WS-5133_17513_CA_MRP_20150831

GROUNDWATER MONITORING REPORT
C&H MARKET,INCIDENT #17513
730 NC HIGHWAY 87
ELON,ALAMANCE CO.,NC 27244
S&ME PROJECT # 4305-15-045
August 31,2015
Prepared For:
NorthCarolina Department ofEnvironmental Quality
Division ofWaste Management
Underground Storage TankSection
1637Mail Service Center
Raleigh,NorthCarolina 27699
Prepared by:
S&ME,Inc.
8646West Market Street,Suite 105
Greensboro,NC 27409
__________________________________________________________
Scott Young Wayne H.Watterson,P.E.
Project Professional Senior Engineer
S&MEis licensed to practice geology/engineering in NorthCarolina.Geology License Certification #C-145 and
Engineering License Certification #F-0176.
Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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TABLE OF CONTENTS
1. STATE-LEAD MONITORING REPORT.............................................................. 1
2. EXECUTIVE SUMMARY ....................................................................................... 2
3. SCOPE OF SERVICES ............................................................................................ 3
3.1 Contract Information ........................................................................................... 3
3.2 Approved Scope of Services ............................................................................... 3
4. SITE HISTORY AND CHARACTERIZATION ................................................... 4
4.1 UST Owner and Operator Information. .............................................................. 5
4.2 UST Information ................................................................................................. 5
4.3 Description of the UST Release .......................................................................... 5
4.4 Site Characteristics.............................................................................................. 5
4.5 Owners and Occupants of Adjoining/Nearby Properties and Land Use............. 6
4.6 Receptors/Potential Receptor Information .......................................................... 6
5. CURRENT SITE ASSESSMENT INFORMATION ............................................. 7
5.1 Current Liquid Levels ......................................................................................... 7
5.2 Groundwater Monitoring Events ........................................................................ 7
5.3 Summary of Groundwater Assessment Information........................................... 7
5.4 Regional and Site Geology and Hydrogeology .................................................. 8
5.4.1 Soil and Bedrock ................................................................................... 8
5.4.2 Hydrogeology ........................................................................................ 8
5.5 Evaluation of Groundwater Assessment Information ......................................... 8
5.5.1 Current Extent and Severity of Contamination ..................................... 8
5.5.2 Cleanup Levels Achieved ...................................................................... 9
6. CONCLUSIONS AND RECOMMENDATIONS ................................................ 10

Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

ii
TABLE OF CONTENTS (continued)

FIGURES

1 Vicinity Map
2 Site Map
3 Groundwater Contour Map
4 Water Supply Well Location Map
5 Groundwater Constituent Map

TABLES

1 UST System Information
2 Monitoring Well Construction and Liquid Level Data
3 Water Supply Well Information
4 Summary of Groundwater Analytical Data

APPENDICES

I Field Notes
II Laboratory Reports
III Photographs

Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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2. EXECUTIVE SUMMARY
Summarize the most pertinent information for the monitoring period presented in this report:

1. Maximum concentrations of groundwater contaminants exceeding 2L Standards:

Contaminant
2L
Standard
(µg/L)
Concentration
(µg/L) Well ID Date
Benzene 1 649 MW-1R 4/29/15
Ethylbenzene 20 1,150 MW-1R 4/29/15
Naphthalene 6 287 MW-1R 4/29/15
n-Propylbenzene 70 193 MW-1R 4/29/15
Toluene 600 5,510 MW-1R 4/29/15
1,2,4-Trimethylbenzene 400 1,460 MW-1R 4/29/15
1,3,5-Trimethylbenzene 400 444 MW-1R 4/29/15
Total Xylenes 500 6,590 MW-1R 4/29/15

2. Current extents of dissolved groundwater contamination compared to the historical
extents:
Compound concentrations detected in the sample collected from monitoring well MW-1R
increased approximately 67% as compared to the sample collected in July 2011.
Detected compound concentrations in the sample collected from monitoring well MW-3
decreased approximately 67%. No compounds were detected above the laboratory
method reporting limits in the samples collected from monitoring wells MW-4, MW-5,
and TW-1.

3. Potential receptors and risk of impact:

Distance from
source (ft)
Municipal
Water
Available
Active
Drinking
Water Well
Inactive
Drinking
Water Well
Surface
Water Body
0 – 500 Yes

5

2 No
500 – 1,000 Yes 6 0 No

4. Feasible pathway to closing the UST Incident.
a) Source area treatment to reduce groundwater contamination concentrations to below
2L Standards.

Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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3. SCOPE OF SERVICES
3.1 Contract Information
The scope of services for this report was performed in general accordance with S&ME’s
proposal number 43-1500107, dated January 27, 2015, and 43-1500228, dated February 20,
2015. The scope of services was authorized by the North Carolina Department of Environment
& Natural Resources (NCDENR’s) Task Authorizations 17513-01, dated February 5, 2015, and
17513-02, dated February 19, 2015, and within contract number N14005i.
3.2 Approved Scope of Services
S&ME’s approved Scope of Services for these Task Authorizations included collecting
groundwater samples from monitoring wells MW-1R, MW-3, MW-4, MW-5, and TW-1, and
water supply wells WSW-1, WSW-2, WSW-3, WSW-4, and WSW-6, and completion of a
federal/state groundwater monitoring report (TA-01), and performing a receptor survey update
(TA-02). These services were completed as proposed, with the exception that the property
serviced by water supply well WSW-4 remains vacant and the well is not currently active. A
sample was collected from water supply well WSW-5 in its place. The updated receptor
information is incorporated into this report. A separate receptor survey update letter report was
not generated.

Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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4. SITE HISTORY AND CHARACTERIZATION
The C&H Market site, identified as NCDENR Incident Number #17513, is located at 730 NC
Highway 87, Elon, Alamance County, North Carolina (Figures 1 and 2). The site is currently
owned by Payne Oil Company, Inc. and contains four above-ground propane storage tanks;
however, the site previously contained four USTs.

In August 1991, three 1,000-gallon gasoline USTs and one 550-gallon kerosene UST were
removed from the site. An assessment and observation of the tank removal was not performed.
On January 29, 1996 a Closure Report issued by Cedar Rock Environmental Services, Inc.
confirmed soil contamination near both the former gasoline USTs and the former kerosene UST.
No contaminated soil has been removed from the site.

In 2004, Geological Resources, Inc. (GRI) installed five shallow monitoring wells (MW-1
through MW-5) and one deep monitoring well (TW-1). Sampling results showed concentrations
of benzene, toluene, ethylbenzene, total xylenes, and naphthalene above their respective 15A
NCAC 2L .0202 Groundwater Quality Standards (2L Standards) in the sample collected from
monitoring well MW-1. Water supply wells WSW-2, WSW-3, WSW-4, WSW-5, and WSW-7
were also sampled in March and April 2004. On March 11, 2004, benzo(a)anthracene was
detected in the sample collected from water supply well WSW-4 and anthracene was detected in
the sample collected from water supply well WSW-5 at concentrations greater than the
laboratory method reporting limits. However water supply wells WSW-4 and WSW-5 were
resampled on April 26, 2004, and the compounds were not detected at concentrations greater
than the laboratory method reporting limits. GRI also conducted soil sampling in the area of the
former USTs. Soil samples collected on March 11, 2004, showed petroleum constituents above
their corresponding Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs).
However, the concentrations did not exceed the Residential MSCCs.

On January 4, 2006, ATC Associates of North Carolina, P.C. (ATC) collected groundwater
samples from the site monitoring wells and water supply wells WSW-1 through WSW-5.
Laboratory analytical results indicted benzene, toluene, ethylbenzene, total xylenes, naphthalene,
and 2-methylnaphthalene present at concentrations greater than their respective 2L Standards in
the sample collected from monitoring well MW-1. In addition, chloroethane was detected in the
sample collected from water supply well WSW-4 and chloroform was detected in the sample
collected from water supply well WSW-5 at concentrations greater than the laboratory reporting
limits, but less than their respective 2L Standards.

On September 29, 2009, S&ME was on-site to gauge depth-to-water and to collect groundwater
samples from monitoring wells MW-1, MW-3, MW-4, and MW-5. The laboratory analytical
results of the groundwater samples indicated several petroleum contaminants in the sample
collected from monitoring well MW-1 at concentrations greater than their respective 2L
Standards. Analysis of groundwater samples collected from monitoring wells MW-3, MW-4 and
MW-5 did not detect target petroleum compounds. Three water supply wells (WSW-2, WSW-3
and WSW-4) were sampled. The laboratory analytical results for each of the water supply well
samples reported no concentrations exceeding the detection limits for the targeted petroleum
constituents.

Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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Water supply well samples were collected from water supply wells WSW-2, WSW-3 and WSW-
4 on January 14 and April 13, 2010. Lead was detected in samples collected from both water
supply wells WSW-3 and WSW-4 exceeding its 2L Standard. Water supply wells WSW-3 and
WSW-4 were sampled again for total lead by EPA Method 3030C with a duplicate sample lab
filtered prior to analysis. Both the lab filtered and non-lab filtered samples from water supply
wells WSW-3 and WSW-4 did not exhibit detections of lead above laboratory detection limits.

On July 19, 2011, S&ME was on-site to gauge depth-to-water from monitoring wells MW-1,
MW-2, MW-3, MW-4, MW-5, and TW-1. Following gauging, samples were collected from
monitoring wells MW-1, MW-3, MW-4, MW-5, and TW-1. Samples were also collected from
water supply wells WSW-2 and WSW-3. Six petroleum related compounds were detected at
concentrations greater than their respective 2L Standards in the sample collected from
monitoring well MW-1. Samples collected from monitoring wells MW-3, MW-4, MW-5, and
TW-1 and water supply wells WSW-2 and WSW-3 did not exhibit concentrations greater than
the laboratory method reporting limits.
4.1 UST Owner and Operator Information.
The former owner of the tanks was Mildred M. Garrison. According to the NCDENR Registered
UST Database the address for Mildred M. Garrison was 4259 NC Highway 87, Elon, North
Carolina 27244. Information regarding the former UST system at the site is summarized in
Table 1 and the locations of the former USTs are depicted on Figure 2.
4.2 UST Information
The former UST system at the site included three 1,000-gallon gasoline USTs and one 550-
gallon kerosene UST. According to the Closure reported submitted by Cedar Rock on January
29, 1996, the USTs were permanently closed by removal on August 22, 1991. However,
according to the NCDENR Registered UST Database, the kerosene UST was removed in January
1978 and the gasoline USTs were removed on August 22, 1991. Information regarding these
USTs is summarized in Table 1 and the locations of the former USTs are depicted on Figure 2.
4.3 Description of the UST Release

 Date reported: August 23, 2010

 Cause and Source (including tank identification number and contents): USTs 1, 2, and 3
(1,000-gallon gasoline UST) and UST 4 (550-gallon kerosene UST)
4.4 Site Characteristics

 Land Use of Site: The site is currently occupied by Payne Oil Company. Historically the
site was retail automotive fueling facility.

 Land Use of Surrounding Area: The land use of the surrounding area includes a mixture
of residential and agricultural properties.

Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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 Topography: The site is approximately 750 feet above the Nation Geodetic Vertical
Datum of 1929. Based upon the topographic map reviewed, the area of the subject
property slopes predominantly to the east. Refer to Figure 1 for a USGS Topographic
Map.

 Vegetation/Surface Cover: The site is predominantly covered by grass; howeve, a A few
landscaped grass areas exist at the site; however, and asphalt and gravel driving area also
exists at the site.

 Surface Water: An unnamed pond is located approximately 820 feet northwest of the
source area.

 Wells: S&ME updated the receptor survey for this report. A public water supply is not
available to the area of the site. Eleven water supply wells used as a primary drinking
water source were identified within 1,000 feet of the site.

 Buildings: No buildings are located at the site.

 Soil Type: Soils underlying the site are characterized as Cecil fine sandy loam, with two
to six percent slopes and is eroded, in the majority of the site; Cecil fine sandy loam, with
six to 10 percent slopes and is eroded in the northwest corner of the site; and Starr loam,
with two to six percent slopes and is occasionally flooded, in the southeast in the
southeast corner.

 Depth to and Nature of Bedrock: According to the 1985 USGS Geologic Map of North
Carolina, the site is underlain by the Carolina Slate Belt of the Piedmont Physiographic
Province. Bedrock in this area is light gray to greenish gray metamorphosed dacitic to
rhyolitic flows and tuffs. They are interbedded with mafic and intermediate metavolcanic
rock, meta-argillite, and metamudstone.

 Depth to Groundwater in Source Area: Based upon data collected on April 29, 2015,
depth to groundwater measurements at the site ranged from 14.59 feet below top of
casing (ft-BTOC) in monitoring well MW-5 to 15.76 ft- BTOC in monitoring well TW-1.
Groundwater depth and elevation measurements are summarized in Table 2.

 Direction of Groundwater Flow: Based upon measurements collected on April 29, 2015,
groundwater at the site flows predominantly west and southwest. Figure 3 graphically
depicts the groundwater elevations at the site based on the April 29, 2015 measurements.
4.5 Owners and Occupants of Adjoining/Nearby Properties and Land Use
Details regarding the adjacent properties are summarized in Table 3. The land use of the
surrounding area includes a mixture of residential and agricultural properties.
4.6 Receptors/Potential Receptor Information
S&ME completed a receptor survey update to identify water supply wells within 1,000 feet of
the source area. The update was completed by performing a site reconnaissance to observe
Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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potential well structures on properties within 1,000 feet. Well survey questionnaires were also
mailed to property owners with observed well and/or residential structures on properties within
1,000 feet of the source area. S&ME referenced the Alamance County, North Carolina GIS
system to identify property owners. The collected data was compiled into Table 3 and the
location of the identified water supply wells are shown on Figure 4.
5. CURRENT SITE ASSESSMENT INFORMATION
5.1 Current Liquid Levels
On April 29, 2015, S&ME was onsite to gauge liquid levels in monitoring wells MW-1R, MW-
3, MW-4, MW-5, and TW-1. The depth-to-water ranged from 14.59 feet ft-BTOC in monitoring
well MW-5 to 15.76 ft- BTOC in monitoring well TW-1. A summary of current and historic
groundwater levels is included in Table 2 and the groundwater elevations based on the April 29,
2015 measurements are depicted in Figure 3.
5.2 Groundwater Monitoring Events
After measuring the depth-to-water, S&ME personnel purged monitoring wells MW-1R, MW-3,
MW-4, MW-5, and TW-1 with disposable polyethylene bailers by evacuating at least three well
volumes. The monitoring wells were allowed to recharge and suspended sediments allowed to
settle.

After completing the well purging, S&ME personnel collected a groundwater sample from the
monitoring wells. The groundwater samples were placed in laboratory-supplied containers,
stored in a cooler with ice, and shipped under chain-of-custody procedures to Pace Analytical
Services, Inc., a North Carolina certified laboratory for laboratory analysis. The groundwater
samples were analyzed for volatile organic compounds (VOCs) by Standard Method 6200B.

S&ME also collected samples from water supply wells WSW-1, WSW-2, WSW-3, WSW-5, and
WSW-6 on April 29, 2015. Each well that was sampled was purged for approximately 15
minutes prior to sampling. The groundwater samples were placed in laboratory-supplied
containers, stored in a cooler with ice, and shipped under chain-of-custody procedures to Pace
for laboratory analysis. The water supply well samples were analyzed for VOCs by Standard
Method 6200B. The locations of the water supply wells are depicted on Figure 4.

A copy of the monitoring well sampling form is included in Appendix I.
5.3 Summary of Groundwater Assessment Information
The monitoring well sampling results are summarized in Table 4. Review of the laboratory
analytical results for the samples collected on April 29, 2015, indicated the following
exceedances of the 2L Standards in the sample collected from monitoring well MW-1R:

Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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Compound Concentrations (g/L) 2L Standard (g/L)
Benzene 649 1
Ethylbenzene 1,150 600
Naphthalene 287 6
n-Propylbenzene 193 70
Toluene 5,510 600
1,2,4-Trimethylbenzene 1,460 400
1,3,5-Trimethylbenzene 444 400
Total Xylenes 6,590 500

Toluene and 1,2,4-trimethylbenzene were detected in the sample collected from monitoring well
MW-3 at concentrations greater than the laboratory method reporting limit, but less than their
respective 2L Standards. No compounds were detected in the samples collected from monitoring
wells MW-4, MW-5, and TW-1 at concentrations greater than the laboratory method reporting
limits.

Figure 5 graphically depicts the contaminants detected at concentrations greater than their
respective 2L Standards in the groundwater samples collected on April 29, 2015. Because target
analytes were only reported in monitor well MW-1R at concentrations greater than 2L Standards,
isoconcentrations maps were not prepared to depict the estimated extent of dissolved petroleum
compounds.

No compounds were detected at concentrations greater than the laboratory method reporting
limits in the samples collected from water supply wells WSW-1, WSW-2, WSW-3, WSW-5, and
WSW-6.

A copy of the laboratory report for the samples collected on April 29, 2015, is included in
Appendix II.
5.4 Regional and Site Geology and Hydrogeology
5.4.1 Soil and Bedrock
See Section 4.4.
5.4.2 Hydrogeology
Based upon measurements collected on April 29, 2015, groundwater at the site flows
predominantly west and southwest with an approximate gradient of 0.022 feet per foot. Figure 3
graphically depicts the approximate groundwater flow at the site based upon the April 29, 2015
measurements.
5.5 Evaluation of Groundwater Assessment Information
5.5.1 Current Extent and Severity of Contamination
Concentrations of eight petroleum related compounds were detected in the samples collected
from monitoring well MW-1R greater than their respective 2L Standards. As compared to the
sample collected in July 2011, compounds concentrations detected in the sample collected from
monitoring well MW-1R collected during this sampling event increased approximately 67%
Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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overall. Compound concentrations detected above the laboratory method reporting limit in the
sample collected from monitoring well MW-3 decreased approximately 67% as compared to the
sample collected in July 2011. Based upon the results of the samples collected from monitoring
wells MW-3, MW-4, MW-5, and TW-1, the down gradient extent of groundwater contamination
at the site has been defined.
5.5.2 Cleanup Levels Achieved
 Soil (soil-to-groundwater maximum soil contaminant concentrations) No
 Groundwater (2L standard concentrations) No

Groundwater Monitoring Report, C&H Market, Inc. #17513 S&ME Project No. 4305-15-045
730 NC Highway 87, Elon, NC August 31, 2015

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6. CONCLUSIONS AND RECOMMENDATIONS
Based on the current and historical assessment information for the site, the following conclusions
are presented:

1. The UST Incident meets the following conditions for a High Risk classification:
a. Eleven water supply wells used as a primary source of drinking water are located
within 1,000 feet of the source area.
b. Contaminant levels in the groundwater exceed the 2L Standards.
2. The extent of groundwater impacts at the site appears to be limited.

Based on the above, the following recommendations are presented:

1. Consider source area treatment to reduce groundwater contaminant concentrations.
2. Conduct annual monitoring of monitoring wells and water supply wells.

FIGURES

DATE:
DRAWN BY:
3201 SPRING FOREST RD, RALEIGH, NC 27616
NC ENGINEER LICENSE #F-0176
SCALE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM C & H MARKET TF-17513 - 730 NC HWY 87
ELON, NORTH CAROLINA
1" = 2000'
BTR
JUNE 2015
4305-15-045
1
A-5252
VICINITY MAP
2000 4000
(IN FEET)GRAPHIC SCALE
0
(IN FEET)GRAPHIC SCALE
Q:\PROJECTS\2015\4305-15-045\CAD\A5252.dwg, FIG1, 6/19/2015 5:11:44 PM, 1:1
DATE:
DRAWN BY:
3201 SPRING FOREST RD, RALEIGH, NC 27616
NC ENGINEER LICENSE #F-0176
SCALE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM C & H MARKET TF-17513 - 730 NC HWY 87
ELON, NORTH CAROLINA
1" = 60'
BTR
JUNE 2015
4305-15-045
2
A-5253
SITE MAP
60 120
(IN FEET)GRAPHIC SCALE
0
(IN FEET)GRAPHIC SCALE
Q:\PROJECTS\2015\4305-15-045\CAD\A5253.dwg, FIG2, 6/19/2015 5:10:51 PM, 1:1
DATE:
DRAWN BY:
3201 SPRING FOREST RD, RALEIGH, NC 27616
NC ENGINEER LICENSE #F-0176
SCALE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM C & H MARKET TF-17513 - 730 NC HWY 87
ELON, NORTH CAROLINA
1" = 30'
BTR
JUNE 2015
4305-15-045
3
A-5254
GROUNDWATER CONTOUR MAP
30 60
(IN FEET)GRAPHIC SCALE
0
(IN FEET)GRAPHIC SCALE
Q:\PROJECTS\2015\4305-15-045\CAD\A5254.dwg, FIG3, 6/23/2015 4:47:38 PM, 1:1
!A
!A
!A
!A
!A
!A
!A
!A
!A
!A
!A
!A
!A
500 FEET 1,000 FEET
S TONEY C RE EK C HURC H RD
NC HWY 87WSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
WSW-13
WSW-12
WSW-11
WSW-10
NC OneMap, NC Center for Geographic Information and Analysis, NC 911Board
WSW LOCATION MAPC&H MARKETNCDENR UST INCIDENT NO. 17513ALAMANCE COUNTY, NORTH CAROLINA
1
4305-15-045
MEM WWW.SMEINC.COM
SCALE:
PROJECT NO:
DATE:
DRAWN BY:
FIGURE NO.
07-22-15
1 " = 300 'Q:\GIS\2015\4305-15-045 C&H Market\Maps\WSW Location Map.mxdENGINEERING LICENSE NO: F-0176
±
REFERENCE:GIS DATA LAYERS WERE OBTAINED FROM ESRI, INC. AND ALAMANCE COUNTY GIS WEBSITE. PLEASENOTE THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. IT IS NOT MEANT FOR DESIGN, LEGAL, ORANY OTHER USES. THERE ARE NO GUARANTEES ABOUT ITS ACCURACY. S&ME, INC. ASSUMES NORESPONSIBILITY FOR ANY DECISION MADE OR ANY ACTIONS TAKEN BY THE USER BASED UPON THIS!A Anticipated WSW
DATE:
DRAWN BY:
3201 SPRING FOREST RD, RALEIGH, NC 27616
NC ENGINEER LICENSE #F-0176
SCALE:
PROJECT NO:
FIGURE NO.
WWW.SMEINC.COM C & H MARKET TF-17513 - 730 NC HWY 87
ELON, NORTH CAROLINA
1" = 30'
BTR
JUNE 2015
4305-15-045
5
A-5255
GROUNDWATER CONSTITUENT MAP
30 60
(IN FEET)GRAPHIC SCALE
0
(IN FEET)GRAPHIC SCALE
Q:\PROJECTS\2015\4305-15-045\CAD\A5255.dwg, FIG5, 6/23/2015 4:47:03 PM, 1:1

