17:29 15831-10-408/22/19 10:08376 94.5 1
Naphthalene ND ug/kg 08/22/19 17:29 91-20-308/22/19 10:08376 89.9 1
2-Nitroaniline ND ug/kg 08/22/19 17:29 88-74-408/22/19 10:081880 189 1
3-Nitroaniline ND ug/kg 08/22/19 17:29 99-09-208/22/19 10:081880 199 1
4-Nitroaniline ND ug/kg 08/22/19 17:29 100-01-608/22/19 10:08751 186 1
Nitrobenzene ND ug/kg 08/22/19 17:29 98-95-308/22/19 10:08376 89.7 1
2-Nitrophenol ND ug/kg 08/22/19 17:29 88-75-508/22/19 10:08376 116 1
4-Nitrophenol ND ug/kg 08/22/19 17:29 100-02-708/22/19 10:081880 599 1
N-Nitrosodimethylamine ND ug/kg 08/22/19 17:29 62-75-908/22/19 10:08376 106 1
N-Nitroso-di-n-propylamine ND ug/kg 08/22/19 17:29 621-64-708/22/19 10:08376 105 1
N-Nitrosodiphenylamine ND ug/kg 08/22/19 17:29 86-30-608/22/19 10:08376 95.8 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 08/22/19 17:29 108-60-108/22/19 10:08376 104 1
Pentachlorophenol ND ug/kg 08/22/19 17:29 87-86-508/22/19 10:081880 172 1
Phenanthrene ND ug/kg 08/22/19 17:29 85-01-808/22/19 10:08376 94.6 1
Phenol ND ug/kg 08/22/19 17:29 108-95-208/22/19 10:08376 89.7 1
Pyrene ND ug/kg 08/22/19 17:29 129-00-008/22/19 10:08376 103 1
1,2,4-Trichlorobenzene ND ug/kg 08/22/19 17:29 120-82-108/22/19 10:08376 86.0 1
2,4,5-Trichlorophenol ND ug/kg 08/22/19 17:29 95-95-408/22/19 10:08376 97.5 1
2,4,6-Trichlorophenol ND ug/kg 08/22/19 17:29 88-06-208/22/19 10:08376 94.4 1
Surrogates
Nitrobenzene-d5 (S)65 %08/22/19 17:29 4165-60-008/22/19 10:0823-110 1
2-Fluorobiphenyl (S)60 %08/22/19 17:29 321-60-808/22/19 10:0830-110 1
Terphenyl-d14 (S)75 %08/22/19 17:29 1718-51-008/22/19 10:0828-110 1
Phenol-d6 (S)64 %08/22/19 17:29 13127-88-308/22/19 10:0822-110 1
2-Fluorophenol (S)64 %08/22/19 17:29 367-12-408/22/19 10:0813-110 1
2,4,6-Tribromophenol (S)69 %08/22/19 17:29 118-79-608/22/19 10:0827-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.4 %08/22/19 13:220.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493892
EPA 7471B
EPA 7471B
7471 Mercury
Associated Lab Samples: 92442356011, 92442356012, 92442356013, 92442356014, 92442356015, 92442356017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2661947
Associated Lab Samples:92442356011, 92442356012, 92442356013, 92442356014, 92442356015, 92442356017
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 08/23/19 15:300.0030
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2661948LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0750.083 90 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2661949MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92441602001
2661950
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 1 81 75-12581 5 201ND0.91 0.86
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493811
EPA 3050B
EPA 6010D
6010 MET
Associated Lab Samples: 92442356011, 92442356012, 92442356013, 92442356014, 92442356015, 92442356017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2661433
Associated Lab Samples:92442356011, 92442356012, 92442356013, 92442356014, 92442356015, 92442356017
Matrix: Solid
AnalyzedMDL
Arsenic mg/kg ND 1.0 08/23/19 10:150.50
Barium mg/kg ND 0.50 08/23/19 10:150.25
Cadmium mg/kg ND 0.10 08/23/19 10:150.050
Chromium mg/kg ND 0.50 08/23/19 10:150.25
Lead mg/kg ND 0.50 08/23/19 10:150.25
Selenium mg/kg ND 1.0 08/23/19 10:150.50
Silver mg/kg ND 0.50 08/23/19 10:150.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2661434LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 45.150 90 80-120
Barium mg/kg 48.950 98 80-120
Cadmium mg/kg 46.050 92 80-120
Chromium mg/kg 48.050 96 80-120
Lead mg/kg 47.150 94 80-120
Selenium mg/kg 43.450 87 80-120
Silver mg/kg 22.225 89 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2661435MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92442356011
2661436
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg M133.8 69 75-12569 11 20380.45J 23.7 26.5
Barium mg/kg 33.8 115 75-12583 6 203891.7 130 123
Cadmium mg/kg 33.8 78 75-12575 8 20380.042J 26.5 28.6
Chromium mg/kg 33.8 93 75-12580 2 203830.8 62.4 61.1
Lead mg/kg M133.8 74 75-12571 7 20383.6 28.7 30.7
Selenium mg/kg M133.8 69 75-12567 8 20380.63J 24.0 26.1
Silver mg/kg M116.9 78 75-12573 5 2019.1ND 13.2 13.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493910
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92442356001, 92442356002, 92442356003, 92442356004, 92442356005, 92442356009, 92442356010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2662023
Associated Lab Samples:92442356001, 92442356002, 92442356003, 92442356004, 92442356005, 92442356009, 92442356010
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/22/19 16:081.2
1,1,1-Trichloroethane ug/kg ND 5.0 08/22/19 16:080.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/22/19 16:081.7
1,1,2-Trichloroethane ug/kg ND 5.0 08/22/19 16:081.1
1,1-Dichloroethane ug/kg ND 5.0 08/22/19 16:080.74
1,1-Dichloroethene ug/kg ND 5.0 08/22/19 16:081.2
1,1-Dichloropropene ug/kg ND 5.0 08/22/19 16:082.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/22/19 16:083.6
1,2,3-Trichloropropane ug/kg ND 5.0 08/22/19 16:081.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/22/19 16:082.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/22/19 16:082.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/22/19 16:082.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/22/19 16:081.1
1,2-Dichlorobenzene ug/kg ND 5.0 08/22/19 16:081.8
1,2-Dichloroethane ug/kg ND 5.0 08/22/19 16:081.0
1,2-Dichloropropane ug/kg ND 5.0 08/22/19 16:081.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/22/19 16:081.7
1,3-Dichlorobenzene ug/kg ND 5.0 08/22/19 16:081.8
1,3-Dichloropropane ug/kg ND 5.0 08/22/19 16:081.9
1,4-Dichlorobenzene ug/kg ND 5.0 08/22/19 16:081.7
2,2-Dichloropropane ug/kg ND 5.0 08/22/19 16:080.49
2-Butanone (MEK)ug/kg ND 100 08/22/19 16:0811.9
2-Chlorotoluene ug/kg ND 5.0 08/22/19 16:081.5
2-Hexanone ug/kg ND 50.0 08/22/19 16:085.2
4-Chlorotoluene ug/kg ND 5.0 08/22/19 16:081.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/22/19 16:083.7
Acetone ug/kg ND 100 08/22/19 16:089.4
Benzene ug/kg ND 5.0 08/22/19 16:080.90
Bromobenzene ug/kg ND 5.0 08/22/19 16:081.4
Bromochloromethane ug/kg ND 5.0 08/22/19 16:081.2
Bromodichloromethane ug/kg ND 5.0 08/22/19 16:080.98
Bromoform ug/kg ND 5.0 08/22/19 16:082.4
Bromomethane ug/kg ND 10.0 08/22/19 16:082.4
Carbon tetrachloride ug/kg ND 5.0 08/22/19 16:080.96
Chlorobenzene ug/kg ND 5.0 08/22/19 16:080.97
Chloroethane ug/kg ND 10.0 08/22/19 16:082.1
Chloroform ug/kg ND 5.0 08/22/19 16:081.1
Chloromethane ug/kg ND 10.0 08/22/19 16:083.3
cis-1,2-Dichloroethene ug/kg ND 5.0 08/22/19 16:080.87
cis-1,3-Dichloropropene ug/kg ND 5.0 08/22/19 16:082.3
Dibromochloromethane ug/kg ND 5.0 08/22/19 16:082.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2662023
Associated Lab Samples:92442356001, 92442356002, 92442356003, 92442356004, 92442356005, 92442356009, 92442356010
Matrix: Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.0 08/22/19 16:081.5
Dichlorodifluoromethane ug/kg ND 10.0 08/22/19 16:084.1
Diisopropyl ether ug/kg ND 5.0 08/22/19 16:082.9
Ethylbenzene ug/kg ND 5.0 08/22/19 16:081.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 08/22/19 16:082.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/22/19 16:081.4
m&p-Xylene ug/kg ND 10.0 08/22/19 16:082.4
Methyl-tert-butyl ether ug/kg ND 5.0 08/22/19 16:082.9
Methylene Chloride ug/kg ND 20.0 08/22/19 16:085.9
n-Butylbenzene ug/kg ND 5.0 08/22/19 16:082.8
n-Propylbenzene ug/kg ND 5.0 08/22/19 16:081.7
Naphthalene ug/kg ND 5.0 08/22/19 16:084.2
o-Xylene ug/kg ND 5.0 08/22/19 16:081.2
p-Isopropyltoluene ug/kg ND 5.0 08/22/19 16:082.4
sec-Butylbenzene ug/kg ND 5.0 08/22/19 16:082.1
Styrene ug/kg ND 5.0 08/22/19 16:081.5
tert-Butylbenzene ug/kg ND 5.0 08/22/19 16:081.7
Tetrachloroethene ug/kg ND 5.0 08/22/19 16:081.6
Toluene ug/kg ND 5.0 08/22/19 16:081.6
trans-1,2-Dichloroethene ug/kg ND 5.0 08/22/19 16:080.98
trans-1,3-Dichloropropene ug/kg ND 5.0 08/22/19 16:080.88
Trichloroethene ug/kg ND 5.0 08/22/19 16:081.3
Trichlorofluoromethane ug/kg ND 5.0 08/22/19 16:081.2
Vinyl acetate ug/kg ND 50.0 08/22/19 16:0816.3
Vinyl chloride ug/kg ND 10.0 08/22/19 16:081.9
Xylene (Total)ug/kg ND 10.0 08/22/19 16:083.5
1,2-Dichloroethane-d4 (S)%103 70-132 08/22/19 16:08
4-Bromofluorobenzene (S)%102 70-130 08/22/19 16:08
Toluene-d8 (S)%98 70-130 08/22/19 16:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2662024LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.450 103 70-130
1,1,1-Trichloroethane ug/kg 51.150 102 70-130
1,1,2,2-Tetrachloroethane ug/kg 52.450 105 55-130
1,1,2-Trichloroethane ug/kg 52.650 105 70-130
1,1-Dichloroethane ug/kg 52.450 105 68-130
1,1-Dichloroethene ug/kg 51.050 102 70-130
1,1-Dichloropropene ug/kg 50.750 101 70-130
1,2,3-Trichlorobenzene ug/kg 52.850 106 70-130
1,2,3-Trichloropropane ug/kg 54.850 110 70-130
1,2,4-Trichlorobenzene ug/kg 50.150 100 70-130
1,2,4-Trimethylbenzene ug/kg 50.250 100 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2662024LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 57.450 115 57-141
1,2-Dibromoethane (EDB)ug/kg 55.150 110 70-130
1,2-Dichlorobenzene ug/kg 50.850 102 70-130
1,2-Dichloroethane ug/kg 50.050 100 70-130
1,2-Dichloropropane ug/kg 52.350 105 70-130
1,3,5-Trimethylbenzene ug/kg 50.850 102 70-130
1,3-Dichlorobenzene ug/kg 49.250 98 70-130
1,3-Dichloropropane ug/kg 56.150 112 70-130
1,4-Dichlorobenzene ug/kg 49.350 99 70-130
2,2-Dichloropropane ug/kg 50.250 100 70-130
2-Butanone (MEK)ug/kg 112100 112 60-130
2-Chlorotoluene ug/kg 50.150 100 70-130
2-Hexanone ug/kg 121100 121 70-132
4-Chlorotoluene ug/kg 49.650 99 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 115100 115 69-130
Acetone ug/kg 100100 100 49-148
Benzene ug/kg 53.250 106 70-130
Bromobenzene ug/kg 51.350 103 70-130
Bromochloromethane ug/kg 52.450 105 70-130
Bromodichloromethane ug/kg 52.250 104 70-130
Bromoform ug/kg 53.950 108 68-136
Bromomethane ug/kg 50.050 100 60-140
Carbon tetrachloride ug/kg 50.450 101 70-130
Chlorobenzene ug/kg 49.550 99 70-130
Chloroethane ug/kg 53.350 107 51-147
Chloroform ug/kg 50.850 102 70-130
Chloromethane ug/kg 45.950 92 48-130
cis-1,2-Dichloroethene ug/kg 51.650 103 70-130
cis-1,3-Dichloropropene ug/kg 55.750 111 70-130
Dibromochloromethane ug/kg 52.550 105 70-130
Dibromomethane ug/kg 51.950 104 70-130
Dichlorodifluoromethane ug/kg 39.950 80 49-130
Diisopropyl ether ug/kg 55.750 111 66-130
Ethylbenzene ug/kg 50.150 100 70-130
Hexachloro-1,3-butadiene ug/kg 50.850 102 70-130
Isopropylbenzene (Cumene)ug/kg 50.150 100 70-130
m&p-Xylene ug/kg 98.8100 99 70-130
Methyl-tert-butyl ether ug/kg 56.750 113 70-130
Methylene Chloride ug/kg 46.150 92 50-137
n-Butylbenzene ug/kg 51.550 103 70-130
n-Propylbenzene ug/kg 50.450 101 70-130
Naphthalene ug/kg 54.450 109 70-131
o-Xylene ug/kg 49.850 100 70-130
p-Isopropyltoluene ug/kg 51.350 103 70-130
sec-Butylbenzene ug/kg 50.750 101 70-130
Styrene ug/kg 50.350 101 70-130
tert-Butylbenzene ug/kg 46.050 92 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2662024LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 48.650 97 56-130
Toluene ug/kg 49.550 99 70-130
trans-1,2-Dichloroethene ug/kg 49.750 99 70-130
trans-1,3-Dichloropropene ug/kg 55.350 111 70-130
Trichloroethene ug/kg 51.150 102 70-141
Trichlorofluoromethane ug/kg 48.550 97 67-130
Vinyl acetate ug/kg 124100 124 10-136
Vinyl chloride ug/kg 48.550 97 67-130
Xylene (Total)ug/kg 149150 99 70-130
1,2-Dichloroethane-d4 (S)%103 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2662025MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92441913019
2662026
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 1170 85 52-13388 4 301170ND991 1030
1,1,1-Trichloroethane ug/kg 1170 87 49-13788 1 301170ND1010 1020
1,1,2,2-Tetrachloroethane ug/kg 1170 85 39-15094 10 301170ND991 1090
1,1,2-Trichloroethane ug/kg 1170 88 48-14095 8 301170ND1030 1110
1,1-Dichloroethane ug/kg 1170 89 46-13592 3 301170ND1040 1070
1,1-Dichloroethene ug/kg 1170 89 38-14990 1 301170ND1040 1050
1,1-Dichloropropene ug/kg 1170 82 41-14083 1 301170ND955 964
1,2,3-Trichlorobenzene ug/kg 1170 80 10-15885 6 301170ND931 988
1,2,3-Trichloropropane ug/kg 1170 106 33-157107 1 301170ND1240 1250
1,2,4-Trichlorobenzene ug/kg 1170 78 10-15581 4 301170ND906 940
1,2,4-Trimethylbenzene ug/kg E,M11170-133 24-154-247 12 3011701350011900 10600
1,2-Dibromo-3-
chloropropane ug/kg 1170 84 33-15887 4 301170ND974 1020
1,2-Dibromoethane (EDB) ug/kg 1170 83 40-13691 9 301170ND963 1060
1,2-Dichlorobenzene ug/kg 1170 80 27-14683 4 301170ND935 973
1,2-Dichloroethane ug/kg 1170 87 49-14090 3 301170ND1020 1050
1,2-Dichloropropane ug/kg 1170 88 44-14391 3 301170ND1030 1050
1,3,5-Trimethylbenzene ug/kg 1170 102 40-14469 9 30117031304320 3940
1,3-Dichlorobenzene ug/kg 1170 80 33-14083 4 301170ND932 968
1,3-Dichloropropane ug/kg 1170 89 47-14792 4 301170ND1040 1070
1,4-Dichlorobenzene ug/kg 1170 79 35-13983 4 301170ND923 962
2,2-Dichloropropane ug/kg 1170 90 41-14087 3 301170ND1050 1020
2-Butanone (MEK)ug/kg 2330 103 10-181108 302330ND2400J 2510J
2-Chlorotoluene ug/kg 1170 131 38-14797 29 301170ND1530 1140
2-Hexanone ug/kg 2330 85 18-16996 302330ND1980J 2230J
4-Chlorotoluene ug/kg 1170 72 36-14576 6 301170ND836 888
4-Methyl-2-pentanone
(MIBK)ug/kg 2330 90 16-17596 302330ND2090J 2230J
Acetone ug/kg 2330 85 10-200128 302330ND1980J 2990J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2662025MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92441913019
2662026
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene ug/kg 1170 106 46-13681 13 30117011302360 2070
Bromobenzene ug/kg 1170 83 38-14986 3 301170ND972 999
Bromochloromethane ug/kg 1170 90 44-14292 2 301170ND1050 1070
Bromodichloromethane ug/kg 1170 85 41-14088 3 301170ND986 1020
Bromoform ug/kg 1170 77 34-14581 5 301170ND898 941
Bromomethane ug/kg 1170 98 14-16289 10 301170ND1140 1040
Carbon tetrachloride ug/kg 1170 82 44-14184 2 301170ND961 977
Chlorobenzene ug/kg 1170 86 39-14190 5 301170ND999 1050
Chloroethane ug/kg 1170 54 10-18257 4 301170ND633 660
Chloroform ug/kg 1170 84 45-14090 6 301170ND985 1050
Chloromethane ug/kg 1170 91 19-14990 0 301170ND1060 1050
cis-1,2-Dichloroethene ug/kg 1170 89 38-15091 2 301170ND1040 1060
cis-1,3-Dichloropropene ug/kg 1170 88 30-14490 3 301170ND1020 1050
Dibromochloromethane ug/kg 1170 79 36-14585 7 301170ND918 989
Dibromomethane ug/kg 1170 83 41-14586 3 301170ND969 999
Dichlorodifluoromethane ug/kg 1170 84 16-14685 1 301170ND985 990
Diisopropyl ether ug/kg 1170 90 41-14393 4 301170ND1050 1090
Ethylbenzene ug/kg 1170 86 35-14447 10 30117036904690 4240
Hexachloro-1,3-butadiene ug/kg 1170 76 10-16079 5 301170ND885 926
Isopropylbenzene(Cumene)ug/kg 1170 84 30-15285 1 3011703001280 1290
m&p-Xylene ug/kg M123307033-145-15 10 3023301940021000 19000
Methyl-tert-butyl ether ug/kg 1170 83 49-14088 6 301170ND967 1030
Methylene Chloride ug/kg 1170 108 10-174116 7 301170ND1250 1350
n-Butylbenzene ug/kg 1170 109 10-160107 2 301170ND1270 1250
n-Propylbenzene ug/kg 1170 75 24-15964 7 30117010201890 1770
Naphthalene ug/kg 1170 51 10-17148 2 30117020502650 2600
o-Xylene ug/kg E,M1117011431-1506 11 3011701020011500 10300
p-Isopropyltoluene ug/kg 1170 79 21-15478 1 3011703101230 1220
sec-Butylbenzene ug/kg 1170 75 19-15983 10 301170ND874 963
Styrene ug/kg 1170 85 15-15287 3 301170ND987 1010
tert-Butylbenzene ug/kg 1170 74 31-14177 4 301170ND863 894
Tetrachloroethene ug/kg 1170 81 19-14184 3 301170ND949 978
Toluene ug/kg E,M11170-222 31-146-377 15 3011701590013300 11500
trans-1,2-Dichloroethene ug/kg 1170 90 28-15789 1 301170ND1050 1040
trans-1,3-Dichloropropene ug/kg 1170 86 25-14690 5 301170ND997 1050
Trichloroethene ug/kg 1170 87 34-14987 1 301170ND1010 1020
Trichlorofluoromethane ug/kg 1170 55 10-16756 1 301170ND645 650
Vinyl acetate ug/kg 2330 84 10-20090 302330ND1970J 2110J
Vinyl chloride ug/kg 1170 92 36-15591 2 301170ND1080 1060
Xylene (Total)ug/kg ES,MS34908429-148-8 10 3034902960032500 29300
1,2-Dichloroethane-d4 (S) %98 70-132106
4-Bromofluorobenzene (S) %103 70-130103
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 49 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
494122
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92442356016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2663064
Associated Lab Samples:92442356016
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/23/19 12:141.2
1,1,1-Trichloroethane ug/kg ND 5.0 08/23/19 12:140.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/23/19 12:141.7
1,1,2-Trichloroethane ug/kg ND 5.0 08/23/19 12:141.1
1,1-Dichloroethane ug/kg ND 5.0 08/23/19 12:140.74
1,1-Dichloroethene ug/kg ND 5.0 08/23/19 12:141.2
1,1-Dichloropropene ug/kg ND 5.0 v108/23/19 12:142.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/23/19 12:143.6
1,2,3-Trichloropropane ug/kg ND 5.0 08/23/19 12:141.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/23/19 12:142.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/23/19 12:142.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/23/19 12:142.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/23/19 12:141.1
1,2-Dichlorobenzene ug/kg ND 5.0 08/23/19 12:141.8
1,2-Dichloroethane ug/kg ND 5.0 08/23/19 12:141.0
1,2-Dichloropropane ug/kg ND 5.0 08/23/19 12:141.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/23/19 12:141.7
1,3-Dichlorobenzene ug/kg ND 5.0 08/23/19 12:141.8
1,3-Dichloropropane ug/kg ND 5.0 08/23/19 12:141.9
1,4-Dichlorobenzene ug/kg ND 5.0 08/23/19 12:141.7
2,2-Dichloropropane ug/kg ND 5.0 08/23/19 12:140.49
2-Butanone (MEK)ug/kg ND 100 08/23/19 12:1411.9
2-Chlorotoluene ug/kg ND 5.0 08/23/19 12:141.5
2-Hexanone ug/kg ND 50.0 08/23/19 12:145.2
4-Chlorotoluene ug/kg ND 5.0 08/23/19 12:141.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/23/19 12:143.7
Acetone ug/kg ND 100 08/23/19 12:149.4
Benzene ug/kg ND 5.0 08/23/19 12:140.90
Bromobenzene ug/kg ND 5.0 08/23/19 12:141.4
Bromochloromethane ug/kg ND 5.0 08/23/19 12:141.2
Bromodichloromethane ug/kg ND 5.0 08/23/19 12:140.98
Bromoform ug/kg ND 5.0 08/23/19 12:142.4
Bromomethane ug/kg ND 10.0 08/23/19 12:142.4
Carbon tetrachloride ug/kg ND 5.0 08/23/19 12:140.96
Chlorobenzene ug/kg ND 5.0 08/23/19 12:140.97
Chloroethane ug/kg ND 10.0 08/23/19 12:142.1
Chloroform ug/kg ND 5.0 08/23/19 12:141.1
Chloromethane ug/kg ND 10.0 08/23/19 12:143.3
cis-1,2-Dichloroethene ug/kg ND 5.0 08/23/19 12:140.87
cis-1,3-Dichloropropene ug/kg ND 5.0 08/23/19 12:142.3
Dibromochloromethane ug/kg ND 5.0 08/23/19 12:142.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
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Huntersville, NC 28078
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Page 50 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2663064
Associated Lab Samples:92442356016
Matrix: Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.0 08/23/19 12:141.5
Dichlorodifluoromethane ug/kg ND 10.0 08/23/19 12:144.1
Diisopropyl ether ug/kg ND 5.0 08/23/19 12:142.9
Ethylbenzene ug/kg ND 5.0 08/23/19 12:141.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 08/23/19 12:142.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/23/19 12:141.4
m&p-Xylene ug/kg ND 10.0 08/23/19 12:142.4
Methyl-tert-butyl ether ug/kg ND 5.0 08/23/19 12:142.9
Methylene Chloride ug/kg ND 20.0 08/23/19 12:145.9
n-Butylbenzene ug/kg ND 5.0 08/23/19 12:142.8
n-Propylbenzene ug/kg ND 5.0 08/23/19 12:141.7
Naphthalene ug/kg ND 5.0 08/23/19 12:144.2
o-Xylene ug/kg ND 5.0 08/23/19 12:141.2
p-Isopropyltoluene ug/kg ND 5.0 08/23/19 12:142.4
sec-Butylbenzene ug/kg ND 5.0 08/23/19 12:142.1
Styrene ug/kg ND 5.0 08/23/19 12:141.5
tert-Butylbenzene ug/kg ND 5.0 08/23/19 12:141.7
Tetrachloroethene ug/kg ND 5.0 08/23/19 12:141.6
Toluene ug/kg ND 5.0 08/23/19 12:141.6
trans-1,2-Dichloroethene ug/kg ND 5.0 08/23/19 12:140.98
trans-1,3-Dichloropropene ug/kg ND 5.0 08/23/19 12:140.88
Trichloroethene ug/kg ND 5.0 08/23/19 12:141.3
Trichlorofluoromethane ug/kg ND 5.0 08/23/19 12:141.2
Vinyl acetate ug/kg ND 50.0 08/23/19 12:1416.3
Vinyl chloride ug/kg ND 10.0 08/23/19 12:141.9
Xylene (Total)ug/kg ND 10.0 08/23/19 12:143.5
1,2-Dichloroethane-d4 (S)%98 70-132 08/23/19 12:14
4-Bromofluorobenzene (S)%103 70-130 08/23/19 12:14
Toluene-d8 (S)%108 70-130 08/23/19 12:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2663065LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 52.450 105 70-130
1,1,1-Trichloroethane ug/kg 53.450 107 70-130
1,1,2,2-Tetrachloroethane ug/kg 50.750 101 55-130
1,1,2-Trichloroethane ug/kg 52.650 105 70-130
1,1-Dichloroethane ug/kg 55.750 111 68-130
1,1-Dichloroethene ug/kg 54.950 110 70-130
1,1-Dichloropropene ug/kg 53.1 v150106 70-130
1,2,3-Trichlorobenzene ug/kg 52.950 106 70-130
1,2,3-Trichloropropane ug/kg 52.450 105 70-130
1,2,4-Trichlorobenzene ug/kg 53.250 106 70-130
1,2,4-Trimethylbenzene ug/kg 48.650 97 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2663065LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 53.550 107 57-141
1,2-Dibromoethane (EDB)ug/kg 48.250 96 70-130
1,2-Dichlorobenzene ug/kg 50.750 101 70-130
1,2-Dichloroethane ug/kg 51.850 104 70-130
1,2-Dichloropropane ug/kg 53.750 107 70-130
1,3,5-Trimethylbenzene ug/kg 52.550 105 70-130
1,3-Dichlorobenzene ug/kg 51.150 102 70-130
1,3-Dichloropropane ug/kg 53.750 107 70-130
1,4-Dichlorobenzene ug/kg 50.250 100 70-130
2,2-Dichloropropane ug/kg 54.350 109 70-130
2-Butanone (MEK)ug/kg 105100 105 60-130
2-Chlorotoluene ug/kg 52.150 104 70-130
2-Hexanone ug/kg 107100 107 70-132
4-Chlorotoluene ug/kg 48.550 97 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 103100 103 69-130
Acetone ug/kg 108100 108 49-148
Benzene ug/kg 54.250 108 70-130
Bromobenzene ug/kg 51.050 102 70-130
Bromochloromethane ug/kg 52.150 104 70-130
Bromodichloromethane ug/kg 53.250 106 70-130
Bromoform ug/kg 51.350 103 68-136
Bromomethane ug/kg 54.750 109 60-140
Carbon tetrachloride ug/kg 53.250 106 70-130
Chlorobenzene ug/kg 50.850 102 70-130
Chloroethane ug/kg 56.850 114 51-147
Chloroform ug/kg 55.150 110 70-130
Chloromethane ug/kg 46.450 93 48-130
cis-1,2-Dichloroethene ug/kg 54.750 109 70-130
cis-1,3-Dichloropropene ug/kg 56.150 112 70-130
Dibromochloromethane ug/kg 46.550 93 70-130
Dibromomethane ug/kg 50.850 102 70-130
