19019-Hillsborough Square-Beneficial Use Soil Assessment Report-20200211

Mid Atlantic
Engineering & Environmental Solutions
February 11, 2020
Ms. Joselyn Harriger
NC Brownfields Program
NC Department of Environmental Quality
Division of Waste Management
Mail Service Center 1646
Raleigh, NC 27699-1646
Reference: BENEFICIAL USE SOIL ASSESSMENT REPORT
409 Rogers View Court
Raleigh, NC 27610
office 919.250.9918
facsimile 919.250.9950
MAAONLINE.COM
HILLSBOROUGH SQUARE AND POWERHOUSE SQUARE
404, 406, AND 414 HILLSBOROUGH ST., 11 AND 15 N. HARRINGTON
ST.; 409 EDENTON ST., AND 505 AND 513 W. JONES ST.
RALEIGH, WAKE COUNTY, NORTH CAROLINA
BROWNFIELDS PROJECT NOS.: 19019-15-092 AND 18026-14-092
MID -ATLANTIC JOB NO. OOOR2650.02
MID -ATLANTIC PE LICENSE NO.: F-0967
Dear Ms. Harriger:
On behalf of TC MidAtlantic Development II, Inc., we are pleased to present this Beneficial
Use Soil Assessment Report for the above -referenced site. Please contact me at 919-
250-9918 if any questions arise or if we may be of further service.
Sincerely,
MID -ATLANTIC ASSOCIATES, INC.
a 4"x
Katie A. Lippard
Senior Project Manager
Enclosure
EXPERIENCED CUSTOMER FOCUSED INNOVATIVE

BENEFICIAL USE SOIL ASSESSMENT REPORT
HILLSBOROUGH SQUARE AND POWERHOUSE SQUARE
4043 406, AND 414 HILLSBOROUGH ST., 11 AND 15 N. HARRINGTON
ST.; 409 EDENTON ST., AND 505 AND 513 W. JONES ST.
RALEIGH, WAKE COUNTY, NORTH CAROLINA
BROWNFIELDS PROJECT NOS.: 19019-15-092 AND 18026-14-092
Prepared For:
Mr. Jerry Ricciardi
TC MidAtlantic Development II, Inc.
1055 Thomas Jefferson Street, NW, Suite 600
Washington, DC 20007
Prepared By:
Mid -Atlantic Associates, Inc.
409 Rogers View Court
Raleigh, North Carolina 27610
Mid -Atlantic Associates, Inc. Job No. OOOR2650.02
Mid -Atlantic PE License No: F-0967
February 11, 2020
5 Atlantic

Ml*
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lc
Engineering & Environmental Solutions
409 Rogers View Court
Raleigh, NC 276 10
office 919.250.9918
facsimile 919.250.9950
MAAONLINE.COM
BENEFICIAL USE SOIL ASSESSMENT REPORT
HILLSBOROUGH SQUARE AND POWERHOUSE SQUARE
4041406, AND 414 HILLSBOROUGH ST., 11 AND 15 N. HARRINGTON
ST.; 409 EDENTON ST., AND 505 AND 513 W. JONES ST.
RALEIGH, WAKE COUNTY, NORTH CAROLINA
BROWNFIELDS PROJECT NOS.: 19019-15-092 AND 18026-14-092
Mid -Atlantic Associated, Inc. Job No. 00OR2650.02
Mid -Atlantic PE License No: F-0967
February 11, 2020
Prepared For:
Mr. Jerry Ricciardi
TC MidAtlantic Development II, Inc.
1055 Thomas Jefferson Street, NW,
Suite 600
Washington, DC 20007
Prepared By:
MID -ATLANTIC ASSOCIATES, INC.
C
F
NCPE License No.
18967
EXPERIENCED CUSTOMER FOCUSED INNOVATIVE

TABLE OF CONTENTS
1.0 INTRODUCTION.....................................................................................................1
2.0 SUMMARY OF FIELD ACTIVITIES........................................................................2
2.1 Utility Clearance and Sampling Location Siting .................................................... 2
2.2 Soil Boring and Sampling..................................................................................... 2
3.0 SUMMARY OF LABORATORY ANALYTICAL RESULTS....................................4
4.0 CONCLUSIONS AND RECOMMENDATIONS....................................................... 5
DRAWINGS
Drawing 1 Topographic Site Map
Drawing 2 Site Map
Drawing 3 Soil Sample Location Map
TABLES
Table 1 Beneficial Use Soil Assessment Sampling Detail
Table 2 Summary of Assessment Soil Sample Analysis
APPENDICES
Appendix A Boring Logs
Appendix B Laboratory Analytical Report and Chain of Custody Record for Soil
Samples
Mid Atlantic

1.0 INTRODUCTION
The subject site is comprised of seven parcels (P1 through P7) totaling 1.16 acres located
in a historic district west of downtown Raleigh, North Carolina (Drawings 1 and 2). The site
has historically been used for commercial and mixed -use purposes and is currently vacant.
The subject site is developed with five of the seven parcels containing masonry block
structures. Four buildings, located in the southern portion of the site on parcels P1 through
P6 (Hillsborough Square site), are enclosed and total approximately 34,349 square feet.
The fifth building is the Powerhouse Square parking structure located on the northwest
parcel (P7) of the subject site. The six parcels on the east side of North West Street, (P1
through P6), are about to undergo redevelopment with a mix of retail, office and residential.
As part of the redevelopment activities on parcels P1 through P6, significant portions of the
site will require soil excavation. Approximately 10,580 cubic yards is planned to be
excavated during redevelopment. An additional volume of soil will be produced during pile
cap excavation and auger cast drilling. The pile cap excavation and drilling spoil volume is
currently estimated to be approximately 1,800 cubic yards. This material is planned to
remain on -site and be used as backfill during redevelopment activities. Therefore, sampling
of this material was not included in this assessment. Management of these soils will be
included the Environmental Management Plan (EMP) that will be prepared for this site.
Subsurface disturbance on parcel P7, containing the Powerhouse Square parking structure,
will be minimal. Redevelopment activities on this parcel include the addition of an elevator
lobby and stairs. Soil volume removal is estimated be approximately 30 yards or less,
although design plans for redevelopment on this parcel are not finalized. Based on the
minimal amount of soil removal anticipated, sampling of this material was not included as
part of this assessment.
The objective of this assessment is to help outline environmental activities required prior
to commencing redevelopment at the subject site. Plans for this assessment were
detailed in a Beneficial Use Soil Assessment Work Plan dated November 13, 2019 and
approved by the North Carolina Brownfields Program (NCBP) on November 22, 2019.
This assessment scope of work included a comprehensive grid -based soil sampling
regime (Drawing 3) to assess the soils targeted for excavation on parcels P1 through P6
during redevelopment of the site. The grid pattern of assessment was intended to provide
an unbiased assessment of the site where soil cuts are anticipated and to characterize
the soil that may be exported from the site (potential beneficial fill). The findings from this
assessment will be used to better define the area targeted for soil removal and support
the EMP development. The remainder of this report details the soil assessment
conducted at the site from January 6 through 8, 2020. The assessment was conducted in
accordance with the November 2019 work plan, with the exception of sampling locations
that were off -set by up to 12 feet from the proposed locations in some areas due to site
constraints, and the addition of one soil sample location.
The opinions included herein are based on our experience and the information obtained
during the study. This report is based on limited observations made on the dates noted
Mid Atlantic

Beneficial Use Soil Assessment Report
Hillsborough Square and Powerhouse Square
Raleigh, North Carolina
February 11, 2020
Page 2
using the procedures described herein. If additional information becomes available, we
request the opportunity to review the information, reassess the potential environmental
concerns and modify our conclusions and recommendations, if appropriate.
2.0 SUMMARY OF FIELD ACTIVITIES
2.1 Utility Clearance and Sampling Location Siting
Prior to commencing field activities at the site, several tasks were accomplished in
preparation for the assessment. A Health and Safety Plan (HASP) was prepared to
include site -specific health information necessary for the field activities. North Carolina -
One -Call (811) was contacted on December 20, 2019 to report the proposed assessment
activities and subsequently notify all affected public utilities. On January 6, 2020, private
utilities were located and marked by KCI Associates of North Carolina (KCI) in the areas of
the proposed sampling locations. The final locations of the soil borings were placed to avoid
the marked utilities and to be situated as close to the proposed sampling locations as could
safely be managed. Modifications from the proposed sampling plan include relocating
several soil borings up to twelve feet from their proposed locations due to site constraints
and proximity to utilities, and collection of an additional soil boring (B2-SB-6) within the
basement of one of the site buildings. Mid -Atlantic does not consider these modifications to
have adversely impacted the objective of this assessment.
2.2 Soil Boring and Sampling
On January 6 and 7, 2020, under the supervision of Mid -Atlantic, Quantex Inc. (Quantex)
used a Geoprobe 7822DT to advance 17 soil borings at the designated locations primarily
in the exterior portions of the site (Drawing 3). Each boring was advanced using
decontaminated equipment. Soil samples were collected via 5-foot macrocores for soil
characterization and laboratory analysis. Soil was screened for the presence of volatile
organic compounds (VOCs) using a photo ionization detector (PID).
From January 6 through 8, 2020, under the supervision of Mid -Atlantic, Environmental Field
Management, Inc. (EFM) used a coring machine to core through the building slab floors
and basement floors to gain access to site soils beneath the buildings on -site. Twenty-
one soil borings were advanced using a decontaminated hand auger bucket (Drawing 3).
Soil samples were collected from each boring for characterization and laboratory analysis.
Soil was screened for the presence of VOCs using a PID. Boring logs for both the Geoprobe
borings and hand augur borings are provided in Appendix A.
A total of nineteen composite soil samples and one duplicate sample were collected from
38 soil borings advanced in a variable grid pattern as illustrated on Drawing 3. The grid
pattern illustrates 12 blocks. Each block includes approximately 1,000 cubic yards of soil
Mid Atlantic

Beneficial Use Soil Assessment Report
Hillsborough Square and Powerhouse Square
Raleigh, North Carolina
February 11, 2020
Page 3
that is targeted for export. The area covered by each block varies with the approximate
depth of the cut in the block. Thus, shallow cuts have blocks that cover a larger area when
compared to blocks with deeper cuts. The soil within each block was assessed using
aliquot samples collected from two to six borings advanced within each block. For blocks
with cut depths extending to five feet below the surface, one sample was collected from
each boring (no vertical stratification). For the blocks where the borings extend from six
to twelve feet, shallow (0 to 5 feet) and deep (6 to 12 feet) strata were evaluated
separately. Soil cuttings from each soil boring were screened using a Photoionization
Detector (PID) to evaluate if VOCs were detected in soil during drilling activities. Soil
samples were collected in 5-foot (or less for more shallow borings) intervals using a
GeoProbe macrocore sampler and direct push technology. A longitudinally split portion
of each soil sample was removed from the sampling device (acetate sleeves from the
macrocore sampler) and placed in a pre -labeled, plastic "ziploc" bag. After several
minutes, the gas contained in the "headspace" or void area within the bag was screened
with a PID. The PID was also used for air monitoring in accordance with provisions in the
site health and safety plan (HASP). The soil samples collected for laboratory analysis
were removed from the acetate sleeve (not the ziploc bags) and placed directly into
laboratory supplied sample jars. Samples were collected from the default depths or from
the intervals where the highest PID readings were recorded. VOCs were not detected in
any of the soils screened with PID, with the exception of soils from boring 1312-SB-1 which
exhibited PID measurements ranging from 0.0 to 53.3 parts per million (ppm) and 1312-
SB-2 which exhibited PID measurements ranging from 0.0 to 0.4 ppm. Soil assessment
sampling depths and additional sampling details are provided in Table 1.
One grab sample from each block that exhibited the highest PID reading was collected
for analysis of VOCs. In blocks with multiple strata, this sampling approach was used for
each strata. One composite soil sample from each block, which was comprised of aliquot
samples collected from each boring within each block, was analyzed for semi-VOCs
(SVOCs) and eight RCRA metals. In blocks with multiple strata, this compositing sampling
approach was used for each strata.
Samples were submitted for laboratory analysis of VOCs by EPA Method 8260, SVOCs
by EPA Method 8270, eight RCRA metals using EPA Methods 6010 & 7471 (for mercury).
Approximately 10% of the composite soil samples containing the highest concentrations
of total chromium were submitted for analysis of hexavalent chromium using EPA Method
7199. One duplicate soil sample (Duplicate) was collected from composite soil sample 13-
12D, from the interval where the highest PID readings were recorded. Soil samples were
shipped to Waypoint Analytical (formerly Prism Laboratories) of Charlotte, North Carolina
for laboratory analysis as shown on the chain of custody record provided in Appendix B.
Mid Atlantic

Beneficial Use Soil Assessment Report February 11, 2020
Hillsborough Square and Powerhouse Square Page 4
Raleigh, North Carolina
3.0 SUMMARY OF LABORATORY ANALYTICAL RESULTS
Soil samples were compared to the Residential Preliminary Soil Remediation Goals
(PSRGs), the Protection of Groundwater PSRGs, and the Industrial PSRGs. As
summarized in Table 2, total chromium was detected in each of the composited soil
samples and the duplicate sample at concentrations exceeding the Residential,
Industrial/Commercial, and Protection of Groundwater PSRGs for total chromium, with
the exception of sample B-12D, where concentrations did not exceed the
Industrial/Commercial PSRGs. Three of the soil samples with the highest total chromium
concentrations [B-4D at 26 milligrams per kilogram (mg/kg), B-6S at 29 mg/kg, and B-7
at 27 mg/kg], making up 10% of the samples collected, were speciated for hexavalent
chromium and the concentrations were below the PSRGs. These speciation results
indicate the chromium concentrations identified in the soil samples consist primarily of
trivalent chromium. Neither the speciated hexavalent chromium concentrations nor the
remaining trivalent chromium concentrations identified in the samples exceed the PSRGs.
Arsenic was detected in 15 of the 19 composite soil samples collected with concentrations
ranging from an estimated concentration of 0.76 mg/kg to 3.9 mg/kg, exceeding either the
Residential and/or the Industrial/commercial PSRGs, but below the Protection of
Groundwater PSRG. Arsenic is a metal that is found naturally occurring in North Carolina
soils. According to the North Carolina Department of Agriculture and Consumer Services
(NCDA), an average concentration of 4.5 mg/Kg of arsenic was detected in laboratory
testing of 3,286 soil samples collected across North Carolina between 2005 and 2007
(NCDA, 2008). Furthermore, the EPA notes that arsenic concentrations typically range
from four to nine mg/Kg in most soils (EPA, 2003). According to the laboratory analysis,
the arsenic concentrations detected in the assessment samples collected from the subject
site fall within levels believed to be found naturally in North Carolina soils.
Additional metals including barium, cadmium, lead, and mercury were detected in some
or all of the composite soil samples and the duplicate sample at concentrations above
laboratory method detection limits but below the PSRGs.
As summarized in Table 2, benzo(a)pyrene was detected in composite soil samples B-3S
collected from the shallow strata of Block 3 and B-4D collected from the deep strata of Block
4 at estimated concentrations exceeding the Residential and the Protection of Groundwater
PSRGs, but below the Industrial/Commercial PSRG. Additional SVOCs were detected in
three of the composite soil samples at concentrations above laboratory method detection
limits but below the PSRGs. VOCs were detected in 13 of the 19 grab soil samples and the
duplicate at concentrations above laboratory method detection limits but below the PSRGs.
Mid Atlantic

Beneficial Use Soil Assessment Report February 11, 2020
Hillsborough Square and Powerhouse Square Page 5
Raleigh, North Carolina
4.0 CONCLUSIONS AND RECOMMENDATIONS
The objective of this assessment was to help outline environmental activities required
prior to commencing redevelopment at the subject site and to help in the preparation of
the site EMP. This assessment scope of work included a comprehensive grid -based soil
sampling regime to assess the soils targeted for excavation on parcels P1 through P6
during site redevelopment. The grid pattern of assessment was intended to provide an
unbiased assessment of the site where soil cuts are anticipated and to characterize the
soil that may be exported from the site (potential beneficial fill). Based on review of the
data collected during this assessment Mid -Atlantic concludes:
• With the exception of arsenic and total chromium detected in some or all of the
composited soil samples, soil quality in the cut areas of the subject site do not
exceed the PSRGs. The arsenic concentrations detected in composited soil
samples and the duplicate fall within levels believed to be found naturally in North
Carolina soils. Soil samples B-4D, B-6S and B-7 were speciated for hexavalent
chromium and the results are below the PSRGs;
• Samples B-3S and B-4D exhibited estimated concentrations of benzo(a)pyrene
slightly above the Residential and Protection of Groundwater PSRGs; and
• The average concentrations of benzo(a)pyrene over the approximately 0.25 acre
area that makes up Blocks 3, 4 and 9 are 0.094 mg/kg for the shallow strata, and
0.058 mg/kg for the deeper strata, both below the Residential and Protection of
Groundwater PSRGs.
Based on the totality of the data collected during this investigation, Mid -Atlantic
recommends that the soil planned for export at this site be treated as unrestricted
beneficial fill. Mid -Atlantic recommends submittal of this report to the NCBP for review.
Mid Atlantic

DRAWINGS
Mid Atlantic

a
REFERENCES:
1. RALEIGH WEST, NC DIGITAL RASTER GRAPHIC, USGS, 2013. SCANNED FROM
1:24,000-SCALE RALEIGH WEST, NC TOPOGRAPHIC MAP, PUBLISHED 2013, USGS.
2. INSET MAP DIGITAL DATA FROM 2002 NATIONAL TRANSPORTATION ATLAS,
BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, D.C.
3. PARCEL DATA FROM WAKE COUNTY GIS.
Mid Atlantic
Engineering & Environmental Solutions
TOPOGRAPHIC SITE MAP
HILLSBOROUGH SQUARE AND
POWERHOUSE SQUARE
400H OFFICE REDEVELOPMENT
HILLSBOROUGH ST. AT N. WEST ST
RALEIGH, NORTH CAROLINA
SCALE: 1:12,000
Feet
0 500 1,000 2,000
DRAWN
DATE:
BY: EBA
APRIL 2019
DRAFT
JOB NO:
CHECK:
OOOR2650.01
ENG.
GIS NO:
CHECK:
01 G-R2650.01-1
APPROVAL:
DWG NO: 1

REFERENCES:
1. 2017 AERIAL IMAGERY FROM NC ONE MAP. SCALE: 1 :1 ,800
2. PARCEL BOUNDARY AND ROAD DATA FROM
WAKE COUNTY GIS. 0 150 300
3. MID —ATLANTIC FIELD NOTES. Feet
SITE MAP DRAWN DATE:
BY: EBA APRIL 201
HILLSBOROUGH SQUARE AND DRAFT JOB NO:
Mid Atlantic POWERHOUSE SQUARE CHECK: OOOR2650.0
Engineering & Environmental Solutions 400H OFFICE REDEVELOPMENT ENG. GIS NO:
HILLSBOROUGH ST. AT N. WEST ST. CHECK: 01G—R2650.c
RALEIGH, NORTH CAROLINA APPROVAL: DWG NO: 2

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TABLES
Mid Atlantic

TABLE 1
BENEFICIAL USE SOIL ASSESSMENT SAMPLING DETAIL
HILLSBOROUGH SQUARE AND POWERHOUSE SQUARE
400H OFFICE REDEVELOPMENT
HILLSBOROUGH STREET AT N. WEST STREET
RALEIGH, NORTH CAROLINA
MID -ATLANTIC JOB NO. R2650.02
Approximate Depth of
Boring and
Boring Depth
Proposed Sample
Actual Sample
VOC Grab
Block
Location
Existing Surface Below
Approximate
3
Alliquote
Below Outside
Depth Below
Depth Below
Soil Sample Name
Sample
VOCs
SVOCs
Metals
Boring Advancement
Outside Grade (ft)
Volume yd
Sample Count
Grade (ft)
Outside Gradel (ft)
Outside Grade' (ft)
Location
Method
Parking Lot and
Parking Lot: 5
Parking Lot: 2
1
At Grade
950
5
2.5 - 9
B-1
Bl-SB-5
G
C
C
Geoprobe
Basement
Basement: 12
Basement:9
2
Basement
8
780
6
12
10
10
B-2
B2-SB-6
G
C
C
Hand Auger
3
Slab on Grade
At Grade
800
2
9
2
2
B-3s
B3-SB-2
G
C
C
Hand Auger
7
7
B-3d
B3-5B-2
G
C
C
4
Slab on Grade
At Grade
850
2
9
2
2
B-4s
B4-SB-2
G
C
C
Hand Auger
7
7
B-4d
B4-5B-2
G
C
C
5
Parking lot
At Grade
950
2
10
2
2
B-5s
B5-SB-2
G
C
C
Geoprobe
7
7
B-Sd
B5-5B-2
G
C
C
6
Parking lot
At Grade
970
2
10
3
3
B-6s
B6-SB-2
G
C
C
Geoprobe
5
5
B-6d
B6-5B-2
G
C
C
7
Parking lot
At Grade
995
4
10
3
3
B-7
B7-SB-4
G
C
C
Geoprobe
8
Basement
10
720
4
14
12
12
B-8
B8-SB-4
G
C
C
Hand Auger
9
Crawlspace
3
985
2
11.5
5
5
B-9s
B9-SB-2
G
C
C
Hand Auger
10
10
B-9d
B9-5B-2
G
C
C
10
Basement
10
970
5
14
1 12
1 12
B-10
B10-SB-5
G
C
C
Hand Auger
11
Parking Lot
At Grade
804
2
15
5
5
B-11s
B11-SB-2
G
C
C
Geoprobe
10
10
B-11d
B11-SB-2
G
C
C
12
Parking Lot
At Grade
805
2
15
5
5
B-12s
B12-SB-1
G
C
C
Geoprobe
10
7-10
B-12d
B12-SB-1
G
C
C
Duplicate Sample (B-
Duplicate
B12-SB-1
1
1
1
12d)
Totals
10579 38
20
20
20
VOCs: Volatile Organic Compounds by EPA Method 8260
SVOCs: Semi -Volatile Organic Compounds by EPA Method 8270
Metals: Eight RCRA metals by EPA 6010D/7471B+ 10% hexavalent chromium by EPA 7199
ft: Foot/Feet
G: Grab Samples
C: Composite Sample
*Duplicate sample was collected at sample interval with highest PID field screening measurement.

TABLE 2
SUMMARY OF ASSESSMENT SOIL SAMPLE ANALYSIS
HILLSBOROUGH SQUARE AND POWERHOUSE SQUARE
400H OFFICE REDEVELOPMENT
HILLSBOROUGH STREET AT N. WEST STREET
RALEIGH, NORTH CAROLINA
MID -ATLANTIC JOB NO. R2650.02
Parameter
SAMPLING LOCATION
Preliminary Soil Remediation Goals (PSRG)
(December 2019)
B-1
B-2
B-3S
B-3D
B-4S
B-4D
B-5S
B-5D
B-6S
B-6D
B-7
B-8
B-9S
B-9D
B-10
B-11S
B-11D
B-12S
B-12D
DUPLICATE
(B-12D)
Residential PSRG mg/kg
Industrial/Commercial PSRG
mg/kg
Protection of
Groundwater PSRG
mg/kg
Sampling Date
1/6/2020
1/7/2020
1/8/2020
1/8/2020
1/8/2020
1/8/2020
1/6/2020
1/6/2020
1/7/2020
1/7/2020
1/6/2020
1/6/2020
1/7/2020
1/7/2020
1/6/2020
1/7/2020
1/7/2020
1/7/2020
1/7/2020
1/7/2020
Sam le Depth in Feet BLS
2
10
2
7
2
7
2
7
3
5
3
12
5
10
2
5
10
5
7-10
7-10
RCRA Metals by Method 6010D 7471E
Arsenic
1.6
1.5
3.9
2.8
2.3
2.3
1.2
1.1
2.3
1.4
1.2 J
0.54 J
3.1
1.9
0.57 J
2.3
0.76 J
0.65 J
0.181
0.36 J
0.68
3
5.8
Barium
71
61
170
44
42
29
27
36
41
360
19
54
62
49
79
55
140
86
54
55
3100
47000
580
Chromium (Total)
30
13
20
24
18
26
17
19
29
23
y 27
8.7
25
16
17
24
13
14
5.7
1111[.5
0.31
6.5
3.8
Cadmium
<0.044
<0.043
<0.039
<0.043
<0.038
<0.042
<0.042
<0.047
<0.044
<0.044
<0.043
<0.042
<0.039
<0.044
0.096 J
<0.040
<0.043
<0.040
<0.041
<0.041
14
200
3
Lead
15
12
140
25
91
14
18
11
15
44
17
13
20
23
32
21
12
13
12
12
400
800
250
Hexavalent Chromium
NT
NT
NT
NT
NT
0.20J
NT
NT
<0.06
NT
0.16J
NT
NT
NT
NT
NT
NT
NT
NT
NT
0.31
6.5
3.8
Mercury<0.022
0.0271
0.2
0.06
0.11
0.069
0.039
0.036
0.0411
0.042 J
0.13
<0.022
0.026 J
0.0321
0.027 J
0.045 J
<0.022
0.029 J
<0.021
0.082
2.3
9.7
1
VOCs by Method 8260D
Acetone
<0.0018
0.0211
0.072
0.076
0.027
0.030
0.0171
<0.0018
0.033
0.0181
0.025
0.0151
0.18
<0.0015
<0.0015
<0.0013
<0.0015
0.061
0.037
0.042
12000
140000
25
Benzene
<0.0011
<0.00093
<0.00067 CCVH
<0.00089
0.014 CCVH
<0.00097
<0.0008
<0.0011
<0.001
<0.00095
<0.00075
<0.00089
0.0011 J
<0.00089
<0.00091
<0.00079
<0.00093
<0.00081
<0.0011
<0.0012
1.2
5.4
0.01
Bromomethane
<0.0034
<0.0029
<0.0021
0.0029 J
<0.0027
<0.0031
<0.0025
<0.0035
<0.0031
<0.003
<0.0024
<0.0028
0.0034 J
<0.0028
<0.0029
<0.0025
<0.0029
0.00281
0.0048 J
<0.0039
1.4
6.4
0.05
2-Butanone
0.0016
<0.0014
<0.001
<0.0013
<0.0013
<0.0015
<0.0012
<0.0017
<0.0015
<0.0014
<0.0011
<0.0013
0.025
<0.0013
<0.0014
<0.0012
<0.0014
<0.0012
<0.0017
<0.0019
5500
40000
17
Naphthalene
<0.00069
<0.0006
<0.00043
<0.00058
<0.00056
<0.00063
<0.00052
<0.00073
<0.00064
<0.00062
<0.00049
<0.00058
<0.00056
<0.0058
<0.00059
<0.00051
<0.0006
<0.00052
0.0055 J
0.00421
4.1
18
0.39
Toluene
<0.0011
<0.00095
<0.00068
<0.00091
0.0026J
<0.00099
<0.00082
<0.0011
<0.0010
<0.00097
<0.00077
<0.00091
<0.00089
<0.00091
<0.00093
<0.00081
<0.00095
<0.00082
<0.0011
<0.0013
990
9700
8.3
1,2,4-Trimethyl benzene
<0.00073
<0.00063
<0.00045
<0.00061
<0.00058
<0.00066
<0.00055
<0.00076
<0.00068
<0.00065
<0.00051
<0.0006
<0.00059
<0.0006
<0.00062
<0.00054
<0.00063
<0.00055
0.0046J
0.00231
63
370
12
1,3,5-Trimethyl benzene
<0.00086
<0.00075
<0.00054
<0.00072
<0.00069
<0.00078
<0.00065
<0.00091
<0.0008
<0.00077
<0.00061
<0.00072
<0.0007
<0.00072
<0.00073
<0.00064
<0.00075
<0.00065
0.0062J
0.00281
56
320
11
o-Xylene
<0.00073
<0.00064
<0.00046
<0.00061
<0.00059
<0.00066
<0.00055
<0.00077
<0.00068
<0.00065
<0.00051
<0.00061
<0.0006
<0.00061
<0.00062
<0.00054
<0.00063
<0.00055
0.000831
0.00098J
140
590
9.8
m,p-Xylenes
<0.0018
<0.0015
<0.0011
<0.0015
<0.0014
<0.0016
<0.0013
<0.0018
<0.0016
<0.0016
<0.0012
<0.0015
<0.0014
<0.0015
<0.0015
<0.0013
<0.0015
<0.0013
0.0023 J
0.00411
120
500
9.8
X lenes, total
<0.0025
<0.0022
<0.0015
<0.0021
<0.002
<0.0022
<0.0019
<0.0026
<0.0023
<0.0022
<0.0017
<0.0021
<0.002
<0.0021
<0.0021
<0.0018
<0.0021
<0.0019
0.0031 J
0.00511
120
530
9.9
SVOCs by Method 8270E
Acenaphthylene
<0.017
<0.016
0.0471
<0.017
<0.015
<0.016
<0.016
<0.018
<0.017
<0.017
<0.016
<0.016
<0.015
<0.017
<0.017
<0.015
<0.016
<0.015
<0.016
<0.016
-
41
Benzo(a)anthracene
<0.010
<0.0099
0.17J
<0.01
<0.009
0.16J
<0.0097
<0.011
<0.010
<0.010
<0.010
<0.0098
<0.0090
<0.010
<0.011
<0.0093
<0.0099
<0.0094
<0.0096
<0.0095
1.1
21
0.35
Benzo(a)pyrene
<0.0076
<0.0074
0.27J
<0.0075
<0.0067
0.16J
<0.0072
<0.0082
<0.0077
<0.0076
<0.0075
<0.0073
<0.0067
<0.0078
<0.0078
<0.007
<0.0074
<0.007
<0.0072
<0.0071
0.11
2.1
0.12
Benzo(b)fluoranthene
<0.0079
<0.0077
0.44J
<0.0078
<0.0069
0.20J
<0.0075
<0.0085
<0.008
<0.0078
<0.0077
<0.0076
<0.007
<0.008
<0.0081
<0.0072
<0.0077
<0.0073
<0.0074
<0.0074
1.1
21
1.2
Benzo(g,h,i)perylene
<0.0084
<0.0082
0.26 J
<0.0083
<0.0074
0.14 J
<0.008
<0.009
<0.0085
<0.0084
<0.0082
<0.0081
<0.0074
<0.0085
<0.0086
<0.0077
<0.0082
<0.0077
<0.0079
<0.0078
-
15600
Benzo(k)fluoranthene
<0.0090
<0.0088
0.16J
<0.0089
<0.0079
0.0751
<0.0086
<0.0097
<0.0092
<0.009
<0.0088
<0.0087
<0.008
<0.0092
<0.0093
<0.0083
<0.0088
<0.0083
<0.0085
<0.0084
1.1
210
1.2
Chrysene
<0.010
<0.0098
0.29 J
<0.0099
<0.0089
0.13 J
<0.0095
<0.011
<0.010
<0.010
<0.0099
<0.0097
<0.0089
<0.010
<0.010
<0.0092
<0.0098
<0.0093
<0.0095
<0.0094
110
2100
36
Dibenzo(a,h)anthracene
<0.025
<0.024
0.0481
<0.024
<0.022
<0.024
<0.023
<0.026
<0.025
<0.024
<0.024
<0.024
<0.022
<0.025
<0.025
<0.022
<0.024
<0.023
<0.023
<0.023
0.11
2.1
0.38
Fluoranthene
<0.0097
<0.0094
0.34 J
<0.0095
<0.0085
0.27 J
<0.0092
<0.01
<0.0098
<0.0096
0.0451
<0.0093
<0.0086
<0.0099
<0.01
<0.0089
<0.0094
<0.0089
<0.0091
<0.0090
480
6000
670
Indeno(1,2,3-cd)pyrene
<0.024
<0.023
0.26J
<0.024
<0.021
0.13J
<0.023
<0.026
<0.024
<0.024
<0.023
<0.023
<0.021
<0.024
<0.025
<0.022
<0.023
<0.022
<0.023
<0.022
1.1
21
3.9
Phenanthrene
<0.0093
<0.009
0.26 J
<0.0092
<0.0082
0.11 J
<0.0088
<0.01
<0.0094
<0.0093
<0.0091
<0.0089
<0.0082
<0.0095
<0.0096
<0.0085
<0.0091
<0.0086
<0.0087
<0.0087
-
134
P rene
<0.012
<0.012
0.32 J
<0.012
<0.011
0.27 J
<0.012
<0.013
<0.013
<0.012
0.0431
<0.012
<0.011
<0.013
<0.013
<0.011
<0.012
<0.011
<0.012
<0.012
360
4500
440
NOTES:
1. NT = Not Tested
2. -= No IHSB Preliminary Soil Remediation Goal (PSRG).
3. All values reported in milligrams per kilogram (mg/kg)
4. VOCs = Volatile Organic Compounds.
S. SVOCs = Semi -Volatile Organic Compounds.
7. <= Less than the method detection limit
6. Underlined values exceed Protection of Groundwater PSRGs
8. Bold values exceed the Residential PSRG
=values in exceed Industrial/Commercial PSRG
Concentrationas detected between the method detection limit and the reporting limit; value is an estimation.
is above control limits but within method parameters. Result is considered estimate
surface

APPENDIX A
SOIL BORING LOGS
Mid Atlantic

Mid Atlantic `°'�°�"2761
Relagh,NC0-991
Engineering & Environmental Solutions Ph: [phone]
LOG OF BORING: B1-SB-1
Pa e: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 12
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
Sampling
Interval,
Odors
d'
F
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Concrete slab
0.0
2
2
Red, orange silty clay
4
4
0.0
6
NR
FR
6
Red, orange clayey silt
0.0
8
8
0.0
10
10
Orange silty clay
0.0
12
12
*Boring terminated by technician at 12 feet BLS
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: BI-SB-2
Raleigh, NC 27610
Mid Atlantic `g"5""—"
Ph:h:(9(919)250-9918
Engineering & Environmental Solutions
e• Pa 1 of 1
Page:
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 12
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
Sampling
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
�
d
Concrete slab
0.0
Firm orange fine silty clay
2
2
4
4
0.0
6
NR
FR
6
Micaceous red, orange silty clay with black marbeling
0.0
8
8
0.0
10
10
Red silty clay and orange silty clay with black marbeling
0.0
12
12
*Boring terminated by technician at 12 feet BLS
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B1-SB-3
Antic 4U9 Rogers View C t.
Raleigh, NC 27610
Mid Atlantic
Ph: (919)260-99I 8
Engineering & Environmental Solutions
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 5
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/8/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
Sampling
cs
g
Interval,
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
?
Odors
d'
F�
Asphalt
Firm red fine silty clay
2
0.0
2
NR
FR
Tan and red silty clay
4
0.0
4
*Boring terminated by technician at 5 feet BLS
6
6
8
8
10
10
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: BI-SB-4
• 409 Rogers View 1Ct
0
Mid Atlantic
h:(919N��blo
en: tviv)zso-vvis
Engineering &Environmental Solutions
Page: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 5
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/8/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
Sampling
a
?
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
sx
F
Asphalt
Firm red, orange fine silty clay
2
0.0
2
NR
FR
Red, orange silty clay with sand
4
0.0
4
*Boring terminated by technician at 5 feet BLS
6
6
8
8
10
10
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B1-SB-5
• 409 0.
igh,N View10
Mid Atlantic ldeleigh,NC24b18
Ph [phone]
Engineering & Environmental Solutions
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft his): 5
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/8/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
8
a
>.
i
y
Samlin
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
s
Interval Odors
w
F
Asphalt
Firm red, orange fine silty clay
2
0.0
2
VOC Grab @ 2'
FR
Firm orange silty clay with tan marbeling
4
0.0
4
*Boring terminated by technician at 5 feet BLS
6
6
8
8
10
10
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B2-SB-1
• Rs Rogers View Ct
10
Mid Atlantic
h:(919N��blo
Ph: (9l9)250-99L8
Engineering &Environmental Solutions
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 12
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
S
�
C4
F
2
2
4
Basement Area
4
Basement Area
6
6
8
8
Concrete Slab
0.0
10
10
NR
FR
Sandy silty clay
0.0
12
12
*Boring terminated by technician at 12 feet BLS
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B2-SB-2
Raleigh, NC 27610
Mid Atlantic 4-R919)25e""
Ph [phone]
Engineering & Emironmencal Solutions
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 12
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring E ui ment PID MAA Field Staff: R. Tull
8
a
a
�
d
DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
s
IntervallOdors
Q.SOIL
09
F
2
2
4
Basement Area
Basement Area
4
6
6
8
8
Concrete Slab
0.0
10
NR
FR
Sandy silty clay
10
0.0
12
12
*Boring terminated by technician at 12 feet BLS
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B2-SB-3
Ct
Raleigh, NC276
Mid Atlantic 409Rogers View 10
0-991
En & Environmental Solutions Ph: (9l9)250-9918
Engineering
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 12
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
S
�
C4
F
2
2
4
Basement Area
4
Basement Area
6
6
8
8
Concrete Slab
0.0
10
10
NR
FR
Sandy silty clay
0.0
12
12
*Boring terminated by technician at 12 feet BLS
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B2-SB-4
• Rs Rogers View Ct
10
Mid Atlantic
h:(919N��blo
Ph: (9l9)250-99L8
Engineering &Environmental Solutions
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 12
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
S
�
C4
F
2
2
4
Basement Area
4
Basement Area
6
6
8
8
Concrete Slab
0.0
10
10
NR
FR
Sandy silty clay
0.0
12
12
*Boring terminated by technician at 12 feet BLS
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B2-SB-5
• Rs Rogers View Ct
10
Mid Atlantic
h:(919N��blo
Ph: (9l9)250-99L8
Engineering &Environmental Solutions
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 12
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
S
�
C4
F
2
2
4
Basement Area
4
Basement Area
6
6
8
8
Concrete Slab
0.0
10
10
NR
FR
Sandy silty clay
0.0
12
12
*Boring terminated by technician at 12 feet BLS
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B2-SB-6
= Relai ,)250-910
Mid Atlantic `°' g� NC "276"
En & Environmental Solutions Ph: [phone]
Engineering
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 12
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
5
�
y
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Interval, Odors
?
d
w
2
2
4
Basement Area
4
Basement Area
6
6
8
8
Concrete Slab
0.0
10
10
VOC Grab @ 10'
FR
Sandy silty clay
0.0
12
12
*Boring terminated by technician at 12 feet BLS
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B3-SB-1
Mid Atlantic `°'R°�"276"
Raleigh, NC0-991
En & Environmental Solutions Ph: [phone]
Engineering
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 9
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/8/2020 Driller: NA DTW : NA
Date Completed: 1/8/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
Sampling
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
to
d
Concrete Slab/Flooring
0.0
0.0
2
2
VOC Grab @ 2'
0.0
4
4
FR
Sandy silty clay
0.0
6
6
0.0
VOC Grab @ 7'
8
0.0
8
*Boring terminated by technician at 9 feet BLS
10
10
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B3-SB-2
Ct
Raleigh, NC276
Mid Atlantic 409Rogers View 10
0-991
En & Environmental Solutions Ph: (9l9)250-9918
Engineering
Page: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 9
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/8/2020 Driller: NA DTW : NA
Date Completed: 1/8/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
Sampling
a
?
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
sx
F
Concrete Slab/Flooring
0.0
0.0
2
2
0.0
4
4
NR
FR
Sandy silty clay
0.0
6
6
0.0
0.0
8
8
*Boring terminated by technician at 9 feet BLS
10
10
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B4-SB-1
—"
Mid Atlantic `°',10,5C"276 10
Rala91
) 2 0-991
En & Environmental Solutions Ph: [phone]
Engineering
Page: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 9
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/8/2020 Driller: NA DTW : NA
Date Completed: 1/8/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
Sampling
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
to
d
Concrete Slab/Flooring
0.0
0.0
2
2
0.0
4
4
NR
FR
Sandy silty clay
0.0
6
6
0.0
0.0
8
8
*Boring terminated by technician at 9 feet BLS
10
10
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B4-SB-2
409 Rogers View 10
Mid Atlantic Raleigh,N276
Ph (919)250-99150-9918
Engineering & Environmental Solutions
e• Pa 1 of 1
Page:
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 9
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/8/2020 Driller: NA DTW : NA
Date Completed: 1/8/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
Sampling
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
d
Concrete Slab/Flooring
0.0
0.0
2
2
VOC Grab @ 2'
0.0
4
4
FR
Sandy silty clay
0.0
6
6
0.0
VOC Grab @ 7'
8
0.0
8
*Boring terminated by technician at 9 feet BLS
10
10
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B5-SB-1
• 409 Rogers View 1Ct
0
Mid Atlantic
h:(919N��blo
en: tviv)zso-vvis
Engineering &Environmental Solutions
Page: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 10
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
Sampling
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
a
F
Top soil and gravel
0.0
2
2
Firm red clay with silt
0.0
4
4
NR
FR
6
0.0
Orange, tan clay with silt
6
8
8
0.0
Micaceous orange, tan clayey silt
10
10
*Boring terminated by technician at 10 feet BLS
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B5-SB-2
Ct
Raleigh, NC276
Mid Atlantic 409Rogers View 10
0-991
En & Environmental Solutions 2h: (9l9)uo-9918
$ineering
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 10
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Interval, Odors
?
g
F
Top soil and gravel
0.0
Firm red clay with silt and white blebs
2
2
VOC Grab @ 2'
0.0
Micaceous firm red, orange clay with silt
4
4
FR
6
0.0
Micaceous orange silty clay
6
VOC Grab @ 7'
8
8
0.0
Micaceous orange silt with clay
10
10
*Boring terminated by technician at 10 feet BLS
12
12
14
14
16
16
18
18
20
20
CONllWENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B6-SB-1
Mid Atlantic `°'R°�"276"
Raleigh, NC0-991
En & Environmental Solutions Ph: [phone]
Engineering
Page: 1 of I
g
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 10
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
as
y
a
Sampling
A
c
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
r:
Interval, Odors
?
d
Top soil and gravel
0.0
Firm red clay with silt
2
2
0.0
4
4
NR
FR
Micaceous red clay with silt
6
6
0.0
8
8
0.0
Micaceous red silt with clay
10
10
*Boring terminated by technician at 10 feet BLS
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B6-SB-2
Ct
Raleigh, NC276
Mid Atlantic 409Rogers View 10
0-991
En & Environmental Solutions Ph: (9l9)250-9918
Engineering
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 10
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
47
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Interval, Odors
?
w
F
Top soil and gravel
0.0
Firm red clay with silt
2
2
VOC Grab @ 3'
0.0
Micaceous red clay with silt
4
4
FR
VOC Grab @ 5'
6
6
0.0
Micaceous red silty clay
8
8
0.0
10
10
*Boring terminated by technician at 10 feet BLS
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B7-SB-1
409 Rogers View G Mid Atlantic Raleigh,N276 10
Ph (919) 250-99150.9918
Engineering &Environmental Solutions
Page: 1 Of l
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 10
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
Sampling
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
d
Gravel and aggregate
0.0
Red clay with silt
2
2
Red silty clay
4
0.0
4
NR
FR
6
Red silly clay with tan marbeling
6
0.0
8
8
0.0
Micaceous red clayey silt
10
10
*Boring terminated by technician at 10 feet BLS
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B7-SB-2
409 Rogers View G Mid Atlantic Raleigh,N276 10
Ph (919) 250-99150.9918
Engineering &Environmental Solutions
Page: 1 Of 1
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 10
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
Sampling
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
d
Gravel and aggregate
0.0
Red, orange clay with silt
2
2
Firm orange clay with silt
4
0.0
4
NR
FR
6
Firm orange clay with silt and tan marbeling
6
0.0
8
8
0.0
Micaceous red silty clay
10
10
*Boring terminated by technician at 10 feet BLS
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B7-SB-3
Ct
Raleigh, NC276
Mid Atlantic 409Rogers View 10
0-991
En & Environmental Solutions Ph: (9l9)250-9918
Engineering
Page: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 10
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
Sampling
a
?
Interval,
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
?
Odors
d
F
Concrete and top soil
0.0
2
2
Firm orange clay with silt
4
0.0
4
NR
FR
6
Firm orange clay with silt and tan marbeling
6
0.0
8
8
0.0
Micaceous red silt with clay
10
10
*Boring terminated by technician at 10 feet BLS
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B7-SB-4
409 Rogers View 1Ct
Mid Atlantic Ralei6h.N 0
Ph: (viv)o-vvis
u0276 -991
Engineering &Environmental Solutions
Page: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 10
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
Sampling
a
?
Interval,
a
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Odors
sx
F
Top soil
0.0
2
2
Firm red clay with silt
VOC Grab @ 3'
0.0
4
4
FR
6
0.0
Micaceous red silt with clay
6
8
8
0.0
Micaceous red silty fine sand with clay
10
10
*Boring terminated by technician at 10 feet BLS
12
12
14
14
16
16
18
18
20
20
COUNTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B8-SB-1
409 Rogers View G Mid Atlantic Raleigh,N276 10
Ph (919) 250-99150.9918
Engineering &Environmental Solutions
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 14
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
5
�
y
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Interval, Odors
?
d
w
2
2
4
4
Basement Area
Basement Area
6
6
8
8
10
10
Concrete Slab
0.0
12
NR
Sandy silty clay
12
0.0
14
14
*Boring terminated by technician at 14 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B8-SB-2
= Relai ,)250-910
Mid Atlantic `°' g� NC "276"
En & Environmental Solutions Ph: [phone]
Engineering
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 14
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
5
�
y
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Interval, Odors
?
d
w
2
2
4
4
Basement Area
Basement Area
6
6
8
8
10
10
Concrete Slab
0.0
12
NR
Sandy silty clay
12
0.0
14
14
*Boring terminated by technician at 14 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B8-SB-3
= Relai ,)250-910
Mid Atlantic `°' g� NC "276"
En & Environmental Solutions Ph: [phone]
Engineering
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 14
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
5
�
y
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Interval, Odors
?
d
w
2
2
4
4
Basement Area
Basement Area
6
6
8
8
10
10
Concrete Slab
0.0
12
NR
Sandy silty clay
12
0.0
14
14
*Boring terminated by technician at 14 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B8-SB-4
• Rs Rogers View Ct
10
Mid Atlantic
h:(919N��blo
Ph: (9l9)250-99L8
Engineering &Environmental Solutions
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 14
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
w
�
F4
F
2
2
4
4
Basement Area
Basement Area
6
6
8
8
10
10
Concrete Slab
0.0
12
VOC Grab at 12'
Sandy silty clay
12
0.0
14
14
*Boring terminated by technician at 14 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B9-SB-1
• 409 Rogers View 1Ct
N��blo
0
Mid Atlantic
h: (91
Ph: (9l9)250-99L8
Engineering &Environmental Solutions
Page: 1 of l
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 12.5
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
w
�
F4
F
Wood Flooring
Crawlspace
Crawlspace
2
2
4
4
0.0
6
6
0.0
8
NR
FR
Sandy silty clay
8
0.0
0.0
10
10
0.0
12
12
*Boring terminated by technician at 12.5 feet BLS
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B9-SB-2
Ct
Raleigh, NC276
Mid Atlantic 409 igh,NView 10
0-991
En & Environmental Solutions Ph: (9l9)250-9918
Engineering
Page: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 11.5
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
w
�
F4
F
Wood Flooring
Crawlspace
Crawlspace
2
2
4
4
0.0
VOC Grab at 5'
6
0.0
6
FR
Sandy silty clay
8
0.0
8
10
10
VOC Grab at 10'
0.0
*Boring terminated by technician at 11.5 feet BLS
12
12
14
14
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B10-SB-1
• 409 Rogers View 1Ct
N��blo
0
Mid Atlantic
h: (91
Ph: (9l9)250-99L8
Engineering &Environmental Solutions
Page: 1 of l
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 14
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
w
�
F4
F
2
2
4
4
Basement Area
Basement Area
6
6
8
8
10
10
Concrete Slab
0.0
12
NR
Sandy silty clay
12
0.0
14
14
*Boring terminated by technician at 14 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Tota] Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B10-SB-2
Ct
Raleigh, NC276
Mid Atlantic 409Rogers View 10
0-991
En & Environmental Solutions Ph: (9l9)250-9918
Engineering
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 14
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
S
�
C4
F
2
2
4
4
Basement Area
Basement Area
6
6
8
8
10
10
Concrete Slab
0.0
12
NR
Sandy silty clay
12
0.0
14
14
*Boring terminated by technician at 14 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B10-SB-3
Ct
Raleigh, NC276
Mid Atlantic 409 igh,NView 10
0-991
En & Environmental Solutions Ph: (9l9)250-9918
Engineering
Page: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 14
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
a
a
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
`.
Interval, Odors
?
S
w
�
C4
F
2
2
4
4
Basement Area
Basement Area
6
6
8
8
10
10
Concrete Slab
0.0
12
NR
Sandy silty clay
12
0.0
14
14
*Boring terminated by technician at 14 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B10-SB-4
a• Mid Atlantic `°' 9�"276"
= Relai ,NC0-991
En & Environmental Solutions Ph: [phone]
Engineering
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 14
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
E
5
�
Sampling
A
o
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Interval, Odors
?
d
2
2
4
4
Basement Area
Basement Area
6
6
8
8
10
10
Concrete Slab
0.0
12
NR
Sandy silty clay
12
0.0
14
14
*Boring terminated by technician at 14 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling fit - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B10-SB-5
Mid Atlantic 4�R°g
Raleigh, NC 27610
25°""
Ph: [phone]
Engineering & EnAronmental Solutions
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Hand Auger Total Boring Depth (ft bls): 14
Project Number: R2650.02 Sampling Method: Continuous Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: EFM, Inc. Screen Depth (ft): NA
Date Started: 1/6/2020 Driller: NA DTW : NA
Date Completed: 1/6/2020 Monitoring Equipment: PH) MAA Field Staff: R. Tull
8
8
�
y
Sampling
ZSOIL
d
DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
Interval, Odors
a
d
�
F
2
2
4
4
Basement Area
Basement Area
6
6
8
8
10
10
Concrete Slab
0.0
12
VOC Grab at 121
Sandy silty clay
12
0.0
14
14
*Boring terminated by technician at 14 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B11-SB-1
• 409RogersViewCt
Mid Atlantic �IeiB�NC-9,o
Engineering & Environmental Solutions rn: (sls)zso-v91s
Pa e: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft his): 15
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
Sampling Interval,
A
a
>
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
w
Odors
w
Concrete
0.0
Red clay with silt
2
2
0.0
Red, orange clay with silt
4
4
6
6
0.0
Micaceous red clay with silt
NR
FR
8
8
0.0
10
Micaceous red, orange clay with silt
10
0.0
12
12
0.0
Micaceous orange silt with clay
14
14
*Boring terminated by technician at 15 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

LOG OF BORING: B11-SB-2
• 409 Rogers View CL
Mid Atlantic �'��NC
"10
Ph. t919)2$0-991g
Engineering & Environmental Solutions
Page: 1 of 1
g '
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft bls): 15
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
8
a
Sampling Interval,
A
o.
>
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
�=
Odors
>
=
d
a
F
Concrete
Red, tan clay with silt and brown marbeling, with brick fragments
0.0
2
2
Orange clay with silt
4
0.0
4
VOC Grab @5'
6
0.0
6
FR
8
8
0.0
Micaceous red, orange clay with silt
10
10
VOC Grab @10'
0.0
12
12
0.0
Micaceous orange, red, brown clay with silt and fine sand
14
14
*Boring terminated by technician at 15 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B12-SB-1
• 40 gb,z View10
Mid Atlantic �ieiB�N�z,�o
Engineering & Environmental Solutions Ph: [phone]
Page: 1 of 1
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft his): 15
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
Sampling Interval,
A
a
>
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
w
Odors
w
Concrete
0.0
Firm orange, red clay with silt
2
2
3'
0.1
Firm red clay with silt
4
4
VOC Grab @ 5'
6
6
2.5
Orange silt
8
8
VOC Grab @T-10'
53.3
10
FR
10
4.5
Micaceous red, orange clayey silt
12
12
7.1
Micaceous orange silty clay
14
14
*Boring terminated by technician at 15 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded VOC - Volatile organic compound

