FA-644_11660_CA_LAB_20191112_ECS Sampling Event 11-2019

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
November 12, 2019
Matt Gillis
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
Project Location: Wade, NC
Client Job Number:
Project Number: 49:1503 f
Laboratory Work Order Number: 19K0437
Enclosed are results of analyses for samples received by the laboratory on November 6, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 42
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 7
Sample Results 8
19K0437-01 8
19K0437-02 10
19K0437-03 12
19K0437-04 14
19K0437-05 16
19K0437-06 18
19K0437-07 20
19K0437-08 22
19K0437-09 24
19K0437-10 26
19K0437-11 28
Sample Preparation Information 30
QC Data 31
Volatile Organic Compounds by GC/MS 31
B245494 31
Flag/Qualifier Summary 36
Certifications 37
Chain of Custody/Sample Receipt 39
Page 2 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
11/12/2019
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
ATTN: Matt Gillis
49:1503 f
19K0437
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Wade, NC
field blank 19K0437-01 Field Blank SM21-22 6200B
MW-6 19K0437-02 Ground Water SM21-22 6200B
MW-5 19K0437-03 Ground Water SM21-22 6200B
MW-4 19K0437-04 Ground Water SM21-22 6200B
MW-3 19K0437-05 Ground Water SM21-22 6200B
MW-2 19K0437-06 Ground Water SM21-22 6200B
MW-1 19K0437-07 Ground Water SM21-22 6200B
MW-2D 19K0437-08 Ground Water SM21-22 6200B
SW-5 19K0437-09 Ground Water SM21-22 6200B
SW-4 19K0437-10 Ground Water SM21-22 6200B
SW-6 19K0437-11 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:19K0437-02MW-6
No Results Detected
Client ID:Lab ID:19K0437-07MW-1
No Results Detected
Client ID:Lab ID:19K0437-09SW-5
No Results Detected
Client ID:Lab ID:19K0437-10SW-4
No Results Detected
Client ID:Lab ID:19K0437-11SW-6
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-01field blank
DL
Methylene Chloride 0.43 5.0 g/L SM21-22 6200BJ0.34
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-03MW-5
DL
1,2,4-Trimethylbenzene 1000 10 g/L SM21-22 6200B3.6
1,3,5-Trimethylbenzene 240 10 g/L SM21-22 6200B2.8
2-Butanone (MEK)66 100 g/L SM21-22 6200BJ39
Ethylbenzene 1900 10 g/L SM21-22 6200B2.6
Isopropylbenzene (Cumene)60 10 g/L SM21-22 6200B3.4
m+p Xylene 6000 20 g/L SM21-22 6200B6.0
Naphthalene 310 100 g/L SM21-22 6200B6.2
n-Butylbenzene 9.6 10 g/L SM21-22 6200BJ4.2
n-Propylbenzene 140 10 g/L SM21-22 6200B2.6
o-Xylene 3400 10 g/L SM21-22 6200B3.4
sec-Butylbenzene 7.0 10 g/L SM21-22 6200BJ3.2
Styrene 9.6 10 g/L SM21-22 6200BJ2.2
Toluene 440 10 g/L SM21-22 6200B2.8
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-04MW-4
DL
Acetone 17 50 g/L SM21-22 6200BL-06, J 3.8
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-05MW-3
DL
1,2,4-Trimethylbenzene 1400 50 g/L SM21-22 6200B18
1,3,5-Trimethylbenzene 370 50 g/L SM21-22 6200B14
Ethylbenzene 900 50 g/L SM21-22 6200B13
Isopropylbenzene (Cumene)68 50 g/L SM21-22 6200B17
m+p Xylene 3100 100 g/L SM21-22 6200B30
Naphthalene 730 500 g/L SM21-22 6200B31
n-Butylbenzene 40 50 g/L SM21-22 6200BJ21
n-Propylbenzene 220 50 g/L SM21-22 6200B13
o-Xylene 1400 50 g/L SM21-22 6200B17
sec-Butylbenzene 27 50 g/L SM21-22 6200BJ16
Toluene 1000 50 g/L SM21-22 6200B14
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-06MW-2
DL
1,2,4-Trimethylbenzene 410 10 g/L SM21-22 6200B3.6
1,3,5-Trimethylbenzene 95 10 g/L SM21-22 6200B2.8
2-Butanone (MEK)60 100 g/L SM21-22 6200BJ39
Ethylbenzene 360 10 g/L SM21-22 6200B2.6
Isopropylbenzene (Cumene)30 10 g/L SM21-22 6200B3.4
m+p Xylene 1100 20 g/L SM21-22 6200B6.0
Naphthalene 160 100 g/L SM21-22 6200B6.2
n-Butylbenzene 11 10 g/L SM21-22 6200B4.2
n-Propylbenzene 83 10 g/L SM21-22 6200B2.6
o-Xylene 580 10 g/L SM21-22 6200B3.4
sec-Butylbenzene 6.4 10 g/L SM21-22 6200BJ3.2
Toluene 440 10 g/L SM21-22 6200B2.8
Page 5 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-08MW-2D
DL
1,2,4-Trimethylbenzene 30 1.0 g/L SM21-22 6200B0.36
1,3,5-Trimethylbenzene 5.5 1.0 g/L SM21-22 6200B0.28
Ethylbenzene 100 1.0 g/L SM21-22 6200B0.26
Isopropylbenzene (Cumene)9.4 1.0 g/L SM21-22 6200B0.34
m+p Xylene 21 2.0 g/L SM21-22 6200B0.60
Naphthalene 29 10 g/L SM21-22 6200B0.62
n-Butylbenzene 2.1 1.0 g/L SM21-22 6200B0.42
n-Propylbenzene 24 1.0 g/L SM21-22 6200B0.26
o-Xylene 22 1.0 g/L SM21-22 6200B0.34
p-Isopropyltoluene (p-Cymene)0.60 1.0 g/L SM21-22 6200BJ0.40
sec-Butylbenzene 1.6 1.0 g/L SM21-22 6200B0.32
Toluene 1.2 1.0 g/L SM21-22 6200B0.28
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 6 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limits for samples 19K0437-03,05,06+08 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
2-Hexanone (MBK)
B245494-BS1, B245494-BSD1
4-Methyl-2-pentanone (MIBK)
B245494-BS1, B245494-BSD1
Ethanol
B245494-BS1, B245494-BSD1
Vinyl Chloride
B245494-BS1, B245494-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the high side.
