22026_JimGriffin_RedevelopmentSummaryReport_2020.01.30

Via E-Mail
January 30, 2020
North Carolina Department of Environmental Quality Division of Waste Management – Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646 Attn: Ms. Joselyn Harriger, PG
Re: Redevelopment Summary Report
Jim Griffin 1120 S. Mint Street Charlotte, North Carolina Brownfields Project No. 22026-18-060
H&H Job No. BOU-010

Dear Ms. Harriger:
1.0 Introduction

On behalf of Boulevard at South Mint, LLC (the Prospective Developer or PD), Hart &
Hickman, PC (H&H) is providing this Redevelopment Summary Report for the Jim Griffin
Roofing Brownfields property (Brownfields Project No. 22026-18-060) located at 1120 South
Mint Street in Charlotte, Mecklenburg County, North Carolina (Site). The Site consists of three
contiguous parcels (Parcel Identification Nos. 07326706, 07326715, and 07326717) totaling
approximately one acre of land located in a commercial and light industrial area of South End
Charlotte. A Site location map is included as Figure 1.

Redevelopment activities completed in 2019 included razing the existing 2,400 square foot (sq
ft) and 3,600 sq ft warehouse buildings, installation of erosion control measures, and initial
grading activities to level the Site for construction of residential townhome buildings.
Redevelopment activities at the Site are being conducted in accordance with the North Carolina
Ms. Joselyn Harriger, PG January 30, 2020
Page 2
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-010 Jim Griffin Brownfields\Redevelopment Report\Final To DEQ\Redevelopment Summary Report_Jim Griffin (BPN 22026-18-060)_20200130.doc
Department of Environmental Quality (DEQ) approved Environmental Management Plan (EMP)
dated November 12, 2019. A rendering of the Site redevelopment is provided in Figure 2.

A Brownfields Agreement between the PD and the DEQ was recorded on May 30, 2019. Land
Use Restriction (LUR) k. of the recorded Brownfields Agreement generally states that a report
documenting environment-related activities occurring at the Site will be submitted in January of
each year for as long as redevelopment activities are ongoing beginning in the January following
the one-year anniversary of the effective date of the Brownfields Agreement. Although it has not
yet been one year since recordation of the Brownfields Agreement, this report has been prepared
to provide a brief summary of the initial redevelopment activities that occurred at the Site in late
2019. In addition, this report has been prepared to document permanent closure of the 4,000-
gallon underground storage tank (UST). Brief summaries of environment-related activities
associated with redevelopment of the Site and closure of the UST are provided in the following
sections.

2.0 Environmental-Related Redevelopment Activities
Previous operations at the Site included use of a 4,000-gallon gasoline UST for refueling fleet
roofing vehicles. The UST was registered with the DEQ UST Section (Facility ID No. 00-0-
0000026067). In accordance with the DEQ-approved EMP, H&H provided oversight during
closure activities associated with the 4,000-gallon gasoline UST on December 16 and 17, 2019.
UST closure and closure soil sampling activities were conducted in accordance with DEQ UST
Section guidelines. A UST Closure Report prepared by H&H and dated January 30, 2020 was
submitted to the DEQ UST Section to document permanent closure of the tank. Details
associated with the UST closure and soil sampling activities are provided in the following
sections.
Ms. Joselyn Harriger, PG January 30, 2020
Page 3
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-010 Jim Griffin Brownfields\Redevelopment Report\Final To DEQ\Redevelopment Summary Report_Jim Griffin (BPN 22026-18-060)_20200130.doc
2.1 UST Closure Activities

Prior to UST closure activities, H&H submitted a Notice of Intent for Permanent Closure or
Change-in-Service (UST-3) Form to the DEQ UST Section. In addition, a Tank Removal and
Safeguarding Permit was obtained from the City of Charlotte Fire Department Fire Prevention
Bureau. Following the removal of the UST, H&H submitted a Site Investigation Report for
Permanent Closure or Change-in-Service of Registered UST (UST-2A) Form. The UST-3 Form,
UST-2A Form, and tank safeguarding permit are provided in Appendix A.

On December 16, 2019, the PD contracted with RCI Demolition (RCI) to remove the 4,000-
gallon gasoline UST system including product piping and a gasoline dispenser. H&H confirmed
that there was no residual gasoline present in the tank, product piping, or dispenser. Following
inspection for the presence of residual fluids, the tank was inerted with dry-ice to purge potential
explosive vapors from the tank. A lower explosion level (LEL) meter was utilized to monitor for
explosive atmospheres in the tank during the purging process. Tank purging continued until
readings within the tank were less than 10% of the LEL. H&H personnel measured the final
LEL reading at approximately 5%.

Once the tank had been adequately purged, overburden soil was removed with an excavator and
stockpiled on plastic sheeting adjacent to the excavation. During removal, the overburden soil
was screened for the presence of impacts using sensory methods (i.e., visual and olfactory
evaluation) as well as for the presence of organic vapors using a photoionization detector (PID).
During the excavation, the overburden soil was determined to be minimally impacted using
sensory methods including PID readings. In accordance with the DEQ-approved EMP, soil
excavated from the UST basin was used as backfill material in the UST basin following removal
of the tank.

Following the removal of overburden soil, the tank was then removed from the UST basin using
an excavator. The tank dimensions were 16 feet (ft) in length and 7 ft in diameter and it was
confirmed that the size of the tank was 4,000-gallons. The tank construction was steel with an
Ms. Joselyn Harriger, PG January 30, 2020
Page 4
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-010 Jim Griffin Brownfields\Redevelopment Report\Final To DEQ\Redevelopment Summary Report_Jim Griffin (BPN 22026-18-060)_20200130.doc
exterior fiberglass coating. Following removal, the tank was inspected and there were no visible
cracks, dents, pits, rusting, or other damage that could lead to potential leaks observed on the
tank or associated fittings and pipes. On December 17, 2019 the tank was transported off-Site
and disposed of at an approved facility. Tank disposal documentation is provided in Appendix
B.

After removal of the tank, four sidewall (SW-1 through SW-4) samples were collected from
approximately 5 ft below ground surface (bgs) and one base (BASE-1) sample was collected
from approximately 10 ft bgs within the UST basin. The sidewall and base samples were
collected from native soil. In addition to the UST removal, the associated gasoline dispenser was
removed and the associated product lines were capped. Following removal of the dispenser
island, a dispenser island closure sample (DI-1) was collected from approximately 2 ft bgs.
Based on the approximate 10 ft length of product piping, one product line closure sample (PL-1)
was also collected from a depth of approximately 4 ft bgs. PID readings from the UST closure
samples ranged from 1.2 parts per million (ppm) from the dispenser island and 8.5 ppm from
sidewall SW-2.

Soil samples selected for laboratory analysis were collected directly into laboratory supplied
sample containers, labeled with the sample identification, date, time, and requested analyses and
placed in a laboratory supplied cooler with ice. The samples were delivered to Waypoint
Analytical, LLC (Waypoint) under standard chain of custody protocols for laboratory analysis of
total petroleum hydrocarbons gasoline range organics (TPH-GRO) by EPA Method 8015C. The
soil samples from the product line (PL-1), dispenser island (DI-1), and base of the UST (BASE-
1) were also analyzed for volatile petroleum hydrocarbons (VPH) by the Massachusetts
Department of Environmental Protection (MADEP) method and volatile organic compounds
(VOCs) by EPA Method 8260B. Additional soil volume from BASE-1 was collected and
analyzed for semi-VOCs (SVOCs) by EPA Method 8270D, Resource Conservation and
Recovery Act (RCRA) metals plus hexavalent chromium by EPA Methods 6020B/7471B/7199,
Ms. Joselyn Harriger, PG January 30, 2020
Page 5
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-010 Jim Griffin Brownfields\Redevelopment Report\Final To DEQ\Redevelopment Summary Report_Jim Griffin (BPN 22026-18-060)_20200130.doc
and extractable petroleum hydrocarbons (EPH) by the MADEP method. The laboratory
analytical report and chain of custody record are provided in Appendix C.

2.2 UST Closure Soil Analytical Results

A tabular summary of soil sample analytical results is provided in Table 1. The laboratory
analytical results were compared to the DEQ Division of Waste Management (DWM) UST
Section Action Levels dated July 2016 and the DEQ Inactive Hazardous Sites Branch (IHSB)
Residential and Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) dated
December 2019. In addition, metals results were compared to published concentrations for
naturally occurring metals in North Carolina soil.

Laboratory analytical results indicate that TPH-GRO was detected in sidewall sample SW-2 [8.4
milligrams per kilogram (mg/kg)] and UST base sample BASE-1 (14 mg/kg). The TPH-GRO
concentrations are below the UST Section Action Level of 50 mg/kg. Several VOCs, SVOCs,
and VPH/EPH compounds were detected above laboratory method detection limits in the BASE-
1, product line (PL-1), and dispenser island (DI-1) samples. Of the compounds detected, only
benzo(a)pyrene was detected in BASE-1 (0.16 mg/kg) at a concentration slightly above the
Residential PSRG of 0.11 mg/kg. Additionally, low levels the metals arsenic, barium, cadmium,
hexavalent chromium, trivalent chromium, lead, and mercury were detected above laboratory
method detection limits from the BASE-1 sample. Of the metal compounds detected in BASE-1,
only hexavalent chromium (19 mg/kg) was detected above both the Residential (0.31 mg/kg) and
Industrial/Commercial PSRG (6.5 mg/kg). No other compounds were detected above the UST
Section Action Level or PSRGs in soil samples collected in the vicinity UST.

