23037_Elan Indian Trail_Brownfields Assessment Reportt 11-22-19

TABLE OF CONTENTS
TABLE OF CONTENTS ............................................................................................................................ 1
FIGURES ..................................................................................................................................................... 1
APPENDICES ............................................................................................................................................. 1
A. SITE INFORMATION ..................................................................................................................... 1
B. INTRODUCTION ............................................................................................................................ 2
C. DATA GAPS .................................................................................................................................... 5
D. ENVIRONMENTAL ASSESSMENT ACTIVITIES ..................................................................... 5
E. QUALITY ASSURANCE/QUALITY CONTROL ......................................................................... 8
F. INVESTIGATIVE DERIVED WASTE MANAGEMENT ............................................................. 9
G. 1,500-FOOT RECEPTOR SURVEY ......................................................................................... 10
H. DISCUSSION OF RESULTS ...................................................................................................... 10
I. LIMITATIONS ............................................................................................................................... 11

FIGURES
Figure 1: Site Location Map
Figure 2: Proposed Sampling Map
Figure 3: Site Map
Figure 4: Soil and Sediment Sample Quality Map
Figure 5: Potentiometric Surface Map
Figure 6: Ground and Surface Water Quality Map
Figure 7: Site Vicinity Map

TABLES

Table 1: Summary of Laboratory Analysis - Soil & Sediment Samples
Table 2: Well Construction and Gauging Information
Table 3: Summary of Laboratory Analysis – Ground & Surface Water Samples

APPENDICES

Appendix A: Soil Boring Logs/Monitoring Well Records
Appendix B: Laboratory Analytical Reports – Soil, Sediment, Surface and Ground Water
Samples

Appendix C: Brownfields Property Receptor Survey Form
Appendix D: Zoning Map – Indian Trail
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A. SITE INFORMATION

 Site Name: Elan Indian Trail
 Location: SE Intersection of Chestnut Parkway and W US
Highway 74
Indian Trail, Union County, NC
 Land Use: Former Residential/Undeveloped
 Property Owner: Parcel 07105005D
Snyder Janice Bivens Lemmond Heirs et al
324 Bubbling Well Road
Matthews, North Carolina 28105

Parcel 07105004
Kay Lemmond Trustee
844 Cherokee Road
Charlotte, North Carolina 28207

 Prospective Developer: Greystar GP II, LLC
465 Meeting Street
Suite 500
Charleston, South Carolina 29403

 Consultant: Resolve Environmental Services, PLLC (Resolve)
500 Devonport Drive
Matthews, North Carolina 28104
[phone]

 Latitude: 35.084307° North
 Longitude: 80.663714° West

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B. INTRODUCTION

1. Site
The subject site consists of two (2) contiguous tracts totaling 31.68 acres identified as Union
County Parcel ID 07105004 (21.6-acres) and 07105005D (10.08-acres). The site is located at
the intersection of Chestnut Parkway and W US Highway 74 in Indian Trail, Union County, North
Carolina (Figure 1).

Resolve Environmental Services, PLLC (Resolve) conducted a Phase I Environmental Site
Assessment (ESA) at the site in May 2019. Based upon the historical information obtained and
reviewed, the property was used as farmland with a residence dating back to at least 1938. The
residence was removed circa 1988 and the farm was no longer in operation. Roadside
businesses operated on a small portion of the property along the eastern property boundary
(along Highway 74) in recent decades. Today the property is heavily wooded and the small area
along the eastern property boundary is being utilized by the NCDOT to store roadway supplies
for a US Highway 74 road improvement project. The surrounding area was primarily farmland
and low-density residential through the 1950’s. However, commercial development began as
early as the 1960’s upon the development of Highway 74. The surrounding area remains a mixed
use of commercial and residential areas.

No RECs were identified at the subject site. One PEC, identified as leaking underground storage
tank (LUST) site “Catawba Food Mart #4”, is located on the adjoining property to the
east/southeast. Confirmed ground water contamination, including concentrations of benzene
exceeding the North Carolina Department of Environmental Quality’s (NCDEQ) Gross
Contamination Level (GCL), have been detected at the site as recent as 2017. Ground water flow
is toward the subject site. The LUST was accepted into the UST State Lead Program, active
corrective action is intended to be conducted at the property.
On July 26, 2019 the subject site was granted eligibility into the NCDEQ’s Brownfields program
and identified as Brownfields Project 23037-19-090. On August 20, 2019, a site meeting was
conducted with representatives from the NCDEQ Brownfields Program, Greystar GP II, LLC,
Parker Poe and Resolve. The purpose of this meeting was to determine the scope of assessment
required at the proposed Elan Indian Trail development prior to preparing a Brownfields
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Agreement for the site. Based upon the meeting, surface water, ground water and soil sampling
activities were proposed.
Based on the August 20, 2019 site meeting, the NCDEQ requested additional assessment
activities in correspondence dated August 22, 2019. Resolve submitted a work plan on
September 18, 2019 for the collection and analyses of soil, sediment, stream and ground water
samples from the site. The work plan was subsequently approved by the NCDEQ on September
25, 2019.
2. Background
On May 15, 2019, Resolve completed a Phase I Environmental Site Assessment Report for the
above referenced property located in Indian Trail, North Carolina. The report was conducted in
accordance with ASTM Standard Practice E1527-13. Based upon the findings in the report,
Resolve recommended the completion of Phase II activities at the site.
No RECs were identified at the subject site. However, an active LUST site “Catawba Food Mart
#4”, is located adjacent to the subject site to the east/southeast. The LUST site has a documented
petroleum release and is identified as Incident 27059 by the North Carolina Department of
Environmental Quality (NCDEQ). The release was initially reported in 2002 following due
diligence activities at the property. Subsequently, five (5) 10,000-gallon petroleum underground
Storage tanks were removed.
The responsible party for the release was Catawba Oil Company (Catawba Oil) of Monroe, North
Carolina. In accordance with NCDEQ guidelines, Catawba Oil completed a Phase I/II Limited
Site Assessment (LSA) in June 2003 and a Comprehensive Site Assessment (CSA) in February
2004. The site was initially ranked high risk following the LSA due to the extent of the ground
water quality violations at the site and proximity of potable water supply wells to the source area.
A total of thirteen (13) Type II monitoring wells (MW-1 through MW-13) and one (1) Type III
monitoring wells were installed as part of LSA, CSA and post-CSA activities between 2003 and
2004.
Based upon assessment sampling results, detectable concentrations exceeding the NCDEQ’s
ground water quality standards specified in 15A NCAC 2L .0202 (2L) were reported in monitoring
wells MW-1, MW-2, MW-3, MW-5, MW-6 MW-7, MW-12, MW-13 and the telescoping well T-1. A
concentration of benzene exceeded the gross contamination levels (GCLs) in MW-1.
4

In 2003, monitoring wells MW-8 and MW-9 were installed along the western property boundary
of the target property of concern. Detectable concentrations of lead, aliphatics and aromatics
were detected ion the ground water sample MW-9; however, the concentrations were below the
2L standards.
The Type III telescoping well (T-1) was installed at the site in 2004 to a total depth of 45 feet below
ground surface with a five foot screen set between 40-45 feet. Detectable concentrations of
benzene, MTBE and IPE above the 2L standard were reported in the sample collected from T-1.
Based upon the CSA, the shallow contaminant plume was determined to be limited to the site and
the immediately adjacent property to the west and toward the subject property. Ground water
flow during the assessment activities was to the west and southwest.
The “Catawba Food Mart #4” and the target property site are underlain by weathered meta-argillite
overlying PWR and more competent metamudstone. The surficial aquifer is semi-confined.
Downward migration of contaminants into the confined and semi-confined fractured mudstone is
common in this portion of Union County. The presence of the 2L violations for benzene, IPE and
MTBE in the telescoping well T-1 support that downward migration is occurring at the site.
Further, the presence of MTBE and IPE in the WSW-5 sample also indicate that the plume may
be moving along deeper fractures as well as the downgradient axis of the surficial aquifer.
A ground water sampling event was conducted in mid-2016. During the event, monitoring wells
MW-7 through MW-15, including the perimeter wells closest to the subject property, could not be
located and were presumed to have been destroyed. Monitoring wells MW-1 through MW-6 and
T-1 were sampled in June 2016. All of the wells had detectable concentrations of contaminants
of concern above the 2L standards. The concentration of benzene in MW-2 also exceeded the
GCLs. Horizontal migration of the plume was not determined during the 2016 sampling events
since none of the perimeter wells were found or sampled.
The approved work plan for the subject site included the installation of two (2) North Carolina
Type II monitoring wells and one (1) Type III well to determine if the release from the adjacent
LUST incident had affected ground water quality at the subject site. Additionally, a background
Type II well was proposed to determine background levels in ground water at the site. The work
5

plan also included the advancement of multiple soil borings across the property, influent and
effluent stream and sediment samples from the onsite creek.
C. DATA GAPS
Areas identified for further investigation at the subject site as addressed in Resolve’s NCDEQ-
approved work plan are listed below and the proposed sampling locations are shown on the
attached Figure 2.