Analyte & Samples(s) Qualified:
L-06
Acetone
19K0437-04[MW-4], B245494-BS1, B245494-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
tert-Amyl Methyl Ether (TAME)
B245494-BS1
tert-Butyl Alcohol (TBA)
B245494-BSD1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
19K0437-03[MW-5], 19K0437-05[MW-3], 19K0437-06[MW-2], 19K0437-08[MW-2D]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-01
Field Sample #: field blank
Sample Matrix: Field Blank
Sampled: 11/5/2019 10:32
[TOC_2]19K0437-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 2:48 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 2:48 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 2:48 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 2:48 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 2:48 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 2:48 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 2:48 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 2:48 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 2:48 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 2:48 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 2:48 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 2:48 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 2:48 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 2:48 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 2:48 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 2:48 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 2:48 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 2:48 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 2:48 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 2:48 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 2:48 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 2:48 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
0.43 5.0 11/9/19 2:48 EEHg/L0.34 11/8/19SM21-22 6200B1JMethylene Chloride
ND 5.0 11/9/19 2:48 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-01
Field Sample #: field blank
Sample Matrix: Field Blank
Sampled: 11/5/2019 10:32
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 2:48 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 2:48 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 2:48 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 2:48 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 2:48 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 2:48 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 2:48 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 2:48 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 11/9/19 2:4870-130
Toluene-d8 101 11/9/19 2:4870-130
4-Bromofluorobenzene 92.8 11/9/19 2:4870-130
Page 9 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-02
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 11/5/2019 10:40
[TOC_2]19K0437-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 3:45 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 3:45 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 3:45 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 3:45 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 3:45 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 3:45 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 3:45 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 3:45 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 3:45 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 3:45 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 3:45 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 3:45 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 3:45 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 3:45 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 3:45 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 3:45 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 3:45 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 3:45 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 3:45 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 3:45 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 3:45 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 3:45 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 3:45 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 3:45 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 10 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-02
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 11/5/2019 10:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 3:45 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 3:45 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 3:45 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 3:45 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 3:45 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 3:45 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 3:45 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 3:45 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 11/9/19 3:4570-130
Toluene-d8 101 11/9/19 3:4570-130
4-Bromofluorobenzene 95.9 11/9/19 3:4570-130
Page 11 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-03
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 11/5/2019 10:52
[TOC_2]19K0437-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 1000 11/9/19 10:00 EEHg/L76 11/8/19SM21-22 6200B20Acetone
ND 10 11/9/19 10:00 EEHg/L3.6 11/8/19SM21-22 6200B20Benzene
ND 10 11/9/19 10:00 EEHg/L3.0 11/8/19SM21-22 6200B20Bromobenzene
ND 10 11/9/19 10:00 EEHg/L6.4 11/8/19SM21-22 6200B20Bromochloromethane
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B20Bromodichloromethane
ND 10 11/9/19 10:00 EEHg/L9.2 11/8/19SM21-22 6200B20Bromoform
ND 20 11/9/19 10:00 EEHg/L16 11/8/19SM21-22 6200B20Bromomethane
66 100 11/9/19 10:00 EEHg/L39 11/8/19SM21-22 6200B20J2-Butanone (MEK)
9.6 10 11/9/19 10:00 EEHg/L4.2 11/8/19SM21-22 6200B20Jn-Butylbenzene
7.0 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B20Jsec-Butylbenzene
ND 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20tert-Butylbenzene
ND 10 11/9/19 10:00 EEHg/L2.2 11/8/19SM21-22 6200B20Carbon Tetrachloride
ND 10 11/9/19 10:00 EEHg/L3.0 11/8/19SM21-22 6200B20Chlorobenzene
ND 1000 11/9/19 10:00 EEHg/L210 11/8/19SM21-22 6200B20Ethanol
ND 10 11/9/19 10:00 EEHg/L4.2 11/8/19SM21-22 6200B20Chlorodibromomethane
ND 10 11/9/19 10:00 EEHg/L7.0 11/8/19SM21-22 6200B20Chloroethane
ND 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20Chloroform
ND 20 11/9/19 10:00 EEHg/L9.0 11/8/19SM21-22 6200B20Chloromethane
ND 10 11/9/19 10:00 EEHg/L2.4 11/8/19SM21-22 6200B202-Chlorotoluene
ND 10 11/9/19 10:00 EEHg/L2.8 11/8/19SM21-22 6200B204-Chlorotoluene