3.0 Summary

Redevelopment activities at the Jim Griffin Brownfields property began in December 2019 and
included razing the Site buildings, installation of erosion control measures, and initial grading to
Table 1
Summary of UST Closure Analytical Data
Jim Griffin
Charlotte, North Carolina
H&H Job No. BOU-010
Sample ID SW-1 SW-2 SW-3 SW-4 PL-1 DI-1 BASE-1
Sample Location Product Lines Dispenser Island UST Base
Depth (ft bgs)5 5 5 5 4 2 10
Date 12/17/2019 12/17/2019 12/17/2019 12/17/2019 12/17/2019 12/17/2019 12/17/2019
Sample Type Grab Grab Grab Grab Grab Grab Grab Range Mean
TPH-GRO (8015C)<2.1 8.4 <1.6 <1.8 <1.3 <2.7 14 50 --------
VPH (MADEP)
Aliphatic (C5-C8)NA NA NA NA <4.2 23 J <5.3 --110 460 ----
Aliphaitc (C9-C12)NA NA NA NA 5.2 28 J 6.8 J --20 93 ----
Aromatic (C9-C10)NA NA NA NA <2.0 <5.2 <2.5 --17 89 ----
EPH (MADEP)
Aliphatic (C9-C18)NA NA NA NA NA NA <1.7 --20 93 ----
Aliphaitc (C19-C36)NA NA NA NA NA NA 7.4 J --47,000 700,000 ----
Aromatic (C11-C22)NA NA NA NA NA NA <9.2 --20 120 ----
VOCs (8260B)
Acetone NA NA NA NA 0.057 0.058 0.042 --12,000 140,000 ----
Benzene NA NA NA NA <0.00094 <0.0014 0.0050 J --1.2 5.4 ----
Ethylbenzene NA NA NA NA <0.00090 <0.0013 0.0031 J --6 27 ----
Methyl Acetate NA NA NA NA <0.00056 <0.00083 0.0045 J --16,000 230,000 ----
Methylcyclohexane NA NA NA NA <0.00035 <0.00053 0.0018 J --58 650 ----
Toluene NA NA NA NA <0.00096 <0.0014 0.034 --NE NE ----
m&p-Xylenes NA NA NA NA <0.0015 <0.0023 0.0092 J --120 520 ----
o-Xylenes NA NA NA NA <0.00064 <0.00095 0.0036 J --140 590 ----
SVOCs (8270D)
Benzo(a)anthracene NA NA NA NA NA NA 0.13 J --1.1 21 ----
Benzo(a)pyrene NA NA NA NA NA NA 0.16 J --0.11 2.1 ----
Benzo(b)fluoranthene NA NA NA NA NA NA 0.26 J --1.1 21 ----
Benzo(g,h,i)perylene NA NA NA NA NA NA 0.14 J --15,600*NE ----
Benzo(k)fluoranthene NA NA NA NA NA NA 0.076 J --11 210 ----
Chrysene NA NA NA NA NA NA 0.16 J --110 2,100 ----
Fluoranthene NA NA NA NA NA NA 0.25 J --480 6,000 ----
Indeno(1,2,3-cd)pyrene NA NA NA NA NA NA 0.13 J --1.1 21 ----
2-Methylnaphthalene NA NA NA NA NA NA 0.049 J --48 600 ----
Phenanthrene NA NA NA NA NA NA 0.11 J --134*NE ----
Pyrene NA NA NA NA NA NA 0.22 J --360 4,500 ----
Metals (6020/7471/7196A)
Arsenic NA NA NA NA NA NA 2.9 --0.68 3.0 1.0 - 18 4.8
Barium NA NA NA NA NA NA 340 --3,100 47,000 50 - 1,000 356
Cadmium NA NA NA NA NA NA 0.51 J --14 200 1.0 - 10*4.3
Chromium (total)NA NA NA NA NA NA 45 --NE NE 7.0 - 300 65
Hexavalent Chromium NA NA NA NA NA NA 19 --0.31 6.5 NS NS
Trivalent Chromium NA NA NA NA NA NA 26 --23,000 350,000 NS NS
Lead NA NA NA NA NA NA 47 --400 800 ND - 50 16
Mercury NA NA NA NA NA NA 0.16 --2.3 9.7 0.03 - 0.52 0.121
Selenium NA NA NA NA NA NA <0.37 --78 1,200 <0.1 - 0.8 0.42
Silver NA NA NA NA NA NA <0.042 --78 1,200 ND - 5.0 NS
PID Reading 1.8 8.5 1.5 5.6 4.4 1.2 7.9 ----------
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) UST Section Action Level (July 2016)
2) North Carolina DEQ Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (December 2019)
3) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils
* = Protection of Groundwater PSRG
PID readings are in parts per million (ppm)
Soil concentrations are reported in milligrams per kilogram (mg/kg)
Compound concentrations are reported to the laboratory method detection limits
Bold values exceed the Residential PSRG and the mean regional background metals concentration
Underlined values exceed the Industrial/Commercial PSRG and the mean regional background metals concentration
Only those compounds detected in at least one sample shown above
Laboratory analytical methods are shown in parentheses
TPH = total petroleum hydrocarbons; GRO = gasolina range organics; VPH = volatile petroleum hydrocarbons; MADEP = Massachusetts Department of Environmental Protection
UST = underground storage tank; VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surfaceNE = Not Established; NS= Not Specified; NA = Not Analyzed; -- = Not Applicable
J = compound was detected above the laboratory method detection limit but below the laboratory reporting limit resulting in an estimated concentration.
UST Basin Sidewalls
Action Level (1)Residential
PSRGs (2)
Industrial/
Commercial
PSRGs (2)
Regional Background
Metals in Soil (3)
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-010 Jim Griffin Brownfields\Redevelopment Report\Tables\Jim Griffin (BOU-010) UST Samples
1/30/2020
Table 1 (Page 1 of 1)
Hart & Hickman, PC
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NORTH CAROLINA 1991
Figure 1 Checklist
•Crop image to 7”x7”
•Delete downloaded .pdf and. jpg
files
•Compress inserted .jpg to remove
cropped area of image
Right-Click here and
select “Open Hyperlink”
to visit
MYTOPO
TITLE
PROJECT
SITE LOCATION MAP
JIM GRIFFIN
1120 SOUTH MINT STREET
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
1-21-20 0
1 BOU-010
SITE
REVISION NO. 0
JOB NO. BOU-010
DATE: 1-28-20
FIGURE NO. 2
JIM GRIFFIN
1120 SOUTH MINT STREET
CHARLOTTE, NORTH CAROLINA
SITE MAP AND REDEVELOPMENT PLANS
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
S. MI
N
T
S
T
R
E
E
T
MULTI-TENANT COMMERCIAL
& OFFICE BUILDING
(1127 S. MINT STREET)
CROSSFIT SOUTHEND
(1115 S. MINT STREET)
PAM BRACKETT PHOTOGRAPHY
(1124 S. MINT STREET)
PALMER STREET GAMEBAR/
TAPROOM/ EATS
(412 W. PALMER STREET)
CHARLOTTE SAW & KNIFE CO. INC.
(420 W. PALMER STREET)MECHA
N
I
C
A
L

S
YSTEM
S
&

S
ERV
I
C
E
S
(EPA

ID
:
NCD
0
9
3
3
4
2
9
0
5
)
(
1
2
0
1

S
.
G
R
AHAM

STREE
T
)
MULTI-TENANT COMMERCIAL & OFFICE BUILDING
(1100 S. MINT STREET)
ROWE CORP PROPERTY/
BOULIGNY SITE
(EPA ID: NCD98083879)
WALL'S WELDING & FABRICATION
(1108 S. GRAHAM STREET)
CHARLOTTE YARD 1128
(UNDER CONSTRUCTION)
(1120 S. GRAHAM STREET)
S. G
R
A
H
A
M
S
T
R
E
E
T
W. CARSON
BOU
LE
V
ARD
W. P
A
LMER

STR
EE
T
ASPHALT PARKING
4,000-GAL. GASOLINE UST
GASOLINE DISPENSER ISLAND
LEGEND
SITE PROPERTY BOUNDARY
UNDERGROUND STORAGE TANK
GRAVEL PARKING
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-010 Jim Griffin Brownfields\Figures\Site Map-R1_recover001.dwg, SITE MAP FIG 2, 1/29/2020 1:11:16 PM, jdemmer
SB-1
SB-2
SW-1
SW-3
SW-4
PL-1
DI-1
SB-3 / TMW-3
BASE-1
SW-2
REVISION NO. 0
JOB NO. BOU-010
DATE: 1-28-20
FIGURE NO. 3
JIM GRIFFIN
1120 SOUTH MINT STREET
CHARLOTTE, NORTH CAROLINA
SOIL CONCENTRATIONS ABOVE SCREENING
LEVELS MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
S. MI
N
T
S
T
R
E
E
T
MULTI-TENANT COMMERCIAL
& OFFICE BUILDING
(1127 S. MINT STREET)
CROSSFIT SOUTHEND
(1115 S. MINT STREET)
PAM BRACKETT PHOTOGRAPHY
(1124 S. MINT STREET)
PALMER STREET GAMEBAR/
TAPROOM/ EATS
(412 W. PALMER STREET)
CHARLOTTE SAW & KNIFE CO. INC.
(420 W. PALMER STREET)MECHA
N
I
C
A
L

S
YST
EM
S
&

S
ERV
I
C
E
S
(EPA

ID
:
NCD
0
9
3
3
4
2
9
0
5
)
(
1
2
0
1

S
.
GR
AHAM

S
TREE
T
)
MULTI-TENANT COMMERCIAL & OFFICE BUILDING
(1100 S. MINT STREET)
ROWE CORP PROPERTY/
BOULIGNY SITE
(EPA ID: NCD98083879)
WALL'S WELDING & FABRICATION
(1108 S. GRAHAM STREET)
CHARLOTTE YARD 1128
(UNDER CONSTRUCTION)
(1120 S. GRAHAM STREET)
S. G
R
A
H
A
M
S
T
R
E
E
T
W. CARSON
BOU
LEV
ARD
W. P
A
LMER

S
TR
EE
T
ASPHALT PARKING
4,000-GAL. GASOLINE UST
GASOLINE DISPENSER ISLAND
LEGEND
SITE PROPERTY BOUNDARY
APPROXIMATE EXTENT OF
EXCAVATION
SOIL BORING LOCATION
CO-LOCATED SOIL BORING /
TEMPORARY MONITORING WELL
LOCATION
UST CLOSURE SOIL SAMPLE
UNDERGROUND STORAGE TANK
GRAVEL PARKING
NOTES:
1. SOIL BORING SAMPLES WERE COLLECTED BETWEEN 1/21/19
AND 1/23/19. UST CLOSURE SOIL SAMPLES WERE
COLLECTED ON 12/17/19.
2. GRO = GASOLINE RANGE ORGANICS
VPH = VOLATILE PETROLEUM HYDROCARBONS
B(A)P = BENZO(a) PYRENE
B(B)F = BENZO(b) FLUORANTHENE
CR(IV) = HEXALALENT CHROMIUM
PSRG = PRELIMINARY SOIL REMEDIATION GOALS
3. CONCENTRATIONS ARE IN MILLIGRAMS PER KILOGRAM
(mg/kg)
4. * = AROMATIC CARBON CHAIN C09-C10.
+ = ALIPHATIC CARBON CHAIN C09-C12.
5.BOLD CONCENTRATIONS EXCEED THE RESIDENTIAL PSRG.
6.UNDERLINED CONCENTRATIONS EXCEED THE
INDUSTRIAL/COMMERCIAL PSRG.
7. J FLAG INDICATES CONCENTRATIONS BETWEEN
LABORATORY METHOD DETECTION LIMITS AND REPORTING
LIMITS.
BASE-1 (10')
B(A)P 0.16 J
Cr(IV)19
CONCENTRATION
SAMPLE ID
AND DEPTH
CONSTITUENT
SB-3 (1-3')
GRO 67.3
VPH*169
B(B)F 1.13 J
BASE-1 (10')
B(A)P 0.16 J
Cr(IV)19
SB-1 (1-3')
B(A)P 0.544 J
DI-1 (2')
VPH+28 J
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-010 Jim Griffin Brownfields\Figures\Site Map-R1_recover001.dwg, SOIL FIG 3, 1/30/2020 12:51:06 PM, jdemmer