1) Ground water quality at the site, especially along the northeastern r property boundary to
determine if the adjacent LUST incident had affected ground water quality at the site.
2) Determine the potential for vapor intrusion and ground water flow direction.
3) Determine soil quality at the site, characterize surface water and underlying sediment
quality entering and exiting the property.
4) 1,500-foot receptor survey/completion of the Brownfields Property Receptor Survey Form.
D. ENVIRONMENTAL ASSESSMENT ACTIVITIES
1. Soil Assessment

Resolve personnel collected an initial seven (7) soil samples at various locations on the property
including adjacent to the two (2) existing buildings located at the northeastern portion of the site.
A soil sample was collected from each of the seven (7) soil borings (SB-1 through SB-7) with a
sampling interval of 0-2 feet below grade surface (BGS). The borings were advanced using a
hand auger. The collected soil samples were immediately placed into laboratory supplied
glassware and shipped for analyses for VOCs and SVOCs by SW-846 Methods 8260 and 8270,
respectively, and for RCRA metals by EPA Method 6020. In addition, one aliquot from each
collected soil sample was submitted for laboratory hold and possible analyses of hexavalent
chromium by EPA Method 7199 depending on chromium concentration results from the RCRA
Metals analysis.
Resolve collected three (3) additional samples soil samples (SB-8 through SB-10) from native soil
along the powerline easement traversing the property in a southeast/northwest strike. The
samples were collected from hand auger soil borings with a sampling interval of 0-2 feet BGS.
The collected soil samples were submitted for analyses for organophosphorus pesticides (OPPs)
by SW-846 Method 8141B, organochlorine pesticides (OCPs) by SW-846 Method 8081B for
RCRA metals by EPA Method 6020. In addition, one aliquot from each collected soil sample was
6

submitted for laboratory hold and possible analyses of hexavalent chromium by EPA Method 7199
depending on chromium concentration results from the RCRA Metals analysis.
Concentrations of arsenic in soil samples SB-1, SB-2, SB-4, SB-5, SB-6, SB-8 and SB-9
exceeded the NCDEQ’s Industrial/Commercial Preliminary Soil Remediation Goals (PSRG).
Concentrations of arsenic in soil samples SB-3, SB-7 and SB-10 exceeded the Residential
PSRGs. All of the concentrations of arsenic detected in soil samples SB-1 through SB-10
exceeded the EPA Regional Screening Levels (RSL) Protection of Groundwater. No other
detectable concentrations of requested method constituents reported in the soil samples collected
at the site exceeded the NCDEQ PSRGs or EPA RSLs. The arsenic levels appear to be
background levels and not associated with operations or activities at the site. A Soil Quality Map
showing those concentrations that exceeded the Industrial/Commercial PSRGs during the
October 2019 assessment is included as Figure 4. A summary of laboratory results is shown on
Table 1.
2. Surface Water and Sediment Assessment
To evaluate the onsite creek, Resolve personnel collected surface water (SW-INF and SW-EFF)
and streambed sediment samples (SED-INF and SED-EFF) form the stream near the
northwestern influent direction near the property boundary and from the downstream effluent
direction near the southeastern property boundary. Sediment samples were collected with a hand
auger form the streambed. Surface water samples were collected with a clean, disposable bailer.
Collected sediment and surface water samples were immediately placed in laboratory glassware
and transported on ice for laboratory analyses for VOCs and SVOCs by SW-846 Methods 8260
and 8270 and for RCRA metals.
Concentrations of arsenic that exceeded the Residential PSRG and EPA RSL were reported in
the sediment samples SED-EFF and SED-INF. The concentrations of arsenic did not exceed the
Industrial/Commercial PSRG in the sediment samples.
Concentrations of arsenic, barium, chromium and lead that exceeded the NC 2L Standards were
reported in the effluent surface water sample, SW-EFF. The concentrations of arsenic, chromium
and lead also exceeded the EPA maximum contamination levels (MCL).
A Ground Water and Surface Water Quality Map showing those surface water contaminant
concentrations that exceeded the NC 2L Standard and/or EPA MCLs during the October 2019
7

assessment is included as Figure 6. Summaries of laboratory results for sediment and surface
water samples are shown on Table 1 and 3, respectively.

3. Ground Water Assessment

Resolve supervised the installation of three (3) North Carolina Type II monitoring wells (MW-1
through MW-3) and one (1) North Carolina Type III monitoring well DW-1 at the site on October
8-9, 2019. Monitoring wells MW-1 through MW-3 were each completed to a total depth of 25 feet
with a 15-foot screen interval set to bracket the water bearing fractures in each well. The
telescoping well DW-1 was set with a 28-foot 6-inch outer casing at the top of competent bed
rock. The well was completed to a total depth of 33 feet BGS with a 5’ section of screen bracketing
the deeper aquifer. The wells were subsequently developed per the 15A NCAC 02C.0101
regulations. Well construction details are summarized in Table 2. Monitoring well construction
records and associated subsurface boring logs are included in Appendix A. An updated site map
showing monitoring well locations is included as Figure 3.

Subsequent to well development, the newly installed monitoring wells at the site were gauged,
purged and sampled on October 13, 2019. Field parameters (dissolved oxygen, pH, conductivity,
temperature and turbidity) were measured and once readings became stable, a ground water
sample from each well was collected. Stabilization was defined as three consecutive readings
where temperature is within ± 10%, pH is within ± 0.1 SU, and conductivity is ± 5%. The ground
water samples from each well were collected by personnel wearing clean, nitrile gloves a
peristaltic pump with and new, disposable Teflon tubing at each well. .

The ground water samples were submitted to a North Carolina certified laboratory for analysis of
VOCs by Method 8260 and for SVOCs by Method 8270D and RCRA Metals. Estimated and/or
detectable concentrations of cis-1,2-Dichloroethylene, IPE, MTBE, 1,2-Diphenylhydrazine, bis(2-
Ethylhexyl)phthalate, barium, chromium, and/or selenium were reported in ground water samples
collected from the monitoring wells. None of the concentrations exceeded the NC 2L Standards
or the EPA MCLs.

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A Ground Water Quality Map is included as Figure 6. Laboratory analytical results from ground
water sampling activities conducted on October 13, 2019 are summarized in Table 3. Copies
of laboratory analytical reports are included as Appendix B.

Drill cuttings, development and purge water from the monitoring well installations were
containerized in 55-gallon drums and temporarily staged on-site. Based on laboratory analytical
results from the ground water samples, the drill cuttings, development and purge water do not
require disposal at a permitted facility and can be spread on sit flowing review of this report the
NCDEQ.

The top-of-casing elevations of the monitoring wells were surveyed in order to determine the
ground water flow direction at the site. The depths to ground water in the Type II monitoring wells
were measured on October 13, 2019 ranged from 11.80 feet BGS to 16.63 feet BGS. The
calculated ground water elevations ranged from 664.56 feet in MW-2 to 665.88 feet in MW-3.
Ground water flow direction across the site was generally toward the east/southeast. A
potentiometric surface map is included as Figure 5.

E. QUALITY ASSURANCE/QUALITY CONTROL
1. Soil Boring and Monitoring Well Installation

All down-hole drilling equipment was be pressure washed, scrubbed and rinsed prior to
use and between each soil boring/monitoring well installation location.

2. Monitoring Well/ Surface Water Sampling

Monitoring wells were developed using submersible pumps to ensure removal of all
introduced drilling fluids. Monitoring wells were purged using low flow techniques prior to
sample collection. Surface water samples were collected with a new, disposable Teflon
bailer. New nitrile gloves were worn by field personnel during sampling activities and
changed between sample locations. All field meters were properly calibrated and
decontaminated prior to use and between sampling locations. Collected samples were
placed directly into laboratory-supplied sample containers and immediately placed on ice
in a sample cooler. The samples were shipped in sealed coolers to the laboratory. Proper
chain of custody procedures were maintained at all times. To evaluate laboratory quality
9

control and repeatability, one duplicate ground water sample was collected (MW-3) and
analyzed for VOCs, SVOCs and RCRA metals during each sampling event and one trip
blank sample (for VOCs) accompanied the samples during each sampling event.

3. Soil/Sediment Sampling

Soil samples were collected using a decontaminated hand auger. Field personnel
collected each soil sample using a new pair of nitrile gloves. The samples were placed
directly into laboratory-supplied sample containers, immediately placed on ice in a sample
cooler and transported to the laboratory in the manner described above. Proper chain of
custody procedures was maintained at all times. To evaluate laboratory quality control
and repeatability, one duplicate soil sample was collected from SB-10 and analyzed for
VOCs, SVOCs, RCRA metals, one duplicate sample was collected from SED-INF and
analyzed for RCRA Metals by EPA Method 6010, OPPs by SW-846 Method 8141B and
OCPs by SW-846 Method 8081B. One (1) trip blank sample accompanied the samples
during the sampling event.

4. Duplicates and Trip Blanks

All sampling activities followed appropriate quality assurance protocols that including
ground water, surface water, sediment and soil duplicate samples. One (1) trip blank was
included with each sample shipment.
F. INVESTIGATIVE DERIVED WASTE MANAGEMENT

Soil cuttings from the installation of soil borings and monitoring wells was initially stockpiled
pending laboratory analytical results and will be subsequently spread onto the ground in the
vicinity of the borings, following review and approval of this report by the NCDEQ.

Monitoring well development and purge water, as well as equipment decontamination water, was
initially placed into 55-gallon drums pending laboratory analyses. Subsequently, the water will be
placed on the ground in the vicinity of each well head, following review and approval of this report
by the NCDEQ.