Dichlorodifluoromethane ug/kg 47.750 95 49-130
Diisopropyl ether ug/kg 46.550 93 66-130
Ethylbenzene ug/kg 51.350 103 70-130
Hexachloro-1,3-butadiene ug/kg 53.050 106 70-130
Isopropylbenzene (Cumene)ug/kg 52.650 105 70-130
m&p-Xylene ug/kg 103100 103 70-130
Methyl-tert-butyl ether ug/kg 48.850 98 70-130
Methylene Chloride ug/kg 46.750 93 50-137
n-Butylbenzene ug/kg 52.750 105 70-130
n-Propylbenzene ug/kg 52.450 105 70-130
Naphthalene ug/kg 52.050 104 70-131
o-Xylene ug/kg 52.050 104 70-130
p-Isopropyltoluene ug/kg 53.450 107 70-130
sec-Butylbenzene ug/kg 53.350 107 70-130
Styrene ug/kg 51.950 104 70-130
tert-Butylbenzene ug/kg 48.350 97 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2663065LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 51.150 102 56-130
Toluene ug/kg 50.850 102 70-130
trans-1,2-Dichloroethene ug/kg 53.650 107 70-130
trans-1,3-Dichloropropene ug/kg 53.750 107 70-130
Trichloroethene ug/kg 53.250 106 70-141
Trichlorofluoromethane ug/kg 52.550 105 67-130
Vinyl acetate ug/kg 112100 112 10-136
Vinyl chloride ug/kg 52.050 104 67-130
Xylene (Total)ug/kg 155150 103 70-130
1,2-Dichloroethane-d4 (S)%97 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2663067MATRIX SPIKE SAMPLE:
MSSpike
Result
92442568003
1,1,1,2-Tetrachloroethane ug/kg 23.127.1 85 52-133<7.0
1,1,1-Trichloroethane ug/kg 23.527.1 87 49-137<7.0
1,1,2,2-Tetrachloroethane ug/kg 24.227.1 89 39-150<7.0
1,1,2-Trichloroethane ug/kg 22.827.1 84 48-140<7.0
1,1-Dichloroethane ug/kg 25.027.1 92 46-135<7.0
1,1-Dichloroethene ug/kg 24.627.1 91 38-149<7.0
1,1-Dichloropropene ug/kg 23.9 v127.1 88 41-140<7.0
1,2,3-Trichlorobenzene ug/kg 23.627.1 87 10-158<7.0
1,2,3-Trichloropropane ug/kg 24.827.1 91 33-157<7.0
1,2,4-Trichlorobenzene ug/kg 23.227.1 86 10-155<7.0
1,2,4-Trimethylbenzene ug/kg 68.227.1 92 24-15443.3
1,2-Dibromo-3-chloropropane ug/kg 22.427.1 83 33-158<7.0
1,2-Dibromoethane (EDB)ug/kg 24.027.1 88 40-136<7.0
1,2-Dichlorobenzene ug/kg 22.527.1 83 27-146<7.0
1,2-Dichloroethane ug/kg 23.727.1 87 49-140<7.0
1,2-Dichloropropane ug/kg 22.827.1 84 44-143<7.0
1,3,5-Trimethylbenzene ug/kg 34.827.1 94 40-1449.4
1,3-Dichlorobenzene ug/kg 22.527.1 83 33-140<7.0
1,3-Dichloropropane ug/kg 24.727.1 91 47-147<7.0
1,4-Dichlorobenzene ug/kg 22.227.1 82 35-139<7.0
2,2-Dichloropropane ug/kg 24.027.1 88 41-140<7.0
2-Butanone (MEK)ug/kg 63.4J54.2 117 10-181<140
2-Chlorotoluene ug/kg 21.827.1 80 38-147<7.0
2-Hexanone ug/kg 46.7J54.2 86 18-169<70.2
4-Chlorotoluene ug/kg 22.327.1 82 36-145<7.0
4-Methyl-2-pentanone (MIBK)ug/kg 49.4J54.2 91 16-175<70.2
Acetone ug/kg 59.6J54.2 110 10-200<140
Benzene ug/kg 265 M127.1 178 46-136217
Bromobenzene ug/kg 22.627.1 83 38-149<7.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2663067MATRIX SPIKE SAMPLE:
MSSpike
Result
92442568003
Bromochloromethane ug/kg 23.627.1 87 44-142<7.0
Bromodichloromethane ug/kg 22.427.1 82 41-140<7.0
Bromoform ug/kg 22.127.1 82 34-145<7.0
Bromomethane ug/kg 27.527.1 101 14-162<14.0
Carbon tetrachloride ug/kg 21.927.1 81 44-141<7.0
Chlorobenzene ug/kg 22.427.1 83 39-141<7.0
Chloroethane ug/kg 24.827.1 91 10-182<14.0
Chloroform ug/kg 21.927.1 81 45-140<7.0
Chloromethane ug/kg 23.427.1 86 19-149<14.0
cis-1,2-Dichloroethene ug/kg 23.527.1 87 38-150<7.0
cis-1,3-Dichloropropene ug/kg 23.127.1 85 30-144<7.0
Dibromochloromethane ug/kg 22.427.1 83 36-145<7.0
Dibromomethane ug/kg 22.127.1 82 41-145<7.0
Dichlorodifluoromethane ug/kg 22.827.1 84 16-146<14.0
Diisopropyl ether ug/kg 24.927.1 92 41-143<7.0
Ethylbenzene ug/kg 83.927.1 109 35-14454.4
Hexachloro-1,3-butadiene ug/kg 22.827.1 84 10-160<7.0
Isopropylbenzene (Cumene)ug/kg 26.727.1 89 30-152<7.0
m&p-Xylene ug/kg 24254.2 113 33-145181
Methyl-tert-butyl ether ug/kg 24.627.1 91 49-140<7.0
Methylene Chloride ug/kg 19.3J27.1 71 10-174<28.1
n-Butylbenzene ug/kg 23.927.1 88 10-160<7.0
n-Propylbenzene ug/kg 30.427.1 90 24-159<7.0
Naphthalene ug/kg 26.327.1 79 10-171<7.0
o-Xylene ug/kg 12927.1 102 31-150101
p-Isopropyltoluene ug/kg 24.527.1 86 21-154<7.0
sec-Butylbenzene ug/kg 24.027.1 88 19-159<7.0
Styrene ug/kg 22.727.1 84 15-152<7.0
tert-Butylbenzene ug/kg 20.427.1 75 31-141<7.0
Tetrachloroethene ug/kg 23.227.1 86 19-141<7.0
Toluene ug/kg 595 E27.1 -5260 31-1462020
trans-1,2-Dichloroethene ug/kg 23.327.1 86 28-157<7.0
trans-1,3-Dichloropropene ug/kg 22.627.1 83 25-146<7.0
Trichloroethene ug/kg 22.727.1 84 34-149<7.0
Trichlorofluoromethane ug/kg 24.427.1 90 10-167<7.0
Vinyl acetate ug/kg 52.3J54.2 96 10-200<70.2
Vinyl chloride ug/kg 22.727.1 84 36-155<14.0
Xylene (Total)ug/kg 37181.5 110 29-148282
1,2-Dichloroethane-d4 (S)%103 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92442261003
2663066SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND<7.1
1,1,1-Trichloroethane ug/kg ND<7.1
1,1,2,2-Tetrachloroethane ug/kg ND<7.1
1,1,2-Trichloroethane ug/kg ND<7.1
1,1-Dichloroethane ug/kg ND<7.1
1,1-Dichloroethene ug/kg ND<7.1
1,1-Dichloropropene ug/kg ND v1<7.1
1,2,3-Trichlorobenzene ug/kg ND<7.1
1,2,3-Trichloropropane ug/kg ND<7.1
1,2,4-Trichlorobenzene ug/kg ND<7.1
1,2,4-Trimethylbenzene ug/kg 223186
1,2-Dibromo-3-chloropropane ug/kg ND<7.1
1,2-Dibromoethane (EDB)ug/kg ND<7.1
1,2-Dichlorobenzene ug/kg ND<7.1
1,2-Dichloroethane ug/kg ND<7.1
1,2-Dichloropropane ug/kg ND<7.1
1,3,5-Trimethylbenzene ug/kg 51.639.2
1,3-Dichlorobenzene ug/kg ND<7.1
1,3-Dichloropropane ug/kg ND<7.1
1,4-Dichlorobenzene ug/kg ND<7.1
2,2-Dichloropropane ug/kg ND<7.1
2-Butanone (MEK)ug/kg ND<142
2-Chlorotoluene ug/kg ND<7.1
2-Hexanone ug/kg ND<70.9
4-Chlorotoluene ug/kg ND<7.1
4-Methyl-2-pentanone (MIBK)ug/kg ND<70.9
Acetone ug/kg ND<142
Benzene ug/kg 1070269
Bromobenzene ug/kg ND<7.1
Bromochloromethane ug/kg ND<7.1
Bromodichloromethane ug/kg ND<7.1
Bromoform ug/kg ND<7.1
Bromomethane ug/kg ND<14.2
Carbon tetrachloride ug/kg ND<7.1
Chlorobenzene ug/kg ND<7.1
Chloroethane ug/kg ND<14.2
Chloroform ug/kg ND<7.1
Chloromethane ug/kg ND<14.2
cis-1,2-Dichloroethene ug/kg ND<7.1
cis-1,3-Dichloropropene ug/kg ND<7.1
Dibromochloromethane ug/kg ND<7.1
Dibromomethane ug/kg ND<7.1
Dichlorodifluoromethane ug/kg ND<14.2
Diisopropyl ether ug/kg ND<7.1
Ethylbenzene ug/kg 149113
Hexachloro-1,3-butadiene ug/kg ND<7.1
Isopropylbenzene (Cumene)ug/kg 10.1<7.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92442261003
2663066SAMPLE DUPLICATE:
m&p-Xylene ug/kg 513399
Methyl-tert-butyl ether ug/kg ND<7.1
Methylene Chloride ug/kg ND<28.4
n-Butylbenzene ug/kg ND<7.1
n-Propylbenzene ug/kg 24.817.1
Naphthalene ug/kg 29.338.3
o-Xylene ug/kg 994267
p-Isopropyltoluene ug/kg 7.6<7.1
sec-Butylbenzene ug/kg ND<7.1
Styrene ug/kg ND<7.1
tert-Butylbenzene ug/kg ND<7.1
Tetrachloroethene ug/kg ND<7.1
Toluene ug/kg 4700 2 304600
trans-1,2-Dichloroethene ug/kg ND<7.1
trans-1,3-Dichloropropene ug/kg ND<7.1
Trichloroethene ug/kg ND<7.1
Trichlorofluoromethane ug/kg ND<7.1
Vinyl acetate ug/kg ND<70.9
Vinyl chloride ug/kg ND<14.2
Xylene (Total)ug/kg 1460666
1,2-Dichloroethane-d4 (S)%110103
4-Bromofluorobenzene (S)%9998
Toluene-d8 (S)%9294
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 56 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
494145
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92442356006, 92442356007, 92442356008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2663208
Associated Lab Samples:92442356006, 92442356007, 92442356008
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/23/19 12:421.2
1,1,1-Trichloroethane ug/kg ND 5.0 08/23/19 12:420.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/23/19 12:421.7
1,1,2-Trichloroethane ug/kg ND 5.0 08/23/19 12:421.1
1,1-Dichloroethane ug/kg ND 5.0 08/23/19 12:420.74
1,1-Dichloroethene ug/kg ND 5.0 08/23/19 12:421.2
1,1-Dichloropropene ug/kg ND 5.0 08/23/19 12:422.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/23/19 12:423.6
1,2,3-Trichloropropane ug/kg ND 5.0 08/23/19 12:421.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/23/19 12:422.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/23/19 12:422.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/23/19 12:422.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/23/19 12:421.1
1,2-Dichlorobenzene ug/kg ND 5.0 08/23/19 12:421.8
1,2-Dichloroethane ug/kg ND 5.0 08/23/19 12:421.0
1,2-Dichloropropane ug/kg ND 5.0 08/23/19 12:421.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/23/19 12:421.7
1,3-Dichlorobenzene ug/kg ND 5.0 08/23/19 12:421.8
1,3-Dichloropropane ug/kg ND 5.0 08/23/19 12:421.9
1,4-Dichlorobenzene ug/kg ND 5.0 08/23/19 12:421.7
2,2-Dichloropropane ug/kg ND 5.0 08/23/19 12:420.49
2-Butanone (MEK)ug/kg ND 100 08/23/19 12:4211.9
2-Chlorotoluene ug/kg ND 5.0 08/23/19 12:421.5
2-Hexanone ug/kg ND 50.0 v108/23/19 12:425.2
4-Chlorotoluene ug/kg ND 5.0 08/23/19 12:421.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/23/19 12:423.7
Acetone ug/kg 40.4J 100 v108/23/19 12:429.4
Benzene ug/kg ND 5.0 08/23/19 12:420.90
Bromobenzene ug/kg ND 5.0 08/23/19 12:421.4
Bromochloromethane ug/kg ND 5.0 08/23/19 12:421.2
Bromodichloromethane ug/kg ND 5.0 08/23/19 12:420.98
Bromoform ug/kg ND 5.0 08/23/19 12:422.4
Bromomethane ug/kg ND 10.0 v108/23/19 12:422.4
Carbon tetrachloride ug/kg ND 5.0 08/23/19 12:420.96
Chlorobenzene ug/kg ND 5.0 08/23/19 12:420.97
Chloroethane ug/kg ND 10.0 08/23/19 12:422.1
Chloroform ug/kg ND 5.0 08/23/19 12:421.1
Chloromethane ug/kg ND 10.0 v108/23/19 12:423.3
cis-1,2-Dichloroethene ug/kg ND 5.0 08/23/19 12:420.87
cis-1,3-Dichloropropene ug/kg ND 5.0 08/23/19 12:422.3
Dibromochloromethane ug/kg ND 5.0 08/23/19 12:422.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2663208
Associated Lab Samples:92442356006, 92442356007, 92442356008
Matrix: Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.0 08/23/19 12:421.5
Dichlorodifluoromethane ug/kg ND 10.0 08/23/19 12:424.1
Diisopropyl ether ug/kg ND 5.0 08/23/19 12:422.9
Ethylbenzene ug/kg ND 5.0 08/23/19 12:421.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 08/23/19 12:422.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/23/19 12:421.4
m&p-Xylene ug/kg ND 10.0 08/23/19 12:422.4
Methyl-tert-butyl ether ug/kg ND 5.0 08/23/19 12:422.9
Methylene Chloride ug/kg ND 20.0 08/23/19 12:425.9
n-Butylbenzene ug/kg ND 5.0 08/23/19 12:422.8
n-Propylbenzene ug/kg ND 5.0 08/23/19 12:421.7
Naphthalene ug/kg ND 5.0 08/23/19 12:424.2
o-Xylene ug/kg ND 5.0 08/23/19 12:421.2
p-Isopropyltoluene ug/kg ND 5.0 08/23/19 12:422.4
sec-Butylbenzene ug/kg ND 5.0 08/23/19 12:422.1
Styrene ug/kg ND 5.0 08/23/19 12:421.5
tert-Butylbenzene ug/kg ND 5.0 08/23/19 12:421.7
Tetrachloroethene ug/kg ND 5.0 08/23/19 12:421.6
Toluene ug/kg ND 5.0 08/23/19 12:421.6
trans-1,2-Dichloroethene ug/kg ND 5.0 08/23/19 12:420.98
trans-1,3-Dichloropropene ug/kg ND 5.0 08/23/19 12:420.88
Trichloroethene ug/kg ND 5.0 08/23/19 12:421.3
Trichlorofluoromethane ug/kg ND 5.0 08/23/19 12:421.2
Vinyl acetate ug/kg ND 50.0 v108/23/19 12:4216.3
Vinyl chloride ug/kg ND 10.0 08/23/19 12:421.9
Xylene (Total)ug/kg ND 10.0 08/23/19 12:423.5
1,2-Dichloroethane-d4 (S)%101 70-132 08/23/19 12:42
4-Bromofluorobenzene (S)%109 70-130 08/23/19 12:42
Toluene-d8 (S)%100 70-130 08/23/19 12:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2663209LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2663210
1,1,1,2-Tetrachloroethane ug/kg 50.650 101 70-13010250.8 0 30
1,1,1-Trichloroethane ug/kg 48.650 97 70-1309848.8 0 30
1,1,2,2-Tetrachloroethane ug/kg 53.050 106 55-13010653.0 0 30
1,1,2-Trichloroethane ug/kg 51.450 103 70-13010452.1 1 30
1,1-Dichloroethane ug/kg 49.550 99 68-1309648.1 3 30
1,1-Dichloroethene ug/kg 50.550 101 70-13010753.3 5 30
1,1-Dichloropropene ug/kg 50.250 100 70-1309849.0 2 30
1,2,3-Trichlorobenzene ug/kg 52.950 106 70-1309849.1 7 30
1,2,3-Trichloropropane ug/kg 56.150 112 70-13011054.8 2 30
1,2,4-Trichlorobenzene ug/kg 52.650 105 70-1309949.3 7 30
1,2,4-Trimethylbenzene ug/kg 51.950 104 69-1309949.6 4 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2663209LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2663210
1,2-Dibromo-3-chloropropane ug/kg 55.550 111 57-14111055.2 0 30
1,2-Dibromoethane (EDB)ug/kg 51.650 103 70-13010150.4 2 30
1,2-Dichlorobenzene ug/kg 50.250 100 70-1309748.6 3 30
1,2-Dichloroethane ug/kg 46.350 93 70-1309446.9 1 30
1,2-Dichloropropane ug/kg 50.950 102 70-13010150.5 1 30
1,3,5-Trimethylbenzene ug/kg 52.050 104 70-13010050.0 4 30
1,3-Dichlorobenzene ug/kg 49.950 100 70-1309848.8 2 30
1,3-Dichloropropane ug/kg 51.150 102 70-13010150.6 1 30
1,4-Dichlorobenzene ug/kg 50.250 100 70-1309648.1 4 30
2,2-Dichloropropane ug/kg 50.450 101 70-13010150.3 0 30
2-Butanone (MEK)ug/kg 108100 108 60-130109109 1 30
2-Chlorotoluene ug/kg 51.550 103 70-13010049.9 3 30
2-Hexanone ug/kg 113 v110011370-132112112 1 30
4-Chlorotoluene ug/kg 51.550 103 70-1309949.4 4 30
4-Methyl-2-pentanone (MIBK)ug/kg 113100 113 69-130114114 1 30
Acetone ug/kg 118 v110011849-148124124 4 30
Benzene ug/kg 51.050 102 70-13010251.1 0 30
Bromobenzene ug/kg 53.650 107 70-13010451.8 3 30
Bromochloromethane ug/kg 48.950 98 70-1309748.7 0 30
Bromodichloromethane ug/kg 51.750 103 70-13010351.5 0 30
Bromoform ug/kg 54.550 109 68-13610753.6 2 30
Bromomethane ug/kg 64.3 v15012960-14013768.7 7 30
Carbon tetrachloride ug/kg 50.250 100 70-1309949.4 2 30
Chlorobenzene ug/kg 50.150 100 70-1309848.8 3 30
Chloroethane ug/kg 50.750 101 51-14710150.7 0 30
Chloroform ug/kg 49.950 100 70-13010049.9 0 30
Chloromethane ug/kg 57.0 v15011448-13011758.6 3 30
cis-1,2-Dichloroethene ug/kg 48.950 98 70-1309949.7 2 30
cis-1,3-Dichloropropene ug/kg 55.250 110 70-13011055.0 0 30
Dibromochloromethane ug/kg 50.950 102 70-13010050.2 1 30
Dibromomethane ug/kg 50.450 101 70-1309949.6 2 30
Dichlorodifluoromethane ug/kg 43.450 87 49-1308341.5 4 30
Diisopropyl ether ug/kg 50.550 101 66-13010351.5 2 30
Ethylbenzene ug/kg 50.750 101 70-1309949.6 2 30
Hexachloro-1,3-butadiene ug/kg 49.450 99 70-1309145.7 8 30
Isopropylbenzene (Cumene)ug/kg 52.050 104 70-13010150.6 3 30
m&p-Xylene ug/kg 103100 103 70-130100100 2 30
Methyl-tert-butyl ether ug/kg 51.450 103 70-13010150.4 2 30
Methylene Chloride ug/kg 48.950 98 50-1379748.6 1 30
n-Butylbenzene ug/kg 50.250 100 70-1309547.7 5 30
n-Propylbenzene ug/kg 52.750 105 70-13010251.0 3 30
Naphthalene ug/kg 52.550 105 70-13110049.9 5 30
o-Xylene ug/kg 51.450 103 70-13010150.7 1 30
p-Isopropyltoluene ug/kg 52.150 104 70-1309949.7 5 30
sec-Butylbenzene ug/kg 52.350 105 70-13010150.5 3 30
Styrene ug/kg 51.650 103 70-13010150.7 2 30
tert-Butylbenzene ug/kg 46.450 93 69-1309045.0 3 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2663209LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2663210
Tetrachloroethene ug/kg 51.050 102 56-1309748.3 6 30
Toluene ug/kg 49.850 100 70-1309849.2 1 30
trans-1,2-Dichloroethene ug/kg 49.850 100 70-1309849.1 1 30
trans-1,3-Dichloropropene ug/kg 54.150 108 70-13010854.2 0 30
Trichloroethene ug/kg 51.150 102 70-14110049.9 3 30
Trichlorofluoromethane ug/kg 48.250 96 67-1309547.6 1 30
Vinyl acetate ug/kg 136 v110013610-136128128 6 30
Vinyl chloride ug/kg 50.950 102 67-13010150.4 1 30
Xylene (Total)ug/kg 154150 103 70-130101151 2 30
1,2-Dichloroethane-d4 (S)%96 70-13298
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%100 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493821
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples: 92442356011, 92442356012, 92442356013, 92442356014, 92442356015, 92442356017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2661491
Associated Lab Samples:92442356011, 92442356012, 92442356013, 92442356014, 92442356015, 92442356017
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 329 08/22/19 13:3775.3
1,2-Dichlorobenzene ug/kg ND 329 08/22/19 13:3771.2
1,3-Dichlorobenzene ug/kg ND 329 08/22/19 13:3774.1
1,4-Dichlorobenzene ug/kg ND 329 08/22/19 13:3772.4
1-Methylnaphthalene ug/kg ND 329 08/22/19 13:3787.6
2,2'-Oxybis(1-chloropropane)ug/kg ND 329 08/22/19 13:3791.4
2,4,5-Trichlorophenol ug/kg ND 329 08/22/19 13:3785.4
2,4,6-Trichlorophenol ug/kg ND 329 08/22/19 13:3782.6
2,4-Dichlorophenol ug/kg ND 329 08/22/19 13:37109
2,4-Dimethylphenol ug/kg ND 329 08/22/19 13:3781.9
2,4-Dinitrophenol ug/kg ND 1640 08/22/19 13:371050
2,4-Dinitrotoluene ug/kg ND 329 08/22/19 13:3787.1
2,6-Dinitrotoluene ug/kg ND 329 08/22/19 13:3786.0
2-Chloronaphthalene ug/kg ND 329 08/22/19 13:3773.3
2-Chlorophenol ug/kg ND 329 08/22/19 13:3776.5
2-Methylnaphthalene ug/kg ND 329 08/22/19 13:3783.7
2-Methylphenol(o-Cresol)ug/kg ND 329 08/22/19 13:3772.9
2-Nitroaniline ug/kg ND 1640 08/22/19 13:37165
2-Nitrophenol ug/kg ND 329 08/22/19 13:37102
3&4-Methylphenol(m&p Cresol)ug/kg ND 329 08/22/19 13:3782.7
3,3'-Dichlorobenzidine ug/kg ND 1640 08/22/19 13:37229
3-Nitroaniline ug/kg ND 1640 08/22/19 13:37174
4,6-Dinitro-2-methylphenol ug/kg ND 658 08/22/19 13:37530
4-Bromophenylphenyl ether ug/kg ND 329 08/22/19 13:3786.3
4-Chloro-3-methylphenol ug/kg ND 658 08/22/19 13:37200
4-Chloroaniline ug/kg ND 1640 08/22/19 13:37201
4-Chlorophenylphenyl ether ug/kg ND 329 08/22/19 13:3785.4
4-Nitroaniline ug/kg ND 658 08/22/19 13:37162
4-Nitrophenol ug/kg ND 1640 08/22/19 13:37524
Acenaphthene ug/kg ND 329 08/22/19 13:3784.6
Acenaphthylene ug/kg ND 329 08/22/19 13:3777.8
Aniline ug/kg ND 329 08/22/19 13:3773.9
Anthracene ug/kg ND 329 08/22/19 13:3785.3
Benzo(a)anthracene ug/kg ND 329 08/22/19 13:37105
Benzo(a)pyrene ug/kg ND 329 08/22/19 13:37143
Benzo(b)fluoranthene ug/kg ND 329 08/22/19 13:37133
Benzo(g,h,i)perylene ug/kg ND 329 08/22/19 13:37129
Benzo(k)fluoranthene ug/kg ND 329 08/22/19 13:37139
Benzoic Acid ug/kg ND 1640 08/22/19 13:37355
Benzyl alcohol ug/kg ND 658 08/22/19 13:37174
bis(2-Chloroethoxy)methane ug/kg ND 329 08/22/19 13:3787.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2661491
Associated Lab Samples:92442356011, 92442356012, 92442356013, 92442356014, 92442356015, 92442356017
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 329 08/22/19 13:3769.9
bis(2-Ethylhexyl)phthalate ug/kg ND 329 08/22/19 13:37108
Butylbenzylphthalate ug/kg ND 329 08/22/19 13:3787.6
Chrysene ug/kg ND 329 08/22/19 13:3795.5
Di-n-butylphthalate ug/kg ND 329 08/22/19 13:3781.1
Di-n-octylphthalate ug/kg ND 329 08/22/19 13:37187
Dibenz(a,h)anthracene ug/kg ND 329 08/22/19 13:37132
Dibenzofuran ug/kg ND 329 08/22/19 13:3782.2
Diethylphthalate ug/kg ND 329 08/22/19 13:3771.4
Dimethylphthalate ug/kg ND 329 08/22/19 13:3774.4
Fluoranthene ug/kg ND 329 08/22/19 13:3799.4
Fluorene ug/kg ND 329 08/22/19 13:3788.0
Hexachloro-1,3-butadiene ug/kg ND 329 08/22/19 13:3779.9
Hexachlorobenzene ug/kg ND 329 08/22/19 13:3783.5
Hexachlorocyclopentadiene ug/kg ND 329 08/22/19 13:37132
Hexachloroethane ug/kg ND 329 08/22/19 13:3775.0
Indeno(1,2,3-cd)pyrene ug/kg ND 329 08/22/19 13:37150
Isophorone ug/kg ND 329 08/22/19 13:3771.5
N-Nitroso-di-n-propylamine ug/kg ND 329 08/22/19 13:3792.1
N-Nitrosodimethylamine ug/kg ND 329 08/22/19 13:3792.5
N-Nitrosodiphenylamine ug/kg ND 329 08/22/19 13:3783.9
Naphthalene ug/kg ND 329 08/22/19 13:3778.7
Nitrobenzene ug/kg ND 329 08/22/19 13:3778.5
Pentachlorophenol ug/kg ND 1640 08/22/19 13:37150
Phenanthrene ug/kg ND 329 08/22/19 13:3782.8
Phenol ug/kg ND 329 08/22/19 13:3778.5
Pyrene ug/kg ND 329 08/22/19 13:3790.5
2,4,6-Tribromophenol (S)%88 27-110 08/22/19 13:37
2-Fluorobiphenyl (S)%72 30-110 08/22/19 13:37
2-Fluorophenol (S)%68 13-110 08/22/19 13:37
Nitrobenzene-d5 (S)%69 23-110 08/22/19 13:37
Phenol-d6 (S)%68 22-110 08/22/19 13:37
Terphenyl-d14 (S)%87 28-110 08/22/19 13:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2661492LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12101660 73 52-130
1,2-Dichlorobenzene ug/kg 11501660 70 51-130
1,3-Dichlorobenzene ug/kg 11601660 70 50-130
1,4-Dichlorobenzene ug/kg 11801660 71 49-130
1-Methylnaphthalene ug/kg 12801660 77 55-130
2,2'-Oxybis(1-chloropropane)ug/kg 15601660 94 30-130
2,4,5-Trichlorophenol ug/kg 12401660 75 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2661492LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 13301660 80 57-130
2,4-Dichlorophenol ug/kg 12801660 77 56-130
2,4-Dimethylphenol ug/kg 13001660 79 51-130
2,4-Dinitrophenol ug/kg 63408280 77 27-133
2,4-Dinitrotoluene ug/kg 12901660 78 61-130
2,6-Dinitrotoluene ug/kg 13101660 79 60-130
2-Chloronaphthalene ug/kg 12101660 73 52-130
2-Chlorophenol ug/kg 12601660 76 54-130
2-Methylnaphthalene ug/kg 13301660 80 54-130
2-Methylphenol(o-Cresol)ug/kg 12001660 72 51-130
2-Nitroaniline ug/kg 29203310 88 51-130
2-Nitrophenol ug/kg 12401660 75 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 12001660 73 11-163
3,3'-Dichlorobenzidine ug/kg 27903310 84 10-132
3-Nitroaniline ug/kg 27003310 81 55-130
4,6-Dinitro-2-methylphenol ug/kg 28703310 87 47-142
4-Bromophenylphenyl ether ug/kg 15101660 91 59-130
4-Chloro-3-methylphenol ug/kg 25503310 77 55-130
4-Chloroaniline ug/kg 27403310 83 54-130
4-Chlorophenylphenyl ether ug/kg 13501660 82 58-130
4-Nitroaniline ug/kg 27303310 82 54-130
4-Nitrophenol ug/kg 66208280 80 48-130
Acenaphthene ug/kg 13801660 84 60-130
Acenaphthylene ug/kg 14501660 88 60-130
Aniline ug/kg 11801660 72 43-130
Anthracene ug/kg 16501660 100 63-130
Benzo(a)anthracene ug/kg 16001660 97 59-130
Benzo(a)pyrene ug/kg 16101660 97 57-130
Benzo(b)fluoranthene ug/kg 16201660 98 54-130
Benzo(g,h,i)perylene ug/kg 16201660 98 59-130
Benzo(k)fluoranthene ug/kg 15701660 95 54-130
Benzoic Acid ug/kg 54208280 65 19-130
Benzyl alcohol ug/kg 23803310 72 50-130
bis(2-Chloroethoxy)methane ug/kg 12701660 77 54-130
bis(2-Chloroethyl) ether ug/kg 12901660 78 48-130
bis(2-Ethylhexyl)phthalate ug/kg 17301660 105 45-134
Butylbenzylphthalate ug/kg 17101660 103 46-138
Chrysene ug/kg 16501660 99 58-130
Di-n-butylphthalate ug/kg 16101660 97 60-130
Di-n-octylphthalate ug/kg 17601660 106 53-130
Dibenz(a,h)anthracene ug/kg 16401660 99 59-130
Dibenzofuran ug/kg 13801660 83 60-130
Diethylphthalate ug/kg 14401660 87 60-130
Dimethylphthalate ug/kg 14901660 90 60-130
Fluoranthene ug/kg 16301660 98 65-130
Fluorene ug/kg 13901660 84 63-130
Hexachloro-1,3-butadiene ug/kg 11201660 68 46-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2661492LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 14501660 87 58-130
Hexachlorocyclopentadiene ug/kg 10901660 66 23-130
Hexachloroethane ug/kg 11801660 71 47-130