Appendix A UST Closure Forms

Appendix B Tank Disposal Certificates

Appendix C Laboratory Analytical Report
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this
case narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
1/23/20 9:33
Hart & Hickman (Charlotte)
Ralph McGee
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: BOU-010
Lab Submittal Date: 12/17/2019
Work Order: 9120279
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Project Management Manager
Reviewed ByAngela D. Overcash Angela D. Overcash
Project Management Manager
Data Qualifiers Key Reference:
A Sample analyzed outide of holding time.
Aa Vials received from client with low soil weight. Ran the vials with sample that the client provided.
D RPD value outside of the control limits.
E Estimated concentration above the calibration range
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
PS Post Spike recovery is outside of the control limits.
Method Detection LimitMDL
Not Detected at the MDLU
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Sample Receipt Summary
01/23/2020
Work Order: 9120279
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
9120279-01 12/17/19 9:20SW-1 (5’)12/17/19 16:00Solid
9120279-02 12/17/19 9:25SW-2 (5’)12/17/19 16:00Solid
9120279-03 12/17/19 9:30SW-3 (5’)12/17/19 16:00Solid
9120279-04 12/17/19 9:35SW-4 (5’)12/17/19 16:00Solid
9120279-05 12/17/19 9:45PL-1 (4’)12/17/19 16:00Solid
9120279-06 12/17/19 9:50DI-1 (2’)12/17/19 16:00Solid
9120279-07 12/17/19 9:40BASE-1 (10’)12/17/19 16:00Solid
Samples were received in good condition at 5.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 9120279
01/23/2020
Summary of Detections
8.4 mg/kg dry9120279-02 SW-2 (5’)Gasoline Range Organics 8015C
0.057 mg/kg dry9120279-05 PL-1 (4’)Acetone 8260D
5.2 J mg/kg dry9120279-05 PL-1 (4’)C9-C12 Aliphatics MADEP VPH
0.058 mg/kg dry9120279-06 DI-1 (2’)Acetone 8260D
23 J mg/kg dry9120279-06 DI-1 (2’)C5-C8 Aliphatics MADEP VPH
28 J mg/kg dry9120279-06 DI-1 (2’)C9-C12 Aliphatics MADEP VPH
7.4 J mg/kg dry9120279-07 BASE-1 (10’)C19-C36 Aliphatics MADEP EPH
14 mg/kg dry9120279-07 BASE-1 (10’)Gasoline Range Organics 8015C
0.049 J mg/kg dry9120279-07 BASE-1 (10’)2-Methylnaphthalene 8270E
0.13 J mg/kg dry9120279-07 BASE-1 (10’)Benzo(a)anthracene 8270E
0.16 J mg/kg dry9120279-07 BASE-1 (10’)Benzo(a)pyrene 8270E
0.26 J mg/kg dry9120279-07 BASE-1 (10’)Benzo(b)fluoranthene 8270E
0.14 J mg/kg dry9120279-07 BASE-1 (10’)Benzo(g,h,i)perylene 8270E
0.076 J mg/kg dry9120279-07 BASE-1 (10’)Benzo(k)fluoranthene 8270E
0.16 J mg/kg dry9120279-07 BASE-1 (10’)Chrysene 8270E
0.25 J mg/kg dry9120279-07 BASE-1 (10’)Fluoranthene 8270E
0.13 J mg/kg dry9120279-07 BASE-1 (10’)Indeno(1,2,3-cd)pyrene 8270E
0.11 J mg/kg dry9120279-07 BASE-1 (10’)Phenanthrene 8270E
0.22 J mg/kg dry9120279-07 BASE-1 (10’)Pyrene 8270E
19 mg/kg dry9120279-07 BASE-1 (10’)Hexavalent Chromium 7196A
0.16 A mg/kg dry9120279-07 BASE-1 (10’)Mercury 7471B
2.9 mg/kg dry9120279-07 BASE-1 (10’)Arsenic 6010D
340 mg/kg dry9120279-07 BASE-1 (10’)Barium 6010D
0.51 J mg/kg dry9120279-07 BASE-1 (10’)Cadmium 6010D
45 mg/kg dry9120279-07 BASE-1 (10’)Chromium 6010D
47 mg/kg dry9120279-07 BASE-1 (10’)Lead 6010D
0.042 mg/kg dry9120279-07 BASE-1 (10’)Acetone 8260D
0.0050 J mg/kg dry9120279-07 BASE-1 (10’)Benzene 8260D
0.0031 J mg/kg dry9120279-07 BASE-1 (10’)Ethylbenzene 8260D
0.0092 J mg/kg dry9120279-07 BASE-1 (10’)m,p-Xylenes 8260D
0.0045 J mg/kg dry9120279-07 BASE-1 (10’)Methyl Acetate 8260D
0.0018 J mg/kg dry9120279-07 BASE-1 (10’)Methylcyclohexane 8260D
0.0036 J mg/kg dry9120279-07 BASE-1 (10’)o-Xylene 8260D
0.034 mg/kg dry9120279-07 BASE-1 (10’)Toluene 8260D
0.013 J mg/kg dry9120279-07 BASE-1 (10’)Xylenes, total 8260D
6.8 J mg/kg dry9120279-07 BASE-1 (10’)C9-C12 Aliphatics MADEP VPH
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-01
Work Order: 9120279
Time Collected: 12/17/19 09:20
Time Submitted: 12/17/19 16:00
SW-1 (5’)
Gasoline Range Organics by GC/FID
8015C P9L0329507.5 12/18/19 18:33 TBLmg/kg dry 2.1Gasoline Range Organics 2.1 U
Surrogate Recovery Control Limits
50-137102 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P9L034010.100 12/19/19 14:04 EDV% by
Weight
0.100% Solids 81.9
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-02
Work Order: 9120279
Time Collected: 12/17/19 09:25
Time Submitted: 12/17/19 16:00
SW-2 (5’)
Gasoline Range Organics by GC/FID
8015C P9L0329505.8 12/18/19 19:01 TBLmg/kg dry 1.6Gasoline Range Organics 8.4
Surrogate Recovery Control Limits
50-137115 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P9L034010.100 12/19/19 14:04 EDV% by
Weight
0.100% Solids 87.3
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-03
Work Order: 9120279
Time Collected: 12/17/19 09:30
Time Submitted: 12/17/19 16:00
SW-3 (5’)
Gasoline Range Organics by GC/FID
8015C P9L0329505.9 12/18/19 19:30 TBLmg/kg dry 1.6Gasoline Range Organics 1.6 U
Surrogate Recovery Control Limits
50-137113 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P9L034010.100 12/19/19 14:04 EDV% by
Weight
0.100% Solids 72.3
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-04
Work Order: 9120279
Time Collected: 12/17/19 09:35
Time Submitted: 12/17/19 16:00
SW-4 (5’)
Gasoline Range Organics by GC/FID
8015C P9L0329506.7 12/18/19 19:58 TBLmg/kg dry 1.8Gasoline Range Organics 1.8 U
Surrogate Recovery Control Limits
50-137112 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P9L034010.100 12/19/19 14:04 EDV% by
Weight
0.100% Solids 87.9
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-05
Work Order: 9120279
Time Collected: 12/17/19 09:45
Time Submitted: 12/17/19 16:00
PL-1 (4’)
Gasoline Range Organics by GC/FID
8015C P9L0329504.8 12/18/19 20:26 TBLmg/kg dry 1.3Gasoline Range Organics 1.3 U
Surrogate Recovery Control Limits
50-137105 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P9L037210.100 12/20/19 13:08 EDV% by
Weight
0.100% Solids 81.6
Volatile Organic Compounds by GC/MS
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.000881,1,1-Trichloroethane 0.00088 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.000441,1,2,2-Tetrachloroethane 0.00044 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.00111,1,2-Trichloro-1,2,2-trifluoroethane 0.0011 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.000651,1,2-Trichloroethane 0.00065 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00111,1-Dichloroethane 0.0011 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00111,1-Dichloroethylene 0.0011 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.000861,2,3-Trichlorobenzene 0.00086 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.000571,2,4-Trichlorobenzene 0.00057 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.000761,2-Dibromo-3-chloropropane 0.00076 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.000541,2-Dibromoethane 0.00054 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.000671,2-Dichlorobenzene 0.00067 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.000721,2-Dichloroethane 0.00072 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.000901,2-Dichloropropane 0.00090 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.000751,3-Dichlorobenzene 0.00075 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.000761,4-Dichlorobenzene 0.00076 U
8260D P9L045610.12 12/26/19 18:04 JLBmg/kg dry 0.0161,4-Dioxane 0.016 U
8260D P9L045610.024 12/26/19 18:04 JLBmg/kg dry 0.0015Acetone0.057
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00094Benzene0.00094 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00099Bromochloromethane0.00099 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00057Bromodichloromethane0.00057 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00047Bromoform0.00047 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.0029Bromomethane0.0029 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.0010Carbon disulfide 0.0010 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.0012Carbon Tetrachloride 0.0012 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00094Chlorobenzene0.00094 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.0011Chloroethane0.0011 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00074Chloroform0.00074 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.0018Chloromethane0.0018 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00095cis-1,2-Dichloroethylene 0.00095 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00059cis-1,3-Dichloropropylene 0.00059 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00073Cyclohexane0.00073 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00040Dibromochloromethane0.00040 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.0017Dichlorodifluoromethane0.0017 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00090Ethylbenzene0.00090 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00070Isopropylbenzene (Cumene)0.00070 U
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-05
Work Order: 9120279
Time Collected: 12/17/19 09:45
Time Submitted: 12/17/19 16:00
PL-1 (4’)
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.0015m,p-Xylenes 0.0015 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00056Methyl Acetate 0.00056 U
8260D P9L045610.024 12/26/19 18:04 JLBmg/kg dry 0.00042Methyl Butyl Ketone (2-Hexanone)0.00042 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00035Methylcyclohexane0.00035 U
8260D P9L045610.024 12/26/19 18:04 JLBmg/kg dry 0.0014Methyl Ethyl Ketone (2-Butanone)0.0014 U