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G. 1,500-FOOT RECEPTOR SURVEY

Resolve personnel conducted a reconnaissance and receptor survey of all properties within a
radius of 1,500-feet of the site on November 16, 2019. The area of reconnaissance is located
within a mixed residential/commercial area of Indian Trail, North Carolina. The site consists of
two tracts totaling 31.68 acres. A tributary of Bear Creek transects the property and flows from
the northwest to the southeast. The majority (95%) of the property ground cover is woodland and
brush. The other five (5) percent of the site is developed along the US 74 DOT right of way and
adjacent to the two buildings on the northeast corner of the site. Municipal water and sewer are
available to the site, as well as fiber, telephone and electrical and natural gas.

The site and the majority of properties in the immediate vicinity to the northwest, northeast, east
and southeast are zoned by the Town of Indian Trail as General Business District. Properties to
the immediate south and west are zoned General Business District and Single-Family Residential
(low density), respectively. No private or municipal water supply wells were identified within 1,500
feet of the site. No basements or subterranean structures were identified within 1,500 feet of the
site during the reconnaissance.

A 1,500-foot Radius Map showing property boundaries and other site and nearby features is
included as Figure 7. A completed copy of the Brownfields Property Receptor form is attached
as Appendix C. An individual zoning map showing the Town of Indian Trail is included in
Appendix D.
H. DISCUSSION OF RESULTS
 Resolve collected a total of ten (10) soil samples (SB-1 through SB-10) from the site on
October 5, 2019. Concentrations of arsenic in soil samples SB-1, SB-2, SB-4, SB-5, SB-
8 and SB-9 exceeded the NCDEQ’s Industrial/Commercial PSRGs. Concentrations of
arsenic in soil samples SB-3, SB-7 and SB-10 exceeded the Residential PSRGs. All of
the concentrations of arsenic detected in soil samples SB-1 through SB-10 exceeded the
EPA RSL Protection of Groundwater. The presence of arsenic is common in Union County
and appears to be natural occurring background levels at the site. No other detectable
concentrations of requested method constituents reported in the soil samples collected at
the site exceeded the NCDEQ PSRGs or EPA RSLs.
 Resolve collected surface water (SW-INF and SW-EFF) and streambed sediment samples
11

(SED-INF and SED-EFF) form the on-site stream. Concentrations of arsenic that
exceeded the Residential PSRG and EPA RSL were reported in the sediment samples
SED-EFF and SED-INF. The concentrations of arsenic did not exceed the
Industrial/Commercial PSRG in the sediment samples. Concentrations of arsenic, barium,
chromium and lead that exceeded the NC 2L Standards were reported in the effluent
surface water sample, SW-EFF. The concentrations of arsenic, chromium and lead also
exceeded the EPA MCLs.
 Resolve personnel supervised the installation of three (3) North Carolina Type II
monitoring wells (MW-1 through MW-3) and one (1) North Carolina Type III monitoring
well (DW-1) at the site on October 8-9, 2019. The measured depths to ground water in
the Type II monitoring wells measured on October 13, 2019 ranged from 11.80 feet BGS
to 16.63 feet BGS. The calculated ground water elevations ranged from 664.56 feet in
MW-2 to 665.88 feet in MW-3. Ground water flow direction across the site was generally
toward the east/southeast.
 Ground water samples were collected from MW-1, MW-2, MW-3 and DW-1 on October
13, 2019. Estimated and/or detectable concentrations of volatile organic compounds,
semi-volatile organic compounds and/or metals were reported in each of the ground water
samples collected from the monitoring wells. None of the concentrations exceeded the
NC 2L Standards or Federal MCLs.
 Resolve personnel conducted a 1,500-foot receptor survey on November 16, 2019. No
private water supply wells were identified within a 1,500-foot radius of the site. The site is
zoned by the Town of Indian Trail as General Business District. Properties to the
immediate south and west are zoned General Business District and Single-Family
Residential (low density), respectively.
 Based on the results discussed above, Resolve believes that all outstanding data gaps
have been filled and that no additional assessment is necessary to develop a Brownfields
Agreement for the site.

I. LIMITATIONS
This report has been prepared for the exclusive use of Greystar II GP LLC and the NCDEQ for
specific application to the referenced site in Union County, North Carolina. The assessment was
conducted based on the scope of work and level of effort specified by the NCDEQ and with
resources adequate only for that scope of work. Our findings have been developed in accordance
12

with generally accepted standards of geology and hydrogeology practices in the State of North
Carolina, available information, and our professional judgment. No other warranty is expressed
or implied.

The data that are presented in this report are indicative of conditions that existed at the precise
locations sampled and at the time the samples were collected. In addition, the data obtained from
samples would be interpreted as being meaningful with respect to parameters indicated in the
laboratory report. No additional information can logically be inferred from these data.

FIGURES
SITE LOCATIONFigure 1 Site Location Elan-Indian Trail SE Intersection of Chestnut Pkwy & Hwy 74Indian Trail, Union County, NCBrownfields Project ID No. 23037-19-090Project No. 5225500 M2000 FTDate: 11/21/19Location: 35.084471° N 80.664309° W Dad
SITE
07105004
07105011
07105005A
07105005D
07084348
07111018K
07105005B
07111018E
07105005
07084345Q
07105005C
M7084345H
07084345F
07084386A 07084471INDEPENDENCE BLVD
CHESTNUT PKWYPAULA LNINDIAN TRAIL RDSMITH FARM RDINDIAN TRAIL FAIRVIEW RDALLEN WAYSHADY BLUFF
GARY DR
NELSON LEMMOND DR
POST OFFICE DR
POSTAGE WAY
VAN BUREN AV
SUNNYSIDE CIR
PEACE DR
BROOKE LNMATTHEWS
I
NDI
AN TRAI
L RDJUNE DR
W
A
M
P
U
M D
R
C R O W E L L L NINDEPENDENCE DRUNITED ENTRANCE SU
NN
Y
S
I
D
E CI
R
CL
E

E
X
TU TURN U TURN INDEPENDENCE BLVDU TURN C rooked C reek³
FIGURE 6: SITE VICINITY MAPELAN INDIAN TRAILSE INTERSECTION OF CHESTNUT PKWY & US HWY 74INDIAN TRAIL, UNION COUNTYNORTH CAROLINABROWNFIELDS PROJECT ID NO. 23037-19-090
PREPARED BY:RESOLVE ENVIRONMENTAL SERVICES, PLLC.NOVEMBER 21, 2019
0 300150Feet1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
Roads_110317
streams_shp
Adjacent Properties
Union County NC_parcels_2019_03_07
lakes