ND 10 11/9/19 10:00 EEHg/L3.8 11/8/19SM21-22 6200B201,2-Dibromoethane (EDB)
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B201,2-Dichlorobenzene
ND 10 11/9/19 10:00 EEHg/L2.4 11/8/19SM21-22 6200B201,3-Dichlorobenzene
ND 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B201,4-Dichlorobenzene
ND 10 11/9/19 10:00 EEHg/L5.2 11/8/19SM21-22 6200B20Dichlorodifluoromethane (Freon 12)
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B201,1-Dichloroethane
ND 20 11/9/19 10:00 EEHg/L8.2 11/8/19SM21-22 6200B201,2-Dichloroethane
ND 10 11/9/19 10:00 EEHg/L6.4 11/8/19SM21-22 6200B201,1-Dichloroethylene
ND 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B20cis-1,2-Dichloroethylene
ND 10 11/9/19 10:00 EEHg/L6.2 11/8/19SM21-22 6200B20trans-1,2-Dichloroethylene
ND 10 11/9/19 10:00 EEHg/L4.0 11/8/19SM21-22 6200B201,2-Dichloropropane
ND 10 11/9/19 10:00 EEHg/L2.2 11/8/19SM21-22 6200B201,3-Dichloropropane
ND 10 11/9/19 10:00 EEHg/L4.0 11/8/19SM21-22 6200B202,2-Dichloropropane
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B201,1-Dichloropropene
ND 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B20cis-1,3-Dichloropropene
ND 10 11/9/19 10:00 EEHg/L4.6 11/8/19SM21-22 6200B20trans-1,3-Dichloropropene
ND 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20Diisopropyl Ether (DIPE)
1900 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B20Ethylbenzene
ND 100 11/9/19 10:00 EEHg/L30 11/8/19SM21-22 6200B202-Hexanone (MBK)
60 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20Isopropylbenzene (Cumene)
ND 10 11/9/19 10:00 EEHg/L4.0 11/8/19SM21-22 6200B20p-Isopropyltoluene (p-Cymene)
ND 10 11/9/19 10:00 EEHg/L5.0 11/8/19SM21-22 6200B20Methyl tert-Butyl Ether (MTBE)
ND 100 11/9/19 10:00 EEHg/L6.8 11/8/19SM21-22 6200B20Methylene Chloride
ND 100 11/9/19 10:00 EEHg/L33 11/8/19SM21-22 6200B204-Methyl-2-pentanone (MIBK)
Page 12 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-03
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 11/5/2019 10:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
310 100 11/9/19 10:00 EEHg/L6.2 11/8/19SM21-22 6200B20Naphthalene
140 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B20n-Propylbenzene
9.6 10 11/9/19 10:00 EEHg/L2.2 11/8/19SM21-22 6200B20JStyrene
ND 10 11/9/19 10:00 EEHg/L4.4 11/8/19SM21-22 6200B201,1,2,2-Tetrachloroethane
ND 10 11/9/19 10:00 EEHg/L3.6 11/8/19SM21-22 6200B20Tetrachloroethylene
440 10 11/9/19 10:00 EEHg/L2.8 11/8/19SM21-22 6200B20Toluene
ND 40 11/9/19 10:00 EEHg/L11 11/8/19SM21-22 6200B201,2,3-Trichlorobenzene
ND 10 11/9/19 10:00 EEHg/L8.0 11/8/19SM21-22 6200B201,2,4-Trichlorobenzene
ND 10 11/9/19 10:00 EEHg/L4.0 11/8/19SM21-22 6200B201,1,1-Trichloroethane
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B201,1,2-Trichloroethane
ND 10 11/9/19 10:00 EEHg/L4.8 11/8/19SM21-22 6200B20Trichloroethylene
ND 10 11/9/19 10:00 EEHg/L6.6 11/8/19SM21-22 6200B20Trichlorofluoromethane (Freon 11)
ND 10 11/9/19 10:00 EEHg/L5.0 11/8/19SM21-22 6200B201,2,3-Trichloropropane
1000 10 11/9/19 10:00 EEHg/L3.6 11/8/19SM21-22 6200B201,2,4-Trimethylbenzene
240 10 11/9/19 10:00 EEHg/L2.8 11/8/19SM21-22 6200B201,3,5-Trimethylbenzene
ND 400 11/9/19 10:00 EEHg/L200 11/8/19SM21-22 6200B20Vinyl Acetate
ND 10 11/9/19 10:00 EEHg/L9.0 11/8/19SM21-22 6200B20Vinyl Chloride
6000 20 11/9/19 10:00 EEHg/L6.0 11/8/19SM21-22 6200B20m+p Xylene
3400 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 111 11/9/19 10:0070-130
Toluene-d8 102 11/9/19 10:0070-130
4-Bromofluorobenzene 95.1 11/9/19 10:0070-130
Page 13 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-04
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:02
[TOC_2]19K0437-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
17 50 11/9/19 4:14 EEHg/L3.8 11/8/19SM21-22 6200B1L-06, JAcetone
ND 0.50 11/9/19 4:14 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 4:14 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 4:14 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 4:14 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 4:14 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 4:14 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 4:14 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 4:14 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 4:14 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 4:14 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 4:14 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 4:14 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 4:14 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 4:14 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 4:14 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 4:14 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 4:14 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 4:14 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 4:14 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 4:14 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 4:14 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 4:14 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 4:14 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 14 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-04
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:02
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 4:14 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 4:14 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 4:14 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 4:14 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 4:14 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 4:14 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 4:14 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 4:14 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 11/9/19 4:1470-130
Toluene-d8 100 11/9/19 4:1470-130
4-Bromofluorobenzene 94.6 11/9/19 4:1470-130
Page 15 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-05
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:13
[TOC_2]19K0437-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 5000 11/9/19 10:28 EEHg/L380 11/8/19SM21-22 6200B100Acetone
ND 50 11/9/19 10:28 EEHg/L18 11/8/19SM21-22 6200B100Benzene
ND 50 11/9/19 10:28 EEHg/L15 11/8/19SM21-22 6200B100Bromobenzene
ND 50 11/9/19 10:28 EEHg/L32 11/8/19SM21-22 6200B100Bromochloromethane
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B100Bromodichloromethane
ND 50 11/9/19 10:28 EEHg/L46 11/8/19SM21-22 6200B100Bromoform
ND 100 11/9/19 10:28 EEHg/L78 11/8/19SM21-22 6200B100Bromomethane
ND 500 11/9/19 10:28 EEHg/L190 11/8/19SM21-22 6200B1002-Butanone (MEK)