8260D P9L045610.024 12/26/19 18:04 JLBmg/kg dry 0.00049Methyl Isobutyl Ketone 0.00049 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00097Methylene Chloride 0.00097 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00084Methyl-tert-Butyl Ether 0.00084 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00064o-Xylene 0.00064 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00058Styrene0.00058 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.0011Tetrachloroethylene0.0011 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00096Toluene0.00096 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.0012trans-1,2-Dichloroethylene 0.0012 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.00051trans-1,3-Dichloropropylene 0.00051 U
8260D P9L045610.0060 12/26/19 18:04 JLBmg/kg dry 0.0012Trichloroethylene0.0012 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.0016Trichlorofluoromethane0.0016 U
8260D P9L045610.012 12/26/19 18:04 JLBmg/kg dry 0.0012Vinyl chloride 0.0012 U
8260D P9L045610.018 12/26/19 18:04 JLBmg/kg dry 0.0022Xylenes, total 0.0022 U
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-12395 %Dibromofluoromethane
76-12984 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID Aa
MADEP VPH P0A0156100211/13/20 12:47 TBLmg/kg dry 4.2C5-C8 Aliphatics 4.2 U
MADEP VPH P0A0156100211/13/20 12:47 TBLmg/kg dry 1.9C9-C12 Aliphatics 5.2 J
MADEP VPH P0A0156100211/13/20 12:47 TBLmg/kg dry 2.0C9-C10 Aromatics 2.0 U
Surrogate Recovery Control Limits
70-130111 %2,5-Dibromotoluene (PID)
70-130114 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-06
Work Order: 9120279
Time Collected: 12/17/19 09:50
Time Submitted: 12/17/19 16:00
DI-1 (2’)
Gasoline Range Organics by GC/FID
8015C P9L0329509.9 12/18/19 20:54 TBLmg/kg dry 2.7Gasoline Range Organics 2.7 U
Surrogate Recovery Control Limits
50-137111 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P9L037210.100 12/20/19 13:08 EDV% by
Weight
0.100% Solids 76.5
Volatile Organic Compounds by GC/MS
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00131,1,1-Trichloroethane 0.0013 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.000651,1,2,2-Tetrachloroethane 0.00065 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.00161,1,2-Trichloro-1,2,2-trifluoroethane 0.0016 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.000971,1,2-Trichloroethane 0.00097 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00161,1-Dichloroethane 0.0016 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00161,1-Dichloroethylene 0.0016 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.00131,2,3-Trichlorobenzene 0.0013 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.000851,2,4-Trichlorobenzene 0.00085 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.00111,2-Dibromo-3-chloropropane 0.0011 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.000801,2-Dibromoethane 0.00080 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00101,2-Dichlorobenzene 0.0010 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00111,2-Dichloroethane 0.0011 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00131,2-Dichloropropane 0.0013 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00111,3-Dichlorobenzene 0.0011 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00111,4-Dichlorobenzene 0.0011 U
8260D P9L045610.18 12/26/19 18:34 JLBmg/kg dry 0.0251,4-Dioxane 0.025 U
8260D P9L045610.036 12/26/19 18:34 JLBmg/kg dry 0.0023Acetone0.058
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0014Benzene0.0014 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0015Bromochloromethane0.0015 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00085Bromodichloromethane0.00085 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00069Bromoform0.00069 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.0044Bromomethane0.0044 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0015Carbon disulfide 0.0015 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0018Carbon Tetrachloride 0.0018 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0014Chlorobenzene0.0014 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.0017Chloroethane0.0017 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0011Chloroform0.0011 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.0027Chloromethane0.0027 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0014cis-1,2-Dichloroethylene 0.0014 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00088cis-1,3-Dichloropropylene 0.00088 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0011Cyclohexane0.0011 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00060Dibromochloromethane0.00060 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.0025Dichlorodifluoromethane0.0025 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0013Ethylbenzene0.0013 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0010Isopropylbenzene (Cumene)0.0010 U
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-06
Work Order: 9120279
Time Collected: 12/17/19 09:50
Time Submitted: 12/17/19 16:00
DI-1 (2’)
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.0023m,p-Xylenes 0.0023 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00083Methyl Acetate 0.00083 U
8260D P9L045610.036 12/26/19 18:34 JLBmg/kg dry 0.00062Methyl Butyl Ketone (2-Hexanone)0.00062 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00053Methylcyclohexane0.00053 U
8260D P9L045610.036 12/26/19 18:34 JLBmg/kg dry 0.0021Methyl Ethyl Ketone (2-Butanone)0.0021 U
8260D P9L045610.036 12/26/19 18:34 JLBmg/kg dry 0.00073Methyl Isobutyl Ketone 0.00073 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0014Methylene Chloride 0.0014 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0013Methyl-tert-Butyl Ether 0.0013 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00095o-Xylene 0.00095 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00087Styrene0.00087 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0016Tetrachloroethylene0.0016 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0014Toluene0.0014 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0017trans-1,2-Dichloroethylene 0.0017 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.00077trans-1,3-Dichloropropylene 0.00077 U
8260D P9L045610.0090 12/26/19 18:34 JLBmg/kg dry 0.0017Trichloroethylene0.0017 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.0024Trichlorofluoromethane0.0024 U
8260D P9L045610.018 12/26/19 18:34 JLBmg/kg dry 0.0018Vinyl chloride 0.0018 U
8260D P9L045610.027 12/26/19 18:34 JLBmg/kg dry 0.0032Xylenes, total 0.0032 U
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-12396 %Dibromofluoromethane
76-12984 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID Aa
MADEP VPH P0A0151100561/10/20 17:34 TBLmg/kg dry 11C5-C8 Aliphatics 23 J
MADEP VPH P0A0151100561/10/20 17:34 TBLmg/kg dry 4.9C9-C12 Aliphatics 28 J
MADEP VPH P0A0151100561/10/20 17:34 TBLmg/kg dry 5.2C9-C10 Aromatics 5.2 U
Surrogate Recovery Control Limits
70-130106 %2,5-Dibromotoluene (PID)
70-130110 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-07
Work Order: 9120279
Time Collected: 12/17/19 09:40
Time Submitted: 12/17/19 16:00
BASE-1 (10’)
Extractable Petroleum Hydrocarbons by GC/FID
MADEP EPH P9L04761341/2/20 15:26 ZRCmg/kg dry 1.7C9-C18 Aliphatics 1.7 U
MADEP EPH P9L04761341/2/20 15:26 ZRCmg/kg dry 5.7C19-C36 Aliphatics 7.4 J
MADEP EPH P9L04761341/2/20 15:26 ZRCmg/kg dry 9.2C11-C22 Aromatics 9.2 U
Surrogate Recovery Control Limits
40-14067 %1-Chlorooctadecane
40-14069 %o-Terphenyl
40-14078 %2-Fluorobiphenyl
40-14081 %2-Bromonaphthalene
Gasoline Range Organics by GC/FID
8015C P9L0329508.8 12/18/19 21:22 TBLmg/kg dry 2.4Gasoline Range Organics 14
Surrogate Recovery Control Limits
50-137112 %a,a,a-Trifluorotoluene
General Chemistry Parameters
SM2540 G P9L037210.100 12/20/19 13:08 EDV% by
Weight
0.100% Solids 73.4
Semivolatile Organic Compounds by GC/MS
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.121,1’-Biphenyl 0.12 U
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.272,3,4,6-Tetrachlorophenol 0.27 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.192,4,5-Trichlorophenol 0.19 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.222,4,6-Trichlorophenol 0.22 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.182,4-Dichlorophenol 0.18 U
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.192,4-Dimethylphenol 0.19 U
8270E P9L044012.0 12/31/19 14:07 JMVmg/kg dry 0.532,4-Dinitrophenol 0.53 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.242,4-Dinitrotoluene 0.24 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.232,6-Dinitrotoluene 0.23 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.222-Chloronaphthalene 0.22 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.172-Chlorophenol 0.17 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.0172-Methylnaphthalene 0.049 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.172-Methylphenol 0.17 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.192-Nitroaniline 0.19 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.152-Nitrophenol 0.15 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.183,3’-Dichlorobenzidine 0.18 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.193/4-Methylphenol 0.19 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.173-Nitroaniline 0.17 U
8270E P9L044012.0 12/31/19 14:07 JMVmg/kg dry 0.504,6-Dinitro-2-methylphenol 0.50 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.214-Bromophenyl phenyl ether 0.21 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.174-Chloro-3-methylphenol 0.17 U
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.114-Chloroaniline 0.11 U
8270E P9L044011.4 12/31/19 14:07 JMVmg/kg dry 0.284-Chlorophenyl phenyl ether 0.28 U
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.144-Nitroaniline 0.14 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.224-Nitrophenol 0.22 U
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-07
Work Order: 9120279