Indeno(1,2,3-cd)pyrene ug/kg 16501660 100 60-130
Isophorone ug/kg 12201660 74 49-130
N-Nitroso-di-n-propylamine ug/kg 13001660 78 47-130
N-Nitrosodimethylamine ug/kg 11601660 70 45-130
N-Nitrosodiphenylamine ug/kg 17001660 103 59-130
Naphthalene ug/kg 13601660 82 55-130
Nitrobenzene ug/kg 11701660 71 49-130
Pentachlorophenol ug/kg 28703310 87 10-132
Phenanthrene ug/kg 16401660 99 62-130
Phenol ug/kg 12301660 74 46-130
Pyrene ug/kg 17001660 103 53-130
2,4,6-Tribromophenol (S)%93 27-110
2-Fluorobiphenyl (S)%74 30-110
2-Fluorophenol (S)%74 13-110
Nitrobenzene-d5 (S)%74 23-110
Phenol-d6 (S)%76 22-110
Terphenyl-d14 (S)%91 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2661493MATRIX SPIKE SAMPLE:
MSSpike
Result
92442356011
1,2,4-Trichlorobenzene ug/kg 10501830 58 18-130ND
1,2-Dichlorobenzene ug/kg 10801830 59 14-130ND
1,3-Dichlorobenzene ug/kg 10501830 57 12-130ND
1,4-Dichlorobenzene ug/kg 10401830 57 10-130ND
1-Methylnaphthalene ug/kg 11101830 61 12-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 13701830 75 10-130ND
2,4,5-Trichlorophenol ug/kg 11401830 62 13-130ND
2,4,6-Trichlorophenol ug/kg 11901830 65 17-130ND
2,4-Dichlorophenol ug/kg 10701830 59 10-130ND
2,4-Dimethylphenol ug/kg 10901830 59 10-130ND
2,4-Dinitrophenol ug/kg 48309120 53 10-130ND
2,4-Dinitrotoluene ug/kg 11801830 65 24-130ND
2,6-Dinitrotoluene ug/kg 11801830 65 23-130ND
2-Chloronaphthalene ug/kg 10601830 58 19-130ND
2-Chlorophenol ug/kg 11201830 61 10-130ND
2-Methylnaphthalene ug/kg 11501830 63 18-130ND
2-Methylphenol(o-Cresol)ug/kg 10301830 56 10-130ND
2-Nitroaniline ug/kg 26903650 74 17-130ND
2-Nitrophenol ug/kg 10901830 60 10-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 10601830 58 10-130ND
3,3'-Dichlorobenzidine ug/kg 25303650 69 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
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Huntersville, NC 28078
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Page 64 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2661493MATRIX SPIKE SAMPLE:
MSSpike
Result
92442356011
3-Nitroaniline ug/kg 24903650 68 24-130ND
4,6-Dinitro-2-methylphenol ug/kg 25203650 69 10-152ND
4-Bromophenylphenyl ether ug/kg 13401830 73 29-130ND
4-Chloro-3-methylphenol ug/kg 23003650 63 17-130ND
4-Chloroaniline ug/kg 22803650 63 14-130ND
4-Chlorophenylphenyl ether ug/kg 12101830 66 25-130ND
4-Nitroaniline ug/kg 24703650 68 22-130ND
4-Nitrophenol ug/kg 61609120 68 10-130ND
Acenaphthene ug/kg 12201830 67 20-130ND
Acenaphthylene ug/kg 12801830 70 25-130ND
Aniline ug/kg 10301830 57 10-130ND
Anthracene ug/kg 15101830 83 29-130ND
Benzo(a)anthracene ug/kg 15501830 79 19-130116J
Benzo(a)pyrene ug/kg 15201830 77 12-130ND
Benzo(b)fluoranthene ug/kg 15801830 77 14-130177J
Benzo(g,h,i)perylene ug/kg 15601830 80 10-130ND
Benzo(k)fluoranthene ug/kg 15501830 81 14-130ND
Benzoic Acid ug/kg 29909120 33 10-130ND
Benzyl alcohol ug/kg 21103650 58 13-130ND
bis(2-Chloroethoxy)methane ug/kg 10801830 59 16-130ND
bis(2-Chloroethyl) ether ug/kg 11301830 62 11-130ND
bis(2-Ethylhexyl)phthalate ug/kg 15601830 86 21-130ND
Butylbenzylphthalate ug/kg 14801830 81 23-130ND
Chrysene ug/kg 16101830 81 22-130127J
Di-n-butylphthalate ug/kg 14101830 77 30-130ND
Di-n-octylphthalate ug/kg 15901830 87 23-142ND
Dibenz(a,h)anthracene ug/kg 14501830 79 10-130ND
Dibenzofuran ug/kg 12101830 66 24-130ND
Diethylphthalate ug/kg 12801830 70 26-130ND
Dimethylphthalate ug/kg 13601830 75 22-130ND
Fluoranthene ug/kg 16701830 77 33-130258J
Fluorene ug/kg 12801830 70 22-130ND
Hexachloro-1,3-butadiene ug/kg 9431830 52 13-130ND
Hexachlorobenzene ug/kg 13301830 73 29-130ND
Hexachlorocyclopentadiene ug/kg 9281830 51 10-130ND
Hexachloroethane ug/kg 10501830 57 10-130ND
Indeno(1,2,3-cd)pyrene ug/kg 15201830 79 10-130ND
Isophorone ug/kg 10201830 56 13-130ND
N-Nitroso-di-n-propylamine ug/kg 11601830 64 12-130ND
N-Nitrosodimethylamine ug/kg 9501830 52 11-130ND
N-Nitrosodiphenylamine ug/kg 15601830 85 15-130ND
Naphthalene ug/kg 11901830 65 15-130ND
Nitrobenzene ug/kg 10101830 55 12-130ND
Pentachlorophenol ug/kg 26503650 73 10-130ND
Phenanthrene ug/kg 16101830 80 27-130155J
Phenol ug/kg 10901830 60 10-130ND
Pyrene ug/kg 16901830 80 19-130228J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
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Huntersville, NC 28078
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Page 65 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2661493MATRIX SPIKE SAMPLE:
MSSpike
Result
92442356011
2,4,6-Tribromophenol (S)%68 27-110
2-Fluorobiphenyl (S)%52 30-110
2-Fluorophenol (S)%53 13-110
Nitrobenzene-d5 (S)%50 23-110
Phenol-d6 (S)%53 22-110
Terphenyl-d14 (S)%68 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92442356014
2661494SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92442356014
2661494SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6263
2-Fluorobiphenyl (S)%5958
2-Fluorophenol (S)%6260
Nitrobenzene-d5 (S)%6463
Phenol-d6 (S)%6562
Terphenyl-d14 (S)%7273
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493887
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92442356001, 92442356002, 92442356003, 92442356004, 92442356005, 92442356006, 92442356007,
92442356011, 92442356012, 92442356013, 92442356014, 92442356015, 92442356017
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92442391001
2661928SAMPLE DUPLICATE:
Percent Moisture %13.0 3 2512.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92442356001
2663207SAMPLE DUPLICATE:
Percent Moisture %12.9 9 2514.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442356
Corey's Transmission
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493980
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92442356008, 92442356009, 92442356010, 92442356016
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92442356008
2662466SAMPLE DUPLICATE:
Percent Moisture %14.9 1 2515.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92442288004
2662467SAMPLE DUPLICATE:
Percent Moisture %25.0 4 2524.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
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Huntersville, NC 28078
[phone]
Page 69 of 77
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92442356
Corey's Transmission
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.1g
Analyte was detected in the associated method blank.B
Analyte concentration exceeded the calibration range. The reported result is estimated.E
The reported result is estimated because one or more of the constituent results are qualified as such.ES
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 77
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92442356
Corey's Transmission
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92442356011 493811 493997AEPA 3050B EPA 6010D
92442356012 493811 493997BEPA 3050B EPA 6010D
92442356013 493811 493997CEPA 3050B EPA 6010D
92442356014 493811 493997DEPA 3050B EPA 6010D
92442356015 493811 493997EEPA 3050B EPA 6010D
92442356017 493811 493997DUP2EPA 3050B EPA 6010D
92442356011 493892 493950AEPA 7471B EPA 7471B
92442356012 493892 493950BEPA 7471B EPA 7471B
92442356013 493892 493950CEPA 7471B EPA 7471B
92442356014 493892 493950DEPA 7471B EPA 7471B
92442356015 493892 493950EEPA 7471B EPA 7471B
92442356017 493892 493950DUP2EPA 7471B EPA 7471B
92442356011 493821 493932AEPA 3546 EPA 8270E
92442356012 493821 493932BEPA 3546 EPA 8270E
92442356013 493821 493932CEPA 3546 EPA 8270E
92442356014 493821 493932DEPA 3546 EPA 8270E
92442356015 493821 493932EEPA 3546 EPA 8270E
92442356017 493821 493932DUP2EPA 3546 EPA 8270E
92442356001 493910 493956A-2 EPA 5035A EPA 8260D
92442356002 493910 493956A-3 EPA 5035A EPA 8260D
92442356003 493910 493956B-1 EPA 5035A EPA 8260D
92442356004 493910 493956B-2 EPA 5035A EPA 8260D
92442356005 493910 493956C-2 EPA 5035A EPA 8260D
92442356006 494145 494149C-3 EPA 5035A EPA 8260D
92442356007 494145 494149D-1 EPA 5035A EPA 8260D
92442356008 494145 494149D-4 EPA 5035A EPA 8260D
92442356009 493910 493956E-3 EPA 5035A EPA 8260D
92442356010 493910 493956E-5 EPA 5035A EPA 8260D
92442356016 494122 494130DUP1EPA 5035A EPA 8260D
92442356001 493887A-2 ASTM D2974-87
92442356002 493887A-3 ASTM D2974-87
92442356003 493887B-1 ASTM D2974-87
92442356004 493887B-2 ASTM D2974-87
92442356005 493887C-2 ASTM D2974-87
92442356006 493887C-3 ASTM D2974-87
92442356007 493887D-1 ASTM D2974-87
92442356008 493980D-4 ASTM D2974-87
92442356009 493980E-3 ASTM D2974-87
92442356010 493980E-5 ASTM D2974-87
92442356011 493887AASTM D2974-87
92442356012 493887BASTM D2974-87
92442356013 493887CASTM D2974-87
92442356014 493887DASTM D2974-87
92442356015 493887EASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 77
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92442356
Corey's Transmission
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92442356016 493980DUP1ASTM D2974-87
92442356017 493887DUP2ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/26/2019 04:34 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 77
Page 73 of 77
Page 74 of 77
Page 75 of 77
Page 76 of 77
Page 77 of 77
#=CL#
August 27, 2019
LIMS USE: FR - JOE NESTOR
LIMS OBJECT ID: 92442461
92442461
Project:
Pace Project No.:
RE:
Joe Nestor
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
COREY'S TRANSMISSION
Dear Joe Nestor:
Enclosed are the analytical results for sample(s) received by the laboratory on August 22, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 51
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Minnesota Certification IDs
1700 Elm Street SE, Minneapolis, MN 55414-2485
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
CNMI Saipan Certification #: MP0003
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8+Wyoming DW Certification #: via MN 027-
053-137
Florida Certification #: E87605
Georgia Certification #: 959
Guam EPA Certification #: MN00064
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: 03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Massachusetts Certification #: M-MN064
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Minnesota Dept of Ag Certifcation #: via MN 027-053-137
Minnesota Petrofund Certification #: 1240
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Vermont Certification #: VT-027053137
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
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Page 2 of 51
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Lab ID Sample ID Matrix Date Collected Date Received
92442461001 SG-1 #2591 Air 08/21/19 12:35 08/22/19 11:23
92442461002 SG-2 #3250 Air 08/21/19 13:21 08/22/19 11:23
92442461003 SG-3 #2791 Air 08/21/19 13:23 08/22/19 11:23
92442461004 SG-4 #893 Air 08/21/19 14:07 08/22/19 11:23
92442461005 SG-5 #3277 Air 08/21/19 14:30 08/22/19 11:23
92442461006 SG-6 #3025 Air 08/21/19 14:56 08/22/19 11:23
92442461007 SG-7 #3035 Air 08/21/19 15:30 08/22/19 11:23
92442461008 SG-8 #2401 Air 08/21/19 15:57 08/22/19 11:23
92442461009 DUP 1 #3252 Air 08/21/19 00:00 08/22/19 11:23
92442461010 SG-1 #2591 - Individual Cert.Air 08/21/19 12:35 08/22/19 11:23
92442461011 SG-2 #3250 - Individual Cert.Air 08/21/19 13:21 08/22/19 11:23
92442461012 SG-3 #2791 - Individual Cert.Air 08/21/19 13:23 08/22/19 11:23
92442461013 SG-4 #893 - Individual Cert.Air 08/21/19 14:07 08/22/19 11:23
92442461014 SG-5 #3277 - Individual Cert.Air 08/21/19 14:30 08/22/19 11:23
92442461015 SG-6 #3025 - Individual Cert.Air 08/21/19 14:56 08/22/19 11:23
92442461016 SG-7 #3035 - Individual Cert.Air 08/21/19 15:30 08/22/19 11:23
92442461017 SG-8 #2401 - Individual Cert.Air 08/21/19 15:57 08/22/19 11:23
92442461018 DUP 1 #3252 - Individual Cert.Air 08/21/19 00:00 08/22/19 11:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Page 3 of 51
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92442461001 SG-1 #2591 TO-15 58 PASI-MMJL
92442461002 SG-2 #3250 TO-15 58 PASI-MMJL
92442461003 SG-3 #2791 TO-15 58 PASI-MMJL
92442461004 SG-4 #893 TO-15 58 PASI-MMJL
92442461005 SG-5 #3277 TO-15 58 PASI-MMJL
92442461006 SG-6 #3025 TO-15 58 PASI-MMJL
92442461007 SG-7 #3035 TO-15 58 PASI-MMJL
92442461008 SG-8 #2401 TO-15 58 PASI-MMJL
92442461009 DUP 1 #3252 TO-15 58 PASI-MMJL
92442461010 SG-1 #2591 - Individual Cert.TO-15 61 PASI-MCH1
92442461011 SG-2 #3250 - Individual Cert.TO-15 61 PASI-MMG2
92442461012 SG-3 #2791 - Individual Cert.TO-15 61 PASI-MCH1
92442461013 SG-4 #893 - Individual Cert.TO-15 61 PASI-MMJL
92442461014 SG-5 #3277 - Individual Cert.TO-15 61 PASI-MCH1
92442461015 SG-6 #3025 - Individual Cert.TO-15 61 PASI-MCH1
92442461016 SG-7 #3035 - Individual Cert.TO-15 61 PASI-MMJL
92442461017 SG-8 #2401 - Individual Cert.TO-15 61 PASI-MMG2
92442461018 DUP 1 #3252 - Individual Cert.TO-15 61 PASI-MMJL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 4 of 51
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442461001 SG-1 #2591
Acetone 1940 ug/m3 08/24/19 15:24 E5.3TO-15
Benzene 16.3 ug/m3 08/24/19 15:240.71TO-15
2-Butanone (MEK)183 ug/m3 08/24/19 15:246.6TO-15
Carbon disulfide 50.6 ug/m3 08/24/19 15:241.4TO-15
Chloroform 9.1 ug/m3 08/24/19 15:241.1TO-15
Chloromethane 6.4 ug/m3 08/24/19 15:240.92TO-15
1,3-Dichlorobenzene 2.0J ug/m3 08/24/19 15:242.7TO-15
Dichlorodifluoromethane 2.5 ug/m3 08/24/19 15:242.2TO-15
1,1-Dichloroethane 0.94J ug/m3 08/24/19 15:241.8TO-15
trans-1,2-Dichloroethene 1.0J ug/m3 08/24/19 15:241.8TO-15
Ethyl acetate 1.7 ug/m3 08/24/19 15:241.6TO-15
Ethylbenzene 9.0 ug/m3 08/24/19 15:241.9TO-15
4-Ethyltoluene 3.9J ug/m3 08/24/19 15:245.5TO-15
n-Heptane 53.0 ug/m3 08/24/19 15:241.8TO-15
n-Hexane 54.1 ug/m3 08/24/19 15:241.6TO-15
2-Hexanone 46.6 ug/m3 08/24/19 15:249.1TO-15
Methylene Chloride 33.2 ug/m3 08/24/19 15:247.7TO-15
Propylene 1140 ug/m3 08/24/19 15:24 E0.77TO-15
Styrene 0.83J ug/m3 08/24/19 15:241.9TO-15
Tetrachloroethene 1.5J ug/m3 08/24/19 15:243.0TO-15
Toluene 36.9 ug/m3 08/24/19 15:241.7TO-15
Trichlorofluoromethane 2.0J ug/m3 08/24/19 15:242.5TO-15
1,1,2-Trichlorotrifluoroethane 1.3J ug/m3 08/24/19 15:243.4TO-15
1,2,4-Trimethylbenzene 12.4 ug/m3 08/24/19 15:242.2TO-15
m&p-Xylene 36.3 ug/m3 08/24/19 15:243.9TO-15
o-Xylene 11.8 ug/m3 08/24/19 15:241.9TO-15
92442461002 SG-2 #3250
Acetone 4400 ug/m3 08/25/19 23:34174TO-15
Benzene 21.2 ug/m3 08/24/19 15:530.78TO-15
2-Butanone (MEK)288 ug/m3 08/25/19 23:34216TO-15
Carbon disulfide 42.7 ug/m3 08/24/19 15:531.5TO-15
Chloroethane 1.6 ug/m3 08/24/19 15:531.3TO-15
Chloroform 21.9 ug/m3 08/24/19 15:531.2TO-15
Chloromethane 6.6 ug/m3 08/24/19 15:531.0TO-15
Dichlorodifluoromethane 2.5 ug/m3 08/24/19 15:532.4TO-15
1,1-Dichloroethane 1.6J ug/m3 08/24/19 15:532.0TO-15
trans-1,2-Dichloroethene 2.0 ug/m3 08/24/19 15:531.9TO-15
Ethylbenzene 5.9 ug/m3 08/24/19 15:532.1TO-15
4-Ethyltoluene 2.4J ug/m3 08/24/19 15:536.0TO-15
n-Heptane 34.3 ug/m3 08/24/19 15:532.0TO-15
n-Hexane 111 ug/m3 08/24/19 15:531.7TO-15
2-Hexanone 64.7 ug/m3 08/24/19 15:5310TO-15
Methylene Chloride 25.1 ug/m3 08/24/19 15:538.5TO-15
4-Methyl-2-pentanone (MIBK)5.7J ug/m3 08/24/19 15:5310TO-15
Propylene 2790 ug/m3 08/25/19 23:3425.2TO-15
Tetrachloroethene 0.82J ug/m3 08/24/19 15:533.3TO-15
Toluene 32.5 ug/m3 08/24/19 15:531.8TO-15
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 5 of 51
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442461002 SG-2 #3250
Trichloroethene 0.71J ug/m3 08/24/19 15:531.3TO-15
Trichlorofluoromethane 1.8J ug/m3 08/24/19 15:532.7TO-15
1,2,4-Trimethylbenzene 7.3 ug/m3 08/24/19 15:532.4TO-15
Vinyl chloride 2.2 ug/m3 08/24/19 15:530.62TO-15
m&p-Xylene 24.3 ug/m3 08/24/19 15:534.2TO-15
o-Xylene 7.6 ug/m3 08/24/19 15:532.1TO-15
92442461003 SG-3 #2791
Acetone 4790 ug/m3 08/26/19 00:01192TO-15
Benzene 28.3 ug/m3 08/24/19 16:220.86TO-15
Bromomethane 5.3 ug/m3 08/24/19 16:222.1TO-15
2-Butanone (MEK)355 ug/m3 08/26/19 00:01239TO-15
Carbon disulfide 47.5 ug/m3 08/24/19 16:221.7TO-15
Chloroform 6.1 ug/m3 08/24/19 16:221.3TO-15
1,3-Dichlorobenzene 1.6J ug/m3 08/24/19 16:223.2TO-15
Dichlorodifluoromethane 2.6J ug/m3 08/24/19 16:222.7TO-15
trans-1,2-Dichloroethene 2.8 ug/m3 08/24/19 16:222.1TO-15
Ethylbenzene 7.9 ug/m3 08/24/19 16:222.3TO-15
4-Ethyltoluene 4.2J ug/m3 08/24/19 16:226.6TO-15
n-Heptane 40.7 ug/m3 08/24/19 16:222.2TO-15
n-Hexane 207 ug/m3 08/24/19 16:221.9TO-15
2-Hexanone 84.4 ug/m3 08/24/19 16:2211.1TO-15
Methylene Chloride 24.2 ug/m3 08/24/19 16:229.4TO-15
4-Methyl-2-pentanone (MIBK)5.0J ug/m3 08/24/19 16:2211.1TO-15
Propylene 7550 ug/m3 08/26/19 00:01 E27.9TO-15
Styrene 1.0J ug/m3 08/24/19 16:222.3TO-15
Tetrachloroethene 5.7 ug/m3 08/24/19 16:223.7TO-15
Toluene 41.6 ug/m3 08/24/19 16:222.0TO-15
Trichlorofluoromethane 3.0J ug/m3 08/24/19 16:223.0TO-15
1,2,4-Trimethylbenzene 10.8 ug/m3 08/24/19 16:222.7TO-15
1,3,5-Trimethylbenzene 3.0 ug/m3 08/24/19 16:222.7TO-15
m&p-Xylene 32.3 ug/m3 08/24/19 16:224.7TO-15
o-Xylene 10.4 ug/m3 08/24/19 16:222.3TO-15
92442461004 SG-4 #893
Acetone 1280 ug/m3 08/24/19 16:51 E5.7TO-15
Benzene 11.6 ug/m3 08/24/19 16:510.76TO-15
2-Butanone (MEK)131 ug/m3 08/24/19 16:517.0TO-15
Carbon disulfide 203 ug/m3 08/24/19 16:511.5TO-15
Chloromethane 1.6 ug/m3 08/24/19 16:510.99TO-15
Dichlorodifluoromethane 1.1J ug/m3 08/24/19 16:512.4TO-15
trans-1,2-Dichloroethene 1.3J ug/m3 08/24/19 16:511.9TO-15
Ethylbenzene 8.0 ug/m3 08/24/19 16:512.1TO-15
4-Ethyltoluene 4.8J ug/m3 08/24/19 16:515.9TO-15
n-Heptane 26.5 ug/m3 08/24/19 16:512.0TO-15
n-Hexane 48.6 ug/m3 08/24/19 16:511.7TO-15
2-Hexanone 35.8 ug/m3 08/24/19 16:519.8TO-15
Methylene Chloride 28.5 ug/m3 08/24/19 16:518.3TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
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[phone]
Page 6 of 51
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442461004 SG-4 #893
Methyl-tert-butyl ether 3.1J ug/m3 08/24/19 16:518.6TO-15
Propylene 207 ug/m3 08/24/19 16:51 E0.82TO-15
Styrene 4.6 ug/m3 08/24/19 16:512.0TO-15
Tetrachloroethene 1.5J ug/m3 08/24/19 16:513.2TO-15
Toluene 22.6 ug/m3 08/24/19 16:511.8TO-15
1,2,4-Trimethylbenzene 12.5 ug/m3 08/24/19 16:512.3TO-15
1,3,5-Trimethylbenzene 3.2 ug/m3 08/24/19 16:512.3TO-15
Vinyl chloride 0.79 ug/m3 08/24/19 16:510.61TO-15
m&p-Xylene 35.2 ug/m3 08/24/19 16:514.2TO-15
o-Xylene 10.2 ug/m3 08/24/19 16:512.1TO-15
92442461005 SG-5 #3277
Acetone 3660 ug/m3 08/26/19 10:262270TO-15
Benzene 2960 ug/m3 08/26/19 10:26306TO-15
Carbon disulfide 40.5 ug/m3 08/24/19 17:201.6TO-15
Cyclohexane 624 ug/m3 08/24/19 17:20 E4.3TO-15
Dichlorodifluoromethane 1.6J ug/m3 08/24/19 17:202.5TO-15
1,1-Dichloroethane 7.0 ug/m3 08/24/19 17:202.0TO-15
trans-1,2-Dichloroethene 1.7J ug/m3 08/24/19 17:202.0TO-15
Ethylbenzene 15400 ug/m3 08/26/19 10:26831TO-15
4-Ethyltoluene 998 ug/m3 08/24/19 17:20 E6.2TO-15
n-Heptane 13600 ug/m3 08/26/19 10:26784TO-15
n-Hexane 5000 ug/m3 08/26/19 10:26674TO-15
2-Hexanone 69.4 ug/m3 08/24/19 17:2010.2TO-15
Methylene Chloride 22.5 ug/m3 08/24/19 17:208.7TO-15
Methyl-tert-butyl ether 210 ug/m3 08/24/19 17:209.0TO-15
Propylene 119 ug/m3 08/24/19 17:200.86TO-15
Styrene 7.3 ug/m3 08/24/19 17:202.1TO-15
Toluene 123 ug/m3 08/24/19 17:201.9TO-15
1,2,4-Trimethylbenzene 461 ug/m3 08/24/19 17:20 E2.5TO-15
1,3,5-Trimethylbenzene 38.0 ug/m3 08/24/19 17:202.5TO-15
m&p-Xylene 4150 ug/m3 08/26/19 10:261670TO-15
o-Xylene 58.0 ug/m3 08/24/19 17:202.2TO-15
92442461006 SG-6 #3025
Acetone 139 ug/m3 08/24/19 17:494.7TO-15
Benzene 3.7 ug/m3 08/24/19 17:490.63TO-15
2-Butanone (MEK)20.3 ug/m3 08/24/19 17:495.8TO-15
Carbon disulfide 4.5 ug/m3 08/24/19 17:491.2TO-15
Chloroform 0.73J ug/m3 08/24/19 17:490.96TO-15
Dichlorodifluoromethane 0.92J ug/m3 08/24/19 17:492.0TO-15
1,1-Dichloroethane 0.96J ug/m3 08/24/19 17:491.6TO-15
trans-1,2-Dichloroethene 71.7 ug/m3 08/24/19 17:491.6TO-15
Ethyl acetate 23.7 ug/m3 08/24/19 17:491.4TO-15
Ethylbenzene 10 ug/m3 08/24/19 17:491.7TO-15
4-Ethyltoluene 7.8 ug/m3 08/24/19 17:494.8TO-15
n-Heptane 9.7 ug/m3 08/24/19 17:491.6TO-15
n-Hexane 10.2 ug/m3 08/24/19 17:491.4TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 7 of 51
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442461006 SG-6 #3025
2-Hexanone 13.6 ug/m3 08/24/19 17:498.1TO-15
Methylene Chloride 12.1 ug/m3 08/24/19 17:496.8TO-15
Methyl-tert-butyl ether 2.6J ug/m3 08/24/19 17:497.1TO-15
Styrene 2.4 ug/m3 08/24/19 17:491.7TO-15
Tetrachloroethene 0.89J ug/m3 08/24/19 17:492.7TO-15
Tetrahydrofuran 1.2 ug/m3 08/24/19 17:491.2TO-15
Toluene 27.0 ug/m3 08/24/19 17:491.5TO-15
Trichloroethene 15.2 ug/m3 08/24/19 17:491.1TO-15
1,2,4-Trimethylbenzene 12.8 ug/m3 08/24/19 17:491.9TO-15
1,3,5-Trimethylbenzene 3.1 ug/m3 08/24/19 17:491.9TO-15
m&p-Xylene 32.3 ug/m3 08/24/19 17:493.4TO-15
o-Xylene 9.4 ug/m3 08/24/19 17:491.7TO-15
92442461007 SG-7 #3035
Acetone 387 ug/m3 08/24/19 18:185.3TO-15
Benzene 6.8 ug/m3 08/24/19 18:180.71TO-15
2-Butanone (MEK)40.5 ug/m3 08/24/19 18:186.6TO-15
Carbon disulfide 8.7 ug/m3 08/24/19 18:181.4TO-15
Chloromethane 1.0 ug/m3 08/24/19 18:180.92TO-15
Cyclohexane 2.7J ug/m3 08/24/19 18:183.8TO-15
Dichlorodifluoromethane 2.0J ug/m3 08/24/19 18:182.2TO-15
Ethylbenzene 2.8 ug/m3 08/24/19 18:181.9TO-15
n-Heptane 4.4 ug/m3 08/24/19 18:181.8TO-15
n-Hexane 7.8 ug/m3 08/24/19 18:181.6TO-15
2-Hexanone 10.3 ug/m3 08/24/19 18:189.1TO-15
Methylene Chloride 12.5 ug/m3 08/24/19 18:187.7TO-15
Propylene 9.6 ug/m3 08/24/19 18:180.77TO-15
Tetrachloroethene 0.70J ug/m3 08/24/19 18:183.0TO-15
Toluene 5.8 ug/m3 08/24/19 18:181.7TO-15
Trichlorofluoromethane 1.1J ug/m3 08/24/19 18:182.5TO-15
1,2,4-Trimethylbenzene 1.6J ug/m3 08/24/19 18:182.2TO-15
m&p-Xylene 5.2 ug/m3 08/24/19 18:183.9TO-15
o-Xylene 1.5J ug/m3 08/24/19 18:181.9TO-15
92442461008 SG-8 #2401
Acetone 689 ug/m3 08/24/19 18:478.7TO-15
Benzene 12.6 ug/m3 08/24/19 18:471.2TO-15
2-Butanone (MEK)62.0 ug/m3 08/24/19 18:4710.8TO-15
Carbon disulfide 4.0 ug/m3 08/24/19 18:472.3TO-15
Chloroform 1.2J ug/m3 08/24/19 18:471.8TO-15
Chloromethane 0.73J ug/m3 08/24/19 18:471.5TO-15
Dichlorodifluoromethane 1.8J ug/m3 08/24/19 18:473.6TO-15
trans-1,2-Dichloroethene 7.1 ug/m3 08/24/19 18:472.9TO-15
Ethyl acetate 1.9J ug/m3 08/24/19 18:472.6TO-15
Ethylbenzene 6.4 ug/m3 08/24/19 18:473.2TO-15
4-Ethyltoluene 2.5J ug/m3 08/24/19 18:479.0TO-15
n-Heptane 8.6 ug/m3 08/24/19 18:473.0TO-15
n-Hexane 17.3 ug/m3 08/24/19 18:472.6TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 8 of 51