LOG OF BORING: B12-SB-2
• 409RogersViewCt
Mid Atlantic �IeiB�NC-9,o
Engineering & Environmental Solutions rn: (sls)zso-v91s
Pa e: 1 of 1
g
Site Name: 400 H Drilling/Boring Method: Geoprobe Total Boring Depth (ft his): 15
Project Number: R2650.02 Sampling Method: Macrocore Well Depth (ft): NA
Location: Raleigh, NC Subcontractor/Drillers: Quantex Screen Depth (ft): NA
Date Started: 1/7/2020 Driller: NA DTW : NA
Date Completed: 1/7/2020 Monitoring Equipment: PID MAA Field Staff: R. Tull
Sampling Interval,
A
a
>
SOIL DESCRIPTION (color, texture, moisture, etc.)
Construction Deatails
w
Odors
w
Concrete
0.0
Micaceous red clay with silt
2
2
0.0
Micaceous red, orange clay with silt
4
4
6
6
0.0
Orange silt with clay
NR
FR
8
8
0.0
Orange clay with silt
10
10
0.0
Brown silty clay
12
12
0.4
Red, orange clay with silt
14
14
*Boring terminated by technician at 15 feet BLS
16
16
18
18
20
20
COMMENTS: in - indicates inches
TD - Total Depth of Boring for Sampling ft - indicates depth in feet ppm - indicates parts per million
DTW - Depth to Water ft-bls - indicates feet below land surface FR - Full Recovery
NR - Not Recorded

APPENDIX B
LABORATORY ANALYTICAL REPORT
AND CHAIN OF CUSTODY RECORD
FOR SOIL SAMPLES
Mid Atlantic

Case Narrative
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh
Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: 400H
Lab Submittal Date: 01/10/2020
Work Order: 0010154
1 /28/20 10:53
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Method 7199 analysis was subcontracted to ALS Global. Laboratory report is attached.
Waypoint Summary of Detections does not include subcontracted data.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
a ---I
Angela D. Overcash
Project Management Manager
Reviewed By Angela D. Overcash
Project Management Manager
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Data Qualifiers Key Reference:
CCVH CCV result is above control limits but within method parameters. Result is considered estimated.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
PS Post Spike recovery is outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way� nt
poiAICAL
NALYT
Sample Receipt Summary
01 /28/2020
Work Order: 0010154
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
B-1
0010154-01
Soil
01/06/20
13:45
01/10/20
16:00
B-2
0010154-02
Soil
01/07/20
14:16
01/10/20
16:00
13-3S
0010154-03
Soil
01/08/20
12:52
01/10/20
16:00
13-3D
0010154-04
Soil
01/08/20
13:06
01/10/20
16:00
13-4S
0010154-05
Soil
01/08/20
10:20
01/10/20
16:00
B-4D
0010154-06
Soil
01/08/20
10:40
01/10/20
16:00
B-5S
0010154-07
Soil
01/06/20
14:55
01/10/20
16:00
13-5D
0010154-08
Soil
01/06/20
15:15
01/10/20
16:00
13-6S
0010154-09
Soil
01/07/20
11:25
01/10/20
16:00
13-6D
0010154-10
Soil
01/07/20
11:30
01/10/20
16:00
B-7
0010154-11
Soil
01/06/20
12:45
01/10/20
16:00
B-8
0010154-12
Soil
01/06/20
16:00
01/10/20
16:00
13-9S
0010154-13
Soil
01/07/20
16:50
01/10/20
16:00
B-9D
0010154-14
Soil
01/07/20
17:00
01/10/20
16:00
B-10
0010154-15
Soil
01/06/20
15:20
01/10/20
16:00
B-11S
0010154-16
Soil
01/07/20
10:10
01/10/20
16:00
B-11D
0010154-17
Soil
01/07/20
10:15
01/10/20
16:00
B-12S
0010154-18
Soil
01/07/20
9:20
01/10/20
16:00
B-12D
0010154-19
Soil
01/07/20
9:15
01/10/20
16:00
Duplicate
0010154-20
Soil
01/07/20
9:45
01/10/20
16:00
Samples were received in good condition at 2.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

WayPAoi n/28/2020
t .
NALYTICAL
Summary of Detections
0110154
Work Order: 0054
Waypoint ID
Client ID
Parameter
Method
Result
Units
0010154-01
B-1
Arsenic
601 OD
1.6
mg/kg dry
0010154-01
B-1
Barium
601 OD
71
mg/kg dry
0010154-01
B-1
Chromium
601 OD
10
mg/kg dry
0010154-01
B-1
Lead
601 OD
15
mg/kg dry
0010154-02
B-2
Mercury
7471B
0.027
J
mg/kg dry
0010154-02
B-2
Arsenic
601 OD
1.5
mg/kg dry
0010154-02
B-2
Barium
601 OD
61
mg/kg dry
0010154-02
B-2
Chromium
601 OD
13
mg/kg dry
0010154-02
B-2
Lead
601 OD
12
mg/kg dry
0010154-02
B-2
Acetone
8260D
0.021
J
mg/kg dry
0010154-03
B-3S
Acenaphthylene
8270E
0.047
J
mg/kg dry
0010154-03
B-3S
Benzo(a)anthracene
8270E
0.17
J
mg/kg dry
0010154-03
B-3S
Benzo(a)pyrene
8270E
0.27
J
mg/kg dry
0010154-03
B-3S
Benzo(b)fluoranthene
8270E
0.44
J
mg/kg dry
0010154-03
B-3S
Benzo(g,h,i)perylene
8270E
0.26
J
mg/kg dry
0010154-03
B-3S
Benzo(k)fluoranthene
8270E
0.16
J
mg/kg dry
0010154-03
B-3S
Chrysene
8270E
0.29
J
mg/kg dry
0010154-03
B-3S
Dibenzo(a,h)anthracene
8270E
0.048
.1
mg/kg dry
0010154-03
B-3S
Fluoranthene
8270E
0.34
J
mg/kg dry
0010154-03
B-3S
Indeno(1,2,3-cd)pyrene
8270E
0.26
J
mg/kg dry
0010154-03
B-3S
Phenanthrene
8270E
0.26
J
mg/kg dry
0010154-03
B-3S
Pyrene
8270E
0.32
J
mg/kg dry
0010154-03
B-3S
Mercury
7471E
0.20
mg/kg dry
0010154-03
B-3S
Arsenic
601 OD
3.9
mg/kg dry
0010154-03
B-3S
Barium
601 OD
170
mg/kg dry
0010154-03
B-3S
Chromium
601 OD
20
mg/kg dry
0010154-03
B-3S
Lead
601 OD
140
mg/kg dry
0010154-03
B-3S
Acetone
8260D
0.072
mg/kg dry
0010154-04
B-31D
Mercury
7471E
0.060
1
mg/kg dry
0010154-04
B-31D
Arsenic
601 OD
2.8
mg/kg dry
0010154-04
B-31D
Barium
601 OD
44
mg/kg dry
0010154-04
B-31D
Chromium
601 OD
24
mg/kg dry
0010154-04
B-31D
Lead
601 OD
25
mg/kg dry
0010154-04
B-31D
Acetone
8260D
0.076
mg/kg dry
0010154-04
B-31D
Bromomethane
8260D
0.0029
J
mg/kg dry
0010154-05
B-4S
Mercury
7471E
0.11
mg/kg dry
0010154-05
B-4S
Arsenic
601 OD
2.3
mg/kg dry
0010154-05
B-4S
Barium
601 OD
42
mg/kg dry
0010154-05
B-4S
Chromium
601 OD
18
mg/kg dry
0010154-05
B-4S
Lead
601 OD
91
mg/kg dry
0010154-05
B-4S
Acetone
8260D
0.027
mg/kg dry
0010154-05
B-4S
Benzene
8260D
0.014
CCVH
mg/kg dry
0010154-05
B-4S
Toluene
8260D
0.0026
J
mg/kg dry
0010154-06
B-41D
Benzo(a)anthracene
8270E
0.16
J
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

• W
Way poi nt .
ANALYTICAL
Summary of Detections
0110154
Work Order: 000154
Waypoint ID
Client ID
Parameter
Method
Result
Units
0010154-06
B-41D
Benzo(a)pyrene
8270E
0.16
J
mg/kg dry
0010154-06
B-41D
Benzo(b)fluoranthene
8270E
0.20
J
mg/kg dry
0010154-06
B-41D
Benzo(g,h,i)perylene
8270E
0.14
J
mg/kg dry
0010154-06
B-41D
Benzo(k)fluoranthene
8270E
0.075
J
mg/kg dry
0010154-06
B-41D
Chrysene
8270E
0.13
J
mg/kg dry
0010154-06
B-41D
Fluoranthene
8270E
0.27
J
mg/kg dry
0010154-06
B-41D
Indeno(1,2,3-cd)pyrene
8270E
0.13
J
mg/kg dry
0010154-06
B-41D
Phenanthrene
8270E
0.11
J
mg/kg dry
0010154-06
B-41D
Pyrene
8270E
0.27
J
mg/kg dry
0010154-06
B-41D
Mercury
7471E
0.069
mg/kg dry
0010154-06
B-41D
Arsenic
601 OD
2.3
mg/kg dry
0010154-06
B-41D
Barium
6010D
29
mg/kg dry
0010154-06
B-41D
Chromium
6010D
26
mg/kg dry
0010154-06
B-41D
Lead
6010D
14
mg/kg dry
0010154-06
B-41D
Acetone
8260D
0.030
mg/kg dry
0010154-07
B-5S
Mercury
7471B
0.039
J
mg/kg dry
0010154-07
B-5S
Arsenic
6010D
1.2
mg/kg dry
0010154-07
B-5S
Barium
6010D
27
mg/kg dry
0010154-07
B-5S
Chromium
6010D
17
mg/kg dry
0010154-07
B-5S
Lead
6010D
18
mg/kg dry
0010154-07
B-5S
Acetone
8260D
0.017
J
mg/kg dry
0010154-08
B-51D
Mercury
7471E
0.036
J
mg/kg dry
0010154-08
B-51D
Arsenic
6010D
1.1
J
mg/kg dry
0010154-08
B-51D
Barium
6010D
36
mg/kg dry
0010154-08
B-51D
Chromium
6010D
19
mg/kg dry
0010154-08
B-51D
Lead
601 OD
11
mg/kg dry
0010154-09
B-6S
Mercury
7471B
0.041
J
mg/kg dry
0010154-09
B-6S
Arsenic
6010D
2.3
mg/kg dry
0010154-09
B-6S
Barium
6010D
41
mg/kg dry
0010154-09
B-6S
Chromium
6010D
29
mg/kg dry
0010154-09
B-6S
Lead
6010D
15
mg/kg dry
0010154-09
B-6S
Acetone
8260D
0.033
mg/kg dry
0010154-10
B-61D
Mercury
7471B
0.042
J
mg/kg dry
0010154-10
B-61D
Arsenic
6010D
1.4
mg/kg dry
0010154-10
B-61D
Barium
601OD
360
mg/kg dry
0010154-10
B-61D
Chromium
6010D
23
mg/kg dry
0010154-10
B-61D
Lead
6010D
44
mg/kg dry
0010154-10
B-61D
Acetone
8260D
0.018
J
mg/kg dry
0010154-11
B-7
Fluoranthene
8270E
0.045
J
mg/kg dry
0010154-11
B-7
Pyrene
8270E
0.043
J
mg/kg dry
0010154-11
B-7
Mercury
7471B
0.13
mg/kg dry
0010154-11
B-7
Arsenic
6010D
1.2
J
mg/kg dry
0010154-11
B-7
Barium
6010D
19
mg/kg dry
0010154-11
B-7
Chromium
6010D
27
mg/kg dry
0010154-11
B-7
Lead
6010D
17
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

