15010_Pennston Property_BF Assessment Report _20200221_Final

Via Email

February 21, 2020

NC DOT Geotechnical Unit
GeoEnvironmental Section
1589 Mail Service Center
Raleigh, North Carolina 27699-1589

Attention: Mr. Gordon Box

Re: Brownfields Assessment Report
NC DOT State Project No. R-4707
WBS Element #36599.1.5
Greeensboro, Guilford County, North Carolina
H&H Job No. ROW-603

Dear Gordon:

Please find the attached electronic copy of the Brownfields Assessment report for the Pennston
Brownfields property located in Greensboro, Guilford County, North Carolina. Please return via
DocuSign for final signatures. If you have any questions or need additional information, please
contact us at [phone].

Sincerely,

Hart & Hickman, PC
David Graham, PG Matt Bramblett, PE
Senior Project Geologist Principal

Attachment
#C-1269 Engineering
#-245 Geology

Brownfields Assessment Report
Pennston Property

Brownfields Project # 15010-11-41
Greensboro, Guilford County
North Carolina

H&H Job No. ROW-603
State Project R-4707
WBS Element #36599.1.5
February 21, 2020

i

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
Brownfields Assessment Report
Pennston Property
Greensboro, North Carolina
H&H Project ROW-603

Table of Contents

Section Page No.
1.0 Introduction and Background .............................................................................................. 1 
2.0 Soil Assessment....................................................................................................................... 4 
2.1 Soil Sampling ........................................................................................................................ 4 
2.2 Soil Analytical Results ......................................................................................................... 5 
3.0 Groundwater Assessment ...................................................................................................... 6 
3.1 Groundwater Sampling ......................................................................................................... 6 
3.2 Groundwater Analytical Results ........................................................................................... 7 
4.0 Investigative Derived Waste.................................................................................................. 8 
5.0 Quality Assurance/Quality Control...................................................................................... 9 
6.0 Summary and Regulatory Considerations ........................................................................ 10 
7.0 Signature Page ...................................................................................................................... 12 

ii

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
List of Tables

Table 1 Summary of Well Construction and Water Level Data
Table 2 Soil Analytical Results
Table 3 Groundwater Analytical Results

List of Figures

Figure 1 Project Location Map
Figure 2 Site Map
Figure 3 Soil Analytical Results
Figure 4 Groundwater Analytical Results

List of Appendices

Appendix A NC DOT Preliminary Plan
Appendix B Environmental Documents
Appendix C Soil Boring Logs and Well Construction Records
Appendix D Laboratory Analytical Reports
Appendix E Groundwater Forms
Appendix F Non-Hazardous Waste Disposal Manifests

1

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
Brownfields Assessment Report
Pennston Property
Greensboro North Carolina
H&H Project ROW-603

1.0 Introduction and Background

Hart & Hickman, PC (H&H) has prepared this Brownfields Assessment report documenting
assessment activities performed on the Brownfields property identified as the Pennston Property
(No. 15010-11-41) located at 3600 Reedy Fork Parkway in Greensboro, Guilford County, North
Carolina. This assessment was conducted on behalf of the North Carolina Department of
Transportation (NC DOT) in accordance with H&H’s May 10, 2019 and November 14, 2019 cost
proposals.

The purpose of this assessment was to evaluate the potential for the presence of impacted soil and/or
groundwater in proposed right of way and construction easement areas on the subject Brownfields
property related to proposed road improvements along Reedy Fork Parkway (State Project R-4707).
The Brownfields property encompasses approximately 78 acres of land on five parcels (Guilford
County Parcel Numbers 0219587, 0219588, 0219589, 0084331, and 0083998) that are separated by
Eckerson Road and Reedy Fork Parkway. The proposed NC DOT construction activities will be
conducted on Parcels 0219587, 0219588, 0219589 (also identified as NC DOT Parcels 14, 13, and
15, respectively). The NC DOT project includes proposed road improvements and installation of
storm water drainage piping and catch basins. A site location map is included as Figure 1, and a site
map is presented as Figure 2. NC DOT’s plan sheets depicting Parcels 13, 14, and 15 are included
in Appendix A.

The NC DOT project will require soil (including potentially impacted soil) to be cut and
removed from certain areas in the proposed right of way and construction easements on the
Brownfields property. Information provided by NC DOT indicates over 69,000 cubic yards of
soil will be cut from the Brownfields property during proposed road construction activities. The
road improvement activities will be conducted to the north and south of Reedy Fork Parkway
between the eastern and western boundaries of the Brownfields property (see Figure 2).
2

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc

H&H reviewed previous environmental documents for the Brownfields property including the
Notice of Brownfields Property and Brownfields Agreement (BFA) dated September 23, 2014.
The source area for contamination on the Brownfields property is reported to be the Wysong &
Miles (Wysong) facility. H&H also reviewed Wysong reports prepared by H&H including the
Phase I Remedial Action Plan dated April 15, 2010 and the Off-Site (Pennston Property)
Groundwater Assessment report dated September 15, 2010. Pertinent information from the
environmental documents is included in Appendix B and discussed below.

The Brownfields property is located in a mixed undeveloped, industrial, and residential area of
Greensboro. It consists primarily of undeveloped wooded land with a single-story office building
and asphalt-covered parking area associated with the Reedy Fork Ranch subdivision. The
property will be redeveloped by Reedy Fork Investments, LLC for commercial, retail, and office
use. The property has been wooded and undeveloped since at least 1937, with the exception of
construction of the single-story office building in 2002 on the parcel located east of Eckerson
Road. Groundwater on the Brownfields property is contaminated from a release associated with
the Wysong facility which is located topographically upgradient and southwest of the
Brownfields property. No release of regulated substances is known or suspected to have
occurred on the Brownfields property.

Wysong manufactures metal working machinery and has been in operation since the 1960s. A
release of 1,1,1-trichloroethane (1,1,1-TCA) was discovered at the Wysong facility in 1987.
Multiple assessment activities have been conducted at Wysong including groundwater
assessment activities on the Brownfields property. Nine monitoring wells (TW-1, TW-15, TW-
16, PWR-1, PWR-2, PWR-4, PWR-7, PWR-8, and BR-1) associated with the Wysong release
have been installed on the Brownfields property to date. TW-15 is located within proposed NC
DOT work areas near the intersection of Eckerson Road and Reedy Fork Parkway. Volatile
organic compounds (VOCs), including 1,1,1-TCA, 1,1-dichloroethene (1,1-DCE), 1,1-
dichloroethane, 1,2-dichloroethane, and 1,4-dioxane, have been detected above the 15A NCAC
2L .0202 Groundwater Quality Standards (2L Standards) in groundwater on the Brownfields
property. The depth to groundwater ranges from approximately 23 to 29 ft below ground surface
3

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
(bgs) near proposed DOT work areas. Previously installed monitoring well locations and
historical groundwater data are shown on the Brownfields survey plat in Appendix B.

Certain land use restrictions set forth in the BFA will affect proposed NC DOT road construction
activities. Land use restrictions in the BFA indicate that no activities that encounter, expose
remove, or use groundwater may occur on the Brownfields property without NC DEQ’s written
approval. Soil may not be disturbed on the Brownfields property at a depth greater than 15 ft bgs
without NC DEQ’s written approval. NC DOT plans indicate that soil will be cut to depths near
25 ft bgs on the Brownfields property. Therefore, an Environmental Management Plan (EMP)
will be required for management of soil and groundwater (if encountered) during road
construction activities.

The results of the assessment activities will be used to develop an EMP for proposed road
construction activities and to determine the proper disposition of impacted soil and/or
groundwater if encountered during road construction activities. Information provided by NC
DOT indicates over 69,000 cubic yards of soil will be cut from the Brownfields property during
proposed road construction activities. Of this amount, approximately 10,000 cubic yards in NC
DOT work areas will be cut below 15 ft bgs. The soil to be cut will be managed in accordance
with the EMP.

Based on discussion between H&H, NC DOT, and Joselyn Harriger of the NC DEQ Brownfields
Program, H&H prepared a Brownfields Assessment Work Plan (Revision 1) (Work Plan) dated
October 4, 2019 to describe sampling protocol for assessment of soil and groundwater on the
Brownfields property. The assessment activities in the Work Plan were developed to characterize
soil that is excavated from below 15 ft bgs for potential reuse as fill on the Brownfields property,
to characterize soil for potential off-site disposition, and to evaluate water levels and current
groundwater concentrations for potential management of groundwater during construction
activities. The Work Plan was approved in NCDEQ’s Work Plan Approval Letter dated October
15, 2019.

4

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
As part of assessment activities, five permanent Type II monitoring wells were installed in NC
DOT work areas near Reedy Fork Parkway on the Brownfields property. The assessment
activities were conducted in general accordance with the NC DEQ’s Inactive Hazardous Sites
Branch (IHSB) Guidelines for Assessment and Cleanup (Guidelines) and most recent versions of
the U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem Support
Division (SESD) Field Branches Quality System and Technical Procedures guidance. The
Brownfields assessment activities are described below.

2.0 Soil Assessment

2.1 Soil Sampling

H&H contracted with Innovative Environmental Technologies (IET) of Concord, North Carolina to
advance the monitoring well borings. On November 19 through 21, 2019, five borings SB-1 (MW-
1), SB-2 (MW-2), SB-3 (MW-3), SB-4 (MW-4), and SB-5 (MW-5) were advanced in proposed NC
DOT work areas on the Brownfields property using a direct push technology (DPT) drill rig. Prior
to conducting monitoring well borings, underground utilities were marked by the NC 811 public
utility locator and a private utility locator. Borings were also cleared up to 5 ft bgs by hand auger.

As mentioned above, the BFA indicates that soil may not be disturbed at the site at a depth of
greater than 15 ft bgs without NC DEQ’s prior written approval. NC DOT plans indicate cut depths
below 15 ft on the Brownfields property. The estimated cut depth is approximately 21.5 ft bgs near
SB-1 (MW-1), 24.5 ft bgs near SB-2 (MW-2), 14 ft bgs (plus 3 additional ft for drainage) near SB-3
(MW-3), 18.5 ft bgs (plus 3.5 additional ft for drainage) near SB-4 (MW-4) and 20 ft bgs (plus 3
additional ft for drainage) near SB-5 (MW-5). During the well installations, soil from each boring
was screened for the presence of VOCs with a photoionization detector (PID). Additionally, H&H
observed the soil for visual and olfactory indications of impacts. Based on field screening, there
were no significant indications of impacts in borings advanced at the site. Soil samples were
collected at or near the depths proposed in the work plan. Samples were collected at depths of 15-
16.5 ft in SB-1, 15-17 ft and 22-24 ft in SB-2, 15-17 ft and 17-19 ft in SB-3, 15-17 ft and 19-21 ft in
SB-4, and 15-17 ft and 19-21 ft in SB-5. Due to the depth of hollow stem auger refusal at 16.5 ft
bgs in boring SB-1, only one soil sample was collected below 15 ft bgs in that boring. In lieu of
5

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
collecting two samples from boring SB-1 as proposed in the Work Plan, an additional soil sample
was collected below 15 ft bgs (17-19 ft bgs) in SB-3. Because there were no indications of potential
impacts in the borings based on field screening, no additional soil samples were collected from the
monitoring well borings. GPS coordinate data for the monitoring well borings are presented in
Table 1. Boring locations are shown on Figure 3. Soil boring logs are included in Appendix C.

H&H submitted a total of nine soil samples from the five monitoring well boring locations for
laboratory analysis. The soil samples were placed into laboratory supplied sample containers
using nitrile glove-covered hands. The containers were then labeled as to content, analyses
requested, sample date and time, and sampler’s name. The samples were placed in an iced cooler
upon collection and were subsequently submitted to Pace Analytical Services, LLC (Pace) of
Huntersville, NC for analysis of VOCs using EPA Method 8260, 1,4-dioxane using EPA Method
8260 Select Ion Monitoring (SIM), semi-VOCs (SVOCs) using EPA Method 8270, and RCRA
metals using EPA Methods 6010/7471. Select samples were also analyzed for hexavalent
chromium using EPA Method 7199. Soil sample depths and analytical results are summarized in
Table 2. Laboratory analytical data sheets and chain-of-custody documentation are provided in
Appendix D. The analytical results are discussed below.

2.2 Soil Analytical Results

Concentrations of 1,4-dioxane (0.0047 J mg/kg and 0.014 mg/kg) were detected in soil samples SB-
2 (15-17 ft) and SB-2 (22-24 ft), respectively. The concentration of 1,4-dioxane (0.014 mg/kg) in
SB-2 (22-24 ft) exceeds the NC DEQ Protection of Groundwater (POG) Preliminary Soil
Remediation Goal (PSRG) of 0.012 mg/kg.

Low level metals were detected in each of the samples collected. An elevated selenium
concentration was detected in sample SB-2 (22-24 ft), above the POG PSRG and more than two
times published background values for North Carolina soils. However, the values for North
Carolina are based on a limited data set and concentrations are within the range of published
background values for eastern United States soils (Dragun and Chekiri, 2005). Due to potentially
elevated chromium detections in soil samples SB-2 (22-24 ft) and SB-3 (17-19 ft), these samples
6

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
were also analyzed for hexavalent chromium. A low level detection of hexavalent chromium (0.870
J mg/kg) was detected in SB-3 (17-19 ft). The hexavalent chromium detection exceeds the
Residential PSRG of 0.31 mg/kg. Because there are no known sources of hexavalent chromium at
the site, the hexavalent chromium detection appears to be naturally occurring. No other metals were
detected above their respective PSRGs. H&H considers the other metals detections indicative of
naturally occurring background conditions. No SVOCs were detected above laboratory method
detection limits in soil samples collected at the site.

Based on the above soil sample results, H&H estimates there are roughly 10,000 cubic yards
(15,000 tons) of soil impacted with 1,4-dioxane and hexavalent chromium (near boring SB-3)
between 15 ft and planned NC DOT cut depths on the Brownfields property. The approximate area
of impacted soil is shown on Figure 3.

3.0 Groundwater Assessment

3.1 Groundwater Sampling
During assessment activities, soil borings SB-1 through SB-5 were converted into permanent
monitoring wells MW-1 through MW-5, respectively. NC DOT requested that the wells be
completed as permanent. As required by Guilford County, H&H obtained a Groundwater
Monitoring Well Permit (No. 014-19-MW5-RW0) from the Guilford County Board of Health
Division of Environmental Health prior to installing the monitoring wells at the site.

The monitoring well borings were installed with the DPT drill rig using hollow stem auger
and/or air rotary drilling methods. Well depths were selected to extend to depths slightly below
the planned cut depths to evaluate the depth to groundwater and potential groundwater
contaminant concentrations. Monitoring wells MW-1, MW-2, MW-3, MW-4 and MW-5 were
installed to total depths of 30 ft bgs, 32 ft bgs, 31 ft bgs, 31 ft bgs, and 30 ft bgs, respectively,
with 2-inch diameter PVC riser and 15 ft of 0.010-inch slotted PVC well screens. Sand filter
pack was placed from the bottom of the well boring to approximately 2 ft above the top of the
well screen, and hydrated bentonite was placed above the sand filter pack. Monitoring wells MW-
1 and MW-5 were completed with flush-mount manhole covers and wells MW-2 through MW-4
were completed with stickup well covers.
7

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc

Once the monitoring wells were installed, IET developed the wells by removing a minimum of
three to five well volumes. MW-3 and MW-5 were dry and were not developed. After
development activities, the wells were allowed to equilibrate, and an electronic water level meter
was used to measure the depth to groundwater relative to the top of casing. The depth to water
ranged from approximately 23.30 ft to 29.23 ft in wells MW-1, MW-2 and MW-4. Monitoring
well construction data and groundwater elevation data are included in Table 1.

Groundwater samples were then collected from wells MW-1, MW-2 and MW-4 utilizing low-
flow/low stress purging techniques using a bladder pump or peristaltic pump and dedicated
polyethylene tubing. Groundwater was removed at a rate no greater than 200 milliliters per
minute. H&H utilized a water quality meter to collect measurements of pH, temperature,
dissolved oxygen, oxidation reduction potential, turbidity, and specific conductivity at
approximate five-minute intervals during the purging process. Purging was considered complete
when the parameters stabilized (pH +/- 0.1 SU, conductivity varied no more than 5%). The
Groundwater Sampling Records are included in Appendix E.

Once groundwater parameters stabilized, groundwater samples were collected directly into
laboratory supplied sample containers. The samples were delivered to Pace under standard chain
of custody protocol for analysis of VOCs by EPA Method 8260, 1,4-dioxane by EPA Method
8260 SIM, and RCRA metals by EPA Methods 6010/7470. Laboratory analytical data sheets
and chain-of-custody documentation are provided in Appendix D. The groundwater sample
analytical results are summarized in Table 3. The analytical results are discussed below.

3.2 Groundwater Analytical Results

VOCs including 1,1-dichloroethane, 1,2-dichloroethane (1,2-DCA), 1,1-dichloroethene, 1,1,1-
trichloroethane, 1,1,2-trichloroethane, and/or 1,4-dioxane were detected in the groundwater
samples collected from MW-2 and MW-4. The concentration of 1,2-DCA (0.63 J ug/L) detected
in MW-2 exceeds the 2L Standard of 0.4 ug/L. The concentrations of 1,4-dioxane (39.9 ug/L
and 8.9 ug/L) detected in wells MW-2 and MW-4, respectively, exceed the 2L Standard of 3.0
8

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
ug/L. No other VOCs exceed the 2L Standard. A low level concentration of diethylphthalate
was detected in MW-4 below the 2L Standard. Low level metals including barium and/or
chromium were also detected in the groundwater samples collected from wells MW-1, MW-2
and MW-4 below the 2L Standards.

NC DEQ regulations allow construction dewatering to surface water if surface water standards
are not contravened. As such, the groundwater concentrations noted above were also compared
to the NC Water Quality Standards for Surface Water (2B Standards). A stream is present on the
western portion of the Brownfields property. This surface water body is alternately titled in NC
Division of Water Resources (NC DWR) references as “Unnamed Tributary at Camp Herman”
and “Smith Branch Reedy Fork” and is defined as Class WS-V, NSW. Based on the
classification of the receiving water body downgradient of the site, concentrations detected in
groundwater were compared to criteria applicable for water supply classifications. Per NC DWR
guidance (NC DWR Surface Water Quality Standards, Criteria & In-Stream Target Values table,
June 2019), if no 2B Standards exist for certain compounds, concentrations were compared to the
lower of the EPA National Recommended Water Quality Criteria or NC In-Stream Target
Values. Based on this comparison, the concentrations of 1,4-dioxane (39.9 ug/L and 8.9 ug/L)
detected in wells MW-2 and MW-4, respectively, exceed the In-Stream Target Value of 0.35
µg/L.

Based on laboratory analytical results for wells MW-2 and MW-4, groundwater is impacted
above 2L Standards and NC surface water criteria in the site area. If impacted groundwater is
encountered and dewatering activities are required during NC DOT construction activities, the
groundwater should be properly managed via an NPDES permit or via containerization and
disposed at a permitted facility. The estimated horizontal extent of impacted groundwater (based
on historical Wysong data and current groundwater data) is shown on Figures 2 and 4.

4.0 Investigative Derived Waste

Soil cuttings and purge/decontamination water generated during the soil and groundwater
sampling activities were containerized in 55-gallon drums. A composite soil sample and a
9

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
composite groundwater sample were collected from the IDW soil and groundwater drums. The
composite soil sample (IDW SOIL) was analyzed for VOCs, 1,4-dioxane, SVOCs, and RCRA
metals analysis using EPA Methods 8260, 8260 SIM, 8270, and 6010/7470. Low level metals
and 1,4-dioxane were detected in the composite soil sample. A composite sample (IDW-GW) of
the IDW water drums was analyzed for VOCs, 1,4-dioxane, SVOCs, and total RCRA metals
using EPA Methods 8260, 8260 SIM, 8270, and 6010/7471, respectively. Low level VOCs,
metals, and di-n-butylphthalate, were detected in the water sample collected from the IDW water
drums. Based on the analytical data, the soil and water drums were disposed as non-hazardous
waste. The IDW drums were removed by EVO Corporation of Winston-Salem, NC for proper
off-site disposal.

Laboratory analytical data sheets and chain-of-custody documentation for IDW are provided in
Appendix D. The non-hazardous waste disposal manifests are included in Appendix F.

5.0 Quality Assurance/Quality Control

For quality assurance/quality control (QA/QC) purposes, field QA/QC samples were analyzed
along with the investigative parent samples to determine the variability introduced in sampling,
handling, shipping, and analysis. One trip blank was submitted with the groundwater shipment
and two trip blanks were submitted with soil sample shipments for analysis of VOCs by EPA
Method 8260. To evaluate the reproducibility of the sample results, H&H collected one duplicate
soil sample and one duplicate groundwater sample that were submitted for the same analysis as
the parent sample.

Trip Blanks
Trip blanks consist of certified-clean sample containers filled with analyte-free water that were
not opened in the field. Trip blanks were prepared by the laboratory and traveled to the site with
the empty sample bottles and back from the site with the collected samples in an effort to
simulate sample handling conditions and the potential for external contaminants. The trip blanks
contained sample bottles for VOC analysis. Laboratory analytical results of the soil trip blank
collected on November 20, 2019 indicated the presence of hexachloro-1,3-butadiene at a
10

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
concentration of 1.1 µg/L. No other VOCs were detected above method detection limits in the
trip blanks.

Field Duplicates
Field duplicate samples were collected to evaluate the precision of the field sampling procedures,
sample matrix variability, and analytical reproducibility. The samples were analyzed for the
same parameters as the original sample, and the analytical results were compared with those of
the original sample. The analytical results of the original samples and the duplicate samples
were used to evaluate the cumulative precision due to potential limitations of the analytical
method, sample matrix, and sample collection techniques. The duplicate sample results for the
soil sample and groundwater sample were comparable to the original samples. The results of the
duplicate samples collected are presented in the summary tables.

Additional QA/QC
Upon review of the laboratory analytical reports, H&H reviewed the qualifiers noted for select
compounds for select samples. After a review of the QA/QC data in each laboratory report, the
qualifiers do not appear to affect the quality of the data produced. It is noted that the soil
hexavalent chromium samples were analyzed outside of hold times.

6.0 Summary and Regulatory Considerations

H&H has completed soil and groundwater assessment activities at the Pennston Brownfields
property (NC DOT Parcels 13, 14, and 15) located in Greensboro, Guilford County, North Carolina.
The Brownfields property encompasses approximately 78 acres of land on five parcels that are
separated by Eckerson Road and Reedy Fork Parkway. A review of historical environmental
documents indicates groundwater on the Brownfields property is contaminated from a release
associated with the Wysong facility that is located topographically upgradient and southwest of the
Brownfields property. Groundwater impacts are located within proposed NC DOT work areas on
Parcels 13, 14 and 15. H&H collected soil and groundwater samples from five monitoring wells on
the Brownfields property to evaluate the potential for impacted soil and/or groundwater in proposed
right of way and construction easement areas related to proposed NC DOT road improvements
along Reedy Fork Parkway.
11

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
Analytical results of soil samples indicate low level concentrations of 1,4-dioxane and hexavalent
chromium above the NC DEQ PSRGs near boring locations SB-2 and SB-3, respectively. No soil
concentrations exceed Industrial PSRGs. Other low level metals were also detected in each of the
soil sample locations. These metal concentrations appear to be naturally occurring. H&H estimates
there are roughly 10,000 cubic yards (15,000 tons) of impacted soil between 15 ft bgs and NC DOT
planned cut depths on the Brownfields property.

Analytical results of groundwater samples indicate concentrations of VOCs including 1,2-DCA
and/or 1,4-dioxane above 2L Standards in monitoring wells MW-2 and MW-4. The 1,4-dioxane
concentrations in MW-2 and MW-4 also exceed NC surface water criteria. Other VOCs and/or
diethylphthalate were also detected in MW-2 and MW-4 below screening levels. Metals were also
detected in the samples from each well; however, detected metals concentrations appear to be
naturally occurring and don’t exceed 2L Standards.

NC DOT plans indicate proposed cuts and fills for road improvement activities, and installation
of proposed drainage structures in proposed NC DOT work areas on the Brownfields property.
Impacted soil will be encountered during the road construction activities. Impacted groundwater
may also be encountered during road construction activities. As indicated in the Brownfields
Agreement, soil may not be disturbed on the Brownfields property at a depth greater than 15 ft
bgs and no activities that encounter, expose, remove, or use groundwater may occur without NC
DEQ’s written approval. Impacted soil that is cut during the road construction activities will be
re-used as fill material on the Brownfields property or properly dispose at an off-site facility. If
impacted groundwater is encountered and dewatering activities are required during NC DOT
construction activities, the water should be properly managed via an NPDES permit or
containerized and disposed at permitted facility.

An EMP will be prepared for management of soil and groundwater (if encountered) during road
construction activities. The EMP will be submitted to the NC DEQ Brownfields Program for
approval and no soil cuts below 15 ft should occur until the EMP is approved. Contingencies will
be included in the EMP to manage other suspected impacts (if identified) during the road
construction activities.
12

S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\R-
4707_BF Assessment Report _20200221.doc
7.0 Signature Page

This report was prepared by:

David Graham, PG
Senior Project Geologist for
Hart & Hickman, PC

This report was reviewed by:

Matt Bramblett, PE
Principal and Project Manager for
Hart & Hickman, PC

Not considered final unless all signatures are completed.

Table 1 (Page 1 of 1) Summary of Well Construction and Water Level DataPennston Brownfields PropertyGreensboro, Guilford County, North CarolinaH&H Job No. ROW-603Monitoring Well ID Latitude Longitude Screened Interval Total Depth Depth to Water(ft bgs)(ft bgs) (ft TOC) 11/22/19MW-136.1727680 -79.710304615 - 303023.30MW-236.1723693 -79.709735917 - 323229.23MW-336.1718009 -79.709357916 - 3131DryMW-436.1719994 -79.710801816 - 313129.05MW-536.1716812 -79.710188115 - 3030DryNotes:1) Well location data collected by H&H using a Trimble GeoExplorer 6000 handheld GPS unit.bgs = Below ground surfaceft TOC = Depth in feet below top of well casing.Monitoring wells MW-1 and MW-5 were completed with flush mount manhole covers. MW-2, MW-3, and MW-4 were completed with sitck-up well covers.The TOC's for monitoring wells MW-2, MW-3, and MW-4 are approximately 1.5 ft, 1.8 ft, and 1.5 ft above ground surface, respectively.S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\[File]2/21/2020Table 1 (Page 1 of 1)Hart & Hickman
Table 2 (Page 1 of 1) Soil Analytical ResultsPennston Brownfields PropertyGreensboro, Guilford County, North CarolinaH&H Job No. ROW-603Sample IDSB-1DUP-1-Soil (SB-5)Sample Depth (ft)15-16.5 15-17 22-24 15-17 17-19 15-17 19-21 15-17 19-21 15-17Sample Date11/19/2019 11/19/2019 11/19/2019 11/20/2019 11/20/2019 11/20/2019 11/20/2019 11/20/2019 11/20/2019 11/20/2019VOCs (8260) (mg/kg)<MDL <MDL <MDL <MDL <MDL <MDL <MDL <MDL <MDL <MDL ‐‐ ‐‐ ‐‐SVOCs (8270) (mg/kg)<MDL <MDL <MDL <MDL <MDL <MDL <MDL <MDL <MDL <MDL ‐‐ ‐‐ ‐‐VOCs (8260 SIM) (mg/kg)1,4-Dioxane<0.00250.0047 J0.014<0.0040 <0.0042 <0.0031 <0.0024 <0.0037 <0.0032 <0.00385.4 25 0.012RCRA Metals (6010/7471) (mg/kg)Arsenic<0.520.78 J 3.3 J 1.5<3.5 <0.53 <0.43 <0.65 <0.55 <0.610.68 3 5.81.0 - 18 4.8Barium 355 453 468 169 323 366 319 96.9 55 643,100 47,000 58050 - 1,000 356Cadmium<0.052 <0.061 <0.32 <0.070 <0.350.073 J 0.069 J<0.065 <0.055 <0.06114 200 31.0 - 10 4.3Chromium518.6 21.4 167 31.6 119 14.5 19.6 9.8 11.8 13.223,000 350,000 360,0007.0 - 300 65Lead 1.2 7.2 8.3 11.1 13.1 1.3 1.5 7.0 2.2 1.6400 800 270N.D. - 50 16Mercury 0.0024 J 0.012 0.0053 0.0044 0.02<0.0017 <0.00110.0042<0.00130.00292.3 9.7 10.03 - 0.52 0.121Selenium* 1.0 J 0.87 J3.7 J<0.70 <3.5 <0.530.64 J 0.86 J 0.71 J 0.63 J78 1,200 2.1<0.1 - 0.8 0.42Silver<0.26 <0.31 <1.6 <0.35 <1.8 <0.26 <0.22 <0.33 <0.28 <0.3178 1,200 3.4N.D. - 5.0 --Hexavalent Chromium (7199) (mg/kg)Hexavalent ChromiumNA NA<0.327NA 0.870 JNA NA NA NA NA0.31 6.5 3.8Notes:1. NC DEQ Residential Health-Based Preliminary Soil Remediation Goals (PSRGs) (December 2019).2. NC DEQ Industrial Health-Based PSRG (December 2019).3. NC DEQ Protection of Groundwater (POG) PSRG (December 2019).4. Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.5. Screening levels for chromium are for chromium III.* = Selenium concentrations in bold are more than two times background levels for published NC soils. However, note that the NC valuesare based on a limited data set and concentrations are within the range of values published for eastern US soils (<0.1 to 3.9).mg/kg = milligrams per kilogram; VOCs = Volatile Organic CompoundsBold = value exceeds Protection of Groundwater PSRG (and twice background value for metals)Underline = value exceeds Residential Health-Based PSRG <MDL = All values below Method Detection Limit; SIM = Select Ion MonitoringJ = Estimated concentration between laboratory Reporting Limit and Method Detection LimitHexavalent chromium samples were analyzed outside of hold time.SB-2SB-3SB-4SB-5Background4MeanRangeNCDEQ POG PSRG3NCDEQ Industrial PSRG2 NCDEQ Residential PSRG1 S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Report\Soil DataTable 22/21/2020Table 2 (Page 1 of 1)Hart & Hickman, PC
Table 3 (Page 1 of 1) Groundwater Analytical ResultsPennston Brownfields PropertyGreensboro, Guilford County, North CarolinaH&H Job No. ROW‐603Sample IDMW-1MW-2MW-4 DUP-2-GW (MW-4)Sample Date11/22/2019 11/22/2019 11/22/2019 11/22/2019VOCs (8260) (ug/L)1,1-Dichloroethane<0.273.2 0.91 J 0.89 J6NE61,2-Dichloroethane<0.340.63 J<0.34 <0.340.4NE9.91,1-Dichloroethene<0.2455.9 23.5 22.3350NE3001,1,1,-Trichloroethane<0.188.4 1.1 1.1200NE10,0001,1,2-Trichloroethane<0.240.32 J<0.24 <0.240.6*NE0.55SVOCs (8270) (ug/L)Diethylphthalate<2.4 <2.46.9 J 10 J 6,000 NE 600VOCs (8260 SIM) (ug/L)1,4-Dioxane<1.239.98.97.43NE0.35RCRA Metals (6010/7470) (ug/L)Barium50440.61261187001,000 ---Chromium48.8<1.0<1.0<1.01037.13 ---Notes:1. NC DEQ 15A NCAC 2L .0202 Groundwater Quality Standards - April 20132. NC DEQ Water Quality Standards for Surface Waters - Class WS-V, NSW (June 2019).3. Lower of EPA Recommended Water Quality Criteria for Aquatic Life & Human Health - Water Supply or NC In-Stream Target Values for Surface Water - Water Supply (June 2019)4. 2B Standard shown for chromium is for chromium III; no confirmed sources of chromium VI have been identified in the area. Standard derived using DEQ Hardness-Dependent Metal Calculator dated June 2019 and DEQ published median hardness for receiving stream (alternately titled Unnamed Tributary at Camp Herman and Smith Branch-Reedy Fork) of 43 milligrams per liter.The nearest dicharge is to a Class WS-V surface water body (alternately titled Unnamed Tributary at Camp Herman and Smith Branch-Reedy Fork). Based on the classification of the receiving water body, surface water standards and criteria are based on water supply classification.* = NC DEQ Interim Maximum Allowable Concentration (August 1, 2010)EPA Method follows parameter in parenthesisug/L = micrograms per liter. NE = Not established.VOCs = Volatile Organic Compounds; SVOCs = semi-VOCsBold indicates above 2L Standard; Underline exceeds 2B Standard or Water Quality Criteria.Water Quality Criteria3NC 2L Standards1 NC 2B Standards2S:\AAA‐Master Projects\NC DOT Right‐of‐Way ‐ROW\ROW‐600s\ROW‐603 Guilford County Phase II Investigations\Brownfields Assessment\Report\GW Table 3Table 3 (Page 1 of 1)Hart & Hickman, PC
TITLE
PROJECT
PROJECT LOCATION MAP
BROWNFIELDS PROJECT #15010-11-41
3600 REEDY FORK PARKWAY
GREENSBORO, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
2-12-20 0
1ROW-603
PROJECT AREA
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
BROWNS SUMMIT, NORTH CAROLINA, 1994
W
W
W WW
WWS
S
MW-4/SB-4
MW-1/SB-1
MW-2/SB-2
MW-5/SB-5 MW-3/SB-3
REVISION NO. 0
JOB NO. ROW-603
DATE: 2-13-2020
FIGURE NO. 2
BROWNFIELDS PROJECT #15010-11-41
ECKERSON ROAD & REEDY FORK PARKWAY
GREENSBORO, NORTH CAROLINA
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
LEGEND
APPROXIMATE BROWNFIELDS PROPERTY
BOUNDARY
EXISTING RIGHT-OF-WAY.
PROPOSED ROAD
PROPOSED RIGHT-OF-WAY
PROPOSED CONSTRUCTION EASEMENT
PROPOSED UTILITY EASEMENT
MONITORING WELL AND SOIL SAMPLE
LOCATIONS
NC DOT PARCEL ID
KNOWN GROUNDWATER CONTAMINATION
KNOWN SOIL CONTAMINATION
SITE MAP
14
13
15
14
REEDY FO
R
K

P
A
R
K
W
A
Y
ECK
E
R
S
O
N
R
O
A
DUS HIGHWAY-29SUM
MIT
A
VE
N
U
E
KYLIND AVENUEW W
S S
S:\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Figures\Parcels-row603-R1-Site Map.dwg, FIG 2, 2/13/2020 2:23:08 PM, jdemmer
MW-1/SB-1
MW-2/SB-2
MW-4/SB-4
MW-5/SB-5 SSS
S
(15-16.5')
[<0.0025]
(15-17') (22-24')
[0.0047J] [0.014]
(15-17') (19-21')
[<0.0037] [<0.0032]
(15-17') (19-21')
[<0.0031] [<0.0024]
MW-3/SB-3
(15-17') (17-19')
[<0.0040] [<0.0042]
{0.870 J}
REVISION NO. 0
JOB NO. ROW-603
DATE: 2-13-2020
FIGURE NO. 3
BROWNFIELDS PROJECT #15010-11-41
ECKERSON ROAD & REEDY FORK PARKWAY
GREENSBORO, NORTH CAROLINA
SOIL ANALYTICAL RESULTS
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
MONITORING WELL AND SOIL SAMPLE
LOCATION
EXISTING RIGHT-OF-WAY
PROPOSED RIGHT-OF-WAY
PROPOSED CONSTRUCTION EASEMENT
PROPOSED UTILITY EASEMENT
PROPOSED CUT LINE
PROPOSED FILL LINE
NC DOT PARCEL ID
PROPOSED DRAINAGE PIPE
PROPOSED CATCH BASIN
KNOWN SOIL CONTAMINATION
1,4-DIOXANE CONCENTRATION (mg/kg)
HEXAVALENT CHROMIUM
CONCENTRATION (mg/kg)
SAMPLE ID/DEPTH
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
[0.014]
PROPOSED ROAD
EXISTING ROAD
-Y-STA.51+00
-Y2-STA.18+00
PROPOSED ROADREEDY FORK
PARKWAY
PROPOSED ROAD
ECKERSON ROADS S
PENNSTON BROWNFIELDS
PROPERTY
PENNSTON BROWNFIELDS
PROPERTY
MW-2/SB-2 (15-17')
{0.870 J}
ALIGNMENT -Y2-
ALIGNMENT -Y-\\HARTHICKMAN.LOCAL\Shares\MasterFiles\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Figures\Parcels-row603-R1.dwg, FIG 3 SOIL, 2/21/2020 3:30:22 PM, jdemmer
DRY
DRYMW-5
MW-4
MW-1
MW-2
MW-3
REVISION NO. 0
JOB NO. ROW-603
DATE: 2-13-2020
FIGURE NO. 4
BROWNFIELDS PROJECT #15010-11-41
ECKERSON ROAD & REEDY FORK PARKWAY
GREENSBORO, NORTH CAROLINA
GROUNDWATER ANALYTICAL RESULTS
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
MONITORING WELL LOCATION
EXISTING RIGHT-OF-WAY
PROPOSED RIGHT-OF-WAY
PROPOSED CONSTRUCTION EASEMENT
PROPOSED UTILITY EASEMENT
PROPOSED CUT LINE
PROPOSED FILL LINE
NC DOT PARCEL ID
PROPOSED DRAINAGE PIPE
PROPOSED CATCH BASIN
KNOWN GROUNDWATER CONTAMINATION
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
PROPOSED ROAD
EXISTING ROAD
-Y-STA.51+00
-Y2-STA.18+00
PROPOSED ROADREEDY FORK
PARKWAY
PROPOSED ROAD
ECKERSON ROADW W
PENNSTON BROWNFIELDS
PROPERTY
PENNSTON BROWNFIELDS
PROPERTY
W
W
W
W
W
MW-4
1,1-DICHLOROETHANE 0.91J
1,1-DICHLOROETHENE 23.5
1,1,1-TRICHLOROETHANE 1.1
DIETHYLPHTHALATE 6.9J
1,4-DIOXANE 8.9
BARIUM 126
MW-1
BARIUM 504
CHROMIUM 8.8
MW-2
1,1-DICHLOROETHANE 3.2
1,2-DICHLOROETHANE 0.63J
1,1-DICHLOROETHENE 55.9
1,1,1-TRICHLOROETHANE 8.4
1,1,2-TRICHLOROETHANE 0.32J
1,4-DIOXANE 39.9
BARIUM 40.6
SAMPLE ID
MW-1
BARIUM 504
CHROMIUM 8.8CONSTITUENT
CONCENTRATION
(ug/L)
NOTES:
1. BOLD EXCEEDS 2L STANDARD.
2.UNDERLINE EXCEEDS 2B STANDARD OR, IF NO 2B
STANDARD EXISTS, LOWER OF EPA NATIONAL
RECOMMENDED WATER QUALITY CRITERIA OR NC
IN-STREAM TARGET VALUES.
ALIGNMENT -Y2-
ALIGNMENT -Y-\\HARTHICKMAN.LOCAL\Shares\MasterFiles\AAA-Master Projects\NC DOT Right-of-Way -ROW\ROW-600s\ROW-603 Guilford County Phase II Investigations\Brownfields Assessment\Figures\Parcels-row603-R1.dwg, FIG 4 GW ANALY, 2/21/2020 3:30:04 PM, jdemmer

Appendix A

NC DOT Preliminary Plan

DOCUMENT NOT CONSIDERED FINAL
UNLESS ALL SIGNATURES COMPLETED
REVISIONS HYDRAULICSROADWAY DESIGN
ENGINEER ENGINEER
R/W SHEET NO.
SHEET NO.PROJECT REFERENCE NO.8/17/99DOCUMENT NOT CONSIDERED FINAL
UNLESS ALL SIGNATURES COMPLETED
06-MAR-2019 17:37R:\Roadway\Proj\R4707_Rdy_psh_09.dgn1784rjdFOR -Y2- PROFILE, SEE SHEET 22
FOR -Y5- PROFILE, SEE SHEET 23MATCHLINE -Y- STA. 47+00.00 SEE SHEET 6R-4707 9
FOR -Y- PROFILE, SEE SHEETS 16 & 17NAD
8
3/2
0
1
1
PI Sta 10+33.66
D
L = 67.29'
T = 33.66'
R = 786.49'
PI Sta 13+21.66
D
L = 453.14'
T = 254.37'
R = 400.00'
PI Sta 19+16.32
D
L = 342.50'
T = 230.56'
R = 200.00'
PI Sta 51+32.55
D
L = 768.57'
T = 385.11'
R = 4,800.00'
PI Sta 57+06.40
D
L = 375.85'
T = 190.39'
R = 955.00'
-Y- CURVE DATA
e = NC e = EXISTING
-Y2- CURVE DATA
e = EXISTING e = 0.04 e = 0.04 FOR INTERSECTION DETAIL, SEE SHEET 2B-2
NC License No. F-1235
919-714-8670 | meadhunt.com
Raleigh, North Carolina 27601
111 E. Hargett Street, Suite 300
BST30" C&G
30" C&G
30" C&G
30" C&G
18" C&G
18" C&G
18" C&G
18" C&G
1SFBUS
DK
5' C
O
N
C
WOODS
WOODS
WOODS
RIP RAP
RIP RAP
5' CONC
5' CONCRIP RAP
CBSS
S
COLUMNSSTONE
REEDY FORK PKWY
CONC WW
CONC WW
36' BST30" C&G30" C&GSWOODS
RIP RAPWD POST
36" RCPCONC WWCONC WW4' WD RAIL PB 183 PG 109 AND 110
AS DRAINAGEWAY AND OPEN SPACE
1.300 ACRES DEDICATED TO THE CITY OF GREENSBORO 28'X28' PB 147 PG 68DUKE POWER EASEMENTS
C
AL
E
D F
R
O
M P
B 1
4
7 P
G 68
3
0'
D
R
AI
N
A
G
E MAIN
TE
N
A
N
C
E
&
U
TILIT
Y
E
AS
E
ME
N
T
10' UTI
LI
TY EASEM
ENT PB 147 PG 6815' S ANIT ARY S E W E R EAS EME NT DB 3517 P G 205310' UTI
LI
TY EASEM
ENT PB 183 PG 11115' SANITARY SEWER EASEMENT DB 3517 PG 2053PB 147 PG 63
COMMON ELEMENTS
10' UTILITY EASEMENT PB 183 PG 115
10' UTILITY EASEMENT PB 183 PG 113
PB 147 PG 68
20' SANITARY SEWER EASEMENT DB 5001 PG 1165 AND PB 147 PG 63AS DRAINAGEWAY AND OPEN SPACE18.452 ACRES DEDICATED TO THE CITY OF GREENSBORO PB 183 PG 109 AND 110
AS DRAINAGEWAY AND OPEN SPACE
4.212 ACRES DEDICATED TO THE CITY OF GREENSBORO EXISTING R/WEXISTING R/W68.00
'VARIABLEEIP
EIP
EIP
EI
PEIP
EIP EIP
EI
PEI
PEIP EIP
E
IP
EIPEIPEIP EIP
EIP
EIP
EIP
EIP
EIP
EIP
EIP
EIPEIP & UTILITY EASEMENT
110' DRAINAGE MAINTANENCE
& UTILITY EASEMENT110' DRAINAGE MAINTANENCE100' STREAM BUFFER100' STREAM BUFFER
30' STREAM BUFFERWI
THI
N ABANDONED R/WOF UNDETERMI
NED WI
DTHEASEMENT FOR UTI
LI
TI
ESDB
5
5
9
5
PG 825
0.22'R/W TO EIP
S
30"DIP
ASSUMED ROUTE
8"PVC 8"PVC
8"P
VC
12 "TCP
12 "T CP 12"UNKLT
LT
E IP
16" CP
P
AND MARKER POSTGAS TEST STATION SCONC CONC
STONE WALLVARIABLE HEIGHT
LT
POSTFO MKRPOSTMTLS
BST
COFFBLOW HH
HH12" DI12" DI
6" PL
6" STL20" DI6" PL6" PL
20" DI6" STLFUTURE USE
CONDUIT STUB
6"DI12"DIN 32°29'12" E76.52'S 74°29'30" W83.70'S 02°16'39" W342.47'AF-REEDY FORK COMMERCIAL, LLC
AF-REEDY FORK COMMERCIAL, LLC
AF-REEDY FORK COMMERCIAL, LLC
DB 7425 PG 292
PB 183 PG 109 & 110
PB 183 PG 113 & 114
DB 7425 PG 292
PB 183 PG 111 & 112
DB 7425 PG 292
S11°38'20"W1408.47'S36°00'57"W313.92'3.14'R/W TO EI
PRCP15"30"DIP
CBCB15"RCP
15"
R
C
P
18"RCP 15"RC
PCB
18"RCP
MH 15"RCPCB
CB
CB15"RCP18"RCP18"RCP
CBCBSR 477
1 REE
D
Y F
OR
K P
K
WY
WOODS
WOODS
BM11
WOODS
WOODS
DELTA PHOENIX, INC.
DB 7309 PG 2280
PB 115 PG 18
-BY1- 41
-BY1- 42
-BY1- 43
-BY1- 44
ECKERSON RDSR 279046.68'
+59.87
5055-Y2- PC Sta. 10+00.00
-Y2- PCC Sta. 10+67.29
-Y2- PT Sta. 15+20.42
-Y2- PC Sta. 16+85.76
-Y- PT Sta. 58+91.86
-Y5- POT Sta. 12+54.62
-Y- PRC Sta. 55+16.01
-Y5- POT Sta. 10+00.00
-Y2- POT Sta. 20+67.26
-Y- POC Sta. 55+46.24 =-Y5--Y2-
-Y2- PT Sta. 20+28.26
-YEB- PT Sta. 49+00.72 (27.00' RT)
-Y- POC Sta. 48+58.58 =
-YWB- PT Sta. 49+13.58 (27.00' LT)
-Y- POC Sta. 48+60.56 =
-YEB- PRC Sta. 48+15.26
-Y- PC Sta. 47+47.44
-SPC- POT Sta. 28+24.47
-YEB- POC Sta. 47+81.23 =
-YWB- PRC Sta. 48+32.89
-SPD- POT Sta. 27+68.60
-YWB- POC Sta. 47+58.39 =
-Y-EX.EX.020100010202020200010102EXIST.
01
01 01
02
02
03
0304
04040403030202010100000101020203030404
03
02
EXIST.
04
01
00
00
00
GREU TL-3 24'41.5'+53.12INC.
26'
+96.00
I
N
C.2
6'
+28.00
-Y5- STA. 12+10.00
END CONSTRUCTION
-Y- STA. 58+80.00
END CONSTRUCTION
+50.0050
' INC.
36
'-Y2- STA. 10+50.00
BEGIN CONSTRUCTION
0202INC.50' +30.00-SPC- STA. 24+50.00END SBGCR
CR CR
CRCR4' PS
4' PS
CR
CRCR
ACCESS
UTILITY
GATE
16'
I
N
C.
2
6'
TO EXISTING
TIE 2'-6" C&G
TO EXISTING
TIE 2'-6" C&G
2GI
2GI
2GI
2GI
CB
BDO
BDO
CBCB
CB
CB
CB
CB CB
CB
CB
901
902
905
906
907
908
909910
911
912
913
914
917
918
920
921
922
923
924
925
926
927
930
931
903
CB
915
919
CB
CB
CBCBREMOVE
RETAIN
REMOVE
REMOVE
RETAIN
RETAIN
REMOVE
REMOVEREMOVE
REMOVE
RETAIN
RETAINRETAIN
REMOVE
REMOVEREMOVE
REMOVE24"w/MH
JB
w/MH
JB
FS
916
940
928
929
15" RCP-IV 15"CB
CB
DI
DI
EST. 14 SY GEOTEXTILE
EST. 5 TONS
CLASS B RIP RAPRETAIN
125.00' RT
+00.00 -Y-
45.28' RT
+26.25 -Y-
90.00' LT
+80.00 -Y2-
51.58' LT
+95.00 -Y-
90.00' LT
+85.76 -Y2-
90.00' LT
+00.00 -Y2-
90.00' LT
+20.42 -Y2-
125.00' LT
+00.00 -Y-
5
5
13
13
14
14
15
51.45' RT
+30.48 -Y-
125.00' RT
+65.00 -Y-
49.42' RT
+22.53 -Y-
141.00' RT
+14.00 -Y-
151.00' RT
125.00' RT
+30.00 -Y-
125.00' LT
152.00' LT
+32.00 -Y-
143.00' RT
+18.00 -Y-
EXIST. R/W
+26.88 -Y-
74.00' LT
+04.00 -Y-
111.00' LT
+74.00 -Y2-
111.00' LT
+85.76 -Y2-111.00' LT
+20.42 -Y2-111.00' LT
+99.82 -Y2-
EXIST. R/W
+69.05 -Y2-
EXIST. R/W
+35.56 -Y2-
47.59' RT
EXIST. R/W
+80.00 -Y-
EXIST. R/W
+14.59 -Y-
EXIST. R/W
+04.05 -Y5-
EXIST. R/W
+10.00 -Y5-
EXIST. R/W
+24.47 -Y5-
218.54' LT
+58.00 -Y-
59.29' LT
+33.76 -Y2-
65.66' LT
+94.18 -Y2-
125.00' RT
+00.00 -Y-
WIRE FENCE
END WOVEN
END FULL C/A
125.00' LT
+00.00 -Y-
WIRE FENCE
END WOVEN
END FULL C/A
15
" RCP
-IV
15" RCP-IV 15"15"15" RCP-IV 15" RCP-IV 18" RCP-IV 15" RCP-IV 15" RCP-IV 15" RCP-IV
15" RCP-IV 15" RCP-IV 15"15"
RCP-
I
V
15" RCP-IV
15" RCP-IV 15"15"
15"18" RCP-IV 18" RCP-IV
15" RCP-IV
15" RCP-IV
EST. 107 SY GEOTEXTILE
EST. 76 TONS
CL 1 RIP RAP
USE DETAIL 'SBDR3'
STANDARD BASE DITCH w/RIP RAP
BDO
CB
DI
USE DETAIL 'BVD1'
BERM V-DITCH
USE DETAIL 'BD1'
BERM BASE-DITCH
USE DETAIL 'BD3'
SPECIAL BERM BASE-DITCH
SEE STD 240.01
BERM DITCH
USE DETAIL 'BD2'
BERM BASE-DITCH RC P-IV 18"FC
C
C
C
C
C
C
C
C
C
C
C
C
C
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
F
C
TRAFFIC VOLUME DATA
3,300
2,400
9,000
4,400
8,100
3,400
2,100
1,700 PARKWAY
REEDY FORK
2040 AADT
2020 AADT
PARKWAY
REEDY FORK
FORK PARKWAY
OLD REEDY
ROAD
ECKERSON
1,200
700

Appendix B

Environmental Documents

WellDateChloroethane 1,1-DCA 1,2-DCA 1,1-DCE cis-1,2-DCE 1,4-Dioxane PCE 1,1,1-TCA 1,1,2-TCA TCE Vinyl Chloride6/22/2006ND9.6ND720ND NS1140 2ND ND12/19/2007ND11ND70ND170 1.2130 2.1ND ND6/26/2008ND13ND55ND140 1.292 1.9ND ND8/25/2005ND ND ND12.5ND NS ND3.78ND ND ND3/13/2006ND ND ND13.6ND NS ND4.08ND ND ND6/19/2006ND ND ND8.7ND NS ND2.8ND ND ND8/17/2004ND1.022.13.73ND NS ND ND ND ND ND3/13/2006ND1.472.32ND ND NS ND ND ND ND ND6/20/2006ND2.826ND NS ND1.2ND ND ND8/25/2005ND ND ND38.7ND NS ND ND ND ND ND3/13/2006ND2.4ND20.2ND NS ND2.4ND ND ND6/20/2006ND1.8ND44ND NS ND1.9ND ND ND8/25/2005ND ND ND87.5ND NS ND27.3ND ND ND3/13/2006ND ND ND96.4ND NS ND25.5ND ND ND6/23/2006ND2.2ND92NDNSND26ND NDND8/17/2004ND ND ND ND ND ND ND ND ND NDND3/13/2006ND ND ND ND ND ND ND ND ND NDND6/22/2006ND ND ND ND ND NS ND ND ND NDND8/25/2005ND ND ND121ND NS ND37.8ND NDND3/13/2006ND ND ND122ND NS ND36.4ND NDND6/22/2006ND6.7ND140ND NS ND40ND NDND3/13/2006ND ND ND ND ND NS ND1,560ND NDND12/19/2007ND85ND390ND240 9.1J 2,0007.4JNDND6/26/2008ND60ND290ND1,662 6.3J 1,3005.4JNDNDNCAC 2L Standard3000 6.0 0.4 7.0 70 3.0 0.7 200 NS 3.00.03Risk Based Screening Level 1NS 65 20 38 NS NS 5.7 1500 44 301.5Concentrations Reported in Micrograms per Liter (μg/L)Bold = Concentration Exceeds NCAC 2L StandardNS = no standardMW-2MW-3MW-5DMW-8MW-9D1. IHSB Residential Vapor Intrusion Screening Level for Groundwater, January 2010H&H Job No. WYM-002MW-4MW-6TABLE 5Summary of Three Most Recent Groundwater Sampling EventWysong & Miles CorporationGreensboro, North CarolinaMW-1S:\AAA-Master Projects\Wysong & Miles - WYM\H&H 2010\RAP\RAP Revision 3-2010\Tables\RAP Tables.xls1 of 5Hart & Hickman, PC
Well DateChloroethane 1,1-DCA 1,2-DCA 1,1-DCE cis-1,2-DCE 1,4-Dioxane PCE 1,1,1-TCA 1,1,2-TCA TCE Vinyl Chloride6/22/2006ND14 7.9 870ND NS ND60 2.2 1.5ND12/19/2007ND15 9.0 870ND952 1.752 2.5 1.8JND6/26/2008ND10 7.1 350ND405 1.131 2.2 1.1JND8/16/2004ND ND ND ND ND NS ND ND ND5.22ND3/13/2006ND ND ND ND ND NS ND ND ND3.82ND6/21/2006ND ND ND ND1.1NS ND ND ND4.1NDMW-125/17/1995ND ND ND2.4ND NS ND2.1ND NDND6/22/2006ND13ND72ND NS ND22ND1.8ND12/19/2007ND13 0.71J 130ND620.62J 45ND0.71J1.2J6/25/2008ND8.4ND140ND174ND26ND NDND3/27/2008ND97 8.6J 1,100ND520ND5506.3JNDND6/27/2008ND110 9.2J 1,700ND2,576ND7506.4JNDND10/1/2008ND100 8.6J 1,400ND490ND5406.2JNDND8/25/2005ND ND ND67ND NS ND108NDNDND3/13/2006NDND ND90.2ND NS ND156ND NDND6/22/2006ND12ND74ND NS ND120 1.1NDND8/16/2004ND ND ND ND ND NS ND ND ND NDND3/14/2006ND ND ND ND ND NS ND ND ND NDND6/21/2006ND ND ND ND ND NS ND ND ND NDND8/17/2004ND ND ND ND ND NS ND ND ND NDND3/13/2006ND ND ND ND ND NS ND ND ND NDND6/19/2006ND ND ND ND ND NS ND ND ND NDNDNCAC 2L Standard3000 6.0 0.4 7.0 70 3.0 0.7 200 NS 3.00.03Risk Based Screening Level 1NS 65 20 38 NS NS 5.7 1500 44 301.5Concentrations Reported in Micrograms per Liter (μg/L)Bold = Concentration Exceeds NCAC 2L StandardNS = no standardMW-13DMW-14Greensboro, North CarolinaTABLE 5Summary of Three Most Recent Groundwater Sampling EventsWysong & Miles CorporationMW-16DH&H Job No. WYM-002MW-10MW-11MW-15MW-171. IHSB Residential Vapor Intrusion Screening Level for Groundwater, January 2010S:\AAA-Master Projects\Wysong & Miles - WYM\H&H 2010\RAP\RAP Revision 3-2010\Tables\RAP Tables.xls2 of 5Hart & Hickman, PC
Well DateChloroethane 1,1-DCA 1,2-DCA 1,1-DCE cis-1,2-DCE 1,4-Dioxane PCE 1,1,1-TCA 1,1,2-TCA TCE Vinyl Chloride8/17/2004ND ND ND93.6ND NS ND12.9ND NDND3/13/2006ND ND NS39.9ND NS ND ND ND NDND6/20/2006ND ND NS81ND NS ND9.5ND NDND2/28/2005ND ND ND ND ND NS ND ND ND NDND8/25/2005ND ND ND ND ND NS ND ND ND NDND6/20/2006ND ND ND ND ND ND ND ND ND NDND8/16/2004ND ND ND ND ND ND ND ND ND NDND6/25/2008ND ND ND ND ND ND ND ND ND NDND10/1/2008ND ND ND ND ND ND ND ND ND NDND3/27/2008ND8.6ND231.261ND13ND5.4ND6/25/2008ND11ND430.98J70ND19ND5.5ND10/1/2008ND10ND321.162ND13ND5.3ND3/27/2008ND ND ND ND ND ND ND ND ND NDND6/26/2008ND ND ND ND ND ND ND ND ND NDND10/1/2008ND ND ND ND ND ND ND ND ND NDND3/27/2008ND84ND950ND2,634ND1,600ND NDND6/26/2008ND98ND1,400ND660ND2,000ND NDND10/1/2008ND78ND920ND560ND1,400ND NDND3/27/2008ND140.88J140ND2080.69J 51 0.51J 0.52JND6/27/2008ND12 0.75J 120ND940.69J 48ND NDND10/1/2008ND9.7 0.55J 110ND1530.63J 32ND NDND8/11/2006ND1.60.625 500ND39ND2502.4 1.7JND12/18/2007ND ND ND290ND ND ND140ND NDND6/25/2008ND0.67JND200ND ND ND110ND0.69JNDNCAC 2L Standard3000 6.0 0.4 7.0 70 3.0 0.7 200 NS 3.00.03Risk Based Screening Level 1NS 65 20 38 NS NS 5.7 1500 44 301.5Concentrations Reported in Micrograms per Liter (μg/L)Bold = Concentration Exceeds NCAC 2L StandardNS = no standardGreensboro, North CarolinaMW-22MW-18Wysong & Miles CorporationMW-19H&H Job No. WYM-002MW-21DWSW-DMW-23DTABLE 5Summary of Three Most Recent Groundwater Sampling Events1. IHSB Residential Vapor Intrusion Screening Level for Groundwater, January 2010MW-20PWR-1S:\AAA-Master Projects\Wysong & Miles - WYM\H&H 2010\RAP\RAP Revision 3-2010\Tables\RAP Tables.xls3 of 5Hart & Hickman, PC
Well DateChloroethane 1,1-DCA 1,2-DCA 1,1-DCE cis-1,2-DCE 1,4-Dioxane PCE 1,1,1-TCA 1,1,2-TCA TCE Vinyl Chloride8/11/2006ND19 2.0 200ND76ND47 1.8NDND12/17/2007ND27ND340ND57ND67ND NDND6/26/2008ND29 3.0 310ND120ND69 2.5 0.66JND5/23/2007NDNDND11ND ND ND1.4ND NDND12/17/2007ND0.74JND16ND ND ND2.0ND NDND6/25/2008ND0.67JND11ND ND ND1.5ND NDND5/23/2007ND45 5.0 590ND200ND95 4 1.1ND12/18/2007ND64 7.4J 600ND210ND140 6.1JNDND6/26/2008ND54 6.1J 700ND270ND100ND NDND5/23/2007ND26ND260ND120 1.4 4603.7NDND12/18/2007ND24ND190ND190ND490ND NDND6/26/2008ND22ND150ND100ND440NDNDND8/30/2007ND170ND1,100ND780ND1,800NDNDND12/19/2007ND170ND1,100ND510ND2,200ND NDND6/27/2008ND140ND960ND480ND1,800ND NDND6/20/2006ND7.2ND77ND29ND16ND NDND12/18/2007ND6.6 0.75J 77ND29ND14 0.61JNDND6/25/2008ND5.00.59J 52ND41ND9.3ND NDND8/26/2005ND ND ND45.6ND NS ND20.8ND NDND3/14/2006ND ND ND12ND NS ND53.8ND NDND6/21/2006ND ND ND40ND ND ND16ND NDND8/26/2005ND ND ND1.7ND NS ND ND ND NDND3/14/2006ND ND ND1.3ND NS ND ND ND NDND6/20/2006ND ND ND2.2ND ND ND ND ND NDNDNCAC 2L Standard3000 6.0 0.4 7.0 70 3.0 0.7 200 NS 3.00.03Risk Based Screening Level 1NS 65 20 38 NS NS 5.7 1500 44 301.5Concentrations Reported in Micrograms per Liter (μg/L)Bold = Concentration Exceeds NCAC 2L StandardNS = no standardGreensboro, North CarolinaH&H Job No. WYM-002TW-3PWR-3PWR-4PWR-5PWR-6TW-1TW-2Summary of Three Most Recent Groundwater Sampling EventsWysong & Miles CorporationPWR-21. IHSB Residential Vapor Intrusion Screening Level for Groundwater, January 2010TABLE 5S:\AAA-Master Projects\Wysong & Miles - WYM\H&H 2010\RAP\RAP Revision 3-2010\Tables\RAP Tables.xls4 of 5Hart & Hickman, PC
Well DateChloroethane 1,1-DCA 1,2-DCA 1,1-DCE cis-1,2-DCE 1,4-Dioxane PCE 1,1,1-TCA 1,1,2-TCA TCE Vinyl Chloride2/21/2000ND ND ND ND ND NS ND ND ND NDND8/15/2000ND ND ND ND ND NS ND ND ND NDND8/23/2001ND ND ND ND ND NS ND ND ND NDND6/21/2006ND1.8ND120ND46ND55 2.3NDND12/18/2007ND2.20.85J 140ND60ND48 2.7 0.64JND6/26/2008ND1.9ND95ND59ND34 2.2NDND6/21/2006ND820.0181,500ND1,000E 2.1 640154.66.112/18/2007ND180 17 2,300ND980ND91015NDND6/26/2008ND170ND2,100ND1,000ND810ND NDND6/22/2006ND70 1.9 330ND NS5.2 1,40010 2.0ND6/27/2008ND5.3ND65ND27ND20ND NDND10/1/2008ND5.4ND46ND820.54J 30ND NDND6/22/2006ND8.3ND86ND NS4.4 1,300ND NDND6/27/2008ND ND ND290ND6.4ND2,700NDNDND10/1/2008ND12ND300ND1,8164.1 1,500ND NDND5/24/2007ND34 3.6 390ND NS ND77 3.1NDND12/19/2007ND44 5.0J 550ND150ND110ND NDND6/26/2008ND38ND500ND190ND79ND NDND8/30/2007ND100ND1,300ND670ND2,300ND NDND12/19/2007ND200ND1,600ND610ND2,600ND NDND6/27/2008ND95ND1,000ND320ND2,200ND NDNDNCAC 2L Standard3000 6.0 0.4 7.0 70 3.0 0.7 200 NS 3.00.03Risk Based Screening Level 1NS 65 20 38 NS NS 5.7 1500 44 301.5Concentrations Reported in Micrograms per Liter (μg/L)Bold = Concentration Exceeds NCAC 2L StandardNS = no standardBR-2TW-14TW-15TW-16RW-1RW-2BR-1H&H Job No. WYM-0021. IHSB Residential Vapor Intrusion Screening Level for Groundwater, January 2010TABLE 5Summary of Three Most Recent Groundwater Sampling EventsWysong & Miles CorporationGreensboro, North CarolinaS:\AAA-Master Projects\Wysong & Miles - WYM\H&H 2010\RAP\RAP Revision 3-2010\Tables\RAP Tables.xls5 of 5Hart & Hickman, PC
Well DateChloroethane 1,1-DCA 1,2-DCA 1,1-DCE cis-1,2-DCE 1,4-Dioxane PCE 1,1,1-TCA 1,1,2-TCA TCE Vinyl ChlorideSW-A10/22/20071.8J 31 3.5 110ND200ND 13ND0.59J188/26/2005ND ND ND ND ND NS ND ND ND NDND3/14/2006ND ND ND ND ND NS ND ND ND NDND6/22/2006ND ND ND ND ND ND ND ND ND NDND8/26/2005ND ND ND ND ND ND ND ND ND NDND3/14/2006ND ND ND ND ND ND ND ND ND NDND6/22/2006ND ND ND ND ND ND ND ND ND NDND8/26/2005ND ND ND0.83ND NS ND ND ND NDND3/14/2006ND ND ND1.4ND NS ND ND ND NDND6/22/2006ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/16/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND NS ND ND ND NDND5/16/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/16/2007ND ND ND ND ND NS ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/23/2007ND ND ND ND ND NS ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/16/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/23/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND11ND ND ND NDND5/16/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND1.7ND24ND ND ND NDND5/16/2007ND ND ND2.2ND ND ND ND ND NDND10/22/2007ND ND NDNDND24ND ND ND NDNDNCAC 2B Standard550 20000 37 5400 4900 110 3.3 2500 16 302.4Risk Based Screening Level 190000 610 40 3000 3900 20000 8.5 80000 61 37038NOTES:Concentrations Reported in Micrograms per Liter (μg/L)Bold = Concentration Exceeds NCAC 2B StandardSW-4SW-5SW-6SW-7SW-10SW-11SW-8SW-9"NCAC 2B Standard" based on the most stringent of human health or freshwater aquatic life values, as applicable to a Class C water per 2-5-2010 EPA and NC standards and criteriaRisk Based Screening Level calculated based on 45-day per year adolescent exposure frequency to Reedy Fork Creek (HHRA, July 2009)SW-1SW-2SW-3TABLE 6Summary of Three Most Recent Surface Water Sampling EventsWysong & Miles CorporationGreensboro, North CarolinaH&H Job No. WYM-002S:\AAA-Master Projects\Wysong & Miles - WYM\H&H 2010\RAP\RAP Revision 3-2010\Tables\RAP Tables.xlsHart & Hickman, PC
Well DateChloroethane 1,1-DCA 1,2-DCA 1,1-DCE cis-1,2-DCE 1,4-Dioxane PCE 1,1,1-TCA 1,1,2-TCA TCE Vinyl Chloride6/23/2006ND ND ND ND ND NS ND ND ND NDND5/16/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND NS ND ND ND NDND5/16/2007ND ND ND ND ND NS ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/16/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/23/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/16/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/23/2007ND ND ND ND ND6.0ND ND ND NDND6/23/2006ND ND ND ND ND11ND ND ND NDND5/16/2007ND ND ND ND ND ND ND ND ND NDND6/23/2006ND ND ND ND ND ND ND ND ND NDND5/16/2007ND ND ND ND ND ND ND ND ND NDNDNCAC 2B Standard550 20000 37 5400 4900 110 3.3 2500 16 302.4Risk Based Screening Level 190000 610 40 3000 3900 20000 8.5 80000 61 37038NOTES:Concentrations Reported in Micrograms per Liter (μg/L)Bold = Concentration Exceeds NCAC 2B StandardH&H Job No. WYM-002SW-10ATABLE 7Summary of Pore Water Sampling EventsWysong & Miles CorporationGreensboro, North Carolina"NCAC 2B Standard" based on the most stringent of human health or freshwater aquatic life values, as applicable to a Class C water per 2-5-2010 EPA and NC standards and criteriaRisk Based Screening Level calculated based on 45-day per year adolescent exposure frequency to Reedy Fork Creek (HHRA, July 2009)SW-11ASW-8ASW-9ASW-4ASW-5ASW-6ASW-7AS:\AAA-Master Projects\Wysong & Miles - WYM\H&H 2010\RAP\RAP Revision 3-2010\Tables\RAP Tables.xlsHart & Hickman, PC
Table1
SummaryofGroundwaterAnalyticalResults
August2010
Wysong&Miles
Greensboro,NorthCarolina
H&HProjectNo.WYMͲ003
compoundsexceeding2L
1,1ͲDichloroethene 7 38 120 170
1,4ͲDioxane 3 NE 37 65
1,2ͲDichloroethane 0.4 20 <1.0 1.4
compoundsbelow2L
1,1,1ͲTrichloroethane 200 1,500 19 37
1,1,2ͲTrichloroethane NE 44 <1.0 2.0
1,1ͲDichloroethane 6 65 4.2 2.0
Chloroform 70 7.3 <1.0 2.2
Notes:
intrusion(1/25/2010)
NE=NotEstablished
BoldvaluesexceedNC2Lgroundwaterstandards.
HighlightedandboxedvaluesexceedIHSBscreeninglevelsforvaporintrusion.
Onlycompoundsdetectedarelisted.
2.NCInactiveHazardousSitesBranch(IHSB)groundwaterscreeninglevelforresidentialvapor
NCGround
Water
Standard1
Vapor
Intrusion
Screening
Levels2
1.NorthCarolina2Lgroundwaterstandards
Compound
Concentrationsin(ђg/L)
Concentrationsin(ђg/L)
PWRͲ8PWRͲ7
S:\AAAͲMasterProjects\Wysong&MilesͲWYM\H&H2010\PennstonWellInstallJune2010\Report\WYMͲ003ReportTables9Ͳ15Ͳ10.xlsx

Appendix C

Soil Boring Logs and Well Construction Records
NOTES: Well completed with flush mount manhole cover.
generated using GroundLogs.online
Client:
Project:
Address:
NC DOT
ROW-603
Greensboro, NC
WELL LOG
Well No.
Page:
MW-1/SB-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/19/2019
11/21/2019
IET
HSA/Air Rotary
AMS Power Probe
M. Tynan
C. Goodwin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
30.0
8.50
Grab
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
30.0
2.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent.-Cement Grout/Bent.Chips
Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
GR
(0') Elastic SILT (MH); soft, moist, brown
(1') Elastic SILT (MH); trace fine-medium sand, medium stiff, moist, brown, orange
(4') SILT (ML); stiff, moist, light brown
(6') SILT (ML); hard, moist, reddish-brown
(16.5') SILT (ML); trace fine-coarse gravel, few fine-medium sand, hard, pale brown,
hollow stem auger refusal
(30') Boring terminated
9.4
2.3
2.5
1.9
1.5
1.9
2.3
1.5
SB-1(15-16.5)
0
5
10
15
20
25
30
35
N/A
23.3
N/A
N/A
NOTES: Well completed with metal stickup cover.
generated using GroundLogs.online
Client:
Project:
Address:
NC DOT
ROW-603
Greensboro, NC
WELL LOG
Well No.
Page:
MW-2/SB-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/19/2019
11/21/2019
IET
HSA
AMS Power Probe
M. Tynan
C. Goodwin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
32.0
8.50
Grab
27.5
29.23
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
32.0
2.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent.-Cement Grout/Bent.Chips
Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
GR
GR
(0') SILT with sand (ML); soft, moist, brown
(0.5') Elastic SILT with sand (MH); stiff, moist, dark red
(5.5') SILT with sand (ML); stiff, moist, reddish, orange
(10') 10-10.5 quartz rock
(10.5') SILT with sand (ML); stiff, moist, light brown
(14') Sandy SILT (ML); medium stiff, moist, light reddish-brown
(23') SILT with sand (ML); stiff, moist, pale white
(24') Elastic SILT with gravel (MH); medium stiff, moist, pale brown
(24.5') As Above: Quartz rock
(27.5') Sandy SILT (ML); soft, wet, white
(29') SILT with sand (ML); medium stiff, wet, very dark white, trace weathered rock
(32') Boring terminated
10.8
2.7
2.3
2.4
2.8
3.4
3.5
2.1
1.2
2.0
2.6
2.0
1.8
SB-2(22-24)
SB-2(15-17)
0
5
10
15
20
25
30
35
N/A
N/A
NOTES: Well completed with metal stickup cover.
generated using GroundLogs.online
Client:
Project:
Address:
NC DOT
ROW-603
Greensboro, NC
WELL LOG
Well No.
Page:
MW-3/SB-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/20/2019
11/21/2019
IET
HSA
AMS Power Probe
M. Tynan
C. Goodwin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
31.0
8.50
Grab
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
31.0
2.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent.-Cement Grout/Bent.Chips
Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
GR
GR
(0') Sandy lean CLAY (CL); medium plasticity, soft, moist, reddish-brown
(1') Elastic SILT (MH); medium stiff, moist, red
(5.5') Sandy SILT (ML); medium stiff, moist, reddish, orange
(8') Sandy SILT (ML); medium stiff, moist, orange, with black flecking
(15') Sandy SILT (ML); medium stiff, moist, orange, with black flecking, micaceous
(19') Sandy lean CLAY (CL); medium plasticity, stiff, moist, red, micaceous
(24') Elastic SILT with sand (MH); stiff, moist, reddish-brown, micaceous
(29') As Above: trace weathered rock
(31') Boring terminated
1.3
1.7
3.7
2.6
3.4
5.7
2.5
3.7
0.6
1.0
2.5
0.2
0.8
1.1
1.5
SB-3(15-17)
SB-3(17-19)
0
5
10
15
20
25
30
35
N/A
N/A
N/A
N/A
NOTES: Well completed with metal stickup cover.
generated using GroundLogs.online
Client:
Project:
Address:
NC DOT
ROW-603
Greensboro, NC
WELL LOG
Well No.
Page:
MW-4/SB-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/20/2019
11/21/2019
IET
HSA
AMS Power Probe
M. Tynan
C. Goodwin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
31.0
8.50
Grab
30.0
29.05
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
31.0
2.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent.-Cement Grout/Bent.Chips
Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
GR
GR
(0') Elastic SILT (MH); stiff, moist, red, micaceous
(5') SILT with sand (ML); soft, moist, orange, micaceous
(10') SILT with sand (ML); soft, moist, gray, orange, micaceous
(11') SILT with sand (ML); soft, moist, light gray, micaceous
(22') SILT with sand (ML); soft, moist, light brown, gray, micaceous
(25') SILT with sand (ML); medium stiff, moist, gray
(26') SILT with sand (ML); soft, moist, light gray
(28.5') BEDROCK: hollow stem auger refusal
(31') Boring terminated
0.5
0.9
0.5
0.2
0.3
0.2
0.2
0.2
0.3
0.0
0.3
0.9
1.0
0.7
1.1
SB-4(15-17)
SB-4(19-21)
0
5
10
15
20
25
30
35
N/A
N/A
NOTES: Well completed with flush mount manhole cover.
generated using GroundLogs.online
Client:
Project:
Address:
NC DOT
ROW-603
Greensboro, NC
WELL LOG
Well No.
Page:
MW-5/SB-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/21/2019
11/21/2019
IET
HSA
AMS Power Probe
M. Tynan
C. Goodwin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
30.0
8.50
Grab
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
30.0
2.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent.-Cement Grout/Bent.Chips
Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
GR
GR
(0') Elastic SILT (MH); medium stiff, moist, reddish-brown
(0.5') Elastic SILT (MH); stiff, moist, red, micaceous
(3') SILT with sand (ML); stiff, moist, red, orange, micaceous
(5.5') SILT (ML); medium stiff, moist, orange
(8.5') SILT with sand (ML); soft, moist, yellow
(11') SILT with sand (ML); soft, moist, white
(14') Elastic SILT (MH); medium stiff, moist, red
(15') SILT with sand (ML); soft, moist, white
(21') SILT with sand (ML); soft, moist, dark yellowish-white
(22') As Above: possible organic material
(24') SILT with sand (ML); soft, moist, brown, black flecking
(30') Boring terminated
2.4
1.1
1.3
0.8
1.0
1.1
0.8
0.6
0.3
0.8
0.7
1.0
1.2
0.8
1.0
SB-5(15-17)
SB-5(19-21)
0
5
10
15
20
25
30
35
N/A
N/A
N/A
N/A
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #: Guilford County #014-19-MW5-RW0
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)