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442461008 SG-8 #2401
2-Hexanone 28.6 ug/m3 08/24/19 18:4715.0TO-15
Methylene Chloride 86.5 ug/m3 08/24/19 18:4712.7TO-15
Propylene 28.1 ug/m3 08/24/19 18:471.3TO-15
Toluene 18.5 ug/m3 08/24/19 18:472.8TO-15
Trichloroethene 1.0J ug/m3 08/24/19 18:472.0TO-15
1,2,4-Trimethylbenzene 6.6 ug/m3 08/24/19 18:473.6TO-15
1,3,5-Trimethylbenzene 2.0J ug/m3 08/24/19 18:473.6TO-15
m&p-Xylene 21.8 ug/m3 08/24/19 18:476.4TO-15
o-Xylene 6.3 ug/m3 08/24/19 18:473.2TO-15
92442461009 DUP 1 #3252
Acetone 1200 ug/m3 08/24/19 19:17 E5.8TO-15
Benzene 14.4 ug/m3 08/24/19 19:170.78TO-15
2-Butanone (MEK)105 ug/m3 08/24/19 19:177.2TO-15
Carbon disulfide 52.9 ug/m3 08/24/19 19:171.5TO-15
Chloroform 19.5 ug/m3 08/24/19 19:171.2TO-15
Chloromethane 1.8 ug/m3 08/24/19 19:171.0TO-15
Cyclohexane 22.3 ug/m3 08/24/19 19:174.2TO-15
1,3-Dichlorobenzene 1.8J ug/m3 08/24/19 19:172.9TO-15
Dichlorodifluoromethane 2.4J ug/m3 08/24/19 19:172.4TO-15
trans-1,2-Dichloroethene 1.6J ug/m3 08/24/19 19:171.9TO-15
Ethylbenzene 9.0 ug/m3 08/24/19 19:172.1TO-15
4-Ethyltoluene 3.8J ug/m3 08/24/19 19:176.0TO-15
n-Heptane 78.8 ug/m3 08/24/19 19:172.0TO-15
n-Hexane 55.2 ug/m3 08/24/19 19:171.7TO-15
2-Hexanone 38.9 ug/m3 08/24/19 19:1710TO-15
Methylene Chloride 21.0 ug/m3 08/24/19 19:178.5TO-15
Propylene 639 ug/m3 08/24/19 19:17 E0.84TO-15
Styrene 0.86J ug/m3 08/24/19 19:172.1TO-15
Tetrachloroethene 1.6J ug/m3 08/24/19 19:173.3TO-15
Toluene 33.4 ug/m3 08/24/19 19:171.8TO-15
Trichlorofluoromethane 1.6J ug/m3 08/24/19 19:172.7TO-15
1,2,4-Trimethylbenzene 10.8 ug/m3 08/24/19 19:172.4TO-15
1,3,5-Trimethylbenzene 3.0 ug/m3 08/24/19 19:172.4TO-15
m&p-Xylene 34.7 ug/m3 08/24/19 19:174.2TO-15
o-Xylene 11.0 ug/m3 08/24/19 19:172.1TO-15
92442461010 SG-1 #2591 - Individual Cert.
2-Propanol 0.81J ug/m3 07/25/19 09:001.2TO-15
92442461012 SG-3 #2791 - Individual Cert.
2-Propanol 1.4J ug/m3 07/26/19 09:132.5TO-15
92442461015 SG-6 #3025 - Individual Cert.
2-Propanol 1.5J ug/m3 07/25/19 09:582.5TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-1 #2591 Lab ID: 92442461001 Collected: 08/21/19 12:35 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 1940 ug/m3 08/24/19 15:24 67-64-1 E5.3 2.6 2.19
Benzene 16.3 ug/m3 08/24/19 15:24 71-43-20.71 0.34 2.19
Bromodichloromethane ND ug/m3 08/24/19 15:24 75-27-43.0 0.80 2.19
Bromoform ND ug/m3 08/24/19 15:24 75-25-211.5 3.1 2.19
Bromomethane ND ug/m3 08/24/19 15:24 74-83-91.7 0.50 2.19
1,3-Butadiene ND ug/m3 08/24/19 15:24 106-99-00.99 0.28 2.19
2-Butanone (MEK)183 ug/m3 08/24/19 15:24 78-93-36.6 0.81 2.19
Carbon disulfide 50.6 ug/m3 08/24/19 15:24 75-15-01.4 0.48 2.19
Carbon tetrachloride ND ug/m3 08/24/19 15:24 56-23-52.8 0.94 2.19
Chlorobenzene ND ug/m3 08/24/19 15:24 108-90-72.0 0.60 2.19
Chloroethane ND ug/m3 08/24/19 15:24 75-00-31.2 0.57 2.19
Chloroform 9.1 ug/m3 08/24/19 15:24 67-66-31.1 0.43 2.19
Chloromethane 6.4 ug/m3 08/24/19 15:24 74-87-30.92 0.34 2.19
Cyclohexane ND ug/m3 08/24/19 15:24 110-82-73.8 0.77 2.19
Dibromochloromethane ND ug/m3 08/24/19 15:24 124-48-13.8 1.6 2.19
1,2-Dibromoethane (EDB)ND ug/m3 08/24/19 15:24 106-93-43.4 0.80 2.19
1,2-Dichlorobenzene ND ug/m3 08/24/19 15:24 95-50-12.7 1.1 2.19
1,3-Dichlorobenzene 2.0J ug/m3 08/24/19 15:24 541-73-12.7 1.3 2.19
1,4-Dichlorobenzene ND ug/m3 08/24/19 15:24 106-46-76.7 2.2 2.19
Dichlorodifluoromethane 2.5 ug/m3 08/24/19 15:24 75-71-82.2 0.64 2.19
1,1-Dichloroethane 0.94J ug/m3 08/24/19 15:24 75-34-31.8 0.49 2.19
1,2-Dichloroethane ND ug/m3 08/24/19 15:24 107-06-20.90 0.33 2.19
1,1-Dichloroethene ND ug/m3 08/24/19 15:24 75-35-41.8 0.60 2.19
cis-1,2-Dichloroethene ND ug/m3 08/24/19 15:24 156-59-21.8 0.48 2.19
trans-1,2-Dichloroethene 1.0J ug/m3 08/24/19 15:24 156-60-51.8 0.62 2.19
1,2-Dichloropropane ND ug/m3 08/24/19 15:24 78-87-52.1 0.50 2.19
cis-1,3-Dichloropropene ND ug/m3 08/24/19 15:24 10061-01-52.0 0.67 2.19
trans-1,3-Dichloropropene ND ug/m3 08/24/19 15:24 10061-02-62.0 0.96 2.19
Dichlorotetrafluoroethane ND ug/m3 08/24/19 15:24 76-14-23.1 0.96 2.19
Ethyl acetate 1.7 ug/m3 08/24/19 15:24 141-78-61.6 0.42 2.19
Ethylbenzene 9.0 ug/m3 08/24/19 15:24 100-41-41.9 0.67 2.19
4-Ethyltoluene 3.9J ug/m3 08/24/19 15:24 622-96-85.5 1.2 2.19
n-Heptane 53.0 ug/m3 08/24/19 15:24 142-82-51.8 0.83 2.19
Hexachloro-1,3-butadiene ND ug/m3 08/24/19 15:24 87-68-311.9 4.3 2.19
n-Hexane 54.1 ug/m3 08/24/19 15:24 110-54-31.6 0.68 2.19
2-Hexanone 46.6 ug/m3 08/24/19 15:24 591-78-69.1 1.6 2.19
Methylene Chloride 33.2 ug/m3 08/24/19 15:24 75-09-27.7 2.1 2.19
4-Methyl-2-pentanone (MIBK)ND ug/m3 08/24/19 15:24 108-10-19.1 1.1 2.19
Methyl-tert-butyl ether ND ug/m3 08/24/19 15:24 1634-04-48.0 1.5 2.19
Naphthalene ND ug/m3 08/24/19 15:24 91-20-35.8 2.9 2.19
Propylene 1140 ug/m3 08/24/19 15:24 115-07-1 E0.77 0.31 2.19
Styrene 0.83J ug/m3 08/24/19 15:24 100-42-51.9 0.75 2.19
1,1,2,2-Tetrachloroethane ND ug/m3 08/24/19 15:24 79-34-51.5 0.64 2.19
Tetrachloroethene 1.5J ug/m3 08/24/19 15:24 127-18-43.0 0.69 2.19
Tetrahydrofuran ND ug/m3 08/24/19 15:24 109-99-91.3 0.57 2.19
Toluene 36.9 ug/m3 08/24/19 15:24 108-88-31.7 0.77 2.19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 10 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-1 #2591 Lab ID: 92442461001 Collected: 08/21/19 12:35 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 08/24/19 15:24 120-82-116.5 8.1 2.19
1,1,1-Trichloroethane ND ug/m3 08/24/19 15:24 71-55-62.4 0.68 2.19
1,1,2-Trichloroethane ND ug/m3 08/24/19 15:24 79-00-51.2 0.55 2.19
Trichloroethene ND ug/m3 08/24/19 15:24 79-01-61.2 0.56 2.19
Trichlorofluoromethane 2.0J ug/m3 08/24/19 15:24 75-69-42.5 0.80 2.19
1,1,2-Trichlorotrifluoroethane 1.3J ug/m3 08/24/19 15:24 76-13-13.4 1.2 2.19
1,2,4-Trimethylbenzene 12.4 ug/m3 08/24/19 15:24 95-63-62.2 0.99 2.19
1,3,5-Trimethylbenzene ND ug/m3 08/24/19 15:24 108-67-82.2 0.87 2.19
Vinyl acetate ND ug/m3 08/24/19 15:24 108-05-41.6 0.59 2.19
Vinyl chloride ND ug/m3 08/24/19 15:24 75-01-40.57 0.28 2.19
m&p-Xylene 36.3 ug/m3 08/24/19 15:24 179601-23-13.9 1.5 2.19
o-Xylene 11.8 ug/m3 08/24/19 15:24 95-47-61.9 0.75 2.19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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9800 Kincey Ave. Suite 100
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Page 11 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-2 #3250 Lab ID: 92442461002 Collected: 08/21/19 13:21 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 4400 ug/m3 08/25/19 23:34 67-64-1174 87.1 72
Benzene 21.2 ug/m3 08/24/19 15:53 71-43-20.78 0.37 2.4
Bromodichloromethane ND ug/m3 08/24/19 15:53 75-27-43.3 0.88 2.4
Bromoform ND ug/m3 08/24/19 15:53 75-25-212.6 3.4 2.4
Bromomethane ND ug/m3 08/24/19 15:53 74-83-91.9 0.54 2.4
1,3-Butadiene ND ug/m3 08/24/19 15:53 106-99-01.1 0.31 2.4
2-Butanone (MEK)288 ug/m3 08/25/19 23:34 78-93-3216 26.6 72
Carbon disulfide 42.7 ug/m3 08/24/19 15:53 75-15-01.5 0.53 2.4
Carbon tetrachloride ND ug/m3 08/24/19 15:53 56-23-53.1 1.0 2.4
Chlorobenzene ND ug/m3 08/24/19 15:53 108-90-72.2 0.66 2.4
Chloroethane 1.6 ug/m3 08/24/19 15:53 75-00-31.3 0.62 2.4
Chloroform 21.9 ug/m3 08/24/19 15:53 67-66-31.2 0.47 2.4
Chloromethane 6.6 ug/m3 08/24/19 15:53 74-87-31.0 0.37 2.4
Cyclohexane ND ug/m3 08/24/19 15:53 110-82-74.2 0.85 2.4
Dibromochloromethane ND ug/m3 08/24/19 15:53 124-48-14.2 1.7 2.4
1,2-Dibromoethane (EDB)ND ug/m3 08/24/19 15:53 106-93-43.7 0.88 2.4
1,2-Dichlorobenzene ND ug/m3 08/24/19 15:53 95-50-12.9 1.2 2.4
1,3-Dichlorobenzene ND ug/m3 08/24/19 15:53 541-73-12.9 1.4 2.4
1,4-Dichlorobenzene ND ug/m3 08/24/19 15:53 106-46-77.3 2.4 2.4
Dichlorodifluoromethane 2.5 ug/m3 08/24/19 15:53 75-71-82.4 0.70 2.4
1,1-Dichloroethane 1.6J ug/m3 08/24/19 15:53 75-34-32.0 0.54 2.4
1,2-Dichloroethane ND ug/m3 08/24/19 15:53 107-06-20.99 0.36 2.4
1,1-Dichloroethene ND ug/m3 08/24/19 15:53 75-35-41.9 0.66 2.4
cis-1,2-Dichloroethene ND ug/m3 08/24/19 15:53 156-59-21.9 0.53 2.4
trans-1,2-Dichloroethene 2.0 ug/m3 08/24/19 15:53 156-60-51.9 0.68 2.4
1,2-Dichloropropane ND ug/m3 08/24/19 15:53 78-87-52.3 0.55 2.4
cis-1,3-Dichloropropene ND ug/m3 08/24/19 15:53 10061-01-52.2 0.73 2.4
trans-1,3-Dichloropropene ND ug/m3 08/24/19 15:53 10061-02-62.2 1.1 2.4
Dichlorotetrafluoroethane ND ug/m3 08/24/19 15:53 76-14-23.4 1.0 2.4
Ethyl acetate ND ug/m3 08/24/19 15:53 141-78-61.8 0.46 2.4
Ethylbenzene 5.9 ug/m3 08/24/19 15:53 100-41-42.1 0.73 2.4
4-Ethyltoluene 2.4J ug/m3 08/24/19 15:53 622-96-86.0 1.4 2.4
n-Heptane 34.3 ug/m3 08/24/19 15:53 142-82-52.0 0.91 2.4
Hexachloro-1,3-butadiene ND ug/m3 08/24/19 15:53 87-68-313.0 4.7 2.4
n-Hexane 111 ug/m3 08/24/19 15:53 110-54-31.7 0.75 2.4
2-Hexanone 64.7 ug/m3 08/24/19 15:53 591-78-610 1.8 2.4
Methylene Chloride 25.1 ug/m3 08/24/19 15:53 75-09-28.5 2.3 2.4
4-Methyl-2-pentanone (MIBK)5.7J ug/m3 08/24/19 15:53 108-10-110 1.2 2.4
Methyl-tert-butyl ether ND ug/m3 08/24/19 15:53 1634-04-48.8 1.6 2.4
Naphthalene ND ug/m3 08/24/19 15:53 91-20-36.4 3.2 2.4
Propylene 2790 ug/m3 08/25/19 23:34 115-07-125.2 10.3 72
Styrene ND ug/m3 08/24/19 15:53 100-42-52.1 0.83 2.4
1,1,2,2-Tetrachloroethane ND ug/m3 08/24/19 15:53 79-34-51.7 0.70 2.4
Tetrachloroethene 0.82J ug/m3 08/24/19 15:53 127-18-43.3 0.75 2.4
Tetrahydrofuran ND ug/m3 08/24/19 15:53 109-99-91.4 0.63 2.4
Toluene 32.5 ug/m3 08/24/19 15:53 108-88-31.8 0.84 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 12 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-2 #3250 Lab ID: 92442461002 Collected: 08/21/19 13:21 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 08/24/19 15:53 120-82-118.1 8.9 2.4
1,1,1-Trichloroethane ND ug/m3 08/24/19 15:53 71-55-62.7 0.74 2.4
1,1,2-Trichloroethane ND ug/m3 08/24/19 15:53 79-00-51.3 0.60 2.4
Trichloroethene 0.71J ug/m3 08/24/19 15:53 79-01-61.3 0.62 2.4
Trichlorofluoromethane 1.8J ug/m3 08/24/19 15:53 75-69-42.7 0.88 2.4
1,1,2-Trichlorotrifluoroethane ND ug/m3 08/24/19 15:53 76-13-13.7 1.4 2.4
1,2,4-Trimethylbenzene 7.3 ug/m3 08/24/19 15:53 95-63-62.4 1.1 2.4
1,3,5-Trimethylbenzene ND ug/m3 08/24/19 15:53 108-67-82.4 0.96 2.4
Vinyl acetate ND ug/m3 08/24/19 15:53 108-05-41.7 0.65 2.4
Vinyl chloride 2.2 ug/m3 08/24/19 15:53 75-01-40.62 0.30 2.4
m&p-Xylene 24.3 ug/m3 08/24/19 15:53 179601-23-14.2 1.7 2.4
o-Xylene 7.6 ug/m3 08/24/19 15:53 95-47-62.1 0.83 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-3 #2791 Lab ID: 92442461003 Collected: 08/21/19 13:23 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 4790 ug/m3 08/26/19 00:01 67-64-1192 96.6 79.8
Benzene 28.3 ug/m3 08/24/19 16:22 71-43-20.86 0.41 2.66
Bromodichloromethane ND ug/m3 08/24/19 16:22 75-27-43.6 0.97 2.66
Bromoform ND ug/m3 08/24/19 16:22 75-25-214.0 3.8 2.66
Bromomethane 5.3 ug/m3 08/24/19 16:22 74-83-92.1 0.60 2.66
1,3-Butadiene ND ug/m3 08/24/19 16:22 106-99-01.2 0.34 2.66
2-Butanone (MEK)355 ug/m3 08/26/19 00:01 78-93-3239 29.4 79.8
Carbon disulfide 47.5 ug/m3 08/24/19 16:22 75-15-01.7 0.58 2.66
Carbon tetrachloride ND ug/m3 08/24/19 16:22 56-23-53.4 1.1 2.66
Chlorobenzene ND ug/m3 08/24/19 16:22 108-90-72.5 0.73 2.66
Chloroethane ND ug/m3 08/24/19 16:22 75-00-31.4 0.69 2.66
Chloroform 6.1 ug/m3 08/24/19 16:22 67-66-31.3 0.52 2.66
Chloromethane ND ug/m3 08/24/19 16:22 74-87-31.1 0.41 2.66
Cyclohexane ND ug/m3 08/24/19 16:22 110-82-74.7 0.94 2.66
Dibromochloromethane ND ug/m3 08/24/19 16:22 124-48-14.6 1.9 2.66
1,2-Dibromoethane (EDB)ND ug/m3 08/24/19 16:22 106-93-44.2 0.97 2.66
1,2-Dichlorobenzene ND ug/m3 08/24/19 16:22 95-50-13.2 1.3 2.66
1,3-Dichlorobenzene 1.6J ug/m3 08/24/19 16:22 541-73-13.2 1.5 2.66
1,4-Dichlorobenzene ND ug/m3 08/24/19 16:22 106-46-78.1 2.7 2.66
Dichlorodifluoromethane 2.6J ug/m3 08/24/19 16:22 75-71-82.7 0.78 2.66
1,1-Dichloroethane ND ug/m3 08/24/19 16:22 75-34-32.2 0.60 2.66
1,2-Dichloroethane ND ug/m3 08/24/19 16:22 107-06-21.1 0.40 2.66
1,1-Dichloroethene ND ug/m3 08/24/19 16:22 75-35-42.1 0.73 2.66
cis-1,2-Dichloroethene ND ug/m3 08/24/19 16:22 156-59-22.1 0.58 2.66
trans-1,2-Dichloroethene 2.8 ug/m3 08/24/19 16:22 156-60-52.1 0.76 2.66
1,2-Dichloropropane ND ug/m3 08/24/19 16:22 78-87-52.5 0.61 2.66
cis-1,3-Dichloropropene ND ug/m3 08/24/19 16:22 10061-01-52.5 0.81 2.66
trans-1,3-Dichloropropene ND ug/m3 08/24/19 16:22 10061-02-62.5 1.2 2.66
Dichlorotetrafluoroethane ND ug/m3 08/24/19 16:22 76-14-23.8 1.2 2.66
Ethyl acetate ND ug/m3 08/24/19 16:22 141-78-61.9 0.51 2.66
Ethylbenzene 7.9 ug/m3 08/24/19 16:22 100-41-42.3 0.81 2.66
4-Ethyltoluene 4.2J ug/m3 08/24/19 16:22 622-96-86.6 1.5 2.66
n-Heptane 40.7 ug/m3 08/24/19 16:22 142-82-52.2 1.0 2.66
Hexachloro-1,3-butadiene ND ug/m3 08/24/19 16:22 87-68-314.4 5.2 2.66
n-Hexane 207 ug/m3 08/24/19 16:22 110-54-31.9 0.83 2.66
2-Hexanone 84.4 ug/m3 08/24/19 16:22 591-78-611.1 2.0 2.66
Methylene Chloride 24.2 ug/m3 08/24/19 16:22 75-09-29.4 2.5 2.66
4-Methyl-2-pentanone (MIBK)5.0J ug/m3 08/24/19 16:22 108-10-111.1 1.4 2.66
Methyl-tert-butyl ether ND ug/m3 08/24/19 16:22 1634-04-49.7 1.8 2.66
Naphthalene ND ug/m3 08/24/19 16:22 91-20-37.1 3.5 2.66
Propylene 7550 ug/m3 08/26/19 00:01 115-07-1 E27.9 11.4 79.8
Styrene 1.0J ug/m3 08/24/19 16:22 100-42-52.3 0.92 2.66
1,1,2,2-Tetrachloroethane ND ug/m3 08/24/19 16:22 79-34-51.9 0.78 2.66
Tetrachloroethene 5.7 ug/m3 08/24/19 16:22 127-18-43.7 0.84 2.66
Tetrahydrofuran ND ug/m3 08/24/19 16:22 109-99-91.6 0.69 2.66
Toluene 41.6 ug/m3 08/24/19 16:22 108-88-32.0 0.93 2.66
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 14 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-3 #2791 Lab ID: 92442461003 Collected: 08/21/19 13:23 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 08/24/19 16:22 120-82-120.1 9.9 2.66
1,1,1-Trichloroethane ND ug/m3 08/24/19 16:22 71-55-63.0 0.82 2.66
1,1,2-Trichloroethane ND ug/m3 08/24/19 16:22 79-00-51.5 0.66 2.66
Trichloroethene ND ug/m3 08/24/19 16:22 79-01-61.5 0.68 2.66
Trichlorofluoromethane 3.0J ug/m3 08/24/19 16:22 75-69-43.0 0.97 2.66
1,1,2-Trichlorotrifluoroethane ND ug/m3 08/24/19 16:22 76-13-14.1 1.5 2.66
1,2,4-Trimethylbenzene 10.8 ug/m3 08/24/19 16:22 95-63-62.7 1.2 2.66
1,3,5-Trimethylbenzene 3.0 ug/m3 08/24/19 16:22 108-67-82.7 1.1 2.66
Vinyl acetate ND ug/m3 08/24/19 16:22 108-05-41.9 0.72 2.66
Vinyl chloride ND ug/m3 08/24/19 16:22 75-01-40.69 0.34 2.66
m&p-Xylene 32.3 ug/m3 08/24/19 16:22 179601-23-14.7 1.9 2.66
o-Xylene 10.4 ug/m3 08/24/19 16:22 95-47-62.3 0.92 2.66
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 15 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-4 #893 Lab ID: 92442461004 Collected: 08/21/19 14:07 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 1280 ug/m3 08/24/19 16:51 67-64-1 E5.7 2.8 2.35
Benzene 11.6 ug/m3 08/24/19 16:51 71-43-20.76 0.36 2.35
Bromodichloromethane ND ug/m3 08/24/19 16:51 75-27-43.2 0.86 2.35
Bromoform ND ug/m3 08/24/19 16:51 75-25-212.3 3.3 2.35
Bromomethane ND ug/m3 08/24/19 16:51 74-83-91.9 0.53 2.35
1,3-Butadiene ND ug/m3 08/24/19 16:51 106-99-01.1 0.30 2.35
2-Butanone (MEK)131 ug/m3 08/24/19 16:51 78-93-37.0 0.87 2.35
Carbon disulfide 203 ug/m3 08/24/19 16:51 75-15-01.5 0.51 2.35
Carbon tetrachloride ND ug/m3 08/24/19 16:51 56-23-53.0 1.0 2.35
Chlorobenzene ND ug/m3 08/24/19 16:51 108-90-72.2 0.65 2.35
Chloroethane ND ug/m3 08/24/19 16:51 75-00-31.3 0.61 2.35
Chloroform ND ug/m3 08/24/19 16:51 67-66-31.2 0.46 2.35
Chloromethane 1.6 ug/m3 08/24/19 16:51 74-87-30.99 0.37 2.35
Cyclohexane ND ug/m3 08/24/19 16:51 110-82-74.1 0.83 2.35
Dibromochloromethane ND ug/m3 08/24/19 16:51 124-48-14.1 1.7 2.35
1,2-Dibromoethane (EDB)ND ug/m3 08/24/19 16:51 106-93-43.7 0.86 2.35
1,2-Dichlorobenzene ND ug/m3 08/24/19 16:51 95-50-12.9 1.2 2.35
1,3-Dichlorobenzene ND ug/m3 08/24/19 16:51 541-73-12.9 1.4 2.35
1,4-Dichlorobenzene ND ug/m3 08/24/19 16:51 106-46-77.2 2.4 2.35
Dichlorodifluoromethane 1.1J ug/m3 08/24/19 16:51 75-71-82.4 0.69 2.35
1,1-Dichloroethane ND ug/m3 08/24/19 16:51 75-34-31.9 0.53 2.35
1,2-Dichloroethane ND ug/m3 08/24/19 16:51 107-06-20.97 0.35 2.35
1,1-Dichloroethene ND ug/m3 08/24/19 16:51 75-35-41.9 0.64 2.35
cis-1,2-Dichloroethene ND ug/m3 08/24/19 16:51 156-59-21.9 0.51 2.35
trans-1,2-Dichloroethene 1.3J ug/m3 08/24/19 16:51 156-60-51.9 0.67 2.35
1,2-Dichloropropane ND ug/m3 08/24/19 16:51 78-87-52.2 0.54 2.35
cis-1,3-Dichloropropene ND ug/m3 08/24/19 16:51 10061-01-52.2 0.71 2.35
trans-1,3-Dichloropropene ND ug/m3 08/24/19 16:51 10061-02-62.2 1.0 2.35
Dichlorotetrafluoroethane ND ug/m3 08/24/19 16:51 76-14-23.3 1.0 2.35
Ethyl acetate ND ug/m3 08/24/19 16:51 141-78-61.7 0.45 2.35
Ethylbenzene 8.0 ug/m3 08/24/19 16:51 100-41-42.1 0.72 2.35
4-Ethyltoluene 4.8J ug/m3 08/24/19 16:51 622-96-85.9 1.3 2.35
n-Heptane 26.5 ug/m3 08/24/19 16:51 142-82-52.0 0.89 2.35
Hexachloro-1,3-butadiene ND ug/m3 08/24/19 16:51 87-68-312.7 4.6 2.35
n-Hexane 48.6 ug/m3 08/24/19 16:51 110-54-31.7 0.73 2.35
2-Hexanone 35.8 ug/m3 08/24/19 16:51 591-78-69.8 1.8 2.35
Methylene Chloride 28.5 ug/m3 08/24/19 16:51 75-09-28.3 2.2 2.35