40 50 11/9/19 10:28 EEHg/L21 11/8/19SM21-22 6200B100Jn-Butylbenzene
27 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B100Jsec-Butylbenzene
ND 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100tert-Butylbenzene
ND 50 11/9/19 10:28 EEHg/L11 11/8/19SM21-22 6200B100Carbon Tetrachloride
ND 50 11/9/19 10:28 EEHg/L15 11/8/19SM21-22 6200B100Chlorobenzene
ND 5000 11/9/19 10:28 EEHg/L1100 11/8/19SM21-22 6200B100Ethanol
ND 50 11/9/19 10:28 EEHg/L21 11/8/19SM21-22 6200B100Chlorodibromomethane
ND 50 11/9/19 10:28 EEHg/L35 11/8/19SM21-22 6200B100Chloroethane
ND 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100Chloroform
ND 100 11/9/19 10:28 EEHg/L45 11/8/19SM21-22 6200B100Chloromethane
ND 50 11/9/19 10:28 EEHg/L12 11/8/19SM21-22 6200B1002-Chlorotoluene
ND 50 11/9/19 10:28 EEHg/L14 11/8/19SM21-22 6200B1004-Chlorotoluene
ND 50 11/9/19 10:28 EEHg/L19 11/8/19SM21-22 6200B1001,2-Dibromoethane (EDB)
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B1001,2-Dichlorobenzene
ND 50 11/9/19 10:28 EEHg/L12 11/8/19SM21-22 6200B1001,3-Dichlorobenzene
ND 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B1001,4-Dichlorobenzene
ND 50 11/9/19 10:28 EEHg/L26 11/8/19SM21-22 6200B100Dichlorodifluoromethane (Freon 12)
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B1001,1-Dichloroethane
ND 100 11/9/19 10:28 EEHg/L41 11/8/19SM21-22 6200B1001,2-Dichloroethane
ND 50 11/9/19 10:28 EEHg/L32 11/8/19SM21-22 6200B1001,1-Dichloroethylene
ND 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B100cis-1,2-Dichloroethylene
ND 50 11/9/19 10:28 EEHg/L31 11/8/19SM21-22 6200B100trans-1,2-Dichloroethylene
ND 50 11/9/19 10:28 EEHg/L20 11/8/19SM21-22 6200B1001,2-Dichloropropane
ND 50 11/9/19 10:28 EEHg/L11 11/8/19SM21-22 6200B1001,3-Dichloropropane
ND 50 11/9/19 10:28 EEHg/L20 11/8/19SM21-22 6200B1002,2-Dichloropropane
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B1001,1-Dichloropropene
ND 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B100cis-1,3-Dichloropropene
ND 50 11/9/19 10:28 EEHg/L23 11/8/19SM21-22 6200B100trans-1,3-Dichloropropene
ND 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100Diisopropyl Ether (DIPE)
900 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B100Ethylbenzene
ND 500 11/9/19 10:28 EEHg/L150 11/8/19SM21-22 6200B1002-Hexanone (MBK)
68 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100Isopropylbenzene (Cumene)
ND 50 11/9/19 10:28 EEHg/L20 11/8/19SM21-22 6200B100p-Isopropyltoluene (p-Cymene)
ND 50 11/9/19 10:28 EEHg/L25 11/8/19SM21-22 6200B100Methyl tert-Butyl Ether (MTBE)
ND 500 11/9/19 10:28 EEHg/L34 11/8/19SM21-22 6200B100Methylene Chloride
ND 500 11/9/19 10:28 EEHg/L170 11/8/19SM21-22 6200B1004-Methyl-2-pentanone (MIBK)
Page 16 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-05
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:13
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
730 500 11/9/19 10:28 EEHg/L31 11/8/19SM21-22 6200B100Naphthalene
220 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B100n-Propylbenzene
ND 50 11/9/19 10:28 EEHg/L11 11/8/19SM21-22 6200B100Styrene
ND 50 11/9/19 10:28 EEHg/L22 11/8/19SM21-22 6200B1001,1,2,2-Tetrachloroethane
ND 50 11/9/19 10:28 EEHg/L18 11/8/19SM21-22 6200B100Tetrachloroethylene
1000 50 11/9/19 10:28 EEHg/L14 11/8/19SM21-22 6200B100Toluene
ND 200 11/9/19 10:28 EEHg/L57 11/8/19SM21-22 6200B1001,2,3-Trichlorobenzene
ND 50 11/9/19 10:28 EEHg/L40 11/8/19SM21-22 6200B1001,2,4-Trichlorobenzene
ND 50 11/9/19 10:28 EEHg/L20 11/8/19SM21-22 6200B1001,1,1-Trichloroethane
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B1001,1,2-Trichloroethane
ND 50 11/9/19 10:28 EEHg/L24 11/8/19SM21-22 6200B100Trichloroethylene
ND 50 11/9/19 10:28 EEHg/L33 11/8/19SM21-22 6200B100Trichlorofluoromethane (Freon 11)
ND 50 11/9/19 10:28 EEHg/L25 11/8/19SM21-22 6200B1001,2,3-Trichloropropane
1400 50 11/9/19 10:28 EEHg/L18 11/8/19SM21-22 6200B1001,2,4-Trimethylbenzene
370 50 11/9/19 10:28 EEHg/L14 11/8/19SM21-22 6200B1001,3,5-Trimethylbenzene
ND 2000 11/9/19 10:28 EEHg/L1000 11/8/19SM21-22 6200B100Vinyl Acetate
ND 50 11/9/19 10:28 EEHg/L45 11/8/19SM21-22 6200B100Vinyl Chloride
3100 100 11/9/19 10:28 EEHg/L30 11/8/19SM21-22 6200B100m+p Xylene
1400 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 109 11/9/19 10:2870-130
Toluene-d8 99.5 11/9/19 10:2870-130
4-Bromofluorobenzene 93.3 11/9/19 10:2870-130
Page 17 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-06
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:23
[TOC_2]19K0437-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 1000 11/9/19 10:57 EEHg/L76 11/8/19SM21-22 6200B20Acetone
ND 10 11/9/19 10:57 EEHg/L3.6 11/8/19SM21-22 6200B20Benzene
ND 10 11/9/19 10:57 EEHg/L3.0 11/8/19SM21-22 6200B20Bromobenzene
ND 10 11/9/19 10:57 EEHg/L6.4 11/8/19SM21-22 6200B20Bromochloromethane
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B20Bromodichloromethane
ND 10 11/9/19 10:57 EEHg/L9.2 11/8/19SM21-22 6200B20Bromoform
ND 20 11/9/19 10:57 EEHg/L16 11/8/19SM21-22 6200B20Bromomethane
60 100 11/9/19 10:57 EEHg/L39 11/8/19SM21-22 6200B20J2-Butanone (MEK)
11 10 11/9/19 10:57 EEHg/L4.2 11/8/19SM21-22 6200B20n-Butylbenzene
6.4 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B20Jsec-Butylbenzene
ND 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20tert-Butylbenzene
ND 10 11/9/19 10:57 EEHg/L2.2 11/8/19SM21-22 6200B20Carbon Tetrachloride
ND 10 11/9/19 10:57 EEHg/L3.0 11/8/19SM21-22 6200B20Chlorobenzene
ND 1000 11/9/19 10:57 EEHg/L210 11/8/19SM21-22 6200B20Ethanol
ND 10 11/9/19 10:57 EEHg/L4.2 11/8/19SM21-22 6200B20Chlorodibromomethane
ND 10 11/9/19 10:57 EEHg/L7.0 11/8/19SM21-22 6200B20Chloroethane
ND 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20Chloroform
ND 20 11/9/19 10:57 EEHg/L9.0 11/8/19SM21-22 6200B20Chloromethane
ND 10 11/9/19 10:57 EEHg/L2.4 11/8/19SM21-22 6200B202-Chlorotoluene
ND 10 11/9/19 10:57 EEHg/L2.8 11/8/19SM21-22 6200B204-Chlorotoluene
ND 10 11/9/19 10:57 EEHg/L3.8 11/8/19SM21-22 6200B201,2-Dibromoethane (EDB)
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B201,2-Dichlorobenzene
ND 10 11/9/19 10:57 EEHg/L2.4 11/8/19SM21-22 6200B201,3-Dichlorobenzene
ND 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B201,4-Dichlorobenzene
ND 10 11/9/19 10:57 EEHg/L5.2 11/8/19SM21-22 6200B20Dichlorodifluoromethane (Freon 12)
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B201,1-Dichloroethane
ND 20 11/9/19 10:57 EEHg/L8.2 11/8/19SM21-22 6200B201,2-Dichloroethane
ND 10 11/9/19 10:57 EEHg/L6.4 11/8/19SM21-22 6200B201,1-Dichloroethylene
ND 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B20cis-1,2-Dichloroethylene