N W
6. Is(are) the well(s):□Permanent or □Temporary
7. Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12.Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
11/21/19 MW-1
NCDOT
3600 Reedy Fork Pkwy, Greensboro 27405
Guilford
36 10 22.195 79 42 37.051
30
~25
8.5
auger & air rotary
11/22/19
25 30 pwr
0 15 2 Sch40 PVC
15 30 2 0.010 Sch40 PVC
0
6
13
6
13
30
concrete
bentonite
#2 silica sand pour through augers
pour
See Report
Well completed at surface with manhole & 2'x2' concrete
pad. (lock & tag)
Print Form
pour
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #:Guilford County #014-19-MW5-RW0
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)

N W
6. Is(are) the well(s):□Permanent or □Temporary
7. Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12.Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
11/21/19 MW-2
NCDOT
3600 Reedy Fork Pkwy, Greensboro 27405
Guilford
36 10 20.219 79 42 35.039
32
~28
8.5
auger
11/22/19
28 32 saprolite
0 17 2 Sch40 PVC
17 32 2 0.010 Sch40 PVC
0
6
15
6
15
32
concrete
bentonite
#2 silica sand pour through augers
pour
See Report
Well completed at surface with aboveground well cover &
2'x2' concrete pad. (lock & tag)
Print Form
pour
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #:Guilford County #014-19-MW5-RW0
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)

N W
6. Is(are) the well(s):□Permanent or □Temporary
7. Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12.Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
11/21/19 MW-3
NCDOT
3600 Reedy Fork Pkwy, Greensboro 27405
Guilford
36 10 18.919 79 42 33.498
31
none
8.5
auger
11/22/19
0 16 2 Sch40 PVC
16 31 2 0.010 Sch40 PVC
0
6
14
6
14
31
concrete
bentonite
#2 silica sand pour through augers
pour
See Report
Well completed at surface with aboveground well cover &
2'x2' concrete pad. (lock & tag)
Print Form
pour
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name
2.Well Construction Permit #:Guilford County #014-19-MW5-RW0
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3.Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)

N W
6. Is(are) the well(s):□Permanent or □Temporary
7. Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
11/21/19 MW-4
NCDOT
3600 Reedy Fork Pkwy, Greensboro 27405
Guilford
36 10 19.171 79 42 39.118
31
28
8.5
auger & air rotary
11/22/19
28 31 pwr
0 16 2 Sch40 PVC
16 31 2 0.010 Sch40 PVC
0
6
14
6
14
31
concrete
bentonite
#2 silica sand pour through augers
pour
See Report
Well completed at surface with aboveground well cover &
2'x2' concrete pad. (lock & tag)
Print Form
pour
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #:Guilford County #014-19-MW5-RW0
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)

N W
6. Is(are) the well(s):□Permanent or □Temporary
7. Is this a repair to an existing well:□Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10.Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12.Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
11/21/19 MW-5
NCDOT
3600 Reedy Fork Pkwy, Greensboro 27405
Guilford
36 10 17.764 79 42 37.422
30
none
8.5
auger
11/22/19
0 15 2 Sch40 PVC
15 30 2 0.010 Sch40 PVC
0
6
13
6
13
30
concrete
bentonite
#2 silica sand pour through augers
pour
See Report
Well completed at surface with manhole & 2'x2' concrete
pad. (lock & tag)
Print Form
pour