• W
Way poi nt .
ANALYTICAL
Summary of Detections
0110154
Work Order: 000154
Waypoint ID
Client ID
Parameter
Method
Result
Units
0010154-11
B-7
Acetone
8260D
0.025
mg/kg dry
0010154-12
B-8
Arsenic
6010D
0.54
J
mg/kg dry
0010154-12
B-8
Barium
6010D
54
mg/kg dry
0010154-12
B-8
Chromium
6010D
8.7
mg/kg dry
0010154-12
B-8
Lead
601 OD
13
mg/kg dry
0010154-12
B-8
Acetone
8260D
0.015
J
mg/kg dry
0010154-13
B-9S
Mercury
7471E
0.026
J
mg/kg dry
0010154-13
B-9S
Arsenic
6010D
3.1
mg/kg dry
0010154-13
B-9S
Barium
6010D
62
mg/kg dry
0010154-13
B-9S
Chromium
6010D
25
mg/kg dry
0010154-13
B-9S
Lead
601 OD
20
mg/kg dry
0010154-13
B-9S
Acetone
8260D
0.18
mg/kg dry
0010154-13
B-9S
Benzene
8260D
0.0011
J
mg/kg dry
0010154-13
B-9S
Bromomethane
8260D
0.0034
J
mg/kg dry
0010154-13
B-9S
Methyl Ethyl Ketone (2-Butanone)
8260D
0.025
mg/kg dry
0010154-14
B-91D
Mercury
7471B
0.032
J
mg/kg dry
0010154-14
B-91D
Arsenic
6010D
1.9
mg/kg dry
0010154-14
B-91D
Barium
6010D
49
mg/kg dry
0010154-14
B-91D
Chromium
6010D
16
mg/kg dry
0010154-14
B-91D
Lead
6010D
23
mg/kg dry
0010154-15
B-10
Mercury
7471E
0.027
J
mg/kg dry
0010154-15
B-10
Arsenic
6010D
0.57
J
mg/kg dry
0010154-15
B-10
Barium
6010D
79
mg/kg dry
0010154-15
B-10
Cadmium
6010D
0.096
J
mg/kg dry
0010154-15
B-10
Chromium
6010D
17
mg/kg dry
0010154-15
B-10
Lead
6010D
32
mg/kg dry
0010154-16
B-11S
Mercury
7471B
0.045
J
mg/kg dry
0010154-16
B-11S
Arsenic
6010D
2.3
mg/kg dry
0010154-16
B-11S
Barium
6010D
55
mg/kg dry
0010154-16
B-11S
Chromium
6010D
24
mg/kg dry
0010154-16
B-11S
Lead
6010D
21
mg/kg dry
0010154-17
B-11 D
Arsenic
6010D
0.76
J
mg/kg dry
0010154-17
B-11D
Barium
6010D
140
mg/kg dry
0010154-17
B-11D
Chromium
6010D
13
mg/kg dry
0010154-17
B-11 D
Lead
6010D
12
mg/kg dry
0010154-18
B-12S
Mercury
7471B
0.029
J
mg/kg dry
0010154-18
B-12S
Arsenic
6010D
0.65
J
mg/kg dry
0010154-18
B-12S
Barium
6010D
86
mg/kg dry
0010154-18
B-12S
Chromium
6010D
14
mg/kg dry
0010154-18
B-12S
Lead
6010D
13
mg/kg dry
0010154-18
B-12S
Acetone
8260D
0.061
mg/kg dry
0010154-18
B-12S
Bromomethane
8260D
0.0028
J
mg/kg dry
0010154-19
B-12D
Arsenic
6010D
0.18
J
mg/kg dry
0010154-19
B-12D
Barium
6010D
54
mg/kg dry
0010154-19
B-12D
Chromium
6010D
5.7
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way poi nt .
ANALYTICAL
Summary of Detections
01/28/2020
Work Order: 0010154
Waypoint ID
Client ID
Parameter
Method
Result
Units
0010154-19
B-12D
Lead
6010D
12
mg/kg dry
0010154-19
B-12D
1,2,4-Trimethylbenzene
8260D
0.0046
J
mg/kg dry
0010154-19
B-12D
1,3,5-Trimethylbenzene
8260D
0.0062
J
mg/kg dry
0010154-19
B-12D
Acetone
8260D
0.037
mg/kg dry
0010154-19
B-12D
Bromomethane
8260D
0.0048
J
mg/kg dry
0010154-19
B-12D
m,p-Xylenes
8260D
0.0023
J
mg/kg dry
0010154-19
B-12D
Naphthalene
8260D
0.0055
J
mg/kg dry
0010154-19
B-12D
o-Xylene
8260D
0.00083
J
mg/kg dry
0010154-19
B-12D
Xylenes, total
8260D
0.0031
J
mg/kg dry
0010154-20
Duplicate
Mercury
7471E
0.082
mg/kg dry
0010154-20
Duplicate
Arsenic
6010D
0.36
J
mg/kg dry
0010154-20
Duplicate
Barium
6010D
55
mg/kg dry
0010154-20
Duplicate
Chromium
6010D
6.5
mg/kg dry
0010154-20
Duplicate
Lead
601OD
12
mg/kg dry
0010154-20
Duplicate
1,2,4-Trimethylbenzene
8260D
0.0023
J
mg/kg dry
0010154-20
Duplicate
1,3,5-Trimethylbenzene
8260D
0.0028
J
mg/kg dry
0010154-20
Duplicate
Acetone
8260D
0.042
mg/kg dry
0010154-20
Duplicate
m,p-Xylenes
8260D
0.0041
J
mg/kg dry
0010154-20
Duplicate
Naphthalene
8260D
0.0042
J
mg/kg dry
0010154-20
Duplicate
o-Xylene
8260D
0.00098
J
mg/kg dry
0010154-20
Duplicate
Xylenes, total
8260D
0.0051
J
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-1
Attn: Katie Lippard Sample ID: 0010154-01
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 13:45
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
77.4
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.85
0.15
1
8270E
1/15/20 18:05
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.85
0.14
1
8270E
1/15/20 18:05
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.85
0.13
1
8270E
1/15/20 18:05
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.13
1
8270E
1/15/20 18:05
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.85
0.013
1
8270E
1/15/20 18:05
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.85
0.18
1
8270E
1/15/20 18:05
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.85
0.21
1
8270E
1/15/20 18:05
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.85
0.17
1
8270E
1/15/20 18:05
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.43
0.18
1
8270E
1/15/20 18:05
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.50
1
8270E
1/15/20 18:05
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.85
0.23
1
8270E
1/15/20 18:05
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.85
0.22
1
8270E
1/15/20 18:05
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.85
0.21
1
8270E
1/15/20 18:05
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 18:05
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.85
0.017
1
8270E
1/15/20 18:05
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 18:05
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.85
0.14
1
8270E
1/15/20 18:05
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.85
0.17
1
8270E
1/15/20 18:05
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.85
0.18
1
8270E
1/15/20 18:05
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.47
1
8270E
1/15/20 18:05
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.85
0.20
1
8270E
1/15/20 18:05
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 18:05
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
8270E
1/15/20 18:05
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
8270E
1/15/20 18:05
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.85
0.21
1
8270E
1/15/20 18:05
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.85
0.019
1
8270E
1/15/20 18:05
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.85
0.017
1
8270E
1/15/20 18:05
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.85
0.0094
1
8270E
1/15/20 18:05
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.85
0.18
1
8270E
1/15/20 18:05
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.85
0.010
1
8270E
1/15/20 18:05
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.85
0.0076
1
8270E
1/15/20 18:05
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.85
0.0079
1
8270E
1/15/20 18:05
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.85
0.0084
1
8270E
1/15/20 18:05
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.85
0.0090
1
8270E
1/15/20 18:05
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.6
0.71
1
8270E
1/15/20 18:05
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 18:05
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 18:05
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.85
0.14
1
8270E
1/15/20 18:05
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
8270E
1/15/20 18:05
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-1
Attn: Katie Lippard Sample ID: 0010154-01
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 13:45
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.85
0.19
1
8270E
1/15/20 18:05
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
8270E
1/15/20 18:05
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.85
0.010
1
8270E
1/15/20 18:05
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.85
0.025
1
8270E
1/15/20 18:05
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.85
0.23
1
8270E
1/15/20 18:05
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.85
0.22
1
8270E
1/15/20 18:05
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.85
0.20
1
8270E
1/15/20 18:05
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.85
0.21
1
8270E
1/15/20 18:05
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
8270E
1/15/20 18:05
JMV
POA0191
Fluoranthene
BRL
mg/kg dry
0.85
0.0097
1
8270E
1/15/20 18:05
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.85
0.015
1
8270E
1/15/20 18:05
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.85
0.19
1
8270E
1/15/20 18:05
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.85
0.19
1
8270E
1/15/20 18:05
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.85
0.29
1
8270E
1/15/20 18:05
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.85
0.13
1
8270E
1/15/20 18:05
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.85
0.024
1
8270E
1/15/20 18:05
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.85
0.18
1
8270E
1/15/20 18:05
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.85
0.018
1
8270E
1/15/20 18:05
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
8270E
1/15/20 18:05
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.85
0.20
1
8270E
1/15/20 18:05
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.85
0.23
1
8270E
1/15/20 18:05
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.3
0.54
1
8270E
1/15/20 18:05
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.85
0.0093
1
8270E
1/15/20 18:05
JMV
POA0191
Phenol
BRL
mg/kg dry
0.85
0.14
1
8270E
1/15/20 18:05
JMV
POA0191
Pyrene
BRL
mg/kg dry
0.85
0.012
1
8270E
1/15/20 18:05
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.43
0.081
1
8270E
1/15/20 18:05
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
82 %
39-132
2-Fluorobiphenyl
76 %
44-115
2-Fluorophenol
74 %
35-115
Nitrobenzene-d5
68 %
37-122
Phenol-d5
71 %
34-121
Terphenyl-d14
81 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.065
0.022
1
7471B
1/16/20 9:39
JAB
POA0212
Arsenic
1.6
mg/kg dry
1.3
0.17
1
6010D
1/17/20 19:25
JAB
POA0162
Barium
71
mg/kg dry
13
3.9
1
6010D
1/17/20 19:25
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.65
0.044
1
6010D
1/17/20 19:25
JAB
POA0162
Chromium
10
mg/kg dry
1.3
0.098
1
6010D
1/17/20 19:25
JAB
POA0162
Lead
15
mg/kg dry
1.3
0.22
1
6010D
1/17/20 19:25
JAB
POA0162
Selenium
BRL
mg/kg dry
1.3
0.36
1
6010D
1/17/20 19:25
JAB
POA0162
Silver
BRL
mg/kg dry
0.65
0.040
1
6010D
1/17/20 19:25
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-1
Attn: Katie Lippard Sample ID: 0010154-01
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 13:45
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0069
0.00084
1
8260D
1/14/20 13:18
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0069
0.0010
1
8260D
1/14/20 13:18
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0069
0.00050
1
8260D
1/14/20 13:18
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0069
0.00074
1
8260D
1/14/20 13:18
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0069
0.0012
1
8260D
1/14/20 13:18
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0069
0.0013
1
8260D
1/14/20 13:18
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0069
0.0011
1
8260D
1/14/20 13:18
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.014
0.00098
1
8260D
1/14/20 13:18
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0069
0.00078
1
8260D
1/14/20 13:18
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.014
0.00066
1
8260D
1/14/20 13:18
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0069
0.00073
1
8260D
1/14/20 13:18
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0069
0.00062
1
8260D
1/14/20 13:18
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0069
0.00077
1
8260D
1/14/20 13:18
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0069
0.00082
1
8260D
1/14/20 13:18
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0069
0.0010
1
8260D
1/14/20 13:18
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0069
0.00086
1
8260D
1/14/20 13:18
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0069
0.00085
1
8260D
1/14/20 13:18
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0069
0.00057
1
8260D
1/14/20 13:18
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0069
0.00087
1
8260D
1/14/20 13:18
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0069
0.00086
1
8260D
1/14/20 13:18
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0069
0.00092
1
8260D
1/14/20 13:18
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0069
0.00078
1
8260D
1/14/20 13:18
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0069
0.0017
1
8260D
1/14/20 13:18
TBL
POA0183
Acetone
BRL
mg/kg dry
0.027
0.0018
1
8260D
1/14/20 13:18
TBL
POA0183
Benzene
BRL
mg/kg dry
0.0069
0.0011
1
8260D
1/14/20 13:18
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0069
0.00095
1
8260D
1/14/20 13:18
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0069
0.0011
1
8260D
1/14/20 13:18
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0069
0.00065
1
8260D
1/14/20 13:18
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0069
0.00053
1
8260D
1/14/20 13:18
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.014
0.0034
1
8260D
1/14/20 13:18
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0069
0.0014
1
8260D
1/14/20 13:18
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0069
0.0011
1
8260D
1/14/20 13:18
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.014
0.0013
1
8260D
1/14/20 13:18
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0069
0.00084
1
8260D
1/14/20 13:18
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.014
0.0021
1
8260D
1/14/20 13:18
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0069
0.0011
1
8260D
1/14/20 13:18
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0069
0.00068
1
8260D
1/14/20 13:18
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0069
0.00046
1
8260D
1/14/20 13:18
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.014
0.0019
1
8260D
1/14/20 13:18
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0069
0.0010
1
8260D
1/14/20 13:18
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0069
0.0010
1
8260D
1/14/20 13:18
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0069
0.00080
1
8260D
1/14/20 13:18
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-1
Attn: Katie Lippard Sample ID: 0010154-01
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 13:45
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.014
0.0018
1
8260D
1/14/20 13:18
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.027
0.00048
1
8260D
1/14/20 13:18
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.027
0.0016
1
8260D
1/14/20 13:18
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.027
0.00056
1
8260D
1/14/20 13:18
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0069
0.0011
1
8260D
1/14/20 13:18
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0069
0.00096
1
8260D
1/14/20 13:18
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.014
0.00069
1
8260D
1/14/20 13:18
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0069
0.00064
1
8260D
1/14/20 13:18
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0069
0.0010
1
8260D
1/14/20 13:18
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0069
0.00073
1
8260D
1/14/20 13:18
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0069
0.00074
1
8260D
1/14/20 13:18
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0069
0.00067
1
8260D
1/14/20 13:18
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0069
0.00082
1
8260D
1/14/20 13:18
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0069
0.0012
1
8260D
1/14/20 13:18
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0069
0.0011
1
8260D
1/14/20 13:18
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0069
0.0013
1
8260D
1/14/20 13:18
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0069
0.00059
1
8260D
1/14/20 13:18
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0069
0.0013
1
8260D
1/14/20 13:18
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.014
0.0019
1
8260D
1/14/20 13:18
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.014
0.00074
1
8260D
1/14/20 13:18
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.014
0.0014
1
8260D
1/14/20 13:18
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.021
0.0025
1
8260D
1/14/20 13:18
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
91 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-2
Attn: Katie Lippard Sample ID: 0010154-02
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 14:16
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
79.3
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.83
0.15
1
8270E
1/15/20 18:27
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.83
0.13
1
8270E
1/15/20 18:27
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.83
0.12
1
8270E
1/15/20 18:27
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.41
0.13
1
8270E
1/15/20 18:27
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.83
0.013
1
8270E
1/15/20 18:27
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 18:27
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.83
0.20
1
8270E
1/15/20 18:27
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 18:27
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.41
0.17
1
8270E
1/15/20 18:27
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.49
1
8270E
1/15/20 18:27
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.83
0.22
1
8270E
1/15/20 18:27
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.83
0.21
1
8270E
1/15/20 18:27
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.83
0.20
1
8270E
1/15/20 18:27
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 18:27
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.83
0.016
1
8270E
1/15/20 18:27
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 18:27
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.83
0.14
1
8270E
1/15/20 18:27
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 18:27
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 18:27
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.46
1
8270E
1/15/20 18:27
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.83
0.19
1
8270E
1/15/20 18:27
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 18:27
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.41
0.10
1
8270E
1/15/20 18:27
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.25
1
8270E
1/15/20 18:27
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.83
0.20
1
8270E
1/15/20 18:27
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.83
0.019
1
8270E
1/15/20 18:27
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.83
0.016
1
8270E
1/15/20 18:27
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.83
0.0092
1
8270E
1/15/20 18:27
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 18:27
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.83
0.0099
1
8270E
1/15/20 18:27
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.83
0.0074
1
8270E
1/15/20 18:27
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.83
0.0077
1
8270E
1/15/20 18:27
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.83
0.0082
1
8270E
1/15/20 18:27
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.83
0.0088
1
8270E
1/15/20 18:27
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.5
0.69
1
8270E
1/15/20 18:27
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 18:27
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 18:27
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.83
0.13
1
8270E
1/15/20 18:27
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.41
0.15
1
8270E
1/15/20 18:27
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-2
Attn: Katie Lippard Sample ID: 0010154-02
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 14:16
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.83
0.19
1
8270E
1/15/20 18:27
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.41
0.14
1
8270E
1/15/20 18:27
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.83
0.0098
1
8270E
1/15/20 18:27
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.83
0.024
1
8270E
1/15/20 18:27
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.83
0.22
1
8270E
1/15/20 18:27
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.83
0.21
1
8270E
1/15/20 18:27
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.83
0.20
1
8270E
1/15/20 18:27
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.83
0.21
1
8270E
1/15/20 18:27
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.41
0.21
1
8270E
1/15/20 18:27
JMV
POA0191
Fluoranthene
BRL
mg/kg dry
0.83
0.0094
1
8270E
1/15/20 18:27
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.83
0.014
1
8270E
1/15/20 18:27
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 18:27
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.83
0.19
1
8270E
1/15/20 18:27
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.83
0.28
1
8270E
1/15/20 18:27
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.83
0.13
1
8270E
1/15/20 18:27
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.83
0.023
1
8270E
1/15/20 18:27
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 18:27
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.83
0.018
1
8270E
1/15/20 18:27
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.41
0.18
1
8270E
1/15/20 18:27
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.83
0.19
1
8270E
1/15/20 18:27
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.83
0.23
1
8270E
1/15/20 18:27
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.3
0.53
1
8270E
1/15/20 18:27
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.83
0.0090
1
8270E
1/15/20 18:27
JMV
POA0191
Phenol
BRL
mg/kg dry
0.83
0.14
1
8270E
1/15/20 18:27
JMV
POA0191
Pyrene
BRL
mg/kg dry
0.83
0.012
1
8270E
1/15/20 18:27
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.41
0.079
1
8270E
1/15/20 18:27
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
84 %
39-132
2-Fluorobiphenyl
79 %
44-115
2-Fluorophenol
78 %
35-115
Nitrobenzene-d5
71 %
37-122
Phenol-d5
74 %
34-121
Terphenyl-d14
81 %
54-127
Total Metals
Mercury
0.027 J
mg/kg dry
0.063
0.022
1
7471B
1/16/20 9:44
JAB
POA0212
Arsenic
1.5
mg/kg dry
1.3
0.17
1
6010D
1/17/20 19:53
JAB
POA0162
Barium
61
mg/kg dry
13
3.8
1
6010D
1/17/20 19:53
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.63
0.043
1
6010D
1/17/20 19:53
JAB
POA0162
Chromium
13
mg/kg dry
1.3
0.096
1
6010D
1/17/20 19:53
JAB
POA0162
Lead
12
mg/kg dry
1.3
0.21
1
6010D
1/17/20 19:53
JAB
POA0162
Selenium
BRL
mg/kg dry
1.3
0.35
1
6010D
1/17/20 19:53
JAB
POA0162
Silver
BRL
mg/kg dry
0.63
0.039
1
6010D
1/17/20 19:53
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-2
Attn: Katie Lippard Sample ID: 0010154-02
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 14:16
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0060
0.00073
1
8260D
1/14/20 13:48
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0060
0.00088
1
8260D
1/14/20 13:48
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0060
0.00044
1
8260D
1/14/20 13:48
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0060
0.00065
1
8260D
1/14/20 13:48
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0060
0.0011
1
8260D
1/14/20 13:48
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0060
0.0011
1
8260D
1/14/20 13:48
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00092
1
8260D
1/14/20 13:48
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00086
1
8260D
1/14/20 13:48
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0060
0.00068
1
8260D
1/14/20 13:48
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00057
1
8260D
1/14/20 13:48
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0060
0.00063
1
8260D
1/14/20 13:48
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0060
0.00054
1
8260D
1/14/20 13:48
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00067
1
8260D
1/14/20 13:48
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0060
0.00071
1
8260D
1/14/20 13:48
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0060
0.00090
1
8260D
1/14/20 13:48
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0060
0.00075
1
8260D
1/14/20 13:48
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00074
1
8260D
1/14/20 13:48
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0060
0.00050
1
8260D
1/14/20 13:48
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00076
1
8260D
1/14/20 13:48
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0060
0.00075
1
8260D
1/14/20 13:48
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0060
0.00080
1
8260D
1/14/20 13:48
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0060
0.00068
1
8260D
1/14/20 13:48
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0060
0.0015
1
8260D
1/14/20 13:48
TBL
POA0183
Acetone
0.021 J
mg/kg dry
0.024
0.0015
1
8260D
1/14/20 13:48
TBL
POA0183
Benzene
BRL
mg/kg dry
0.0060
0.00093
1
8260D
1/14/20 13:48
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0060
0.00083
1
8260D
1/14/20 13:48
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0060
0.00098
1
8260D
1/14/20 13:48
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0060
0.00057
1
8260D
1/14/20 13:48
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0060
0.00046
1
8260D
1/14/20 13:48
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.012
0.0029
1
8260D
1/14/20 13:48
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0060
0.0012
1
8260D
1/14/20 13:48
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0060
0.00093
1
8260D
1/14/20 13:48
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.012
0.0011
1
8260D
1/14/20 13:48
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0060
0.00073
1
8260D
1/14/20 13:48
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
8260D
1/14/20 13:48
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0060
0.00094
1
8260D
1/14/20 13:48
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00059
1
8260D
1/14/20 13:48
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0060
0.00040
1
8260D
1/14/20 13:48
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
1/14/20 13:48
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0060
0.00090
1
8260D
1/14/20 13:48
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0060
0.00088
1
8260D
1/14/20 13:48
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0060
0.00070
1
8260D
1/14/20 13:48
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-2
Attn: Katie Lippard Sample ID: 0010154-02
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 14:16
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0015
1
8260D
1/14/20 13:48
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.024
0.00041
1
8260D
1/14/20 13:48
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.024
0.0014
1
8260D
1/14/20 13:48
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.024
0.00049
1
8260D
1/14/20 13:48
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0060
0.00097
1
8260D
1/14/20 13:48
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0060
0.00084
1
8260D
1/14/20 13:48
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.012
0.00060
1
8260D
1/14/20 13:48
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0060
0.00056
1
8260D
1/14/20 13:48
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0060
0.00087
1
8260D
1/14/20 13:48
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0060
0.00064
1
8260D
1/14/20 13:48
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0060
0.00065
1
8260D
1/14/20 13:48
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0060
0.00058
1
8260D
1/14/20 13:48
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0060
0.00071
1
8260D
1/14/20 13:48
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0060
0.0011
1
8260D
1/14/20 13:48
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0060
0.00095
1
8260D
1/14/20 13:48
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0060
0.0011
1
8260D
1/14/20 13:48
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00051
1
8260D
1/14/20 13:48
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0060
0.0012
1
8260D
1/14/20 13:48
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
1/14/20 13:48
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.012
0.00065
1
8260D
1/14/20 13:48
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
1/14/20 13:48
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.018
0.0022
1
8260D
1/14/20 13:48
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
103 %
70-130
Dibromofluoromethane
109 %
84-123
Toluene-d8
88 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-3S
Attn: Katie Lippard Sample ID: 0010154-03
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 12:52
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
86.6
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.76
0.13
1
8270E
1/15/20 23:20
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.76
0.12
1
8270E
1/15/20 23:20
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.76
0.11
1
8270E
1/15/20 23:20
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.38
0.12
1
8270E
1/15/20 23:20
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.76
0.012
1
8270E
1/15/20 23:20
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.76
0.16
1
8270E
1/15/20 23:20
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.76
0.18
1
8270E
1/15/20 23:20
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.76
0.15
1
8270E
1/15/20 23:20
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.38
0.16
1
8270E
1/15/20 23:20
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.7
0.45
1
8270E
1/15/20 23:20
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.76
0.20
1
8270E
1/15/20 23:20
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.76
0.20
1
8270E
1/15/20 23:20
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.76
0.19
1
8270E
1/15/20 23:20
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.76
0.15
1
8270E
1/15/20 23:20
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.76
0.015
1
8270E
1/15/20 23:20
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.76
0.15
1
8270E
1/15/20 23:20
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.76
0.13
1
8270E
1/15/20 23:20
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.76
0.15
1
8270E
1/15/20 23:20
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.76
0.16
1
8270E
1/15/20 23:20
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.7
0.42
1
8270E
1/15/20 23:20
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.76
0.18
1
8270E
1/15/20 23:20
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.76
0.15
1
8270E
1/15/20 23:20
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.38
0.092
1
8270E
1/15/20 23:20
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.23
1
8270E
1/15/20 23:20
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.76
0.19
1
8270E
1/15/20 23:20
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.76
0.017
1
8270E
1/15/20 23:20
JMV
POA0191
Acenaphthylene
0.047 J
mg/kg dry
0.76
0.015
1
8270E
1/15/20 23:20
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.76
0.0084
1
8270E
1/15/20 23:20
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.76
0.16
1
8270E
1/15/20 23:20
JMV
POA0191
Benzo(a)anthracene
0.17 J
mg/kg dry
0.76
0.0091
1
8270E
1/15/20 23:20
JMV
POA0191
Benzo(a)pyrene
0.27 J
mg/kg dry
0.76
0.0068
1
8270E
1/15/20 23:20
JMV
POA0191
Benzo(b)fluoranthene
0.44 J
mg/kg dry
0.76
0.0070
1
8270E
1/15/20 23:20
JMV
POA0191
Benzo(g,h,i)perylene
0.26 J
mg/kg dry
0.76
0.0075
1
8270E
1/15/20 23:20
JMV
POA0191
Benzo(k)fluoranthene
0.16 J
mg/kg dry
0.76
0.0081
1
8270E
1/15/20 23:20
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.3
0.63
1
8270E
1/15/20 23:20
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.76
0.14
1
8270E
1/15/20 23:20
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.76
0.15
1
8270E
1/15/20 23:20
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.76
0.12
1
8270E
1/15/20 23:20
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.38
0.14
1
8270E
1/15/20 23:20
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-3S
Attn: Katie Lippard Sample ID: 0010154-03
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 12:52
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.76
0.17
1
8270E
1/15/20 23:20
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.38
0.13
1
8270E
1/15/20 23:20
JMV
POA0191
Chrysene
0.29 J
mg/kg dry
0.76
0.0090
1
8270E
1/15/20 23:20
JMV
POA0191
Dibenzo(a,h)anthracene
0.048 J
mg/kg dry
0.76
0.022
1
8270E
1/15/20 23:20
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.76
0.21
1
8270E
1/15/20 23:20
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.76
0.20
1
8270E
1/15/20 23:20
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.76
0.18
1
8270E
1/15/20 23:20
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.76
0.19
1
8270E
1/15/20 23:20
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.38
0.20
1
8270E
1/15/20 23:20
JMV
POA0191
Fluoranthene
0.34 J
mg/kg dry
0.76
0.0086
1
8270E
1/15/20 23:20
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.76
0.013
1
8270E
1/15/20 23:20
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.76
0.17
1
8270E
1/15/20 23:20
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.76
0.17
1
8270E
1/15/20 23:20
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.76
0.26
1
8270E
1/15/20 23:20
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.76
0.12
1
8270E
1/15/20 23:20
JMV
POA0191
Indeno(1,2,3-cd)pyrene
0.26 J
mg/kg dry
0.76
0.021
1
8270E
1/15/20 23:20
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.76
0.16
1
8270E
1/15/20 23:20
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.76
0.016
1
8270E
1/15/20 23:20
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.38
0.16
1
8270E
1/15/20 23:20
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.76
0.18
1
8270E
1/15/20 23:20
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.76
0.21
1
8270E
1/15/20 23:20
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.2
0.49
1
8270E
1/15/20 23:20
JMV
POA0191
Phenanthrene
0.26 J
mg/kg dry
0.76
0.0083
1
8270E
1/15/20 23:20
JMV
POA0191
Phenol
BRL
mg/kg dry
0.76
0.12
1
8270E
1/15/20 23:20
JMV
POA0191
Pyrene
0.32 J
mg/kg dry
0.76
0.011
1
8270E
1115/20 23:20
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.38
0.073
1
8270E
1/15/20 23:20
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
73 %
39-132
2-Fluorobiphenyl
71 %
44-115
2-Fluorophenol
65 %
35-115
Nitrobenzene-d5
64 %
37-122
Phenol-d5
65 %
34-121
Terphenyl-d14
78 %
54-127
Total Metals
Mercury
0.20
mg/kg dry
0.058
0.020
1
7471B
1/16/20 9:49
JAB
POA0212
Arsenic
3.9
mg/kg dry
1.2
0.15
1
6010D
1/17/20 20:02
JAB
POA0162
Barium
170
mg/kg dry
58
17
5
6010D
1/20/20 12:19
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.58
0.039
1
6010D
1/17/20 20:02
JAB
POA0162
Chromium
20
mg/kg dry
1.2
0.087
1
6010D
1/17/20 20:02
JAB
POA0162
Lead
140
mg/kg dry
1.2
0.19
1
6010D
1/17/20 20:02
JAB
POA0162
Selenium
BRL
mg/kg dry
1.2
0.32
1
6010D
1/17/20 20:02
JAB
POA0162
Silver
BRL
mg/kg dry
0.58
0.035
1
6010D
1/17/20 20:02
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-3S
Attn: Katie Lippard Sample ID: 0010154-03
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 12:52
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0043
0.00052
1
8260D
1/14/20 14:18
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0043
0.00063
1
8260D
1/14/20 14:18
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0043
0.00031
1
8260D
1/14/20 14:18
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0043
0.00046
1
8260D
1/14/20 14:18
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0043
0.00077
1
8260D
1/14/20 14:18
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0043
0.00079
1
8260D
1/14/20 14:18
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0043
0.00066
1
8260D
1/14/20 14:18
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0086
0.00061
1
8260D
1/14/20 14:18
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0043
0.00049
1
8260D
1/14/20 14:18
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0086
0.00041
1
8260D
1/14/20 14:18
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0043
0.00045
1
8260D
1/14/20 14:18
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0043
0.00038
1
8260D
1/14/20 14:18
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0043
0.00048
1
8260D
1/14/20 14:18
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0043
0.00051
1
8260D
1/14/20 14:18
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0043
0.00064
1
8260D
1/14/20 14:18
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0043
0.00054
1
8260D
1/14/20 14:18
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0043
0.00053
1
8260D
1/14/20 14:18
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0043
0.00036
1
8260D
1/14/20 14:18
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0043
0.00054
1
8260D
1/14/20 14:18
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0043
0.00053
1
8260D
1/14/20 14:18
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0043
0.00057
1
8260D
1/14/20 14:18
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0043
0.00049
1
8260D
1/14/20 14:18
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0043
0.0011
1
8260D
1/14/20 14:18
TBL
POA0183
Acetone
0.072
mg/kg dry
0.017
0.0011
1
8260D
1/14/20 14:18
TBL
POA0183
Benzene
BRL CCVH
mg/kg dry
0.0043
0.00067
1
8260D
1/14/20 14:18
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0043
0.00059
1
8260D
1/14/20 14:18
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0043
0.00070
1
8260D
1/14/20 14:18
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0043
0.00041
1
8260D
1/14/20 14:18
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0043
0.00033
1
8260D
1/14/20 14:18
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.0086
0.0021
1
8260D
1/14/20 14:18
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0043
0.00084
1
8260D
1/14/20 14:18
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0043
0.00067
1
8260D
1/14/20 14:18
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.0086
0.00082
1
8260D
1/14/20 14:18
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0043
0.00052
1
8260D
1/14/20 14:18
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.0086
0.0013
1
8260D
1/14/20 14:18
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0043
0.00067
1
8260D
1/14/20 14:18
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0043
0.00042
1
8260D
1/14/20 14:18
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0043
0.00029
1
8260D
1/14/20 14:18
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.0086
0.0012
1
8260D
1/14/20 14:18
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0043
0.00064
1
8260D
1/14/20 14:18
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0043
0.00063
1
8260D
1/14/20 14:18
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0043
0.00050
1
8260D
1/14/20 14:18
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-3S
Attn: Katie Lippard Sample ID: 0010154-03
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 12:52
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.0086
0.0011
1
8260D
1/14/20 14:18
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.017
0.00030
1
8260D
1/14/20 14:18
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.017
0.0010
1
8260D
1/14/20 14:18
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.017
0.00035
1
8260D
1/14/20 14:18
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0043
0.00069
1
8260D
1/14/20 14:18
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0043
0.00060
1
8260D
1/14/20 14:18
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.0086
0.00043
1
8260D
1/14/20 14:18
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0043
0.00040
1
8260D
1/14/20 14:18
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0043
0.00062
1
8260D
1/14/20 14:18
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0043
0.00046
1
8260D
1/14/20 14:18
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0043
0.00046
1
8260D
1/14/20 14:18
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0043
0.00042
1
8260D
1/14/20 14:18
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0043
0.00051
1
8260D
1/14/20 14:18
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0043
0.00077
1
8260D
1/14/20 14:18
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0043
0.00068
1
8260D
1/14/20 14:18
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0043
0.00082
1
8260D
1/14/20 14:18
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0043
0.00037
1
8260D
1/14/20 14:18
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0043
0.00083
1
8260D
1/14/20 14:18
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.0086
0.0012
1
8260D
1/14/20 14:18
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.0086
0.00046
1
8260D
1/14/20 14:18
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.0086
0.00085
1
8260D
1/14/20 14:18
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.013
0.0015
1
8260D
1/14/20 14:18
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101 %
70-130
Dibromofluoromethane
114 %
84-123
Toluene-d8
89 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-3D
Attn: Katie Lippard Sample ID: 0010154-04
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 13:06
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
78.3
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.84
0.15
1
8270E
1/15/20 18:50
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.84
0.14
1
8270E
1/15/20 18:50
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.84
0.12
1
8270E
1/15/20 18:50
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.42
0.13
1
8270E
1/15/20 18:50
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.84
0.013
1
8270E
1/15/20 18:50
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.84
0.18
1
8270E
1/15/20 18:50
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.84
0.20
1
8270E
1/15/20 18:50
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.84
0.16
1
8270E
1/15/20 18:50
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.42
0.17
1
8270E
1/15/20 18:50
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.49
1
8270E
1/15/20 18:50
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.84
0.22
1
8270E
1/15/20 18:50
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.84
0.22
1
8270E
1/15/20 18:50
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.84
0.20
1
8270E
1/15/20 18:50
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.84
0.16
1
8270E
1/15/20 18:50
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.84
0.016
1
8270E
1/15/20 18:50
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.84
0.16
1
8270E
1/15/20 18:50
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.84
0.14
1
8270E
1/15/20 18:50
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.84
0.17
1
8270E
1/15/20 18:50
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.84
0.18
1
8270E
1/15/20 18:50
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.46
1
8270E
1/15/20 18:50
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.84
0.20
1
8270E
1/15/20 18:50
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.84
0.16
1
8270E
1/15/20 18:50
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.42
0.10
1
8270E
1/15/20 18:50
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
8270E
1/15/20 18:50
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.84
0.21
1
8270E
1/15/20 18:50
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.84
0.019
1
8270E
1/15/20 18:50
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.84
0.017
1
8270E
1/15/20 18:50
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.84
0.0093
1
8270E
1/15/20 18:50
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.84
0.18
1
8270E
1/15/20 18:50
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.84
0.010
1
8270E
1/15/20 18:50
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.84
0.0075
1
8270E
1/15/20 18:50
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.84
0.0078
1
8270E
1/15/20 18:50
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.84
0.0083
1
8270E
1/15/20 18:50
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.84
0.0089
1
8270E
1/15/20 18:50
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.5
0.70
1
8270E
1/15/20 18:50
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.84
0.16
1
8270E
1/15/20 18:50
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.84
0.16
1
8270E
1/15/20 18:50
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.84
0.13
1
8270E
1/15/20 18:50
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.42
0.15
1
8270E
1/15/20 18:50
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-3D
Attn: Katie Lippard Sample ID: 0010154-04
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 13:06
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.84
0.19
1
8270E
1/15/20 18:50
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.42
0.14
1
8270E
1/15/20 18:50
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.84
0.0099
1
8270E
1/15/20 18:50
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.84
0.024
1
8270E
1/15/20 18:50
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.84
0.23
1
8270E
1/15/20 18:50
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.84
0.22
1
8270E
1/15/20 18:50
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.84
0.20
1
8270E
1/15/20 18:50
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.84
0.21
1
8270E
1/15/20 18:50
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.42
0.22
1
8270E
1/15/20 18:50
JMV
POA0191
Fluoranthene
BRL
mg/kg dry
0.84
0.0095
1
8270E
1/15/20 18:50
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.84
0.014
1
8270E
1/15/20 18:50
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.84
0.18
1
8270E
1/15/20 18:50
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.84
0.19
1
8270E
1/15/20 18:50
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.84
0.29
1
8270E
1/15/20 18:50
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.84
0.13
1
8270E
1/15/20 18:50
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.84
0.024
1
8270E
1/15/20 18:50
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.84
0.18
1
8270E
1/15/20 18:50
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.84
0.018
1
8270E
1/15/20 18:50
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.42
0.18
1
8270E
1/15/20 18:50
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.84
0.19
1
8270E
1/15/20 18:50
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.84
0.23
1
8270E
1/15/20 18:50
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.3
0.54
1
8270E
1/15/20 18:50
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.84
0.0092
1
8270E
1/15/20 18:50
JMV
POA0191
Phenol
BRL
mg/kg dry
0.84
0.14
1
8270E
1/15/20 18:50
JMV
POA0191
Pyrene
BRL
mg/kg dry
0.84
0.012
1
8270E
1/15/20 18:50
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.42
0.080
1
8270E
1/15/20 18:50
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
75 %
39-132
2-Fluorobiphenyl
76 %
44-115
2-Fluorophenol
71 %
35-115
Nitrobenzene-d5
71 %
37-122
Phenol-d5
71 %
34-121
Terphenyl-d14
78 %
54-127
Total Metals
Mercury
0.060 J
mg/kg dry
0.064
0.022
1
7471B
1/16/20 9:53
JAB
POA0212
Arsenic
2.8
mg/kg dry
1.3
0.17
1
6010D
1117/20 20:10
JAB
POA0162
Barium
44
mg/kg dry
13
3.8
1
6010D
1/17/20 20:10
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.64
0.043
1
6010D
1/17/20 20:10
JAB
POA0162
Chromium
24
mg/kg dry
1.3
0.097
1
6010D
1/17/20 20:10
JAB
POA0162
Lead
25
mg/kg dry
1.3
0.21
1
6010D
1/17/20 20:10
JAB
POA0162
Selenium
BRL
mg/kg dry
1.3
0.35
1
6010D
1/17/20 20:10
JAB
POA0162
Silver
BRL
mg/kg dry
0.64
0.039
1
6010D
1/17/20 20:10
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-3D
Attn: Katie Lippard Sample ID: 0010154-04
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 13:06
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0057
0.00070
1
8260D
1/14/20 14:48
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0057
0.00084
1
8260D
1/14/20 14:48
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0057
0.00042
1
8260D
1/14/20 14:48
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0057
0.00062
1
8260D
1/14/20 14:48
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0057
0.0010
1
8260D
1/14/20 14:48
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0057
0.0010
1
8260D
1/14/20 14:48
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00088
1
8260D
1/14/20 14:48
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00082
1
8260D
1/14/20 14:48
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0057
0.00065
1
8260D
1/14/20 14:48
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00055
1
8260D
1/14/20 14:48
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0057
0.00061
1
8260D
1/14/20 14:48
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0057
0.00051
1
8260D
1/14/20 14:48
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00064
1
8260D
1/14/20 14:48
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0057
0.00068
1
8260D
1/14/20 14:48
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0057
0.00086
1
8260D
1/14/20 14:48
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0057
0.00072
1
8260D
1/14/20 14:48
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00071
1
8260D
1/14/20 14:48
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0057
0.00048
1
8260D
1/14/20 14:48
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00073
1
8260D
1/14/20 14:48
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0057
0.00071
1
8260D
1/14/20 14:48
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0057
0.00077
1
8260D
1/14/20 14:48
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0057
0.00065
1
8260D
1/14/20 14:48
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0057
0.0014
1
8260D
1/14/20 14:48
TBL
POA0183
Acetone
0.076
mg/kg dry
0.023
0.0015
1
8260D
1/14/20 14:48
TBL
POA0183
Benzene
BRL
mg/kg dry
0.0057
0.00089
1
8260D
1/14/20 14:48
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0057
0.00079
1
8260D
1/14/20 14:48
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0057
0.00094
1
8260D
1/14/20 14:48
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0057
0.00054
1
8260D
1/14/20 14:48
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0057
0.00044
1
8260D
1/14/20 14:48
TBL
POA0183
Bromomethane
0.0029 J
mg/kg dry
0.011
0.0028
1
8260D
1/14/20 14:48
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0057
0.0011
1
8260D
1/14/20 14:48
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0057
0.00089
1
8260D
1/14/20 14:48
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.011
0.0011
1
8260D
1/14/20 14:48
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0057
0.00070
1
8260D
1/14/20 14:48
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.011
0.0017
1
8260D
1/14/20 14:48
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0057
0.00090
1
8260D
1/14/20 14:48
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00056
1
8260D
1/14/20 14:48
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0057
0.00038
1
8260D
1/14/20 14:48
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0016
1
8260D
1/14/20 14:48
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0057
0.00086
1
8260D
1/14/20 14:48
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0057
0.00084
1
8260D
1/14/20 14:48
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0057
0.00067
1
8260D
1/14/20 14:48
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-3D
Attn: Katie Lippard Sample ID: 0010154-04
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 13:06
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.011
0.0015
1
8260D
1/14/20 14:48
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.023
0.00040
1
8260D
1/14/20 14:48
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.023
0.0013
1
8260D
1/14/20 14:48
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.023
0.00047
1
8260D
1/14/20 14:48
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0057
0.00093
1
8260D
1/14/20 14:48
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0057
0.00080
1
8260D
1/14/20 14:48
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.011
0.00058
1
8260D
1/14/20 14:48
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0057
0.00054
1
8260D
1/14/20 14:48
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0057
0.00083
1
8260D
1/14/20 14:48
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0057
0.00061
1
8260D
1/14/20 14:48
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0057
0.00062
1
8260D
1/14/20 14:48
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0057
0.00056
1
8260D
1/14/20 14:48
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0057
0.00068
1
8260D
1/14/20 14:48
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0057
0.0010
1
8260D
1/14/20 14:48
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0057
0.00091
1
8260D
1/14/20 14:48
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0057
0.0011
1
8260D
1/14/20 14:48
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00049
1
8260D
1/14/20 14:48
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0057
0.0011
1
8260D
1/14/20 14:48
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
1/14/20 14:48
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.011
0.00062
1
8260D
1/14/20 14:48
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260D
1/14/20 14:48
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.017
0.0021
1
8260D
1/14/20 14:48
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101 %
70-130
Dibromofluoromethane
107 %
84-123
Toluene-d8
91 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-4S
Attn: Katie Lippard Sample ID: 0010154-05
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 10:20
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
88.0
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.75
0.13
1
8270E
1/15/20 19:12
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.75
0.12
1
8270E
1/15/20 19:12
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.75
0.11
1
8270E
1/15/20 19:12
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.37
0.12
1
8270E
1/15/20 19:12
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.75
0.011
1
8270E
1/15/20 19:12
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.75
0.16
1
8270E
1/15/20 19:12
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.75
0.18
1
8270E
1/15/20 19:12
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.75
0.15
1
8270E
1/15/20 19:12
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.37
0.16
1
8270E
1/15/20 19:12
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.7
0.44
1
8270E
1/15/20 19:12
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.75
0.20
1
8270E
1/15/20 19:12
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.75
0.19
1
8270E
1/15/20 19:12
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.75
0.18
1
8270E
1/15/20 19:12
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.75
0.14
1
8270E
1/15/20 19:12
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.75
0.015
1
8270E
1/15/20 19:12
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.75
0.14
1
8270E
1/15/20 19:12
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.75
0.12
1
8270E
1/15/20 19:12
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.75
0.15
1
8270E
1/15/20 19:12
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.75
0.16
1
8270E
1/15/20 19:12
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.7
0.41
1
8270E
1/15/20 19:12
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.75
0.18
1
8270E
1/15/20 19:12
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.75
0.14
1
8270E
1/15/20 19:12
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.37
0.091
1
8270E
1/15/20 19:12
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.1
0.23
1
8270E
1/15/20 19:12
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.75
0.19
1
8270E
1/15/20 19:12
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.75
0.017
1
8270E
1/15/20 19:12
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.75
0.015
1
8270E
1/15/20 19:12
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.75
0.0083
1
8270E
1/15/20 19:12
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.75
0.16
1
8270E
1/15/20 19:12
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.75
0.0090
1
8270E
1/15/20 19:12
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.75
0.0067
1
8270E
1/15/20 19:12
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.75
0.0069
1
8270E
1/15/20 19:12
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.75
0.0074
1
8270E
1/15/20 19:12
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.75
0.0079
1
8270E
1/15/20 19:12
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.3
0.62
1
8270E
1/15/20 19:12
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.75
0.14
1
8270E
1/15/20 19:12
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.75
0.14
1
8270E
1/15/20 19:12
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.75
0.12
1
8270E
1/15/20 19:12
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.37
0.13
1
8270E
1/15/20 19:12
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-4S
Attn: Katie Lippard Sample ID: 0010154-05
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 10:20
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.75
0.17
1
8270E
1/15/20 19:12
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.37
0.13
1
8270E
1/15/20 19:12
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.75
0.0089
1
8270E
1/15/20 19:12
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.75
0.022
1
8270E
1/15/20 19:12
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.75
0.20
1
8270E
1/15/20 19:12
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.75
0.19
1
8270E
1/15/20 19:12
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.75
0.18
1
8270E
1/15/20 19:12
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.75
0.19
1
8270E
1/15/20 19:12
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.37
0.19
1
8270E
1/15/20 19:12
JMV
POA0191
Fluoranthene
BRL
mg/kg dry
0.75
0.0085
1
8270E
1/15/20 19:12
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.75
0.013
1
8270E
1/15/20 19:12
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.75
0.16
1
8270E
1/15/20 19:12
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.75
0.17
1
8270E
1/15/20 19:12
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.75
0.26
1
8270E
1/15/20 19:12
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.75
0.12
1
8270E
1/15/20 19:12
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.75
0.021
1
8270E
1/15/20 19:12
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.75
0.16
1
8270E
1/15/20 19:12
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.75
0.016
1
8270E
1/15/20 19:12
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.37
0.16
1
8270E
1/15/20 19:12
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.75
0.17
1
8270E
1/15/20 19:12
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.75
0.21
1
8270E
1/15/20 19:12
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.1
0.48
1
8270E
1/15/20 19:12
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.75
0.0082
1
8270E
1/15/20 19:12
JMV
POA0191
Phenol
BRL
mg/kg dry
0.75
0.12
1
8270E
1/15/20 19:12
JMV
POA0191
Pyrene
BRL
mg/kg dry
0.75
0.011
1
8270E
1/15/20 19:12
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.37
0.072
1
8270E
1/15/20 19:12
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
77 %
39-132
2-Fluorobiphenyl
72 %
44-115
2-Fluorophenol
71 %
35-115
Nitrobenzene-d5
64 %
37-122
Phenol-d5
68 %
34-121
Terphenyl-d14
76 %
54-127
Total Metals
Mercury
0.11
mg/kg dry
0.057
0.020
1
7471B
1/16/20 9:58
JAB
POA0212
Arsenic
2.3
mg/kg dry
1.1
0.15
1
6010D
1/17/20 20:18
JAB
POA0162
Barium
42
mg/kg dry
11
3.4
1
6010D
1/17/20 20:18
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.57
0.038
1
6010D
1/17/20 20:18
JAB
POA0162
Chromium
18
mg/kg dry
1.1
0.086
1
6010D
1/17/20 20:18
JAB
POA0162
Lead
91
mg/kg dry
1.1
0.19
1
6010D
1/17/20 20:18
JAB
POA0162
Selenium
BRL
mg/kg dry
1.1
0.31
1
6010D
1/17/20 20:18
JAB
POA0162
Silver
BRL
mg/kg dry
0.57
0.035
1
6010D
1/17/20 20:18
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-4S
Attn: Katie Lippard Sample ID: 0010154-05
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 10:20
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0055
0.00067
1
8260D
1/14/20 15:18
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0055
0.00081
1
8260D
1/14/20 15:18
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0055
0.00040
1
8260D
1/14/20 15:18
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0055
0.00060
1
8260D
1/14/20 15:18
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0055
0.00099
1
8260D
1/14/20 15:18
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0055
0.0010
1
8260D
1/14/20 15:18
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0055
0.00085
1
8260D
1/14/20 15:18
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00079
1
8260D
1/14/20 15:18
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0055
0.00063
1
8260D
1/14/20 15:18
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00053
1
8260D
1/14/20 15:18
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0055
0.00058
1
8260D
1/14/20 15:18
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0055
0.00049
1
8260D
1/14/20 15:18
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0055
0.00062
1
8260D
1/14/20 15:18
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0055
0.00066
1
8260D
1/14/20 15:18
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0055
0.00083
1
8260D
1/14/20 15:18
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0055
0.00069
1
8260D
1/14/20 15:18
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0055
0.00069
1
8260D
1/14/20 15:18
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0055
0.00046
1
8260D
1/14/20 15:18
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0055
0.00070
1
8260D
1/14/20 15:18
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0055
0.00069
1
8260D
1/14/20 15:18
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0055
0.00074
1
8260D
1/14/20 15:18
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0055
0.00063
1
8260D
1/14/20 15:18
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0055
0.0014
1
8260D
1/14/20 15:18
TBL
POA0183
Acetone
0.027
mg/kg dry
0.022
0.0014
1
8260D
1/14/20 15:18
TBL
POA0183
Benzene
0.014 CCVH
mg/kg dry
0.0055
0.00086
1
8260D
1114/20 15:18
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0055
0.00077
1
8260D
1/14/20 15:18
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0055
0.00091
1
8260D
1/14/20 15:18
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0055
0.00052
1
8260D
1/14/20 15:18
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0055
0.00043
1
8260D
1/14/20 15:18
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.011
0.0027
1
8260D
1/14/20 15:18
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0055
0.0011
1
8260D
1/14/20 15:18
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0055
0.00086
1
8260D
1/14/20 15:18
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.011
0.0010
1
8260D
1/14/20 15:18
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0055
0.00067
1
8260D
1/14/20 15:18
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.011
0.0017
1
8260D
1/14/20 15:18
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0055
0.00087
1
8260D
1/14/20 15:18
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0055
0.00054
1
8260D
1/14/20 15:18
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0055
0.00037
1
8260D
1/14/20 15:18
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0016
1
8260D
1/14/20 15:18
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0055
0.00083
1
8260D
1/14/20 15:18
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0055
0.00081
1
8260D
1/14/20 15:18
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0055
0.00064
1
8260D
1/14/20 15:18
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-4S
Attn: Katie Lippard Sample ID: 0010154-05
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 10:20
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.011
0.0014
1
8260D
1/14/20 15:18
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.022
0.00038
1
8260D
1/14/20 15:18
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.022
0.0013
1
8260D
1/14/20 15:18
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.022
0.00045
1
8260D
1/14/20 15:18
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0055
0.00089
1
8260D
1/14/20 15:18
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0055
0.00077
1
8260D
1/14/20 15:18
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.011
0.00056
1
8260D
1/14/20 15:18
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0055
0.00052
1
8260D
1/14/20 15:18
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0055
0.00080
1
8260D
1/14/20 15:18
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0055
0.00059
1
8260D
1/14/20 15:18
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0055
0.00060
1
8260D
1/14/20 15:18
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0055
0.00053
1
8260D
1/14/20 15:18
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0055
0.00066
1
8260D
1/14/20 15:18
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0055
0.0010
1
8260D
1/14/20 15:18
TBL
POA0183
Toluene
0.0026 J
mg/kg dry
0.0055
0.00088
1
8260D
1/14/20 15:18
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0055
0.0011
1
8260D
1/14/20 15:18
TBL
POA0183
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0055
0.00047
1
8260D
1/14/20 15:18
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0055
0.0011
1
8260D
1/14/20 15:18
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
1/14/20 15:18
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.011
0.00060
1
8260D
1/14/20 15:18
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260D
1/14/20 15:18
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.017
0.0020
1
8260D
1/14/20 15:18
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
106 %
84-123
Toluene-d8
89 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-41D
Attn: Katie Lippard Sample ID: 0010154-06
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 10:40
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
79.7
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.82
0.15
1
8270E
1/15/20 19:57
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.82
0.13
1
8270E
1/15/20 19:57
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.82
0.12
1
8270E
1/15/20 19:57
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.41
0.13
1
8270E
1/15/20 19:57
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.82
0.013
1
8270E
1/15/20 19:57
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.82
0.17
1
8270E
1/15/20 19:57
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 19:57
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 19:57
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.41
0.17
1
8270E
1/15/20 19:57
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.48
1
8270E
1/15/20 19:57
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.82
0.22
1
8270E
1/15/20 19:57
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.82
0.21
1
8270E
1/15/20 19:57
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 19:57
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 19:57
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.82
0.016
1
8270E
1/15/20 19:57
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 19:57
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.82
0.14
1
8270E
1/15/20 19:57
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 19:57
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.82
0.18
1
8270E
1/15/20 19:57
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.45
1
8270E
1/15/20 19:57
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.82
0.19
1
8270E
1/15/20 19:57
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 19:57
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.41
0.10
1
8270E
1/15/20 19:57
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.25
1
8270E
1/15/20 19:57
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 19:57
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.82
0.019
1
8270E
1/15/20 19:57
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.82
0.016
1
8270E
1/15/20 19:57
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.82
0.0091
1
8270E
1/15/20 19:57
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.82
0.18
1
8270E
1/15/20 19:57
JMV
POA0191
Benzo(a)anthracene
0.16 J
mg/kg dry
0.82
0.0098
1
8270E
1/15/20 19:57
JMV
POA0191
Benzo(a)pyrene
0.16 J
mg/kg dry
0.82
0.0074
1
8270E
1/15/20 19:57
JMV
POA0191
Benzo(k)fluoranthene
0.20 J
mg/kg dry
0.82
0.0076
1
8270E
1/15/20 19:57
JMV
POA0191
Benzo(g,h,i)perylene
0.14 J
mg/kg dry
0.82
0.0081
1
8270E
1/15/20 19:57
JMV
POA0191
Benzo(k)fluoranthene
0.075 J
mg/kg dry
0.82
0.0087
1
8270E
1/15/20 19:57
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.5
0.68
1
8270E
1/15/20 19:57
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.82
0.15
1
8270E
1/15/20 19:57
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 19:57
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.82
0.13
1
8270E
1/15/20 19:57
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.41
0.15
1
8270E
1/15/20 19:57
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-41D
Attn: Katie Lippard Sample ID: 0010154-06
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 10:40
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.82
0.19
1
8270E
1/15/20 19:57
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.41
0.14
1
8270E
1/15/20 19:57
JMV
POA0191
Chrysene
0.13 J
mg/kg dry
0.82
0.0097
1
8270E
1/15/20 19:57
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.82
0.024
1
8270E
1/15/20 19:57
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.82
0.22
1
8270E
1/15/20 19:57
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.82
0.21
1
8270E
1/15/20 19:57
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 19:57
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 19:57
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.41
0.21
1
8270E
1/15/20 19:57
JMV
POA0191
Fluoranthene
0.27 J
mg/kg dry
0.82
0.0093
1
8270E
1115/20 19:57
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.82
0.014
1
8270E
1/15/20 19:57
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.82
0.18
1
8270E
1/15/20 19:57
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.82
0.19
1
8270E
1/15/20 19:57
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.82
0.28
1
8270E
1/15/20 19:57
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.82
0.13
1
8270E
1/15/20 19:57
JMV
POA0191
Indeno(1,2,3-cd)pyrene
0.13 J
mg/kg dry
0.82
0.023
1
8270E
1/15/20 19:57
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.82
0.18
1
8270E
1/15/20 19:57
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.82
0.017
1
8270E
1/15/20 19:57
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.41
0.17
1
8270E
1/15/20 19:57
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.82
0.19
1
8270E
1/15/20 19:57
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.82
0.23
1
8270E
1/15/20 19:57
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.2
0.52
1
8270E
1/15/20 19:57
JMV
POA0191
Phenanthrene
0.11 J
mg/kg dry
0.82
0.0090
1
8270E
1/15/20 19:57
JMV
POA0191
Phenol
BRL
mg/kg dry
0.82
0.13
1
8270E
1/15/20 19:57
JMV
POA0191
Pyrene
0.27 J
mg/kg dry
0.82
0.012
1
8270E
1/15/20 19:57
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.41
0.079
1
8270E
1/15/20 19:57
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
66 %
39-132
2-Fluorobiphenyl
76 %
44-115
2-Fluorophenol
70 %
35-115
Nitrobenzene-d5
67 %
37-122
Phenol-d5
69 %
34-121
Terphenyl-d14
79 %
54-127
Total Metals
Mercury
0.069
mg/kg dry
0.063
0.022
1
7471B
1/16/20 10:02
JAB
POA0212
Arsenic
2.3
mg/kg dry
1.3
0.17
1
6010D
1/17/20 20:25
JAB
POA0162
Barium
29
mg/kg dry
13
3.8
1
6010D
1/17/20 20:25
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.63
0.042
1
6010D
1/17/20 20:25
JAB
POA0162
Chromium
26
mg/kg dry
1.3
0.095
1
6010D
1/17/20 20:25
JAB
POA0162
Lead
14
mg/kg dry
1.3
0.21
1
6010D
1/17/20 20:25
JAB
POA0162
Selenium
BRL
mg/kg dry
1.3
0.35
1
6010D
1/17/20 20:25
JAB
POA0162
Silver
BRL
mg/kg dry
0.63
0.039
1
6010D
1/17/20 20:25
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-41D
Attn: Katie Lippard Sample ID: 0010154-06
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 10:40
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0062
0.00076
1
8260D
1/14/20 15:48
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0062
0.00092
1
8260D
1/14/20 15:48
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0062
0.00045
1
8260D
1/14/20 15:48
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0062
0.00067
1
8260D
1/14/20 15:48
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0062
0.0011
1
8260D
1/14/20 15:48
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0062
0.0011
1
8260D
1/14/20 15:48
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0062
0.00096
1
8260D
1/14/20 15:48
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00089
1
8260D
1/14/20 15:48
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0062
0.00071
1
8260D
1/14/20 15:48
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00059
1
8260D
1/14/20 15:48
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0062
0.00066
1
8260D
1/14/20 15:48
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0062
0.00056
1
8260D
1/14/20 15:48
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0062
0.00069
1
8260D
1/14/20 15:48
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0062
0.00074
1
8260D
1/14/20 15:48
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0062
0.00094
1
8260D
1/14/20 15:48
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0062
0.00078
1
8260D
1/14/20 15:48
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0062
0.00077
1
8260D
1/14/20 15:48
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0062
0.00052
1
8260D
1/14/20 15:48
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0062
0.00079
1
8260D
1/14/20 15:48
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0062
0.00078
1
8260D
1/14/20 15:48
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0062
0.00083
1
8260D
1/14/20 15:48
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0062
0.00071
1
8260D
1/14/20 15:48
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0062
0.0016
1
8260D
1/14/20 15:48
TBL
POA0183
Acetone
0.030
mg/kg dry
0.025
0.0016
1
8260D
1/14/20 15:48
TBL
POA0183
Benzene
BRL
mg/kg dry
0.0062
0.00097
1
8260D
1/14/20 15:48
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0062
0.00086
1
8260D
1/14/20 15:48
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0062
0.0010
1
8260D
1/14/20 15:48
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0062
0.00059
1
8260D
1/14/20 15:48
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0062
0.00048
1
8260D
1/14/20 15:48
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.012
0.0031
1
8260D
1/14/20 15:48
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0062
0.0012
1
8260D
1/14/20 15:48
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0062
0.00097
1
8260D
1/14/20 15:48
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.012
0.0012
1
8260D
1/14/20 15:48
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0062
0.00076
1
8260D
1/14/20 15:48
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.012
0.0019
1
8260D
1/14/20 15:48
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0062
0.00098
1
8260D
1/14/20 15:48
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0062
0.00061
1
8260D
1/14/20 15:48
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0062
0.00042
1
8260D
1/14/20 15:48
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0018
1
8260D
1/14/20 15:48
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0062
0.00094
1
8260D
1/14/20 15:48
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0062
0.00091
1
8260D
1/14/20 15:48
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0062
0.00072
1
8260D
1/14/20 15:48
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-41D
Attn: Katie Lippard Sample ID: 0010154-06
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/08/20 10:40
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0016
1
8260D
1/14/20 15:48
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.025
0.00043
1
8260D
1/14/20 15:48
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.025
0.0015
1
8260D
1/14/20 15:48
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.025
0.00051
1
8260D
1/14/20 15:48
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0062
0.0010
1
8260D
1/14/20 15:48
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0062
0.00087
1
8260D
1/14/20 15:48
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.012
0.00063
1
8260D
1/14/20 15:48
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0062
0.00058
1
8260D
1/14/20 15:48
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0062
0.00090
1
8260D
1/14/20 15:48
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0062
0.00066
1
8260D
1/14/20 15:48
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0062
0.00067
1
8260D
1/14/20 15:48
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0062
0.00060
1
8260D
1/14/20 15:48
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0062
0.00074
1
8260D
1/14/20 15:48
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0062
0.0011
1
8260D
1/14/20 15:48
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0062
0.00099
1
8260D
1/14/20 15:48
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0062
0.0012
1
8260D
1/14/20 15:48
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0062
0.00053
1
8260D
1/14/20 15:48
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0062
0.0012
1
8260D
1/14/20 15:48
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
1/14/20 15:48
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.012
0.00067
1
8260D
1/14/20 15:48
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
1/14/20 15:48
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.019
0.0022
1
8260D
1/14/20 15:48
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
70-130
Dibromofluoromethane
110 %
84-123
Toluene-d8
84 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-5S
Attn: Katie Lippard Sample ID: 0010154-07
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 14:55
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
81.3
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.81
0.14
1
8270E
1/15/20 20:20
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.81
0.13
1
8270E
1/15/20 20:20
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.81
0.12
1
8270E
1/15/20 20:20
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.40
0.13
1
8270E
1/15/20 20:20
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.81
0.012
1
8270E
1/15/20 20:20
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.81
0.17
1
8270E
1/15/20 20:20
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.81
0.20
1
8270E
1/15/20 20:20
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.81
0.16
1
8270E
1/15/20 20:20
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.40
0.17
1
8270E
1/15/20 20:20
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.8
0.47
1
8270E
1/15/20 20:20
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.81
0.21
1
8270E
1/15/20 20:20
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.81
0.21
1
8270E
1/15/20 20:20
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.81
0.20
1
8270E
1/15/20 20:20
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.81
0.15
1
8270E
1/15/20 20:20
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.81
0.016
1
8270E
1/15/20 20:20
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.81
0.15
1
8270E
1/15/20 20:20
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.81
0.13
1
8270E
1/15/20 20:20
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.81
0.16
1
8270E
1/15/20 20:20
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.81
0.18
1
8270E
1/15/20 20:20
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.8
0.45
1
8270E
1/15/20 20:20
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.81
0.19
1
8270E
1/15/20 20:20
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.81
0.15
1
8270E
1/15/20 20:20
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.40
0.098
1
8270E
1/15/20 20:20
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.25
1
8270E
1/15/20 20:20
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.81
0.20
1
8270E
1/15/20 20:20
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.81
0.018
1
8270E
1/15/20 20:20
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.81
0.016
1
8270E
1/15/20 20:20
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.81
0.0089
1
8270E
1/15/20 20:20
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.81
0.17
1
8270E
1/15/20 20:20
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.81
0.0097
1
8270E
1/15/20 20:20
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.81
0.0072
1
8270E
1/15/20 20:20
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.81
0.0075
1
8270E
1/15/20 20:20
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.81
0.0080
1
8270E
1/15/20 20:20
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.81
0.0086
1
8270E
1/15/20 20:20
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.4
0.67
1
8270E
1/15/20 20:20
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.81
0.15
1
8270E
1/15/20 20:20
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.81
0.15
1
8270E
1/15/20 20:20
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.81
0.13
1
8270E
1/15/20 20:20
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.40
0.14
1
8270E
1/15/20 20:20
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-5S
Attn: Katie Lippard Sample ID: 0010154-07
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 14:55
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.81
0.18
1
8270E
1/15/20 20:20
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.40
0.14
1
8270E
1/15/20 20:20
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.81
0.0095
1
8270E
1/15/20 20:20
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.81
0.023
1
8270E
1/15/20 20:20
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.81
0.22
1
8270E
1/15/20 20:20
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.81
0.21
1
8270E
1/15/20 20:20
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.81
0.19
1
8270E
1/15/20 20:20
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.81
0.20
1
8270E
1/15/20 20:20
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.40
0.21
1
8270E
1/15/20 20:20
JMV
POA0191
Fluoranthene
BRL
mg/kg dry
0.81
0.0092
1
8270E
1/15/20 20:20
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.81
0.014
1
8270E
1/15/20 20:20
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.81
0.18
1
8270E
1/15/20 20:20
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.81
0.18
1
8270E
1/15/20 20:20
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.81
0.28
1
8270E
1/15/20 20:20
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.81
0.13
1
8270E
1/15/20 20:20
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.81
0.023
1
8270E
1/15/20 20:20
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.81
0.17
1
8270E
1/15/20 20:20
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.81
0.017
1
8270E
1/15/20 20:20
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.40
0.17
1
8270E
1/15/20 20:20
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.81
0.19
1
8270E
1/15/20 20:20
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.81
0.22
1
8270E
1/15/20 20:20
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.2
0.52
1
8270E
1/15/20 20:20
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.81
0.0088
1
8270E
1/15/20 20:20
JMV
POA0191
Phenol
BRL
mg/kg dry
0.81
0.13
1
8270E
1/15/20 20:20
JMV
POA0191
Pyrene
BRL
mg/kg dry
0.81
0.012
1
8270E
1/15/20 20:20
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.40
0.077
1
8270E
1/15/20 20:20
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
82 %
39-132
2-Fluorobiphenyl
75 %
44-115
2-Fluorophenol
71 %
35-115
Nitrobenzene-d5
67 %
37-122
Phenol-d5
70 %
34-121
Terphenyl-d14
78 %
54-127
Total Metals
Mercury
0.039 J
mg/kg dry
0.061
0.021
1
7471B
1/16/20 10:07
JAB
POA0212
Arsenic
1.2
mg/kg dry
1.2
0.16
1
6010D
1/17/20 20:34
JAB
POA0162
Barium
27
mg/kg dry
12
3.7
1
6010D
1/17/20 20:34
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.61
0.042
1
6010D
1/17/20 20:34
JAB
POA0162
Chromium
17
mg/kg dry
1.2
0.093
1
6010D
1/17/20 20:34
JAB
POA0162
Lead
18
mg/kg dry
1.2
0.21
1
6010D
1/17/20 20:34
JAB
POA0162
Selenium
BRL
mg/kg dry
1.2
0.34
1
6010D
1/17/20 20:34
JAB
POA0162
Silver
BRL
mg/kg dry
0.61
0.038
1
6010D
1/17/20 20:34
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-5S
Attn: Katie Lippard Sample ID: 0010154-07
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 14:55
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0052
0.00063
1
8260D
1/14/20 16:19
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0052
0.00076
1
8260D
1/14/20 16:19
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0052
0.00038
1
8260D
1/14/20 16:19
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0052
0.00056
1
8260D
1/14/20 16:19
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0052
0.00093
1
8260D
1/14/20 16:19
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0052
0.00095
1
8260D
1/14/20 16:19
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0052
0.00080
1
8260D
1/14/20 16:19
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.010
0.00074
1
8260D
1/14/20 16:19
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0052
0.00059
1
8260D
1/14/20 16:19
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.010
0.00049
1
8260D
1/14/20 16:19
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0052
0.00055
1
8260D
1/14/20 16:19
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0052
0.00046
1
8260D
1/14/20 16:19
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0052
0.00058
1
8260D
1/14/20 16:19
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0052
0.00061
1
8260D
1/14/20 16:19
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0052
0.00078
1
8260D
1/14/20 16:19
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0052
0.00065
1
8260D
1/14/20 16:19
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0052
0.00064
1
8260D
1/14/20 16:19
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0052
0.00043
1
8260D
1/14/20 16:19
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0052
0.00065
1
8260D
1/14/20 16:19
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0052
0.00064
1
8260D
1/14/20 16:19
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0052
0.00069
1
8260D
1/14/20 16:19
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0052
0.00059
1
8260D
1/14/20 16:19
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0052
0.0013
1
8260D
1/14/20 16:19
TBL
POA0183
Acetone
0.017 J
mg/kg dry
0.021
0.0013
1
8260D
1/14/20 16:19
TBL
POA0183
Benzene
BRL
mg/kg dry
0.0052
0.00080
1
8260D
1/14/20 16:19
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0052
0.00072
1
8260D
1/14/20 16:19
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0052
0.00085
1
8260D
1/14/20 16:19
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0052
0.00049
1
8260D
1/14/20 16:19
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0052
0.00040
1
8260D
1/14/20 16:19
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.010
0.0025
1
8260D
1/14/20 16:19
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0052
0.0010
1
8260D
1/14/20 16:19
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0052
0.00081
1
8260D
1/14/20 16:19
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.010
0.00098
1
8260D
1/14/20 16:19
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0052
0.00063
1
8260D
1/14/20 16:19
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.010
0.0016
1
8260D
1/14/20 16:19
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0052
0.00081
1
8260D
1/14/20 16:19
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0052
0.00051
1
8260D
1/14/20 16:19
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0052
0.00035
1
8260D
1/14/20 16:19
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.010
0.0015
1
8260D
1/14/20 16:19
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0052
0.00078
1
8260D
1/14/20 16:19
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0052
0.00076
1
8260D
1/14/20 16:19
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0052
0.00060
1
8260D
1/14/20 16:19
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-5S
Attn: Katie Lippard Sample ID: 0010154-07
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 14:55
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.010
0.0013
1
8260D
1/14/20 16:19
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.021
0.00036
1
8260D
1/14/20 16:19
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.021
0.0012
1
8260D
1/14/20 16:19
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.021
0.00042
1
8260D
1/14/20 16:19
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0052
0.00083
1
8260D
1/14/20 16:19
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0052
0.00072
1
8260D
1/14/20 16:19
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.010
0.00052
1
8260D
1/14/20 16:19
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0052
0.00048
1
8260D
1/14/20 16:19
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0052
0.00075
1
8260D
1/14/20 16:19
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0052
0.00055
1
8260D
1/14/20 16:19
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0052
0.00056
1
8260D
1/14/20 16:19
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0052
0.00050
1
8260D
1/14/20 16:19
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0052
0.00061
1
8260D
1/14/20 16:19
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0052
0.00093
1
8260D
1/14/20 16:19
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0052
0.00082
1
8260D
1/14/20 16:19
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0052
0.00099
1
8260D
1/14/20 16:19
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0052
0.00044
1
8260D
1/14/20 16:19
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0052
0.0010
1
8260D
1/14/20 16:19
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.010
0.0014
1
8260D
1/14/20 16:19
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.010
0.00056
1
8260D
1/14/20 16:19
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.010
0.0010
1
8260D
1/14/20 16:19
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.015
0.0019
1
8260D
1/14/20 16:19
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
104 %
70-130
Dibromofluoromethane
107 %
84-123
Toluene-d8
89 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-51D
Attn: Katie Lippard Sample ID: 0010154-08
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 15:15
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
71.5
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.92
0.16
1
8270E
1/15/20 20:42
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.92
0.15
1
8270E
1/15/20 20:42
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.92
0.13
1
8270E
1/15/20 20:42
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.46
0.14
1
8270E
1/15/20 20:42
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.92
0.014
1
8270E
1/15/20 20:42
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.92
0.19
1
8270E
1/15/20 20:42
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.92
0.22
1
8270E
1/15/20 20:42
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.92
0.18
1
8270E
1/15/20 20:42
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.46
0.19
1
8270E
1/15/20 20:42
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
2.1
0.54
1
8270E
1/15/20 20:42
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.92
0.24
1
8270E
1/15/20 20:42
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.92
0.24
1
8270E
1/15/20 20:42
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.92
0.22
1
8270E
1/15/20 20:42
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.92
0.18
1
8270E
1/15/20 20:42
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.92
0.018
1
8270E
1/15/20 20:42
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.92
0.18
1
8270E
1/15/20 20:42
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.92
0.15
1
8270E
1/15/20 20:42
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.92
0.18
1
8270E
1/15/20 20:42
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.92
0.20
1
8270E
1/15/20 20:42
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.1
0.51
1
8270E
1/15/20 20:42
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.92
0.22
1
8270E
1/15/20 20:42
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.92
0.18
1
8270E
1/15/20 20:42
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.46
0.11
1
8270E
1/15/20 20:42
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.4
0.28
1
8270E
1/15/20 20:42
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.92
0.23
1
8270E
1/15/20 20:42
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.92
0.021
1
8270E
1/15/20 20:42
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.92
0.018
1
8270E
1/15/20 20:42
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.92
0.010
1
8270E
1/15/20 20:42
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.92
0.20
1
8270E
1/15/20 20:42
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.92
0.011
1
8270E
1/15/20 20:42
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.92
0.0082
1
8270E
1/15/20 20:42
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.92
0.0085
1
8270E
1/15/20 20:42
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.92
0.0090
1
8270E
1/15/20 20:42
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.92
0.0097
1
8270E
1/15/20 20:42
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.8
0.76
1
8270E
1/15/20 20:42
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.92
0.17
1
8270E
1/15/20 20:42
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.92
0.18
1
8270E
1/15/20 20:42
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.92
0.15
1
8270E
1/15/20 20:42
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.46
0.16
1
8270E
1/15/20 20:42
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-51D
Attn: Katie Lippard Sample ID: 0010154-08
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 15:15
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.92
0.21
1
8270E
1/15/20 20:42
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.46
0.16
1
8270E
1/15/20 20:42
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.92
0.011
1
8270E
1/15/20 20:42
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.92
0.026
1
8270E
1/15/20 20:42
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.92
0.25
1
8270E
1/15/20 20:42
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.92
0.24
1
8270E
1/15/20 20:42
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.92
0.22
1
8270E
1/15/20 20:42
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.92
0.23
1
8270E
1/15/20 20:42
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.46
0.24
1
8270E
1/15/20 20:42
JMV
POA0191
Fluoranthene
BRL
mg/kg dry
0.92
0.010
1
8270E
1/15/20 20:42
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.92
0.016
1
8270E
1/15/20 20:42
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.92
0.20
1
8270E
1/15/20 20:42
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.92
0.21
1
8270E
1/15/20 20:42
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.92
0.32
1
8270E
1/15/20 20:42
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.92
0.14
1
8270E
1/15/20 20:42
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.92
0.026
1
8270E
1/15/20 20:42
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.92
0.20
1
8270E
1/15/20 20:42
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.92
0.019
1
8270E
1/15/20 20:42
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.46
0.19
1
8270E
1/15/20 20:42
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.92
0.21
1
8270E
1/15/20 20:42
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.92
0.25
1
8270E
1/15/20 20:42
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.4
0.59
1
8270E
1/15/20 20:42
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.92
0.010
1
8270E
1/15/20 20:42
JMV
POA0191
Phenol
BRL
mg/kg dry
0.92
0.15
1
8270E
1/15/20 20:42
JMV
POA0191
Pyrene
BRL
mg/kg dry
0.92
0.013
1
8270E
1/15/20 20:42
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.46
0.088
1
8270E
1/15/20 20:42
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
79 %
39-132
2-Fluorobiphenyl
73 %
44-115
2-Fluorophenol
74 %
35-115
Nitrobenzene-d5
66 %
37-122
Phenol-d5
70 %
34-121
Terphenyl-d14
76 %
54-127
Total Metals
Mercury
0.036 J
mg/kg dry
0.070
0.024
1
7471B
1/16/20 10:21
JAB
POA0212
Arsenic
1.1 J
mg/kg dry
1.4
0.18
1
6010D
1117/20 20:56
JAB
POA0162
Barium
36
mg/kg dry
14
4.2
1
6010D
1/17/20 20:56
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.70
0.047
1
6010D
1/17/20 20:56
JAB
POA0162
Chromium
19
mg/kg dry
1.4
0.11
1
6010D
1/17/20 20:56
JAB
POA0162
Lead
11
mg/kg dry
1.4
0.23
1
6010D
1/17/20 20:56
JAB
POA0162
Selenium
BRL
mg/kg dry
1.4
0.38
1
6010D
1/17/20 20:56
JAB
POA0162
Silver
BRL
mg/kg dry
0.70
0.043
1
6010D
1/17/20 20:56
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-51D
Attn: Katie Lippard Sample ID: 0010154-08
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 15:15
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0072
0.00088
1
8260D
1/14/20 16:48
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0072
0.0011
1
8260D
1/14/20 16:48
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0072
0.00053
1
8260D
1/14/20 16:48
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0072
0.00078
1
8260D
1/14/20 16:48
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0072
0.0013
1
8260D
1/14/20 16:48
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0072
0.0013
1
8260D
1/14/20 16:48
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0072
0.0011
1
8260D
1/14/20 16:48
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.014
0.0010
1
8260D
1/14/20 16:48
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0072
0.00082
1
8260D
1/14/20 16:48
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.014
0.00069
1
8260D
1/14/20 16:48
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0072
0.00076
1
8260D
1/14/20 16:48
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0072
0.00065
1
8260D
1/14/20 16:48
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0072
0.00080
1
8260D
1/14/20 16:48
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0072
0.00086
1
8260D
1/14/20 16:48
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0072
0.0011
1
8260D
1/14/20 16:48
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0072
0.00091
1
8260D
1/14/20 16:48
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0072
0.00090
1
8260D
1/14/20 16:48
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0072
0.00060
1
8260D
1/14/20 16:48
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0072
0.00091
1
8260D
1/14/20 16:48
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0072
0.00090
1
8260D
1/14/20 16:48
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0072
0.00097
1
8260D
1/14/20 16:48
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0072
0.00082
1
8260D
1/14/20 16:48
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0072
0.0018
1
8260D
1/14/20 16:48
TBL
POA0183
Acetone
BRL
mg/kg dry
0.029
0.0018
1
8260D
1/14/20 16:48
TBL
POA0183
Benzene
BRL
mg/kg dry
0.0072
0.0011
1
8260D
1/14/20 16:48
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0072
0.0010
1
8260D
1/14/20 16:48
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0072
0.0012
1
8260D
1/14/20 16:48
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0072
0.00069
1
8260D
1/14/20 16:48
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0072
0.00056
1
8260D
1/14/20 16:48
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.014
0.0035
1
8260D
1/14/20 16:48
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0072
0.0014
1
8260D
1/14/20 16:48
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0072
0.0011
1
8260D
1/14/20 16:48
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.014
0.0014
1
8260D
1/14/20 16:48
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0072
0.00088
1
8260D
1/14/20 16:48
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.014
0.0022
1
8260D
1/14/20 16:48
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0072
0.0011
1
8260D
1/14/20 16:48
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0072
0.00071
1
8260D
1/14/20 16:48
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0072
0.00048
1
8260D
1/14/20 16:48
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.014
0.0020
1
8260D
1/14/20 16:48
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0072
0.0011
1
8260D
1/14/20 16:48
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0072
0.0011
1
8260D
1/14/20 16:48
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0072
0.00084
1
8260D
1/14/20 16:48
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-51D
Attn: Katie Lippard Sample ID: 0010154-08
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 15:15
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.014
0.0018
1
8260D
1/14/20 16:48
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.029
0.00050
1
8260D
1/14/20 16:48
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.029
0.0017
1
8260D
1/14/20 16:48
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.029
0.00059
1
8260D
1/14/20 16:48
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0072
0.0012
1
8260D
1/14/20 16:48
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0072
0.0010
1
8260D
1/14/20 16:48
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.014
0.00073
1
8260D
1/14/20 16:48
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0072
0.00068
1
8260D
1/14/20 16:48
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0072
0.0010
1
8260D
1/14/20 16:48
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0072
0.00077
1
8260D
1/14/20 16:48
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0072
0.00078
1
8260D
1/14/20 16:48
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0072
0.00070
1
8260D
1/14/20 16:48
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0072
0.00086
1
8260D
1/14/20 16:48
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0072
0.0013
1
8260D
1/14/20 16:48
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0072
0.0011
1
8260D
1/14/20 16:48
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0072
0.0014
1
8260D
1/14/20 16:48
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0072
0.00062
1
8260D
1/14/20 16:48
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0072
0.0014
1
8260D
1/14/20 16:48
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.014
0.0019
1
8260D
1/14/20 16:48
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.014
0.00078
1
8260D
1/14/20 16:48
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.014
0.0014
1
8260D
1/14/20 16:48
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.022
0.0026
1
8260D
1/14/20 16:48
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
93 %
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
89 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-6S
Attn: Katie Lippard Sample ID: 0010154-09
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 11:25
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
76.2
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.87
0.15
1
8270E
1/15/20 21:05
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.87
0.14
1
8270E
1/15/20 21:05
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.87
0.13
1
8270E
1/15/20 21:05
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.14
1
8270E
1/15/20 21:05
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.87
0.013
1
8270E
1/15/20 21:05
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.87
0.18
1
8270E
1/15/20 21:05
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.87
0.21
1
8270E
1/15/20 21:05
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.87
0.17
1
8270E
1/15/20 21:05
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.43
0.18
1
8270E
1/15/20 21:05
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
2.0
0.51
1
8270E
1/15/20 21:05
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.87
0.23
1
8270E
1/15/20 21:05
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.87
0.22
1
8270E
1/15/20 21:05
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.87
0.21
1
8270E
1/15/20 21:05
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.87
0.17
1
8270E
1/15/20 21:05
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.87
0.017
1
8270E
1/15/20 21:05
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.87
0.17
1
8270E
1/15/20 21:05
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.87
0.14
1
8270E
1/15/20 21:05
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.87
0.17
1
8270E
1/15/20 21:05
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.87
0.19
1
8270E
1/15/20 21:05
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.0
0.48
1
8270E
1/15/20 21:05
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.87
0.20
1
8270E
1/15/20 21:05
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.87
0.17
1
8270E
1/15/20 21:05
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
8270E
1/15/20 21:05
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
8270E
1/15/20 21:05
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.87
0.21
1
8270E
1/15/20 21:05
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.87
0.020
1
8270E
1/15/20 21:05
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.87
0.017
1
8270E
1/15/20 21:05
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.87
0.0096
1
8270E
1/15/20 21:05
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.87
0.18
1
8270E
1/15/20 21:05
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.87
0.010
1
8270E
1/15/20 21:05
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.87
0.0077
1
8270E
1/15/20 21:05
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.87
0.0080
1
8270E
1/15/20 21:05
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.87
0.0085
1
8270E
1/15/20 21:05
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.87
0.0092
1
8270E
1/15/20 21:05
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.6
0.72
1
8270E
1/15/20 21:05
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.87
0.16
1
8270E
1/15/20 21:05
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.87
0.17
1
8270E
1/15/20 21:05
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.87
0.14
1
8270E
1/15/20 21:05
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
8270E
1/15/20 21:05
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-6S
Attn: Katie Lippard Sample ID: 0010154-09
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 11:25
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.87
0.20
1
8270E
1/15/20 21:05
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
8270E
1/15/20 21:05
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.87
0.010
1
8270E
1/15/20 21:05
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.87
0.025
1
8270E
1/15/20 21:05
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.87
0.23
1
8270E
1/15/20 21:05
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.87
0.22
1
8270E
1/15/20 21:05
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.87
0.21
1
8270E
1/15/20 21:05
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.87
0.22
1
8270E
1/15/20 21:05
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
8270E
1/15/20 21:05
JMV
POA0191
Fluoranthene
BRL
mg/kg dry
0.87
0.0098
1
8270E
1/15/20 21:05
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.87
0.015
1
8270E
1/15/20 21:05
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.87
0.19
1
8270E
1/15/20 21:05
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.87
0.20
1
8270E
1/15/20 21:05
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.87
0.30
1
8270E
1/15/20 21:05
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.87
0.14
1
8270E
1/15/20 21:05
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.87
0.024
1
8270E
1/15/20 21:05
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.87
0.19
1
8270E
1/15/20 21:05
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.87
0.018
1
8270E
1/15/20 21:05
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
8270E
1/15/20 21:05
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.87
0.20
1
8270E
1/15/20 21:05
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.87
0.24
1
8270E
1/15/20 21:05
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.3
0.55
1
8270E
1/15/20 21:05
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.87
0.0094
1
8270E
1/15/20 21:05
JMV
POA0191
Phenol
BRL
mg/kg dry
0.87
0.14
1
8270E
1/15/20 21:05
JMV
POA0191
Pyrene
BRL
mg/kg dry
0.87
0.013
1
8270E
1/15/20 21:05
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.43
0.083
1
8270E
1/15/20 21:05
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
83 %
39-132
2-Fluorobiphenyl
78 %
44-115
2-Fluorophenol
78 %
35-115
Nitrobenzene-d5
71 %
37-122
Phenol-d5
73 %
34-121
Terphenyl-d14
82 %
54-127
Total Metals
Mercury
0.041 J
mg/kg dry
0.066
0.023
1
7471B
1/16/20 10:25
JAB
POA0212
Arsenic
2.3
mg/kg dry
1.3
0.17
1
6010D
1/17/20 21:04
JAB
POA0162
Barium
41
mg/kg dry
13
3.9
1
6010D
1/17/20 21:04
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.66
0.044
1
6010D
1/17/20 21:04
JAB
POA0162
Chromium
29
mg/kg dry
1.3
0.099
1
6010D
1/17/20 21:04
JAB
POA0162
Lead
15
mg/kg dry
1.3
0.22
1
6010D
1/17/20 21:04
JAB
POA0162
Selenium
BRL
mg/kg dry
1.3
0.36
1
6010D
1/17/20 21:04
JAB
POA0162
Silver
BRL
mg/kg dry
0.66
0.040
1
6010D
1/17/20 21:04
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-6S
Attn: Katie Lippard Sample ID: 0010154-09
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 11:25
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0064
0.00078
1
8260D
1/14/20 17:18
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0064
0.00094
1
8260D
1/14/20 17:18
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0064
0.00046
1
8260D
1/14/20 17:18
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0064
0.00069
1
8260D
1/14/20 17:18
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0064
0.0012
1
8260D
1/14/20 17:18
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
8260D
1/14/20 17:18
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0064
0.00098
1
8260D
1/14/20 17:18
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00091
1
8260D
1/14/20 17:18
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0064
0.00073
1
8260D
1/14/20 17:18
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00061
1
8260D
1/14/20 17:18
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0064
0.00068
1
8260D
1/14/20 17:18
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0064
0.00057
1
8260D
1/14/20 17:18
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0064
0.00071
1
8260D
1/14/20 17:18
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0064
0.00076
1
8260D
1/14/20 17:18
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0064
0.00096
1
8260D
1/14/20 17:18
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0064
0.00080
1
8260D
1/14/20 17:18
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0064
0.00079
1
8260D
1/14/20 17:18
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0064
0.00053
1
8260D
1/14/20 17:18
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0064
0.00081
1
8260D
1/14/20 17:18
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0064
0.00080
1
8260D
1/14/20 17:18
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0064
0.00086
1
8260D
1/14/20 17:18
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0064
0.00073
1
8260D
1/14/20 17:18
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0064
0.0016
1
8260D
1/14/20 17:18
TBL
POA0183
Acetone
0.033
mg/kg dry
0.026
0.0016
1
8260D
1/14/20 17:18
TBL
POA0183
Benzene
BRL
mg/kg dry
0.0064
0.0010
1
8260D
1/14/20 17:18
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0064
0.00089
1
8260D
1/14/20 17:18
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0064
0.0010
1
8260D
1/14/20 17:18
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0064
0.00061
1
8260D
1/14/20 17:18
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0064
0.00049
1
8260D
1/14/20 17:18
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.013
0.0031
1
8260D
1/14/20 17:18
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0064
0.0013
1
8260D
1/14/20 17:18
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0064
0.0010
1
8260D
1/14/20 17:18
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.013
0.0012
1
8260D
1/14/20 17:18
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0064
0.00078
1
8260D
1/14/20 17:18
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.013
0.0019
1
8260D
1/14/20 17:18
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0064
0.0010
1
8260D
1/14/20 17:18
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0064
0.00063
1
8260D
1/14/20 17:18
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0064
0.00043
1
8260D
1/14/20 17:18
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.013
0.0018
1
8260D
1/14/20 17:18
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0064
0.00096
1
8260D
1/14/20 17:18
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0064
0.00094
1
8260D
1/14/20 17:18
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0064
0.00074
1
8260D
1/14/20 17:18
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-6S
Attn: Katie Lippard Sample ID: 0010154-09
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 11:25
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.013
0.0016
1
8260D
1/14/20 17:18
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.026
0.00044
1
8260D
1/14/20 17:18
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.026
0.0015
1
8260D
1/14/20 17:18
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.026
0.00052
1
8260D
1/14/20 17:18
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0064
0.0010
1
8260D
1/14/20 17:18
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0064
0.00089
1
8260D
1/14/20 17:18
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.013
0.00064
1
8260D
1/14/20 17:18
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0064
0.00060
1
8260D
1/14/20 17:18
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0064
0.00093
1
8260D
1/14/20 17:18
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0064
0.00068
1
8260D
1/14/20 17:18
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0064
0.00069
1
8260D
1/14/20 17:18
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0064
0.00062
1
8260D
1/14/20 17:18
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0064
0.00076
1
8260D
1/14/20 17:18
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
8260D
1/14/20 17:18
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0064
0.0010
1
8260D
1/14/20 17:18
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
8260D
1/14/20 17:18
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0064
0.00055
1
8260D
1/14/20 17:18
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
8260D
1/14/20 17:18
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.013
0.0017
1
8260D
1/14/20 17:18
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.013
0.00069
1
8260D
1/14/20 17:18
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.013
0.0013
1
8260D
1/14/20 17:18
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.019
0.0023
1
8260D
1/14/20 17:18
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
70-130
Dibromofluoromethane
110 %
84-123
Toluene-d8
86 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-6D
Attn: Katie Lippard Sample ID: 0010154-10
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 11:30
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
77.6
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.85
0.15
1
8270E
1/15/20 21:27
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.85
0.14
1
8270E
1/15/20 21:27
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.85
0.12
1
8270E
1/15/20 21:27
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.42
0.13
1
8270E
1/15/20 21:27
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.85
0.013
1
8270E
1/15/20 21:27
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.85
0.18
1
8270E
1/15/20 21:27
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.85
0.21
1
8270E
1/15/20 21:27
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.85
0.17
1
8270E
1/15/20 21:27
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.42
0.18
1
8270E
1/15/20 21:27
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.50
1
8270E
1/15/20 21:27
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.85
0.23
1
8270E
1/15/20 21:27
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.85
0.22
1
8270E
1/15/20 21:27
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.85
0.21
1
8270E
1/15/20 21:27
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 21:27
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.85
0.016
1
8270E
1/15/20 21:27
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 21:27
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.85
0.14
1
8270E
1/15/20 21:27
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.85
0.17
1
8270E
1/15/20 21:27
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.85
0.18
1
8270E
1/15/20 21:27
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.47
1
8270E
1/15/20 21:27
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.85
0.20
1
8270E
1/15/20 21:27
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 21:27
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.42
0.10
1
8270E
1/15/20 21:27
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
8270E
1/15/20 21:27
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.85
0.21
1
8270E
1/15/20 21:27
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.85
0.019
1
8270E
1/15/20 21:27
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.85
0.017
1
8270E
1/15/20 21:27
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.85
0.0094
1
8270E
1/15/20 21:27
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.85
0.18
1
8270E
1/15/20 21:27
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.85
0.010
1
8270E
1/15/20 21:27
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.85
0.0076
1
8270E
1/15/20 21:27
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.85
0.0078
1
8270E
1/15/20 21:27
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.85
0.0084
1
8270E
1/15/20 21:27
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.85
0.0090
1
8270E
1/15/20 21:27
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.6
0.70
1
8270E
1/15/20 21:27
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 21:27
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.85
0.16
1
8270E
1/15/20 21:27
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.85
0.14
1
8270E
1/15/20 21:27
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.42
0.15
1
8270E
1/15/20 21:27
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-6D
Attn: Katie Lippard Sample ID: 0010154-10
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 11:30
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.85
0.19
1
8270E
1/15/20 21:27
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.42
0.15
1
8270E
1/15/20 21:27
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.85
0.010
1
8270E
1/15/20 21:27
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.85
0.024
1
8270E
1/15/20 21:27
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.85
0.23
1
8270E
1/15/20 21:27
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.85
0.22
1
8270E
1/15/20 21:27
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.85
0.20
1
8270E
1/15/20 21:27
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.85
0.21
1
8270E
1/15/20 21:27
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.42
0.22
1
8270E
1/15/20 21:27
JMV
POA0191
Fluoranthene
BRL
mg/kg dry
0.85
0.0096
1
8270E
1/15/20 21:27
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.85
0.015
1
8270E
1/15/20 21:27
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.85
0.19
1
8270E
1/15/20 21:27
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.85
0.19
1
8270E
1/15/20 21:27
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.85
0.29
1
8270E
1/15/20 21:27
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.85
0.13
1
8270E
1/15/20 21:27
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.85
0.024
1
8270E
1/15/20 21:27
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.85
0.18
1
8270E
1/15/20 21:27
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.85
0.018
1
8270E
1/15/20 21:27
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.42
0.18
1
8270E
1/15/20 21:27
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.85
0.20
1
8270E
1/15/20 21:27
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.85
0.23
1
8270E
1/15/20 21:27
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.3
0.54
1
8270E
1/15/20 21:27
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.85
0.0093
1
8270E
1/15/20 21:27
JMV
POA0191
Phenol
BRL
mg/kg dry
0.85
0.14
1
8270E
1/15/20 21:27
JMV
POA0191
Pyrene
BRL
mg/kg dry
0.85
0.012
1
8270E
1/15/20 21:27
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.42
0.081
1
8270E
1/15/20 21:27
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
83 %
39-132
2-Fluorobiphenyl
83 %
44-115
2-Fluorophenol
82 %
35-115
Nitrobenzene-d5
74 %
37-122
Phenol-d5
77 %
34-121
Terphenyl-d14
79 %
54-127
Total Metals
Mercury
0.042 J
mg/kg dry
0.064
0.022
1
7471B
1/16/20 10:30
JAB
POA0212
Arsenic
1.4
mg/kg dry
1.3
0.17
1
6010D
1/17/20 21:13
JAB
POA0162
Barium
360
mg/kg dry
64
19
5
6010D
1/20/20 12:27
JAB
POA0162
Cadmium
BRL
mg/kg dry
0.64
0.044
1
6010D
1/17/20 21:13
JAB
POA0162
Chromium
23
mg/kg dry
1.3
0.098
1
6010D
1/17/20 21:13
JAB
POA0162
Lead
44
mg/kg dry
1.3
0.22
1
6010D
1/17/20 21:13
JAB
POA0162
Selenium
BRL
mg/kg dry
1.3
0.35
1
6010D
1/17/20 21:13
JAB
POA0162
Silver
BRL
mg/kg dry
0.64
0.040
1
6010D
1/17/20 21:13
JAB
POA0162
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-6D
Attn: Katie Lippard Sample ID: 0010154-10
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 11:30
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0061
0.00074
1
8260D
1/14/20 17:48
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0061
0.00090
1
8260D
1/14/20 17:48
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0061
0.00044
1
8260D
1/14/20 17:48
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0061
0.00066
1
8260D
1/14/20 17:48
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0061
0.0011
1
8260D
1/14/20 17:48
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0061
0.0011
1
8260D
1/14/20 17:48
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00094
1
8260D
1/14/20 17:48
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00087
1
8260D
1/14/20 17:48
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0061
0.00069
1
8260D
1/14/20 17:48
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00058
1
8260D
1/14/20 17:48
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0061
0.00065
1
8260D
1/14/20 17:48
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0061
0.00055
1
8260D
1/14/20 17:48
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00068
1
8260D
1/14/20 17:48
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0061
0.00072
1
8260D
1/14/20 17:48
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0061
0.00092
1
8260D
1/14/20 17:48
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0061
0.00077
1
8260D
1/14/20 17:48
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00076
1
8260D
1/14/20 17:48
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0061
0.00051
1
8260D
1/14/20 17:48
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00077
1
8260D
1/14/20 17:48
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0061
0.00076
1
8260D
1/14/20 17:48
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0061
0.00082
1
8260D
1/14/20 17:48
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0061
0.00069
1
8260D
1/14/20 17:48
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0061
0.0015
1
8260D
1/14/20 17:48
TBL
POA0183
Acetone
0.018 J
mg/kg dry
0.024
0.0016
1
8260D
1/14/20 17:48
TBL
POA0183
Benzene
BRL
mg/kg dry
0.0061
0.00095
1
8260D
1/14/20 17:48
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0061
0.00085
1
8260D
1/14/20 17:48
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0061
0.0010
1
8260D
1/14/20 17:48
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0061
0.00058
1
8260D
1/14/20 17:48
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0061
0.00047
1
8260D
1/14/20 17:48
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.012
0.0030
1
8260D
1/14/20 17:48
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0061
0.0012
1
8260D
1/14/20 17:48
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0061
0.00095
1
8260D
1/14/20 17:48
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.012
0.0012
1
8260D
1/14/20 17:48
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0061
0.00075
1
8260D
1/14/20 17:48
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.012
0.0019
1
8260D
1/14/20 17:48
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0061
0.00096
1
8260D
1/14/20 17:48
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00060
1
8260D
1/14/20 17:48
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0061
0.00041
1
8260D
1/14/20 17:48
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
1/14/20 17:48
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0061
0.00092
1
8260D
1/14/20 17:48
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0061
0.00089
1
8260D
1/14/20 17:48
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0061
0.00071
1
8260D
1/14/20 17:48
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-6D
Attn: Katie Lippard Sample ID: 0010154-10
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 11:30
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0016
1
8260D
1/14/20 17:48
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.024
0.00042
1
8260D
1/14/20 17:48
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.024
0.0014
1
8260D
1/14/20 17:48
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.024
0.00050
1
8260D
1/14/20 17:48
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0061
0.00099
1
8260D
1/14/20 17:48
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0061
0.00085
1
8260D
1/14/20 17:48
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.012
0.00062
1
8260D
1/14/20 17:48
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0061
0.00057
1
8260D
1/14/20 17:48
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0061
0.00088
1
8260D
1/14/20 17:48
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0061
0.00065
1
8260D
1/14/20 17:48
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0061
0.00066
1
8260D
1/14/20 17:48
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0061
0.00059
1
8260D
1/14/20 17:48
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0061
0.00072
1
8260D
1/14/20 17:48
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0061
0.0011
1
8260D
1/14/20 17:48
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0061
0.00097
1
8260D
1/14/20 17:48
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0061
0.0012
1
8260D
1/14/20 17:48
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00052
1
8260D
1/14/20 17:48
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0061
0.0012
1
8260D
1/14/20 17:48
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
1/14/20 17:48
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.012
0.00066
1
8260D
1/14/20 17:48
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
1/14/20 17:48
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.018
0.0022
1
8260D
1/14/20 17:48
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
111 %
84-123
Toluene-d8
88 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-7
Attn: Katie Lippard Sample ID: 0010154-11
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 12:45
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
79.0
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.83
0.15
1
8270E
1/15/20 21:50
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.83
0.14
1
8270E
1/15/20 21:50
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.83
0.12
1
8270E
1/15/20 21:50
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.42
0.13
1
8270E
1/15/20 21:50
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.83
0.013
1
8270E
1/15/20 21:50
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 21:50
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.83
0.20
1
8270E
1/15/20 21:50
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 21:50
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.42
0.17
1
8270E
1/15/20 21:50
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.49
1
8270E
1/15/20 21:50
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.83
0.22
1
8270E
1/15/20 21:50
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.83
0.22
1
8270E
1/15/20 21:50
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.83
0.20
1
8270E
1/15/20 21:50
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 21:50
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.83
0.016
1
8270E
1/15/20 21:50
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 21:50
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.83
0.14
1
8270E
1/15/20 21:50
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.83
0.17
1
8270E
1/15/20 21:50
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 21:50
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.46
1
8270E
1/15/20 21:50
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.83
0.20
1
8270E
1/15/20 21:50
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 21:50
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.42
0.10
1
8270E
1/15/20 21:50
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
8270E
1/15/20 21:50
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.83
0.21
1
8270E
1/15/20 21:50
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.83
0.019
1
8270E
1/15/20 21:50
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.83
0.016
1
8270E
1/15/20 21:50
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.83
0.0092
1
8270E
1/15/20 21:50
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 21:50
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.83
0.010
1
8270E
1/15/20 21:50
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.83
0.0075
1
8270E
1/15/20 21:50
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.83
0.0077
1
8270E
1/15/20 21:50
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.83
0.0082
1
8270E
1/15/20 21:50
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.83
0.0088
1
8270E
1/15/20 21:50
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.5
0.69
1
8270E
1/15/20 21:50
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 21:50
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.83
0.16
1
8270E
1/15/20 21:50
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.83
0.13
1
8270E
1/15/20 21:50
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.42
0.15
1
8270E
1/15/20 21:50
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