ND 10 11/9/19 10:57 EEHg/L6.2 11/8/19SM21-22 6200B20trans-1,2-Dichloroethylene
ND 10 11/9/19 10:57 EEHg/L4.0 11/8/19SM21-22 6200B201,2-Dichloropropane
ND 10 11/9/19 10:57 EEHg/L2.2 11/8/19SM21-22 6200B201,3-Dichloropropane
ND 10 11/9/19 10:57 EEHg/L4.0 11/8/19SM21-22 6200B202,2-Dichloropropane
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B201,1-Dichloropropene
ND 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B20cis-1,3-Dichloropropene
ND 10 11/9/19 10:57 EEHg/L4.6 11/8/19SM21-22 6200B20trans-1,3-Dichloropropene
ND 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20Diisopropyl Ether (DIPE)
360 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B20Ethylbenzene
ND 100 11/9/19 10:57 EEHg/L30 11/8/19SM21-22 6200B202-Hexanone (MBK)
30 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20Isopropylbenzene (Cumene)
ND 10 11/9/19 10:57 EEHg/L4.0 11/8/19SM21-22 6200B20p-Isopropyltoluene (p-Cymene)
ND 10 11/9/19 10:57 EEHg/L5.0 11/8/19SM21-22 6200B20Methyl tert-Butyl Ether (MTBE)
ND 100 11/9/19 10:57 EEHg/L6.8 11/8/19SM21-22 6200B20Methylene Chloride
ND 100 11/9/19 10:57 EEHg/L33 11/8/19SM21-22 6200B204-Methyl-2-pentanone (MIBK)
Page 18 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-06
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:23
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
160 100 11/9/19 10:57 EEHg/L6.2 11/8/19SM21-22 6200B20Naphthalene
83 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B20n-Propylbenzene
ND 10 11/9/19 10:57 EEHg/L2.2 11/8/19SM21-22 6200B20Styrene
ND 10 11/9/19 10:57 EEHg/L4.4 11/8/19SM21-22 6200B201,1,2,2-Tetrachloroethane
ND 10 11/9/19 10:57 EEHg/L3.6 11/8/19SM21-22 6200B20Tetrachloroethylene
440 10 11/9/19 10:57 EEHg/L2.8 11/8/19SM21-22 6200B20Toluene
ND 40 11/9/19 10:57 EEHg/L11 11/8/19SM21-22 6200B201,2,3-Trichlorobenzene
ND 10 11/9/19 10:57 EEHg/L8.0 11/8/19SM21-22 6200B201,2,4-Trichlorobenzene
ND 10 11/9/19 10:57 EEHg/L4.0 11/8/19SM21-22 6200B201,1,1-Trichloroethane
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B201,1,2-Trichloroethane
ND 10 11/9/19 10:57 EEHg/L4.8 11/8/19SM21-22 6200B20Trichloroethylene
ND 10 11/9/19 10:57 EEHg/L6.6 11/8/19SM21-22 6200B20Trichlorofluoromethane (Freon 11)
ND 10 11/9/19 10:57 EEHg/L5.0 11/8/19SM21-22 6200B201,2,3-Trichloropropane
410 10 11/9/19 10:57 EEHg/L3.6 11/8/19SM21-22 6200B201,2,4-Trimethylbenzene
95 10 11/9/19 10:57 EEHg/L2.8 11/8/19SM21-22 6200B201,3,5-Trimethylbenzene
ND 400 11/9/19 10:57 EEHg/L200 11/8/19SM21-22 6200B20Vinyl Acetate
ND 10 11/9/19 10:57 EEHg/L9.0 11/8/19SM21-22 6200B20Vinyl Chloride
1100 20 11/9/19 10:57 EEHg/L6.0 11/8/19SM21-22 6200B20m+p Xylene
580 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 113 11/9/19 10:5770-130
Toluene-d8 100 11/9/19 10:5770-130
4-Bromofluorobenzene 96.8 11/9/19 10:5770-130
Page 19 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:32
[TOC_2]19K0437-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 4:43 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 4:43 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 4:43 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 4:43 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 4:43 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 4:43 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 4:43 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 4:43 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 4:43 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 4:43 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 4:43 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 4:43 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 4:43 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 4:43 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 4:43 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 4:43 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 4:43 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 4:43 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 4:43 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 4:43 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 4:43 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 4:43 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 4:43 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 4:43 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 20 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:32
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 4:43 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 4:43 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 4:43 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 4:43 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 4:43 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 4:43 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 4:43 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 4:43 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 11/9/19 4:4370-130
Toluene-d8 101 11/9/19 4:4370-130
4-Bromofluorobenzene 93.2 11/9/19 4:4370-130
Page 21 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-08
Field Sample #: MW-2D
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:47
[TOC_2]19K0437-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 100 11/9/19 9:31 EEHg/L7.6 11/8/19SM21-22 6200B2Acetone
ND 1.0 11/9/19 9:31 EEHg/L0.36 11/8/19SM21-22 6200B2Benzene
ND 1.0 11/9/19 9:31 EEHg/L0.30 11/8/19SM21-22 6200B2Bromobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.64 11/8/19SM21-22 6200B2Bromochloromethane
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B2Bromodichloromethane
ND 1.0 11/9/19 9:31 EEHg/L0.92 11/8/19SM21-22 6200B2Bromoform
ND 2.0 11/9/19 9:31 EEHg/L1.6 11/8/19SM21-22 6200B2Bromomethane
ND 10 11/9/19 9:31 EEHg/L3.9 11/8/19SM21-22 6200B22-Butanone (MEK)
2.1 1.0 11/9/19 9:31 EEHg/L0.42 11/8/19SM21-22 6200B2n-Butylbenzene
1.6 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B2sec-Butylbenzene
ND 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2tert-Butylbenzene
ND 1.0 11/9/19 9:31 EEHg/L0.22 11/8/19SM21-22 6200B2Carbon Tetrachloride
ND 1.0 11/9/19 9:31 EEHg/L0.30 11/8/19SM21-22 6200B2Chlorobenzene
ND 100 11/9/19 9:31 EEHg/L21 11/8/19SM21-22 6200B2Ethanol
ND 1.0 11/9/19 9:31 EEHg/L0.42 11/8/19SM21-22 6200B2Chlorodibromomethane
ND 1.0 11/9/19 9:31 EEHg/L0.70 11/8/19SM21-22 6200B2Chloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2Chloroform
ND 2.0 11/9/19 9:31 EEHg/L0.90 11/8/19SM21-22 6200B2Chloromethane
ND 1.0 11/9/19 9:31 EEHg/L0.24 11/8/19SM21-22 6200B22-Chlorotoluene
ND 1.0 11/9/19 9:31 EEHg/L0.28 11/8/19SM21-22 6200B24-Chlorotoluene
ND 1.0 11/9/19 9:31 EEHg/L0.38 11/8/19SM21-22 6200B21,2-Dibromoethane (EDB)