TABLES

Table 1
UST SYSTEM INFORMATION
C&H Market
730NC Highway 87
Elon,Alamance County,NorthCarolina
NCDENR Incident No.17513
S&ME Project No.4305-15-045
UST ID
Number Product Capacity
(gallons)Owner/Operator Date
Installed
Date
Closed
Was Release
Associated With
UST System?
1 Gasoline 1,000 04/06/79 08/22/91 Yes
2 Gasoline 1,000 04/07/74 08/22/91 Yes
3 Gasoline 1,000 01/01/64 08/22/91 Yes
4 Kerosene 550 01/01/64 01/01/78 Yes
NOTES:
USTInformation from NCDENR Registered USTDatabase
Mildred M. Garrison
4259 NC Highway 87
Elon, North Carolina 27244
TABLE 2
MONITORING WELL CONSTRUCTION AND LIQUID LEVEL DATA
C&H Market
730NC Highway 87
Elon,Alamance County,NorthCarolina
NCDENR Incident No.17513
S&ME Project No.4305-15-045
Well
ID
Date
Installed
Top ofCasing
Elevation
(ft)
Well
Diameter
(in)
Well Casing
Depth
(ft-BGS)
Screen Interval
(ft-BGS)
Date of
Measurement
Depthto
Product
(ft-BTOC)
DepthTo Water
(ft-BTOC)
Product
Thickness
(ft)
Groundwater
Elevation
(ft)
11/19/04 NP 15.45 NA 84.55
09/29/09 NP 20.43 NA 79.57
07/19/11 NP 19.45 NA 80.55
04/29/15 NP 15.69 NA 84.31
11/19/04 NP 17.04 NA 83.66
09/29/09 NP NM NA NA
07/19/11 NP 20.02 NA 80.68
04/29/15 NP NM NA NA
11/19/04 NP 14.74 NA 84.28
09/29/09 NP 19.72 NA 79.30
07/19/11 NP 18.92 NA 80.10
04/29/15 NP 15.05 NA 83.97
11/19/04 NP 15.38 NA 83.55
09/29/09 NP 20.76 NA 78.17
07/19/11 NP 19.78 NA 79.15
04/29/15 NP 15.73 NA 83.20
11/19/04 NP 14.23 NA 84.37
09/29/09 NP 19.32 NA 79.28
07/19/11 NP 18.26 NA 80.34
04/29/15 NP 14.59 NA 84.01
11/19/04 NP 15.59 NA 84.27
09/29/09 NP 20.50 NA 79.36
07/19/11 NP 19.56 NA 80.30
04/29/15 NP 15.76 NA 84.10
NOTES:
All measurements based on an estimated topographic elevation of 100 feet at monitor well MW-2 top-of-casing
ft : feet
in : inches
ft-BGS : feet below ground surface
TOC : Top-of-casing
BTOC: Below top-of-casing
NP : Not Present
NM : Not Measured
NA : Not Applicable
MW-1/
MW-1R 10.00 - 25.0025.002.00100.0003/11/04
TW-1
MW-5
MW-4
MW-3
MW-2 04/27/04 100.70 2.00 25.00 10.00 - 25.00
04/27/04 99.02 2.00 25.00 10.00 - 25.00
04/27/04 98.93 2.00 25.00 10.00 - 25.00
11/18/04 98.60 2.00 25.00 10.00 - 25.00
04/28/04 99.86 2.00 51.00 46.00 - 51.00
Page 2of4
W ell #Parcel #W ell Owner/User
(indicate which)Owner Address PropertyAddress Phone Number W ell Use Distance from source
area of release (ft)
WSW-1 155739 Willie & EdithGilliam 4413 N NC 87Elon,NC
27244 4413 N NC 87HWY 336-584-4361 Yes 245
WSW-2 111084 Hulon & Frances
Gerringer
4307N NC 87Elon,NC
27244 4307N NC HWY Yes 660
WSW-3 111082 LD & Linda Saul 4324 N NC 87Elon,NC
27244 4324 N NC 87HWY 584-9941 Yes 450
WSW-4 155737 Gary Johnson 4410 N NC 87Elon,NC
27244 4338N NC 87HWY 336-212-3308 not in use 210
WSW-5 155734 Gary Johnson 4410 N NC 87Elon,NC
27244 4410 N NC 87HWY 336-212-3308 Yes 450
WSW-6 155741 Donald Moore 3634 Stoney CreekChurch
Road Elon,NC 27244
4171 Stoney CreekChurch
Road
336-584-3195 (h)
336-213-3138(c)Yes 330
WSW-7 155735 James & Janice
Patrum
4414 N NC 87Elon,NC
27244 4414 N NC 87HWY Yes 360
WSW-8 155736 Gary Johnson 4410 N NC 87Elon,NC
27244 N NC 87HWY 336-212-3308 not in use 150
WSW-9 155726 Stevie & RuthGilliam 4450 NorthNC 87Elon,
NC 27244 4450 N NC HWY 336-584-5435 Yes 850
WSW-10 155725 Michael & Peggy
Alcon
4444 NC Hwy 87N Elon,
NC 27244 4444 NC HWY87 Yes 560
WSW-11 111086 Mildred & Billy
Garrison
4259N NC 87Elon,NC
27244 4259N NC 87HWY Yes 890
WSW-12 171721
Altamahaw Ossippee
Fire Department,Inc
Michael Barnette
2806N Old NC 87Elon,
NC 27244
4168Stoney CreekChurch
Road 336-584-0526 Yes 425
WSW-13 155750 Rance HEtal
Gerringer
724 Trail 8Burlington,NC
27215
4145 Stoney CreekChurch
Road 336-227-6167 Yes/not in use 660
NCDENR UST Incident No. 17513
S&ME Project No. 4305-15-045
Table 3
Water Supply Well Information
C&H Market
730 NC Highway 87
TABLE 4
SUMMARY OFGROUNDWATER ANALYTICAL DATA
C&H Market
730NC Highway 87
Elon,Alamance County,NorthCarolina
NCDENR Incident No.17513
S&ME Project No.4305-15-045
Volatile Organic Compounds by Standard Method 6200B or equivalent
Compounds of
Concern
Sample Date
11/19/04 ND ND 1,930 ND ND ND 2,520 ND ND 1,010 ND 13,500 ND ND 13,800
09/29/09 ND 48 374 33 3.7 1.6 607 28 ND 72 108 1,810 1,140 151 3,246
07/19/11 110J ND 350 38 ND ND 470 40 20 46 110 2,000 640 200 2,200
04/29/15 NA NA 649 <25.0 <25.0 <25.0 1,150 51.2 NA 287 193 5,510 1,460 444 6,590
11/19/04 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
09/29/09 NO SAMPLE COLLECTED
07/19/11 NO SAMPLE COLLECTED
04/29/15 NO SAMPLE COLLECTED
11/19/04 ND ND ND ND ND ND 1.1 ND ND 36.2 ND 2.9 ND ND 4.5
09/29/09 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07/19/11 ND ND ND ND ND ND ND ND ND ND ND 0.66 ND ND 3.4
04/29/15 NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <2.0 <0.50 0.59 0.74 <0.50 <1.5
11/19/04 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
09/29/09 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07/19/11 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/29/15 NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <2.0 <0.50 <0.50 <0.50 <0.50 <1.5
11/19/04 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
09/29/09 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07/19/11 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
04/29/15 NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <2.0 <0.50 <0.50 <0.50 <0.50 <1.5
11/19/04 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
09/29/09 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
07/19/11 ND ND ND ND ND ND 0.59 ND ND ND ND 2.9 2.0 1.7 7.1
04/29/15 NA NA <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NA <2.0 <0.50 <0.50 <0.50 <0.50 <1.5
6,000 3 1 70 0.02 0.4 600 70 25 6 70 600 400 400 500
6,000,000 170 5,000 6,900 50 400 84,500 25,000 11,700 6,000 30,000 260,000 28,500 25,000 85,500
NOTES:
Analytes that are not shown were not detected
Data presented in micrograms per liter ormg/L
2LStandard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202
Value Concentration exceeds the 2LStandards
Value Concentration exceeds the Gross Contamination Levels 1,2-DichloroethaneBis(2-ethylhexyl)phthalateTotalXylenesn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneNaphthaleneToluenep-IsopropyltolueneEthylbenzeneIsopropylbenzene1,2-Dibromoethanen-ButylbenzeneGross Contamination Level
Sample ID
Benzene2L Standard
MW-4
MW-3
MW-2
MW-1/
MW-1R
MW-5
TW-1 AcetonePage 4 of 4