TABLES
Soil DUP A Soil DUP B SED-EFF SED-INF
Date Sampled 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019 10/5/2019
Acetone 0.186 J 0.667 0.161 J 0.536 0.199 J 0.376 0.414 0.157 J NR NR NR NR ND 0.269 0.230 J ND 61,000 670,000 2.9
Benzene ND ND ND ND ND ND ND ND NR NR NR NR ND ND 0.0040 J ND 1.2 5.1 0.00023
2-Butanone (MEK)ND 0.0320 J ND ND ND ND 0.0128 J ND NR NR NR NR ND 0.0093 J 0.0268 J ND 27,000 190,000 1.2
Ethyl Alcohol ND 0.185 J ND ND ND ND 0.120 J 0.355 J NR NR NR NR ND 0.255 J 0.935 ND NE NE NE
p-Isopropyltoluene ND ND ND 0.0161 0.0058 J 0.0121 ND ND NR NR NR NR ND ND ND ND NE NE NE
Toluene ND ND ND ND ND ND ND ND NR NR NR NR ND ND 0.0346 ND 4,900 47,000 0.69
Benzoic Acid ND ND ND ND ND 1.49 ND ND NR NR NR NR ND ND ND NR 250,000 3,300,000 15
Benzo(b)flouranthene ND 0.0341 J ND ND ND ND ND ND NR NR NR NR ND ND ND NR 1.1 21 0.3
Benzo(g,h,i)perylene ND ND ND ND ND ND ND ND NR NR NR NR ND ND 0.273 J NR NE NE NE
bis(2-Ethylhexyl)phthalate 0.0818 J 0.0619 J ND 0.0516 J ND ND 0.0403 J ND NR NR NR NR ND ND ND NR 39 160 1.3
Flouranthene ND 0.0528 J ND ND ND ND ND ND NR NR NR NR ND ND ND NR 24,000 30,000 89
Phenanthrene ND 0.0619 J ND ND ND ND ND ND NR NR NR NR ND ND ND NR NE NE NE
Pyrene ND 0.0528 J ND ND ND ND ND ND NR NR NR NR ND ND ND NR 1,800 23,000 13
Arsenic 18.6 10.8 2.4 7.3 4.1 3.2 1.8 20.8 3.9 6.7 2.0 2.5 2.7 1.7 ND NR 0.68 3.0 0.0015
Barium 14.9 104 25.0 36.0 57.6 11.8 35.9 12.5 42.8 51.8 33.7 33.3 26.2 27.3 24.4 NR 15,000 220,000 82
Cadmium ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NR 71 980 0.38
Chromium 15.2 37.5 8.9 32.5 39.6 31.4 14.0 14.3 26.1 26.8 9.9 10.1 10.1 8.5 8.1 NR NE NE 180,000
Lead 7.1 15.8 6.9 6.5 16.0 7.2 10.3 7.1 13.5 8.7 18.6 15.5 10.6 3.5 3.1 NR 400 800 14
Mercury 0.063 ND ND ND 0.074 ND ND 0.065 ND 0.091 ND ND ND ND ND NR 11 460 0.033
Selenium 2.0 9.6 ND ND ND 0.93 1.2 2.5 2.0 1.6 ND ND ND 1.5 1.7 NR 390 5,800 0.26
Silver ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NR 390 5,800 0.80
Notes: .
Soil and Sediment results reported in milligrams per kilogram
Trip blank results reported in micrograms per liter.
Concentrations in bold font exceed the NC Residential Preliminary Soil Remediation Goals.
Concentrations in bold font and italics exceed the NC Industrial/Commercial Preliminary Soil Remediation Goals.
J: Estimated value
ND: Not detected.
NR: Not requested.
Summary of Laboratory Analyses-Soil Samples
Elan - Indian Trail
Indian Trail, NC
Project ID: 21037-19-090
All results reported in milligrams per kilogram (mg/kg)
GC/MS Semi-volatiles (SW846 8270D)
Metals Analysis
Table 1
SB-6 (2')
NCDEQ Preliminary
Soil Remediation
Goals ResIdential
(mg/kg)
SB-1 (2')SB-2 (2')SB-5 (2')SB-9 (2')SB-10 (2')SED DUP DSample ID:SB-4 (2')SB-3 (2')
EPA Regional Screening
Levels Protection of
Groundwater
(mg/kg)
SB-7 (2')SB-8 (2')Trip Blank
NCDEQ Preliminary Soil
Remediation Goals
Industrial/Commercial
(mg/kg)
Date:9/18/19
MW-1 10/9/2019 10/13/2019 10 10-25 25 681.74 16.63 0.00 665.11 Stand-up
cover
MW-2 10/8/2019 10/13/2019 10 10-25 25 676.36 11.80 0.00 664.56 Stand-up
cover
MW-3 10/8/2019 10/13/2019 10 10-25 25 680.63 14.75 0.00 665.88 Stand-up
cover
DW-1 10/9/2019 10/13/2019 28 28-33 33 676.43 11.16 0.00 665.27 Stand-up
cover
Notes:
• ft BGS : feet below ground surface.
• NA: Not available.
• NM: Not measured.
INDIAN TRAIL, UNION COUNTY
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free
Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 2
WELL CONSTRUCTION AND GAUGING INFORMATION
ELAN INDIAN TRAIL
PROJECT ID: 23037-19-090
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
11/23/2019
MW-1 MW-2 MW-3 DW-1 DUP TRIP BLANK SW-INF SW-EFF SW-DUP C
GC/MS Volatiles 8260D unit
Acetone ug/l <10 <10 <10 <10 <10 <10 <10 20.4J <10 6,000 NE
cis-1,2-Dichloroethylene ug/l <0.28 0.44 J <0.28 <0.28 <0.28 <0.28 <0.28 <0.28 <0.28 70 70
Di-Isopropyl Ether ug/l <0.24 0.52J <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 70 NE
Methyl Tert Butyl Ether ug/l <0.23 3.1 <0.23 0.70J <0.23 <0.23 <0.23 <0.23 <0.23 20 NE
p-Isopropyltoluene ug/l <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 <0.21 1.1 <0.21 25 NE
Toluene ug/l <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 1.7 <0.30 600 1,000
GC/MS Semi-volatiles 8270 unit
1,2-Diphenylhydrazine ug/l <0.72 <0.72 0.83J <0.72 <0.72 NR <0.72 <7.6 <0.72 NE NE
bis(2-Ethylhexyl)phthalate ug/l <0.94 <0.94 <0.94 1.1J <0.94 NR <0.95 <10 <0.95 3 6
3&4-Methylphenol ug/l <0.92 <0.92 <0.92 <0.92 <0.92 NR <0.93 18.0J <0.93 NE NE
Phenol ug/l <0.47 <0.47 <0.47 <0.47 <0.47 NR <0.48 7.5J <0.48 30 NE
Metals Analysis unit
Arsenic ug/l <2.0 <2.0 <2.0 <2.0 <2.0 NR 2.3 23.3 <2.0 10 10
Barium ug/l 31.7 12.2 15.6 10.8 14.8 NR 177 1,630 99.7 700 2,000
Cadmium ug/l <2.0 <2.0 <2.0 <2.0 <2.0 NR <2.0 <20 <2.0 2 5
Chromium ug/l 6.4 <2.0 4.2 2.0 4.4 NR 7.6 277 2.5 10 100
Lead ug/l <2.0 <2.0 <2.0 <2.0 <2.0 NR 6.2 194 <2.0 15 15
Mercury ug/l <0.50 <0.50 <0.50 <0.50 <0.50 NR <0.50 <0.50 <0.50 1 2
Selenium ug/l 2.1 <2.0 <2.0 <2.0 <2.0 NR <2.0 <20 <2.0 20 50
Silver ug/l <2.0 <2.0 <2.0 <2.0 <2.0 NR <2.0 <20 <2.0 20 NE
Notes:
Results reported in micrograms per liter.
J: Estimated value.
MCL: Maximum contamination level.
NE: Not established.
NR: Analysis not requested.
TABLE 3
ELAN INDIAN TRAIL
INDIAN TRAIL, NORTH CAROLINA
Sample
Date Sampled 10/14/2019 10/14/2019
PROJECT ID 23037-19-090
10/14/2019 10/14/2019 10/14/2019 10/14/2019
NC 2L
Standard EPA MCL
SUMMARY OF LABORATORY ANALYSIS-GROUND & SURFACE WATER SAMPLES
10/5/2019 10/5/201910/5/2019
Page 3

APPENDICES

APPENDIX A

Soil Boring Logs/Monitoring Well Records
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-1 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Tan Mudstone/Argillite
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-2 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Tan Mudstone/Argillite
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-3 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Tan Silt
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-4 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Orange Silt
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-5 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Orange Silt
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-6 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Tan Silt w/Rock
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-7 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Tan Silt
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-8 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Tan Silt
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-9 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Tan Silt
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number SB-10 Date Drilled
Sample Method Grab Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller W. Scott Ball Log By W. Scott Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 2.0 0 - 2.0' Tan Silt
2 TD 2'
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/05/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number MW-1 Date Drilled
Sample Method NA Drilling Method SSA
Completion Details 15' screen, 13' riser, sand 13-25', bentonite 11-12', Portland cement 0-11'
Driller Samuel Bowers NC 3220-A Log By Terry Kennedy
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0
2
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/09/19
12'-25'; Meta Argillite
0-6'; Light Brown SILT
6-12'; Partially Weathered ROCK
TD 25'
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number MW-2 Date Drilled
Sample Method NA Drilling Method SSA
Completion Details 15' screen, 13' riser, sand 13-25', bentonite 11-12', Portland cement 0-11'
Driller Samuel Bowers NC 3220-A Log By Terry Kennedy
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0
2
4
6
8
10

12
14
16

18
20
22

24
26
28

30
10/08/19
0-4'; Light Brown SILT
TD 25'
4-9'; Partially Weathered ROCK
9'-25'; Meta Argillite
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number MW-3 Date Drilled
Sample Method NA Drilling Method SSA
Completion Details 15' screen, 13' riser, sand 13-25', bentonite 11-12', Portland cement 0-11'
Driller Samuel Bowers NC 3220-A Log By Terry Kennedy
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0
2
4
6
8
10

12
14
16

18
20
22
23'-25'; Blue Slate
24
26
28

30
TD 25'
5-14'; Partially Weathered ROCK
14'-23'; Meta Argillite
10/08/19
0-5'; Light Brown SILT
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Elan-Indian Trail
Address Chestnut Parkway and West U.S. Highway 74, Indian Trail, North Carolina
Boring Number DW-1 Date Drilled
Sample Method NA Drilling Method SSA/Air Hammer
Completion Details 6" Outer casing to 25' ; 5'screen, 28' riser, sand 26-33', bentonite 24-26', Portland cement 0-24'
Driller Samuel Bowers NC 3220-A Log By Terry Kennedy
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0
2
4
6
8
10

12
14
16

18
20
22

24
26
28

30
32
33' hammer refusal, competent bedrock; TD 33'
34
9'-33'; Meta Argillite
10/08-10/9/2019
0-3'; Light Brown SILT
3-9'; Partially Weathered ROCK
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:

APPENDIX B

Laboratory Analytical Reports – Soil, Sediment, Surface and Ground Water
Samples
10/21/19
Technical Report for
Resolve Environmental
Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
23037-19-090
SGS Job Number: FA68836
Sampling Date: 10/05/19
Report to:
Resolve Environmental
500 Devonport Dr
Matthews, NC 28104
[e-mail]
ATTN: Laura Minor
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 10/21/19
Reissue #1
e-Hardcopy 2.0
Automated Report
189
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 189
FA68836
Florida  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]

October 18, 2019

Ms. Laura Minor
Resolve
500 Devonport Dr
Matthews, NC 28104

RE: SGS North America Inc. - Orlando job FA68836 Reissue

Dear Ms. Minor,

The final report for job number FA68836 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.

The sample ID has been revised.