Appendix D

Laboratory Analytical Reports
#=CL#
January 14, 2020
LIMS USE: FR - DAVID GRAHAM
LIMS OBJECT ID: 92454623
92454623
Project:
Pace Project No.:
RE:
David Graham
Hart & Hickman
2923 S. Tryon Street
Charlotte, NC 28203
ROW-603
Dear David Graham:
Enclosed are the analytical results for sample(s) received by the laboratory on November 20, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 63
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92454623
ROW-603
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 63
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92454623
ROW-603
Lab ID Sample ID Matrix Date Collected Date Received
92454623001 SB-1 (15-16.5)Solid 11/19/19 12:35 11/20/19 10:26
92454623002 SB-2 (15-17)Solid 11/19/19 15:10 11/20/19 10:26
92454623003 SB-2 (22-24)Solid 11/19/19 15:45 11/20/19 10:26
92454623004 SB-3 (15-17)Solid 11/20/19 09:20 11/20/19 10:26
92454623005 SB-3 (17-19)Solid 11/20/19 10:05 11/20/19 10:26
92454623006 Trip Blank Water 11/20/19 00:00 11/20/19 10:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 63
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92454623
ROW-603
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92454623001 SB-1 (15-16.5)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
92454623002 SB-2 (15-17)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
92454623003 SB-2 (22-24)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92454623004 SB-3 (15-17)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
92454623005 SB-3 (17-19)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92454623006 Trip Blank EPA 8260D 63 PASI-CGAW
EPA 8260D Mod.3 PASI-CLMB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-1 (15-16.5)Lab ID: 92454623001 Collected: 11/19/19 12:35 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic ND mg/kg 11/23/19 01:32 7440-38-211/21/19 16:351.0 0.52 1
Barium 355 mg/kg 11/23/19 01:32 7440-39-311/21/19 16:350.52 0.26 1
Cadmium ND mg/kg 11/23/19 01:32 7440-43-911/21/19 16:350.10 0.052 1
Chromium 18.6 mg/kg 11/23/19 01:32 7440-47-311/21/19 16:350.52 0.26 1
Lead 1.2 mg/kg 11/23/19 01:32 7439-92-111/21/19 16:350.52 0.26 1
Selenium 1.0J mg/kg 11/23/19 01:32 7782-49-211/21/19 16:351.0 0.52 1
Silver ND mg/kg 11/23/19 01:32 7440-22-411/21/19 16:350.52 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.0024J mg/kg 11/22/19 12:04 7439-97-6 B,BC11/21/19 11:570.0025 0.0012 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/25/19 20:29 83-32-911/23/19 13:400.35 0.089 1
Acenaphthylene ND mg/kg 11/25/19 20:29 208-96-811/23/19 13:400.35 0.082 1
Aniline ND mg/kg 11/25/19 20:29 62-53-311/23/19 13:400.35 0.078 1
Anthracene ND mg/kg 11/25/19 20:29 120-12-711/23/19 13:400.35 0.090 1
Benzo(a)anthracene ND mg/kg 11/25/19 20:29 56-55-311/23/19 13:400.35 0.11 1
Benzo(a)pyrene ND mg/kg 11/25/19 20:29 50-32-811/23/19 13:400.35 0.15 1
Benzo(b)fluoranthene ND mg/kg 11/25/19 20:29 205-99-211/23/19 13:400.35 0.14 1
Benzo(g,h,i)perylene ND mg/kg 11/25/19 20:29 191-24-211/23/19 13:400.35 0.14 1
Benzo(k)fluoranthene ND mg/kg 11/25/19 20:29 207-08-911/23/19 13:400.35 0.15 1
Benzoic Acid ND mg/kg 11/25/19 20:29 65-85-011/23/19 13:401.7 0.37 1
Benzyl alcohol ND mg/kg 11/25/19 20:29 100-51-611/23/19 13:400.69 0.18 1
4-Bromophenylphenyl ether ND mg/kg 11/25/19 20:29 101-55-311/23/19 13:400.35 0.091 1
Butylbenzylphthalate ND mg/kg 11/25/19 20:29 85-68-711/23/19 13:400.35 0.092 1
4-Chloro-3-methylphenol ND mg/kg 11/25/19 20:29 59-50-711/23/19 13:400.69 0.21 1
4-Chloroaniline ND mg/kg 11/25/19 20:29 106-47-811/23/19 13:401.7 0.21 1
bis(2-Chloroethoxy)methane ND mg/kg 11/25/19 20:29 111-91-111/23/19 13:400.35 0.093 1
bis(2-Chloroethyl) ether ND mg/kg 11/25/19 20:29 111-44-411/23/19 13:400.35 0.074 1
2-Chloronaphthalene ND mg/kg 11/25/19 20:29 91-58-711/23/19 13:400.35 0.077 1
2-Chlorophenol ND mg/kg 11/25/19 20:29 95-57-811/23/19 13:400.35 0.081 1
4-Chlorophenylphenyl ether ND mg/kg 11/25/19 20:29 7005-72-311/23/19 13:400.35 0.090 1
Chrysene ND mg/kg 11/25/19 20:29 218-01-911/23/19 13:400.35 0.10 1
Dibenz(a,h)anthracene ND mg/kg 11/25/19 20:29 53-70-311/23/19 13:400.35 0.14 1
Dibenzofuran ND mg/kg 11/25/19 20:29 132-64-911/23/19 13:400.35 0.087 1
1,2-Dichlorobenzene ND mg/kg 11/25/19 20:29 95-50-111/23/19 13:400.35 0.075 1
1,3-Dichlorobenzene ND mg/kg 11/25/19 20:29 541-73-111/23/19 13:400.35 0.078 1
1,4-Dichlorobenzene ND mg/kg 11/25/19 20:29 106-46-711/23/19 13:400.35 0.076 1
3,3'-Dichlorobenzidine ND mg/kg 11/25/19 20:29 91-94-111/23/19 13:401.7 0.24 1
2,4-Dichlorophenol ND mg/kg 11/25/19 20:29 120-83-211/23/19 13:400.35 0.11 1
Diethylphthalate ND mg/kg 11/25/19 20:29 84-66-211/23/19 13:400.35 0.075 1
2,4-Dimethylphenol ND mg/kg 11/25/19 20:29 105-67-911/23/19 13:400.35 0.086 1
Dimethylphthalate ND mg/kg 11/25/19 20:29 131-11-311/23/19 13:400.35 0.078 1
Di-n-butylphthalate ND mg/kg 11/25/19 20:29 84-74-211/23/19 13:400.35 0.086 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/25/19 20:29 534-52-111/23/19 13:400.69 0.56 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-1 (15-16.5)Lab ID: 92454623001 Collected: 11/19/19 12:35 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/25/19 20:29 51-28-511/23/19 13:401.7 1.1 1
2,4-Dinitrotoluene ND mg/kg 11/25/19 20:29 121-14-211/23/19 13:400.35 0.092 1
2,6-Dinitrotoluene ND mg/kg 11/25/19 20:29 606-20-211/23/19 13:400.35 0.091 1
Di-n-octylphthalate ND mg/kg 11/25/19 20:29 117-84-011/23/19 13:400.35 0.20 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/25/19 20:29 117-81-711/23/19 13:400.35 0.11 1
Fluoranthene ND mg/kg 11/25/19 20:29 206-44-011/23/19 13:400.35 0.10 1
Fluorene ND mg/kg 11/25/19 20:29 86-73-711/23/19 13:400.35 0.093 1
Hexachloro-1,3-butadiene ND mg/kg 11/25/19 20:29 87-68-311/23/19 13:400.35 0.084 1
Hexachlorobenzene ND mg/kg 11/25/19 20:29 118-74-111/23/19 13:400.35 0.088 1
Hexachlorocyclopentadiene ND mg/kg 11/25/19 20:29 77-47-411/23/19 13:400.35 0.14 1
Hexachloroethane ND mg/kg 11/25/19 20:29 67-72-111/23/19 13:400.35 0.079 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/25/19 20:29 193-39-511/23/19 13:400.35 0.16 1
Isophorone ND mg/kg 11/25/19 20:29 78-59-111/23/19 13:400.35 0.075 1
1-Methylnaphthalene ND mg/kg 11/25/19 20:29 90-12-011/23/19 13:400.35 0.092 1
2-Methylnaphthalene ND mg/kg 11/25/19 20:29 91-57-611/23/19 13:400.35 0.088 1
2-Methylphenol(o-Cresol)ND mg/kg 11/25/19 20:29 95-48-711/23/19 13:400.35 0.077 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/25/19 20:29 15831-10-411/23/19 13:400.35 0.087 1
Naphthalene ND mg/kg 11/25/19 20:29 91-20-311/23/19 13:400.35 0.083 1
2-Nitroaniline ND mg/kg 11/25/19 20:29 88-74-411/23/19 13:401.7 0.17 1
3-Nitroaniline ND mg/kg 11/25/19 20:29 99-09-211/23/19 13:401.7 0.18 1
4-Nitroaniline ND mg/kg 11/25/19 20:29 100-01-611/23/19 13:400.69 0.17 1
Nitrobenzene ND mg/kg 11/25/19 20:29 98-95-311/23/19 13:400.35 0.083 1
2-Nitrophenol ND mg/kg 11/25/19 20:29 88-75-511/23/19 13:400.35 0.11 1
4-Nitrophenol ND mg/kg 11/25/19 20:29 100-02-711/23/19 13:401.7 0.55 1
N-Nitrosodimethylamine ND mg/kg 11/25/19 20:29 62-75-911/23/19 13:400.35 0.098 1
N-Nitroso-di-n-propylamine ND mg/kg 11/25/19 20:29 621-64-711/23/19 13:400.35 0.097 1
N-Nitrosodiphenylamine ND mg/kg 11/25/19 20:29 86-30-611/23/19 13:400.35 0.089 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/25/19 20:29 108-60-111/23/19 13:400.35 0.096 1
Pentachlorophenol ND mg/kg 11/25/19 20:29 87-86-511/23/19 13:401.7 0.16 1
Phenanthrene ND mg/kg 11/25/19 20:29 85-01-811/23/19 13:400.35 0.087 1
Phenol ND mg/kg 11/25/19 20:29 108-95-211/23/19 13:400.35 0.083 1
Pyrene ND mg/kg 11/25/19 20:29 129-00-011/23/19 13:400.35 0.096 1
Pyridine ND mg/kg 11/25/19 20:29 110-86-111/23/19 13:400.35 0.088 1
1,2,4-Trichlorobenzene ND mg/kg 11/25/19 20:29 120-82-111/23/19 13:400.35 0.080 1
2,4,5-Trichlorophenol ND mg/kg 11/25/19 20:29 95-95-411/23/19 13:400.35 0.090 1
2,4,6-Trichlorophenol ND mg/kg 11/25/19 20:29 88-06-211/23/19 13:400.35 0.087 1
Surrogates
Nitrobenzene-d5 (S)38 %11/25/19 20:29 4165-60-011/23/19 13:4023-110 1
2-Fluorobiphenyl (S)40 %11/25/19 20:29 321-60-811/23/19 13:4030-110 1
Terphenyl-d14 (S)58 %11/25/19 20:29 1718-51-011/23/19 13:4028-110 1
Phenol-d6 (S)38 %11/25/19 20:29 13127-88-311/23/19 13:4022-110 1
2-Fluorophenol (S)40 %11/25/19 20:29 367-12-411/23/19 13:4013-110 1
2,4,6-Tribromophenol (S)39 %11/25/19 20:29 118-79-611/23/19 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-1 (15-16.5)Lab ID: 92454623001 Collected: 11/19/19 12:35 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 11/24/19 20:19 67-64-111/24/19 13:480.087 0.0082 1
Benzene ND mg/kg 11/24/19 20:19 71-43-211/24/19 13:480.0043 0.00078 1
Bromobenzene ND mg/kg 11/24/19 20:19 108-86-111/24/19 13:480.0043 0.0012 1
Bromochloromethane ND mg/kg 11/24/19 20:19 74-97-511/24/19 13:480.0043 0.0011 1
Bromodichloromethane ND mg/kg 11/24/19 20:19 75-27-411/24/19 13:480.0043 0.00085 1
Bromoform ND mg/kg 11/24/19 20:19 75-25-211/24/19 13:480.0043 0.0021 1
Bromomethane ND mg/kg 11/24/19 20:19 74-83-9 IH11/24/19 13:480.0087 0.0020 1
2-Butanone (MEK)ND mg/kg 11/24/19 20:19 78-93-311/24/19 13:480.087 0.010 1
n-Butylbenzene ND mg/kg 11/24/19 20:19 104-51-811/24/19 13:480.0043 0.0024 1
sec-Butylbenzene ND mg/kg 11/24/19 20:19 135-98-811/24/19 13:480.0043 0.0018 1
tert-Butylbenzene ND mg/kg 11/24/19 20:19 98-06-611/24/19 13:480.0043 0.0015 1
Carbon tetrachloride ND mg/kg 11/24/19 20:19 56-23-511/24/19 13:480.0043 0.00083 1
Chlorobenzene ND mg/kg 11/24/19 20:19 108-90-711/24/19 13:480.0043 0.00084 1
Chloroethane ND mg/kg 11/24/19 20:19 75-00-311/24/19 13:480.0087 0.0018 1
Chloroform ND mg/kg 11/24/19 20:19 67-66-311/24/19 13:480.0043 0.00092 1
Chloromethane ND mg/kg 11/24/19 20:19 74-87-311/24/19 13:480.0087 0.0028 1
2-Chlorotoluene ND mg/kg 11/24/19 20:19 95-49-811/24/19 13:480.0043 0.0013 1
4-Chlorotoluene ND mg/kg 11/24/19 20:19 106-43-411/24/19 13:480.0043 0.0013 1
1,2-Dibromo-3-chloropropane ND mg/kg 11/24/19 20:19 96-12-811/24/19 13:480.0043 0.0022 1
Dibromochloromethane ND mg/kg 11/24/19 20:19 124-48-111/24/19 13:480.0043 0.0022 1
1,2-Dibromoethane (EDB)ND mg/kg 11/24/19 20:19 106-93-411/24/19 13:480.0043 0.00097 1
Dibromomethane ND mg/kg 11/24/19 20:19 74-95-311/24/19 13:480.0043 0.0013 1
1,2-Dichlorobenzene ND mg/kg 11/24/19 20:19 95-50-111/24/19 13:480.0043 0.0015 1
1,3-Dichlorobenzene ND mg/kg 11/24/19 20:19 541-73-111/24/19 13:480.0043 0.0015 1
1,4-Dichlorobenzene ND mg/kg 11/24/19 20:19 106-46-711/24/19 13:480.0043 0.0015 1
Dichlorodifluoromethane ND mg/kg 11/24/19 20:19 75-71-811/24/19 13:480.0087 0.0036 1
1,1-Dichloroethane ND mg/kg 11/24/19 20:19 75-34-311/24/19 13:480.0043 0.00064 1
1,2-Dichloroethane ND mg/kg 11/24/19 20:19 107-06-211/24/19 13:480.0043 0.00087 1
1,1-Dichloroethene ND mg/kg 11/24/19 20:19 75-35-411/24/19 13:480.0043 0.0010 1
cis-1,2-Dichloroethene ND mg/kg 11/24/19 20:19 156-59-211/24/19 13:480.0043 0.00075 1
trans-1,2-Dichloroethene ND mg/kg 11/24/19 20:19 156-60-511/24/19 13:480.0043 0.00085 1
1,2-Dichloropropane ND mg/kg 11/24/19 20:19 78-87-511/24/19 13:480.0043 0.0016 1
1,3-Dichloropropane ND mg/kg 11/24/19 20:19 142-28-911/24/19 13:480.0043 0.0016 1
2,2-Dichloropropane ND mg/kg 11/24/19 20:19 594-20-711/24/19 13:480.0043 0.00043 1
1,1-Dichloropropene ND mg/kg 11/24/19 20:19 563-58-611/24/19 13:480.0043 0.0018 1
cis-1,3-Dichloropropene ND mg/kg 11/24/19 20:19 10061-01-511/24/19 13:480.0043 0.0020 1
trans-1,3-Dichloropropene ND mg/kg 11/24/19 20:19 10061-02-611/24/19 13:480.0043 0.00076 1
Diisopropyl ether ND mg/kg 11/24/19 20:19 108-20-311/24/19 13:480.0043 0.0025 1
Ethylbenzene ND mg/kg 11/24/19 20:19 100-41-411/24/19 13:480.0043 0.00092 1
Hexachloro-1,3-butadiene ND mg/kg 11/24/19 20:19 87-68-311/24/19 13:480.0043 0.0021 1
2-Hexanone ND mg/kg 11/24/19 20:19 591-78-611/24/19 13:480.043 0.0045 1
Isopropylbenzene (Cumene)ND mg/kg 11/24/19 20:19 98-82-811/24/19 13:480.0043 0.0013 1
p-Isopropyltoluene ND mg/kg 11/24/19 20:19 99-87-611/24/19 13:480.0043 0.0021 1
Methylene Chloride ND mg/kg 11/24/19 20:19 75-09-211/24/19 13:480.017 0.0051 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 11/24/19 20:19 108-10-111/24/19 13:480.043 0.0032 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-1 (15-16.5)Lab ID: 92454623001 Collected: 11/19/19 12:35 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 11/24/19 20:19 1634-04-411/24/19 13:480.0043 0.0025 1
Naphthalene ND mg/kg 11/24/19 20:19 91-20-311/24/19 13:480.0043 0.0037 1
n-Propylbenzene ND mg/kg 11/24/19 20:19 103-65-111/24/19 13:480.0043 0.0014 1
Styrene ND mg/kg 11/24/19 20:19 100-42-511/24/19 13:480.0043 0.0013 1
1,1,1,2-Tetrachloroethane ND mg/kg 11/24/19 20:19 630-20-611/24/19 13:480.0043 0.0011 1
1,1,2,2-Tetrachloroethane ND mg/kg 11/24/19 20:19 79-34-511/24/19 13:480.0043 0.0015 1
Tetrachloroethene ND mg/kg 11/24/19 20:19 127-18-411/24/19 13:480.0043 0.0014 1
Toluene ND mg/kg 11/24/19 20:19 108-88-311/24/19 13:480.0043 0.0014 1
1,2,3-Trichlorobenzene ND mg/kg 11/24/19 20:19 87-61-611/24/19 13:480.0043 0.0031 1
1,2,4-Trichlorobenzene ND mg/kg 11/24/19 20:19 120-82-111/24/19 13:480.0043 0.0023 1
1,1,1-Trichloroethane ND mg/kg 11/24/19 20:19 71-55-611/24/19 13:480.0043 0.00075 1
1,1,2-Trichloroethane ND mg/kg 11/24/19 20:19 79-00-511/24/19 13:480.0043 0.00098 1
Trichloroethene ND mg/kg 11/24/19 20:19 79-01-611/24/19 13:480.0043 0.0011 1
Trichlorofluoromethane ND mg/kg 11/24/19 20:19 75-69-411/24/19 13:480.0043 0.0010 1
1,2,3-Trichloropropane ND mg/kg 11/24/19 20:19 96-18-411/24/19 13:480.0043 0.0015 1
1,2,4-Trimethylbenzene ND mg/kg 11/24/19 20:19 95-63-611/24/19 13:480.0043 0.0017 1
1,3,5-Trimethylbenzene ND mg/kg 11/24/19 20:19 108-67-811/24/19 13:480.0043 0.0014 1
Vinyl acetate ND mg/kg 11/24/19 20:19 108-05-4 IL11/24/19 13:480.043 0.014 1
Vinyl chloride ND mg/kg 11/24/19 20:19 75-01-411/24/19 13:480.0087 0.0016 1
Xylene (Total)ND mg/kg 11/24/19 20:19 1330-20-711/24/19 13:480.0087 0.0030 1
m&p-Xylene ND mg/kg 11/24/19 20:19 179601-23-111/24/19 13:480.0087 0.0020 1
o-Xylene ND mg/kg 11/24/19 20:19 95-47-611/24/19 13:480.0043 0.0010 1
Surrogates
Toluene-d8 (S)110 %11/24/19 20:19 2037-26-511/24/19 13:4870-130 1
4-Bromofluorobenzene (S)103 %11/24/19 20:19 460-00-411/24/19 13:4870-130 1
1,2-Dichloroethane-d4 (S)103 %11/24/19 20:19 17060-07-011/24/19 13:4870-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)ND mg/kg 11/25/19 12:16 123-91-111/25/19 11:520.0084 0.0025 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %11/25/19 12:16 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)100 %11/25/19 12:16 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 3.7 %11/21/19 13:250.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-2 (15-17)Lab ID: 92454623002 Collected: 11/19/19 15:10 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 0.78J mg/kg 11/23/19 01:41 7440-38-211/21/19 16:351.2 0.61 1
Barium 453 mg/kg 11/23/19 01:41 7440-39-311/21/19 16:350.61 0.31 1
Cadmium ND mg/kg 11/23/19 01:41 7440-43-911/21/19 16:350.12 0.061 1
Chromium 21.4 mg/kg 11/23/19 01:41 7440-47-311/21/19 16:350.61 0.31 1
Lead 7.2 mg/kg 11/23/19 01:41 7439-92-111/21/19 16:350.61 0.31 1
Selenium 0.87J mg/kg 11/23/19 01:41 7782-49-211/21/19 16:351.2 0.61 1
Silver ND mg/kg 11/23/19 01:41 7440-22-411/21/19 16:350.61 0.31 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.012 mg/kg 11/22/19 12:06 7439-97-6 B,BC11/21/19 11:570.0048 0.0024 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/25/19 21:02 83-32-911/23/19 13:400.41 0.10 1
Acenaphthylene ND mg/kg 11/25/19 21:02 208-96-811/23/19 13:400.41 0.096 1
Aniline ND mg/kg 11/25/19 21:02 62-53-311/23/19 13:400.41 0.091 1
Anthracene ND mg/kg 11/25/19 21:02 120-12-711/23/19 13:400.41 0.11 1
Benzo(a)anthracene ND mg/kg 11/25/19 21:02 56-55-311/23/19 13:400.41 0.13 1
Benzo(a)pyrene ND mg/kg 11/25/19 21:02 50-32-811/23/19 13:400.41 0.18 1
Benzo(b)fluoranthene ND mg/kg 11/25/19 21:02 205-99-211/23/19 13:400.41 0.16 1
Benzo(g,h,i)perylene ND mg/kg 11/25/19 21:02 191-24-211/23/19 13:400.41 0.16 1
Benzo(k)fluoranthene ND mg/kg 11/25/19 21:02 207-08-911/23/19 13:400.41 0.17 1
Benzoic Acid ND mg/kg 11/25/19 21:02 65-85-011/23/19 13:402.0 0.44 1
Benzyl alcohol ND mg/kg 11/25/19 21:02 100-51-611/23/19 13:400.81 0.22 1
4-Bromophenylphenyl ether ND mg/kg 11/25/19 21:02 101-55-311/23/19 13:400.41 0.11 1
Butylbenzylphthalate ND mg/kg 11/25/19 21:02 85-68-711/23/19 13:400.41 0.11 1
4-Chloro-3-methylphenol ND mg/kg 11/25/19 21:02 59-50-711/23/19 13:400.81 0.25 1
4-Chloroaniline ND mg/kg 11/25/19 21:02 106-47-811/23/19 13:402.0 0.25 1
bis(2-Chloroethoxy)methane ND mg/kg 11/25/19 21:02 111-91-111/23/19 13:400.41 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 11/25/19 21:02 111-44-411/23/19 13:400.41 0.086 1
2-Chloronaphthalene ND mg/kg 11/25/19 21:02 91-58-711/23/19 13:400.41 0.091 1
2-Chlorophenol ND mg/kg 11/25/19 21:02 95-57-811/23/19 13:400.41 0.095 1
4-Chlorophenylphenyl ether ND mg/kg 11/25/19 21:02 7005-72-311/23/19 13:400.41 0.11 1
Chrysene ND mg/kg 11/25/19 21:02 218-01-911/23/19 13:400.41 0.12 1
Dibenz(a,h)anthracene ND mg/kg 11/25/19 21:02 53-70-311/23/19 13:400.41 0.16 1
Dibenzofuran ND mg/kg 11/25/19 21:02 132-64-911/23/19 13:400.41 0.10 1
1,2-Dichlorobenzene ND mg/kg 11/25/19 21:02 95-50-111/23/19 13:400.41 0.088 1
1,3-Dichlorobenzene ND mg/kg 11/25/19 21:02 541-73-111/23/19 13:400.41 0.092 1
1,4-Dichlorobenzene ND mg/kg 11/25/19 21:02 106-46-711/23/19 13:400.41 0.089 1
3,3'-Dichlorobenzidine ND mg/kg 11/25/19 21:02 91-94-111/23/19 13:402.0 0.28 1
2,4-Dichlorophenol ND mg/kg 11/25/19 21:02 120-83-211/23/19 13:400.41 0.13 1
Diethylphthalate ND mg/kg 11/25/19 21:02 84-66-211/23/19 13:400.41 0.088 1
2,4-Dimethylphenol ND mg/kg 11/25/19 21:02 105-67-911/23/19 13:400.41 0.10 1
Dimethylphthalate ND mg/kg 11/25/19 21:02 131-11-311/23/19 13:400.41 0.092 1
Di-n-butylphthalate ND mg/kg 11/25/19 21:02 84-74-211/23/19 13:400.41 0.10 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/25/19 21:02 534-52-111/23/19 13:400.81 0.66 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-2 (15-17)Lab ID: 92454623002 Collected: 11/19/19 15:10 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/25/19 21:02 51-28-511/23/19 13:402.0 1.3 1
2,4-Dinitrotoluene ND mg/kg 11/25/19 21:02 121-14-211/23/19 13:400.41 0.11 1
2,6-Dinitrotoluene ND mg/kg 11/25/19 21:02 606-20-211/23/19 13:400.41 0.11 1
Di-n-octylphthalate ND mg/kg 11/25/19 21:02 117-84-011/23/19 13:400.41 0.23 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/25/19 21:02 117-81-711/23/19 13:400.41 0.13 1
Fluoranthene ND mg/kg 11/25/19 21:02 206-44-011/23/19 13:400.41 0.12 1
Fluorene ND mg/kg 11/25/19 21:02 86-73-711/23/19 13:400.41 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 11/25/19 21:02 87-68-311/23/19 13:400.41 0.099 1
Hexachlorobenzene ND mg/kg 11/25/19 21:02 118-74-111/23/19 13:400.41 0.10 1
Hexachlorocyclopentadiene ND mg/kg 11/25/19 21:02 77-47-4 M1,v211/23/19 13:400.41 0.16 1
Hexachloroethane ND mg/kg 11/25/19 21:02 67-72-111/23/19 13:400.41 0.093 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/25/19 21:02 193-39-511/23/19 13:400.41 0.19 1
Isophorone ND mg/kg 11/25/19 21:02 78-59-111/23/19 13:400.41 0.088 1
1-Methylnaphthalene ND mg/kg 11/25/19 21:02 90-12-011/23/19 13:400.41 0.11 1
2-Methylnaphthalene ND mg/kg 11/25/19 21:02 91-57-611/23/19 13:400.41 0.10 1
2-Methylphenol(o-Cresol)ND mg/kg 11/25/19 21:02 95-48-711/23/19 13:400.41 0.090 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/25/19 21:02 15831-10-411/23/19 13:400.41 0.10 1
Naphthalene ND mg/kg 11/25/19 21:02 91-20-311/23/19 13:400.41 0.097 1
2-Nitroaniline ND mg/kg 11/25/19 21:02 88-74-4 v111/23/19 13:402.0 0.20 1
3-Nitroaniline ND mg/kg 11/25/19 21:02 99-09-211/23/19 13:402.0 0.22 1
4-Nitroaniline ND mg/kg 11/25/19 21:02 100-01-611/23/19 13:400.81 0.20 1
Nitrobenzene ND mg/kg 11/25/19 21:02 98-95-311/23/19 13:400.41 0.097 1
2-Nitrophenol ND mg/kg 11/25/19 21:02 88-75-511/23/19 13:400.41 0.13 1
4-Nitrophenol ND mg/kg 11/25/19 21:02 100-02-711/23/19 13:402.0 0.65 1
N-Nitrosodimethylamine ND mg/kg 11/25/19 21:02 62-75-911/23/19 13:400.41 0.11 1
N-Nitroso-di-n-propylamine ND mg/kg 11/25/19 21:02 621-64-711/23/19 13:400.41 0.11 1
N-Nitrosodiphenylamine ND mg/kg 11/25/19 21:02 86-30-611/23/19 13:400.41 0.10 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/25/19 21:02 108-60-111/23/19 13:400.41 0.11 1
Pentachlorophenol ND mg/kg 11/25/19 21:02 87-86-511/23/19 13:402.0 0.19 1
Phenanthrene ND mg/kg 11/25/19 21:02 85-01-811/23/19 13:400.41 0.10 1
Phenol ND mg/kg 11/25/19 21:02 108-95-211/23/19 13:400.41 0.097 1
Pyrene ND mg/kg 11/25/19 21:02 129-00-011/23/19 13:400.41 0.11 1
Pyridine ND mg/kg 11/25/19 21:02 110-86-111/23/19 13:400.41 0.10 1
1,2,4-Trichlorobenzene ND mg/kg 11/25/19 21:02 120-82-111/23/19 13:400.41 0.093 1
2,4,5-Trichlorophenol ND mg/kg 11/25/19 21:02 95-95-411/23/19 13:400.41 0.11 1
2,4,6-Trichlorophenol ND mg/kg 11/25/19 21:02 88-06-211/23/19 13:400.41 0.10 1
Surrogates
Nitrobenzene-d5 (S)53 %11/25/19 21:02 4165-60-011/23/19 13:4023-110 1
2-Fluorobiphenyl (S)59 %11/25/19 21:02 321-60-811/23/19 13:4030-110 1
Terphenyl-d14 (S)68 %11/25/19 21:02 1718-51-011/23/19 13:4028-110 1
Phenol-d6 (S)51 %11/25/19 21:02 13127-88-311/23/19 13:4022-110 1
2-Fluorophenol (S)50 %11/25/19 21:02 367-12-411/23/19 13:4013-110 1
2,4,6-Tribromophenol (S)66 %11/25/19 21:02 118-79-611/23/19 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-2 (15-17)Lab ID: 92454623002 Collected: 11/19/19 15:10 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 11/24/19 20:44 67-64-111/24/19 13:480.11 0.010 1
Benzene ND mg/kg 11/24/19 20:44 71-43-211/24/19 13:480.0054 0.00098 1
Bromobenzene ND mg/kg 11/24/19 20:44 108-86-111/24/19 13:480.0054 0.0015 1
Bromochloromethane ND mg/kg 11/24/19 20:44 74-97-511/24/19 13:480.0054 0.0013 1
Bromodichloromethane ND mg/kg 11/24/19 20:44 75-27-411/24/19 13:480.0054 0.0011 1
Bromoform ND mg/kg 11/24/19 20:44 75-25-211/24/19 13:480.0054 0.0027 1
Bromomethane ND mg/kg 11/24/19 20:44 74-83-9 IH11/24/19 13:480.011 0.0026 1
2-Butanone (MEK)ND mg/kg 11/24/19 20:44 78-93-311/24/19 13:480.11 0.013 1
n-Butylbenzene ND mg/kg 11/24/19 20:44 104-51-811/24/19 13:480.0054 0.0031 1
sec-Butylbenzene ND mg/kg 11/24/19 20:44 135-98-811/24/19 13:480.0054 0.0023 1
tert-Butylbenzene ND mg/kg 11/24/19 20:44 98-06-611/24/19 13:480.0054 0.0018 1
Carbon tetrachloride ND mg/kg 11/24/19 20:44 56-23-511/24/19 13:480.0054 0.0010 1
Chlorobenzene ND mg/kg 11/24/19 20:44 108-90-711/24/19 13:480.0054 0.0011 1
Chloroethane ND mg/kg 11/24/19 20:44 75-00-311/24/19 13:480.011 0.0023 1
Chloroform ND mg/kg 11/24/19 20:44 67-66-311/24/19 13:480.0054 0.0012 1
Chloromethane ND mg/kg 11/24/19 20:44 74-87-311/24/19 13:480.011 0.0036 1
2-Chlorotoluene ND mg/kg 11/24/19 20:44 95-49-811/24/19 13:480.0054 0.0017 1
4-Chlorotoluene ND mg/kg 11/24/19 20:44 106-43-411/24/19 13:480.0054 0.0016 1
1,2-Dibromo-3-chloropropane ND mg/kg 11/24/19 20:44 96-12-811/24/19 13:480.0054 0.0028 1
Dibromochloromethane ND mg/kg 11/24/19 20:44 124-48-111/24/19 13:480.0054 0.0027 1
1,2-Dibromoethane (EDB)ND mg/kg 11/24/19 20:44 106-93-411/24/19 13:480.0054 0.0012 1
Dibromomethane ND mg/kg 11/24/19 20:44 74-95-311/24/19 13:480.0054 0.0016 1
1,2-Dichlorobenzene ND mg/kg 11/24/19 20:44 95-50-111/24/19 13:480.0054 0.0019 1
1,3-Dichlorobenzene ND mg/kg 11/24/19 20:44 541-73-111/24/19 13:480.0054 0.0019 1
1,4-Dichlorobenzene ND mg/kg 11/24/19 20:44 106-46-711/24/19 13:480.0054 0.0019 1
Dichlorodifluoromethane ND mg/kg 11/24/19 20:44 75-71-811/24/19 13:480.011 0.0045 1
1,1-Dichloroethane ND mg/kg 11/24/19 20:44 75-34-311/24/19 13:480.0054 0.00080 1
1,2-Dichloroethane ND mg/kg 11/24/19 20:44 107-06-211/24/19 13:480.0054 0.0011 1
1,1-Dichloroethene ND mg/kg 11/24/19 20:44 75-35-411/24/19 13:480.0054 0.0013 1
cis-1,2-Dichloroethene ND mg/kg 11/24/19 20:44 156-59-211/24/19 13:480.0054 0.00094 1
trans-1,2-Dichloroethene ND mg/kg 11/24/19 20:44 156-60-511/24/19 13:480.0054 0.0011 1
1,2-Dichloropropane ND mg/kg 11/24/19 20:44 78-87-511/24/19 13:480.0054 0.0020 1
1,3-Dichloropropane ND mg/kg 11/24/19 20:44 142-28-911/24/19 13:480.0054 0.0021 1
2,2-Dichloropropane ND mg/kg 11/24/19 20:44 594-20-711/24/19 13:480.0054 0.00054 1
1,1-Dichloropropene ND mg/kg 11/24/19 20:44 563-58-611/24/19 13:480.0054 0.0023 1
cis-1,3-Dichloropropene ND mg/kg 11/24/19 20:44 10061-01-511/24/19 13:480.0054 0.0025 1
trans-1,3-Dichloropropene ND mg/kg 11/24/19 20:44 10061-02-611/24/19 13:480.0054 0.00095 1
Diisopropyl ether ND mg/kg 11/24/19 20:44 108-20-311/24/19 13:480.0054 0.0031 1
Ethylbenzene ND mg/kg 11/24/19 20:44 100-41-411/24/19 13:480.0054 0.0012 1
Hexachloro-1,3-butadiene ND mg/kg 11/24/19 20:44 87-68-311/24/19 13:480.0054 0.0027 1
2-Hexanone ND mg/kg 11/24/19 20:44 591-78-611/24/19 13:480.054 0.0056 1
Isopropylbenzene (Cumene)ND mg/kg 11/24/19 20:44 98-82-811/24/19 13:480.0054 0.0016 1
p-Isopropyltoluene ND mg/kg 11/24/19 20:44 99-87-611/24/19 13:480.0054 0.0026 1
Methylene Chloride ND mg/kg 11/24/19 20:44 75-09-211/24/19 13:480.022 0.0064 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 11/24/19 20:44 108-10-111/24/19 13:480.054 0.0041 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-2 (15-17)Lab ID: 92454623002 Collected: 11/19/19 15:10 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 11/24/19 20:44 1634-04-411/24/19 13:480.0054 0.0031 1
Naphthalene ND mg/kg 11/24/19 20:44 91-20-311/24/19 13:480.0054 0.0046 1
n-Propylbenzene ND mg/kg 11/24/19 20:44 103-65-111/24/19 13:480.0054 0.0018 1
Styrene ND mg/kg 11/24/19 20:44 100-42-511/24/19 13:480.0054 0.0016 1
1,1,1,2-Tetrachloroethane ND mg/kg 11/24/19 20:44 630-20-611/24/19 13:480.0054 0.0013 1
1,1,2,2-Tetrachloroethane ND mg/kg 11/24/19 20:44 79-34-511/24/19 13:480.0054 0.0019 1
Tetrachloroethene ND mg/kg 11/24/19 20:44 127-18-411/24/19 13:480.0054 0.0017 1
Toluene ND mg/kg 11/24/19 20:44 108-88-311/24/19 13:480.0054 0.0018 1
1,2,3-Trichlorobenzene ND mg/kg 11/24/19 20:44 87-61-611/24/19 13:480.0054 0.0039 1
1,2,4-Trichlorobenzene ND mg/kg 11/24/19 20:44 120-82-111/24/19 13:480.0054 0.0029 1
1,1,1-Trichloroethane ND mg/kg 11/24/19 20:44 71-55-611/24/19 13:480.0054 0.00095 1
1,1,2-Trichloroethane ND mg/kg 11/24/19 20:44 79-00-511/24/19 13:480.0054 0.0012 1
Trichloroethene ND mg/kg 11/24/19 20:44 79-01-611/24/19 13:480.0054 0.0014 1
Trichlorofluoromethane ND mg/kg 11/24/19 20:44 75-69-411/24/19 13:480.0054 0.0013 1
1,2,3-Trichloropropane ND mg/kg 11/24/19 20:44 96-18-411/24/19 13:480.0054 0.0018 1
1,2,4-Trimethylbenzene ND mg/kg 11/24/19 20:44 95-63-611/24/19 13:480.0054 0.0021 1
1,3,5-Trimethylbenzene ND mg/kg 11/24/19 20:44 108-67-811/24/19 13:480.0054 0.0018 1
Vinyl acetate ND mg/kg 11/24/19 20:44 108-05-4 IL11/24/19 13:480.054 0.018 1
Vinyl chloride ND mg/kg 11/24/19 20:44 75-01-411/24/19 13:480.011 0.0021 1
Xylene (Total)ND mg/kg 11/24/19 20:44 1330-20-711/24/19 13:480.011 0.0038 1
m&p-Xylene ND mg/kg 11/24/19 20:44 179601-23-111/24/19 13:480.011 0.0026 1
o-Xylene ND mg/kg 11/24/19 20:44 95-47-611/24/19 13:480.0054 0.0013 1
Surrogates
Toluene-d8 (S)106 %11/24/19 20:44 2037-26-511/24/19 13:4870-130 1
4-Bromofluorobenzene (S)101 %11/24/19 20:44 460-00-411/24/19 13:4870-130 1
1,2-Dichloroethane-d4 (S)100 %11/24/19 20:44 17060-07-011/24/19 13:4870-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)0.0047J mg/kg 11/25/19 12:36 123-91-111/25/19 11:520.011 0.0034 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/25/19 12:36 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)103 %11/25/19 12:36 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.5 %11/21/19 13:250.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-2 (22-24)Lab ID: 92454623003 Collected: 11/19/19 15:45 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 3.3J mg/kg 11/23/19 15:50 7440-38-2 D311/21/19 16:356.4 3.2 5
Barium 468 mg/kg 11/23/19 15:50 7440-39-3 D311/21/19 16:353.2 1.6 5
Cadmium ND mg/kg 11/23/19 15:50 7440-43-9 D311/21/19 16:350.64 0.32 5
Chromium 167 mg/kg 11/23/19 15:50 7440-47-3 D311/21/19 16:353.2 1.6 5
Lead 8.3 mg/kg 11/23/19 15:50 7439-92-1 D311/21/19 16:353.2 1.6 5
Selenium 3.7J mg/kg 11/23/19 15:50 7782-49-2 D311/21/19 16:356.4 3.2 5
Silver ND mg/kg 11/23/19 15:50 7440-22-4 D311/21/19 16:353.2 1.6 5
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.0053 mg/kg 11/22/19 12:09 7439-97-6 B,BC11/21/19 11:570.0026 0.0013 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/25/19 16:49 83-32-911/23/19 13:400.43 0.11 1
Acenaphthylene ND mg/kg 11/25/19 16:49 208-96-811/23/19 13:400.43 0.10 1
Aniline ND mg/kg 11/25/19 16:49 62-53-311/23/19 13:400.43 0.096 1
Anthracene ND mg/kg 11/25/19 16:49 120-12-711/23/19 13:400.43 0.11 1
Benzo(a)anthracene ND mg/kg 11/25/19 16:49 56-55-311/23/19 13:400.43 0.14 1
Benzo(a)pyrene ND mg/kg 11/25/19 16:49 50-32-811/23/19 13:400.43 0.19 1
Benzo(b)fluoranthene ND mg/kg 11/25/19 16:49 205-99-211/23/19 13:400.43 0.17 1
Benzo(g,h,i)perylene ND mg/kg 11/25/19 16:49 191-24-211/23/19 13:400.43 0.17 1
Benzo(k)fluoranthene ND mg/kg 11/25/19 16:49 207-08-911/23/19 13:400.43 0.18 1
Benzoic Acid ND mg/kg 11/25/19 16:49 65-85-011/23/19 13:402.1 0.46 1
Benzyl alcohol ND mg/kg 11/25/19 16:49 100-51-611/23/19 13:400.86 0.23 1
4-Bromophenylphenyl ether ND mg/kg 11/25/19 16:49 101-55-311/23/19 13:400.43 0.11 1
Butylbenzylphthalate ND mg/kg 11/25/19 16:49 85-68-711/23/19 13:400.43 0.11 1
4-Chloro-3-methylphenol ND mg/kg 11/25/19 16:49 59-50-711/23/19 13:400.86 0.26 1
4-Chloroaniline ND mg/kg 11/25/19 16:49 106-47-811/23/19 13:402.1 0.26 1
bis(2-Chloroethoxy)methane ND mg/kg 11/25/19 16:49 111-91-111/23/19 13:400.43 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 11/25/19 16:49 111-44-411/23/19 13:400.43 0.091 1
2-Chloronaphthalene ND mg/kg 11/25/19 16:49 91-58-711/23/19 13:400.43 0.095 1
2-Chlorophenol ND mg/kg 11/25/19 16:49 95-57-811/23/19 13:400.43 0.10 1
4-Chlorophenylphenyl ether ND mg/kg 11/25/19 16:49 7005-72-311/23/19 13:400.43 0.11 1
Chrysene ND mg/kg 11/25/19 16:49 218-01-911/23/19 13:400.43 0.12 1
Dibenz(a,h)anthracene ND mg/kg 11/25/19 16:49 53-70-311/23/19 13:400.43 0.17 1
Dibenzofuran ND mg/kg 11/25/19 16:49 132-64-911/23/19 13:400.43 0.11 1
1,2-Dichlorobenzene ND mg/kg 11/25/19 16:49 95-50-111/23/19 13:400.43 0.093 1
1,3-Dichlorobenzene ND mg/kg 11/25/19 16:49 541-73-111/23/19 13:400.43 0.097 1
1,4-Dichlorobenzene ND mg/kg 11/25/19 16:49 106-46-711/23/19 13:400.43 0.094 1
3,3'-Dichlorobenzidine ND mg/kg 11/25/19 16:49 91-94-111/23/19 13:402.1 0.30 1
2,4-Dichlorophenol ND mg/kg 11/25/19 16:49 120-83-211/23/19 13:400.43 0.14 1
Diethylphthalate ND mg/kg 11/25/19 16:49 84-66-211/23/19 13:400.43 0.093 1
2,4-Dimethylphenol ND mg/kg 11/25/19 16:49 105-67-911/23/19 13:400.43 0.11 1
Dimethylphthalate ND mg/kg 11/25/19 16:49 131-11-311/23/19 13:400.43 0.097 1
Di-n-butylphthalate ND mg/kg 11/25/19 16:49 84-74-211/23/19 13:400.43 0.11 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/25/19 16:49 534-52-111/23/19 13:400.86 0.69 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-2 (22-24)Lab ID: 92454623003 Collected: 11/19/19 15:45 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/25/19 16:49 51-28-511/23/19 13:402.1 1.4 1
2,4-Dinitrotoluene ND mg/kg 11/25/19 16:49 121-14-211/23/19 13:400.43 0.11 1
2,6-Dinitrotoluene ND mg/kg 11/25/19 16:49 606-20-211/23/19 13:400.43 0.11 1
Di-n-octylphthalate ND mg/kg 11/25/19 16:49 117-84-011/23/19 13:400.43 0.24 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/25/19 16:49 117-81-711/23/19 13:400.43 0.14 1
Fluoranthene ND mg/kg 11/25/19 16:49 206-44-011/23/19 13:400.43 0.13 1
Fluorene ND mg/kg 11/25/19 16:49 86-73-711/23/19 13:400.43 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 11/25/19 16:49 87-68-311/23/19 13:400.43 0.10 1
Hexachlorobenzene ND mg/kg 11/25/19 16:49 118-74-111/23/19 13:400.43 0.11 1
Hexachlorocyclopentadiene ND mg/kg 11/25/19 16:49 77-47-4 v211/23/19 13:400.43 0.17 1
Hexachloroethane ND mg/kg 11/25/19 16:49 67-72-111/23/19 13:400.43 0.098 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/25/19 16:49 193-39-511/23/19 13:400.43 0.20 1
Isophorone ND mg/kg 11/25/19 16:49 78-59-111/23/19 13:400.43 0.093 1
1-Methylnaphthalene ND mg/kg 11/25/19 16:49 90-12-011/23/19 13:400.43 0.11 1
2-Methylnaphthalene ND mg/kg 11/25/19 16:49 91-57-611/23/19 13:400.43 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 11/25/19 16:49 95-48-711/23/19 13:400.43 0.095 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/25/19 16:49 15831-10-411/23/19 13:400.43 0.11 1
Naphthalene ND mg/kg 11/25/19 16:49 91-20-311/23/19 13:400.43 0.10 1
2-Nitroaniline ND mg/kg 11/25/19 16:49 88-74-4 v111/23/19 13:402.1 0.22 1
3-Nitroaniline ND mg/kg 11/25/19 16:49 99-09-211/23/19 13:402.1 0.23 1
4-Nitroaniline ND mg/kg 11/25/19 16:49 100-01-611/23/19 13:400.86 0.21 1
Nitrobenzene ND mg/kg 11/25/19 16:49 98-95-311/23/19 13:400.43 0.10 1
2-Nitrophenol ND mg/kg 11/25/19 16:49 88-75-511/23/19 13:400.43 0.13 1
4-Nitrophenol ND mg/kg 11/25/19 16:49 100-02-711/23/19 13:402.1 0.68 1
N-Nitrosodimethylamine ND mg/kg 11/25/19 16:49 62-75-911/23/19 13:400.43 0.12 1
N-Nitroso-di-n-propylamine ND mg/kg 11/25/19 16:49 621-64-711/23/19 13:400.43 0.12 1
N-Nitrosodiphenylamine ND mg/kg 11/25/19 16:49 86-30-611/23/19 13:400.43 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/25/19 16:49 108-60-111/23/19 13:400.43 0.12 1
Pentachlorophenol ND mg/kg 11/25/19 16:49 87-86-511/23/19 13:402.1 0.20 1
Phenanthrene ND mg/kg 11/25/19 16:49 85-01-811/23/19 13:400.43 0.11 1
Phenol ND mg/kg 11/25/19 16:49 108-95-211/23/19 13:400.43 0.10 1
Pyrene ND mg/kg 11/25/19 16:49 129-00-011/23/19 13:400.43 0.12 1
Pyridine ND mg/kg 11/25/19 16:49 110-86-111/23/19 13:400.43 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 11/25/19 16:49 120-82-111/23/19 13:400.43 0.098 1
2,4,5-Trichlorophenol ND mg/kg 11/25/19 16:49 95-95-411/23/19 13:400.43 0.11 1
2,4,6-Trichlorophenol ND mg/kg 11/25/19 16:49 88-06-211/23/19 13:400.43 0.11 1
Surrogates
Nitrobenzene-d5 (S)46 %11/25/19 16:49 4165-60-011/23/19 13:4023-110 1
2-Fluorobiphenyl (S)44 %11/25/19 16:49 321-60-811/23/19 13:4030-110 1
Terphenyl-d14 (S)46 %11/25/19 16:49 1718-51-011/23/19 13:4028-110 1
Phenol-d6 (S)44 %11/25/19 16:49 13127-88-311/23/19 13:4022-110 1
2-Fluorophenol (S)43 %11/25/19 16:49 367-12-411/23/19 13:4013-110 1
2,4,6-Tribromophenol (S)39 %11/25/19 16:49 118-79-611/23/19 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-2 (22-24)Lab ID: 92454623003 Collected: 11/19/19 15:45 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 11/24/19 21:08 67-64-111/24/19 13:480.11 0.011 1
Benzene ND mg/kg 11/24/19 21:08 71-43-211/24/19 13:480.0056 0.0010 1
Bromobenzene ND mg/kg 11/24/19 21:08 108-86-111/24/19 13:480.0056 0.0015 1
Bromochloromethane ND mg/kg 11/24/19 21:08 74-97-511/24/19 13:480.0056 0.0014 1
Bromodichloromethane ND mg/kg 11/24/19 21:08 75-27-411/24/19 13:480.0056 0.0011 1
Bromoform ND mg/kg 11/24/19 21:08 75-25-211/24/19 13:480.0056 0.0027 1
Bromomethane ND mg/kg 11/24/19 21:08 74-83-9 IH11/24/19 13:480.011 0.0026 1
2-Butanone (MEK)ND mg/kg 11/24/19 21:08 78-93-311/24/19 13:480.11 0.013 1
n-Butylbenzene ND mg/kg 11/24/19 21:08 104-51-811/24/19 13:480.0056 0.0032 1
sec-Butylbenzene ND mg/kg 11/24/19 21:08 135-98-811/24/19 13:480.0056 0.0024 1
tert-Butylbenzene ND mg/kg 11/24/19 21:08 98-06-611/24/19 13:480.0056 0.0019 1
Carbon tetrachloride ND mg/kg 11/24/19 21:08 56-23-511/24/19 13:480.0056 0.0011 1
Chlorobenzene ND mg/kg 11/24/19 21:08 108-90-711/24/19 13:480.0056 0.0011 1
Chloroethane ND mg/kg 11/24/19 21:08 75-00-311/24/19 13:480.011 0.0023 1
Chloroform ND mg/kg 11/24/19 21:08 67-66-311/24/19 13:480.0056 0.0012 1
Chloromethane ND mg/kg 11/24/19 21:08 74-87-311/24/19 13:480.011 0.0037 1
2-Chlorotoluene ND mg/kg 11/24/19 21:08 95-49-811/24/19 13:480.0056 0.0017 1
4-Chlorotoluene ND mg/kg 11/24/19 21:08 106-43-411/24/19 13:480.0056 0.0017 1
1,2-Dibromo-3-chloropropane ND mg/kg 11/24/19 21:08 96-12-811/24/19 13:480.0056 0.0029 1
Dibromochloromethane ND mg/kg 11/24/19 21:08 124-48-111/24/19 13:480.0056 0.0028 1
1,2-Dibromoethane (EDB)ND mg/kg 11/24/19 21:08 106-93-411/24/19 13:480.0056 0.0013 1
Dibromomethane ND mg/kg 11/24/19 21:08 74-95-311/24/19 13:480.0056 0.0017 1
1,2-Dichlorobenzene ND mg/kg 11/24/19 21:08 95-50-111/24/19 13:480.0056 0.0020 1
1,3-Dichlorobenzene ND mg/kg 11/24/19 21:08 541-73-111/24/19 13:480.0056 0.0020 1
1,4-Dichlorobenzene ND mg/kg 11/24/19 21:08 106-46-711/24/19 13:480.0056 0.0019 1
Dichlorodifluoromethane ND mg/kg 11/24/19 21:08 75-71-811/24/19 13:480.011 0.0046 1
1,1-Dichloroethane ND mg/kg 11/24/19 21:08 75-34-311/24/19 13:480.0056 0.00082 1
1,2-Dichloroethane ND mg/kg 11/24/19 21:08 107-06-211/24/19 13:480.0056 0.0011 1
1,1-Dichloroethene ND mg/kg 11/24/19 21:08 75-35-411/24/19 13:480.0056 0.0013 1
cis-1,2-Dichloroethene ND mg/kg 11/24/19 21:08 156-59-211/24/19 13:480.0056 0.00097 1
trans-1,2-Dichloroethene ND mg/kg 11/24/19 21:08 156-60-511/24/19 13:480.0056 0.0011 1
1,2-Dichloropropane ND mg/kg 11/24/19 21:08 78-87-511/24/19 13:480.0056 0.0021 1
1,3-Dichloropropane ND mg/kg 11/24/19 21:08 142-28-911/24/19 13:480.0056 0.0021 1
2,2-Dichloropropane ND mg/kg 11/24/19 21:08 594-20-711/24/19 13:480.0056 0.00055 1
1,1-Dichloropropene ND mg/kg 11/24/19 21:08 563-58-611/24/19 13:480.0056 0.0024 1
cis-1,3-Dichloropropene ND mg/kg 11/24/19 21:08 10061-01-511/24/19 13:480.0056 0.0025 1
trans-1,3-Dichloropropene ND mg/kg 11/24/19 21:08 10061-02-611/24/19 13:480.0056 0.00098 1
Diisopropyl ether ND mg/kg 11/24/19 21:08 108-20-311/24/19 13:480.0056 0.0032 1
Ethylbenzene ND mg/kg 11/24/19 21:08 100-41-411/24/19 13:480.0056 0.0012 1
Hexachloro-1,3-butadiene ND mg/kg 11/24/19 21:08 87-68-311/24/19 13:480.0056 0.0028 1
2-Hexanone ND mg/kg 11/24/19 21:08 591-78-611/24/19 13:480.056 0.0058 1
Isopropylbenzene (Cumene)ND mg/kg 11/24/19 21:08 98-82-811/24/19 13:480.0056 0.0016 1
p-Isopropyltoluene ND mg/kg 11/24/19 21:08 99-87-611/24/19 13:480.0056 0.0027 1
Methylene Chloride ND mg/kg 11/24/19 21:08 75-09-211/24/19 13:480.022 0.0066 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 11/24/19 21:08 108-10-111/24/19 13:480.056 0.0042 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-2 (22-24)Lab ID: 92454623003 Collected: 11/19/19 15:45 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 11/24/19 21:08 1634-04-411/24/19 13:480.0056 0.0032 1
Naphthalene ND mg/kg 11/24/19 21:08 91-20-311/24/19 13:480.0056 0.0048 1
n-Propylbenzene ND mg/kg 11/24/19 21:08 103-65-111/24/19 13:480.0056 0.0019 1
Styrene ND mg/kg 11/24/19 21:08 100-42-511/24/19 13:480.0056 0.0017 1
1,1,1,2-Tetrachloroethane ND mg/kg 11/24/19 21:08 630-20-611/24/19 13:480.0056 0.0014 1
1,1,2,2-Tetrachloroethane ND mg/kg 11/24/19 21:08 79-34-511/24/19 13:480.0056 0.0019 1
Tetrachloroethene ND mg/kg 11/24/19 21:08 127-18-411/24/19 13:480.0056 0.0018 1
Toluene ND mg/kg 11/24/19 21:08 108-88-311/24/19 13:480.0056 0.0018 1
1,2,3-Trichlorobenzene ND mg/kg 11/24/19 21:08 87-61-611/24/19 13:480.0056 0.0040 1
1,2,4-Trichlorobenzene ND mg/kg 11/24/19 21:08 120-82-111/24/19 13:480.0056 0.0030 1
1,1,1-Trichloroethane ND mg/kg 11/24/19 21:08 71-55-611/24/19 13:480.0056 0.00098 1
1,1,2-Trichloroethane ND mg/kg 11/24/19 21:08 79-00-511/24/19 13:480.0056 0.0013 1
Trichloroethene ND mg/kg 11/24/19 21:08 79-01-611/24/19 13:480.0056 0.0015 1
Trichlorofluoromethane ND mg/kg 11/24/19 21:08 75-69-411/24/19 13:480.0056 0.0013 1
1,2,3-Trichloropropane ND mg/kg 11/24/19 21:08 96-18-411/24/19 13:480.0056 0.0019 1
1,2,4-Trimethylbenzene ND mg/kg 11/24/19 21:08 95-63-611/24/19 13:480.0056 0.0022 1
1,3,5-Trimethylbenzene ND mg/kg 11/24/19 21:08 108-67-811/24/19 13:480.0056 0.0019 1
Vinyl acetate ND mg/kg 11/24/19 21:08 108-05-411/24/19 13:480.056 0.018 1
Vinyl chloride ND mg/kg 11/24/19 21:08 75-01-411/24/19 13:480.011 0.0021 1
Xylene (Total)ND mg/kg 11/24/19 21:08 1330-20-711/24/19 13:480.011 0.0039 1
m&p-Xylene ND mg/kg 11/24/19 21:08 179601-23-111/24/19 13:480.011 0.0026 1
o-Xylene ND mg/kg 11/24/19 21:08 95-47-611/24/19 13:480.0056 0.0013 1
Surrogates
Toluene-d8 (S)110 %11/24/19 21:08 2037-26-511/24/19 13:4870-130 1
4-Bromofluorobenzene (S)105 %11/24/19 21:08 460-00-411/24/19 13:4870-130 1
1,2-Dichloroethane-d4 (S)90 %11/24/19 21:08 17060-07-011/24/19 13:4870-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)0.014 mg/kg 11/25/19 12:56 123-91-111/25/19 11:520.012 0.0035 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %11/25/19 12:56 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)103 %11/25/19 12:56 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.0 %11/21/19 13:250.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 78.1 %01/10/20 14:55 H301/10/20 14:451
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 01/11/20 14:27 18540-29-9 H301/10/20 20:501.28 0.327 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-3 (15-17)Lab ID: 92454623004 Collected: 11/20/19 09:20 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 1.5 mg/kg 11/23/19 01:47 7440-38-211/21/19 16:351.4 0.70 1
Barium 169 mg/kg 11/23/19 01:47 7440-39-311/21/19 16:350.70 0.35 1
Cadmium ND mg/kg 11/23/19 01:47 7440-43-911/21/19 16:350.14 0.070 1
Chromium 31.6 mg/kg 11/23/19 01:47 7440-47-311/21/19 16:350.70 0.35 1
Lead 11.1 mg/kg 11/23/19 01:47 7439-92-111/21/19 16:350.70 0.35 1
Selenium ND mg/kg 11/23/19 01:47 7782-49-211/21/19 16:351.4 0.70 1
Silver ND mg/kg 11/23/19 01:47 7440-22-411/21/19 16:350.70 0.35 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.0044 mg/kg 11/22/19 12:11 7439-97-6 B,BC11/21/19 11:570.0027 0.0014 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/25/19 17:18 83-32-911/23/19 13:400.47 0.12 1
Acenaphthylene ND mg/kg 11/25/19 17:18 208-96-811/23/19 13:400.47 0.11 1
Aniline ND mg/kg 11/25/19 17:18 62-53-311/23/19 13:400.47 0.10 1
Anthracene ND mg/kg 11/25/19 17:18 120-12-711/23/19 13:400.47 0.12 1
Benzo(a)anthracene ND mg/kg 11/25/19 17:18 56-55-311/23/19 13:400.47 0.15 1
Benzo(a)pyrene ND mg/kg 11/25/19 17:18 50-32-811/23/19 13:400.47 0.20 1
Benzo(b)fluoranthene ND mg/kg 11/25/19 17:18 205-99-211/23/19 13:400.47 0.19 1
Benzo(g,h,i)perylene ND mg/kg 11/25/19 17:18 191-24-211/23/19 13:400.47 0.18 1
Benzo(k)fluoranthene ND mg/kg 11/25/19 17:18 207-08-911/23/19 13:400.47 0.20 1
Benzoic Acid ND mg/kg 11/25/19 17:18 65-85-011/23/19 13:402.3 0.50 1
Benzyl alcohol ND mg/kg 11/25/19 17:18 100-51-611/23/19 13:400.93 0.25 1
4-Bromophenylphenyl ether ND mg/kg 11/25/19 17:18 101-55-311/23/19 13:400.47 0.12 1
Butylbenzylphthalate ND mg/kg 11/25/19 17:18 85-68-711/23/19 13:400.47 0.12 1
4-Chloro-3-methylphenol ND mg/kg 11/25/19 17:18 59-50-711/23/19 13:400.93 0.28 1
4-Chloroaniline ND mg/kg 11/25/19 17:18 106-47-811/23/19 13:402.3 0.28 1
bis(2-Chloroethoxy)methane ND mg/kg 11/25/19 17:18 111-91-111/23/19 13:400.47 0.12 1
bis(2-Chloroethyl) ether ND mg/kg 11/25/19 17:18 111-44-411/23/19 13:400.47 0.099 1
2-Chloronaphthalene ND mg/kg 11/25/19 17:18 91-58-711/23/19 13:400.47 0.10 1
2-Chlorophenol ND mg/kg 11/25/19 17:18 95-57-811/23/19 13:400.47 0.11 1
4-Chlorophenylphenyl ether ND mg/kg 11/25/19 17:18 7005-72-311/23/19 13:400.47 0.12 1
Chrysene ND mg/kg 11/25/19 17:18 218-01-911/23/19 13:400.47 0.14 1
Dibenz(a,h)anthracene ND mg/kg 11/25/19 17:18 53-70-311/23/19 13:400.47 0.19 1
Dibenzofuran ND mg/kg 11/25/19 17:18 132-64-911/23/19 13:400.47 0.12 1
1,2-Dichlorobenzene ND mg/kg 11/25/19 17:18 95-50-111/23/19 13:400.47 0.10 1
1,3-Dichlorobenzene ND mg/kg 11/25/19 17:18 541-73-111/23/19 13:400.47 0.10 1
1,4-Dichlorobenzene ND mg/kg 11/25/19 17:18 106-46-711/23/19 13:400.47 0.10 1
3,3'-Dichlorobenzidine ND mg/kg 11/25/19 17:18 91-94-111/23/19 13:402.3 0.32 1
2,4-Dichlorophenol ND mg/kg 11/25/19 17:18 120-83-211/23/19 13:400.47 0.15 1
Diethylphthalate ND mg/kg 11/25/19 17:18 84-66-211/23/19 13:400.47 0.10 1
2,4-Dimethylphenol ND mg/kg 11/25/19 17:18 105-67-911/23/19 13:400.47 0.12 1
Dimethylphthalate ND mg/kg 11/25/19 17:18 131-11-311/23/19 13:400.47 0.11 1
Di-n-butylphthalate ND mg/kg 11/25/19 17:18 84-74-211/23/19 13:400.47 0.11 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/25/19 17:18 534-52-111/23/19 13:400.93 0.75 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-3 (15-17)Lab ID: 92454623004 Collected: 11/20/19 09:20 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/25/19 17:18 51-28-511/23/19 13:402.3 1.5 1
2,4-Dinitrotoluene ND mg/kg 11/25/19 17:18 121-14-211/23/19 13:400.47 0.12 1
2,6-Dinitrotoluene ND mg/kg 11/25/19 17:18 606-20-211/23/19 13:400.47 0.12 1
Di-n-octylphthalate ND mg/kg 11/25/19 17:18 117-84-011/23/19 13:400.47 0.27 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/25/19 17:18 117-81-711/23/19 13:400.47 0.15 1
Fluoranthene ND mg/kg 11/25/19 17:18 206-44-011/23/19 13:400.47 0.14 1
Fluorene ND mg/kg 11/25/19 17:18 86-73-711/23/19 13:400.47 0.12 1
Hexachloro-1,3-butadiene ND mg/kg 11/25/19 17:18 87-68-311/23/19 13:400.47 0.11 1
Hexachlorobenzene ND mg/kg 11/25/19 17:18 118-74-111/23/19 13:400.47 0.12 1
Hexachlorocyclopentadiene ND mg/kg 11/25/19 17:18 77-47-4 v211/23/19 13:400.47 0.19 1
Hexachloroethane ND mg/kg 11/25/19 17:18 67-72-111/23/19 13:400.47 0.11 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/25/19 17:18 193-39-511/23/19 13:400.47 0.21 1
Isophorone ND mg/kg 11/25/19 17:18 78-59-111/23/19 13:400.47 0.10 1
1-Methylnaphthalene ND mg/kg 11/25/19 17:18 90-12-011/23/19 13:400.47 0.12 1
2-Methylnaphthalene ND mg/kg 11/25/19 17:18 91-57-611/23/19 13:400.47 0.12 1
2-Methylphenol(o-Cresol)ND mg/kg 11/25/19 17:18 95-48-711/23/19 13:400.47 0.10 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/25/19 17:18 15831-10-411/23/19 13:400.47 0.12 1
Naphthalene ND mg/kg 11/25/19 17:18 91-20-311/23/19 13:400.47 0.11 1
2-Nitroaniline ND mg/kg 11/25/19 17:18 88-74-4 v111/23/19 13:402.3 0.23 1
3-Nitroaniline ND mg/kg 11/25/19 17:18 99-09-211/23/19 13:402.3 0.25 1
4-Nitroaniline ND mg/kg 11/25/19 17:18 100-01-611/23/19 13:400.93 0.23 1
Nitrobenzene ND mg/kg 11/25/19 17:18 98-95-311/23/19 13:400.47 0.11 1
2-Nitrophenol ND mg/kg 11/25/19 17:18 88-75-511/23/19 13:400.47 0.14 1
4-Nitrophenol ND mg/kg 11/25/19 17:18 100-02-711/23/19 13:402.3 0.74 1
N-Nitrosodimethylamine ND mg/kg 11/25/19 17:18 62-75-911/23/19 13:400.47 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 11/25/19 17:18 621-64-711/23/19 13:400.47 0.13 1
N-Nitrosodiphenylamine ND mg/kg 11/25/19 17:18 86-30-611/23/19 13:400.47 0.12 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/25/19 17:18 108-60-111/23/19 13:400.47 0.13 1
Pentachlorophenol ND mg/kg 11/25/19 17:18 87-86-511/23/19 13:402.3 0.21 1
Phenanthrene ND mg/kg 11/25/19 17:18 85-01-811/23/19 13:400.47 0.12 1
Phenol ND mg/kg 11/25/19 17:18 108-95-211/23/19 13:400.47 0.11 1
Pyrene ND mg/kg 11/25/19 17:18 129-00-011/23/19 13:400.47 0.13 1
Pyridine ND mg/kg 11/25/19 17:18 110-86-111/23/19 13:400.47 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 11/25/19 17:18 120-82-111/23/19 13:400.47 0.11 1
2,4,5-Trichlorophenol ND mg/kg 11/25/19 17:18 95-95-411/23/19 13:400.47 0.12 1
2,4,6-Trichlorophenol ND mg/kg 11/25/19 17:18 88-06-211/23/19 13:400.47 0.12 1
Surrogates
Nitrobenzene-d5 (S)69 %11/25/19 17:18 4165-60-011/23/19 13:4023-110 1
2-Fluorobiphenyl (S)67 %11/25/19 17:18 321-60-811/23/19 13:4030-110 1
Terphenyl-d14 (S)77 %11/25/19 17:18 1718-51-011/23/19 13:4028-110 1
Phenol-d6 (S)65 %11/25/19 17:18 13127-88-311/23/19 13:4022-110 1
2-Fluorophenol (S)58 %11/25/19 17:18 367-12-411/23/19 13:4013-110 1
2,4,6-Tribromophenol (S)55 %11/25/19 17:18 118-79-611/23/19 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-3 (15-17)Lab ID: 92454623004 Collected: 11/20/19 09:20 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 11/25/19 17:18 67-64-111/25/19 10:080.14 0.013 1
Benzene ND mg/kg 11/25/19 17:18 71-43-211/25/19 10:080.0068 0.0012 1
Bromobenzene ND mg/kg 11/25/19 17:18 108-86-111/25/19 10:080.0068 0.0018 1
Bromochloromethane ND mg/kg 11/25/19 17:18 74-97-511/25/19 10:080.0068 0.0017 1
Bromodichloromethane ND mg/kg 11/25/19 17:18 75-27-411/25/19 10:080.0068 0.0013 1
Bromoform ND mg/kg 11/25/19 17:18 75-25-211/25/19 10:080.0068 0.0033 1
Bromomethane ND mg/kg 11/25/19 17:18 74-83-911/25/19 10:080.014 0.0032 1
2-Butanone (MEK)ND mg/kg 11/25/19 17:18 78-93-311/25/19 10:080.14 0.016 1
n-Butylbenzene ND mg/kg 11/25/19 17:18 104-51-811/25/19 10:080.0068 0.0038 1
sec-Butylbenzene ND mg/kg 11/25/19 17:18 135-98-811/25/19 10:080.0068 0.0029 1
tert-Butylbenzene ND mg/kg 11/25/19 17:18 98-06-611/25/19 10:080.0068 0.0023 1
Carbon tetrachloride ND mg/kg 11/25/19 17:18 56-23-511/25/19 10:080.0068 0.0013 1
Chlorobenzene ND mg/kg 11/25/19 17:18 108-90-711/25/19 10:080.0068 0.0013 1
Chloroethane ND mg/kg 11/25/19 17:18 75-00-3 IK11/25/19 10:080.014 0.0028 1
Chloroform ND mg/kg 11/25/19 17:18 67-66-311/25/19 10:080.0068 0.0014 1
Chloromethane ND mg/kg 11/25/19 17:18 74-87-311/25/19 10:080.014 0.0045 1
2-Chlorotoluene ND mg/kg 11/25/19 17:18 95-49-811/25/19 10:080.0068 0.0021 1
4-Chlorotoluene ND mg/kg 11/25/19 17:18 106-43-411/25/19 10:080.0068 0.0020 1
1,2-Dibromo-3-chloropropane ND mg/kg 11/25/19 17:18 96-12-811/25/19 10:080.0068 0.0035 1
Dibromochloromethane ND mg/kg 11/25/19 17:18 124-48-111/25/19 10:080.0068 0.0034 1
1,2-Dibromoethane (EDB)ND mg/kg 11/25/19 17:18 106-93-411/25/19 10:080.0068 0.0015 1
Dibromomethane ND mg/kg 11/25/19 17:18 74-95-311/25/19 10:080.0068 0.0020 1
1,2-Dichlorobenzene ND mg/kg 11/25/19 17:18 95-50-111/25/19 10:080.0068 0.0024 1
1,3-Dichlorobenzene ND mg/kg 11/25/19 17:18 541-73-111/25/19 10:080.0068 0.0024 1
1,4-Dichlorobenzene ND mg/kg 11/25/19 17:18 106-46-711/25/19 10:080.0068 0.0024 1
Dichlorodifluoromethane ND mg/kg 11/25/19 17:18 75-71-811/25/19 10:080.014 0.0056 1
1,1-Dichloroethane ND mg/kg 11/25/19 17:18 75-34-311/25/19 10:080.0068 0.0010 1
1,2-Dichloroethane ND mg/kg 11/25/19 17:18 107-06-211/25/19 10:080.0068 0.0014 1
1,1-Dichloroethene ND mg/kg 11/25/19 17:18 75-35-411/25/19 10:080.0068 0.0016 1
cis-1,2-Dichloroethene ND mg/kg 11/25/19 17:18 156-59-211/25/19 10:080.0068 0.0012 1
trans-1,2-Dichloroethene ND mg/kg 11/25/19 17:18 156-60-511/25/19 10:080.0068 0.0013 1
1,2-Dichloropropane ND mg/kg 11/25/19 17:18 78-87-511/25/19 10:080.0068 0.0026 1
1,3-Dichloropropane ND mg/kg 11/25/19 17:18 142-28-911/25/19 10:080.0068 0.0026 1
2,2-Dichloropropane ND mg/kg 11/25/19 17:18 594-20-711/25/19 10:080.0068 0.00067 1
1,1-Dichloropropene ND mg/kg 11/25/19 17:18 563-58-611/25/19 10:080.0068 0.0029 1
cis-1,3-Dichloropropene ND mg/kg 11/25/19 17:18 10061-01-511/25/19 10:080.0068 0.0031 1
trans-1,3-Dichloropropene ND mg/kg 11/25/19 17:18 10061-02-611/25/19 10:080.0068 0.0012 1
Diisopropyl ether ND mg/kg 11/25/19 17:18 108-20-311/25/19 10:080.0068 0.0039 1
Ethylbenzene ND mg/kg 11/25/19 17:18 100-41-411/25/19 10:080.0068 0.0014 1
Hexachloro-1,3-butadiene ND mg/kg 11/25/19 17:18 87-68-311/25/19 10:080.0068 0.0034 1
2-Hexanone ND mg/kg 11/25/19 17:18 591-78-611/25/19 10:080.068 0.0070 1
Isopropylbenzene (Cumene)ND mg/kg 11/25/19 17:18 98-82-811/25/19 10:080.0068 0.0020 1
p-Isopropyltoluene ND mg/kg 11/25/19 17:18 99-87-611/25/19 10:080.0068 0.0033 1
Methylene Chloride ND mg/kg 11/25/19 17:18 75-09-211/25/19 10:080.027 0.0080 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 11/25/19 17:18 108-10-111/25/19 10:080.068 0.0051 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-3 (15-17)Lab ID: 92454623004 Collected: 11/20/19 09:20 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 11/25/19 17:18 1634-04-411/25/19 10:080.0068 0.0039 1
Naphthalene ND mg/kg 11/25/19 17:18 91-20-311/25/19 10:080.0068 0.0058 1
n-Propylbenzene ND mg/kg 11/25/19 17:18 103-65-111/25/19 10:080.0068 0.0023 1
Styrene ND mg/kg 11/25/19 17:18 100-42-511/25/19 10:080.0068 0.0020 1
1,1,1,2-Tetrachloroethane ND mg/kg 11/25/19 17:18 630-20-611/25/19 10:080.0068 0.0017 1
1,1,2,2-Tetrachloroethane ND mg/kg 11/25/19 17:18 79-34-511/25/19 10:080.0068 0.0024 1
Tetrachloroethene ND mg/kg 11/25/19 17:18 127-18-411/25/19 10:080.0068 0.0021 1
Toluene ND mg/kg 11/25/19 17:18 108-88-311/25/19 10:080.0068 0.0022 1
1,2,3-Trichlorobenzene ND mg/kg 11/25/19 17:18 87-61-611/25/19 10:080.0068 0.0048 1
1,2,4-Trichlorobenzene ND mg/kg 11/25/19 17:18 120-82-111/25/19 10:080.0068 0.0036 1
1,1,1-Trichloroethane ND mg/kg 11/25/19 17:18 71-55-611/25/19 10:080.0068 0.0012 1
1,1,2-Trichloroethane ND mg/kg 11/25/19 17:18 79-00-511/25/19 10:080.0068 0.0015 1
Trichloroethene ND mg/kg 11/25/19 17:18 79-01-611/25/19 10:080.0068 0.0018 1
Trichlorofluoromethane ND mg/kg 11/25/19 17:18 75-69-411/25/19 10:080.0068 0.0016 1
1,2,3-Trichloropropane ND mg/kg 11/25/19 17:18 96-18-411/25/19 10:080.0068 0.0023 1
1,2,4-Trimethylbenzene ND mg/kg 11/25/19 17:18 95-63-6 v111/25/19 10:080.0068 0.0026 1
1,3,5-Trimethylbenzene ND mg/kg 11/25/19 17:18 108-67-811/25/19 10:080.0068 0.0023 1
Vinyl acetate ND mg/kg 11/25/19 17:18 108-05-4 v111/25/19 10:080.068 0.022 1
Vinyl chloride ND mg/kg 11/25/19 17:18 75-01-411/25/19 10:080.014 0.0026 1
Xylene (Total)ND mg/kg 11/25/19 17:18 1330-20-711/25/19 10:080.014 0.0048 1
m&p-Xylene ND mg/kg 11/25/19 17:18 179601-23-111/25/19 10:080.014 0.0032 1
o-Xylene ND mg/kg 11/25/19 17:18 95-47-611/25/19 10:080.0068 0.0016 1
Surrogates
Toluene-d8 (S)117 %11/25/19 17:18 2037-26-511/25/19 10:0870-130 1
4-Bromofluorobenzene (S)102 %11/25/19 17:18 460-00-411/25/19 10:0870-130 1
1,2-Dichloroethane-d4 (S)87 %11/25/19 17:18 17060-07-011/25/19 10:0870-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)ND mg/kg 11/25/19 13:16 123-91-111/25/19 11:520.013 0.0040 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %11/25/19 13:16 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)102 %11/25/19 13:16 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 28.1 %11/21/19 13:250.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-3 (17-19)Lab ID: 92454623005 Collected: 11/20/19 10:05 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic ND mg/kg 11/23/19 15:53 7440-38-2 D311/21/19 16:357.0 3.5 5
Barium 323 mg/kg 11/23/19 15:53 7440-39-3 D311/21/19 16:353.5 1.8 5
Cadmium ND mg/kg 11/23/19 15:53 7440-43-9 D311/21/19 16:350.70 0.35 5
Chromium 119 mg/kg 11/23/19 15:53 7440-47-3 D311/21/19 16:353.5 1.8 5
Lead 13.1 mg/kg 11/23/19 15:53 7439-92-1 D311/21/19 16:353.5 1.8 5
Selenium ND mg/kg 11/23/19 15:53 7782-49-2 D311/21/19 16:357.0 3.5 5
Silver ND mg/kg 11/23/19 15:53 7440-22-4 D311/21/19 16:353.5 1.8 5
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.020 mg/kg 11/22/19 12:14 7439-97-6 B,BC11/21/19 11:570.0029 0.0014 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/25/19 18:14 83-32-911/23/19 13:400.47 0.12 1
Acenaphthylene ND mg/kg 11/25/19 18:14 208-96-811/23/19 13:400.47 0.11 1
Aniline ND mg/kg 11/25/19 18:14 62-53-311/23/19 13:400.47 0.11 1
Anthracene ND mg/kg 11/25/19 18:14 120-12-711/23/19 13:400.47 0.12 1
Benzo(a)anthracene ND mg/kg 11/25/19 18:14 56-55-311/23/19 13:400.47 0.15 1
Benzo(a)pyrene ND mg/kg 11/25/19 18:14 50-32-811/23/19 13:400.47 0.20 1
Benzo(b)fluoranthene ND mg/kg 11/25/19 18:14 205-99-211/23/19 13:400.47 0.19 1
Benzo(g,h,i)perylene ND mg/kg 11/25/19 18:14 191-24-211/23/19 13:400.47 0.18 1
Benzo(k)fluoranthene ND mg/kg 11/25/19 18:14 207-08-911/23/19 13:400.47 0.20 1
Benzoic Acid ND mg/kg 11/25/19 18:14 65-85-011/23/19 13:402.3 0.51 1
Benzyl alcohol ND mg/kg 11/25/19 18:14 100-51-611/23/19 13:400.94 0.25 1
4-Bromophenylphenyl ether ND mg/kg 11/25/19 18:14 101-55-311/23/19 13:400.47 0.12 1
Butylbenzylphthalate ND mg/kg 11/25/19 18:14 85-68-711/23/19 13:400.47 0.12 1
4-Chloro-3-methylphenol ND mg/kg 11/25/19 18:14 59-50-711/23/19 13:400.94 0.29 1
4-Chloroaniline ND mg/kg 11/25/19 18:14 106-47-811/23/19 13:402.3 0.29 1
bis(2-Chloroethoxy)methane ND mg/kg 11/25/19 18:14 111-91-111/23/19 13:400.47 0.13 1
bis(2-Chloroethyl) ether ND mg/kg 11/25/19 18:14 111-44-411/23/19 13:400.47 0.10 1
2-Chloronaphthalene ND mg/kg 11/25/19 18:14 91-58-711/23/19 13:400.47 0.10 1
2-Chlorophenol ND mg/kg 11/25/19 18:14 95-57-811/23/19 13:400.47 0.11 1
4-Chlorophenylphenyl ether ND mg/kg 11/25/19 18:14 7005-72-311/23/19 13:400.47 0.12 1
Chrysene ND mg/kg 11/25/19 18:14 218-01-911/23/19 13:400.47 0.14 1
Dibenz(a,h)anthracene ND mg/kg 11/25/19 18:14 53-70-311/23/19 13:400.47 0.19 1
Dibenzofuran ND mg/kg 11/25/19 18:14 132-64-911/23/19 13:400.47 0.12 1
1,2-Dichlorobenzene ND mg/kg 11/25/19 18:14 95-50-111/23/19 13:400.47 0.10 1
1,3-Dichlorobenzene ND mg/kg 11/25/19 18:14 541-73-111/23/19 13:400.47 0.11 1
1,4-Dichlorobenzene ND mg/kg 11/25/19 18:14 106-46-711/23/19 13:400.47 0.10 1
3,3'-Dichlorobenzidine ND mg/kg 11/25/19 18:14 91-94-111/23/19 13:402.3 0.33 1
2,4-Dichlorophenol ND mg/kg 11/25/19 18:14 120-83-211/23/19 13:400.47 0.15 1
Diethylphthalate ND mg/kg 11/25/19 18:14 84-66-211/23/19 13:400.47 0.10 1
2,4-Dimethylphenol ND mg/kg 11/25/19 18:14 105-67-911/23/19 13:400.47 0.12 1
Dimethylphthalate ND mg/kg 11/25/19 18:14 131-11-311/23/19 13:400.47 0.11 1
Di-n-butylphthalate ND mg/kg 11/25/19 18:14 84-74-211/23/19 13:400.47 0.12 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/25/19 18:14 534-52-111/23/19 13:400.94 0.76 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-3 (17-19)Lab ID: 92454623005 Collected: 11/20/19 10:05 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/25/19 18:14 51-28-511/23/19 13:402.3 1.5 1
2,4-Dinitrotoluene ND mg/kg 11/25/19 18:14 121-14-211/23/19 13:400.47 0.12 1
2,6-Dinitrotoluene ND mg/kg 11/25/19 18:14 606-20-211/23/19 13:400.47 0.12 1
Di-n-octylphthalate ND mg/kg 11/25/19 18:14 117-84-011/23/19 13:400.47 0.27 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/25/19 18:14 117-81-711/23/19 13:400.47 0.15 1
Fluoranthene ND mg/kg 11/25/19 18:14 206-44-011/23/19 13:400.47 0.14 1
Fluorene ND mg/kg 11/25/19 18:14 86-73-711/23/19 13:400.47 0.13 1
Hexachloro-1,3-butadiene ND mg/kg 11/25/19 18:14 87-68-311/23/19 13:400.47 0.11 1
Hexachlorobenzene ND mg/kg 11/25/19 18:14 118-74-111/23/19 13:400.47 0.12 1
Hexachlorocyclopentadiene ND mg/kg 11/25/19 18:14 77-47-4 v211/23/19 13:400.47 0.19 1
Hexachloroethane ND mg/kg 11/25/19 18:14 67-72-111/23/19 13:400.47 0.11 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/25/19 18:14 193-39-511/23/19 13:400.47 0.21 1
Isophorone ND mg/kg 11/25/19 18:14 78-59-111/23/19 13:400.47 0.10 1
1-Methylnaphthalene ND mg/kg 11/25/19 18:14 90-12-011/23/19 13:400.47 0.12 1
2-Methylnaphthalene ND mg/kg 11/25/19 18:14 91-57-611/23/19 13:400.47 0.12 1
2-Methylphenol(o-Cresol)ND mg/kg 11/25/19 18:14 95-48-711/23/19 13:400.47 0.10 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/25/19 18:14 15831-10-411/23/19 13:400.47 0.12 1
Naphthalene ND mg/kg 11/25/19 18:14 91-20-311/23/19 13:400.47 0.11 1
2-Nitroaniline ND mg/kg 11/25/19 18:14 88-74-4 v111/23/19 13:402.3 0.24 1
3-Nitroaniline ND mg/kg 11/25/19 18:14 99-09-211/23/19 13:402.3 0.25 1
4-Nitroaniline ND mg/kg 11/25/19 18:14 100-01-611/23/19 13:400.94 0.23 1
Nitrobenzene ND mg/kg 11/25/19 18:14 98-95-311/23/19 13:400.47 0.11 1
2-Nitrophenol ND mg/kg 11/25/19 18:14 88-75-511/23/19 13:400.47 0.14 1
4-Nitrophenol ND mg/kg 11/25/19 18:14 100-02-711/23/19 13:402.3 0.75 1
N-Nitrosodimethylamine ND mg/kg 11/25/19 18:14 62-75-911/23/19 13:400.47 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 11/25/19 18:14 621-64-711/23/19 13:400.47 0.13 1
N-Nitrosodiphenylamine ND mg/kg 11/25/19 18:14 86-30-611/23/19 13:400.47 0.12 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/25/19 18:14 108-60-111/23/19 13:400.47 0.13 1
Pentachlorophenol ND mg/kg 11/25/19 18:14 87-86-511/23/19 13:402.3 0.21 1
Phenanthrene ND mg/kg 11/25/19 18:14 85-01-811/23/19 13:400.47 0.12 1
Phenol ND mg/kg 11/25/19 18:14 108-95-211/23/19 13:400.47 0.11 1
Pyrene ND mg/kg 11/25/19 18:14 129-00-011/23/19 13:400.47 0.13 1
Pyridine ND mg/kg 11/25/19 18:14 110-86-111/23/19 13:400.47 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 11/25/19 18:14 120-82-111/23/19 13:400.47 0.11 1
2,4,5-Trichlorophenol ND mg/kg 11/25/19 18:14 95-95-411/23/19 13:400.47 0.12 1
2,4,6-Trichlorophenol ND mg/kg 11/25/19 18:14 88-06-211/23/19 13:400.47 0.12 1
Surrogates
Nitrobenzene-d5 (S)44 %11/25/19 18:14 4165-60-011/23/19 13:4023-110 1
2-Fluorobiphenyl (S)44 %11/25/19 18:14 321-60-811/23/19 13:4030-110 1
Terphenyl-d14 (S)47 %11/25/19 18:14 1718-51-011/23/19 13:4028-110 1
Phenol-d6 (S)42 %11/25/19 18:14 13127-88-311/23/19 13:4022-110 1
2-Fluorophenol (S)39 %11/25/19 18:14 367-12-411/23/19 13:4013-110 1
2,4,6-Tribromophenol (S)34 %11/25/19 18:14 118-79-611/23/19 13:4027-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-3 (17-19)Lab ID: 92454623005 Collected: 11/20/19 10:05 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 11/25/19 17:43 67-64-111/25/19 10:080.12 0.011 1
Benzene ND mg/kg 11/25/19 17:43 71-43-211/25/19 10:080.0060 0.0011 1
Bromobenzene ND mg/kg 11/25/19 17:43 108-86-111/25/19 10:080.0060 0.0016 1
Bromochloromethane ND mg/kg 11/25/19 17:43 74-97-511/25/19 10:080.0060 0.0015 1
Bromodichloromethane ND mg/kg 11/25/19 17:43 75-27-411/25/19 10:080.0060 0.0012 1
Bromoform ND mg/kg 11/25/19 17:43 75-25-211/25/19 10:080.0060 0.0029 1
Bromomethane ND mg/kg 11/25/19 17:43 74-83-911/25/19 10:080.012 0.0028 1
2-Butanone (MEK)ND mg/kg 11/25/19 17:43 78-93-311/25/19 10:080.12 0.014 1
n-Butylbenzene ND mg/kg 11/25/19 17:43 104-51-811/25/19 10:080.0060 0.0034 1
sec-Butylbenzene ND mg/kg 11/25/19 17:43 135-98-811/25/19 10:080.0060 0.0025 1
tert-Butylbenzene ND mg/kg 11/25/19 17:43 98-06-611/25/19 10:080.0060 0.0020 1
Carbon tetrachloride ND mg/kg 11/25/19 17:43 56-23-511/25/19 10:080.0060 0.0012 1
Chlorobenzene ND mg/kg 11/25/19 17:43 108-90-711/25/19 10:080.0060 0.0012 1
Chloroethane ND mg/kg 11/25/19 17:43 75-00-3 IK11/25/19 10:080.012 0.0025 1
Chloroform ND mg/kg 11/25/19 17:43 67-66-311/25/19 10:080.0060 0.0013 1
Chloromethane ND mg/kg 11/25/19 17:43 74-87-311/25/19 10:080.012 0.0039 1
2-Chlorotoluene ND mg/kg 11/25/19 17:43 95-49-811/25/19 10:080.0060 0.0018 1
4-Chlorotoluene ND mg/kg 11/25/19 17:43 106-43-411/25/19 10:080.0060 0.0018 1
1,2-Dibromo-3-chloropropane ND mg/kg 11/25/19 17:43 96-12-811/25/19 10:080.0060 0.0031 1
Dibromochloromethane ND mg/kg 11/25/19 17:43 124-48-111/25/19 10:080.0060 0.0030 1
1,2-Dibromoethane (EDB)ND mg/kg 11/25/19 17:43 106-93-411/25/19 10:080.0060 0.0013 1
Dibromomethane ND mg/kg 11/25/19 17:43 74-95-311/25/19 10:080.0060 0.0018 1
1,2-Dichlorobenzene ND mg/kg 11/25/19 17:43 95-50-111/25/19 10:080.0060 0.0021 1
1,3-Dichlorobenzene ND mg/kg 11/25/19 17:43 541-73-111/25/19 10:080.0060 0.0021 1
1,4-Dichlorobenzene ND mg/kg 11/25/19 17:43 106-46-711/25/19 10:080.0060 0.0021 1
Dichlorodifluoromethane ND mg/kg 11/25/19 17:43 75-71-811/25/19 10:080.012 0.0049 1
1,1-Dichloroethane ND mg/kg 11/25/19 17:43 75-34-311/25/19 10:080.0060 0.00088 1
1,2-Dichloroethane ND mg/kg 11/25/19 17:43 107-06-211/25/19 10:080.0060 0.0012 1
1,1-Dichloroethene ND mg/kg 11/25/19 17:43 75-35-411/25/19 10:080.0060 0.0014 1
cis-1,2-Dichloroethene ND mg/kg 11/25/19 17:43 156-59-211/25/19 10:080.0060 0.0010 1
trans-1,2-Dichloroethene ND mg/kg 11/25/19 17:43 156-60-511/25/19 10:080.0060 0.0012 1
1,2-Dichloropropane ND mg/kg 11/25/19 17:43 78-87-511/25/19 10:080.0060 0.0023 1
1,3-Dichloropropane ND mg/kg 11/25/19 17:43 142-28-911/25/19 10:080.0060 0.0023 1
2,2-Dichloropropane ND mg/kg 11/25/19 17:43 594-20-711/25/19 10:080.0060 0.00059 1
1,1-Dichloropropene ND mg/kg 11/25/19 17:43 563-58-611/25/19 10:080.0060 0.0025 1
cis-1,3-Dichloropropene ND mg/kg 11/25/19 17:43 10061-01-511/25/19 10:080.0060 0.0027 1
trans-1,3-Dichloropropene ND mg/kg 11/25/19 17:43 10061-02-611/25/19 10:080.0060 0.0011 1
Diisopropyl ether ND mg/kg 11/25/19 17:43 108-20-311/25/19 10:080.0060 0.0034 1
Ethylbenzene ND mg/kg 11/25/19 17:43 100-41-411/25/19 10:080.0060 0.0013 1
Hexachloro-1,3-butadiene ND mg/kg 11/25/19 17:43 87-68-311/25/19 10:080.0060 0.0030 1
2-Hexanone ND mg/kg 11/25/19 17:43 591-78-611/25/19 10:080.060 0.0062 1
Isopropylbenzene (Cumene)ND mg/kg 11/25/19 17:43 98-82-811/25/19 10:080.0060 0.0017 1
p-Isopropyltoluene ND mg/kg 11/25/19 17:43 99-87-611/25/19 10:080.0060 0.0029 1
Methylene Chloride ND mg/kg 11/25/19 17:43 75-09-211/25/19 10:080.024 0.0071 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 11/25/19 17:43 108-10-111/25/19 10:080.060 0.0045 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: SB-3 (17-19)Lab ID: 92454623005 Collected: 11/20/19 10:05 Received: 11/20/19 10:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 11/25/19 17:43 1634-04-411/25/19 10:080.0060 0.0034 1
Naphthalene ND mg/kg 11/25/19 17:43 91-20-311/25/19 10:080.0060 0.0051 1
n-Propylbenzene ND mg/kg 11/25/19 17:43 103-65-111/25/19 10:080.0060 0.0020 1
Styrene ND mg/kg 11/25/19 17:43 100-42-511/25/19 10:080.0060 0.0018 1
1,1,1,2-Tetrachloroethane ND mg/kg 11/25/19 17:43 630-20-611/25/19 10:080.0060 0.0015 1
1,1,2,2-Tetrachloroethane ND mg/kg 11/25/19 17:43 79-34-511/25/19 10:080.0060 0.0021 1
Tetrachloroethene ND mg/kg 11/25/19 17:43 127-18-411/25/19 10:080.0060 0.0019 1
Toluene ND mg/kg 11/25/19 17:43 108-88-311/25/19 10:080.0060 0.0019 1
1,2,3-Trichlorobenzene ND mg/kg 11/25/19 17:43 87-61-611/25/19 10:080.0060 0.0043 1
1,2,4-Trichlorobenzene ND mg/kg 11/25/19 17:43 120-82-111/25/19 10:080.0060 0.0032 1
1,1,1-Trichloroethane ND mg/kg 11/25/19 17:43 71-55-611/25/19 10:080.0060 0.0010 1
1,1,2-Trichloroethane ND mg/kg 11/25/19 17:43 79-00-511/25/19 10:080.0060 0.0014 1
Trichloroethene ND mg/kg 11/25/19 17:43 79-01-611/25/19 10:080.0060 0.0016 1
Trichlorofluoromethane ND mg/kg 11/25/19 17:43 75-69-411/25/19 10:080.0060 0.0014 1
1,2,3-Trichloropropane ND mg/kg 11/25/19 17:43 96-18-411/25/19 10:080.0060 0.0020 1
1,2,4-Trimethylbenzene ND mg/kg 11/25/19 17:43 95-63-6 v111/25/19 10:080.0060 0.0023 1
1,3,5-Trimethylbenzene ND mg/kg 11/25/19 17:43 108-67-811/25/19 10:080.0060 0.0020 1
Vinyl acetate ND mg/kg 11/25/19 17:43 108-05-4 v111/25/19 10:080.060 0.020 1
Vinyl chloride ND mg/kg 11/25/19 17:43 75-01-411/25/19 10:080.012 0.0023 1
Xylene (Total)ND mg/kg 11/25/19 17:43 1330-20-711/25/19 10:080.012 0.0042 1
m&p-Xylene ND mg/kg 11/25/19 17:43 179601-23-111/25/19 10:080.012 0.0028 1
o-Xylene ND mg/kg 11/25/19 17:43 95-47-611/25/19 10:080.0060 0.0014 1
Surrogates
Toluene-d8 (S)114 %11/25/19 17:43 2037-26-511/25/19 10:0870-130 1
4-Bromofluorobenzene (S)99 %11/25/19 17:43 460-00-411/25/19 10:0870-130 1
1,2-Dichloroethane-d4 (S)87 %11/25/19 17:43 17060-07-011/25/19 10:0870-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)ND mg/kg 11/25/19 13:36 123-91-111/25/19 11:520.014 0.0042 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %11/25/19 13:36 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)105 %11/25/19 13:36 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 28.8 %11/21/19 13:250.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 73.3 %01/10/20 14:55 H301/10/20 14:451
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.870J mg/kg 01/11/20 14:33 18540-29-9 H3,J01/10/20 20:501.36 0.348 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: Trip Blank Lab ID: 92454623006 Collected: 11/20/19 00:00 Received: 11/20/19 10:26 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 11/25/19 14:40 67-64-125.0 6.2 1
Benzene ND ug/L 11/25/19 14:40 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/25/19 14:40 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/25/19 14:40 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/25/19 14:40 75-27-41.0 0.26 1
Bromoform ND ug/L 11/25/19 14:40 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/25/19 14:40 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 11/25/19 14:40 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/25/19 14:40 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/25/19 14:40 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/25/19 14:40 75-00-31.0 0.49 1
Chloroform ND ug/L 11/25/19 14:40 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/25/19 14:40 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/25/19 14:40 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/25/19 14:40 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/25/19 14:40 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/25/19 14:40 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/25/19 14:40 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/25/19 14:40 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/25/19 14:40 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/25/19 14:40 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/25/19 14:40 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/25/19 14:40 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/25/19 14:40 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/25/19 14:40 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/25/19 14:40 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 11/25/19 14:40 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/25/19 14:40 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/25/19 14:40 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/25/19 14:40 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/25/19 14:40 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/25/19 14:40 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/25/19 14:40 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/25/19 14:40 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/25/19 14:40 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/25/19 14:40 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene 1.1 ug/L 11/25/19 14:40 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/25/19 14:40 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/25/19 14:40 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/25/19 14:40 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/25/19 14:40 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/25/19 14:40 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/25/19 14:40 91-20-31.0 0.35 1
Styrene ND ug/L 11/25/19 14:40 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/25/19 14:40 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 11/25/19 14:40 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 63
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454623
ROW-603
Sample: Trip Blank Lab ID: 92454623006 Collected: 11/20/19 00:00 Received: 11/20/19 10:26 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 11/25/19 14:40 127-18-41.0 0.16 1
Toluene ND ug/L 11/25/19 14:40 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/25/19 14:40 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/25/19 14:40 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/25/19 14:40 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/25/19 14:40 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/25/19 14:40 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/25/19 14:40 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/25/19 14:40 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/25/19 14:40 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/25/19 14:40 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/25/19 14:40 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/25/19 14:40 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/25/19 14:40 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %11/25/19 14:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/25/19 14:40 17060-07-070-130 1
Toluene-d8 (S)98 %11/25/19 14:40 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/21/19 19:58 123-91-12.0 1.2 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %11/21/19 19:58 17060-07-050-150 1
Toluene-d8 (S)103 %11/21/19 19:58 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
510897
EPA 7471B
EPA 7471B
7471 Mercury
Associated Lab Samples: 92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2740675
Associated Lab Samples:92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Matrix: Solid
AnalyzedMDL
Mercury mg/kg 0.0057J 0.0060 BC11/22/19 12:180.0030
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2740676LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0810.083 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2740677MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454343006
2740678
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg M6,R10.38 15 75-125335 37 200.352.4 2.4 3.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511039
EPA 3050B
EPA 6010D
6010 MET
Associated Lab Samples: 92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2741663
Associated Lab Samples:92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Matrix: Solid
AnalyzedMDL
Arsenic mg/kg ND 1.0 11/23/19 00:140.50
Barium mg/kg ND 0.50 11/23/19 00:140.25
Cadmium mg/kg ND 0.10 11/23/19 00:140.050
Chromium mg/kg ND 0.50 11/23/19 00:140.25
Lead mg/kg ND 0.50 11/23/19 00:140.25
Selenium mg/kg ND 1.0 11/23/19 00:140.50
Silver mg/kg ND 0.50 11/23/19 00:140.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2741664LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 47.950 96 80-120
Barium mg/kg 48.550 97 80-120
Cadmium mg/kg 49.050 98 80-120
Chromium mg/kg 49.750 99 80-120
Lead mg/kg 47.550 95 80-120
Selenium mg/kg 45.950 92 80-120
Silver mg/kg 23.925 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2741665MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454168005
2741666
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 55.6 90 75-12589 2 2055.61.9 52.0 51.1
Barium mg/kg 55.6 95 75-12598 2 2055.635.0 87.9 89.6
Cadmium mg/kg 55.6 96 75-12593 4 2055.6ND 53.3 51.5
Chromium mg/kg 55.6 105 75-125109 3 2055.612.8 71.4 73.3
Lead mg/kg 55.6 93 75-125106 12 2055.66.6 58.2 65.4
Selenium mg/kg 55.6 85 75-12582 4 2055.6ND 47.7 45.9
Silver mg/kg 27.8 97 75-12594 3 2027.8ND 27.0 26.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511468
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92454623001, 92454623002, 92454623003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743576
Associated Lab Samples:92454623001, 92454623002, 92454623003
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 11/24/19 13:300.0012
1,1,1-Trichloroethane mg/kg ND 0.0050 11/24/19 13:300.00087
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 11/24/19 13:300.0017
1,1,2-Trichloroethane mg/kg ND 0.0050 11/24/19 13:300.0011
1,1-Dichloroethane mg/kg ND 0.0050 11/24/19 13:300.00074
1,1-Dichloroethene mg/kg ND 0.0050 11/24/19 13:300.0012
1,1-Dichloropropene mg/kg ND 0.0050 11/24/19 13:300.0021
1,2,3-Trichlorobenzene mg/kg ND 0.0050 11/24/19 13:300.0036
1,2,3-Trichloropropane mg/kg ND 0.0050 11/24/19 13:300.0017
1,2,4-Trichlorobenzene mg/kg ND 0.0050 11/24/19 13:300.0026
1,2,4-Trimethylbenzene mg/kg ND 0.0050 11/24/19 13:300.0020
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 11/24/19 13:300.0025
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 11/24/19 13:300.0011
1,2-Dichlorobenzene mg/kg ND 0.0050 11/24/19 13:300.0018
1,2-Dichloroethane mg/kg ND 0.0050 11/24/19 13:300.0010
1,2-Dichloropropane mg/kg ND 0.0050 11/24/19 13:300.0019
1,3,5-Trimethylbenzene mg/kg ND 0.0050 11/24/19 13:300.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 11/24/19 13:300.0018
1,3-Dichloropropane mg/kg ND 0.0050 11/24/19 13:300.0019
1,4-Dichlorobenzene mg/kg ND 0.0050 11/24/19 13:300.0017
2,2-Dichloropropane mg/kg ND 0.0050 11/24/19 13:300.00049
2-Butanone (MEK)mg/kg ND 0.10 11/24/19 13:300.012
2-Chlorotoluene mg/kg ND 0.0050 11/24/19 13:300.0015
2-Hexanone mg/kg ND 0.050 11/24/19 13:300.0052
4-Chlorotoluene mg/kg ND 0.0050 11/24/19 13:300.0015
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 11/24/19 13:300.0037
Acetone mg/kg ND 0.10 11/24/19 13:300.0094
Benzene mg/kg ND 0.0050 11/24/19 13:300.00090
Bromobenzene mg/kg ND 0.0050 11/24/19 13:300.0014
Bromochloromethane mg/kg ND 0.0050 11/24/19 13:300.0012
Bromodichloromethane mg/kg ND 0.0050 11/24/19 13:300.00098
Bromoform mg/kg ND 0.0050 11/24/19 13:300.0024
Bromomethane mg/kg ND 0.010 IH11/24/19 13:300.0024
Carbon tetrachloride mg/kg ND 0.0050 11/24/19 13:300.00096
Chlorobenzene mg/kg ND 0.0050 11/24/19 13:300.00097
Chloroethane mg/kg ND 0.010 11/24/19 13:300.0021
Chloroform mg/kg ND 0.0050 11/24/19 13:300.0011
Chloromethane mg/kg ND 0.010 11/24/19 13:300.0033
cis-1,2-Dichloroethene mg/kg ND 0.0050 11/24/19 13:300.00087
cis-1,3-Dichloropropene mg/kg ND 0.0050 11/24/19 13:300.0023
Dibromochloromethane mg/kg ND 0.0050 11/24/19 13:300.0025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743576
Associated Lab Samples:92454623001, 92454623002, 92454623003
Matrix: Solid
AnalyzedMDL
Dibromomethane mg/kg ND 0.0050 11/24/19 13:300.0015
Dichlorodifluoromethane mg/kg ND 0.010 11/24/19 13:300.0041
Diisopropyl ether mg/kg ND 0.0050 11/24/19 13:300.0029
Ethylbenzene mg/kg ND 0.0050 11/24/19 13:300.0011
Hexachloro-1,3-butadiene mg/kg ND 0.0050 11/24/19 13:300.0025
Isopropylbenzene (Cumene)mg/kg ND 0.0050 11/24/19 13:300.0014
m&p-Xylene mg/kg ND 0.010 11/24/19 13:300.0024
Methyl-tert-butyl ether mg/kg ND 0.0050 11/24/19 13:300.0029
Methylene Chloride mg/kg ND 0.020 11/24/19 13:300.0059
n-Butylbenzene mg/kg ND 0.0050 11/24/19 13:300.0028
n-Propylbenzene mg/kg ND 0.0050 11/24/19 13:300.0017
Naphthalene mg/kg ND 0.0050 11/24/19 13:300.0042
o-Xylene mg/kg ND 0.0050 11/24/19 13:300.0012
p-Isopropyltoluene mg/kg ND 0.0050 11/24/19 13:300.0024
sec-Butylbenzene mg/kg ND 0.0050 11/24/19 13:300.0021
Styrene mg/kg ND 0.0050 11/24/19 13:300.0015
tert-Butylbenzene mg/kg ND 0.0050 11/24/19 13:300.0017
Tetrachloroethene mg/kg ND 0.0050 11/24/19 13:300.0016
Toluene mg/kg ND 0.0050 11/24/19 13:300.0016
trans-1,2-Dichloroethene mg/kg ND 0.0050 11/24/19 13:300.00098
trans-1,3-Dichloropropene mg/kg ND 0.0050 11/24/19 13:300.00088
Trichloroethene mg/kg ND 0.0050 11/24/19 13:300.0013
Trichlorofluoromethane mg/kg ND 0.0050 11/24/19 13:300.0012
Vinyl acetate mg/kg ND 0.050 IL11/24/19 13:300.016
Vinyl chloride mg/kg ND 0.010 11/24/19 13:300.0019
Xylene (Total)mg/kg ND 0.010 11/24/19 13:300.0035
1,2-Dichloroethane-d4 (S)%96 70-132 11/24/19 13:30
4-Bromofluorobenzene (S)%102 70-130 11/24/19 13:30
Toluene-d8 (S)%105 70-130 11/24/19 13:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743577LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.0510.05 103 70-130
1,1,1-Trichloroethane mg/kg 0.0590.05 117 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.0480.05 97 55-130
1,1,2-Trichloroethane mg/kg 0.0510.05 102 70-130
1,1-Dichloroethane mg/kg 0.0520.05 104 68-130
1,1-Dichloroethene mg/kg 0.0580.05 116 70-130
1,1-Dichloropropene mg/kg 0.0640.05 129 70-130
1,2,3-Trichlorobenzene mg/kg 0.0490.05 98 70-130
1,2,3-Trichloropropane mg/kg 0.0480.05 96 70-130
1,2,4-Trichlorobenzene mg/kg 0.0470.05 95 70-130
1,2,4-Trimethylbenzene mg/kg 0.0490.05 98 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743577LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane mg/kg 0.0500.05 100 57-141
1,2-Dibromoethane (EDB)mg/kg 0.0490.05 98 70-130
1,2-Dichlorobenzene mg/kg 0.0490.05 98 70-130
1,2-Dichloroethane mg/kg 0.0470.05 95 70-130
1,2-Dichloropropane mg/kg 0.0530.05 107 70-130