®
Laboratory Report
•
Waynt.
01/28/2020
PA
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh
Project: 400H
Client Sample ID: B-7
Attn: Katie Lippard
Sample ID: 0010154-11
409 Rogers View Court
Work Order: 0010154
Raleigh, NC 27610
Sample Matrix: Soil
Time Collected:
01/06/20 12:45
Time Submitted:
01/10/20 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.83
0.19
1
8270E
1/15/20 21:50
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.42
0.14
1
8270E
1/15/20 21:50
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.83
0.0099
1
8270E
1/15/20 21:50
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.83
0.024
1
8270E
1/15/20 21:50
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.83
0.22
1
8270E
1/15/20 21:50
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.83
0.21
1
8270E
1/15/20 21:50
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.83
0.20
1
8270E
1/15/20 21:50
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.83
0.21
1
8270E
1/15/20 21:50
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.42
0.22
1
8270E
1/15/20 21:50
JMV
POA0191
Fluoranthene
0.045 J
mg/kg dry
0.83
0.0095
1
8270E
1/15/20 21:50
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.83
0.014
1
8270E
1/15/20 21:50
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 21:50
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.83
0.19
1
8270E
1/15/20 21:50
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.83
0.29
1
8270E
1/15/20 21:50
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.83
0.13
1
8270E
1/15/20 21:50
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.83
0.023
1
8270E
1/15/20 21:50
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.83
0.18
1
8270E
1/15/20 21:50
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.83
0.018
1
8270E
1/15/20 21:50
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.42
0.18
1
8270E
1/15/20 21:50
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.83
0.19
1
8270E
1/15/20 21:50
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.83
0.23
1
8270E
1/15/20 21:50
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.3
0.53
1
8270E
1/15/20 21:50
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.83
0.0091
1
8270E
1/15/20 21:50
JMV
POA0191
Phenol
BRL
mg/kg dry
0.83
0.14
1
8270E
1/15/20 21:50
JMV
POA0191
Pyrene
0.043 J
mg/kg dry
0.83
0.012
1
8270E
1/15/20 21:50
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.42
0.080
1
8270E
1/15/20 21:50
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
80 %
39-132
2-Fluorobiphenyl
80 %
44-115
2-Fluorophenol
76 %
35-115
Nitrobenzene-d5
73 %
37-122
Phenol-d5
74 %
34-121
Terphenyl-d14
83 %
54-127
Total Metals
Mercury
0.13
mg/kg dry
0.063
0.022
1
7471B
1/16/20 10:34
JAB
POA0212
Arsenic
1.2 J
mg/kg dry
1.3
0.17
1
6010D
1/18/20 0:25
JAB
POA0181
Barium
19
mg/kg dry
13
3.8
1
6010D
1/18120 0:25
JAB
POA0181
Cadmium
BRL
mg/kg dry
0.63
0.043
1
6010D
1/18/20 0:25
JAB
POA0181
Chromium
27
mg/kg dry
1.3
0.096
1
6010D
1/18/20 0:25
JAB
POA0181
Lead
17
mg/kg dry
1.3
0.21
1
6010D
1/18/20 0:25
JAB
POA0181
Selenium
BRL
mg/kg dry
1.3
0.35
1
6010D
1/18/20 0:25
JAB
POA0181
Silver
BRL
mg/kg dry
0.63
0.039
1
6010D
1/18/20 0:25
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-7
Attn: Katie Lippard Sample ID: 0010154-11
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 12:45
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0048
0.00059
1
8260D
1/14/20 18:19
TBL
POA0183
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0048
0.00071
1
8260D
1/14/20 18:19
TBL
POA0183
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0048
0.00035
1
8260D
1/14/20 18:19
TBL
POA0183
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0048
0.00052
1
8260D
1/14/20 18:19
TBL
POA0183
1,1-Dichloroethane
BRL
mg/kg dry
0.0048
0.00087
1
8260D
1/14/20 18:19
TBL
POA0183
1,1-Dichloroethylene
BRL
mg/kg dry
0.0048
0.00088
1
8260D
1/14/20 18:19
TBL
POA0183
1,1-Dichloropropylene
BRL
mg/kg dry
0.0048
0.00074
1
8260D
1/14/20 18:19
TBL
POA0183
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0096
0.00069
1
8260D
1/14/20 18:19
TBL
POA0183
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0048
0.00055
1
8260D
1/14/20 18:19
TBL
POA0183
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0096
0.00046
1
8260D
1/14/20 18:19
TBL
POA0183
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0048
0.00051
1
8260D
1/14/20 18:19
TBL
POA0183
1,2-Dibromoethane
BRL
mg/kg dry
0.0048
0.00043
1
8260D
1/14/20 18:19
TBL
POA0183
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0048
0.00054
1
8260D
1/14/20 18:19
TBL
POA0183
1,2-Dichloroethane
BRL
mg/kg dry
0.0048
0.00057
1
8260D
1/14/20 18:19
TBL
POA0183
1,2-Dichloropropane
BRL
mg/kg dry
0.0048
0.00073
1
8260D
1/14/20 18:19
TBL
POA0183
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0048
0.00061
1
8260D
1/14/20 18:19
TBL
POA0183
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0048
0.00060
1
8260D
1/14/20 18:19
TBL
POA0183
1,3-Dichloropropane
BRL
mg/kg dry
0.0048
0.00040
1
8260D
1/14/20 18:19
TBL
POA0183
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0048
0.00061
1
8260D
1/14/20 18:19
TBL
POA0183
2,2-Dichloropropane
BRL
mg/kg dry
0.0048
0.00060
1
8260D
1/14/20 18:19
TBL
POA0183
2-Chlorotoluene
BRL
mg/kg dry
0.0048
0.00065
1
8260D
1/14/20 18:19
TBL
POA0183
4-Chlorotoluene
BRL
mg/kg dry
0.0048
0.00055
1
8260D
1/14/20 18:19
TBL
POA0183
4-Isopropyltoluene
BRL
mg/kg dry
0.0048
0.0012
1
8260D
1/14/20 18:19
TBL
POA0183
Acetone
0.025
mg/kg dry
0.019
0.0012
1
8260D
1/14/20 18:19
TBL
POA0183
Benzene
BRL
mg/kg dry
0.0048
0.00075
1
8260D
1/14/20 18:19
TBL
POA0183
Bromobenzene
BRL
mg/kg dry
0.0048
0.00067
1
8260D
1/14/20 18:19
TBL
POA0183
Bromochloromethane
BRL
mg/kg dry
0.0048
0.00079
1
8260D
1/14/20 18:19
TBL
POA0183
Bromodichloromethane
BRL
mg/kg dry
0.0048
0.00046
1
8260D
1/14/20 18:19
TBL
POA0183
Bromoform
BRL
mg/kg dry
0.0048
0.00037
1
8260D
1/14/20 18:19
TBL
POA0183
Bromomethane
BRL
mg/kg dry
0.0096
0.0024
1
8260D
1/14/20 18:19
TBL
POA0183
Carbon Tetrachloride
BRL
mg/kg dry
0.0048
0.00095
1
8260D
1/14/20 18:19
TBL
POA0183
Chlorobenzene
BRL
mg/kg dry
0.0048
0.00075
1
8260D
1/14/20 18:19
TBL
POA0183
Chloroethane
BRL
mg/kg dry
0.0096
0.00092
1
8260D
1/14/20 18:19
TBL
POA0183
Chloroform
BRL
mg/kg dry
0.0048
0.00059
1
8260D
1/14/20 18:19
TBL
POA0183
Chloromethane
BRL
mg/kg dry
0.0096
0.0015
1
8260D
1/14/20 18:19
TBL
POA0183
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0048
0.00076
1
8260D
1/14/20 18:19
TBL
POA0183
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0048
0.00048
1
8260D
1/14/20 18:19
TBL
POA0183
Dibromochloromethane
BRL
mg/kg dry
0.0048
0.00032
1
8260D
1/14/20 18:19
TBL
POA0183
Dichlorodifluoromethane
BRL
mg/kg dry
0.0096
0.0014
1
8260D
1/14/20 18:19
TBL
POA0183
Ethylbenzene
BRL
mg/kg dry
0.0048
0.00073
1
8260D
1/14/20 18:19
TBL
POA0183
Isopropyl Ether
BRL
mg/kg dry
0.0048
0.00071
1
8260D
1/14/20 18:19
TBL
POA0183
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0048
0.00056
1
8260D
1/14/20 18:19
TBL
POA0183
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-7
Attn: Katie Lippard Sample ID: 0010154-11
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 12:45
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.0096
0.0012
1
8260D
1/14/20 18:19
TBL
POA0183
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.019
0.00033
1
8260D
1/14/20 18:19
TBL
POA0183
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.019
0.0011
1
8260D
1/14/20 18:19
TBL
POA0183
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.019
0.00039
1
8260D
1/14/20 18:19
TBL
POA0183
Methylene Chloride
BRL
mg/kg dry
0.0048
0.00078
1
8260D
1/14/20 18:19
TBL
POA0183
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0048
0.00068
1
8260D
1/14/20 18:19
TBL
POA0183
Naphthalene
BRL
mg/kg dry
0.0096
0.00049
1
8260D
1/14/20 18:19
TBL
POA0183
n-Butylbenzene
BRL
mg/kg dry
0.0048
0.00045
1
8260D
1/14/20 18:19
TBL
POA0183
n-Propylbenzene
BRL
mg/kg dry
0.0048
0.00070
1
8260D
1/14/20 18:19
TBL
POA0183
o-Xylene
BRL
mg/kg dry
0.0048
0.00051
1
8260D
1/14/20 18:19
TBL
POA0183
sec-Butylbenzene
BRL
mg/kg dry
0.0048
0.00052
1
8260D
1/14/20 18:19
TBL
POA0183
Styrene
BRL
mg/kg dry
0.0048
0.00047
1
8260D
1/14/20 18:19
TBL
POA0183
tert-Butylbenzene
BRL
mg/kg dry
0.0048
0.00057
1
8260D
1/14/20 18:19
TBL
POA0183
Tetrachloroethylene
BRL
mg/kg dry
0.0048
0.00087
1
8260D
1/14/20 18:19
TBL
POA0183
Toluene
BRL
mg/kg dry
0.0048
0.00077
1
8260D
1/14/20 18:19
TBL
POA0183
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0048
0.00092
1
8260D
1/14/20 18:19
TBL
POA0183
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0048
0.00041
1
8260D
1/14/20 18:19
TBL
POA0183
Trichloroethylene
BRL
mg/kg dry
0.0048
0.00094
1
8260D
1/14/20 18:19
TBL
POA0183
Trichlorofluoromethane
BRL
mg/kg dry
0.0096
0.0013
1
8260D
1/14/20 18:19
TBL
POA0183
Vinyl acetate
BRL
mg/kg dry
0.0096
0.00052
1
8260D
1/14/20 18:19
TBL
POA0183
Vinyl chloride
BRL
mg/kg dry
0.0096
0.00095
1
8260D
1/14/20 18:19
TBL
POA0183
Xylenes, total
BRL
mg/kg dry
0.014
0.0017
1
8260D
1/14/20 18:19
TBL
POA0183
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
104 %
70-130
Dibromofluoromethane
111 %
84-123
Toluene-d8
83 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-8
Attn: Katie Lippard Sample ID: 0010154-12
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 16:00
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
80.4
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.82
0.15
1
8270E
1/15/20 22:12
JMV
POA0191
1,2-Dichlorobenzene
BRL
mg/kg dry
0.82
0.13
1
8270E
1/15/20 22:12
JMV
POA0191
1,3-Dichlorobenzene
BRL
mg/kg dry
0.82
0.12
1
8270E
1/15/20 22:12
JMV
POA0191
1,4-Dichlorobenzene
BRL
mg/kg dry
0.41
0.13
1
8270E
1/15/20 22:12
JMV
POA0191
1-Methyl naphthalene
BRL
mg/kg dry
0.82
0.013
1
8270E
1/15/20 22:12
JMV
POA0191
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.82
0.17
1
8270E
1/15/20 22:12
JMV
POA0191
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 22:12
JMV
POA0191
2,4-Dichlorophenol
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 22:12
JMV
POA0191
2,4-Dimethylphenol
BRL
mg/kg dry
0.41
0.17
1
8270E
1/15/20 22:12
JMV
POA0191
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.48
1
8270E
1/15/20 22:12
JMV
POA0191
2,4-Dinitrotoluene
BRL
mg/kg dry
0.82
0.22
1
8270E
1/15/20 22:12
JMV
POA0191
2,6-Dinitrotoluene
BRL
mg/kg dry
0.82
0.21
1
8270E
1/15/20 22:12
JMV
POA0191
2-Chloronaphthalene
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 22:12
JMV
POA0191
2-Chlorophenol
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 22:12
JMV
POA0191
2-Methyl naphthalene
BRL
mg/kg dry
0.82
0.016
1
8270E
1/15/20 22:12
JMV
POA0191
2-Methylphenol
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 22:12
JMV
POA0191
2-Nitrophenol
BRL
mg/kg dry
0.82
0.14
1
8270E
1/15/20 22:12
JMV
POA0191
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 22:12
JMV
POA0191
3/4-Methyl phenol
BRL
mg/kg dry
0.82
0.18
1
8270E
1/15/20 22:12
JMV
POA0191
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.45
1
8270E
1/15/20 22:12
JMV
POA0191
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.82
0.19
1
8270E
1/15/20 22:12
JMV
POA0191
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 22:12
JMV
POA0191
4-Chloroaniline
BRL
mg/kg dry
0.41
0.099
1
8270E
1/15/20 22:12
JMV
POA0191
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.25
1
8270E
1/15/20 22:12
JMV
POA0191
4-Nitrophenol
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 22:12
JMV
POA0191
Acenaphthene
BRL
mg/kg dry
0.82
0.019
1
8270E
1/15/20 22:12
JMV
POA0191
Acenaphthylene
BRL
mg/kg dry
0.82
0.016
1
8270E
1/15/20 22:12
JMV
POA0191
Anthracene
BRL
mg/kg dry
0.82
0.0091
1
8270E
1/15/20 22:12
JMV
POA0191
Azobenzene
BRL
mg/kg dry
0.82
0.17
1
8270E
1/15/20 22:12
JMV
POA0191
Benzo(a)anthracene
BRL
mg/kg dry
0.82
0.0098
1
8270E
1/15/20 22:12
JMV
POA0191
Benzo(a)pyrene
BRL
mg/kg dry
0.82
0.0073
1
8270E
1/15/20 22:12
JMV
POA0191
Benzo(b)fluoranthene
BRL
mg/kg dry
0.82
0.0076
1
8270E
1/15/20 22:12
JMV
POA0191
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.82
0.0081
1
8270E
1/15/20 22:12
JMV
POA0191
Benzo(k)fluoranthene
BRL
mg/kg dry
0.82
0.0087
1
8270E
1/15/20 22:12
JMV
POA0191
Benzoic Acid
BRL
mg/kg dry
2.5
0.68
1
8270E
1/15/20 22:12
JMV
POA0191
Benzyl alcohol
BRL
mg/kg dry
0.82
0.15
1
8270E
1/15/20 22:12
JMV
POA0191
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.82
0.16
1
8270E
1/15/20 22:12
JMV
POA0191
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.82
0.13
1
8270E
1/15/20 22:12
JMV
POA0191
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.41
0.15
1
8270E
1/15/20 22:12
JMV
POA0191
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-8
Attn: Katie Lippard Sample ID: 0010154-12
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 16:00
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.82
0.18
1
8270E
1/15/20 22:12
JMV
POA0191
Butyl benzyl phthalate
BRL
mg/kg dry
0.41
0.14
1
8270E
1/15/20 22:12
JMV
POA0191
Chrysene
BRL
mg/kg dry
0.82
0.0097
1
8270E
1/15/20 22:12
JMV
POA0191
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.82
0.024
1
8270E
1/15/20 22:12
JMV
POA0191
Dibenzofuran
BRL
mg/kg dry
0.82
0.22
1
8270E
1/15/20 22:12
JMV
POA0191
Diethyl phthalate
BRL
mg/kg dry
0.82
0.21
1
8270E
1/15/20 22:12
JMV
POA0191
Dimethyl phthalate
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 22:12
JMV
POA0191
Di-n-butyl phthalate
BRL
mg/kg dry
0.82
0.20
1
8270E
1/15/20 22:12
JMV
POA0191
Di-n-octyl phthalate
BRL
mg/kg dry
0.41
0.21
1
8270E
1/15/20 22:12
JMV
POA0191
Fluoranthene
BRL
mg/kg dry
0.82
0.0093
1
8270E
1/15/20 22:12
JMV
POA0191
Fluorene
BRL
mg/kg dry
0.82
0.014
1
8270E
1/15/20 22:12
JMV
POA0191
Hexachlorobenzene
BRL
mg/kg dry
0.82
0.18
1
8270E
1/15/20 22:12
JMV
POA0191
Hexachlorobutadiene
BRL
mg/kg dry
0.82
0.18
1
8270E
1/15/20 22:12
JMV
POA0191
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.82
0.28
1
8270E
1/15/20 22:12
JMV
POA0191
Hexachloroethane
BRL
mg/kg dry
0.82
0.13
1
8270E
1/15/20 22:12
JMV
POA0191
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.82
0.023
1
8270E
1/15/20 22:12
JMV
POA0191
Isophorone
BRL
mg/kg dry
0.82
0.18
1
8270E
1/15/20 22:12
JMV
POA0191
Naphthalene
BRL
mg/kg dry
0.82
0.017
1
8270E
1/15/20 22:12
JMV
POA0191
Nitrobenzene
BRL
mg/kg dry
0.41
0.17
1
8270E
1/15/20 22:12
JMV
POA0191
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.82
0.19
1
8270E
1/15/20 22:12
JMV
POA0191
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.82
0.22
1
8270E
1/15/20 22:12
JMV
POA0191
Pentachlorophenol
BRL
mg/kg dry
1.2
0.52
1
8270E
1/15/20 22:12
JMV
POA0191
Phenanthrene
BRL
mg/kg dry
0.82
0.0089
1
8270E
1/15/20 22:12
JMV
POA0191
Phenol
BRL
mg/kg dry
0.82
0.13
1
8270E
1/15/20 22:12
JMV
POA0191
Pyrene
BRL
mg/kg dry
0.82
0.012
1
8270E
1/15/20 22:12
JMV
POA0191
Pyridine
BRL
mg/kg dry
0.41
0.078
1
8270E
1/15/20 22:12
JMV
POA0191
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
72 %
39-132
2-Fluorobiphenyl
67 %
44-115
2-Fluorophenol
67 %
35-115
Nitrobenzene-d5
59 %
37-122
Phenol-d5
64 %
34-121
Terphenyl-d14
71 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.062
0.022
1
7471B
1/16/20 10:39
JAB
POA0212
Arsenic
0.54 J
mg/kg dry
1.2
0.16
1
6010D
1/18/20
0:50
JAB
POA0181
Barium
54
mg/kg dry
12
3.7
1
6010D
1/18/20
0:50
JAB
POA0181
Cadmium
BRL
mg/kg dry
0.62
0.042
1
6010D
1/18/20
0:50
JAB
POA0181
Chromium
8.7
mg/kg dry
1.2
0.094
1
6010D
1/18/20
0:50
JAB
POA0181
Lead
13
mg/kg dry
1.2
0.21
1
6010D
1/18/20
0:50
JAB
POA0181
Selenium
BRL
mg/kg dry
1.2
0.34
1
6010D
1/18/20
0:50
JAB
POA0181
Silver
BRL
mg/kg dry
0.62
0.038
1
6010D
1/18/20
0:50
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-8
Attn: Katie Lippard Sample ID: 0010154-12
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 16:00
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0057
0.00070
1
8260D
1/16/20 17:34
TBL
POA0231
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0057
0.00084
1
8260D
1/16/20 17:34
TBL
POA0231
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0057
0.00042
1
8260D
1/16/20 17:34
TBL
POA0231
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0057
0.00062
1
8260D
1/16/20 17:34
TBL
POA0231
1,1-Dichloroethane
BRL
mg/kg dry
0.0057
0.0010
1
8260D
1/16/20 17:34
TBL
POA0231
1,1-Dichloroethylene
BRL
mg/kg dry
0.0057
0.0010
1
8260D
1/16/20 17:34
TBL
POA0231
1,1-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00088
1
8260D
1/16/20 17:34
TBL
POA0231
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00082
1
8260D
1/16/20 17:34
TBL
POA0231
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0057
0.00065
1
8260D
1/16/20 17:34
TBL
POA0231
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00054
1
8260D
1/16/20 17:34
TBL
POA0231
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0057
0.00060
1
8260D
1/16/20 17:34
TBL
POA0231
1,2-Dibromoethane
BRL
mg/kg dry
0.0057
0.00051
1
8260D
1/16/20 17:34
TBL
POA0231
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00064
1
8260D
1/16/20 17:34
TBL
POA0231
1,2-Dichloroethane
BRL
mg/kg dry
0.0057
0.00068
1
8260D
1/16/20 17:34
TBL
POA0231
1,2-Dichloropropane
BRL
mg/kg dry
0.0057
0.00086
1
8260D
1/16/20 17:34
TBL
POA0231
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0057
0.00072
1
8260D
1/16/20 17:34
TBL
POA0231
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00071
1
8260D
1/16/20 17:34
TBL
POA0231
1,3-Dichloropropane
BRL
mg/kg dry
0.0057
0.00048
1
8260D
1/16/20 17:34
TBL
POA0231
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00072
1
8260D
1/16/20 17:34
TBL
POA0231
2,2-Dichloropropane
BRL
mg/kg dry
0.0057
0.00071
1
8260D
1/16/20 17:34
TBL
POA0231
2-Chlorotoluene
BRL
mg/kg dry
0.0057
0.00076
1
8260D
1/16/20 17:34
TBL
POA0231
4-Chlorotoluene
BRL
mg/kg dry
0.0057
0.00065
1
8260D
1/16/20 17:34
TBL
POA0231
4-Isopropyltoluene
BRL
mg/kg dry
0.0057
0.0014
1
8260D
1/16/20 17:34
TBL
POA0231
Acetone
0.015 J
mg/kg dry
0.023
0.0015
1
8260D
1/16/20 17:34
TBL
POA0231
Benzene
BRL
mg/kg dry
0.0057
0.00089
1
8260D
1/16/20 17:34
TBL
POA0231
Bromobenzene
BRL
mg/kg dry
0.0057
0.00079
1
8260D
1/16/20 17:34
TBL
POA0231
Bromochloromethane
BRL
mg/kg dry
0.0057
0.00094
1
8260D
1/16/20 17:34
TBL
POA0231
Bromodichloromethane
BRL
mg/kg dry
0.0057
0.00054
1
8260D
1/16/20 17:34
TBL
POA0231
Bromoform
BRL
mg/kg dry
0.0057
0.00044
1
8260D
1/16/20 17:34
TBL
POA0231
Bromomethane
BRL
mg/kg dry
0.011
0.0028
1
8260D
1/16/20 17:34
TBL
POA0231
Carbon Tetrachloride
BRL
mg/kg dry
0.0057
0.0011
1
8260D
1/16/20 17:34
TBL
POA0231
Chlorobenzene
BRL
mg/kg dry
0.0057
0.00089
1
8260D
1/16/20 17:34
TBL
POA0231
Chloroethane
BRL
mg/kg dry
0.011
0.0011
1
8260D
1/16/20 17:34
TBL
POA0231
Chloroform
BRL
mg/kg dry
0.0057
0.00070
1
8260D
1/16/20 17:34
TBL
POA0231
Chloromethane
BRL
mg/kg dry
0.011
0.0017
1
8260D
1/16/20 17:34
TBL
POA0231
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0057
0.00090
1
8260D
1/16/20 17:34
TBL
POA0231
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00056
1
8260D
1/16/20 17:34
TBL
POA0231
Dibromochloromethane
BRL
mg/kg dry
0.0057
0.00038
1
8260D
1/16/20 17:34
TBL
POA0231
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0016
1
8260D
1/16/20 17:34
TBL
POA0231
Ethylbenzene
BRL
mg/kg dry
0.0057
0.00086
1
8260D
1/16/20 17:34
TBL
POA0231
Isopropyl Ether
BRL
mg/kg dry
0.0057
0.00084
1
8260D
1/16/20 17:34
TBL
POA0231
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0057
0.00066
1
8260D
1/16/20 17:34
TBL
POA0231
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-8
Attn: Katie Lippard Sample ID: 0010154-12
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 16:00
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.011
0.0015
1
8260D
1/16/20 17:34
TBL
POA0231
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.023
0.00039
1
8260D
1/16/20 17:34
TBL
POA0231
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.023
0.0013
1
8260D
1/16/20 17:34
TBL
POA0231
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.023
0.00047
1
8260D
1/16/20 17:34
TBL
POA0231
Methylene Chloride
BRL
mg/kg dry
0.0057
0.00092
1
8260D
1/16/20 17:34
TBL
POA0231
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0057
0.00080
1
8260D
1/16/20 17:34
TBL
POA0231
Naphthalene
BRL
mg/kg dry
0.011
0.00058
1
8260D
1/16/20 17:34
TBL
POA0231
n-Butylbenzene
BRL
mg/kg dry
0.0057
0.00053
1
8260D
1/16/20 17:34
TBL
POA0231
n-Propylbenzene
BRL
mg/kg dry
0.0057
0.00083
1
8260D
1/16/20 17:34
TBL
POA0231
o-Xylene
BRL
mg/kg dry
0.0057
0.00061
1
8260D
1/16/20 17:34
TBL
POA0231
sec-Butylbenzene
BRL
mg/kg dry
0.0057
0.00062
1
8260D
1/16/20 17:34
TBL
POA0231
Styrene
BRL
mg/kg dry
0.0057
0.00055
1
8260D
1/16/20 17:34
TBL
POA0231
tert-Butylbenzene
BRL
mg/kg dry
0.0057
0.00068
1
8260D
1/16/20 17:34
TBL
POA0231
Tetrachloroethylene
BRL
mg/kg dry
0.0057
0.0010
1
8260D
1/16/20 17:34
TBL
POA0231
Toluene
BRL
mg/kg dry
0.0057
0.00091
1
8260D
1/16/20 17:34
TBL
POA0231
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0057
0.0011
1
8260D
1/16/20 17:34
TBL
POA0231
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00049
1
8260D
1/16/20 17:34
TBL
POA0231
Trichloroethylene
BRL
mg/kg dry
0.0057
0.0011
1
8260D
1/16/20 17:34
TBL
POA0231
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
1/16/20 17:34
TBL
POA0231
Vinyl acetate
BRL
mg/kg dry
0.011
0.00062
1
8260D
1/16/20 17:34
TBL
POA0231
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260D
1/16/20 17:34
TBL
POA0231
Xylenes, total
BRL
mg/kg dry
0.017
0.0021
1
8260D
1/16/20 17:34
TBL
POA0231
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
83 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-9S
Attn: Katie Lippard Sample ID: 0010154-13
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 16:50
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
87.1
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.75
0.13
1
8270E
1/16/20 17:58
JMV
POA0221
1,2-Dichlorobenzene
BRL
mg/kg dry
0.75
0.12
1
8270E
1/16/20 17:58
JMV
POA0221
1,3-Dichlorobenzene
BRL
mg/kg dry
0.75
0.11
1
8270E
1/16/20 17:58
JMV
POA0221
1,4-Dichlorobenzene
BRL
mg/kg dry
0.38
0.12
1
8270E
1/16/20 17:58
JMV
POA0221
1-Methyl naphthalene
BRL
mg/kg dry
0.75
0.012
1
8270E
1/16/20 17:58
JMV
POA0221
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.75
0.16
1
8270E
1/16/20 17:58
JMV
POA0221
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.75
0.18
1
8270E
1/16/20 17:58
JMV
POA0221
2,4-Dichlorophenol
BRL
mg/kg dry
0.75
0.15
1
8270E
1/16/20 17:58
JMV
POA0221
2,4-Dimethylphenol
BRL
mg/kg dry
0.38
0.16
1
8270E
1/16/20 17:58
JMV
POA0221
2,4-Dinitrophenol
BRL
mg/kg dry
1.7
0.44
1
8270E
1/16/20 17:58
JMV
POA0221
2,4-Dinitrotoluene
BRL
mg/kg dry
0.75
0.20
1
8270E
1/16/20 17:58
JMV
POA0221
2,6-Dinitrotoluene
BRL
mg/kg dry
0.75
0.20
1
8270E
1/16/20 17:58
JMV
POA0221
2-Chloronaphthalene
BRL
mg/kg dry
0.75
0.18
1
8270E
1/16/20 17:58
JMV
POA0221
2-Chlorophenol
BRL
mg/kg dry
0.75
0.14
1
8270E
1/16/20 17:58
JMV
POA0221
2-Methyl naphthalene
BRL
mg/kg dry
0.75
0.015
1
8270E
1/16/20 17:58
JMV
POA0221
2-Methylphenol
BRL
mg/kg dry
0.75
0.14
1
8270E
1/16/20 17:58
JMV
POA0221
2-Nitrophenol
BRL
mg/kg dry
0.75
0.13
1
8270E
1/16/20 17:58
JMV
POA0221
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.75
0.15
1
8270E
1/16/20 17:58
JMV
POA0221
3/4-Methyl phenol
BRL
mg/kg dry
0.75
0.16
1
8270E
1/16/20 17:58
JMV
POA0221
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.7
0.42
1
8270E
1/16/20 17:58
JMV
POA0221
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.75
0.18
1
8270E
1/16/20 17:58
JMV
POA0221
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.75
0.14
1
8270E
1/16/20 17:58
JMV
POA0221
4-Chloroaniline
BRL
mg/kg dry
0.38
0.091
1
8270E
1/16/20 17:58
JMV
POA0221
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.1
0.23
1
8270E
1/16/20 17:58
JMV
POA0221
4-Nitrophenol
BRL
mg/kg dry
0.75
0.19
1
8270E
1/16/20 17:58
JMV
POA0221
Acenaphthene
BRL
mg/kg dry
0.75
0.017
1
8270E
1/16/20 17:58
JMV
POA0221
Acenaphthylene
BRL
mg/kg dry
0.75
0.015
1
8270E
1/16/20 17:58
JMV
POA0221
Anthracene
BRL
mg/kg dry
0.75
0.0083
1
8270E
1/16/20 17:58
JMV
POA0221
Azobenzene
BRL
mg/kg dry
0.75
0.16
1
8270E
1/16/20 17:58
JMV
POA0221
Benzo(a)anthracene
BRL
mg/kg dry
0.75
0.0090
1
8270E
1/16/20 17:58
JMV
POA0221
Benzo(a)pyrene
BRL
mg/kg dry
0.75
0.0067
1
8270E
1/16/20 17:58
JMV
POA0221
Benzo(b)fluoranthene
BRL
mg/kg dry
0.75
0.0070
1
8270E
1/16/20 17:58
JMV
POA0221
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.75
0.0074
1
8270E
1/16/20 17:58
JMV
POA0221
Benzo(k)fluoranthene
BRL
mg/kg dry
0.75
0.0080
1
8270E
1/16/20 17:58
JMV
POA0221
Benzoic Acid
BRL
mg/kg dry
2.3
0.63
1
8270E
1/16/20 17:58
JMV
POA0221
Benzyl alcohol
BRL
mg/kg dry
0.75
0.14
1
8270E
1/16/20 17:58
JMV
POA0221
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.75
0.14
1
8270E
1/16/20 17:58
JMV
POA0221
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.75
0.12
1
8270E
1/16/20 17:58
JMV
POA0221
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.38
0.13
1
8270E
1/16/20 17:58
JMV
POA0221
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-9S
Attn: Katie Lippard Sample ID: 0010154-13
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 16:50
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.75
0.17
1
8270E
1/16/20 17:58
JMV
POA0221
Butyl benzyl phthalate
BRL
mg/kg dry
0.38
0.13
1
8270E
1/16/20 17:58
JMV
POA0221
Chrysene
BRL
mg/kg dry
0.75
0.0089
1
8270E
1/16/20 17:58
JMV
POA0221
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.75
0.022
1
8270E
1/16/20 17:58
JMV
POA0221
Dibenzofuran
BRL
mg/kg dry
0.75
0.20
1
8270E
1/16/20 17:58
JMV
POA0221
Diethyl phthalate
BRL
mg/kg dry
0.75
0.19
1
8270E
1/16/20 17:58
JMV
POA0221
Dimethyl phthalate
BRL
mg/kg dry
0.75
0.18
1
8270E
1/16/20 17:58
JMV
POA0221
Di-n-butyl phthalate
BRL
mg/kg dry
0.75
0.19
1
8270E
1/16/20 17:58
JMV
POA0221
Di-n-octyl phthalate
BRL
mg/kg dry
0.38
0.20
1
8270E
1/16/20 17:58
JMV
POA0221
Fluoranthene
BRL
mg/kg dry
0.75
0.0086
1
8270E
1/16/20 17:58
JMV
POA0221
Fluorene
BRL
mg/kg dry
0.75
0.013
1
8270E
1/16/20 17:58
JMV
POA0221
Hexachlorobenzene
BRL
mg/kg dry
0.75
0.17
1
8270E
1/16/20 17:58
JMV
POA0221
Hexachlorobutadiene
BRL
mg/kg dry
0.75
0.17
1
8270E
1/16/20 17:58
JMV
POA0221
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.75
0.26
1
8270E
1/16/20 17:58
JMV
POA0221
Hexachloroethane
BRL
mg/kg dry
0.75
0.12
1
8270E
1/16/20 17:58
JMV
POA0221
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.75
0.021
1
8270E
1/16/20 17:58
JMV
POA0221
Isophorone
BRL
mg/kg dry
0.75
0.16
1
8270E
1/16/20 17:58
JMV
POA0221
Naphthalene
BRL
mg/kg dry
0.75
0.016
1
8270E
1/16/20 17:58
JMV
POA0221
Nitrobenzene
BRL
mg/kg dry
0.38
0.16
1
8270E
1/16/20 17:58
JMV
POA0221
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.75
0.17
1
8270E
1/16/20 17:58
JMV
POA0221
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.75
0.21
1
8270E
1/16/20 17:58
JMV
POA0221
Pentachlorophenol
BRL
mg/kg dry
1.1
0.48
1
8270E
1/16/20 17:58
JMV
POA0221
Phenanthrene
BRL
mg/kg dry
0.75
0.0082
1
8270E
1/16/20 17:58
JMV
POA0221
Phenol
BRL
mg/kg dry
0.75
0.12
1
8270E
1/16/20 17:58
JMV
POA0221
Pyrene
BRL
mg/kg dry
0.75
0.011
1
8270E
1/16/20 17:58
JMV
POA0221
Pyridine
BRL
mg/kg dry
0.38
0.072
1
8270E
1/16/20 17:58
JMV
POA0221
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
77 %
39-132
2-Fluorobiphenyl
77 %
44-115
2-Fluorophenol
71 %
35-115
Nitrobenzene-d5
70 %
37-122
Phenol-d5
72 %
34-121
Terphenyl-d14
78 %
54-127
Total Metals
Mercury
0.026 J
mg/kg dry
0.057
0.020
1
7471B
1/16/20 10:44
JAB
POA0212
Arsenic
3.1
mg/kg dry
1.1
0.15
1
6010D
1/18/20
0:58
JAB
POA0181
Barium
62
mg/kg dry
11
3.4
1
6010D
1/18/20
0:58
JAB
POA0181
Cadmium
BRL
mg/kg dry
0.57
0.039
1
6010D
1/18/20
0:58
JAB
POA0181
Chromium
25
mg/kg dry
1.1
0.087
1
6010D
1/18/20
0:58
JAB
POA0181
Lead
20
mg/kg dry
1.1
0.19
1
6010D
1/18/20
0:58
JAB
POA0181
Selenium
BRL
mg/kg dry
1.1
0.32
1
6010D
1/18/20
0:58
JAB
POA0181
Silver
BRL
mg/kg dry
0.57
0.035
1
6010D
1/18/20
0:58
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-9S
Attn: Katie Lippard Sample ID: 0010154-13
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 16:50
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0056
0.00068
1
8260D
1/16/20 18:04
TBL
POA0231
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0056
0.00082
1
8260D
1/16/20 18:04
TBL
POA0231
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0056
0.00041
1
8260D
1/16/20 18:04
TBL
POA0231
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0056
0.00060
1
8260D
1/16/20 18:04
TBL
POA0231
1,1-Dichloroethane
BRL
mg/kg dry
0.0056
0.0010
1
8260D
1/16/20 18:04
TBL
POA0231
1,1-Dichloroethylene
BRL
mg/kg dry
0.0056
0.0010
1
8260D
1/16/20 18:04
TBL
POA0231
1,1-Dichloropropylene
BRL
mg/kg dry
0.0056
0.00086
1
8260D
1/16/20 18:04
TBL
POA0231
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00080
1
8260D
1/16/20 18:04
TBL
POA0231
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0056
0.00064
1
8260D
1/16/20 18:04
TBL
POA0231
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00053
1
8260D
1/16/20 18:04
TBL
POA0231
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0056
0.00059
1
8260D
1/16/20 18:04
TBL
POA0231
1,2-Dibromoethane
BRL
mg/kg dry
0.0056
0.00050
1
8260D
1/16/20 18:04
TBL
POA0231
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0056
0.00062
1
8260D
1/16/20 18:04
TBL
POA0231
1,2-Dichloroethane
BRL
mg/kg dry
0.0056
0.00067
1
8260D
1/16/20 18:04
TBL
POA0231
1,2-Dichloropropane
BRL
mg/kg dry
0.0056
0.00084
1
8260D
1/16/20 18:04
TBL
POA0231
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0056
0.00070
1
8260D
1/16/20 18:04
TBL
POA0231
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0056
0.00070
1
8260D
1/16/20 18:04
TBL
POA0231
1,3-Dichloropropane
BRL
mg/kg dry
0.0056
0.00047
1
8260D
1/16/20 18:04
TBL
POA0231
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0056
0.00071
1
8260D
1/16/20 18:04
TBL
POA0231
2,2-Dichloropropane
BRL
mg/kg dry
0.0056
0.00070
1
8260D
1/16/20 18:04
TBL
POA0231
2-Chlorotoluene
BRL
mg/kg dry
0.0056
0.00075
1
8260D
1/16/20 18:04
TBL
POA0231
4-Chlorotoluene
BRL
mg/kg dry
0.0056
0.00064
1
8260D
1/16/20 18:04
TBL
POA0231
4-Isopropyltoluene
BRL
mg/kg dry
0.0056
0.0014
1
8260D
1/16/20 18:04
TBL
POA0231
Acetone
0.18
mg/kg dry
0.022
0.0014
1
8260D
1/16/20 18:04
TBL
POA0231
Benzene
0.0011 J
mg/kg dry
0.0056
0.00087
1
8260D
1/16/20 18:04
TBL
POA0231
Bromobenzene
BRL
mg/kg dry
0.0056
0.00078
1
8260D
1/16/20 18:04
TBL
POA0231
Bromochloromethane
BRL
mg/kg dry
0.0056
0.00092
1
8260D
1/16/20 18:04
TBL
POA0231
Bromodichloromethane
BRL
mg/kg dry
0.0056
0.00053
1
8260D
1/16/20 18:04
TBL
POA0231
Bromoform
BRL
mg/kg dry
0.0056
0.00043
1
8260D
1/16/20 18:04
TBL
POA0231
Bromomethane
0.0034 J
mg/kg dry
0.011
0.0027
1
8260D
1/16/20 18:04
TBL
POA0231
Carbon Tetrachloride
BRL
mg/kg dry
0.0056
0.0011
1
8260D
1/16/20 18:04
TBL
POA0231
Chlorobenzene
BRL
mg/kg dry
0.0056
0.00087
1
8260D
1/16/20 18:04
TBL
POA0231
Chloroethane
BRL
mg/kg dry
0.011
0.0011
1
8260D
1/16/20 18:04
TBL
POA0231
Chloroform
BRL
mg/kg dry
0.0056
0.00068
1
8260D
1/16/20 18:04
TBL
POA0231
Chloromethane
BRL
mg/kg dry
0.011
0.0017
1
8260D
1/16/20 18:04
TBL
POA0231
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0056
0.00088
1
8260D
1/16/20 18:04
TBL
POA0231
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0056
0.00055
1
8260D
1/16/20 18:04
TBL
POA0231
Dibromochloromethane
BRL
mg/kg dry
0.0056
0.00037
1
8260D
1/16/20 18:04
TBL
POA0231
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0016
1
8260D
1/16/20 18:04
TBL
POA0231
Ethylbenzene
BRL
mg/kg dry
0.0056
0.00084
1
8260D
1/16/20 18:04
TBL
POA0231
Isopropyl Ether
BRL
mg/kg dry
0.0056
0.00082
1
8260D
1/16/20 18:04
TBL
POA0231
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0056
0.00065
1
8260D
1/16/20 18:04
TBL
POA0231
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-9S
Attn: Katie Lippard Sample ID: 0010154-13
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 16:50
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.011
0.0014
1
8260D
1/16/20 18:04
TBL
POA0231
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.022
0.00039
1
8260D
1/16/20 18:04
TBL
POA0231
Methyl Ethyl Ketone (2-Butanone)
0.025
mg/kg dry
0.022
0.0013
1
8260D
1/16/20 18:04
TBL
POA0231
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.022
0.00046
1
8260D
1/16/20 18:04
TBL
POA0231
Methylene Chloride
BRL
mg/kg dry
0.0056
0.00090
1
8260D
1/16/20 18:04
TBL
POA0231
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0056
0.00078
1
8260D
1/16/20 18:04
TBL
POA0231
Naphthalene
BRL
mg/kg dry
0.011
0.00056
1
8260D
1/16/20 18:04
TBL
POA0231
n-Butylbenzene
BRL
mg/kg dry
0.0056
0.00052
1
8260D
1/16/20 18:04
TBL
POA0231
n-Propylbenzene
BRL
mg/kg dry
0.0056
0.00081
1
8260D
1/16/20 18:04
TBL
POA0231
o-Xylene
BRL
mg/kg dry
0.0056
0.00060
1
8260D
1/16/20 18:04
TBL
POA0231
sec-Butylbenzene
BRL
mg/kg dry
0.0056
0.00060
1
8260D
1/16/20 18:04
TBL
POA0231
Styrene
BRL
mg/kg dry
0.0056
0.00054
1
8260D
1/16/20 18:04
TBL
POA0231
tert-Butylbenzene
BRL
mg/kg dry
0.0056
0.00066
1
8260D
1/16/20 18:04
TBL
POA0231
Tetrachloroethylene
BRL
mg/kg dry
0.0056
0.0010
1
8260D
1/16/20 18:04
TBL
POA0231
Toluene
BRL
mg/kg dry
0.0056
0.00089
1
8260D
1/16/20 18:04
TBL
POA0231
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0056
0.0011
1
8260D
1/16/20 18:04
TBL
POA0231
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0056
0.00048
1
8260D
1/16/20 18:04
TBL
POA0231
Trichloroethylene
BRL
mg/kg dry
0.0056
0.0011
1
8260D
1/16/20 18:04
TBL
POA0231
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
1/16/20 18:04
TBL
POA0231
Vinyl acetate
BRL
mg/kg dry
0.011
0.00061
1
8260D
1/16/20 18:04
TBL
POA0231
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260D
1/16/20 18:04
TBL
POA0231
Xylenes, total
BRL
mg/kg dry
0.017
0.0020
1
8260D
1/16/20 18:04
TBL
POA0231
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
70-130
Dibromofluoromethane
106 %
84-123
Toluene-d8
84 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-91D
Attn: Katie Lippard Sample ID: 0010154-14
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 17:00
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
76.0
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.87
0.15
1
8270E
1/16/20 18:20
JMV
POA0221
1,2-Dichlorobenzene
BRL
mg/kg dry
0.87
0.14
1
8270E
1/16/20 18:20
JMV
POA0221
1,3-Dichlorobenzene
BRL
mg/kg dry
0.87
0.13
1
8270E
1/16/20 18:20
JMV
POA0221
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.14
1
8270E
1/16/20 18:20
JMV
POA0221
1-Methyl naphthalene
BRL
mg/kg dry
0.87
0.013
1
8270E
1/16/20 18:20
JMV
POA0221
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.87
0.18
1
8270E
1/16/20 18:20
JMV
POA0221
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.87
0.21
1
8270E
1/16/20 18:20
JMV
POA0221
2,4-Dichlorophenol
BRL
mg/kg dry
0.87
0.17
1
8270E
1/16/20 18:20
JMV
POA0221
2,4-Dimethylphenol
BRL
mg/kg dry
0.43
0.18
1
8270E
1/16/20 18:20
JMV
POA0221
2,4-Dinitrophenol
BRL
mg/kg dry
2.0
0.51
1
8270E
1/16/20 18:20
JMV
POA0221
2,4-Dinitrotoluene
BRL
mg/kg dry
0.87
0.23
1
8270E
1/16/20 18:20
JMV
POA0221
2,6-Dinitrotoluene
BRL
mg/kg dry
0.87
0.22
1
8270E
1/16/20 18:20
JMV
POA0221
2-Chloronaphthalene
BRL
mg/kg dry
0.87
0.21
1
8270E
1/16/20 18:20
JMV
POA0221
2-Chlorophenol
BRL
mg/kg dry
0.87
0.17
1
8270E
1/16/20 18:20
JMV
POA0221
2-Methyl naphthalene
BRL
mg/kg dry
0.87
0.017
1
8270E
1/16/20 18:20
JMV
POA0221
2-Methylphenol
BRL
mg/kg dry
0.87
0.17
1
8270E
1/16/20 18:20
JMV
POA0221
2-Nitrophenol
BRL
mg/kg dry
0.87
0.14
1
8270E
1/16/20 18:20
JMV
POA0221
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.87
0.17
1
8270E
1/16/20 18:20
JMV
POA0221
3/4-Methyl phenol
BRL
mg/kg dry
0.87
0.19
1
8270E
1/16/20 18:20
JMV
POA0221
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.0
0.48
1
8270E
1/16/20 18:20
JMV
POA0221
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.87
0.20
1
8270E
1/16/20 18:20
JMV
POA0221
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.87
0.17
1
8270E
1/16/20 18:20
JMV
POA0221
4-Chloroaniline
BRL
mg/kg dry
0.43
0.11
1
8270E
1/16/20 18:20
JMV
POA0221
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.27
1
8270E
1/16/20 18:20
JMV
POA0221
4-Nitrophenol
BRL
mg/kg dry
0.87
0.21
1
8270E
1/16/20 18:20
JMV
POA0221
Acenaphthene
BRL
mg/kg dry
0.87
0.020
1
8270E
1/16/20 18:20
JMV
POA0221
Acenaphthylene
BRL
mg/kg dry
0.87
0.017
1
8270E
1/16/20 18:20
JMV
POA0221
Anthracene
BRL
mg/kg dry
0.87
0.0096
1
8270E
1/16/20 18:20
JMV
POA0221
Azobenzene
BRL
mg/kg dry
0.87
0.19
1
8270E
1/16/20 18:20
JMV
POA0221
Benzo(a)anthracene
BRL
mg/kg dry
0.87
0.010
1
8270E
1/16/20 18:20
JMV
POA0221
Benzo(a)pyrene
BRL
mg/kg dry
0.87
0.0078
1
8270E
1/16/20 18:20
JMV
POA0221
Benzo(b)fluoranthene
BRL
mg/kg dry
0.87
0.0080
1
8270E
1/16/20 18:20
JMV
POA0221
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.87
0.0085
1
8270E
1/16/20 18:20
JMV
POA0221
Benzo(k)fluoranthene
BRL
mg/kg dry
0.87
0.0092
1
8270E
1/16/20 18:20
JMV
POA0221
Benzoic Acid
BRL
mg/kg dry
2.6
0.72
1
8270E
1/16/20 18:20
JMV
POA0221
Benzyl alcohol
BRL
mg/kg dry
0.87
0.16
1
8270E
1/16/20 18:20
JMV
POA0221
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.87
0.17
1
8270E
1/16/20 18:20
JMV
POA0221
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.87
0.14
1
8270E
1/16/20 18:20
JMV
POA0221
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.16
1
8270E
1/16/20 18:20
JMV
POA0221
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-91D
Attn: Katie Lippard Sample ID: 0010154-14
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 17:00
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.87
0.20
1
8270E
1/16/20 18:20
JMV
POA0221
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
8270E
1/16/20 18:20
JMV
POA0221
Chrysene
BRL
mg/kg dry
0.87
0.010
1
8270E
1/16/20 18:20
JMV
POA0221
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.87
0.025
1
8270E
1/16/20 18:20
JMV
POA0221
Dibenzofuran
BRL
mg/kg dry
0.87
0.23
1
8270E
1/16/20 18:20
JMV
POA0221
Diethyl phthalate
BRL
mg/kg dry
0.87
0.22
1
8270E
1/16/20 18:20
JMV
POA0221
Dimethyl phthalate
BRL
mg/kg dry
0.87
0.21
1
8270E
1/16/20 18:20
JMV
POA0221
Di-n-butyl phthalate
BRL
mg/kg dry
0.87
0.22
1
8270E
1/16/20 18:20
JMV
POA0221
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
8270E
1/16/20 18:20
JMV
POA0221
Fluoranthene
BRL
mg/kg dry
0.87
0.0099
1
8270E
1/16/20 18:20
JMV
POA0221
Fluorene
BRL
mg/kg dry
0.87
0.015
1
8270E
1/16/20 18:20
JMV
POA0221
Hexachlorobenzene
BRL
mg/kg dry
0.87
0.19
1
8270E
1/16/20 18:20
JMV
POA0221
Hexachlorobutadiene
BRL
mg/kg dry
0.87
0.20
1
8270E
1/16/20 18:20
JMV
POA0221
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.87
0.30
1
8270E
1/16/20 18:20
JMV
POA0221
Hexachloroethane
BRL
mg/kg dry
0.87
0.14
1
8270E
1/16/20 18:20
JMV
POA0221
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.87
0.024
1
8270E
1/16/20 18:20
JMV
POA0221
Isophorone
BRL
mg/kg dry
0.87
0.19
1
8270E
1/16/20 18:20
JMV
POA0221
Naphthalene
BRL
mg/kg dry
0.87
0.018
1
8270E
1/16/20 18:20
JMV
POA0221
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
8270E
1/16/20 18:20
JMV
POA0221
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.87
0.20
1
8270E
1/16/20 18:20
JMV
POA0221
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.87
0.24
1
8270E
1/16/20 18:20
JMV
POA0221
Pentachlorophenol
BRL
mg/kg dry
1.3
0.55
1
8270E
1/16/20 18:20
JMV
POA0221
Phenanthrene
BRL
mg/kg dry
0.87
0.0095
1
8270E
1/16/20 18:20
JMV
POA0221
Phenol
BRL
mg/kg dry
0.87
0.14
1
8270E
1/16/20 18:20
JMV
POA0221
Pyrene
BRL
mg/kg dry
0.87
0.013
1
8270E
1/16/20 18:20
JMV
POA0221
Pyridine
BRL
mg/kg dry
0.43
0.083
1
8270E
1/16/20 18:20
JMV
POA0221
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
92 %
39-132
2-Fluorobiphenyl
76 %
44-115
2-Fluorophenol
77 %
35-115
Nitrobenzene-d5
71 %
37-122
Phenol-d5
74 %
34-121
Terphenyl-d14
78 %
54-127
Total Metals
Mercury
0.032 J
mg/kg dry
0.066
0.023
1
7471B
1/16/20 10:48
JAB
POA0212
Arsenic
1.9
mg/kg dry
1.3
0.17
1
6010D
1/18/20
1:07
JAB
POA0181
Barium
49
mg/kg dry
13
3.9
1
6010D
1/18/20
1:07
JAB
POA0181
Cadmium
BRL
mg/kg dry
0.66
0.044
1
6010D
1/18/20
1:07
JAB
POA0181
Chromium
16
mg/kg dry
1.3
0.10
1
6010D
1/18/20
1:07
JAB
POA0181
Lead
23
mg/kg dry
1.3
0.22
1
6010D
1/18/20
1:07
JAB
POA0181
Selenium
BRL
mg/kg dry
1.3
0.36
1
6010D
1/18/20
1:07
JAB
POA0181
Silver
BRL
mg/kg dry
0.66
0.040
1
6010D
1/18/20
1:07
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-91D
Attn: Katie Lippard Sample ID: 0010154-14
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 17:00
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0057
0.00070
1
8260D
1/16/20 18:34
TBL
POA0231
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0057
0.00084
1
8260D
1/16/20 18:34
TBL
POA0231
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0057
0.00041
1
8260D
1/16/20 18:34
TBL
POA0231
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0057
0.00062
1
8260D
1/16/20 18:34
TBL
POA0231
1,1-Dichloroethane
BRL
mg/kg dry
0.0057
0.0010
1
8260D
1/16/20 18:34
TBL
POA0231
1,1-Dichloroethylene
BRL
mg/kg dry
0.0057
0.0010
1
8260D
1/16/20 18:34
TBL
POA0231
1,1-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00088
1
8260D
1/16/20 18:34
TBL
POA0231
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00082
1
8260D
1/16/20 18:34
TBL
POA0231
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0057
0.00065
1
8260D
1/16/20 18:34
TBL
POA0231
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00054
1
8260D
1/16/20 18:34
TBL
POA0231
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0057
0.00060
1
8260D
1/16/20 18:34
TBL
POA0231
1,2-Dibromoethane
BRL
mg/kg dry
0.0057
0.00051
1
8260D
1/16/20 18:34
TBL
POA0231
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00064
1
8260D
1/16/20 18:34
TBL
POA0231
1,2-Dichloroethane
BRL
mg/kg dry
0.0057
0.00068
1
8260D
1/16/20 18:34
TBL
POA0231
1,2-Dichloropropane
BRL
mg/kg dry
0.0057
0.00086
1
8260D
1/16/20 18:34
TBL
POA0231
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0057
0.00072
1
8260D
1/16/20 18:34
TBL
POA0231
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00071
1
8260D
1/16/20 18:34
TBL
POA0231
1,3-Dichloropropane
BRL
mg/kg dry
0.0057
0.00048
1
8260D
1/16/20 18:34
TBL
POA0231
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00072
1
8260D
1/16/20 18:34
TBL
POA0231
2,2-Dichloropropane
BRL
mg/kg dry
0.0057
0.00071
1
8260D
1/16/20 18:34
TBL
POA0231
2-Chlorotoluene
BRL
mg/kg dry
0.0057
0.00076
1
8260D
1/16/20 18:34
TBL
POA0231
4-Chlorotoluene
BRL
mg/kg dry
0.0057
0.00065
1
8260D
1/16/20 18:34
TBL
POA0231
4-Isopropyltoluene
BRL
mg/kg dry
0.0057
0.0014
1
8260D
1/16/20 18:34
TBL
POA0231
Acetone
BRL
mg/kg dry
0.023
0.0015
1
8260D
1/16/20 18:34
TBL
POA0231
Benzene
BRL
mg/kg dry
0.0057
0.00089
1
8260D
1/16/20 18:34
TBL
POA0231
Bromobenzene
BRL
mg/kg dry
0.0057
0.00079
1
8260D
1/16/20 18:34
TBL
POA0231
Bromochloromethane
BRL
mg/kg dry
0.0057
0.00094
1
8260D
1/16/20 18:34
TBL
POA0231
Bromodichloromethane
BRL
mg/kg dry
0.0057
0.00054
1
8260D
1/16/20 18:34
TBL
POA0231
Bromoform
BRL
mg/kg dry
0.0057
0.00044
1
8260D
1/16/20 18:34
TBL
POA0231
Bromomethane
BRL
mg/kg dry
0.011
0.0028
1
8260D
1/16/20 18:34
TBL
POA0231
Carbon Tetrachloride
BRL
mg/kg dry
0.0057
0.0011
1
8260D
1/16/20 18:34
TBL
POA0231
Chlorobenzene
BRL
mg/kg dry
0.0057
0.00089
1
8260D
1/16/20 18:34
TBL
POA0231
Chloroethane
BRL
mg/kg dry
0.011
0.0011
1
8260D
1/16/20 18:34
TBL
POA0231
Chloroform
BRL
mg/kg dry
0.0057
0.00070
1
8260D
1/16/20 18:34
TBL
POA0231
Chloromethane
BRL
mg/kg dry
0.011
0.0017
1
8260D
1/16/20 18:34
TBL
POA0231
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0057
0.00090
1
8260D
1/16/20 18:34
TBL
POA0231
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00056
1
8260D
1/16/20 18:34
TBL
POA0231
Dibromochloromethane
BRL
mg/kg dry
0.0057
0.00038
1
8260D
1/16/20 18:34
TBL
POA0231
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0016
1
8260D
1/16/20 18:34
TBL
POA0231
Ethylbenzene
BRL
mg/kg dry
0.0057
0.00086
1
8260D
1/16/20 18:34
TBL
POA0231
Isopropyl Ether
BRL
mg/kg dry
0.0057
0.00084
1
8260D
1/16/20 18:34
TBL
POA0231
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0057
0.00066
1
8260D
1/16/20 18:34
TBL
POA0231
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: 13-91D
Attn: Katie Lippard Sample ID: 0010154-14
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 17:00
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.011
0.0015
1
8260D
1/16/20 18:34
TBL
POA0231
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.023
0.00039
1
8260D
1/16/20 18:34
TBL
POA0231
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.023
0.0013
1
8260D
1/16/20 18:34
TBL
POA0231
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.023
0.00047
1
8260D
1/16/20 18:34
TBL
POA0231
Methylene Chloride
BRL
mg/kg dry
0.0057
0.00092
1
8260D
1/16/20 18:34
TBL
POA0231
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0057
0.00080
1
8260D
1/16/20 18:34
TBL
POA0231
Naphthalene
BRL
mg/kg dry
0.011
0.00058
1
8260D
1/16/20 18:34
TBL
POA0231
n-Butylbenzene
BRL
mg/kg dry
0.0057
0.00053
1
8260D
1/16/20 18:34
TBL
POA0231
n-Propylbenzene
BRL
mg/kg dry
0.0057
0.00083
1
8260D
1/16/20 18:34
TBL
POA0231
o-Xylene
BRL
mg/kg dry
0.0057
0.00061
1
8260D
1/16/20 18:34
TBL
POA0231
sec-Butylbenzene
BRL
mg/kg dry
0.0057
0.00062
1
8260D
1/16/20 18:34
TBL
POA0231
Styrene
BRL
mg/kg dry
0.0057
0.00055
1
8260D
1/16/20 18:34
TBL
POA0231
tert-Butylbenzene
BRL
mg/kg dry
0.0057
0.00068
1
8260D
1/16/20 18:34
TBL
POA0231
Tetrachloroethylene
BRL
mg/kg dry
0.0057
0.0010
1
8260D
1/16/20 18:34
TBL
POA0231
Toluene
BRL
mg/kg dry
0.0057
0.00091
1
8260D
1/16/20 18:34
TBL
POA0231
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0057
0.0011
1
8260D
1/16/20 18:34
TBL
POA0231
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00049
1
8260D
1/16/20 18:34
TBL
POA0231
Trichloroethylene
BRL
mg/kg dry
0.0057
0.0011
1
8260D
1/16/20 18:34
TBL
POA0231
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
1/16/20 18:34
TBL
POA0231
Vinyl acetate
BRL
mg/kg dry
0.011
0.00062
1
8260D
1/16/20 18:34
TBL
POA0231
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260D
1/16/20 18:34
TBL
POA0231
Xylenes, total
BRL
mg/kg dry
0.017
0.0021
1
8260D
1/16/20 18:34
TBL
POA0231
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
98 %
70-130
Dibromofluoromethane
108 %
84-123
Toluene-d8
84 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-10
Attn: Katie Lippard Sample ID: 0010154-15
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 15:20
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
75.2
% by
0.100
0.100
1
SM2540 G
1/16/20 13:45
EDV
POA0227
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.88
0.16
1
8270E
1/16/20 18:43
JMV
POA0221
1,2-Dichlorobenzene
BRL
mg/kg dry
0.88
0.14
1
8270E
1/16/20 18:43
JMV
POA0221
1,3-Dichlorobenzene
BRL
mg/kg dry
0.88
0.13
1
8270E
1/16/20 18:43
JMV
POA0221
1,4-Dichlorobenzene
BRL
mg/kg dry
0.44
0.14
1
8270E
1/16/20 18:43
JMV
POA0221
1-Methyl naphthalene
BRL
mg/kg dry
0.88
0.013
1
8270E
1/16/20 18:43
JMV
POA0221
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.88
0.19
1
8270E
1/16/20 18:43
JMV
POA0221
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.88
0.21
1
8270E
1/16/20 18:43
JMV
POA0221
2,4-Dichlorophenol
BRL
mg/kg dry
0.88
0.17
1
8270E
1/16/20 18:43
JMV
POA0221
2,4-Dimethylphenol
BRL
mg/kg dry
0.44
0.18
1
8270E
1/16/20 18:43
JMV
POA0221
2,4-Dinitrophenol
BRL
mg/kg dry
2.0
0.51
1
8270E
1/16/20 18:43
JMV
POA0221
2,4-Dinitrotoluene
BRL
mg/kg dry
0.88
0.23
1
8270E
1/16/20 18:43
JMV
POA0221
2,6-Dinitrotoluene
BRL
mg/kg dry
0.88
0.23
1
8270E
1/16/20 18:43
JMV
POA0221
2-Chloronaphthalene
BRL
mg/kg dry
0.88
0.21
1
8270E
1/16/20 18:43
JMV
POA0221
2-Chlorophenol
BRL
mg/kg dry
0.88
0.17
1
8270E
1/16/20 18:43
JMV
POA0221
2-Methyl naphthalene
BRL
mg/kg dry
0.88
0.017
1
8270E
1/16/20 18:43
JMV
POA0221
2-Methylphenol
BRL
mg/kg dry
0.88
0.17
1
8270E
1/16/20 18:43
JMV
POA0221
2-Nitrophenol
BRL
mg/kg dry
0.88
0.15
1
8270E
1/16/20 18:43
JMV
POA0221
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.88
0.17
1
8270E
1/16/20 18:43
JMV
POA0221
3/4-Methyl phenol
BRL
mg/kg dry
0.88
0.19
1
8270E
1/16/20 18:43
JMV
POA0221
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.0
0.48
1
8270E
1/16/20 18:43
JMV
POA0221
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.88
0.21
1
8270E
1/16/20 18:43
JMV
POA0221
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.88
0.17
1
8270E
1/16/20 18:43
JMV
POA0221
4-Chloroaniline
BRL
mg/kg dry
0.44
0.11
1
8270E
1/16/20 18:43
JMV
POA0221
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.27
1
8270E
1/16/20 18:43
JMV
POA0221
4-Nitrophenol
BRL
mg/kg dry
0.88
0.22
1
8270E
1/16/20 18:43
JMV
POA0221
Acenaphthene
BRL
mg/kg dry
0.88
0.020
1
8270E
1/16/20 18:43
JMV
POA0221
Acenaphthylene
BRL
mg/kg dry
0.88
0.017
1
8270E
1/16/20 18:43
JMV
POA0221
Anthracene
BRL
mg/kg dry
0.88
0.0097
1
8270E
1/16/20 18:43
JMV
POA0221
Azobenzene
BRL
mg/kg dry
0.88
0.19
1
8270E
1/16/20 18:43
JMV
POA0221
Benzo(a)anthracene
BRL
mg/kg dry
0.88
0.011
1
8270E
1/16/20 18:43
JMV
POA0221
Benzo(a)pyrene
BRL
mg/kg dry
0.88
0.0078
1
8270E
1/16/20 18:43
JMV
POA0221
Benzo(b)fluoranthene
BRL
mg/kg dry
0.88
0.0081
1
8270E
1/16/20 18:43
JMV
POA0221
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.88
0.0086
1
8270E
1/16/20 18:43
JMV
POA0221
Benzo(k)fluoranthene
BRL
mg/kg dry
0.88
0.0093
1
8270E
1/16/20 18:43
JMV
POA0221
Benzoic Acid
BRL
mg/kg dry
2.7
0.73
1
8270E
1/16/20 18:43
JMV
POA0221
Benzyl alcohol
BRL
mg/kg dry
0.88
0.16
1
8270E
1/16/20 18:43
JMV
POA0221
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.88
0.17
1
8270E
1/16/20 18:43
JMV
POA0221
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.88
0.14
1
8270E
1/16/20 18:43
JMV
POA0221
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.44
0.16
1
8270E
1/16/20 18:43
JMV
POA0221
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-10
Attn: Katie Lippard Sample ID: 0010154-15
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 15:20
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.88
0.20
1
8270E
1/16/20 18:43
JMV
POA0221
Butyl benzyl phthalate
BRL
mg/kg dry
0.44
0.15
1
8270E
1/16/20 18:43
JMV
POA0221
Chrysene
BRL
mg/kg dry
0.88
0.010
1
8270E
1/16/20 18:43
JMV
POA0221
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.88
0.025
1
8270E
1/16/20 18:43
JMV
POA0221
Dibenzofuran
BRL
mg/kg dry
0.88
0.24
1
8270E
1/16/20 18:43
JMV
POA0221
Diethyl phthalate
BRL
mg/kg dry
0.88
0.23
1
8270E
1/16/20 18:43
JMV
POA0221
Dimethyl phthalate
BRL
mg/kg dry
0.88
0.21
1
8270E
1/16/20 18:43
JMV
POA0221
Di-n-butyl phthalate
BRL
mg/kg dry
0.88
0.22
1
8270E
1/16/20 18:43
JMV
POA0221
Di-n-octyl phthalate
BRL
mg/kg dry
0.44
0.23
1
8270E
1/16/20 18:43
JMV
POA0221
Fluoranthene
BRL
mg/kg dry
0.88
0.010
1
8270E
1/16/20 18:43
JMV
POA0221
Fluorene
BRL
mg/kg dry
0.88
0.015
1
8270E
1/16/20 18:43
JMV
POA0221
Hexachlorobenzene
BRL
mg/kg dry
0.88
0.19
1
8270E
1/16/20 18:43
JMV
POA0221
Hexachlorobutadiene
BRL
mg/kg dry
0.88
0.20
1
8270E
1/16/20 18:43
JMV
POA0221
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.88
0.30
1
8270E
1/16/20 18:43
JMV
POA0221
Hexachloroethane
BRL
mg/kg dry
0.88
0.14
1
8270E
1/16/20 18:43
JMV
POA0221
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.88
0.025
1
8270E
1/16/20 18:43
JMV
POA0221
Isophorone
BRL
mg/kg dry
0.88
0.19
1
8270E
1/16/20 18:43
JMV
POA0221
Naphthalene
BRL
mg/kg dry
0.88
0.019
1
8270E
1/16/20 18:43
JMV
POA0221
Nitrobenzene
BRL
mg/kg dry
0.44
0.19
1
8270E
1/16/20 18:43
JMV
POA0221
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.88
0.20
1
8270E
1/16/20 18:43
JMV
POA0221
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.88
0.24
1
8270E
1/16/20 18:43
JMV
POA0221
Pentachlorophenol
BRL
mg/kg dry
1.3
0.56
1
8270E
1/16/20 18:43
JMV
POA0221
Phenanthrene
BRL
mg/kg dry
0.88
0.0096
1
8270E
1/16/20 18:43
JMV
POA0221
Phenol
BRL
mg/kg dry
0.88
0.14
1
8270E
1/16/20 18:43
JMV
POA0221
Pyrene
BRL
mg/kg dry
0.88
0.013
1
8270E
1/16/20 18:43
JMV
POA0221
Pyridine
BRL
mg/kg dry
0.44
0.084
1
8270E
1/16/20 18:43
JMV
POA0221
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
88 %
39-132
2-Fluorobiphenyl
75 %
44-115
2-Fluorophenol
78 %
35-115
Nitrobenzene-d5
71 %
37-122
Phenol-d5
74 %
34-121
Terphenyl-d14
75 %
54-127
Total Metals
Mercury
0.027 J
mg/kg dry
0.067
0.023
1
7471B
1/16/20 10:53
JAB
POA0212
Arsenic
0.57 J
mg/kg dry
1.3
0.18
1
6010D
1/18/20
1:15
JAB
POA0181
Barium
79
mg/kg dry
13
4.0
1
6010D
1/18/20
1:15
JAB
POA0181
Cadmium
0.096 J
mg/kg dry
0.67
0.045
1
6010D
1/18/20
1:15
JAB
POA0181
Chromium
17
mg/kg dry
1.3
0.10
1
6010D
1/18/20
1:15
JAB
POA0181
Lead
32
mg/kg dry
1.3
0.22
1
6010D
1/18/20
1:15
JAB
POA0181
Selenium
BRL
mg/kg dry
1.3
0.37
1
6010D
1/18/20
1:15
JAB
POA0181
Silver
BRL
mg/kg dry
0.67
0.041
1
6010D
1/18/20
1:15
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-10
Attn: Katie Lippard Sample ID: 0010154-15
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 15:20
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0058
0.00071
1
8260D
1/16/20 19:04
TBL
POA0231
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0058
0.00086
1
8260D
1/16/20 19:04
TBL
POA0231
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0058
0.00042
1
8260D
1/16/20 19:04
TBL
POA0231
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0058
0.00063
1
8260D
1/16/20 19:04
TBL
POA0231
1,1-Dichloroethane
BRL
mg/kg dry
0.0058
0.0011
1
8260D
1/16/20 19:04
TBL
POA0231
1,1-Dichloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260D
1/16/20 19:04
TBL
POA0231
1,1-Dichloropropylene
BRL
mg/kg dry
0.0058
0.00090
1
8260D
1/16/20 19:04
TBL
POA0231
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00083
1
8260D
1/16/20 19:04
TBL
POA0231
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0058
0.00066
1
8260D
1/16/20 19:04
TBL
POA0231
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00056
1
8260D
1/16/20 19:04
TBL
POA0231
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0058
0.00062
1
8260D
1/16/20 19:04
TBL
POA0231
1,2-Dibromoethane
BRL
mg/kg dry
0.0058
0.00052
1
8260D
1/16/20 19:04
TBL
POA0231
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0058
0.00065
1
8260D
1/16/20 19:04
TBL
POA0231
1,2-Dichloroethane
BRL
mg/kg dry
0.0058
0.00069
1
8260D
1/16/20 19:04
TBL
POA0231
1,2-Dichloropropane
BRL
mg/kg dry
0.0058
0.00088
1
8260D
1/16/20 19:04
TBL
POA0231
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0058
0.00073
1
8260D
1/16/20 19:04
TBL
POA0231
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0058
0.00072
1
8260D
1/16/20 19:04
TBL
POA0231
1,3-Dichloropropane
BRL
mg/kg dry
0.0058
0.00049
1
8260D
1/16/20 19:04
TBL
POA0231
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0058
0.00074
1
8260D
1/16/20 19:04
TBL
POA0231
2,2-Dichloropropane
BRL
mg/kg dry
0.0058
0.00073
1
8260D
1/16/20 19:04
TBL
POA0231
2-Chlorotoluene
BRL
mg/kg dry
0.0058
0.00078
1
8260D
1/16/20 19:04
TBL
POA0231
4-Chlorotoluene
BRL
mg/kg dry
0.0058
0.00066
1
8260D
1/16/20 19:04
TBL
POA0231
4-Isopropyltoluene
BRL
mg/kg dry
0.0058
0.0015
1
8260D
1/16/20 19:04
TBL
POA0231
Acetone
BRL
mg/kg dry
0.023
0.0015
1
8260D
1/16/20 19:04
TBL
POA0231
Benzene
BRL
mg/kg dry
0.0058
0.00091
1
8260D
1/16/20 19:04
TBL
POA0231
Bromobenzene
BRL
mg/kg dry
0.0058
0.00081
1
8260D
1/16/20 19:04
TBL
POA0231
Bromochloromethane
BRL
mg/kg dry
0.0058
0.00096
1
8260D
1/16/20 19:04
TBL
POA0231
Bromodichloromethane
BRL
mg/kg dry
0.0058
0.00055
1
8260D
1/16/20 19:04
TBL
POA0231
Bromoform
BRL
mg/kg dry
0.0058
0.00045
1
8260D
1/16/20 19:04
TBL
POA0231
Bromomethane
BRL
mg/kg dry
0.012
0.0029
1
8260D
1/16/20 19:04
TBL
POA0231
Carbon Tetrachloride
BRL
mg/kg dry
0.0058
0.0011
1
8260D
1/16/20 19:04
TBL
POA0231
Chlorobenzene
BRL
mg/kg dry
0.0058
0.00091
1
8260D
1/16/20 19:04
TBL
POA0231
Chloroethane
BRL
mg/kg dry
0.012
0.0011
1
8260D
1/16/20 19:04
TBL
POA0231
Chloroform
BRL
mg/kg dry
0.0058
0.00071
1
8260D
1/16/20 19:04
TBL
POA0231
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
8260D
1/16/20 19:04
TBL
POA0231
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0058
0.00092
1
8260D
1/16/20 19:04
TBL
POA0231
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0058
0.00057
1
8260D
1/16/20 19:04
TBL
POA0231
Dibromochloromethane
BRL
mg/kg dry
0.0058
0.00039
1
8260D
1/16/20 19:04
TBL
POA0231
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
1/16/20 19:04
TBL
POA0231
Ethylbenzene
BRL
mg/kg dry
0.0058
0.00088
1
8260D
1/16/20 19:04
TBL
POA0231
Isopropyl Ether
BRL
mg/kg dry
0.0058
0.00086
1
8260D
1/16/20 19:04
TBL
POA0231
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0058
0.00068
1
8260D
1/16/20 19:04
TBL
POA0231
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-10
Attn: Katie Lippard Sample ID: 0010154-15
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/06/20 15:20
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0015
1
8260D
1/16/20 19:04
TBL
POA0231
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.023
0.00040
1
8260D
1/16/20 19:04
TBL
POA0231
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.023
0.0014
1
8260D
1/16/20 19:04
TBL
POA0231
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.023
0.00048
1
8260D
1/16/20 19:04
TBL
POA0231
Methylene Chloride
BRL
mg/kg dry
0.0058
0.00094
1
8260D
1/16/20 19:04
TBL
POA0231
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0058
0.00082
1
8260D
1/16/20 19:04
TBL
POA0231
Naphthalene
BRL
mg/kg dry
0.012
0.00059
1
8260D
1/16/20 19:04
TBL
POA0231
n-Butylbenzene
BRL
mg/kg dry
0.0058
0.00055
1
8260D
1/16/20 19:04
TBL
POA0231
n-Propylbenzene
BRL
mg/kg dry
0.0058
0.00084
1
8260D
1/16/20 19:04
TBL
POA0231
o-Xylene
BRL
mg/kg dry
0.0058
0.00062
1
8260D
1/16/20 19:04
TBL
POA0231
sec-Butylbenzene
BRL
mg/kg dry
0.0058
0.00063
1
8260D
1/16/20 19:04
TBL
POA0231
Styrene
BRL
mg/kg dry
0.0058
0.00057
1
8260D
1/16/20 19:04
TBL
POA0231
tert-Butylbenzene
BRL
mg/kg dry
0.0058
0.00069
1
8260D
1/16/20 19:04
TBL
POA0231
Tetrachloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260D
1/16/20 19:04
TBL
POA0231
Toluene
BRL
mg/kg dry
0.0058
0.00093
1
8260D
1/16/20 19:04
TBL
POA0231
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260D
1/16/20 19:04
TBL
POA0231
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0058
0.00050
1
8260D
1/16/20 19:04
TBL
POA0231
Trichloroethylene
BRL
mg/kg dry
0.0058
0.0011
1
8260D
1/16/20 19:04
TBL
POA0231
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
1/16/20 19:04
TBL
POA0231
Vinyl acetate
BRL
mg/kg dry
0.012
0.00063
1
8260D
1/16/20 19:04
TBL
POA0231
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
1/16/20 19:04
TBL
POA0231
Xylenes, total
BRL
mg/kg dry
0.017
0.0021
1
8260D
1/16/20 19:04
TBL
POA0231
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
95 %
70-130
Dibromofluoromethane
108 %
84-123
Toluene-d8
83 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-11 S
Attn: Katie Lippard Sample ID: 0010154-16
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 10:10
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
84.1
% by
0.100
0.100
1
SM2540 G
1/16/20 14:09
EDV
POA0228
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.78
0.14
1
8270E
1/16/20 19:06
JMV
POA0221
1,2-Dichlorobenzene
BRL
mg/kg dry
0.78
0.13
1
8270E
1/16/20 19:06
JMV
POA0221
1,3-Dichlorobenzene
BRL
mg/kg dry
0.78
0.11
1
8270E
1/16/20 19:06
JMV
POA0221
1,4-Dichlorobenzene
BRL
mg/kg dry
0.39
0.12
1
8270E
1/16/20 19:06
JMV
POA0221
1-Methyl naphthalene
BRL
mg/kg dry
0.78
0.012
1
8270E
1/16/20 19:06
JMV
POA0221
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.78
0.17
1
8270E
1/16/20 19:06
JMV
POA0221
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.78
0.19
1
8270E
1/16/20 19:06
JMV
POA0221
2,4-Dichlorophenol
BRL
mg/kg dry
0.78
0.15
1
8270E
1/16/20 19:06
JMV
POA0221
2,4-Dimethylphenol
BRL
mg/kg dry
0.39
0.16
1
8270E
1/16/20 19:06
JMV
POA0221
2,4-Dinitrophenol
BRL
mg/kg dry
1.8
0.46
1
8270E
1/16/20 19:06
JMV
POA0221
2,4-Dinitrotoluene
BRL
mg/kg dry
0.78
0.21
1
8270E
1/16/20 19:06
JMV
POA0221
2,6-Dinitrotoluene
BRL
mg/kg dry
0.78
0.20
1
8270E
1/16/20 19:06
JMV
POA0221
2-Chloronaphthalene
BRL
mg/kg dry
0.78
0.19
1
8270E
1/16/20 19:06
JMV
POA0221
2-Chlorophenol
BRL
mg/kg dry
0.78
0.15
1
8270E
1/16/20 19:06
JMV
POA0221
2-Methyl naphthalene
BRL
mg/kg dry
0.78
0.015
1
8270E
1/16/20 19:06
JMV
POA0221
2-Methylphenol
BRL
mg/kg dry
0.78
0.15
1
8270E
1/16/20 19:06
JMV
POA0221
2-Nitrophenol
BRL
mg/kg dry
0.78
0.13
1
8270E
1/16/20 19:06
JMV
POA0221
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.78
0.15
1
8270E
1/16/20 19:06
JMV
POA0221
3/4-Methyl phenol
BRL
mg/kg dry
0.78
0.17
1
8270E
1/16/20 19:06
JMV
POA0221
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.8
0.43
1
8270E
1/16/20 19:06
JMV
POA0221
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.78
0.18
1
8270E
1/16/20 19:06
JMV
POA0221
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.78
0.15
1
8270E
1/16/20 19:06
JMV
POA0221
4-Chloroaniline
BRL
mg/kg dry
0.39
0.095
1
8270E
1/16/20 19:06
JMV
POA0221
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.24
1
8270E
1/16/20 19:06
JMV
POA0221
4-Nitrophenol
BRL
mg/kg dry
0.78
0.19
1
8270E
1/16/20 19:06
JMV
POA0221
Acenaphthene
BRL
mg/kg dry
0.78
0.018
1
8270E
1/16/20 19:06
JMV
POA0221
Acenaphthylene
BRL
mg/kg dry
0.78
0.015
1
8270E
1/16/20 19:06
JMV
POA0221
Anthracene
BRL
mg/kg dry
0.78
0.0086
1
8270E
1/16/20 19:06
JMV
POA0221
Azobenzene
BRL
mg/kg dry
0.78
0.17
1
8270E
1/16/20 19:06
JMV
POA0221
Benzo(a)anthracene
BRL
mg/kg dry
0.78
0.0093
1
8270E
1/16/20 19:06
JMV
POA0221
Benzo(a)pyrene
BRL
mg/kg dry
0.78
0.0070
1
8270E
1/16/20 19:06
JMV
POA0221
Benzo(b)fluoranthene
BRL
mg/kg dry
0.78
0.0072
1
8270E
1/16/20 19:06
JMV
POA0221
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.78
0.0077
1
8270E
1/16/20 19:06
JMV
POA0221
Benzo(k)fluoranthene
BRL
mg/kg dry
0.78
0.0083
1
8270E
1/16/20 19:06
JMV
POA0221
Benzoic Acid
BRL
mg/kg dry
2.4
0.65
1
8270E
1/16/20 19:06
JMV
POA0221
Benzyl alcohol
BRL
mg/kg dry
0.78
0.15
1
8270E
1/16/20 19:06
JMV
POA0221
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.78
0.15
1
8270E
1/16/20 19:06
JMV
POA0221
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.78
0.13
1
8270E
1/16/20 19:06
JMV
POA0221
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.39
0.14
1
8270E
1/16/20 19:06
JMV
POA0221
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-11 S
Attn: Katie Lippard Sample ID: 0010154-16
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 10:10
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.78
0.18
1
8270E
1/16/20 19:06
JMV
POA0221
Butyl benzyl phthalate
BRL
mg/kg dry
0.39
0.13
1
8270E
1/16/20 19:06
JMV
POA0221
Chrysene
BRL
mg/kg dry
0.78
0.0092
1
8270E
1/16/20 19:06
JMV
POA0221
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.78
0.022
1
8270E
1/16/20 19:06
JMV
POA0221
Dibenzofuran
BRL
mg/kg dry
0.78
0.21
1
8270E
1/16/20 19:06
JMV
POA0221
Diethyl phthalate
BRL
mg/kg dry
0.78
0.20
1
8270E
1/16/20 19:06
JMV
POA0221
Dimethyl phthalate
BRL
mg/kg dry
0.78
0.19
1
8270E
1/16/20 19:06
JMV
POA0221
Di-n-butyl phthalate
BRL
mg/kg dry
0.78
0.19
1
8270E
1/16/20 19:06
JMV
POA0221
Di-n-octyl phthalate
BRL
mg/kg dry
0.39
0.20
1
8270E
1/16/20 19:06
JMV
POA0221
Fluoranthene
BRL
mg/kg dry
0.78
0.0089
1
8270E
1/16/20 19:06
JMV
POA0221
Fluorene
BRL
mg/kg dry
0.78
0.013
1
8270E
1/16/20 19:06
JMV
POA0221
Hexachlorobenzene
BRL
mg/kg dry
0.78
0.17
1
8270E
1/16/20 19:06
JMV
POA0221
Hexachlorobutadiene
BRL
mg/kg dry
0.78
0.18
1
8270E
1/16/20 19:06
JMV
POA0221
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.78
0.27
1
8270E
1/16/20 19:06
JMV
POA0221
Hexachloroethane
BRL
mg/kg dry
0.78
0.12
1
8270E
1/16/20 19:06
JMV
POA0221
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.78
0.022
1
8270E
1/16/20 19:06
JMV
POA0221
Isophorone
BRL
mg/kg dry
0.78
0.17
1
8270E
1/16/20 19:06
JMV
POA0221
Naphthalene
BRL
mg/kg dry
0.78
0.017
1
8270E
1/16/20 19:06
JMV
POA0221
Nitrobenzene
BRL
mg/kg dry
0.39
0.17
1
8270E
1/16/20 19:06
JMV
POA0221
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.78
0.18
1
8270E
1/16/20 19:06
JMV
POA0221
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.78
0.21
1
8270E
1/16/20 19:06
JMV
POA0221
Pentachlorophenol
BRL
mg/kg dry
1.2
0.50
1
8270E
1/16/20 19:06
JMV
POA0221
Phenanthrene
BRL
mg/kg dry
0.78
0.0085
1
8270E
1/16/20 19:06
JMV
POA0221
Phenol
BRL
mg/kg dry
0.78
0.13
1
8270E
1/16/20 19:06
JMV
POA0221
Pyrene
BRL
mg/kg dry
0.78
0.011
1
8270E
1/16/20 19:06
JMV
POA0221
Pyridine
BRL
mg/kg dry
0.39
0.074
1
8270E
1/16/20 19:06
JMV
POA0221
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
90 %
39-132
2-Fluorobiphenyl
80 %
44-115
2-Fluorophenol
82 %
35-115
Nitrobenzene-d5
75 %
37-122
Phenol-d5
78 %
34-121
Terphenyl-d14
80 %
54-127
Total Metals
Mercury
0.045 J
mg/kg dry
0.059
0.021
1
7471B
1/16/20 10:57
JAB
POA0212
Arsenic
2.3
mg/kg dry
1.2
0.16
1
6010D
1/18/20
1:24
JAB
POA0181
Barium
55
mg/kg dry
12
3.6
1
6010D
1118/20
1:24
JAB
POA0181
Cadmium
BRL
mg/kg dry
0.59
0.040
1
6010D
1/18/20
1:24
JAB
POA0181
Chromium
24
mg/kg dry
1.2
0.090
1
6010D
1/18/20
1:24
JAB
POA0181
Lead
21
mg/kg dry
1.2
0.20
1
6010D
1/18/20
1:24
JAB
POA0181
Selenium
BRL
mg/kg dry
1.2
0.33
1
6010D
1/18/20
1:24
JAB
POA0181
Silver
BRL
mg/kg dry
0.59
0.037
1
6010D
1/18/20
1:24
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-11 S
Attn: Katie Lippard Sample ID: 0010154-16
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 10:10
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0051
0.00062
1
8260D
1/16/20 19:34
TBL
POA0231
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0051
0.00075
1
8260D
1/16/20 19:34
TBL
POA0231
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0051
0.00037
1
8260D
1/16/20 19:34
TBL
POA0231
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0051
0.00055
1
8260D
1/16/20 19:34
TBL
POA0231
1,1-Dichloroethane
BRL
mg/kg dry
0.0051
0.00092
1
8260D
1/16/20 19:34
TBL
POA0231
1,1-Dichloroethylene
BRL
mg/kg dry
0.0051
0.00093
1
8260D
1/16/20 19:34
TBL
POA0231
1,1-Dichloropropylene
BRL
mg/kg dry
0.0051
0.00078
1
8260D
1/16/20 19:34
TBL
POA0231
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.010
0.00073
1
8260D
1/16/20 19:34
TBL
POA0231
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0051
0.00058
1
8260D
1/16/20 19:34
TBL
POA0231
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.010
0.00048
1
8260D
1/16/20 19:34
TBL
POA0231
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0051
0.00054
1
8260D
1/16/20 19:34
TBL
POA0231
1,2-Dibromoethane
BRL
mg/kg dry
0.0051
0.00046
1
8260D
1/16/20 19:34
TBL
POA0231
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0051
0.00057
1
8260D
1/16/20 19:34
TBL
POA0231
1,2-Dichloroethane
BRL
mg/kg dry
0.0051
0.00060
1
8260D
1/16/20 19:34
TBL
POA0231
1,2-Dichloropropane
BRL
mg/kg dry
0.0051
0.00076
1
8260D
1/16/20 19:34
TBL
POA0231
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0051
0.00064
1
8260D
1/16/20 19:34
TBL
POA0231
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0051
0.00063
1
8260D
1/16/20 19:34
TBL
POA0231
1,3-Dichloropropane
BRL
mg/kg dry
0.0051
0.00042
1
8260D
1/16/20 19:34
TBL
POA0231
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0051
0.00064
1
8260D
1/16/20 19:34
TBL
POA0231
2,2-Dichloropropane
BRL
mg/kg dry
0.0051
0.00063
1
8260D
1/16/20 19:34
TBL
POA0231
2-Chlorotoluene
BRL
mg/kg dry
0.0051
0.00068
1
8260D
1/16/20 19:34
TBL
POA0231
4-Chlorotoluene
BRL
mg/kg dry
0.0051
0.00058
1
8260D
1/16/20 19:34
TBL
POA0231
4-Isopropyltoluene
BRL
mg/kg dry
0.0051
0.0013
1
8260D
1/16/20 19:34
TBL
POA0231
Acetone
BRL
mg/kg dry
0.020
0.0013
1
8260D
1/16/20 19:34
TBL
POA0231
Benzene
BRL
mg/kg dry
0.0051
0.00079
1
8260D
1/16/20 19:34
TBL
POA0231
Bromobenzene
BRL
mg/kg dry
0.0051
0.00071
1
8260D
1/16/20 19:34
TBL
POA0231
Bromochloromethane
BRL
mg/kg dry
0.0051
0.00084
1
8260D
1/16/20 19:34
TBL
POA0231
Bromodichloromethane
BRL
mg/kg dry
0.0051
0.00048
1
8260D
1/16/20 19:34
TBL
POA0231
Bromoform
BRL
mg/kg dry
0.0051
0.00039
1
8260D
1/16/20 19:34
TBL
POA0231
Bromomethane
BRL
mg/kg dry
0.010
0.0025
1
8260D
1/16/20 19:34
TBL
POA0231
Carbon Tetrachloride
BRL
mg/kg dry
0.0051
0.0010
1
8260D
1/16/20 19:34
TBL
POA0231
Chlorobenzene
BRL
mg/kg dry
0.0051
0.00079
1
8260D
1/16/20 19:34
TBL
POA0231
Chloroethane
BRL
mg/kg dry
0.010
0.00097
1
8260D
1/16/20 19:34
TBL
POA0231
Chloroform
BRL
mg/kg dry
0.0051
0.00062
1
8260D
1/16/20 19:34
TBL
POA0231
Chloromethane
BRL
mg/kg dry
0.010
0.0015
1
8260D
1/16/20 19:34
TBL
POA0231
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0051
0.00080
1
8260D
1/16/20 19:34
TBL
POA0231
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0051
0.00050
1
8260D
1/16/20 19:34
TBL
POA0231
Dibromochloromethane
BRL
mg/kg dry
0.0051
0.00034
1
8260D
1/16/20 19:34
TBL
POA0231
Dichlorodifluoromethane
BRL
mg/kg dry
0.010
0.0014
1
8260D
1/16/20 19:34
TBL
POA0231
Ethylbenzene
BRL
mg/kg dry
0.0051
0.00076
1
8260D
1/16/20 19:34
TBL
POA0231
Isopropyl Ether
BRL
mg/kg dry
0.0051
0.00075
1
8260D
1/16/20 19:34
TBL
POA0231
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0051
0.00059
1
8260D
1/16/20 19:34
TBL
POA0231
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-11 S
Attn: Katie Lippard Sample ID: 0010154-16
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 10:10
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.010
0.0013
1
8260D
1/16/20 19:34
TBL
POA0231
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.020
0.00035
1
8260D
1/16/20 19:34
TBL
POA0231
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.020
0.0012
1
8260D
1/16/20 19:34
TBL
POA0231
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.020
0.00041
1
8260D
1/16/20 19:34
TBL
POA0231
Methylene Chloride
BRL
mg/kg dry
0.0051
0.00082
1
8260D
1/16/20 19:34
TBL
POA0231
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0051
0.00071
1
8260D
1/16/20 19:34
TBL
POA0231
Naphthalene
BRL
mg/kg dry
0.010
0.00051
1
8260D
1/16/20 19:34
TBL
POA0231
n-Butylbenzene
BRL
mg/kg dry
0.0051
0.00048
1
8260D
1/16/20 19:34
TBL
POA0231
n-Propylbenzene
BRL
mg/kg dry
0.0051
0.00074
1
8260D
1/16/20 19:34
TBL
POA0231
o-Xylene
BRL
mg/kg dry
0.0051
0.00054
1
8260D
1/16/20 19:34
TBL
POA0231
sec-Butylbenzene
BRL
mg/kg dry
0.0051
0.00055
1
8260D
1/16/20 19:34
TBL
POA0231
Styrene
BRL
mg/kg dry
0.0051
0.00049
1
8260D
1/16/20 19:34
TBL
POA0231
tert-Butylbenzene
BRL
mg/kg dry
0.0051
0.00060
1
8260D
1/16/20 19:34
TBL
POA0231
Tetrachloroethylene
BRL
mg/kg dry
0.0051
0.00092
1
8260D
1/16/20 19:34
TBL
POA0231
Toluene
BRL
mg/kg dry
0.0051
0.00081
1
8260D
1/16/20 19:34
TBL
POA0231
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0051
0.00097
1
8260D
1/16/20 19:34
TBL
POA0231
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0051
0.00043
1
8260D
1/16/20 19:34
TBL
POA0231
Trichloroethylene
BRL
mg/kg dry
0.0051
0.00099
1
8260D
1/16/20 19:34
TBL
POA0231
Trichlorofluoromethane
BRL
mg/kg dry
0.010
0.0014
1
8260D
1/16/20 19:34
TBL
POA0231
Vinyl acetate
BRL
mg/kg dry
0.010
0.00055
1
8260D
1/16/20 19:34
TBL
POA0231
Vinyl chloride
BRL
mg/kg dry
0.010
0.0010
1
8260D
1/16/20 19:34
TBL
POA0231
Xylenes, total
BRL
mg/kg dry
0.015
0.0018
1
8260D
1/16/20 19:34
TBL
POA0231
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
98 %
70-130
Dibromofluoromethane
107 %
84-123
Toluene-d8
81 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-11 D
Attn: Katie Lippard Sample ID: 0010154-17
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 10:15
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
79.5
% by
0.100
0.100
1
SM2540 G
1/16/20 14:09
EDV
POA0228
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.83
0.15
1
8270E
1/16/20 19:28
JMV
POA0221
1,2-Dichlorobenzene
BRL
mg/kg dry
0.83
0.13
1
8270E
1/16/20 19:28
JMV
POA0221
1,3-Dichlorobenzene
BRL
mg/kg dry
0.83
0.12
1
8270E
1/16/20 19:28
JMV
POA0221
1,4-Dichlorobenzene
BRL
mg/kg dry
0.41
0.13
1
8270E
1/16/20 19:28
JMV
POA0221
1-Methyl naphthalene
BRL
mg/kg dry
0.83
0.013
1
8270E
1/16/20 19:28
JMV
POA0221
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.83
0.18
1
8270E
1/16/20 19:28
JMV
POA0221
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.83
0.20
1
8270E
1/16/20 19:28
JMV
POA0221
2,4-Dichlorophenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/16/20 19:28
JMV
POA0221
2,4-Dimethylphenol
BRL
mg/kg dry
0.41
0.17
1
8270E
1/16/20 19:28
JMV
POA0221
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.49
1
8270E
1/16/20 19:28
JMV
POA0221
2,4-Dinitrotoluene
BRL
mg/kg dry
0.83
0.22
1
8270E
1/16/20 19:28
JMV
POA0221
2,6-Dinitrotoluene
BRL
mg/kg dry
0.83
0.21
1
8270E
1/16/20 19:28
JMV
POA0221
2-Chloronaphthalene
BRL
mg/kg dry
0.83
0.20
1
8270E
1/16/20 19:28
JMV
POA0221
2-Chlorophenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/16/20 19:28
JMV
POA0221
2-Methyl naphthalene
BRL
mg/kg dry
0.83
0.016
1
8270E
1/16/20 19:28
JMV
POA0221
2-Methylphenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/16/20 19:28
JMV
POA0221
2-Nitrophenol
BRL
mg/kg dry
0.83
0.14
1
8270E
1/16/20 19:28
JMV
POA0221
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.83
0.16
1
8270E
1/16/20 19:28
JMV
POA0221
3/4-Methyl phenol
BRL
mg/kg dry
0.83
0.18
1
8270E
1/16/20 19:28
JMV
POA0221
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.46
1
8270E
1/16/20 19:28
JMV
POA0221
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.83
0.19
1
8270E
1/16/20 19:28
JMV
POA0221
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/16/20 19:28
JMV
POA0221
4-Chloroaniline
BRL
mg/kg dry
0.41
0.10
1
8270E
1/16/20 19:28
JMV
POA0221
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.25
1
8270E
1/16/20 19:28
JMV
POA0221
4-Nitrophenol
BRL
mg/kg dry
0.83
0.20
1
8270E
1/16/20 19:28
JMV
POA0221
Acenaphthene
BRL
mg/kg dry
0.83
0.019
1
8270E
1/16/20 19:28
JMV
POA0221
Acenaphthylene
BRL
mg/kg dry
0.83
0.016
1
8270E
1/16/20 19:28
JMV
POA0221
Anthracene
BRL
mg/kg dry
0.83
0.0092
1
8270E
1/16/20 19:28
JMV
POA0221
Azobenzene
BRL
mg/kg dry
0.83
0.18
1
8270E
1/16/20 19:28
JMV
POA0221
Benzo(a)anthracene
BRL
mg/kg dry
0.83
0.0099
1
8270E
1/16/20 19:28
JMV
POA0221
Benzo(a)pyrene
BRL
mg/kg dry
0.83
0.0074
1
8270E
1/16/20 19:28
JMV
POA0221
Benzo(b)fluoranthene
BRL
mg/kg dry
0.83
0.0077
1
8270E
1/16/20 19:28
JMV
POA0221
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.83
0.0082
1
8270E
1/16/20 19:28
JMV
POA0221
Benzo(k)fluoranthene
BRL
mg/kg dry
0.83
0.0088
1
8270E
1/16/20 19:28
JMV
POA0221
Benzoic Acid
BRL
mg/kg dry
2.5
0.69
1
8270E
1/16/20 19:28
JMV
POA0221
Benzyl alcohol
BRL
mg/kg dry
0.83
0.16
1
8270E
1/16/20 19:28
JMV
POA0221
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.83
0.16
1
8270E
1/16/20 19:28
JMV
POA0221
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.83
0.13
1
8270E
1/16/20 19:28
JMV
POA0221
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.41
0.15
1
8270E
1/16/20 19:28
JMV
POA0221
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-11 D
Attn: Katie Lippard Sample ID: 0010154-17
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 10:15
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.83
0.19
1
8270E
1/16/20 19:28
JMV
POA0221
Butyl benzyl phthalate
BRL
mg/kg dry
0.41
0.14
1
8270E
1/16/20 19:28
JMV
POA0221
Chrysene
BRL
mg/kg dry
0.83
0.0098
1
8270E
1/16/20 19:28
JMV
POA0221
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.83
0.024
1
8270E
1/16/20 19:28
JMV
POA0221
Dibenzofuran
BRL
mg/kg dry
0.83
0.22
1
8270E
1/16/20 19:28
JMV
POA0221
Diethyl phthalate
BRL
mg/kg dry
0.83
0.21
1
8270E
1/16/20 19:28
JMV
POA0221
Dimethyl phthalate
BRL
mg/kg dry
0.83
0.20
1
8270E
1/16/20 19:28
JMV
POA0221
Di-n-butyl phthalate
BRL
mg/kg dry
0.83
0.21
1
8270E
1/16/20 19:28
JMV
POA0221
Di-n-octyl phthalate
BRL
mg/kg dry
0.41
0.21
1
8270E
1/16/20 19:28
JMV
POA0221
Fluoranthene
BRL
mg/kg dry
0.83
0.0094
1
8270E
1/16/20 19:28
JMV
POA0221
Fluorene
BRL
mg/kg dry
0.83
0.014
1
8270E
1/16/20 19:28
JMV
POA0221
Hexachlorobenzene
BRL
mg/kg dry
0.83
0.18
1
8270E
1/16/20 19:28
JMV
POA0221
Hexachlorobutadiene
BRL
mg/kg dry
0.83
0.19
1
8270E
1/16/20 19:28
JMV
POA0221
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.83
0.29
1
8270E
1/16/20 19:28
JMV
POA0221
Hexachloroethane
BRL
mg/kg dry
0.83
0.13
1
8270E
1/16/20 19:28
JMV
POA0221
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.83
0.023
1
8270E
1/16/20 19:28
JMV
POA0221
Isophorone
BRL
mg/kg dry
0.83
0.18
1
8270E
1/16/20 19:28
JMV
POA0221
Naphthalene
BRL
mg/kg dry
0.83
0.018
1
8270E
1/16/20 19:28
JMV
POA0221
Nitrobenzene
BRL
mg/kg dry
0.41
0.18
1
8270E
1/16/20 19:28
JMV
POA0221
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.83
0.19
1
8270E
1/16/20 19:28
JMV
POA0221
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.83
0.23
1
8270E
1/16/20 19:28
JMV
POA0221
Pentachlorophenol
BRL
mg/kg dry
1.3
0.53
1
8270E
1/16/20 19:28
JMV
POA0221
Phenanthrene
BRL
mg/kg dry
0.83
0.0091
1
8270E
1/16/20 19:28
JMV
POA0221
Phenol
BRL
mg/kg dry
0.83
0.14
1
8270E
1/16/20 19:28
JMV
POA0221
Pyrene
BRL
mg/kg dry
0.83
0.012
1
8270E
1/16/20 19:28
JMV
POA0221
Pyridine
BRL
mg/kg dry
0.41
0.079
1
8270E
1/16/20 19:28
JMV
POA0221
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
96 %
39-132
2-Fluorobiphenyl
82 %
44-115
2-Fluorophenol
84 %
35-115
Nitrobenzene-d5
76 %
37-122
Phenol-d5
80 %
34-121
Terphenyl-d14
83 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.063
0.022
1
7471B
1/16/20 11:02
JAB
POA0212
Arsenic
0.76 J
mg/kg dry
1.3
0.17
1
6010D
1/18/20
1:31
JAB
POA0181
Barium
140
mg/kg dry
13
3.8
1
6010D
1/18/20
1:31
JAB
POA0181
Cadmium
BRL
mg/kg dry
0.63
0.043
1
6010D
1/18/20
1:31
JAB
POA0181
Chromium
13
mg/kg dry
1.3
0.095