4-Methyl-2-pentanone (MIBK)ND ug/m3 08/24/19 16:51 108-10-19.8 1.2 2.35
Methyl-tert-butyl ether 3.1J ug/m3 08/24/19 16:51 1634-04-48.6 1.6 2.35
Naphthalene ND ug/m3 08/24/19 16:51 91-20-36.3 3.1 2.35
Propylene 207 ug/m3 08/24/19 16:51 115-07-1 E0.82 0.34 2.35
Styrene 4.6 ug/m3 08/24/19 16:51 100-42-52.0 0.81 2.35
1,1,2,2-Tetrachloroethane ND ug/m3 08/24/19 16:51 79-34-51.6 0.69 2.35
Tetrachloroethene 1.5J ug/m3 08/24/19 16:51 127-18-43.2 0.74 2.35
Tetrahydrofuran ND ug/m3 08/24/19 16:51 109-99-91.4 0.61 2.35
Toluene 22.6 ug/m3 08/24/19 16:51 108-88-31.8 0.82 2.35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 16 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-4 #893 Lab ID: 92442461004 Collected: 08/21/19 14:07 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 08/24/19 16:51 120-82-117.7 8.7 2.35
1,1,1-Trichloroethane ND ug/m3 08/24/19 16:51 71-55-62.6 0.73 2.35
1,1,2-Trichloroethane ND ug/m3 08/24/19 16:51 79-00-51.3 0.59 2.35
Trichloroethene ND ug/m3 08/24/19 16:51 79-01-61.3 0.60 2.35
Trichlorofluoromethane ND ug/m3 08/24/19 16:51 75-69-42.7 0.86 2.35
1,1,2-Trichlorotrifluoroethane ND ug/m3 08/24/19 16:51 76-13-13.7 1.3 2.35
1,2,4-Trimethylbenzene 12.5 ug/m3 08/24/19 16:51 95-63-62.3 1.1 2.35
1,3,5-Trimethylbenzene 3.2 ug/m3 08/24/19 16:51 108-67-82.3 0.94 2.35
Vinyl acetate ND ug/m3 08/24/19 16:51 108-05-41.7 0.63 2.35
Vinyl chloride 0.79 ug/m3 08/24/19 16:51 75-01-40.61 0.30 2.35
m&p-Xylene 35.2 ug/m3 08/24/19 16:51 179601-23-14.2 1.6 2.35
o-Xylene 10.2 ug/m3 08/24/19 16:51 95-47-62.1 0.81 2.35
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 17 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-5 #3277 Lab ID: 92442461005 Collected: 08/21/19 14:30 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 3660 ug/m3 08/26/19 10:26 67-64-12270 1140 940.8
Benzene 2960 ug/m3 08/26/19 10:26 71-43-2306 144 940.8
Bromodichloromethane ND ug/m3 08/24/19 17:20 75-27-43.3 0.90 2.46
Bromoform ND ug/m3 08/24/19 17:20 75-25-212.9 3.5 2.46
Bromomethane ND ug/m3 08/24/19 17:20 74-83-91.9 0.56 2.46
1,3-Butadiene ND ug/m3 08/24/19 17:20 106-99-01.1 0.31 2.46
2-Butanone (MEK)ND ug/m3 08/24/19 17:20 78-93-37.4 0.91 2.46
Carbon disulfide 40.5 ug/m3 08/24/19 17:20 75-15-01.6 0.54 2.46
Carbon tetrachloride ND ug/m3 08/24/19 17:20 56-23-53.1 1.1 2.46
Chlorobenzene ND ug/m3 08/24/19 17:20 108-90-72.3 0.68 2.46
Chloroethane ND ug/m3 08/24/19 17:20 75-00-31.3 0.64 2.46
Chloroform ND ug/m3 08/24/19 17:20 67-66-31.2 0.48 2.46
Chloromethane ND ug/m3 08/24/19 17:20 74-87-31.0 0.38 2.46
Cyclohexane 624 ug/m3 08/24/19 17:20 110-82-7 E4.3 0.87 2.46
Dibromochloromethane ND ug/m3 08/24/19 17:20 124-48-14.3 1.8 2.46
1,2-Dibromoethane (EDB)ND ug/m3 08/24/19 17:20 106-93-43.8 0.90 2.46
1,2-Dichlorobenzene ND ug/m3 08/24/19 17:20 95-50-13.0 1.2 2.46
1,3-Dichlorobenzene ND ug/m3 08/24/19 17:20 541-73-13.0 1.4 2.46
1,4-Dichlorobenzene ND ug/m3 08/24/19 17:20 106-46-77.5 2.5 2.46
Dichlorodifluoromethane 1.6J ug/m3 08/24/19 17:20 75-71-82.5 0.72 2.46
1,1-Dichloroethane 7.0 ug/m3 08/24/19 17:20 75-34-32.0 0.55 2.46
1,2-Dichloroethane ND ug/m3 08/24/19 17:20 107-06-21.0 0.37 2.46
1,1-Dichloroethene ND ug/m3 08/24/19 17:20 75-35-42.0 0.67 2.46
cis-1,2-Dichloroethene ND ug/m3 08/24/19 17:20 156-59-22.0 0.54 2.46
trans-1,2-Dichloroethene 1.7J ug/m3 08/24/19 17:20 156-60-52.0 0.70 2.46
1,2-Dichloropropane ND ug/m3 08/24/19 17:20 78-87-52.3 0.57 2.46
cis-1,3-Dichloropropene ND ug/m3 08/24/19 17:20 10061-01-52.3 0.75 2.46
trans-1,3-Dichloropropene ND ug/m3 08/24/19 17:20 10061-02-62.3 1.1 2.46
Dichlorotetrafluoroethane ND ug/m3 08/24/19 17:20 76-14-23.5 1.1 2.46
Ethyl acetate ND ug/m3 08/24/19 17:20 141-78-61.8 0.47 2.46
Ethylbenzene 15400 ug/m3 08/26/19 10:26 100-41-4831 287 940.8
4-Ethyltoluene 998 ug/m3 08/24/19 17:20 622-96-8 E6.2 1.4 2.46
n-Heptane 13600 ug/m3 08/26/19 10:26 142-82-5784 358 940.8
Hexachloro-1,3-butadiene ND ug/m3 08/24/19 17:20 87-68-313.3 4.8 2.46
n-Hexane 5000 ug/m3 08/26/19 10:26 110-54-3674 293 940.8
2-Hexanone 69.4 ug/m3 08/24/19 17:20 591-78-610.2 1.8 2.46
Methylene Chloride 22.5 ug/m3 08/24/19 17:20 75-09-28.7 2.3 2.46
4-Methyl-2-pentanone (MIBK)ND ug/m3 08/24/19 17:20 108-10-110.2 1.3 2.46
Methyl-tert-butyl ether 210 ug/m3 08/24/19 17:20 1634-04-49.0 1.6 2.46
Naphthalene ND ug/m3 08/24/19 17:20 91-20-36.5 3.2 2.46
Propylene 119 ug/m3 08/24/19 17:20 115-07-10.86 0.35 2.46
Styrene 7.3 ug/m3 08/24/19 17:20 100-42-52.1 0.85 2.46
1,1,2,2-Tetrachloroethane ND ug/m3 08/24/19 17:20 79-34-51.7 0.72 2.46
Tetrachloroethene ND ug/m3 08/24/19 17:20 127-18-43.4 0.77 2.46
Tetrahydrofuran ND ug/m3 08/24/19 17:20 109-99-91.5 0.64 2.46
Toluene 123 ug/m3 08/24/19 17:20 108-88-31.9 0.86 2.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 18 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-5 #3277 Lab ID: 92442461005 Collected: 08/21/19 14:30 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 08/24/19 17:20 120-82-118.5 9.2 2.46
1,1,1-Trichloroethane ND ug/m3 08/24/19 17:20 71-55-62.7 0.76 2.46
1,1,2-Trichloroethane ND ug/m3 08/24/19 17:20 79-00-51.4 0.62 2.46
Trichloroethene ND ug/m3 08/24/19 17:20 79-01-61.3 0.63 2.46
Trichlorofluoromethane ND ug/m3 08/24/19 17:20 75-69-42.8 0.90 2.46
1,1,2-Trichlorotrifluoroethane ND ug/m3 08/24/19 17:20 76-13-13.8 1.4 2.46
1,2,4-Trimethylbenzene 461 ug/m3 08/24/19 17:20 95-63-6 E2.5 1.1 2.46
1,3,5-Trimethylbenzene 38.0 ug/m3 08/24/19 17:20 108-67-82.5 0.98 2.46
Vinyl acetate ND ug/m3 08/24/19 17:20 108-05-41.8 0.66 2.46
Vinyl chloride ND ug/m3 08/24/19 17:20 75-01-40.64 0.31 2.46
m&p-Xylene 4150 ug/m3 08/26/19 10:26 179601-23-11670 658 940.8
o-Xylene 58.0 ug/m3 08/24/19 17:20 95-47-62.2 0.85 2.46
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 19 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-6 #3025 Lab ID: 92442461006 Collected: 08/21/19 14:56 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 139 ug/m3 08/24/19 17:49 67-64-14.7 2.3 1.94
Benzene 3.7 ug/m3 08/24/19 17:49 71-43-20.63 0.30 1.94
Bromodichloromethane ND ug/m3 08/24/19 17:49 75-27-42.6 0.71 1.94
Bromoform ND ug/m3 08/24/19 17:49 75-25-210.2 2.8 1.94
Bromomethane ND ug/m3 08/24/19 17:49 74-83-91.5 0.44 1.94
1,3-Butadiene ND ug/m3 08/24/19 17:49 106-99-00.87 0.25 1.94
2-Butanone (MEK)20.3 ug/m3 08/24/19 17:49 78-93-35.8 0.72 1.94
Carbon disulfide 4.5 ug/m3 08/24/19 17:49 75-15-01.2 0.42 1.94
Carbon tetrachloride ND ug/m3 08/24/19 17:49 56-23-52.5 0.83 1.94
Chlorobenzene ND ug/m3 08/24/19 17:49 108-90-71.8 0.53 1.94
Chloroethane ND ug/m3 08/24/19 17:49 75-00-31.0 0.50 1.94
Chloroform 0.73J ug/m3 08/24/19 17:49 67-66-30.96 0.38 1.94
Chloromethane ND ug/m3 08/24/19 17:49 74-87-30.81 0.30 1.94
Cyclohexane ND ug/m3 08/24/19 17:49 110-82-73.4 0.68 1.94
Dibromochloromethane ND ug/m3 08/24/19 17:49 124-48-13.4 1.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 08/24/19 17:49 106-93-43.0 0.71 1.94
1,2-Dichlorobenzene ND ug/m3 08/24/19 17:49 95-50-12.4 0.97 1.94
1,3-Dichlorobenzene ND ug/m3 08/24/19 17:49 541-73-12.4 1.1 1.94
1,4-Dichlorobenzene ND ug/m3 08/24/19 17:49 106-46-75.9 1.9 1.94
Dichlorodifluoromethane 0.92J ug/m3 08/24/19 17:49 75-71-82.0 0.57 1.94
1,1-Dichloroethane 0.96J ug/m3 08/24/19 17:49 75-34-31.6 0.44 1.94
1,2-Dichloroethane ND ug/m3 08/24/19 17:49 107-06-20.80 0.29 1.94
1,1-Dichloroethene ND ug/m3 08/24/19 17:49 75-35-41.6 0.53 1.94
cis-1,2-Dichloroethene ND ug/m3 08/24/19 17:49 156-59-21.6 0.42 1.94
trans-1,2-Dichloroethene 71.7 ug/m3 08/24/19 17:49 156-60-51.6 0.55 1.94
1,2-Dichloropropane ND ug/m3 08/24/19 17:49 78-87-51.8 0.45 1.94
cis-1,3-Dichloropropene ND ug/m3 08/24/19 17:49 10061-01-51.8 0.59 1.94
trans-1,3-Dichloropropene ND ug/m3 08/24/19 17:49 10061-02-61.8 0.85 1.94
Dichlorotetrafluoroethane ND ug/m3 08/24/19 17:49 76-14-22.8 0.85 1.94
Ethyl acetate 23.7 ug/m3 08/24/19 17:49 141-78-61.4 0.37 1.94
Ethylbenzene 10 ug/m3 08/24/19 17:49 100-41-41.7 0.59 1.94
4-Ethyltoluene 7.8 ug/m3 08/24/19 17:49 622-96-84.8 1.1 1.94
n-Heptane 9.7 ug/m3 08/24/19 17:49 142-82-51.6 0.74 1.94
Hexachloro-1,3-butadiene ND ug/m3 08/24/19 17:49 87-68-310.5 3.8 1.94
n-Hexane 10.2 ug/m3 08/24/19 17:49 110-54-31.4 0.60 1.94
2-Hexanone 13.6 ug/m3 08/24/19 17:49 591-78-68.1 1.4 1.94
Methylene Chloride 12.1 ug/m3 08/24/19 17:49 75-09-26.8 1.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 08/24/19 17:49 108-10-18.1 1.0 1.94
Methyl-tert-butyl ether 2.6J ug/m3 08/24/19 17:49 1634-04-47.1 1.3 1.94
Naphthalene ND ug/m3 08/24/19 17:49 91-20-35.2 2.6 1.94
Propylene ND ug/m3 08/24/19 17:49 115-07-10.68 0.28 1.94
Styrene 2.4 ug/m3 08/24/19 17:49 100-42-51.7 0.67 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 08/24/19 17:49 79-34-51.4 0.57 1.94
Tetrachloroethene 0.89J ug/m3 08/24/19 17:49 127-18-42.7 0.61 1.94
Tetrahydrofuran 1.2 ug/m3 08/24/19 17:49 109-99-91.2 0.51 1.94
Toluene 27.0 ug/m3 08/24/19 17:49 108-88-31.5 0.68 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
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Page 20 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-6 #3025 Lab ID: 92442461006 Collected: 08/21/19 14:56 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 08/24/19 17:49 120-82-114.6 7.2 1.94
1,1,1-Trichloroethane ND ug/m3 08/24/19 17:49 71-55-62.2 0.60 1.94
1,1,2-Trichloroethane ND ug/m3 08/24/19 17:49 79-00-51.1 0.48 1.94
Trichloroethene 15.2 ug/m3 08/24/19 17:49 79-01-61.1 0.50 1.94
Trichlorofluoromethane ND ug/m3 08/24/19 17:49 75-69-42.2 0.71 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 08/24/19 17:49 76-13-13.0 1.1 1.94
1,2,4-Trimethylbenzene 12.8 ug/m3 08/24/19 17:49 95-63-61.9 0.88 1.94
1,3,5-Trimethylbenzene 3.1 ug/m3 08/24/19 17:49 108-67-81.9 0.77 1.94
Vinyl acetate ND ug/m3 08/24/19 17:49 108-05-41.4 0.52 1.94
Vinyl chloride ND ug/m3 08/24/19 17:49 75-01-40.50 0.24 1.94
m&p-Xylene 32.3 ug/m3 08/24/19 17:49 179601-23-13.4 1.4 1.94
o-Xylene 9.4 ug/m3 08/24/19 17:49 95-47-61.7 0.67 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
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Page 21 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-7 #3035 Lab ID: 92442461007 Collected: 08/21/19 15:30 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 387 ug/m3 08/24/19 18:18 67-64-15.3 2.6 2.19
Benzene 6.8 ug/m3 08/24/19 18:18 71-43-20.71 0.34 2.19
Bromodichloromethane ND ug/m3 08/24/19 18:18 75-27-43.0 0.80 2.19
Bromoform ND ug/m3 08/24/19 18:18 75-25-211.5 3.1 2.19
Bromomethane ND ug/m3 08/24/19 18:18 74-83-91.7 0.50 2.19
1,3-Butadiene ND ug/m3 08/24/19 18:18 106-99-00.99 0.28 2.19
2-Butanone (MEK)40.5 ug/m3 08/24/19 18:18 78-93-36.6 0.81 2.19
Carbon disulfide 8.7 ug/m3 08/24/19 18:18 75-15-01.4 0.48 2.19
Carbon tetrachloride ND ug/m3 08/24/19 18:18 56-23-52.8 0.94 2.19
Chlorobenzene ND ug/m3 08/24/19 18:18 108-90-72.0 0.60 2.19
Chloroethane ND ug/m3 08/24/19 18:18 75-00-31.2 0.57 2.19
Chloroform ND ug/m3 08/24/19 18:18 67-66-31.1 0.43 2.19
Chloromethane 1.0 ug/m3 08/24/19 18:18 74-87-30.92 0.34 2.19
Cyclohexane 2.7J ug/m3 08/24/19 18:18 110-82-73.8 0.77 2.19
Dibromochloromethane ND ug/m3 08/24/19 18:18 124-48-13.8 1.6 2.19
1,2-Dibromoethane (EDB)ND ug/m3 08/24/19 18:18 106-93-43.4 0.80 2.19
1,2-Dichlorobenzene ND ug/m3 08/24/19 18:18 95-50-12.7 1.1 2.19
1,3-Dichlorobenzene ND ug/m3 08/24/19 18:18 541-73-12.7 1.3 2.19
1,4-Dichlorobenzene ND ug/m3 08/24/19 18:18 106-46-76.7 2.2 2.19
Dichlorodifluoromethane 2.0J ug/m3 08/24/19 18:18 75-71-82.2 0.64 2.19
1,1-Dichloroethane ND ug/m3 08/24/19 18:18 75-34-31.8 0.49 2.19
1,2-Dichloroethane ND ug/m3 08/24/19 18:18 107-06-20.90 0.33 2.19
1,1-Dichloroethene ND ug/m3 08/24/19 18:18 75-35-41.8 0.60 2.19
cis-1,2-Dichloroethene ND ug/m3 08/24/19 18:18 156-59-21.8 0.48 2.19
trans-1,2-Dichloroethene ND ug/m3 08/24/19 18:18 156-60-51.8 0.62 2.19
1,2-Dichloropropane ND ug/m3 08/24/19 18:18 78-87-52.1 0.50 2.19
cis-1,3-Dichloropropene ND ug/m3 08/24/19 18:18 10061-01-52.0 0.67 2.19
trans-1,3-Dichloropropene ND ug/m3 08/24/19 18:18 10061-02-62.0 0.96 2.19
Dichlorotetrafluoroethane ND ug/m3 08/24/19 18:18 76-14-23.1 0.96 2.19
Ethyl acetate ND ug/m3 08/24/19 18:18 141-78-61.6 0.42 2.19
Ethylbenzene 2.8 ug/m3 08/24/19 18:18 100-41-41.9 0.67 2.19
4-Ethyltoluene ND ug/m3 08/24/19 18:18 622-96-85.5 1.2 2.19
n-Heptane 4.4 ug/m3 08/24/19 18:18 142-82-51.8 0.83 2.19
Hexachloro-1,3-butadiene ND ug/m3 08/24/19 18:18 87-68-311.9 4.3 2.19
n-Hexane 7.8 ug/m3 08/24/19 18:18 110-54-31.6 0.68 2.19
2-Hexanone 10.3 ug/m3 08/24/19 18:18 591-78-69.1 1.6 2.19
Methylene Chloride 12.5 ug/m3 08/24/19 18:18 75-09-27.7 2.1 2.19
4-Methyl-2-pentanone (MIBK)ND ug/m3 08/24/19 18:18 108-10-19.1 1.1 2.19
Methyl-tert-butyl ether ND ug/m3 08/24/19 18:18 1634-04-48.0 1.5 2.19
Naphthalene ND ug/m3 08/24/19 18:18 91-20-35.8 2.9 2.19
Propylene 9.6 ug/m3 08/24/19 18:18 115-07-10.77 0.31 2.19
Styrene ND ug/m3 08/24/19 18:18 100-42-51.9 0.75 2.19
1,1,2,2-Tetrachloroethane ND ug/m3 08/24/19 18:18 79-34-51.5 0.64 2.19
Tetrachloroethene 0.70J ug/m3 08/24/19 18:18 127-18-43.0 0.69 2.19
Tetrahydrofuran ND ug/m3 08/24/19 18:18 109-99-91.3 0.57 2.19
Toluene 5.8 ug/m3 08/24/19 18:18 108-88-31.7 0.77 2.19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 22 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-7 #3035 Lab ID: 92442461007 Collected: 08/21/19 15:30 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 08/24/19 18:18 120-82-116.5 8.1 2.19
1,1,1-Trichloroethane ND ug/m3 08/24/19 18:18 71-55-62.4 0.68 2.19
1,1,2-Trichloroethane ND ug/m3 08/24/19 18:18 79-00-51.2 0.55 2.19
Trichloroethene ND ug/m3 08/24/19 18:18 79-01-61.2 0.56 2.19
Trichlorofluoromethane 1.1J ug/m3 08/24/19 18:18 75-69-42.5 0.80 2.19
1,1,2-Trichlorotrifluoroethane ND ug/m3 08/24/19 18:18 76-13-13.4 1.2 2.19
1,2,4-Trimethylbenzene 1.6J ug/m3 08/24/19 18:18 95-63-62.2 0.99 2.19
1,3,5-Trimethylbenzene ND ug/m3 08/24/19 18:18 108-67-82.2 0.87 2.19
Vinyl acetate ND ug/m3 08/24/19 18:18 108-05-41.6 0.59 2.19
Vinyl chloride ND ug/m3 08/24/19 18:18 75-01-40.57 0.28 2.19
m&p-Xylene 5.2 ug/m3 08/24/19 18:18 179601-23-13.9 1.5 2.19
o-Xylene 1.5J ug/m3 08/24/19 18:18 95-47-61.9 0.75 2.19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 23 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-8 #2401 Lab ID: 92442461008 Collected: 08/21/19 15:57 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 689 ug/m3 08/24/19 18:47 67-64-18.7 4.4 3.61
Benzene 12.6 ug/m3 08/24/19 18:47 71-43-21.2 0.55 3.61
Bromodichloromethane ND ug/m3 08/24/19 18:47 75-27-44.9 1.3 3.61
Bromoform ND ug/m3 08/24/19 18:47 75-25-219.0 5.1 3.61
Bromomethane ND ug/m3 08/24/19 18:47 74-83-92.8 0.82 3.61
1,3-Butadiene ND ug/m3 08/24/19 18:47 106-99-01.6 0.46 3.61
2-Butanone (MEK)62.0 ug/m3 08/24/19 18:47 78-93-310.8 1.3 3.61
Carbon disulfide 4.0 ug/m3 08/24/19 18:47 75-15-02.3 0.79 3.61
Carbon tetrachloride ND ug/m3 08/24/19 18:47 56-23-54.6 1.5 3.61
Chlorobenzene ND ug/m3 08/24/19 18:47 108-90-73.4 0.99 3.61
Chloroethane ND ug/m3 08/24/19 18:47 75-00-31.9 0.94 3.61
Chloroform 1.2J ug/m3 08/24/19 18:47 67-66-31.8 0.71 3.61
Chloromethane 0.73J ug/m3 08/24/19 18:47 74-87-31.5 0.56 3.61
Cyclohexane ND ug/m3 08/24/19 18:47 110-82-76.3 1.3 3.61
Dibromochloromethane ND ug/m3 08/24/19 18:47 124-48-16.2 2.6 3.61
1,2-Dibromoethane (EDB)ND ug/m3 08/24/19 18:47 106-93-45.6 1.3 3.61
1,2-Dichlorobenzene ND ug/m3 08/24/19 18:47 95-50-14.4 1.8 3.61
1,3-Dichlorobenzene ND ug/m3 08/24/19 18:47 541-73-14.4 2.1 3.61
1,4-Dichlorobenzene ND ug/m3 08/24/19 18:47 106-46-711.0 3.6 3.61
Dichlorodifluoromethane 1.8J ug/m3 08/24/19 18:47 75-71-83.6 1.1 3.61
1,1-Dichloroethane ND ug/m3 08/24/19 18:47 75-34-33.0 0.81 3.61
1,2-Dichloroethane ND ug/m3 08/24/19 18:47 107-06-21.5 0.54 3.61
1,1-Dichloroethene ND ug/m3 08/24/19 18:47 75-35-42.9 0.99 3.61
cis-1,2-Dichloroethene ND ug/m3 08/24/19 18:47 156-59-22.9 0.79 3.61
trans-1,2-Dichloroethene 7.1 ug/m3 08/24/19 18:47 156-60-52.9 1.0 3.61
1,2-Dichloropropane ND ug/m3 08/24/19 18:47 78-87-53.4 0.83 3.61
cis-1,3-Dichloropropene ND ug/m3 08/24/19 18:47 10061-01-53.3 1.1 3.61
trans-1,3-Dichloropropene ND ug/m3 08/24/19 18:47 10061-02-63.3 1.6 3.61
Dichlorotetrafluoroethane ND ug/m3 08/24/19 18:47 76-14-25.1 1.6 3.61
Ethyl acetate 1.9J ug/m3 08/24/19 18:47 141-78-62.6 0.69 3.61
Ethylbenzene 6.4 ug/m3 08/24/19 18:47 100-41-43.2 1.1 3.61
4-Ethyltoluene 2.5J ug/m3 08/24/19 18:47 622-96-89.0 2.1 3.61
n-Heptane 8.6 ug/m3 08/24/19 18:47 142-82-53.0 1.4 3.61
Hexachloro-1,3-butadiene ND ug/m3 08/24/19 18:47 87-68-319.6 7.1 3.61
n-Hexane 17.3 ug/m3 08/24/19 18:47 110-54-32.6 1.1 3.61
2-Hexanone 28.6 ug/m3 08/24/19 18:47 591-78-615.0 2.7 3.61
Methylene Chloride 86.5 ug/m3 08/24/19 18:47 75-09-212.7 3.4 3.61
4-Methyl-2-pentanone (MIBK)ND ug/m3 08/24/19 18:47 108-10-115.0 1.9 3.61
Methyl-tert-butyl ether ND ug/m3 08/24/19 18:47 1634-04-413.2 2.4 3.61
Naphthalene ND ug/m3 08/24/19 18:47 91-20-39.6 4.8 3.61
Propylene 28.1 ug/m3 08/24/19 18:47 115-07-11.3 0.52 3.61
Styrene ND ug/m3 08/24/19 18:47 100-42-53.1 1.2 3.61