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B21,2-Dichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.24 11/8/19SM21-22 6200B21,3-Dichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B21,4-Dichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.52 11/8/19SM21-22 6200B2Dichlorodifluoromethane (Freon 12)
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B21,1-Dichloroethane
ND 2.0 11/9/19 9:31 EEHg/L0.82 11/8/19SM21-22 6200B21,2-Dichloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.64 11/8/19SM21-22 6200B21,1-Dichloroethylene
ND 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B2cis-1,2-Dichloroethylene
ND 1.0 11/9/19 9:31 EEHg/L0.62 11/8/19SM21-22 6200B2trans-1,2-Dichloroethylene
ND 1.0 11/9/19 9:31 EEHg/L0.40 11/8/19SM21-22 6200B21,2-Dichloropropane
ND 1.0 11/9/19 9:31 EEHg/L0.22 11/8/19SM21-22 6200B21,3-Dichloropropane
ND 1.0 11/9/19 9:31 EEHg/L0.40 11/8/19SM21-22 6200B22,2-Dichloropropane
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B21,1-Dichloropropene
ND 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B2cis-1,3-Dichloropropene
ND 1.0 11/9/19 9:31 EEHg/L0.46 11/8/19SM21-22 6200B2trans-1,3-Dichloropropene
ND 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2Diisopropyl Ether (DIPE)
100 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B2Ethylbenzene
ND 10 11/9/19 9:31 EEHg/L3.0 11/8/19SM21-22 6200B22-Hexanone (MBK)
9.4 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2Isopropylbenzene (Cumene)
0.60 1.0 11/9/19 9:31 EEHg/L0.40 11/8/19SM21-22 6200B2Jp-Isopropyltoluene (p-Cymene)
ND 1.0 11/9/19 9:31 EEHg/L0.50 11/8/19SM21-22 6200B2Methyl tert-Butyl Ether (MTBE)
ND 10 11/9/19 9:31 EEHg/L0.68 11/8/19SM21-22 6200B2Methylene Chloride
ND 10 11/9/19 9:31 EEHg/L3.3 11/8/19SM21-22 6200B24-Methyl-2-pentanone (MIBK)
Page 22 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-08
Field Sample #: MW-2D
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:47
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
29 10 11/9/19 9:31 EEHg/L0.62 11/8/19SM21-22 6200B2Naphthalene
24 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B2n-Propylbenzene
ND 1.0 11/9/19 9:31 EEHg/L0.22 11/8/19SM21-22 6200B2Styrene
ND 1.0 11/9/19 9:31 EEHg/L0.44 11/8/19SM21-22 6200B21,1,2,2-Tetrachloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.36 11/8/19SM21-22 6200B2Tetrachloroethylene
1.2 1.0 11/9/19 9:31 EEHg/L0.28 11/8/19SM21-22 6200B2Toluene
ND 4.0 11/9/19 9:31 EEHg/L1.1 11/8/19SM21-22 6200B21,2,3-Trichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.80 11/8/19SM21-22 6200B21,2,4-Trichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.40 11/8/19SM21-22 6200B21,1,1-Trichloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B21,1,2-Trichloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.48 11/8/19SM21-22 6200B2Trichloroethylene
ND 1.0 11/9/19 9:31 EEHg/L0.66 11/8/19SM21-22 6200B2Trichlorofluoromethane (Freon 11)
ND 1.0 11/9/19 9:31 EEHg/L0.50 11/8/19SM21-22 6200B21,2,3-Trichloropropane
30 1.0 11/9/19 9:31 EEHg/L0.36 11/8/19SM21-22 6200B21,2,4-Trimethylbenzene
5.5 1.0 11/9/19 9:31 EEHg/L0.28 11/8/19SM21-22 6200B21,3,5-Trimethylbenzene
ND 40 11/9/19 9:31 EEHg/L20 11/8/19SM21-22 6200B2Vinyl Acetate
ND 1.0 11/9/19 9:31 EEHg/L0.90 11/8/19SM21-22 6200B2Vinyl Chloride
21 2.0 11/9/19 9:31 EEHg/L0.60 11/8/19SM21-22 6200B2m+p Xylene
22 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 11/9/19 9:3170-130
Toluene-d8 101 11/9/19 9:3170-130
4-Bromofluorobenzene 98.6 11/9/19 9:3170-130
Page 23 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-09
Field Sample #: SW-5
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:09
[TOC_2]19K0437-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 5:12 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 5:12 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 5:12 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 5:12 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 5:12 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 5:12 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 5:12 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 5:12 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 5:12 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 5:12 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 5:12 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 5:12 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 5:12 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 5:12 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 5:12 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 5:12 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 5:12 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 5:12 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 5:12 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 5:12 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 5:12 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 5:12 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 5:12 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 5:12 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 24 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-09
Field Sample #: SW-5
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:09
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 5:12 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 5:12 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 5:12 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 5:12 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 5:12 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 5:12 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 5:12 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 5:12 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 11/9/19 5:1270-130
Toluene-d8 99.8 11/9/19 5:1270-130
4-Bromofluorobenzene 94.6 11/9/19 5:1270-130
Page 25 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-10
Field Sample #: SW-4
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:30