1,3,5-Trimethylbenzene mg/kg 0.0510.05 103 70-130
1,3-Dichlorobenzene mg/kg 0.0490.05 97 70-130
1,3-Dichloropropane mg/kg 0.0520.05 103 70-130
1,4-Dichlorobenzene mg/kg 0.0480.05 95 70-130
2,2-Dichloropropane mg/kg 0.0590.05 117 70-130
2-Butanone (MEK)mg/kg 0.090J0.1 90 60-130
2-Chlorotoluene mg/kg 0.0510.05 101 70-130
2-Hexanone mg/kg 0.100.1 103 70-132
4-Chlorotoluene mg/kg 0.0500.05 100 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.0980.1 98 69-130
Acetone mg/kg 0.097J0.1 97 49-148
Benzene mg/kg 0.0540.05 109 70-130
Bromobenzene mg/kg 0.0500.05 99 70-130
Bromochloromethane mg/kg 0.0470.05 94 70-130
Bromodichloromethane mg/kg 0.0500.05 101 70-130
Bromoform mg/kg 0.0500.05 100 68-136
Bromomethane mg/kg 0.066 IH0.05 132 60-140
Carbon tetrachloride mg/kg 0.0620.05 123 70-130
Chlorobenzene mg/kg 0.0500.05 100 70-130
Chloroethane mg/kg 0.0590.05 118 51-147
Chloroform mg/kg 0.0480.05 97 70-130
Chloromethane mg/kg 0.0510.05 102 48-130
cis-1,2-Dichloroethene mg/kg 0.0500.05 100 70-130
cis-1,3-Dichloropropene mg/kg 0.0550.05 109 70-130
Dibromochloromethane mg/kg 0.0510.05 101 70-130
Dibromomethane mg/kg 0.0490.05 97 70-130
Dichlorodifluoromethane mg/kg 0.0550.05 110 49-130
Diisopropyl ether mg/kg 0.0520.05 103 66-130
Ethylbenzene mg/kg 0.0530.05 106 70-130
Hexachloro-1,3-butadiene mg/kg 0.0510.05 102 70-130
Isopropylbenzene (Cumene)mg/kg 0.0540.05 109 70-130
m&p-Xylene mg/kg 0.100.1 104 70-130
Methyl-tert-butyl ether mg/kg 0.0580.05 116 70-130
Methylene Chloride mg/kg 0.0470.05 94 50-137
n-Butylbenzene mg/kg 0.0520.05 103 70-130
n-Propylbenzene mg/kg 0.0510.05 102 70-130
Naphthalene mg/kg 0.0500.05 100 70-131
o-Xylene mg/kg 0.0520.05 103 70-130
p-Isopropyltoluene mg/kg 0.0520.05 103 70-130
sec-Butylbenzene mg/kg 0.0520.05 105 70-130
Styrene mg/kg 0.0500.05 100 70-130
tert-Butylbenzene mg/kg 0.0430.05 87 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743577LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene mg/kg 0.0540.05 107 56-130
Toluene mg/kg 0.0510.05 102 70-130
trans-1,2-Dichloroethene mg/kg 0.0550.05 109 70-130
trans-1,3-Dichloropropene mg/kg 0.0510.05 102 70-130
Trichloroethene mg/kg 0.0570.05 115 70-141
Trichlorofluoromethane mg/kg 0.0610.05 122 67-130
Vinyl acetate mg/kg 0.091 IL0.1 91 10-136
Vinyl chloride mg/kg 0.0640.05 129 67-130
Xylene (Total)mg/kg 0.160.15 104 70-130
1,2-Dichloroethane-d4 (S)%102 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2743579MATRIX SPIKE SAMPLE:
MSSpike
Result
92454281007
1,1,1,2-Tetrachloroethane mg/kg 0.0140.018 78 52-133ND
1,1,1-Trichloroethane mg/kg 0.0140.018 78 49-137ND
1,1,2,2-Tetrachloroethane mg/kg 0.0150.018 84 39-150ND
1,1,2-Trichloroethane mg/kg 0.0160.018 85 48-140ND
1,1-Dichloroethane mg/kg 0.0140.018 78 46-135ND
1,1-Dichloroethene mg/kg 0.0160.018 86 38-149ND
1,1-Dichloropropene mg/kg 0.0150.018 81 41-140ND
1,2,3-Trichlorobenzene mg/kg 0.0140.018 79 10-158ND
1,2,3-Trichloropropane mg/kg 0.0160.018 87 33-157ND
1,2,4-Trichlorobenzene mg/kg 0.0140.018 79 10-155ND
1,2,4-Trimethylbenzene mg/kg 0.0140.018 74 24-154ND
1,2-Dibromo-3-chloropropane mg/kg 0.0160.018 90 33-158ND
1,2-Dibromoethane (EDB)mg/kg 0.0150.018 80 40-136ND
1,2-Dichlorobenzene mg/kg 0.0140.018 80 27-146ND
1,2-Dichloroethane mg/kg 0.0150.018 81 49-140ND
1,2-Dichloropropane mg/kg 0.0150.018 83 44-143ND
1,3,5-Trimethylbenzene mg/kg 0.0140.018 77 40-144ND
1,3-Dichlorobenzene mg/kg 0.0140.018 77 33-140ND
1,3-Dichloropropane mg/kg 0.0150.018 81 47-147ND
1,4-Dichlorobenzene mg/kg 0.0140.018 79 35-139ND
2,2-Dichloropropane mg/kg 0.0140.018 77 41-140ND
2-Butanone (MEK)mg/kg 0.027J0.036 74 10-181ND
2-Chlorotoluene mg/kg 0.0140.018 78 38-147ND
2-Hexanone mg/kg 0.034J0.036 93 18-169ND
4-Chlorotoluene mg/kg 0.0150.018 80 36-145ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.032J0.036 88 16-175ND
Acetone mg/kg 0.036J0.036 98 10-200ND
Benzene mg/kg 0.0150.018 80 46-136ND
Bromobenzene mg/kg 0.0150.018 80 38-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2743579MATRIX SPIKE SAMPLE:
MSSpike
Result
92454281007
Bromochloromethane mg/kg 0.0150.018 81 44-142ND
Bromodichloromethane mg/kg 0.0150.018 83 41-140ND
Bromoform mg/kg 0.0160.018 87 34-145ND
Bromomethane mg/kg 0.020 IH0.018 112 14-162ND
Carbon tetrachloride mg/kg 0.0190.018 102 44-141ND
Chlorobenzene mg/kg 0.0140.018 80 39-141ND
Chloroethane mg/kg 0.019 v10.018 104 10-182ND
Chloroform mg/kg 0.0140.018 77 45-140ND
Chloromethane mg/kg 0.0140.018 79 19-149ND
cis-1,2-Dichloroethene mg/kg 0.0140.018 78 38-150ND
cis-1,3-Dichloropropene mg/kg 0.0140.018 80 30-144ND
Dibromochloromethane mg/kg 0.0140.018 79 36-145ND
Dibromomethane mg/kg 0.0160.018 86 41-145ND
Dichlorodifluoromethane mg/kg 0.0130.018 69 16-146ND
Diisopropyl ether mg/kg 0.0140.018 77 41-143ND
Ethylbenzene mg/kg 0.0150.018 83 35-144ND
Hexachloro-1,3-butadiene mg/kg 0.0120.018 68 10-160ND
Isopropylbenzene (Cumene)mg/kg 0.0150.018 82 30-152ND
m&p-Xylene mg/kg 0.0290.036 80 33-145ND
Methyl-tert-butyl ether mg/kg 0.0160.018 88 49-140ND
Methylene Chloride mg/kg 0.010J0.018 57 10-174ND
n-Butylbenzene mg/kg 0.0130.018 74 10-160ND
n-Propylbenzene mg/kg 0.0140.018 76 24-159ND
Naphthalene mg/kg 0.0160.018 90 10-171ND
o-Xylene mg/kg 0.0140.018 79 31-150ND
p-Isopropyltoluene mg/kg 0.0140.018 75 21-154ND
sec-Butylbenzene mg/kg 0.0140.018 77 19-159ND
Styrene mg/kg 0.0150.018 80 15-152ND
tert-Butylbenzene mg/kg 0.0120.018 65 31-141ND
Tetrachloroethene mg/kg 0.0140.018 77 19-141ND
Toluene mg/kg 0.0150.018 80 31-146ND
trans-1,2-Dichloroethene mg/kg 0.0150.018 84 28-157ND
trans-1,3-Dichloropropene mg/kg 0.0140.018 79 25-146ND
Trichloroethene mg/kg 0.0140.018 77 34-149ND
Trichlorofluoromethane mg/kg 0.0160.018 87 10-167ND
Vinyl acetate mg/kg 0.024J IL0.036 65 10-200ND
Vinyl chloride mg/kg 0.0160.018 90 36-155ND
Xylene (Total)mg/kg 0.0440.054 80 29-148ND
1,2-Dichloroethane-d4 (S)%100 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454281006
2743578SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND IH30ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454281006
2743578SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND IL30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9795
4-Bromofluorobenzene (S)%104100
Toluene-d8 (S)%108106
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511519
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92454623004, 92454623005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743732
Associated Lab Samples:92454623004, 92454623005
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 11/25/19 10:540.0012
1,1,1-Trichloroethane mg/kg ND 0.0050 11/25/19 10:540.00087
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 11/25/19 10:540.0017
1,1,2-Trichloroethane mg/kg ND 0.0050 11/25/19 10:540.0011
1,1-Dichloroethane mg/kg ND 0.0050 11/25/19 10:540.00074
1,1-Dichloroethene mg/kg ND 0.0050 11/25/19 10:540.0012
1,1-Dichloropropene mg/kg ND 0.0050 11/25/19 10:540.0021
1,2,3-Trichlorobenzene mg/kg ND 0.0050 11/25/19 10:540.0036
1,2,3-Trichloropropane mg/kg ND 0.0050 11/25/19 10:540.0017
1,2,4-Trichlorobenzene mg/kg ND 0.0050 11/25/19 10:540.0026
1,2,4-Trimethylbenzene mg/kg ND 0.0050 v111/25/19 10:540.0020
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 11/25/19 10:540.0025
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 11/25/19 10:540.0011
1,2-Dichlorobenzene mg/kg ND 0.0050 11/25/19 10:540.0018
1,2-Dichloroethane mg/kg ND 0.0050 11/25/19 10:540.0010
1,2-Dichloropropane mg/kg ND 0.0050 11/25/19 10:540.0019
1,3,5-Trimethylbenzene mg/kg ND 0.0050 11/25/19 10:540.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 11/25/19 10:540.0018
1,3-Dichloropropane mg/kg ND 0.0050 11/25/19 10:540.0019
1,4-Dichlorobenzene mg/kg ND 0.0050 11/25/19 10:540.0017
2,2-Dichloropropane mg/kg ND 0.0050 11/25/19 10:540.00049
2-Butanone (MEK)mg/kg ND 0.10 11/25/19 10:540.012
2-Chlorotoluene mg/kg ND 0.0050 11/25/19 10:540.0015
2-Hexanone mg/kg ND 0.050 11/25/19 10:540.0052
4-Chlorotoluene mg/kg ND 0.0050 11/25/19 10:540.0015
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 11/25/19 10:540.0037
Acetone mg/kg ND 0.10 11/25/19 10:540.0094
Benzene mg/kg ND 0.0050 11/25/19 10:540.00090
Bromobenzene mg/kg ND 0.0050 11/25/19 10:540.0014
Bromochloromethane mg/kg ND 0.0050 11/25/19 10:540.0012
Bromodichloromethane mg/kg ND 0.0050 11/25/19 10:540.00098
Bromoform mg/kg ND 0.0050 11/25/19 10:540.0024
Bromomethane mg/kg ND 0.010 11/25/19 10:540.0024
Carbon tetrachloride mg/kg ND 0.0050 11/25/19 10:540.00096
Chlorobenzene mg/kg ND 0.0050 11/25/19 10:540.00097
Chloroethane mg/kg ND 0.010 IK11/25/19 10:540.0021
Chloroform mg/kg ND 0.0050 11/25/19 10:540.0011
Chloromethane mg/kg ND 0.010 11/25/19 10:540.0033
cis-1,2-Dichloroethene mg/kg ND 0.0050 11/25/19 10:540.00087
cis-1,3-Dichloropropene mg/kg ND 0.0050 11/25/19 10:540.0023
Dibromochloromethane mg/kg ND 0.0050 11/25/19 10:540.0025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743732
Associated Lab Samples:92454623004, 92454623005
Matrix: Solid
AnalyzedMDL
Dibromomethane mg/kg ND 0.0050 11/25/19 10:540.0015
Dichlorodifluoromethane mg/kg ND 0.010 11/25/19 10:540.0041
Diisopropyl ether mg/kg ND 0.0050 11/25/19 10:540.0029
Ethylbenzene mg/kg ND 0.0050 11/25/19 10:540.0011
Hexachloro-1,3-butadiene mg/kg ND 0.0050 11/25/19 10:540.0025
Isopropylbenzene (Cumene)mg/kg ND 0.0050 11/25/19 10:540.0014
m&p-Xylene mg/kg ND 0.010 11/25/19 10:540.0024
Methyl-tert-butyl ether mg/kg ND 0.0050 11/25/19 10:540.0029
Methylene Chloride mg/kg ND 0.020 11/25/19 10:540.0059
n-Butylbenzene mg/kg ND 0.0050 11/25/19 10:540.0028
n-Propylbenzene mg/kg ND 0.0050 11/25/19 10:540.0017
Naphthalene mg/kg ND 0.0050 11/25/19 10:540.0042
o-Xylene mg/kg ND 0.0050 11/25/19 10:540.0012
p-Isopropyltoluene mg/kg ND 0.0050 11/25/19 10:540.0024
sec-Butylbenzene mg/kg ND 0.0050 11/25/19 10:540.0021
Styrene mg/kg ND 0.0050 11/25/19 10:540.0015
tert-Butylbenzene mg/kg ND 0.0050 11/25/19 10:540.0017
Tetrachloroethene mg/kg ND 0.0050 11/25/19 10:540.0016
Toluene mg/kg ND 0.0050 11/25/19 10:540.0016
trans-1,2-Dichloroethene mg/kg ND 0.0050 11/25/19 10:540.00098
trans-1,3-Dichloropropene mg/kg ND 0.0050 11/25/19 10:540.00088
Trichloroethene mg/kg ND 0.0050 11/25/19 10:540.0013
Trichlorofluoromethane mg/kg ND 0.0050 11/25/19 10:540.0012
Vinyl acetate mg/kg ND 0.050 v111/25/19 10:540.016
Vinyl chloride mg/kg ND 0.010 11/25/19 10:540.0019
Xylene (Total)mg/kg ND 0.010 11/25/19 10:540.0035
1,2-Dichloroethane-d4 (S)%80 70-132 11/25/19 10:54
4-Bromofluorobenzene (S)%99 70-130 11/25/19 10:54
Toluene-d8 (S)%114 70-130 11/25/19 10:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743733LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2743734
1,1,1,2-Tetrachloroethane mg/kg 0.0570.05 114 70-1301030.052 10 30
1,1,1-Trichloroethane mg/kg 0.0520.05 103 70-130960.048 7 30
1,1,2,2-Tetrachloroethane mg/kg 0.0540.05 108 55-1301040.052 3 30
1,1,2-Trichloroethane mg/kg 0.0540.05 108 70-1301020.051 6 30
1,1-Dichloroethane mg/kg 0.0500.05 101 68-130980.049 3 30
1,1-Dichloroethene mg/kg 0.0530.05 107 70-130980.049 8 30
1,1-Dichloropropene mg/kg 0.0590.05 118 70-1301050.053 11 30
1,2,3-Trichlorobenzene mg/kg 0.0550.05 110 70-1301000.050 9 30
1,2,3-Trichloropropane mg/kg 0.0540.05 108 70-1301020.051 5 30
1,2,4-Trichlorobenzene mg/kg 0.0540.05 108 70-1301000.050 7 30
1,2,4-Trimethylbenzene mg/kg 0.059 v10.05 118 69-1301040.052 13 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743733LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2743734
1,2-Dibromo-3-chloropropane mg/kg 0.0580.05 116 57-1411060.053 9 30
1,2-Dibromoethane (EDB)mg/kg 0.0580.05 115 70-1301050.052 10 30
1,2-Dichlorobenzene mg/kg 0.0530.05 105 70-130980.049 7 30
1,2-Dichloroethane mg/kg 0.0500.05 100 70-130940.047 6 30
1,2-Dichloropropane mg/kg 0.0560.05 111 70-1301020.051 9 30
1,3,5-Trimethylbenzene mg/kg 0.0540.05 108 70-130990.049 9 30
1,3-Dichlorobenzene mg/kg 0.0530.05 106 70-130990.050 7 30
1,3-Dichloropropane mg/kg 0.0580.05 116 70-1301060.053 9 30
1,4-Dichlorobenzene mg/kg 0.0530.05 106 70-130980.049 8 30
2,2-Dichloropropane mg/kg 0.0520.05 105 70-130970.048 8 30
2-Butanone (MEK)mg/kg 0.110.1 113 60-1301100.11 3 30
2-Chlorotoluene mg/kg 0.0530.05 105 70-130970.049 8 30
2-Hexanone mg/kg 0.120.1 116 70-1321080.11 7 30
4-Chlorotoluene mg/kg 0.0530.05 106 70-130970.049 8 30
4-Methyl-2-pentanone (MIBK)mg/kg 0.110.1 106 69-1301020.10 3 30
Acetone mg/kg 0.100.1 101 49-148970.097J 30
Benzene mg/kg 0.0560.05 111 70-1301020.051 9 30
Bromobenzene mg/kg 0.0550.05 110 70-1301010.051 9 30
Bromochloromethane mg/kg 0.0530.05 106 70-1301030.052 3 30
Bromodichloromethane mg/kg 0.0520.05 104 70-130980.049 6 30
Bromoform mg/kg 0.0580.05 115 68-1361080.054 6 30
Bromomethane mg/kg 0.0560.05 111 60-1401060.053 5 30
Carbon tetrachloride mg/kg 0.0550.05 109 70-130980.049 10 30
Chlorobenzene mg/kg 0.0540.05 108 70-130980.049 9 30
Chloroethane mg/kg 0.059 IK0.05 118 51-1471060.053 11 30
Chloroform mg/kg 0.0510.05 102 70-130960.048 6 30
Chloromethane mg/kg 0.0460.05 92 48-130870.044 5 30
cis-1,2-Dichloroethene mg/kg 0.0500.05 100 70-130930.047 7 30
cis-1,3-Dichloropropene mg/kg 0.0560.05 112 70-1301050.053 7 30
Dibromochloromethane mg/kg 0.0580.05 115 70-1301060.053 8 30
Dibromomethane mg/kg 0.0530.05 106 70-1301000.050 6 30
Dichlorodifluoromethane mg/kg 0.0470.05 93 49-130870.043 7 30
Diisopropyl ether mg/kg 0.0580.05 117 66-1301070.054 8 30
Ethylbenzene mg/kg 0.0540.05 108 70-130970.049 11 30
Hexachloro-1,3-butadiene mg/kg 0.0540.05 108 70-130970.049 11 30
Isopropylbenzene (Cumene)mg/kg 0.0550.05 110 70-130990.049 11 30
m&p-Xylene mg/kg 0.110.1 109 70-130960.096 12 30
Methyl-tert-butyl ether mg/kg 0.0580.05 117 70-1301090.055 6 30
Methylene Chloride mg/kg 0.0480.05 96 50-137890.045 7 30
n-Butylbenzene mg/kg 0.0520.05 103 70-130960.048 7 30
n-Propylbenzene mg/kg 0.0520.05 105 70-130960.048 9 30
Naphthalene mg/kg 0.0550.05 110 70-1311030.052 7 30
o-Xylene mg/kg 0.0540.05 109 70-130970.049 11 30
p-Isopropyltoluene mg/kg 0.0520.05 104 70-130960.048 8 30
sec-Butylbenzene mg/kg 0.0530.05 106 70-130980.049 8 30
Styrene mg/kg 0.0550.05 110 70-130990.050 10 30
tert-Butylbenzene mg/kg 0.0470.05 95 69-130870.043 8 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743733LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2743734
Tetrachloroethene mg/kg 0.0570.05 115 56-1301040.052 10 30
Toluene mg/kg 0.0500.05 101 70-130940.047 8 30
trans-1,2-Dichloroethene mg/kg 0.0540.05 108 70-130960.048 12 30
trans-1,3-Dichloropropene mg/kg 0.0550.05 110 70-1301010.051 8 30
Trichloroethene mg/kg 0.0580.05 115 70-1411050.053 9 30
Trichlorofluoromethane mg/kg 0.0540.05 108 67-130990.050 8 30
Vinyl acetate mg/kg 0.13 v10.1 133 10-1361200.12 10 30
Vinyl chloride mg/kg 0.0570.05 114 67-1301080.054 6 30
Xylene (Total)mg/kg 0.160.15 109 70-130960.14 12 30
1,2-Dichloroethane-d4 (S)%94 70-13294
4-Bromofluorobenzene (S)%99 70-13098
Toluene-d8 (S)%94 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511601
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples: 92454623006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744248
Associated Lab Samples:92454623006
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/25/19 11:280.34
1,1,1-Trichloroethane ug/L ND 1.0 11/25/19 11:280.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/25/19 11:280.22
1,1,2-Trichloroethane ug/L ND 1.0 11/25/19 11:280.24
1,1-Dichloroethane ug/L ND 1.0 11/25/19 11:280.27
1,1-Dichloroethene ug/L ND 1.0 11/25/19 11:280.24
1,1-Dichloropropene ug/L ND 1.0 11/25/19 11:280.21
1,2,3-Trichlorobenzene ug/L ND 1.0 11/25/19 11:280.34
1,2,3-Trichloropropane ug/L ND 1.0 11/25/19 11:280.35
1,2,4-Trichlorobenzene ug/L ND 1.0 11/25/19 11:280.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 11/25/19 11:280.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/25/19 11:280.26
1,2-Dichlorobenzene ug/L ND 1.0 11/25/19 11:280.29
1,2-Dichloroethane ug/L ND 1.0 11/25/19 11:280.34
1,2-Dichloropropane ug/L ND 1.0 11/25/19 11:280.19
1,3-Dichlorobenzene ug/L ND 1.0 11/25/19 11:280.22
1,3-Dichloropropane ug/L ND 1.0 11/25/19 11:280.16
1,4-Dichlorobenzene ug/L ND 1.0 11/25/19 11:280.26
2,2-Dichloropropane ug/L ND 1.0 11/25/19 11:280.27
2-Butanone (MEK)ug/L ND 5.0 11/25/19 11:283.3
2-Chlorotoluene ug/L ND 1.0 11/25/19 11:280.20
2-Hexanone ug/L ND 5.0 11/25/19 11:280.57
4-Chlorotoluene ug/L ND 1.0 11/25/19 11:280.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/25/19 11:284.5
Acetone ug/L ND 25.0 11/25/19 11:286.2
Benzene ug/L ND 1.0 11/25/19 11:280.15
Bromobenzene ug/L ND 1.0 11/25/19 11:280.22
Bromochloromethane ug/L ND 1.0 11/25/19 11:280.34
Bromodichloromethane ug/L ND 1.0 11/25/19 11:280.26
Bromoform ug/L ND 1.0 11/25/19 11:280.62
Bromomethane ug/L ND 2.0 v211/25/19 11:280.62
Carbon tetrachloride ug/L ND 1.0 11/25/19 11:280.22
Chlorobenzene ug/L ND 1.0 11/25/19 11:280.23
Chloroethane ug/L ND 1.0 11/25/19 11:280.49
Chloroform ug/L ND 5.0 11/25/19 11:282.3
Chloromethane ug/L ND 1.0 11/25/19 11:280.39
cis-1,2-Dichloroethene ug/L ND 1.0 11/25/19 11:280.29
cis-1,3-Dichloropropene ug/L ND 1.0 11/25/19 11:280.30
Dibromochloromethane ug/L ND 1.0 11/25/19 11:280.41
Dibromomethane ug/L ND 1.0 11/25/19 11:280.46
Dichlorodifluoromethane ug/L ND 1.0 11/25/19 11:280.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744248
Associated Lab Samples:92454623006
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 11/25/19 11:280.22
Ethylbenzene ug/L ND 1.0 11/25/19 11:280.26
Hexachloro-1,3-butadiene ug/L ND 1.0 11/25/19 11:280.44
m&p-Xylene ug/L ND 2.0 11/25/19 11:280.41
Methyl-tert-butyl ether ug/L ND 1.0 11/25/19 11:280.28
Methylene Chloride ug/L ND 5.0 11/25/19 11:283.7
Naphthalene ug/L ND 1.0 11/25/19 11:280.35
o-Xylene ug/L ND 1.0 11/25/19 11:280.22
p-Isopropyltoluene ug/L ND 1.0 11/25/19 11:280.21
Styrene ug/L ND 1.0 11/25/19 11:280.27
Tetrachloroethene ug/L ND 1.0 11/25/19 11:280.16
Toluene ug/L ND 1.0 11/25/19 11:280.24
trans-1,2-Dichloroethene ug/L ND 1.0 11/25/19 11:280.25
trans-1,3-Dichloropropene ug/L ND 1.0 11/25/19 11:280.31
Trichloroethene ug/L ND 1.0 11/25/19 11:280.22
Trichlorofluoromethane ug/L ND 1.0 11/25/19 11:280.31
Vinyl acetate ug/L ND 2.0 11/25/19 11:281.4
Vinyl chloride ug/L ND 1.0 11/25/19 11:280.24
Xylene (Total)ug/L ND 1.0 11/25/19 11:280.63
1,2-Dichloroethane-d4 (S)%103 70-130 11/25/19 11:28
4-Bromofluorobenzene (S)%99 70-130 11/25/19 11:28
Toluene-d8 (S)%99 70-130 11/25/19 11:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744249LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.150 102 70-130
1,1,1-Trichloroethane ug/L 46.450 93 70-130
1,1,2,2-Tetrachloroethane ug/L 50.050 100 70-130
1,1,2-Trichloroethane ug/L 47.950 96 70-130
1,1-Dichloroethane ug/L 45.650 91 70-130
1,1-Dichloroethene ug/L 45.750 91 70-130
1,1-Dichloropropene ug/L 49.250 98 70-130
1,2,3-Trichlorobenzene ug/L 47.350 95 70-130
1,2,3-Trichloropropane ug/L 52.550 105 70-130
1,2,4-Trichlorobenzene ug/L 47.050 94 70-130
1,2-Dibromo-3-chloropropane ug/L 53.250 106 70-130
1,2-Dibromoethane (EDB)ug/L 51.350 103 70-130
1,2-Dichlorobenzene ug/L 47.650 95 70-130
1,2-Dichloroethane ug/L 44.250 88 70-130
1,2-Dichloropropane ug/L 47.150 94 70-130
1,3-Dichlorobenzene ug/L 47.250 94 70-130
1,3-Dichloropropane ug/L 50.450 101 70-131
1,4-Dichlorobenzene ug/L 46.750 93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744249LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 47.650 95 69-130
2-Butanone (MEK)ug/L 103100 103 64-135
2-Chlorotoluene ug/L 48.050 96 70-130
2-Hexanone ug/L 113100 113 66-135
4-Chlorotoluene ug/L 48.450 97 70-130
4-Methyl-2-pentanone (MIBK)ug/L 105100 105 70-130
Acetone ug/L 107100 107 61-157
Benzene ug/L 47.050 94 70-130
Bromobenzene ug/L 49.450 99 70-130
Bromochloromethane ug/L 47.250 94 70-130
Bromodichloromethane ug/L 48.150 96 70-130
Bromoform ug/L 51.350 103 70-130
Bromomethane ug/L 47.1 v35094 38-130
Carbon tetrachloride ug/L 48.450 97 70-130
Chlorobenzene ug/L 47.250 94 70-130
Chloroethane ug/L 40.450 81 37-142
Chloroform ug/L 46.350 93 70-130
Chloromethane ug/L 40.350 81 48-130
cis-1,2-Dichloroethene ug/L 45.050 90 70-130
cis-1,3-Dichloropropene ug/L 51.050 102 70-130
Dibromochloromethane ug/L 50.950 102 70-130
Dibromomethane ug/L 47.650 95 70-130
Dichlorodifluoromethane ug/L 42.950 86 53-134
Diisopropyl ether ug/L 47.350 95 70-135
Ethylbenzene ug/L 47.850 96 70-130
Hexachloro-1,3-butadiene ug/L 46.650 93 68-132
m&p-Xylene ug/L 95.3100 95 70-130
Methyl-tert-butyl ether ug/L 48.150 96 70-130
Methylene Chloride ug/L 43.050 86 67-132
Naphthalene ug/L 49.850 100 70-130
o-Xylene ug/L 48.950 98 70-131
p-Isopropyltoluene ug/L 47.050 94 70-130
Styrene ug/L 49.850 100 70-130
Tetrachloroethene ug/L 49.350 99 69-130
Toluene ug/L 45.750 91 70-130
trans-1,2-Dichloroethene ug/L 45.450 91 70-130
trans-1,3-Dichloropropene ug/L 49.950 100 70-130
Trichloroethene ug/L 46.950 94 70-130
Trichlorofluoromethane ug/L 44.150 88 63-130
Vinyl acetate ug/L 97.8100 98 55-143
Vinyl chloride ug/L 48.050 96 70-131
Xylene (Total)ug/L 144150 96 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2744251MATRIX SPIKE SAMPLE:
MSSpike
Result
92454676008
1,1,1,2-Tetrachloroethane ug/L 22.720 113 73-134ND
1,1,1-Trichloroethane ug/L 24.620 123 82-143ND
1,1,2,2-Tetrachloroethane ug/L 23.720 119 70-136ND
1,1,2-Trichloroethane ug/L 23.220 116 70-135ND
1,1-Dichloroethane ug/L 24.220 121 70-139ND
1,1-Dichloroethene ug/L 25.220 123 70-1540.52J
1,1-Dichloropropene ug/L 26.220 131 70-149ND
1,2,3-Trichlorobenzene ug/L 23.520 118 70-135ND
1,2,3-Trichloropropane ug/L 23.920 119 71-137ND
1,2,4-Trichlorobenzene ug/L 22.720 114 73-140ND
1,2-Dibromo-3-chloropropane ug/L 22.920 114 65-134ND
1,2-Dibromoethane (EDB)ug/L 23.820 119 70-137ND
1,2-Dichlorobenzene ug/L 21.220 106 70-133ND
1,2-Dichloroethane ug/L 23.020 115 70-137ND
1,2-Dichloropropane ug/L 23.420 117 70-140ND
1,3-Dichlorobenzene ug/L 21.020 105 70-135ND
1,3-Dichloropropane ug/L 24.120 120 70-143ND
1,4-Dichlorobenzene ug/L 20.920 104 70-133ND
2,2-Dichloropropane ug/L 25.220 126 61-148ND
2-Butanone (MEK)ug/L 49.740 124 60-139ND
2-Chlorotoluene ug/L 21.420 107 70-144ND
2-Hexanone ug/L 56.4 M140141 65-138ND
4-Chlorotoluene ug/L 21.820 109 70-137ND
4-Methyl-2-pentanone (MIBK)ug/L 51.440 128 65-135ND
Acetone ug/L 52.440 131 60-148ND
Benzene ug/L 23.920 120 70-151ND
Bromobenzene ug/L 21.620 108 70-136ND
Bromochloromethane ug/L 24.320 121 70-141ND
Bromodichloromethane ug/L 23.520 118 70-138ND
Bromoform ug/L 22.320 111 63-130ND
Bromomethane ug/L 28.820 144 15-152ND
Carbon tetrachloride ug/L 24.920 125 70-143ND
Chlorobenzene ug/L 21.720 109 70-138ND
Chloroethane ug/L 22.720 113 52-163ND
Chloroform ug/L 24.020 120 70-139ND
Chloromethane ug/L 22.220 111 41-139ND
cis-1,2-Dichloroethene ug/L 23.820 119 70-141ND
cis-1,3-Dichloropropene ug/L 23.920 120 70-137ND
Dibromochloromethane ug/L 22.920 115 70-134ND
Dibromomethane ug/L 22.920 115 70-138ND
Dichlorodifluoromethane ug/L 23.220 116 47-155ND
Diisopropyl ether ug/L 23.820 119 63-144ND
Ethylbenzene ug/L 22.320 111 66-153ND
Hexachloro-1,3-butadiene ug/L 27.120 136 65-149ND
m&p-Xylene ug/L 44.640 111 69-152ND
Methyl-tert-butyl ether ug/L 24.020 120 54-156ND
Methylene Chloride ug/L 23.220 116 42-159ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2744251MATRIX SPIKE SAMPLE:
MSSpike
Result
92454676008
Naphthalene ug/L 22.420 112 61-148ND
o-Xylene ug/L 21.820 109 70-148ND
p-Isopropyltoluene ug/L 22.120 111 70-146ND
Styrene ug/L 22.420 112 70-135ND
Tetrachloroethene ug/L 23.120 111 59-1430.95J
Toluene ug/L 22.320 112 59-148ND
trans-1,2-Dichloroethene ug/L 24.620 123 70-146ND
trans-1,3-Dichloropropene ug/L 24.020 120 70-135ND
Trichloroethene ug/L 23.220 116 70-147ND
Trichlorofluoromethane ug/L 23.920 120 70-148ND
Vinyl acetate ug/L 50.440 126 49-151ND
Vinyl chloride ug/L 26.620 133 70-156ND
Xylene (Total)ug/L 66.460 111 63-158ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454537001
2744250SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454537001
2744250SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%109105
4-Bromofluorobenzene (S)%98100
Toluene-d8 (S)%9997
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511059
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Associated Lab Samples: 92454623006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2741816
Associated Lab Samples:92454623006
Matrix: Water
AnalyzedMDL
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/21/19 19:381.2
1,2-Dichloroethane-d4 (S)%98 50-150 11/21/19 19:38
Toluene-d8 (S)%104 50-150 11/21/19 19:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2741817LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 20.920 105 70-130
1,2-Dichloroethane-d4 (S)%98 50-150
Toluene-d8 (S)%103 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2741818MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92453977019
2741819
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane) ug/L 20 96 50-15088 8 30202.7 21.9 20.2
1,2-Dichloroethane-d4 (S) %106 50-150109 30
Toluene-d8 (S)%101 50-150102 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511556
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV Soil SIM
Associated Lab Samples: 92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743926
Associated Lab Samples:92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Matrix: Solid
AnalyzedMDL
1,4-Dioxane (p-Dioxane)mg/kg ND 0.010 11/25/19 11:150.0030
1,2-Dichloroethane-d4 (S)%103 50-150 11/25/19 11:15
Toluene-d8 (S)%99 50-150 11/25/19 11:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743927LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)mg/kg 0.0400.04 99 50-150
1,2-Dichloroethane-d4 (S)%103 50-150
Toluene-d8 (S)%103 50-150
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2744454MATRIX SPIKE SAMPLE:
MSSpike
Result
92454623002
1,4-Dioxane (p-Dioxane)mg/kg 0.0520.045 104 50-1500.0047J
1,2-Dichloroethane-d4 (S)%95 50-150
Toluene-d8 (S)%105 50-150
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454623001
2744453SAMPLE DUPLICATE:
1,4-Dioxane (p-Dioxane)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%95 3099
Toluene-d8 (S)%109 30100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511397
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples: 92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743393
Associated Lab Samples:92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 11/25/19 19:190.075
1,2-Dichlorobenzene mg/kg ND 0.33 11/25/19 19:190.071
1,3-Dichlorobenzene mg/kg ND 0.33 11/25/19 19:190.074
1,4-Dichlorobenzene mg/kg ND 0.33 11/25/19 19:190.072
1-Methylnaphthalene mg/kg ND 0.33 11/25/19 19:190.087
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 11/25/19 19:190.091
2,4,5-Trichlorophenol mg/kg ND 0.33 11/25/19 19:190.085
2,4,6-Trichlorophenol mg/kg ND 0.33 11/25/19 19:190.082
2,4-Dichlorophenol mg/kg ND 0.33 11/25/19 19:190.11
2,4-Dimethylphenol mg/kg ND 0.33 11/25/19 19:190.082
2,4-Dinitrophenol mg/kg ND 1.6 11/25/19 19:191.0
2,4-Dinitrotoluene mg/kg ND 0.33 11/25/19 19:190.087
2,6-Dinitrotoluene mg/kg ND 0.33 11/25/19 19:190.086
2-Chloronaphthalene mg/kg ND 0.33 11/25/19 19:190.073
2-Chlorophenol mg/kg ND 0.33 11/25/19 19:190.076
2-Methylnaphthalene mg/kg ND 0.33 11/25/19 19:190.083
2-Methylphenol(o-Cresol)mg/kg ND 0.33 11/25/19 19:190.073
2-Nitroaniline mg/kg ND 1.6 11/25/19 19:190.16
2-Nitrophenol mg/kg ND 0.33 11/25/19 19:190.10
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 11/25/19 19:190.082
3,3'-Dichlorobenzidine mg/kg ND 1.6 11/25/19 19:190.23
3-Nitroaniline mg/kg ND 1.6 11/25/19 19:190.17
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 11/25/19 19:190.53
4-Bromophenylphenyl ether mg/kg ND 0.33 11/25/19 19:190.086
4-Chloro-3-methylphenol mg/kg ND 0.66 11/25/19 19:190.20
4-Chloroaniline mg/kg ND 1.6 11/25/19 19:190.20
4-Chlorophenylphenyl ether mg/kg ND 0.33 11/25/19 19:190.085
4-Nitroaniline mg/kg ND 0.66 11/25/19 19:190.16
4-Nitrophenol mg/kg ND 1.6 11/25/19 19:190.52
Acenaphthene mg/kg ND 0.33 11/25/19 19:190.084
Acenaphthylene mg/kg ND 0.33 11/25/19 19:190.078
Aniline mg/kg ND 0.33 11/25/19 19:190.074
Anthracene mg/kg ND 0.33 11/25/19 19:190.085
Benzo(a)anthracene mg/kg ND 0.33 11/25/19 19:190.10
Benzo(a)pyrene mg/kg ND 0.33 11/25/19 19:190.14
Benzo(b)fluoranthene mg/kg ND 0.33 11/25/19 19:190.13
Benzo(g,h,i)perylene mg/kg ND 0.33 11/25/19 19:190.13
Benzo(k)fluoranthene mg/kg ND 0.33 11/25/19 19:190.14
Benzoic Acid mg/kg ND 1.6 11/25/19 19:190.35
Benzyl alcohol mg/kg ND 0.66 11/25/19 19:190.17
bis(2-Chloroethoxy)methane mg/kg ND 0.33 11/25/19 19:190.088
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743393
Associated Lab Samples:92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether mg/kg ND 0.33 11/25/19 19:190.070
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 11/25/19 19:190.11
Butylbenzylphthalate mg/kg ND 0.33 11/25/19 19:190.087
Chrysene mg/kg ND 0.33 11/25/19 19:190.095
Di-n-butylphthalate mg/kg ND 0.33 11/25/19 19:190.081
Di-n-octylphthalate mg/kg ND 0.33 11/25/19 19:190.19
Dibenz(a,h)anthracene mg/kg ND 0.33 11/25/19 19:190.13
Dibenzofuran mg/kg ND 0.33 11/25/19 19:190.082
Diethylphthalate mg/kg ND 0.33 11/25/19 19:190.071
Dimethylphthalate mg/kg ND 0.33 11/25/19 19:190.074
Fluoranthene mg/kg ND 0.33 11/25/19 19:190.099
Fluorene mg/kg ND 0.33 11/25/19 19:190.088
Hexachloro-1,3-butadiene mg/kg ND 0.33 11/25/19 19:190.080
Hexachlorobenzene mg/kg ND 0.33 11/25/19 19:190.083
Hexachlorocyclopentadiene mg/kg ND 0.33 11/25/19 19:190.13
Hexachloroethane mg/kg ND 0.33 11/25/19 19:190.075
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 11/25/19 19:190.15
Isophorone mg/kg ND 0.33 11/25/19 19:190.071
N-Nitroso-di-n-propylamine mg/kg ND 0.33 11/25/19 19:190.092
N-Nitrosodimethylamine mg/kg ND 0.33 11/25/19 19:190.092
N-Nitrosodiphenylamine mg/kg ND 0.33 11/25/19 19:190.084
Naphthalene mg/kg ND 0.33 11/25/19 19:190.078
Nitrobenzene mg/kg ND 0.33 11/25/19 19:190.078
Pentachlorophenol mg/kg ND 1.6 11/25/19 19:190.15
Phenanthrene mg/kg ND 0.33 11/25/19 19:190.083
Phenol mg/kg ND 0.33 11/25/19 19:190.078
Pyrene mg/kg ND 0.33 11/25/19 19:190.090
Pyridine mg/kg ND 0.33 11/25/19 19:190.083
2,4,6-Tribromophenol (S)%85 27-110 11/25/19 19:19
2-Fluorobiphenyl (S)%72 30-110 11/25/19 19:19
2-Fluorophenol (S)%67 13-110 11/25/19 19:19
Nitrobenzene-d5 (S)%66 23-110 11/25/19 19:19
Phenol-d6 (S)%67 22-110 11/25/19 19:19
Terphenyl-d14 (S)%77 28-110 11/25/19 19:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743394LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.21.6 75 52-130
1,2-Dichlorobenzene mg/kg 1.21.6 75 51-130
1,3-Dichlorobenzene mg/kg 1.21.6 76 50-130
1,4-Dichlorobenzene mg/kg 1.21.6 74 49-130
1-Methylnaphthalene mg/kg 1.21.6 74 55-130
2,2'-Oxybis(1-chloropropane)mg/kg 1.11.6 68 30-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743394LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol mg/kg 1.31.6 77 55-130
2,4,6-Trichlorophenol mg/kg 1.31.6 80 57-130
2,4-Dichlorophenol mg/kg 1.21.6 75 56-130
2,4-Dimethylphenol mg/kg 1.21.6 73 51-130
2,4-Dinitrophenol mg/kg 5.08.2 61 27-133
2,4-Dinitrotoluene mg/kg 1.31.6 79 61-130
2,6-Dinitrotoluene mg/kg 1.31.6 79 60-130
2-Chloronaphthalene mg/kg 1.31.6 79 52-130
2-Chlorophenol mg/kg 1.21.6 75 54-130
2-Methylnaphthalene mg/kg 1.21.6 75 54-130
2-Methylphenol(o-Cresol)mg/kg 1.21.6 72 51-130
2-Nitroaniline mg/kg 2.53.3 77 51-130
2-Nitrophenol mg/kg 1.21.6 74 49-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.11.6 70 11-163
3,3'-Dichlorobenzidine mg/kg 2.23.3 66 10-132
3-Nitroaniline mg/kg 2.23.3 67 55-130
4,6-Dinitro-2-methylphenol mg/kg 2.53.3 75 47-142
4-Bromophenylphenyl ether mg/kg 1.31.6 80 59-130
4-Chloro-3-methylphenol mg/kg 2.43.3 74 55-130
4-Chloroaniline mg/kg 2.43.3 72 54-130
4-Chlorophenylphenyl ether mg/kg 1.31.6 77 58-130
4-Nitroaniline mg/kg 2.33.3 70 54-130
4-Nitrophenol mg/kg 5.88.2 71 48-130
Acenaphthene mg/kg 1.31.6 80 60-130
Acenaphthylene mg/kg 1.41.6 87 60-130
Aniline mg/kg 1.11.6 69 43-130
Anthracene mg/kg 1.41.6 86 63-130
Benzo(a)anthracene mg/kg 1.31.6 81 59-130
Benzo(a)pyrene mg/kg 1.41.6 85 57-130
Benzo(b)fluoranthene mg/kg 1.41.6 84 54-130
Benzo(g,h,i)perylene mg/kg 1.41.6 86 59-130
Benzo(k)fluoranthene mg/kg 1.41.6 84 54-130
Benzoic Acid mg/kg 4.88.2 59 19-130
Benzyl alcohol mg/kg 2.43.3 74 50-130
bis(2-Chloroethoxy)methane mg/kg 1.21.6 72 54-130
bis(2-Chloroethyl) ether mg/kg 1.31.6 77 48-130
bis(2-Ethylhexyl)phthalate mg/kg 1.31.6 77 45-134
Butylbenzylphthalate mg/kg 1.21.6 75 46-138
Chrysene mg/kg 1.21.6 76 58-130
Di-n-butylphthalate mg/kg 1.21.6 75 60-130
Di-n-octylphthalate mg/kg 1.31.6 80 53-130
Dibenz(a,h)anthracene mg/kg 1.31.6 82 59-130
Dibenzofuran mg/kg 1.31.6 78 60-130
Diethylphthalate mg/kg 1.21.6 75 60-130
Dimethylphthalate mg/kg 1.31.6 77 60-130
Fluoranthene mg/kg 1.41.6 83 65-130
Fluorene mg/kg 1.31.6 81 63-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743394LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene mg/kg 1.21.6 74 46-130
Hexachlorobenzene mg/kg 1.31.6 80 58-130
Hexachlorocyclopentadiene mg/kg 1.11.6 66 23-130
Hexachloroethane mg/kg 1.21.6 75 47-130
Indeno(1,2,3-cd)pyrene mg/kg 1.41.6 83 60-130
Isophorone mg/kg 1.11.6 70 49-130
N-Nitroso-di-n-propylamine mg/kg 1.21.6 70 47-130
N-Nitrosodimethylamine mg/kg 1.21.6 73 45-130
N-Nitrosodiphenylamine mg/kg 1.21.6 75 59-130
Naphthalene mg/kg 1.31.6 77 55-130
Nitrobenzene mg/kg 1.21.6 71 49-130
Pentachlorophenol mg/kg 2.73.3 83 10-132
Phenanthrene mg/kg 1.41.6 83 62-130
Phenol mg/kg 1.31.6 81 46-130
Pyrene mg/kg 1.41.6 83 53-130
Pyridine mg/kg 0.911.6 56 37-130
2,4,6-Tribromophenol (S)%96 27-110
2-Fluorobiphenyl (S)%80 30-110
2-Fluorophenol (S)%81 13-110
Nitrobenzene-d5 (S)%74 23-110
Phenol-d6 (S)%79 22-110
Terphenyl-d14 (S)%80 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2743395MATRIX SPIKE SAMPLE:
MSSpike
Result
92454623002
1,2,4-Trichlorobenzene mg/kg 1.12 53 18-130ND
1,2-Dichlorobenzene mg/kg 1.12 54 14-130ND
1,3-Dichlorobenzene mg/kg 1.12 52 12-130ND
1,4-Dichlorobenzene mg/kg 1.12 53 10-130ND
1-Methylnaphthalene mg/kg 1.12 55 12-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.22 60 10-130ND
2,4,5-Trichlorophenol mg/kg 1.02 51 13-130ND
2,4,6-Trichlorophenol mg/kg 1.12 57 17-130ND
2,4-Dichlorophenol mg/kg 1.12 53 10-130ND
2,4-Dimethylphenol mg/kg 0.982 49 10-130ND
2,4-Dinitrophenol mg/kg 2.510.1 25 10-130ND
2,4-Dinitrotoluene mg/kg 1.22 60 24-130ND
2,6-Dinitrotoluene mg/kg 1.22 62 23-130ND
2-Chloronaphthalene mg/kg 1.12 56 19-130ND
2-Chlorophenol mg/kg 1.12 53 10-130ND
2-Methylnaphthalene mg/kg 1.12 56 18-130ND
2-Methylphenol(o-Cresol)mg/kg 1.02 51 10-130ND
2-Nitroaniline mg/kg 2.8 v14.1 70 17-130ND
2-Nitrophenol mg/kg 1.02 51 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2743395MATRIX SPIKE SAMPLE:
MSSpike
Result
92454623002
3&4-Methylphenol(m&p Cresol)mg/kg 1.12 53 10-130ND
3,3'-Dichlorobenzidine mg/kg 1.7J4.1 41 10-130ND
3-Nitroaniline mg/kg 2.34.1 57 24-130ND
4,6-Dinitro-2-methylphenol mg/kg 1.34.1 33 10-152ND
4-Bromophenylphenyl ether mg/kg 1.12 56 29-130ND
4-Chloro-3-methylphenol mg/kg 2.44.1 60 17-130ND
4-Chloroaniline mg/kg 2.24.1 55 14-130ND
4-Chlorophenylphenyl ether mg/kg 1.22 60 25-130ND
4-Nitroaniline mg/kg 2.34.1 58 22-130ND
4-Nitrophenol mg/kg 5.410.1 53 10-130ND
Acenaphthene mg/kg 1.22 62 20-130ND
Acenaphthylene mg/kg 1.32 65 25-130ND
Aniline mg/kg 0.412 20 10-130ND
Anthracene mg/kg 1.32 65 29-130ND
Benzo(a)anthracene mg/kg 1.22 62 19-130ND
Benzo(a)pyrene mg/kg 1.22 61 12-130ND
Benzo(b)fluoranthene mg/kg 1.22 59 14-130ND
Benzo(g,h,i)perylene mg/kg 1.32 64 10-130ND
Benzo(k)fluoranthene mg/kg 1.22 58 14-130ND
Benzoic Acid mg/kg 4.610.1 45 10-130ND
Benzyl alcohol mg/kg 2.34.1 57 13-130ND
bis(2-Chloroethoxy)methane mg/kg 1.12 52 16-130ND
bis(2-Chloroethyl) ether mg/kg 1.12 55 11-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.52 72 21-130ND
Butylbenzylphthalate mg/kg 1.42 70 23-130ND
Chrysene mg/kg 1.12 56 22-130ND
Di-n-butylphthalate mg/kg 1.32 64 30-130ND
Di-n-octylphthalate mg/kg 1.42 70 23-142ND
Dibenz(a,h)anthracene mg/kg 1.32 64 10-130ND
Dibenzofuran mg/kg 1.22 58 24-130ND
Diethylphthalate mg/kg 1.22 60 26-130ND
Dimethylphthalate mg/kg 1.22 58 22-130ND
Fluoranthene mg/kg 1.22 60 33-130ND
Fluorene mg/kg 1.32 64 22-130ND
Hexachloro-1,3-butadiene mg/kg 1.02 50 13-130ND
Hexachlorobenzene mg/kg 1.12 55 29-130ND
Hexachlorocyclopentadiene mg/kg 0.18J M1,v229 10-130ND
Hexachloroethane mg/kg 1.02 49 10-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.32 64 10-130ND
Isophorone mg/kg 1.22 57 13-130ND
N-Nitroso-di-n-propylamine mg/kg 1.22 61 12-130ND
N-Nitrosodimethylamine mg/kg 1.12 52 11-130ND
N-Nitrosodiphenylamine mg/kg 1.22 59 15-130ND
Naphthalene mg/kg 1.22 58 15-130ND
Nitrobenzene mg/kg 1.22 57 12-130ND
Pentachlorophenol mg/kg 1.8J4.1 45 10-130ND
Phenanthrene mg/kg 1.22 62 27-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2743395MATRIX SPIKE SAMPLE:
MSSpike
Result
92454623002
Phenol mg/kg 1.12 53 10-130ND
Pyrene mg/kg 1.42 67 19-130ND
Pyridine mg/kg 0.40J2 20 10-130ND
2,4,6-Tribromophenol (S)%60 27-110
2-Fluorobiphenyl (S)%60 30-110
2-Fluorophenol (S)%57 13-110
Nitrobenzene-d5 (S)%60 23-110
Phenol-d6 (S)%57 22-110
Terphenyl-d14 (S)%69 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454623004
2743396SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg ND 30ND
2,2'-Oxybis(1-chloropropane)mg/kg ND 30ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
2-Chlorophenol mg/kg ND 30ND
2-Methylnaphthalene mg/kg ND 30ND
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Nitroaniline mg/kg ND v130ND
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND 30ND
3-Nitroaniline mg/kg ND 30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND 30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
Aniline mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454623004
2743396SAMPLE DUPLICATE:
Anthracene mg/kg ND 30ND
Benzo(a)anthracene mg/kg ND 30ND
Benzo(a)pyrene mg/kg ND 30ND
Benzo(b)fluoranthene mg/kg ND 30ND
Benzo(g,h,i)perylene mg/kg ND 30ND
Benzo(k)fluoranthene mg/kg ND 30ND
Benzoic Acid mg/kg ND 30ND
Benzyl alcohol mg/kg ND 30ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg ND 30ND
Butylbenzylphthalate mg/kg ND 30ND
Chrysene mg/kg ND 30ND
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg ND 30ND
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzofuran mg/kg ND 30ND
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg ND 30ND
Fluorene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND v230ND
Hexachloroethane mg/kg ND 30ND
Indeno(1,2,3-cd)pyrene mg/kg ND 30ND
Isophorone mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND 30ND
N-Nitrosodimethylamine mg/kg ND 30ND
N-Nitrosodiphenylamine mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg ND 30ND
Phenanthrene mg/kg ND 30ND
Phenol mg/kg ND 30ND
Pyrene mg/kg ND 30ND
Pyridine mg/kg ND 30ND
2,4,6-Tribromophenol (S)%4755
2-Fluorobiphenyl (S)%5967
2-Fluorophenol (S)%5058
Nitrobenzene-d5 (S)%6069
Phenol-d6 (S)%5565
Terphenyl-d14 (S)%6977
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
510962
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92454623001, 92454623002, 92454623003, 92454623004, 92454623005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454610001
2741107SAMPLE DUPLICATE:
Percent Moisture %22.2 2 2522.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454598005
2741124SAMPLE DUPLICATE:
Percent Moisture %17.9 1 2518.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1408861
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples: 92454623003, 92454623005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3490112-1
Associated Lab Samples:92454623003, 92454623005
Matrix: Solid
AnalyzedMDL
Total Solids %ND 01/10/20 14:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3490112-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1177618-01
R3490112-3SAMPLE DUPLICATE:
Total Solids %81.3 0.832 1082.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 63
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454623
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1408881
3060A
EPA 7199
Wet Chemistry 7199
Associated Lab Samples: 92454623003, 92454623005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3490056-1
Associated Lab Samples:92454623003, 92454623005
Matrix: Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 01/11/20 12:500.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3490056-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.210.0 102 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3490056-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1177018-01
R3490056-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 29.6 98.4 75.0-12595.8 2.56 2029.60.726 29.8 29.1
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3490056-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1177018-01
Chromium, Hexavalent mg/kg 745 ML157047.5 75.0-1250.726
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1176980-01
R3490056-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454623005
R3490056-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.850J J2.29 200.870
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 63
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92454623
ROW-603
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.BC
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Sample was received or analysis requested beyond the recognized method holding time.H3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 63
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92454623
ROW-603
ANALYTE QUALIFIERS
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 63
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92454623
ROW-603
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92454623001 511039 511120SB-1 (15-16.5)EPA 3050B EPA 6010D
92454623002 511039 511120SB-2 (15-17)EPA 3050B EPA 6010D
92454623003 511039 511120SB-2 (22-24)EPA 3050B EPA 6010D
92454623004 511039 511120SB-3 (15-17)EPA 3050B EPA 6010D
92454623005 511039 511120SB-3 (17-19)EPA 3050B EPA 6010D
92454623001 510897 511054SB-1 (15-16.5)EPA 7471B EPA 7471B
92454623002 510897 511054SB-2 (15-17)EPA 7471B EPA 7471B
92454623003 510897 511054SB-2 (22-24)EPA 7471B EPA 7471B
92454623004 510897 511054SB-3 (15-17)EPA 7471B EPA 7471B
92454623005 510897 511054SB-3 (17-19)EPA 7471B EPA 7471B
92454623001 511397 511592SB-1 (15-16.5)EPA 3546 EPA 8270E
92454623002 511397 511592SB-2 (15-17)EPA 3546 EPA 8270E
92454623003 511397 511592SB-2 (22-24)EPA 3546 EPA 8270E
92454623004 511397 511592SB-3 (15-17)EPA 3546 EPA 8270E
92454623005 511397 511592SB-3 (17-19)EPA 3546 EPA 8270E
92454623001 511468 511475SB-1 (15-16.5)EPA 5035A EPA 8260D
92454623002 511468 511475SB-2 (15-17)EPA 5035A EPA 8260D
92454623003 511468 511475SB-2 (22-24)EPA 5035A EPA 8260D
92454623004 511519 511533SB-3 (15-17)EPA 5035A EPA 8260D
92454623005 511519 511533SB-3 (17-19)EPA 5035A EPA 8260D
92454623006 511601Trip Blank EPA 8260D
92454623006 511059Trip Blank EPA 8260D Mod.
92454623001 511556 511649SB-1 (15-16.5)EPA 8260D Mod.EPA 8260D Mod.
92454623002 511556 511649SB-2 (15-17)EPA 8260D Mod.EPA 8260D Mod.
92454623003 511556 511649SB-2 (22-24)EPA 8260D Mod.EPA 8260D Mod.
92454623004 511556 511649SB-3 (15-17)EPA 8260D Mod.EPA 8260D Mod.
92454623005 511556 511649SB-3 (17-19)EPA 8260D Mod.EPA 8260D Mod.
92454623001 510962SB-1 (15-16.5)ASTM D2974-87
92454623002 510962SB-2 (15-17)ASTM D2974-87
92454623003 510962SB-2 (22-24)ASTM D2974-87
92454623004 510962SB-3 (15-17)ASTM D2974-87
92454623005 510962SB-3 (17-19)ASTM D2974-87
92454623003 1408861 1408861SB-2 (22-24)SM 2540 G SM 2540G
92454623005 1408861 1408861SB-3 (17-19)SM 2540 G SM 2540G
92454623003 1408881 1408881SB-2 (22-24)3060A EPA 7199
92454623005 1408881 1408881SB-3 (17-19)3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/14/2020 02:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 63
Page 61 of 63
Page 62 of 63
Page 63 of 63
#=CL#
December 04, 2019
LIMS USE: FR - DAVID GRAHAM
LIMS OBJECT ID: 92454745
92454745
Project:
Pace Project No.:
RE:
David Graham
Hart & Hickman
2923 S. Tryon Street
Charlotte, NC 28203
ROW-603
Dear David Graham:
Enclosed are the analytical results for sample(s) received by the laboratory on November 21, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell for
[e-mail]
Project Manager
Kevin Godwin
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92454745
ROW-603
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 55
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92454745
ROW-603
Lab ID Sample ID Matrix Date Collected Date Received
92454745001 SB-4 (15-17)Solid 11/20/19 13:30 11/21/19 10:37
92454745002 SB-4 (19-21)Solid 11/20/19 13:50 11/21/19 10:37
92454745003 SB-5 (15-17)Solid 11/20/19 14:15 11/21/19 10:37
92454745004 SB-5 (19-21)Solid 11/20/19 14:50 11/21/19 10:37
92454745005 DUP-1-SOIL Solid 11/20/19 00:00 11/21/19 10:37
92454745006 TRIP BLANK Water 11/20/19 00:00 11/21/19 10:37
92454745007 IDW SOIL Solid 11/21/19 10:15 11/21/19 10:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92454745
ROW-603
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92454745001 SB-4 (15-17)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
92454745002 SB-4 (19-21)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
92454745003 SB-5 (15-17)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
92454745004 SB-5 (19-21)EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
92454745005 DUP-1-SOIL EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
92454745006 TRIP BLANK EPA 8260D 63 PASI-CGAW
EPA 8260D Mod.3 PASI-CLMB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-4 (15-17)Lab ID: 92454745001 Collected: 11/20/19 13:30 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic ND mg/kg 11/26/19 19:14 7440-38-211/25/19 12:161.1 0.53 1
Barium 366 mg/kg 11/26/19 19:14 7440-39-3 M111/25/19 12:160.53 0.26 1
Cadmium 0.073J mg/kg 11/26/19 19:14 7440-43-911/25/19 12:160.11 0.053 1
Chromium 14.5 mg/kg 11/26/19 19:14 7440-47-311/25/19 12:160.53 0.26 1
Lead 1.3 mg/kg 11/26/19 19:14 7439-92-111/25/19 12:160.53 0.26 1
Selenium ND mg/kg 11/26/19 19:14 7782-49-211/25/19 12:161.1 0.53 1
Silver ND mg/kg 11/26/19 19:14 7440-22-411/25/19 12:160.53 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury ND mg/kg 11/22/19 15:24 7439-97-611/22/19 11:500.0034 0.0017 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/27/19 10:26 83-32-911/26/19 10:110.39 0.099 1
Acenaphthylene ND mg/kg 11/27/19 10:26 208-96-811/26/19 10:110.39 0.091 1
Aniline ND mg/kg 11/27/19 10:26 62-53-311/26/19 10:110.39 0.087 1
Anthracene ND mg/kg 11/27/19 10:26 120-12-711/26/19 10:110.39 0.10 1
Benzo(a)anthracene ND mg/kg 11/27/19 10:26 56-55-311/26/19 10:110.39 0.12 1
Benzo(a)pyrene ND mg/kg 11/27/19 10:26 50-32-811/26/19 10:110.39 0.17 1
Benzo(b)fluoranthene ND mg/kg 11/27/19 10:26 205-99-211/26/19 10:110.39 0.16 1
Benzo(g,h,i)perylene ND mg/kg 11/27/19 10:26 191-24-211/26/19 10:110.39 0.15 1
Benzo(k)fluoranthene ND mg/kg 11/27/19 10:26 207-08-911/26/19 10:110.39 0.16 1
Benzoic Acid ND mg/kg 11/27/19 10:26 65-85-011/26/19 10:111.9 0.42 1
Benzyl alcohol ND mg/kg 11/27/19 10:26 100-51-611/26/19 10:110.77 0.20 1
4-Bromophenylphenyl ether ND mg/kg 11/27/19 10:26 101-55-311/26/19 10:110.39 0.10 1
Butylbenzylphthalate ND mg/kg 11/27/19 10:26 85-68-711/26/19 10:110.39 0.10 1
4-Chloro-3-methylphenol ND mg/kg 11/27/19 10:26 59-50-711/26/19 10:110.77 0.23 1
4-Chloroaniline ND mg/kg 11/27/19 10:26 106-47-811/26/19 10:111.9 0.24 1
bis(2-Chloroethoxy)methane ND mg/kg 11/27/19 10:26 111-91-111/26/19 10:110.39 0.10 1
bis(2-Chloroethyl) ether ND mg/kg 11/27/19 10:26 111-44-411/26/19 10:110.39 0.082 1
2-Chloronaphthalene ND mg/kg 11/27/19 10:26 91-58-711/26/19 10:110.39 0.086 1
2-Chlorophenol ND mg/kg 11/27/19 10:26 95-57-811/26/19 10:110.39 0.090 1
4-Chlorophenylphenyl ether ND mg/kg 11/27/19 10:26 7005-72-311/26/19 10:110.39 0.10 1
Chrysene ND mg/kg 11/27/19 10:26 218-01-911/26/19 10:110.39 0.11 1
Dibenz(a,h)anthracene ND mg/kg 11/27/19 10:26 53-70-311/26/19 10:110.39 0.15 1
Dibenzofuran ND mg/kg 11/27/19 10:26 132-64-911/26/19 10:110.39 0.096 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 10:26 95-50-111/26/19 10:110.39 0.083 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 10:26 541-73-111/26/19 10:110.39 0.087 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 10:26 106-46-711/26/19 10:110.39 0.085 1
3,3'-Dichlorobenzidine ND mg/kg 11/27/19 10:26 91-94-111/26/19 10:111.9 0.27 1
2,4-Dichlorophenol ND mg/kg 11/27/19 10:26 120-83-211/26/19 10:110.39 0.13 1
Diethylphthalate ND mg/kg 11/27/19 10:26 84-66-211/26/19 10:110.39 0.084 1
2,4-Dimethylphenol ND mg/kg 11/27/19 10:26 105-67-911/26/19 10:110.39 0.096 1
Dimethylphthalate ND mg/kg 11/27/19 10:26 131-11-311/26/19 10:110.39 0.087 1
Di-n-butylphthalate ND mg/kg 11/27/19 10:26 84-74-211/26/19 10:110.39 0.095 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/27/19 10:26 534-52-111/26/19 10:110.77 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-4 (15-17)Lab ID: 92454745001 Collected: 11/20/19 13:30 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/27/19 10:26 51-28-511/26/19 10:111.9 1.2 1
2,4-Dinitrotoluene ND mg/kg 11/27/19 10:26 121-14-211/26/19 10:110.39 0.10 1
2,6-Dinitrotoluene ND mg/kg 11/27/19 10:26 606-20-211/26/19 10:110.39 0.10 1
Di-n-octylphthalate ND mg/kg 11/27/19 10:26 117-84-011/26/19 10:110.39 0.22 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/27/19 10:26 117-81-711/26/19 10:110.39 0.13 1
Fluoranthene ND mg/kg 11/27/19 10:26 206-44-011/26/19 10:110.39 0.12 1
Fluorene ND mg/kg 11/27/19 10:26 86-73-711/26/19 10:110.39 0.10 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 10:26 87-68-311/26/19 10:110.39 0.094 1
Hexachlorobenzene ND mg/kg 11/27/19 10:26 118-74-111/26/19 10:110.39 0.098 1
Hexachlorocyclopentadiene ND mg/kg 11/27/19 10:26 77-47-411/26/19 10:110.39 0.15 1
Hexachloroethane ND mg/kg 11/27/19 10:26 67-72-111/26/19 10:110.39 0.088 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/27/19 10:26 193-39-511/26/19 10:110.39 0.18 1
Isophorone ND mg/kg 11/27/19 10:26 78-59-111/26/19 10:110.39 0.084 1
1-Methylnaphthalene ND mg/kg 11/27/19 10:26 90-12-011/26/19 10:110.39 0.10 1
2-Methylnaphthalene ND mg/kg 11/27/19 10:26 91-57-611/26/19 10:110.39 0.098 1
2-Methylphenol(o-Cresol)ND mg/kg 11/27/19 10:26 95-48-711/26/19 10:110.39 0.085 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/27/19 10:26 15831-10-411/26/19 10:110.39 0.097 1
Naphthalene ND mg/kg 11/27/19 10:26 91-20-311/26/19 10:110.39 0.092 1
2-Nitroaniline ND mg/kg 11/27/19 10:26 88-74-411/26/19 10:111.9 0.19 1
3-Nitroaniline ND mg/kg 11/27/19 10:26 99-09-211/26/19 10:111.9 0.20 1
4-Nitroaniline ND mg/kg 11/27/19 10:26 100-01-611/26/19 10:110.77 0.19 1
Nitrobenzene ND mg/kg 11/27/19 10:26 98-95-311/26/19 10:110.39 0.092 1
2-Nitrophenol ND mg/kg 11/27/19 10:26 88-75-511/26/19 10:110.39 0.12 1
4-Nitrophenol ND mg/kg 11/27/19 10:26 100-02-711/26/19 10:111.9 0.61 1
N-Nitrosodimethylamine ND mg/kg 11/27/19 10:26 62-75-911/26/19 10:110.39 0.11 1
N-Nitroso-di-n-propylamine ND mg/kg 11/27/19 10:26 621-64-711/26/19 10:110.39 0.11 1
N-Nitrosodiphenylamine ND mg/kg 11/27/19 10:26 86-30-611/26/19 10:110.39 0.098 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/27/19 10:26 108-60-111/26/19 10:110.39 0.11 1
Pentachlorophenol ND mg/kg 11/27/19 10:26 87-86-511/26/19 10:111.9 0.18 1
Phenanthrene ND mg/kg 11/27/19 10:26 85-01-811/26/19 10:110.39 0.097 1
Phenol ND mg/kg 11/27/19 10:26 108-95-211/26/19 10:110.39 0.092 1
Pyrene ND mg/kg 11/27/19 10:26 129-00-011/26/19 10:110.39 0.11 1
Pyridine ND mg/kg 11/27/19 10:26 110-86-111/26/19 10:110.39 0.098 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 10:26 120-82-111/26/19 10:110.39 0.088 1
2,4,5-Trichlorophenol ND mg/kg 11/27/19 10:26 95-95-411/26/19 10:110.39 0.10 1
2,4,6-Trichlorophenol ND mg/kg 11/27/19 10:26 88-06-211/26/19 10:110.39 0.097 1
Surrogates
Nitrobenzene-d5 (S)62 %11/27/19 10:26 4165-60-011/26/19 10:1123-110 1
2-Fluorobiphenyl (S)61 %11/27/19 10:26 321-60-811/26/19 10:1130-110 1
Terphenyl-d14 (S)64 %11/27/19 10:26 1718-51-011/26/19 10:1128-110 1
Phenol-d6 (S)58 %11/27/19 10:26 13127-88-311/26/19 10:1122-110 1
2-Fluorophenol (S)59 %11/27/19 10:26 367-12-411/26/19 10:1113-110 1
2,4,6-Tribromophenol (S)67 %11/27/19 10:26 118-79-611/26/19 10:1127-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-4 (15-17)Lab ID: 92454745001 Collected: 11/20/19 13:30 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 11/27/19 15:18 67-64-111/27/19 12:210.091 0.0086 1
Benzene ND mg/kg 11/27/19 15:18 71-43-211/27/19 12:210.0046 0.00082 1
Bromobenzene ND mg/kg 11/27/19 15:18 108-86-111/27/19 12:210.0046 0.0012 1
Bromochloromethane ND mg/kg 11/27/19 15:18 74-97-511/27/19 12:210.0046 0.0011 1
Bromodichloromethane ND mg/kg 11/27/19 15:18 75-27-411/27/19 12:210.0046 0.00089 1
Bromoform ND mg/kg 11/27/19 15:18 75-25-211/27/19 12:210.0046 0.0022 1
Bromomethane ND mg/kg 11/27/19 15:18 74-83-9 IH11/27/19 12:210.0091 0.0022 1
2-Butanone (MEK)ND mg/kg 11/27/19 15:18 78-93-311/27/19 12:210.091 0.011 1
n-Butylbenzene ND mg/kg 11/27/19 15:18 104-51-811/27/19 12:210.0046 0.0026 1
sec-Butylbenzene ND mg/kg 11/27/19 15:18 135-98-811/27/19 12:210.0046 0.0019 1
tert-Butylbenzene ND mg/kg 11/27/19 15:18 98-06-6 v211/27/19 12:210.0046 0.0015 1
Carbon tetrachloride ND mg/kg 11/27/19 15:18 56-23-511/27/19 12:210.0046 0.00087 1
Chlorobenzene ND mg/kg 11/27/19 15:18 108-90-711/27/19 12:210.0046 0.00088 1
Chloroethane ND mg/kg 11/27/19 15:18 75-00-3 IK11/27/19 12:210.0091 0.0019 1
Chloroform ND mg/kg 11/27/19 15:18 67-66-311/27/19 12:210.0046 0.00097 1
Chloromethane ND mg/kg 11/27/19 15:18 74-87-311/27/19 12:210.0091 0.0030 1
2-Chlorotoluene ND mg/kg 11/27/19 15:18 95-49-811/27/19 12:210.0046 0.0014 1
4-Chlorotoluene ND mg/kg 11/27/19 15:18 106-43-411/27/19 12:210.0046 0.0014 1
1,2-Dibromo-3-chloropropane ND mg/kg 11/27/19 15:18 96-12-811/27/19 12:210.0046 0.0023 1
Dibromochloromethane ND mg/kg 11/27/19 15:18 124-48-111/27/19 12:210.0046 0.0023 1
1,2-Dibromoethane (EDB)ND mg/kg 11/27/19 15:18 106-93-411/27/19 12:210.0046 0.0010 1
Dibromomethane ND mg/kg 11/27/19 15:18 74-95-311/27/19 12:210.0046 0.0014 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 15:18 95-50-111/27/19 12:210.0046 0.0016 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 15:18 541-73-111/27/19 12:210.0046 0.0016 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 15:18 106-46-711/27/19 12:210.0046 0.0016 1
Dichlorodifluoromethane ND mg/kg 11/27/19 15:18 75-71-811/27/19 12:210.0091 0.0038 1
1,1-Dichloroethane ND mg/kg 11/27/19 15:18 75-34-311/27/19 12:210.0046 0.00067 1
1,2-Dichloroethane ND mg/kg 11/27/19 15:18 107-06-211/27/19 12:210.0046 0.00091 1
1,1-Dichloroethene ND mg/kg 11/27/19 15:18 75-35-411/27/19 12:210.0046 0.0011 1
cis-1,2-Dichloroethene ND mg/kg 11/27/19 15:18 156-59-211/27/19 12:210.0046 0.00079 1
trans-1,2-Dichloroethene ND mg/kg 11/27/19 15:18 156-60-511/27/19 12:210.0046 0.00090 1
1,2-Dichloropropane ND mg/kg 11/27/19 15:18 78-87-511/27/19 12:210.0046 0.0017 1
1,3-Dichloropropane ND mg/kg 11/27/19 15:18 142-28-911/27/19 12:210.0046 0.0017 1
2,2-Dichloropropane ND mg/kg 11/27/19 15:18 594-20-711/27/19 12:210.0046 0.00045 1
1,1-Dichloropropene ND mg/kg 11/27/19 15:18 563-58-611/27/19 12:210.0046 0.0019 1
cis-1,3-Dichloropropene ND mg/kg 11/27/19 15:18 10061-01-511/27/19 12:210.0046 0.0021 1
trans-1,3-Dichloropropene ND mg/kg 11/27/19 15:18 10061-02-611/27/19 12:210.0046 0.00080 1
Diisopropyl ether ND mg/kg 11/27/19 15:18 108-20-311/27/19 12:210.0046 0.0026 1
Ethylbenzene ND mg/kg 11/27/19 15:18 100-41-411/27/19 12:210.0046 0.00097 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 15:18 87-68-311/27/19 12:210.0046 0.0023 1
2-Hexanone ND mg/kg 11/27/19 15:18 591-78-611/27/19 12:210.046 0.0047 1
Isopropylbenzene (Cumene)ND mg/kg 11/27/19 15:18 98-82-811/27/19 12:210.0046 0.0013 1
p-Isopropyltoluene ND mg/kg 11/27/19 15:18 99-87-611/27/19 12:210.0046 0.0022 1
Methylene Chloride ND mg/kg 11/27/19 15:18 75-09-2 IH,v111/27/19 12:210.018 0.0054 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 11/27/19 15:18 108-10-111/27/19 12:210.046 0.0034 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-4 (15-17)Lab ID: 92454745001 Collected: 11/20/19 13:30 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 11/27/19 15:18 1634-04-411/27/19 12:210.0046 0.0026 1
Naphthalene ND mg/kg 11/27/19 15:18 91-20-311/27/19 12:210.0046 0.0039 1
n-Propylbenzene ND mg/kg 11/27/19 15:18 103-65-111/27/19 12:210.0046 0.0015 1
Styrene ND mg/kg 11/27/19 15:18 100-42-511/27/19 12:210.0046 0.0014 1
1,1,1,2-Tetrachloroethane ND mg/kg 11/27/19 15:18 630-20-611/27/19 12:210.0046 0.0011 1
1,1,2,2-Tetrachloroethane ND mg/kg 11/27/19 15:18 79-34-511/27/19 12:210.0046 0.0016 1
Tetrachloroethene ND mg/kg 11/27/19 15:18 127-18-411/27/19 12:210.0046 0.0014 1
Toluene ND mg/kg 11/27/19 15:18 108-88-311/27/19 12:210.0046 0.0015 1
1,2,3-Trichlorobenzene ND mg/kg 11/27/19 15:18 87-61-611/27/19 12:210.0046 0.0033 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 15:18 120-82-111/27/19 12:210.0046 0.0024 1
1,1,1-Trichloroethane ND mg/kg 11/27/19 15:18 71-55-611/27/19 12:210.0046 0.00079 1
1,1,2-Trichloroethane ND mg/kg 11/27/19 15:18 79-00-511/27/19 12:210.0046 0.0010 1
Trichloroethene ND mg/kg 11/27/19 15:18 79-01-611/27/19 12:210.0046 0.0012 1
Trichlorofluoromethane ND mg/kg 11/27/19 15:18 75-69-411/27/19 12:210.0046 0.0011 1
1,2,3-Trichloropropane ND mg/kg 11/27/19 15:18 96-18-411/27/19 12:210.0046 0.0015 1
1,2,4-Trimethylbenzene ND mg/kg 11/27/19 15:18 95-63-611/27/19 12:210.0046 0.0018 1
1,3,5-Trimethylbenzene ND mg/kg 11/27/19 15:18 108-67-811/27/19 12:210.0046 0.0015 1
Vinyl acetate ND mg/kg 11/27/19 15:18 108-05-411/27/19 12:210.046 0.015 1
Vinyl chloride ND mg/kg 11/27/19 15:18 75-01-411/27/19 12:210.0091 0.0017 1
Xylene (Total)ND mg/kg 11/27/19 15:18 1330-20-711/27/19 12:210.0091 0.0032 1
m&p-Xylene ND mg/kg 11/27/19 15:18 179601-23-111/27/19 12:210.0091 0.0022 1
o-Xylene ND mg/kg 11/27/19 15:18 95-47-611/27/19 12:210.0046 0.0011 1
Surrogates
Toluene-d8 (S)105 %11/27/19 15:18 2037-26-511/27/19 12:2170-130 1
4-Bromofluorobenzene (S)108 %11/27/19 15:18 460-00-411/27/19 12:2170-130 1
1,2-Dichloroethane-d4 (S)96 %11/27/19 15:18 17060-07-011/27/19 12:2170-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)ND mg/kg 11/25/19 13:57 123-91-111/25/19 11:520.010 0.0031 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %11/25/19 13:57 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)105 %11/25/19 13:57 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.8 %11/22/19 13:280.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-4 (19-21)Lab ID: 92454745002 Collected: 11/20/19 13:50 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic ND mg/kg 11/26/19 19:26 7440-38-211/25/19 12:160.87 0.43 1
Barium 319 mg/kg 11/26/19 19:26 7440-39-311/25/19 12:160.43 0.22 1
Cadmium 0.069J mg/kg 11/26/19 19:26 7440-43-911/25/19 12:160.087 0.043 1
Chromium 19.6 mg/kg 11/26/19 19:26 7440-47-311/25/19 12:160.43 0.22 1
Lead 1.5 mg/kg 11/26/19 19:26 7439-92-111/25/19 12:160.43 0.22 1
Selenium 0.64J mg/kg 11/26/19 19:26 7782-49-2 B11/25/19 12:160.87 0.43 1
Silver ND mg/kg 11/26/19 19:26 7440-22-411/25/19 12:160.43 0.22 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury ND mg/kg 11/22/19 15:27 7439-97-611/22/19 11:500.0022 0.0011 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/27/19 11:01 83-32-911/26/19 10:110.39 0.10 1
Acenaphthylene ND mg/kg 11/27/19 11:01 208-96-811/26/19 10:110.39 0.093 1
Aniline ND mg/kg 11/27/19 11:01 62-53-311/26/19 10:110.39 0.089 1
Anthracene ND mg/kg 11/27/19 11:01 120-12-711/26/19 10:110.39 0.10 1
Benzo(a)anthracene ND mg/kg 11/27/19 11:01 56-55-311/26/19 10:110.39 0.13 1
Benzo(a)pyrene ND mg/kg 11/27/19 11:01 50-32-811/26/19 10:110.39 0.17 1
Benzo(b)fluoranthene ND mg/kg 11/27/19 11:01 205-99-211/26/19 10:110.39 0.16 1
Benzo(g,h,i)perylene ND mg/kg 11/27/19 11:01 191-24-211/26/19 10:110.39 0.15 1
Benzo(k)fluoranthene ND mg/kg 11/27/19 11:01 207-08-911/26/19 10:110.39 0.17 1
Benzoic Acid ND mg/kg 11/27/19 11:01 65-85-011/26/19 10:112.0 0.43 1
Benzyl alcohol ND mg/kg 11/27/19 11:01 100-51-611/26/19 10:110.79 0.21 1
4-Bromophenylphenyl ether ND mg/kg 11/27/19 11:01 101-55-311/26/19 10:110.39 0.10 1
Butylbenzylphthalate ND mg/kg 11/27/19 11:01 85-68-711/26/19 10:110.39 0.11 1
4-Chloro-3-methylphenol ND mg/kg 11/27/19 11:01 59-50-711/26/19 10:110.79 0.24 1
4-Chloroaniline ND mg/kg 11/27/19 11:01 106-47-811/26/19 10:112.0 0.24 1
bis(2-Chloroethoxy)methane ND mg/kg 11/27/19 11:01 111-91-111/26/19 10:110.39 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 11/27/19 11:01 111-44-411/26/19 10:110.39 0.084 1
2-Chloronaphthalene ND mg/kg 11/27/19 11:01 91-58-711/26/19 10:110.39 0.088 1
2-Chlorophenol ND mg/kg 11/27/19 11:01 95-57-811/26/19 10:110.39 0.092 1
4-Chlorophenylphenyl ether ND mg/kg 11/27/19 11:01 7005-72-311/26/19 10:110.39 0.10 1
Chrysene ND mg/kg 11/27/19 11:01 218-01-911/26/19 10:110.39 0.11 1
Dibenz(a,h)anthracene ND mg/kg 11/27/19 11:01 53-70-311/26/19 10:110.39 0.16 1
Dibenzofuran ND mg/kg 11/27/19 11:01 132-64-911/26/19 10:110.39 0.099 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 11:01 95-50-111/26/19 10:110.39 0.085 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 11:01 541-73-111/26/19 10:110.39 0.089 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 11:01 106-46-711/26/19 10:110.39 0.087 1
3,3'-Dichlorobenzidine ND mg/kg 11/27/19 11:01 91-94-111/26/19 10:112.0 0.27 1
2,4-Dichlorophenol ND mg/kg 11/27/19 11:01 120-83-211/26/19 10:110.39 0.13 1
Diethylphthalate ND mg/kg 11/27/19 11:01 84-66-211/26/19 10:110.39 0.086 1
2,4-Dimethylphenol ND mg/kg 11/27/19 11:01 105-67-911/26/19 10:110.39 0.098 1
Dimethylphthalate ND mg/kg 11/27/19 11:01 131-11-311/26/19 10:110.39 0.089 1
Di-n-butylphthalate ND mg/kg 11/27/19 11:01 84-74-211/26/19 10:110.39 0.097 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/27/19 11:01 534-52-111/26/19 10:110.79 0.64 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-4 (19-21)Lab ID: 92454745002 Collected: 11/20/19 13:50 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/27/19 11:01 51-28-511/26/19 10:112.0 1.3 1
2,4-Dinitrotoluene ND mg/kg 11/27/19 11:01 121-14-211/26/19 10:110.39 0.10 1
2,6-Dinitrotoluene ND mg/kg 11/27/19 11:01 606-20-211/26/19 10:110.39 0.10 1
Di-n-octylphthalate ND mg/kg 11/27/19 11:01 117-84-011/26/19 10:110.39 0.22 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/27/19 11:01 117-81-711/26/19 10:110.39 0.13 1
Fluoranthene ND mg/kg 11/27/19 11:01 206-44-011/26/19 10:110.39 0.12 1
Fluorene ND mg/kg 11/27/19 11:01 86-73-711/26/19 10:110.39 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 11:01 87-68-311/26/19 10:110.39 0.096 1
Hexachlorobenzene ND mg/kg 11/27/19 11:01 118-74-111/26/19 10:110.39 0.10 1
Hexachlorocyclopentadiene ND mg/kg 11/27/19 11:01 77-47-411/26/19 10:110.39 0.16 1
Hexachloroethane ND mg/kg 11/27/19 11:01 67-72-111/26/19 10:110.39 0.090 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/27/19 11:01 193-39-511/26/19 10:110.39 0.18 1
Isophorone ND mg/kg 11/27/19 11:01 78-59-111/26/19 10:110.39 0.086 1
1-Methylnaphthalene ND mg/kg 11/27/19 11:01 90-12-011/26/19 10:110.39 0.11 1
2-Methylnaphthalene ND mg/kg 11/27/19 11:01 91-57-611/26/19 10:110.39 0.10 1
2-Methylphenol(o-Cresol)ND mg/kg 11/27/19 11:01 95-48-711/26/19 10:110.39 0.087 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/27/19 11:01 15831-10-411/26/19 10:110.39 0.099 1
Naphthalene ND mg/kg 11/27/19 11:01 91-20-311/26/19 10:110.39 0.094 1
2-Nitroaniline ND mg/kg 11/27/19 11:01 88-74-411/26/19 10:112.0 0.20 1
3-Nitroaniline ND mg/kg 11/27/19 11:01 99-09-211/26/19 10:112.0 0.21 1
4-Nitroaniline ND mg/kg 11/27/19 11:01 100-01-611/26/19 10:110.79 0.19 1
Nitrobenzene ND mg/kg 11/27/19 11:01 98-95-311/26/19 10:110.39 0.094 1
2-Nitrophenol ND mg/kg 11/27/19 11:01 88-75-511/26/19 10:110.39 0.12 1
4-Nitrophenol ND mg/kg 11/27/19 11:01 100-02-711/26/19 10:112.0 0.63 1
N-Nitrosodimethylamine ND mg/kg 11/27/19 11:01 62-75-911/26/19 10:110.39 0.11 1
N-Nitroso-di-n-propylamine ND mg/kg 11/27/19 11:01 621-64-711/26/19 10:110.39 0.11 1
N-Nitrosodiphenylamine ND mg/kg 11/27/19 11:01 86-30-611/26/19 10:110.39 0.10 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/27/19 11:01 108-60-111/26/19 10:110.39 0.11 1
Pentachlorophenol ND mg/kg 11/27/19 11:01 87-86-511/26/19 10:112.0 0.18 1
Phenanthrene ND mg/kg 11/27/19 11:01 85-01-811/26/19 10:110.39 0.099 1
Phenol ND mg/kg 11/27/19 11:01 108-95-211/26/19 10:110.39 0.094 1
Pyrene ND mg/kg 11/27/19 11:01 129-00-011/26/19 10:110.39 0.11 1
Pyridine ND mg/kg 11/27/19 11:01 110-86-111/26/19 10:110.39 0.10 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 11:01 120-82-111/26/19 10:110.39 0.090 1
2,4,5-Trichlorophenol ND mg/kg 11/27/19 11:01 95-95-411/26/19 10:110.39 0.10 1
2,4,6-Trichlorophenol ND mg/kg 11/27/19 11:01 88-06-211/26/19 10:110.39 0.099 1
Surrogates
Nitrobenzene-d5 (S)59 %11/27/19 11:01 4165-60-011/26/19 10:1123-110 1
2-Fluorobiphenyl (S)59 %11/27/19 11:01 321-60-811/26/19 10:1130-110 1
Terphenyl-d14 (S)65 %11/27/19 11:01 1718-51-011/26/19 10:1128-110 1
Phenol-d6 (S)57 %11/27/19 11:01 13127-88-311/26/19 10:1122-110 1
2-Fluorophenol (S)58 %11/27/19 11:01 367-12-411/26/19 10:1113-110 1
2,4,6-Tribromophenol (S)66 %11/27/19 11:01 118-79-611/26/19 10:1127-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-4 (19-21)Lab ID: 92454745002 Collected: 11/20/19 13:50 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 12/02/19 12:13 67-64-111/27/19 12:210.084 0.0079 1
Benzene ND mg/kg 12/02/19 12:13 71-43-211/27/19 12:210.0042 0.00075 1
Bromobenzene ND mg/kg 12/02/19 12:13 108-86-111/27/19 12:210.0042 0.0011 1
Bromochloromethane ND mg/kg 12/02/19 12:13 74-97-511/27/19 12:210.0042 0.0010 1
Bromodichloromethane ND mg/kg 12/02/19 12:13 75-27-411/27/19 12:210.0042 0.00082 1
Bromoform ND mg/kg 12/02/19 12:13 75-25-211/27/19 12:210.0042 0.0020 1
Bromomethane ND mg/kg 12/02/19 12:13 74-83-9 IH11/27/19 12:210.0084 0.0020 1
2-Butanone (MEK)ND mg/kg 12/02/19 12:13 78-93-311/27/19 12:210.084 0.010 1
n-Butylbenzene ND mg/kg 12/02/19 12:13 104-51-811/27/19 12:210.0042 0.0024 1
sec-Butylbenzene ND mg/kg 12/02/19 12:13 135-98-811/27/19 12:210.0042 0.0018 1
tert-Butylbenzene ND mg/kg 12/02/19 12:13 98-06-6 v311/27/19 12:210.0042 0.0014 1
Carbon tetrachloride ND mg/kg 12/02/19 12:13 56-23-511/27/19 12:210.0042 0.00080 1
Chlorobenzene ND mg/kg 12/02/19 12:13 108-90-711/27/19 12:210.0042 0.00081 1
Chloroethane ND mg/kg 12/02/19 12:13 75-00-3 IK11/27/19 12:210.0084 0.0017 1
Chloroform ND mg/kg 12/02/19 12:13 67-66-311/27/19 12:210.0042 0.00089 1
Chloromethane ND mg/kg 12/02/19 12:13 74-87-311/27/19 12:210.0084 0.0027 1
2-Chlorotoluene ND mg/kg 12/02/19 12:13 95-49-811/27/19 12:210.0042 0.0013 1
4-Chlorotoluene ND mg/kg 12/02/19 12:13 106-43-411/27/19 12:210.0042 0.0013 1
1,2-Dibromo-3-chloropropane ND mg/kg 12/02/19 12:13 96-12-811/27/19 12:210.0042 0.0021 1
Dibromochloromethane ND mg/kg 12/02/19 12:13 124-48-111/27/19 12:210.0042 0.0021 1
1,2-Dibromoethane (EDB)ND mg/kg 12/02/19 12:13 106-93-411/27/19 12:210.0042 0.00094 1
Dibromomethane ND mg/kg 12/02/19 12:13 74-95-311/27/19 12:210.0042 0.0012 1
1,2-Dichlorobenzene ND mg/kg 12/02/19 12:13 95-50-111/27/19 12:210.0042 0.0015 1
1,3-Dichlorobenzene ND mg/kg 12/02/19 12:13 541-73-111/27/19 12:210.0042 0.0015 1
1,4-Dichlorobenzene ND mg/kg 12/02/19 12:13 106-46-711/27/19 12:210.0042 0.0014 1
Dichlorodifluoromethane ND mg/kg 12/02/19 12:13 75-71-811/27/19 12:210.0084 0.0034 1
1,1-Dichloroethane ND mg/kg 12/02/19 12:13 75-34-311/27/19 12:210.0042 0.00062 1
1,2-Dichloroethane ND mg/kg 12/02/19 12:13 107-06-211/27/19 12:210.0042 0.00084 1
1,1-Dichloroethene ND mg/kg 12/02/19 12:13 75-35-411/27/19 12:210.0042 0.00097 1
cis-1,2-Dichloroethene ND mg/kg 12/02/19 12:13 156-59-211/27/19 12:210.0042 0.00073 1
trans-1,2-Dichloroethene ND mg/kg 12/02/19 12:13 156-60-511/27/19 12:210.0042 0.00082 1
1,2-Dichloropropane ND mg/kg 12/02/19 12:13 78-87-511/27/19 12:210.0042 0.0016 1
1,3-Dichloropropane ND mg/kg 12/02/19 12:13 142-28-911/27/19 12:210.0042 0.0016 1
2,2-Dichloropropane ND mg/kg 12/02/19 12:13 594-20-711/27/19 12:210.0042 0.00041 1
1,1-Dichloropropene ND mg/kg 12/02/19 12:13 563-58-611/27/19 12:210.0042 0.0018 1
cis-1,3-Dichloropropene ND mg/kg 12/02/19 12:13 10061-01-511/27/19 12:210.0042 0.0019 1
trans-1,3-Dichloropropene ND mg/kg 12/02/19 12:13 10061-02-611/27/19 12:210.0042 0.00073 1
Diisopropyl ether ND mg/kg 12/02/19 12:13 108-20-311/27/19 12:210.0042 0.0024 1
Ethylbenzene ND mg/kg 12/02/19 12:13 100-41-411/27/19 12:210.0042 0.00089 1
Hexachloro-1,3-butadiene ND mg/kg 12/02/19 12:13 87-68-311/27/19 12:210.0042 0.0021 1
2-Hexanone ND mg/kg 12/02/19 12:13 591-78-611/27/19 12:210.042 0.0043 1
Isopropylbenzene (Cumene)ND mg/kg 12/02/19 12:13 98-82-811/27/19 12:210.0042 0.0012 1
p-Isopropyltoluene ND mg/kg 12/02/19 12:13 99-87-611/27/19 12:210.0042 0.0020 1
Methylene Chloride ND mg/kg 12/02/19 12:13 75-09-2 IH,v111/27/19 12:210.017 0.0049 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 12/02/19 12:13 108-10-111/27/19 12:210.042 0.0031 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-4 (19-21)Lab ID: 92454745002 Collected: 11/20/19 13:50 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 12/02/19 12:13 1634-04-411/27/19 12:210.0042 0.0024 1
Naphthalene ND mg/kg 12/02/19 12:13 91-20-311/27/19 12:210.0042 0.0036 1
n-Propylbenzene ND mg/kg 12/02/19 12:13 103-65-111/27/19 12:210.0042 0.0014 1
Styrene ND mg/kg 12/02/19 12:13 100-42-511/27/19 12:210.0042 0.0012 1
1,1,1,2-Tetrachloroethane ND mg/kg 12/02/19 12:13 630-20-611/27/19 12:210.0042 0.0010 1
1,1,2,2-Tetrachloroethane ND mg/kg 12/02/19 12:13 79-34-511/27/19 12:210.0042 0.0014 1
Tetrachloroethene ND mg/kg 12/02/19 12:13 127-18-411/27/19 12:210.0042 0.0013 1
Toluene ND mg/kg 12/02/19 12:13 108-88-311/27/19 12:210.0042 0.0014 1
1,2,3-Trichlorobenzene ND mg/kg 12/02/19 12:13 87-61-611/27/19 12:210.0042 0.0030 1
1,2,4-Trichlorobenzene ND mg/kg 12/02/19 12:13 120-82-111/27/19 12:210.0042 0.0022 1
1,1,1-Trichloroethane ND mg/kg 12/02/19 12:13 71-55-611/27/19 12:210.0042 0.00073 1
1,1,2-Trichloroethane ND mg/kg 12/02/19 12:13 79-00-511/27/19 12:210.0042 0.00095 1
Trichloroethene ND mg/kg 12/02/19 12:13 79-01-611/27/19 12:210.0042 0.0011 1
Trichlorofluoromethane ND mg/kg 12/02/19 12:13 75-69-411/27/19 12:210.0042 0.00099 1
1,2,3-Trichloropropane ND mg/kg 12/02/19 12:13 96-18-411/27/19 12:210.0042 0.0014 1
1,2,4-Trimethylbenzene ND mg/kg 12/02/19 12:13 95-63-611/27/19 12:210.0042 0.0016 1
1,3,5-Trimethylbenzene ND mg/kg 12/02/19 12:13 108-67-811/27/19 12:210.0042 0.0014 1
Vinyl acetate ND mg/kg 12/02/19 12:13 108-05-411/27/19 12:210.042 0.014 1
Vinyl chloride ND mg/kg 12/02/19 12:13 75-01-411/27/19 12:210.0084 0.0016 1
Xylene (Total)ND mg/kg 12/02/19 12:13 1330-20-711/27/19 12:210.0084 0.0029 1
m&p-Xylene ND mg/kg 12/02/19 12:13 179601-23-111/27/19 12:210.0084 0.0020 1
o-Xylene ND mg/kg 12/02/19 12:13 95-47-611/27/19 12:210.0042 0.00098 1
Surrogates
Toluene-d8 (S)107 %12/02/19 12:13 2037-26-511/27/19 12:2170-130 1
4-Bromofluorobenzene (S)108 %12/02/19 12:13 460-00-411/27/19 12:2170-130 1
1,2-Dichloroethane-d4 (S)108 %12/02/19 12:13 17060-07-011/27/19 12:2170-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)ND mg/kg 11/25/19 14:17 123-91-111/25/19 11:520.0081 0.0024 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/25/19 14:17 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)101 %11/25/19 14:17 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.7 %11/22/19 13:280.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-5 (15-17)Lab ID: 92454745003 Collected: 11/20/19 14:15 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic ND mg/kg 11/26/19 19:29 7440-38-211/25/19 12:161.3 0.65 1
Barium 96.9 mg/kg 11/26/19 19:29 7440-39-311/25/19 12:160.65 0.33 1
Cadmium ND mg/kg 11/26/19 19:29 7440-43-911/25/19 12:160.13 0.065 1
Chromium 9.8 mg/kg 11/26/19 19:29 7440-47-311/25/19 12:160.65 0.33 1
Lead 7.0 mg/kg 11/26/19 19:29 7439-92-111/25/19 12:160.65 0.33 1
Selenium 0.86J mg/kg 11/26/19 19:29 7782-49-211/25/19 12:161.3 0.65 1
Silver ND mg/kg 11/26/19 19:29 7440-22-411/25/19 12:160.65 0.33 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.0042 mg/kg 11/22/19 15:29 7439-97-611/22/19 11:500.0034 0.0017 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/27/19 11:36 83-32-911/26/19 10:110.49 0.13 1
Acenaphthylene ND mg/kg 11/27/19 11:36 208-96-811/26/19 10:110.49 0.12 1
Aniline ND mg/kg 11/27/19 11:36 62-53-311/26/19 10:110.49 0.11 1
Anthracene ND mg/kg 11/27/19 11:36 120-12-711/26/19 10:110.49 0.13 1
Benzo(a)anthracene ND mg/kg 11/27/19 11:36 56-55-311/26/19 10:110.49 0.16 1
Benzo(a)pyrene ND mg/kg 11/27/19 11:36 50-32-811/26/19 10:110.49 0.21 1
Benzo(b)fluoranthene ND mg/kg 11/27/19 11:36 205-99-211/26/19 10:110.49 0.20 1
Benzo(g,h,i)perylene ND mg/kg 11/27/19 11:36 191-24-211/26/19 10:110.49 0.19 1
Benzo(k)fluoranthene ND mg/kg 11/27/19 11:36 207-08-911/26/19 10:110.49 0.21 1
Benzoic Acid ND mg/kg 11/27/19 11:36 65-85-011/26/19 10:112.4 0.53 1
Benzyl alcohol ND mg/kg 11/27/19 11:36 100-51-611/26/19 10:110.98 0.26 1
4-Bromophenylphenyl ether ND mg/kg 11/27/19 11:36 101-55-311/26/19 10:110.49 0.13 1
Butylbenzylphthalate ND mg/kg 11/27/19 11:36 85-68-711/26/19 10:110.49 0.13 1
4-Chloro-3-methylphenol ND mg/kg 11/27/19 11:36 59-50-711/26/19 10:110.98 0.30 1
4-Chloroaniline ND mg/kg 11/27/19 11:36 106-47-811/26/19 10:112.4 0.30 1
bis(2-Chloroethoxy)methane ND mg/kg 11/27/19 11:36 111-91-111/26/19 10:110.49 0.13 1
bis(2-Chloroethyl) ether ND mg/kg 11/27/19 11:36 111-44-411/26/19 10:110.49 0.10 1
2-Chloronaphthalene ND mg/kg 11/27/19 11:36 91-58-711/26/19 10:110.49 0.11 1
2-Chlorophenol ND mg/kg 11/27/19 11:36 95-57-811/26/19 10:110.49 0.11 1
4-Chlorophenylphenyl ether ND mg/kg 11/27/19 11:36 7005-72-311/26/19 10:110.49 0.13 1
Chrysene ND mg/kg 11/27/19 11:36 218-01-911/26/19 10:110.49 0.14 1
Dibenz(a,h)anthracene ND mg/kg 11/27/19 11:36 53-70-311/26/19 10:110.49 0.20 1
Dibenzofuran ND mg/kg 11/27/19 11:36 132-64-911/26/19 10:110.49 0.12 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 11:36 95-50-111/26/19 10:110.49 0.11 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 11:36 541-73-111/26/19 10:110.49 0.11 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 11:36 106-46-711/26/19 10:110.49 0.11 1
3,3'-Dichlorobenzidine ND mg/kg 11/27/19 11:36 91-94-111/26/19 10:112.4 0.34 1
2,4-Dichlorophenol ND mg/kg 11/27/19 11:36 120-83-211/26/19 10:110.49 0.16 1
Diethylphthalate ND mg/kg 11/27/19 11:36 84-66-211/26/19 10:110.49 0.11 1
2,4-Dimethylphenol ND mg/kg 11/27/19 11:36 105-67-911/26/19 10:110.49 0.12 1
Dimethylphthalate ND mg/kg 11/27/19 11:36 131-11-311/26/19 10:110.49 0.11 1
Di-n-butylphthalate ND mg/kg 11/27/19 11:36 84-74-211/26/19 10:110.49 0.12 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/27/19 11:36 534-52-111/26/19 10:110.98 0.79 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-5 (15-17)Lab ID: 92454745003 Collected: 11/20/19 14:15 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/27/19 11:36 51-28-511/26/19 10:112.4 1.6 1
2,4-Dinitrotoluene ND mg/kg 11/27/19 11:36 121-14-211/26/19 10:110.49 0.13 1
2,6-Dinitrotoluene ND mg/kg 11/27/19 11:36 606-20-211/26/19 10:110.49 0.13 1
Di-n-octylphthalate ND mg/kg 11/27/19 11:36 117-84-011/26/19 10:110.49 0.28 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/27/19 11:36 117-81-711/26/19 10:110.49 0.16 1
Fluoranthene ND mg/kg 11/27/19 11:36 206-44-011/26/19 10:110.49 0.15 1
Fluorene ND mg/kg 11/27/19 11:36 86-73-711/26/19 10:110.49 0.13 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 11:36 87-68-311/26/19 10:110.49 0.12 1
Hexachlorobenzene ND mg/kg 11/27/19 11:36 118-74-111/26/19 10:110.49 0.12 1
Hexachlorocyclopentadiene ND mg/kg 11/27/19 11:36 77-47-411/26/19 10:110.49 0.20 1
Hexachloroethane ND mg/kg 11/27/19 11:36 67-72-111/26/19 10:110.49 0.11 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/27/19 11:36 193-39-511/26/19 10:110.49 0.22 1
Isophorone ND mg/kg 11/27/19 11:36 78-59-111/26/19 10:110.49 0.11 1
1-Methylnaphthalene ND mg/kg 11/27/19 11:36 90-12-011/26/19 10:110.49 0.13 1
2-Methylnaphthalene ND mg/kg 11/27/19 11:36 91-57-611/26/19 10:110.49 0.12 1
2-Methylphenol(o-Cresol)ND mg/kg 11/27/19 11:36 95-48-711/26/19 10:110.49 0.11 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/27/19 11:36 15831-10-411/26/19 10:110.49 0.12 1
Naphthalene ND mg/kg 11/27/19 11:36 91-20-311/26/19 10:110.49 0.12 1
2-Nitroaniline ND mg/kg 11/27/19 11:36 88-74-411/26/19 10:112.4 0.25 1
3-Nitroaniline ND mg/kg 11/27/19 11:36 99-09-211/26/19 10:112.4 0.26 1
4-Nitroaniline ND mg/kg 11/27/19 11:36 100-01-611/26/19 10:110.98 0.24 1
Nitrobenzene ND mg/kg 11/27/19 11:36 98-95-311/26/19 10:110.49 0.12 1
2-Nitrophenol ND mg/kg 11/27/19 11:36 88-75-511/26/19 10:110.49 0.15 1
4-Nitrophenol ND mg/kg 11/27/19 11:36 100-02-711/26/19 10:112.4 0.78 1
N-Nitrosodimethylamine ND mg/kg 11/27/19 11:36 62-75-911/26/19 10:110.49 0.14 1
N-Nitroso-di-n-propylamine ND mg/kg 11/27/19 11:36 621-64-711/26/19 10:110.49 0.14 1
N-Nitrosodiphenylamine ND mg/kg 11/27/19 11:36 86-30-611/26/19 10:110.49 0.13 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/27/19 11:36 108-60-111/26/19 10:110.49 0.14 1
Pentachlorophenol ND mg/kg 11/27/19 11:36 87-86-511/26/19 10:112.4 0.22 1
Phenanthrene ND mg/kg 11/27/19 11:36 85-01-811/26/19 10:110.49 0.12 1
Phenol ND mg/kg 11/27/19 11:36 108-95-211/26/19 10:110.49 0.12 1
Pyrene ND mg/kg 11/27/19 11:36 129-00-011/26/19 10:110.49 0.13 1
Pyridine ND mg/kg 11/27/19 11:36 110-86-111/26/19 10:110.49 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 11:36 120-82-111/26/19 10:110.49 0.11 1
2,4,5-Trichlorophenol ND mg/kg 11/27/19 11:36 95-95-411/26/19 10:110.49 0.13 1
2,4,6-Trichlorophenol ND mg/kg 11/27/19 11:36 88-06-211/26/19 10:110.49 0.12 1
Surrogates
Nitrobenzene-d5 (S)59 %11/27/19 11:36 4165-60-011/26/19 10:1123-110 1
2-Fluorobiphenyl (S)60 %11/27/19 11:36 321-60-811/26/19 10:1130-110 1
Terphenyl-d14 (S)64 %11/27/19 11:36 1718-51-011/26/19 10:1128-110 1
Phenol-d6 (S)56 %11/27/19 11:36 13127-88-311/26/19 10:1122-110 1
2-Fluorophenol (S)57 %11/27/19 11:36 367-12-411/26/19 10:1113-110 1
2,4,6-Tribromophenol (S)61 %11/27/19 11:36 118-79-611/26/19 10:1127-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-5 (15-17)Lab ID: 92454745003 Collected: 11/20/19 14:15 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 11/27/19 16:30 67-64-111/27/19 12:210.13 0.012 1
Benzene ND mg/kg 11/27/19 16:30 71-43-211/27/19 12:210.0065 0.0012 1
Bromobenzene ND mg/kg 11/27/19 16:30 108-86-111/27/19 12:210.0065 0.0018 1
Bromochloromethane ND mg/kg 11/27/19 16:30 74-97-511/27/19 12:210.0065 0.0016 1
Bromodichloromethane ND mg/kg 11/27/19 16:30 75-27-411/27/19 12:210.0065 0.0013 1
Bromoform ND mg/kg 11/27/19 16:30 75-25-211/27/19 12:210.0065 0.0032 1