Time Collected: 12/17/19 09:40
Time Submitted: 12/17/19 16:00
BASE-1 (10’)
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.021Acenaphthene0.021 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.018Acenaphthylene0.018 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.22Acetophenone0.22 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.0099Anthracene0.0099 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.11Atrazine0.11 U
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.078Benzaldehyde0.078 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.011Benzo(a)anthracene 0.13 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.0080Benzo(a)pyrene 0.16 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.0083Benzo(b)fluoranthene 0.26 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.0089Benzo(g,h,i)perylene 0.14 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.0095Benzo(k)fluoranthene 0.076 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.17bis(2-Chloroethoxy)methane 0.17 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.14Bis(2-Chloroethyl)ether 0.14 U
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.16Bis(2-chloroisopropyl)ether 0.16 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.20Bis(2-Ethylhexyl)phthalate 0.20 U
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.16Butyl benzyl phthalate 0.16 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.17Caprolactam0.17 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.21Carbazole0.21 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.011Chrysene0.16 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.026Dibenzo(a,h)anthracene 0.026 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.24Dibenzofuran0.24 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.23Diethyl phthalate 0.23 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.22Dimethyl phthalate 0.22 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.22Di-n-butyl phthalate 0.22 U
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.23Di-n-octyl phthalate 0.23 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.010Fluoranthene0.25 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.016Fluorene0.016 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.20Hexachlorobenzene0.20 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.20Hexachlorobutadiene0.20 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.31Hexachlorocyclopentadiene0.31 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.14Hexachloroethane0.14 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.025Indeno(1,2,3-cd)pyrene 0.13 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.19Isophorone0.19 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.019Naphthalene0.019 U
8270E P9L044010.45 12/31/19 14:07 JMVmg/kg dry 0.19Nitrobenzene0.19 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.21N-Nitroso-di-n-propylamine 0.21 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.25N-Nitrosodiphenylamine 0.25 U
8270E P9L044011.4 12/31/19 14:07 JMVmg/kg dry 0.57Pentachlorophenol0.57 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.0098Phenanthrene0.11 J
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.15Phenol0.15 U
8270E P9L044010.90 12/31/19 14:07 JMVmg/kg dry 0.013Pyrene0.22 J
Surrogate Recovery Control Limits
37-13174 %2,4,6-Tribromophenol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-07
Work Order: 9120279
Time Collected: 12/17/19 09:40
Time Submitted: 12/17/19 16:00
BASE-1 (10’)
47-13077 %2-Fluorobiphenyl
44-11772 %2-Fluorophenol
45-12169 %Nitrobenzene-d5
37-12768 %Phenol-d5
38-13579 %Terphenyl-d14
Total Metals
7196A P0A021910.55 1/15/20 14:05 BMSmg/kg dry 0.13Hexavalent Chromium 19
7471B P0A028910.068 1/20/20 15:10 JABmg/kg dry 0.024Mercury0.16 A
6010D P0A023911.4 1/22/20 12:22 JABmg/kg dry 0.18Arsenic2.9
6010D P0A0239101401/22/20 15:48 JABmg/kg dry 41Barium340
6010D P0A023910.68 1/22/20 12:22 JABmg/kg dry 0.046Cadmium0.51 J
6010D P0A023911.4 1/22/20 12:22 JABmg/kg dry 0.10Chromium45
6010D P0A023911.4 1/22/20 12:22 JABmg/kg dry 0.23Lead47
6010D P0A023911.4 1/22/20 12:22 JABmg/kg dry 0.37Selenium0.37 U
6010D P0A023910.68 1/22/20 12:22 JABmg/kg dry 0.042Silver0.042 U
Volatile Organic Compounds by GC/MS
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00141,1,1-Trichloroethane 0.0014 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.000691,1,2,2-Tetrachloroethane 0.00069 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.00161,1,2-Trichloro-1,2,2-trifluoroethane 0.0016 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00101,1,2-Trichloroethane 0.0010 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00171,1-Dichloroethane 0.0017 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00171,1-Dichloroethylene 0.0017 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.00131,2,3-Trichlorobenzene 0.0013 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.000901,2,4-Trichlorobenzene 0.00090 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.00121,2-Dibromo-3-chloropropane 0.0012 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.000841,2-Dibromoethane 0.00084 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00111,2-Dichlorobenzene 0.0011 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00111,2-Dichloroethane 0.0011 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00141,2-Dichloropropane 0.0014 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00121,3-Dichlorobenzene 0.0012 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00121,4-Dichlorobenzene 0.0012 U
8260D P9L045610.19 12/26/19 19:04 JLBmg/kg dry 0.0261,4-Dioxane 0.026 U
8260D P9L045610.038 12/26/19 19:04 JLBmg/kg dry 0.0024Acetone0.042
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0015Benzene0.0050 J
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0015Bromochloromethane0.0015 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00089Bromodichloromethane0.00089 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00073Bromoform0.00073 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.0046Bromomethane0.0046 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0016Carbon disulfide 0.0016 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0019Carbon Tetrachloride 0.0019 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0015Chlorobenzene0.0015 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.0018Chloroethane0.0018 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0012Chloroform0.0012 U
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/23/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Sample Matrix: Solid
Client Sample ID:
Sample ID: 9120279-07
Work Order: 9120279
Time Collected: 12/17/19 09:40
Time Submitted: 12/17/19 16:00
BASE-1 (10’)
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.0029Chloromethane0.0029 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0015cis-1,2-Dichloroethylene 0.0015 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00093cis-1,3-Dichloropropylene 0.00093 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0011Cyclohexane0.0011 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00063Dibromochloromethane0.00063 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.0027Dichlorodifluoromethane0.0027 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0014Ethylbenzene0.0031 J
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0011Isopropylbenzene (Cumene)0.0011 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.0024m,p-Xylenes 0.0092 J
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00087Methyl Acetate 0.0045 J
8260D P9L045610.038 12/26/19 19:04 JLBmg/kg dry 0.00065Methyl Butyl Ketone (2-Hexanone)0.00065 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00056Methylcyclohexane0.0018 J
8260D P9L045610.038 12/26/19 19:04 JLBmg/kg dry 0.0022Methyl Ethyl Ketone (2-Butanone)0.0022 U
8260D P9L045610.038 12/26/19 19:04 JLBmg/kg dry 0.00077Methyl Isobutyl Ketone 0.00077 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0015Methylene Chloride 0.0015 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0013Methyl-tert-Butyl Ether 0.0013 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0010o-Xylene 0.0036 J
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00091Styrene0.00091 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0017Tetrachloroethylene0.0017 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0015Toluene0.034
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0018trans-1,2-Dichloroethylene 0.0018 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.00081trans-1,3-Dichloropropylene 0.00081 U
8260D P9L045610.0094 12/26/19 19:04 JLBmg/kg dry 0.0018Trichloroethylene0.0018 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.0025Trichlorofluoromethane0.0025 U
8260D P9L045610.019 12/26/19 19:04 JLBmg/kg dry 0.0019Vinyl chloride 0.0019 U
8260D P9L045610.028 12/26/19 19:04 JLBmg/kg dry 0.0034Xylenes, total 0.013 J
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-12394 %Dibromofluoromethane
76-12984 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID Aa
MADEP VPH P0A0151100271/10/20 18:03 TBLmg/kg dry 5.3C5-C8 Aliphatics 5.3 U
MADEP VPH P0A0151100271/10/20 18:03 TBLmg/kg dry 2.4C9-C12 Aliphatics 6.8 J
MADEP VPH P0A0151100271/10/20 18:03 TBLmg/kg dry 2.5C9-C10 Aromatics 2.5 U
Surrogate Recovery Control Limits
70-130124 %2,5-Dibromotoluene (PID)
70-130127 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9L0456 - 5035
Blank (P9L0456-BLK1)Prepared & Analyzed: 12/26/19
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wetBRL0.010
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.010
1,2,4-Trichlorobenzene mg/kg wetBRL0.010
1,2-Dibromo-3-chloropropane mg/kg wetBRL0.010