[TOC_2]19K0437-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 5:41 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 5:41 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 5:41 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 5:41 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 5:41 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 5:41 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 5:41 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 5:41 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 5:41 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 5:41 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 5:41 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 5:41 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 5:41 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 5:41 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 5:41 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 5:41 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 5:41 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 5:41 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 5:41 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 5:41 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 5:41 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 5:41 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 5:41 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 5:41 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 26 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-10
Field Sample #: SW-4
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 5:41 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 5:41 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 5:41 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 5:41 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 5:41 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 5:41 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 5:41 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 5:41 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 109 11/9/19 5:4170-130
Toluene-d8 101 11/9/19 5:4170-130
4-Bromofluorobenzene 93.0 11/9/19 5:4170-130
Page 27 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-11
Field Sample #: SW-6
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:50
[TOC_2]19K0437-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 6:09 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 6:09 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 6:09 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 6:09 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 6:09 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 6:09 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 6:09 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 6:09 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 6:09 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 6:09 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 6:09 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 6:09 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 6:09 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 6:09 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 6:09 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 6:09 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 6:09 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 6:09 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 6:09 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 6:09 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 6:09 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 6:09 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 6:09 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 6:09 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 28 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-11
Field Sample #: SW-6
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 6:09 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 6:09 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 6:09 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 6:09 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 6:09 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 6:09 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 6:09 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 6:09 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 104 11/9/19 6:0970-130
Toluene-d8 99.8 11/9/19 6:0970-130
4-Bromofluorobenzene 92.4 11/9/19 6:0970-130
Page 29 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B245494 11/08/195 5.0019K0437-01 [field blank]
B245494 11/08/195 5.0019K0437-02 [MW-6]
B245494 11/08/190.25 5.0019K0437-03 [MW-5]
B245494 11/08/195 5.0019K0437-04 [MW-4]
B245494 11/08/190.05 5.0019K0437-05 [MW-3]
B245494 11/08/190.25 5.0019K0437-06 [MW-2]
B245494 11/08/195 5.0019K0437-07 [MW-1]
B245494 11/08/192.5 5.0019K0437-08 [MW-2D]
B245494 11/08/195 5.0019K0437-09 [SW-5]
B245494 11/08/195 5.0019K0437-10 [SW-4]
B245494 11/08/195 5.0019K0437-11 [SW-6]
[TOC_1]Sample Preparation Information[TOC]
Page 30 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B245494 - SW-846 5030B
[TOC_3]B245494[TOC]
Blank (B245494-BLK1) Prepared: 11/08/19 Analyzed: 11/09/19
Acetone g/L50ND
tert-Amyl Methyl Ether (TAME)g/L0.50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
tert-Butyl Alcohol (TBA)g/L20ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
tert-Butyl Ethyl Ether (TBEE)g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 31 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245494 - SW-846 5030B
Blank (B245494-BLK1) Prepared: 11/08/19 Analyzed: 11/09/19
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10927.2
g/L 25.0 70-130Surrogate: Toluene-d8 10125.3
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.224.1
LCS (B245494-BS1) Prepared & Analyzed: 11/08/19
Acetone g/L50 100 L-0670-130138*138
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 L-0770-13066.4 *6.64
Benzene g/L0.50 10.0 70-13095.49.54
Bromobenzene g/L0.50 10.0 70-13010510.5
Bromochloromethane g/L0.50 10.0 70-13011011.0
Bromodichloromethane g/L0.50 10.0 70-13011011.0
Bromoform g/L0.50 10.0 70-13095.39.53
Bromomethane g/L1.0 10.0 60-14011011.0
2-Butanone (MEK)g/L5.0 100 70-130112112
tert-Butyl Alcohol (TBA)g/L20 100 40-130121121
n-Butylbenzene g/L0.50 10.0 70-13011911.9
sec-Butylbenzene g/L0.50 10.0 70-13011711.7
tert-Butylbenzene g/L0.50 10.0 70-13011611.6
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 70-13078.97.89
Carbon Tetrachloride g/L0.50 10.0 70-13010610.6
Chlorobenzene g/L0.50 10.0 70-13010410.4
Ethanol g/L50 100 L-0270-130199*199
Chlorodibromomethane g/L0.50 10.0 70-13010510.5
Chloroethane g/L0.50 10.0 60-14096.69.66
Chloroform g/L0.50 10.0 70-13096.99.69
Chloromethane g/L0.60 10.0 60-14010410.4
2-Chlorotoluene g/L0.50 10.0 70-13010110.1
4-Chlorotoluene g/L0.50 10.0 70-13010610.6
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010310.3
1,2-Dichlorobenzene g/L0.50 10.0 70-13010810.8
1,3-Dichlorobenzene g/L0.50 10.0 70-13010910.9
1,4-Dichlorobenzene g/L0.50 10.0 70-13010710.7
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14081.58.15
1,1-Dichloroethane g/L0.50 10.0 70-13010310.3