APPENDICES

APPENDIX I

Field Notes

APPENDIX II

Laboratory Reports
#=CL#
May 11, 2015
LIMS USE: FR - WAYNE WATTERSON
LIMS OBJECT ID: 92247831
92247831
Project:
Pace Project No.:
RE:
Mr. Wayne Watterson
S&ME, Inc.
8646 West Market Street
Greensboro, NC 27409
C&W MARKET
Dear Mr. Watterson:
Enclosed are the analytical results for sample(s) received by the laboratory on April 30, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92247831
C&W MARKET
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 35
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92247831
C&W MARKET
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92247831001 MW-1R SM 6200B 63 PASI-CGAW
92247831002 MW-3 SM 6200B 63 PASI-CGAW
92247831003 MW-4 SM 6200B 63 PASI-CGAW
92247831004 MW-5 SM 6200B 63 PASI-CGAW
92247831005 TW-1 SM 6200B 63 PASI-CGAW
92247831006 WSW-1 SM 6200B 63 PASI-CGAW
92247831007 WSW-2 SM 6200B 63 PASI-CGAW
92247831008 WSW-3 SM 6200B 63 PASI-CGAW
92247831009 WSW-5 SM 6200B 63 PASI-CGAW
92247831010 WSW-6 SM 6200B 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 35
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92247831
C&W MARKET
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92247831001 MW-1R
Benzene 649 ug/L 05/09/15 16:1825.0SM 6200B
1,2-Dibromoethane (EDB)<25.0 ug/L 05/09/15 16:1825.0SM 6200B
Ethylbenzene 1150 ug/L 05/09/15 16:1825.0SM 6200B
Isopropylbenzene (Cumene)51.2 ug/L 05/09/15 16:1825.0SM 6200B
Naphthalene 287 ug/L 05/09/15 16:18100SM 6200B
n-Propylbenzene 193 ug/L 05/09/15 16:1825.0SM 6200B
Toluene 5510 ug/L 05/09/15 16:18 P825.0SM 6200B
1,2,4-Trimethylbenzene 1460 ug/L 05/09/15 16:1825.0SM 6200B
1,3,5-Trimethylbenzene 444 ug/L 05/09/15 16:1825.0SM 6200B
m&p-Xylene 4700 ug/L 05/09/15 16:1850.0SM 6200B
o-Xylene 1890 ug/L 05/09/15 16:1825.0SM 6200B
92247831002 MW-3
Toluene 0.59 ug/L 05/10/15 17:160.50SM 6200B
1,2,4-Trimethylbenzene 0.74 ug/L 05/10/15 17:160.50SM 6200B
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 17:160.50SM 6200B
m&p-Xylene <1.0 ug/L 05/10/15 17:161.0SM 6200B
o-Xylene <0.50 ug/L 05/10/15 17:160.50SM 6200B
92247831003 MW-4
Toluene <0.50 ug/L 05/10/15 17:320.50SM 6200B
92247831004 MW-5
Toluene <0.50 ug/L 05/10/15 17:490.50SM 6200B
92247831005 TW-1
Toluene <0.50 ug/L 05/10/15 18:050.50SM 6200B
92247831008 WSW-3
Chloroform <0.50 ug/L 05/10/15 18:550.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 35
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92247831
C&W MARKET
Method:
Client:S&ME, Inc.
SM 6200B
Date:May 11, 2015
Description:6200B MSV
General Information:
10 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: MSV/31540
P8: Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than the blank
or were below the reporting limit.
• MW-1R (Lab ID: 92247831001)
• Toluene
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:MW-1R Lab ID:92247831001 Collected:04/29/15 13:30 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 649 ug/L 05/09/15 16:18 71-43-225.0 50
Bromobenzene <25.0 ug/L 05/09/15 16:18 108-86-125.0 50
Bromochloromethane <25.0 ug/L 05/09/15 16:18 74-97-525.0 50
Bromodichloromethane <25.0 ug/L 05/09/15 16:18 75-27-425.0 50
Bromoform <25.0 ug/L 05/09/15 16:18 75-25-225.0 50
Bromomethane <250 ug/L 05/09/15 16:18 74-83-925050
n-Butylbenzene <25.0 ug/L 05/09/15 16:18 104-51-825.0 50
sec-Butylbenzene <25.0 ug/L 05/09/15 16:18 135-98-825.0 50
tert-Butylbenzene <25.0 ug/L 05/09/15 16:18 98-06-625.0 50
Carbon tetrachloride <25.0 ug/L 05/09/15 16:18 56-23-525.0 50
Chlorobenzene <25.0 ug/L 05/09/15 16:18 108-90-725.0 50
Chloroethane <50.0 ug/L 05/09/15 16:18 75-00-350.0 50
Chloroform <25.0 ug/L 05/09/15 16:18 67-66-325.0 50
Chloromethane <50.0 ug/L 05/09/15 16:18 74-87-350.0 50
2-Chlorotoluene <25.0 ug/L 05/09/15 16:18 95-49-825.0 50
4-Chlorotoluene <25.0 ug/L 05/09/15 16:18 106-43-425.0 50
1,2-Dibromo-3-chloropropane <50.0 ug/L 05/09/15 16:18 96-12-850.0 50
Dibromochloromethane <25.0 ug/L 05/09/15 16:18 124-48-125.0 50
1,2-Dibromoethane (EDB)<25.0 ug/L 05/09/15 16:18 106-93-425.0 50
Dibromomethane <25.0 ug/L 05/09/15 16:18 74-95-325.0 50
1,2-Dichlorobenzene <25.0 ug/L 05/09/15 16:18 95-50-125.0 50
1,3-Dichlorobenzene <25.0 ug/L 05/09/15 16:18 541-73-125.0 50
1,4-Dichlorobenzene <25.0 ug/L 05/09/15 16:18 106-46-725.0 50
Dichlorodifluoromethane <25.0 ug/L 05/09/15 16:18 75-71-825.0 50
1,1-Dichloroethane <25.0 ug/L 05/09/15 16:18 75-34-325.0 50
1,2-Dichloroethane <25.0 ug/L 05/09/15 16:18 107-06-225.0 50
1,1-Dichloroethene <25.0 ug/L 05/09/15 16:18 75-35-425.0 50
cis-1,2-Dichloroethene <25.0 ug/L 05/09/15 16:18 156-59-225.0 50
trans-1,2-Dichloroethene <25.0 ug/L 05/09/15 16:18 156-60-525.0 50
1,2-Dichloropropane <25.0 ug/L 05/09/15 16:18 78-87-525.0 50
1,3-Dichloropropane <25.0 ug/L 05/09/15 16:18 142-28-925.0 50
2,2-Dichloropropane <25.0 ug/L 05/09/15 16:18 594-20-725.0 50
1,1-Dichloropropene <25.0 ug/L 05/09/15 16:18 563-58-625.0 50
cis-1,3-Dichloropropene <25.0 ug/L 05/09/15 16:18 10061-01-525.0 50
trans-1,3-Dichloropropene <25.0 ug/L 05/09/15 16:18 10061-02-625.0 50
Diisopropyl ether <25.0 ug/L 05/09/15 16:18 108-20-325.0 50
Ethylbenzene 1150 ug/L 05/09/15 16:18 100-41-425.0 50
Hexachloro-1,3-butadiene <100 ug/L 05/09/15 16:18 87-68-310050
Isopropylbenzene (Cumene)51.2 ug/L 05/09/15 16:18 98-82-825.0 50
Methylene Chloride <100 ug/L 05/09/15 16:18 75-09-210050
Methyl-tert-butyl ether <25.0 ug/L 05/09/15 16:18 1634-04-425.0 50
Naphthalene 287 ug/L 05/09/15 16:18 91-20-310050
n-Propylbenzene 193 ug/L 05/09/15 16:18 103-65-125.0 50
Styrene <25.0 ug/L 05/09/15 16:18 100-42-525.0 50
1,1,1,2-Tetrachloroethane <25.0 ug/L 05/09/15 16:18 630-20-625.0 50
1,1,2,2-Tetrachloroethane <25.0 ug/L 05/09/15 16:18 79-34-525.0 50
Tetrachloroethene <25.0 ug/L 05/09/15 16:18 127-18-425.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:MW-1R Lab ID:92247831001 Collected:04/29/15 13:30 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 5510 ug/L 05/09/15 16:18 108-88-3 P825.0 50
1,2,3-Trichlorobenzene <100 ug/L 05/09/15 16:18 87-61-610050
1,2,4-Trichlorobenzene <100 ug/L 05/09/15 16:18 120-82-110050
1,1,1-Trichloroethane <25.0 ug/L 05/09/15 16:18 71-55-625.0 50
1,1,2-Trichloroethane <25.0 ug/L 05/09/15 16:18 79-00-525.0 50
Trichloroethene <25.0 ug/L 05/09/15 16:18 79-01-625.0 50
Trichlorofluoromethane <50.0 ug/L 05/09/15 16:18 75-69-450.0 50
1,2,3-Trichloropropane <25.0 ug/L 05/09/15 16:18 96-18-425.0 50
1,2,4-Trimethylbenzene 1460 ug/L 05/09/15 16:18 95-63-625.0 50
1,3,5-Trimethylbenzene 444 ug/L 05/09/15 16:18 108-67-825.0 50
Vinyl chloride <50.0 ug/L 05/09/15 16:18 75-01-450.0 50
m&p-Xylene 4700 ug/L 05/09/15 16:18 179601-23-150.0 50
o-Xylene 1890 ug/L 05/09/15 16:18 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)101 %05/09/15 16:18 17060-07-070-130 50
4-Bromofluorobenzene (S)97 %05/09/15 16:18 460-00-470-130 50
Toluene-d8 (S)100 %05/09/15 16:18 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:MW-3 Lab ID:92247831002 Collected:04/29/15 14:00 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 05/10/15 17:16 71-43-20.50 1
Bromobenzene <0.50 ug/L 05/10/15 17:16 108-86-10.50 1
Bromochloromethane <0.50 ug/L 05/10/15 17:16 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 05/10/15 17:16 75-27-40.50 1
Bromoform <0.50 ug/L 05/10/15 17:16 75-25-20.50 1
Bromomethane <5.0 ug/L 05/10/15 17:16 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 05/10/15 17:16 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 05/10/15 17:16 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 05/10/15 17:16 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 05/10/15 17:16 56-23-50.50 1
Chlorobenzene <0.50 ug/L 05/10/15 17:16 108-90-70.50 1
Chloroethane <1.0 ug/L 05/10/15 17:16 75-00-31.0 1
Chloroform <0.50 ug/L 05/10/15 17:16 67-66-30.50 1
Chloromethane <1.0 ug/L 05/10/15 17:16 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 05/10/15 17:16 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 05/10/15 17:16 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 05/10/15 17:16 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 05/10/15 17:16 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 05/10/15 17:16 106-93-40.50 1
Dibromomethane <0.50 ug/L 05/10/15 17:16 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 05/10/15 17:16 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 05/10/15 17:16 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 05/10/15 17:16 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 05/10/15 17:16 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 05/10/15 17:16 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 05/10/15 17:16 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 05/10/15 17:16 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 05/10/15 17:16 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 05/10/15 17:16 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 05/10/15 17:16 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 05/10/15 17:16 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 05/10/15 17:16 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 05/10/15 17:16 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 05/10/15 17:16 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 05/10/15 17:16 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 05/10/15 17:16 108-20-30.50 1
Ethylbenzene <0.50 ug/L 05/10/15 17:16 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 05/10/15 17:16 87-68-32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 05/10/15 17:16 98-82-80.50 1
Methylene Chloride <2.0 ug/L 05/10/15 17:16 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 05/10/15 17:16 1634-04-40.50 1
Naphthalene <2.0 ug/L 05/10/15 17:16 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 05/10/15 17:16 103-65-10.50 1
Styrene <0.50 ug/L 05/10/15 17:16 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 05/10/15 17:16 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 05/10/15 17:16 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 05/10/15 17:16 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:MW-3 Lab ID:92247831002 Collected:04/29/15 14:00 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 0.59 ug/L 05/10/15 17:16 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 05/10/15 17:16 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 05/10/15 17:16 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 05/10/15 17:16 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 05/10/15 17:16 79-00-50.50 1
Trichloroethene <0.50 ug/L 05/10/15 17:16 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 05/10/15 17:16 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 05/10/15 17:16 96-18-40.50 1
1,2,4-Trimethylbenzene 0.74 ug/L 05/10/15 17:16 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 17:16 108-67-80.50 1
Vinyl chloride <1.0 ug/L 05/10/15 17:16 75-01-41.0 1
m&p-Xylene <1.0 ug/L 05/10/15 17:16 179601-23-11.0 1
o-Xylene <0.50 ug/L 05/10/15 17:16 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %05/10/15 17:16 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %05/10/15 17:16 460-00-470-130 1
Toluene-d8 (S)101 %05/10/15 17:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:MW-4 Lab ID:92247831003 Collected:04/29/15 14:30 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 05/10/15 17:32 71-43-20.50 1
Bromobenzene <0.50 ug/L 05/10/15 17:32 108-86-10.50 1
Bromochloromethane <0.50 ug/L 05/10/15 17:32 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 05/10/15 17:32 75-27-40.50 1
Bromoform <0.50 ug/L 05/10/15 17:32 75-25-20.50 1
Bromomethane <5.0 ug/L 05/10/15 17:32 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 05/10/15 17:32 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 05/10/15 17:32 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 05/10/15 17:32 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 05/10/15 17:32 56-23-50.50 1
Chlorobenzene <0.50 ug/L 05/10/15 17:32 108-90-70.50 1