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
1,4-Dioxane mg/kg wetBRL0.10
Acetone mg/kg wetBRL0.020
Benzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon disulfide mg/kg wetBRL0.0050
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.010
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Cyclohexane mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.010
Ethylbenzene mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Acetate mg/kg wetBRL0.0050
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.020
Methylcyclohexane mg/kg wetBRL0.0050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.020
Methyl Isobutyl Ketone mg/kg wetBRL0.020
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9L0456 - 5035
Blank (P9L0456-BLK1)Prepared & Analyzed: 12/26/19
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.010
Vinyl chloride mg/kg wetBRL0.010
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9447.2
ug/L 50.00 76-129Surrogate: Toluene-d8 8441.9
LCS (P9L0456-BS1)Prepared & Analyzed: 12/26/19
1,1,1-Trichloroethane mg/kg wet0.0574 0.0050 0.05000 67-131115
1,1,2,2-Tetrachloroethane mg/kg wet0.0394 0.0050 0.05000 56-12679
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wet0.0589 0.010 0.05000 70-130118
1,1,2-Trichloroethane mg/kg wet0.0477 0.0050 0.05000 70-13395
1,1-Dichloroethane mg/kg wet0.0560 0.0050 0.05000 74-127112
1,1-Dichloroethylene mg/kg wet0.0533 0.0050 0.05000 67-149107
1,2,3-Trichlorobenzene mg/kg wet0.0421 0.010 0.05000 68-13084
1,2,4-Trichlorobenzene mg/kg wet0.0438 0.010 0.05000 66-12588
1,2-Dibromo-3-chloropropane mg/kg wet0.0441 0.010 0.05000 55-15788
1,2-Dibromoethane mg/kg wet0.0488 0.0050 0.05000 70-13298
1,2-Dichlorobenzene mg/kg wet0.0415 0.0050 0.05000 72-12383
1,2-Dichloroethane mg/kg wet0.0504 0.0050 0.05000 68-128101
1,2-Dichloropropane mg/kg wet0.0568 0.0050 0.05000 73-130114
1,3-Dichlorobenzene mg/kg wet0.0415 0.0050 0.05000 71-12083
1,4-Dichlorobenzene mg/kg wet0.0408 0.0050 0.05000 71-12382
1,4-Dioxane mg/kg wet0.548 0.10 0.5000 70-130110
Acetone mg/kg wet0.103 0.020 0.1000 29-198103
Benzene mg/kg wet0.0558 0.0050 0.05000 74-127112
Bromochloromethane mg/kg wet0.0581 0.0050 0.05000 72-134116
Bromodichloromethane mg/kg wet0.0568 0.0050 0.05000 75-122114
Bromoform mg/kg wet0.0532 0.0050 0.05000 66-135106
Bromomethane mg/kg wet0.0490 0.010 0.05000 20-18098
Carbon disulfide mg/kg wet0.0582 0.0050 0.05000 61-129116
Carbon Tetrachloride mg/kg wet0.0573 0.0050 0.05000 64-143115
Chlorobenzene mg/kg wet0.0469 0.0050 0.05000 74-11894
Chloroethane mg/kg wet0.0506 0.010 0.05000 33-149101
Chloroform mg/kg wet0.0562 0.0050 0.05000 73-127112
Chloromethane mg/kg wet0.0520 0.010 0.05000 45-143104
cis-1,2-Dichloroethylene mg/kg wet0.0534 0.0050 0.05000 76-134107
cis-1,3-Dichloropropylene mg/kg wet0.0614 0.0050 0.05000 71-125123
Cyclohexane mg/kg wet0.0555 0.0050 0.05000 70-130111
Dibromochloromethane mg/kg wet0.0498 0.0050 0.05000 73-122100
Dichlorodifluoromethane mg/kg wet0.0376 0.010 0.05000 26-14675
Ethylbenzene mg/kg wet0.0484 0.0050 0.05000 74-12897
Isopropylbenzene (Cumene)mg/kg wet0.0439 0.0050 0.05000 68-12688
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9L0456 - 5035
LCS (P9L0456-BS1)Prepared & Analyzed: 12/26/19
m,p-Xylenes mg/kg wet0.0975 0.010 0.1000 75-12497
Methyl Acetate mg/kg wet0.0428 0.0050 0.05000 70-13086
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0486 0.020 0.05000 61-15797
Methylcyclohexane mg/kg wet0.0559 0.0050 0.05000 70-130112
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0523 0.020 0.05000 63-149105
Methyl Isobutyl Ketone mg/kg wet0.0558 0.020 0.05000 57-162112
Methylene Chloride mg/kg wet0.0490 0.0050 0.05000 74-12998
Methyl-tert-Butyl Ether mg/kg wet0.0594 0.0050 0.05000 70-130119
o-Xylene mg/kg wet0.0488 0.0050 0.05000 74-12698
Styrene mg/kg wet0.0513 0.0050 0.05000 77-121103
Tetrachloroethylene mg/kg wet0.0606 0.0050 0.05000 68-130121
Toluene mg/kg wet0.0566 0.0050 0.05000 71-129113
trans-1,2-Dichloroethylene mg/kg wet0.0541 0.0050 0.05000 73-132108
trans-1,3-Dichloropropylene mg/kg wet0.0608 0.0050 0.05000 68-123122
Trichloroethylene mg/kg wet0.0578 0.0050 0.05000 75-133116
Trichlorofluoromethane mg/kg wet0.0506 0.010 0.05000 44-146101
Vinyl chloride mg/kg wet0.0523 0.010 0.05000 48-147105
Xylenes, total mg/kg wet0.146 0.015 0.1500 74-12698
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.6
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9346.4
ug/L 50.00 76-129Surrogate: Toluene-d8 8442.0
LCS Dup (P9L0456-BSD1)Prepared & Analyzed: 12/26/19
1,1,1-Trichloroethane mg/kg wet0.0575 0.0050 0.05000 2067-131115 0.2
1,1,2,2-Tetrachloroethane mg/kg wet0.0398 0.0050 0.05000 2056-12680 0.9
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wet0.0582 0.010 0.05000 2070-130116 1
1,1,2-Trichloroethane mg/kg wet0.0481 0.0050 0.05000 2070-13396 0.9
1,1-Dichloroethane mg/kg wet0.0560 0.0050 0.05000 2074-127112 0.1
1,1-Dichloroethylene mg/kg wet0.0524 0.0050 0.05000 2067-149105 2
1,2,3-Trichlorobenzene mg/kg wet0.0427 0.010 0.05000 2068-13085 1
1,2,4-Trichlorobenzene mg/kg wet0.0432 0.010 0.05000 2066-12586 1
1,2-Dibromo-3-chloropropane mg/kg wet0.0454 0.010 0.05000 2055-15791 3
1,2-Dibromoethane mg/kg wet0.0497 0.0050 0.05000 2070-13299 2
1,2-Dichlorobenzene mg/kg wet0.0419 0.0050 0.05000 2072-12384 1
1,2-Dichloroethane mg/kg wet0.0515 0.0050 0.05000 2068-128103 2
1,2-Dichloropropane mg/kg wet0.0572 0.0050 0.05000 2073-130114 0.6
1,3-Dichlorobenzene mg/kg wet0.0413 0.0050 0.05000 2071-12083 0.5
1,4-Dichlorobenzene mg/kg wet0.0408 0.0050 0.05000 2071-12382 0.1
1,4-Dioxane mg/kg wet0.570 0.10 0.5000 2070-130114 4
Acetone mg/kg wet0.103 0.020 0.1000 2029-198103 0.09
Benzene mg/kg wet0.0561 0.0050 0.05000 2074-127112 0.6
Bromochloromethane mg/kg wet0.0598 0.0050 0.05000 2072-134120 3
Bromodichloromethane mg/kg wet0.0577 0.0050 0.05000 2075-122115 2
Bromoform mg/kg wet0.0539 0.0050 0.05000 2066-135108 1
Bromomethane mg/kg wet0.0520 0.010 0.05000 2020-180104 6
Carbon disulfide mg/kg wet0.0580 0.0050 0.05000 2061-129116 0.2
Carbon Tetrachloride mg/kg wet0.0578 0.0050 0.05000 2064-143116 0.9
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9L0456 - 5035
LCS Dup (P9L0456-BSD1)Prepared & Analyzed: 12/26/19
Chlorobenzene mg/kg wet0.0465 0.0050 0.05000 2074-11893 0.8
Chloroethane mg/kg wet0.0506 0.010 0.05000 2033-149101 0
Chloroform mg/kg wet0.0560 0.0050 0.05000 2073-127112 0.3
Chloromethane mg/kg wet0.0520 0.010 0.05000 2045-143104 0.04
cis-1,2-Dichloroethylene mg/kg wet0.0536 0.0050 0.05000 2076-134107 0.4
cis-1,3-Dichloropropylene mg/kg wet0.0624 0.0050 0.05000 2071-125125 2
Cyclohexane mg/kg wet0.0548 0.0050 0.05000 2070-130110 1
Dibromochloromethane mg/kg wet0.0508 0.0050 0.05000 2073-122102 2
Dichlorodifluoromethane mg/kg wet0.0374 0.010 0.05000 2026-14675 0.8
Ethylbenzene mg/kg wet0.0478 0.0050 0.05000 2074-12896 1
Isopropylbenzene (Cumene)mg/kg wet0.0435 0.0050 0.05000 2068-12687 1
m,p-Xylenes mg/kg wet0.0964 0.010 0.1000 2075-12496 1
Methyl Acetate mg/kg wet0.0443 0.0050 0.05000 2070-13089 3
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0485 0.020 0.05000 2061-15797 0.2
Methylcyclohexane mg/kg wet0.0555 0.0050 0.05000 2070-130111 0.7
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0532 0.020 0.05000 2063-149106 2
Methyl Isobutyl Ketone mg/kg wet0.0569 0.020 0.05000 2057-162114 2
Methylene Chloride mg/kg wet0.0501 0.0050 0.05000 2074-129100 2
Methyl-tert-Butyl Ether mg/kg wet0.0611 0.0050 0.05000 2070-130122 3
o-Xylene mg/kg wet0.0486 0.0050 0.05000 2074-12697 0.4
Styrene mg/kg wet0.0514 0.0050 0.05000 2077-121103 0.1
Tetrachloroethylene mg/kg wet0.0598 0.0050 0.05000 2068-130120 1
Toluene mg/kg wet0.0568 0.0050 0.05000 2071-129114 0.4
trans-1,2-Dichloroethylene mg/kg wet0.0534 0.0050 0.05000 2073-132107 1
trans-1,3-Dichloropropylene mg/kg wet0.0622 0.0050 0.05000 20 L268-123124 2
Trichloroethylene mg/kg wet0.0581 0.0050 0.05000 2075-133116 0.5
Trichlorofluoromethane mg/kg wet0.0504 0.010 0.05000 2044-146101 0.5
Vinyl chloride mg/kg wet0.0513 0.010 0.05000 2048-147103 2
Xylenes, total mg/kg wet0.145 0.015 0.1500 2074-12697 0.9
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.7
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9346.4
ug/L 50.00 76-129Surrogate: Toluene-d8 8341.3
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9L0440 - 3546
Blank (P9L0440-BLK1)Prepared: 12/26/19 Analyzed: 12/31/19
1,1’-Biphenyl mg/kg wetBRL0.33
2,3,4,6-Tetrachlorophenol mg/kg wetBRL0.33
2,4,5-Trichlorophenol mg/kg wetBRL0.66
2,4,6-Trichlorophenol mg/kg wetBRL0.66
2,4-Dichlorophenol mg/kg wetBRL0.66
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL1.5
2,4-Dinitrotoluene mg/kg wetBRL0.66
2,6-Dinitrotoluene mg/kg wetBRL0.66
2-Chloronaphthalene mg/kg wetBRL0.66
2-Chlorophenol mg/kg wetBRL0.66
2-Methylnaphthalene mg/kg wetBRL0.66
2-Methylphenol mg/kg wetBRL0.66
2-Nitroaniline mg/kg wetBRL0.66
2-Nitrophenol mg/kg wetBRL0.66
3,3’-Dichlorobenzidine mg/kg wetBRL0.66
3/4-Methylphenol mg/kg wetBRL0.66
3-Nitroaniline mg/kg wetBRL0.66
4,6-Dinitro-2-methylphenol mg/kg wetBRL1.5
4-Bromophenyl phenyl ether mg/kg wetBRL0.66
4-Chloro-3-methylphenol mg/kg wetBRL0.66
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL1.0
4-Nitroaniline mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.66
Acenaphthene mg/kg wetBRL0.66
Acenaphthylene mg/kg wetBRL0.66
Acetophenone mg/kg wetBRL0.66
Anthracene mg/kg wetBRL0.66
Atrazine mg/kg wetBRL0.66
Benzaldehyde mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.66
Benzo(a)pyrene mg/kg wetBRL0.66
Benzo(b)fluoranthene mg/kg wetBRL0.66
Benzo(g,h,i)perylene mg/kg wetBRL0.66
Benzo(k)fluoranthene mg/kg wetBRL0.66
bis(2-Chloroethoxy)methane mg/kg wetBRL0.66
Bis(2-Chloroethyl)ether mg/kg wetBRL0.66
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.66