1,2-Dichloroethane g/L0.50 10.0 70-13011711.7
1,1-Dichloroethylene g/L0.50 10.0 70-13011411.4
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010810.8
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010710.7
Page 32 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245494 - SW-846 5030B
LCS (B245494-BS1) Prepared & Analyzed: 11/08/19
1,2-Dichloropropane g/L0.50 10.0 70-13010910.9
1,3-Dichloropropane g/L0.50 10.0 70-13010910.9
2,2-Dichloropropane g/L0.50 10.0 70-13093.99.39
1,1-Dichloropropene g/L0.50 10.0 70-13010410.4
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010810.8
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010310.3
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13011711.7
Ethylbenzene g/L0.50 10.0 70-13010810.8
2-Hexanone (MBK)g/L5.0 100 L-0270-130132*132
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011011.0
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011011.0
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13089.78.97
Methylene Chloride g/L5.0 10.0 70-13011711.7
4-Methyl-2-pentanone (MIBK)g/L5.0 100 L-0270-130138*138
Naphthalene g/L0.50 10.0 70-13010810.8
n-Propylbenzene g/L0.50 10.0 70-13011011.0
Styrene g/L0.50 10.0 70-13098.69.86
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010910.9
Tetrachloroethylene g/L0.50 10.0 70-13010810.8
Toluene g/L0.50 10.0 70-13010510.5
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13087.38.73
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13097.79.77
1,1,1-Trichloroethane g/L0.50 10.0 70-13011111.1
1,1,2-Trichloroethane g/L0.50 10.0 70-13010210.2
Trichloroethylene g/L0.50 10.0 70-13011011.0
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13011011.0
1,2,3-Trichloropropane g/L0.50 10.0 70-13011511.5
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011011.0
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010610.6
Vinyl Acetate g/L20 100 70-130104104
Vinyl Chloride g/L0.50 10.0 L-0260-140302*30.2
m+p Xylene g/L1.0 20.0 70-13010721.4
o-Xylene g/L0.50 10.0 70-13010910.9
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10927.3
g/L 25.0 70-130Surrogate: Toluene-d8 10225.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.224.3
LCS Dup (B245494-BSD1) Prepared: 11/08/19 Analyzed: 11/09/19
Acetone g/L50 100 25 L-0670-130154 10.7*154
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 2570-13072.6 8.927.26
Benzene g/L0.50 10.0 2570-13096.6 1.259.66
Bromobenzene g/L0.50 10.0 2570-130107 1.4110.7
Bromochloromethane g/L0.50 10.0 2570-130112 1.5311.2
Bromodichloromethane g/L0.50 10.0 2570-130108 1.1910.8
Bromoform g/L0.50 10.0 2570-130104 9.2110.4
Bromomethane g/L1.0 10.0 2560-140105 4.9410.5
2-Butanone (MEK)g/L5.0 100 2570-130124 9.73124
tert-Butyl Alcohol (TBA)g/L20 100 25 L-0740-130136 11.4*136
n-Butylbenzene g/L0.50 10.0 2570-130114 4.0311.4
sec-Butylbenzene g/L0.50 10.0 2570-130112 4.5511.2
tert-Butylbenzene g/L0.50 10.0 2570-130110 5.3311.0
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 2570-13084.6 6.978.46
Page 33 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245494 - SW-846 5030B
LCS Dup (B245494-BSD1) Prepared: 11/08/19 Analyzed: 11/09/19
Carbon Tetrachloride g/L0.50 10.0 2570-130106 0.28310.6
Chlorobenzene g/L0.50 10.0 2570-130102 2.8110.2
Ethanol g/L50 100 25 L-0270-130203 1.70*203
Chlorodibromomethane g/L0.50 10.0 2570-130104 1.0510.4
Chloroethane g/L0.50 10.0 2560-14098.2 1.649.82
Chloroform g/L0.50 10.0 2570-13098.7 1.849.87
Chloromethane g/L0.60 10.0 2560-14097.3 7.049.73
2-Chlorotoluene g/L0.50 10.0 2570-130102 0.59310.2
4-Chlorotoluene g/L0.50 10.0 2570-130110 3.0511.0
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130104 0.96710.4
1,2-Dichlorobenzene g/L0.50 10.0 2570-130107 0.93010.7
1,3-Dichlorobenzene g/L0.50 10.0 2570-130110 0.45711.0
1,4-Dichlorobenzene g/L0.50 10.0 2570-130106 1.3110.6
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14078.4 3.887.84
1,1-Dichloroethane g/L0.50 10.0 2570-130104 1.2610.4
1,2-Dichloroethane g/L0.50 10.0 2570-130118 0.25511.8
1,1-Dichloroethylene g/L0.50 10.0 2570-130114 0.43911.4
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130107 0.74610.7
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130108 0.46510.8
1,2-Dichloropropane g/L0.50 10.0 2570-130106 2.5110.6
1,3-Dichloropropane g/L0.50 10.0 2570-130109 0.55010.9
2,2-Dichloropropane g/L0.50 10.0 2570-13092.0 2.049.20
1,1-Dichloropropene g/L0.50 10.0 2570-130106 1.3310.6
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130106 2.7110.6
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130107 3.1410.7
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130116 0.86111.6
Ethylbenzene g/L0.50 10.0 2570-130106 2.0610.6
2-Hexanone (MBK)g/L5.0 100 25 L-0270-130152 13.9*152
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130110 0.54611.0
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130107 2.4910.7
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13098.6 9.459.86
Methylene Chloride g/L5.0 10.0 2570-130122 4.1912.2
4-Methyl-2-pentanone (MIBK)g/L5.0 100 25 L-0270-130150 8.49*150
Naphthalene g/L0.50 10.0 2570-130116 7.2511.6
n-Propylbenzene g/L0.50 10.0 2570-130108 1.4710.8
Styrene g/L0.50 10.0 2570-13095.4 3.309.54
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130118 8.2011.8
Tetrachloroethylene g/L0.50 10.0 2570-130104 3.5010.4
Toluene g/L0.50 10.0 2570-130104 1.4310.4
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130107 20.210.7
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130109 10.610.9
1,1,1-Trichloroethane g/L0.50 10.0 2570-130107 3.4910.7
1,1,2-Trichloroethane g/L0.50 10.0 2570-130105 2.8010.5
Trichloroethylene g/L0.50 10.0 2570-130104 5.5910.4
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130109 0.54710.9
1,2,3-Trichloropropane g/L0.50 10.0 2570-130123 6.4612.3
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130104 6.1610.4
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130106 0.18810.6
Vinyl Acetate g/L20 100 2570-130117 11.9117
Vinyl Chloride g/L0.50 10.0 25 L-0260-140269 11.4*26.9
m+p Xylene g/L1.0 20.0 2570-130107 0.23321.4
o-Xylene g/L0.50 10.0 2570-130110 0.91211.0
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245494 - SW-846 5030B
LCS Dup (B245494-BSD1) Prepared: 11/08/19 Analyzed: 11/09/19
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11127.8
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.324.6
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*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the high side.
L-06
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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