Bromomethane ND mg/kg 11/27/19 16:30 74-83-9 IH11/27/19 12:210.013 0.0031 1
2-Butanone (MEK)ND mg/kg 11/27/19 16:30 78-93-311/27/19 12:210.13 0.015 1
n-Butylbenzene ND mg/kg 11/27/19 16:30 104-51-811/27/19 12:210.0065 0.0037 1
sec-Butylbenzene ND mg/kg 11/27/19 16:30 135-98-811/27/19 12:210.0065 0.0027 1
tert-Butylbenzene ND mg/kg 11/27/19 16:30 98-06-6 v211/27/19 12:210.0065 0.0022 1
Carbon tetrachloride ND mg/kg 11/27/19 16:30 56-23-511/27/19 12:210.0065 0.0012 1
Chlorobenzene ND mg/kg 11/27/19 16:30 108-90-711/27/19 12:210.0065 0.0013 1
Chloroethane ND mg/kg 11/27/19 16:30 75-00-3 IK11/27/19 12:210.013 0.0027 1
Chloroform ND mg/kg 11/27/19 16:30 67-66-311/27/19 12:210.0065 0.0014 1
Chloromethane ND mg/kg 11/27/19 16:30 74-87-311/27/19 12:210.013 0.0042 1
2-Chlorotoluene ND mg/kg 11/27/19 16:30 95-49-811/27/19 12:210.0065 0.0020 1
4-Chlorotoluene ND mg/kg 11/27/19 16:30 106-43-411/27/19 12:210.0065 0.0019 1
1,2-Dibromo-3-chloropropane ND mg/kg 11/27/19 16:30 96-12-811/27/19 12:210.0065 0.0033 1
Dibromochloromethane ND mg/kg 11/27/19 16:30 124-48-111/27/19 12:210.0065 0.0032 1
1,2-Dibromoethane (EDB)ND mg/kg 11/27/19 16:30 106-93-411/27/19 12:210.0065 0.0015 1
Dibromomethane ND mg/kg 11/27/19 16:30 74-95-311/27/19 12:210.0065 0.0019 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 16:30 95-50-111/27/19 12:210.0065 0.0023 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 16:30 541-73-111/27/19 12:210.0065 0.0023 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 16:30 106-46-711/27/19 12:210.0065 0.0022 1
Dichlorodifluoromethane ND mg/kg 11/27/19 16:30 75-71-811/27/19 12:210.013 0.0053 1
1,1-Dichloroethane ND mg/kg 11/27/19 16:30 75-34-311/27/19 12:210.0065 0.00095 1
1,2-Dichloroethane ND mg/kg 11/27/19 16:30 107-06-211/27/19 12:210.0065 0.0013 1
1,1-Dichloroethene ND mg/kg 11/27/19 16:30 75-35-411/27/19 12:210.0065 0.0015 1
cis-1,2-Dichloroethene ND mg/kg 11/27/19 16:30 156-59-211/27/19 12:210.0065 0.0011 1
trans-1,2-Dichloroethene ND mg/kg 11/27/19 16:30 156-60-511/27/19 12:210.0065 0.0013 1
1,2-Dichloropropane ND mg/kg 11/27/19 16:30 78-87-511/27/19 12:210.0065 0.0024 1
1,3-Dichloropropane ND mg/kg 11/27/19 16:30 142-28-911/27/19 12:210.0065 0.0024 1
2,2-Dichloropropane ND mg/kg 11/27/19 16:30 594-20-711/27/19 12:210.0065 0.00064 1
1,1-Dichloropropene ND mg/kg 11/27/19 16:30 563-58-611/27/19 12:210.0065 0.0027 1
cis-1,3-Dichloropropene ND mg/kg 11/27/19 16:30 10061-01-511/27/19 12:210.0065 0.0029 1
trans-1,3-Dichloropropene ND mg/kg 11/27/19 16:30 10061-02-611/27/19 12:210.0065 0.0011 1
Diisopropyl ether ND mg/kg 11/27/19 16:30 108-20-311/27/19 12:210.0065 0.0037 1
Ethylbenzene ND mg/kg 11/27/19 16:30 100-41-411/27/19 12:210.0065 0.0014 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 16:30 87-68-311/27/19 12:210.0065 0.0032 1
2-Hexanone ND mg/kg 11/27/19 16:30 591-78-611/27/19 12:210.065 0.0067 1
Isopropylbenzene (Cumene)ND mg/kg 11/27/19 16:30 98-82-811/27/19 12:210.0065 0.0019 1
p-Isopropyltoluene ND mg/kg 11/27/19 16:30 99-87-611/27/19 12:210.0065 0.0031 1
Methylene Chloride ND mg/kg 11/27/19 16:30 75-09-2 IH,v111/27/19 12:210.026 0.0077 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 11/27/19 16:30 108-10-111/27/19 12:210.065 0.0048 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-5 (15-17)Lab ID: 92454745003 Collected: 11/20/19 14:15 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 11/27/19 16:30 1634-04-411/27/19 12:210.0065 0.0037 1
Naphthalene ND mg/kg 11/27/19 16:30 91-20-311/27/19 12:210.0065 0.0055 1
n-Propylbenzene ND mg/kg 11/27/19 16:30 103-65-111/27/19 12:210.0065 0.0022 1
Styrene ND mg/kg 11/27/19 16:30 100-42-511/27/19 12:210.0065 0.0019 1
1,1,1,2-Tetrachloroethane ND mg/kg 11/27/19 16:30 630-20-611/27/19 12:210.0065 0.0016 1
1,1,2,2-Tetrachloroethane ND mg/kg 11/27/19 16:30 79-34-511/27/19 12:210.0065 0.0022 1
Tetrachloroethene ND mg/kg 11/27/19 16:30 127-18-411/27/19 12:210.0065 0.0020 1
Toluene ND mg/kg 11/27/19 16:30 108-88-311/27/19 12:210.0065 0.0021 1
1,2,3-Trichlorobenzene ND mg/kg 11/27/19 16:30 87-61-611/27/19 12:210.0065 0.0046 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 16:30 120-82-111/27/19 12:210.0065 0.0034 1
1,1,1-Trichloroethane ND mg/kg 11/27/19 16:30 71-55-611/27/19 12:210.0065 0.0011 1
1,1,2-Trichloroethane ND mg/kg 11/27/19 16:30 79-00-511/27/19 12:210.0065 0.0015 1
Trichloroethene ND mg/kg 11/27/19 16:30 79-01-611/27/19 12:210.0065 0.0017 1
Trichlorofluoromethane ND mg/kg 11/27/19 16:30 75-69-411/27/19 12:210.0065 0.0015 1
1,2,3-Trichloropropane ND mg/kg 11/27/19 16:30 96-18-411/27/19 12:210.0065 0.0022 1
1,2,4-Trimethylbenzene ND mg/kg 11/27/19 16:30 95-63-611/27/19 12:210.0065 0.0025 1
1,3,5-Trimethylbenzene ND mg/kg 11/27/19 16:30 108-67-811/27/19 12:210.0065 0.0022 1
Vinyl acetate ND mg/kg 11/27/19 16:30 108-05-411/27/19 12:210.065 0.021 1
Vinyl chloride ND mg/kg 11/27/19 16:30 75-01-411/27/19 12:210.013 0.0025 1
Xylene (Total)ND mg/kg 11/27/19 16:30 1330-20-711/27/19 12:210.013 0.0045 1
m&p-Xylene ND mg/kg 11/27/19 16:30 179601-23-111/27/19 12:210.013 0.0031 1
o-Xylene ND mg/kg 11/27/19 16:30 95-47-611/27/19 12:210.0065 0.0015 1
Surrogates
Toluene-d8 (S)113 %11/27/19 16:30 2037-26-511/27/19 12:2170-130 1
4-Bromofluorobenzene (S)108 %11/27/19 16:30 460-00-411/27/19 12:2170-130 1
1,2-Dichloroethane-d4 (S)102 %11/27/19 16:30 17060-07-011/27/19 12:2170-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)ND mg/kg 11/25/19 14:37 123-91-111/25/19 11:520.012 0.0037 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %11/25/19 14:37 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)104 %11/25/19 14:37 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 32.9 %11/22/19 13:280.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-5 (19-21)Lab ID: 92454745004 Collected: 11/20/19 14:50 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic ND mg/kg 11/26/19 19:32 7440-38-211/25/19 12:161.1 0.55 1
Barium 55.0 mg/kg 11/26/19 19:32 7440-39-311/25/19 12:160.55 0.28 1
Cadmium ND mg/kg 11/26/19 19:32 7440-43-911/25/19 12:160.11 0.055 1
Chromium 11.8 mg/kg 11/26/19 19:32 7440-47-311/25/19 12:160.55 0.28 1
Lead 2.2 mg/kg 11/26/19 19:32 7439-92-111/25/19 12:160.55 0.28 1
Selenium 0.71J mg/kg 11/26/19 19:32 7782-49-211/25/19 12:161.1 0.55 1
Silver ND mg/kg 11/26/19 19:32 7440-22-411/25/19 12:160.55 0.28 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury ND mg/kg 11/22/19 15:31 7439-97-611/22/19 11:500.0026 0.0013 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/27/19 12:11 83-32-911/26/19 10:110.42 0.11 1
Acenaphthylene ND mg/kg 11/27/19 12:11 208-96-811/26/19 10:110.42 0.10 1
Aniline ND mg/kg 11/27/19 12:11 62-53-311/26/19 10:110.42 0.095 1
Anthracene ND mg/kg 11/27/19 12:11 120-12-711/26/19 10:110.42 0.11 1
Benzo(a)anthracene ND mg/kg 11/27/19 12:11 56-55-311/26/19 10:110.42 0.14 1
Benzo(a)pyrene ND mg/kg 11/27/19 12:11 50-32-811/26/19 10:110.42 0.18 1
Benzo(b)fluoranthene ND mg/kg 11/27/19 12:11 205-99-211/26/19 10:110.42 0.17 1
Benzo(g,h,i)perylene ND mg/kg 11/27/19 12:11 191-24-211/26/19 10:110.42 0.17 1
Benzo(k)fluoranthene ND mg/kg 11/27/19 12:11 207-08-911/26/19 10:110.42 0.18 1
Benzoic Acid ND mg/kg 11/27/19 12:11 65-85-011/26/19 10:112.1 0.46 1
Benzyl alcohol ND mg/kg 11/27/19 12:11 100-51-611/26/19 10:110.85 0.23 1
4-Bromophenylphenyl ether ND mg/kg 11/27/19 12:11 101-55-311/26/19 10:110.42 0.11 1
Butylbenzylphthalate ND mg/kg 11/27/19 12:11 85-68-711/26/19 10:110.42 0.11 1
4-Chloro-3-methylphenol ND mg/kg 11/27/19 12:11 59-50-711/26/19 10:110.85 0.26 1
4-Chloroaniline ND mg/kg 11/27/19 12:11 106-47-811/26/19 10:112.1 0.26 1
bis(2-Chloroethoxy)methane ND mg/kg 11/27/19 12:11 111-91-111/26/19 10:110.42 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 11/27/19 12:11 111-44-411/26/19 10:110.42 0.090 1
2-Chloronaphthalene ND mg/kg 11/27/19 12:11 91-58-711/26/19 10:110.42 0.095 1
2-Chlorophenol ND mg/kg 11/27/19 12:11 95-57-811/26/19 10:110.42 0.099 1
4-Chlorophenylphenyl ether ND mg/kg 11/27/19 12:11 7005-72-311/26/19 10:110.42 0.11 1
Chrysene ND mg/kg 11/27/19 12:11 218-01-911/26/19 10:110.42 0.12 1
Dibenz(a,h)anthracene ND mg/kg 11/27/19 12:11 53-70-311/26/19 10:110.42 0.17 1
Dibenzofuran ND mg/kg 11/27/19 12:11 132-64-911/26/19 10:110.42 0.11 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 12:11 95-50-111/26/19 10:110.42 0.092 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 12:11 541-73-111/26/19 10:110.42 0.096 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 12:11 106-46-711/26/19 10:110.42 0.093 1
3,3'-Dichlorobenzidine ND mg/kg 11/27/19 12:11 91-94-111/26/19 10:112.1 0.30 1
2,4-Dichlorophenol ND mg/kg 11/27/19 12:11 120-83-211/26/19 10:110.42 0.14 1
Diethylphthalate ND mg/kg 11/27/19 12:11 84-66-211/26/19 10:110.42 0.092 1
2,4-Dimethylphenol ND mg/kg 11/27/19 12:11 105-67-911/26/19 10:110.42 0.11 1
Dimethylphthalate ND mg/kg 11/27/19 12:11 131-11-311/26/19 10:110.42 0.096 1
Di-n-butylphthalate ND mg/kg 11/27/19 12:11 84-74-211/26/19 10:110.42 0.10 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/27/19 12:11 534-52-111/26/19 10:110.85 0.68 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-5 (19-21)Lab ID: 92454745004 Collected: 11/20/19 14:50 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/27/19 12:11 51-28-511/26/19 10:112.1 1.4 1
2,4-Dinitrotoluene ND mg/kg 11/27/19 12:11 121-14-211/26/19 10:110.42 0.11 1
2,6-Dinitrotoluene ND mg/kg 11/27/19 12:11 606-20-211/26/19 10:110.42 0.11 1
Di-n-octylphthalate ND mg/kg 11/27/19 12:11 117-84-011/26/19 10:110.42 0.24 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/27/19 12:11 117-81-711/26/19 10:110.42 0.14 1
Fluoranthene ND mg/kg 11/27/19 12:11 206-44-011/26/19 10:110.42 0.13 1
Fluorene ND mg/kg 11/27/19 12:11 86-73-711/26/19 10:110.42 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 12:11 87-68-311/26/19 10:110.42 0.10 1
Hexachlorobenzene ND mg/kg 11/27/19 12:11 118-74-111/26/19 10:110.42 0.11 1
Hexachlorocyclopentadiene ND mg/kg 11/27/19 12:11 77-47-411/26/19 10:110.42 0.17 1
Hexachloroethane ND mg/kg 11/27/19 12:11 67-72-111/26/19 10:110.42 0.097 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/27/19 12:11 193-39-511/26/19 10:110.42 0.19 1
Isophorone ND mg/kg 11/27/19 12:11 78-59-111/26/19 10:110.42 0.092 1
1-Methylnaphthalene ND mg/kg 11/27/19 12:11 90-12-011/26/19 10:110.42 0.11 1
2-Methylnaphthalene ND mg/kg 11/27/19 12:11 91-57-611/26/19 10:110.42 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 11/27/19 12:11 95-48-711/26/19 10:110.42 0.094 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/27/19 12:11 15831-10-411/26/19 10:110.42 0.11 1
Naphthalene ND mg/kg 11/27/19 12:11 91-20-311/26/19 10:110.42 0.10 1
2-Nitroaniline ND mg/kg 11/27/19 12:11 88-74-411/26/19 10:112.1 0.21 1
3-Nitroaniline ND mg/kg 11/27/19 12:11 99-09-211/26/19 10:112.1 0.23 1
4-Nitroaniline ND mg/kg 11/27/19 12:11 100-01-611/26/19 10:110.85 0.21 1
Nitrobenzene ND mg/kg 11/27/19 12:11 98-95-311/26/19 10:110.42 0.10 1
2-Nitrophenol ND mg/kg 11/27/19 12:11 88-75-511/26/19 10:110.42 0.13 1
4-Nitrophenol ND mg/kg 11/27/19 12:11 100-02-711/26/19 10:112.1 0.68 1
N-Nitrosodimethylamine ND mg/kg 11/27/19 12:11 62-75-911/26/19 10:110.42 0.12 1
N-Nitroso-di-n-propylamine ND mg/kg 11/27/19 12:11 621-64-711/26/19 10:110.42 0.12 1
N-Nitrosodiphenylamine ND mg/kg 11/27/19 12:11 86-30-611/26/19 10:110.42 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/27/19 12:11 108-60-111/26/19 10:110.42 0.12 1
Pentachlorophenol ND mg/kg 11/27/19 12:11 87-86-511/26/19 10:112.1 0.19 1
Phenanthrene ND mg/kg 11/27/19 12:11 85-01-811/26/19 10:110.42 0.11 1
Phenol ND mg/kg 11/27/19 12:11 108-95-211/26/19 10:110.42 0.10 1
Pyrene ND mg/kg 11/27/19 12:11 129-00-011/26/19 10:110.42 0.12 1
Pyridine ND mg/kg 11/27/19 12:11 110-86-111/26/19 10:110.42 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 12:11 120-82-111/26/19 10:110.42 0.097 1
2,4,5-Trichlorophenol ND mg/kg 11/27/19 12:11 95-95-411/26/19 10:110.42 0.11 1
2,4,6-Trichlorophenol ND mg/kg 11/27/19 12:11 88-06-211/26/19 10:110.42 0.11 1
Surrogates
Nitrobenzene-d5 (S)62 %11/27/19 12:11 4165-60-011/26/19 10:1123-110 1
2-Fluorobiphenyl (S)65 %11/27/19 12:11 321-60-811/26/19 10:1130-110 1
Terphenyl-d14 (S)68 %11/27/19 12:11 1718-51-011/26/19 10:1128-110 1
Phenol-d6 (S)59 %11/27/19 12:11 13127-88-311/26/19 10:1122-110 1
2-Fluorophenol (S)61 %11/27/19 12:11 367-12-411/26/19 10:1113-110 1
2,4,6-Tribromophenol (S)69 %11/27/19 12:11 118-79-611/26/19 10:1127-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-5 (19-21)Lab ID: 92454745004 Collected: 11/20/19 14:50 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 12/02/19 12:37 67-64-111/27/19 12:210.11 0.011 1
Benzene ND mg/kg 12/02/19 12:37 71-43-211/27/19 12:210.0056 0.0010 1
Bromobenzene ND mg/kg 12/02/19 12:37 108-86-111/27/19 12:210.0056 0.0015 1
Bromochloromethane ND mg/kg 12/02/19 12:37 74-97-511/27/19 12:210.0056 0.0014 1
Bromodichloromethane ND mg/kg 12/02/19 12:37 75-27-411/27/19 12:210.0056 0.0011 1
Bromoform ND mg/kg 12/02/19 12:37 75-25-211/27/19 12:210.0056 0.0027 1
Bromomethane ND mg/kg 12/02/19 12:37 74-83-9 IH11/27/19 12:210.011 0.0026 1
2-Butanone (MEK)ND mg/kg 12/02/19 12:37 78-93-311/27/19 12:210.11 0.013 1
n-Butylbenzene ND mg/kg 12/02/19 12:37 104-51-811/27/19 12:210.0056 0.0031 1
sec-Butylbenzene ND mg/kg 12/02/19 12:37 135-98-811/27/19 12:210.0056 0.0024 1
tert-Butylbenzene ND mg/kg 12/02/19 12:37 98-06-611/27/19 12:210.0056 0.0019 1
Carbon tetrachloride ND mg/kg 12/02/19 12:37 56-23-511/27/19 12:210.0056 0.0011 1
Chlorobenzene ND mg/kg 12/02/19 12:37 108-90-711/27/19 12:210.0056 0.0011 1
Chloroethane ND mg/kg 12/02/19 12:37 75-00-3 IK11/27/19 12:210.011 0.0023 1
Chloroform ND mg/kg 12/02/19 12:37 67-66-311/27/19 12:210.0056 0.0012 1
Chloromethane ND mg/kg 12/02/19 12:37 74-87-311/27/19 12:210.011 0.0037 1
2-Chlorotoluene ND mg/kg 12/02/19 12:37 95-49-811/27/19 12:210.0056 0.0017 1
4-Chlorotoluene ND mg/kg 12/02/19 12:37 106-43-411/27/19 12:210.0056 0.0017 1
1,2-Dibromo-3-chloropropane ND mg/kg 12/02/19 12:37 96-12-811/27/19 12:210.0056 0.0028 1
Dibromochloromethane ND mg/kg 12/02/19 12:37 124-48-111/27/19 12:210.0056 0.0028 1
1,2-Dibromoethane (EDB)ND mg/kg 12/02/19 12:37 106-93-411/27/19 12:210.0056 0.0012 1
Dibromomethane ND mg/kg 12/02/19 12:37 74-95-311/27/19 12:210.0056 0.0017 1
1,2-Dichlorobenzene ND mg/kg 12/02/19 12:37 95-50-111/27/19 12:210.0056 0.0020 1
1,3-Dichlorobenzene ND mg/kg 12/02/19 12:37 541-73-111/27/19 12:210.0056 0.0020 1
1,4-Dichlorobenzene ND mg/kg 12/02/19 12:37 106-46-711/27/19 12:210.0056 0.0019 1
Dichlorodifluoromethane ND mg/kg 12/02/19 12:37 75-71-811/27/19 12:210.011 0.0046 1
1,1-Dichloroethane ND mg/kg 12/02/19 12:37 75-34-311/27/19 12:210.0056 0.00082 1
1,2-Dichloroethane ND mg/kg 12/02/19 12:37 107-06-211/27/19 12:210.0056 0.0011 1
1,1-Dichloroethene ND mg/kg 12/02/19 12:37 75-35-411/27/19 12:210.0056 0.0013 1
cis-1,2-Dichloroethene ND mg/kg 12/02/19 12:37 156-59-211/27/19 12:210.0056 0.00097 1
trans-1,2-Dichloroethene ND mg/kg 12/02/19 12:37 156-60-511/27/19 12:210.0056 0.0011 1
1,2-Dichloropropane ND mg/kg 12/02/19 12:37 78-87-511/27/19 12:210.0056 0.0021 1
1,3-Dichloropropane ND mg/kg 12/02/19 12:37 142-28-911/27/19 12:210.0056 0.0021 1
2,2-Dichloropropane ND mg/kg 12/02/19 12:37 594-20-711/27/19 12:210.0056 0.00055 1
1,1-Dichloropropene ND mg/kg 12/02/19 12:37 563-58-611/27/19 12:210.0056 0.0024 1
cis-1,3-Dichloropropene ND mg/kg 12/02/19 12:37 10061-01-511/27/19 12:210.0056 0.0025 1
trans-1,3-Dichloropropene ND mg/kg 12/02/19 12:37 10061-02-611/27/19 12:210.0056 0.00097 1
Diisopropyl ether ND mg/kg 12/02/19 12:37 108-20-311/27/19 12:210.0056 0.0032 1
Ethylbenzene ND mg/kg 12/02/19 12:37 100-41-411/27/19 12:210.0056 0.0012 1
Hexachloro-1,3-butadiene ND mg/kg 12/02/19 12:37 87-68-311/27/19 12:210.0056 0.0028 1
2-Hexanone ND mg/kg 12/02/19 12:37 591-78-611/27/19 12:210.056 0.0058 1
Isopropylbenzene (Cumene)ND mg/kg 12/02/19 12:37 98-82-811/27/19 12:210.0056 0.0016 1
p-Isopropyltoluene ND mg/kg 12/02/19 12:37 99-87-611/27/19 12:210.0056 0.0027 1
Methylene Chloride ND mg/kg 12/02/19 12:37 75-09-2 IH11/27/19 12:210.022 0.0066 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 12/02/19 12:37 108-10-111/27/19 12:210.056 0.0042 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: SB-5 (19-21)Lab ID: 92454745004 Collected: 11/20/19 14:50 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 12/02/19 12:37 1634-04-411/27/19 12:210.0056 0.0032 1
Naphthalene ND mg/kg 12/02/19 12:37 91-20-311/27/19 12:210.0056 0.0047 1
n-Propylbenzene ND mg/kg 12/02/19 12:37 103-65-111/27/19 12:210.0056 0.0019 1
Styrene ND mg/kg 12/02/19 12:37 100-42-511/27/19 12:210.0056 0.0016 1
1,1,1,2-Tetrachloroethane ND mg/kg 12/02/19 12:37 630-20-611/27/19 12:210.0056 0.0014 1
1,1,2,2-Tetrachloroethane ND mg/kg 12/02/19 12:37 79-34-511/27/19 12:210.0056 0.0019 1
Tetrachloroethene ND mg/kg 12/02/19 12:37 127-18-411/27/19 12:210.0056 0.0018 1
Toluene ND mg/kg 12/02/19 12:37 108-88-311/27/19 12:210.0056 0.0018 1
1,2,3-Trichlorobenzene ND mg/kg 12/02/19 12:37 87-61-611/27/19 12:210.0056 0.0040 1
1,2,4-Trichlorobenzene ND mg/kg 12/02/19 12:37 120-82-111/27/19 12:210.0056 0.0030 1
1,1,1-Trichloroethane ND mg/kg 12/02/19 12:37 71-55-611/27/19 12:210.0056 0.00097 1
1,1,2-Trichloroethane ND mg/kg 12/02/19 12:37 79-00-511/27/19 12:210.0056 0.0013 1
Trichloroethene ND mg/kg 12/02/19 12:37 79-01-611/27/19 12:210.0056 0.0014 1
Trichlorofluoromethane ND mg/kg 12/02/19 12:37 75-69-411/27/19 12:210.0056 0.0013 1
1,2,3-Trichloropropane ND mg/kg 12/02/19 12:37 96-18-411/27/19 12:210.0056 0.0019 1
1,2,4-Trimethylbenzene ND mg/kg 12/02/19 12:37 95-63-611/27/19 12:210.0056 0.0022 1
1,3,5-Trimethylbenzene ND mg/kg 12/02/19 12:37 108-67-811/27/19 12:210.0056 0.0019 1
Vinyl acetate ND mg/kg 12/02/19 12:37 108-05-411/27/19 12:210.056 0.018 1
Vinyl chloride ND mg/kg 12/02/19 12:37 75-01-411/27/19 12:210.011 0.0021 1
Xylene (Total)ND mg/kg 12/02/19 12:37 1330-20-711/27/19 12:210.011 0.0039 1
m&p-Xylene ND mg/kg 12/02/19 12:37 179601-23-111/27/19 12:210.011 0.0026 1
o-Xylene ND mg/kg 12/02/19 12:37 95-47-611/27/19 12:210.0056 0.0013 1
Surrogates
Toluene-d8 (S)107 %12/02/19 12:37 2037-26-511/27/19 12:2170-130 1
4-Bromofluorobenzene (S)104 %12/02/19 12:37 460-00-411/27/19 12:2170-130 1
1,2-Dichloroethane-d4 (S)106 %12/02/19 12:37 17060-07-011/27/19 12:2170-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)ND mg/kg 11/25/19 14:57 123-91-111/25/19 11:520.011 0.0032 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %11/25/19 14:57 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)101 %11/25/19 14:57 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.5 %11/22/19 13:280.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: DUP-1-SOIL Lab ID: 92454745005 Collected: 11/20/19 00:00 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic ND mg/kg 11/26/19 19:35 7440-38-211/25/19 12:161.2 0.61 1
Barium 64.0 mg/kg 11/26/19 19:35 7440-39-311/25/19 12:160.61 0.31 1
Cadmium ND mg/kg 11/26/19 19:35 7440-43-911/25/19 12:160.12 0.061 1
Chromium 13.2 mg/kg 11/26/19 19:35 7440-47-311/25/19 12:160.61 0.31 1
Lead 1.6 mg/kg 11/26/19 19:35 7439-92-111/25/19 12:160.61 0.31 1
Selenium 0.63J mg/kg 11/26/19 19:35 7782-49-211/25/19 12:161.2 0.61 1
Silver ND mg/kg 11/26/19 19:35 7440-22-411/25/19 12:160.61 0.31 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.0029 mg/kg 11/22/19 15:38 7439-97-611/22/19 11:500.0027 0.0013 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/27/19 12:46 83-32-911/26/19 10:110.43 0.11 1
Acenaphthylene ND mg/kg 11/27/19 12:46 208-96-811/26/19 10:110.43 0.10 1
Aniline ND mg/kg 11/27/19 12:46 62-53-311/26/19 10:110.43 0.097 1
Anthracene ND mg/kg 11/27/19 12:46 120-12-711/26/19 10:110.43 0.11 1
Benzo(a)anthracene ND mg/kg 11/27/19 12:46 56-55-311/26/19 10:110.43 0.14 1
Benzo(a)pyrene ND mg/kg 11/27/19 12:46 50-32-811/26/19 10:110.43 0.19 1
Benzo(b)fluoranthene ND mg/kg 11/27/19 12:46 205-99-211/26/19 10:110.43 0.17 1
Benzo(g,h,i)perylene ND mg/kg 11/27/19 12:46 191-24-211/26/19 10:110.43 0.17 1
Benzo(k)fluoranthene ND mg/kg 11/27/19 12:46 207-08-911/26/19 10:110.43 0.18 1
Benzoic Acid ND mg/kg 11/27/19 12:46 65-85-011/26/19 10:112.2 0.46 1
Benzyl alcohol ND mg/kg 11/27/19 12:46 100-51-611/26/19 10:110.86 0.23 1
4-Bromophenylphenyl ether ND mg/kg 11/27/19 12:46 101-55-311/26/19 10:110.43 0.11 1
Butylbenzylphthalate ND mg/kg 11/27/19 12:46 85-68-711/26/19 10:110.43 0.11 1
4-Chloro-3-methylphenol ND mg/kg 11/27/19 12:46 59-50-711/26/19 10:110.86 0.26 1
4-Chloroaniline ND mg/kg 11/27/19 12:46 106-47-811/26/19 10:112.2 0.26 1
bis(2-Chloroethoxy)methane ND mg/kg 11/27/19 12:46 111-91-111/26/19 10:110.43 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 11/27/19 12:46 111-44-411/26/19 10:110.43 0.091 1
2-Chloronaphthalene ND mg/kg 11/27/19 12:46 91-58-711/26/19 10:110.43 0.096 1
2-Chlorophenol ND mg/kg 11/27/19 12:46 95-57-811/26/19 10:110.43 0.10 1
4-Chlorophenylphenyl ether ND mg/kg 11/27/19 12:46 7005-72-311/26/19 10:110.43 0.11 1
Chrysene ND mg/kg 11/27/19 12:46 218-01-911/26/19 10:110.43 0.12 1
Dibenz(a,h)anthracene ND mg/kg 11/27/19 12:46 53-70-311/26/19 10:110.43 0.17 1
Dibenzofuran ND mg/kg 11/27/19 12:46 132-64-911/26/19 10:110.43 0.11 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 12:46 95-50-111/26/19 10:110.43 0.093 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 12:46 541-73-111/26/19 10:110.43 0.097 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 12:46 106-46-711/26/19 10:110.43 0.095 1
3,3'-Dichlorobenzidine ND mg/kg 11/27/19 12:46 91-94-111/26/19 10:112.2 0.30 1
2,4-Dichlorophenol ND mg/kg 11/27/19 12:46 120-83-211/26/19 10:110.43 0.14 1
Diethylphthalate ND mg/kg 11/27/19 12:46 84-66-211/26/19 10:110.43 0.093 1
2,4-Dimethylphenol ND mg/kg 11/27/19 12:46 105-67-911/26/19 10:110.43 0.11 1
Dimethylphthalate ND mg/kg 11/27/19 12:46 131-11-311/26/19 10:110.43 0.097 1
Di-n-butylphthalate ND mg/kg 11/27/19 12:46 84-74-211/26/19 10:110.43 0.11 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/27/19 12:46 534-52-111/26/19 10:110.86 0.69 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: DUP-1-SOIL Lab ID: 92454745005 Collected: 11/20/19 00:00 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/27/19 12:46 51-28-511/26/19 10:112.2 1.4 1
2,4-Dinitrotoluene ND mg/kg 11/27/19 12:46 121-14-211/26/19 10:110.43 0.11 1
2,6-Dinitrotoluene ND mg/kg 11/27/19 12:46 606-20-211/26/19 10:110.43 0.11 1
Di-n-octylphthalate ND mg/kg 11/27/19 12:46 117-84-011/26/19 10:110.43 0.25 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/27/19 12:46 117-81-711/26/19 10:110.43 0.14 1
Fluoranthene ND mg/kg 11/27/19 12:46 206-44-011/26/19 10:110.43 0.13 1
Fluorene ND mg/kg 11/27/19 12:46 86-73-711/26/19 10:110.43 0.12 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 12:46 87-68-311/26/19 10:110.43 0.10 1
Hexachlorobenzene ND mg/kg 11/27/19 12:46 118-74-111/26/19 10:110.43 0.11 1
Hexachlorocyclopentadiene ND mg/kg 11/27/19 12:46 77-47-411/26/19 10:110.43 0.17 1
Hexachloroethane ND mg/kg 11/27/19 12:46 67-72-111/26/19 10:110.43 0.098 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/27/19 12:46 193-39-511/26/19 10:110.43 0.20 1
Isophorone ND mg/kg 11/27/19 12:46 78-59-111/26/19 10:110.43 0.094 1
1-Methylnaphthalene ND mg/kg 11/27/19 12:46 90-12-011/26/19 10:110.43 0.11 1
2-Methylnaphthalene ND mg/kg 11/27/19 12:46 91-57-611/26/19 10:110.43 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 11/27/19 12:46 95-48-711/26/19 10:110.43 0.095 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/27/19 12:46 15831-10-411/26/19 10:110.43 0.11 1
Naphthalene ND mg/kg 11/27/19 12:46 91-20-311/26/19 10:110.43 0.10 1
2-Nitroaniline ND mg/kg 11/27/19 12:46 88-74-411/26/19 10:112.2 0.22 1
3-Nitroaniline ND mg/kg 11/27/19 12:46 99-09-211/26/19 10:112.2 0.23 1
4-Nitroaniline ND mg/kg 11/27/19 12:46 100-01-611/26/19 10:110.86 0.21 1
Nitrobenzene ND mg/kg 11/27/19 12:46 98-95-311/26/19 10:110.43 0.10 1
2-Nitrophenol ND mg/kg 11/27/19 12:46 88-75-511/26/19 10:110.43 0.13 1
4-Nitrophenol ND mg/kg 11/27/19 12:46 100-02-711/26/19 10:112.2 0.69 1
N-Nitrosodimethylamine ND mg/kg 11/27/19 12:46 62-75-911/26/19 10:110.43 0.12 1
N-Nitroso-di-n-propylamine ND mg/kg 11/27/19 12:46 621-64-711/26/19 10:110.43 0.12 1
N-Nitrosodiphenylamine ND mg/kg 11/27/19 12:46 86-30-611/26/19 10:110.43 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/27/19 12:46 108-60-111/26/19 10:110.43 0.12 1
Pentachlorophenol ND mg/kg 11/27/19 12:46 87-86-511/26/19 10:112.2 0.20 1
Phenanthrene ND mg/kg 11/27/19 12:46 85-01-811/26/19 10:110.43 0.11 1
Phenol ND mg/kg 11/27/19 12:46 108-95-211/26/19 10:110.43 0.10 1
Pyrene ND mg/kg 11/27/19 12:46 129-00-011/26/19 10:110.43 0.12 1
Pyridine ND mg/kg 11/27/19 12:46 110-86-111/26/19 10:110.43 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 12:46 120-82-111/26/19 10:110.43 0.099 1
2,4,5-Trichlorophenol ND mg/kg 11/27/19 12:46 95-95-411/26/19 10:110.43 0.11 1
2,4,6-Trichlorophenol ND mg/kg 11/27/19 12:46 88-06-211/26/19 10:110.43 0.11 1
Surrogates
Nitrobenzene-d5 (S)59 %11/27/19 12:46 4165-60-011/26/19 10:1123-110 1
2-Fluorobiphenyl (S)62 %11/27/19 12:46 321-60-811/26/19 10:1130-110 1
Terphenyl-d14 (S)66 %11/27/19 12:46 1718-51-011/26/19 10:1128-110 1
Phenol-d6 (S)56 %11/27/19 12:46 13127-88-311/26/19 10:1122-110 1
2-Fluorophenol (S)58 %11/27/19 12:46 367-12-411/26/19 10:1113-110 1
2,4,6-Tribromophenol (S)66 %11/27/19 12:46 118-79-611/26/19 10:1127-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: DUP-1-SOIL Lab ID: 92454745005 Collected: 11/20/19 00:00 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 11/27/19 17:18 67-64-111/27/19 12:210.12 0.011 1
Benzene ND mg/kg 11/27/19 17:18 71-43-211/27/19 12:210.0059 0.0011 1
Bromobenzene ND mg/kg 11/27/19 17:18 108-86-111/27/19 12:210.0059 0.0016 1
Bromochloromethane ND mg/kg 11/27/19 17:18 74-97-511/27/19 12:210.0059 0.0015 1
Bromodichloromethane ND mg/kg 11/27/19 17:18 75-27-411/27/19 12:210.0059 0.0012 1
Bromoform ND mg/kg 11/27/19 17:18 75-25-211/27/19 12:210.0059 0.0029 1
Bromomethane ND mg/kg 11/27/19 17:18 74-83-9 IH11/27/19 12:210.012 0.0028 1
2-Butanone (MEK)ND mg/kg 11/27/19 17:18 78-93-311/27/19 12:210.12 0.014 1
n-Butylbenzene ND mg/kg 11/27/19 17:18 104-51-811/27/19 12:210.0059 0.0033 1
sec-Butylbenzene ND mg/kg 11/27/19 17:18 135-98-811/27/19 12:210.0059 0.0025 1
tert-Butylbenzene ND mg/kg 11/27/19 17:18 98-06-6 v211/27/19 12:210.0059 0.0020 1
Carbon tetrachloride ND mg/kg 11/27/19 17:18 56-23-511/27/19 12:210.0059 0.0011 1
Chlorobenzene ND mg/kg 11/27/19 17:18 108-90-711/27/19 12:210.0059 0.0011 1
Chloroethane ND mg/kg 11/27/19 17:18 75-00-3 IK11/27/19 12:210.012 0.0025 1
Chloroform ND mg/kg 11/27/19 17:18 67-66-311/27/19 12:210.0059 0.0013 1
Chloromethane ND mg/kg 11/27/19 17:18 74-87-311/27/19 12:210.012 0.0039 1
2-Chlorotoluene ND mg/kg 11/27/19 17:18 95-49-811/27/19 12:210.0059 0.0018 1
4-Chlorotoluene ND mg/kg 11/27/19 17:18 106-43-411/27/19 12:210.0059 0.0018 1
1,2-Dibromo-3-chloropropane ND mg/kg 11/27/19 17:18 96-12-811/27/19 12:210.0059 0.0030 1
Dibromochloromethane ND mg/kg 11/27/19 17:18 124-48-111/27/19 12:210.0059 0.0030 1
1,2-Dibromoethane (EDB)ND mg/kg 11/27/19 17:18 106-93-411/27/19 12:210.0059 0.0013 1
Dibromomethane ND mg/kg 11/27/19 17:18 74-95-311/27/19 12:210.0059 0.0018 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 17:18 95-50-111/27/19 12:210.0059 0.0021 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 17:18 541-73-111/27/19 12:210.0059 0.0021 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 17:18 106-46-711/27/19 12:210.0059 0.0021 1
Dichlorodifluoromethane ND mg/kg 11/27/19 17:18 75-71-811/27/19 12:210.012 0.0049 1
1,1-Dichloroethane ND mg/kg 11/27/19 17:18 75-34-311/27/19 12:210.0059 0.00087 1
1,2-Dichloroethane ND mg/kg 11/27/19 17:18 107-06-211/27/19 12:210.0059 0.0012 1
1,1-Dichloroethene ND mg/kg 11/27/19 17:18 75-35-411/27/19 12:210.0059 0.0014 1
cis-1,2-Dichloroethene ND mg/kg 11/27/19 17:18 156-59-211/27/19 12:210.0059 0.0010 1
trans-1,2-Dichloroethene ND mg/kg 11/27/19 17:18 156-60-511/27/19 12:210.0059 0.0012 1
1,2-Dichloropropane ND mg/kg 11/27/19 17:18 78-87-511/27/19 12:210.0059 0.0022 1
1,3-Dichloropropane ND mg/kg 11/27/19 17:18 142-28-911/27/19 12:210.0059 0.0022 1
2,2-Dichloropropane ND mg/kg 11/27/19 17:18 594-20-711/27/19 12:210.0059 0.00059 1
1,1-Dichloropropene ND mg/kg 11/27/19 17:18 563-58-611/27/19 12:210.0059 0.0025 1
cis-1,3-Dichloropropene ND mg/kg 11/27/19 17:18 10061-01-511/27/19 12:210.0059 0.0027 1
trans-1,3-Dichloropropene ND mg/kg 11/27/19 17:18 10061-02-611/27/19 12:210.0059 0.0010 1
Diisopropyl ether ND mg/kg 11/27/19 17:18 108-20-311/27/19 12:210.0059 0.0034 1
Ethylbenzene ND mg/kg 11/27/19 17:18 100-41-411/27/19 12:210.0059 0.0013 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 17:18 87-68-311/27/19 12:210.0059 0.0029 1
2-Hexanone ND mg/kg 11/27/19 17:18 591-78-611/27/19 12:210.059 0.0061 1
Isopropylbenzene (Cumene)ND mg/kg 11/27/19 17:18 98-82-811/27/19 12:210.0059 0.0017 1
p-Isopropyltoluene ND mg/kg 11/27/19 17:18 99-87-611/27/19 12:210.0059 0.0029 1
Methylene Chloride ND mg/kg 11/27/19 17:18 75-09-2 IH,v111/27/19 12:210.024 0.0070 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 11/27/19 17:18 108-10-111/27/19 12:210.059 0.0044 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: DUP-1-SOIL Lab ID: 92454745005 Collected: 11/20/19 00:00 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 11/27/19 17:18 1634-04-411/27/19 12:210.0059 0.0034 1
Naphthalene ND mg/kg 11/27/19 17:18 91-20-311/27/19 12:210.0059 0.0050 1
n-Propylbenzene ND mg/kg 11/27/19 17:18 103-65-111/27/19 12:210.0059 0.0020 1
Styrene ND mg/kg 11/27/19 17:18 100-42-511/27/19 12:210.0059 0.0018 1
1,1,1,2-Tetrachloroethane ND mg/kg 11/27/19 17:18 630-20-611/27/19 12:210.0059 0.0015 1
1,1,2,2-Tetrachloroethane ND mg/kg 11/27/19 17:18 79-34-511/27/19 12:210.0059 0.0021 1
Tetrachloroethene ND mg/kg 11/27/19 17:18 127-18-411/27/19 12:210.0059 0.0019 1
Toluene ND mg/kg 11/27/19 17:18 108-88-311/27/19 12:210.0059 0.0019 1
1,2,3-Trichlorobenzene ND mg/kg 11/27/19 17:18 87-61-611/27/19 12:210.0059 0.0042 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 17:18 120-82-111/27/19 12:210.0059 0.0031 1
1,1,1-Trichloroethane ND mg/kg 11/27/19 17:18 71-55-611/27/19 12:210.0059 0.0010 1
1,1,2-Trichloroethane ND mg/kg 11/27/19 17:18 79-00-511/27/19 12:210.0059 0.0013 1
Trichloroethene ND mg/kg 11/27/19 17:18 79-01-611/27/19 12:210.0059 0.0015 1
Trichlorofluoromethane ND mg/kg 11/27/19 17:18 75-69-411/27/19 12:210.0059 0.0014 1
1,2,3-Trichloropropane ND mg/kg 11/27/19 17:18 96-18-411/27/19 12:210.0059 0.0020 1
1,2,4-Trimethylbenzene ND mg/kg 11/27/19 17:18 95-63-611/27/19 12:210.0059 0.0023 1
1,3,5-Trimethylbenzene ND mg/kg 11/27/19 17:18 108-67-811/27/19 12:210.0059 0.0020 1
Vinyl acetate ND mg/kg 11/27/19 17:18 108-05-411/27/19 12:210.059 0.019 1
Vinyl chloride ND mg/kg 11/27/19 17:18 75-01-411/27/19 12:210.012 0.0023 1
Xylene (Total)ND mg/kg 11/27/19 17:18 1330-20-711/27/19 12:210.012 0.0042 1
m&p-Xylene ND mg/kg 11/27/19 17:18 179601-23-111/27/19 12:210.012 0.0028 1
o-Xylene ND mg/kg 11/27/19 17:18 95-47-611/27/19 12:210.0059 0.0014 1
Surrogates
Toluene-d8 (S)112 %11/27/19 17:18 2037-26-511/27/19 12:2170-130 1
4-Bromofluorobenzene (S)109 %11/27/19 17:18 460-00-411/27/19 12:2170-130 1
1,2-Dichloroethane-d4 (S)97 %11/27/19 17:18 17060-07-011/27/19 12:2170-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)ND mg/kg 11/25/19 15:17 123-91-111/25/19 11:520.013 0.0038 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %11/25/19 15:17 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)104 %11/25/19 15:17 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.8 %11/22/19 13:280.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: TRIP BLANK Lab ID: 92454745006 Collected: 11/20/19 00:00 Received: 11/21/19 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 11/27/19 17:00 67-64-125.0 6.2 1
Benzene ND ug/L 11/27/19 17:00 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/27/19 17:00 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/27/19 17:00 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/27/19 17:00 75-27-41.0 0.26 1
Bromoform ND ug/L 11/27/19 17:00 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/27/19 17:00 74-83-9 IH,L12.0 0.62 1
2-Butanone (MEK)ND ug/L 11/27/19 17:00 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/27/19 17:00 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/27/19 17:00 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/27/19 17:00 75-00-31.0 0.49 1
Chloroform ND ug/L 11/27/19 17:00 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/27/19 17:00 74-87-3 IK1.0 0.39 1
2-Chlorotoluene ND ug/L 11/27/19 17:00 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/27/19 17:00 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/27/19 17:00 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/27/19 17:00 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/27/19 17:00 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/27/19 17:00 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/27/19 17:00 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/27/19 17:00 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/27/19 17:00 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/27/19 17:00 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/27/19 17:00 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/27/19 17:00 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/27/19 17:00 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 11/27/19 17:00 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/27/19 17:00 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/27/19 17:00 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/27/19 17:00 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/27/19 17:00 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/27/19 17:00 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/27/19 17:00 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/27/19 17:00 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/27/19 17:00 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/27/19 17:00 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/27/19 17:00 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/27/19 17:00 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/27/19 17:00 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/27/19 17:00 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/27/19 17:00 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/27/19 17:00 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/27/19 17:00 91-20-31.0 0.35 1
Styrene ND ug/L 11/27/19 17:00 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/27/19 17:00 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 11/27/19 17:00 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454745
ROW-603
Sample: TRIP BLANK Lab ID: 92454745006 Collected: 11/20/19 00:00 Received: 11/21/19 10:37 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 11/27/19 17:00 127-18-41.0 0.16 1
Toluene ND ug/L 11/27/19 17:00 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/27/19 17:00 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/27/19 17:00 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/27/19 17:00 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/27/19 17:00 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/27/19 17:00 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/27/19 17:00 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/27/19 17:00 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/27/19 17:00 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/27/19 17:00 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/27/19 17:00 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/27/19 17:00 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/27/19 17:00 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)101 %11/27/19 17:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %11/27/19 17:00 17060-07-070-130 1
Toluene-d8 (S)89 %11/27/19 17:00 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/23/19 20:02 123-91-12.0 1.2 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %11/23/19 20:02 17060-07-050-150 1
Toluene-d8 (S)105 %11/23/19 20:02 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511178
EPA 7471B
EPA 7471B
7471 Mercury
Associated Lab Samples: 92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2742192
Associated Lab Samples:92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 11/22/19 14:420.0030
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2742193LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0770.083 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2742194MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454639001
2742195
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.042 88 75-12580 12 200.041ND 0.040 0.035
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511524
EPA 3050B
EPA 6010D
6010 MET
Associated Lab Samples: 92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743755
Associated Lab Samples:92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Matrix: Solid
AnalyzedMDL
Arsenic mg/kg ND 1.0 11/26/19 19:080.50
Barium mg/kg ND 0.50 11/26/19 19:080.25
Cadmium mg/kg ND 0.10 11/26/19 19:080.050
Chromium mg/kg ND 0.50 11/26/19 19:080.25
Lead mg/kg ND 0.50 11/26/19 19:080.25
Selenium mg/kg ND 1.0 11/26/19 19:080.50
Silver mg/kg ND 0.50 11/26/19 19:080.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743756LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 48.950 98 80-120
Barium mg/kg 49.550 99 80-120
Cadmium mg/kg 49.150 98 80-120
Chromium mg/kg 49.650 99 80-120
Lead mg/kg 48.550 97 80-120
Selenium mg/kg 46.750 93 80-120
Silver mg/kg 24.625 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2743757MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454745001
2743758
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 51 88 75-12587 2 2051ND45.2 44.4
Barium mg/kg M151-40 75-12579 16 2051366346 406
Cadmium mg/kg 51 89 75-12586 4 20510.073J 45.2 43.6
Chromium mg/kg 51 84 75-12584 0 205114.5 57.4 57.4
Lead mg/kg 51 86 75-12583 3 20511.3 45.1 43.6
Selenium mg/kg 51 85 75-12580 7 2051ND43.2 40.5
Silver mg/kg 25.4 102 75-12599 2 2025.4ND 25.9 25.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512117
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2746337
Associated Lab Samples:92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 11/27/19 10:530.0012
1,1,1-Trichloroethane mg/kg ND 0.0050 11/27/19 10:530.00087
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 11/27/19 10:530.0017
1,1,2-Trichloroethane mg/kg ND 0.0050 11/27/19 10:530.0011
1,1-Dichloroethane mg/kg ND 0.0050 11/27/19 10:530.00074
1,1-Dichloroethene mg/kg ND 0.0050 11/27/19 10:530.0012
1,1-Dichloropropene mg/kg ND 0.0050 11/27/19 10:530.0021
1,2,3-Trichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0036
1,2,3-Trichloropropane mg/kg ND 0.0050 11/27/19 10:530.0017
1,2,4-Trichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0026
1,2,4-Trimethylbenzene mg/kg ND 0.0050 11/27/19 10:530.0020
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 11/27/19 10:530.0025
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 11/27/19 10:530.0011
1,2-Dichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0018
1,2-Dichloroethane mg/kg ND 0.0050 11/27/19 10:530.0010
1,2-Dichloropropane mg/kg ND 0.0050 11/27/19 10:530.0019
1,3,5-Trimethylbenzene mg/kg ND 0.0050 11/27/19 10:530.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0018
1,3-Dichloropropane mg/kg ND 0.0050 11/27/19 10:530.0019
1,4-Dichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0017
2,2-Dichloropropane mg/kg ND 0.0050 11/27/19 10:530.00049
2-Butanone (MEK)mg/kg ND 0.10 11/27/19 10:530.012
2-Chlorotoluene mg/kg ND 0.0050 11/27/19 10:530.0015
2-Hexanone mg/kg ND 0.050 11/27/19 10:530.0052
4-Chlorotoluene mg/kg ND 0.0050 11/27/19 10:530.0015
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 11/27/19 10:530.0037
Acetone mg/kg ND 0.10 11/27/19 10:530.0094
Benzene mg/kg ND 0.0050 11/27/19 10:530.00090
Bromobenzene mg/kg ND 0.0050 11/27/19 10:530.0014
Bromochloromethane mg/kg ND 0.0050 11/27/19 10:530.0012
Bromodichloromethane mg/kg ND 0.0050 11/27/19 10:530.00098
Bromoform mg/kg ND 0.0050 11/27/19 10:530.0024
Bromomethane mg/kg ND 0.010 IH11/27/19 10:530.0024
Carbon tetrachloride mg/kg ND 0.0050 11/27/19 10:530.00096
Chlorobenzene mg/kg ND 0.0050 11/27/19 10:530.00097
Chloroethane mg/kg ND 0.010 IK11/27/19 10:530.0021
Chloroform mg/kg ND 0.0050 11/27/19 10:530.0011
Chloromethane mg/kg ND 0.010 11/27/19 10:530.0033
cis-1,2-Dichloroethene mg/kg ND 0.0050 11/27/19 10:530.00087
cis-1,3-Dichloropropene mg/kg ND 0.0050 11/27/19 10:530.0023
Dibromochloromethane mg/kg ND 0.0050 11/27/19 10:530.0025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2746337
Associated Lab Samples:92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Matrix: Solid
AnalyzedMDL
Dibromomethane mg/kg ND 0.0050 11/27/19 10:530.0015
Dichlorodifluoromethane mg/kg ND 0.010 11/27/19 10:530.0041
Diisopropyl ether mg/kg ND 0.0050 11/27/19 10:530.0029
Ethylbenzene mg/kg ND 0.0050 11/27/19 10:530.0011
Hexachloro-1,3-butadiene mg/kg ND 0.0050 11/27/19 10:530.0025
Isopropylbenzene (Cumene)mg/kg ND 0.0050 11/27/19 10:530.0014
m&p-Xylene mg/kg ND 0.010 11/27/19 10:530.0024
Methyl-tert-butyl ether mg/kg ND 0.0050 11/27/19 10:530.0029
Methylene Chloride mg/kg 0.014J 0.020 IH,v111/27/19 10:530.0059
n-Butylbenzene mg/kg ND 0.0050 11/27/19 10:530.0028
n-Propylbenzene mg/kg ND 0.0050 11/27/19 10:530.0017
Naphthalene mg/kg ND 0.0050 11/27/19 10:530.0042
o-Xylene mg/kg ND 0.0050 11/27/19 10:530.0012
p-Isopropyltoluene mg/kg ND 0.0050 11/27/19 10:530.0024
sec-Butylbenzene mg/kg ND 0.0050 11/27/19 10:530.0021
Styrene mg/kg ND 0.0050 11/27/19 10:530.0015
tert-Butylbenzene mg/kg ND 0.0050 v211/27/19 10:530.0017
Tetrachloroethene mg/kg ND 0.0050 11/27/19 10:530.0016
Toluene mg/kg ND 0.0050 11/27/19 10:530.0016
trans-1,2-Dichloroethene mg/kg ND 0.0050 11/27/19 10:530.00098
trans-1,3-Dichloropropene mg/kg ND 0.0050 11/27/19 10:530.00088
Trichloroethene mg/kg ND 0.0050 11/27/19 10:530.0013
Trichlorofluoromethane mg/kg ND 0.0050 11/27/19 10:530.0012
Vinyl acetate mg/kg ND 0.050 11/27/19 10:530.016
Vinyl chloride mg/kg ND 0.010 11/27/19 10:530.0019
Xylene (Total)mg/kg ND 0.010 11/27/19 10:530.0035
1,2-Dichloroethane-d4 (S)%95 70-132 11/27/19 10:53
4-Bromofluorobenzene (S)%105 70-130 11/27/19 10:53
Toluene-d8 (S)%105 70-130 11/27/19 10:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746338LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.0500.05 100 70-130
1,1,1-Trichloroethane mg/kg 0.0500.05 101 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.0490.05 98 55-130
1,1,2-Trichloroethane mg/kg 0.0490.05 98 70-130
1,1-Dichloroethane mg/kg 0.0470.05 93 68-130
1,1-Dichloroethene mg/kg 0.0490.05 98 70-130
1,1-Dichloropropene mg/kg 0.0540.05 109 70-130
1,2,3-Trichlorobenzene mg/kg 0.0460.05 93 70-130
1,2,3-Trichloropropane mg/kg 0.0500.05 99 70-130
1,2,4-Trichlorobenzene mg/kg 0.0470.05 93 70-130
1,2,4-Trimethylbenzene mg/kg 0.0480.05 96 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746338LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane mg/kg 0.0490.05 99 57-141
1,2-Dibromoethane (EDB)mg/kg 0.0500.05 100 70-130
1,2-Dichlorobenzene mg/kg 0.0460.05 92 70-130
1,2-Dichloroethane mg/kg 0.0460.05 92 70-130
1,2-Dichloropropane mg/kg 0.0480.05 96 70-130
1,3,5-Trimethylbenzene mg/kg 0.0480.05 96 70-130
1,3-Dichlorobenzene mg/kg 0.0480.05 95 70-130
1,3-Dichloropropane mg/kg 0.0500.05 100 70-130
1,4-Dichlorobenzene mg/kg 0.0470.05 94 70-130
2,2-Dichloropropane mg/kg 0.0500.05 101 70-130
2-Butanone (MEK)mg/kg 0.10J0.1 100 60-130
2-Chlorotoluene mg/kg 0.0490.05 97 70-130
2-Hexanone mg/kg 0.100.1 105 70-132
4-Chlorotoluene mg/kg 0.0480.05 96 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.100.1 102 69-130
Acetone mg/kg 0.095J0.1 95 49-148
Benzene mg/kg 0.0500.05 99 70-130
Bromobenzene mg/kg 0.0470.05 95 70-130
Bromochloromethane mg/kg 0.0440.05 87 70-130
Bromodichloromethane mg/kg 0.0480.05 97 70-130
Bromoform mg/kg 0.0500.05 100 68-136
Bromomethane mg/kg 0.055 IH0.05 110 60-140
Carbon tetrachloride mg/kg 0.0510.05 101 70-130
Chlorobenzene mg/kg 0.0490.05 98 70-130
Chloroethane mg/kg 0.057 IK0.05 114 51-147
Chloroform mg/kg 0.0460.05 93 70-130
Chloromethane mg/kg 0.0530.05 106 48-130
cis-1,2-Dichloroethene mg/kg 0.0460.05 93 70-130
cis-1,3-Dichloropropene mg/kg 0.0490.05 98 70-130
Dibromochloromethane mg/kg 0.0510.05 102 70-130
Dibromomethane mg/kg 0.0460.05 91 70-130
Dichlorodifluoromethane mg/kg 0.0540.05 109 49-130
Diisopropyl ether mg/kg 0.0480.05 96 66-130
Ethylbenzene mg/kg 0.0500.05 100 70-130
Hexachloro-1,3-butadiene mg/kg 0.0490.05 99 70-130
Isopropylbenzene (Cumene)mg/kg 0.0510.05 102 70-130
m&p-Xylene mg/kg 0.100.1 100 70-130
Methyl-tert-butyl ether mg/kg 0.0490.05 98 70-130
Methylene Chloride mg/kg 0.064 IH,v10.05 128 50-137
n-Butylbenzene mg/kg 0.0490.05 98 70-130
n-Propylbenzene mg/kg 0.0500.05 100 70-130
Naphthalene mg/kg 0.0470.05 94 70-131
o-Xylene mg/kg 0.0500.05 100 70-130
p-Isopropyltoluene mg/kg 0.0490.05 99 70-130
sec-Butylbenzene mg/kg 0.0500.05 100 70-130
Styrene mg/kg 0.0500.05 99 70-130
tert-Butylbenzene mg/kg 0.050 v30.05 100 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746338LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene mg/kg 0.0510.05 102 56-130
Toluene mg/kg 0.0470.05 93 70-130
trans-1,2-Dichloroethene mg/kg 0.0470.05 94 70-130
trans-1,3-Dichloropropene mg/kg 0.0500.05 100 70-130
Trichloroethene mg/kg 0.0520.05 104 70-141
Trichlorofluoromethane mg/kg 0.0570.05 114 67-130
Vinyl acetate mg/kg 0.0960.1 96 10-136
Vinyl chloride mg/kg 0.0550.05 109 67-130
Xylene (Total)mg/kg 0.150.15 100 70-130
1,2-Dichloroethane-d4 (S)%95 70-132
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2746340MATRIX SPIKE SAMPLE:
MSSpike
Result
92454745002
1,1,1,2-Tetrachloroethane mg/kg 0.00900.016 56 52-133ND
1,1,1-Trichloroethane mg/kg 0.00840.016 52 49-137ND
1,1,2,2-Tetrachloroethane mg/kg 0.0120.016 72 39-150ND
1,1,2-Trichloroethane mg/kg 0.0110.016 70 48-140ND
1,1-Dichloroethane mg/kg 0.00960.016 60 46-135ND
1,1-Dichloroethene mg/kg 0.00900.016 56 38-149ND
1,1-Dichloropropene mg/kg 0.00840.016 52 41-140ND
1,2,3-Trichlorobenzene mg/kg 0.0100.016 64 10-158ND
1,2,3-Trichloropropane mg/kg 0.0120.016 75 33-157ND
1,2,4-Trichlorobenzene mg/kg 0.00990.016 61 10-155ND
1,2,4-Trimethylbenzene mg/kg 0.00910.016 57 24-154ND
1,2-Dibromo-3-chloropropane mg/kg 0.0130.016 81 33-158ND
1,2-Dibromoethane (EDB)mg/kg 0.0110.016 66 40-136ND
1,2-Dichlorobenzene mg/kg 0.0100.016 63 27-146ND
1,2-Dichloroethane mg/kg 0.0110.016 69 49-140ND
1,2-Dichloropropane mg/kg 0.0100.016 62 44-143ND
1,3,5-Trimethylbenzene mg/kg 0.00870.016 54 40-144ND
1,3-Dichlorobenzene mg/kg 0.00970.016 60 33-140ND
1,3-Dichloropropane mg/kg 0.0110.016 66 47-147ND
1,4-Dichlorobenzene mg/kg 0.0100.016 62 35-139ND
2,2-Dichloropropane mg/kg 0.00860.016 53 41-140ND
2-Butanone (MEK)mg/kg 0.021J0.032 64 10-181ND
2-Chlorotoluene mg/kg 0.00920.016 57 38-147ND
2-Hexanone mg/kg 0.025J0.032 76 18-169ND
4-Chlorotoluene mg/kg 0.00920.016 57 36-145ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.025J0.032 78 16-175ND
Acetone mg/kg 0.029J0.032 89 10-200ND
Benzene mg/kg 0.00940.016 58 46-136ND
Bromobenzene mg/kg 0.0110.016 67 38-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2746340MATRIX SPIKE SAMPLE:
MSSpike
Result
92454745002
Bromochloromethane mg/kg 0.0100.016 65 44-142ND
Bromodichloromethane mg/kg 0.00990.016 62 41-140ND
Bromoform mg/kg 0.0100.016 65 34-145ND
Bromomethane mg/kg 0.0084 IH0.016 52 14-162ND
Carbon tetrachloride mg/kg 0.0110.016 67 44-141ND
Chlorobenzene mg/kg 0.00950.016 59 39-141ND
Chloroethane mg/kg 0.011 IK0.016 70 10-182ND
Chloroform mg/kg 0.0100.016 64 45-140ND
Chloromethane mg/kg 0.0100.016 62 19-149ND
cis-1,2-Dichloroethene mg/kg 0.00940.016 58 38-150ND
cis-1,3-Dichloropropene mg/kg 0.00990.016 61 30-144ND
Dibromochloromethane mg/kg 0.0100.016 63 36-145ND
Dibromomethane mg/kg 0.0120.016 74 41-145ND
Dichlorodifluoromethane mg/kg 0.00910.016 57 16-146ND
Diisopropyl ether mg/kg 0.00970.016 60 41-143ND
Ethylbenzene mg/kg 0.00920.016 57 35-144ND
Hexachloro-1,3-butadiene mg/kg 0.00810.016 50 10-160ND
Isopropylbenzene (Cumene)mg/kg 0.00860.016 53 30-152ND
m&p-Xylene mg/kg 0.0180.032 56 33-145ND
Methyl-tert-butyl ether mg/kg 0.0110.016 68 49-140ND
Methylene Chloride mg/kg 0.011J IH,v10.016 66 10-174ND
n-Butylbenzene mg/kg 0.00810.016 50 10-160ND
n-Propylbenzene mg/kg 0.00850.016 53 24-159ND
Naphthalene mg/kg 0.0120.016 73 10-171ND
o-Xylene mg/kg 0.00960.016 59 31-150ND
p-Isopropyltoluene mg/kg 0.00830.016 52 21-154ND
sec-Butylbenzene mg/kg 0.00820.016 51 19-159ND
Styrene mg/kg 0.00980.016 61 15-152ND
tert-Butylbenzene mg/kg 0.0073 v30.016 45 31-141ND
Tetrachloroethene mg/kg 0.00770.016 48 19-141ND
Toluene mg/kg 0.00940.016 59 31-146ND
trans-1,2-Dichloroethene mg/kg 0.0100.016 62 28-157ND
trans-1,3-Dichloropropene mg/kg 0.0100.016 64 25-146ND
Trichloroethene mg/kg 0.00870.016 54 34-149ND
Trichlorofluoromethane mg/kg 0.00930.016 58 10-167ND
Vinyl acetate mg/kg 0.025J0.032 78 10-200ND
Vinyl chloride mg/kg 0.0100.016 64 36-155ND
Xylene (Total)mg/kg 0.0280.049 57 29-148ND
1,2-Dichloroethane-d4 (S)%99 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454745001
2746339SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND IH30ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND IK30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454745001
2746339SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND IH,v130ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND v230ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9196
4-Bromofluorobenzene (S)%102108
Toluene-d8 (S)%105105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512130
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples: 92454745006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2746406
Associated Lab Samples:92454745006
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/27/19 16:250.34
1,1,1-Trichloroethane ug/L ND 1.0 11/27/19 16:250.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/27/19 16:250.22
1,1,2-Trichloroethane ug/L ND 1.0 11/27/19 16:250.24
1,1-Dichloroethane ug/L ND 1.0 11/27/19 16:250.27
1,1-Dichloroethene ug/L ND 1.0 11/27/19 16:250.24
1,1-Dichloropropene ug/L ND 1.0 11/27/19 16:250.21
1,2,3-Trichlorobenzene ug/L ND 1.0 11/27/19 16:250.34
1,2,3-Trichloropropane ug/L ND 1.0 11/27/19 16:250.35
1,2,4-Trichlorobenzene ug/L ND 1.0 11/27/19 16:250.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 11/27/19 16:250.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/27/19 16:250.26
1,2-Dichlorobenzene ug/L ND 1.0 11/27/19 16:250.29
1,2-Dichloroethane ug/L ND 1.0 11/27/19 16:250.34
1,2-Dichloropropane ug/L ND 1.0 11/27/19 16:250.19
1,3-Dichlorobenzene ug/L ND 1.0 11/27/19 16:250.22
1,3-Dichloropropane ug/L ND 1.0 11/27/19 16:250.16
1,4-Dichlorobenzene ug/L ND 1.0 11/27/19 16:250.26
2,2-Dichloropropane ug/L ND 1.0 11/27/19 16:250.27
2-Butanone (MEK)ug/L ND 5.0 11/27/19 16:253.3
2-Chlorotoluene ug/L ND 1.0 11/27/19 16:250.20
2-Hexanone ug/L ND 5.0 11/27/19 16:250.57
4-Chlorotoluene ug/L ND 1.0 11/27/19 16:250.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/27/19 16:254.5
Acetone ug/L ND 25.0 11/27/19 16:256.2
Benzene ug/L ND 1.0 11/27/19 16:250.15
Bromobenzene ug/L ND 1.0 11/27/19 16:250.22
Bromochloromethane ug/L ND 1.0 11/27/19 16:250.34
Bromodichloromethane ug/L ND 1.0 11/27/19 16:250.26
Bromoform ug/L ND 1.0 11/27/19 16:250.62
Bromomethane ug/L ND 2.0 IH11/27/19 16:250.62
Carbon tetrachloride ug/L ND 1.0 11/27/19 16:250.22
Chlorobenzene ug/L ND 1.0 11/27/19 16:250.23
Chloroethane ug/L ND 1.0 11/27/19 16:250.49
Chloroform ug/L ND 5.0 11/27/19 16:252.3
Chloromethane ug/L ND 1.0 IK11/27/19 16:250.39
cis-1,2-Dichloroethene ug/L ND 1.0 11/27/19 16:250.29
cis-1,3-Dichloropropene ug/L ND 1.0 11/27/19 16:250.30
Dibromochloromethane ug/L ND 1.0 11/27/19 16:250.41
Dibromomethane ug/L ND 1.0 11/27/19 16:250.46
Dichlorodifluoromethane ug/L ND 1.0 11/27/19 16:250.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2746406
Associated Lab Samples:92454745006
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 11/27/19 16:250.22
Ethylbenzene ug/L ND 1.0 11/27/19 16:250.26
Hexachloro-1,3-butadiene ug/L ND 1.0 11/27/19 16:250.44
m&p-Xylene ug/L ND 2.0 11/27/19 16:250.41
Methyl-tert-butyl ether ug/L ND 1.0 11/27/19 16:250.28
Methylene Chloride ug/L ND 5.0 11/27/19 16:253.7
Naphthalene ug/L ND 1.0 11/27/19 16:250.35
o-Xylene ug/L ND 1.0 11/27/19 16:250.22
p-Isopropyltoluene ug/L ND 1.0 11/27/19 16:250.21
Styrene ug/L ND 1.0 11/27/19 16:250.27
Tetrachloroethene ug/L ND 1.0 11/27/19 16:250.16
Toluene ug/L 0.79J 1.0 11/27/19 16:250.24
trans-1,2-Dichloroethene ug/L ND 1.0 11/27/19 16:250.25
trans-1,3-Dichloropropene ug/L ND 1.0 11/27/19 16:250.31
Trichloroethene ug/L ND 1.0 11/27/19 16:250.22
Trichlorofluoromethane ug/L ND 1.0 11/27/19 16:250.31
Vinyl acetate ug/L ND 2.0 11/27/19 16:251.4
Vinyl chloride ug/L ND 1.0 11/27/19 16:250.24
Xylene (Total)ug/L ND 1.0 11/27/19 16:250.63
1,2-Dichloroethane-d4 (S)%103 70-130 11/27/19 16:25
4-Bromofluorobenzene (S)%103 70-130 11/27/19 16:25
Toluene-d8 (S)%89 70-130 11/27/19 16:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746407LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.950 98 70-130
1,1,1-Trichloroethane ug/L 50.750 101 70-130
1,1,2,2-Tetrachloroethane ug/L 49.050 98 70-130
1,1,2-Trichloroethane ug/L 47.950 96 70-130
1,1-Dichloroethane ug/L 50.350 101 70-130
1,1-Dichloroethene ug/L 48.150 96 70-130
1,1-Dichloropropene ug/L 51.450 103 70-130
1,2,3-Trichlorobenzene ug/L 50.550 101 70-130
1,2,3-Trichloropropane ug/L 51.750 103 70-130
1,2,4-Trichlorobenzene ug/L 50.750 101 70-130
1,2-Dibromo-3-chloropropane ug/L 56.350 113 70-130
1,2-Dibromoethane (EDB)ug/L 52.550 105 70-130
1,2-Dichlorobenzene ug/L 51.150 102 70-130
1,2-Dichloroethane ug/L 47.350 95 70-130
1,2-Dichloropropane ug/L 45.550 91 70-130
1,3-Dichlorobenzene ug/L 51.550 103 70-130
1,3-Dichloropropane ug/L 52.050 104 70-131
1,4-Dichlorobenzene ug/L 46.850 94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746407LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 49.250 98 69-130
2-Butanone (MEK)ug/L 99.1100 99 64-135
2-Chlorotoluene ug/L 50.450 101 70-130
2-Hexanone ug/L 107100 107 66-135
4-Chlorotoluene ug/L 52.350 105 70-130
4-Methyl-2-pentanone (MIBK)ug/L 92.2100 92 70-130
Acetone ug/L 114100 114 61-157
Benzene ug/L 47.650 95 70-130
Bromobenzene ug/L 47.350 95 70-130
Bromochloromethane ug/L 46.950 94 70-130
Bromodichloromethane ug/L 44.750 89 70-130
Bromoform ug/L 56.250 112 70-130
Bromomethane ug/L 68.3 IH,L150137 38-130
Carbon tetrachloride ug/L 48.050 96 70-130
Chlorobenzene ug/L 47.650 95 70-130
Chloroethane ug/L 41.350 83 37-142
Chloroform ug/L 50.250 100 70-130
Chloromethane ug/L 50.7 IK50101 48-130
cis-1,2-Dichloroethene ug/L 49.050 98 70-130
cis-1,3-Dichloropropene ug/L 50.850 102 70-130
Dibromochloromethane ug/L 54.150 108 70-130
Dibromomethane ug/L 42.950 86 70-130
Dichlorodifluoromethane ug/L 54.750 109 53-134
Diisopropyl ether ug/L 51.550 103 70-135
Ethylbenzene ug/L 47.550 95 70-130
Hexachloro-1,3-butadiene ug/L 51.150 102 68-132
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 50.450 101 70-130
Methylene Chloride ug/L 45.750 91 67-132
Naphthalene ug/L 52.950 106 70-130
o-Xylene ug/L 55.150 110 70-131
p-Isopropyltoluene ug/L 50.350 101 70-130
Styrene ug/L 53.650 107 70-130
Tetrachloroethene ug/L 46.450 93 69-130
Toluene ug/L 44.350 89 70-130
trans-1,2-Dichloroethene ug/L 50.250 100 70-130
trans-1,3-Dichloropropene ug/L 47.350 95 70-130
Trichloroethene ug/L 48.150 96 70-130
Trichlorofluoromethane ug/L 39.250 78 63-130
Vinyl acetate ug/L 113100 113 55-143
Vinyl chloride ug/L 49.450 99 70-131
Xylene (Total)ug/L 156150 104 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2746417MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454959005
2746418
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 108 73-134121 12 3020ND21.6 24.2
1,1,1-Trichloroethane ug/L 20 115 82-143124 7 3020ND23.1 24.8
1,1,2,2-Tetrachloroethane ug/L 20 104 70-136112 7 3020ND20.8 22.3
1,1,2-Trichloroethane ug/L 20 109 70-135118 8 3020ND21.8 23.7
1,1-Dichloroethane ug/L 20 108 70-139117 8 30201.4 23.0 24.9
1,1-Dichloroethene ug/L 20 111 70-154121 8 30201.2 23.5 25.4
1,1-Dichloropropene ug/L 20 118 70-149130 9 3020ND23.7 26.0
1,2,3-Trichlorobenzene ug/L 20 99 70-135111 11 3020ND19.9 22.2
1,2,3-Trichloropropane ug/L 20 105 71-137115 9 3020ND21.0 23.0
1,2,4-Trichlorobenzene ug/L 20 99 73-140109 10 3020ND19.8 21.9
1,2-Dibromo-3-
chloropropane ug/L 20 108 65-134118 9 3020ND21.6 23.7
1,2-Dibromoethane (EDB) ug/L 20 108 70-137120 10 3020ND21.6 24.0
1,2-Dichlorobenzene ug/L 20 99 70-133111 12 3020ND19.7 22.2
1,2-Dichloroethane ug/L 20 104 70-137113 8 3020ND20.7 22.5
1,2-Dichloropropane ug/L 20 108 70-140115 7 3020ND21.5 23.0
1,3-Dichlorobenzene ug/L 20 99 70-135110 10 3020ND19.8 22.0
1,3-Dichloropropane ug/L 20 110 70-143118 7 3020ND22.0 23.7
1,4-Dichlorobenzene ug/L 20 98 70-133110 12 3020ND19.5 21.9
2,2-Dichloropropane ug/L 20 116 61-148128 10 3020ND23.2 25.6
2-Butanone (MEK)ug/L 40 102 60-139111 8 3040ND41.0 44.3
2-Chlorotoluene ug/L 20 99 70-144109 10 3020ND19.8 21.8
2-Hexanone ug/L 40 103 65-138111 7 3040ND41.3 44.3
4-Chlorotoluene ug/L 20 98 70-137110 11 3020ND19.7 22.1
4-Methyl-2-pentanone
(MIBK)ug/L 40 104 65-135114 8 3040ND41.8 45.4
Acetone ug/L 40 93 60-148106 13 3040ND37.2 42.6
Benzene ug/L 20 109 70-151117 7 3020ND21.8 23.3
Bromobenzene ug/L 20 104 70-136116 11 3020ND20.8 23.3
Bromochloromethane ug/L 20 117 70-141130 10 3020ND23.4 25.9
Bromodichloromethane ug/L 20 108 70-138117 8 3020ND21.7 23.5
Bromoform ug/L 20 110 63-130121 9 3020ND22.0 24.2
Bromomethane ug/L 20 125 15-152131 4 3020ND25.0 26.1
Carbon tetrachloride ug/L 20 115 70-143124 7 3020ND23.0 24.7
Chlorobenzene ug/L 20 103 70-138112 9 3020ND20.6 22.5
Chloroethane ug/L 20 100 52-163108 8 3020ND19.9 21.6
Chloroform ug/L 20 113 70-139122 7 3020ND22.7 24.4
Chloromethane ug/L 20 102 41-139110 7 3020ND20.5 21.9
cis-1,2-Dichloroethene ug/L 20 106 70-141118 11 3020ND21.1 23.6
cis-1,3-Dichloropropene ug/L 20 112 70-137121 8 3020ND22.3 24.2
Dibromochloromethane ug/L 20 111 70-134120 8 3020ND22.1 24.1
Dibromomethane ug/L 20 110 70-138123 11 3020ND22.0 24.5
Dichlorodifluoromethane ug/L 20 124 47-155131 6 3020ND24.8 26.3
Diisopropyl ether ug/L 20 106 63-144121 13 3020ND21.3 24.1
Ethylbenzene ug/L 20 103 66-153112 8 3020ND20.6 22.4
Hexachloro-1,3-butadiene ug/L 20 114 65-149114 0 3020ND22.9 22.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2746417MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454959005
2746418
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 102 69-152111 9 3040ND40.8 44.5
Methyl-tert-butyl ether ug/L 20 110 54-156123 11 3020ND22.1 24.6
Methylene Chloride ug/L 20 103 42-159115 11 3020ND20.6 23.1
Naphthalene ug/L 20 96 61-148111 14 3020ND19.2 22.1
o-Xylene ug/L 20 103 70-148114 10 3020ND20.7 22.9
p-Isopropyltoluene ug/L 20 100 70-146107 7 3020ND19.9 21.3
Styrene ug/L 20 101 70-135112 10 3020ND20.3 22.3
Tetrachloroethene ug/L 20 110 59-143117 6 3020ND21.9 23.3
Toluene ug/L 20 103 59-148114 10 3020ND20.6 22.9
trans-1,2-Dichloroethene ug/L 20 110 70-146121 10 3020ND22.0 24.2
trans-1,3-Dichloropropene ug/L 20 112 70-135123 9 3020ND22.3 24.5
Trichloroethene ug/L 20 110 70-147119 8 3020ND22.0 23.8
Trichlorofluoromethane ug/L 20 111 70-148119 6 3020ND22.3 23.7
Vinyl acetate ug/L 40 103 49-151113 10 3040ND41.1 45.3
Vinyl chloride ug/L 20 124 70-156133 7 3020ND24.8 26.5
Xylene (Total)ug/L 60 102 63-158112 9 3060ND61.5 67.4
1,2-Dichloroethane-d4 (S) %96 70-13099
4-Bromofluorobenzene (S) %100 70-130100
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511424
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Associated Lab Samples: 92454745006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743471
Associated Lab Samples:92454745006
Matrix: Water
AnalyzedMDL
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/23/19 19:221.2
1,2-Dichloroethane-d4 (S)%98 50-150 11/23/19 19:22
Toluene-d8 (S)%109 50-150 11/23/19 19:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743472LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 18.820 94 70-130
1,2-Dichloroethane-d4 (S)%101 50-150
Toluene-d8 (S)%107 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2743473MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454805004
2743474
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane) ug/L 20 87 50-15093 1 302079.9 97.3 98.5
1,2-Dichloroethane-d4 (S) %120 50-150116 30
Toluene-d8 (S)%109 50-150108 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511556
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV Soil SIM
Associated Lab Samples: 92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743926
Associated Lab Samples:92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Matrix: Solid
AnalyzedMDL
1,4-Dioxane (p-Dioxane)mg/kg ND 0.010 11/25/19 11:150.0030
1,2-Dichloroethane-d4 (S)%103 50-150 11/25/19 11:15
Toluene-d8 (S)%99 50-150 11/25/19 11:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743927LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)mg/kg 0.0400.04 99 50-150
1,2-Dichloroethane-d4 (S)%103 50-150
Toluene-d8 (S)%103 50-150
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2744454MATRIX SPIKE SAMPLE:
MSSpike
Result
92454623002
1,4-Dioxane (p-Dioxane)mg/kg 0.0520.045 104 50-1500.0047J
1,2-Dichloroethane-d4 (S)%95 50-150
Toluene-d8 (S)%105 50-150
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454623001
2744453SAMPLE DUPLICATE:
1,4-Dioxane (p-Dioxane)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%95 3099
Toluene-d8 (S)%109 30100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511777
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples: 92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744914
Associated Lab Samples:92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 11/26/19 20:280.076
1,2-Dichlorobenzene mg/kg ND 0.33 11/26/19 20:280.071
1,3-Dichlorobenzene mg/kg ND 0.33 11/26/19 20:280.074
1,4-Dichlorobenzene mg/kg ND 0.33 11/26/19 20:280.073
1-Methylnaphthalene mg/kg ND 0.33 11/26/19 20:280.088
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 11/26/19 20:280.092
2,4,5-Trichlorophenol mg/kg ND 0.33 11/26/19 20:280.086
2,4,6-Trichlorophenol mg/kg ND 0.33 11/26/19 20:280.083
2,4-Dichlorophenol mg/kg ND 0.33 11/26/19 20:280.11
2,4-Dimethylphenol mg/kg ND 0.33 11/26/19 20:280.082
2,4-Dinitrophenol mg/kg ND 1.6 11/26/19 20:281.1
2,4-Dinitrotoluene mg/kg ND 0.33 11/26/19 20:280.087
2,6-Dinitrotoluene mg/kg ND 0.33 11/26/19 20:280.086
2-Chloronaphthalene mg/kg ND 0.33 11/26/19 20:280.074
2-Chlorophenol mg/kg ND 0.33 11/26/19 20:280.077
2-Methylnaphthalene mg/kg ND 0.33 11/26/19 20:280.084
2-Methylphenol(o-Cresol)mg/kg ND 0.33 11/26/19 20:280.073
2-Nitroaniline mg/kg ND 1.6 11/26/19 20:280.17
2-Nitrophenol mg/kg ND 0.33 11/26/19 20:280.10
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 11/26/19 20:280.083
3,3'-Dichlorobenzidine mg/kg ND 1.6 11/26/19 20:280.23
3-Nitroaniline mg/kg ND 1.6 11/26/19 20:280.18
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 11/26/19 20:280.53
4-Bromophenylphenyl ether mg/kg ND 0.33 11/26/19 20:280.087
4-Chloro-3-methylphenol mg/kg ND 0.66 11/26/19 20:280.20
4-Chloroaniline mg/kg ND 1.6 11/26/19 20:280.20
4-Chlorophenylphenyl ether mg/kg ND 0.33 11/26/19 20:280.086
4-Nitroaniline mg/kg ND 0.66 11/26/19 20:280.16
4-Nitrophenol mg/kg ND 1.6 11/26/19 20:280.53
Acenaphthene mg/kg ND 0.33 11/26/19 20:280.085
Acenaphthylene mg/kg ND 0.33 11/26/19 20:280.078
Aniline mg/kg ND 0.33 11/26/19 20:280.074
Anthracene mg/kg ND 0.33 11/26/19 20:280.086
Benzo(a)anthracene mg/kg ND 0.33 11/26/19 20:280.10
Benzo(a)pyrene mg/kg ND 0.33 11/26/19 20:280.14
Benzo(b)fluoranthene mg/kg ND 0.33 11/26/19 20:280.13
Benzo(g,h,i)perylene mg/kg ND 0.33 11/26/19 20:280.13
Benzo(k)fluoranthene mg/kg ND 0.33 11/26/19 20:280.14
Benzoic Acid mg/kg ND 1.6 11/26/19 20:280.36
Benzyl alcohol mg/kg ND 0.66 11/26/19 20:280.18
bis(2-Chloroethoxy)methane mg/kg ND 0.33 11/26/19 20:280.088
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744914
Associated Lab Samples:92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether mg/kg ND 0.33 11/26/19 20:280.070
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 11/26/19 20:280.11
Butylbenzylphthalate mg/kg ND 0.33 11/26/19 20:280.088
Chrysene mg/kg ND 0.33 11/26/19 20:280.096
Di-n-butylphthalate mg/kg ND 0.33 11/26/19 20:280.081
Di-n-octylphthalate mg/kg ND 0.33 11/26/19 20:280.19
Dibenz(a,h)anthracene mg/kg ND 0.33 11/26/19 20:280.13
Dibenzofuran mg/kg ND 0.33 11/26/19 20:280.082
Diethylphthalate mg/kg ND 0.33 11/26/19 20:280.072
Dimethylphthalate mg/kg ND 0.33 11/26/19 20:280.075
Fluoranthene mg/kg ND 0.33 11/26/19 20:280.10
Fluorene mg/kg ND 0.33 11/26/19 20:280.088
Hexachloro-1,3-butadiene mg/kg ND 0.33 11/26/19 20:280.080
Hexachlorobenzene mg/kg ND 0.33 11/26/19 20:280.084
Hexachlorocyclopentadiene mg/kg ND 0.33 11/26/19 20:280.13
Hexachloroethane mg/kg ND 0.33 11/26/19 20:280.075
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 11/26/19 20:280.15
Isophorone mg/kg ND 0.33 11/26/19 20:280.072
N-Nitroso-di-n-propylamine mg/kg ND 0.33 11/26/19 20:280.092
N-Nitrosodimethylamine mg/kg ND 0.33 11/26/19 20:280.093
N-Nitrosodiphenylamine mg/kg ND 0.33 11/26/19 20:280.084
Naphthalene mg/kg ND 0.33 11/26/19 20:280.079
Nitrobenzene mg/kg ND 0.33 11/26/19 20:280.079
Pentachlorophenol mg/kg ND 1.6 11/26/19 20:280.15
Phenanthrene mg/kg ND 0.33 11/26/19 20:280.083
Phenol mg/kg ND 0.33 11/26/19 20:280.079
Pyrene mg/kg ND 0.33 11/26/19 20:280.091
Pyridine mg/kg ND 0.33 11/26/19 20:280.084
2,4,6-Tribromophenol (S)%97 27-110 11/26/19 20:28
2-Fluorobiphenyl (S)%83 30-110 11/26/19 20:28
2-Fluorophenol (S)%82 13-110 11/26/19 20:28
Nitrobenzene-d5 (S)%80 23-110 11/26/19 20:28
Phenol-d6 (S)%79 22-110 11/26/19 20:28
Terphenyl-d14 (S)%95 28-110 11/26/19 20:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744915LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.41.7 86 52-130
1,2-Dichlorobenzene mg/kg 1.41.7 86 51-130
1,3-Dichlorobenzene mg/kg 1.41.7 85 50-130
1,4-Dichlorobenzene mg/kg 1.41.7 84 49-130
1-Methylnaphthalene mg/kg 1.51.7 87 55-130
2,2'-Oxybis(1-chloropropane)mg/kg 1.31.7 78 30-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744915LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol mg/kg 1.51.7 88 55-130
2,4,6-Trichlorophenol mg/kg 1.51.7 92 57-130
2,4-Dichlorophenol mg/kg 1.51.7 88 56-130
2,4-Dimethylphenol mg/kg 1.51.7 90 51-130
2,4-Dinitrophenol mg/kg 7.38.4 87 27-133
2,4-Dinitrotoluene mg/kg 1.51.7 92 61-130
2,6-Dinitrotoluene mg/kg 1.51.7 92 60-130
2-Chloronaphthalene mg/kg 1.51.7 89 52-130
2-Chlorophenol mg/kg 1.51.7 87 54-130
2-Methylnaphthalene mg/kg 1.51.7 89 54-130
2-Methylphenol(o-Cresol)mg/kg 1.41.7 84 51-130
2-Nitroaniline mg/kg 3.03.3 90 51-130
2-Nitrophenol mg/kg 1.51.7 88 49-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.41.7 83 11-163
3,3'-Dichlorobenzidine mg/kg 2.53.3 75 10-132
3-Nitroaniline mg/kg 2.63.3 78 55-130
4,6-Dinitro-2-methylphenol mg/kg 3.63.3 107 47-142
4-Bromophenylphenyl ether mg/kg 1.51.7 91 59-130
4-Chloro-3-methylphenol mg/kg 2.93.3 88 55-130
4-Chloroaniline mg/kg 2.93.3 86 54-130
4-Chlorophenylphenyl ether mg/kg 1.51.7 90 58-130
4-Nitroaniline mg/kg 2.83.3 83 54-130
4-Nitrophenol mg/kg 6.98.4 83 48-130
Acenaphthene mg/kg 1.61.7 95 60-130
Acenaphthylene mg/kg 1.71.7 101 60-130
Aniline mg/kg 1.31.7 81 43-130
Anthracene mg/kg 1.71.7 101 63-130
Benzo(a)anthracene mg/kg 1.61.7 93 59-130
Benzo(a)pyrene mg/kg 1.81.7 105 57-130
Benzo(b)fluoranthene mg/kg 1.71.7 100 54-130
Benzo(g,h,i)perylene mg/kg 1.81.7 108 59-130
Benzo(k)fluoranthene mg/kg 1.71.7 103 54-130
Benzoic Acid mg/kg 6.28.4 74 19-130
Benzyl alcohol mg/kg 2.83.3 85 50-130
bis(2-Chloroethoxy)methane mg/kg 1.51.7 87 54-130
bis(2-Chloroethyl) ether mg/kg 1.51.7 92 48-130
bis(2-Ethylhexyl)phthalate mg/kg 1.41.7 86 45-134
Butylbenzylphthalate mg/kg 1.51.7 87 46-138
Chrysene mg/kg 1.51.7 89 58-130
Di-n-butylphthalate mg/kg 1.41.7 86 60-130
Di-n-octylphthalate mg/kg 1.51.7 91 53-130
Dibenz(a,h)anthracene mg/kg 1.71.7 102 59-130
Dibenzofuran mg/kg 1.51.7 90 60-130
Diethylphthalate mg/kg 1.41.7 85 60-130
Dimethylphthalate mg/kg 1.41.7 86 60-130
Fluoranthene mg/kg 1.61.7 95 65-130
Fluorene mg/kg 1.61.7 94 63-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744915LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene mg/kg 1.41.7 86 46-130
Hexachlorobenzene mg/kg 1.51.7 92 58-130
Hexachlorocyclopentadiene mg/kg 1.81.7 107 23-130
Hexachloroethane mg/kg 1.51.7 87 47-130
Indeno(1,2,3-cd)pyrene mg/kg 1.71.7 104 60-130
Isophorone mg/kg 1.41.7 86 49-130
N-Nitroso-di-n-propylamine mg/kg 1.41.7 86 47-130
N-Nitrosodimethylamine mg/kg 1.51.7 91 45-130
N-Nitrosodiphenylamine mg/kg 1.51.7 87 59-130
Naphthalene mg/kg 1.51.7 91 55-130
Nitrobenzene mg/kg 1.41.7 86 49-130
Pentachlorophenol mg/kg 2.93.3 88 10-132
Phenanthrene mg/kg 1.61.7 97 62-130
Phenol mg/kg 1.61.7 95 46-130
Pyrene mg/kg 1.61.7 98 53-130
Pyridine mg/kg 1.11.7 67 37-130
2,4,6-Tribromophenol (S)%S0111 27-110
2-Fluorobiphenyl (S)%96 30-110
2-Fluorophenol (S)%95 13-110
Nitrobenzene-d5 (S)%88 23-110
Phenol-d6 (S)%94 22-110
Terphenyl-d14 (S)%99 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744916MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92449762007
2744917
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene mg/kg 1.7 74 18-13076 301.7ND 1.2J 1.3J
1,2-Dichlorobenzene mg/kg 1.7 68 14-13073 301.7ND 1.2J 1.2J
1,3-Dichlorobenzene mg/kg 1.7 65 12-13073 301.7ND 1.1J 1.2J
1,4-Dichlorobenzene mg/kg 1.7 65 10-13069 301.7ND 1.1J 1.2J
1-Methylnaphthalene mg/kg M11.7 15 12-13010 301.7ND 1.6J 1.6J
2,2'-Oxybis(1-
chloropropane)mg/kg 1.7 64 10-13067 301.7ND 1.1J 1.1J
2,4,5-Trichlorophenol mg/kg 1.7 63 13-13072 301.7ND 1.1J 1.2J
2,4,6-Trichlorophenol mg/kg 1.7 66 17-13071 301.7ND 1.1J 1.2J
2,4-Dichlorophenol mg/kg 1.7 69 10-13073 301.7ND 1.2J 1.2J
2,4-Dimethylphenol mg/kg 1.7 117 10-13099 16 301.7ND 2.0 1.7
2,4-Dinitrophenol mg/kg 8.4 41 10-13041 308.4ND ND ND
2,4-Dinitrotoluene mg/kg 1.7 64 24-13071 301.7ND 1.1J 1.2J
2,6-Dinitrotoluene mg/kg 1.7 114 23-13094 301.7ND 1.9 1.6J
2-Chloronaphthalene mg/kg 1.7 74 19-13075 301.7ND 1.2J 1.3J
2-Chlorophenol mg/kg 1.7 67 10-13072 301.7ND 1.1J 1.2J
2-Methylnaphthalene mg/kg 1.7 46 18-13044 301.7ND 1.4J 1.4J
2-Methylphenol(o-Cresol) mg/kg 1.7 62 10-13063 301.7ND 1.0J 1.1J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744916MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92449762007
2744917
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitroaniline mg/kg 3.4 56 17-13059 303.4ND 1.9J 2.0J
2-Nitrophenol mg/kg 1.7 73 10-13078 301.7ND 1.2J 1.3J
3&4-Methylphenol(m&p
Cresol)mg/kg 1.7 60 10-13064 301.7ND 1.0J 1.1J
3,3'-Dichlorobenzidine mg/kg 3.4 30 10-13021 303.4ND ND ND
3-Nitroaniline mg/kg 3.4 79 24-130103 303.4ND 2.7J 3.5J
4,6-Dinitro-2-methylphenol mg/kg 3.4 50 10-15262 303.4ND ND ND
4-Bromophenylphenyl ether mg/kg 1.7 82 29-13089 301.7ND 1.4J 1.5J
4-Chloro-3-methylphenol mg/kg 3.4 62 17-13068 303.4ND 2.1J 2.3J
4-Chloroaniline mg/kg 3.4 58 14-13063 303.4ND 1.9J 2.1J
4-Chlorophenylphenyl ether mg/kg 1.7 92 25-13084 301.7ND 1.6J 1.4J
4-Nitroaniline mg/kg 3.4 62 22-13069 303.4ND 2.1J 2.3J
4-Nitrophenol mg/kg 8.4 75 10-13070 308.4ND 6.3J 5.9J
Acenaphthene mg/kg 1.7 71 20-13078 301.7ND 1.2J 1.3J
Acenaphthylene mg/kg 1.7 85 25-13077 301.7ND 1.4J 1.3J
Aniline mg/kg 1.7 49 10-13052 301.7ND 0.83J 0.88J
Anthracene mg/kg 1.7 79 29-13082 301.7ND 1.3J 1.4J
Benzo(a)anthracene mg/kg 1.7 70 19-13075 301.7ND 1.2J 1.3J
Benzo(a)pyrene mg/kg 1.7 70 12-13075 301.7ND 1.2J 1.3J
Benzo(b)fluoranthene mg/kg 1.7 67 14-13071 301.7ND 1.1J 1.2J
Benzo(g,h,i)perylene mg/kg 1.7 72 10-13074 301.7ND 1.2J 1.3J
Benzo(k)fluoranthene mg/kg 1.7 66 14-13073 301.7ND 1.1J 1.2J
Benzoic Acid mg/kg 8.4 59 10-13061 308.4ND 5.0J 5.1J
Benzyl alcohol mg/kg 3.4 57 13-13065 303.4ND 1.9J 2.2J
bis(2-
Chloroethoxy)methane mg/kg 1.7 70 16-13073 301.7ND 1.2J 1.2J
bis(2-Chloroethyl) ether mg/kg 1.7 67 11-13068 301.7ND 1.1J 1.1J
bis(2-Ethylhexyl)phthalate mg/kg 1.7 64 21-13070 301.7ND 1.1J 1.2J
Butylbenzylphthalate mg/kg 1.7 68 23-13071 301.7ND 1.1J 1.2J
Chrysene mg/kg 1.7 66 22-13068 301.7ND 1.1J 1.2J
Di-n-butylphthalate mg/kg 1.7 64 30-13069 301.7ND 1.1J 1.2J
Di-n-octylphthalate mg/kg 1.7 66 23-14272 301.7ND 1.1J 1.2J
Dibenz(a,h)anthracene mg/kg 1.7 64 10-13067 301.7ND 1.1J 1.1J
Dibenzofuran mg/kg 1.7 75 24-13080 301.7ND 1.3J 1.3J
Diethylphthalate mg/kg 1.7 66 26-13064 301.7ND 1.1J 1.1J
Dimethylphthalate mg/kg 1.7 72 22-13066 301.7ND 1.2J 1.1J
Fluoranthene mg/kg 1.7 72 33-13074 301.7ND 1.2J 1.3J
Fluorene mg/kg 1.7 82 22-13076 301.7ND 1.4J 1.3J
Hexachloro-1,3-butadiene mg/kg 1.7 73 13-13076 301.7ND 1.2J 1.3J
Hexachlorobenzene mg/kg 1.7 80 29-13087 301.7ND 1.3J 1.5J
Hexachlorocyclopentadiene mg/kg 1.7 65 10-13069 301.7ND 1.1J 1.2J
Hexachloroethane mg/kg 1.7 63 10-13074 301.7ND 1.1J 1.3J
Indeno(1,2,3-cd)pyrene mg/kg 1.7 67 10-13074 301.7ND 1.1J 1.3J
Isophorone mg/kg 1.7 70 13-13072 301.7ND 1.2J 1.2J
N-Nitroso-di-n-propylamine mg/kg 1.7 67 12-13071 301.7ND 1.1J 1.2J
N-Nitrosodimethylamine mg/kg 1.7 35 11-13035 301.7ND 0.58J 0.60J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744916MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92449762007
2744917
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodiphenylamine mg/kg M1,R11.7 180 15-130117 42 301.7ND 3.0 2.0
Naphthalene mg/kg 1.7 77 15-13079 301.7ND 1.3J 1.3J
Nitrobenzene mg/kg 1.7 68 12-13069 301.7ND 1.1J 1.2J
Pentachlorophenol mg/kg 3.4 65 10-13068 303.4ND 2.2J 2.3J
Phenanthrene mg/kg 1.7 82 27-13084 301.7ND 1.4J 1.4J
Phenol mg/kg 1.7 66 10-13071 301.7ND 1.1J 1.2J
Pyrene mg/kg 1.7 62 19-13057 301.7ND 1.6J 1.6J
Pyridine mg/kg 1.7 23 10-13027 301.7ND ND 0.46J
2,4,6-Tribromophenol (S) %89 27-11093
2-Fluorobiphenyl (S)%57 30-11067
2-Fluorophenol (S)%56 13-11065
Nitrobenzene-d5 (S)%D36523-11066
Phenol-d6 (S)%55 22-11061
Terphenyl-d14 (S)%59 28-11071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454745
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511267
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92454745001, 92454745002, 92454745003, 92454745004, 92454745005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454760002
2742668SAMPLE DUPLICATE:
Percent Moisture %12.4 3 2512.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454817001
2742669SAMPLE DUPLICATE:
Percent Moisture %91.4 0 2591.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 55
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92454745
ROW-603
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 55
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92454745
ROW-603
ANALYTE QUALIFIERS
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92454745
ROW-603
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92454745001 511524 511736SB-4 (15-17)EPA 3050B EPA 6010D
92454745002 511524 511736SB-4 (19-21)EPA 3050B EPA 6010D
92454745003 511524 511736SB-5 (15-17)EPA 3050B EPA 6010D
92454745004 511524 511736SB-5 (19-21)EPA 3050B EPA 6010D
92454745005 511524 511736DUP-1-SOIL EPA 3050B EPA 6010D
92454745001 511178 511280SB-4 (15-17)EPA 7471B EPA 7471B
92454745002 511178 511280SB-4 (19-21)EPA 7471B EPA 7471B
92454745003 511178 511280SB-5 (15-17)EPA 7471B EPA 7471B
92454745004 511178 511280SB-5 (19-21)EPA 7471B EPA 7471B
92454745005 511178 511280DUP-1-SOIL EPA 7471B EPA 7471B
92454745001 511777 512023SB-4 (15-17)EPA 3546 EPA 8270E
92454745002 511777 512023SB-4 (19-21)EPA 3546 EPA 8270E
92454745003 511777 512023SB-5 (15-17)EPA 3546 EPA 8270E
92454745004 511777 512023SB-5 (19-21)EPA 3546 EPA 8270E
92454745005 511777 512023DUP-1-SOIL EPA 3546 EPA 8270E
92454745001 512117 512123SB-4 (15-17)EPA 5035A EPA 8260D
92454745002 512117 512123SB-4 (19-21)EPA 5035A EPA 8260D
92454745003 512117 512123SB-5 (15-17)EPA 5035A EPA 8260D
92454745004 512117 512123SB-5 (19-21)EPA 5035A EPA 8260D
92454745005 512117 512123DUP-1-SOIL EPA 5035A EPA 8260D
92454745006 512130TRIP BLANK EPA 8260D
92454745006 511424TRIP BLANK EPA 8260D Mod.
92454745001 511556 511649SB-4 (15-17)EPA 8260D Mod.EPA 8260D Mod.
92454745002 511556 511649SB-4 (19-21)EPA 8260D Mod.EPA 8260D Mod.
92454745003 511556 511649SB-5 (15-17)EPA 8260D Mod.EPA 8260D Mod.
92454745004 511556 511649SB-5 (19-21)EPA 8260D Mod.EPA 8260D Mod.
92454745005 511556 511649DUP-1-SOIL EPA 8260D Mod.EPA 8260D Mod.
92454745001 511267SB-4 (15-17)ASTM D2974-87
92454745002 511267SB-4 (19-21)ASTM D2974-87
92454745003 511267SB-5 (15-17)ASTM D2974-87
92454745004 511267SB-5 (19-21)ASTM D2974-87
92454745005 511267DUP-1-SOIL ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/04/2019 08:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 55
Page 53 of 55
Page 54 of 55
Page 55 of 55
#=CL#
December 06, 2019
LIMS USE: FR - DAVID GRAHAM
LIMS OBJECT ID: 92455128
92455128
Project:
Pace Project No.:
RE:
David Graham
Hart & Hickman
2923 S. Tryon Street
Charlotte, NC 28203
ROW-603
Dear David Graham:
Enclosed are the analytical results for sample(s) received by the laboratory on November 22, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 43
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92455128
ROW-603
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 43
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92455128
ROW-603
Lab ID Sample ID Matrix Date Collected Date Received
92455128001 MW-2 Water 11/22/19 09:05 11/22/19 15:57
92455128002 MW-1 Water 11/22/19 11:30 11/22/19 15:57
92455128003 MW-4 Water 11/22/19 12:55 11/22/19 15:57
92455128004 DUP-2-GW Water 11/22/19 00:00 11/22/19 15:57
92455128005 TRIP BLANK Water 11/22/19 00:00 11/22/19 15:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 43
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92455128
ROW-603
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92455128001 MW-2 EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CGAW
EPA 8260D Mod.3 PASI-CLMB
92455128002 MW-1 EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CGAW
EPA 8260D Mod.3 PASI-CLMB
92455128003 MW-4 EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CGAW
EPA 8260D Mod.3 PASI-CLMB
92455128004 DUP-2-GW EPA 6010D 7 PASI-ADS
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CGAW
EPA 8260D Mod.3 PASI-CLMB
92455128005 TRIP BLANK EPA 8260D 63 PASI-CGAW
EPA 8260D Mod.3 PASI-CLMB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-2 Lab ID: 92455128001 Collected: 11/22/19 09:05 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/26/19 22:41 7440-38-211/26/19 02:2410.0 4.7 1