Butyl benzyl phthalate mg/kg wetBRL0.33
Caprolactam mg/kg wetBRL0.66
Carbazole mg/kg wetBRL0.66
Chrysene mg/kg wetBRL0.66
Dibenzo(a,h)anthracene mg/kg wetBRL0.66
Dibenzofuran mg/kg wetBRL0.66
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9L0440 - 3546
Blank (P9L0440-BLK1)Prepared: 12/26/19 Analyzed: 12/31/19
Diethyl phthalate mg/kg wetBRL0.66
Dimethyl phthalate mg/kg wetBRL0.66
Di-n-butyl phthalate mg/kg wetBRL0.66
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.66
Fluorene mg/kg wetBRL0.66
Hexachlorobenzene mg/kg wetBRL0.66
Hexachlorobutadiene mg/kg wetBRL0.66
Hexachlorocyclopentadiene mg/kg wetBRL0.66
Hexachloroethane mg/kg wetBRL0.66
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.66
Isophorone mg/kg wetBRL0.66
Naphthalene mg/kg wetBRL0.66
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.66
N-Nitrosodiphenylamine mg/kg wetBRL0.66
Pentachlorophenol mg/kg wetBRL1.0
Phenanthrene mg/kg wetBRL0.66
Phenol mg/kg wetBRL0.66
Pyrene mg/kg wetBRL0.66
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 852.83
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 861.44
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 882.92
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 781.30
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 812.69
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 901.51
LCS (P9L0440-BS1)Prepared: 12/26/19 Analyzed: 12/31/19
2,4,5-Trichlorophenol mg/kg wet1.52 0.66 1.665 41-12491
2,4,6-Trichlorophenol mg/kg wet1.55 0.66 1.665 39-12693
2,4-Dichlorophenol mg/kg wet1.28 0.66 1.665 40-12277
2,4-Dimethylphenol mg/kg wet1.43 0.33 1.665 30-12786
2,4-Dinitrophenol mg/kg wet0.826 1.5 1.665 J27-12950
2,4-Dinitrotoluene mg/kg wet1.54 0.66 1.665 48-12693
2,6-Dinitrotoluene mg/kg wet1.55 0.66 1.665 46-12493
2-Chloronaphthalene mg/kg wet1.41 0.66 1.665 41-11485
2-Chlorophenol mg/kg wet1.46 0.66 1.665 34-12188
2-Methylnaphthalene mg/kg wet1.25 0.66 1.665 38-12275
2-Methylphenol mg/kg wet1.47 0.66 1.665 32-12288
2-Nitroaniline mg/kg wet1.37 0.66 1.665 44-12782
2-Nitrophenol mg/kg wet1.25 0.66 1.665 36-12375
3,3’-Dichlorobenzidine mg/kg wet1.48 0.66 1.665 22-12189
3/4-Methylphenol mg/kg wet1.35 0.66 1.665 34-11981
3-Nitroaniline mg/kg wet1.35 0.66 1.665 33-11981
4,6-Dinitro-2-methylphenol mg/kg wet1.38 1.5 1.665 J29-13283
4-Bromophenyl phenyl ether mg/kg wet1.52 0.66 1.665 46-12491
4-Chloro-3-methylphenol mg/kg wet1.35 0.66 1.665 45-12281
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9L0440 - 3546
LCS (P9L0440-BS1)Prepared: 12/26/19 Analyzed: 12/31/19
4-Chloroaniline mg/kg wet1.13 0.33 1.665 17-10668
4-Chlorophenyl phenyl ether mg/kg wet1.44 1.0 1.665 45-12187
4-Nitroaniline mg/kg wet1.38 0.33 1.665 63-14783
4-Nitrophenol mg/kg wet1.53 0.66 1.665 30-13292
Acenaphthene mg/kg wet1.50 0.66 1.665 40-12390
Acenaphthylene mg/kg wet1.59 0.66 1.665 32-13296
Acetophenone mg/kg wet1.36 0.66 1.665 33-11582
Anthracene mg/kg wet1.58 0.66 1.665 47-12395
Benzo(a)anthracene mg/kg wet1.50 0.66 1.665 49-12690
Benzo(a)pyrene mg/kg wet1.65 0.66 1.665 45-12999
Benzo(b)fluoranthene mg/kg wet1.57 0.66 1.665 45-13294
Benzo(g,h,i)perylene mg/kg wet1.63 0.66 1.665 43-13498
Benzo(k)fluoranthene mg/kg wet1.64 0.66 1.665 47-13299
bis(2-Chloroethoxy)methane mg/kg wet1.17 0.66 1.665 36-12170
Bis(2-Chloroethyl)ether mg/kg wet1.37 0.66 1.665 31-12082
Bis(2-chloroisopropyl)ether mg/kg wet1.23 0.33 1.665 33-13174
Bis(2-Ethylhexyl)phthalate mg/kg wet1.58 0.66 1.665 51-13395
Butyl benzyl phthalate mg/kg wet1.55 0.33 1.665 48-13293
Carbazole mg/kg wet1.60 0.66 1.665 50-12396
Chrysene mg/kg wet1.55 0.66 1.665 50-12493
Dibenzo(a,h)anthracene mg/kg wet1.38 0.66 1.665 45-13483
Dibenzofuran mg/kg wet1.45 0.66 1.665 44-12087
Diethyl phthalate mg/kg wet1.46 0.66 1.665 50-12488
Dimethyl phthalate mg/kg wet1.43 0.66 1.665 48-12486
Di-n-butyl phthalate mg/kg wet1.61 0.66 1.665 51-12897
Di-n-octyl phthalate mg/kg wet1.63 0.33 1.665 45-14098
Fluoranthene mg/kg wet1.59 0.66 1.665 50-12795
Fluorene mg/kg wet1.51 0.66 1.665 43-12591
Hexachlorobenzene mg/kg wet1.51 0.66 1.665 45-12290
Hexachlorobutadiene mg/kg wet1.30 0.66 1.665 32-12378
Hexachlorocyclopentadiene mg/kg wet1.31 0.66 1.665 32-11779
Hexachloroethane mg/kg wet1.24 0.66 1.665 28-11774
Indeno(1,2,3-cd)pyrene mg/kg wet1.51 0.66 1.665 45-13391
Isophorone mg/kg wet1.01 0.66 1.665 30-12261
Naphthalene mg/kg wet1.20 0.66 1.665 35-12372
Nitrobenzene mg/kg wet1.09 0.33 1.665 34-12265
N-Nitroso-di-n-propylamine mg/kg wet1.39 0.66 1.665 36-12084
N-Nitrosodiphenylamine mg/kg wet1.89 0.66 1.665 38-127114
Pentachlorophenol mg/kg wet1.66 1.0 1.665 25-133100
Phenanthrene mg/kg wet1.56 0.66 1.665 50-12194
Phenol mg/kg wet1.41 0.66 1.665 34-12185
Pyrene mg/kg wet1.64 0.66 1.665 47-12798
mg/kg wet 3.330 37-131Surrogate: 2,4,6-Tribromophenol 913.03
mg/kg wet 1.665 47-130Surrogate: 2-Fluorobiphenyl 811.35
mg/kg wet 3.330 44-117Surrogate: 2-Fluorophenol 862.87
mg/kg wet 1.665 45-121Surrogate: Nitrobenzene-d5 661.10
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9L0440 - 3546
LCS (P9L0440-BS1)Prepared: 12/26/19 Analyzed: 12/31/19
mg/kg wet 3.330 37-127Surrogate: Phenol-d5 802.65
mg/kg wet 1.665 38-135Surrogate: Terphenyl-d14 881.46
LCS (P9L0440-BS2)Prepared: 12/26/19 Analyzed: 12/31/19
1,1’-Biphenyl mg/kg wet1.15 0.33 1.666 40-11769
2,3,4,6-Tetrachlorophenol mg/kg wet1.08 0.33 1.666 44-12565
Atrazine mg/kg wet1.26 0.66 1.666 47-12775
Benzaldehyde mg/kg wet0.936 0.33 1.666 35-11556
Caprolactam mg/kg wet1.12 0.66 1.666 46-11767
mg/kg wet 3.332 37-131Surrogate: 2,4,6-Tribromophenol 642.13
mg/kg wet 1.666 47-130Surrogate: 2-Fluorobiphenyl 651.08
mg/kg wet 3.332 44-117Surrogate: 2-Fluorophenol 652.15
mg/kg wet 1.666 45-121Surrogate: Nitrobenzene-d5 580.958
mg/kg wet 3.332 37-127Surrogate: Phenol-d5 602.00
mg/kg wet 1.666 38-135Surrogate: Terphenyl-d14 651.08
LCS Dup (P9L0440-BSD1)Prepared: 12/26/19 Analyzed: 12/31/19
2,4,5-Trichlorophenol mg/kg wet1.38 0.66 1.662 2041-12483 10
2,4,6-Trichlorophenol mg/kg wet1.39 0.66 1.662 2039-12684 11
2,4-Dichlorophenol mg/kg wet1.19 0.66 1.662 2040-12272 8
2,4-Dimethylphenol mg/kg wet1.29 0.33 1.662 2030-12777 11
2,4-Dinitrophenol mg/kg wet0.677 1.5 1.662 20 J27-12941 20
2,4-Dinitrotoluene mg/kg wet1.38 0.66 1.662 2048-12683 11
2,6-Dinitrotoluene mg/kg wet1.41 0.66 1.662 2046-12485 9
2-Chloronaphthalene mg/kg wet1.30 0.66 1.662 2041-11478 8
2-Chlorophenol mg/kg wet1.24 0.66 1.662 2034-12174 16
2-Methylnaphthalene mg/kg wet1.15 0.66 1.662 2038-12269 8
2-Methylphenol mg/kg wet1.31 0.66 1.662 2032-12279 11
2-Nitroaniline mg/kg wet1.25 0.66 1.662 2044-12775 9
2-Nitrophenol mg/kg wet1.14 0.66 1.662 2036-12368 9
3,3’-Dichlorobenzidine mg/kg wet1.34 0.66 1.662 2022-12181 10
3/4-Methylphenol mg/kg wet1.19 0.66 1.662 2034-11971 13
3-Nitroaniline mg/kg wet1.23 0.66 1.662 2033-11974 10
4,6-Dinitro-2-methylphenol mg/kg wet1.14 1.5 1.662 20 J29-13269 19
4-Bromophenyl phenyl ether mg/kg wet1.35 0.66 1.662 2046-12481 12
4-Chloro-3-methylphenol mg/kg wet1.24 0.66 1.662 2045-12275 8
4-Chloroaniline mg/kg wet1.08 0.33 1.662 2017-10665 5
4-Chlorophenyl phenyl ether mg/kg wet1.30 1.0 1.662 2045-12178 10
4-Nitroaniline mg/kg wet1.23 0.33 1.662 2063-14774 12
4-Nitrophenol mg/kg wet1.31 0.66 1.662 2030-13279 15
Acenaphthene mg/kg wet1.35 0.66 1.662 2040-12381 10
Acenaphthylene mg/kg wet1.44 0.66 1.662 2032-13287 10
Acetophenone mg/kg wet1.17 0.66 1.662 2033-11570 15
Anthracene mg/kg wet1.38 0.66 1.662 2047-12383 13
Benzo(a)anthracene mg/kg wet1.31 0.66 1.662 2049-12679 13
Benzo(a)pyrene mg/kg wet1.44 0.66 1.662 2045-12987 13
Benzo(b)fluoranthene mg/kg wet1.39 0.66 1.662 2045-13283 13
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9L0440 - 3546
LCS Dup (P9L0440-BSD1)Prepared: 12/26/19 Analyzed: 12/31/19
Benzo(g,h,i)perylene mg/kg wet1.43 0.66 1.662 2043-13486 13
Benzo(k)fluoranthene mg/kg wet1.43 0.66 1.662 2047-13286 13
bis(2-Chloroethoxy)methane mg/kg wet1.06 0.66 1.662 2036-12164 10
Bis(2-Chloroethyl)ether mg/kg wet0.964 0.66 1.662 20 D31-12058 35
Bis(2-chloroisopropyl)ether mg/kg wet1.02 0.33 1.662 2033-13162 18
Bis(2-Ethylhexyl)phthalate mg/kg wet1.39 0.66 1.662 2051-13384 12
Butyl benzyl phthalate mg/kg wet1.33 0.33 1.662 2048-13280 15
Carbazole mg/kg wet1.40 0.66 1.662 2050-12384 13
Chrysene mg/kg wet1.36 0.66 1.662 2050-12482 13
Dibenzo(a,h)anthracene mg/kg wet0.979 0.66 1.662 20 D45-13459 34
Dibenzofuran mg/kg wet1.32 0.66 1.662 2044-12079 10
Diethyl phthalate mg/kg wet1.32 0.66 1.662 2050-12479 10
Dimethyl phthalate mg/kg wet1.31 0.66 1.662 2048-12479 9
Di-n-butyl phthalate mg/kg wet1.40 0.66 1.662 2051-12884 14
Di-n-octyl phthalate mg/kg wet1.42 0.33 1.662 2045-14085 14
Fluoranthene mg/kg wet1.39 0.66 1.662 2050-12783 13
Fluorene mg/kg wet1.37 0.66 1.662 2043-12582 10
Hexachlorobenzene mg/kg wet1.31 0.66 1.662 2045-12279 14
Hexachlorobutadiene mg/kg wet1.16 0.66 1.662 2032-12370 11
Hexachlorocyclopentadiene mg/kg wet1.22 0.66 1.662 2032-11773 7
Hexachloroethane mg/kg wet1.04 0.66 1.662 2028-11763 17
Indeno(1,2,3-cd)pyrene mg/kg wet1.56 0.66 1.662 2045-13394 3
Isophorone mg/kg wet0.919 0.66 1.662 2030-12255 9
Naphthalene mg/kg wet1.09 0.66 1.662 2035-12366 9
Nitrobenzene mg/kg wet0.969 0.33 1.662 2034-12258 11
N-Nitroso-di-n-propylamine mg/kg wet1.20 0.66 1.662 2036-12072 15
N-Nitrosodiphenylamine mg/kg wet1.68 0.66 1.662 2038-127101 12
Pentachlorophenol mg/kg wet1.45 1.0 1.662 2025-13388 13
Phenanthrene mg/kg wet1.37 0.66 1.662 2050-12182 13
Phenol mg/kg wet1.24 0.66 1.662 2034-12174 13
Pyrene mg/kg wet1.46 0.66 1.662 2047-12788 11
mg/kg wet 3.324 37-131Surrogate: 2,4,6-Tribromophenol 832.75
mg/kg wet 1.662 47-130Surrogate: 2-Fluorobiphenyl 731.22
mg/kg wet 3.324 44-117Surrogate: 2-Fluorophenol 732.42
mg/kg wet 1.662 45-121Surrogate: Nitrobenzene-d5 600.995