1,1,2,2-Tetrachloroethane ND ug/m3 08/24/19 18:47 79-34-52.5 1.1 3.61
Tetrachloroethene ND ug/m3 08/24/19 18:47 127-18-45.0 1.1 3.61
Tetrahydrofuran ND ug/m3 08/24/19 18:47 109-99-92.2 0.94 3.61
Toluene 18.5 ug/m3 08/24/19 18:47 108-88-32.8 1.3 3.61
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 24 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-8 #2401 Lab ID: 92442461008 Collected: 08/21/19 15:57 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 08/24/19 18:47 120-82-127.2 13.4 3.61
1,1,1-Trichloroethane ND ug/m3 08/24/19 18:47 71-55-64.0 1.1 3.61
1,1,2-Trichloroethane ND ug/m3 08/24/19 18:47 79-00-52.0 0.90 3.61
Trichloroethene 1.0J ug/m3 08/24/19 18:47 79-01-62.0 0.93 3.61
Trichlorofluoromethane ND ug/m3 08/24/19 18:47 75-69-44.1 1.3 3.61
1,1,2-Trichlorotrifluoroethane ND ug/m3 08/24/19 18:47 76-13-15.6 2.0 3.61
1,2,4-Trimethylbenzene 6.6 ug/m3 08/24/19 18:47 95-63-63.6 1.6 3.61
1,3,5-Trimethylbenzene 2.0J ug/m3 08/24/19 18:47 108-67-83.6 1.4 3.61
Vinyl acetate ND ug/m3 08/24/19 18:47 108-05-42.6 0.97 3.61
Vinyl chloride ND ug/m3 08/24/19 18:47 75-01-40.94 0.45 3.61
m&p-Xylene 21.8 ug/m3 08/24/19 18:47 179601-23-16.4 2.5 3.61
o-Xylene 6.3 ug/m3 08/24/19 18:47 95-47-63.2 1.2 3.61
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 25 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: DUP 1 #3252 Lab ID: 92442461009 Collected: 08/21/19 00:00 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
Acetone 1200 ug/m3 08/24/19 19:17 67-64-1 E5.8 2.9 2.4
Benzene 14.4 ug/m3 08/24/19 19:17 71-43-20.78 0.37 2.4
Bromodichloromethane ND ug/m3 08/24/19 19:17 75-27-43.3 0.88 2.4
Bromoform ND ug/m3 08/24/19 19:17 75-25-212.6 3.4 2.4
Bromomethane ND ug/m3 08/24/19 19:17 74-83-91.9 0.54 2.4
1,3-Butadiene ND ug/m3 08/24/19 19:17 106-99-01.1 0.31 2.4
2-Butanone (MEK)105 ug/m3 08/24/19 19:17 78-93-37.2 0.89 2.4
Carbon disulfide 52.9 ug/m3 08/24/19 19:17 75-15-01.5 0.53 2.4
Carbon tetrachloride ND ug/m3 08/24/19 19:17 56-23-53.1 1.0 2.4
Chlorobenzene ND ug/m3 08/24/19 19:17 108-90-72.2 0.66 2.4
Chloroethane ND ug/m3 08/24/19 19:17 75-00-31.3 0.62 2.4
Chloroform 19.5 ug/m3 08/24/19 19:17 67-66-31.2 0.47 2.4
Chloromethane 1.8 ug/m3 08/24/19 19:17 74-87-31.0 0.37 2.4
Cyclohexane 22.3 ug/m3 08/24/19 19:17 110-82-74.2 0.85 2.4
Dibromochloromethane ND ug/m3 08/24/19 19:17 124-48-14.2 1.7 2.4
1,2-Dibromoethane (EDB)ND ug/m3 08/24/19 19:17 106-93-43.7 0.88 2.4
1,2-Dichlorobenzene ND ug/m3 08/24/19 19:17 95-50-12.9 1.2 2.4
1,3-Dichlorobenzene 1.8J ug/m3 08/24/19 19:17 541-73-12.9 1.4 2.4
1,4-Dichlorobenzene ND ug/m3 08/24/19 19:17 106-46-77.3 2.4 2.4
Dichlorodifluoromethane 2.4J ug/m3 08/24/19 19:17 75-71-82.4 0.70 2.4
1,1-Dichloroethane ND ug/m3 08/24/19 19:17 75-34-32.0 0.54 2.4
1,2-Dichloroethane ND ug/m3 08/24/19 19:17 107-06-20.99 0.36 2.4
1,1-Dichloroethene ND ug/m3 08/24/19 19:17 75-35-41.9 0.66 2.4
cis-1,2-Dichloroethene ND ug/m3 08/24/19 19:17 156-59-21.9 0.53 2.4
trans-1,2-Dichloroethene 1.6J ug/m3 08/24/19 19:17 156-60-51.9 0.68 2.4
1,2-Dichloropropane ND ug/m3 08/24/19 19:17 78-87-52.3 0.55 2.4
cis-1,3-Dichloropropene ND ug/m3 08/24/19 19:17 10061-01-52.2 0.73 2.4
trans-1,3-Dichloropropene ND ug/m3 08/24/19 19:17 10061-02-62.2 1.1 2.4
Dichlorotetrafluoroethane ND ug/m3 08/24/19 19:17 76-14-23.4 1.0 2.4
Ethyl acetate ND ug/m3 08/24/19 19:17 141-78-61.8 0.46 2.4
Ethylbenzene 9.0 ug/m3 08/24/19 19:17 100-41-42.1 0.73 2.4
4-Ethyltoluene 3.8J ug/m3 08/24/19 19:17 622-96-86.0 1.4 2.4
n-Heptane 78.8 ug/m3 08/24/19 19:17 142-82-52.0 0.91 2.4
Hexachloro-1,3-butadiene ND ug/m3 08/24/19 19:17 87-68-313.0 4.7 2.4
n-Hexane 55.2 ug/m3 08/24/19 19:17 110-54-31.7 0.75 2.4
2-Hexanone 38.9 ug/m3 08/24/19 19:17 591-78-610 1.8 2.4
Methylene Chloride 21.0 ug/m3 08/24/19 19:17 75-09-28.5 2.3 2.4
4-Methyl-2-pentanone (MIBK)ND ug/m3 08/24/19 19:17 108-10-110 1.2 2.4
Methyl-tert-butyl ether ND ug/m3 08/24/19 19:17 1634-04-48.8 1.6 2.4
Naphthalene ND ug/m3 08/24/19 19:17 91-20-36.4 3.2 2.4
Propylene 639 ug/m3 08/24/19 19:17 115-07-1 E0.84 0.34 2.4
Styrene 0.86J ug/m3 08/24/19 19:17 100-42-52.1 0.83 2.4
1,1,2,2-Tetrachloroethane ND ug/m3 08/24/19 19:17 79-34-51.7 0.70 2.4
Tetrachloroethene 1.6J ug/m3 08/24/19 19:17 127-18-43.3 0.75 2.4
Tetrahydrofuran ND ug/m3 08/24/19 19:17 109-99-91.4 0.63 2.4
Toluene 33.4 ug/m3 08/24/19 19:17 108-88-31.8 0.84 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 26 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: DUP 1 #3252 Lab ID: 92442461009 Collected: 08/21/19 00:00 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15TO15 MSV AIR
1,2,4-Trichlorobenzene ND ug/m3 08/24/19 19:17 120-82-118.1 8.9 2.4
1,1,1-Trichloroethane ND ug/m3 08/24/19 19:17 71-55-62.7 0.74 2.4
1,1,2-Trichloroethane ND ug/m3 08/24/19 19:17 79-00-51.3 0.60 2.4
Trichloroethene ND ug/m3 08/24/19 19:17 79-01-61.3 0.62 2.4
Trichlorofluoromethane 1.6J ug/m3 08/24/19 19:17 75-69-42.7 0.88 2.4
1,1,2-Trichlorotrifluoroethane ND ug/m3 08/24/19 19:17 76-13-13.7 1.4 2.4
1,2,4-Trimethylbenzene 10.8 ug/m3 08/24/19 19:17 95-63-62.4 1.1 2.4
1,3,5-Trimethylbenzene 3.0 ug/m3 08/24/19 19:17 108-67-82.4 0.96 2.4
Vinyl acetate ND ug/m3 08/24/19 19:17 108-05-41.7 0.65 2.4
Vinyl chloride ND ug/m3 08/24/19 19:17 75-01-40.62 0.30 2.4
m&p-Xylene 34.7 ug/m3 08/24/19 19:17 179601-23-14.2 1.7 2.4
o-Xylene 11.0 ug/m3 08/24/19 19:17 95-47-62.1 0.83 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 27 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-1 #2591 - Individual
Cert.
Lab ID: 92442461010 Collected: 08/21/19 12:35 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Acetone ND ug/m3 07/25/19 09:00 67-64-11.2 0.60 0.5
Benzene ND ug/m3 07/25/19 09:00 71-43-20.16 0.076 0.5
Benzyl chloride ND ug/m3 07/25/19 09:00 100-44-71.3 0.60 0.5
Bromodichloromethane ND ug/m3 07/25/19 09:00 75-27-40.68 0.18 0.5
Bromoform ND ug/m3 07/25/19 09:00 75-25-22.6 0.71 0.5
Bromomethane ND ug/m3 07/25/19 09:00 74-83-90.39 0.11 0.5
1,3-Butadiene ND ug/m3 07/25/19 09:00 106-99-00.22 0.064 0.5
2-Butanone (MEK)ND ug/m3 07/25/19 09:00 78-93-31.5 0.18 0.5
Carbon disulfide ND ug/m3 07/25/19 09:00 75-15-00.32 0.11 0.5
Carbon tetrachloride ND ug/m3 07/25/19 09:00 56-23-50.64 0.21 0.5
Chlorobenzene ND ug/m3 07/25/19 09:00 108-90-70.47 0.14 0.5
Chloroethane ND ug/m3 07/25/19 09:00 75-00-30.27 0.13 0.5
Chloroform ND ug/m3 07/25/19 09:00 67-66-30.25 0.098 0.5
Chloromethane ND ug/m3 07/25/19 09:00 74-87-30.21 0.078 0.5
Cyclohexane ND ug/m3 07/25/19 09:00 110-82-70.88 0.18 0.5
Dibromochloromethane ND ug/m3 07/25/19 09:00 124-48-10.86 0.36 0.5
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 09:00 106-93-40.39 0.18 0.5
1,2-Dichlorobenzene ND ug/m3 07/25/19 09:00 95-50-10.61 0.25 0.5
1,3-Dichlorobenzene ND ug/m3 07/25/19 09:00 541-73-10.61 0.29 0.5
1,4-Dichlorobenzene ND ug/m3 07/25/19 09:00 106-46-71.5 0.50 0.5
Dichlorodifluoromethane ND ug/m3 07/25/19 09:00 75-71-80.50 0.15 0.5
1,1-Dichloroethane ND ug/m3 07/25/19 09:00 75-34-30.41 0.11 0.5
1,2-Dichloroethane ND ug/m3 07/25/19 09:00 107-06-20.21 0.075 0.5
1,1-Dichloroethene ND ug/m3 07/25/19 09:00 75-35-40.40 0.14 0.5
cis-1,2-Dichloroethene ND ug/m3 07/25/19 09:00 156-59-20.40 0.11 0.5
trans-1,2-Dichloroethene ND ug/m3 07/25/19 09:00 156-60-50.40 0.14 0.5
1,2-Dichloropropane ND ug/m3 07/25/19 09:00 78-87-50.47 0.12 0.5
cis-1,3-Dichloropropene ND ug/m3 07/25/19 09:00 10061-01-50.46 0.15 0.5
trans-1,3-Dichloropropene ND ug/m3 07/25/19 09:00 10061-02-60.46 0.22 0.5
Dichlorotetrafluoroethane ND ug/m3 07/25/19 09:00 76-14-20.71 0.22 0.5
Ethanol ND ug/m3 07/25/19 09:00 64-17-50.96 0.41 0.5
Ethyl acetate ND ug/m3 07/25/19 09:00 141-78-60.37 0.095 0.5
Ethylbenzene ND ug/m3 07/25/19 09:00 100-41-40.44 0.15 0.5
4-Ethyltoluene ND ug/m3 07/25/19 09:00 622-96-81.2 0.28 0.5
n-Heptane ND ug/m3 07/25/19 09:00 142-82-50.42 0.19 0.5
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 09:00 87-68-32.7 0.98 0.5
n-Hexane ND ug/m3 07/25/19 09:00 110-54-30.36 0.16 0.5
2-Hexanone ND ug/m3 07/25/19 09:00 591-78-62.1 0.37 0.5
Methylene Chloride ND ug/m3 07/25/19 09:00 75-09-21.8 0.47 0.5
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 09:00 108-10-12.1 0.26 0.5
Methyl-tert-butyl ether ND ug/m3 07/25/19 09:00 1634-04-41.8 0.33 0.5
Naphthalene ND ug/m3 07/25/19 09:00 91-20-31.3 0.66 0.5
2-Propanol 0.81J ug/m3 07/25/19 09:00 67-63-01.2 0.35 0.5
Propylene ND ug/m3 07/25/19 09:00 115-07-10.18 0.072 0.5
Styrene ND ug/m3 07/25/19 09:00 100-42-50.43 0.17 0.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 28 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-1 #2591 - Individual
Cert.
Lab ID: 92442461010 Collected: 08/21/19 12:35 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 09:00 79-34-50.35 0.15 0.5
Tetrachloroethene ND ug/m3 07/25/19 09:00 127-18-40.34 0.16 0.5
Tetrahydrofuran ND ug/m3 07/25/19 09:00 109-99-90.30 0.13 0.5
Toluene ND ug/m3 07/25/19 09:00 108-88-30.38 0.18 0.5
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 09:00 120-82-13.8 1.9 0.5
1,1,1-Trichloroethane ND ug/m3 07/25/19 09:00 71-55-60.56 0.15 0.5
1,1,2-Trichloroethane ND ug/m3 07/25/19 09:00 79-00-50.28 0.12 0.5
Trichloroethene ND ug/m3 07/25/19 09:00 79-01-60.27 0.13 0.5
Trichlorofluoromethane ND ug/m3 07/25/19 09:00 75-69-40.57 0.18 0.5
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 09:00 76-13-10.78 0.28 0.5
1,2,4-Trimethylbenzene ND ug/m3 07/25/19 09:00 95-63-60.50 0.23 0.5
1,3,5-Trimethylbenzene ND ug/m3 07/25/19 09:00 108-67-80.50 0.20 0.5
Vinyl acetate ND ug/m3 07/25/19 09:00 108-05-40.89 0.14 0.5
Vinyl chloride ND ug/m3 07/25/19 09:00 75-01-40.13 0.063 0.5
m&p-Xylene ND ug/m3 07/25/19 09:00 179601-23-10.88 0.35 0.5
o-Xylene ND ug/m3 07/25/19 09:00 95-47-60.44 0.17 0.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 29 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-2 #3250 - Individual
Cert.
Lab ID: 92442461011 Collected: 08/21/19 13:21 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Acetone ND ug/m3 06/01/19 09:32 67-64-12.4 1.2 1
Benzene ND ug/m3 06/01/19 09:32 71-43-20.32 0.15 1
Benzyl chloride ND ug/m3 06/01/19 09:32 100-44-72.6 1.2 1
Bromodichloromethane ND ug/m3 06/01/19 09:32 75-27-41.4 0.37 1
Bromoform ND ug/m3 06/01/19 09:32 75-25-25.2 1.4 1
Bromomethane ND ug/m3 06/01/19 09:32 74-83-90.79 0.23 1
1,3-Butadiene ND ug/m3 06/01/19 09:32 106-99-00.45 0.13 1
2-Butanone (MEK)ND ug/m3 06/01/19 09:32 78-93-33.0 0.37 1
Carbon disulfide ND ug/m3 06/01/19 09:32 75-15-00.63 0.22 1
Carbon tetrachloride ND ug/m3 06/01/19 09:32 56-23-51.3 0.43 1
Chlorobenzene ND ug/m3 06/01/19 09:32 108-90-70.94 0.28 1
Chloroethane ND ug/m3 06/01/19 09:32 75-00-31.3 0.26 1
Chloroform ND ug/m3 06/01/19 09:32 67-66-30.50 0.20 1
Chloromethane ND ug/m3 06/01/19 09:32 74-87-30.42 0.16 1
Cyclohexane ND ug/m3 06/01/19 09:32 110-82-71.8 0.35 1
Dibromochloromethane ND ug/m3 06/01/19 09:32 124-48-11.7 0.72 1
1,2-Dibromoethane (EDB)ND ug/m3 06/01/19 09:32 106-93-40.78 0.37 1
1,2-Dichlorobenzene ND ug/m3 06/01/19 09:32 95-50-11.2 0.50 1
1,3-Dichlorobenzene ND ug/m3 06/01/19 09:32 541-73-11.2 0.58 1
1,4-Dichlorobenzene ND ug/m3 06/01/19 09:32 106-46-73.1 1.0 1
Dichlorodifluoromethane ND ug/m3 06/01/19 09:32 75-71-81.0 0.29 1
1,1-Dichloroethane ND ug/m3 06/01/19 09:32 75-34-30.82 0.22 1
1,2-Dichloroethane ND ug/m3 06/01/19 09:32 107-06-20.41 0.15 1
1,1-Dichloroethene ND ug/m3 06/01/19 09:32 75-35-40.81 0.27 1
cis-1,2-Dichloroethene ND ug/m3 06/01/19 09:32 156-59-20.81 0.22 1
trans-1,2-Dichloroethene ND ug/m3 06/01/19 09:32 156-60-50.81 0.28 1
1,2-Dichloropropane ND ug/m3 06/01/19 09:32 78-87-50.94 0.23 1
cis-1,3-Dichloropropene ND ug/m3 06/01/19 09:32 10061-01-50.92 0.30 1
trans-1,3-Dichloropropene ND ug/m3 06/01/19 09:32 10061-02-60.92 0.44 1
Dichlorotetrafluoroethane ND ug/m3 06/01/19 09:32 76-14-21.4 0.44 1
Ethanol ND ug/m3 06/01/19 09:32 64-17-51.9 0.81 1
Ethyl acetate ND ug/m3 06/01/19 09:32 141-78-60.73 0.19 1
Ethylbenzene ND ug/m3 06/01/19 09:32 100-41-40.88 0.30 1
4-Ethyltoluene ND ug/m3 06/01/19 09:32 622-96-82.5 0.57 1
n-Heptane ND ug/m3 06/01/19 09:32 142-82-50.83 0.38 1
Hexachloro-1,3-butadiene ND ug/m3 06/01/19 09:32 87-68-35.4 2.0 1
n-Hexane ND ug/m3 06/01/19 09:32 110-54-30.72 0.31 1
2-Hexanone ND ug/m3 06/01/19 09:32 591-78-64.2 0.74 1
Methylene Chloride ND ug/m3 06/01/19 09:32 75-09-23.5 0.94 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 06/01/19 09:32 108-10-14.2 0.52 1
Methyl-tert-butyl ether ND ug/m3 06/01/19 09:32 1634-04-43.7 0.66 1
Naphthalene ND ug/m3 06/01/19 09:32 91-20-32.7 1.3 1
2-Propanol ND ug/m3 06/01/19 09:32 67-63-02.5 0.70 1
Propylene ND ug/m3 06/01/19 09:32 115-07-10.35 0.14 1
Styrene ND ug/m3 06/01/19 09:32 100-42-50.87 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 30 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-2 #3250 - Individual
Cert.
Lab ID: 92442461011 Collected: 08/21/19 13:21 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
1,1,2,2-Tetrachloroethane ND ug/m3 06/01/19 09:32 79-34-50.70 0.29 1
Tetrachloroethene ND ug/m3 06/01/19 09:32 127-18-40.69 0.31 1
Tetrahydrofuran ND ug/m3 06/01/19 09:32 109-99-90.60 0.26 1
Toluene ND ug/m3 06/01/19 09:32 108-88-30.77 0.35 1
1,2,4-Trichlorobenzene ND ug/m3 06/01/19 09:32 120-82-17.5 3.7 1
1,1,1-Trichloroethane ND ug/m3 06/01/19 09:32 71-55-61.1 0.31 1
1,1,2-Trichloroethane ND ug/m3 06/01/19 09:32 79-00-50.56 0.25 1
Trichloroethene ND ug/m3 06/01/19 09:32 79-01-60.55 0.26 1
Trichlorofluoromethane ND ug/m3 06/01/19 09:32 75-69-41.1 0.37 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 06/01/19 09:32 76-13-11.6 0.56 1
1,2,4-Trimethylbenzene ND ug/m3 06/01/19 09:32 95-63-61.0 0.45 1
1,3,5-Trimethylbenzene ND ug/m3 06/01/19 09:32 108-67-81.0 0.40 1
Vinyl acetate ND ug/m3 06/01/19 09:32 108-05-40.72 0.27 1
Vinyl chloride ND ug/m3 06/01/19 09:32 75-01-40.52 0.13 1
m&p-Xylene ND ug/m3 06/01/19 09:32 179601-23-11.8 0.70 1
o-Xylene ND ug/m3 06/01/19 09:32 95-47-60.88 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 31 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-3 #2791 - Individual
Cert.
Lab ID: 92442461012 Collected: 08/21/19 13:23 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Acetone ND ug/m3 07/26/19 09:13 67-64-12.4 1.2 1
Benzene ND ug/m3 07/26/19 09:13 71-43-20.32 0.15 1
Benzyl chloride ND ug/m3 07/26/19 09:13 100-44-72.6 1.2 1
Bromodichloromethane ND ug/m3 07/26/19 09:13 75-27-41.4 0.37 1
Bromoform ND ug/m3 07/26/19 09:13 75-25-25.2 1.4 1
Bromomethane ND ug/m3 07/26/19 09:13 74-83-90.79 0.23 1
1,3-Butadiene ND ug/m3 07/26/19 09:13 106-99-00.45 0.13 1
2-Butanone (MEK)ND ug/m3 07/26/19 09:13 78-93-33.0 0.37 1
Carbon disulfide ND ug/m3 07/26/19 09:13 75-15-00.63 0.22 1
Carbon tetrachloride ND ug/m3 07/26/19 09:13 56-23-51.3 0.43 1
Chlorobenzene ND ug/m3 07/26/19 09:13 108-90-70.94 0.28 1
Chloroethane ND ug/m3 07/26/19 09:13 75-00-30.54 0.26 1
Chloroform ND ug/m3 07/26/19 09:13 67-66-30.50 0.20 1
Chloromethane ND ug/m3 07/26/19 09:13 74-87-30.42 0.16 1
Cyclohexane ND ug/m3 07/26/19 09:13 110-82-71.8 0.35 1
Dibromochloromethane ND ug/m3 07/26/19 09:13 124-48-11.7 0.72 1
1,2-Dibromoethane (EDB)ND ug/m3 07/26/19 09:13 106-93-40.78 0.37 1
1,2-Dichlorobenzene ND ug/m3 07/26/19 09:13 95-50-11.2 0.50 1
1,3-Dichlorobenzene ND ug/m3 07/26/19 09:13 541-73-11.2 0.58 1
1,4-Dichlorobenzene ND ug/m3 07/26/19 09:13 106-46-73.1 1.0 1
Dichlorodifluoromethane ND ug/m3 07/26/19 09:13 75-71-81.0 0.29 1
1,1-Dichloroethane ND ug/m3 07/26/19 09:13 75-34-30.82 0.22 1
1,2-Dichloroethane ND ug/m3 07/26/19 09:13 107-06-20.41 0.15 1
1,1-Dichloroethene ND ug/m3 07/26/19 09:13 75-35-40.81 0.27 1
cis-1,2-Dichloroethene ND ug/m3 07/26/19 09:13 156-59-20.81 0.22 1
trans-1,2-Dichloroethene ND ug/m3 07/26/19 09:13 156-60-50.81 0.28 1
1,2-Dichloropropane ND ug/m3 07/26/19 09:13 78-87-50.94 0.23 1
cis-1,3-Dichloropropene ND ug/m3 07/26/19 09:13 10061-01-50.92 0.30 1
trans-1,3-Dichloropropene ND ug/m3 07/26/19 09:13 10061-02-60.92 0.44 1
Dichlorotetrafluoroethane ND ug/m3 07/26/19 09:13 76-14-21.4 0.44 1
Ethanol ND ug/m3 07/26/19 09:13 64-17-51.9 0.81 1
Ethyl acetate ND ug/m3 07/26/19 09:13 141-78-60.73 0.19 1
Ethylbenzene ND ug/m3 07/26/19 09:13 100-41-40.88 0.30 1
4-Ethyltoluene ND ug/m3 07/26/19 09:13 622-96-82.5 0.57 1
n-Heptane ND ug/m3 07/26/19 09:13 142-82-50.83 0.38 1
Hexachloro-1,3-butadiene ND ug/m3 07/26/19 09:13 87-68-35.4 2.0 1
n-Hexane ND ug/m3 07/26/19 09:13 110-54-30.72 0.31 1
2-Hexanone ND ug/m3 07/26/19 09:13 591-78-64.2 0.74 1
Methylene Chloride ND ug/m3 07/26/19 09:13 75-09-23.5 0.94 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/19 09:13 108-10-14.2 0.52 1
Methyl-tert-butyl ether ND ug/m3 07/26/19 09:13 1634-04-43.7 0.66 1
Naphthalene ND ug/m3 07/26/19 09:13 91-20-32.7 1.3 1
2-Propanol 1.4J ug/m3 07/26/19 09:13 67-63-02.5 0.70 1
Propylene ND ug/m3 07/26/19 09:13 115-07-10.35 0.14 1
Styrene ND ug/m3 07/26/19 09:13 100-42-50.87 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-3 #2791 - Individual
Cert.