Barium 40.6 ug/L 11/26/19 22:41 7440-39-311/26/19 02:245.0 1.0 1
Cadmium ND ug/L 11/26/19 22:41 7440-43-911/26/19 02:241.0 0.40 1
Chromium ND ug/L 11/26/19 22:41 7440-47-311/26/19 02:245.0 1.0 1
Lead ND ug/L 11/26/19 22:41 7439-92-111/26/19 02:245.0 1.6 1
Selenium ND ug/L 11/26/19 22:41 7782-49-211/26/19 02:2410.0 4.7 1
Silver ND ug/L 11/26/19 22:41 7440-22-411/26/19 02:245.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 12/03/19 14:41 7439-97-612/03/19 11:020.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 12/02/19 16:42 83-32-911/26/19 18:2310.0 1.6 1
Acenaphthylene ND ug/L 12/02/19 16:42 208-96-811/26/19 18:2310.0 1.6 1
Aniline ND ug/L 12/02/19 16:42 62-53-3 v211/26/19 18:2310.0 1.9 1
Anthracene ND ug/L 12/02/19 16:42 120-12-711/26/19 18:2310.0 1.7 1
Benzo(a)anthracene ND ug/L 12/02/19 16:42 56-55-311/26/19 18:2310.0 1.8 1
Benzo(a)pyrene ND ug/L 12/02/19 16:42 50-32-811/26/19 18:2310.0 2.1 1
Benzo(b)fluoranthene ND ug/L 12/02/19 16:42 205-99-211/26/19 18:2310.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 12/02/19 16:42 191-24-211/26/19 18:2310.0 1.4 1
Benzo(k)fluoranthene ND ug/L 12/02/19 16:42 207-08-911/26/19 18:2310.0 1.9 1
Benzoic Acid ND ug/L 12/02/19 16:42 65-85-011/26/19 18:2350.0 43.0 1
Benzyl alcohol ND ug/L 12/02/19 16:42 100-51-611/26/19 18:2320.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 12/02/19 16:42 101-55-311/26/19 18:2310.0 1.6 1
Butylbenzylphthalate ND ug/L 12/02/19 16:42 85-68-711/26/19 18:2310.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 12/02/19 16:42 59-50-711/26/19 18:2320.0 2.8 1
4-Chloroaniline ND ug/L 12/02/19 16:42 106-47-811/26/19 18:2320.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 12/02/19 16:42 111-91-111/26/19 18:2310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 12/02/19 16:42 111-44-4 v111/26/19 18:2310.0 1.8 1
2-Chloronaphthalene ND ug/L 12/02/19 16:42 91-58-711/26/19 18:2310.0 1.5 1
2-Chlorophenol ND ug/L 12/02/19 16:42 95-57-811/26/19 18:2310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 12/02/19 16:42 7005-72-311/26/19 18:2310.0 1.6 1
Chrysene ND ug/L 12/02/19 16:42 218-01-911/26/19 18:2310.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 12/02/19 16:42 53-70-311/26/19 18:2310.0 1.6 1
Dibenzofuran ND ug/L 12/02/19 16:42 132-64-911/26/19 18:2310.0 1.5 1
1,2-Dichlorobenzene ND ug/L 12/02/19 16:42 95-50-111/26/19 18:2310.0 1.3 1
1,3-Dichlorobenzene ND ug/L 12/02/19 16:42 541-73-111/26/19 18:2310.0 1.5 1
1,4-Dichlorobenzene ND ug/L 12/02/19 16:42 106-46-711/26/19 18:2310.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 12/02/19 16:42 91-94-111/26/19 18:2320.0 3.0 1
2,4-Dichlorophenol ND ug/L 12/02/19 16:42 120-83-211/26/19 18:2310.0 1.4 1
Diethylphthalate ND ug/L 12/02/19 16:42 84-66-211/26/19 18:2310.0 2.4 1
2,4-Dimethylphenol ND ug/L 12/02/19 16:42 105-67-911/26/19 18:2310.0 1.4 1
Dimethylphthalate ND ug/L 12/02/19 16:42 131-11-311/26/19 18:2310.0 1.6 1
Di-n-butylphthalate ND ug/L 12/02/19 16:42 84-74-211/26/19 18:2310.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 12/02/19 16:42 534-52-111/26/19 18:2320.0 15.2 1
2,4-Dinitrophenol ND ug/L 12/02/19 16:42 51-28-511/26/19 18:2350.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-2 Lab ID: 92455128001 Collected: 11/22/19 09:05 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 12/02/19 16:42 121-14-211/26/19 18:2310.0 1.2 1
2,6-Dinitrotoluene ND ug/L 12/02/19 16:42 606-20-211/26/19 18:2310.0 1.4 1
Di-n-octylphthalate ND ug/L 12/02/19 16:42 117-84-011/26/19 18:2310.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/02/19 16:42 117-81-711/26/19 18:236.0 2.1 1
Fluoranthene ND ug/L 12/02/19 16:42 206-44-011/26/19 18:2310.0 1.7 1
Fluorene ND ug/L 12/02/19 16:42 86-73-711/26/19 18:2310.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 12/02/19 16:42 87-68-311/26/19 18:2310.0 2.0 1
Hexachlorobenzene ND ug/L 12/02/19 16:42 118-74-111/26/19 18:2310.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 12/02/19 16:42 77-47-411/26/19 18:2310.0 1.7 1
Hexachloroethane ND ug/L 12/02/19 16:42 67-72-111/26/19 18:2310.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 12/02/19 16:42 193-39-511/26/19 18:2310.0 1.6 1
Isophorone ND ug/L 12/02/19 16:42 78-59-111/26/19 18:2310.0 1.6 1
1-Methylnaphthalene ND ug/L 12/02/19 16:42 90-12-011/26/19 18:2310.0 1.4 1
2-Methylnaphthalene ND ug/L 12/02/19 16:42 91-57-611/26/19 18:2310.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 12/02/19 16:42 95-48-711/26/19 18:2310.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/02/19 16:42 15831-10-411/26/19 18:2310.0 1.2 1
Naphthalene ND ug/L 12/02/19 16:42 91-20-311/26/19 18:2310.0 1.4 1
2-Nitroaniline ND ug/L 12/02/19 16:42 88-74-411/26/19 18:2320.0 4.2 1
3-Nitroaniline ND ug/L 12/02/19 16:42 99-09-211/26/19 18:2320.0 2.3 1
4-Nitroaniline ND ug/L 12/02/19 16:42 100-01-611/26/19 18:2320.0 2.2 1
Nitrobenzene ND ug/L 12/02/19 16:42 98-95-311/26/19 18:2310.0 2.1 1
2-Nitrophenol ND ug/L 12/02/19 16:42 88-75-511/26/19 18:2310.0 1.4 1
4-Nitrophenol ND ug/L 12/02/19 16:42 100-02-711/26/19 18:2350.0 3.5 1
N-Nitrosodimethylamine ND ug/L 12/02/19 16:42 62-75-911/26/19 18:2310.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 12/02/19 16:42 621-64-711/26/19 18:2310.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 12/02/19 16:42 86-30-611/26/19 18:2310.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 12/02/19 16:42 108-60-111/26/19 18:2310.0 2.8 1
Pentachlorophenol ND ug/L 12/02/19 16:42 87-86-511/26/19 18:2325.0 2.2 1
Phenanthrene ND ug/L 12/02/19 16:42 85-01-811/26/19 18:2310.0 1.7 1
Phenol ND ug/L 12/02/19 16:42 108-95-211/26/19 18:2310.0 0.92 1
Pyrene ND ug/L 12/02/19 16:42 129-00-011/26/19 18:2310.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 12/02/19 16:42 120-82-111/26/19 18:2310.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 12/02/19 16:42 95-95-411/26/19 18:2310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 12/02/19 16:42 88-06-211/26/19 18:2310.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)75 %12/02/19 16:42 4165-60-011/26/19 18:2313-130 1
2-Fluorobiphenyl (S)73 %12/02/19 16:42 321-60-811/26/19 18:2313-130 1
Terphenyl-d14 (S)103 %12/02/19 16:42 1718-51-011/26/19 18:2325-130 1
Phenol-d6 (S)46 %12/02/19 16:42 13127-88-311/26/19 18:2310-130 1
2-Fluorophenol (S)59 %12/02/19 16:42 367-12-411/26/19 18:2310-130 1
2,4,6-Tribromophenol (S)107 %12/02/19 16:42 118-79-611/26/19 18:2310-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 12/06/19 03:14 67-64-125.0 6.2 1
Benzene ND ug/L 12/06/19 03:14 71-43-21.0 0.15 1
Bromobenzene ND ug/L 12/06/19 03:14 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-2 Lab ID: 92455128001 Collected: 11/22/19 09:05 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 12/06/19 03:14 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 12/06/19 03:14 75-27-41.0 0.26 1
Bromoform ND ug/L 12/06/19 03:14 75-25-21.0 0.62 1
Bromomethane ND ug/L 12/06/19 03:14 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 12/06/19 03:14 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 12/06/19 03:14 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 12/06/19 03:14 108-90-71.0 0.23 1
Chloroethane ND ug/L 12/06/19 03:14 75-00-31.0 0.49 1
Chloroform ND ug/L 12/06/19 03:14 67-66-35.0 2.3 1
Chloromethane ND ug/L 12/06/19 03:14 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 12/06/19 03:14 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 12/06/19 03:14 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/19 03:14 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 12/06/19 03:14 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/19 03:14 106-93-41.0 0.26 1
Dibromomethane ND ug/L 12/06/19 03:14 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 12/06/19 03:14 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 12/06/19 03:14 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 12/06/19 03:14 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 12/06/19 03:14 75-71-81.0 0.23 1
1,1-Dichloroethane 3.2 ug/L 12/06/19 03:14 75-34-31.0 0.27 1
1,2-Dichloroethane 0.63J ug/L 12/06/19 03:14 107-06-21.0 0.34 1
1,1-Dichloroethene 55.9 ug/L 12/06/19 03:14 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 12/06/19 03:14 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 12/06/19 03:14 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 12/06/19 03:14 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 12/06/19 03:14 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 12/06/19 03:14 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 12/06/19 03:14 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 12/06/19 03:14 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 12/06/19 03:14 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 12/06/19 03:14 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 12/06/19 03:14 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 12/06/19 03:14 87-68-31.0 0.44 1
2-Hexanone ND ug/L 12/06/19 03:14 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 12/06/19 03:14 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 12/06/19 03:14 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/19 03:14 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 12/06/19 03:14 1634-04-41.0 0.28 1
Naphthalene ND ug/L 12/06/19 03:14 91-20-31.0 0.35 1
Styrene ND ug/L 12/06/19 03:14 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/19 03:14 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/19 03:14 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 12/06/19 03:14 127-18-41.0 0.16 1
Toluene ND ug/L 12/06/19 03:14 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/06/19 03:14 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-2 Lab ID: 92455128001 Collected: 11/22/19 09:05 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 12/06/19 03:14 120-82-11.0 0.22 1
1,1,1-Trichloroethane 8.4 ug/L 12/06/19 03:14 71-55-61.0 0.18 1
1,1,2-Trichloroethane 0.32J ug/L 12/06/19 03:14 79-00-51.0 0.24 1
Trichloroethene ND ug/L 12/06/19 03:14 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 12/06/19 03:14 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 12/06/19 03:14 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 12/06/19 03:14 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 12/06/19 03:14 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 12/06/19 03:14 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 12/06/19 03:14 179601-23-12.0 0.41 1
o-Xylene ND ug/L 12/06/19 03:14 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)97 %12/06/19 03:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %12/06/19 03:14 17060-07-070-130 1
Toluene-d8 (S)96 %12/06/19 03:14 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.8260D MSV SIM
1,4-Dioxane (p-Dioxane)39.9 ug/L 11/26/19 13:40 123-91-12.0 1.2 1
Surrogates
1,2-Dichloroethane-d4 (S)113 %11/26/19 13:40 17060-07-050-150 1
Toluene-d8 (S)92 %11/26/19 13:40 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-1 Lab ID: 92455128002 Collected: 11/22/19 11:30 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/26/19 22:44 7440-38-211/26/19 02:2410.0 4.7 1
Barium 504 ug/L 11/26/19 22:44 7440-39-311/26/19 02:245.0 1.0 1
Cadmium ND ug/L 11/26/19 22:44 7440-43-911/26/19 02:241.0 0.40 1
Chromium 8.8 ug/L 11/26/19 22:44 7440-47-311/26/19 02:245.0 1.0 1
Lead ND ug/L 11/26/19 22:44 7439-92-111/26/19 02:245.0 1.6 1
Selenium ND ug/L 11/26/19 22:44 7782-49-211/26/19 02:2410.0 4.7 1
Silver ND ug/L 11/26/19 22:44 7440-22-411/26/19 02:245.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 12/03/19 14:44 7439-97-612/03/19 11:020.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 12/02/19 17:13 83-32-911/26/19 18:2310.0 1.6 1
Acenaphthylene ND ug/L 12/02/19 17:13 208-96-811/26/19 18:2310.0 1.6 1
Aniline ND ug/L 12/02/19 17:13 62-53-3 v211/26/19 18:2310.0 1.9 1
Anthracene ND ug/L 12/02/19 17:13 120-12-711/26/19 18:2310.0 1.7 1
Benzo(a)anthracene ND ug/L 12/02/19 17:13 56-55-311/26/19 18:2310.0 1.8 1
Benzo(a)pyrene ND ug/L 12/02/19 17:13 50-32-811/26/19 18:2310.0 2.1 1
Benzo(b)fluoranthene ND ug/L 12/02/19 17:13 205-99-211/26/19 18:2310.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 12/02/19 17:13 191-24-211/26/19 18:2310.0 1.4 1
Benzo(k)fluoranthene ND ug/L 12/02/19 17:13 207-08-911/26/19 18:2310.0 1.9 1
Benzoic Acid ND ug/L 12/02/19 17:13 65-85-011/26/19 18:2350.0 43.0 1
Benzyl alcohol ND ug/L 12/02/19 17:13 100-51-611/26/19 18:2320.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 12/02/19 17:13 101-55-311/26/19 18:2310.0 1.6 1
Butylbenzylphthalate ND ug/L 12/02/19 17:13 85-68-711/26/19 18:2310.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 12/02/19 17:13 59-50-711/26/19 18:2320.0 2.8 1
4-Chloroaniline ND ug/L 12/02/19 17:13 106-47-811/26/19 18:2320.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 12/02/19 17:13 111-91-111/26/19 18:2310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 12/02/19 17:13 111-44-4 v111/26/19 18:2310.0 1.8 1
2-Chloronaphthalene ND ug/L 12/02/19 17:13 91-58-711/26/19 18:2310.0 1.5 1
2-Chlorophenol ND ug/L 12/02/19 17:13 95-57-811/26/19 18:2310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 12/02/19 17:13 7005-72-311/26/19 18:2310.0 1.6 1
Chrysene ND ug/L 12/02/19 17:13 218-01-911/26/19 18:2310.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 12/02/19 17:13 53-70-311/26/19 18:2310.0 1.6 1
Dibenzofuran ND ug/L 12/02/19 17:13 132-64-911/26/19 18:2310.0 1.5 1
1,2-Dichlorobenzene ND ug/L 12/02/19 17:13 95-50-111/26/19 18:2310.0 1.3 1
1,3-Dichlorobenzene ND ug/L 12/02/19 17:13 541-73-111/26/19 18:2310.0 1.5 1
1,4-Dichlorobenzene ND ug/L 12/02/19 17:13 106-46-711/26/19 18:2310.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 12/02/19 17:13 91-94-111/26/19 18:2320.0 3.0 1
2,4-Dichlorophenol ND ug/L 12/02/19 17:13 120-83-211/26/19 18:2310.0 1.4 1
Diethylphthalate ND ug/L 12/02/19 17:13 84-66-211/26/19 18:2310.0 2.4 1
2,4-Dimethylphenol ND ug/L 12/02/19 17:13 105-67-911/26/19 18:2310.0 1.4 1
Dimethylphthalate ND ug/L 12/02/19 17:13 131-11-311/26/19 18:2310.0 1.6 1
Di-n-butylphthalate ND ug/L 12/02/19 17:13 84-74-211/26/19 18:2310.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 12/02/19 17:13 534-52-111/26/19 18:2320.0 15.2 1
2,4-Dinitrophenol ND ug/L 12/02/19 17:13 51-28-511/26/19 18:2350.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-1 Lab ID: 92455128002 Collected: 11/22/19 11:30 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 12/02/19 17:13 121-14-211/26/19 18:2310.0 1.2 1
2,6-Dinitrotoluene ND ug/L 12/02/19 17:13 606-20-211/26/19 18:2310.0 1.4 1
Di-n-octylphthalate ND ug/L 12/02/19 17:13 117-84-011/26/19 18:2310.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/02/19 17:13 117-81-711/26/19 18:236.0 2.1 1
Fluoranthene ND ug/L 12/02/19 17:13 206-44-011/26/19 18:2310.0 1.7 1
Fluorene ND ug/L 12/02/19 17:13 86-73-711/26/19 18:2310.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 12/02/19 17:13 87-68-311/26/19 18:2310.0 2.0 1
Hexachlorobenzene ND ug/L 12/02/19 17:13 118-74-111/26/19 18:2310.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 12/02/19 17:13 77-47-411/26/19 18:2310.0 1.7 1
Hexachloroethane ND ug/L 12/02/19 17:13 67-72-111/26/19 18:2310.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 12/02/19 17:13 193-39-511/26/19 18:2310.0 1.6 1
Isophorone ND ug/L 12/02/19 17:13 78-59-111/26/19 18:2310.0 1.6 1
1-Methylnaphthalene ND ug/L 12/02/19 17:13 90-12-011/26/19 18:2310.0 1.4 1
2-Methylnaphthalene ND ug/L 12/02/19 17:13 91-57-611/26/19 18:2310.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 12/02/19 17:13 95-48-711/26/19 18:2310.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/02/19 17:13 15831-10-411/26/19 18:2310.0 1.2 1
Naphthalene ND ug/L 12/02/19 17:13 91-20-311/26/19 18:2310.0 1.4 1
2-Nitroaniline ND ug/L 12/02/19 17:13 88-74-411/26/19 18:2320.0 4.2 1
3-Nitroaniline ND ug/L 12/02/19 17:13 99-09-211/26/19 18:2320.0 2.3 1
4-Nitroaniline ND ug/L 12/02/19 17:13 100-01-611/26/19 18:2320.0 2.2 1
Nitrobenzene ND ug/L 12/02/19 17:13 98-95-311/26/19 18:2310.0 2.1 1
2-Nitrophenol ND ug/L 12/02/19 17:13 88-75-511/26/19 18:2310.0 1.4 1
4-Nitrophenol ND ug/L 12/02/19 17:13 100-02-711/26/19 18:2350.0 3.5 1
N-Nitrosodimethylamine ND ug/L 12/02/19 17:13 62-75-911/26/19 18:2310.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 12/02/19 17:13 621-64-711/26/19 18:2310.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 12/02/19 17:13 86-30-611/26/19 18:2310.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 12/02/19 17:13 108-60-111/26/19 18:2310.0 2.8 1
Pentachlorophenol ND ug/L 12/02/19 17:13 87-86-511/26/19 18:2325.0 2.2 1
Phenanthrene ND ug/L 12/02/19 17:13 85-01-811/26/19 18:2310.0 1.7 1
Phenol ND ug/L 12/02/19 17:13 108-95-211/26/19 18:2310.0 0.92 1
Pyrene ND ug/L 12/02/19 17:13 129-00-011/26/19 18:2310.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 12/02/19 17:13 120-82-111/26/19 18:2310.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 12/02/19 17:13 95-95-411/26/19 18:2310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 12/02/19 17:13 88-06-211/26/19 18:2310.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)78 %12/02/19 17:13 4165-60-011/26/19 18:2313-130 1
2-Fluorobiphenyl (S)81 %12/02/19 17:13 321-60-811/26/19 18:2313-130 1
Terphenyl-d14 (S)97 %12/02/19 17:13 1718-51-011/26/19 18:2325-130 1
Phenol-d6 (S)51 %12/02/19 17:13 13127-88-311/26/19 18:2310-130 1
2-Fluorophenol (S)64 %12/02/19 17:13 367-12-411/26/19 18:2310-130 1
2,4,6-Tribromophenol (S)104 %12/02/19 17:13 118-79-611/26/19 18:2310-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 12/06/19 03:32 67-64-125.0 6.2 1
Benzene ND ug/L 12/06/19 03:32 71-43-21.0 0.15 1
Bromobenzene ND ug/L 12/06/19 03:32 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-1 Lab ID: 92455128002 Collected: 11/22/19 11:30 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 12/06/19 03:32 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 12/06/19 03:32 75-27-41.0 0.26 1
Bromoform ND ug/L 12/06/19 03:32 75-25-21.0 0.62 1
Bromomethane ND ug/L 12/06/19 03:32 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 12/06/19 03:32 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 12/06/19 03:32 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 12/06/19 03:32 108-90-71.0 0.23 1
Chloroethane ND ug/L 12/06/19 03:32 75-00-31.0 0.49 1
Chloroform ND ug/L 12/06/19 03:32 67-66-35.0 2.3 1
Chloromethane ND ug/L 12/06/19 03:32 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 12/06/19 03:32 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 12/06/19 03:32 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/19 03:32 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 12/06/19 03:32 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/19 03:32 106-93-41.0 0.26 1
Dibromomethane ND ug/L 12/06/19 03:32 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 12/06/19 03:32 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 12/06/19 03:32 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 12/06/19 03:32 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 12/06/19 03:32 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 12/06/19 03:32 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 12/06/19 03:32 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 12/06/19 03:32 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 12/06/19 03:32 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 12/06/19 03:32 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 12/06/19 03:32 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 12/06/19 03:32 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 12/06/19 03:32 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 12/06/19 03:32 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 12/06/19 03:32 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 12/06/19 03:32 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 12/06/19 03:32 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 12/06/19 03:32 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 12/06/19 03:32 87-68-31.0 0.44 1
2-Hexanone ND ug/L 12/06/19 03:32 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 12/06/19 03:32 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 12/06/19 03:32 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/19 03:32 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 12/06/19 03:32 1634-04-41.0 0.28 1
Naphthalene ND ug/L 12/06/19 03:32 91-20-31.0 0.35 1
Styrene ND ug/L 12/06/19 03:32 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/19 03:32 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/19 03:32 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 12/06/19 03:32 127-18-41.0 0.16 1
Toluene ND ug/L 12/06/19 03:32 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/06/19 03:32 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-1 Lab ID: 92455128002 Collected: 11/22/19 11:30 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 12/06/19 03:32 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 12/06/19 03:32 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 12/06/19 03:32 79-00-51.0 0.24 1
Trichloroethene ND ug/L 12/06/19 03:32 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 12/06/19 03:32 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 12/06/19 03:32 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 12/06/19 03:32 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 12/06/19 03:32 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 12/06/19 03:32 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 12/06/19 03:32 179601-23-12.0 0.41 1
o-Xylene ND ug/L 12/06/19 03:32 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)95 %12/06/19 03:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %12/06/19 03:32 17060-07-070-130 1
Toluene-d8 (S)97 %12/06/19 03:32 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/26/19 13:59 123-91-12.0 1.2 1
Surrogates
1,2-Dichloroethane-d4 (S)115 %11/26/19 13:59 17060-07-050-150 1
Toluene-d8 (S)95 %11/26/19 13:59 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-4 Lab ID: 92455128003 Collected: 11/22/19 12:55 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/26/19 22:47 7440-38-211/26/19 02:2410.0 4.7 1
Barium 126 ug/L 11/26/19 22:47 7440-39-311/26/19 02:245.0 1.0 1
Cadmium ND ug/L 11/26/19 22:47 7440-43-911/26/19 02:241.0 0.40 1
Chromium ND ug/L 11/26/19 22:47 7440-47-311/26/19 02:245.0 1.0 1
Lead ND ug/L 11/26/19 22:47 7439-92-111/26/19 02:245.0 1.6 1
Selenium ND ug/L 11/26/19 22:47 7782-49-211/26/19 02:2410.0 4.7 1
Silver ND ug/L 11/26/19 22:47 7440-22-411/26/19 02:245.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 12/03/19 14:46 7439-97-612/03/19 11:020.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 12/02/19 17:44 83-32-911/26/19 18:2310.0 1.6 1
Acenaphthylene ND ug/L 12/02/19 17:44 208-96-811/26/19 18:2310.0 1.6 1
Aniline ND ug/L 12/02/19 17:44 62-53-3 v211/26/19 18:2310.0 1.9 1
Anthracene ND ug/L 12/02/19 17:44 120-12-711/26/19 18:2310.0 1.7 1
Benzo(a)anthracene ND ug/L 12/02/19 17:44 56-55-311/26/19 18:2310.0 1.8 1
Benzo(a)pyrene ND ug/L 12/02/19 17:44 50-32-811/26/19 18:2310.0 2.1 1
Benzo(b)fluoranthene ND ug/L 12/02/19 17:44 205-99-211/26/19 18:2310.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 12/02/19 17:44 191-24-211/26/19 18:2310.0 1.4 1
Benzo(k)fluoranthene ND ug/L 12/02/19 17:44 207-08-911/26/19 18:2310.0 1.9 1
Benzoic Acid ND ug/L 12/02/19 17:44 65-85-011/26/19 18:2350.0 43.0 1
Benzyl alcohol ND ug/L 12/02/19 17:44 100-51-611/26/19 18:2320.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 12/02/19 17:44 101-55-311/26/19 18:2310.0 1.6 1
Butylbenzylphthalate ND ug/L 12/02/19 17:44 85-68-711/26/19 18:2310.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 12/02/19 17:44 59-50-711/26/19 18:2320.0 2.8 1
4-Chloroaniline ND ug/L 12/02/19 17:44 106-47-811/26/19 18:2320.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 12/02/19 17:44 111-91-111/26/19 18:2310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 12/02/19 17:44 111-44-4 v111/26/19 18:2310.0 1.8 1
2-Chloronaphthalene ND ug/L 12/02/19 17:44 91-58-711/26/19 18:2310.0 1.5 1
2-Chlorophenol ND ug/L 12/02/19 17:44 95-57-811/26/19 18:2310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 12/02/19 17:44 7005-72-311/26/19 18:2310.0 1.6 1
Chrysene ND ug/L 12/02/19 17:44 218-01-911/26/19 18:2310.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 12/02/19 17:44 53-70-311/26/19 18:2310.0 1.6 1
Dibenzofuran ND ug/L 12/02/19 17:44 132-64-911/26/19 18:2310.0 1.5 1
1,2-Dichlorobenzene ND ug/L 12/02/19 17:44 95-50-111/26/19 18:2310.0 1.3 1
1,3-Dichlorobenzene ND ug/L 12/02/19 17:44 541-73-111/26/19 18:2310.0 1.5 1
1,4-Dichlorobenzene ND ug/L 12/02/19 17:44 106-46-711/26/19 18:2310.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 12/02/19 17:44 91-94-111/26/19 18:2320.0 3.0 1
2,4-Dichlorophenol ND ug/L 12/02/19 17:44 120-83-211/26/19 18:2310.0 1.4 1
Diethylphthalate 6.9J ug/L 12/02/19 17:44 84-66-211/26/19 18:2310.0 2.4 1
2,4-Dimethylphenol ND ug/L 12/02/19 17:44 105-67-911/26/19 18:2310.0 1.4 1
Dimethylphthalate ND ug/L 12/02/19 17:44 131-11-311/26/19 18:2310.0 1.6 1
Di-n-butylphthalate ND ug/L 12/02/19 17:44 84-74-211/26/19 18:2310.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 12/02/19 17:44 534-52-111/26/19 18:2320.0 15.2 1
2,4-Dinitrophenol ND ug/L 12/02/19 17:44 51-28-511/26/19 18:2350.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-4 Lab ID: 92455128003 Collected: 11/22/19 12:55 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 12/02/19 17:44 121-14-211/26/19 18:2310.0 1.2 1
2,6-Dinitrotoluene ND ug/L 12/02/19 17:44 606-20-211/26/19 18:2310.0 1.4 1
Di-n-octylphthalate ND ug/L 12/02/19 17:44 117-84-011/26/19 18:2310.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/02/19 17:44 117-81-711/26/19 18:236.0 2.1 1
Fluoranthene ND ug/L 12/02/19 17:44 206-44-011/26/19 18:2310.0 1.7 1
Fluorene ND ug/L 12/02/19 17:44 86-73-711/26/19 18:2310.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 12/02/19 17:44 87-68-311/26/19 18:2310.0 2.0 1
Hexachlorobenzene ND ug/L 12/02/19 17:44 118-74-111/26/19 18:2310.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 12/02/19 17:44 77-47-411/26/19 18:2310.0 1.7 1
Hexachloroethane ND ug/L 12/02/19 17:44 67-72-111/26/19 18:2310.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 12/02/19 17:44 193-39-511/26/19 18:2310.0 1.6 1
Isophorone ND ug/L 12/02/19 17:44 78-59-111/26/19 18:2310.0 1.6 1
1-Methylnaphthalene ND ug/L 12/02/19 17:44 90-12-011/26/19 18:2310.0 1.4 1
2-Methylnaphthalene ND ug/L 12/02/19 17:44 91-57-611/26/19 18:2310.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 12/02/19 17:44 95-48-711/26/19 18:2310.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/02/19 17:44 15831-10-411/26/19 18:2310.0 1.2 1
Naphthalene ND ug/L 12/02/19 17:44 91-20-311/26/19 18:2310.0 1.4 1
2-Nitroaniline ND ug/L 12/02/19 17:44 88-74-411/26/19 18:2320.0 4.2 1
3-Nitroaniline ND ug/L 12/02/19 17:44 99-09-211/26/19 18:2320.0 2.3 1
4-Nitroaniline ND ug/L 12/02/19 17:44 100-01-611/26/19 18:2320.0 2.2 1
Nitrobenzene ND ug/L 12/02/19 17:44 98-95-311/26/19 18:2310.0 2.1 1
2-Nitrophenol ND ug/L 12/02/19 17:44 88-75-511/26/19 18:2310.0 1.4 1
4-Nitrophenol ND ug/L 12/02/19 17:44 100-02-711/26/19 18:2350.0 3.5 1
N-Nitrosodimethylamine ND ug/L 12/02/19 17:44 62-75-911/26/19 18:2310.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 12/02/19 17:44 621-64-711/26/19 18:2310.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 12/02/19 17:44 86-30-611/26/19 18:2310.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 12/02/19 17:44 108-60-111/26/19 18:2310.0 2.8 1
Pentachlorophenol ND ug/L 12/02/19 17:44 87-86-511/26/19 18:2325.0 2.2 1
Phenanthrene ND ug/L 12/02/19 17:44 85-01-811/26/19 18:2310.0 1.7 1
Phenol ND ug/L 12/02/19 17:44 108-95-211/26/19 18:2310.0 0.92 1
Pyrene ND ug/L 12/02/19 17:44 129-00-011/26/19 18:2310.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 12/02/19 17:44 120-82-111/26/19 18:2310.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 12/02/19 17:44 95-95-411/26/19 18:2310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 12/02/19 17:44 88-06-211/26/19 18:2310.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)36 %12/02/19 17:44 4165-60-011/26/19 18:2313-130 1
2-Fluorobiphenyl (S)32 %12/02/19 17:44 321-60-811/26/19 18:2313-130 1
Terphenyl-d14 (S)43 %12/02/19 17:44 1718-51-011/26/19 18:2325-130 1
Phenol-d6 (S)24 %12/02/19 17:44 13127-88-311/26/19 18:2310-130 1
2-Fluorophenol (S)30 %12/02/19 17:44 367-12-411/26/19 18:2310-130 1
2,4,6-Tribromophenol (S)41 %12/02/19 17:44 118-79-611/26/19 18:2310-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 12/06/19 03:49 67-64-125.0 6.2 1
Benzene ND ug/L 12/06/19 03:49 71-43-21.0 0.15 1
Bromobenzene ND ug/L 12/06/19 03:49 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-4 Lab ID: 92455128003 Collected: 11/22/19 12:55 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 12/06/19 03:49 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 12/06/19 03:49 75-27-41.0 0.26 1
Bromoform ND ug/L 12/06/19 03:49 75-25-21.0 0.62 1
Bromomethane ND ug/L 12/06/19 03:49 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 12/06/19 03:49 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 12/06/19 03:49 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 12/06/19 03:49 108-90-71.0 0.23 1
Chloroethane ND ug/L 12/06/19 03:49 75-00-31.0 0.49 1
Chloroform ND ug/L 12/06/19 03:49 67-66-35.0 2.3 1
Chloromethane ND ug/L 12/06/19 03:49 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 12/06/19 03:49 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 12/06/19 03:49 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/19 03:49 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 12/06/19 03:49 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/19 03:49 106-93-41.0 0.26 1
Dibromomethane ND ug/L 12/06/19 03:49 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 12/06/19 03:49 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 12/06/19 03:49 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 12/06/19 03:49 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 12/06/19 03:49 75-71-81.0 0.23 1
1,1-Dichloroethane 0.91J ug/L 12/06/19 03:49 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 12/06/19 03:49 107-06-21.0 0.34 1
1,1-Dichloroethene 23.5 ug/L 12/06/19 03:49 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 12/06/19 03:49 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 12/06/19 03:49 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 12/06/19 03:49 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 12/06/19 03:49 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 12/06/19 03:49 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 12/06/19 03:49 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 12/06/19 03:49 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 12/06/19 03:49 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 12/06/19 03:49 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 12/06/19 03:49 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 12/06/19 03:49 87-68-31.0 0.44 1
2-Hexanone ND ug/L 12/06/19 03:49 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 12/06/19 03:49 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 12/06/19 03:49 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/19 03:49 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 12/06/19 03:49 1634-04-41.0 0.28 1
Naphthalene ND ug/L 12/06/19 03:49 91-20-31.0 0.35 1
Styrene ND ug/L 12/06/19 03:49 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/19 03:49 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/19 03:49 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 12/06/19 03:49 127-18-41.0 0.16 1
Toluene ND ug/L 12/06/19 03:49 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/06/19 03:49 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: MW-4 Lab ID: 92455128003 Collected: 11/22/19 12:55 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 12/06/19 03:49 120-82-11.0 0.22 1
1,1,1-Trichloroethane 1.1 ug/L 12/06/19 03:49 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 12/06/19 03:49 79-00-51.0 0.24 1
Trichloroethene ND ug/L 12/06/19 03:49 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 12/06/19 03:49 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 12/06/19 03:49 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 12/06/19 03:49 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 12/06/19 03:49 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 12/06/19 03:49 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 12/06/19 03:49 179601-23-12.0 0.41 1
o-Xylene ND ug/L 12/06/19 03:49 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)98 %12/06/19 03:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %12/06/19 03:49 17060-07-070-130 1
Toluene-d8 (S)96 %12/06/19 03:49 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.8260D MSV SIM
1,4-Dioxane (p-Dioxane)8.9 ug/L 11/26/19 14:19 123-91-12.0 1.2 1
Surrogates
1,2-Dichloroethane-d4 (S)116 %11/26/19 14:19 17060-07-050-150 1
Toluene-d8 (S)95 %11/26/19 14:19 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: DUP-2-GW Lab ID: 92455128004 Collected: 11/22/19 00:00 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/27/19 23:44 7440-38-211/26/19 02:2410.0 4.7 1
Barium 118 ug/L 11/27/19 23:44 7440-39-311/26/19 02:245.0 1.0 1
Cadmium ND ug/L 11/27/19 23:44 7440-43-911/26/19 02:241.0 0.40 1
Chromium ND ug/L 11/27/19 23:44 7440-47-311/26/19 02:245.0 1.0 1
Lead ND ug/L 11/27/19 23:44 7439-92-111/26/19 02:245.0 1.6 1
Selenium ND ug/L 11/27/19 23:44 7782-49-211/26/19 02:2410.0 4.7 1
Silver ND ug/L 11/27/19 23:44 7440-22-411/26/19 02:245.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 12/03/19 14:51 7439-97-612/03/19 11:020.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 12/02/19 18:14 83-32-911/26/19 18:2310.0 1.6 1
Acenaphthylene ND ug/L 12/02/19 18:14 208-96-811/26/19 18:2310.0 1.6 1
Aniline ND ug/L 12/02/19 18:14 62-53-3 v211/26/19 18:2310.0 1.9 1
Anthracene ND ug/L 12/02/19 18:14 120-12-711/26/19 18:2310.0 1.7 1
Benzo(a)anthracene ND ug/L 12/02/19 18:14 56-55-311/26/19 18:2310.0 1.8 1
Benzo(a)pyrene ND ug/L 12/02/19 18:14 50-32-811/26/19 18:2310.0 2.1 1
Benzo(b)fluoranthene ND ug/L 12/02/19 18:14 205-99-211/26/19 18:2310.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 12/02/19 18:14 191-24-211/26/19 18:2310.0 1.4 1
Benzo(k)fluoranthene ND ug/L 12/02/19 18:14 207-08-911/26/19 18:2310.0 1.9 1
Benzoic Acid ND ug/L 12/02/19 18:14 65-85-011/26/19 18:2350.0 43.0 1
Benzyl alcohol ND ug/L 12/02/19 18:14 100-51-611/26/19 18:2320.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 12/02/19 18:14 101-55-311/26/19 18:2310.0 1.6 1
Butylbenzylphthalate ND ug/L 12/02/19 18:14 85-68-711/26/19 18:2310.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 12/02/19 18:14 59-50-711/26/19 18:2320.0 2.8 1
4-Chloroaniline ND ug/L 12/02/19 18:14 106-47-811/26/19 18:2320.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 12/02/19 18:14 111-91-111/26/19 18:2310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 12/02/19 18:14 111-44-4 v111/26/19 18:2310.0 1.8 1
2-Chloronaphthalene ND ug/L 12/02/19 18:14 91-58-711/26/19 18:2310.0 1.5 1
2-Chlorophenol ND ug/L 12/02/19 18:14 95-57-811/26/19 18:2310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 12/02/19 18:14 7005-72-311/26/19 18:2310.0 1.6 1
Chrysene ND ug/L 12/02/19 18:14 218-01-911/26/19 18:2310.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 12/02/19 18:14 53-70-311/26/19 18:2310.0 1.6 1
Dibenzofuran ND ug/L 12/02/19 18:14 132-64-911/26/19 18:2310.0 1.5 1
1,2-Dichlorobenzene ND ug/L 12/02/19 18:14 95-50-111/26/19 18:2310.0 1.3 1
1,3-Dichlorobenzene ND ug/L 12/02/19 18:14 541-73-111/26/19 18:2310.0 1.5 1
1,4-Dichlorobenzene ND ug/L 12/02/19 18:14 106-46-711/26/19 18:2310.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 12/02/19 18:14 91-94-111/26/19 18:2320.0 3.0 1
2,4-Dichlorophenol ND ug/L 12/02/19 18:14 120-83-211/26/19 18:2310.0 1.4 1
Diethylphthalate 10J ug/L 12/02/19 18:14 84-66-211/26/19 18:2310.0 2.4 1
2,4-Dimethylphenol ND ug/L 12/02/19 18:14 105-67-911/26/19 18:2310.0 1.4 1
Dimethylphthalate ND ug/L 12/02/19 18:14 131-11-311/26/19 18:2310.0 1.6 1
Di-n-butylphthalate ND ug/L 12/02/19 18:14 84-74-211/26/19 18:2310.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 12/02/19 18:14 534-52-111/26/19 18:2320.0 15.2 1
2,4-Dinitrophenol ND ug/L 12/02/19 18:14 51-28-511/26/19 18:2350.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: DUP-2-GW Lab ID: 92455128004 Collected: 11/22/19 00:00 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 12/02/19 18:14 121-14-211/26/19 18:2310.0 1.2 1
2,6-Dinitrotoluene ND ug/L 12/02/19 18:14 606-20-211/26/19 18:2310.0 1.4 1
Di-n-octylphthalate ND ug/L 12/02/19 18:14 117-84-011/26/19 18:2310.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 12/02/19 18:14 117-81-711/26/19 18:236.0 2.1 1
Fluoranthene ND ug/L 12/02/19 18:14 206-44-011/26/19 18:2310.0 1.7 1
Fluorene ND ug/L 12/02/19 18:14 86-73-711/26/19 18:2310.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 12/02/19 18:14 87-68-311/26/19 18:2310.0 2.0 1
Hexachlorobenzene ND ug/L 12/02/19 18:14 118-74-111/26/19 18:2310.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 12/02/19 18:14 77-47-411/26/19 18:2310.0 1.7 1
Hexachloroethane ND ug/L 12/02/19 18:14 67-72-111/26/19 18:2310.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 12/02/19 18:14 193-39-511/26/19 18:2310.0 1.6 1
Isophorone ND ug/L 12/02/19 18:14 78-59-111/26/19 18:2310.0 1.6 1
1-Methylnaphthalene ND ug/L 12/02/19 18:14 90-12-011/26/19 18:2310.0 1.4 1
2-Methylnaphthalene ND ug/L 12/02/19 18:14 91-57-611/26/19 18:2310.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 12/02/19 18:14 95-48-711/26/19 18:2310.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 12/02/19 18:14 15831-10-411/26/19 18:2310.0 1.2 1
Naphthalene ND ug/L 12/02/19 18:14 91-20-311/26/19 18:2310.0 1.4 1
2-Nitroaniline ND ug/L 12/02/19 18:14 88-74-411/26/19 18:2320.0 4.2 1
3-Nitroaniline ND ug/L 12/02/19 18:14 99-09-211/26/19 18:2320.0 2.3 1
4-Nitroaniline ND ug/L 12/02/19 18:14 100-01-611/26/19 18:2320.0 2.2 1
Nitrobenzene ND ug/L 12/02/19 18:14 98-95-311/26/19 18:2310.0 2.1 1
2-Nitrophenol ND ug/L 12/02/19 18:14 88-75-511/26/19 18:2310.0 1.4 1
4-Nitrophenol ND ug/L 12/02/19 18:14 100-02-711/26/19 18:2350.0 3.5 1
N-Nitrosodimethylamine ND ug/L 12/02/19 18:14 62-75-911/26/19 18:2310.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 12/02/19 18:14 621-64-711/26/19 18:2310.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 12/02/19 18:14 86-30-611/26/19 18:2310.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 12/02/19 18:14 108-60-111/26/19 18:2310.0 2.8 1
Pentachlorophenol ND ug/L 12/02/19 18:14 87-86-511/26/19 18:2325.0 2.2 1
Phenanthrene ND ug/L 12/02/19 18:14 85-01-811/26/19 18:2310.0 1.7 1
Phenol ND ug/L 12/02/19 18:14 108-95-211/26/19 18:2310.0 0.92 1
Pyrene ND ug/L 12/02/19 18:14 129-00-011/26/19 18:2310.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 12/02/19 18:14 120-82-111/26/19 18:2310.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 12/02/19 18:14 95-95-411/26/19 18:2310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 12/02/19 18:14 88-06-211/26/19 18:2310.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)68 %12/02/19 18:14 4165-60-011/26/19 18:2313-130 1
2-Fluorobiphenyl (S)64 %12/02/19 18:14 321-60-811/26/19 18:2313-130 1
Terphenyl-d14 (S)87 %12/02/19 18:14 1718-51-011/26/19 18:2325-130 1
Phenol-d6 (S)44 %12/02/19 18:14 13127-88-311/26/19 18:2310-130 1
2-Fluorophenol (S)55 %12/02/19 18:14 367-12-411/26/19 18:2310-130 1
2,4,6-Tribromophenol (S)91 %12/02/19 18:14 118-79-611/26/19 18:2310-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 12/06/19 04:06 67-64-125.0 6.2 1
Benzene ND ug/L 12/06/19 04:06 71-43-21.0 0.15 1
Bromobenzene ND ug/L 12/06/19 04:06 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: DUP-2-GW Lab ID: 92455128004 Collected: 11/22/19 00:00 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 12/06/19 04:06 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 12/06/19 04:06 75-27-41.0 0.26 1
Bromoform ND ug/L 12/06/19 04:06 75-25-21.0 0.62 1
Bromomethane ND ug/L 12/06/19 04:06 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 12/06/19 04:06 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 12/06/19 04:06 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 12/06/19 04:06 108-90-71.0 0.23 1
Chloroethane ND ug/L 12/06/19 04:06 75-00-31.0 0.49 1
Chloroform ND ug/L 12/06/19 04:06 67-66-35.0 2.3 1
Chloromethane ND ug/L 12/06/19 04:06 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 12/06/19 04:06 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 12/06/19 04:06 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 12/06/19 04:06 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 12/06/19 04:06 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 12/06/19 04:06 106-93-41.0 0.26 1
Dibromomethane ND ug/L 12/06/19 04:06 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 12/06/19 04:06 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 12/06/19 04:06 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 12/06/19 04:06 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 12/06/19 04:06 75-71-81.0 0.23 1
1,1-Dichloroethane 0.89J ug/L 12/06/19 04:06 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 12/06/19 04:06 107-06-21.0 0.34 1
1,1-Dichloroethene 22.3 ug/L 12/06/19 04:06 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 12/06/19 04:06 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 12/06/19 04:06 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 12/06/19 04:06 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 12/06/19 04:06 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 12/06/19 04:06 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 12/06/19 04:06 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 12/06/19 04:06 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 12/06/19 04:06 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 12/06/19 04:06 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 12/06/19 04:06 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 12/06/19 04:06 87-68-31.0 0.44 1
2-Hexanone ND ug/L 12/06/19 04:06 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 12/06/19 04:06 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 12/06/19 04:06 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/06/19 04:06 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 12/06/19 04:06 1634-04-41.0 0.28 1
Naphthalene ND ug/L 12/06/19 04:06 91-20-31.0 0.35 1
Styrene ND ug/L 12/06/19 04:06 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 12/06/19 04:06 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 12/06/19 04:06 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 12/06/19 04:06 127-18-41.0 0.16 1
Toluene ND ug/L 12/06/19 04:06 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/06/19 04:06 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: DUP-2-GW Lab ID: 92455128004 Collected: 11/22/19 00:00 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 12/06/19 04:06 120-82-11.0 0.22 1
1,1,1-Trichloroethane 1.1 ug/L 12/06/19 04:06 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 12/06/19 04:06 79-00-51.0 0.24 1
Trichloroethene ND ug/L 12/06/19 04:06 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 12/06/19 04:06 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 12/06/19 04:06 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 12/06/19 04:06 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 12/06/19 04:06 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 12/06/19 04:06 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 12/06/19 04:06 179601-23-12.0 0.41 1
o-Xylene ND ug/L 12/06/19 04:06 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)95 %12/06/19 04:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %12/06/19 04:06 17060-07-070-130 1
Toluene-d8 (S)96 %12/06/19 04:06 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.8260D MSV SIM
1,4-Dioxane (p-Dioxane)7.4 ug/L 11/26/19 14:39 123-91-12.0 1.2 1
Surrogates
1,2-Dichloroethane-d4 (S)117 %11/26/19 14:39 17060-07-050-150 1
Toluene-d8 (S)94 %11/26/19 14:39 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: TRIP BLANK Lab ID: 92455128005 Collected: 11/22/19 00:00 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 12/05/19 23:29 67-64-125.0 6.2 1
Benzene ND ug/L 12/05/19 23:29 71-43-21.0 0.15 1
Bromobenzene ND ug/L 12/05/19 23:29 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 12/05/19 23:29 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 12/05/19 23:29 75-27-41.0 0.26 1
Bromoform ND ug/L 12/05/19 23:29 75-25-21.0 0.62 1
Bromomethane ND ug/L 12/05/19 23:29 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 12/05/19 23:29 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 12/05/19 23:29 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 12/05/19 23:29 108-90-71.0 0.23 1
Chloroethane ND ug/L 12/05/19 23:29 75-00-31.0 0.49 1
Chloroform ND ug/L 12/05/19 23:29 67-66-35.0 2.3 1
Chloromethane ND ug/L 12/05/19 23:29 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 12/05/19 23:29 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 12/05/19 23:29 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 12/05/19 23:29 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 12/05/19 23:29 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 12/05/19 23:29 106-93-41.0 0.26 1
Dibromomethane ND ug/L 12/05/19 23:29 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 12/05/19 23:29 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 12/05/19 23:29 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 12/05/19 23:29 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 12/05/19 23:29 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 12/05/19 23:29 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 12/05/19 23:29 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 12/05/19 23:29 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 12/05/19 23:29 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 12/05/19 23:29 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 12/05/19 23:29 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 12/05/19 23:29 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 12/05/19 23:29 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 12/05/19 23:29 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 12/05/19 23:29 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 12/05/19 23:29 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 12/05/19 23:29 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 12/05/19 23:29 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 12/05/19 23:29 87-68-31.0 0.44 1
2-Hexanone ND ug/L 12/05/19 23:29 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 12/05/19 23:29 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 12/05/19 23:29 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/05/19 23:29 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 12/05/19 23:29 1634-04-41.0 0.28 1
Naphthalene ND ug/L 12/05/19 23:29 91-20-31.0 0.35 1
Styrene ND ug/L 12/05/19 23:29 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 12/05/19 23:29 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 12/05/19 23:29 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455128
ROW-603
Sample: TRIP BLANK Lab ID: 92455128005 Collected: 11/22/19 00:00 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 12/05/19 23:29 127-18-41.0 0.16 1
Toluene ND ug/L 12/05/19 23:29 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/05/19 23:29 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 12/05/19 23:29 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 12/05/19 23:29 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 12/05/19 23:29 79-00-51.0 0.24 1
Trichloroethene ND ug/L 12/05/19 23:29 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 12/05/19 23:29 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 12/05/19 23:29 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 12/05/19 23:29 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 12/05/19 23:29 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 12/05/19 23:29 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 12/05/19 23:29 179601-23-12.0 0.41 1
o-Xylene ND ug/L 12/05/19 23:29 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)97 %12/05/19 23:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %12/05/19 23:29 17060-07-070-130 1
Toluene-d8 (S)97 %12/05/19 23:29 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.8260D MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 11/26/19 13:20 123-91-12.0 1.2 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %11/26/19 13:20 17060-07-050-150 1
Toluene-d8 (S)94 %11/26/19 13:20 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512546
EPA 7470A
EPA 7470A
7470 Mercury
Associated Lab Samples: 92455128001, 92455128002, 92455128003, 92455128004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2748079
Associated Lab Samples:92455128001, 92455128002, 92455128003, 92455128004
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 12/03/19 14:010.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2748080LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2748081MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454007002
2748082
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 89 75-12595 6 252.5ND 2.3 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511713
EPA 3010A
EPA 6010D
6010 MET
Associated Lab Samples: 92455128001, 92455128002, 92455128003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744759
Associated Lab Samples:92455128001, 92455128002, 92455128003
Matrix: Water
AnalyzedMDL
Arsenic ug/L ND 10.0 11/26/19 21:174.7
Barium ug/L ND 5.0 11/26/19 21:171.0
Cadmium ug/L ND 1.0 11/26/19 21:170.40
Chromium ug/L ND 5.0 11/26/19 21:171.0
Lead ug/L ND 5.0 11/26/19 21:171.6
Selenium ug/L ND 10.0 11/26/19 21:174.7
Silver ug/L ND 5.0 11/26/19 21:172.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744760LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 496500 99 80-120
Barium ug/L 496500 99 80-120
Cadmium ug/L 495500 99 80-120
Chromium ug/L 490500 98 80-120
Lead ug/L 488500 98 80-120
Selenium ug/L 512500 102 80-120
Silver ug/L 251250 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744761MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454823018
2744762
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 101 75-125101 0 205005.6J 512 511
Barium ug/L 500 101 75-125102 1 2050044.4 550 553
Cadmium ug/L 500 100 75-125101 1 20500ND502 507
Chromium ug/L 500 100 75-125100 0 2050013.7 514 516
Lead ug/L 500 98 75-12599 1 20500ND493 496
Selenium ug/L 500 106 75-125110 4 20500ND529 549
Silver ug/L 250 101 75-125102 1 20250ND252 255
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511715
EPA 3010A
EPA 6010D
6010 MET
Associated Lab Samples: 92455128004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744767
Associated Lab Samples:92455128004
Matrix: Water
AnalyzedMDL
Arsenic ug/L ND 10.0 12/02/19 04:234.7
Barium ug/L ND 5.0 12/02/19 04:231.0
Cadmium ug/L ND 1.0 12/02/19 04:230.40
Chromium ug/L ND 5.0 12/02/19 04:231.0
Lead ug/L ND 5.0 12/02/19 04:231.6
Selenium ug/L ND 10.0 12/02/19 04:234.7
Silver ug/L ND 5.0 12/02/19 04:232.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744768LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 493500 99 80-120
Barium ug/L 496500 99 80-120
Cadmium ug/L 483500 97 80-120
Chromium ug/L 476500 95 80-120
Lead ug/L 480500 96 80-120
Selenium ug/L 490500 98 80-120
Silver ug/L 249250 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744769MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92455130001
2744770
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 95 75-12595 1 20500ND481 477
Barium ug/L 500 94 75-12593 1 20500253725 719
Cadmium ug/L 500 96 75-12595 1 20500ND481 477
Chromium ug/L 500 95 75-12595 1 2050017.1 494 490
Lead ug/L 500 95 75-12594 1 20500ND473 469
Selenium ug/L 500 100 75-12599 1 20500ND500 496
Silver ug/L 250 98 75-12597 0 20250ND244 243
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
513057
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples: 92455128001, 92455128002, 92455128003, 92455128004, 92455128005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2750390
Associated Lab Samples:92455128001, 92455128002, 92455128003, 92455128004, 92455128005
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 12/05/19 22:550.34
1,1,1-Trichloroethane ug/L ND 1.0 12/05/19 22:550.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/05/19 22:550.22
1,1,2-Trichloroethane ug/L ND 1.0 12/05/19 22:550.24
1,1-Dichloroethane ug/L ND 1.0 12/05/19 22:550.27
1,1-Dichloroethene ug/L ND 1.0 12/05/19 22:550.24
1,1-Dichloropropene ug/L ND 1.0 12/05/19 22:550.21
1,2,3-Trichlorobenzene ug/L ND 1.0 12/05/19 22:550.34
1,2,3-Trichloropropane ug/L ND 1.0 12/05/19 22:550.35
1,2,4-Trichlorobenzene ug/L ND 1.0 12/05/19 22:550.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 12/05/19 22:550.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/05/19 22:550.26
1,2-Dichlorobenzene ug/L ND 1.0 12/05/19 22:550.29
1,2-Dichloroethane ug/L ND 1.0 12/05/19 22:550.34
1,2-Dichloropropane ug/L ND 1.0 12/05/19 22:550.19
1,3-Dichlorobenzene ug/L ND 1.0 12/05/19 22:550.22
1,3-Dichloropropane ug/L ND 1.0 12/05/19 22:550.16
1,4-Dichlorobenzene ug/L ND 1.0 12/05/19 22:550.26
2,2-Dichloropropane ug/L ND 1.0 12/05/19 22:550.27
2-Butanone (MEK)ug/L ND 5.0 12/05/19 22:553.3
2-Chlorotoluene ug/L ND 1.0 12/05/19 22:550.20
2-Hexanone ug/L ND 5.0 12/05/19 22:550.57
4-Chlorotoluene ug/L ND 1.0 12/05/19 22:550.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 12/05/19 22:554.5
Acetone ug/L ND 25.0 12/05/19 22:556.2
Benzene ug/L ND 1.0 12/05/19 22:550.15
Bromobenzene ug/L ND 1.0 12/05/19 22:550.22
Bromochloromethane ug/L ND 1.0 12/05/19 22:550.34
Bromodichloromethane ug/L ND 1.0 12/05/19 22:550.26
Bromoform ug/L ND 1.0 12/05/19 22:550.62
Bromomethane ug/L ND 2.0 12/05/19 22:550.62
Carbon tetrachloride ug/L ND 1.0 12/05/19 22:550.22
Chlorobenzene ug/L ND 1.0 12/05/19 22:550.23
Chloroethane ug/L ND 1.0 12/05/19 22:550.49
Chloroform ug/L ND 5.0 12/05/19 22:552.3
Chloromethane ug/L ND 1.0 12/05/19 22:550.39
cis-1,2-Dichloroethene ug/L ND 1.0 12/05/19 22:550.29
cis-1,3-Dichloropropene ug/L ND 1.0 12/05/19 22:550.30
Dibromochloromethane ug/L ND 1.0 12/05/19 22:550.41
Dibromomethane ug/L ND 1.0 12/05/19 22:550.46
Dichlorodifluoromethane ug/L ND 1.0 12/05/19 22:550.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2750390
Associated Lab Samples:92455128001, 92455128002, 92455128003, 92455128004, 92455128005
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 12/05/19 22:550.22
Ethylbenzene ug/L ND 1.0 12/05/19 22:550.26
Hexachloro-1,3-butadiene ug/L ND 1.0 12/05/19 22:550.44
m&p-Xylene ug/L ND 2.0 12/05/19 22:550.41
Methyl-tert-butyl ether ug/L ND 1.0 12/05/19 22:550.28
Methylene Chloride ug/L ND 5.0 12/05/19 22:553.7
Naphthalene ug/L ND 1.0 12/05/19 22:550.35
o-Xylene ug/L ND 1.0 12/05/19 22:550.22
p-Isopropyltoluene ug/L ND 1.0 12/05/19 22:550.21
Styrene ug/L ND 1.0 12/05/19 22:550.27
Tetrachloroethene ug/L ND 1.0 12/05/19 22:550.16
Toluene ug/L ND 1.0 12/05/19 22:550.24
trans-1,2-Dichloroethene ug/L ND 1.0 12/05/19 22:550.25
trans-1,3-Dichloropropene ug/L ND 1.0 12/05/19 22:550.31
Trichloroethene ug/L ND 1.0 12/05/19 22:550.22
Trichlorofluoromethane ug/L ND 1.0 12/05/19 22:550.31
Vinyl acetate ug/L ND 2.0 12/05/19 22:551.4
Vinyl chloride ug/L ND 1.0 12/05/19 22:550.24
Xylene (Total)ug/L ND 1.0 12/05/19 22:550.63
1,2-Dichloroethane-d4 (S)%104 70-130 12/05/19 22:55
4-Bromofluorobenzene (S)%96 70-130 12/05/19 22:55
Toluene-d8 (S)%95 70-130 12/05/19 22:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2750391LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 57.250 114 70-130
1,1,1-Trichloroethane ug/L 52.150 104 70-130
1,1,2,2-Tetrachloroethane ug/L 55.450 111 70-130
1,1,2-Trichloroethane ug/L 52.650 105 70-130
1,1-Dichloroethane ug/L 49.450 99 70-130
1,1-Dichloroethene ug/L 49.550 99 70-130
1,1-Dichloropropene ug/L 53.750 107 70-130
1,2,3-Trichlorobenzene ug/L 52.450 105 70-130
1,2,3-Trichloropropane ug/L 57.150 114 70-130
1,2,4-Trichlorobenzene ug/L 52.350 105 70-130
1,2-Dibromo-3-chloropropane ug/L 56.750 113 70-130
1,2-Dibromoethane (EDB)ug/L 56.950 114 70-130
1,2-Dichlorobenzene ug/L 52.850 106 70-130
1,2-Dichloroethane ug/L 48.450 97 70-130
1,2-Dichloropropane ug/L 51.450 103 70-130
1,3-Dichlorobenzene ug/L 52.550 105 70-130
1,3-Dichloropropane ug/L 55.650 111 70-131
1,4-Dichlorobenzene ug/L 52.250 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2750391LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 51.650 103 69-130
2-Butanone (MEK)ug/L 103100 103 64-135
2-Chlorotoluene ug/L 53.450 107 70-130
2-Hexanone ug/L 116100 116 66-135
4-Chlorotoluene ug/L 55.050 110 70-130
4-Methyl-2-pentanone (MIBK)ug/L 110100 110 70-130
Acetone ug/L 115100 115 61-157
Benzene ug/L 51.350 103 70-130
Bromobenzene ug/L 55.450 111 70-130
Bromochloromethane ug/L 51.350 103 70-130
Bromodichloromethane ug/L 53.550 107 70-130
Bromoform ug/L 55.250 110 70-130
Bromomethane ug/L 49.450 99 38-130
Carbon tetrachloride ug/L 54.750 109 70-130
Chlorobenzene ug/L 52.750 105 70-130
Chloroethane ug/L 47.550 95 37-142
Chloroform ug/L 51.250 102 70-130
Chloromethane ug/L 41.550 83 48-130
cis-1,2-Dichloroethene ug/L 49.150 98 70-130
cis-1,3-Dichloropropene ug/L 55.550 111 70-130
Dibromochloromethane ug/L 56.450 113 70-130
Dibromomethane ug/L 52.450 105 70-130
Dichlorodifluoromethane ug/L 43.550 87 53-134
Diisopropyl ether ug/L 51.250 102 70-135
Ethylbenzene ug/L 53.250 106 70-130
Hexachloro-1,3-butadiene ug/L 51.550 103 68-132
m&p-Xylene ug/L 105100 105 70-130
Methyl-tert-butyl ether ug/L 53.350 107 70-130
Methylene Chloride ug/L 48.250 96 67-132
Naphthalene ug/L 56.450 113 70-130
o-Xylene ug/L 54.350 109 70-131
p-Isopropyltoluene ug/L 53.050 106 70-130
Styrene ug/L 55.450 111 70-130
Tetrachloroethene ug/L 53.550 107 69-130
Toluene ug/L 50.850 102 70-130
trans-1,2-Dichloroethene ug/L 49.450 99 70-130
trans-1,3-Dichloropropene ug/L 55.050 110 70-130
Trichloroethene ug/L 51.650 103 70-130
Trichlorofluoromethane ug/L 45.850 92 63-130
Vinyl acetate ug/L 99.0100 99 55-143
Vinyl chloride ug/L 47.950 96 70-131
Xylene (Total)ug/L 159150 106 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2750393MATRIX SPIKE SAMPLE:
MSSpike
Result
92454943002
1,1,1,2-Tetrachloroethane ug/L 17.920 90 73-134ND
1,1,1-Trichloroethane ug/L 18.920 94 82-143ND
1,1,2,2-Tetrachloroethane ug/L 17.520 87 70-136ND
1,1,2-Trichloroethane ug/L 17.120 85 70-135ND
1,1-Dichloroethane ug/L 17.620 88 70-139ND
1,1-Dichloroethene ug/L 18.620 93 70-154ND
1,1-Dichloropropene ug/L 19.720 98 70-149ND
1,2,3-Trichlorobenzene ug/L 15.220 76 70-135ND
1,2,3-Trichloropropane ug/L 17.520 88 71-137ND
1,2,4-Trichlorobenzene ug/L 14.920 74 73-140ND
1,2-Dibromo-3-chloropropane ug/L 15.820 79 65-134ND
1,2-Dibromoethane (EDB)ug/L 18.520 92 70-137ND
1,2-Dichlorobenzene ug/L 17.220 86 70-133ND
1,2-Dichloroethane ug/L 17.720 89 70-137ND
1,2-Dichloropropane ug/L 16.820 84 70-140ND
1,3-Dichlorobenzene ug/L 17.520 88 70-135ND
1,3-Dichloropropane ug/L 18.920 95 70-143ND
1,4-Dichlorobenzene ug/L 17.320 87 70-133ND
2,2-Dichloropropane ug/L 18.620 93 61-148ND
2-Butanone (MEK)ug/L 31.040 78 60-139ND
2-Chlorotoluene ug/L 18.520 92 70-144ND
2-Hexanone ug/L 31.240 78 65-138ND
4-Chlorotoluene ug/L 18.320 92 70-137ND
4-Methyl-2-pentanone (MIBK)ug/L 29.940 75 65-135ND
Acetone ug/L 31.740 79 60-148ND
Benzene ug/L 17.420 87 70-151ND
Bromobenzene ug/L 17.920 89 70-136ND
Bromochloromethane ug/L 18.520 92 70-141ND
Bromodichloromethane ug/L 17.320 87 70-138ND
Bromoform ug/L 16.020 80 63-130ND
Bromomethane ug/L 23.6 v320118 15-152ND
Carbon tetrachloride ug/L 18.720 93 70-143ND
Chlorobenzene ug/L 17.520 88 70-138ND
Chloroethane ug/L 18.320 91 52-163ND
Chloroform ug/L 18.820 94 70-139ND
Chloromethane ug/L 14.520 73 41-139ND
cis-1,2-Dichloroethene ug/L 17.320 87 70-141ND
cis-1,3-Dichloropropene ug/L 16.920 84 70-137ND
Dibromochloromethane ug/L 17.520 87 70-134ND
Dibromomethane ug/L 16.620 83 70-138ND
Dichlorodifluoromethane ug/L 17.820 89 47-155ND
Diisopropyl ether ug/L 16.820 84 63-144ND
Ethylbenzene ug/L 18.320 91 66-153ND
Hexachloro-1,3-butadiene ug/L 14.720 74 65-149ND
m&p-Xylene ug/L 36.340 91 69-152ND
Methyl-tert-butyl ether ug/L 18.020 90 54-156ND
Methylene Chloride ug/L 18.120 90 42-159ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2750393MATRIX SPIKE SAMPLE:
MSSpike
Result
92454943002
Naphthalene ug/L 14.920 75 61-148ND
o-Xylene ug/L 17.820 89 70-148ND
p-Isopropyltoluene ug/L 17.420 87 70-146ND
Styrene ug/L 17.820 89 70-135ND
Tetrachloroethene ug/L 17.820 89 59-143ND
Toluene ug/L 16.720 84 59-148ND
trans-1,2-Dichloroethene ug/L 17.820 89 70-146ND
trans-1,3-Dichloropropene ug/L 16.720 83 70-135ND
Trichloroethene ug/L 17.220 86 70-147ND
Trichlorofluoromethane ug/L 18.020 90 70-148ND
Vinyl acetate ug/L 31.940 80 49-151ND
Vinyl chloride ug/L 17.220 86 70-156ND
Xylene (Total)ug/L 54.160 90 63-158ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454943001
2750392SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454943001
2750392SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L 6.3 1 306.3
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%110103
4-Bromofluorobenzene (S)%9794
Toluene-d8 (S)%9698
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511851
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Associated Lab Samples: 92455128001, 92455128002, 92455128003, 92455128004, 92455128005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2745156
Associated Lab Samples:92455128001, 92455128002, 92455128003, 92455128004, 92455128005
Matrix: Water
AnalyzedMDL
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/26/19 13:001.2
1,2-Dichloroethane-d4 (S)%99 50-150 11/26/19 13:00
Toluene-d8 (S)%91 50-150 11/26/19 13:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745157LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 19.120 95 70-130
1,2-Dichloroethane-d4 (S)%116 50-150
Toluene-d8 (S)%95 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745381MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92455128002
2745382
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane) ug/L 20 94 50-15094 0 3020ND18.9 18.9
1,2-Dichloroethane-d4 (S) %119 50-150119 30
Toluene-d8 (S)%98 50-15099 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511822
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Associated Lab Samples: 92455128001, 92455128002, 92455128003, 92455128004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2745012
Associated Lab Samples:92455128001, 92455128002, 92455128003, 92455128004
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 11/27/19 17:131.5
1,2-Dichlorobenzene ug/L ND 10.0 11/27/19 17:131.3
1,3-Dichlorobenzene ug/L ND 10.0 11/27/19 17:131.5
1,4-Dichlorobenzene ug/L ND 10.0 11/27/19 17:132.1
1-Methylnaphthalene ug/L ND 10.0 11/27/19 17:131.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 11/27/19 17:132.8
2,4,5-Trichlorophenol ug/L ND 10.0 11/27/19 17:131.4
2,4,6-Trichlorophenol ug/L ND 10.0 11/27/19 17:131.5
2,4-Dichlorophenol ug/L ND 10.0 11/27/19 17:131.4
2,4-Dimethylphenol ug/L ND 10.0 11/27/19 17:131.4
2,4-Dinitrophenol ug/L ND 50.0 11/27/19 17:1340.5
2,4-Dinitrotoluene ug/L ND 10.0 11/27/19 17:131.2
2,6-Dinitrotoluene ug/L ND 10.0 11/27/19 17:131.4
2-Chloronaphthalene ug/L ND 10.0 11/27/19 17:131.5
2-Chlorophenol ug/L ND 10.0 11/27/19 17:131.2
2-Methylnaphthalene ug/L ND 10.0 11/27/19 17:131.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 11/27/19 17:131.2
2-Nitroaniline ug/L ND 20.0 11/27/19 17:134.2
2-Nitrophenol ug/L ND 10.0 11/27/19 17:131.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 11/27/19 17:131.2
3,3'-Dichlorobenzidine ug/L ND 20.0 11/27/19 17:133.0
3-Nitroaniline ug/L ND 20.0 11/27/19 17:132.3
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/27/19 17:1315.2
4-Bromophenylphenyl ether ug/L ND 10.0 11/27/19 17:131.6
4-Chloro-3-methylphenol ug/L ND 20.0 11/27/19 17:132.8
4-Chloroaniline ug/L ND 20.0 11/27/19 17:132.8
4-Chlorophenylphenyl ether ug/L ND 10.0 11/27/19 17:131.6
4-Nitroaniline ug/L ND 20.0 11/27/19 17:132.2
4-Nitrophenol ug/L ND 50.0 11/27/19 17:133.5
Acenaphthene ug/L ND 10.0 11/27/19 17:131.6
Acenaphthylene ug/L ND 10.0 11/27/19 17:131.6
Aniline ug/L ND 10.0 11/27/19 17:131.9
Anthracene ug/L ND 10.0 11/27/19 17:131.7
Benzo(a)anthracene ug/L ND 10.0 11/27/19 17:131.8
Benzo(a)pyrene ug/L ND 10.0 11/27/19 17:132.1
Benzo(b)fluoranthene ug/L ND 10.0 11/27/19 17:131.9
Benzo(g,h,i)perylene ug/L ND 10.0 11/27/19 17:131.4
Benzo(k)fluoranthene ug/L ND 10.0 11/27/19 17:131.9
Benzoic Acid ug/L ND 50.0 11/27/19 17:1343.0
Benzyl alcohol ug/L ND 20.0 11/27/19 17:132.6
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/27/19 17:131.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2745012
Associated Lab Samples:92455128001, 92455128002, 92455128003, 92455128004
Matrix: Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 11/27/19 17:131.8
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/27/19 17:132.1
Butylbenzylphthalate ug/L ND 10.0 11/27/19 17:131.6
Chrysene ug/L ND 10.0 11/27/19 17:131.7
Di-n-butylphthalate ug/L 2.9J 10.0 11/27/19 17:131.8
Di-n-octylphthalate ug/L ND 10.0 11/27/19 17:131.8
Dibenz(a,h)anthracene ug/L ND 10.0 11/27/19 17:131.6
Dibenzofuran ug/L ND 10.0 11/27/19 17:131.5
Diethylphthalate ug/L ND 10.0 11/27/19 17:132.4
Dimethylphthalate ug/L ND 10.0 11/27/19 17:131.6
Fluoranthene ug/L ND 10.0 11/27/19 17:131.7
Fluorene ug/L ND 10.0 11/27/19 17:131.6
Hexachloro-1,3-butadiene ug/L ND 10.0 11/27/19 17:132.0
Hexachlorobenzene ug/L ND 10.0 11/27/19 17:131.7
Hexachlorocyclopentadiene ug/L ND 10.0 11/27/19 17:131.7
Hexachloroethane ug/L ND 10.0 11/27/19 17:132.0
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/27/19 17:131.6
Isophorone ug/L ND 10.0 11/27/19 17:131.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 11/27/19 17:132.2
N-Nitrosodimethylamine ug/L ND 10.0 11/27/19 17:131.2
N-Nitrosodiphenylamine ug/L ND 10.0 11/27/19 17:131.7
Naphthalene ug/L ND 10.0 11/27/19 17:131.4
Nitrobenzene ug/L ND 10.0 11/27/19 17:132.1
Pentachlorophenol ug/L ND 25.0 11/27/19 17:132.2
Phenanthrene ug/L ND 10.0 11/27/19 17:131.7
Phenol ug/L ND 10.0 11/27/19 17:130.92
Pyrene ug/L ND 10.0 11/27/19 17:132.1
2,4,6-Tribromophenol (S)%86 10-137 11/27/19 17:13
2-Fluorobiphenyl (S)%79 13-130 11/27/19 17:13
2-Fluorophenol (S)%80 10-130 11/27/19 17:13
Nitrobenzene-d5 (S)%74 13-130 11/27/19 17:13
Phenol-d6 (S)%84 10-130 11/27/19 17:13
Terphenyl-d14 (S)%84 25-130 11/27/19 17:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745013LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 43.650 87 30-130
1,2-Dichlorobenzene ug/L 43.650 87 30-130
1,3-Dichlorobenzene ug/L 43.050 86 20-130
1,4-Dichlorobenzene ug/L 43.450 87 30-130
1-Methylnaphthalene ug/L 45.850 92 30-130
2,2'-Oxybis(1-chloropropane)ug/L 39.850 80 20-130
2,4,5-Trichlorophenol ug/L 45.250 90 40-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745013LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 46.950 94 40-130
2,4-Dichlorophenol ug/L 46.450 93 31-130
2,4-Dimethylphenol ug/L 46.250 92 30-130
2,4-Dinitrophenol ug/L 226250 90 30-130
2,4-Dinitrotoluene ug/L 50.350 101 49-130
2,6-Dinitrotoluene ug/L 49.750 99 50-130
2-Chloronaphthalene ug/L 45.250 90 30-130
2-Chlorophenol ug/L 45.050 90 30-130
2-Methylnaphthalene ug/L 45.050 90 30-130
2-Methylphenol(o-Cresol)ug/L 43.050 86 30-130
2-Nitroaniline ug/L 95.4100 95 40-130
2-Nitrophenol ug/L 47.550 95 20-130
3&4-Methylphenol(m&p Cresol)ug/L 43.550 87 20-130
3,3'-Dichlorobenzidine ug/L 83.6100 84 10-150
3-Nitroaniline ug/L 98.6100 99 40-130
4,6-Dinitro-2-methylphenol ug/L 99.5100 99 40-130
4-Bromophenylphenyl ether ug/L 44.250 88 30-130
4-Chloro-3-methylphenol ug/L 92.9100 93 30-130
4-Chloroaniline ug/L 90.3100 90 20-130
4-Chlorophenylphenyl ether ug/L 43.950 88 20-130
4-Nitroaniline ug/L 91.6100 92 40-130
4-Nitrophenol ug/L 243250 97 10-130
Acenaphthene ug/L 46.850 94 30-130
Acenaphthylene ug/L 50.150 100 30-130
Aniline ug/L 40.950 82 20-130
Anthracene ug/L 50.350 101 50-130
Benzo(a)anthracene ug/L 47.950 96 50-130
Benzo(a)pyrene ug/L 51.750 103 50-130
Benzo(b)fluoranthene ug/L 50.350 101 50-130
Benzo(g,h,i)perylene ug/L 50.150 100 50-130
Benzo(k)fluoranthene ug/L 50.250 100 50-130
Benzoic Acid ug/L 202250 81 10-130
Benzyl alcohol ug/L 88.7100 89 20-130
bis(2-Chloroethoxy)methane ug/L 42.150 84 30-130
bis(2-Chloroethyl) ether ug/L 42.950 86 30-130
bis(2-Ethylhexyl)phthalate ug/L 45.950 92 50-130
Butylbenzylphthalate ug/L 46.550 93 50-150
Chrysene ug/L 45.950 92 50-130
Di-n-butylphthalate ug/L 49.350 99 50-130
Di-n-octylphthalate ug/L 48.650 97 50-130
Dibenz(a,h)anthracene ug/L 50.950 102 40-130
Dibenzofuran ug/L 45.250 90 40-130
Diethylphthalate ug/L 45.450 91 40-130
Dimethylphthalate ug/L 44.650 89 40-130
Fluoranthene ug/L 49.050 98 30-130
Fluorene ug/L 47.250 94 20-130
Hexachloro-1,3-butadiene ug/L 43.250 86 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745013LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 46.650 93 30-130
Hexachlorocyclopentadiene ug/L 50.150 100 10-150
Hexachloroethane ug/L 43.550 87 10-130
Indeno(1,2,3-cd)pyrene ug/L 50.550 101 40-130
Isophorone ug/L 43.650 87 30-130
N-Nitroso-di-n-propylamine ug/L 43.650 87 30-130
N-Nitrosodimethylamine ug/L 41.550 83 10-130
N-Nitrosodiphenylamine ug/L 46.550 93 30-130
Naphthalene ug/L 45.850 92 20-130
Nitrobenzene ug/L 43.850 88 20-130
Pentachlorophenol ug/L 109100 109 10-140
Phenanthrene ug/L 47.350 95 50-130
Phenol ug/L 46.350 93 10-130
Pyrene ug/L 47.150 94 50-130
2,4,6-Tribromophenol (S)%109 10-137
2-Fluorobiphenyl (S)%83 13-130
2-Fluorophenol (S)%89 10-130
Nitrobenzene-d5 (S)%80 13-130
Phenol-d6 (S)%94 10-130
Terphenyl-d14 (S)%85 25-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745014MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454931001
2745015
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 52 30-13045 14 3050ND26.0 22.5
1,2-Dichlorobenzene ug/L 50 52 30-13045 14 3050ND26.2 22.7
1,3-Dichlorobenzene ug/L 50 51 20-13044 14 3050ND25.5 22.2
1,4-Dichlorobenzene ug/L 50 52 30-13045 14 3050ND25.9 22.6
1-Methylnaphthalene ug/L 50 54 30-13048 11 3050ND27.0 24.1
2,2'-Oxybis(1-
chloropropane)ug/L 50 48 20-13042 13 3050ND24.2 21.1
2,4,5-Trichlorophenol ug/L 50 52 40-13046 11 3050ND26.0 23.2
2,4,6-Trichlorophenol ug/L 50 54 40-13048 12 3050ND27.2 24.0
2,4-Dichlorophenol ug/L 50 53 31-13047 12 3050ND26.6 23.6
2,4-Dimethylphenol ug/L 50 54 30-13047 15 3050ND27.2 23.4
2,4-Dinitrophenol ug/L 250 57 30-13058 1 30250ND142 144
2,4-Dinitrotoluene ug/L 50 67 49-13065 3 3050ND33.6 32.6
2,6-Dinitrotoluene ug/L 50 61 50-13056 7 3050ND30.3 28.2
2-Chloronaphthalene ug/L 50 54 30-13049 11 3050ND27.1 24.3
2-Chlorophenol ug/L 50 53 30-13047 13 3050ND26.4 23.3
2-Methylnaphthalene ug/L 50 53 30-13048 10 3050ND26.3 23.9
2-Methylphenol(o-Cresol) ug/L 50 45 30-13040 11 3050ND22.7 20.2
2-Nitroaniline ug/L 100 59 40-13054 8 30100ND58.6 53.8
2-Nitrophenol ug/L 50 58 20-13050 14 3050ND28.9 25.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745014MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454931001
2745015
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/L 50 42 20-13039 8 3050ND21.0 19.4
3,3'-Dichlorobenzidine ug/L 100 64 10-15060 6 30100ND63.5 59.7
3-Nitroaniline ug/L 100 60 40-13056 7 30100ND60.0 55.9
4,6-Dinitro-2-methylphenol ug/L 100 69 40-13068 2 30100ND69.3 67.8
4-Bromophenylphenyl ether ug/L 50 55 30-13051 8 3050ND27.7 25.7
4-Chloro-3-methylphenol ug/L 100 52 30-13047 9 30100ND51.8 47.4
4-Chloroaniline ug/L 100 55 20-13049 12 30100ND55.0 48.8
4-Chlorophenylphenyl ether ug/L 50 54 20-13049 10 3050ND26.9 24.4
4-Nitroaniline ug/L 100 65 40-13064 1 30100ND64.9 64.3
4-Nitrophenol ug/L 250 35 10-13040 12 30250ND88.0 99.0
Acenaphthene ug/L 50 57 30-13051 10 3050ND28.5 25.7
Acenaphthylene ug/L 50 61 30-13055 11 3050ND30.5 27.4
Aniline ug/L 50 43 20-13036 18 3050ND21.4 17.9
Anthracene ug/L 50 69 50-13066 4 3050ND34.4 32.9
Benzo(a)anthracene ug/L 50 73 50-13070 4 3050ND36.5 35.2
Benzo(a)pyrene ug/L 50 78 50-13076 3 3050ND39.0 37.8
Benzo(b)fluoranthene ug/L 50 74 50-13074 0 3050ND36.9 36.8
Benzo(g,h,i)perylene ug/L 50 80 50-13077 4 3050ND39.9 38.4
Benzo(k)fluoranthene ug/L 50 76 50-13074 3 3050ND38.0 36.8
Benzoic Acid ug/L 250 25 10-13026 3 30250ND63.3 65.1
Benzyl alcohol ug/L 100 49 20-13045 9 30100ND48.9 44.8
bis(2-
Chloroethoxy)methane ug/L 50 51 30-13045 12 3050ND25.4 22.5
bis(2-Chloroethyl) ether ug/L 50 55 30-13048 14 3050ND27.6 24.0
bis(2-Ethylhexyl)phthalate ug/L 50 66 50-13064 2 3050ND32.8 32.1
Butylbenzylphthalate ug/L 50 66 50-15064 2 3050ND32.9 32.2
Chrysene ug/L 50 71 50-13068 5 3050ND35.7 34.1
Di-n-butylphthalate ug/L 50 67 50-13065 3 3050ND33.6 32.7
Di-n-octylphthalate ug/L 50 68 50-13067 2 3050ND34.1 33.3
Dibenz(a,h)anthracene ug/L 50 80 40-13075 6 3050ND39.9 37.6
Dibenzofuran ug/L 50 56 40-13050 12 3050ND28.2 25.1
Diethylphthalate ug/L 50 62 40-13061 1 3050ND31.0 30.6
Dimethylphthalate ug/L 50 57 40-13054 5 3050ND28.4 27.0
Fluoranthene ug/L 50 74 30-13072 3 3050ND37.1 36.1
Fluorene ug/L 50 59 20-13053 11 3050ND29.7 26.6
Hexachloro-1,3-butadiene ug/L 50 49 10-13042 14 3050ND24.4 21.2
Hexachlorobenzene ug/L 50 61 30-13057 6 3050ND30.3 28.6
Hexachlorocyclopentadiene ug/L 50 54 10-15047 13 3050ND26.8 23.4
Hexachloroethane ug/L 50 50 10-13043 14 3050ND24.9 21.6
Indeno(1,2,3-cd)pyrene ug/L 50 79 40-13075 6 3050ND39.7 37.5
Isophorone ug/L 50 53 30-13048 10 3050ND26.4 23.9
N-Nitroso-di-n-propylamine ug/L 50 52 30-13046 11 3050ND26.0 23.2
N-Nitrosodimethylamine ug/L 50 43 10-13040 7 3050ND21.4 20.0
N-Nitrosodiphenylamine ug/L 50 59 30-13056 6 3050ND29.6 27.9
Naphthalene ug/L 50 56 20-13049 12 3050ND27.9 24.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455128
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745014MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454931001
2745015
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrobenzene ug/L 50 57 20-13051 13 3050ND28.7 25.3
Pentachlorophenol ug/L 100 72 10-14070 4 30100ND72.2 69.6
Phenanthrene ug/L 50 65 50-13063 4 3050ND32.7 31.4
Phenol ug/L 50 30 10-13029 4 3050ND15.2 14.6
Pyrene ug/L 50 71 50-13070 2 3050ND35.5 34.8
2,4,6-Tribromophenol (S) %78 10-13771
2-Fluorobiphenyl (S)%59 13-13051
2-Fluorophenol (S)%47 10-13041
Nitrobenzene-d5 (S)%60 13-13051
Phenol-d6 (S)%34 10-13032
Terphenyl-d14 (S)%70 25-13064
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 43
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92455128
ROW-603
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 43
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92455128
ROW-603
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92455128001 511713 511721MW-2 EPA 3010A EPA 6010D
92455128002 511713 511721MW-1 EPA 3010A EPA 6010D
92455128003 511713 511721MW-4 EPA 3010A EPA 6010D
92455128004 511715 511722DUP-2-GW EPA 3010A EPA 6010D
92455128001 512546 512624MW-2 EPA 7470A EPA 7470A
92455128002 512546 512624MW-1 EPA 7470A EPA 7470A
92455128003 512546 512624MW-4 EPA 7470A EPA 7470A
92455128004 512546 512624DUP-2-GW EPA 7470A EPA 7470A
92455128001 511822 512197MW-2 EPA 3510C EPA 8270E
92455128002 511822 512197MW-1 EPA 3510C EPA 8270E
92455128003 511822 512197MW-4 EPA 3510C EPA 8270E
92455128004 511822 512197DUP-2-GW EPA 3510C EPA 8270E
92455128001 513057MW-2 EPA 8260D
92455128002 513057MW-1 EPA 8260D
92455128003 513057MW-4 EPA 8260D
92455128004 513057DUP-2-GW EPA 8260D
92455128005 513057TRIP BLANK EPA 8260D
92455128001 511851MW-2 EPA 8260D Mod.
92455128002 511851MW-1 EPA 8260D Mod.
92455128003 511851MW-4 EPA 8260D Mod.
92455128004 511851DUP-2-GW EPA 8260D Mod.
92455128005 511851TRIP BLANK EPA 8260D Mod.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/06/2019 06:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 43
Page 41 of 43
Page 42 of 43
Page 43 of 43
#=CL#
December 03, 2019
LIMS USE: FR - DAVID GRAHAM
LIMS OBJECT ID: 92454751
92454751
Project:
Pace Project No.:
RE:
David Graham
Hart & Hickman
2923 S. Tryon Street
Charlotte, NC 28203
ROW-603
Dear David Graham:
Enclosed are the analytical results for sample(s) received by the laboratory on November 21, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring for
[e-mail]
Project Manager
Kevin Godwin
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92454751
ROW-603
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 31
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92454751
ROW-603
Lab ID Sample ID Matrix Date Collected Date Received
92454751001 IDW SOIL Solid 11/21/19 10:15 11/21/19 10:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92454751
ROW-603
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92454751001 IDW SOIL EPA 6010D 7 PASI-AKQ
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
EPA 8260D Mod.3 PASI-CLMB
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454751
ROW-603
Sample: IDW SOIL Lab ID: 92454751001 Collected: 11/21/19 10:15 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 0.80J mg/kg 12/01/19 22:43 7440-38-211/26/19 12:130.91 0.46 1
Barium 218 mg/kg 12/01/19 22:43 7440-39-311/26/19 12:130.46 0.23 1
Cadmium 0.087J mg/kg 12/01/19 22:43 7440-43-911/26/19 12:130.091 0.046 1
Chromium 30.8 mg/kg 12/01/19 22:43 7440-47-311/26/19 12:130.46 0.23 1
Lead 2.6 mg/kg 12/01/19 22:43 7439-92-111/26/19 12:130.46 0.23 1
Selenium 0.64J mg/kg 12/01/19 22:43 7782-49-2 B11/26/19 12:130.91 0.46 1
Silver ND mg/kg 12/01/19 22:43 7440-22-411/26/19 12:130.46 0.23 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.0055 mg/kg 11/22/19 15:41 7439-97-611/22/19 11:500.0023 0.0011 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 11/27/19 15:39 83-32-911/27/19 09:170.42 0.11 1
Acenaphthylene ND mg/kg 11/27/19 15:39 208-96-811/27/19 09:170.42 0.098 1
Aniline ND mg/kg 11/27/19 15:39 62-53-311/27/19 09:170.42 0.093 1
Anthracene ND mg/kg 11/27/19 15:39 120-12-711/27/19 09:170.42 0.11 1
Benzo(a)anthracene ND mg/kg 11/27/19 15:39 56-55-311/27/19 09:170.42 0.13 1
Benzo(a)pyrene ND mg/kg 11/27/19 15:39 50-32-811/27/19 09:170.42 0.18 1
Benzo(b)fluoranthene ND mg/kg 11/27/19 15:39 205-99-211/27/19 09:170.42 0.17 1
Benzo(g,h,i)perylene ND mg/kg 11/27/19 15:39 191-24-211/27/19 09:170.42 0.16 1
Benzo(k)fluoranthene ND mg/kg 11/27/19 15:39 207-08-911/27/19 09:170.42 0.18 1