Chloroethane <1.0 ug/L 05/10/15 17:32 75-00-31.0 1
Chloroform <0.50 ug/L 05/10/15 17:32 67-66-30.50 1
Chloromethane <1.0 ug/L 05/10/15 17:32 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 05/10/15 17:32 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 05/10/15 17:32 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 05/10/15 17:32 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 05/10/15 17:32 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 05/10/15 17:32 106-93-40.50 1
Dibromomethane <0.50 ug/L 05/10/15 17:32 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 05/10/15 17:32 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 05/10/15 17:32 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 05/10/15 17:32 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 05/10/15 17:32 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 05/10/15 17:32 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 05/10/15 17:32 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 05/10/15 17:32 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 05/10/15 17:32 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 05/10/15 17:32 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 05/10/15 17:32 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 05/10/15 17:32 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 05/10/15 17:32 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 05/10/15 17:32 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 05/10/15 17:32 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 05/10/15 17:32 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 05/10/15 17:32 108-20-30.50 1
Ethylbenzene <0.50 ug/L 05/10/15 17:32 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 05/10/15 17:32 87-68-32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 05/10/15 17:32 98-82-80.50 1
Methylene Chloride <2.0 ug/L 05/10/15 17:32 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 05/10/15 17:32 1634-04-40.50 1
Naphthalene <2.0 ug/L 05/10/15 17:32 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 05/10/15 17:32 103-65-10.50 1
Styrene <0.50 ug/L 05/10/15 17:32 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 05/10/15 17:32 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 05/10/15 17:32 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 05/10/15 17:32 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:MW-4 Lab ID:92247831003 Collected:04/29/15 14:30 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 05/10/15 17:32 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 05/10/15 17:32 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 05/10/15 17:32 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 05/10/15 17:32 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 05/10/15 17:32 79-00-50.50 1
Trichloroethene <0.50 ug/L 05/10/15 17:32 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 05/10/15 17:32 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 05/10/15 17:32 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/10/15 17:32 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 17:32 108-67-80.50 1
Vinyl chloride <1.0 ug/L 05/10/15 17:32 75-01-41.0 1
m&p-Xylene <1.0 ug/L 05/10/15 17:32 179601-23-11.0 1
o-Xylene <0.50 ug/L 05/10/15 17:32 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %05/10/15 17:32 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %05/10/15 17:32 460-00-470-130 1
Toluene-d8 (S)99 %05/10/15 17:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:MW-5 Lab ID:92247831004 Collected:04/29/15 15:00 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 05/10/15 17:49 71-43-20.50 1
Bromobenzene <0.50 ug/L 05/10/15 17:49 108-86-10.50 1
Bromochloromethane <0.50 ug/L 05/10/15 17:49 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 05/10/15 17:49 75-27-40.50 1
Bromoform <0.50 ug/L 05/10/15 17:49 75-25-20.50 1
Bromomethane <5.0 ug/L 05/10/15 17:49 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 05/10/15 17:49 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 05/10/15 17:49 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 05/10/15 17:49 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 05/10/15 17:49 56-23-50.50 1
Chlorobenzene <0.50 ug/L 05/10/15 17:49 108-90-70.50 1
Chloroethane <1.0 ug/L 05/10/15 17:49 75-00-31.0 1
Chloroform <0.50 ug/L 05/10/15 17:49 67-66-30.50 1
Chloromethane <1.0 ug/L 05/10/15 17:49 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 05/10/15 17:49 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 05/10/15 17:49 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 05/10/15 17:49 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 05/10/15 17:49 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 05/10/15 17:49 106-93-40.50 1
Dibromomethane <0.50 ug/L 05/10/15 17:49 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 05/10/15 17:49 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 05/10/15 17:49 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 05/10/15 17:49 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 05/10/15 17:49 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 05/10/15 17:49 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 05/10/15 17:49 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 05/10/15 17:49 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 05/10/15 17:49 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 05/10/15 17:49 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 05/10/15 17:49 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 05/10/15 17:49 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 05/10/15 17:49 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 05/10/15 17:49 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 05/10/15 17:49 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 05/10/15 17:49 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 05/10/15 17:49 108-20-30.50 1
Ethylbenzene <0.50 ug/L 05/10/15 17:49 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 05/10/15 17:49 87-68-32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 05/10/15 17:49 98-82-80.50 1
Methylene Chloride <2.0 ug/L 05/10/15 17:49 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 05/10/15 17:49 1634-04-40.50 1
Naphthalene <2.0 ug/L 05/10/15 17:49 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 05/10/15 17:49 103-65-10.50 1
Styrene <0.50 ug/L 05/10/15 17:49 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 05/10/15 17:49 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 05/10/15 17:49 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 05/10/15 17:49 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:MW-5 Lab ID:92247831004 Collected:04/29/15 15:00 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 05/10/15 17:49 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 05/10/15 17:49 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 05/10/15 17:49 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 05/10/15 17:49 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 05/10/15 17:49 79-00-50.50 1
Trichloroethene <0.50 ug/L 05/10/15 17:49 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 05/10/15 17:49 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 05/10/15 17:49 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/10/15 17:49 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 17:49 108-67-80.50 1
Vinyl chloride <1.0 ug/L 05/10/15 17:49 75-01-41.0 1
m&p-Xylene <1.0 ug/L 05/10/15 17:49 179601-23-11.0 1
o-Xylene <0.50 ug/L 05/10/15 17:49 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %05/10/15 17:49 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %05/10/15 17:49 460-00-470-130 1
Toluene-d8 (S)99 %05/10/15 17:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:TW-1 Lab ID:92247831005 Collected:04/29/15 13:00 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 05/10/15 18:05 71-43-20.50 1
Bromobenzene <0.50 ug/L 05/10/15 18:05 108-86-10.50 1
Bromochloromethane <0.50 ug/L 05/10/15 18:05 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 05/10/15 18:05 75-27-40.50 1
Bromoform <0.50 ug/L 05/10/15 18:05 75-25-20.50 1
Bromomethane <5.0 ug/L 05/10/15 18:05 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 05/10/15 18:05 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 05/10/15 18:05 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 05/10/15 18:05 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 05/10/15 18:05 56-23-50.50 1
Chlorobenzene <0.50 ug/L 05/10/15 18:05 108-90-70.50 1
Chloroethane <1.0 ug/L 05/10/15 18:05 75-00-31.0 1
Chloroform <0.50 ug/L 05/10/15 18:05 67-66-30.50 1
Chloromethane <1.0 ug/L 05/10/15 18:05 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 05/10/15 18:05 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 05/10/15 18:05 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 05/10/15 18:05 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 05/10/15 18:05 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 05/10/15 18:05 106-93-40.50 1
Dibromomethane <0.50 ug/L 05/10/15 18:05 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 05/10/15 18:05 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 05/10/15 18:05 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 05/10/15 18:05 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 05/10/15 18:05 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 05/10/15 18:05 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 05/10/15 18:05 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 05/10/15 18:05 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 05/10/15 18:05 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 05/10/15 18:05 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 05/10/15 18:05 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 05/10/15 18:05 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 05/10/15 18:05 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 05/10/15 18:05 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 05/10/15 18:05 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 05/10/15 18:05 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 05/10/15 18:05 108-20-30.50 1
Ethylbenzene <0.50 ug/L 05/10/15 18:05 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 05/10/15 18:05 87-68-32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 05/10/15 18:05 98-82-80.50 1
Methylene Chloride <2.0 ug/L 05/10/15 18:05 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 05/10/15 18:05 1634-04-40.50 1
Naphthalene <2.0 ug/L 05/10/15 18:05 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 05/10/15 18:05 103-65-10.50 1
Styrene <0.50 ug/L 05/10/15 18:05 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 05/10/15 18:05 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 05/10/15 18:05 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 05/10/15 18:05 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:TW-1 Lab ID:92247831005 Collected:04/29/15 13:00 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 05/10/15 18:05 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 05/10/15 18:05 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 05/10/15 18:05 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 05/10/15 18:05 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 05/10/15 18:05 79-00-50.50 1
Trichloroethene <0.50 ug/L 05/10/15 18:05 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 05/10/15 18:05 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 05/10/15 18:05 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/10/15 18:05 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 18:05 108-67-80.50 1
Vinyl chloride <1.0 ug/L 05/10/15 18:05 75-01-41.0 1
m&p-Xylene <1.0 ug/L 05/10/15 18:05 179601-23-11.0 1
o-Xylene <0.50 ug/L 05/10/15 18:05 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %05/10/15 18:05 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %05/10/15 18:05 460-00-470-130 1