1
6010D
1/18/20
1:31
JAB
POA0181
Lead
12
mg/kg dry
1.3
0.21
1
6010D
1/18/20
1:31
JAB
POA0181
Selenium
BRL
mg/kg dry
1.3
0.35
1
6010D
1/18/20
1:31
JAB
POA0181
Silver
BRL
mg/kg dry
0.63
0.039
1
6010D
1/18/20
1:31
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-11 D
Attn: Katie Lippard Sample ID: 0010154-17
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 10:15
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0060
0.00073
1
8260D
1/16/20 20:04
TBL
POA0231
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0060
0.00088
1
8260D
1/16/20 20:04
TBL
POA0231
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0060
0.00043
1
8260D
1/16/20 20:04
TBL
POA0231
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0060
0.00064
1
8260D
1/16/20 20:04
TBL
POA0231
1,1-Dichloroethane
BRL
mg/kg dry
0.0060
0.0011
1
8260D
1/16/20 20:04
TBL
POA0231
1,1-Dichloroethylene
BRL
mg/kg dry
0.0060
0.0011
1
8260D
1/16/20 20:04
TBL
POA0231
1,1-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00092
1
8260D
1/16/20 20:04
TBL
POA0231
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00085
1
8260D
1/16/20 20:04
TBL
POA0231
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0060
0.00068
1
8260D
1/16/20 20:04
TBL
POA0231
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00057
1
8260D
1/16/20 20:04
TBL
POA0231
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0060
0.00063
1
8260D
1/16/20 20:04
TBL
POA0231
1,2-Dibromoethane
BRL
mg/kg dry
0.0060
0.00053
1
8260D
1/16/20 20:04
TBL
POA0231
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00067
1
8260D
1/16/20 20:04
TBL
POA0231
1,2-Dichloroethane
BRL
mg/kg dry
0.0060
0.00071
1
8260D
1/16/20 20:04
TBL
POA0231
1,2-Dichloropropane
BRL
mg/kg dry
0.0060
0.00090
1
8260D
1/16/20 20:04
TBL
POA0231
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0060
0.00075
1
8260D
1/16/20 20:04
TBL
POA0231
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00074
1
8260D
1/16/20 20:04
TBL
POA0231
1,3-Dichloropropane
BRL
mg/kg dry
0.0060
0.00050
1
8260D
1/16/20 20:04
TBL
POA0231
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00076
1
8260D
1/16/20 20:04
TBL
POA0231
2,2-Dichloropropane
BRL
mg/kg dry
0.0060
0.00074
1
8260D
1/16/20 20:04
TBL
POA0231
2-Chlorotoluene
BRL
mg/kg dry
0.0060
0.00080
1
8260D
1/16/20 20:04
TBL
POA0231
4-Chlorotoluene
BRL
mg/kg dry
0.0060
0.00068
1
8260D
1/16/20 20:04
TBL
POA0231
4-Isopropyltoluene
BRL
mg/kg dry
0.0060
0.0015
1
8260D
1/16/20 20:04
TBL
POA0231
Acetone
BRL
mg/kg dry
0.024
0.0015
1
8260D
1/16/20 20:04
TBL
POA0231
Benzene
BRL
mg/kg dry
0.0060
0.00093
1
8260D
1/16/20 20:04
TBL
POA0231
Bromobenzene
BRL
mg/kg dry
0.0060
0.00083
1
8260D
1/16/20 20:04
TBL
POA0231
Bromochloromethane
BRL
mg/kg dry
0.0060
0.00098
1
8260D
1/16/20 20:04
TBL
POA0231
Bromodichloromethane
BRL
mg/kg dry
0.0060
0.00057
1
8260D
1/16/20 20:04
TBL
POA0231
Bromoform
BRL
mg/kg dry
0.0060
0.00046
1
8260D
1/16/20 20:04
TBL
POA0231
Bromomethane
BRL
mg/kg dry
0.012
0.0029
1
8260D
1/16/20 20:04
TBL
POA0231
Carbon Tetrachloride
BRL
mg/kg dry
0.0060
0.0012
1
8260D
1/16/20 20:04
TBL
POA0231
Chlorobenzene
BRL
mg/kg dry
0.0060
0.00093
1
8260D
1/16/20 20:04
TBL
POA0231
Chloroethane
BRL
mg/kg dry
0.012
0.0011
1
8260D
1/16/20 20:04
TBL
POA0231
Chloroform
BRL
mg/kg dry
0.0060
0.00073
1
8260D
1/16/20 20:04
TBL
POA0231
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
8260D
1/16/20 20:04
TBL
POA0231
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0060
0.00094
1
8260D
1/16/20 20:04
TBL
POA0231
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00059
1
8260D
1/16/20 20:04
TBL
POA0231
Dibromochloromethane
BRL
mg/kg dry
0.0060
0.00040
1
8260D
1/16/20 20:04
TBL
POA0231
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0017
1
8260D
1/16/20 20:04
TBL
POA0231
Ethylbenzene
BRL
mg/kg dry
0.0060
0.00090
1
8260D
1/16/20 20:04
TBL
POA0231
Isopropyl Ether
BRL
mg/kg dry
0.0060
0.00088
1
8260D
1/16/20 20:04
TBL
POA0231
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0060
0.00069
1
8260D
1/16/20 20:04
TBL
POA0231
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-11 D
Attn: Katie Lippard Sample ID: 0010154-17
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 10:15
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0015
1
8260D
1/16/20 20:04
TBL
POA0231
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.024
0.00041
1
8260D
1/16/20 20:04
TBL
POA0231
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.024
0.0014
1
8260D
1/16/20 20:04
TBL
POA0231
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.024
0.00049
1
8260D
1/16/20 20:04
TBL
POA0231
Methylene Chloride
BRL
mg/kg dry
0.0060
0.00097
1
8260D
1/16/20 20:04
TBL
POA0231
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0060
0.00084
1
8260D
1/16/20 20:04
TBL
POA0231
Naphthalene
BRL
mg/kg dry
0.012
0.00060
1
8260D
1/16/20 20:04
TBL
POA0231
n-Butylbenzene
BRL
mg/kg dry
0.0060
0.00056
1
8260D
1/16/20 20:04
TBL
POA0231
n-Propylbenzene
BRL
mg/kg dry
0.0060
0.00087
1
8260D
1/16/20 20:04
TBL
POA0231
o-Xylene
BRL
mg/kg dry
0.0060
0.00063
1
8260D
1/16/20 20:04
TBL
POA0231
sec-Butylbenzene
BRL
mg/kg dry
0.0060
0.00064
1
8260D
1/16/20 20:04
TBL
POA0231
Styrene
BRL
mg/kg dry
0.0060
0.00058
1
8260D
1/16/20 20:04
TBL
POA0231
tert-Butylbenzene
BRL
mg/kg dry
0.0060
0.00071
1
8260D
1/16/20 20:04
TBL
POA0231
Tetrachloroethylene
BRL
mg/kg dry
0.0060
0.0011
1
8260D
1/16/20 20:04
TBL
POA0231
Toluene
BRL
mg/kg dry
0.0060
0.00095
1
8260D
1/16/20 20:04
TBL
POA0231
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0060
0.0011
1
8260D
1/16/20 20:04
TBL
POA0231
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00051
1
8260D
1/16/20 20:04
TBL
POA0231
Trichloroethylene
BRL
mg/kg dry
0.0060
0.0012
1
8260D
1/16/20 20:04
TBL
POA0231
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
8260D
1/16/20 20:04
TBL
POA0231
Vinyl acetate
BRL
mg/kg dry
0.012
0.00065
1
8260D
1/16/20 20:04
TBL
POA0231
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
8260D
1/16/20 20:04
TBL
POA0231
Xylenes, total
BRL
mg/kg dry
0.018
0.0021
1
8260D
1/16/20 20:04
TBL
POA0231
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
96 %
70-130
Dibromofluoromethane
107 %
84-123
Toluene-d8
83 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-12S
Attn: Katie Lippard Sample ID: 0010154-18
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:20
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
83.8
% by
0.100
0.100
1
SM2540 G
1/16/20 14:09
EDV
POA0228
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.79
0.14
1
8270E
1/16/20 19:51
JMV
POA0221
1,2-Dichlorobenzene
BRL
mg/kg dry
0.79
0.13
1
8270E
1/16/20 19:51
JMV
POA0221
1,3-Dichlorobenzene
BRL
mg/kg dry
0.79
0.12
1
8270E
1/16/20 19:51
JMV
POA0221
1,4-Dichlorobenzene
BRL
mg/kg dry
0.39
0.12
1
8270E
1/16/20 19:51
JMV
POA0221
1-Methyl naphthalene
BRL
mg/kg dry
0.79
0.012
1
8270E
1/16/20 19:51
JMV
POA0221
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.79
0.17
1
8270E
1/16/20 19:51
JMV
POA0221
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.79
0.19
1
8270E
1/16/20 19:51
JMV
POA0221
2,4-Dichlorophenol
BRL
mg/kg dry
0.79
0.15
1
8270E
1/16/20 19:51
JMV
POA0221
2,4-Dimethylphenol
BRL
mg/kg dry
0.39
0.16
1
8270E
1/16/20 19:51
JMV
POA0221
2,4-Dinitrophenol
BRL
mg/kg dry
1.8
0.46
1
8270E
1/16/20 19:51
JMV
POA0221
2,4-Dinitrotoluene
BRL
mg/kg dry
0.79
0.21
1
8270E
1/16/20 19:51
JMV
POA0221
2,6-Dinitrotoluene
BRL
mg/kg dry
0.79
0.20
1
8270E
1/16/20 19:51
JMV
POA0221
2-Chloronaphthalene
BRL
mg/kg dry
0.79
0.19
1
8270E
1/16/20 19:51
JMV
POA0221
2-Chlorophenol
BRL
mg/kg dry
0.79
0.15
1
8270E
1/16/20 19:51
JMV
POA0221
2-Methyl naphthalene
BRL
mg/kg dry
0.79
0.015
1
8270E
1/16/20 19:51
JMV
POA0221
2-Methylphenol
BRL
mg/kg dry
0.79
0.15
1
8270E
1/16/20 19:51
JMV
POA0221
2-Nitrophenol
BRL
mg/kg dry
0.79
0.13
1
8270E
1/16/20 19:51
JMV
POA0221
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.79
0.16
1
8270E
1/16/20 19:51
JMV
POA0221
3/4-Methyl phenol
BRL
mg/kg dry
0.79
0.17
1
8270E
1/16/20 19:51
JMV
POA0221
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.8
0.43
1
8270E
1/16/20 19:51
JMV
POA0221
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.79
0.18
1
8270E
1/16/20 19:51
JMV
POA0221
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.79
0.15
1
8270E
1/16/20 19:51
JMV
POA0221
4-Chloroaniline
BRL
mg/kg dry
0.39
0.095
1
8270E
1/16/20 19:51
JMV
POA0221
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.24
1
8270E
1/16/20 19:51
JMV
POA0221
4-Nitrophenol
BRL
mg/kg dry
0.79
0.19
1
8270E
1/16/20 19:51
JMV
POA0221
Acenaphthene
BRL
mg/kg dry
0.79
0.018
1
8270E
1/16/20 19:51
JMV
POA0221
Acenaphthylene
BRL
mg/kg dry
0.79
0.015
1
8270E
1/16/20 19:51
JMV
POA0221
Anthracene
BRL
mg/kg dry
0.79
0.0087
1
8270E
1/16/20 19:51
JMV
POA0221
Azobenzene
BRL
mg/kg dry
0.79
0.17
1
8270E
1/16/20 19:51
JMV
POA0221
Benzo(a)anthracene
BRL
mg/kg dry
0.79
0.0094
1
8270E
1/16/20 19:51
JMV
POA0221
Benzo(a)pyrene
BRL
mg/kg dry
0.79
0.0070
1
8270E
1/16/20 19:51
JMV
POA0221
Benzo(b)fluoranthene
BRL
mg/kg dry
0.79
0.0073
1
8270E
1/16/20 19:51
JMV
POA0221
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.79
0.0077
1
8270E
1/16/20 19:51
JMV
POA0221
Benzo(k)fluoranthene
BRL
mg/kg dry
0.79
0.0083
1
8270E
1/16/20 19:51
JMV
POA0221
Benzoic Acid
BRL
mg/kg dry
2.4
0.65
1
8270E
1/16/20 19:51
JMV
POA0221
Benzyl alcohol
BRL
mg/kg dry
0.79
0.15
1
8270E
1/16/20 19:51
JMV
POA0221
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.79
0.15
1
8270E
1/16/20 19:51
JMV
POA0221
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.79
0.13
1
8270E
1/16/20 19:51
JMV
POA0221
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.39
0.14
1
8270E
1/16/20 19:51
JMV
POA0221
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-12S
Attn: Katie Lippard Sample ID: 0010154-18
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:20
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.79
0.18
1
8270E
1/16/20 19:51
JMV
POA0221
Butyl benzyl phthalate
BRL
mg/kg dry
0.39
0.14
1
8270E
1/16/20 19:51
JMV
POA0221
Chrysene
BRL
mg/kg dry
0.79
0.0093
1
8270E
1/16/20 19:51
JMV
POA0221
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.79
0.023
1
8270E
1/16/20 19:51
JMV
POA0221
Dibenzofuran
BRL
mg/kg dry
0.79
0.21
1
8270E
1/16/20 19:51
JMV
POA0221
Diethyl phthalate
BRL
mg/kg dry
0.79
0.20
1
8270E
1/16/20 19:51
JMV
POA0221
Dimethyl phthalate
BRL
mg/kg dry
0.79
0.19
1
8270E
1/16/20 19:51
JMV
POA0221
Di-n-butyl phthalate
BRL
mg/kg dry
0.79
0.20
1
8270E
1/16/20 19:51
JMV
POA0221
Di-n-octyl phthalate
BRL
mg/kg dry
0.39
0.20
1
8270E
1/16/20 19:51
JMV
POA0221
Fluoranthene
BRL
mg/kg dry
0.79
0.0089
1
8270E
1/16/20 19:51
JMV
POA0221
Fluorene
BRL
mg/kg dry
0.79
0.014
1
8270E
1/16/20 19:51
JMV
POA0221
Hexachlorobenzene
BRL
mg/kg dry
0.79
0.17
1
8270E
1/16/20 19:51
JMV
POA0221
Hexachlorobutadiene
BRL
mg/kg dry
0.79
0.18
1
8270E
1/16/20 19:51
JMV
POA0221
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.79
0.27
1
8270E
1/16/20 19:51
JMV
POA0221
Hexachloroethane
BRL
mg/kg dry
0.79
0.12
1
8270E
1/16/20 19:51
JMV
POA0221
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.79
0.022
1
8270E
1/16/20 19:51
JMV
POA0221
Isophorone
BRL
mg/kg dry
0.79
0.17
1
8270E
1/16/20 19:51
JMV
POA0221
Naphthalene
BRL
mg/kg dry
0.79
0.017
1
8270E
1/16/20 19:51
JMV
POA0221
Nitrobenzene
BRL
mg/kg dry
0.39
0.17
1
8270E
1/16/20 19:51
JMV
POA0221
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.79
0.18
1
8270E
1/16/20 19:51
JMV
POA0221
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.79
0.22
1
8270E
1/16/20 19:51
JMV
POA0221
Pentachlorophenol
BRL
mg/kg dry
1.2
0.50
1
8270E
1/16/20 19:51
JMV
POA0221
Phenanthrene
BRL
mg/kg dry
0.79
0.0086
1
8270E
1/16/20 19:51
JMV
POA0221
Phenol
BRL
mg/kg dry
0.79
0.13
1
8270E
1/16/20 19:51
JMV
POA0221
Pyrene
BRL
mg/kg dry
0.79
0.011
1
8270E
1/16/20 19:51
JMV
POA0221
Pyridine
BRL
mg/kg dry
0.39
0.075
1
8270E
1/16/20 19:51
JMV
POA0221
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
92 %
39-132
2-Fluorobiphenyl
79 %
44-115
2-Fluorophenol
78 %
35-115
Nitrobenzene-d5
73 %
37-122
Phenol-d5
75 %
34-121
Terphenyl-d14
79 %
54-127
Total Metals
Mercury
0.029 J
mg/kg dry
0.060
0.021
1
7471B
1/16/20 11:48
JAB
POA0214
Arsenic
0.65 J
mg/kg dry
1.2
0.16
1
6010D
1/18/20
1:39
JAB
POA0181
Barium
86
mg/kg dry
12
3.6
1
6010D
1/18/20
1:39
JAB
POA0181
Cadmium
BRL
mg/kg dry
0.60
0.040
1
6010D
1/18/20
1:39
JAB
POA0181
Chromium
14
mg/kg dry
1.2
0.090
1
6010D
1/18/20
1:39
JAB
POA0181
Lead
13
mg/kg dry
1.2
0.20
1
6010D
1/18/20
1:39
JAB
POA0181
Selenium
BRL
mg/kg dry
1.2
0.33
1
6010D
1/18/20
1:39
JAB
POA0181
Silver
BRL
mg/kg dry
0.60
0.037
1
6010D
1/18/20
1:39
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-12S
Attn: Katie Lippard Sample ID: 0010154-18
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:20
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0052
0.00063
1
8260D
1/16/20 20:34
TBL
POA0231
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0052
0.00076
1
8260D
1/16/20 20:34
TBL
POA0231
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0052
0.00038
1
8260D
1/16/20 20:34
TBL
POA0231
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0052
0.00056
1
8260D
1/16/20 20:34
TBL
POA0231
1,1-Dichloroethane
BRL
mg/kg dry
0.0052
0.00093
1
8260D
1/16/20 20:34
TBL
POA0231
1,1-Dichloroethylene
BRL
mg/kg dry
0.0052
0.00095
1
8260D
1/16/20 20:34
TBL
POA0231
1,1-Dichloropropylene
BRL
mg/kg dry
0.0052
0.00080
1
8260D
1/16/20 20:34
TBL
POA0231
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.010
0.00074
1
8260D
1/16/20 20:34
TBL
POA0231
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0052
0.00059
1
8260D
1/16/20 20:34
TBL
POA0231
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.010
0.00049
1
8260D
1/16/20 20:34
TBL
POA0231
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0052
0.00055
1
8260D
1/16/20 20:34
TBL
POA0231
1,2-Dibromoethane
BRL
mg/kg dry
0.0052
0.00046
1
8260D
1/16/20 20:34
TBL
POA0231
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0052
0.00058
1
8260D
1/16/20 20:34
TBL
POA0231
1,2-Dichloroethane
BRL
mg/kg dry
0.0052
0.00062
1
8260D
1/16/20 20:34
TBL
POA0231
1,2-Dichloropropane
BRL
mg/kg dry
0.0052
0.00078
1
8260D
1/16/20 20:34
TBL
POA0231
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0052
0.00065
1
8260D
1/16/20 20:34
TBL
POA0231
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0052
0.00064
1
8260D
1/16/20 20:34
TBL
POA0231
1,3-Dichloropropane
BRL
mg/kg dry
0.0052
0.00043
1
8260D
1/16/20 20:34
TBL
POA0231
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0052
0.00066
1
8260D
1/16/20 20:34
TBL
POA0231
2,2-Dichloropropane
BRL
mg/kg dry
0.0052
0.00064
1
8260D
1/16/20 20:34
TBL
POA0231
2-Chlorotoluene
BRL
mg/kg dry
0.0052
0.00069
1
8260D
1/16/20 20:34
TBL
POA0231
4-Chlorotoluene
BRL
mg/kg dry
0.0052
0.00059
1
8260D
1/16/20 20:34
TBL
POA0231
4-Isopropyltoluene
BRL
mg/kg dry
0.0052
0.0013
1
8260D
1/16/20 20:34
TBL
POA0231
Acetone
0.061
mg/kg dry
0.021
0.0013
1
8260D
1/16/20 20:34
TBL
POA0231
Benzene
BRL
mg/kg dry
0.0052
0.00081
1
8260D
1/16/20 20:34
TBL
POA0231
Bromobenzene
BRL
mg/kg dry
0.0052
0.00072
1
8260D
1/16/20 20:34
TBL
POA0231
Bromochloromethane
BRL
mg/kg dry
0.0052
0.00085
1
8260D
1/16/20 20:34
TBL
POA0231
Bromodichloromethane
BRL
mg/kg dry
0.0052
0.00049
1
8260D
1/16/20 20:34
TBL
POA0231
Bromoform
BRL
mg/kg dry
0.0052
0.00040
1
8260D
1/16/20 20:34
TBL
POA0231
Bromomethane
0.0028 J
mg/kg dry
0.010
0.0025
1
8260D
1/16/20 20:34
TBL
POA0231
Carbon Tetrachloride
BRL
mg/kg dry
0.0052
0.0010
1
8260D
1/16/20 20:34
TBL
POA0231
Chlorobenzene
BRL
mg/kg dry
0.0052
0.00081
1
8260D
1/16/20 20:34
TBL
POA0231
Chloroethane
BRL
mg/kg dry
0.010
0.00098
1
8260D
1/16/20 20:34
TBL
POA0231
Chloroform
BRL
mg/kg dry
0.0052
0.00063
1
8260D
1/16/20 20:34
TBL
POA0231
Chloromethane
BRL
mg/kg dry
0.010
0.0016
1
8260D
1/16/20 20:34
TBL
POA0231
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0052
0.00081
1
8260D
1/16/20 20:34
TBL
POA0231
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0052
0.00051
1
8260D
1/16/20 20:34
TBL
POA0231
Dibromochloromethane
BRL
mg/kg dry
0.0052
0.00035
1
8260D
1/16/20 20:34
TBL
POA0231
Dichlorodifluoromethane
BRL
mg/kg dry
0.010
0.0015
1
8260D
1/16/20 20:34
TBL
POA0231
Ethylbenzene
BRL
mg/kg dry
0.0052
0.00078
1
8260D
1/16/20 20:34
TBL
POA0231
Isopropyl Ether
BRL
mg/kg dry
0.0052
0.00076
1
8260D
1/16/20 20:34
TBL
POA0231
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0052
0.00060
1
8260D
1/16/20 20:34
TBL
POA0231
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-12S
Attn: Katie Lippard Sample ID: 0010154-18
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:20
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
BRL
mg/kg dry
0.010
0.0013
1
8260D
1/16/20 20:34
TBL
POA0231
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.021
0.00036
1
8260D
1/16/20 20:34
TBL
POA0231
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.021
0.0012
1
8260D
1/16/20 20:34
TBL
POA0231
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.021
0.00042
1
8260D
1/16/20 20:34
TBL
POA0231
Methylene Chloride
BRL
mg/kg dry
0.0052
0.00084
1
8260D
1/16/20 20:34
TBL
POA0231
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0052
0.00072
1
8260D
1/16/20 20:34
TBL
POA0231
Naphthalene
BRL
mg/kg dry
0.010
0.00052
1
8260D
1/16/20 20:34
TBL
POA0231
n-Butylbenzene
BRL
mg/kg dry
0.0052
0.00048
1
8260D
1/16/20 20:34
TBL
POA0231
n-Propylbenzene
BRL
mg/kg dry
0.0052
0.00075
1
8260D
1/16/20 20:34
TBL
POA0231
o-Xylene
BRL
mg/kg dry
0.0052
0.00055
1
8260D
1/16/20 20:34
TBL
POA0231
sec-Butylbenzene
BRL
mg/kg dry
0.0052
0.00056
1
8260D
1/16/20 20:34
TBL
POA0231
Styrene
BRL
mg/kg dry
0.0052
0.00050
1
8260D
1/16/20 20:34
TBL
POA0231
tert-Butylbenzene
BRL
mg/kg dry
0.0052
0.00061
1
8260D
1/16/20 20:34
TBL
POA0231
Tetrachloroethylene
BRL
mg/kg dry
0.0052
0.00094
1
8260D
1/16/20 20:34
TBL
POA0231
Toluene
BRL
mg/kg dry
0.0052
0.00082
1
8260D
1/16/20 20:34
TBL
POA0231
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0052
0.00099
1
8260D
1/16/20 20:34
TBL
POA0231
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0052
0.00044
1
8260D
1/16/20 20:34
TBL
POA0231
Trichloroethylene
BRL
mg/kg dry
0.0052
0.0010
1
8260D
1/16/20 20:34
TBL
POA0231
Trichlorofluoromethane
BRL
mg/kg dry
0.010
0.0014
1
8260D
1/16/20 20:34
TBL
POA0231
Vinyl acetate
BRL
mg/kg dry
0.010
0.00056
1
8260D
1/16/20 20:34
TBL
POA0231
Vinyl chloride
BRL
mg/kg dry
0.010
0.0010
1
8260D
1/16/20 20:34
TBL
POA0231
Xylenes, total
BRL
mg/kg dry
0.016
0.0019
1
8260D
1/16/20 20:34
TBL
POA0231
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
96 %
70-130
Dibromofluoromethane
107 %
84-123
Toluene-d8
81 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-12D
Attn: Katie Lippard Sample ID: 0010154-19
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:15
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
82.4
% by
0.100
0.100
1
SM2540 G
1/16/20 14:09
EDV
POA0228
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.80
0.14
1
8270E
1/16/20 20:14
JMV
POA0221
1,2-Dichlorobenzene
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:14
JMV
POA0221
1,3-Dichlorobenzene
BRL
mg/kg dry
0.80
0.12
1
8270E
1/16/20 20:14
JMV
POA0221
1,4-Dichlorobenzene
BRL
mg/kg dry
0.40
0.13
1
8270E
1/16/20 20:14
JMV
POA0221
1-Methyl naphthalene
BRL
mg/kg dry
0.80
0.012
1
8270E
1/16/20 20:14
JMV
POA0221
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.80
0.17
1
8270E
1/16/20 20:14
JMV
POA0221
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.80
0.19
1
8270E
1/16/20 20:14
JMV
POA0221
2,4-Dichlorophenol
BRL
mg/kg dry
0.80
0.16
1
8270E
1/16/20 20:14
JMV
POA0221
2,4-Dimethylphenol
BRL
mg/kg dry
0.40
0.17
1
8270E
1/16/20 20:14
JMV
POA0221
2,4-Dinitrophenol
BRL
mg/kg dry
1.8
0.47
1
8270E
1/16/20 20:14
JMV
POA0221
2,4-Dinitrotoluene
BRL
mg/kg dry
0.80
0.21
1
8270E
1/16/20 20:14
JMV
POA0221
2,6-Dinitrotoluene
BRL
mg/kg dry
0.80
0.21
1
8270E
1/16/20 20:14
JMV
POA0221
2-Chloronaphthalene
BRL
mg/kg dry
0.80
0.20
1
8270E
1/16/20 20:14
JMV
POA0221
2-Chlorophenol
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:14
JMV
POA0221
2-Methyl naphthalene
BRL
mg/kg dry
0.80
0.016
1
8270E
1/16/20 20:14
JMV
POA0221
2-Methylphenol
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:14
JMV
POA0221
2-Nitrophenol
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:14
JMV
POA0221
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.80
0.16
1
8270E
1/16/20 20:14
JMV
POA0221
3/4-Methyl phenol
BRL
mg/kg dry
0.80
0.17
1
8270E
1/16/20 20:14
JMV
POA0221
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.8
0.44
1
8270E
1/16/20 20:14
JMV
POA0221
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.80
0.19
1
8270E
1/16/20 20:14
JMV
POA0221
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:14
JMV
POA0221
4-Chloroaniline
BRL
mg/kg dry
0.40
0.097
1
8270E
1/16/20 20:14
JMV
POA0221
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.24
1
8270E
1/16/20 20:14
JMV
POA0221
4-Nitrophenol
BRL
mg/kg dry
0.80
0.20
1
8270E
1/16/20 20:14
JMV
POA0221
Acenaphthene
BRL
mg/kg dry
0.80
0.018
1
8270E
1/16/20 20:14
JMV
POA0221
Acenaphthylene
BRL
mg/kg dry
0.80
0.016
1
8270E
1/16/20 20:14
JMV
POA0221
Anthracene
BRL
mg/kg dry
0.80
0.0089
1
8270E
1/16/20 20:14
JMV
POA0221
Azobenzene
BRL
mg/kg dry
0.80
0.17
1
8270E
1/16/20 20:14
JMV
POA0221
Benzo(a)anthracene
BRL
mg/kg dry
0.80
0.0096
1
8270E
1/16/20 20:14
JMV
POA0221
Benzo(a)pyrene
BRL
mg/kg dry
0.80
0.0072
1
8270E
1/16/20 20:14
JMV
POA0221
Benzo(b)fluoranthene
BRL
mg/kg dry
0.80
0.0074
1
8270E
1/16/20 20:14
JMV
POA0221
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.80
0.0079
1
8270E
1/16/20 20:14
JMV
POA0221
Benzo(k)fluoranthene
BRL
mg/kg dry
0.80
0.0085
1
8270E
1/16/20 20:14
JMV
POA0221
Benzoic Acid
BRL
mg/kg dry
2.4
0.66
1
8270E
1/16/20 20:14
JMV
POA0221
Benzyl alcohol
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:14
JMV
POA0221
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:14
JMV
POA0221
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:14
JMV
POA0221
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.40
0.14
1
8270E
1/16/20 20:14
JMV
POA0221
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-12D
Attn: Katie Lippard Sample ID: 0010154-19
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:15
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.80
0.18
1
8270E
1/16/20 20:14
JMV
POA0221
Butyl benzyl phthalate
BRL
mg/kg dry
0.40
0.14
1
8270E
1/16/20 20:14
JMV
POA0221
Chrysene
BRL
mg/kg dry
0.80
0.0095
1
8270E
1/16/20 20:14
JMV
POA0221
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.80
0.023
1
8270E
1/16/20 20:14
JMV
POA0221
Dibenzofuran
BRL
mg/kg dry
0.80
0.22
1
8270E
1/16/20 20:14
JMV
POA0221
Diethyl phthalate
BRL
mg/kg dry
0.80
0.21
1
8270E
1/16/20 20:14
JMV
POA0221
Dimethyl phthalate
BRL
mg/kg dry
0.80
0.19
1
8270E
1/16/20 20:14
JMV
POA0221
Di-n-butyl phthalate
BRL
mg/kg dry
0.80
0.20
1
8270E
1/16/20 20:14
JMV
POA0221
Di-n-octyl phthalate
BRL
mg/kg dry
0.40
0.21
1
8270E
1/16/20 20:14
JMV
POA0221
Fluoranthene
BRL
mg/kg dry
0.80
0.0091
1
8270E
1/16/20 20:14
JMV
POA0221
Fluorene
BRL
mg/kg dry
0.80
0.014
1
8270E
1/16/20 20:14
JMV
POA0221
Hexachlorobenzene
BRL
mg/kg dry
0.80
0.18
1
8270E
1/16/20 20:14
JMV
POA0221
Hexachlorobutadiene
BRL
mg/kg dry
0.80
0.18
1
8270E
1/16/20 20:14
JMV
POA0221
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.80
0.28
1
8270E
1/16/20 20:14
JMV
POA0221
Hexachloroethane
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:14
JMV
POA0221
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.80
0.023
1
8270E
1/16/20 20:14
JMV
POA0221
Isophorone
BRL
mg/kg dry
0.80
0.17
1
8270E
1/16/20 20:14
JMV
POA0221
Naphthalene
BRL
mg/kg dry
0.80
0.017
1
8270E
1/16/20 20:14
JMV
POA0221
Nitrobenzene
BRL
mg/kg dry
0.40
0.17
1
8270E
1/16/20 20:14
JMV
POA0221
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.80
0.18
1
8270E
1/16/20 20:14
JMV
POA0221
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.80
0.22
1
8270E
1/16/20 20:14
JMV
POA0221
Pentachlorophenol
BRL
mg/kg dry
1.2
0.51
1
8270E
1/16/20 20:14
JMV
POA0221
Phenanthrene
BRL
mg/kg dry
0.80
0.0087
1
8270E
1/16/20 20:14
JMV
POA0221
Phenol
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:14
JMV
POA0221
Pyrene
BRL
mg/kg dry
0.80
0.012
1
8270E
1/16/20 20:14
JMV
POA0221
Pyridine
BRL
mg/kg dry
0.40
0.076
1
8270E
1/16/20 20:14
JMV
POA0221
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
92 %
39-132
2-Fluorobiphenyl
78 %
44-115
2-Fluorophenol
79 %
35-115
Nitrobenzene-d5
73 %
37-122
Phenol-d5
76 %
34-121
Terphenyl-d14
77 %
54-127
Total Metals
Mercury
BRL
mg/kg dry
0.061
0.021
1
7471B
1/16/20 11:53
JAB
POA0214
Arsenic
0.18 J
mg/kg dry
1.2
0.16
1
6010D
1/18/20
1:47
JAB
POA0181
Barium
54
mg/kg dry
12
3.6
1
6010D
1/18/20
1:47
JAB
POA0181
Cadmium
BRL
mg/kg dry
0.61
0.041
1
6010D
1/18/20
1:47
JAB
POA0181
Chromium
5.7
mg/kg dry
1.2
0.092
1
6010D
1/18/20
1:47
JAB
POA0181
Lead
12
mg/kg dry
1.2
0.20
1
6010D
1/18/20
1:47
JAB
POA0181
Selenium
BRL
mg/kg dry
1.2
0.33
1
6010D
1/18/20
1:47
JAB
POA0181
Silver
BRL
mg/kg dry
0.61
0.037
1
6010D
1/18/20
1:47
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-12D
Attn: Katie Lippard Sample ID: 0010154-19
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:15
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0071
0.00087
1
8260D
1/16/20 21:04
TBL
POA0231
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0071
0.0010
1
8260D
1/16/20 21:04
TBL
POA0231
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0071
0.00052
1
8260D
1/16/20 21:04
TBL
POA0231
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0071
0.00077
1
8260D
1/16/20 21:04
TBL
POA0231
1,1-Dichloroethane
BRL
mg/kg dry
0.0071
0.0013
1
8260D
1/16/20 21:04
TBL
POA0231
1,1-Dichloroethylene
BRL
mg/kg dry
0.0071
0.0013
1
8260D
1/16/20 21:04
TBL
POA0231
1,1-Dichloropropylene
BRL
mg/kg dry
0.0071
0.0011
1
8260D
1/16/20 21:04
TBL
POA0231
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.014
0.0010
1
8260D
1/16/20 21:04
TBL
POA0231
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0071
0.00081
1
8260D
1/16/20 21:04
TBL
POA0231
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.014
0.00068
1
8260D
1/16/20 21:04
TBL
POA0231
1,2,4-Trimethylbenzene
0.0046 J
mg/kg dry
0.0071
0.00075
1
8260D
1/16/20 21:04
TBL
POA0231
1,2-Dibromoethane
BRL
mg/kg dry
0.0071
0.00064
1
8260D
1/16/20 21:04
TBL
POA0231
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0071
0.00079
1
8260D
1/16/20 21:04
TBL
POA0231
1,2-Dichloroethane
BRL
mg/kg dry
0.0071
0.00085
1
8260D
1/16/20 21:04
TBL
POA0231
1,2-Dichloropropane
BRL
mg/kg dry
0.0071
0.0011
1
8260D
1/16/20 21:04
TBL
POA0231
1,3,5-Trimethylbenzene
0.0062 J
mg/kg dry
0.0071
0.00089
1
8260D
1/16/20 21:04
TBL
POA0231
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0071
0.00089
1
8260D
1/16/20 21:04
TBL
POA0231
1,3-Dichloropropane
BRL
mg/kg dry
0.0071
0.00060
1
8260D
1/16/20 21:04
TBL
POA0231
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0071
0.00090
1
8260D
1/16/20 21:04
TBL
POA0231
2,2-Dichloropropane
BRL
mg/kg dry
0.0071
0.00089
1
8260D
1/16/20 21:04
TBL
POA0231
2-Chlorotoluene
BRL
mg/kg dry
0.0071
0.00095
1
8260D
1/16/20 21:04
TBL
POA0231
4-Chlorotoluene
BRL
mg/kg dry
0.0071
0.00081
1
8260D
1/16/20 21:04
TBL
POA0231
4-Isopropyltoluene
BRL
mg/kg dry
0.0071
0.0018
1
8260D
1/16/20 21:04
TBL
POA0231
Acetone
0.037
mg/kg dry
0.028
0.0018
1
8260D
1/16/20 21:04
TBL
POA0231
Benzene
BRL
mg/kg dry
0.0071
0.0011
1
8260D
1/16/20 21:04
TBL
POA0231
Bromobenzene
BRL
mg/kg dry
0.0071
0.00099
1
8260D
1/16/20 21:04
TBL
POA0231
Bromochloromethane
BRL
mg/kg dry
0.0071
0.0012
1
8260D
1/16/20 21:04
TBL
POA0231
Bromodichloromethane
BRL
mg/kg dry
0.0071
0.00068
1
8260D
1/16/20 21:04
TBL
POA0231
Bromoform
BRL
mg/kg dry
0.0071
0.00055
1
8260D
1/16/20 21:04
TBL
POA0231
Bromomethane
0.0048 J
mg/kg dry
0.014
0.0035
1
8260D
1/16/20 21:04
TBL
POA0231
Carbon Tetrachloride
BRL
mg/kg dry
0.0071
0.0014
1
8260D
1/16/20 21:04
TBL
POA0231
Chlorobenzene
BRL
mg/kg dry
0.0071
0.0011
1
8260D
1/16/20 21:04
TBL
POA0231
Chloroethane
BRL
mg/kg dry
0.014
0.0014
1
8260D
1/16/20 21:04
TBL
POA0231
Chloroform
BRL
mg/kg dry
0.0071
0.00087
1
8260D
1/16/20 21:04
TBL
POA0231
Chloromethane
BRL
mg/kg dry
0.014
0.0022
1
8260D
1/16/20 21:04
TBL
POA0231
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0071
0.0011
1
8260D
1/16/20 21:04
TBL
POA0231
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0071
0.00070
1
8260D
1/16/20 21:04
TBL
POA0231
Dibromochloromethane
BRL
mg/kg dry
0.0071
0.00048
1
8260D
1/16/20 21:04
TBL
POA0231
Dichlorodifluoromethane
BRL
mg/kg dry
0.014
0.0020
1
8260D
1/16/20 21:04
TBL
POA0231
Ethylbenzene
BRL
mg/kg dry
0.0071
0.0011
1
8260D
1/16/20 21:04
TBL
POA0231
Isopropyl Ether
BRL
mg/kg dry
0.0071
0.0010
1
8260D
1/16/20 21:04
TBL
POA0231
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0071
0.00083
1
8260D
1/16/20 21:04
TBL
POA0231
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: B-12D
Attn: Katie Lippard Sample ID: 0010154-19
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:15
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
0.0023 J
mg/kg dry
0.014
0.0018
1
8260D
1/16/20 21:04
TBL
POA0231
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.028
0.00049
1
8260D
1/16/20 21:04
TBL
POA0231
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.028
0.0017
1
8260D
1/16/20 21:04
TBL
POA0231
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.028
0.00058
1
8260D
1/16/20 21:04
TBL
POA0231
Methylene Chloride
BRL
mg/kg dry
0.0071
0.0012
1
8260D
1/16/20 21:04
TBL
POA0231
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0071
0.0010
1
8260D
1/16/20 21:04
TBL
POA0231
Naphthalene
0.0055 J
mg/kg dry
0.014
0.00072
1
8260D
1/16/20 21:04
TBL
POA0231
n-Butylbenzene
BRL
mg/kg dry
0.0071
0.00067
1
8260D
1/16/20 21:04
TBL
POA0231
n-Propylbenzene
BRL
mg/kg dry
0.0071
0.0010
1
8260D
1/16/20 21:04
TBL
POA0231
o-Xylene
0.00083 J
mg/kg dry
0.0071
0.00076
1
8260D
1/16/20 21:04
TBL
POA0231
sec-Butylbenzene
BRL
mg/kg dry
0.0071
0.00077
1
8260D
1/16/20 21:04
TBL
POA0231
Styrene
BRL
mg/kg dry
0.0071
0.00069
1
8260D
1/16/20 21:04
TBL
POA0231
tert-Butylbenzene
BRL
mg/kg dry
0.0071
0.00085
1
8260D
1/16/20 21:04
TBL
POA0231
Tetrachloroethylene
BRL
mg/kg dry
0.0071
0.0013
1
8260D
1/16/20 21:04
TBL
POA0231
Toluene
BRL
mg/kg dry
0.0071
0.0011
1
8260D
1/16/20 21:04
TBL
POA0231
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0071
0.0014
1
8260D
1/16/20 21:04
TBL
POA0231
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0071
0.00061
1
8260D
1/16/20 21:04
TBL
POA0231
Trichloroethylene
BRL
mg/kg dry
0.0071
0.0014
1
8260D
1/16/20 21:04
TBL
POA0231
Trichlorofluoromethane
BRL
mg/kg dry
0.014
0.0019
1
8260D
1/16/20 21:04
TBL
POA0231
Vinyl acetate
BRL
mg/kg dry
0.014
0.00077
1
8260D
1/16/20 21:04
TBL
POA0231
Vinyl chloride
BRL
mg/kg dry
0.014
0.0014
1
8260D
1/16/20 21:04
TBL
POA0231
Xylenes, total
0.0031 J
mg/kg dry
0.021
0.0026
1
8260D
1/16/20 21:04
TBL
POA0231
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
93 %
70-130
Dibromofluoromethane
99 %
84-123
Toluene-d8
84 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• ® 01/28/2020
PA Waynt.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: Duplicate
Attn: Katie Lippard Sample ID: 0010154-20
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:45
Time Submitted: 01/10/20 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
82.7
% by
0.100
0.100
1
SM2540 G
1/16/20 14:09
EDV
POA0228
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.80
0.14
1
8270E
1/16/20 20:36
JMV
POA0221
1,2-Dichlorobenzene
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:36
JMV
POA0221
1,3-Dichlorobenzene
BRL
mg/kg dry
0.80
0.12
1
8270E
1/16/20 20:36
JMV
POA0221
1,4-Dichlorobenzene
BRL
mg/kg dry
0.40
0.13
1
8270E
1/16/20 20:36
JMV
POA0221
1-Methyl naphthalene
BRL
mg/kg dry
0.80
0.012
1
8270E
1/16/20 20:36
JMV
POA0221
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.80
0.17
1
8270E
1/16/20 20:36
JMV
POA0221
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.80
0.19
1
8270E
1/16/20 20:36
JMV
POA0221
2,4-Dichlorophenol
BRL
mg/kg dry
0.80
0.16
1
8270E
1/16/20 20:36
JMV
POA0221
2,4-Dimethylphenol
BRL
mg/kg dry
0.40
0.17
1
8270E
1/16/20 20:36
JMV
POA0221
2,4-Dinitrophenol
BRL
mg/kg dry
1.8
0.47
1
8270E
1/16/20 20:36
JMV
POA0221
2,4-Dinitrotoluene
BRL
mg/kg dry
0.80
0.21
1
8270E
1/16/20 20:36
JMV
POA0221
2,6-Dinitrotoluene
BRL
mg/kg dry
0.80
0.21
1
8270E
1/16/20 20:36
JMV
POA0221
2-Chloronaphthalene
BRL
mg/kg dry
0.80
0.19
1
8270E
1/16/20 20:36
JMV
POA0221
2-Chlorophenol
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:36
JMV
POA0221
2-Methyl naphthalene
BRL
mg/kg dry
0.80
0.015
1
8270E
1/16/20 20:36
JMV
POA0221
2-Methylphenol
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:36
JMV
POA0221
2-Nitrophenol
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:36
JMV
POA0221
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.80
0.16
1
8270E
1/16/20 20:36
JMV
POA0221
3/4-Methyl phenol
BRL
mg/kg dry
0.80
0.17
1
8270E
1/16/20 20:36
JMV
POA0221
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.8
0.44
1
8270E
1/16/20 20:36
JMV
POA0221
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.80
0.19
1
8270E
1/16/20 20:36
JMV
POA0221
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:36
JMV
POA0221
4-Chloroaniline
BRL
mg/kg dry
0.40
0.096
1
8270E
1/16/20 20:36
JMV
POA0221
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.24
1
8270E
1/16/20 20:36
JMV
POA0221
4-Nitrophenol
BRL
mg/kg dry
0.80
0.20
1
8270E
1/16/20 20:36
JMV
POA0221
Acenaphthene
BRL
mg/kg dry
0.80
0.018
1
8270E
1/16/20 20:36
JMV
POA0221
Acenaphthylene
BRL
mg/kg dry
0.80
0.016
1
8270E
1/16/20 20:36
JMV
POA0221
Anthracene
BRL
mg/kg dry
0.80
0.0088
1
8270E
1/16/20 20:36
JMV
POA0221
Azobenzene
BRL
mg/kg dry
0.80
0.17
1
8270E
1/16/20 20:36
JMV
POA0221
Benzo(a)anthracene
BRL
mg/kg dry
0.80
0.0095
1
8270E
1/16/20 20:36
JMV
POA0221
Benzo(a)pyrene
BRL
mg/kg dry
0.80
0.0071
1
8270E
1/16/20 20:36
JMV
POA0221
Benzo(b)fluoranthene
BRL
mg/kg dry
0.80
0.0074
1
8270E
1/16/20 20:36
JMV
POA0221
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.80
0.0078
1
8270E
1/16/20 20:36
JMV
POA0221
Benzo(k)fluoranthene
BRL
mg/kg dry
0.80
0.0084
1
8270E
1/16/20 20:36
JMV
POA0221
Benzoic Acid
BRL
mg/kg dry
2.4
0.66
1
8270E
1/16/20 20:36
JMV
POA0221
Benzyl alcohol
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:36
JMV
POA0221
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.80
0.15
1
8270E
1/16/20 20:36
JMV
POA0221
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:36
JMV
POA0221
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.40
0.14
1
8270E
1/16/20 20:36
JMV
POA0221
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01 /28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: Duplicate
Attn: Katie Lippard Sample ID: 0010154-20
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:45
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Bis(2-Ethylhexyl)phthaIate
BRL
mg/kg dry
0.80
0.18
1
8270E
1/16/20 20:36
JMV
POA0221
Butyl benzyl phthalate
BRL
mg/kg dry
0.40
0.14
1
8270E
1/16/20 20:36
JMV
POA0221
Chrysene
BRL
mg/kg dry
0.80
0.0094
1
8270E
1/16/20 20:36
JMV
POA0221
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.80
0.023
1
8270E
1/16/20 20:36
JMV
POA0221
Dibenzofuran
BRL
mg/kg dry
0.80
0.21
1
8270E
1/16/20 20:36
JMV
POA0221
Diethyl phthalate
BRL
mg/kg dry
0.80
0.20
1
8270E
1/16/20 20:36
JMV
POA0221
Dimethyl phthalate
BRL
mg/kg dry
0.80
0.19
1
8270E
1/16/20 20:36
JMV
POA0221
Di-n-butyl phthalate
BRL
mg/kg dry
0.80
0.20
1
8270E
1/16/20 20:36
JMV
POA0221
Di-n-octyl phthalate
BRL
mg/kg dry
0.40
0.21
1
8270E
1/16/20 20:36
JMV
POA0221
Fluoranthene
BRL
mg/kg dry
0.80
0.0090
1
8270E
1/16/20 20:36
JMV
POA0221
Fluorene
BRL
mg/kg dry
0.80
0.014
1
8270E
1/16/20 20:36
JMV
POA0221
Hexachlorobenzene
BRL
mg/kg dry
0.80
0.17
1
8270E
1/16/20 20:36
JMV
POA0221
Hexachlorobutadiene
BRL
mg/kg dry
0.80
0.18
1
8270E
1/16/20 20:36
JMV
POA0221
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.80
0.27
1
8270E
1/16/20 20:36
JMV
POA0221
Hexachloroethane
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:36
JMV
POA0221
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.80
0.022
1
8270E
1/16/20 20:36
JMV
POA0221
Isophorone
BRL
mg/kg dry
0.80
0.17
1
8270E
1/16/20 20:36
JMV
POA0221
Naphthalene
BRL
mg/kg dry
0.80
0.017
1
8270E
1/16/20 20:36
JMV
POA0221
Nitrobenzene
BRL
mg/kg dry
0.40
0.17
1
8270E
1/16/20 20:36
JMV
POA0221
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.80
0.18
1
8270E
1/16/20 20:36
JMV
POA0221
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.80
0.22
1
8270E
1/16/20 20:36
JMV
POA0221
Pentachlorophenol
BRL
mg/kg dry
1.2
0.51
1
8270E
1/16/20 20:36
JMV
POA0221
Phenanthrene
BRL
mg/kg dry
0.80
0.0087
1
8270E
1/16/20 20:36
JMV
POA0221
Phenol
BRL
mg/kg dry
0.80
0.13
1
8270E
1/16/20 20:36
JMV
POA0221
Pyrene
BRL
mg/kg dry
0.80
0.012
1
8270E
1/16/20 20:36
JMV
POA0221
Pyridine
BRL
mg/kg dry
0.40
0.076
1
8270E
1/16/20 20:36
JMV
POA0221
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
85 %
39-132
2-Fluorobiphenyl
74 %
44-115
2-Fluorophenol
75 %
35-115
Nitrobenzene-d5
68 %
37-122
Phenol-d5
72 %
34-121
Terphenyl-d14
73 %
54-127
Total Metals
Mercury
0.082
mg/kg dry
0.060
0.021
1
7471B
1/16/20 11:57
JAB
POA0214
Arsenic
0.36 J
mg/kg dry
1.2
0.16
1
6010D
1/18/20
1:55
JAB
POA0181
Barium
55
mg/kg dry
12
3.6
1
6010D
1/18/20
1:55
JAB
POA0181
Cadmium
BRL
mg/kg dry
0.60
0.041
1
6010D
1/18/20
1:55
JAB
POA0181
Chromium
6.5
mg/kg dry
1.2
0.092
1
6010D
1/18/20
1:55
JAB
POA0181
Lead
12
mg/kg dry
1.2
0.20
1
6010D
1/18/20
1:55
JAB
POA0181
Selenium
BRL
mg/kg dry
1.2
0.33
1
6010D
1/18/20
1:55
JAB
POA0181
Silver
BRL
mg/kg dry
0.60
0.037
1
6010D
1/18/20
1:55
JAB
POA0181
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: Duplicate
Attn: Katie Lippard Sample ID: 0010154-20
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:45
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0079
0.00097
1
8260D
1/16/20 21:34
TBL
POA0231
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0079
0.0012
1
8260D
1/16/20 21:34
TBL
POA0231
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0079
0.00058
1
8260D
1/16/20 21:34
TBL
POA0231
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0079
0.00085
1
8260D
1/16/20 21:34
TBL
POA0231
1,1-Dichloroethane
BRL
mg/kg dry
0.0079
0.0014
1
8260D
1/16/20 21:34
TBL
POA0231
1,1-Dichloroethylene
BRL
mg/kg dry
0.0079
0.0015
1
8260D
1/16/20 21:34
TBL
POA0231
1,1-Dichloropropylene
BRL
mg/kg dry
0.0079
0.0012
1
8260D
1/16/20 21:34
TBL
POA0231
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.016
0.0011
1
8260D
1/16/20 21:34
TBL
POA0231
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0079
0.00090
1
8260D
1/16/20 21:34
TBL
POA0231
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.016
0.00075
1
8260D
1/16/20 21:34
TBL
POA0231
1,2,4-Trimethylbenzene
0.0023 J
mg/kg dry
0.0079
0.00084
1
8260D
1/16/20 21:34
TBL
POA0231
1,2-Dibromoethane
BRL
mg/kg dry
0.0079
0.00071
1
8260D
1/16/20 21:34
TBL
POA0231
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0079
0.00088
1
8260D
1/16/20 21:34
TBL
POA0231
1,2-Dichloroethane
BRL
mg/kg dry
0.0079
0.00094
1
8260D
1/16/20 21:34
TBL
POA0231
1,2-Dichloropropane
BRL
mg/kg dry
0.0079
0.0012
1
8260D
1/16/20 21:34
TBL
POA0231
1,3,5-Trimethylbenzene
0.0028 J
mg/kg dry
0.0079
0.00099
1
8260D
1/16/20 21:34
TBL
POA0231
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0079
0.00098
1
8260D
1/16/20 21:34
TBL
POA0231
1,3-Dichloropropane
BRL
mg/kg dry
0.0079
0.00066
1
8260D
1/16/20 21:34
TBL
POA0231
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0079
0.0010
1
8260D
1/16/20 21:34
TBL
POA0231
2,2-Dichloropropane
BRL
mg/kg dry
0.0079
0.00099
1
8260D
1/16/20 21:34
TBL
POA0231
2-Chlorotoluene
BRL
mg/kg dry
0.0079
0.0011
1
8260D
1/16/20 21:34
TBL
POA0231
4-Chlorotoluene
BRL
mg/kg dry
0.0079
0.00090
1
8260D
1/16/20 21:34
TBL
POA0231
4-Isopropyltoluene
BRL
mg/kg dry
0.0079
0.0020
1
8260D
1/16/20 21:34
TBL
POA0231
Acetone
0.042
mg/kg dry
0.032
0.0020
1
8260D
1/16/20 21:34
TBL
POA0231
Benzene
BRL
mg/kg dry
0.0079
0.0012
1
8260D
1/16/20 21:34
TBL
POA0231
Bromobenzene
BRL
mg/kg dry
0.0079
0.0011
1
8260D
1/16/20 21:34
TBL
POA0231
Bromochloromethane
BRL
mg/kg dry
0.0079
0.0013
1
8260D
1/16/20 21:34
TBL
POA0231
Bromodichloromethane
BRL
mg/kg dry
0.0079
0.00075
1
8260D
1/16/20 21:34
TBL
POA0231
Bromoform
BRL
mg/kg dry
0.0079
0.00061
1
8260D
1/16/20 21:34
TBL
POA0231
Bromomethane
BRL
mg/kg dry
0.016
0.0039
1
8260D
1/16/20 21:34
TBL
POA0231
Carbon Tetrachloride
BRL
mg/kg dry
0.0079
0.0016
1
8260D
1/16/20 21:34
TBL
POA0231
Chlorobenzene
BRL
mg/kg dry
0.0079
0.0012
1
8260D
1/16/20 21:34
TBL
POA0231
Chloroethane
BRL
mg/kg dry
0.016
0.0015
1
8260D
1/16/20 21:34
TBL
POA0231
Chloroform
BRL
mg/kg dry
0.0079
0.00097
1
8260D
1/16/20 21:34
TBL
POA0231
Chloromethane
BRL
mg/kg dry
0.016
0.0024
1
8260D
1/16/20 21:34
TBL
POA0231
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0079
0.0012
1
8260D
1/16/20 21:34
TBL
POA0231
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0079
0.00078
1
8260D
1/16/20 21:34
TBL
POA0231
Dibromochloromethane
BRL
mg/kg dry
0.0079
0.00053
1
8260D
1/16/20 21:34
TBL
POA0231
Dichlorodifluoromethane
BRL
mg/kg dry
0.016
0.0022
1
8260D
1/16/20 21:34
TBL
POA0231
Ethylbenzene
BRL
mg/kg dry
0.0079
0.0012
1
8260D
1/16/20 21:34
TBL
POA0231
Isopropyl Ether
BRL
mg/kg dry
0.0079
0.0012
1
8260D
1/16/20 21:34
TBL
POA0231
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0079
0.00092
1
8260D
1/16/20 21:34
TBL
POA0231
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
_ • _ . 0 01/28/2020
- -ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Client Sample ID: Duplicate
Attn: Katie Lippard Sample ID: 0010154-20
409 Rogers View Court Work Order: 0010154
Raleigh, NC 27610 Sample Matrix: Soil Time Collected: 01/07/20 09:45
Time Submitted: 01/10/20 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
m,p-Xylenes
0.0041 J
mg/kg dry
0.016
0.0020
1
8260D
1/16/20 21:34
TBL
POA0231
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.032
0.00055
1
8260D
1/16/20 21:34
TBL
POA0231
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.032
0.0019
1
8260D
1/16/20 21:34
TBL
POA0231
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.032
0.00065
1
8260D
1/16/20 21:34
TBL
POA0231
Methylene Chloride
BRL
mg/kg dry
0.0079
0.0013
1
8260D
1/16/20 21:34
TBL
POA0231
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0079
0.0011
1
8260D
1/16/20 21:34
TBL
POA0231
Naphthalene
0.0042 J
mg/kg dry
0.016
0.00080
1
8260D
1/16/20 21:34
TBL
POA0231
n-Butylbenzene
BRL
mg/kg dry
0.0079
0.00074
1
8260D
1/16/20 21:34
TBL
POA0231
n-Propylbenzene
BRL
mg/kg dry
0.0079
0.0011
1
8260D
1/16/20 21:34
TBL
POA0231
o-Xylene
0.00098 J
mg/kg dry
0.0079
0.00084
1
8260D
1/16/20 21:34
TBL
POA0231
sec-Butylbenzene
BRL
mg/kg dry
0.0079
0.00085
1
8260D
1/16/20 21:34
TBL
POA0231
Styrene
BRL
mg/kg dry
0.0079
0.00077
1
8260D
1/16/20 21:34
TBL
POA0231
tert-Butylbenzene
BRL
mg/kg dry
0.0079
0.00094
1
8260D
1/16/20 21:34
TBL
POA0231
Tetrachloroethylene
BRL
mg/kg dry
0.0079
0.0014
1
8260D
1/16/20 21:34
TBL
POA0231
Toluene
BRL
mg/kg dry
0.0079
0.0013
1
8260D
1/16/20 21:34
TBL
POA0231
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0079
0.0015
1
8260D
1/16/20 21:34
TBL
POA0231
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0079
0.00068
1
8260D
1/16/20 21:34
TBL
POA0231
Trichloroethylene
BRL
mg/kg dry
0.0079
0.0015
1
8260D
1/16/20 21:34
TBL
POA0231
Trichlorofluoromethane
BRL
mg/kg dry
0.016
0.0021
1
8260D
1/16/20 21:34
TBL
POA0231
Vinyl acetate
BRL
mg/kg dry
0.016
0.00086
1
8260D
1/16/20 21:34
TBL
POA0231
Vinyl chloride
BRL
mg/kg dry
0.016
0.0016
1
8260D
1/16/20 21:34
TBL
POA0231
Xylenes, total
0.0051 J
mg/kg dry
0.024
0.0028
1
8260D
1/16/20 21:34
TBL
POA0231
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
92 %
70-130
Dibromofluoromethane
100 %
84-123
Toluene-d8
84 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0183 - 5035
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POA0183-BLK1)
Prepared &Analyzed: 01/14/20
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0183 - 5035
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POA0183-BLK1)
Prepared & Analyzed: 01/14/20
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
48.9
ug/L
50.00 98 70-130
Surrogate: Dibromofluoromethane
50.6
ug/L
50.00 101 84-123
Surrogate: Toluene-d8
45.0
ug/L
50.00 90 76-129
LCS (POA0183-BSI)
Prepared &Analyzed:
01/14/20
1,1,1,2-Tetrachloroethane
0.0485
0.0050
mg/kg wet
0.05000
97
72-115
1, 1,1 -Trichloroethane
0.0555
0.0050
mg/kg wet
0.05000
ill
67-131
1,1,2,2-Tetrachloroethane
0.0430
0.0050
mg/kg wet
0.05000
86
56-126
1,1,2-Trichloroethane
0.0459
0.0050
mg/kg wet
0.05000
92
70-133
1,1-Dichloroethane
0.0575
0.0050
mg/kg wet
0.05000
115
74-127
1,1-Dichloroethylene
0.0571
0.0050
mg/kg wet
0.05000
114
67-149
1, 1 -Dichloropropylene
0.0567
0.0050
mg/kg wet
0.05000
113
71-130
1,2,3-Trichlorobenzene
0.0445
0.010
mg/kg wet
0.05000
89
68-130
1,2,3-Trichloropropane
0.0424
0.0050
mg/kg wet
0.05000
85
60-137
1,2,4-Trichlorobenzene
0.0450
0.010
mg/kg wet
0.05000
90
66-125
1,2,4-Trimethylbenzene
0.0486
0.0050
mg/kg wet
0.05000
97
69-129
1,2-Dibromoethane
0.0452
0.0050
mg/kg wet
0.05000
90
70-132
1,2-Dichlorobenzene
0.0453
0.0050
mg/kg wet
0.05000
91
72-123
1,2-Dichloroethane
0.0522
0.0050
mg/kg wet
0.05000
104
68-128
1,2-Dichloropropane
0.0563
0.0050
mg/kg wet
0.05000
113
73-130
1,3,5-Trimethylbenzene
0.0486
0.0050
mg/kg wet
0.05000
97
69-128
1,3-Dichlorobenzene
0.0464
0.0050
mg/kg wet
0.05000
93
71-120
1,3-Dichloropropane
0.0471
0.0050
mg/kg wet
0.05000
94
75-124
1,4-Dichlorobenzene
0.0460
0.0050
mg/kg wet
0.05000
92
71-123
2,2-Dichloropropane
0.0562
0.0050
mg/kg wet
0.05000
112
50-142
2-Chlorotoluene
0.0476
0.0050
mg/kg wet
0.05000
95
67-124
4-Chlorotoluene
0.0482
0.0050
mg/kg wet
0.05000
96
71-126
4-Isopropyltoluene
0.0496
0.0050
mg/kg wet
0.05000
99
68-129
Acetone
0.0607
0.020
mg/kg wet
0.1000
61
29-198
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0183 - 5035
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (POA0183-BS1)
Prepared &Analyzed: 01/14/20
Benzene
0.0567
0.0050
mg/kg wet
0.05000
113
74-127
Bromobenzene
0.0472
0.0050
mg/kg wet
0.05000
94
73-125
Bromochloromethane
0.0532
0.0050
mg/kg wet
0.05000
106
72-134
Bromodichloromethane
0.0556
0.0050
mg/kg wet
0.05000
ill
75-122
Bromoform
0.0467
0.0050
mg/kg wet
0.05000
93
66-135
Bromomethane
0.0470
0.010
mg/kg wet
0.05000
94
20-180
Carbon Tetrachloride
0.0544
0.0050
mg/kg wet
0.05000
109
64-143
Chlorobenzene
0.0486
0.0050
mg/kg wet
0.05000
97
74-118
Chloroethane
0.0502
0.010
mg/kg wet
0.05000
100
33-149
Chloroform
0.0562
0.0050
mg/kg wet
0.05000
112
73-127
Chloromethane
0.0438
0.010
mg/kg wet
0.05000
88
45-143
cis-1,2-Dichloroethylene
0.0542
0.0050
mg/kg wet
0.05000
108
76-134
cis-1,3-Dichloropropylene
0.0590
0.0050
mg/kg wet
0.05000
118
71-125
Dibromochloromethane
0.0474
0.0050
mg/kg wet
0.05000
95
73-122
Dichlorodifluoromethane
0.0366
0.010
mg/kg wet
0.05000
73
26-146
Ethylbenzene
0.0514
0.0050
mg/kg wet
0.05000
103
74-128
Isopropyl Ether
0.0570
0.0050
mg/kg wet
0.05000
114
59-159
Isopropylbenzene (Cumene)
0.0497
0.0050
mg/kg wet
0.05000
99
68-126
m,p-Xylenes
0.104
0.010
mg/kg wet
0.1000
104
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0427
0.020
mg/kg wet
0.05000
85
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0373
0.020
mg/kg wet
0.05000
75
63-149
Methyl Isobutyl Ketone
0.0496
0.020
mg/kg wet
0.05000
99
57-162
Methylene Chloride
0.0545
0.0050
mg/kg wet
0.05000
109
74-129
Methyl-tert-Butyl Ether
0.0566
0.0050
mg/kg wet
0.05000
113
70-130
Naphthalene
0.0437
0.010
mg/kg wet
0.05000
87
57-157
n-Butylbenzene
0.0500
0.0050
mg/kg wet
0.05000
100
65-135
n-Propylbenzene
0.0485
0.0050
mg/kg wet
0.05000
97
67-130
o-Xylene
0.0515
0.0050
mg/kg wet
0.05000
103
74-126
sec-Butylbenzene
0.0489
0.0050
mg/kg wet
0.05000
98
66-131
Styrene
0.0528
0.0050
mg/kg wet
0.05000
106
77-121
tert-Butyl benzene
0.0486
0.0050
mg/kg wet
0.05000
97
67-132
Tetrachloroethylene
0.0556
0.0050
mg/kg wet
0.05000
ill
68-130
Toluene
0.0561
0.0050
mg/kg wet
0.05000
112
71-129
trans- 1,2-Dichloroethylene
0.0570
0.0050
mg/kg wet
0.05000
114
73-132
trans- 1,3-Dichloropropylene
0.0576
0.0050
mg/kg wet
0.05000
115
68-123
Trichloroethylene
0.0548
0.0050
mg/kg wet
0.05000
110
75-133
Trichlorofluoromethane
0.0471
0.010
mg/kg wet
0.05000
94
44-146
Vinyl acetate
0.0492
0.010
mg/kg wet
0.05000
98
85-161
Vinyl chloride
0.0519
0.010
mg/kg wet
0.05000
104
48-147
Xylenes, total
0.156
0.015
mg/kg wet
0.1500
104
74-126
Surrogate:4-Bromofluorobenzene
49.0
ug/L
50.00
98
70-130
Surrogate: Dibromofluoromethane
47.9
ug/L
50.00
96
84-123
Surrogate: Toluene-d8
43.3
ug/L
50.00
87
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0231 - 5035
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POA0231-BLK1)
Prepared &Analyzed: 01/16/20
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0231 - 5035
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POA0231-BLK1)
Prepared & Analyzed: 01/16/20
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
49.1
ug/L
50.00
98
70-130
Surrogate: Dibromofluoromethane
52.3
ug/L
50.00
105
84-123
Surrogate: Toluene-d8
41.8
ug/L
50.00
84
76-129
LCS (POA0231-BSI)
Prepared &Analyzed:
01/16/20
1,1,1,2-Tetrachloroethane
0.0448
0.0050
mg/kg wet
0.05000
90
72-115
1, 1,1 -Trichloroethane
0.0528
0.0050
mg/kg wet
0.05000
106
67-131
1,1,2,2-Tetrachloroethane
0.0428
0.0050
mg/kg wet
0.05000
86
56-126
1,1,2-Trichloroethane
0.0464
0.0050
mg/kg wet
0.05000
93
70-133
1,1-Dichloroethane
0.0547
0.0050
mg/kg wet
0.05000
109
74-127
1,1-Dichloroethylene
0.0524
0.0050
mg/kg wet
0.05000
105
67-149
1, 1 -Dichloropropylene
0.0543
0.0050
mg/kg wet
0.05000
109
71-130
1,2,3-Trichlorobenzene
0.0404
0.010
mg/kg wet
0.05000
81
68-130
1,2,3-Trichloropropane
0.0432
0.0050
mg/kg wet
0.05000
86
60-137
1,2,4-Trichlorobenzene
0.0404
0.010
mg/kg wet
0.05000
81
66-125
1,2,4-Trimethylbenzene
0.0406
0.0050
mg/kg wet
0.05000
81
69-129
1,2-Dibromoethane
0.0469
0.0050
mg/kg wet
0.05000
94
70-132
1,2-Dichlorobenzene
0.0393
0.0050
mg/kg wet
0.05000
79
72-123
1,2-Dichloroethane
0.0524
0.0050
mg/kg wet
0.05000
105
68-128
1,2-Dichloropropane
0.0544
0.0050
mg/kg wet
0.05000
109
73-130
1,3,5-Trimethylbenzene
0.0409
0.0050
mg/kg wet
0.05000
82
69-128
1,3-Dichlorobenzene
0.0389
0.0050
mg/kg wet
0.05000
78
71-120
1,3-Dichloropropane
0.0478
0.0050
mg/kg wet
0.05000
96
75-124
1,4-Dichlorobenzene
0.0388
0.0050
mg/kg wet
0.05000
78
71-123
2,2-Dichloropropane
0.0526
0.0050
mg/kg wet
0.05000
105
50-142
2-Chlorotoluene
0.0401
0.0050
mg/kg wet
0.05000
80
67-124
4-Chlorotoluene
0.0407
0.0050
mg/kg wet
0.05000
81
71-126
4-Isopropyltoluene
0.0411
0.0050
mg/kg wet
0.05000
82
68-129
Acetone
0.121
0.020
mg/kg wet
0.1000
121
29-198
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0231 - 5035
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (POA0231-BS1)
Prepared &Analyzed: 01/16/20
Benzene
0.0540
0.0050
mg/kg wet
0.05000
108
74-127
Bromobenzene
0.0410
0.0050
mg/kg wet
0.05000
82
73-125
Bromochloromethane
0.0516
0.0050
mg/kg wet
0.05000
103
72-134
Bromodichloromethane
0.0536
0.0050
mg/kg wet
0.05000
107
75-122
Bromoform
0.0478
0.0050
mg/kg wet
0.05000
96
66-135
Bromomethane
0.0433
0.010
mg/kg wet
0.05000
87
20-180
Carbon Tetrachloride
0.0512
0.0050
mg/kg wet
0.05000
102
64-143
Chlorobenzene
0.0442
0.0050
mg/kg wet
0.05000
88
74-118
Chloroethane
0.0483
0.010
mg/kg wet
0.05000
97
33-149
Chloroform
0.0541
0.0050
mg/kg wet
0.05000
108
73-127
Chloromethane
0.0505
0.010
mg/kg wet
0.05000
101
45-143
cis-1,2-Dichloroethylene
0.0523
0.0050
mg/kg wet
0.05000
105
76-134
cis-1,3-Dichloropropylene
0.0568
0.0050
mg/kg wet
0.05000
114
71-125
Dibromochloromethane
0.0460
0.0050
mg/kg wet
0.05000
92
73-122
Dichlorodifluoromethane
0.0487
0.010
mg/kg wet
0.05000
97
26-146
Ethylbenzene
0.0466
0.0050
mg/kg wet
0.05000
93
74-128
Isopropyl Ether
0.0532
0.0050
mg/kg wet
0.05000
106
59-159
Isopropylbenzene (Cumene)
0.0425
0.0050
mg/kg wet
0.05000
85
68-126
m,p-Xylenes
0.0961
0.010
mg/kg wet
0.1000
96
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0586
0.020
mg/kg wet
0.05000
117
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0607
0.020
mg/kg wet
0.05000
121
63-149
Methyl Isobutyl Ketone
0.0638
0.020
mg/kg wet
0.05000
128
57-162
Methylene Chloride
0.0516
0.0050
mg/kg wet
0.05000
103
74-129
Methyl-tert-Butyl Ether
0.0560
0.0050
mg/kg wet
0.05000
112
70-130
Naphthalene
0.0447
0.010
mg/kg wet
0.05000
89
57-157
n-Butylbenzene
0.0420
0.0050
mg/kg wet
0.05000
84
65-135
n-Propylbenzene
0.0411
0.0050
mg/kg wet
0.05000
82
67-130
o-Xylene
0.0480
0.0050
mg/kg wet
0.05000
96
74-126
sec-Butylbenzene
0.0413
0.0050
mg/kg wet
0.05000
83
66-131
Styrene
0.0497
0.0050
mg/kg wet
0.05000
99
77-121
tert-Butyl benzene
0.0404
0.0050
mg/kg wet
0.05000
81
67-132
Tetrachloroethylene
0.0518
0.0050
mg/kg wet
0.05000
104
68-130
Toluene
0.0532
0.0050
mg/kg wet
0.05000
106
71-129
trans- 1,2-Dichloroethylene
0.0528
0.0050
mg/kg wet
0.05000
106
73-132
trans- 1,3-Dichloropropylene
0.0574
0.0050
mg/kg wet
0.05000
115
68-123
Trichloroethylene
0.0527
0.0050
mg/kg wet
0.05000
105
75-133
Trichlorofluoromethane
0.0472
0.010
mg/kg wet
0.05000
94
44-146
Vinyl acetate
0.0498
0.010
mg/kg wet
0.05000
100
85-161
Vinyl chloride
0.0557
0.010
mg/kg wet
0.05000
ill
48-147
Xylenes, total
0.144
0.015
mg/kg wet
0.1500
96
74-126
Surrogate:4-Bromofluorobenzene
48.4
ug/L
50.00
97
70-130
Surrogate: Dibromofluoromethane
46.8
ug/L
50.00
94
84-123
Surrogate: Toluene-d8
42.5
ug/L
50.00
85
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POA0191 - 3546
Blank (POA01 91 -BLK1)
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methyl naphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methyl naphthalene
2-Methylphenol
2-Nitrophenol
3,3'-Dichlorobenzidine
3/4-Methyl phenol
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-C h loro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
B is(2-Chloroethyl )ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
1.5 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
1.5 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
1.0 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
2.0 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
Prepared:01/14/20 Analyzed: 01/15/20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0191 - 3546
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POA01 91 -BLK1)
Prepared: 01/14/20 Analyzed: 01/15/20
Di-n-butyl phthalate
BRL
0.66
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.66
mg/kg wet
Fluorene
BRL
0.66
mg/kg wet
Hexachlorobenzene
BRL
0.66
mg/kg wet
Hexachlorobutadiene
BRL
0.66
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.66
mg/kg wet
Hexachloroethane
BRL
0.66
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.66
mg/kg wet
Isophorone
BRL
0.66
mg/kg wet
Naphthalene
BRL
0.66
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.66
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.66
mg/kg wet
Pentachlorophenol
BRL
1.0
mg/kg wet
Phenanthrene
BRL
0.66
mg/kg wet
Phenol
BRL
0.66
mg/kg wet
Pyrene
BRL
0.66
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
3.33
mg/kg wet
3.326
100
39-132
Surrogate: 2-Fluorobiphenyl
1.49
mg/kg wet
1.663
90
44-115
Surrogate: 2-Fluorophenol
3.05
mg/kg wet
3.326
92
35-115
Surrogate: Nitrobenzene-d5
1.37
mg/kg wet
1.663
82
37-122
Surrogate: Phenol-d5
2.89
mg/kg wet
3.326
87
34-121
Surrogate: Terphenyl-d14
1.63
mg/kg wet
1.663
98
54-127
LCS (POA0191-BS1)
Prepared: 01/14/20 Analyzed: 01/15/20
1,2,4-Trichlorobenzene
1.11
0.66
mg/kg wet
1.663
67
34-118
1,2-Dichlorobenzene
1.09
0.66
mg/kg wet
1.663
66
33-117
1,3-Dichlorobenzene
1.07
0.66
mg/kg wet
1.663
64
30-115
1,4-Dichlorobenzene
1.07
0.33
mg/kg wet
1.663
64
31-115
1-Methyl naphthalene
1.27
0.66
mg/kg wet
1.663
77
40-119
2,4,5-Trichlorophenol
1.47
0.66
mg/kg wet
1.663
88
62-124
2,4,6-Trichlorophenol
1.50
0.66
mg/kg wet
1.663
90
39-126
2,4-Dichlorophenol
1.24
0.66
mg/kg wet
1.663
75
40-122
2,4-Dimethylphenol
1.42
0.33
mg/kg wet
1.663
86
30-127
2,4-Dinitrophenol
1.64
1.5
mg/kg wet
1.663
99
27-129
2,4-Dinitrotoluene
1.53
0.66
mg/kg wet
1.663
92
48-126
2,6-Dinitrotoluene
1.53
0.66
mg/kg wet
1.663
92
46-124
2-Chloronaphthalene
1.38
0.66
mg/kg wet
1.663
83
41-114
2-Chlorophenol
1.25
0.66
mg/kg wet
1.663
75
34-121
2-Methyl naphthalene
1.21
0.66
mg/kg wet
1.663
73
38-122
2-Methylphenol
1.32
0.66
mg/kg wet
1.663
79
32-122
2-Nitrophenol
1.14
0.66
mg/kg wet
1.663
69
36-123
3,3'-Dichlorobenzidine
1.60
0.66
mg/kg wet
1.663
96
22-121
3/4-Methyl phenol
1.22
0.66
mg/kg wet
1.663
74
34-119
4,6-Dinitro-2-methylphenol
1.71
1.5
mg/kg wet
1.663
103
29-132
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0191 - 3546
LCS (POA0191-BSI)
4-Bromophenyl phenyl ether
4-C h loro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,hJ)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
B is(2-Ch loroethyl )ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Dibenzo(a, h )anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-N itroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Surrogate: 2, 4, 6-Tribromophenol
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Prepared:01/14/20 Analyzed: 01/15/20
1.47
0.66
mg/kg wet
1.663
89
46-124
1.33
0.66
mg/kg wet
1.663
80
45-122
1.08
0.33
mg/kg wet
1.663
65
17-106
1.38
1.0
mg/kg wet
1.663
83
45-121
1.63
0.66
mg/kg wet
1.663
98
30-132
1.53
0.66
mg/kg wet
1.663
92
40-123
1.55
0.66
mg/kg wet
1.663
93
32-132
1.56
0.66
mg/kg wet
1.663
94
47-123
1.59
0.66
mg/kg wet
1.663
96
39-125
1.50
0.66
mg/kg wet
1.663
90
49-126
1.64
0.66
mg/kg wet
1.663
99
45-129
1.59
0.66
mg/kg wet
1.663
96
45-132
1.65
0.66
mg/kg wet
1.663
99
43-134
1.61
0.66
mg/kg wet
1.663
97
47-132
0.879
2.0
mg/kg wet
1.663
53
10-83
1.33
0.66
mg/kg wet
1.663
80
29-122
1.10
0.66
mg/kg wet
1.663
66
36-121
1.03
0.66
mg/kg wet
1.663
62
31-120
1.02
0.33
mg/kg wet
1.663
62
33-131
1.60
0.66
mg/kg wet
1.663
96
51-133
1.57
0.33
mg/kg wet
1.663
94
48-132
1.55
0.66
mg/kg wet
1.663
93
50-124
0.938
0.66
mg/kg wet
1.663
56
45-134
1.42
0.66
mg/kg wet
1.663
86
44-120
1.47
0.66
mg/kg wet
1.663
88
50-124
1.46
0.66
mg/kg wet
1.663
88
48-124
1.62
0.66
mg/kg wet
1.663
97
51-128
1.62
0.33
mg/kg wet
1.663
98
45-140
1.59
0.66
mg/kg wet
1.663
96
50-127
1.48
0.66
mg/kg wet
1.663
89
43-125
1.44
0.66
mg/kg wet
1.663
87
45-122
1.13
0.66
mg/kg wet
1.663
68
32-123
0.810
0.66
mg/kg wet
1.663
49
32-117
1.00
0.66
mg/kg wet
1.663
60
28-117
1.56
0.66
mg/kg wet
1.663
94
45-133
0.975
0.66
mg/kg wet
1.663
59
30-122
1.11
0.66
mg/kg wet
1.663
67
35-123
1.01
0.33
mg/kg wet
1.663
61
34-122
1.26
0.66
mg/kg wet
1.663
76
36-120
1.88
0.66
mg/kg wet
1.663
113
38-127
2.01
1.0
mg/kg wet
1.663
121
25-133
1.53
0.66
mg/kg wet
1.663
92
50-121
1.27
0.66
mg/kg wet
1.663
76
34-121
1.64
0.66
mg/kg wet
1.663
98
47-127
0.772
0.33
mg/kg wet
1.663
46
10-60
3.02
mg/kg wet
3.326
91
39-132
J
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0191 - 3546
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (POA0191-BSI)
Prepared: 01/14/20 Analyzed: 01/15/20
Surrogate: 2-Fluorobiphenyl
1.29
mg/kg wet
1.663 78 44-115
Surrogate: 2-Fluorophenol
2.48
mg/kg wet
3.326 75 35-115
Surrogate: Nitrobenzene-d5
1.02
mg/kg wet
1.663 61 37-122
Surrogate: Phenol-d5
2.43
mg/kg wet
3.326 73 34-121
Surrogate: Terphenyl-d14
1.45
mg/kg wet
1.663 87 54-127
Batch POA0221 - 3546
Blank (POA0221-BLK1)
Prepared: 01/15/20 Analyzed: 01/16/20
1,2,4-Trichlorobenzene
BRL
0.66
mg/kg wet
1,2-Dichlorobenzene
BRL
0.66
mg/kg wet
1,3-Dichlorobenzene
BRL
0.66
mg/kg wet
1,4-Dichlorobenzene
BRL
0.33
mg/kg wet
1-Methyl naphthalene
BRL
0.66
mg/kg wet
2,4,5-Trichlorophenol
BRL
0.66
mg/kg wet
2,4,6-Trichlorophenol
BRL
0.66
mg/kg wet
2,4-Dichlorophenol
BRL
0.66
mg/kg wet
2,4-Dimethylphenol
BRL
0.33
mg/kg wet
2,4-Dinitrophenol
BRL
1.5
mg/kg wet
2,4-Dinitrotoluene
BRL
0.66
mg/kg wet
2,6-Dinitrotoluene
BRL
0.66
mg/kg wet
2-Chloronaphthalene
BRL
0.66
mg/kg wet
2-Chlorophenol
BRL
0.66
mg/kg wet
2-Methyl naphthalene
BRL
0.66
mg/kg wet
2-Methylphenol
BRL
0.66
mg/kg wet
2-Nitrophenol
BRL
0.66
mg/kg wet
3,3'-Dichlorobenzidine
BRL
0.66
mg/kg wet
3/4-Methyl phenol
BRL
0.66
mg/kg wet
4,6-Dinitro-2-methylphenol
BRL
1.5
mg/kg wet
4-Bromophenyl phenyl ether
BRL
0.66
mg/kg wet
4-Chloro-3-methylphenol
BRL
0.66
mg/kg wet
4-Chloroaniline
BRL
0.33
mg/kg wet
4-Chlorophenyl phenyl ether
BRL
1.0
mg/kg wet
4-Nitrophenol
BRL
0.66
mg/kg wet
Acenaphthene
BRL
0.66
mg/kg wet
Acenaphthylene
BRL
0.66
mg/kg wet
Anthracene
BRL
0.66
mg/kg wet
Azobenzene
BRL
0.66
mg/kg wet
Benzo(a)anthracene
BRL
0.66
mg/kg wet
Benzo(a)pyrene
BRL
0.66
mg/kg wet
Benzo(b)fluoranthene
BRL
0.66
mg/kg wet
Benzo(g,h,i)perylene
BRL
0.66
mg/kg wet
Benzo(k)fluoranthene
BRL
0.66
mg/kg wet
Benzoic Acid
BRL
2.0
mg/kg wet
Benzyl alcohol
BRL
0.66
mg/kg wet
bis(2-Chloroethoxy)methane
BRL
0.66
mg/kg wet
Bis(2-Chloroethyl)ether
BRL
0.66
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POA0221 - 3546
Blank (POA0221-BLK1)
Prepared: 01/15/20 Analyzed: 01/16/20
Bis(2-chloroisopropyl)ether
BRL
0.33
mg/kg wet
Bis(2-Ethylhexyl)phthalate
BRL
0.66
mg/kg wet
Butyl benzyl phthalate
BRL
0.33
mg/kg wet
Chrysene
BRL
0.66
mg/kg wet
Dibenzo(a,h)anthracene
BRL
0.66
mg/kg wet
Dibenzofuran
BRL
0.66
mg/kg wet
Diethyl phthalate
BRL
0.66
mg/kg wet
Dimethyl phthalate
BRL
0.66
mg/kg wet
Di-n-butyl phthalate
BRL
0.66
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.66
mg/kg wet
Fluorene
BRL
0.66
mg/kg wet
Hexachlorobenzene
BRL
0.66
mg/kg wet
Hexachlorobutadiene
BRL
0.66
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.66
mg/kg wet
Hexachloroethane
BRL
0.66
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.66
mg/kg wet
Isophorone
BRL
0.66
mg/kg wet
Naphthalene
BRL
0.66
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.66
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.66
mg/kg wet
Pentachlorophenol
BRL
1.0
mg/kg wet
Phenanthrene
BRL
0.66
mg/kg wet
Phenol
BRL
0.66
mg/kg wet
Pyrene
BRL
0.66
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
3.90
mg/kg wet
3.332
117
39-132
Surrogate: 2-Fluorobiphenyl
1.73
mg/kg wet
1.666
104
44-115
Surrogate: 2-Fluorophenol
3.44
mg/kg wet
3.332
103
35-115
Surrogate: Nitrobenzene-d5
1.59
mg/kg wet
1.666
96
37-122
Surrogate: Phenol-d5
3.37
mg/kg wet
3.332
101
34-121
Surrogate: Terphenyl-d14
1.70
mg/kg wet
1.666
102
54-127
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0221 - 3546
LCS (POA0221-BSI)
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methyl naphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methyl naphthalene
2-Methylphenol
2-Nitrophenol
3,3'-Dichlorobenzidine
3/4-Methyl phenol
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-C h loro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
B is(2-Chloroethyl )ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Prepared:01/15/20 Analyzed: 01/16/20
1.30
0.66
mg/kg wet
1.662
78
34-118
1.32
0.66
mg/kg wet
1.662
79
33-117
1.30
0.66
mg/kg wet
1.662
78
30-115
1.29
0.33
mg/kg wet
1.662
77
31-115
1.46
0.66
mg/kg wet
1.662
88
40-119
1.61
0.66
mg/kg wet
1.662
97
62-124
1.69
0.66
mg/kg wet
1.662
102
39-126
1.42
0.66
mg/kg wet
1.662
85
40-122
1.62
0.33
mg/kg wet
1.662
98
30-127
1.47
1.5
mg/kg wet
1.662
89
27-129
1.69
0.66
mg/kg wet
1.662
102
48-126
1.67
0.66
mg/kg wet
1.662
101
46-124
1.51
0.66
mg/kg wet
1.662
91
41-114
1.52
0.66
mg/kg wet
1.662
91
34-121
1.38
0.66
mg/kg wet
1.662
83
38-122
1.59
0.66
mg/kg wet
1.662
96
32-122
1.39
0.66
mg/kg wet
1.662
84
36-123
1.54
0.66
mg/kg wet
1.662
93
22-121
1.45
0.66
mg/kg wet
1.662
87
34-119
1.77
1.5
mg/kg wet
1.662
106
29-132
1.63
0.66
mg/kg wet
1.662
98
46-124
1.47
0.66
mg/kg wet
1.662
89
45-122
1.20
0.33
mg/kg wet
1.662
72
17-106
1.53
1.0
mg/kg wet
1.662
92
45-121
1.86
0.66
mg/kg wet
1.662
112
30-132
1.66
0.66
mg/kg wet
1.662
100
40-123
1.68
0.66
mg/kg wet
1.662
101
32-132
1.68
0.66
mg/kg wet
1.662
101
47-123
1.70
0.66
mg/kg wet
1.662
103
39-125
1.54
0.66
mg/kg wet
1.662
93
49-126
1.71
0.66
mg/kg wet
1.662
103
45-129
1.71
0.66
mg/kg wet
1.662
103
45-132
1.66
0.66
mg/kg wet
1.662
100
43-134
1.61
0.66
mg/kg wet
1.662
97
47-132
0.926
2.0
mg/kg wet
1.662
56
10-83
1.48
0.66
mg/kg wet
1.662
89
29-122
1.27
0.66
mg/kg wet
1.662
77
36-121
1.35
0.66
mg/kg wet
1.662
81
31-120
1.30
0.33
mg/kg wet
1.662
78
33-131
1.65
0.66
mg/kg wet
1.662
99
51-133
1.61
0.33
mg/kg wet
1.662
97
48-132
1.61
0.66
mg/kg wet
1.662
97
50-124
1.22
0.66
mg/kg wet
1.662
73
45-134
1.55
0.66
mg/kg wet
1.662
93
44-120
1.53
0.66
mg/kg wet
1.662
92
50-124
1.51
0.66
mg/kg wet
1.662
91
48-124
J
J
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0221 - 3546
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (POA0221-BSI)
Prepared: 01/15/20 Analyzed: 01/16/20
Di-n-butyl phthalate
1.69
0.66
mg/kg wet
1.662
102
51-128
Di-n-octyl phthalate
1.70
0.33
mg/kg wet
1.662
102
45-140
Fluoranthene
1.64
0.66
mg/kg wet
1.662
99
50-127
Fluorene
1.60
0.66
mg/kg wet
1.662
96
43-125
Hexachlorobenzene
1.59
0.66
mg/kg wet
1.662
96
45-122
Hexachlorobutadiene
1.34
0.66
mg/kg wet
1.662
81
32-123
Hexachlorocyclopentadiene
1.45
0.66
mg/kg wet
1.662
88
32-117
Hexachloroethane
1.23
0.66
mg/kg wet
1.662
74
28-117
Indeno(1,2,3-cd)pyrene
1.54
0.66
mg/kg wet
1.662
93
45-133
Isophorone
1.10
0.66
mg/kg wet
1.662
66
30-122
Naphthalene
1.29
0.66
mg/kg wet
1.662
78
35-123
Nitrobenzene
1.19
0.33
mg/kg wet
1.662
71
34-122
N-Nitroso-di-n-propylamine
1.50
0.66
mg/kg wet
1.662
90
36-120
N-Nitrosodiphenylamine
2.01
0.66
mg/kg wet
1.662
121
38-127
Pentachlorophenol
2.00
1.0
mg/kg wet
1.662
120
25-133
Phenanthrene
1.64
0.66
mg/kg wet
1.662
99
50-121
Phenol
1.52
0.66
mg/kg wet
1.662
92
34-121
Pyrene
1.68
0.66
mg/kg wet
1.662
101
47-127
Pyridine
0.908
0.33
mg/kg wet
1.662
55
10-60
Surrogate: 2,4,6-Tribromophenol
3.50
mg/kg wet
3.323
105
39-132
Surrogate: 2-Fluorobiphenyl
1.45
mg/kg wet
1.662
88
44-115
Surrogate: 2-Fluorophenol
3.02
mg/kg wet
3.323
91
35-115
Surrogate: Nitrobenzene-d5
1.23
mg/kg wet
1.662
74
37-122
Surrogate: Phenol-d5
2.90
mg/kg wet
3.323
87
34-121
Surrogate: Terphenyl-d14
1.52
mg/kg wet
1.662
92
54-127
Matrix Spike (POA0221-MS1)
Source: 0010154-13
Prepared:
01/15/20
Analyzed: 01/16/20
1,2,4-Trichlorobenzene
1.40
0.75
mg/kg dry
1.902
BRL
74
34-118
1,2-Dichlorobenzene
1.41
0.75
mg/kg dry
1.902
BRL
74
33-117
1,3-Dichlorobenzene
1.37
0.75
mg/kg dry
1.902
BRL
72
30-115
1,4-Dichlorobenzene
1.34
0.38
mg/kg dry
1.902
BRL
70
31-115
1-Methyl naphthalene
1.56
0.75
mg/kg dry
1.902
BRL
82
40-119
2,4,5-Trichlorophenol
1.69
0.75
mg/kg dry
1.902
BRL
89
45-121
2,4,6-Trichlorophenol
1.61
0.75
mg/kg dry
1.902
BRL
84
39-126
2,4-Dichlorophenol
1.43
0.75
mg/kg dry
1.902
BRL
75
40-122
2,4-Dimethylphenol
0.843
0.38
mg/kg dry
1.902
BRL
44
30-127
2,4-Dinitrophenol
1.37
1.7
mg/kg dry
1.902
BRL
72
27-129 J
2,4-Dinitrotoluene
1.75
0.75
mg/kg dry
1.902
BRL
92
48-126
2,6-Dinitrotoluene
1.75
0.75
mg/kg dry
1.902
BRL
92
46-124
2-Chloronaphthalene
1.60
0.75
mg/kg dry
1.902
BRL
84
41-114
2-Chlorophenol
1.54
0.75
mg/kg dry
1.902
BRL
81
34-121
2-Methyl naphthalene
1.48
0.75
mg/kg dry
1.902
BRL
78
38-122
2-Methylphenol
1.39
0.75
mg/kg dry
1.902
BRL
73
32-122
2-Nitrophenol
1.48
0.75
mg/kg dry
1.902
BRL
78
36-123
3,3'-Dichlorobenzidine
0.841
0.75
mg/kg dry
1.902
BRL
44
22-121
3/4-Methyl phenol
1.32
0.75
mg/kg dry
1.902
BRL
69
34-119
4,6-Dinitro-2-methylphenol
1.62
1.7
mg/kg dry
1.902
BRL
85
29-132 J
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0221 - 3546
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (POA0221-MS1)
Source: 0010154-13
Prepared: 01/15/20 Analyzed: 01/16/20
4-Bromophenyl phenyl ether
1.70
0.75
mg/kg dry
1.902
BRL
89
46-124
4-Chloro-3-methyl phenol
1.47
0.75
mg/kg dry
1.902
BRL
77
45-122
4-Chloroaniline
1.26
0.38
mg/kg dry
1.902
BRL
66
17-106
4-Chlorophenyl phenyl ether
1.59
1.1
mg/kg dry
1.902
BRL
84
45-121
4-Nitrophenol
1.97
0.75
mg/kg dry
1.902
BRL
103
30-132
Acenaphthene
1.75
0.75
mg/kg dry
1.902
BRL
92
40-123
Acenaphthylene
1.77
0.75
mg/kg dry
1.902
BRL
93
32-132
Anthracene
1.75
0.75
mg/kg dry
1.902
BRL
92
47-123
Azobenzene
1.76
0.75
mg/kg dry
1.902
BRL
92
39-125
Benzo(a)anthracene
1.60
0.75
mg/kg dry
1.902
BRL
84
49-126
Benzo(a)pyrene
1.79
0.75
mg/kg dry
1.902
BRL
94
45-129
Benzo(b)fluoranthene
1.72
0.75
mg/kg dry
1.902
BRL
91
45-132
Benzo(g,h,i)perylene
1.75
0.75
mg/kg dry
1.902
BRL
92
43-134
Benzo(k)fluoranthene
1.81
0.75
mg/kg dry
1.902
BRL
95
47-132
Benzoic Acid
0.725
2.3
mg/kg dry
1.902
BRL
38
10-83
Benzyl alcohol
1.54
0.75
mg/kg dry
1.902
BRL
81
29-122
bis(2-Chloroethoxy)methane
1.36
0.75
mg/kg dry
1.902
BRL
71
36-121
Bis(2-Chloroethyl)ether
1.47
0.75
mg/kg dry
1.902
BRL
77
31-120
Bis(2-chloroisopropyl)ether
1.34
0.38
mg/kg dry
1.902
BRL
71
33-131
Bis(2-Ethylhexyl)phthalate
1.73
0.75
mg/kg dry
1.902
BRL
91
51-133
Butyl benzyl phthalate
1.66
0.38
mg/kg dry
1.902
BRL
87
48-132
Chrysene
1.67
0.75
mg/kg dry
1.902
BRL
88
50-124
Dibenzo(a,h)anthracene
1.36
0.75
mg/kg dry
1.902
BRL
72
45-134
Dibenzofuran
1.63
0.75
mg/kg dry
1.902
BRL
86
44-120
Diethyl phthalate
1.62
0.75
mg/kg dry
1.902
BRL
85
50-124
Dimethyl phthalate
1.58
0.75
mg/kg dry
1.902
BRL
83
48-124
Di-n-butyl phthalate
1.75
0.75
mg/kg dry
1.902
BRL
92
51-128
Di-n-octyl phthalate
1.80
0.38
mg/kg dry
1.902
BRL
95
45-140
Fluoranthene
1.72
0.75
mg/kg dry
1.902
BRL
90
50-127
Fluorene
1.69
0.75
mg/kg dry
1.902
BRL
89
43-125
Hexachlorobenzene
1.64
0.75
mg/kg dry
1.902
BRL
86
45-122
Hexachlorobutadiene
1.44
0.75
mg/kg dry
1.902
BRL
76
32-123
Hexachlorocyclopentadiene
1.55
0.75
mg/kg dry
1.902
BRL
82
32-117
Hexachloroethane
1.30
0.75
mg/kg dry
1.902
BRL
69
28-117
Indeno(1,2,3-cd)pyrene
1.67
0.75
mg/kg dry
1.902
BRL
88
45-133
Isophorone
1.16
0.75
mg/kg dry
1.902
BRL
61
30-122
Naphthalene
1.38
0.75
mg/kg dry
1.902
BRL
73
35-123
Nitrobenzene
1.26
0.38
mg/kg dry
1.902
BRL
66
34-122
N-Nitroso-di-n-propylamine
1.54
0.75
mg/kg dry
1.902
BRL
81
36-120
N-Nitrosodiphenylamine
1.85
0.75
mg/kg dry
1.902
BRL
97
38-127
Pentachlorophenol
1.65
1.1
mg/kg dry
1.902
BRL
87
25-133
Phenanthrene
1.70
0.75
mg/kg dry
1.902
BRL
89
50-121
Phenol
1.51
0.75
mg/kg dry
1.902
BRL
79
34-121
Pyrene
1.77
0.75
mg/kg dry
1.902
BRL
93
47-127
Pyridine
0.969
0.38
mg/kg dry
1.902
BRL
51
20-150
Surrogate: 2,4,6-Tiibromophenol
3.25
mg/kg dry
3.804
86
39-132
J
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0221 - 3546
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (POA0221-MS1)
Source: 0010154-13
Prepared: 01/15/20 Analyzed: 01/16/20
Surrogate: 2-Fluorobiphenyl
1.55 mg/kg dry
1.902
82
44-115
Surrogate: 2-Fluorophenol
2.99 mg/kg dry
3.804
79
35-115
Surrogate: Nitrobenzene-d5
1.34 mg/kg dry
1.902
70
37-122
Surrogate: Phenol-d5
2.96 mg/kg dry
3.804
78
34-121
Surrogate: Terphenyl-04
1.59 mg/kg dry
1.902
84
54-127
Matrix Spike Dup (POA0221-MSD1)
Source: 0010154-13
Prepared: 01/15/20 Analyzed: 01/16/20
1,2,4-Trichlorobenzene
1.37
0.75
mg/kg dry
1.906
BRL
72
34-118
2
20
1,2-Dichlorobenzene
1.38
0.75
mg/kg dry
1.906
BRL
72
33-117
2
20
1,3-Dichlorobenzene
1.32
0.75
mg/kg dry
1.906
BRL
69
30-115
3
20
1,4-Dichlorobenzene
1.32
0.38
mg/kg dry
1.906
BRL
69
31-115
2
20
1-Methyl naphthalene
1.52
0.75
mg/kg dry
1.906
BRL
80
40-119
2
20
2,4,5-Trichlorophenol
1.61
0.75
mg/kg dry
1.906
BRL
84
45-121
5
35
2,4,6-Trichlorophenol
1.52
0.75
mg/kg dry
1.906
BRL
80
39-126
6
20
2,4-Dichlorophenol
1.40
0.75
mg/kg dry
1.906
BRL
73
40-122
2
20
2,4-Dimethylphenol
0.772
0.38
mg/kg dry
1.906
BRL
40
30-127
9
20
2,4-Dinitrophenol
1.36
1.7
mg/kg dry
1.906
BRL
71
27-129
0.8
20 J
2,4-Dinitrotoluene
1.66
0.75
mg/kg dry
1.906
BRL
87
48-126
5
20
2,6-Dinitrotoluene
1.67
0.75
mg/kg dry
1.906
BRL
88
46-124
4
20
2-Chloronaphthalene
1.54
0.75
mg/kg dry
1.906
BRL
81
41-114
4
20
2-Chlorophenol
1.50
0.75
mg/kg dry
1.906
BRL
79
34-121
3
20
2-Methyl naphthalene
1.42
0.75
mg/kg dry
1.906
BRL
74
38-122
4
20
2-Methylphenol
1.33
0.75
mg/kg dry
1.906
BRL
70
32-122
4
20
2-Nitrophenol
1.39
0.75
mg/kg dry
1.906
BRL
73
36-123
6
20
3,3'-Dichlorobenzidine
0.794
0.75
mg/kg dry
1.906
BRL
42
22-121
6
20
3/4-Methyl phenol
1.26
0.75
mg/kg dry
1.906
BRL
66
34-119
5
20
4,6-Dinitro-2-methylphenol
1.61
1.7
mg/kg dry
1.906
BRL
85
29-132
0.3
20 J
4-Bromophenyl phenyl ether
1.58
0.75
mg/kg dry
1.906
BRL
83
46-124
7
20
4-Chloro-3-methylphenol
1.46
0.75
mg/kg dry
1.906
BRL
76
45-122
1
20
4-Chloroaniline
1.22
0.38
mg/kg dry
1.906
BRL
64
17-106
4
20
4-Chlorophenyl phenyl ether
1.54
1.1
mg/kg dry
1.906
BRL
81
45-121
3
20
4-Nitrophenol
1.91
0.75
mg/kg dry
1.906
BRL
100
30-132
3
20
Acenaphthene
1.68
0.75
mg/kg dry
1.906
BRL
88
40-123
4
20
Acenaphthylene
1.72
0.75
mg/kg dry
1.906
BRL
90
32-132
3
20
Anthracene
1.66
0.75
mg/kg dry
1.906
BRL
87
47-123
6
20
Azobenzene
1.67
0.75
mg/kg dry
1.906
BRL
88
39-125
5
20
Benzo(a)anthracene
1.55
0.75
mg/kg dry
1.906
BRL
81
49-126
3
20
Benzo(a)pyrene
1.74
0.75
mg/kg dry
1.906
BRL
91
45-129
3
20
Benzo(b)fluoranthene
1.65
0.75
mg/kg dry
1.906
BRL
86
45-132
5
20
Benzo(g,h,i)perylene
1.68
0.75
mg/kg dry
1.906
BRL
88
43-134
4
20
Benzo(k)fluoranthene
1.69
0.75
mg/kg dry
1.906
BRL
89
47-132
7
20
Benzoic Acid
0.870
2.3
mg/kg dry
1.906
BRL
46
10-83
18
20 J
Benzyl alcohol
1.52
0.75
mg/kg dry
1.906
BRL
80
29-122
1
20
bis(2-Chloroethoxy)methane
1.32
0.75
mg/kg dry
1.906
BRL
69
36-121
3
20
Bis(2-Chloroethyl)ether
1.36
0.75
mg/kg dry
1.906
BRL
71
31-120
8
20
Bis(2-chloroisopropyl)ether
1.31
0.38
mg/kg dry
1.906
BRL
69
33-131
2
20
Bis(2-Ethylhexyl)phthalate
1.65
0.75
mg/kg dry
1.906
BRL
86
51-133
5
20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch POA0221 - 3546
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (POA0221-MSD1)
Source: 0010154-13
Prepared: 01/15/20 Analyzed: 01/16/20
Butyl benzyl phthalate
1.61
0.38
mg/kg dry
1.906
BRL
84
48-132
Chrysene
1.61
0.75
mg/kg dry
1.906
BRL
85
50-124
Dibenzo(a,h)anthracene
1.23
0.75
mg/kg dry
1.906
BRL
65
45-134
Dibenzofuran
1.58
0.75
mg/kg dry
1.906
BRL
83
44-120
Diethyl phthalate
1.54
0.75
mg/kg dry
1.906
BRL
81
50-124
Dimethyl phthalate
1.50
0.75
mg/kg dry
1.906
BRL
79
48-124
Di-n-butyl phthalate
1.67
0.75
mg/kg dry
1.906
BRL
87
51-128
Di-n-octyl phthalate
1.72
0.38
mg/kg dry
1.906
BRL
90
45-140
Fluoranthene
1.65
0.75
mg/kg dry
1.906
BRL
87
50-127
Fluorene
1.62
0.75
mg/kg dry
1.906
BRL
85
43-125
Hexachlorobenzene
1.56
0.75
mg/kg dry
1.906
BRL
82
45-122
Hexachlorobutadiene
1.40
0.75
mg/kg dry
1.906
BRL
73
32-123
Hexachlorocyclopentadiene
1.50
0.75
mg/kg dry
1.906
BRL
79
32-117
Hexachloroethane
1.25
0.75
mg/kg dry
1.906
BRL
66
28-117
Indeno(1,2,3-cd)pyrene
1.56
0.75
mg/kg dry
1.906
BRL
82
45-133
Isophorone
1.12
0.75
mg/kg dry
1.906
BRL
59
30-122
Naphthalene
1.35
0.75
mg/kg dry
1.906
BRL
71
35-123
Nitrobenzene
1.22
0.38
mg/kg dry
1.906
BRL
64
34-122
N-Nitroso-di-n-propylamine
1.54
0.75
mg/kg dry
1.906
BRL
81
36-120
N-Nitrosodiphenylamine
1.69
0.75
mg/kg dry
1.906
BRL
89
38-127
Pentachlorophenol
1.59
1.1
mg/kg dry
1.906
BRL
84
25-133
Phenanthrene
1.62
0.75
mg/kg dry
1.906
BRL
85
50-121
Phenol
1.50
0.75
mg/kg dry
1.906
BRL
78
34-121
Pyrene
1.67
0.75
mg/kg dry
1.906
BRL
87
47-127
Pyridine
0.950
0.38
mg/kg dry
1.906
BRL
50
20-150
Surrogate: 2,4,6-Tribromophenol
2.97
mg/kg dry
3.813
78
39-132
Surrogate: 2-Fluorobiphenyl
1.49
mg/kg dry
1.906
78
44-115
Surrogate: 2-Fluorophenol
2.88
mg/kg dry
3.813
76
35-115
Surrogate: Nitrobenzene-d5
1.29
mg/kg dry
1.906
68
37-122
Surrogate: Phenol-d5
2.86
mg/kg dry
3.813
75
34-121
Surrogate: Terphenyl-04
1.53
mg/kg dry
1.906
80
54-127
3 20
4 20
10 20
3 20
5 20
5 20
5 20
5 20
4 20
4 20
5 20
3 20
3 20
4 20
6 20
4 20
2 20
3 20
0.3 20
9 20
4 20
5 20
0.9 20
6 20
2 60
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Total Metals - Quality Control
Analyte
Batch POA0162 - 3050B
Project: 400H
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (POA0162-BLK1)
Prepared: 01/13/20 Analyzed: 01/17/20
Arsenic
BRL
1.0
mg/kg wet
Barium
BRL
10
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Chromium
BRL
1.0
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Silver
BRL
0.50
mg/kg wet
LCS (POA0162-BSI)
Prepared: 01/13/20 Analyzed: 01/17/20
Arsenic
12.7
1.0
mg/kg wet
12.50 102 80-120
Barium
13.4
10
mg/kg wet
12.50 107 80-120
Cadmium
12.9
0.50
mg/kg wet
12.50 103 80-120
Chromium
13.3
1.0
mg/kg wet
12.50 106 80-120
Lead
12.9
1.0
mg/kg wet
12.50 103 80-120
Selenium
12.4
1.0
mg/kg wet
12.50 99 80-120
Silver
5.02
0.50
mg/kg wet
5.000 100 80-120
Matrix Spike (POA0162-MS1)
Source: 0010154-01
Prepared: 01/13/20 Analyzed: 01/17/20
Arsenic
13.3
1.3
mg/kg dry
16.15 1.58 72 75-125
M
Barium
98.7
13
mg/kg dry
16.15 71.0 172 75-125
MC
Cadmium
11.5
0.65
mg/kg dry
16.15 BRL 71 75-125
M
Chromium
25.5
1.3
mg/kg dry
16.15 10.5 93 75-125
Lead
24.8
1.3
mg/kg dry
16.15 14.8 62 75-125
M
Selenium
9.30
1.3
mg/kg dry
16.15 BRL 58 75-125
M
Silver
4.67
0.65
mg/kg dry
6.460 BRL 72 75-125
M
Matrix Spike Dup (POA0162-MSD1)
Source: 0010154-01
Prepared: 01/13/20 Analyzed: 01/17/20
Arsenic
13.3
1.3
mg/kg dry
16.15 1.58 73 75-125
0.5
20
M
Barium
101
13
mg/kg dry
16.15 71.0 187 75-125
2
20
MC
Cadmium
11.6
0.65
mg/kg dry
16.15 BRL 72 75-125
2
20
M
Chromium
25.3
1.3
mg/kg dry
16.15 10.5 92 75-125
1
20
Lead
22.8
1.3
mg/kg dry
16.15 14.8 49 75-125
8
20
M
Selenium
9.49
1.3
mg/kg dry
16.15 BRL 59 75-125
2
20
M
Silver
4.78
0.65
mg/kg dry
6.460 BRL 74 75-125
2
20
M
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