Benzoic Acid ND mg/kg 11/27/19 15:39 65-85-011/27/19 09:172.1 0.45 1
Benzyl alcohol ND mg/kg 11/27/19 15:39 100-51-611/27/19 09:170.83 0.22 1
4-Bromophenylphenyl ether ND mg/kg 11/27/19 15:39 101-55-311/27/19 09:170.42 0.11 1
Butylbenzylphthalate ND mg/kg 11/27/19 15:39 85-68-711/27/19 09:170.42 0.11 1
4-Chloro-3-methylphenol ND mg/kg 11/27/19 15:39 59-50-711/27/19 09:170.83 0.25 1
4-Chloroaniline ND mg/kg 11/27/19 15:39 106-47-811/27/19 09:172.1 0.25 1
bis(2-Chloroethoxy)methane ND mg/kg 11/27/19 15:39 111-91-111/27/19 09:170.42 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 11/27/19 15:39 111-44-411/27/19 09:170.42 0.088 1
2-Chloronaphthalene ND mg/kg 11/27/19 15:39 91-58-711/27/19 09:170.42 0.093 1
2-Chlorophenol ND mg/kg 11/27/19 15:39 95-57-811/27/19 09:170.42 0.097 1
4-Chlorophenylphenyl ether ND mg/kg 11/27/19 15:39 7005-72-311/27/19 09:170.42 0.11 1
Chrysene ND mg/kg 11/27/19 15:39 218-01-911/27/19 09:170.42 0.12 1
Dibenz(a,h)anthracene ND mg/kg 11/27/19 15:39 53-70-311/27/19 09:170.42 0.17 1
Dibenzofuran ND mg/kg 11/27/19 15:39 132-64-911/27/19 09:170.42 0.10 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 15:39 95-50-111/27/19 09:170.42 0.090 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 15:39 541-73-111/27/19 09:170.42 0.094 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 15:39 106-46-711/27/19 09:170.42 0.091 1
3,3'-Dichlorobenzidine ND mg/kg 11/27/19 15:39 91-94-111/27/19 09:172.1 0.29 1
2,4-Dichlorophenol ND mg/kg 11/27/19 15:39 120-83-211/27/19 09:170.42 0.14 1
Diethylphthalate ND mg/kg 11/27/19 15:39 84-66-211/27/19 09:170.42 0.090 1
2,4-Dimethylphenol ND mg/kg 11/27/19 15:39 105-67-911/27/19 09:170.42 0.10 1
Dimethylphthalate ND mg/kg 11/27/19 15:39 131-11-311/27/19 09:170.42 0.094 1
Di-n-butylphthalate ND mg/kg 11/27/19 15:39 84-74-211/27/19 09:170.42 0.10 1
4,6-Dinitro-2-methylphenol ND mg/kg 11/27/19 15:39 534-52-111/27/19 09:170.83 0.67 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454751
ROW-603
Sample: IDW SOIL Lab ID: 92454751001 Collected: 11/21/19 10:15 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 11/27/19 15:39 51-28-511/27/19 09:172.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 11/27/19 15:39 121-14-211/27/19 09:170.42 0.11 1
2,6-Dinitrotoluene ND mg/kg 11/27/19 15:39 606-20-211/27/19 09:170.42 0.11 1
Di-n-octylphthalate ND mg/kg 11/27/19 15:39 117-84-011/27/19 09:170.42 0.24 1
bis(2-Ethylhexyl)phthalate ND mg/kg 11/27/19 15:39 117-81-711/27/19 09:170.42 0.14 1
Fluoranthene ND mg/kg 11/27/19 15:39 206-44-011/27/19 09:170.42 0.13 1
Fluorene ND mg/kg 11/27/19 15:39 86-73-711/27/19 09:170.42 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 15:39 87-68-311/27/19 09:170.42 0.10 1
Hexachlorobenzene ND mg/kg 11/27/19 15:39 118-74-111/27/19 09:170.42 0.11 1
Hexachlorocyclopentadiene ND mg/kg 11/27/19 15:39 77-47-411/27/19 09:170.42 0.17 1
Hexachloroethane ND mg/kg 11/27/19 15:39 67-72-111/27/19 09:170.42 0.095 1
Indeno(1,2,3-cd)pyrene ND mg/kg 11/27/19 15:39 193-39-511/27/19 09:170.42 0.19 1
Isophorone ND mg/kg 11/27/19 15:39 78-59-111/27/19 09:170.42 0.090 1
1-Methylnaphthalene ND mg/kg 11/27/19 15:39 90-12-011/27/19 09:170.42 0.11 1
2-Methylnaphthalene ND mg/kg 11/27/19 15:39 91-57-611/27/19 09:170.42 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 11/27/19 15:39 95-48-711/27/19 09:170.42 0.092 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 11/27/19 15:39 15831-10-411/27/19 09:170.42 0.10 1
Naphthalene ND mg/kg 11/27/19 15:39 91-20-311/27/19 09:170.42 0.099 1
2-Nitroaniline ND mg/kg 11/27/19 15:39 88-74-411/27/19 09:172.1 0.21 1
3-Nitroaniline ND mg/kg 11/27/19 15:39 99-09-211/27/19 09:172.1 0.22 1
4-Nitroaniline ND mg/kg 11/27/19 15:39 100-01-611/27/19 09:170.83 0.21 1
Nitrobenzene ND mg/kg 11/27/19 15:39 98-95-311/27/19 09:170.42 0.099 1
2-Nitrophenol ND mg/kg 11/27/19 15:39 88-75-511/27/19 09:170.42 0.13 1
4-Nitrophenol ND mg/kg 11/27/19 15:39 100-02-711/27/19 09:172.1 0.66 1
N-Nitrosodimethylamine ND mg/kg 11/27/19 15:39 62-75-911/27/19 09:170.42 0.12 1
N-Nitroso-di-n-propylamine ND mg/kg 11/27/19 15:39 621-64-711/27/19 09:170.42 0.12 1
N-Nitrosodiphenylamine ND mg/kg 11/27/19 15:39 86-30-611/27/19 09:170.42 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 11/27/19 15:39 108-60-111/27/19 09:170.42 0.12 1
Pentachlorophenol ND mg/kg 11/27/19 15:39 87-86-511/27/19 09:172.1 0.19 1
Phenanthrene ND mg/kg 11/27/19 15:39 85-01-811/27/19 09:170.42 0.10 1
Phenol ND mg/kg 11/27/19 15:39 108-95-211/27/19 09:170.42 0.099 1
Pyrene ND mg/kg 11/27/19 15:39 129-00-011/27/19 09:170.42 0.11 1
Pyridine ND mg/kg 11/27/19 15:39 110-86-111/27/19 09:170.42 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 15:39 120-82-111/27/19 09:170.42 0.095 1
2,4,5-Trichlorophenol ND mg/kg 11/27/19 15:39 95-95-411/27/19 09:170.42 0.11 1
2,4,6-Trichlorophenol ND mg/kg 11/27/19 15:39 88-06-211/27/19 09:170.42 0.10 1
Surrogates
Nitrobenzene-d5 (S)59 %11/27/19 15:39 4165-60-011/27/19 09:1723-110 1
2-Fluorobiphenyl (S)65 %11/27/19 15:39 321-60-811/27/19 09:1730-110 1
Terphenyl-d14 (S)71 %11/27/19 15:39 1718-51-011/27/19 09:1728-110 1
Phenol-d6 (S)58 %11/27/19 15:39 13127-88-311/27/19 09:1722-110 1
2-Fluorophenol (S)61 %11/27/19 15:39 367-12-411/27/19 09:1713-110 1
2,4,6-Tribromophenol (S)86 %11/27/19 15:39 118-79-611/27/19 09:1727-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454751
ROW-603
Sample: IDW SOIL Lab ID: 92454751001 Collected: 11/21/19 10:15 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 11/27/19 17:43 67-64-111/27/19 12:210.13 0.013 1
Benzene ND mg/kg 11/27/19 17:43 71-43-211/27/19 12:210.0066 0.0012 1
Bromobenzene ND mg/kg 11/27/19 17:43 108-86-111/27/19 12:210.0066 0.0018 1
Bromochloromethane ND mg/kg 11/27/19 17:43 74-97-511/27/19 12:210.0066 0.0016 1
Bromodichloromethane ND mg/kg 11/27/19 17:43 75-27-411/27/19 12:210.0066 0.0013 1
Bromoform ND mg/kg 11/27/19 17:43 75-25-211/27/19 12:210.0066 0.0032 1
Bromomethane ND mg/kg 11/27/19 17:43 74-83-9 IH11/27/19 12:210.013 0.0031 1
2-Butanone (MEK)ND mg/kg 11/27/19 17:43 78-93-311/27/19 12:210.13 0.016 1
n-Butylbenzene ND mg/kg 11/27/19 17:43 104-51-811/27/19 12:210.0066 0.0037 1
sec-Butylbenzene ND mg/kg 11/27/19 17:43 135-98-811/27/19 12:210.0066 0.0028 1
tert-Butylbenzene ND mg/kg 11/27/19 17:43 98-06-6 v211/27/19 12:210.0066 0.0022 1
Carbon tetrachloride ND mg/kg 11/27/19 17:43 56-23-511/27/19 12:210.0066 0.0013 1
Chlorobenzene ND mg/kg 11/27/19 17:43 108-90-711/27/19 12:210.0066 0.0013 1
Chloroethane ND mg/kg 11/27/19 17:43 75-00-3 IK11/27/19 12:210.013 0.0028 1
Chloroform ND mg/kg 11/27/19 17:43 67-66-311/27/19 12:210.0066 0.0014 1
Chloromethane ND mg/kg 11/27/19 17:43 74-87-311/27/19 12:210.013 0.0044 1
2-Chlorotoluene ND mg/kg 11/27/19 17:43 95-49-811/27/19 12:210.0066 0.0020 1
4-Chlorotoluene ND mg/kg 11/27/19 17:43 106-43-411/27/19 12:210.0066 0.0020 1
1,2-Dibromo-3-chloropropane ND mg/kg 11/27/19 17:43 96-12-811/27/19 12:210.0066 0.0034 1
Dibromochloromethane ND mg/kg 11/27/19 17:43 124-48-111/27/19 12:210.0066 0.0033 1
1,2-Dibromoethane (EDB)ND mg/kg 11/27/19 17:43 106-93-411/27/19 12:210.0066 0.0015 1
Dibromomethane ND mg/kg 11/27/19 17:43 74-95-311/27/19 12:210.0066 0.0020 1
1,2-Dichlorobenzene ND mg/kg 11/27/19 17:43 95-50-111/27/19 12:210.0066 0.0023 1
1,3-Dichlorobenzene ND mg/kg 11/27/19 17:43 541-73-111/27/19 12:210.0066 0.0024 1
1,4-Dichlorobenzene ND mg/kg 11/27/19 17:43 106-46-711/27/19 12:210.0066 0.0023 1
Dichlorodifluoromethane ND mg/kg 11/27/19 17:43 75-71-811/27/19 12:210.013 0.0055 1
1,1-Dichloroethane ND mg/kg 11/27/19 17:43 75-34-311/27/19 12:210.0066 0.00098 1
1,2-Dichloroethane ND mg/kg 11/27/19 17:43 107-06-211/27/19 12:210.0066 0.0013 1
1,1-Dichloroethene ND mg/kg 11/27/19 17:43 75-35-411/27/19 12:210.0066 0.0015 1
cis-1,2-Dichloroethene ND mg/kg 11/27/19 17:43 156-59-211/27/19 12:210.0066 0.0012 1
trans-1,2-Dichloroethene ND mg/kg 11/27/19 17:43 156-60-511/27/19 12:210.0066 0.0013 1
1,2-Dichloropropane ND mg/kg 11/27/19 17:43 78-87-511/27/19 12:210.0066 0.0025 1
1,3-Dichloropropane ND mg/kg 11/27/19 17:43 142-28-911/27/19 12:210.0066 0.0025 1
2,2-Dichloropropane ND mg/kg 11/27/19 17:43 594-20-711/27/19 12:210.0066 0.00066 1
1,1-Dichloropropene ND mg/kg 11/27/19 17:43 563-58-611/27/19 12:210.0066 0.0028 1
cis-1,3-Dichloropropene ND mg/kg 11/27/19 17:43 10061-01-511/27/19 12:210.0066 0.0030 1
trans-1,3-Dichloropropene ND mg/kg 11/27/19 17:43 10061-02-611/27/19 12:210.0066 0.0012 1
Diisopropyl ether ND mg/kg 11/27/19 17:43 108-20-311/27/19 12:210.0066 0.0038 1
Ethylbenzene ND mg/kg 11/27/19 17:43 100-41-411/27/19 12:210.0066 0.0014 1
Hexachloro-1,3-butadiene ND mg/kg 11/27/19 17:43 87-68-311/27/19 12:210.0066 0.0033 1
2-Hexanone ND mg/kg 11/27/19 17:43 591-78-611/27/19 12:210.066 0.0069 1
Isopropylbenzene (Cumene)ND mg/kg 11/27/19 17:43 98-82-811/27/19 12:210.0066 0.0019 1
p-Isopropyltoluene ND mg/kg 11/27/19 17:43 99-87-611/27/19 12:210.0066 0.0032 1
Methylene Chloride ND mg/kg 11/27/19 17:43 75-09-2 IH,v111/27/19 12:210.027 0.0078 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 11/27/19 17:43 108-10-111/27/19 12:210.066 0.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92454751
ROW-603
Sample: IDW SOIL Lab ID: 92454751001 Collected: 11/21/19 10:15 Received: 11/21/19 10:37 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND mg/kg 11/27/19 17:43 1634-04-411/27/19 12:210.0066 0.0038 1
Naphthalene ND mg/kg 11/27/19 17:43 91-20-311/27/19 12:210.0066 0.0056 1
n-Propylbenzene ND mg/kg 11/27/19 17:43 103-65-111/27/19 12:210.0066 0.0022 1
Styrene ND mg/kg 11/27/19 17:43 100-42-511/27/19 12:210.0066 0.0020 1
1,1,1,2-Tetrachloroethane ND mg/kg 11/27/19 17:43 630-20-611/27/19 12:210.0066 0.0016 1
1,1,2,2-Tetrachloroethane ND mg/kg 11/27/19 17:43 79-34-511/27/19 12:210.0066 0.0023 1
Tetrachloroethene ND mg/kg 11/27/19 17:43 127-18-411/27/19 12:210.0066 0.0021 1
Toluene ND mg/kg 11/27/19 17:43 108-88-311/27/19 12:210.0066 0.0022 1
1,2,3-Trichlorobenzene ND mg/kg 11/27/19 17:43 87-61-611/27/19 12:210.0066 0.0047 1
1,2,4-Trichlorobenzene ND mg/kg 11/27/19 17:43 120-82-111/27/19 12:210.0066 0.0035 1
1,1,1-Trichloroethane ND mg/kg 11/27/19 17:43 71-55-611/27/19 12:210.0066 0.0012 1
1,1,2-Trichloroethane ND mg/kg 11/27/19 17:43 79-00-511/27/19 12:210.0066 0.0015 1
Trichloroethene ND mg/kg 11/27/19 17:43 79-01-611/27/19 12:210.0066 0.0017 1
Trichlorofluoromethane ND mg/kg 11/27/19 17:43 75-69-411/27/19 12:210.0066 0.0016 1
1,2,3-Trichloropropane ND mg/kg 11/27/19 17:43 96-18-411/27/19 12:210.0066 0.0022 1
1,2,4-Trimethylbenzene ND mg/kg 11/27/19 17:43 95-63-611/27/19 12:210.0066 0.0026 1
1,3,5-Trimethylbenzene ND mg/kg 11/27/19 17:43 108-67-811/27/19 12:210.0066 0.0022 1
Vinyl acetate ND mg/kg 11/27/19 17:43 108-05-411/27/19 12:210.066 0.022 1
Vinyl chloride ND mg/kg 11/27/19 17:43 75-01-411/27/19 12:210.013 0.0025 1
Xylene (Total)ND mg/kg 11/27/19 17:43 1330-20-711/27/19 12:210.013 0.0046 1
m&p-Xylene ND mg/kg 11/27/19 17:43 179601-23-111/27/19 12:210.013 0.0031 1
o-Xylene ND mg/kg 11/27/19 17:43 95-47-611/27/19 12:210.0066 0.0016 1
Surrogates
Toluene-d8 (S)110 %11/27/19 17:43 2037-26-511/27/19 12:2170-130 1
4-Bromofluorobenzene (S)106 %11/27/19 17:43 460-00-411/27/19 12:2170-130 1
1,2-Dichloroethane-d4 (S)90 %11/27/19 17:43 17060-07-011/27/19 12:2170-132 1
Analytical Method: EPA 8260D Mod. Preparation Method: EPA 8260D Mod.8260D MSV SIM Soil
1,4-Dioxane (p-Dioxane)0.0084J mg/kg 11/25/19 15:37 123-91-111/25/19 11:520.014 0.0042 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/25/19 15:37 17060-07-011/25/19 11:5250-150 1
Toluene-d8 (S)104 %11/25/19 15:37 2037-26-511/25/19 11:5250-150 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.5 %11/21/19 16:550.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511178
EPA 7471B
EPA 7471B
7471 Mercury
Associated Lab Samples: 92454751001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2742192
Associated Lab Samples:92454751001
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 11/22/19 14:420.0030
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2742193LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0770.083 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2742194MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454639001
2742195
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.042 88 75-12580 12 200.041ND 0.040 0.035
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511799
EPA 3050B
EPA 6010D
6010 MET
Associated Lab Samples: 92454751001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744960
Associated Lab Samples:92454751001
Matrix: Solid
AnalyzedMDL
Arsenic mg/kg ND 1.0 12/01/19 22:130.50
Barium mg/kg ND 0.50 12/01/19 22:130.25
Cadmium mg/kg ND 0.10 12/01/19 22:130.050
Chromium mg/kg ND 0.50 12/01/19 22:130.25
Lead mg/kg ND 0.50 12/01/19 22:130.25
Selenium mg/kg 0.73J 1.0 BC12/02/19 13:150.50
Silver mg/kg ND 0.50 12/01/19 22:130.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744961LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 45.450 91 80-120
Barium mg/kg 48.850 98 80-120
Cadmium mg/kg 46.150 92 80-120
Chromium mg/kg 46.250 92 80-120
Lead mg/kg 47.050 94 80-120
Selenium mg/kg 40.0 BC5080 80-120
Silver mg/kg 23.425 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744962MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454748002
2744963
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 250 94 75-12591 1 20262ND236 238
Barium mg/kg 250 97 75-125116 5 202629301170 1230
Cadmium mg/kg 250 95 75-12592 1 202620.87 239 242
Chromium mg/kg 250 96 75-12594 2 2026218.9 259 265
Lead mg/kg 250 92 75-12587 0 2026239.8 269 268
Selenium mg/kg BC2507975-12576 1 20262ND200 202
Silver mg/kg 126 92 75-125105 8 20131158272 296
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512117
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92454751001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2746337
Associated Lab Samples:92454751001
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 11/27/19 10:530.0012
1,1,1-Trichloroethane mg/kg ND 0.0050 11/27/19 10:530.00087
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 11/27/19 10:530.0017
1,1,2-Trichloroethane mg/kg ND 0.0050 11/27/19 10:530.0011
1,1-Dichloroethane mg/kg ND 0.0050 11/27/19 10:530.00074
1,1-Dichloroethene mg/kg ND 0.0050 11/27/19 10:530.0012
1,1-Dichloropropene mg/kg ND 0.0050 11/27/19 10:530.0021
1,2,3-Trichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0036
1,2,3-Trichloropropane mg/kg ND 0.0050 11/27/19 10:530.0017
1,2,4-Trichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0026
1,2,4-Trimethylbenzene mg/kg ND 0.0050 11/27/19 10:530.0020
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 11/27/19 10:530.0025
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 11/27/19 10:530.0011
1,2-Dichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0018
1,2-Dichloroethane mg/kg ND 0.0050 11/27/19 10:530.0010
1,2-Dichloropropane mg/kg ND 0.0050 11/27/19 10:530.0019
1,3,5-Trimethylbenzene mg/kg ND 0.0050 11/27/19 10:530.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0018
1,3-Dichloropropane mg/kg ND 0.0050 11/27/19 10:530.0019
1,4-Dichlorobenzene mg/kg ND 0.0050 11/27/19 10:530.0017
2,2-Dichloropropane mg/kg ND 0.0050 11/27/19 10:530.00049
2-Butanone (MEK)mg/kg ND 0.10 11/27/19 10:530.012
2-Chlorotoluene mg/kg ND 0.0050 11/27/19 10:530.0015
2-Hexanone mg/kg ND 0.050 11/27/19 10:530.0052
4-Chlorotoluene mg/kg ND 0.0050 11/27/19 10:530.0015
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 11/27/19 10:530.0037
Acetone mg/kg ND 0.10 11/27/19 10:530.0094
Benzene mg/kg ND 0.0050 11/27/19 10:530.00090
Bromobenzene mg/kg ND 0.0050 11/27/19 10:530.0014
Bromochloromethane mg/kg ND 0.0050 11/27/19 10:530.0012
Bromodichloromethane mg/kg ND 0.0050 11/27/19 10:530.00098
Bromoform mg/kg ND 0.0050 11/27/19 10:530.0024
Bromomethane mg/kg ND 0.010 IH11/27/19 10:530.0024
Carbon tetrachloride mg/kg ND 0.0050 11/27/19 10:530.00096
Chlorobenzene mg/kg ND 0.0050 11/27/19 10:530.00097
Chloroethane mg/kg ND 0.010 IK11/27/19 10:530.0021
Chloroform mg/kg ND 0.0050 11/27/19 10:530.0011
Chloromethane mg/kg ND 0.010 11/27/19 10:530.0033
cis-1,2-Dichloroethene mg/kg ND 0.0050 11/27/19 10:530.00087
cis-1,3-Dichloropropene mg/kg ND 0.0050 11/27/19 10:530.0023
Dibromochloromethane mg/kg ND 0.0050 11/27/19 10:530.0025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2746337
Associated Lab Samples:92454751001
Matrix: Solid
AnalyzedMDL
Dibromomethane mg/kg ND 0.0050 11/27/19 10:530.0015
Dichlorodifluoromethane mg/kg ND 0.010 11/27/19 10:530.0041
Diisopropyl ether mg/kg ND 0.0050 11/27/19 10:530.0029
Ethylbenzene mg/kg ND 0.0050 11/27/19 10:530.0011
Hexachloro-1,3-butadiene mg/kg ND 0.0050 11/27/19 10:530.0025
Isopropylbenzene (Cumene)mg/kg ND 0.0050 11/27/19 10:530.0014
m&p-Xylene mg/kg ND 0.010 11/27/19 10:530.0024
Methyl-tert-butyl ether mg/kg ND 0.0050 11/27/19 10:530.0029
Methylene Chloride mg/kg 0.014J 0.020 IH,v111/27/19 10:530.0059
n-Butylbenzene mg/kg ND 0.0050 11/27/19 10:530.0028
n-Propylbenzene mg/kg ND 0.0050 11/27/19 10:530.0017
Naphthalene mg/kg ND 0.0050 11/27/19 10:530.0042
o-Xylene mg/kg ND 0.0050 11/27/19 10:530.0012
p-Isopropyltoluene mg/kg ND 0.0050 11/27/19 10:530.0024
sec-Butylbenzene mg/kg ND 0.0050 11/27/19 10:530.0021
Styrene mg/kg ND 0.0050 11/27/19 10:530.0015
tert-Butylbenzene mg/kg ND 0.0050 v211/27/19 10:530.0017
Tetrachloroethene mg/kg ND 0.0050 11/27/19 10:530.0016
Toluene mg/kg ND 0.0050 11/27/19 10:530.0016
trans-1,2-Dichloroethene mg/kg ND 0.0050 11/27/19 10:530.00098
trans-1,3-Dichloropropene mg/kg ND 0.0050 11/27/19 10:530.00088
Trichloroethene mg/kg ND 0.0050 11/27/19 10:530.0013
Trichlorofluoromethane mg/kg ND 0.0050 11/27/19 10:530.0012
Vinyl acetate mg/kg ND 0.050 11/27/19 10:530.016
Vinyl chloride mg/kg ND 0.010 11/27/19 10:530.0019
Xylene (Total)mg/kg ND 0.010 11/27/19 10:530.0035
1,2-Dichloroethane-d4 (S)%95 70-132 11/27/19 10:53
4-Bromofluorobenzene (S)%105 70-130 11/27/19 10:53
Toluene-d8 (S)%105 70-130 11/27/19 10:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746338LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.0500.05 100 70-130
1,1,1-Trichloroethane mg/kg 0.0500.05 101 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.0490.05 98 55-130
1,1,2-Trichloroethane mg/kg 0.0490.05 98 70-130
1,1-Dichloroethane mg/kg 0.0470.05 93 68-130
1,1-Dichloroethene mg/kg 0.0490.05 98 70-130
1,1-Dichloropropene mg/kg 0.0540.05 109 70-130
1,2,3-Trichlorobenzene mg/kg 0.0460.05 93 70-130
1,2,3-Trichloropropane mg/kg 0.0500.05 99 70-130
1,2,4-Trichlorobenzene mg/kg 0.0470.05 93 70-130
1,2,4-Trimethylbenzene mg/kg 0.0480.05 96 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746338LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane mg/kg 0.0490.05 99 57-141
1,2-Dibromoethane (EDB)mg/kg 0.0500.05 100 70-130
1,2-Dichlorobenzene mg/kg 0.0460.05 92 70-130
1,2-Dichloroethane mg/kg 0.0460.05 92 70-130
1,2-Dichloropropane mg/kg 0.0480.05 96 70-130
1,3,5-Trimethylbenzene mg/kg 0.0480.05 96 70-130
1,3-Dichlorobenzene mg/kg 0.0480.05 95 70-130
1,3-Dichloropropane mg/kg 0.0500.05 100 70-130
1,4-Dichlorobenzene mg/kg 0.0470.05 94 70-130
2,2-Dichloropropane mg/kg 0.0500.05 101 70-130
2-Butanone (MEK)mg/kg 0.10J0.1 100 60-130
2-Chlorotoluene mg/kg 0.0490.05 97 70-130
2-Hexanone mg/kg 0.100.1 105 70-132
4-Chlorotoluene mg/kg 0.0480.05 96 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.100.1 102 69-130
Acetone mg/kg 0.095J0.1 95 49-148
Benzene mg/kg 0.0500.05 99 70-130
Bromobenzene mg/kg 0.0470.05 95 70-130
Bromochloromethane mg/kg 0.0440.05 87 70-130
Bromodichloromethane mg/kg 0.0480.05 97 70-130
Bromoform mg/kg 0.0500.05 100 68-136
Bromomethane mg/kg 0.055 IH0.05 110 60-140
Carbon tetrachloride mg/kg 0.0510.05 101 70-130
Chlorobenzene mg/kg 0.0490.05 98 70-130
Chloroethane mg/kg 0.057 IK0.05 114 51-147
Chloroform mg/kg 0.0460.05 93 70-130
Chloromethane mg/kg 0.0530.05 106 48-130
cis-1,2-Dichloroethene mg/kg 0.0460.05 93 70-130
cis-1,3-Dichloropropene mg/kg 0.0490.05 98 70-130
Dibromochloromethane mg/kg 0.0510.05 102 70-130
Dibromomethane mg/kg 0.0460.05 91 70-130
Dichlorodifluoromethane mg/kg 0.0540.05 109 49-130
Diisopropyl ether mg/kg 0.0480.05 96 66-130
Ethylbenzene mg/kg 0.0500.05 100 70-130
Hexachloro-1,3-butadiene mg/kg 0.0490.05 99 70-130
Isopropylbenzene (Cumene)mg/kg 0.0510.05 102 70-130
m&p-Xylene mg/kg 0.100.1 100 70-130
Methyl-tert-butyl ether mg/kg 0.0490.05 98 70-130
Methylene Chloride mg/kg 0.064 IH,v10.05 128 50-137
n-Butylbenzene mg/kg 0.0490.05 98 70-130
n-Propylbenzene mg/kg 0.0500.05 100 70-130
Naphthalene mg/kg 0.0470.05 94 70-131
o-Xylene mg/kg 0.0500.05 100 70-130
p-Isopropyltoluene mg/kg 0.0490.05 99 70-130
sec-Butylbenzene mg/kg 0.0500.05 100 70-130
Styrene mg/kg 0.0500.05 99 70-130
tert-Butylbenzene mg/kg 0.050 v30.05 100 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2746338LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene mg/kg 0.0510.05 102 56-130
Toluene mg/kg 0.0470.05 93 70-130
trans-1,2-Dichloroethene mg/kg 0.0470.05 94 70-130
trans-1,3-Dichloropropene mg/kg 0.0500.05 100 70-130
Trichloroethene mg/kg 0.0520.05 104 70-141
Trichlorofluoromethane mg/kg 0.0570.05 114 67-130
Vinyl acetate mg/kg 0.0960.1 96 10-136
Vinyl chloride mg/kg 0.0550.05 109 67-130
Xylene (Total)mg/kg 0.150.15 100 70-130
1,2-Dichloroethane-d4 (S)%95 70-132
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2746340MATRIX SPIKE SAMPLE:
MSSpike
Result
92454745002
1,1,1,2-Tetrachloroethane mg/kg 0.00900.016 56 52-133ND
1,1,1-Trichloroethane mg/kg 0.00840.016 52 49-137ND
1,1,2,2-Tetrachloroethane mg/kg 0.0120.016 72 39-150ND
1,1,2-Trichloroethane mg/kg 0.0110.016 70 48-140ND
1,1-Dichloroethane mg/kg 0.00960.016 60 46-135ND
1,1-Dichloroethene mg/kg 0.00900.016 56 38-149ND
1,1-Dichloropropene mg/kg 0.00840.016 52 41-140ND
1,2,3-Trichlorobenzene mg/kg 0.0100.016 64 10-158ND
1,2,3-Trichloropropane mg/kg 0.0120.016 75 33-157ND
1,2,4-Trichlorobenzene mg/kg 0.00990.016 61 10-155ND
1,2,4-Trimethylbenzene mg/kg 0.00910.016 57 24-154ND
1,2-Dibromo-3-chloropropane mg/kg 0.0130.016 81 33-158ND
1,2-Dibromoethane (EDB)mg/kg 0.0110.016 66 40-136ND
1,2-Dichlorobenzene mg/kg 0.0100.016 63 27-146ND
1,2-Dichloroethane mg/kg 0.0110.016 69 49-140ND
1,2-Dichloropropane mg/kg 0.0100.016 62 44-143ND
1,3,5-Trimethylbenzene mg/kg 0.00870.016 54 40-144ND
1,3-Dichlorobenzene mg/kg 0.00970.016 60 33-140ND
1,3-Dichloropropane mg/kg 0.0110.016 66 47-147ND
1,4-Dichlorobenzene mg/kg 0.0100.016 62 35-139ND
2,2-Dichloropropane mg/kg 0.00860.016 53 41-140ND
2-Butanone (MEK)mg/kg 0.021J0.032 64 10-181ND
2-Chlorotoluene mg/kg 0.00920.016 57 38-147ND
2-Hexanone mg/kg 0.025J0.032 76 18-169ND
4-Chlorotoluene mg/kg 0.00920.016 57 36-145ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.025J0.032 78 16-175ND
Acetone mg/kg 0.029J0.032 89 10-200ND
Benzene mg/kg 0.00940.016 58 46-136ND
Bromobenzene mg/kg 0.0110.016 67 38-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2746340MATRIX SPIKE SAMPLE:
MSSpike
Result
92454745002
Bromochloromethane mg/kg 0.0100.016 65 44-142ND
Bromodichloromethane mg/kg 0.00990.016 62 41-140ND
Bromoform mg/kg 0.0100.016 65 34-145ND
Bromomethane mg/kg 0.0084 IH0.016 52 14-162ND
Carbon tetrachloride mg/kg 0.0110.016 67 44-141ND
Chlorobenzene mg/kg 0.00950.016 59 39-141ND
Chloroethane mg/kg 0.011 IK0.016 70 10-182ND
Chloroform mg/kg 0.0100.016 64 45-140ND
Chloromethane mg/kg 0.0100.016 62 19-149ND
cis-1,2-Dichloroethene mg/kg 0.00940.016 58 38-150ND
cis-1,3-Dichloropropene mg/kg 0.00990.016 61 30-144ND
Dibromochloromethane mg/kg 0.0100.016 63 36-145ND
Dibromomethane mg/kg 0.0120.016 74 41-145ND
Dichlorodifluoromethane mg/kg 0.00910.016 57 16-146ND
Diisopropyl ether mg/kg 0.00970.016 60 41-143ND
Ethylbenzene mg/kg 0.00920.016 57 35-144ND
Hexachloro-1,3-butadiene mg/kg 0.00810.016 50 10-160ND
Isopropylbenzene (Cumene)mg/kg 0.00860.016 53 30-152ND
m&p-Xylene mg/kg 0.0180.032 56 33-145ND
Methyl-tert-butyl ether mg/kg 0.0110.016 68 49-140ND
Methylene Chloride mg/kg 0.011J IH,v10.016 66 10-174ND
n-Butylbenzene mg/kg 0.00810.016 50 10-160ND
n-Propylbenzene mg/kg 0.00850.016 53 24-159ND
Naphthalene mg/kg 0.0120.016 73 10-171ND
o-Xylene mg/kg 0.00960.016 59 31-150ND
p-Isopropyltoluene mg/kg 0.00830.016 52 21-154ND
sec-Butylbenzene mg/kg 0.00820.016 51 19-159ND
Styrene mg/kg 0.00980.016 61 15-152ND
tert-Butylbenzene mg/kg 0.0073 v30.016 45 31-141ND
Tetrachloroethene mg/kg 0.00770.016 48 19-141ND
Toluene mg/kg 0.00940.016 59 31-146ND
trans-1,2-Dichloroethene mg/kg 0.0100.016 62 28-157ND
trans-1,3-Dichloropropene mg/kg 0.0100.016 64 25-146ND
Trichloroethene mg/kg 0.00870.016 54 34-149ND
Trichlorofluoromethane mg/kg 0.00930.016 58 10-167ND
Vinyl acetate mg/kg 0.025J0.032 78 10-200ND
Vinyl chloride mg/kg 0.0100.016 64 36-155ND
Xylene (Total)mg/kg 0.0280.049 57 29-148ND
1,2-Dichloroethane-d4 (S)%99 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454745001
2746339SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND IH30ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND IK30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454745001
2746339SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND IH,v130ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND v230ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9196
4-Bromofluorobenzene (S)%102108
Toluene-d8 (S)%105105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511556
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV Soil SIM
Associated Lab Samples: 92454751001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2743926
Associated Lab Samples:92454751001
Matrix: Solid
AnalyzedMDL
1,4-Dioxane (p-Dioxane)mg/kg ND 0.010 11/25/19 11:150.0030
1,2-Dichloroethane-d4 (S)%103 50-150 11/25/19 11:15
Toluene-d8 (S)%99 50-150 11/25/19 11:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2743927LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)mg/kg 0.0400.04 99 50-150
1,2-Dichloroethane-d4 (S)%103 50-150
Toluene-d8 (S)%103 50-150
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2744454MATRIX SPIKE SAMPLE:
MSSpike
Result
92454623002
1,4-Dioxane (p-Dioxane)mg/kg 0.0520.045 104 50-1500.0047J
1,2-Dichloroethane-d4 (S)%95 50-150
Toluene-d8 (S)%105 50-150
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454623001
2744453SAMPLE DUPLICATE:
1,4-Dioxane (p-Dioxane)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%95 3099
Toluene-d8 (S)%109 30100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511777
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples: 92454751001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744914
Associated Lab Samples:92454751001
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 11/26/19 20:280.076
1,2-Dichlorobenzene mg/kg ND 0.33 11/26/19 20:280.071
1,3-Dichlorobenzene mg/kg ND 0.33 11/26/19 20:280.074
1,4-Dichlorobenzene mg/kg ND 0.33 11/26/19 20:280.073
1-Methylnaphthalene mg/kg ND 0.33 11/26/19 20:280.088
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 11/26/19 20:280.092
2,4,5-Trichlorophenol mg/kg ND 0.33 11/26/19 20:280.086
2,4,6-Trichlorophenol mg/kg ND 0.33 11/26/19 20:280.083
2,4-Dichlorophenol mg/kg ND 0.33 11/26/19 20:280.11
2,4-Dimethylphenol mg/kg ND 0.33 11/26/19 20:280.082
2,4-Dinitrophenol mg/kg ND 1.6 11/26/19 20:281.1
2,4-Dinitrotoluene mg/kg ND 0.33 11/26/19 20:280.087
2,6-Dinitrotoluene mg/kg ND 0.33 11/26/19 20:280.086
2-Chloronaphthalene mg/kg ND 0.33 11/26/19 20:280.074
2-Chlorophenol mg/kg ND 0.33 11/26/19 20:280.077
2-Methylnaphthalene mg/kg ND 0.33 11/26/19 20:280.084
2-Methylphenol(o-Cresol)mg/kg ND 0.33 11/26/19 20:280.073
2-Nitroaniline mg/kg ND 1.6 11/26/19 20:280.17
2-Nitrophenol mg/kg ND 0.33 11/26/19 20:280.10
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 11/26/19 20:280.083
3,3'-Dichlorobenzidine mg/kg ND 1.6 11/26/19 20:280.23
3-Nitroaniline mg/kg ND 1.6 11/26/19 20:280.18
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 11/26/19 20:280.53
4-Bromophenylphenyl ether mg/kg ND 0.33 11/26/19 20:280.087
4-Chloro-3-methylphenol mg/kg ND 0.66 11/26/19 20:280.20
4-Chloroaniline mg/kg ND 1.6 11/26/19 20:280.20
4-Chlorophenylphenyl ether mg/kg ND 0.33 11/26/19 20:280.086
4-Nitroaniline mg/kg ND 0.66 11/26/19 20:280.16
4-Nitrophenol mg/kg ND 1.6 11/26/19 20:280.53
Acenaphthene mg/kg ND 0.33 11/26/19 20:280.085
Acenaphthylene mg/kg ND 0.33 11/26/19 20:280.078
Aniline mg/kg ND 0.33 11/26/19 20:280.074
Anthracene mg/kg ND 0.33 11/26/19 20:280.086
Benzo(a)anthracene mg/kg ND 0.33 11/26/19 20:280.10
Benzo(a)pyrene mg/kg ND 0.33 11/26/19 20:280.14
Benzo(b)fluoranthene mg/kg ND 0.33 11/26/19 20:280.13
Benzo(g,h,i)perylene mg/kg ND 0.33 11/26/19 20:280.13
Benzo(k)fluoranthene mg/kg ND 0.33 11/26/19 20:280.14
Benzoic Acid mg/kg ND 1.6 11/26/19 20:280.36
Benzyl alcohol mg/kg ND 0.66 11/26/19 20:280.18
bis(2-Chloroethoxy)methane mg/kg ND 0.33 11/26/19 20:280.088
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744914
Associated Lab Samples:92454751001
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether mg/kg ND 0.33 11/26/19 20:280.070
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 11/26/19 20:280.11
Butylbenzylphthalate mg/kg ND 0.33 11/26/19 20:280.088
Chrysene mg/kg ND 0.33 11/26/19 20:280.096
Di-n-butylphthalate mg/kg ND 0.33 11/26/19 20:280.081
Di-n-octylphthalate mg/kg ND 0.33 11/26/19 20:280.19
Dibenz(a,h)anthracene mg/kg ND 0.33 11/26/19 20:280.13
Dibenzofuran mg/kg ND 0.33 11/26/19 20:280.082
Diethylphthalate mg/kg ND 0.33 11/26/19 20:280.072
Dimethylphthalate mg/kg ND 0.33 11/26/19 20:280.075
Fluoranthene mg/kg ND 0.33 11/26/19 20:280.10
Fluorene mg/kg ND 0.33 11/26/19 20:280.088
Hexachloro-1,3-butadiene mg/kg ND 0.33 11/26/19 20:280.080
Hexachlorobenzene mg/kg ND 0.33 11/26/19 20:280.084
Hexachlorocyclopentadiene mg/kg ND 0.33 11/26/19 20:280.13
Hexachloroethane mg/kg ND 0.33 11/26/19 20:280.075
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 11/26/19 20:280.15
Isophorone mg/kg ND 0.33 11/26/19 20:280.072
N-Nitroso-di-n-propylamine mg/kg ND 0.33 11/26/19 20:280.092
N-Nitrosodimethylamine mg/kg ND 0.33 11/26/19 20:280.093
N-Nitrosodiphenylamine mg/kg ND 0.33 11/26/19 20:280.084
Naphthalene mg/kg ND 0.33 11/26/19 20:280.079
Nitrobenzene mg/kg ND 0.33 11/26/19 20:280.079
Pentachlorophenol mg/kg ND 1.6 11/26/19 20:280.15
Phenanthrene mg/kg ND 0.33 11/26/19 20:280.083
Phenol mg/kg ND 0.33 11/26/19 20:280.079
Pyrene mg/kg ND 0.33 11/26/19 20:280.091
Pyridine mg/kg ND 0.33 11/26/19 20:280.084
2,4,6-Tribromophenol (S)%97 27-110 11/26/19 20:28
2-Fluorobiphenyl (S)%83 30-110 11/26/19 20:28
2-Fluorophenol (S)%82 13-110 11/26/19 20:28
Nitrobenzene-d5 (S)%80 23-110 11/26/19 20:28
Phenol-d6 (S)%79 22-110 11/26/19 20:28
Terphenyl-d14 (S)%95 28-110 11/26/19 20:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744915LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.41.7 86 52-130
1,2-Dichlorobenzene mg/kg 1.41.7 86 51-130
1,3-Dichlorobenzene mg/kg 1.41.7 85 50-130
1,4-Dichlorobenzene mg/kg 1.41.7 84 49-130
1-Methylnaphthalene mg/kg 1.51.7 87 55-130
2,2'-Oxybis(1-chloropropane)mg/kg 1.31.7 78 30-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744915LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol mg/kg 1.51.7 88 55-130
2,4,6-Trichlorophenol mg/kg 1.51.7 92 57-130
2,4-Dichlorophenol mg/kg 1.51.7 88 56-130
2,4-Dimethylphenol mg/kg 1.51.7 90 51-130
2,4-Dinitrophenol mg/kg 7.38.4 87 27-133
2,4-Dinitrotoluene mg/kg 1.51.7 92 61-130
2,6-Dinitrotoluene mg/kg 1.51.7 92 60-130
2-Chloronaphthalene mg/kg 1.51.7 89 52-130
2-Chlorophenol mg/kg 1.51.7 87 54-130
2-Methylnaphthalene mg/kg 1.51.7 89 54-130
2-Methylphenol(o-Cresol)mg/kg 1.41.7 84 51-130
2-Nitroaniline mg/kg 3.03.3 90 51-130
2-Nitrophenol mg/kg 1.51.7 88 49-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.41.7 83 11-163
3,3'-Dichlorobenzidine mg/kg 2.53.3 75 10-132
3-Nitroaniline mg/kg 2.63.3 78 55-130
4,6-Dinitro-2-methylphenol mg/kg 3.63.3 107 47-142
4-Bromophenylphenyl ether mg/kg 1.51.7 91 59-130
4-Chloro-3-methylphenol mg/kg 2.93.3 88 55-130
4-Chloroaniline mg/kg 2.93.3 86 54-130
4-Chlorophenylphenyl ether mg/kg 1.51.7 90 58-130
4-Nitroaniline mg/kg 2.83.3 83 54-130
4-Nitrophenol mg/kg 6.98.4 83 48-130
Acenaphthene mg/kg 1.61.7 95 60-130
Acenaphthylene mg/kg 1.71.7 101 60-130
Aniline mg/kg 1.31.7 81 43-130
Anthracene mg/kg 1.71.7 101 63-130
Benzo(a)anthracene mg/kg 1.61.7 93 59-130
Benzo(a)pyrene mg/kg 1.81.7 105 57-130
Benzo(b)fluoranthene mg/kg 1.71.7 100 54-130
Benzo(g,h,i)perylene mg/kg 1.81.7 108 59-130
Benzo(k)fluoranthene mg/kg 1.71.7 103 54-130
Benzoic Acid mg/kg 6.28.4 74 19-130
Benzyl alcohol mg/kg 2.83.3 85 50-130
bis(2-Chloroethoxy)methane mg/kg 1.51.7 87 54-130
bis(2-Chloroethyl) ether mg/kg 1.51.7 92 48-130
bis(2-Ethylhexyl)phthalate mg/kg 1.41.7 86 45-134
Butylbenzylphthalate mg/kg 1.51.7 87 46-138
Chrysene mg/kg 1.51.7 89 58-130
Di-n-butylphthalate mg/kg 1.41.7 86 60-130
Di-n-octylphthalate mg/kg 1.51.7 91 53-130
Dibenz(a,h)anthracene mg/kg 1.71.7 102 59-130
Dibenzofuran mg/kg 1.51.7 90 60-130
Diethylphthalate mg/kg 1.41.7 85 60-130
Dimethylphthalate mg/kg 1.41.7 86 60-130
Fluoranthene mg/kg 1.61.7 95 65-130
Fluorene mg/kg 1.61.7 94 63-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744915LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene mg/kg 1.41.7 86 46-130
Hexachlorobenzene mg/kg 1.51.7 92 58-130
Hexachlorocyclopentadiene mg/kg 1.81.7 107 23-130
Hexachloroethane mg/kg 1.51.7 87 47-130
Indeno(1,2,3-cd)pyrene mg/kg 1.71.7 104 60-130
Isophorone mg/kg 1.41.7 86 49-130
N-Nitroso-di-n-propylamine mg/kg 1.41.7 86 47-130
N-Nitrosodimethylamine mg/kg 1.51.7 91 45-130
N-Nitrosodiphenylamine mg/kg 1.51.7 87 59-130
Naphthalene mg/kg 1.51.7 91 55-130
Nitrobenzene mg/kg 1.41.7 86 49-130
Pentachlorophenol mg/kg 2.93.3 88 10-132
Phenanthrene mg/kg 1.61.7 97 62-130
Phenol mg/kg 1.61.7 95 46-130
Pyrene mg/kg 1.61.7 98 53-130
Pyridine mg/kg 1.11.7 67 37-130
2,4,6-Tribromophenol (S)%S0111 27-110
2-Fluorobiphenyl (S)%96 30-110
2-Fluorophenol (S)%95 13-110
Nitrobenzene-d5 (S)%88 23-110
Phenol-d6 (S)%94 22-110
Terphenyl-d14 (S)%99 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744916MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92449762007
2744917
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene mg/kg 1.7 74 18-13076 301.7ND 1.2J 1.3J
1,2-Dichlorobenzene mg/kg 1.7 68 14-13073 301.7ND 1.2J 1.2J
1,3-Dichlorobenzene mg/kg 1.7 65 12-13073 301.7ND 1.1J 1.2J
1,4-Dichlorobenzene mg/kg 1.7 65 10-13069 301.7ND 1.1J 1.2J
1-Methylnaphthalene mg/kg M11.7 15 12-13010 301.7ND 1.6J 1.6J
2,2'-Oxybis(1-
chloropropane)mg/kg 1.7 64 10-13067 301.7ND 1.1J 1.1J
2,4,5-Trichlorophenol mg/kg 1.7 63 13-13072 301.7ND 1.1J 1.2J
2,4,6-Trichlorophenol mg/kg 1.7 66 17-13071 301.7ND 1.1J 1.2J
2,4-Dichlorophenol mg/kg 1.7 69 10-13073 301.7ND 1.2J 1.2J
2,4-Dimethylphenol mg/kg 1.7 117 10-13099 16 301.7ND 2.0 1.7
2,4-Dinitrophenol mg/kg 8.4 41 10-13041 308.4ND ND ND
2,4-Dinitrotoluene mg/kg 1.7 64 24-13071 301.7ND 1.1J 1.2J
2,6-Dinitrotoluene mg/kg 1.7 114 23-13094 301.7ND 1.9 1.6J
2-Chloronaphthalene mg/kg 1.7 74 19-13075 301.7ND 1.2J 1.3J
2-Chlorophenol mg/kg 1.7 67 10-13072 301.7ND 1.1J 1.2J
2-Methylnaphthalene mg/kg 1.7 46 18-13044 301.7ND 1.4J 1.4J
2-Methylphenol(o-Cresol) mg/kg 1.7 62 10-13063 301.7ND 1.0J 1.1J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744916MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92449762007
2744917
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitroaniline mg/kg 3.4 56 17-13059 303.4ND 1.9J 2.0J
2-Nitrophenol mg/kg 1.7 73 10-13078 301.7ND 1.2J 1.3J
3&4-Methylphenol(m&p
Cresol)mg/kg 1.7 60 10-13064 301.7ND 1.0J 1.1J
3,3'-Dichlorobenzidine mg/kg 3.4 30 10-13021 303.4ND ND ND
3-Nitroaniline mg/kg 3.4 79 24-130103 303.4ND 2.7J 3.5J
4,6-Dinitro-2-methylphenol mg/kg 3.4 50 10-15262 303.4ND ND ND
4-Bromophenylphenyl ether mg/kg 1.7 82 29-13089 301.7ND 1.4J 1.5J
4-Chloro-3-methylphenol mg/kg 3.4 62 17-13068 303.4ND 2.1J 2.3J
4-Chloroaniline mg/kg 3.4 58 14-13063 303.4ND 1.9J 2.1J
4-Chlorophenylphenyl ether mg/kg 1.7 92 25-13084 301.7ND 1.6J 1.4J
4-Nitroaniline mg/kg 3.4 62 22-13069 303.4ND 2.1J 2.3J
4-Nitrophenol mg/kg 8.4 75 10-13070 308.4ND 6.3J 5.9J
Acenaphthene mg/kg 1.7 71 20-13078 301.7ND 1.2J 1.3J
Acenaphthylene mg/kg 1.7 85 25-13077 301.7ND 1.4J 1.3J
Aniline mg/kg 1.7 49 10-13052 301.7ND 0.83J 0.88J
Anthracene mg/kg 1.7 79 29-13082 301.7ND 1.3J 1.4J
Benzo(a)anthracene mg/kg 1.7 70 19-13075 301.7ND 1.2J 1.3J
Benzo(a)pyrene mg/kg 1.7 70 12-13075 301.7ND 1.2J 1.3J
Benzo(b)fluoranthene mg/kg 1.7 67 14-13071 301.7ND 1.1J 1.2J
Benzo(g,h,i)perylene mg/kg 1.7 72 10-13074 301.7ND 1.2J 1.3J
Benzo(k)fluoranthene mg/kg 1.7 66 14-13073 301.7ND 1.1J 1.2J
Benzoic Acid mg/kg 8.4 59 10-13061 308.4ND 5.0J 5.1J
Benzyl alcohol mg/kg 3.4 57 13-13065 303.4ND 1.9J 2.2J
bis(2-
Chloroethoxy)methane mg/kg 1.7 70 16-13073 301.7ND 1.2J 1.2J
bis(2-Chloroethyl) ether mg/kg 1.7 67 11-13068 301.7ND 1.1J 1.1J
bis(2-Ethylhexyl)phthalate mg/kg 1.7 64 21-13070 301.7ND 1.1J 1.2J
Butylbenzylphthalate mg/kg 1.7 68 23-13071 301.7ND 1.1J 1.2J
Chrysene mg/kg 1.7 66 22-13068 301.7ND 1.1J 1.2J
Di-n-butylphthalate mg/kg 1.7 64 30-13069 301.7ND 1.1J 1.2J
Di-n-octylphthalate mg/kg 1.7 66 23-14272 301.7ND 1.1J 1.2J
Dibenz(a,h)anthracene mg/kg 1.7 64 10-13067 301.7ND 1.1J 1.1J
Dibenzofuran mg/kg 1.7 75 24-13080 301.7ND 1.3J 1.3J
Diethylphthalate mg/kg 1.7 66 26-13064 301.7ND 1.1J 1.1J
Dimethylphthalate mg/kg 1.7 72 22-13066 301.7ND 1.2J 1.1J
Fluoranthene mg/kg 1.7 72 33-13074 301.7ND 1.2J 1.3J
Fluorene mg/kg 1.7 82 22-13076 301.7ND 1.4J 1.3J
Hexachloro-1,3-butadiene mg/kg 1.7 73 13-13076 301.7ND 1.2J 1.3J
Hexachlorobenzene mg/kg 1.7 80 29-13087 301.7ND 1.3J 1.5J
Hexachlorocyclopentadiene mg/kg 1.7 65 10-13069 301.7ND 1.1J 1.2J
Hexachloroethane mg/kg 1.7 63 10-13074 301.7ND 1.1J 1.3J
Indeno(1,2,3-cd)pyrene mg/kg 1.7 67 10-13074 301.7ND 1.1J 1.3J
Isophorone mg/kg 1.7 70 13-13072 301.7ND 1.2J 1.2J
N-Nitroso-di-n-propylamine mg/kg 1.7 67 12-13071 301.7ND 1.1J 1.2J
N-Nitrosodimethylamine mg/kg 1.7 35 11-13035 301.7ND 0.58J 0.60J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744916MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92449762007
2744917
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodiphenylamine mg/kg M1,R11.7 180 15-130117 42 301.7ND 3.0 2.0
Naphthalene mg/kg 1.7 77 15-13079 301.7ND 1.3J 1.3J
Nitrobenzene mg/kg 1.7 68 12-13069 301.7ND 1.1J 1.2J
Pentachlorophenol mg/kg 3.4 65 10-13068 303.4ND 2.2J 2.3J
Phenanthrene mg/kg 1.7 82 27-13084 301.7ND 1.4J 1.4J
Phenol mg/kg 1.7 66 10-13071 301.7ND 1.1J 1.2J
Pyrene mg/kg 1.7 62 19-13057 301.7ND 1.6J 1.6J
Pyridine mg/kg 1.7 23 10-13027 301.7ND ND 0.46J
2,4,6-Tribromophenol (S) %89 27-11093
2-Fluorobiphenyl (S)%57 30-11067
2-Fluorophenol (S)%56 13-11065
Nitrobenzene-d5 (S)%D36523-11066
Phenol-d6 (S)%55 22-11061
Terphenyl-d14 (S)%59 28-11071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92454751
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511055
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92454751001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92452974014
2741784SAMPLE DUPLICATE:
Percent Moisture %12.415.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92454622005
2741793SAMPLE DUPLICATE:
Percent Moisture %21.8 1 2521.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92454751
ROW-603
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.BC
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92454751
ROW-603
ANALYTE QUALIFIERS
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92454751
ROW-603
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92454751001 511799 511946IDW SOIL EPA 3050B EPA 6010D
92454751001 511178 511280IDW SOIL EPA 7471B EPA 7471B
92454751001 511777 512023IDW SOIL EPA 3546 EPA 8270E
92454751001 512117 512123IDW SOIL EPA 5035A EPA 8260D
92454751001 511556 511649IDW SOIL EPA 8260D Mod.EPA 8260D Mod.
92454751001 511055IDW SOIL ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/03/2019 09:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 31
Page 29 of 31
Page 30 of 31
Page 31 of 31
#=CL#
December 10, 2019
LIMS USE: FR - DAVID GRAHAM
LIMS OBJECT ID: 92455130
92455130
Project:
Pace Project No.:
RE:
David Graham
Hart & Hickman
2923 S. Tryon Street
Charlotte, NC 28203
ROW-603
Dear David Graham:
Enclosed are the analytical results for sample(s) received by the laboratory on November 22, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92455130
ROW-603
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92455130
ROW-603
Lab ID Sample ID Matrix Date Collected Date Received
92455130001 IDW-GW Water 11/22/19 13:30 11/22/19 15:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92455130
ROW-603
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92455130001 IDW-GW EPA 6010D 7 PASI-ADS
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CDLK
EPA 8260D Mod.3 PASI-CLMB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455130
ROW-603
Sample: IDW-GW Lab ID: 92455130001 Collected: 11/22/19 13:30 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/27/19 23:32 7440-38-211/26/19 02:2410.0 4.7 1
Barium 253 ug/L 11/27/19 23:32 7440-39-311/26/19 02:245.0 1.0 1
Cadmium ND ug/L 11/27/19 23:32 7440-43-911/26/19 02:241.0 0.40 1
Chromium 17.1 ug/L 11/27/19 23:32 7440-47-311/26/19 02:245.0 1.0 1
Lead ND ug/L 11/27/19 23:32 7439-92-111/26/19 02:245.0 1.6 1
Selenium ND ug/L 11/27/19 23:32 7782-49-211/26/19 02:2410.0 4.7 1
Silver ND ug/L 11/27/19 23:32 7440-22-411/26/19 02:245.0 2.5 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 12/03/19 14:48 7439-97-612/03/19 11:020.20 0.10 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 11/27/19 20:12 83-32-911/26/19 18:2310.0 1.6 1
Acenaphthylene ND ug/L 11/27/19 20:12 208-96-811/26/19 18:2310.0 1.6 1
Aniline ND ug/L 11/27/19 20:12 62-53-311/26/19 18:2310.0 1.9 1
Anthracene ND ug/L 11/27/19 20:12 120-12-711/26/19 18:2310.0 1.7 1
Benzo(a)anthracene ND ug/L 11/27/19 20:12 56-55-311/26/19 18:2310.0 1.8 1
Benzo(a)pyrene ND ug/L 11/27/19 20:12 50-32-811/26/19 18:2310.0 2.1 1
Benzo(b)fluoranthene ND ug/L 11/27/19 20:12 205-99-211/26/19 18:2310.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 11/27/19 20:12 191-24-211/26/19 18:2310.0 1.4 1
Benzo(k)fluoranthene ND ug/L 11/27/19 20:12 207-08-911/26/19 18:2310.0 1.9 1
Benzoic Acid ND ug/L 11/27/19 20:12 65-85-011/26/19 18:2350.0 43.0 1
Benzyl alcohol ND ug/L 11/27/19 20:12 100-51-611/26/19 18:2320.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 11/27/19 20:12 101-55-311/26/19 18:2310.0 1.6 1
Butylbenzylphthalate ND ug/L 11/27/19 20:12 85-68-711/26/19 18:2310.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 11/27/19 20:12 59-50-711/26/19 18:2320.0 2.8 1
4-Chloroaniline ND ug/L 11/27/19 20:12 106-47-811/26/19 18:2320.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 11/27/19 20:12 111-91-111/26/19 18:2310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 11/27/19 20:12 111-44-411/26/19 18:2310.0 1.8 1
2-Chloronaphthalene ND ug/L 11/27/19 20:12 91-58-711/26/19 18:2310.0 1.5 1
2-Chlorophenol ND ug/L 11/27/19 20:12 95-57-811/26/19 18:2310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 11/27/19 20:12 7005-72-311/26/19 18:2310.0 1.6 1
Chrysene ND ug/L 11/27/19 20:12 218-01-911/26/19 18:2310.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 11/27/19 20:12 53-70-311/26/19 18:2310.0 1.6 1
Dibenzofuran ND ug/L 11/27/19 20:12 132-64-911/26/19 18:2310.0 1.5 1
1,2-Dichlorobenzene ND ug/L 11/27/19 20:12 95-50-111/26/19 18:2310.0 1.3 1
1,3-Dichlorobenzene ND ug/L 11/27/19 20:12 541-73-111/26/19 18:2310.0 1.5 1
1,4-Dichlorobenzene ND ug/L 11/27/19 20:12 106-46-711/26/19 18:2310.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 11/27/19 20:12 91-94-111/26/19 18:2320.0 3.0 1
2,4-Dichlorophenol ND ug/L 11/27/19 20:12 120-83-211/26/19 18:2310.0 1.4 1
Diethylphthalate ND ug/L 11/27/19 20:12 84-66-211/26/19 18:2310.0 2.4 1
2,4-Dimethylphenol ND ug/L 11/27/19 20:12 105-67-911/26/19 18:2310.0 1.4 1
Dimethylphthalate ND ug/L 11/27/19 20:12 131-11-311/26/19 18:2310.0 1.6 1
Di-n-butylphthalate 3.2J ug/L 11/27/19 20:12 84-74-2 B,C911/26/19 18:2310.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 11/27/19 20:12 534-52-111/26/19 18:2320.0 15.2 1
2,4-Dinitrophenol ND ug/L 11/27/19 20:12 51-28-511/26/19 18:2350.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455130
ROW-603
Sample: IDW-GW Lab ID: 92455130001 Collected: 11/22/19 13:30 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 11/27/19 20:12 121-14-211/26/19 18:2310.0 1.2 1
2,6-Dinitrotoluene ND ug/L 11/27/19 20:12 606-20-211/26/19 18:2310.0 1.4 1
Di-n-octylphthalate ND ug/L 11/27/19 20:12 117-84-011/26/19 18:2310.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/27/19 20:12 117-81-711/26/19 18:236.0 2.1 1
Fluoranthene ND ug/L 11/27/19 20:12 206-44-011/26/19 18:2310.0 1.7 1
Fluorene ND ug/L 11/27/19 20:12 86-73-711/26/19 18:2310.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 11/27/19 20:12 87-68-311/26/19 18:2310.0 2.0 1
Hexachlorobenzene ND ug/L 11/27/19 20:12 118-74-111/26/19 18:2310.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 11/27/19 20:12 77-47-411/26/19 18:2310.0 1.7 1
Hexachloroethane ND ug/L 11/27/19 20:12 67-72-111/26/19 18:2310.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/27/19 20:12 193-39-511/26/19 18:2310.0 1.6 1
Isophorone ND ug/L 11/27/19 20:12 78-59-111/26/19 18:2310.0 1.6 1
1-Methylnaphthalene ND ug/L 11/27/19 20:12 90-12-011/26/19 18:2310.0 1.4 1
2-Methylnaphthalene ND ug/L 11/27/19 20:12 91-57-611/26/19 18:2310.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 11/27/19 20:12 95-48-711/26/19 18:2310.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/27/19 20:12 15831-10-411/26/19 18:2310.0 1.2 1
Naphthalene ND ug/L 11/27/19 20:12 91-20-311/26/19 18:2310.0 1.4 1
2-Nitroaniline ND ug/L 11/27/19 20:12 88-74-411/26/19 18:2320.0 4.2 1
3-Nitroaniline ND ug/L 11/27/19 20:12 99-09-211/26/19 18:2320.0 2.3 1
4-Nitroaniline ND ug/L 11/27/19 20:12 100-01-611/26/19 18:2320.0 2.2 1
Nitrobenzene ND ug/L 11/27/19 20:12 98-95-311/26/19 18:2310.0 2.1 1
2-Nitrophenol ND ug/L 11/27/19 20:12 88-75-511/26/19 18:2310.0 1.4 1
4-Nitrophenol ND ug/L 11/27/19 20:12 100-02-711/26/19 18:2350.0 3.5 1
N-Nitrosodimethylamine ND ug/L 11/27/19 20:12 62-75-911/26/19 18:2310.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 11/27/19 20:12 621-64-711/26/19 18:2310.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 11/27/19 20:12 86-30-611/26/19 18:2310.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/27/19 20:12 108-60-111/26/19 18:2310.0 2.8 1
Pentachlorophenol ND ug/L 11/27/19 20:12 87-86-511/26/19 18:2325.0 2.2 1
Phenanthrene ND ug/L 11/27/19 20:12 85-01-811/26/19 18:2310.0 1.7 1
Phenol ND ug/L 11/27/19 20:12 108-95-211/26/19 18:2310.0 0.92 1
Pyrene ND ug/L 11/27/19 20:12 129-00-011/26/19 18:2310.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 11/27/19 20:12 120-82-111/26/19 18:2310.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 11/27/19 20:12 95-95-411/26/19 18:2310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 11/27/19 20:12 88-06-211/26/19 18:2310.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)31 %11/27/19 20:12 4165-60-011/26/19 18:2313-130 1
2-Fluorobiphenyl (S)33 %11/27/19 20:12 321-60-811/26/19 18:2313-130 1
Terphenyl-d14 (S)130 %11/27/19 20:12 1718-51-011/26/19 18:2325-130 1
Phenol-d6 (S)36 %11/27/19 20:12 13127-88-311/26/19 18:2310-130 1
2-Fluorophenol (S)36 %11/27/19 20:12 367-12-411/26/19 18:2310-130 1
2,4,6-Tribromophenol (S)87 %11/27/19 20:12 118-79-611/26/19 18:2310-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone 16.3J ug/L 12/05/19 18:42 67-64-1 v125.0 6.2 1
Benzene ND ug/L 12/05/19 18:42 71-43-21.0 0.15 1
Bromobenzene ND ug/L 12/05/19 18:42 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455130
ROW-603
Sample: IDW-GW Lab ID: 92455130001 Collected: 11/22/19 13:30 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 12/05/19 18:42 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 12/05/19 18:42 75-27-41.0 0.26 1
Bromoform ND ug/L 12/05/19 18:42 75-25-21.0 0.62 1
Bromomethane ND ug/L 12/05/19 18:42 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 12/05/19 18:42 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 12/05/19 18:42 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 12/05/19 18:42 108-90-71.0 0.23 1
Chloroethane ND ug/L 12/05/19 18:42 75-00-31.0 0.49 1
Chloroform ND ug/L 12/05/19 18:42 67-66-35.0 2.3 1
Chloromethane ND ug/L 12/05/19 18:42 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 12/05/19 18:42 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 12/05/19 18:42 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 12/05/19 18:42 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 12/05/19 18:42 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 12/05/19 18:42 106-93-41.0 0.26 1
Dibromomethane ND ug/L 12/05/19 18:42 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 12/05/19 18:42 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 12/05/19 18:42 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 12/05/19 18:42 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 12/05/19 18:42 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 12/05/19 18:42 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 12/05/19 18:42 107-06-21.0 0.34 1
1,1-Dichloroethene 1.4 ug/L 12/05/19 18:42 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 12/05/19 18:42 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 12/05/19 18:42 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 12/05/19 18:42 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 12/05/19 18:42 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 12/05/19 18:42 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 12/05/19 18:42 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 12/05/19 18:42 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 12/05/19 18:42 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 12/05/19 18:42 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 12/05/19 18:42 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 12/05/19 18:42 87-68-31.0 0.44 1
2-Hexanone ND ug/L 12/05/19 18:42 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 12/05/19 18:42 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 12/05/19 18:42 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/05/19 18:42 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 12/05/19 18:42 1634-04-41.0 0.28 1
Naphthalene ND ug/L 12/05/19 18:42 91-20-31.0 0.35 1
Styrene ND ug/L 12/05/19 18:42 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 12/05/19 18:42 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 12/05/19 18:42 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 12/05/19 18:42 127-18-41.0 0.16 1
Toluene 0.97J ug/L 12/05/19 18:42 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 12/05/19 18:42 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92455130
ROW-603
Sample: IDW-GW Lab ID: 92455130001 Collected: 11/22/19 13:30 Received: 11/22/19 15:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 12/05/19 18:42 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 12/05/19 18:42 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 12/05/19 18:42 79-00-51.0 0.24 1
Trichloroethene ND ug/L 12/05/19 18:42 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 12/05/19 18:42 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 12/05/19 18:42 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 12/05/19 18:42 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 12/05/19 18:42 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 12/05/19 18:42 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 12/05/19 18:42 179601-23-12.0 0.41 1
o-Xylene ND ug/L 12/05/19 18:42 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)103 %12/05/19 18:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %12/05/19 18:42 17060-07-070-130 1
Toluene-d8 (S)99 %12/05/19 18:42 2037-26-570-130 1
Analytical Method: EPA 8260D Mod.8260D MSV SIM
1,4-Dioxane (p-Dioxane)2.5 ug/L 11/26/19 14:59 123-91-12.0 1.2 1
Surrogates
1,2-Dichloroethane-d4 (S)119 %11/26/19 14:59 17060-07-050-150 1
Toluene-d8 (S)95 %11/26/19 14:59 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
512546
EPA 7470A
EPA 7470A
7470 Mercury
Associated Lab Samples: 92455130001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2748079
Associated Lab Samples:92455130001
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 12/03/19 14:010.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2748080LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2748081MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454007002
2748082
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 89 75-12595 6 252.5ND 2.3 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511715
EPA 3010A
EPA 6010D
6010 MET
Associated Lab Samples: 92455130001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2744767
Associated Lab Samples:92455130001
Matrix: Water
AnalyzedMDL
Arsenic ug/L ND 10.0 12/02/19 04:234.7
Barium ug/L ND 5.0 12/02/19 04:231.0
Cadmium ug/L ND 1.0 12/02/19 04:230.40
Chromium ug/L ND 5.0 12/02/19 04:231.0
Lead ug/L ND 5.0 12/02/19 04:231.6
Selenium ug/L ND 10.0 12/02/19 04:234.7
Silver ug/L ND 5.0 12/02/19 04:232.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2744768LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 493500 99 80-120
Barium ug/L 496500 99 80-120
Cadmium ug/L 483500 97 80-120
Chromium ug/L 476500 95 80-120
Lead ug/L 480500 96 80-120
Selenium ug/L 490500 98 80-120
Silver ug/L 249250 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2744769MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92455130001
2744770
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 95 75-12595 1 20500ND481 477
Barium ug/L 500 94 75-12593 1 20500253725 719
Cadmium ug/L 500 96 75-12595 1 20500ND481 477
Chromium ug/L 500 95 75-12595 1 2050017.1 494 490
Lead ug/L 500 95 75-12594 1 20500ND473 469
Selenium ug/L 500 100 75-12599 1 20500ND500 496
Silver ug/L 250 98 75-12597 0 20250ND244 243
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
513060
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples: 92455130001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2750394
Associated Lab Samples:92455130001
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 12/05/19 17:140.34
1,1,1-Trichloroethane ug/L ND 1.0 12/05/19 17:140.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/05/19 17:140.22
1,1,2-Trichloroethane ug/L ND 1.0 12/05/19 17:140.24
1,1-Dichloroethane ug/L ND 1.0 12/05/19 17:140.27
1,1-Dichloroethene ug/L ND 1.0 12/05/19 17:140.24
1,1-Dichloropropene ug/L ND 1.0 12/05/19 17:140.21
1,2,3-Trichlorobenzene ug/L ND 1.0 12/05/19 17:140.34
1,2,3-Trichloropropane ug/L ND 1.0 12/05/19 17:140.35
1,2,4-Trichlorobenzene ug/L ND 1.0 12/05/19 17:140.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 12/05/19 17:140.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/05/19 17:140.26
1,2-Dichlorobenzene ug/L ND 1.0 12/05/19 17:140.29
1,2-Dichloroethane ug/L ND 1.0 12/05/19 17:140.34
1,2-Dichloropropane ug/L ND 1.0 12/05/19 17:140.19
1,3-Dichlorobenzene ug/L ND 1.0 12/05/19 17:140.22
1,3-Dichloropropane ug/L ND 1.0 12/05/19 17:140.16
1,4-Dichlorobenzene ug/L ND 1.0 12/05/19 17:140.26
2,2-Dichloropropane ug/L ND 1.0 12/05/19 17:140.27
2-Butanone (MEK)ug/L ND 5.0 12/05/19 17:143.3
2-Chlorotoluene ug/L ND 1.0 12/05/19 17:140.20
2-Hexanone ug/L ND 5.0 12/05/19 17:140.57
4-Chlorotoluene ug/L ND 1.0 12/05/19 17:140.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 12/05/19 17:144.5
Acetone ug/L ND 25.0 v112/05/19 17:146.2
Benzene ug/L ND 1.0 12/05/19 17:140.15
Bromobenzene ug/L ND 1.0 12/05/19 17:140.22
Bromochloromethane ug/L ND 1.0 12/05/19 17:140.34
Bromodichloromethane ug/L ND 1.0 12/05/19 17:140.26
Bromoform ug/L ND 1.0 12/05/19 17:140.62
Bromomethane ug/L ND 2.0 v212/05/19 17:140.62
Carbon tetrachloride ug/L ND 1.0 12/05/19 17:140.22
Chlorobenzene ug/L ND 1.0 12/05/19 17:140.23
Chloroethane ug/L ND 1.0 12/05/19 17:140.49
Chloroform ug/L ND 5.0 12/05/19 17:142.3
Chloromethane ug/L ND 1.0 v212/05/19 17:140.39
cis-1,2-Dichloroethene ug/L ND 1.0 12/05/19 17:140.29
cis-1,3-Dichloropropene ug/L ND 1.0 12/05/19 17:140.30
Dibromochloromethane ug/L ND 1.0 12/05/19 17:140.41
Dibromomethane ug/L ND 1.0 12/05/19 17:140.46
Dichlorodifluoromethane ug/L ND 1.0 12/05/19 17:140.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2750394
Associated Lab Samples:92455130001
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 12/05/19 17:140.22
Ethylbenzene ug/L ND 1.0 12/05/19 17:140.26
Hexachloro-1,3-butadiene ug/L ND 1.0 12/05/19 17:140.44
m&p-Xylene ug/L ND 2.0 12/05/19 17:140.41
Methyl-tert-butyl ether ug/L ND 1.0 12/05/19 17:140.28
Methylene Chloride ug/L ND 5.0 12/05/19 17:143.7
Naphthalene ug/L ND 1.0 12/05/19 17:140.35
o-Xylene ug/L ND 1.0 12/05/19 17:140.22
p-Isopropyltoluene ug/L ND 1.0 12/05/19 17:140.21
Styrene ug/L ND 1.0 12/05/19 17:140.27
Tetrachloroethene ug/L ND 1.0 12/05/19 17:140.16
Toluene ug/L ND 1.0 12/05/19 17:140.24
trans-1,2-Dichloroethene ug/L ND 1.0 12/05/19 17:140.25
trans-1,3-Dichloropropene ug/L ND 1.0 12/05/19 17:140.31
Trichloroethene ug/L ND 1.0 12/05/19 17:140.22
Trichlorofluoromethane ug/L ND 1.0 12/05/19 17:140.31
Vinyl acetate ug/L ND 2.0 12/05/19 17:141.4
Vinyl chloride ug/L ND 1.0 12/05/19 17:140.24
Xylene (Total)ug/L ND 1.0 12/05/19 17:140.63
1,2-Dichloroethane-d4 (S)%102 70-130 12/05/19 17:14
4-Bromofluorobenzene (S)%103 70-130 12/05/19 17:14
Toluene-d8 (S)%101 70-130 12/05/19 17:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2750395LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.550 107 70-130
1,1,1-Trichloroethane ug/L 50.450 101 70-130
1,1,2,2-Tetrachloroethane ug/L 49.650 99 70-130
1,1,2-Trichloroethane ug/L 47.850 96 70-130
1,1-Dichloroethane ug/L 50.550 101 70-130
1,1-Dichloroethene ug/L 44.750 89 70-130
1,1-Dichloropropene ug/L 54.350 109 70-130
1,2,3-Trichlorobenzene ug/L 53.650 107 70-130
1,2,3-Trichloropropane ug/L 48.150 96 70-130
1,2,4-Trichlorobenzene ug/L 54.450 109 70-130
1,2-Dibromo-3-chloropropane ug/L 53.050 106 70-130
1,2-Dibromoethane (EDB)ug/L 52.050 104 70-130
1,2-Dichlorobenzene ug/L 52.050 104 70-130
1,2-Dichloroethane ug/L 49.550 99 70-130
1,2-Dichloropropane ug/L 49.750 99 70-130
1,3-Dichlorobenzene ug/L 51.050 102 70-130
1,3-Dichloropropane ug/L 53.150 106 70-131
1,4-Dichlorobenzene ug/L 52.750 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2750395LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 53.150 106 69-130
2-Butanone (MEK)ug/L 107100 107 64-135
2-Chlorotoluene ug/L 48.950 98 70-130
2-Hexanone ug/L 105100 105 66-135
4-Chlorotoluene ug/L 49.850 100 70-130
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-130
Acetone ug/L 134 v1100134 61-157
Benzene ug/L 49.450 99 70-130
Bromobenzene ug/L 51.450 103 70-130
Bromochloromethane ug/L 46.950 94 70-130
Bromodichloromethane ug/L 49.250 98 70-130
Bromoform ug/L 52.950 106 70-130
Bromomethane ug/L 34.6 v35069 38-130
Carbon tetrachloride ug/L 50.850 102 70-130
Chlorobenzene ug/L 50.750 101 70-130
Chloroethane ug/L 43.650 87 37-142
Chloroform ug/L 50.650 101 70-130
Chloromethane ug/L 38.3 v35077 48-130
cis-1,2-Dichloroethene ug/L 49.550 99 70-130
cis-1,3-Dichloropropene ug/L 52.650 105 70-130
Dibromochloromethane ug/L 54.350 109 70-130
Dibromomethane ug/L 49.350 99 70-130
Dichlorodifluoromethane ug/L 44.650 89 53-134
Diisopropyl ether ug/L 53.750 107 70-135
Ethylbenzene ug/L 49.850 100 70-130
Hexachloro-1,3-butadiene ug/L 52.850 106 68-132
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 51.550 103 70-130
Methylene Chloride ug/L 51.650 103 67-132
Naphthalene ug/L 53.950 108 70-130
o-Xylene ug/L 49.450 99 70-131
p-Isopropyltoluene ug/L 53.350 107 70-130
Styrene ug/L 52.350 105 70-130
Tetrachloroethene ug/L 49.950 100 69-130
Toluene ug/L 48.350 97 70-130
trans-1,2-Dichloroethene ug/L 50.750 101 70-130
trans-1,3-Dichloropropene ug/L 51.750 103 70-130
Trichloroethene ug/L 48.750 97 70-130
Trichlorofluoromethane ug/L 43.450 87 63-130
Vinyl acetate ug/L 102100 102 55-143
Vinyl chloride ug/L 45.650 91 70-131
Xylene (Total)ug/L 150150 100 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2750397MATRIX SPIKE SAMPLE:
MSSpike
Result
92455130001
1,1,1,2-Tetrachloroethane ug/L 17.820 89 73-134ND
1,1,1-Trichloroethane ug/L 18.320 92 82-143ND
1,1,2,2-Tetrachloroethane ug/L 17.720 89 70-136ND
1,1,2-Trichloroethane ug/L 17.820 89 70-135ND
1,1-Dichloroethane ug/L 18.220 91 70-139ND
1,1-Dichloroethene ug/L 20.820 97 70-1541.4
1,1-Dichloropropene ug/L 19.120 95 70-149ND
1,2,3-Trichlorobenzene ug/L 16.420 82 70-135ND
1,2,3-Trichloropropane ug/L 17.820 89 71-137ND
1,2,4-Trichlorobenzene ug/L 17.420 87 73-140ND
1,2-Dibromo-3-chloropropane ug/L 17.120 86 65-134ND
1,2-Dibromoethane (EDB)ug/L 18.120 91 70-137ND
1,2-Dichlorobenzene ug/L 16.820 84 70-133ND
1,2-Dichloroethane ug/L 17.520 88 70-137ND
1,2-Dichloropropane ug/L 17.920 90 70-140ND
1,3-Dichlorobenzene ug/L 16.720 83 70-135ND
1,3-Dichloropropane ug/L 18.720 94 70-143ND
1,4-Dichlorobenzene ug/L 16.820 84 70-133ND
2,2-Dichloropropane ug/L 19.320 96 61-148ND
2-Butanone (MEK)ug/L 35.740 89 60-139ND
2-Chlorotoluene ug/L 17.320 87 70-144ND
2-Hexanone ug/L 35.940 90 65-138ND
4-Chlorotoluene ug/L 17.020 85 70-137ND
4-Methyl-2-pentanone (MIBK)ug/L 46.340 116 65-135ND
Acetone ug/L 51.740 89 60-14816.3J
Benzene ug/L 18.320 92 70-151ND
Bromobenzene ug/L 17.520 87 70-136ND
Bromochloromethane ug/L 18.620 93 70-141ND
Bromodichloromethane ug/L 18.820 94 70-138ND
Bromoform ug/L 17.920 89 63-130ND
Bromomethane ug/L 21.220 106 15-152ND
Carbon tetrachloride ug/L 19.320 97 70-143ND
Chlorobenzene ug/L 17.820 89 70-138ND
Chloroethane ug/L 18.520 93 52-163ND
Chloroform ug/L 19.020 89 70-139ND
Chloromethane ug/L 14.020 69 41-139ND
cis-1,2-Dichloroethene ug/L 17.920 90 70-141ND
cis-1,3-Dichloropropene ug/L 18.920 94 70-137ND
Dibromochloromethane ug/L 18.420 92 70-134ND
Dibromomethane ug/L 18.920 95 70-138ND
Dichlorodifluoromethane ug/L 16.920 84 47-155ND
Diisopropyl ether ug/L 18.220 91 63-144ND
Ethylbenzene ug/L 18.320 91 66-153ND
Hexachloro-1,3-butadiene ug/L 17.120 86 65-149ND
m&p-Xylene ug/L 36.240 90 69-152ND
Methyl-tert-butyl ether ug/L 18.620 93 54-156ND
Methylene Chloride ug/L 18.020 90 42-159ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2750397MATRIX SPIKE SAMPLE:
MSSpike
Result
92455130001
Naphthalene ug/L 15.320 77 61-148ND
o-Xylene ug/L 17.520 88 70-148ND
p-Isopropyltoluene ug/L 17.920 90 70-146ND
Styrene ug/L 17.620 88 70-135ND
Tetrachloroethene ug/L 17.520 87 59-143ND
Toluene ug/L 19.120 91 59-1480.97J
trans-1,2-Dichloroethene ug/L 18.220 91 70-146ND
trans-1,3-Dichloropropene ug/L 17.920 90 70-135ND
Trichloroethene ug/L 18.020 90 70-147ND
Trichlorofluoromethane ug/L 18.620 93 70-148ND
Vinyl acetate ug/L 34.940 87 49-151ND
Vinyl chloride ug/L 19.320 96 70-156ND
Xylene (Total)ug/L 53.760 89 63-158ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92455089018
2750396SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND H130ND
1,1,1-Trichloroethane ug/L ND H130ND
1,1,2,2-Tetrachloroethane ug/L ND H130ND
1,1,2-Trichloroethane ug/L ND H130ND
1,1-Dichloroethane ug/L ND H130ND
1,1-Dichloroethene ug/L ND H130ND
1,1-Dichloropropene ug/L ND H1
1,2,3-Trichlorobenzene ug/L 1.2 H1
1,2,3-Trichloropropane ug/L ND H130ND
1,2,4-Trichlorobenzene ug/L 0.73J H1
1,2-Dibromo-3-chloropropane ug/L ND H130ND
1,2-Dibromoethane (EDB)ug/L ND H130ND
1,2-Dichlorobenzene ug/L 0.33J H130ND
1,2-Dichloroethane ug/L ND H130ND
1,2-Dichloropropane ug/L ND H130ND
1,3-Dichlorobenzene ug/L 0.33J H1
1,3-Dichloropropane ug/L ND H1
1,4-Dichlorobenzene ug/L 0.38J H130ND
2,2-Dichloropropane ug/L ND H1
2-Butanone (MEK)ug/L ND H130ND
2-Chlorotoluene ug/L ND H1
2-Hexanone ug/L ND H130ND
4-Chlorotoluene ug/L ND H1
4-Methyl-2-pentanone (MIBK)ug/L ND H130ND
Acetone ug/L ND H130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92455089018
2750396SAMPLE DUPLICATE:
Benzene ug/L ND H130ND
Bromobenzene ug/L ND H1
Bromochloromethane ug/L ND H130ND
Bromodichloromethane ug/L ND H130ND
Bromoform ug/L ND H130ND
Bromomethane ug/L ND H130ND
Carbon tetrachloride ug/L ND H130ND
Chlorobenzene ug/L ND H130ND
Chloroethane ug/L ND H130ND
Chloroform ug/L ND H130ND
Chloromethane ug/L ND H130ND
cis-1,2-Dichloroethene ug/L ND H130ND
cis-1,3-Dichloropropene ug/L ND H130ND
Dibromochloromethane ug/L ND H130ND
Dibromomethane ug/L ND H130ND
Dichlorodifluoromethane ug/L ND H1
Diisopropyl ether ug/L ND H1
Ethylbenzene ug/L ND H130ND
Hexachloro-1,3-butadiene ug/L 1.3 H1
m&p-Xylene ug/L ND H130
Methyl-tert-butyl ether ug/L ND H1
Methylene Chloride ug/L ND H130ND
Naphthalene ug/L 1.3 H1
o-Xylene ug/L ND H130
p-Isopropyltoluene ug/L 0.51J H1
Styrene ug/L ND H130ND
Tetrachloroethene ug/L 5.5 D6,H142303.6
Toluene ug/L ND H130ND
trans-1,2-Dichloroethene ug/L ND H130ND
trans-1,3-Dichloropropene ug/L ND H130ND
Trichloroethene ug/L ND H130ND
Trichlorofluoromethane ug/L ND H130ND
Vinyl acetate ug/L ND H130ND
Vinyl chloride ug/L ND H130ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%93103
4-Bromofluorobenzene (S)%98101
Toluene-d8 (S)%100100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511851
EPA 8260D Mod.
EPA 8260D Mod.
8260D MSV SIM
Associated Lab Samples: 92455130001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2745156
Associated Lab Samples:92455130001
Matrix: Water
AnalyzedMDL
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 11/26/19 13:001.2
1,2-Dichloroethane-d4 (S)%99 50-150 11/26/19 13:00
Toluene-d8 (S)%91 50-150 11/26/19 13:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745157LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 19.120 95 70-130
1,2-Dichloroethane-d4 (S)%116 50-150
Toluene-d8 (S)%95 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745381MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92455128002
2745382
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane) ug/L 20 94 50-15094 0 3020ND18.9 18.9
1,2-Dichloroethane-d4 (S) %119 50-150119 30
Toluene-d8 (S)%98 50-15099 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
511822
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Associated Lab Samples: 92455130001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2745012
Associated Lab Samples:92455130001
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 11/27/19 17:131.5
1,2-Dichlorobenzene ug/L ND 10.0 11/27/19 17:131.3
1,3-Dichlorobenzene ug/L ND 10.0 11/27/19 17:131.5
1,4-Dichlorobenzene ug/L ND 10.0 11/27/19 17:132.1
1-Methylnaphthalene ug/L ND 10.0 11/27/19 17:131.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 11/27/19 17:132.8
2,4,5-Trichlorophenol ug/L ND 10.0 11/27/19 17:131.4
2,4,6-Trichlorophenol ug/L ND 10.0 11/27/19 17:131.5
2,4-Dichlorophenol ug/L ND 10.0 11/27/19 17:131.4
2,4-Dimethylphenol ug/L ND 10.0 11/27/19 17:131.4
2,4-Dinitrophenol ug/L ND 50.0 11/27/19 17:1340.5
2,4-Dinitrotoluene ug/L ND 10.0 11/27/19 17:131.2
2,6-Dinitrotoluene ug/L ND 10.0 11/27/19 17:131.4
2-Chloronaphthalene ug/L ND 10.0 11/27/19 17:131.5
2-Chlorophenol ug/L ND 10.0 11/27/19 17:131.2
2-Methylnaphthalene ug/L ND 10.0 11/27/19 17:131.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 11/27/19 17:131.2
2-Nitroaniline ug/L ND 20.0 11/27/19 17:134.2
2-Nitrophenol ug/L ND 10.0 11/27/19 17:131.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 11/27/19 17:131.2
3,3'-Dichlorobenzidine ug/L ND 20.0 11/27/19 17:133.0
3-Nitroaniline ug/L ND 20.0 11/27/19 17:132.3
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/27/19 17:1315.2
4-Bromophenylphenyl ether ug/L ND 10.0 11/27/19 17:131.6
4-Chloro-3-methylphenol ug/L ND 20.0 11/27/19 17:132.8
4-Chloroaniline ug/L ND 20.0 11/27/19 17:132.8
4-Chlorophenylphenyl ether ug/L ND 10.0 11/27/19 17:131.6
4-Nitroaniline ug/L ND 20.0 11/27/19 17:132.2
4-Nitrophenol ug/L ND 50.0 11/27/19 17:133.5
Acenaphthene ug/L ND 10.0 11/27/19 17:131.6
Acenaphthylene ug/L ND 10.0 11/27/19 17:131.6
Aniline ug/L ND 10.0 11/27/19 17:131.9
Anthracene ug/L ND 10.0 11/27/19 17:131.7
Benzo(a)anthracene ug/L ND 10.0 11/27/19 17:131.8
Benzo(a)pyrene ug/L ND 10.0 11/27/19 17:132.1
Benzo(b)fluoranthene ug/L ND 10.0 11/27/19 17:131.9
Benzo(g,h,i)perylene ug/L ND 10.0 11/27/19 17:131.4
Benzo(k)fluoranthene ug/L ND 10.0 11/27/19 17:131.9
Benzoic Acid ug/L ND 50.0 11/27/19 17:1343.0
Benzyl alcohol ug/L ND 20.0 11/27/19 17:132.6
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/27/19 17:131.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2745012
Associated Lab Samples:92455130001
Matrix: Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 11/27/19 17:131.8
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/27/19 17:132.1
Butylbenzylphthalate ug/L ND 10.0 11/27/19 17:131.6
Chrysene ug/L ND 10.0 11/27/19 17:131.7
Di-n-butylphthalate ug/L 2.9J 10.0 11/27/19 17:131.8
Di-n-octylphthalate ug/L ND 10.0 11/27/19 17:131.8
Dibenz(a,h)anthracene ug/L ND 10.0 11/27/19 17:131.6
Dibenzofuran ug/L ND 10.0 11/27/19 17:131.5
Diethylphthalate ug/L ND 10.0 11/27/19 17:132.4
Dimethylphthalate ug/L ND 10.0 11/27/19 17:131.6
Fluoranthene ug/L ND 10.0 11/27/19 17:131.7
Fluorene ug/L ND 10.0 11/27/19 17:131.6
Hexachloro-1,3-butadiene ug/L ND 10.0 11/27/19 17:132.0
Hexachlorobenzene ug/L ND 10.0 11/27/19 17:131.7
Hexachlorocyclopentadiene ug/L ND 10.0 11/27/19 17:131.7
Hexachloroethane ug/L ND 10.0 11/27/19 17:132.0
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/27/19 17:131.6
Isophorone ug/L ND 10.0 11/27/19 17:131.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 11/27/19 17:132.2
N-Nitrosodimethylamine ug/L ND 10.0 11/27/19 17:131.2
N-Nitrosodiphenylamine ug/L ND 10.0 11/27/19 17:131.7
Naphthalene ug/L ND 10.0 11/27/19 17:131.4
Nitrobenzene ug/L ND 10.0 11/27/19 17:132.1
Pentachlorophenol ug/L ND 25.0 11/27/19 17:132.2
Phenanthrene ug/L ND 10.0 11/27/19 17:131.7
Phenol ug/L ND 10.0 11/27/19 17:130.92
Pyrene ug/L ND 10.0 11/27/19 17:132.1
2,4,6-Tribromophenol (S)%86 10-137 11/27/19 17:13
2-Fluorobiphenyl (S)%79 13-130 11/27/19 17:13
2-Fluorophenol (S)%80 10-130 11/27/19 17:13
Nitrobenzene-d5 (S)%74 13-130 11/27/19 17:13
Phenol-d6 (S)%84 10-130 11/27/19 17:13
Terphenyl-d14 (S)%84 25-130 11/27/19 17:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745013LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 43.650 87 30-130
1,2-Dichlorobenzene ug/L 43.650 87 30-130
1,3-Dichlorobenzene ug/L 43.050 86 20-130
1,4-Dichlorobenzene ug/L 43.450 87 30-130
1-Methylnaphthalene ug/L 45.850 92 30-130
2,2'-Oxybis(1-chloropropane)ug/L 39.850 80 20-130
2,4,5-Trichlorophenol ug/L 45.250 90 40-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745013LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 46.950 94 40-130
2,4-Dichlorophenol ug/L 46.450 93 31-130
2,4-Dimethylphenol ug/L 46.250 92 30-130
2,4-Dinitrophenol ug/L 226250 90 30-130
2,4-Dinitrotoluene ug/L 50.350 101 49-130
2,6-Dinitrotoluene ug/L 49.750 99 50-130
2-Chloronaphthalene ug/L 45.250 90 30-130
2-Chlorophenol ug/L 45.050 90 30-130
2-Methylnaphthalene ug/L 45.050 90 30-130
2-Methylphenol(o-Cresol)ug/L 43.050 86 30-130
2-Nitroaniline ug/L 95.4100 95 40-130
2-Nitrophenol ug/L 47.550 95 20-130
3&4-Methylphenol(m&p Cresol)ug/L 43.550 87 20-130
3,3'-Dichlorobenzidine ug/L 83.6100 84 10-150
3-Nitroaniline ug/L 98.6100 99 40-130
4,6-Dinitro-2-methylphenol ug/L 99.5100 99 40-130
4-Bromophenylphenyl ether ug/L 44.250 88 30-130
4-Chloro-3-methylphenol ug/L 92.9100 93 30-130
4-Chloroaniline ug/L 90.3100 90 20-130
4-Chlorophenylphenyl ether ug/L 43.950 88 20-130
4-Nitroaniline ug/L 91.6100 92 40-130
4-Nitrophenol ug/L 243250 97 10-130
Acenaphthene ug/L 46.850 94 30-130
Acenaphthylene ug/L 50.150 100 30-130
Aniline ug/L 40.950 82 20-130
Anthracene ug/L 50.350 101 50-130
Benzo(a)anthracene ug/L 47.950 96 50-130
Benzo(a)pyrene ug/L 51.750 103 50-130
Benzo(b)fluoranthene ug/L 50.350 101 50-130
Benzo(g,h,i)perylene ug/L 50.150 100 50-130
Benzo(k)fluoranthene ug/L 50.250 100 50-130
Benzoic Acid ug/L 202250 81 10-130
Benzyl alcohol ug/L 88.7100 89 20-130
bis(2-Chloroethoxy)methane ug/L 42.150 84 30-130
bis(2-Chloroethyl) ether ug/L 42.950 86 30-130
bis(2-Ethylhexyl)phthalate ug/L 45.950 92 50-130
Butylbenzylphthalate ug/L 46.550 93 50-150
Chrysene ug/L 45.950 92 50-130
Di-n-butylphthalate ug/L 49.350 99 50-130
Di-n-octylphthalate ug/L 48.650 97 50-130
Dibenz(a,h)anthracene ug/L 50.950 102 40-130
Dibenzofuran ug/L 45.250 90 40-130
Diethylphthalate ug/L 45.450 91 40-130
Dimethylphthalate ug/L 44.650 89 40-130
Fluoranthene ug/L 49.050 98 30-130
Fluorene ug/L 47.250 94 20-130
Hexachloro-1,3-butadiene ug/L 43.250 86 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2745013LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 46.650 93 30-130
Hexachlorocyclopentadiene ug/L 50.150 100 10-150
Hexachloroethane ug/L 43.550 87 10-130
Indeno(1,2,3-cd)pyrene ug/L 50.550 101 40-130
Isophorone ug/L 43.650 87 30-130
N-Nitroso-di-n-propylamine ug/L 43.650 87 30-130
N-Nitrosodimethylamine ug/L 41.550 83 10-130
N-Nitrosodiphenylamine ug/L 46.550 93 30-130
Naphthalene ug/L 45.850 92 20-130
Nitrobenzene ug/L 43.850 88 20-130
Pentachlorophenol ug/L 109100 109 10-140
Phenanthrene ug/L 47.350 95 50-130
Phenol ug/L 46.350 93 10-130
Pyrene ug/L 47.150 94 50-130
2,4,6-Tribromophenol (S)%109 10-137
2-Fluorobiphenyl (S)%83 13-130
2-Fluorophenol (S)%89 10-130
Nitrobenzene-d5 (S)%80 13-130
Phenol-d6 (S)%94 10-130
Terphenyl-d14 (S)%85 25-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745014MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454931001
2745015
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 52 30-13045 14 3050ND26.0 22.5
1,2-Dichlorobenzene ug/L 50 52 30-13045 14 3050ND26.2 22.7
1,3-Dichlorobenzene ug/L 50 51 20-13044 14 3050ND25.5 22.2
1,4-Dichlorobenzene ug/L 50 52 30-13045 14 3050ND25.9 22.6
1-Methylnaphthalene ug/L 50 54 30-13048 11 3050ND27.0 24.1
2,2'-Oxybis(1-
chloropropane)ug/L 50 48 20-13042 13 3050ND24.2 21.1
2,4,5-Trichlorophenol ug/L 50 52 40-13046 11 3050ND26.0 23.2
2,4,6-Trichlorophenol ug/L 50 54 40-13048 12 3050ND27.2 24.0
2,4-Dichlorophenol ug/L 50 53 31-13047 12 3050ND26.6 23.6
2,4-Dimethylphenol ug/L 50 54 30-13047 15 3050ND27.2 23.4
2,4-Dinitrophenol ug/L 250 57 30-13058 1 30250ND142 144
2,4-Dinitrotoluene ug/L 50 67 49-13065 3 3050ND33.6 32.6
2,6-Dinitrotoluene ug/L 50 61 50-13056 7 3050ND30.3 28.2
2-Chloronaphthalene ug/L 50 54 30-13049 11 3050ND27.1 24.3
2-Chlorophenol ug/L 50 53 30-13047 13 3050ND26.4 23.3
2-Methylnaphthalene ug/L 50 53 30-13048 10 3050ND26.3 23.9
2-Methylphenol(o-Cresol) ug/L 50 45 30-13040 11 3050ND22.7 20.2
2-Nitroaniline ug/L 100 59 40-13054 8 30100ND58.6 53.8
2-Nitrophenol ug/L 50 58 20-13050 14 3050ND28.9 25.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745014MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454931001
2745015
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/L 50 42 20-13039 8 3050ND21.0 19.4
3,3'-Dichlorobenzidine ug/L 100 64 10-15060 6 30100ND63.5 59.7
3-Nitroaniline ug/L 100 60 40-13056 7 30100ND60.0 55.9
4,6-Dinitro-2-methylphenol ug/L 100 69 40-13068 2 30100ND69.3 67.8
4-Bromophenylphenyl ether ug/L 50 55 30-13051 8 3050ND27.7 25.7
4-Chloro-3-methylphenol ug/L 100 52 30-13047 9 30100ND51.8 47.4
4-Chloroaniline ug/L 100 55 20-13049 12 30100ND55.0 48.8
4-Chlorophenylphenyl ether ug/L 50 54 20-13049 10 3050ND26.9 24.4
4-Nitroaniline ug/L 100 65 40-13064 1 30100ND64.9 64.3
4-Nitrophenol ug/L 250 35 10-13040 12 30250ND88.0 99.0
Acenaphthene ug/L 50 57 30-13051 10 3050ND28.5 25.7
Acenaphthylene ug/L 50 61 30-13055 11 3050ND30.5 27.4
Aniline ug/L 50 43 20-13036 18 3050ND21.4 17.9
Anthracene ug/L 50 69 50-13066 4 3050ND34.4 32.9
Benzo(a)anthracene ug/L 50 73 50-13070 4 3050ND36.5 35.2
Benzo(a)pyrene ug/L 50 78 50-13076 3 3050ND39.0 37.8
Benzo(b)fluoranthene ug/L 50 74 50-13074 0 3050ND36.9 36.8
Benzo(g,h,i)perylene ug/L 50 80 50-13077 4 3050ND39.9 38.4
Benzo(k)fluoranthene ug/L 50 76 50-13074 3 3050ND38.0 36.8
Benzoic Acid ug/L 250 25 10-13026 3 30250ND63.3 65.1
Benzyl alcohol ug/L 100 49 20-13045 9 30100ND48.9 44.8
bis(2-
Chloroethoxy)methane ug/L 50 51 30-13045 12 3050ND25.4 22.5
bis(2-Chloroethyl) ether ug/L 50 55 30-13048 14 3050ND27.6 24.0
bis(2-Ethylhexyl)phthalate ug/L 50 66 50-13064 2 3050ND32.8 32.1
Butylbenzylphthalate ug/L 50 66 50-15064 2 3050ND32.9 32.2
Chrysene ug/L 50 71 50-13068 5 3050ND35.7 34.1
Di-n-butylphthalate ug/L 50 67 50-13065 3 3050ND33.6 32.7
Di-n-octylphthalate ug/L 50 68 50-13067 2 3050ND34.1 33.3
Dibenz(a,h)anthracene ug/L 50 80 40-13075 6 3050ND39.9 37.6
Dibenzofuran ug/L 50 56 40-13050 12 3050ND28.2 25.1
Diethylphthalate ug/L 50 62 40-13061 1 3050ND31.0 30.6
Dimethylphthalate ug/L 50 57 40-13054 5 3050ND28.4 27.0
Fluoranthene ug/L 50 74 30-13072 3 3050ND37.1 36.1
Fluorene ug/L 50 59 20-13053 11 3050ND29.7 26.6
Hexachloro-1,3-butadiene ug/L 50 49 10-13042 14 3050ND24.4 21.2
Hexachlorobenzene ug/L 50 61 30-13057 6 3050ND30.3 28.6
Hexachlorocyclopentadiene ug/L 50 54 10-15047 13 3050ND26.8 23.4
Hexachloroethane ug/L 50 50 10-13043 14 3050ND24.9 21.6
Indeno(1,2,3-cd)pyrene ug/L 50 79 40-13075 6 3050ND39.7 37.5
Isophorone ug/L 50 53 30-13048 10 3050ND26.4 23.9
N-Nitroso-di-n-propylamine ug/L 50 52 30-13046 11 3050ND26.0 23.2
N-Nitrosodimethylamine ug/L 50 43 10-13040 7 3050ND21.4 20.0
N-Nitrosodiphenylamine ug/L 50 59 30-13056 6 3050ND29.6 27.9
Naphthalene ug/L 50 56 20-13049 12 3050ND27.9 24.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92455130
ROW-603
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2745014MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92454931001
2745015
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrobenzene ug/L 50 57 20-13051 13 3050ND28.7 25.3
Pentachlorophenol ug/L 100 72 10-14070 4 30100ND72.2 69.6
Phenanthrene ug/L 50 65 50-13063 4 3050ND32.7 31.4
Phenol ug/L 50 30 10-13029 4 3050ND15.2 14.6
Pyrene ug/L 50 71 50-13070 2 3050ND35.5 34.8
2,4,6-Tribromophenol (S) %78 10-13771
2-Fluorobiphenyl (S)%59 13-13051
2-Fluorophenol (S)%47 10-13041
Nitrobenzene-d5 (S)%60 13-13051
Phenol-d6 (S)%34 10-13032
Terphenyl-d14 (S)%70 25-13064
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92455130
ROW-603
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Analysis conducted outside the EPA method holding time.H1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92455130
ROW-603
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92455130001 511715 511722IDW-GW EPA 3010A EPA 6010D
92455130001 512546 512624IDW-GW EPA 7470A EPA 7470A
92455130001 511822 512197IDW-GW EPA 3510C EPA 8270E
92455130001 513060IDW-GW EPA 8260D
92455130001 511851IDW-GW EPA 8260D Mod.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/10/2019 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 28
Page 26 of 28
Page 27 of 28
Page 28 of 28