SGS North America Inc. - Orlando apologies for any inconvenience this may have caused.
Please feel free to contact us if we can be of further assistance.

Sincerely,

SGS North America, Inc. - Orlando

2 of 189
FA68836
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................6
Section 3: Sample Results ........................................................................................................11
3.1: FA68836-1: SB-1 (2') ....................................................................................................12
3.2: FA68836-2: SB-2 (2') ....................................................................................................18
3.3: FA68836-3: SB-3 (2') ....................................................................................................24
3.4: FA68836-4: SB-4 (2') ....................................................................................................30
3.5: FA68836-5: SB-5 (2') ....................................................................................................36
3.6: FA68836-6: SB-6 (2') ....................................................................................................42
3.7: FA68836-7: SB-7 (2') ....................................................................................................48
3.8: FA68836-8: SOIL-DUP-A ............................................................................................54
3.9: FA68836-9: SB-8 (2') ....................................................................................................60
3.10: FA68836-10: SB-9 (2') ................................................................................................64
3.11: FA68836-11: SB-10 (2') ..............................................................................................68
3.12: FA68836-12: SOIL DUP-B ........................................................................................72
3.13: FA68836-13: SW-EFF ................................................................................................76
3.14: FA68836-14: SED-EFF ..............................................................................................81
3.15: FA68836-15: SW-INF .................................................................................................87
3.16: FA68836-16: SED-INF ...............................................................................................92
3.17: FA68836-17: SW DUP-C ...........................................................................................98
3.18: FA68836-18: SED DUP-D .........................................................................................103
3.19: FA68836-19: TRIP BLANK .......................................................................................109
Section 4: Misc. Forms ............................................................................................................111
4.1: Chain of Custody ...........................................................................................................112
Section 5: MS Volatiles - QC Data Summaries .....................................................................115
5.1: Method Blank Summary ................................................................................................116
5.2: Blank Spike Summary ...................................................................................................125
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................134
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................143
6.1: Method Blank Summary ................................................................................................144
6.2: Blank Spike Summary ...................................................................................................148
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................152
Section 7: GC/LC Semi-volatiles - QC Data Summaries .....................................................156
7.1: Method Blank Summary ................................................................................................157
7.2: Blank Spike Summary ...................................................................................................159
7.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................162
Section 8: Metals Analysis - QC Data Summaries ................................................................164
8.1: Prep QC MP36236: Hg ..................................................................................................165
8.2: Prep QC MP36237: Hg ..................................................................................................170
8.3: Prep QC MP36244: Hg ..................................................................................................175
8.4: Prep QC MP36254: As,Ba,Cd,Cr,Pb,Se,Ag ..................................................................180
8.5: Prep QC MP36255: As,Ba,Cd,Cr,Pb,Se,Ag ..................................................................185 123456783 of 189
FA68836
SGS North America Inc.
Sample Summary
Resolve Environmental
Job No:FA68836
Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Project No: 23037-19-090
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA68836-1 10/05/19 07:46 SB 10/09/19 SO Soil SB-1 (2')
FA68836-2 10/05/19 08:09 SB 10/09/19 SO Soil SB-2 (2')
FA68836-3 10/05/19 10:26 SB 10/09/19 SO Soil SB-3 (2')
FA68836-4 10/05/19 10:07 SB 10/09/19 SO Soil SB-4 (2')
FA68836-5 10/05/19 10:55 SB 10/09/19 SO Soil SB-5 (2')
FA68836-6 10/05/19 11:25 SB 10/09/19 SO Soil SB-6 (2')
FA68836-7 10/05/19 12:34 SB 10/09/19 SO Soil SB-7 (2')
FA68836-8 10/05/19 00:00 SB 10/09/19 SO Soil SOIL-DUP-A
FA68836-9 10/05/19 11:14 SB 10/09/19 SO Soil SB-8 (2')
FA68836-10 10/05/19 10:37 SB 10/09/19 SO Soil SB-9 (2')
FA68836-11 10/05/19 08:58 SB 10/09/19 SO Soil SB-10 (2')
FA68836-12 10/05/19 00:00 SB 10/09/19 SO Soil SOIL DUP-B
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
4 of 189
FA688361
SGS North America Inc.
Sample Summary
(continued)
Resolve Environmental
Job No:FA68836
Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Project No: 23037-19-090
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA68836-13 10/05/19 09:33 SB 10/09/19 AQ Surface Water SW-EFF
FA68836-14 10/05/19 09:40 SB 10/09/19 SO Soil SED-EFF
FA68836-15 10/05/19 12:08 SB 10/09/19 AQ Surface Water SW-INF
FA68836-16 10/05/19 12:15 SB 10/09/19 SO Soil SED-INF
FA68836-17 10/05/19 00:00 SB 10/09/19 AQ Surface Water SW DUP-C
FA68836-18 10/05/19 00:00 SB 10/09/19 SO Soil SED DUP-D
FA68836-19 10/05/19 00:00 SB 10/09/19 AQ Trip Blank Water TRIP BLANK
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
5 of 189
FA688361
Summary of Hits Page 1 of 5
Job Number:FA68836
Account:Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Collected:10/05/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA68836-1 SB-1 (2')
Acetone a 0.186 J 0.25 0.12 mg/kg SW846 8260D
bis(2-Ethylhexyl)phthalate 0.0818 J 0.37 0.037 mg/kg SW846 8270E
Arsenic b 18.6 1.1 mg/kg SW846 6020B
Barium b 14.9 1.1 mg/kg SW846 6020B
Chromium b 15.2 1.1 mg/kg SW846 6020B
Lead b 7.1 1.1 mg/kg SW846 6020B
Mercury 0.063 0.043 mg/kg SW846 7471B
Selenium b 2.0 1.1 mg/kg SW846 6020B
FA68836-2 SB-2 (2')
Acetone a 0.667 0.31 0.16 mg/kg SW846 8260D
2-Butanone (MEK) a 0.0320 J 0.039 0.011 mg/kg SW846 8260D
Ethyl Alcohol c 0.185 J 0.62 0.12 mg/kg SW846 8260D
Benzo(b)fluoranthene 0.0341 J 0.18 0.020 mg/kg SW846 8270E
Chrysene 0.0318 J 0.18 0.019 mg/kg SW846 8270E
bis(2-Ethylhexyl)phthalate 0.0619 J 0.37 0.037 mg/kg SW846 8270E
Fluoranthene 0.0528 J 0.18 0.018 mg/kg SW846 8270E
Phenanthrene 0.0190 J 0.18 0.018 mg/kg SW846 8270E
Pyrene 0.0424 J 0.18 0.021 mg/kg SW846 8270E
Arsenic b 10.8 1.1 mg/kg SW846 6020B
Barium b 104 1.1 mg/kg SW846 6020B
Chromium b 37.5 1.1 mg/kg SW846 6020B
Lead b 15.8 1.1 mg/kg SW846 6020B
Selenium b 9.6 1.1 mg/kg SW846 6020B
FA68836-3 SB-3 (2')
Acetone c 0.161 J 0.26 0.13 mg/kg SW846 8260D
Arsenic b 2.4 1.0 mg/kg SW846 6020B
Barium b 25.0 1.0 mg/kg SW846 6020B
Chromium b 8.9 1.0 mg/kg SW846 6020B
Lead b 6.9 1.0 mg/kg SW846 6020B
FA68836-4 SB-4 (2')
Acetone a 0.536 0.32 0.16 mg/kg SW846 8260D
p-Isopropyltoluene d 0.0161 0.0079 0.0016 mg/kg SW846 8260D
bis(2-Ethylhexyl)phthalate 0.0516 J 0.40 0.040 mg/kg SW846 8270E
Arsenic b 7.3 1.1 mg/kg SW846 6020B
Barium b 36.0 1.1 mg/kg SW846 6020B
Chromium b 32.5 1.1 mg/kg SW846 6020B
Lead b 6.5 1.1 mg/kg SW846 6020B
6 of 189
FA688362
Summary of Hits Page 2 of 5
Job Number:FA68836
Account:Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Collected:10/05/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA68836-5 SB-5 (2')
Acetone a 0.199 J 0.38 0.19 mg/kg SW846 8260D
p-Isopropyltoluene a 0.0058 J 0.0096 0.0019 mg/kg SW846 8260D
Arsenic b 4.1 1.1 mg/kg SW846 6020B
Barium b 57.6 1.1 mg/kg SW846 6020B
Chromium b 39.6 1.1 mg/kg SW846 6020B
Lead b 16.0 1.1 mg/kg SW846 6020B
Mercury 0.074 0.044 mg/kg SW846 7471B
FA68836-6 SB-6 (2')
Acetone a 0.376 0.23 0.11 mg/kg SW846 8260D
p-Isopropyltoluene a 0.0121 0.0057 0.0011 mg/kg SW846 8260D
Benzoic Acid 1.49 0.90 0.18 mg/kg SW846 8270E
Arsenic b 3.2 0.83 mg/kg SW846 6020B
Barium b 11.8 0.83 mg/kg SW846 6020B
Chromium b 31.4 0.83 mg/kg SW846 6020B
Lead b 7.2 0.83 mg/kg SW846 6020B
Selenium b 0.93 0.83 mg/kg SW846 6020B
FA68836-7 SB-7 (2')
Acetone a 0.414 0.30 0.15 mg/kg SW846 8260D
2-Butanone (MEK) a 0.0128 J 0.030 0.0088 mg/kg SW846 8260D
Ethyl Alcohol e 0.120 J 0.48 0.091 mg/kg SW846 8260D