Toluene-d8 (S)100 %05/10/15 18:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-1 Lab ID:92247831006 Collected:04/29/15 15:45 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 05/10/15 18:22 71-43-20.50 1
Bromobenzene <0.50 ug/L 05/10/15 18:22 108-86-10.50 1
Bromochloromethane <0.50 ug/L 05/10/15 18:22 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 05/10/15 18:22 75-27-40.50 1
Bromoform <0.50 ug/L 05/10/15 18:22 75-25-20.50 1
Bromomethane <5.0 ug/L 05/10/15 18:22 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 05/10/15 18:22 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 05/10/15 18:22 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 05/10/15 18:22 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 05/10/15 18:22 56-23-50.50 1
Chlorobenzene <0.50 ug/L 05/10/15 18:22 108-90-70.50 1
Chloroethane <1.0 ug/L 05/10/15 18:22 75-00-31.0 1
Chloroform <0.50 ug/L 05/10/15 18:22 67-66-30.50 1
Chloromethane <1.0 ug/L 05/10/15 18:22 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 05/10/15 18:22 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 05/10/15 18:22 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 05/10/15 18:22 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 05/10/15 18:22 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 05/10/15 18:22 106-93-40.50 1
Dibromomethane <0.50 ug/L 05/10/15 18:22 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 05/10/15 18:22 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 05/10/15 18:22 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 05/10/15 18:22 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 05/10/15 18:22 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 05/10/15 18:22 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 05/10/15 18:22 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 05/10/15 18:22 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 05/10/15 18:22 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 05/10/15 18:22 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 05/10/15 18:22 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 05/10/15 18:22 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 05/10/15 18:22 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 05/10/15 18:22 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 05/10/15 18:22 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 05/10/15 18:22 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 05/10/15 18:22 108-20-30.50 1
Ethylbenzene <0.50 ug/L 05/10/15 18:22 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 05/10/15 18:22 87-68-32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 05/10/15 18:22 98-82-80.50 1
Methylene Chloride <2.0 ug/L 05/10/15 18:22 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 05/10/15 18:22 1634-04-40.50 1
Naphthalene <2.0 ug/L 05/10/15 18:22 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 05/10/15 18:22 103-65-10.50 1
Styrene <0.50 ug/L 05/10/15 18:22 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 05/10/15 18:22 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 05/10/15 18:22 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 05/10/15 18:22 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-1 Lab ID:92247831006 Collected:04/29/15 15:45 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 05/10/15 18:22 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 05/10/15 18:22 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 05/10/15 18:22 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 05/10/15 18:22 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 05/10/15 18:22 79-00-50.50 1
Trichloroethene <0.50 ug/L 05/10/15 18:22 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 05/10/15 18:22 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 05/10/15 18:22 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/10/15 18:22 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 18:22 108-67-80.50 1
Vinyl chloride <1.0 ug/L 05/10/15 18:22 75-01-41.0 1
m&p-Xylene <1.0 ug/L 05/10/15 18:22 179601-23-11.0 1
o-Xylene <0.50 ug/L 05/10/15 18:22 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %05/10/15 18:22 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %05/10/15 18:22 460-00-470-130 1
Toluene-d8 (S)100 %05/10/15 18:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-2 Lab ID:92247831007 Collected:04/29/15 17:25 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 05/10/15 18:38 71-43-20.50 1
Bromobenzene <0.50 ug/L 05/10/15 18:38 108-86-10.50 1
Bromochloromethane <0.50 ug/L 05/10/15 18:38 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 05/10/15 18:38 75-27-40.50 1
Bromoform <0.50 ug/L 05/10/15 18:38 75-25-20.50 1
Bromomethane <5.0 ug/L 05/10/15 18:38 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 05/10/15 18:38 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 05/10/15 18:38 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 05/10/15 18:38 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 05/10/15 18:38 56-23-50.50 1
Chlorobenzene <0.50 ug/L 05/10/15 18:38 108-90-70.50 1
Chloroethane <1.0 ug/L 05/10/15 18:38 75-00-31.0 1
Chloroform <0.50 ug/L 05/10/15 18:38 67-66-30.50 1
Chloromethane <1.0 ug/L 05/10/15 18:38 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 05/10/15 18:38 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 05/10/15 18:38 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 05/10/15 18:38 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 05/10/15 18:38 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 05/10/15 18:38 106-93-40.50 1
Dibromomethane <0.50 ug/L 05/10/15 18:38 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 05/10/15 18:38 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 05/10/15 18:38 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 05/10/15 18:38 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 05/10/15 18:38 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 05/10/15 18:38 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 05/10/15 18:38 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 05/10/15 18:38 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 05/10/15 18:38 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 05/10/15 18:38 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 05/10/15 18:38 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 05/10/15 18:38 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 05/10/15 18:38 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 05/10/15 18:38 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 05/10/15 18:38 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 05/10/15 18:38 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 05/10/15 18:38 108-20-30.50 1
Ethylbenzene <0.50 ug/L 05/10/15 18:38 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 05/10/15 18:38 87-68-32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 05/10/15 18:38 98-82-80.50 1
Methylene Chloride <2.0 ug/L 05/10/15 18:38 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 05/10/15 18:38 1634-04-40.50 1
Naphthalene <2.0 ug/L 05/10/15 18:38 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 05/10/15 18:38 103-65-10.50 1
Styrene <0.50 ug/L 05/10/15 18:38 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 05/10/15 18:38 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 05/10/15 18:38 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 05/10/15 18:38 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-2 Lab ID:92247831007 Collected:04/29/15 17:25 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 05/10/15 18:38 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 05/10/15 18:38 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 05/10/15 18:38 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 05/10/15 18:38 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 05/10/15 18:38 79-00-50.50 1
Trichloroethene <0.50 ug/L 05/10/15 18:38 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 05/10/15 18:38 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 05/10/15 18:38 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/10/15 18:38 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 18:38 108-67-80.50 1
Vinyl chloride <1.0 ug/L 05/10/15 18:38 75-01-41.0 1
m&p-Xylene <1.0 ug/L 05/10/15 18:38 179601-23-11.0 1
o-Xylene <0.50 ug/L 05/10/15 18:38 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %05/10/15 18:38 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %05/10/15 18:38 460-00-470-130 1
Toluene-d8 (S)100 %05/10/15 18:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-3 Lab ID:92247831008 Collected:04/29/15 17:00 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 05/10/15 18:55 71-43-20.50 1
Bromobenzene <0.50 ug/L 05/10/15 18:55 108-86-10.50 1
Bromochloromethane <0.50 ug/L 05/10/15 18:55 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 05/10/15 18:55 75-27-40.50 1
Bromoform <0.50 ug/L 05/10/15 18:55 75-25-20.50 1
Bromomethane <5.0 ug/L 05/10/15 18:55 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 05/10/15 18:55 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 05/10/15 18:55 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 05/10/15 18:55 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 05/10/15 18:55 56-23-50.50 1
Chlorobenzene <0.50 ug/L 05/10/15 18:55 108-90-70.50 1
Chloroethane <1.0 ug/L 05/10/15 18:55 75-00-31.0 1
Chloroform <0.50 ug/L 05/10/15 18:55 67-66-30.50 1
Chloromethane <1.0 ug/L 05/10/15 18:55 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 05/10/15 18:55 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 05/10/15 18:55 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 05/10/15 18:55 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 05/10/15 18:55 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 05/10/15 18:55 106-93-40.50 1
Dibromomethane <0.50 ug/L 05/10/15 18:55 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 05/10/15 18:55 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 05/10/15 18:55 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 05/10/15 18:55 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 05/10/15 18:55 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 05/10/15 18:55 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 05/10/15 18:55 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 05/10/15 18:55 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 05/10/15 18:55 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 05/10/15 18:55 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 05/10/15 18:55 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 05/10/15 18:55 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 05/10/15 18:55 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 05/10/15 18:55 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 05/10/15 18:55 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 05/10/15 18:55 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 05/10/15 18:55 108-20-30.50 1
Ethylbenzene <0.50 ug/L 05/10/15 18:55 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 05/10/15 18:55 87-68-32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 05/10/15 18:55 98-82-80.50 1
Methylene Chloride <2.0 ug/L 05/10/15 18:55 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 05/10/15 18:55 1634-04-40.50 1
Naphthalene <2.0 ug/L 05/10/15 18:55 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 05/10/15 18:55 103-65-10.50 1
Styrene <0.50 ug/L 05/10/15 18:55 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 05/10/15 18:55 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 05/10/15 18:55 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 05/10/15 18:55 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-3 Lab ID:92247831008 Collected:04/29/15 17:00 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 05/10/15 18:55 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 05/10/15 18:55 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 05/10/15 18:55 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 05/10/15 18:55 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 05/10/15 18:55 79-00-50.50 1