® 1/2s/2o
Level II QC Report
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H Work Order: 0010154
Attn: Katie Lippard Time Submitted: 1/10/2020 4:00:OOPM
409 Rogers View Court
Raleigh, NC 27610
Total Metals - Quality Control
Reporting
Spike
Source
%REC
RPD
Analyte
Result
Limit
Units
Level
Result
%REC
Limits RPD
Limit Notes
Batch POA0162 - 3050B
Post Spike (POA0162-PS1)
Source: 0010154-01
Prepared: 01/13/20 Analyzed: 01/17/20
Arsenic
0.429
mg/L
0.5001
0.0489
76
75-125
Barium
2.51
mg/L
0.5000
2.20
62
75-125
MC, PS
Cadmium
0.337
mg/L
0.5000
-0.00146
67
75-125
PS
Chromium
0.684
mg/L
0.5001
0.324
72
75-125
PS
Lead
0.778
mg/L
0.5001
0.459
64
75-125
PS
Selenium
0.296
mg/L
0.4999
-0.0592
59
75-125
PS
Silver
0.138
mg/L
0.2000
-0.0180
69
75-125
PS
Batch POA0181 - 3050B
Blank (POA01 81 -BLK1)
Prepared:
01/14/20 Analyzed:
01/18/20
Arsenic
BRL
1.0
mg/kg wet
Barium
BRL
10
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Chromium
BRL
1.0
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Silver
BRL
0.50
mg/kg wet
LCS (POA0181-BSI)
Prepared:
01/14/20
Analyzed:
01/18/20
Arsenic
12.6
1.0
mg/kg wet
12.50
101
80-120
Barium
13.4
10
mg/kg wet
12.50
107
80-120
Cadmium
12.9
0.50
mg/kg wet
12.50
103
80-120
Chromium
13.2
1.0
mg/kg wet
12.50
106
80-120
Lead
12.7
1.0
mg/kg wet
12.50
102
80-120
Selenium
12.2
1.0
mg/kg wet
12.50
98
80-120
Silver
5.10
0.50
mg/kg wet
5.000
102
80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Total Metals - Quality Control
Analyte
Batch POA0181 - 3050B
Project: 400H
Reporting
Result Limit Units
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (POA0181-MS1)
Source: 0010154-11
Prepared: 01/14/20 Analyzed: 01/18/20
Arsenic
14.1
1.3
mg/kg dry
15.82
1.23
81
75-125
Barium
38.5
13
mg/kg dry
15.82
19.3
122
75-125
Cadmium
13.2
0.63
mg/kg dry
15.82
BRL
83
75-125
Chromium
39.5
1.3
mg/kg dry
15.82
26.6
82
75-125
Lead
30.9
1.3
mg/kg dry
15.82
16.6
91
75-125
Selenium
10.8
1.3
mg/kg dry
15.82
BRL
69
75-125
M
Silver
5.32
0.63
mg/kg dry
6.328
BRL
84
75-125
Matrix Spike Dup (POA0181-MSD1)
Source: 0010154-11
Prepared:
01/14/20 Analyzed: 01/18/20
Arsenic
14.7
1.3
mg/kg dry
15.82
1.23
85
75-125
4
20
Barium
59.2
13
mg/kg dry
15.82
19.3
253
75-125
42
20
M
Cadmium
13.4
0.63
mg/kg dry
15.82
BRL
84
75-125
1
20
Chromium
38.9
1.3
mg/kg dry
15.82
26.6
78
75-125
2
20
Lead
33.5
1.3
mg/kg dry
15.82
16.6
107
75-125
8
20
Selenium
10.7
1.3
mg/kg dry
15.82
BRL
68
75-125
2
20
M
Silver
5.39
0.63
mg/kg dry
6.328
BRL
85
75-125
1
20
Post Spike (POA01 81 -PSI)
Source: 0010154-11
Prepared:
01/14/20 Analyzed: 01/18/20
Arsenic
0.435
mg/L
0.5001
0.0390
79
75-125
Barium
1.00
mg/L
0.5000
0.610
78
75-125
Cadmium
0.377
mg/L
0.5000
-0.00175
75
75-125
Chromium
1.21
mg/L
0.5001
0.841
73
75-125
PS
Lead
0.885
mg/L
0.5001
0.523
72
75-125
PS
Selenium
0.347
mg/L
0.4999
-0.0684
70
75-125
PS
Silver
0.146
mg/L
0.2000
-0.0202
73
75-125
PS
Batch POA0212 - 7471 B
Blank (POA0212-BLK1) Prepared: 01/15/20 Analyzed: 01/16/20
Mercury BRL 0.050 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh Project: 400H
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
Total Metals - Quality Control
Level II QC Report
1 /28/20
Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POA0212 - 7471 B
LCS (POA0212-BSI)
Mercury
Batch POA0214 - 7471 B
Prepared: 01/15/20 Analyzed: 01/16/20
0.419 0.050 mg/kg wet 0.4167 101 80-120
Blank (POA0214-BLK1) Prepared: 01/15/20 Analyzed: 01/16/20
Mercury BRL 0.050 mg/kg wet
LCS (POA0214-BSI) Prepared: 01/15/20 Analyzed: 01/16/20
Mercury 0.439 0.050 mg/kg wet 0.4167 105 80-120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Mid -Atlantic Associates, Inc. - Raleigh
Attn: Katie Lippard
409 Rogers View Court
Raleigh, NC 27610
General Chemistry Parameters - Quality Control
Analyte
Level II QC Report
1 /28/20
Project: 400H Work Order: 0010154
Time Submitted: 1/10/2020 4:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POA0227 - Solids, Dry Weight
Duplicate (POA0227-DUP1) Source: 0010154-12 Prepared &Analyzed: 01/16/20
% Solids 78.5 0.100 % by Weight 80.4 2 20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/Time
0010154-01
POA0227
30
g 30 g
01/16/20
7:45
0010154-02
POA0227
30
g 30 g
01/16/20
7:45
0010154-03
POA0227
30
g 30 g
01/16/20
7:45
0010154-04
POA0227
30
g 30 g
01/16/20
7:45
0010154-05
POA0227
30
g 30 g
01/16/20
7:45
0010154-06
POA0227
30
g 30 g
01/16/20
7:45
0010154-07
POA0227
30
g 30 g
01/16/20
7:45
0010154-08
POA0227
30
g 30 g
01/16/20
7:45
0010154-09
POA0227
30
g 30 g
01/16/20
7:45
0010154-10
POA0227
30
g 30 g
01/16/20
7:45
0010154-11
POA0227
30
g 30 g
01/16/20
7:45
0010154-12
POA0227
30
g 30 g
01/16/20
7:45
0010154-13
POA0227
30
g 30 g
01/16/20
7:45
0010154-14
POA0227
30
g 30 g
01/16/20
7:45
0010154-15
POA0227
30
g 30 g
01/16/20
7:45
0010154-16
POA0228
30
g 30 g
01/16/20
8:09
0010154-17
POA0228
30
g 30 g
01/16/20
8:09
0010154-18
POA0228
30
g 30 g
01/16/20
8:09
0010154-19
POA0228
30
g 30 g
01/16/20
8:09
0010154-20
POA0228
30
g 30 g
01/16/20
8:09
Prep Method: 3546
Lab Number Batch Initial Final Date/Time
0010154-01
POA0191
30.03
g 1 mL
01/14/20
11:45
0010154-02
POA0191
30.15
g 1 mL
01/14/20
11:45
0010154-03
POA0191
30.03
g 1 mL
01/14/20
11:45
0010154-04
POA0191
30.16
g 1 mL
01/14/20
11:45
0010154-05
POA0191
30.01
g 1 mL
01/14/20
11:45
0010154-06
POA0191
30.21
g 1 mL
01/14/20
11:45
0010154-07
POA0191
30.13
g 1 mL
01/14/20
11:45
0010154-08
POA0191
30.2
g 1 mL
01/14/20
11:45
0010154-09
POA0191
30.03
g 1 mL
01/14/20
11:45
0010154-10
POA0191
30.07
g 1 mL
01/14/20
11:45
0010154-11
POA0191
30.06
g 1 mL
01/14/20
11:45
0010154-12
POA0191
30.08
g 1 mL
01/14/20
11:45
0010154-13
POA0221
30.15
g 1 mL
01/15/20
15:00
0010154-14
POA0221
30.03
g 1 mL
01/15/20
15:00
0010154-15
POA0221
30
g 1 mL
01/15/20
15:00
0010154-16
POA0221
30.18
g 1 mL
01/15/20
15:00
0010154-17
POA0221
30.01
g 1 mL
01/15/20
15:00
0010154-18
POA0221
30.09
g 1 mL
01/15/20
15:00
0010154-19
POA0221
30.01
g 1 mL
01/15/20
15:00
0010154-20
POA0221
30.09
g 1 mL
01/15/20
15:00
Prep Method: 3050E
Lab Number Batch Initial Final Date/Time
0010154-01
POA0162
2
g 50 mL
01/13/20
9:13
0010154-02
POA0162
2
g 50 mL
01/13/20
9:13
0010154-03
POA0162
2
g 50 mL
01/13/20
9:13
0010154-03
POA0162
2
g 50 mL
01/13/20
9:13
0010154-04
POA0162
2
g 50 mL
01/13/20
9:13
0010154-05
POA0162
2
g 50 mL
01/13/20
9:13
0010154-06
POA0162
2
g 50 mL
01/13/20
9:13
0010154-07
POA0162
2
g 50 mL
01/13/20
9:13
0010154-08
POA0162
2
g 50 mL
01/13/20
9:13
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Date/Time
0010154-09
POA0162
2
g 50 mL
01/13/20
9:13
0010154-10
POA0162
2
g 50 mL
01/13/20
9:13
0010154-10
POA0162
2
g 50 mL
01/13/20
9:13
0010154-11
POA0181
2
g 50 mL
01/14/20
9:04
0010154-12
POA0181
2
g 50 mL
01/14/20
9:04
0010154-13
POA0181
2
g 50 mL
01/14/20
9:04
0010154-14
POA0181
2
g 50 mL
01/14/20
9:04
0010154-15
POA0181
2
g 50 mL
01/14/20
9:04
0010154-16
POA0181
2
g 50 mL
01/14/20
9:04
0010154-17
POA0181
2
g 50 mL
01/14/20
9:04
0010154-18
POA0181
2
g 50 mL
01/14/20
9:04
0010154-19
POA0181
2
g 50 mL
01/14/20
9:04
0010154-20
POA0181
2
g 50 mL
01/14/20
9:04
Prep Method: 7471E
Lab Number Batch Initial Final Date/Time
0010154-01
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-02
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-03
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-04
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-05
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-06
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-07
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-08
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-09
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-10
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-11
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-12
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-13
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-14
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-15
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-16
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-17
POA0212
0.6
g 50 mL
01/15/20 12:10
0010154-18
POA0214
0.6
g 50 mL
01/15/20 12:10
0010154-19
POA0214
0.6
g 50 mL
01/15/20 12:10
0010154-20
POA0214
0.6
g 50 mL
01/15/20 12:10
Prep Method: 5035
Lab Number
Batch
Initial
Final
Date/Time
0010154-01
POA0183
4.7
g 5 mL
01/14/20 10:23
0010154-02
POA0183
5.27
g 5 mL
01/14/20 10:23
0010154-03
POA0183
6.74
g 5 mL
01/14/20 10:23
0010154-04
POA0183
5.58
g 5 mL
01/14/20 10:23
0010154-05
POA0183
5.15
g 5 mL
01/14/20 10:23
0010154-06
POA0183
5.04
g 5 mL
01/14/20 10:23
0010154-07
POA0183
5.96
g 5 mL
01/14/20 10:23
0010154-08
POA0183
4.85
g 5 mL
01/14/20 10:23
0010154-09
POA0183
5.14
g 5 mL
01/14/20 10:23
0010154-10
POA0183
5.29
g 5 mL
01/14/20 10:23
0010154-11
POA0183
6.56
g 5 mL
01/14/20 10:23
0010154-12
POA0231
5.45
g 5 mL
01/16/20 9:48
0010154-13
POA0231
5.13
g 5 mL
01/16/20 9:48
0010154-14
POA0231
5.77
g 5 mL
01/16/20 9:48
0010154-15
POA0231
5.71
g 5 mL
01/16/20 9:48
0010154-16
POA0231
5.85
g 5 mL
01/16/20 9:48
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: 5035
Lab Number Batch Initial Final Date/Time
0010154-17
POA0231
5.27
g 5 mL
01/16/20
9:48
0010154-18
POA0231
5.77
g 5 mL
01/16/20
9:48
0010154-19
POA0231
4.26
g 5 mL
01/16/20
9:48
0010154-20
POA0231
3.82
g 5 mL
01/16/20
9:48
Subcontracted Analyses
The following analyses were subcontracted to ALS - Rochester, NY
Lab Number
Analysis
0010154-06
Hexavalent Chromium by 7199 (Sub)
0010154-09
Hexavalent Chromium by 7199 (Sub)
0010154-11
Hexavalent Chromium by 7199 (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