Lab ID: 92442461012 Collected: 08/21/19 13:23 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
1,1,2,2-Tetrachloroethane ND ug/m3 07/26/19 09:13 79-34-50.70 0.29 1
Tetrachloroethene ND ug/m3 07/26/19 09:13 127-18-40.69 0.31 1
Tetrahydrofuran ND ug/m3 07/26/19 09:13 109-99-90.60 0.26 1
Toluene ND ug/m3 07/26/19 09:13 108-88-30.77 0.35 1
1,2,4-Trichlorobenzene ND ug/m3 07/26/19 09:13 120-82-17.5 3.7 1
1,1,1-Trichloroethane ND ug/m3 07/26/19 09:13 71-55-61.1 0.31 1
1,1,2-Trichloroethane ND ug/m3 07/26/19 09:13 79-00-50.56 0.25 1
Trichloroethene ND ug/m3 07/26/19 09:13 79-01-60.55 0.26 1
Trichlorofluoromethane ND ug/m3 07/26/19 09:13 75-69-41.1 0.37 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/19 09:13 76-13-11.6 0.56 1
1,2,4-Trimethylbenzene ND ug/m3 07/26/19 09:13 95-63-61.0 0.45 1
1,3,5-Trimethylbenzene ND ug/m3 07/26/19 09:13 108-67-81.0 0.40 1
Vinyl acetate ND ug/m3 07/26/19 09:13 108-05-41.8 0.27 1
Vinyl chloride ND ug/m3 07/26/19 09:13 75-01-40.26 0.13 1
m&p-Xylene ND ug/m3 07/26/19 09:13 179601-23-11.8 0.70 1
o-Xylene ND ug/m3 07/26/19 09:13 95-47-60.88 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-4 #893 - Individual Cert. Lab ID: 92442461013 Collected: 08/21/19 14:07 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Acetone ND ug/m3 05/29/19 08:43 67-64-12.4 1.2 1
Benzene ND ug/m3 05/29/19 08:43 71-43-20.32 0.15 1
Benzyl chloride ND ug/m3 05/29/19 08:43 100-44-72.6 1.2 1
Bromodichloromethane ND ug/m3 05/29/19 08:43 75-27-41.4 0.37 1
Bromoform ND ug/m3 05/29/19 08:43 75-25-25.2 1.4 1
Bromomethane ND ug/m3 05/29/19 08:43 74-83-90.79 0.23 1
1,3-Butadiene ND ug/m3 05/29/19 08:43 106-99-00.45 0.13 1
2-Butanone (MEK)ND ug/m3 05/29/19 08:43 78-93-33.0 0.37 1
Carbon disulfide ND ug/m3 05/29/19 08:43 75-15-00.63 0.22 1
Carbon tetrachloride ND ug/m3 05/29/19 08:43 56-23-51.3 0.43 1
Chlorobenzene ND ug/m3 05/29/19 08:43 108-90-70.94 0.28 1
Chloroethane ND ug/m3 05/29/19 08:43 75-00-30.54 0.26 1
Chloroform ND ug/m3 05/29/19 08:43 67-66-30.50 0.20 1
Chloromethane ND ug/m3 05/29/19 08:43 74-87-30.42 0.16 1
Cyclohexane ND ug/m3 05/29/19 08:43 110-82-71.8 0.35 1
Dibromochloromethane ND ug/m3 05/29/19 08:43 124-48-11.7 0.72 1
1,2-Dibromoethane (EDB)ND ug/m3 05/29/19 08:43 106-93-40.78 0.37 1
1,2-Dichlorobenzene ND ug/m3 05/29/19 08:43 95-50-11.2 0.50 1
1,3-Dichlorobenzene ND ug/m3 05/29/19 08:43 541-73-11.2 0.58 1
1,4-Dichlorobenzene ND ug/m3 05/29/19 08:43 106-46-73.1 1.0 1
Dichlorodifluoromethane ND ug/m3 05/29/19 08:43 75-71-81.0 0.29 1
1,1-Dichloroethane ND ug/m3 05/29/19 08:43 75-34-30.82 0.22 1
1,2-Dichloroethane ND ug/m3 05/29/19 08:43 107-06-20.41 0.15 1
1,1-Dichloroethene ND ug/m3 05/29/19 08:43 75-35-40.81 0.27 1
cis-1,2-Dichloroethene ND ug/m3 05/29/19 08:43 156-59-20.81 0.22 1
trans-1,2-Dichloroethene ND ug/m3 05/29/19 08:43 156-60-50.81 0.28 1
1,2-Dichloropropane ND ug/m3 05/29/19 08:43 78-87-50.94 0.23 1
cis-1,3-Dichloropropene ND ug/m3 05/29/19 08:43 10061-01-50.92 0.30 1
trans-1,3-Dichloropropene ND ug/m3 05/29/19 08:43 10061-02-60.92 0.44 1
Dichlorotetrafluoroethane ND ug/m3 05/29/19 08:43 76-14-21.4 0.44 1
Ethanol ND ug/m3 05/29/19 08:43 64-17-51.9 0.81 1
Ethyl acetate ND ug/m3 05/29/19 08:43 141-78-60.73 0.19 1
Ethylbenzene ND ug/m3 05/29/19 08:43 100-41-40.88 0.30 1
4-Ethyltoluene ND ug/m3 05/29/19 08:43 622-96-82.5 0.57 1
n-Heptane ND ug/m3 05/29/19 08:43 142-82-50.83 0.38 1
Hexachloro-1,3-butadiene ND ug/m3 05/29/19 08:43 87-68-35.4 2.0 1
n-Hexane ND ug/m3 05/29/19 08:43 110-54-30.72 0.31 1
2-Hexanone ND ug/m3 05/29/19 08:43 591-78-64.2 0.74 1
Methylene Chloride ND ug/m3 05/29/19 08:43 75-09-23.5 0.94 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 05/29/19 08:43 108-10-14.2 0.52 1
Methyl-tert-butyl ether ND ug/m3 05/29/19 08:43 1634-04-43.7 0.66 1
Naphthalene ND ug/m3 05/29/19 08:43 91-20-32.7 1.3 1
2-Propanol ND ug/m3 05/29/19 08:43 67-63-02.5 0.70 1
Propylene ND ug/m3 05/29/19 08:43 115-07-10.35 0.14 1
Styrene ND ug/m3 05/29/19 08:43 100-42-50.87 0.34 1
1,1,2,2-Tetrachloroethane ND ug/m3 05/29/19 08:43 79-34-50.70 0.29 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-4 #893 - Individual Cert. Lab ID: 92442461013 Collected: 08/21/19 14:07 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Tetrachloroethene ND ug/m3 05/29/19 08:43 127-18-40.69 0.31 1
Tetrahydrofuran ND ug/m3 05/29/19 08:43 109-99-90.60 0.26 1
Toluene ND ug/m3 05/29/19 08:43 108-88-30.77 0.35 1
1,2,4-Trichlorobenzene ND ug/m3 05/29/19 08:43 120-82-17.5 3.7 1
1,1,1-Trichloroethane ND ug/m3 05/29/19 08:43 71-55-61.1 0.31 1
1,1,2-Trichloroethane ND ug/m3 05/29/19 08:43 79-00-50.56 0.25 1
Trichloroethene ND ug/m3 05/29/19 08:43 79-01-60.55 0.26 1
Trichlorofluoromethane ND ug/m3 05/29/19 08:43 75-69-41.1 0.37 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 05/29/19 08:43 76-13-11.6 0.56 1
1,2,4-Trimethylbenzene ND ug/m3 05/29/19 08:43 95-63-61.0 0.45 1
1,3,5-Trimethylbenzene ND ug/m3 05/29/19 08:43 108-67-81.0 0.40 1
Vinyl acetate ND ug/m3 05/29/19 08:43 108-05-40.72 0.27 1
Vinyl chloride ND ug/m3 05/29/19 08:43 75-01-40.26 0.13 1
m&p-Xylene ND ug/m3 05/29/19 08:43 179601-23-11.8 0.70 1
o-Xylene ND ug/m3 05/29/19 08:43 95-47-60.88 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-5 #3277 - Individual
Cert.
Lab ID: 92442461014 Collected: 08/21/19 14:30 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Acetone ND ug/m3 07/03/19 11:05 67-64-12.4 1.2 1
Benzene ND ug/m3 07/03/19 11:05 71-43-20.32 0.15 1
Benzyl chloride ND ug/m3 07/03/19 11:05 100-44-72.6 1.2 1
Bromodichloromethane ND ug/m3 07/03/19 11:05 75-27-41.4 0.37 1
Bromoform ND ug/m3 07/03/19 11:05 75-25-25.2 1.4 1
Bromomethane ND ug/m3 07/03/19 11:05 74-83-90.79 0.23 1
1,3-Butadiene ND ug/m3 07/03/19 11:05 106-99-00.45 0.13 1
2-Butanone (MEK)ND ug/m3 07/03/19 11:05 78-93-33.0 0.37 1
Carbon disulfide ND ug/m3 07/03/19 11:05 75-15-00.63 0.22 1
Carbon tetrachloride ND ug/m3 07/03/19 11:05 56-23-51.3 0.43 1
Chlorobenzene ND ug/m3 07/03/19 11:05 108-90-70.94 0.28 1
Chloroethane ND ug/m3 07/03/19 11:05 75-00-30.54 0.26 1
Chloroform ND ug/m3 07/03/19 11:05 67-66-30.50 0.20 1
Chloromethane ND ug/m3 07/03/19 11:05 74-87-30.42 0.16 1
Cyclohexane ND ug/m3 07/03/19 11:05 110-82-71.8 0.35 1
Dibromochloromethane ND ug/m3 07/03/19 11:05 124-48-11.7 0.72 1
1,2-Dibromoethane (EDB)ND ug/m3 07/03/19 11:05 106-93-40.78 0.37 1
1,2-Dichlorobenzene ND ug/m3 07/03/19 11:05 95-50-11.2 0.50 1
1,3-Dichlorobenzene ND ug/m3 07/03/19 11:05 541-73-11.2 0.58 1
1,4-Dichlorobenzene ND ug/m3 07/03/19 11:05 106-46-73.1 1.0 1
Dichlorodifluoromethane ND ug/m3 07/03/19 11:05 75-71-81.0 0.29 1
1,1-Dichloroethane ND ug/m3 07/03/19 11:05 75-34-30.82 0.22 1
1,2-Dichloroethane ND ug/m3 07/03/19 11:05 107-06-20.41 0.15 1
1,1-Dichloroethene ND ug/m3 07/03/19 11:05 75-35-40.81 0.27 1
cis-1,2-Dichloroethene ND ug/m3 07/03/19 11:05 156-59-20.81 0.22 1
trans-1,2-Dichloroethene ND ug/m3 07/03/19 11:05 156-60-50.81 0.28 1
1,2-Dichloropropane ND ug/m3 07/03/19 11:05 78-87-50.94 0.23 1
cis-1,3-Dichloropropene ND ug/m3 07/03/19 11:05 10061-01-50.92 0.30 1
trans-1,3-Dichloropropene ND ug/m3 07/03/19 11:05 10061-02-60.92 0.44 1
Dichlorotetrafluoroethane ND ug/m3 07/03/19 11:05 76-14-21.4 0.44 1
Ethanol ND ug/m3 07/03/19 11:05 64-17-51.9 0.81 1
Ethyl acetate ND ug/m3 07/03/19 11:05 141-78-60.73 0.19 1
Ethylbenzene ND ug/m3 07/03/19 11:05 100-41-40.88 0.30 1
4-Ethyltoluene ND ug/m3 07/03/19 11:05 622-96-82.5 0.57 1
n-Heptane ND ug/m3 07/03/19 11:05 142-82-50.83 0.38 1
Hexachloro-1,3-butadiene ND ug/m3 07/03/19 11:05 87-68-35.4 2.0 1
n-Hexane ND ug/m3 07/03/19 11:05 110-54-30.72 0.31 1
2-Hexanone ND ug/m3 07/03/19 11:05 591-78-64.2 0.74 1
Methylene Chloride ND ug/m3 07/03/19 11:05 75-09-23.5 0.94 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/03/19 11:05 108-10-14.2 0.52 1
Methyl-tert-butyl ether ND ug/m3 07/03/19 11:05 1634-04-43.7 0.66 1
Naphthalene ND ug/m3 07/03/19 11:05 91-20-32.7 1.3 1
2-Propanol ND ug/m3 07/03/19 11:05 67-63-02.5 0.70 1
Propylene ND ug/m3 07/03/19 11:05 115-07-10.35 0.14 1
Styrene ND ug/m3 07/03/19 11:05 100-42-50.87 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 36 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-5 #3277 - Individual
Cert.
Lab ID: 92442461014 Collected: 08/21/19 14:30 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
1,1,2,2-Tetrachloroethane ND ug/m3 07/03/19 11:05 79-34-50.70 0.29 1
Tetrachloroethene ND ug/m3 07/03/19 11:05 127-18-40.69 0.31 1
Tetrahydrofuran ND ug/m3 07/03/19 11:05 109-99-90.60 0.26 1
Toluene ND ug/m3 07/03/19 11:05 108-88-30.77 0.35 1
1,2,4-Trichlorobenzene ND ug/m3 07/03/19 11:05 120-82-17.5 3.7 1
1,1,1-Trichloroethane ND ug/m3 07/03/19 11:05 71-55-61.1 0.31 1
1,1,2-Trichloroethane ND ug/m3 07/03/19 11:05 79-00-50.56 0.25 1
Trichloroethene ND ug/m3 07/03/19 11:05 79-01-60.55 0.26 1
Trichlorofluoromethane ND ug/m3 07/03/19 11:05 75-69-41.1 0.37 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/03/19 11:05 76-13-11.6 0.56 1
1,2,4-Trimethylbenzene ND ug/m3 07/03/19 11:05 95-63-61.0 0.45 1
1,3,5-Trimethylbenzene ND ug/m3 07/03/19 11:05 108-67-81.0 0.40 1
Vinyl acetate ND ug/m3 07/03/19 11:05 108-05-40.72 0.27 1
Vinyl chloride ND ug/m3 07/03/19 11:05 75-01-40.26 0.13 1
m&p-Xylene ND ug/m3 07/03/19 11:05 179601-23-11.8 0.70 1
o-Xylene ND ug/m3 07/03/19 11:05 95-47-60.88 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 37 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-6 #3025 - Individual
Cert.
Lab ID: 92442461015 Collected: 08/21/19 14:56 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Acetone ND ug/m3 07/25/19 09:58 67-64-12.4 1.2 1
Benzene ND ug/m3 07/25/19 09:58 71-43-20.32 0.15 1
Benzyl chloride ND ug/m3 07/25/19 09:58 100-44-72.6 1.2 1
Bromodichloromethane ND ug/m3 07/25/19 09:58 75-27-41.4 0.37 1
Bromoform ND ug/m3 07/25/19 09:58 75-25-25.2 1.4 1
Bromomethane ND ug/m3 07/25/19 09:58 74-83-90.79 0.23 1
1,3-Butadiene ND ug/m3 07/25/19 09:58 106-99-00.45 0.13 1
2-Butanone (MEK)ND ug/m3 07/25/19 09:58 78-93-33.0 0.37 1
Carbon disulfide ND ug/m3 07/25/19 09:58 75-15-00.63 0.22 1
Carbon tetrachloride ND ug/m3 07/25/19 09:58 56-23-51.3 0.43 1
Chlorobenzene ND ug/m3 07/25/19 09:58 108-90-70.94 0.28 1
Chloroethane ND ug/m3 07/25/19 09:58 75-00-30.54 0.26 1
Chloroform ND ug/m3 07/25/19 09:58 67-66-30.50 0.20 1
Chloromethane ND ug/m3 07/25/19 09:58 74-87-30.42 0.16 1
Cyclohexane ND ug/m3 07/25/19 09:58 110-82-71.8 0.35 1
Dibromochloromethane ND ug/m3 07/25/19 09:58 124-48-11.7 0.72 1
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 09:58 106-93-40.78 0.37 1
1,2-Dichlorobenzene ND ug/m3 07/25/19 09:58 95-50-11.2 0.50 1
1,3-Dichlorobenzene ND ug/m3 07/25/19 09:58 541-73-11.2 0.58 1
1,4-Dichlorobenzene ND ug/m3 07/25/19 09:58 106-46-73.1 1.0 1
Dichlorodifluoromethane ND ug/m3 07/25/19 09:58 75-71-81.0 0.29 1
1,1-Dichloroethane ND ug/m3 07/25/19 09:58 75-34-30.82 0.22 1
1,2-Dichloroethane ND ug/m3 07/25/19 09:58 107-06-20.41 0.15 1
1,1-Dichloroethene ND ug/m3 07/25/19 09:58 75-35-40.81 0.27 1
cis-1,2-Dichloroethene ND ug/m3 07/25/19 09:58 156-59-20.81 0.22 1
trans-1,2-Dichloroethene ND ug/m3 07/25/19 09:58 156-60-50.81 0.28 1
1,2-Dichloropropane ND ug/m3 07/25/19 09:58 78-87-50.94 0.23 1
cis-1,3-Dichloropropene ND ug/m3 07/25/19 09:58 10061-01-50.92 0.30 1
trans-1,3-Dichloropropene ND ug/m3 07/25/19 09:58 10061-02-60.92 0.44 1
Dichlorotetrafluoroethane ND ug/m3 07/25/19 09:58 76-14-21.4 0.44 1
Ethanol ND ug/m3 07/25/19 09:58 64-17-51.9 0.81 1
Ethyl acetate ND ug/m3 07/25/19 09:58 141-78-60.73 0.19 1
Ethylbenzene ND ug/m3 07/25/19 09:58 100-41-40.88 0.30 1
4-Ethyltoluene ND ug/m3 07/25/19 09:58 622-96-82.5 0.57 1
n-Heptane ND ug/m3 07/25/19 09:58 142-82-50.83 0.38 1
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 09:58 87-68-35.4 2.0 1
n-Hexane ND ug/m3 07/25/19 09:58 110-54-30.72 0.31 1
2-Hexanone ND ug/m3 07/25/19 09:58 591-78-64.2 0.74 1
Methylene Chloride ND ug/m3 07/25/19 09:58 75-09-23.5 0.94 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 09:58 108-10-14.2 0.52 1
Methyl-tert-butyl ether ND ug/m3 07/25/19 09:58 1634-04-43.7 0.66 1
Naphthalene ND ug/m3 07/25/19 09:58 91-20-32.7 1.3 1
2-Propanol 1.5J ug/m3 07/25/19 09:58 67-63-02.5 0.70 1
Propylene ND ug/m3 07/25/19 09:58 115-07-10.35 0.14 1
Styrene ND ug/m3 07/25/19 09:58 100-42-50.87 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-6 #3025 - Individual
Cert.
Lab ID: 92442461015 Collected: 08/21/19 14:56 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 09:58 79-34-50.70 0.29 1
Tetrachloroethene ND ug/m3 07/25/19 09:58 127-18-40.69 0.31 1
Tetrahydrofuran ND ug/m3 07/25/19 09:58 109-99-90.60 0.26 1
Toluene ND ug/m3 07/25/19 09:58 108-88-30.77 0.35 1
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 09:58 120-82-17.5 3.7 1
1,1,1-Trichloroethane ND ug/m3 07/25/19 09:58 71-55-61.1 0.31 1
1,1,2-Trichloroethane ND ug/m3 07/25/19 09:58 79-00-50.56 0.25 1
Trichloroethene ND ug/m3 07/25/19 09:58 79-01-60.55 0.26 1
Trichlorofluoromethane ND ug/m3 07/25/19 09:58 75-69-41.1 0.37 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 09:58 76-13-11.6 0.56 1
1,2,4-Trimethylbenzene ND ug/m3 07/25/19 09:58 95-63-61.0 0.45 1
1,3,5-Trimethylbenzene ND ug/m3 07/25/19 09:58 108-67-81.0 0.40 1
Vinyl acetate ND ug/m3 07/25/19 09:58 108-05-41.8 0.27 1
Vinyl chloride ND ug/m3 07/25/19 09:58 75-01-40.26 0.13 1
m&p-Xylene ND ug/m3 07/25/19 09:58 179601-23-11.8 0.70 1
o-Xylene ND ug/m3 07/25/19 09:58 95-47-60.88 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-7 #3035 - Individual
Cert.
Lab ID: 92442461016 Collected: 08/21/19 15:30 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Acetone ND ug/m3 06/04/19 08:31 67-64-12.4 1.2 1
Benzene ND ug/m3 06/04/19 08:31 71-43-20.32 0.15 1
Benzyl chloride ND ug/m3 06/04/19 08:31 100-44-72.6 1.2 1
Bromodichloromethane ND ug/m3 06/04/19 08:31 75-27-41.4 0.37 1
Bromoform ND ug/m3 06/04/19 08:31 75-25-25.2 1.4 1
Bromomethane ND ug/m3 06/04/19 08:31 74-83-90.79 0.23 1
1,3-Butadiene ND ug/m3 06/04/19 08:31 106-99-00.45 0.13 1
2-Butanone (MEK)ND ug/m3 06/04/19 08:31 78-93-33.0 0.37 1
Carbon disulfide ND ug/m3 06/04/19 08:31 75-15-00.63 0.22 1
Carbon tetrachloride ND ug/m3 06/04/19 08:31 56-23-51.3 0.43 1
Chlorobenzene ND ug/m3 06/04/19 08:31 108-90-70.94 0.28 1
Chloroethane ND ug/m3 06/04/19 08:31 75-00-30.54 0.26 1
Chloroform ND ug/m3 06/04/19 08:31 67-66-30.50 0.20 1
Chloromethane ND ug/m3 06/04/19 08:31 74-87-30.42 0.16 1
Cyclohexane ND ug/m3 06/04/19 08:31 110-82-71.8 0.35 1
Dibromochloromethane ND ug/m3 06/04/19 08:31 124-48-11.7 0.72 1
1,2-Dibromoethane (EDB)ND ug/m3 06/04/19 08:31 106-93-40.78 0.37 1
1,2-Dichlorobenzene ND ug/m3 06/04/19 08:31 95-50-11.2 0.50 1
1,3-Dichlorobenzene ND ug/m3 06/04/19 08:31 541-73-11.2 0.58 1
1,4-Dichlorobenzene ND ug/m3 06/04/19 08:31 106-46-73.1 1.0 1
Dichlorodifluoromethane ND ug/m3 06/04/19 08:31 75-71-81.0 0.29 1
1,1-Dichloroethane ND ug/m3 06/04/19 08:31 75-34-30.82 0.22 1
1,2-Dichloroethane ND ug/m3 06/04/19 08:31 107-06-20.41 0.15 1
1,1-Dichloroethene ND ug/m3 06/04/19 08:31 75-35-40.81 0.27 1
cis-1,2-Dichloroethene ND ug/m3 06/04/19 08:31 156-59-20.81 0.22 1
trans-1,2-Dichloroethene ND ug/m3 06/04/19 08:31 156-60-50.81 0.28 1
1,2-Dichloropropane ND ug/m3 06/04/19 08:31 78-87-50.94 0.23 1
cis-1,3-Dichloropropene ND ug/m3 06/04/19 08:31 10061-01-50.92 0.30 1
trans-1,3-Dichloropropene ND ug/m3 06/04/19 08:31 10061-02-60.92 0.44 1
Dichlorotetrafluoroethane ND ug/m3 06/04/19 08:31 76-14-21.4 0.44 1
Ethanol ND ug/m3 06/04/19 08:31 64-17-51.9 0.81 1
Ethyl acetate ND ug/m3 06/04/19 08:31 141-78-60.73 0.19 1
Ethylbenzene ND ug/m3 06/04/19 08:31 100-41-40.88 0.30 1
4-Ethyltoluene ND ug/m3 06/04/19 08:31 622-96-82.5 0.57 1
n-Heptane ND ug/m3 06/04/19 08:31 142-82-50.83 0.38 1
Hexachloro-1,3-butadiene ND ug/m3 06/04/19 08:31 87-68-35.4 2.0 1
n-Hexane ND ug/m3 06/04/19 08:31 110-54-30.72 0.31 1
2-Hexanone ND ug/m3 06/04/19 08:31 591-78-64.2 0.74 1
Methylene Chloride ND ug/m3 06/04/19 08:31 75-09-23.5 0.94 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 06/04/19 08:31 108-10-14.2 0.52 1
Methyl-tert-butyl ether ND ug/m3 06/04/19 08:31 1634-04-43.7 0.66 1
Naphthalene ND ug/m3 06/04/19 08:31 91-20-32.7 1.3 1
2-Propanol ND ug/m3 06/04/19 08:31 67-63-02.5 0.70 1
Propylene ND ug/m3 06/04/19 08:31 115-07-10.35 0.14 1
Styrene ND ug/m3 06/04/19 08:31 100-42-50.87 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-7 #3035 - Individual
Cert.
Lab ID: 92442461016 Collected: 08/21/19 15:30 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
1,1,2,2-Tetrachloroethane ND ug/m3 06/04/19 08:31 79-34-50.70 0.29 1
Tetrachloroethene ND ug/m3 06/04/19 08:31 127-18-40.69 0.31 1
Tetrahydrofuran ND ug/m3 06/04/19 08:31 109-99-90.60 0.26 1
Toluene ND ug/m3 06/04/19 08:31 108-88-30.77 0.35 1
1,2,4-Trichlorobenzene ND ug/m3 06/04/19 08:31 120-82-17.5 3.7 1
1,1,1-Trichloroethane ND ug/m3 06/04/19 08:31 71-55-61.1 0.31 1
1,1,2-Trichloroethane ND ug/m3 06/04/19 08:31 79-00-50.56 0.25 1
Trichloroethene ND ug/m3 06/04/19 08:31 79-01-60.55 0.26 1
Trichlorofluoromethane ND ug/m3 06/04/19 08:31 75-69-41.1 0.37 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 06/04/19 08:31 76-13-11.6 0.56 1
1,2,4-Trimethylbenzene ND ug/m3 06/04/19 08:31 95-63-61.0 0.45 1
1,3,5-Trimethylbenzene ND ug/m3 06/04/19 08:31 108-67-81.0 0.40 1
Vinyl acetate ND ug/m3 06/04/19 08:31 108-05-40.72 0.27 1
Vinyl chloride ND ug/m3 06/04/19 08:31 75-01-40.26 0.13 1
m&p-Xylene ND ug/m3 06/04/19 08:31 179601-23-11.8 0.70 1
o-Xylene ND ug/m3 06/04/19 08:31 95-47-60.88 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-8 #2401 - Individual
Cert.
Lab ID: 92442461017 Collected: 08/21/19 15:57 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Acetone ND ug/m3 07/25/19 09:15 67-64-12.4 1.2 1
Benzene ND ug/m3 07/25/19 09:15 71-43-20.32 0.15 1
Benzyl chloride ND ug/m3 07/25/19 09:15 100-44-72.6 1.2 1
Bromodichloromethane ND ug/m3 07/25/19 09:15 75-27-41.4 0.37 1
Bromoform ND ug/m3 07/25/19 09:15 75-25-25.2 1.4 1
Bromomethane ND ug/m3 07/25/19 09:15 74-83-90.79 0.23 1
1,3-Butadiene ND ug/m3 07/25/19 09:15 106-99-00.45 0.13 1
2-Butanone (MEK)ND ug/m3 07/25/19 09:15 78-93-33.0 0.37 1
Carbon disulfide ND ug/m3 07/25/19 09:15 75-15-00.63 0.22 1
Carbon tetrachloride ND ug/m3 07/25/19 09:15 56-23-51.3 0.43 1
Chlorobenzene ND ug/m3 07/25/19 09:15 108-90-70.94 0.28 1
Chloroethane ND ug/m3 07/25/19 09:15 75-00-30.54 0.26 1
Chloroform ND ug/m3 07/25/19 09:15 67-66-30.50 0.20 1
Chloromethane ND ug/m3 07/25/19 09:15 74-87-30.42 0.16 1
Cyclohexane ND ug/m3 07/25/19 09:15 110-82-71.8 0.35 1
Dibromochloromethane ND ug/m3 07/25/19 09:15 124-48-11.7 0.72 1
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 09:15 106-93-40.78 0.37 1
1,2-Dichlorobenzene ND ug/m3 07/25/19 09:15 95-50-11.2 0.50 1
1,3-Dichlorobenzene ND ug/m3 07/25/19 09:15 541-73-11.2 0.58 1
1,4-Dichlorobenzene ND ug/m3 07/25/19 09:15 106-46-73.1 1.0 1
Dichlorodifluoromethane ND ug/m3 07/25/19 09:15 75-71-81.0 0.29 1
1,1-Dichloroethane ND ug/m3 07/25/19 09:15 75-34-30.82 0.22 1
1,2-Dichloroethane ND ug/m3 07/25/19 09:15 107-06-20.41 0.15 1
1,1-Dichloroethene ND ug/m3 07/25/19 09:15 75-35-40.81 0.27 1
cis-1,2-Dichloroethene ND ug/m3 07/25/19 09:15 156-59-20.81 0.22 1
trans-1,2-Dichloroethene ND ug/m3 07/25/19 09:15 156-60-50.81 0.28 1
1,2-Dichloropropane ND ug/m3 07/25/19 09:15 78-87-50.94 0.23 1
cis-1,3-Dichloropropene ND ug/m3 07/25/19 09:15 10061-01-50.92 0.30 1
trans-1,3-Dichloropropene ND ug/m3 07/25/19 09:15 10061-02-60.92 0.44 1
Dichlorotetrafluoroethane ND ug/m3 07/25/19 09:15 76-14-21.4 0.44 1
Ethanol ND ug/m3 07/25/19 09:15 64-17-51.9 0.81 1
Ethyl acetate ND ug/m3 07/25/19 09:15 141-78-60.73 0.19 1
Ethylbenzene ND ug/m3 07/25/19 09:15 100-41-40.88 0.30 1
4-Ethyltoluene ND ug/m3 07/25/19 09:15 622-96-82.5 0.57 1
n-Heptane ND ug/m3 07/25/19 09:15 142-82-50.83 0.38 1
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 09:15 87-68-35.4 2.0 1
n-Hexane ND ug/m3 07/25/19 09:15 110-54-30.72 0.31 1
2-Hexanone ND ug/m3 07/25/19 09:15 591-78-64.2 0.74 1
Methylene Chloride ND ug/m3 07/25/19 09:15 75-09-23.5 0.94 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 09:15 108-10-14.2 0.52 1
Methyl-tert-butyl ether ND ug/m3 07/25/19 09:15 1634-04-43.7 0.66 1
Naphthalene ND ug/m3 07/25/19 09:15 91-20-32.7 1.3 1
2-Propanol ND ug/m3 07/25/19 09:15 67-63-02.5 0.70 1
Propylene ND ug/m3 07/25/19 09:15 115-07-10.35 0.14 1
Styrene ND ug/m3 07/25/19 09:15 100-42-50.87 0.34 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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Page 42 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: SG-8 #2401 - Individual
Cert.