Appendix E

Groundwater Forms
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/ROW.603NCDOT Pennston PropertyGreensboro, nc11/22/1930.0023.30CDGJS27-29.5Cloudy 37F 5mph NW windTurbididtynot <10 NTU. Wellgoingdry.Totalpurge time 1hr 35 min Sheet 1 of 209:5510:0010:0510:1010:1510:2010:2510:3010:3510:4010:4510:5023.8924.2224.7025.2125.8326.0326.5027.0027.2027.4027.6727.89750 mL1.5 L2.25 L3mL3.75 L4.5 L5.25 L6L6.75 L7.5 L8.25 L9L~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m6.516.446.696.546.506.466.676.616.616.775.054.9515.515.815.615.715.915.915.915.514.814.414.715.3609.6613.0617.0619.0621.0625.0628.0632.0634.0610.3610.56.706.666.676.686.696.716.736.736.746.696.646.63214.9210.4209.9209.6209.7210.0209.8212.2219.5219.0214.2209.854.5391.9530.7225.3723.5020.5928.5434.4762.92109.30218.20176.20N/AYSI Pro, MicroTPI turbidimeterFedExVOCs by8260, 1,4-Dioxane by8260 SIM, RCRA metals by6010,SVOCs by8270BladderPVC2-inch11:30Pace AnalyticalMW-11.09gal1530Bondedpolyethylene bgs618.3
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/ROW.603NCDOT Pennston PropertyGreensboro, nc11/22/1930.0023.30CDGJS27-29.5Cloudy 37F 5mph NW wind Turbididty not <10 NTU. Wellgoingdry.Totalpurge time 1hr 35 min Sheet 2 of 210:5511:0011:0511:1011:1511:2011:2511:3028.2028.3928.6528.7228.9929.0729.1929.279.75 L10.5 L11.25 L12 L12.75 L13.5 L14.25 L15 L~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m4.875.335.025.034.965.604.273.7515.515.515.315.215.616.016.216.3620.0627.0644.0637.0632.0628.0623.0617.06.646.666.676.666.646.626.626.61207.7208.3208.5208.9210.2210.7212.3212.4167.20117.6052.7736.8919.2827.7639.5959.92YSI Pro, MicroTPI turbididmeterFedExVOCs by8260, 1,4-Dioxane by8260 SIM, RCRA metals by6010,SVOCs by8270BladderPVC2-inch11:30Pace AnalyticalMW-11.09gal1530Bondedpolyethylene bgs
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/ROW.603NCDOT Pennston PropertyGreensboro NC11/22/1932.0029.23CDGJS~31Cloudy 42F 3mph NW windUnable to measure DTW below 31.6 ft, WLMseatingon topofpump. Sheet 1 of 208:0008:0508:1008:1508:2008:2508:3008:3508:4008:4508:5008:5530.9831.0631.1931.3031.4831.60500 mL1L1.5 L2.0 L2.5 L3.0 L3.5 L4.0 L4.5 L5.0 L5.5 L6.0 L~100 mL/m~100 mL/m~100 mL/m~100 mL/m~100 mL/m~100 mL/m~100 mL/m~100 mL/m~100 mL/m~100 mL/m~100 mL/m~100 mL/m11.2510.7110.3610.2010.1710.1410.0310.0610.2110.2610.3510.5213.013.213.713.713.713.813.913.713.613.413.513.6136.0122.9120.3121.1119.9116.9115.1114.4115.7115.1114.67.236.556.436.406.386.366.366.366.366.396.386.43194.8197.0185.7176.1160.5136.0102.474.585.4118.7143.1158.6250.00217.30206.20135.1059.5431.0018.9918.8132.6359.1133.5418.42N/AYSI Pro, MicroTPI turbidimeterFedExVOCs by8260, 1,4-Dioxane by8260 SIM, RCRA metals by6010,SVOCs by8270BladderPVC2-inch09:05Pace AnalyticalMW-20.45gal1732Bonded polyethylene bgs115.7
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/ROW.603NCDOT Pennston PropertyGreensboro, NC11/22/1932.0029.23CDGJS~31Cloudy 42F 3mph NW wind Turbididty not <10 NTU. Wellgoingdry.WLMseatingon topofpump. Sheet 2 of 209:0009:056.5 L7.0 L~100 mL/m~100 mL/m10.7410.6113.613.6114.0112.56.446.47165.7174.715.0510.86N/AYSI Pro, MicroTPI turbididmeterFedExVOCs by8260, 1,4-Dioxane by8260 SIM, RCRA metals by6010,SVOCs by8270BladderPVC2-inch09:05Pace AnalyticalMW-20.45gal1732Bondedpolyethylene bgs
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/ROW.603NCDOT Pennston PropertyGreensboro,nc11/22/1931.0029.05CDGJS30Cloudy 47F 2 mph NW wind12:3012:3512:4012:4512:5012:5529.1729.1829.1929.1929.2029.20750 mL1.5 L2.25 L3.0 L3.75 L4.5 L~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m~150 mL/m5.134.714.864.784.364.3216.616.316.316.417.217.2166.5156.2159.0163.8163.4163.37.056.806.776.786.776.77-13.5-13.317.836.654.359.2428.00156.3066.6730.3323.135.85N/AYSI Pro, MicroTPI turbidimeterFedExVOCs by8260, 1,4-Dioxane by8260 SIM, RCRA metals by6010,SVOCs by8270PeristalticPVC2-inch12:55Pace AnalyticalMW-40.291631Polyethylene bgs

Appendix F

Non-Hazardous Waste Disposal Manifests