bis(2-Ethylhexyl)phthalate 0.0403 J 0.36 0.036 mg/kg SW846 8270E
Arsenic b 1.8 0.98 mg/kg SW846 6020B
Barium b 35.9 0.98 mg/kg SW846 6020B
Chromium b 14.0 0.98 mg/kg SW846 6020B
Lead b 10.3 0.98 mg/kg SW846 6020B
Selenium b 1.2 0.98 mg/kg SW846 6020B
FA68836-8 SOIL-DUP-A
Acetone c 0.157 J 0.20 0.10 mg/kg SW846 8260D
Ethyl Alcohol f 0.355 J 0.41 0.077 mg/kg SW846 8260D
Arsenic b 20.8 1.1 mg/kg SW846 6020B
Barium b 12.5 1.1 mg/kg SW846 6020B
Chromium b 14.3 1.1 mg/kg SW846 6020B
Lead b 7.1 1.1 mg/kg SW846 6020B
Mercury 0.065 0.046 mg/kg SW846 7471B
Selenium b 2.5 1.1 mg/kg SW846 6020B
7 of 189
FA688362
Summary of Hits Page 3 of 5
Job Number:FA68836
Account:Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Collected:10/05/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA68836-9 SB-8 (2')
Arsenic b 3.9 0.96 mg/kg SW846 6020B
Barium b 42.8 0.96 mg/kg SW846 6020B
Chromium b 26.1 0.96 mg/kg SW846 6020B
Lead b 13.5 0.96 mg/kg SW846 6020B
Selenium b 2.0 0.96 mg/kg SW846 6020B
FA68836-10 SB-9 (2')
Arsenic b 6.7 0.94 mg/kg SW846 6020B
Barium b 51.8 0.94 mg/kg SW846 6020B
Chromium b 26.8 0.94 mg/kg SW846 6020B
Lead b 8.7 0.94 mg/kg SW846 6020B
Mercury 0.091 0.047 mg/kg SW846 7471B
Selenium b 1.6 0.94 mg/kg SW846 6020B
FA68836-11 SB-10 (2')
Arsenic b 2.0 0.84 mg/kg SW846 6020B
Barium b 33.7 0.84 mg/kg SW846 6020B
Chromium b 9.9 0.84 mg/kg SW846 6020B
Lead b 18.6 0.84 mg/kg SW846 6020B
FA68836-12 SOIL DUP-B
Arsenic b 2.5 0.93 mg/kg SW846 6020B
Barium b 33.3 0.93 mg/kg SW846 6020B
Chromium b 10.1 0.93 mg/kg SW846 6020B
Lead b 15.5 0.93 mg/kg SW846 6020B
FA68836-13 SW-EFF
Acetone 20.4 J 25 10 ug/l SW846 8260D
p-Isopropyltoluene 1.1 1.0 0.21 ug/l SW846 8260D
Toluene 1.7 1.0 0.30 ug/l SW846 8260D
3&4-Methylphenol 18.0 J 50 9.8 ug/l SW846 8270E
Phenol 7.5 J 50 5.0 ug/l SW846 8270E
Arsenic b 23.3 20 ug/l SW846 6020B
Barium b 1630 20 ug/l SW846 6020B
Chromium b 277 20 ug/l SW846 6020B
Lead b 194 20 ug/l SW846 6020B
8 of 189
FA688362
Summary of Hits Page 4 of 5
Job Number:FA68836
Account:Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Collected:10/05/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA68836-14 SED-EFF
Arsenic b 2.7 1.0 mg/kg SW846 6020B
Barium b 26.2 1.0 mg/kg SW846 6020B
Chromium b 10.1 1.0 mg/kg SW846 6020B
Lead b 10.6 1.0 mg/kg SW846 6020B
FA68836-15 SW-INF
Arsenic 2.3 2.0 ug/l SW846 6020B
Barium 177 2.0 ug/l SW846 6020B
Chromium 7.6 2.0 ug/l SW846 6020B
Lead 6.2 2.0 ug/l SW846 6020B
FA68836-16 SED-INF
Acetone c 0.269 0.22 0.11 mg/kg SW846 8260D
2-Butanone (MEK) a 0.0093 J 0.028 0.0080 mg/kg SW846 8260D
Ethyl Alcohol g 0.255 J 0.44 0.083 mg/kg SW846 8260D
Arsenic b 1.7 0.78 mg/kg SW846 6020B
Barium b 27.3 0.78 mg/kg SW846 6020B
Chromium b 8.5 0.78 mg/kg SW846 6020B
Lead b 3.5 0.78 mg/kg SW846 6020B
Selenium b 1.5 0.78 mg/kg SW846 6020B
FA68836-17 SW DUP-C
Barium 99.7 2.0 ug/l SW846 6020B
Chromium 2.5 2.0 ug/l SW846 6020B
FA68836-18 SED DUP-D
Acetone c 0.230 J 0.34 0.17 mg/kg SW846 8260D
Benzene a 0.0040 J 0.0086 0.0021 mg/kg SW846 8260D
2-Butanone (MEK) a 0.0268 J 0.043 0.013 mg/kg SW846 8260D
Ethyl Alcohol g 0.935 0.69 0.13 mg/kg SW846 8260D
Toluene a 0.0346 0.034 0.017 mg/kg SW846 8260D
Benzo(g,h,i)perylene 0.273 J 2.0 0.21 mg/kg SW846 8270E
Barium b 24.4 1.1 mg/kg SW846 6020B
Chromium b 8.1 1.1 mg/kg SW846 6020B
Lead b 3.1 1.1 mg/kg SW846 6020B
Selenium b 1.7 1.1 mg/kg SW846 6020B
9 of 189
FA688362
Summary of Hits Page 5 of 5
Job Number:FA68836
Account:Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Collected:10/05/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA68836-19 TRIP BLANK
No hits reported in this sample.
(a) Results reported from Bisulfate preserved sample.
(b) Sample dilution required due to difficult matrix.
(c) Results reported from Bisulfate preserved sample. Associated CCV outside of control limits high.
(d) Results reported from Bisulfate preserved sample. Internal standard response outside control limits. Confirmed
by MS/MSD.
(e) Results reported from Bisulfate preserved sample. Associated BS recovery outside control limits high.
Associated CCV outside of control limits high. Results from different vials are not consistent; higher results
were reported.
(f) Results reported from Bisulfate preserved sample. Associated BS recovery outside control limits high.
Associated CCV outside of control limits high.
(g) Results reported from Bisulfate preserved sample. Associated BS recovery outside control limits, high.
Associated CCV outside of control limits high.
10 of 189
FA688362
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
11 of 189
FA688363
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-1 (2')
Lab Sample ID:FA68836-1 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:88.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13598.D 1 10/11/19 16:14 SP n/a n/a V2B518
Run #2 b 2B13566.D 1 10/10/19 15:42 SP n/a n/a V2B517
Initial Weight Final Volume
Run #1 4.52 g 5.0 ml
Run #2 4.54 g 5.0 ml
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.186 0.25 0.12 mg/kg J
71-43-2 Benzene ND 0.0062 0.0015 mg/kg
108-86-1 Bromobenzene ND 0.0062 0.0012 mg/kg
74-97-5 Bromochloromethane ND 0.0062 0.0018 mg/kg
75-27-4 Bromodichloromethane c ND 0.0062 0.0012 mg/kg
75-25-2 Bromoform ND 0.0062 0.0012 mg/kg
78-93-3 2-Butanone (MEK)ND 0.031 0.0091 mg/kg
104-51-8 n-Butylbenzene ND 0.0062 0.0012 mg/kg
135-98-8 sec-Butylbenzene ND 0.0062 0.0012 mg/kg
98-06-6 tert-Butylbenzene ND 0.0062 0.0012 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0062 0.0013 mg/kg
108-90-7 Chlorobenzene ND 0.0062 0.0012 mg/kg
75-00-3 Chloroethane d ND 0.0062 0.0025 mg/kg
67-66-3 Chloroform ND 0.0062 0.0017 mg/kg
95-49-8 o-Chlorotoluene ND 0.0062 0.0012 mg/kg
106-43-4 p-Chlorotoluene ND 0.0062 0.0012 mg/kg
124-48-1 Dibromochloromethane ND 0.0062 0.0012 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0062 0.0012 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0062 0.0025 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0062 0.0012 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0062 0.0012 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0062 0.0014 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0062 0.0022 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0062 0.0012 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0062 0.0012 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0062 0.0017 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0062 0.0012 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0062 0.0012 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0062 0.0012 mg/kg
594-20-7 2,2-Dichloropropane e ND 0.0062 0.0012 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0062 0.0013 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0062 0.0012 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 189
FA6883633.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-1 (2')
Lab Sample ID:FA68836-1 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:88.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0062 0.0012 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0062 0.0029 mg/kg
64-17-5 Ethyl Alcohol e ND 0.50 0.094 mg/kg
100-41-4 Ethylbenzene ND 0.0062 0.0012 mg/kg
591-78-6 2-Hexanone ND 0.031 0.0094 mg/kg
98-82-8 Isopropylbenzene ND 0.0062 0.0012 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0062 0.0012 mg/kg
74-83-9 Methyl Bromide ND 0.0062 0.0025 mg/kg
74-87-3 Methyl Chloride ND 0.0062 0.0025 mg/kg
75-09-2 Methylene Chloride e ND 0.025 0.014 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.031 0.0094 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0062 0.0012 mg/kg
91-20-3 Naphthalene ND 0.0062 0.0025 mg/kg
103-65-1 n-Propylbenzene ND 0.0062 0.0012 mg/kg
100-42-5 Styrene ND 0.0062 0.0012 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0062 0.0013 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0062 0.0012 mg/kg
127-18-4 Tetrachloroethylene ND 0.0062 0.0016 mg/kg
108-88-3 Toluene ND 0.025 0.012 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0062 0.0017 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0062 0.0012 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0062 0.0012 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0062 0.0012 mg/kg
79-01-6 Trichloroethylene ND 0.0062 0.0012 mg/kg
75-69-4 Trichlorofluoromethane e ND 0.0062 0.0025 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0062 0.0016 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0062 0.0012 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0062 0.0012 mg/kg
108-05-4 Vinyl Acetate ND 0.031 0.020 mg/kg
75-01-4 Vinyl Chloride ND 0.0062 0.0012 mg/kg
m,p-Xylene ND 0.012 0.0014 mg/kg
95-47-6 o-Xylene ND 0.0062 0.0012 mg/kg
1330-20-7 Xylene (total)ND 0.019 0.0026 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%98%75-124%
17060-07-0 1,2-Dichloroethane-D4 118%113%72-135%
2037-26-5 Toluene-D8 100%100%75-126%
460-00-4 4-Bromofluorobenzene 93%95%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 189
FA6883633.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-1 (2')
Lab Sample ID:FA68836-1 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:88.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Results reported from Bisulfate preserved sample. Confirmation run.
(c) Initial calibration response factors not 8260D compliant.
(d) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(e) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 189
FA6883633.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-1 (2')