Lab ID: 92442461017 Collected: 08/21/19 15:57 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 09:15 79-34-50.70 0.29 1
Tetrachloroethene ND ug/m3 07/25/19 09:15 127-18-40.69 0.31 1
Tetrahydrofuran ND ug/m3 07/25/19 09:15 109-99-90.60 0.26 1
Toluene ND ug/m3 07/25/19 09:15 108-88-30.77 0.35 1
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 09:15 120-82-17.5 3.7 1
1,1,1-Trichloroethane ND ug/m3 07/25/19 09:15 71-55-61.1 0.31 1
1,1,2-Trichloroethane ND ug/m3 07/25/19 09:15 79-00-50.56 0.25 1
Trichloroethene ND ug/m3 07/25/19 09:15 79-01-60.55 0.26 1
Trichlorofluoromethane ND ug/m3 07/25/19 09:15 75-69-41.1 0.37 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 09:15 76-13-11.6 0.56 1
1,2,4-Trimethylbenzene ND ug/m3 07/25/19 09:15 95-63-61.0 0.45 1
1,3,5-Trimethylbenzene ND ug/m3 07/25/19 09:15 108-67-81.0 0.40 1
Vinyl acetate ND ug/m3 07/25/19 09:15 108-05-40.72 0.27 1
Vinyl chloride ND ug/m3 07/25/19 09:15 75-01-40.26 0.13 1
m&p-Xylene ND ug/m3 07/25/19 09:15 179601-23-11.8 0.70 1
o-Xylene ND ug/m3 07/25/19 09:15 95-47-60.88 0.34 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: DUP 1 #3252 - Individual
Cert.
Lab ID: 92442461018 Collected: 08/21/19 00:00 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
Acetone ND ug/m3 07/27/19 07:41 67-64-12.4 1.2 1
Benzene ND ug/m3 07/27/19 07:41 71-43-20.32 0.15 1
Benzyl chloride ND ug/m3 07/27/19 07:41 100-44-72.6 1.2 1
Bromodichloromethane ND ug/m3 07/27/19 07:41 75-27-41.4 0.37 1
Bromoform ND ug/m3 07/27/19 07:41 75-25-25.2 1.4 1
Bromomethane ND ug/m3 07/27/19 07:41 74-83-90.79 0.23 1
1,3-Butadiene ND ug/m3 07/27/19 07:41 106-99-00.45 0.13 1
2-Butanone (MEK)ND ug/m3 07/27/19 07:41 78-93-33.0 0.37 1
Carbon disulfide ND ug/m3 07/27/19 07:41 75-15-00.63 0.22 1
Carbon tetrachloride ND ug/m3 07/27/19 07:41 56-23-51.3 0.43 1
Chlorobenzene ND ug/m3 07/27/19 07:41 108-90-70.94 0.28 1
Chloroethane ND ug/m3 07/27/19 07:41 75-00-30.54 0.26 1
Chloroform ND ug/m3 07/27/19 07:41 67-66-30.50 0.20 1
Chloromethane ND ug/m3 07/27/19 07:41 74-87-30.42 0.16 1
Cyclohexane ND ug/m3 07/27/19 07:41 110-82-71.8 0.35 1
Dibromochloromethane ND ug/m3 07/27/19 07:41 124-48-11.7 0.72 1
1,2-Dibromoethane (EDB)ND ug/m3 07/27/19 07:41 106-93-40.78 0.37 1
1,2-Dichlorobenzene ND ug/m3 07/27/19 07:41 95-50-11.2 0.50 1
1,3-Dichlorobenzene ND ug/m3 07/27/19 07:41 541-73-11.2 0.58 1
1,4-Dichlorobenzene ND ug/m3 07/27/19 07:41 106-46-73.1 1.0 1
Dichlorodifluoromethane ND ug/m3 07/27/19 07:41 75-71-81.0 0.29 1
1,1-Dichloroethane ND ug/m3 07/27/19 07:41 75-34-30.82 0.22 1
1,2-Dichloroethane ND ug/m3 07/27/19 07:41 107-06-20.41 0.15 1
1,1-Dichloroethene ND ug/m3 07/27/19 07:41 75-35-40.81 0.27 1
cis-1,2-Dichloroethene ND ug/m3 07/27/19 07:41 156-59-20.81 0.22 1
trans-1,2-Dichloroethene ND ug/m3 07/27/19 07:41 156-60-50.81 0.28 1
1,2-Dichloropropane ND ug/m3 07/27/19 07:41 78-87-50.94 0.23 1
cis-1,3-Dichloropropene ND ug/m3 07/27/19 07:41 10061-01-50.92 0.30 1
trans-1,3-Dichloropropene ND ug/m3 07/27/19 07:41 10061-02-60.92 0.44 1
Dichlorotetrafluoroethane ND ug/m3 07/27/19 07:41 76-14-21.4 0.44 1
Ethanol ND ug/m3 07/27/19 07:41 64-17-51.9 0.81 1
Ethyl acetate ND ug/m3 07/27/19 07:41 141-78-60.73 0.19 1
Ethylbenzene ND ug/m3 07/27/19 07:41 100-41-40.88 0.30 1
4-Ethyltoluene ND ug/m3 07/27/19 07:41 622-96-82.5 0.57 1
n-Heptane ND ug/m3 07/27/19 07:41 142-82-50.83 0.38 1
Hexachloro-1,3-butadiene ND ug/m3 07/27/19 07:41 87-68-35.4 2.0 1
n-Hexane ND ug/m3 07/27/19 07:41 110-54-30.72 0.31 1
2-Hexanone ND ug/m3 07/27/19 07:41 591-78-64.2 0.74 1
Methylene Chloride ND ug/m3 07/27/19 07:41 75-09-23.5 0.94 1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/27/19 07:41 108-10-14.2 0.52 1
Methyl-tert-butyl ether ND ug/m3 07/27/19 07:41 1634-04-43.7 0.66 1
Naphthalene ND ug/m3 07/27/19 07:41 91-20-32.7 1.3 1
2-Propanol ND ug/m3 07/27/19 07:41 67-63-02.5 0.70 1
Propylene ND ug/m3 07/27/19 07:41 115-07-10.35 0.14 1
Styrene ND ug/m3 07/27/19 07:41 100-42-50.87 0.34 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Sample: DUP 1 #3252 - Individual
Cert.
Lab ID: 92442461018 Collected: 08/21/19 00:00 Received: 08/22/19 11:23 Matrix: Air
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: TO-15Individual Can Certification
1,1,2,2-Tetrachloroethane ND ug/m3 07/27/19 07:41 79-34-50.70 0.29 1
Tetrachloroethene ND ug/m3 07/27/19 07:41 127-18-40.69 0.31 1
Tetrahydrofuran ND ug/m3 07/27/19 07:41 109-99-90.60 0.26 1
Toluene ND ug/m3 07/27/19 07:41 108-88-30.77 0.35 1
1,2,4-Trichlorobenzene ND ug/m3 07/27/19 07:41 120-82-17.5 3.7 1
1,1,1-Trichloroethane ND ug/m3 07/27/19 07:41 71-55-61.1 0.31 1
1,1,2-Trichloroethane ND ug/m3 07/27/19 07:41 79-00-50.56 0.25 1
Trichloroethene ND ug/m3 07/27/19 07:41 79-01-60.55 0.26 1
Trichlorofluoromethane ND ug/m3 07/27/19 07:41 75-69-41.1 0.37 1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/27/19 07:41 76-13-11.6 0.56 1
1,2,4-Trimethylbenzene ND ug/m3 07/27/19 07:41 95-63-61.0 0.45 1
1,3,5-Trimethylbenzene ND ug/m3 07/27/19 07:41 108-67-81.0 0.40 1
Vinyl acetate ND ug/m3 07/27/19 07:41 108-05-40.72 0.27 1
Vinyl chloride ND ug/m3 07/27/19 07:41 75-01-40.26 0.13 1
m&p-Xylene ND ug/m3 07/27/19 07:41 179601-23-11.8 0.70 1
o-Xylene ND ug/m3 07/27/19 07:41 95-47-60.88 0.34 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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[phone]
Page 45 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628281
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92442461001, 92442461002, 92442461003, 92442461004, 92442461005, 92442461006, 92442461007,
92442461008, 92442461009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3390147
Associated Lab Samples: 92442461001, 92442461002, 92442461003, 92442461004, 92442461005, 92442461006, 92442461007,
92442461008, 92442461009
Matrix: Air
AnalyzedMDL
1,1,1-Trichloroethane ug/m3 ND 1.1 08/24/19 11:590.31
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 08/24/19 11:590.29
1,1,2-Trichloroethane ug/m3 ND 0.56 08/24/19 11:590.25
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 08/24/19 11:590.56
1,1-Dichloroethane ug/m3 ND 0.82 08/24/19 11:590.22
1,1-Dichloroethene ug/m3 ND 0.81 08/24/19 11:590.27
1,2,4-Trichlorobenzene ug/m3 ND 7.5 08/24/19 11:593.7
1,2,4-Trimethylbenzene ug/m3 ND 1.0 08/24/19 11:590.45
1,2-Dibromoethane (EDB)ug/m3 ND 1.6 MN08/24/19 11:590.37
1,2-Dichlorobenzene ug/m3 ND 1.2 08/24/19 11:590.50
1,2-Dichloroethane ug/m3 ND 0.41 08/24/19 11:590.15
1,2-Dichloropropane ug/m3 ND 0.94 08/24/19 11:590.23
1,3,5-Trimethylbenzene ug/m3 ND 1.0 08/24/19 11:590.40
1,3-Butadiene ug/m3 ND 0.45 08/24/19 11:590.13
1,3-Dichlorobenzene ug/m3 ND 1.2 08/24/19 11:590.58
1,4-Dichlorobenzene ug/m3 ND 3.1 08/24/19 11:591.0
2-Butanone (MEK)ug/m3 ND 3.0 08/24/19 11:590.37
2-Hexanone ug/m3 ND 4.2 08/24/19 11:590.74
4-Ethyltoluene ug/m3 ND 2.5 08/24/19 11:590.57
4-Methyl-2-pentanone (MIBK)ug/m3 ND 4.2 08/24/19 11:590.52
Acetone ug/m3 ND 2.4 08/24/19 11:591.2
Benzene ug/m3 ND 0.32 08/24/19 11:590.15
Bromodichloromethane ug/m3 ND 1.4 08/24/19 11:590.37
Bromoform ug/m3 ND 5.2 08/24/19 11:591.4
Bromomethane ug/m3 ND 0.79 08/24/19 11:590.23
Carbon disulfide ug/m3 ND 0.63 08/24/19 11:590.22
Carbon tetrachloride ug/m3 ND 1.3 08/24/19 11:590.43
Chlorobenzene ug/m3 ND 0.94 08/24/19 11:590.28
Chloroethane ug/m3 ND 0.54 08/24/19 11:590.26
Chloroform ug/m3 ND 0.50 08/24/19 11:590.20
Chloromethane ug/m3 ND 0.42 08/24/19 11:590.16
cis-1,2-Dichloroethene ug/m3 ND 0.81 08/24/19 11:590.22
cis-1,3-Dichloropropene ug/m3 ND 0.92 08/24/19 11:590.30
Cyclohexane ug/m3 ND 1.8 08/24/19 11:590.35
Dibromochloromethane ug/m3 ND 1.7 08/24/19 11:590.72
Dichlorodifluoromethane ug/m3 ND 1.0 08/24/19 11:590.29
Dichlorotetrafluoroethane ug/m3 ND 1.4 08/24/19 11:590.44
Ethyl acetate ug/m3 ND 0.73 08/24/19 11:590.19
Ethylbenzene ug/m3 ND 0.88 08/24/19 11:590.30
Hexachloro-1,3-butadiene ug/m3 ND 5.4 08/24/19 11:592.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3390147
Associated Lab Samples: 92442461001, 92442461002, 92442461003, 92442461004, 92442461005, 92442461006, 92442461007,
92442461008, 92442461009
Matrix: Air
AnalyzedMDL
m&p-Xylene ug/m3 ND 1.8 08/24/19 11:590.70
Methyl-tert-butyl ether ug/m3 ND 3.7 08/24/19 11:590.66
Methylene Chloride ug/m3 ND 3.5 08/24/19 11:590.94
n-Heptane ug/m3 ND 0.83 08/24/19 11:590.38
n-Hexane ug/m3 ND 0.72 08/24/19 11:590.31
Naphthalene ug/m3 ND 2.7 08/24/19 11:591.3
o-Xylene ug/m3 ND 0.88 08/24/19 11:590.34
Propylene ug/m3 ND 0.35 08/24/19 11:590.14
Styrene ug/m3 ND 0.87 08/24/19 11:590.34
Tetrachloroethene ug/m3 ND 1.4 MN08/24/19 11:590.31
Tetrahydrofuran ug/m3 ND 0.60 08/24/19 11:590.26
Toluene ug/m3 ND 0.77 08/24/19 11:590.35
trans-1,2-Dichloroethene ug/m3 ND 0.81 08/24/19 11:590.28
trans-1,3-Dichloropropene ug/m3 ND 0.92 08/24/19 11:590.44
Trichloroethene ug/m3 ND 0.55 08/24/19 11:590.26
Trichlorofluoromethane ug/m3 ND 1.1 08/24/19 11:590.37
Vinyl acetate ug/m3 ND 0.72 08/24/19 11:590.27
Vinyl chloride ug/m3 ND 0.26 08/24/19 11:590.13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3390148LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 56.255.5 101 70-130
1,1,2,2-Tetrachloroethane ug/m3 83.969.8 120 70-132
1,1,2-Trichloroethane ug/m3 58.855.5 106 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 82.677.9 106 70-130
1,1-Dichloroethane ug/m3 45.541.1 111 70-130
1,1-Dichloroethene ug/m3 43.540.3 108 70-130
1,2,4-Trichlorobenzene ug/m3 72.875.4 96 56-130
1,2,4-Trimethylbenzene ug/m3 54.850 110 70-134
1,2-Dibromoethane (EDB)ug/m3 80.478.1 103 70-130
1,2-Dichlorobenzene ug/m3 63.661.1 104 70-132
1,2-Dichloroethane ug/m3 47.541.1 115 70-130
1,2-Dichloropropane ug/m3 53.747 114 70-130
1,3,5-Trimethylbenzene ug/m3 55.250 110 70-132
1,3-Butadiene ug/m3 25.822.5 115 65-130
1,3-Dichlorobenzene ug/m3 63.461.1 104 70-137
1,4-Dichlorobenzene ug/m3 63.461.1 104 70-134
2-Butanone (MEK)ug/m3 37.330 124 70-130
2-Hexanone ug/m3 49.341.6 118 70-135
4-Ethyltoluene ug/m3 57.050 114 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 51.541.6 124 70-131
Acetone ug/m3 124121 102 67-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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[phone]
Page 47 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3390148LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/m3 37.832.5 116 70-130
Bromodichloromethane ug/m3 73.168.1 107 70-130
Bromoform ug/m3 97.5105 93 70-132
Bromomethane ug/m3 40.039.5 101 69-130
Carbon disulfide ug/m3 34.531.6 109 56-137
Carbon tetrachloride ug/m3 65.364 102 66-131
Chlorobenzene ug/m3 47.946.8 102 70-130
Chloroethane ug/m3 30.526.8 114 70-130
Chloroform ug/m3 57.349.6 115 70-130
Chloromethane ug/m3 23.421 111 66-130
cis-1,2-Dichloroethene ug/m3 41.440.3 103 70-130
cis-1,3-Dichloropropene ug/m3 50.146.1 109 70-133
Cyclohexane ug/m3 38.535 110 68-132
Dibromochloromethane ug/m3 89.686.6 104 70-130
Dichlorodifluoromethane ug/m3 49.850.3 99 70-130
Dichlorotetrafluoroethane ug/m3 74.971 105 70-130
Ethyl acetate ug/m3 40.836.6 111 69-130
Ethylbenzene ug/m3 48.644.1 110 67-131
Hexachloro-1,3-butadiene ug/m3 98.7108 91 66-137
m&p-Xylene ug/m3 95.288.3 108 70-132
Methyl-tert-butyl ether ug/m3 39.536.6 108 70-130
Methylene Chloride ug/m3 218177 123 65-130
n-Heptane ug/m3 46.841.7 112 65-130
n-Hexane ug/m3 44.835.8 125 66-130
Naphthalene ug/m3 54.553.3 102 56-130
o-Xylene ug/m3 48.044.1 109 70-130
Propylene ug/m3 19.417.5 111 67-130
Styrene ug/m3 48.643.3 112 69-136
Tetrachloroethene ug/m3 69.068.9 100 70-130
Tetrahydrofuran ug/m3 35.730 119 68-131
Toluene ug/m3 39.038.3 102 70-130
trans-1,2-Dichloroethene ug/m3 42.640.3 106 70-130
trans-1,3-Dichloropropene ug/m3 48.246.1 105 70-134
Trichloroethene ug/m3 53.354.6 98 70-130
Trichlorofluoromethane ug/m3 57.057.1 100 65-130
Vinyl acetate ug/m3 41.235.8 115 61-133
Vinyl chloride ug/m3 28.626 110 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
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[phone]
Page 48 of 51
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
The reporting limit has been raised in accordance with Minnesota Statutes 4740.2100 Subpart 8. C, D. Reporting Limit
Evaluation Rule.MN
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 51
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92442461
COREY'S TRANSMISSION
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92442461001 628281SG-1 #2591 TO-15
92442461002 628281SG-2 #3250 TO-15
92442461003 628281SG-3 #2791 TO-15
92442461004 628281SG-4 #893 TO-15
92442461005 628281SG-5 #3277 TO-15
92442461006 628281SG-6 #3025 TO-15
92442461007 628281SG-7 #3035 TO-15
92442461008 628281SG-8 #2401 TO-15
92442461009 628281DUP 1 #3252 TO-15
92442461010 628615SG-1 #2591 - Individual Cert.TO-15
92442461011 628615SG-2 #3250 - Individual Cert.TO-15
92442461012 628615SG-3 #2791 - Individual Cert.TO-15
92442461013 628615SG-4 #893 - Individual Cert.TO-15
92442461014 628615SG-5 #3277 - Individual Cert.TO-15
92442461015 628615SG-6 #3025 - Individual Cert.TO-15
92442461016 628615SG-7 #3035 - Individual Cert.TO-15
92442461017 628615SG-8 #2401 - Individual Cert.TO-15
92442461018 628615DUP 1 #3252 - Individual Cert.TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 11:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 51
Page 51 of 51
#=CL#
August 27, 2019
LIMS USE: FR - JOE NESTOR
LIMS OBJECT ID: 92442890
92442890
Project:
Pace Project No.:
RE:
Joe Nestor
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
COREY'S TRANSMISSION
Dear Joe Nestor:
Enclosed are the analytical results for sample(s) received by the laboratory on August 26, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 11
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92442890
COREY'S TRANSMISSION
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 11
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92442890
COREY'S TRANSMISSION
Lab ID Sample ID Matrix Date Collected Date Received
92442890001 MW-5 Water 08/26/19 13:50 08/26/19 15:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 11
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92442890
COREY'S TRANSMISSION
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92442890001 MW-5 EPA 7470A 1 PASI-AJMW1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 11
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92442890
COREY'S TRANSMISSION
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92442890001 MW-5
Mercury 0.70 ug/L 08/27/19 14:300.20EPA 7470A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92442890
COREY'S TRANSMISSION
Sample: MW-5 Lab ID: 92442890001 Collected: 08/26/19 13:50 Received: 08/26/19 15:27 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury 0.70 ug/L 08/27/19 14:30 7439-97-608/27/19 10:450.20 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 03:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92442890
COREY'S TRANSMISSION
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
494614
EPA 7470A
EPA 7470A
7470 Mercury
Associated Lab Samples: 92442890001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2665221
Associated Lab Samples:92442890001
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 08/27/19 14:250.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2665222LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2665223MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92442890001
2665224
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 81 75-12582 1 252.50.70 2.7 2.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 03:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 11
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92442890
COREY'S TRANSMISSION
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 03:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 11
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92442890
COREY'S TRANSMISSION
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92442890001 494614 494678MW-5 EPA 7470A EPA 7470A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/27/2019 03:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 11
Page 10 of 11
Page 11 of 11
Fax:[phone]
Phone:[phone]
8/26/2019Attn:ECS Southeast, LLP - Charlotte
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
The samples associated with this report were received in good condition unless otherwise noted. This report relates only to those items tested as received by
the laboratory. The QC data associated with the sample results meet the recovery and precision requirements, unless specifically indicated. The final results are not field blank corrected. The laboratory is not responsible for final results calculated using air volumes that have been provided by non-laboratory
personnel. This report may not be reproduced except in full and without written approval by EMSL Analytical, Inc.
Lee Plumley, Laboratory Manager
Approved By:
The following analytical report covers the analysis performed on samples submitted to EMSL
Analytical, Inc. on 8/26/2019. The results are tabulated on the attached data pages for the following client designated project:
8458-B
The reference number for these samples is EMSL Order #411908463. Please use this
reference when calling about these samples. If you have any questions, please do not hesitate to contact me at [phone].
EMSL Analytical, Inc.
10801 Southern Loop Blvd, Pineville, NC 28134
Phone: [phone] Fax: [phone] Email: [e-mail]
Page 1 of 2
EMSL Analytical, Inc.
10801 Southern Loop Blvd, Pineville, NC 28134
Phone/Fax:[phone]
http://www.EMSL.com [e-mail]
411908463
CustomerID:ENCS55
CustomerPO:
ProjectID:
EMSL Order:
Analytical Results
Attn:ECS Southeast, LLP - Charlotte
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
Received: 08/26/19 12:20 PM
8458-B
Fax:[phone]
Phone:[phone]
Project:
8/26/2019Collected:
Client Sample Description Lab ID:(1) 7971702411 411908463-0001
Immediatelty adjacent to MW-5
Collected:8/26/2019
Method Parameter Result Units
Analysis
Date & AnalystRL
Prep
Date & Analyst
METALS
NIOSH 6009 Mercury KCNDmg/m³8/26/20190.00033 8/26/2019 KC
Client Sample Description Lab ID:(FB) 7971702414 411908463-0002
Blank
Collected:8/26/2019
Method Parameter Result Units
Analysis
Date & AnalystRL
Prep
Date & Analyst
METALS
NIOSH 6009 Mercury KCNDµg/tube 8/26/20190.010 8/26/2019 KC
MDL - method detection limitJ - Result was below the reporting limit, but at or above the MDLND - indicates that the analyte was not detected at the reporting limit
RL - Reporting Limit (Analytical)D - Dilution
Definitions:
Page 2 of 2ChemSmplw/RDL/NELAC-2.4.0.0 Printed: 8/26/2019 4:16:54 PM
OrderID: 411908463
Page 1 Of 1
APPENDIX G
APPENDIX H
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Rev. 09/2015 Page 1 of 3
Site:Corey Transmission
Address:511 and 527 West Tremont Ave
City:Charlotte
County:Mecklenburg
Brownfields Project Number:23018-19-060
Property and Building Characteristics
a. Provide occupancy and use information.
The subject proeprty is occupied by Corey Transmission Service Inc., an automotive repair facility. The
proeprty is devloped with an approximate 17,500-square foot building and an approximate 3,600-square
foot building.
The buildings are one-story and are made of modular metal with metal framing. Several metal garage bay
doors are located on the buildings.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
The foundation is a concrete slab.
The building uses forced air that is not ducted.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
No subslab ventilation systems in place. It is not known if moisture barriers are in place.
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets
as needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may be
needed.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings
(e.g. windows, bay doors), and height (number of stories).
% of property that is covered by buildings
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the
information requested below. Distances are measured from the site property boundary unless otherwise indicated
by the DEQ Brownfield’s Project Manager (PM).
Current Usage Proposed UsageSurface Conditions
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved NA
NA~ 9
NA
NA
NA
NA
Size of Property (acres)
% of property that is wooded/brush
~ 5.58
~ 5
~ 71
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air
return, and design considerations (e.g. positive pressure?).
0
~ 15
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Rev. 09/2015 Page 2 of 3
Surrounding Property Land Use
North
South
East
West
N
Y 45 N, W & S
Y 500-670 N
Utilities
Is there a septic system on-site? (Y or N) ________N
Please provide the utility providers for the subject property
a. Natural Gas ___Piedmont Natural Gas
b. Sewer ___CMUD
c. Electricity ___Duke Energy
d. Other ___CMUD Stormwater
For surrounding properties, please complete the following table with available information.
Y 5 N
Y 10 N
N
Y 10 N
Y 10 N
Y 10 N
N
utilities included sanitary sewer, potable water, natural gas, telephone, and electric.
Same
Same
Same
Is there a basement within 1,000 ft of the Property?
Gas and sanitary sewer lines run along north side of Tremont
Avenue
Duke Energy Electric lines are overhead lines.
CMUD Stormwater lines run through site (See Figures).
Is there a residence within 1,000 ft of the Property?
Utility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
See Figures
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with
the subject property. A map showing stormwater structures is attached. ECS Southeast, LLP observed evidence of underground
utilities running in a West-East direction along West Tremont Avenue. Underground
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Residences
Gas-Fired Products Inc. and Inner Peaks Climbing
Residences
For the subject property, please provide a map of known buried utilites. If available, include depth to top,
construction material, and diameter of the utilities. In addition, please provide the following information on utilty
providers. If additional assessment is required, the public utility locators should be contacted. This information can
then be added to a site map.
Y/N *
Is a school or daycare center within 1,000 ft of the Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific
addresses.
Distance
(ft)
DirectionDistance
(ft)Address
Same
Please provide information on the following land uses in the vicinity of the subject site, including a map of the
surrounding areas. If specific receptors are present, please provide addresses of the facilities.
West Tremont Ave followed by vacant land
Zoning/Land Use Proposed Usage Current Use/Occupant
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Rev. 09/2015 Page 3 of 3
Water Supply
What is the potable water supply for the property? Public blic X
N
N
N
Surface Water & Wetlands
NA
Tributary of Irwin Creek approximately 730 feet south
No/No
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Are there any wetlands present on the property?
If no wetlands on-site, are wetlands suspected
on adjoining properties?
NA
NA
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property
b d ?Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the
vicinity of the Property.
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public,
please include the water providers name.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
a. Is the water body naturally developed or
man-made?NA
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a
minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if
water supply or irrigation wells may be present. Information from applicable databases can and should be utilized;
however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested
radius, please provide a map of the well locations. If needed, please attach a separate table to list all wells. Please
note, the PM may opt for a more extensive water supply well survey if needed.
Are there surface water features on the
property? (If yes, please complete a. to d.)
Provide Information regarding Surface Water
and Wetlands
Distance
(ft)Direction Address
No
FIGURE 1SITE TOPOGRAPHIC MAP
511 and 527 West Tremont AvenueCharlotte, Mecklenburg County, North Carolina
ECS Project Number 49:8458-A
SOURCE:USGS Topographic MapCharlotte East & West North Carolina Quadrangle2016
Scale
1-inch = 2,000 feet
SITE
1’2,000’1,000’
FIGURE 2RESIDENTIAL PROPERTYMAP
511 and 527 West Tremont AvenueCharlotte, Mecklenburg County, North Carolina
ECS Project Number 49:8458-A
SOURCE:
MECKLENBURG COUNTY GEOGRAPHIC
INFORMATION SYSTEM
AUGUST 29, 2019
SCALE AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
AREAS WITH MULTIPLE RESIDENTIAL STRUCTURES
1,500-FOOT BUFFER AROUND SUBJECT PROPERTY
BROOKHILL VILLAGE TWO
INDIVIDUAL SINGLE-FAMILY RESIDENCES
FIGURE 3STORMWATER UTILITY MAP
511 and 527 West Tremont AvenueCharlotte, Mecklenburg County, North Carolina
ECS Project Number 49:8458-A
SOURCE:
VIRTUAL CHARLOTTE WEBPAGE, AUGUST 30, 2019
(http://vc.charmeck.org/)
SCALE:
NOT INDICATED
APPROXIMATE SITE BOUNDARY
LEGEND
DROP INLET
UNDERGROUND STORMWATER PIPE
STORM CHANNEL