mg/kg wet 3.324 37-127Surrogate: Phenol-d5 692.29
mg/kg wet 1.662 38-135Surrogate: Terphenyl-d14 791.31
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9L0440 - 3546
LCS Dup (P9L0440-BSD2)Prepared: 12/26/19 Analyzed: 12/31/19
1,1’-Biphenyl mg/kg wet1.26 0.33 1.666 2040-11776 9
2,3,4,6-Tetrachlorophenol mg/kg wet1.31 0.33 1.666 2044-12579 20
Atrazine mg/kg wet1.40 0.66 1.666 2047-12784 11
Benzaldehyde mg/kg wet1.03 0.33 1.666 2035-11562 10
Caprolactam mg/kg wet1.25 0.66 1.666 2046-11775 11
mg/kg wet 3.332 37-131Surrogate: 2,4,6-Tribromophenol 732.42
mg/kg wet 1.666 47-130Surrogate: 2-Fluorobiphenyl 721.19
mg/kg wet 3.332 44-117Surrogate: 2-Fluorophenol 732.42
mg/kg wet 1.666 45-121Surrogate: Nitrobenzene-d5 641.07
mg/kg wet 3.332 37-127Surrogate: Phenol-d5 672.22
mg/kg wet 1.666 38-135Surrogate: Terphenyl-d14 741.23
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Batch P0A0151 - MADEP VPH (S)
Blank (P0A0151-BLK1)Prepared & Analyzed: 01/10/20
C5-C8 Aliphatics mg/kg wetBRL5.0
C9-C12 Aliphatics mg/kg wetBRL5.0
C9-C10 Aromatics mg/kg wetBRL5.0
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)11111100
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)11311300
LCS (P0A0151-BS1)Prepared & Analyzed: 01/10/20
C5-C8 Aliphatics mg/kg wet35.1 5.0 32.00 70-130110
C9-C10 Aromatics mg/kg wet10.9 5.0 10.67 70-130102
C9-C12 Aliphatic mg/kg wet35.3 5.0 32.00 70-130110
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)10910900
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)11211200
LCS Dup (P0A0151-BSD1)Prepared & Analyzed: 01/10/20
C5-C8 Aliphatics mg/kg wet34.0 5.0 32.00 5070-130106 3
C9-C10 Aromatics mg/kg wet10.4 5.0 10.67 5070-13097 5
C9-C12 Aliphatic mg/kg wet34.8 5.0 32.00 5070-130109 2
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)10810800
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)11111100
Batch P0A0156 - MADEP VPH (S)
Blank (P0A0156-BLK1)Prepared & Analyzed: 01/13/20
C5-C8 Aliphatics mg/kg wetBRL5.0
C9-C12 Aliphatics mg/kg wetBRL5.0
C9-C10 Aromatics mg/kg wetBRL5.0
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)11511500
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)12012000
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Batch P0A0156 - MADEP VPH (S)
LCS (P0A0156-BS1)Prepared & Analyzed: 01/13/20
C5-C8 Aliphatics mg/kg wet34.7 5.0 32.00 70-130109
C9-C10 Aromatics mg/kg wet11.2 5.0 10.67 70-130105
C9-C12 Aliphatic mg/kg wet36.9 5.0 32.00 70-130115
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)11011000
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)11411400
LCS Dup (P0A0156-BSD1)Prepared & Analyzed: 01/13/20
C5-C8 Aliphatics mg/kg wet36.5 5.0 32.00 5070-130114 5
C9-C10 Aromatics mg/kg wet11.1 5.0 10.67 5070-130104 0.7
C9-C12 Aliphatic mg/kg wet37.2 5.0 32.00 5070-130116 0.8
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (PID)10910900
ug/L 10000 70-130Surrogate: 2,5-Dibromotoluene (FID)11411400
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Gasoline Range Organics by GC/FID - Quality Control
Batch P9L0329 - 5030B
Blank (P9L0329-BLK1)Prepared & Analyzed: 12/18/19
Gasoline Range Organics mg/kg wetBRL5.0
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1095.45
LCS (P9L0329-BS1)Prepared & Analyzed: 12/18/19
Gasoline Range Organics mg/kg wet62.6 5.0 50.00 41-138125
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1165.80
LCS Dup (P9L0329-BSD1)Prepared & Analyzed: 12/18/19
Gasoline Range Organics mg/kg wet60.4 5.0 50.00 2041-138121 4
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1155.75
Matrix Spike (P9L0329-MS1)Prepared & Analyzed: 12/18/19 Source: 9120279-07
Gasoline Range Organics mg/kg dry94.7 6.8 68.17 13.5 41-138119
mg/kg dry 6.817 50-137Surrogate: a,a,a-Trifluorotoluene 1248.45
Matrix Spike Dup (P9L0329-MSD1)Prepared & Analyzed: 12/18/19 Source: 9120279-07
Gasoline Range Organics mg/kg dry92.3 6.8 68.17 13.5 3441-138116 3
mg/kg dry 6.817 50-137Surrogate: a,a,a-Trifluorotoluene 1218.25
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Batch P9L0476 - 3546
Blank (P9L0476-BLK1)Prepared: 12/30/19 Analyzed: 01/02/20
C9-C18 Aliphatics mg/kg wetBRL25
C19-C36 Aliphatics mg/kg wet5.44 25 J
C11-C22 Aromatics mg/kg wetBRL25
mg/kg wet 1.992 40-140Surrogate: 1-Chlorooctadecane 721.44
mg/kg wet 1.992 40-140Surrogate: o-Terphenyl 731.45
mg/kg wet 3.984 40-140Surrogate: 2-Fluorobiphenyl 813.22
mg/kg wet 3.984 40-140Surrogate: 2-Bromonaphthalene 883.50
LCS (P9L0476-BS1)Prepared: 12/30/19 Analyzed: 01/02/20
C9-C18 Aliphatics mg/kg wet31.9 25 59.82 40-14053
C19-C36 Aliphatics mg/kg wet63.0 25 79.76 40-14079
C11-C22 Aromatics mg/kg wet10525 169.5 40-14062
mg/kg wet 1.994 40-140Surrogate: 1-Chlorooctadecane 711.41
mg/kg wet 1.994 40-140Surrogate: o-Terphenyl 691.38
mg/kg wet 3.988 40-140Surrogate: 2-Fluorobiphenyl 773.07
mg/kg wet 3.988 40-140Surrogate: 2-Bromonaphthalene 793.15
LCS Dup (P9L0476-BSD1)Prepared: 12/30/19 Analyzed: 01/02/20
C9-C18 Aliphatics mg/kg wet27.9 25 60.00 5040-14047 13
C19-C36 Aliphatics mg/kg wet56.0 25 80.00 5040-14070 12
C11-C22 Aromatics mg/kg wet10225 170.0 5040-14060 3
mg/kg wet 2.000 40-140Surrogate: 1-Chlorooctadecane 581.17
mg/kg wet 2.000 40-140Surrogate: o-Terphenyl 661.33
mg/kg wet 4.000 40-140Surrogate: 2-Fluorobiphenyl 803.18
mg/kg wet 4.000 40-140Surrogate: 2-Bromonaphthalene 793.17
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P0A0219 - 3060A
Blank (P0A0219-BLK1)Prepared & Analyzed: 01/15/20
Hexavalent Chromium mg/kg wetBRL0.40
LCS (P0A0219-BS1)Prepared & Analyzed: 01/15/20
Hexavalent Chromium mg/kg wet15.7 0.40 16.00 80-12098
Batch P0A0239 - 3050B
Blank (P0A0239-BLK1)Prepared: 01/16/20 Analyzed: 01/22/20
Arsenic mg/kg wetBRL1.0
Barium mg/kg wetBRL10
Cadmium mg/kg wetBRL0.50
Chromium mg/kg wetBRL1.0
Lead mg/kg wetBRL1.0
Selenium mg/kg wetBRL1.0
Silver mg/kg wetBRL0.50
LCS (P0A0239-BS1)Prepared: 01/16/20 Analyzed: 01/22/20
Arsenic mg/kg wet12.3 1.0 12.50 80-12099
Barium mg/kg wet12.8 10 12.50 80-120103
Cadmium mg/kg wet12.5 0.50 12.50 80-120100
Chromium mg/kg wet12.8 1.0 12.50 80-120102
Lead mg/kg wet12.5 1.0 12.50 80-120100
Selenium mg/kg wet12.0 1.0 12.50 80-12096
Silver mg/kg wet4.94 0.50 5.000 80-12099
Matrix Spike (P0A0239-MS1)Prepared: 01/16/20 Analyzed: 01/22/20 Source: 9120279-07
Arsenic mg/kg dry14.7 1.4 17.04 2.92 M75-12569
Barium mg/kg dry21014 17.04 340 E, MC75-125NR
Cadmium mg/kg dry14.1 0.68 17.04 0.512 75-12580
Chromium mg/kg dry68.4 1.4 17.04 45.1 M75-125137
Lead mg/kg dry56.6 1.4 17.04 46.6 M75-12558
Selenium mg/kg dry8.86 1.4 17.04 BRL M75-12552
Silver mg/kg dry5.45 0.68 6.817 BRL 75-12580
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P0A0239 - 3050B
Matrix Spike Dup (P0A0239-MSD1)Prepared: 01/16/20 Analyzed: 01/22/20 Source: 9120279-07
Arsenic mg/kg dry15.6 1.4 17.04 2.92 2075-12575 6
Barium mg/kg dry14814 17.04 340 20 D, MC75-125NR 34
Cadmium mg/kg dry14.6 0.68 17.04 0.512 2075-12583 3
Chromium mg/kg dry63.6 1.4 17.04 45.1 2075-125109 7
Lead mg/kg dry72.0 1.4 17.04 46.6 20 D, M75-125149 24
Selenium mg/kg dry10.5 1.4 17.04 BRL 20 M75-12562 17
Silver mg/kg dry5.74 0.68 6.817 BRL 2075-12584 5
Post Spike (P0A0239-PS1)Prepared: 01/16/20 Analyzed: 01/22/20 Source: 9120279-07
Arsenic mg/L0.499 0.5001 0.00857 75-12598
Barium mg/L1.00E9 0.5000 0.998 MC75-125NR
Cadmium mg/L0.412 0.5000 0.00150 75-12582
Chromium mg/L1.74 0.5001 0.132 PS75-125321
Lead mg/L1.75 0.5001 0.137 PS75-125322
Selenium mg/L0.316 0.4999 -0.00787 PS75-12563
Silver mg/L0.159 0.2000 -0.00169 75-12580
Batch P0A0289 - 7471B
Blank (P0A0289-BLK1)Prepared & Analyzed: 01/20/20
Mercury mg/kg wetBRL0.050
LCS (P0A0289-BS1)Prepared & Analyzed: 01/20/20
Mercury mg/kg wet0.390 0.050 0.4167 80-12094
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/23/20
Level II QC Report
2923 South Tryon St. Ste 100
Project: BOU-010Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ralph McGee
Work Order: 9120279
Time Submitted: 12/17/2019 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P9L0372 - Solids, Dry Weight
Duplicate (P9L0372-DUP1)Prepared: 12/19/19 Analyzed: 12/20/19 Source: 9120279-05
% Solids % by Weight81.0 0.100 81.6 200.8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P9L04769120279-07 12/30/19 11:3010.12 2g mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P9L03299120279-01 12/18/19 10:184.06 5mL mL
P9L03299120279-02 12/18/19 10:184.96 5mL mL
P9L03299120279-03 12/18/19 10:185.84 5mL mL
P9L03299120279-04 12/18/19 10:184.22 5mL mL
P9L03299120279-05 12/18/19 10:186.37 5mL mL
P9L03299120279-06 12/18/19 10:183.3 5mL mL
P9L03299120279-07 12/18/19 10:183.86 5mL mL
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P9L03409120279-01 12/18/19 13:1830 30g g
P9L03409120279-02 12/18/19 13:1830 30g g
P9L03409120279-03 12/18/19 13:1830 30g g
P9L03409120279-04 12/18/19 13:1830 30g g
P9L03729120279-05 12/19/19 13:2030 30g g
P9L03729120279-06 12/19/19 13:2030 30g g
P9L03729120279-07 12/19/19 13:2030 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P9L04409120279-07 12/26/19 11:3030.01 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P0A02399120279-07 01/16/20 9:502 50g mL
P0A02399120279-07 01/16/20 9:502 50g mL
Prep Method: 3060A
Lab Number Batch Date/TimeInitialFinal
P0A02199120279-07 01/15/20 9:502.5 100g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P0A02899120279-07 01/20/20 11:210.6 50g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P9L04569120279-05 12/26/19 9:175.09 5g mL
P9L04569120279-06 12/26/19 9:173.65 5g mL
P9L04569120279-07 12/26/19 9:173.62 5g mL
Prep Method: MADEP VPH (S)
Lab Number Batch Date/TimeInitialFinal
P0A01569120279-05 01/13/20 9:104.34 16g mL
P0A01519120279-06 01/10/20 14:481.76 16g mL
P0A01519120279-07 01/10/20 14:483.8 16g mL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]