Lab Sample ID:FA68836-1 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:88.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006764.D 1 10/15/19 15:22 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 0.94 0.19 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.19 0.021 mg/kg
95-57-8 2-Chlorophenol ND 0.19 0.023 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.19 0.021 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.19 0.050 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.94 0.19 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.37 0.075 mg/kg
95-48-7 2-Methylphenol ND 0.19 0.023 mg/kg
3&4-Methylphenol ND 0.19 0.031 mg/kg
88-75-5 2-Nitrophenol ND 0.19 0.020 mg/kg
100-02-7 4-Nitrophenol ND 0.94 0.19 mg/kg
87-86-5 Pentachlorophenol ND 0.94 0.19 mg/kg
108-95-2 Phenol ND 0.19 0.019 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.19 0.022 mg/kg
83-32-9 Acenaphthene ND 0.19 0.020 mg/kg
208-96-8 Acenaphthylene ND 0.19 0.019 mg/kg
120-12-7 Anthracene ND 0.19 0.021 mg/kg
56-55-3 Benzo(a)anthracene ND 0.19 0.019 mg/kg
50-32-8 Benzo(a)pyrene ND 0.19 0.022 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.19 0.021 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.19 0.019 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.19 0.025 mg/kg
100-51-6 Benzyl Alcohol ND 0.19 0.019 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.19 0.019 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.19 0.037 mg/kg
106-47-8 4-Chloroaniline ND 0.19 0.047 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.19 0.019 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.19 0.022 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.19 0.024 mg/kg
91-58-7 2-Chloronaphthalene ND 0.19 0.019 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.19 0.019 mg/kg
218-01-9 Chrysene ND 0.19 0.019 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 189
FA6883633.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-1 (2')
Lab Sample ID:FA68836-1 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:88.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.19 0.023 mg/kg
132-64-9 Dibenzofuran ND 0.19 0.019 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.19 0.019 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.19 0.020 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.19 0.025 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.19 0.045 mg/kg
84-66-2 Diethyl Phthalate ND 0.37 0.037 mg/kg
131-11-3 Dimethyl Phthalate ND 0.19 0.037 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.19 0.037 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.37 0.075 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 0.19 0.019 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate 0.0818 0.37 0.037 mg/kg J
206-44-0 Fluoranthene ND 0.19 0.019 mg/kg
86-73-7 Fluorene ND 0.19 0.020 mg/kg
118-74-1 Hexachlorobenzene ND 0.19 0.019 mg/kg
87-68-3 Hexachlorobutadiene ND 0.19 0.019 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.19 0.037 mg/kg
67-72-1 Hexachloroethane ND 0.19 0.022 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.19 0.023 mg/kg
78-59-1 Isophorone ND 0.19 0.019 mg/kg
90-12-0 1-Methylnaphthalene ND 0.19 0.019 mg/kg
91-57-6 2-Methylnaphthalene ND 0.19 0.019 mg/kg
91-20-3 Naphthalene ND 0.19 0.019 mg/kg
98-95-3 Nitrobenzene ND 0.19 0.019 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.19 0.019 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.19 0.020 mg/kg
85-01-8 Phenanthrene ND 0.19 0.019 mg/kg
129-00-0 Pyrene ND 0.19 0.022 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.19 0.022 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 64%40-102%
4165-62-2 Phenol-d5 67%41-100%
118-79-6 2,4,6-Tribromophenol 74%42-108%
4165-60-0 Nitrobenzene-d5 63%40-105%
321-60-8 2-Fluorobiphenyl 69%43-107%
1718-51-0 Terphenyl-d14 71%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 189
FA6883633.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-1 (2')
Lab Sample ID:FA68836-1 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:88.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 18.6 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 14.9 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 15.2 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 7.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury 0.063 0.043 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a 2.0 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36236
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
17 of 189
FA6883633.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-2 (2')
Lab Sample ID:FA68836-2 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:89.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13599.D 1 10/11/19 16:39 SP n/a n/a V2B518
Run #2 b 2B13567.D 1 10/10/19 16:08 SP n/a n/a V2B517
Initial Weight Final Volume
Run #1 3.60 g 5.0 ml
Run #2 4.96 g 5.0 ml
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.667 0.31 0.16 mg/kg
71-43-2 Benzene ND 0.0078 0.0019 mg/kg
108-86-1 Bromobenzene ND 0.0078 0.0016 mg/kg
74-97-5 Bromochloromethane ND 0.0078 0.0023 mg/kg
75-27-4 Bromodichloromethane c ND 0.0078 0.0016 mg/kg
75-25-2 Bromoform ND 0.0078 0.0016 mg/kg
78-93-3 2-Butanone (MEK)0.0320 0.039 0.011 mg/kg J
104-51-8 n-Butylbenzene ND 0.0078 0.0016 mg/kg
135-98-8 sec-Butylbenzene ND 0.0078 0.0016 mg/kg
98-06-6 tert-Butylbenzene ND 0.0078 0.0016 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0078 0.0016 mg/kg
108-90-7 Chlorobenzene ND 0.0078 0.0016 mg/kg
75-00-3 Chloroethane d ND 0.0078 0.0031 mg/kg
67-66-3 Chloroform ND 0.0078 0.0021 mg/kg
95-49-8 o-Chlorotoluene ND 0.0078 0.0016 mg/kg
106-43-4 p-Chlorotoluene ND 0.0078 0.0016 mg/kg
124-48-1 Dibromochloromethane ND 0.0078 0.0016 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0078 0.0016 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0078 0.0031 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0078 0.0016 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0078 0.0016 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0078 0.0018 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0078 0.0027 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0078 0.0016 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0078 0.0016 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0078 0.0021 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0078 0.0016 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0078 0.0016 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0078 0.0016 mg/kg
594-20-7 2,2-Dichloropropane e ND 0.0078 0.0016 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0078 0.0016 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0078 0.0016 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 189
FA6883633.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-2 (2')
Lab Sample ID:FA68836-2 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:89.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0078 0.0016 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0078 0.0036 mg/kg
64-17-5 Ethyl Alcohol f 0.185 0.62 0.12 mg/kg J
100-41-4 Ethylbenzene ND 0.0078 0.0016 mg/kg
591-78-6 2-Hexanone ND 0.039 0.012 mg/kg
98-82-8 Isopropylbenzene ND 0.0078 0.0016 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0078 0.0016 mg/kg
74-83-9 Methyl Bromide ND 0.0078 0.0031 mg/kg
74-87-3 Methyl Chloride ND 0.0078 0.0031 mg/kg
75-09-2 Methylene Chloride e ND 0.031 0.017 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.039 0.012 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0078 0.0016 mg/kg
91-20-3 Naphthalene ND 0.0078 0.0031 mg/kg
103-65-1 n-Propylbenzene ND 0.0078 0.0016 mg/kg
100-42-5 Styrene ND 0.0078 0.0016 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0078 0.0016 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0078 0.0016 mg/kg
127-18-4 Tetrachloroethylene ND 0.0078 0.0020 mg/kg
108-88-3 Toluene ND 0.031 0.016 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0078 0.0022 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0078 0.0016 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0078 0.0016 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0078 0.0016 mg/kg
79-01-6 Trichloroethylene ND 0.0078 0.0016 mg/kg
75-69-4 Trichlorofluoromethane e ND 0.0078 0.0031 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0078 0.0019 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0078 0.0016 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0078 0.0016 mg/kg
108-05-4 Vinyl Acetate ND 0.039 0.025 mg/kg
75-01-4 Vinyl Chloride ND 0.0078 0.0016 mg/kg
m,p-Xylene ND 0.016 0.0017 mg/kg
95-47-6 o-Xylene ND 0.0078 0.0016 mg/kg
1330-20-7 Xylene (total)ND 0.023 0.0033 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%99%75-124%
17060-07-0 1,2-Dichloroethane-D4 124%115%72-135%
2037-26-5 Toluene-D8 107%109%75-126%
460-00-4 4-Bromofluorobenzene 108%108%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 189
FA6883633.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-2 (2')
Lab Sample ID:FA68836-2 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:89.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Results reported from Bisulfate preserved sample. Confirmation run.
(c) Initial calibration response factors not 8260D compliant.
(d) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(e) Associated CCV outside of control limits high, sample was ND.
(f) Associated CCV outside of control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 189
FA6883633.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-2 (2')