Trichloroethene <0.50 ug/L 05/10/15 18:55 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 05/10/15 18:55 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 05/10/15 18:55 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/10/15 18:55 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 18:55 108-67-80.50 1
Vinyl chloride <1.0 ug/L 05/10/15 18:55 75-01-41.0 1
m&p-Xylene <1.0 ug/L 05/10/15 18:55 179601-23-11.0 1
o-Xylene <0.50 ug/L 05/10/15 18:55 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %05/10/15 18:55 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %05/10/15 18:55 460-00-470-130 1
Toluene-d8 (S)100 %05/10/15 18:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-5 Lab ID:92247831009 Collected:04/29/15 16:35 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 05/10/15 19:11 71-43-20.50 1
Bromobenzene <0.50 ug/L 05/10/15 19:11 108-86-10.50 1
Bromochloromethane <0.50 ug/L 05/10/15 19:11 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 05/10/15 19:11 75-27-40.50 1
Bromoform <0.50 ug/L 05/10/15 19:11 75-25-20.50 1
Bromomethane <5.0 ug/L 05/10/15 19:11 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 05/10/15 19:11 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 05/10/15 19:11 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 05/10/15 19:11 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 05/10/15 19:11 56-23-50.50 1
Chlorobenzene <0.50 ug/L 05/10/15 19:11 108-90-70.50 1
Chloroethane <1.0 ug/L 05/10/15 19:11 75-00-31.0 1
Chloroform <0.50 ug/L 05/10/15 19:11 67-66-30.50 1
Chloromethane <1.0 ug/L 05/10/15 19:11 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 05/10/15 19:11 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 05/10/15 19:11 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 05/10/15 19:11 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 05/10/15 19:11 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 05/10/15 19:11 106-93-40.50 1
Dibromomethane <0.50 ug/L 05/10/15 19:11 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 05/10/15 19:11 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 05/10/15 19:11 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 05/10/15 19:11 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 05/10/15 19:11 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 05/10/15 19:11 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 05/10/15 19:11 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 05/10/15 19:11 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 05/10/15 19:11 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 05/10/15 19:11 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 05/10/15 19:11 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 05/10/15 19:11 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 05/10/15 19:11 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 05/10/15 19:11 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 05/10/15 19:11 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 05/10/15 19:11 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 05/10/15 19:11 108-20-30.50 1
Ethylbenzene <0.50 ug/L 05/10/15 19:11 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 05/10/15 19:11 87-68-32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 05/10/15 19:11 98-82-80.50 1
Methylene Chloride <2.0 ug/L 05/10/15 19:11 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 05/10/15 19:11 1634-04-40.50 1
Naphthalene <2.0 ug/L 05/10/15 19:11 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 05/10/15 19:11 103-65-10.50 1
Styrene <0.50 ug/L 05/10/15 19:11 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 05/10/15 19:11 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 05/10/15 19:11 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 05/10/15 19:11 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-5 Lab ID:92247831009 Collected:04/29/15 16:35 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 05/10/15 19:11 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 05/10/15 19:11 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 05/10/15 19:11 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 05/10/15 19:11 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 05/10/15 19:11 79-00-50.50 1
Trichloroethene <0.50 ug/L 05/10/15 19:11 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 05/10/15 19:11 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 05/10/15 19:11 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/10/15 19:11 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 19:11 108-67-80.50 1
Vinyl chloride <1.0 ug/L 05/10/15 19:11 75-01-41.0 1
m&p-Xylene <1.0 ug/L 05/10/15 19:11 179601-23-11.0 1
o-Xylene <0.50 ug/L 05/10/15 19:11 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %05/10/15 19:11 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %05/10/15 19:11 460-00-470-130 1
Toluene-d8 (S)99 %05/10/15 19:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-6 Lab ID:92247831010 Collected:04/29/15 16:10 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 05/10/15 19:28 71-43-20.50 1
Bromobenzene <0.50 ug/L 05/10/15 19:28 108-86-10.50 1
Bromochloromethane <0.50 ug/L 05/10/15 19:28 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 05/10/15 19:28 75-27-40.50 1
Bromoform <0.50 ug/L 05/10/15 19:28 75-25-20.50 1
Bromomethane <5.0 ug/L 05/10/15 19:28 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 05/10/15 19:28 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 05/10/15 19:28 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 05/10/15 19:28 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 05/10/15 19:28 56-23-50.50 1
Chlorobenzene <0.50 ug/L 05/10/15 19:28 108-90-70.50 1
Chloroethane <1.0 ug/L 05/10/15 19:28 75-00-31.0 1
Chloroform <0.50 ug/L 05/10/15 19:28 67-66-30.50 1
Chloromethane <1.0 ug/L 05/10/15 19:28 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 05/10/15 19:28 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 05/10/15 19:28 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 05/10/15 19:28 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 05/10/15 19:28 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 05/10/15 19:28 106-93-40.50 1
Dibromomethane <0.50 ug/L 05/10/15 19:28 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 05/10/15 19:28 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 05/10/15 19:28 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 05/10/15 19:28 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 05/10/15 19:28 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 05/10/15 19:28 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 05/10/15 19:28 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 05/10/15 19:28 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 05/10/15 19:28 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 05/10/15 19:28 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 05/10/15 19:28 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 05/10/15 19:28 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 05/10/15 19:28 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 05/10/15 19:28 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 05/10/15 19:28 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 05/10/15 19:28 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 05/10/15 19:28 108-20-30.50 1
Ethylbenzene <0.50 ug/L 05/10/15 19:28 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 05/10/15 19:28 87-68-32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 05/10/15 19:28 98-82-80.50 1
Methylene Chloride <2.0 ug/L 05/10/15 19:28 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 05/10/15 19:28 1634-04-40.50 1
Naphthalene <2.0 ug/L 05/10/15 19:28 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 05/10/15 19:28 103-65-10.50 1
Styrene <0.50 ug/L 05/10/15 19:28 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 05/10/15 19:28 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 05/10/15 19:28 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 05/10/15 19:28 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92247831
C&W MARKET
Sample:WSW-6 Lab ID:92247831010 Collected:04/29/15 16:10 Received:04/30/15 16:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 05/10/15 19:28 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 05/10/15 19:28 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 05/10/15 19:28 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 05/10/15 19:28 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 05/10/15 19:28 79-00-50.50 1
Trichloroethene <0.50 ug/L 05/10/15 19:28 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 05/10/15 19:28 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 05/10/15 19:28 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 05/10/15 19:28 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 05/10/15 19:28 108-67-80.50 1
Vinyl chloride <1.0 ug/L 05/10/15 19:28 75-01-41.0 1
m&p-Xylene <1.0 ug/L 05/10/15 19:28 179601-23-11.0 1
o-Xylene <0.50 ug/L 05/10/15 19:28 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %05/10/15 19:28 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %05/10/15 19:28 460-00-470-130 1
Toluene-d8 (S)101 %05/10/15 19:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92247831
C&W MARKET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31540
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92247831001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1454146
Associated Lab Samples:92247831001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 05/09/15 13:16
1,1,1-Trichloroethane ug/L <0.50 0.50 05/09/15 13:16
1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 05/09/15 13:16
1,1,2-Trichloroethane ug/L <0.50 0.50 05/09/15 13:16
1,1-Dichloroethane ug/L <0.50 0.50 05/09/15 13:16
1,1-Dichloroethene ug/L <0.50 0.50 05/09/15 13:16
1,1-Dichloropropene ug/L <0.50 0.50 05/09/15 13:16
1,2,3-Trichlorobenzene ug/L <2.0 2.0 05/09/15 13:16
1,2,3-Trichloropropane ug/L <0.50 0.50 05/09/15 13:16
1,2,4-Trichlorobenzene ug/L <2.0 2.0 05/09/15 13:16
1,2,4-Trimethylbenzene ug/L <0.50 0.50 05/09/15 13:16
1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 05/09/15 13:16
1,2-Dibromoethane (EDB)ug/L <0.50 0.50 05/09/15 13:16
1,2-Dichlorobenzene ug/L <0.50 0.50 05/09/15 13:16
1,2-Dichloroethane ug/L <0.50 0.50 05/09/15 13:16
1,2-Dichloropropane ug/L <0.50 0.50 05/09/15 13:16
1,3,5-Trimethylbenzene ug/L <0.50 0.50 05/09/15 13:16
1,3-Dichlorobenzene ug/L <0.50 0.50 05/09/15 13:16
1,3-Dichloropropane ug/L <0.50 0.50 05/09/15 13:16
1,4-Dichlorobenzene ug/L <0.50 0.50 05/09/15 13:16
2,2-Dichloropropane ug/L <0.50 0.50 05/09/15 13:16
2-Chlorotoluene ug/L <0.50 0.50 05/09/15 13:16
4-Chlorotoluene ug/L <0.50 0.50 05/09/15 13:16
Benzene ug/L <0.50 0.50 05/09/15 13:16
Bromobenzene ug/L <0.50 0.50 05/09/15 13:16
Bromochloromethane ug/L <0.50 0.50 05/09/15 13:16
Bromodichloromethane ug/L <0.50 0.50 05/09/15 13:16
Bromoform ug/L <0.50 0.50 05/09/15 13:16
Bromomethane ug/L <5.0 5.0 05/09/15 13:16
Carbon tetrachloride ug/L <0.50 0.50 05/09/15 13:16
Chlorobenzene ug/L <0.50 0.50 05/09/15 13:16
Chloroethane ug/L <1.0 1.0 05/09/15 13:16
Chloroform ug/L <0.50 0.50 05/09/15 13:16
Chloromethane ug/L <1.0 1.0 05/09/15 13:16
cis-1,2-Dichloroethene ug/L <0.50 0.50 05/09/15 13:16
cis-1,3-Dichloropropene ug/L <0.50 0.50 05/09/15 13:16
Dibromochloromethane ug/L <0.50 0.50 05/09/15 13:16
Dibromomethane ug/L <0.50 0.50 05/09/15 13:16
Dichlorodifluoromethane ug/L <0.50 0.50 05/09/15 13:16
Diisopropyl ether ug/L <0.50 0.50 05/09/15 13:16