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A
January 27, 2020
Angela Overcash
Prism Laboratories, Inc.
P.O. Box 240543
Charlotte, NC 28224-0543
Laboratory Results for: 0010154
Dear Angela,
Service Request No:R2000593
Enclosed are the results of the sample(s) submitted to our laboratory January 22, 2020
For your reference, these analyses have been assigned our service request number R2000593.
All testing was performed according to our laboratory's quality assurance program and met the
requirements of the TNI standards except as noted in the case narrative report. Any testing not
included in the lab's accreditation is identified on a Non -Certified Analytes report. All results are
intended to be considered in their entirety. ALS Environmental is not responsible for use of less than
the complete report. Results apply only to the individual samples submitted to the lab for analysis, as
listed in the report. The measurement uncertainty of the results included in this report is within that
expected when using the prescribed method(s), and represented by Laboratory Control Sample
control limits. Any events, such as QC failures or Holding Time exceedances, which may add to the
uncertainty are explained in the report narrative or are flagged with qualifiers. The flags are explained
in the Report Qualifiers and Definitions page of this report.
Please contact me if you have any questions. My extension is 7475. You may also contact me via
email at [e-mail].
Respectfully submitted,
ALS Group USA, Corp. dba ALS Environmental
r
Meghan Pedro
Project Manager
ADDRESS 1565 Jefferson Road, Building 300. Suite 360, Rochester, NY 14623
PHIONE [phone] FAX [phone]
Ai.S Groin) USA. Coif;.
dba ALS Environmental
Page 1 of 28

AALS`--in'uironmental
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsgiobal.com
Page 2 of 28

1565 Jefferson Rd, Building 300, Rochester, NY 14623 1 585-288-5380 1 www.aisgiobal.com
AL5
Client:
Project:
Sample Matrix
Waypoint Analytical formerly Prism Laboratories, Inc.
0010154
Soil
CASE NARRATIVE
Service Request: R2000593
Date Received: 01/22/2020
All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains
analytical results for samples for the Tier II level requested by the client.
Sample Receivt:
Three soil samples were received for analysis at ALS Environmental on 01/22/2020. Any discrepancies upon initial sample
inspection are annotated on the sample receipt and preservation form included within this report. The samples were stored at
minimum in accordance with the analytical method requirements.
General Chemistry:
No significant anomalies were noted with this analysis.
60
Approved by
Date
01 /27/2020
Page 3 of 28

AALSEnuir©nmental
SAMPLE DETECTION SUMMARY
LIENT ID: B-4D Lab ID: R2000593-001
Analyte Results Flag MDL MRL Units Method
---------------------------- - - .. .... .....-
Chromium, Hexavalent 0.20 J 0.06 0.51 mg/Kg 7199
Chromium, Hexavalent
Total Solids
0.20 J 0.06 0.51 mg/Kg 7199
77.2 Percent ALS SOP
CLIENT ID: B-6S Lab ID: R2000593-002
Analyte Results Flag MDL MRL Units Method
.... .... ----- --------------------------------------------- ---- - -- ----
Total Solids 72.7 Percent ALS SOP
LIENT ID: B-7 Lab ID: R2000593-003
Analyte Results Flag MDL MRL Units Method
------------------- - ------ -- ----. ... ... .......-...-.. __... ----_.
Chromium, Hexavalent 0.16 J 0.06 0.50 mg/Kg 7199
Chromium, Hexavalent
Total Solids
0.16 J 0.06 0.50 mg/Kg 7199
80.5 Percent ALS SOP
Page 4 of 28

AEnWr®nmantal
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsgiobal.com
Page 5 of 28

Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Project: 0010154
SAMPLE CROSS-REFERENCE
SAMPLE # CLIENT SAMPLE ID
R2000593-001 B-4D
R2000593-002 B-6S
R2000593-003 B-7
Service Request:R2000593
DATE
1 /8/2020
1 /7/2020
1 /6/2020
TIME
1040
1125
1245
Page 6 of 28
Printed 1/27/2020 7:10:39 AM Sample Summary

R2000593 5 _
Pdtm Laboratories, Inc.
3 ~ fliil'llllllllllllllifllllllilfllilllllllilflllllil
WayRount-
A�fALYTICAI. 5
SUBCONTRACT ORDER v
Certification : *LAC_ USACE
Waypoint Analytical NC— ✓ SC_ Other
0010154 N/A
SENDING LABORATORY: RECEIVING LABORATORY:
Waypoint Analytical ALS - Rochester, NY
P. O. Box 240543 1565 Jefferson .Rd. Bldg 300, Ste 360
Charlotte, NC 28224-0543 Rochester, NY 14623
Phone: [phone] Phone :[phone]
Fax:[phone] Fax: -
Project Manager: Angela D. Overcash
Analysis Due Expires Laboratory ID Comments
Sample ID: 0010154-06 Solid Sampled:01108/20 10:40 LA
liccavalent Chromium by 7199 01/09/20 10:40
CanioinersSupplied: � 6Z C I n C --{o�—
Sample ID: 00 10 154-09 Solid Sampled:01/07/20 11:25
liexavalent Chromium by 7199 01/08/20 11:25
Containers Supplied.'
Sample Ill: 0010154-11 Solid slit,hted:01/06/20 12:45 �.
I-lexavalcnt Chromium by 7199 01/07/20 12:45
Containers Supplied:
�!
--),I ,,� 0
I V
lt64mscd 13s'
[l:nc
N, :c:rr r l
Bate
a
Rekasacl I'-�
I}i�l�
IZ� aii el i3�
3]!C
Released By
Date
Received 13,,
bate
Released 13v
Date
Received l3v
Dale
Page 7 of 28
Page ! of I

d �000593 5
Fnam Canaruerfra, tne.
oo:a�+al�r J j I )jI +I
ALS Cooler Receipt and Preservation Check Form � ��+1f111�1��11��1�1��IIJll11i��IllUllll11111�1
Project/CIient Folder Number
Cooler received vn �Zf) by: 11 , COURIER: ALS UPS F.f71; VELOCITY CLIENT
1
I Were Custody seals on outside of cooler?
Y
2
Custody papers properly completed (ink, signed)?
0 N
3
Did all bottles arrive in good condition (unbroken)?
N
4
Circlo: et I Dry lee Cei packs present?
11N
8. Temperature Readings
Sa
Perchlorate samples have required headspace?
N
5b
Did VOA vials, Alk,or Sulfide have sig* bubbles?
N A6
VY
Where did the blmles originate? ALSIIZOC:L
7
5oi1 VOA received as: Faulk Encore 5035set
-Time:—/_
ID: 'IR#7 R#1 From: Temp Blank 45 ple Bottle
Observed Temp ('C) /
Within 0-6'C? N Y N Y N Y N Y N Y N Y N
If meC, were samples frozen? Y N Y N_L Y N Y N Y N Y N Y N
If out of Temperature, note packinglice condition: Ice melted Poorly Packed (described below) Same Day Rule
&Client Approval to Run Samples: Standing Approval Client aware at drop-off Client notified by:_
All samples held in storage location: y? by on I .mat /D/p
Z
5035 samples placed in storage location: by on at
Cooler Breakdown/Preservation Check**: Dater O Ti
9. Were all bottle labels complete (i.e. analysis, res rvation, etc.)?
10. Did all bottle labels and tags agree with custody papers?
it. Were correct containers used for the tests indicated?
12. Were 5035 vials acceptable (no extra labels, not leaking)?
13: Air Samples: Cassettes / Tubes Intact with MS? Canisters Pr
pH I Lot of test I -Reagent I Preserved? I Lot Received
> 12
NaOH
<�
HNO�
HISO4
<4
NaHSO4
5-9
For 608pest
No=Noti fy for 3day
Residual
For CN,
If+, contact PM to add
Chlorine
Phenol, 625,
NatS2.03 (625, 609,
f-1
608oest. 522
CN), ascorbic (phenol).
ZnAcetate -
HCI ** **
Bottle lot numbers:
Explain all ❑iscrcpancteV Other Comments:
Labels secondary reviewed by:
PC Secondary Review:
P:Vtrl'RANET\QAQC\Forms ControlledlCooler Receipt r16 2 doc
�1}1 7
NO
NO
E
NO
YES
NO
prized Tedlar©
Inflated 1
Exp
'Sample ID
Vol.
Lot Added
Final
Adjusted I
Added
pH
**VOAs and 1664 Not to be tested before analysis.
Otherwise, all bottles orall samples with chemical preservatives
are checked [not lust representatiYes)
HPROD BULK
HTR FLDT
SUB HGFB
ALS LL3541
*significant air bubbles: VOA > 5-6 mm : WC>1 in. diameter
Page 8 of 28
111919

AALSEnuir®nmentae
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
Page 9 of 28

AlEnuironmental
REPORT QUALIFIERS AND DEFINITIONS
U Analyte was analyzed for but not detected.
The sample quantitation limit has been
corrected for dilution and for percent
moisture, unless otherwise noted in the case
narrative.
Estimated value due to either being a
Tentatively Identified Compound (TIC) or
that the concentration is between the MRL
and the MDL. Concentrations are not verified
within the linear range of the calibration. For
DoD: concentration >40% difference between
two GC columns (pesticides/Arclors).
B Analyte was also detected in the associated
method blank at a concentration that may
have contributed to the sample result.
E Inorganics- Concentration is estimated due to
the serial dilution was outside control limits.
E Organics- Concentration has exceeded the
calibration range for that specific analysis.
D Concentration is a result of a dilution,
typically a secondary analysis of the sample
due to exceeding the calibration range or that
a surrogate has been diluted out of the sample
and cannot be assessed.
* Indicates that a quality control parameter has
exceeded laboratory limits. Under the
Tlotes❑column of the Form 1, this qualifier
denotes analysis was performed out of
Holding Time.
+ Correlation coefficient for MSA is <0.995.
N Inorganics- Matrix spike recovery was outside
laboratory limits.
N Organics- Presumptive evidence of a compound
(reported as a TIC) based on the MS library search.
S Concentration has been determined using Method
of Standard Additions (MSA).
W Post -Digestion Spike recovery is outside control
limits and the sample absorbance is <50% of the
spike absorbance.
P Concentration >40% difference between the two
GC columns.
C Confirmed by GC/MS
Q DoD reports: indicates a pesti ci de/Aroclor is not
confirmed (El00% Difference between two GC
columns).
X See Case Narrative for discussion.
MRL Method Reporting Limit. Also known as:
LOQ Limit of Quantitation (LOQ)
The lowest concentration at which the method
analyte may be reliably quantified under the
method conditions.
MDL Method Detection Limit. A statistical value
derived from a study designed to provide the lowest
concentration that will be detected 99% of the
time. Values between the MDL and MRL are
estimated (see J qualifier).
H Analysis was performed out of hold time for LOD Limit of Detection. A value at or above the MDL
tests that have an Ctmmediate❑hold time which has been verified to be detectable.
criteria. ND Non -Detect. Analyte was not detected at the
# Spike was diluted out. concentration listed. Same as U qualifier.
,N ACCCAA
9 ,.
,4 �o,
U
Rochester Lab ID # for State Certifications'
Connecticut ID # PH0556
Maine ID #NY0032
Pennsylvania ID# 68-786
Delaware Approved
New Hampshire ID # 2941
Rhode Island ID # 158
DoD ELAP #65817
New York ID # 10145
Virginia 4460167
Florida ID # E87674
North Carolina #676
' Analyses were performed according to our laboratory-s NELAP-approved quality assurance program and any applicable state or agency
requirements. The test results meet requirements ofthe Current NELAP/TNI standards or state or agency requirements, where applicable, except as
noted in the case narrative. Since not all analyte/method/matrix combinations are offered for state/NELAC accreditation, this report may contain
results which are not accredited. For a specific list of accredited analytes. contact the laboratory or go to
Bttpi-, +,k u L eonf Inintlo*JamCricar 'Borth-aingrita i uC2'ilcu-yt7rk/rnchcstcr-enviroil mental
Page 10 of 28
P-JN'TRANET0AQCFonos Con utdled\QUA LI F—roucine rev 5.doc 91,18, I F

ALS Laboratory Group
Acronyms
ASTM
American Society for Testing and Materials
A2LA
American Association for Laboratory Accreditation
CARB
California Air Resources Board
CAS Number
Chemical Abstract Service registry Number
CFC
Chlorofluorocarbon
CFU
Colony -Forming Unit
DEC
Department of Environmental Conservation
DEQ
Department of Environmental Quality
DHS
Department of Health Services
DOE
Department of Ecology
DOH
Department of Health
EPA
U. S. Environmental Protection Agency
ELAP
Environmental Laboratory Accreditation Program
GC
Gas Chromatography
GC/MS
Gas Chromatography/Mass Spectrometry
LUFT
Leaking Underground Fuel Tank
M
Modified
MCL
Maximum Contaminant Level is the highest permissible concentration of a
substance allowed in drinking water as established by the USEPA.
MDL
Method Detection Limit
MPN
Most Probable Number
MRL
Method Reporting Limit
NA
Not Applicable
NC
Not Calculated
NCASI
National Council of the Paper Industry for Air and Stream Improvement
ND
Not Detected
NIOSH
National Institute for Occupational Safety and Health
PQL
Practical Quantitation Limit
RCRA
Resource Conservation and Recovery Act
SIM
Selected Ion Monitoring
TPH
Total Petroleum Hydrocarbons
tr
Trace level is the concentration of an analyte that is less than the PQL but
greater than or equal to the MDL.
Page 11 of 28

ALS Group USA, Corp.
dba ALS Environmental
Analyst Summary report
Client: Waypoint Analytical formerly Prism Laboratories, Inc. Service Request: R2000593
Project: 0010154/
Sample Name: B-4D Date Collected: 01/8/20
Lab Code: R2000593-001 Date Received: 01/22/20
Sample Matrix: Soil
Analysis Method Extracted/Digested By Analyzed By
7199 CWOODS CWOODS
ALS SOP KAWONG
Sample Name: B-6S Date Collected: 01/7/20
Lab Code: R2000593-002 Date Received: 01/22/20
Sample Matrix: Soil
Analysis Method Extracted/Digested By Analyzed By
7199 CWOODS CWOODS
ALS SOP KAWONG
Sample Name: B-7 Date Collected: 01/6/20
Lab Code: R2000593-003 Date Received: 01/22/20
Sample Matrix: Soil
Analysis Method Extracted/Digested By Analyzed By
7199 CWOODS CWOODS
ALS SOP KAWONG
Printed 1 /27/2020 7:10:43 AM Superset Reference:20-0000537645 rev 00 '
Page 12 of 28

INORGANIC PREPARATION METHODS
ALS
The preparation methods associated with this report are found in these tables unless discussed in the case narrative.
Water/Liquid Matrix
Analytical Method
200.7
Preparation Method
200.2
200.8
200.2
6010C
3005A/3010A
6020A
ILM05.3
003013
9034 Sulfide Acid Soluble
SM 4500-CN-E Residual
Cyanide
SM 4500-CN-G
SM 4500-CN-E WAD
Cyanide
SM 4500-CN-1
Solid/Soil/Non-Aqueous Matrix
Analytical Method
Preparation
Method
6010C
3050B
6020A
3050B
6010C TCLP (1 31 1)
3005A/3010A
extract
3005A/3010A
6010 SPLP (131 2) extract
7199
3060A
300.0 Anions/ 350.1 /
DI extraction
353.2/ SM 232013/ SM
5210B 9056A Anions
For analytical methods not listed, the preparation
method is the same as the analytical method
reference.
P:\INTRANET\QAQC\Forms Controlled\Prep Methods Inorganic rev 2-doc 1 2/20/1 9
Page 13 of 28

AALSEnuironmentad
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
Page 14 of 28

AALSEnuir®nmenta#
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
Page 15 of 28

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Project: 0010154
Sample Matrix: Soil
Sample Name: 13-41)
Lab Code: R2000593-001
Inorganic Parameters
Service Request: R2000593
Date Collected: 01 /08/20 10:40
Date Received: 01/22/20 09:55
Basis: Dry
Analysis
Date
Anaiyte Name N-ILthod
Result Units MRL MDL
Dil. Date Analyzed Extracted Q
Chromium, Hexavalent 7199
0.20 J mg/Kg 0.51 0.06
1 01/24/20 21:13 01/24/20
Chromium, Hexavalent 7199
0.20 J mg/Kg 0.51 0.06
1 01/24/20 21:22 01/24/20
Printed 1/27/2020 7:10:44 AM Superset Reference:20-0000537645 rev 00
Page 16 of 28

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Project: 0010154
Sample Matrix: Soil
Sample Name: 13-41)
Lab Code: R2000593-001
Inorganic Parameters
Service Request: R2000593
Date Collected: 01 /08/20 10:40
Date Received: 01/22/20 09:55
Basis: As Received
Analysis Date
Analyte Name Method Result Units MRL MDL Dil. Date Analyzed Extracted Q
Total Solids ALS SOP 77.2 Percent - - 1 01/23/20 08:35 NA
Printed 1/27/2020 7:10:44 AM Superset Reference:20-0000537645 rev 00
Page 17 of 28

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Project: 0010154
Sample Matrix: Soil
Sample Name: B-6S
Lab Code: R2000593-002
Inorganic Parameters
Service Request: R2000593
Date Collected: 01 /07/20 11:25
Date Received: 01/22/20 09:55
Basis: Dry
Analysis
Date
Anal to Name Method
Result Units MRL MDL
Dil. Date .Analyzed Extracted Q
Chromium, Hexavalent 7199
0.55 U mg/Kg 0.55 0.06
l 01/24/20 23:19 01/24/20
Chromium, Hexavalent 7199
0.55 U mg/Kg 0.55 0.06
l 01/24/20 23:10 01/24/20
Printed 1/27/2020 7:10:44 AM Superset Reference:20-0000537645 rev 00
Page 18 of 28

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Project: 0010154
Sample Matrix: Soil
Sample Name: B-6S
Lab Code: R2000593-002
Inorganic Parameters
Service Request: R2000593
Date Collected: 01/07/20 11:25
Date Received: 01/22/20 09:55
Basis: As Received
Analysis Date
Analyte Name Method Result Units MRL MDL Dil. Date Analyzed _ Extracted Q
Total Solids ALS SOP 72.7 Percent - - 1 01/23/20 08:35 NA
Printed 1 /27/2020 7:10:44 AM Superset Reference:20-0000537645 rev 00
Page 19 of 28

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Project: 0010154
Sample Matrix: Soil
Sample Name: B-7
Lab Code: R2000593-003
Inorganic Parameters
Service Request: R2000593
Date Collected: 01/06/20 12:45
Date Received: 01/22/20 09:55
Basis: Dry
Analysis
Date
Analyte Name Method
Result Units MRL MDL
Dil. Date Analyzed Extracted Q
Chromium, Hexavalent 7199
0.16 J mg/Kg 0.50 0.06
1 01/24/20 23:26 01/24/20
Chromium, Hexavalent 7199
0.16 J mg/Kg 0.50 0.06
1 01/24/20 23:35 01/24/20
Printed 1/27/2020 7:10:44 AM Superset Reference:20-0000537645 rev, 00
Page 20 of 28

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Project: 0010154
Sample Matrix: Soil
Sample Name: B-7
Lab Code: R2000593-003
Inorganic Parameters
Service Request: R2000593
Date Collected: 01 /06/20 12:45
Date Received: 01/22/20 09:55
Basis: As Received
Analysis Date
Analyte.Name Method Result Units MRL MDL Dil. Date Analyzed Extracted Q
Total Solids ALS SOP 80.5 Percent - - 1 01/23/20 08:35 NA
Printed 1/27/2020 7:10:44 AM Superset Reference:20-0000537645 rev 00
Page 21 of 28

AAL-SEnuir®nmantal
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
Page 22 of 28

AALSEn uironmental
ALS Environmental —Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.aisglobal.com
Page 23 of 28

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client:
Waypoint Analytical formerly Prism Laboratories, Inc.
Project:
0010154
Sample Matrix:
Soil
Sample Name:
Method Blank
Lab Code:
R2000593-MB
Inorganic Parameters
Service Request: R2000593
Date Collected: NA
Date Received: NA
Basis: Dry
Analysis
Date
Analyte Name
Method
Result Units MRL MDL
Dil- Date Aualwed Extracted
Chromium, Hexavalent
7199
0.40 U mg/Kg 0.40 0.05
1 01/24/20 19:13 01/24/20
Chromium, Hexavalent
7199
0.40 U mg/Kg 0.40 0.05
1 01/24/20 19:04 01/24/20
Painted 1 /27/2020 7:10:44 AM Superset Reference:20-0000537645 rev 00
Page 24 of 28

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Service Request:
R2000593
Project: 0010154
Date Collected:
01/08/20
Sample Matrix: Soil
Date Received:
01/22/20
Date Analyzed:
01/24/20
Date Extracted:
01/24/20
Matrix Spike Summary
Chromium, Hexavalent
Sample Name: 13 4D
Units:
mg/Kg
Lab Code: R2000593-001
Basis:
Dry
Analysis Method: 7199
Prep Method: EPA 3060A
Matrix Spike
R2000593-OO1MS1
Analyte name
Sample Result Result Spike Amount % Rec
% Rec Limits
Chromium, Hexavalent
0.20 J 49.4
50.8 97
75-125
Chromium, Hexavalent
0.20 J 49.3
50.8 97
75-125
Results flagged with an asterisk (') indicate values outside control criteria.
Results nagged with it pound (M) indicate the control criteria is not applicable.
Percent recoveries and relative percent ddYctences (RPD) :tie determined by the suf vane using values in the calculation which have not been rounded
Printed 1/27/2020 7:10:44 AM Page 25 of 28 Superset Reference:20-0000537645 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Service Request:
R2000593
Project: 0010154
Date Collected:
01/08/20
Sample Matrix: Soil
Date Received:
01/22/20
Date Analyzed:
01/24/20
Date Extracted:
01/24/20
Matrix Spike Summary
Chromium, Hexavalent
Sample Name: 13 4D
Units:
mg/Kg
Lab Code: R2000593-001
Basis:
Dry
Analysis Method: 7199
Prep Method: EPA 3060A
Matrix Spike
R2000593-001 MS2
Analyte Name
Samelle Result Result Spike Amount % Rec
% Rec Limits
Chromium, Hexavalent
0.20 J 792
828 96
75-125
Chromium, Hexavalent
0.20 J 792
828 96
75-125
Results flagged with an asterisk (') indicate values outside control criteria.
Results flagged with a pound (4) indicate the control criteria is not applicable.
Percent recoveries and relative percent dill"ciences (RPD) are determined by the sofhvare using values in the calculation which have not been rounded
Printed 1/27/2020 7:10:44 AM Page 26 of 28 Superset Relerence:20-0000537645 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client:
Waypoint Analytical formerly Prism Laboratories, Inc.
Service Request:
R2000593
Project
0010154
Date Collected:
01/08/20
Sample Matrix:
Soil
Date Received:
01/22/20
Date Analyzed:
01/24/20
Replicate Sample Summary
General Chemistry Parameters
Sample Name:
B-4D
Units:
mg/Kg
Lab Code:
R2000593-001
Basis:
Dry
Duplicate
Sample
R2000593-
Analysis
Sample 001DUP
Analyte Name
Method
MRL MDL Result Result
Average
RPD RPD Limit
Chromium, Hexavalent
7199
0.50 0.06 0.20 J 0.21 J
0.204
<1 20
Chromium, Hexavalent
7199
0.50 0.06 0.20 J 0.21 J
0.204
<1 20
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are detennined by the software using values in the calculation which have not been rounded.
Printed 1/27/20207:10:44AMi Page 27 of 28 Superset Refercnce20-0000537645 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: Waypoint Analytical formerly Prism Laboratories, Inc.
Project: 0010154
Sample Matrix: Soil
Lab Control Sample Summary
General Chemistry Parameters
Lab Control Sample
R2000593-LCS
Service Request: R2000593
Date Analyzed: 01/24/20
Units:mg/Kg
Basis:Dry
Analyte Name Analytical Method Result Spike Amount % Rec % Rec Limits
Chromium, Hexavalent 7199 661 662 100 80-120
Chromium, Hexavalent 7199 660 662 100 80-120
Printed 1/27/2020 7:10:44 AM Superset Relerence:20-0000537645 rev 00
Page 28 of 28