Ethylbenzene ug/L <0.50 0.50 05/09/15 13:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92247831
C&W MARKET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1454146
Associated Lab Samples:92247831001
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L <2.0 2.0 05/09/15 13:16
Isopropylbenzene (Cumene)ug/L <0.50 0.50 05/09/15 13:16
m&p-Xylene ug/L <1.0 1.0 05/09/15 13:16
Methyl-tert-butyl ether ug/L <0.50 0.50 05/09/15 13:16
Methylene Chloride ug/L <2.0 2.0 05/09/15 13:16
n-Butylbenzene ug/L <0.50 0.50 05/09/15 13:16
n-Propylbenzene ug/L <0.50 0.50 05/09/15 13:16
Naphthalene ug/L <2.0 2.0 05/09/15 13:16
o-Xylene ug/L <0.50 0.50 05/09/15 13:16
sec-Butylbenzene ug/L <0.50 0.50 05/09/15 13:16
Styrene ug/L <0.50 0.50 05/09/15 13:16
tert-Butylbenzene ug/L <0.50 0.50 05/09/15 13:16
Tetrachloroethene ug/L <0.50 0.50 05/09/15 13:16
Toluene ug/L 0.76 0.50 05/09/15 13:16
trans-1,2-Dichloroethene ug/L <0.50 0.50 05/09/15 13:16
trans-1,3-Dichloropropene ug/L <0.50 0.50 05/09/15 13:16
Trichloroethene ug/L <0.50 0.50 05/09/15 13:16
Trichlorofluoromethane ug/L <1.0 1.0 05/09/15 13:16
Vinyl chloride ug/L <1.0 1.0 05/09/15 13:16
1,2-Dichloroethane-d4 (S)%100 70-130 05/09/15 13:16
4-Bromofluorobenzene (S)%96 70-130 05/09/15 13:16
Toluene-d8 (S)%99 70-130 05/09/15 13:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1454147LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.950 108 60-140
1,1,1-Trichloroethane ug/L 51.050 102 60-140
1,1,2,2-Tetrachloroethane ug/L 49.850 100 60-140
1,1,2-Trichloroethane ug/L 50.650 101 60-140
1,1-Dichloroethane ug/L 52.550 105 60-140
1,1-Dichloroethene ug/L 49.350 99 60-140
1,1-Dichloropropene ug/L 57.250 114 60-140
1,2,3-Trichlorobenzene ug/L 51.150 102 60-140
1,2,3-Trichloropropane ug/L 50.950 102 60-140
1,2,4-Trichlorobenzene ug/L 50.850 102 60-140
1,2,4-Trimethylbenzene ug/L 53.450 107 60-140
1,2-Dibromo-3-chloropropane ug/L 57.750 115 60-140
1,2-Dibromoethane (EDB)ug/L 51.750 103 60-140
1,2-Dichlorobenzene ug/L 50.750 101 60-140
1,2-Dichloroethane ug/L 47.050 94 60-140
1,2-Dichloropropane ug/L 51.950 104 60-140
1,3,5-Trimethylbenzene ug/L 52.350 105 60-140
1,3-Dichlorobenzene ug/L 50.050 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92247831
C&W MARKET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1454147LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 49.750 99 60-140
1,4-Dichlorobenzene ug/L 48.650 97 60-140
2,2-Dichloropropane ug/L 53.250 106 60-140
2-Chlorotoluene ug/L 50.950 102 60-140
4-Chlorotoluene ug/L 51.150 102 60-140
Benzene ug/L 50.350 101 60-140
Bromobenzene ug/L 53.650 107 60-140
Bromochloromethane ug/L 51.850 104 60-140
Bromodichloromethane ug/L 49.350 99 60-140
Bromoform ug/L 44.750 89 60-140
Bromomethane ug/L 46.650 93 60-140
Carbon tetrachloride ug/L 53.050 106 60-140
Chlorobenzene ug/L 49.250 98 60-140
Chloroethane ug/L 51.550 103 60-140
Chloroform ug/L 45.850 92 60-140
Chloromethane ug/L 48.550 97 60-140
cis-1,2-Dichloroethene ug/L 51.450 103 60-140
cis-1,3-Dichloropropene ug/L 56.250 112 60-140
Dibromochloromethane ug/L 52.250 104 60-140
Dibromomethane ug/L 48.850 98 60-140
Dichlorodifluoromethane ug/L 53.750 107 60-140
Diisopropyl ether ug/L 51.350 103 60-140
Ethylbenzene ug/L 50.250 100 60-140
Hexachloro-1,3-butadiene ug/L 53.950 108 60-140
Isopropylbenzene (Cumene)ug/L 53.650 107 60-140
m&p-Xylene ug/L 99.9100 100 60-140
Methyl-tert-butyl ether ug/L 50.650 101 60-140
Methylene Chloride ug/L 55.350 111 60-140
n-Butylbenzene ug/L 54.050 108 60-140
n-Propylbenzene ug/L 51.450 103 60-140
Naphthalene ug/L 52.850 106 60-140
o-Xylene ug/L 50.150 100 60-140
sec-Butylbenzene ug/L 55.950 112 60-140
Styrene ug/L 53.250 106 60-140
tert-Butylbenzene ug/L 45.550 91 60-140
Tetrachloroethene ug/L 49.350 99 60-140
Toluene ug/L 49.950 100 60-140
trans-1,2-Dichloroethene ug/L 50.850 102 60-140
trans-1,3-Dichloropropene ug/L 56.950 114 60-140
Trichloroethene ug/L 46.350 93 60-140
Trichlorofluoromethane ug/L 49.950 100 60-140
Vinyl chloride ug/L 51.150 102 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92247831
C&W MARKET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/31570
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92247831002, 92247831003, 92247831004, 92247831005, 92247831006, 92247831007, 92247831008,
92247831009, 92247831010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455197
Associated Lab Samples:92247831002, 92247831003, 92247831004, 92247831005, 92247831006, 92247831007, 92247831008,
92247831009, 92247831010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 05/10/15 15:20
1,1,1-Trichloroethane ug/L <0.50 0.50 05/10/15 15:20
1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 05/10/15 15:20
1,1,2-Trichloroethane ug/L <0.50 0.50 05/10/15 15:20
1,1-Dichloroethane ug/L <0.50 0.50 05/10/15 15:20
1,1-Dichloroethene ug/L <0.50 0.50 05/10/15 15:20
1,1-Dichloropropene ug/L <0.50 0.50 05/10/15 15:20
1,2,3-Trichlorobenzene ug/L <2.0 2.0 05/10/15 15:20
1,2,3-Trichloropropane ug/L <0.50 0.50 05/10/15 15:20
1,2,4-Trichlorobenzene ug/L <2.0 2.0 05/10/15 15:20
1,2,4-Trimethylbenzene ug/L <0.50 0.50 05/10/15 15:20
1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 05/10/15 15:20
1,2-Dibromoethane (EDB)ug/L <0.50 0.50 05/10/15 15:20
1,2-Dichlorobenzene ug/L <0.50 0.50 05/10/15 15:20
1,2-Dichloroethane ug/L <0.50 0.50 05/10/15 15:20
1,2-Dichloropropane ug/L <0.50 0.50 05/10/15 15:20
1,3,5-Trimethylbenzene ug/L <0.50 0.50 05/10/15 15:20
1,3-Dichlorobenzene ug/L <0.50 0.50 05/10/15 15:20
1,3-Dichloropropane ug/L <0.50 0.50 05/10/15 15:20
1,4-Dichlorobenzene ug/L <0.50 0.50 05/10/15 15:20
2,2-Dichloropropane ug/L <0.50 0.50 05/10/15 15:20
2-Chlorotoluene ug/L <0.50 0.50 05/10/15 15:20
4-Chlorotoluene ug/L <0.50 0.50 05/10/15 15:20
Benzene ug/L <0.50 0.50 05/10/15 15:20
Bromobenzene ug/L <0.50 0.50 05/10/15 15:20
Bromochloromethane ug/L <0.50 0.50 05/10/15 15:20
Bromodichloromethane ug/L <0.50 0.50 05/10/15 15:20
Bromoform ug/L <0.50 0.50 05/10/15 15:20
Bromomethane ug/L <5.0 5.0 05/10/15 15:20
Carbon tetrachloride ug/L <0.50 0.50 05/10/15 15:20
Chlorobenzene ug/L <0.50 0.50 05/10/15 15:20
Chloroethane ug/L <1.0 1.0 05/10/15 15:20
Chloroform ug/L <0.50 0.50 05/10/15 15:20
Chloromethane ug/L <1.0 1.0 05/10/15 15:20
cis-1,2-Dichloroethene ug/L <0.50 0.50 05/10/15 15:20
cis-1,3-Dichloropropene ug/L <0.50 0.50 05/10/15 15:20
Dibromochloromethane ug/L <0.50 0.50 05/10/15 15:20
Dibromomethane ug/L <0.50 0.50 05/10/15 15:20
Dichlorodifluoromethane ug/L <0.50 0.50 05/10/15 15:20
Diisopropyl ether ug/L <0.50 0.50 05/10/15 15:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92247831
C&W MARKET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1455197
Associated Lab Samples:92247831002, 92247831003, 92247831004, 92247831005, 92247831006, 92247831007, 92247831008,
92247831009, 92247831010
Matrix:Water
Analyzed
Ethylbenzene ug/L <0.50 0.50 05/10/15 15:20
Hexachloro-1,3-butadiene ug/L <2.0 2.0 05/10/15 15:20
Isopropylbenzene (Cumene)ug/L <0.50 0.50 05/10/15 15:20
m&p-Xylene ug/L <1.0 1.0 05/10/15 15:20
Methyl-tert-butyl ether ug/L <0.50 0.50 05/10/15 15:20
Methylene Chloride ug/L <2.0 2.0 05/10/15 15:20
n-Butylbenzene ug/L <0.50 0.50 05/10/15 15:20
n-Propylbenzene ug/L <0.50 0.50 05/10/15 15:20
Naphthalene ug/L <2.0 2.0 05/10/15 15:20
o-Xylene ug/L <0.50 0.50 05/10/15 15:20
sec-Butylbenzene ug/L <0.50 0.50 05/10/15 15:20
Styrene ug/L <0.50 0.50 05/10/15 15:20
tert-Butylbenzene ug/L <0.50 0.50 05/10/15 15:20
Tetrachloroethene ug/L <0.50 0.50 05/10/15 15:20
Toluene ug/L <0.50 0.50 05/10/15 15:20
trans-1,2-Dichloroethene ug/L <0.50 0.50 05/10/15 15:20
trans-1,3-Dichloropropene ug/L <0.50 0.50 05/10/15 15:20
Trichloroethene ug/L <0.50 0.50 05/10/15 15:20
Trichlorofluoromethane ug/L <1.0 1.0 05/10/15 15:20
Vinyl chloride ug/L <1.0 1.0 05/10/15 15:20
1,2-Dichloroethane-d4 (S)%102 70-130 05/10/15 15:20
4-Bromofluorobenzene (S)%98 70-130 05/10/15 15:20
Toluene-d8 (S)%99 70-130 05/10/15 15:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455198LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.450 107 60-140
1,1,1-Trichloroethane ug/L 48.850 98 60-140
1,1,2,2-Tetrachloroethane ug/L 49.450 99 60-140
1,1,2-Trichloroethane ug/L 50.350 101 60-140
1,1-Dichloroethane ug/L 50.750 101 60-140
1,1-Dichloroethene ug/L 48.050 96 60-140
1,1-Dichloropropene ug/L 55.950 112 60-140
1,2,3-Trichlorobenzene ug/L 49.050 98 60-140
1,2,3-Trichloropropane ug/L 51.250 102 60-140
1,2,4-Trichlorobenzene ug/L 49.650 99 60-140
1,2,4-Trimethylbenzene ug/L 51.150 102 60-140
1,2-Dibromo-3-chloropropane ug/L 57.050 114 60-140
1,2-Dibromoethane (EDB)ug/L 51.850 104 60-140
1,2-Dichlorobenzene ug/L 48.750 97 60-140
1,2-Dichloroethane ug/L 45.950 92 60-140
1,2-Dichloropropane ug/L 51.050 102 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92247831
C&W MARKET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1455198LABORATORY CONTROL SAMPLE:
LCSSpike
1,3,5-Trimethylbenzene ug/L 50.850 102 60-140
1,3-Dichlorobenzene ug/L 48.250 96 60-140
1,3-Dichloropropane ug/L 50.850 102 60-140
1,4-Dichlorobenzene ug/L 47.150 94 60-140
2,2-Dichloropropane ug/L 51.450 103 60-140
2-Chlorotoluene ug/L 48.850 98 60-140
4-Chlorotoluene ug/L 48.950 98 60-140
Benzene ug/L 49.650 99 60-140
Bromobenzene ug/L 46.850 94 60-140
Bromochloromethane ug/L 49.350 99 60-140
Bromodichloromethane ug/L 48.650 97 60-140
Bromoform ug/L 45.650 91 60-140
Bromomethane ug/L 47.150 94 60-140
Carbon tetrachloride ug/L 51.850 104 60-140
Chlorobenzene ug/L 48.350 97 60-140
Chloroethane ug/L 48.850 98 60-140
Chloroform ug/L 44.550 89 60-140
Chloromethane ug/L 49.050 98 60-140
cis-1,2-Dichloroethene ug/L 50.150 100 60-140
cis-1,3-Dichloropropene ug/L 56.050 112 60-140
Dibromochloromethane ug/L 52.750 105 60-140
Dibromomethane ug/L 47.850 96 60-140
Dichlorodifluoromethane ug/L 48.950 98 60-140
Diisopropyl ether ug/L 50.550 101 60-140
Ethylbenzene ug/L 49.550 99 60-140
Hexachloro-1,3-butadiene ug/L 50.650 101 60-140
Isopropylbenzene (Cumene)ug/L 53.650 107 60-140
m&p-Xylene ug/L 98.3100 98 60-140
Methyl-tert-butyl ether ug/L 49.650 99 60-140
Methylene Chloride ug/L 52.650 105 60-140
n-Butylbenzene ug/L 53.650 107 60-140
n-Propylbenzene ug/L 49.850 100 60-140
Naphthalene ug/L 51.650 103 60-140
o-Xylene ug/L 49.750 99 60-140
sec-Butylbenzene ug/L 54.850 110 60-140
Styrene ug/L 52.550 105 60-140
tert-Butylbenzene ug/L 44.050 88 60-140
Tetrachloroethene ug/L 48.250 96 60-140
Toluene ug/L 48.650 97 60-140
trans-1,2-Dichloroethene ug/L 48.750 97 60-140
trans-1,3-Dichloropropene ug/L 56.350 113 60-140
Trichloroethene ug/L 46.150 92 60-140
Trichlorofluoromethane ug/L 47.850 96 60-140
Vinyl chloride ug/L 49.650 99 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92247831
C&W MARKET
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than
the blank or were below the reporting limit.P8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92247831
C&W MARKET
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92247831001 MSV/31540MW-1R SM 6200B
92247831002 MSV/31570MW-3 SM 6200B
92247831003 MSV/31570MW-4 SM 6200B
92247831004 MSV/31570MW-5 SM 6200B
92247831005 MSV/31570TW-1 SM 6200B
92247831006 MSV/31570WSW-1 SM 6200B
92247831007 MSV/31570WSW-2 SM 6200B
92247831008 MSV/31570WSW-3 SM 6200B
92247831009 MSV/31570WSW-5 SM 6200B
92247831010 MSV/31570WSW-6 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/11/2015 03:38 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 35
Page 34 of 35
Page 35 of 35
APPENDIXIII
Photographs
TF-17513 Former C&H Market
Project#: 4358-15-045
Sheet1of2 3718 Old Battleground Rd.
Greensboro, NC 27410
Source:GoogleMaps1
Location / Orientation Toward the northeast
Remarks Site
Source:GoogleMaps2
Location / Orientation Toward the southwest
Remarks Site
TF-17513 Former C&H Market
Project#: 4358-15-045
Sheet2of2 3718 Old Battleground Rd.
Greensboro, NC 27410
Source:GoogleMaps3
Location / Orientation Toward the east
Remarks Site
Source:GoogleMaps4
Location / Orientation Toward the south
Remarks Site