Lab Sample ID:FA68836-2 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:89.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006767.D 1 10/15/19 16:43 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.5 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 0.91 0.18 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.18 0.021 mg/kg
95-57-8 2-Chlorophenol ND 0.18 0.022 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.18 0.021 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.18 0.049 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.91 0.18 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.37 0.073 mg/kg
95-48-7 2-Methylphenol ND 0.18 0.022 mg/kg
3&4-Methylphenol ND 0.18 0.030 mg/kg
88-75-5 2-Nitrophenol ND 0.18 0.020 mg/kg
100-02-7 4-Nitrophenol ND 0.91 0.18 mg/kg
87-86-5 Pentachlorophenol ND 0.91 0.18 mg/kg
108-95-2 Phenol ND 0.18 0.018 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.18 0.021 mg/kg
83-32-9 Acenaphthene ND 0.18 0.019 mg/kg
208-96-8 Acenaphthylene ND 0.18 0.018 mg/kg
120-12-7 Anthracene ND 0.18 0.020 mg/kg
56-55-3 Benzo(a)anthracene ND 0.18 0.018 mg/kg
50-32-8 Benzo(a)pyrene ND 0.18 0.022 mg/kg
205-99-2 Benzo(b)fluoranthene 0.0341 0.18 0.020 mg/kg J
191-24-2 Benzo(g,h,i)perylene ND 0.18 0.019 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.18 0.024 mg/kg
100-51-6 Benzyl Alcohol ND 0.18 0.018 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.18 0.019 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.18 0.037 mg/kg
106-47-8 4-Chloroaniline ND 0.18 0.046 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.18 0.018 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.18 0.021 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.18 0.023 mg/kg
91-58-7 2-Chloronaphthalene ND 0.18 0.018 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.18 0.018 mg/kg
218-01-9 Chrysene 0.0318 0.18 0.019 mg/kg J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 189
FA6883633.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-2 (2')
Lab Sample ID:FA68836-2 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:89.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.18 0.023 mg/kg
132-64-9 Dibenzofuran ND 0.18 0.018 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.18 0.018 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.18 0.020 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.18 0.024 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.18 0.044 mg/kg
84-66-2 Diethyl Phthalate ND 0.37 0.037 mg/kg
131-11-3 Dimethyl Phthalate ND 0.18 0.037 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.18 0.037 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.37 0.073 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 0.18 0.018 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate 0.0619 0.37 0.037 mg/kg J
206-44-0 Fluoranthene 0.0528 0.18 0.018 mg/kg J
86-73-7 Fluorene ND 0.18 0.020 mg/kg
118-74-1 Hexachlorobenzene ND 0.18 0.019 mg/kg
87-68-3 Hexachlorobutadiene ND 0.18 0.019 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.18 0.037 mg/kg
67-72-1 Hexachloroethane ND 0.18 0.022 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.18 0.022 mg/kg
78-59-1 Isophorone ND 0.18 0.018 mg/kg
90-12-0 1-Methylnaphthalene ND 0.18 0.018 mg/kg
91-57-6 2-Methylnaphthalene ND 0.18 0.018 mg/kg
91-20-3 Naphthalene ND 0.18 0.018 mg/kg
98-95-3 Nitrobenzene ND 0.18 0.018 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.18 0.018 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.18 0.020 mg/kg
85-01-8 Phenanthrene 0.0190 0.18 0.018 mg/kg J
129-00-0 Pyrene 0.0424 0.18 0.021 mg/kg J
120-82-1 1,2,4-Trichlorobenzene ND 0.18 0.022 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 65%40-102%
4165-62-2 Phenol-d5 69%41-100%
118-79-6 2,4,6-Tribromophenol 78%42-108%
4165-60-0 Nitrobenzene-d5 66%40-105%
321-60-8 2-Fluorobiphenyl 73%43-107%
1718-51-0 Terphenyl-d14 77%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 189
FA6883633.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-2 (2')
Lab Sample ID:FA68836-2 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:89.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 10.8 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 104 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 37.5 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 15.8 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.040 0.040 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a 9.6 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36236
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
23 of 189
FA6883633.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-3 (2')
Lab Sample ID:FA68836-3 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:92.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13568.D 1 10/10/19 16:34 SP n/a n/a V2B517
Run #2
Initial Weight Final Volume
Run #1 4.12 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone b 0.161 0.26 0.13 mg/kg J
71-43-2 Benzene ND 0.0065 0.0016 mg/kg
108-86-1 Bromobenzene ND 0.0065 0.0013 mg/kg
74-97-5 Bromochloromethane ND 0.0065 0.0019 mg/kg
75-27-4 Bromodichloromethane c ND 0.0065 0.0013 mg/kg
75-25-2 Bromoform ND 0.0065 0.0013 mg/kg
78-93-3 2-Butanone (MEK)ND 0.033 0.0095 mg/kg
104-51-8 n-Butylbenzene ND 0.0065 0.0013 mg/kg
135-98-8 sec-Butylbenzene ND 0.0065 0.0013 mg/kg
98-06-6 tert-Butylbenzene ND 0.0065 0.0013 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0065 0.0013 mg/kg
108-90-7 Chlorobenzene ND 0.0065 0.0013 mg/kg
75-00-3 Chloroethane d ND 0.0065 0.0026 mg/kg
67-66-3 Chloroform ND 0.0065 0.0017 mg/kg
95-49-8 o-Chlorotoluene ND 0.0065 0.0013 mg/kg
106-43-4 p-Chlorotoluene ND 0.0065 0.0013 mg/kg
124-48-1 Dibromochloromethane ND 0.0065 0.0013 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0065 0.0013 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0065 0.0026 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0065 0.0013 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0065 0.0013 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0065 0.0015 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0065 0.0023 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0065 0.0013 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0065 0.0013 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0065 0.0018 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0065 0.0013 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0065 0.0013 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0065 0.0013 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0065 0.0013 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0065 0.0013 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0065 0.0013 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 189
FA6883633.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-3 (2')
Lab Sample ID:FA68836-3 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:92.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0065 0.0013 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0065 0.0030 mg/kg
64-17-5 Ethyl Alcohol e ND 0.52 0.098 mg/kg
100-41-4 Ethylbenzene ND 0.0065 0.0013 mg/kg
591-78-6 2-Hexanone ND 0.033 0.0098 mg/kg
98-82-8 Isopropylbenzene ND 0.0065 0.0013 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0065 0.0013 mg/kg
74-83-9 Methyl Bromide ND 0.0065 0.0026 mg/kg
74-87-3 Methyl Chloride ND 0.0065 0.0026 mg/kg
75-09-2 Methylene Chloride f ND 0.026 0.014 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.033 0.0098 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0065 0.0013 mg/kg
91-20-3 Naphthalene ND 0.0065 0.0026 mg/kg
103-65-1 n-Propylbenzene ND 0.0065 0.0013 mg/kg
100-42-5 Styrene ND 0.0065 0.0013 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0065 0.0013 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0065 0.0013 mg/kg
127-18-4 Tetrachloroethylene ND 0.0065 0.0017 mg/kg
108-88-3 Toluene ND 0.026 0.013 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0065 0.0018 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0065 0.0013 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0065 0.0013 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0065 0.0013 mg/kg
79-01-6 Trichloroethylene ND 0.0065 0.0013 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0065 0.0026 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0065 0.0016 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0065 0.0013 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0065 0.0013 mg/kg
108-05-4 Vinyl Acetate ND 0.033 0.021 mg/kg
75-01-4 Vinyl Chloride ND 0.0065 0.0013 mg/kg
m,p-Xylene ND 0.013 0.0014 mg/kg
95-47-6 o-Xylene ND 0.0065 0.0013 mg/kg
1330-20-7 Xylene (total)ND 0.020 0.0027 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%75-124%
17060-07-0 1,2-Dichloroethane-D4 114%72-135%
2037-26-5 Toluene-D8 104%75-126%
460-00-4 4-Bromofluorobenzene 103%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 189
FA6883633.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-3 (2')
Lab Sample ID:FA68836-3 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:92.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Associated CCV outside of control limits high.
(c) Initial calibration response factors not 8260D compliant.
(d) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(e) Associated BS recovery outside control limits high; however sample is ND. Associated CCV outside of control
limits high, sample was ND.
(f) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 189
FA6883633.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-3 (2')
Lab Sample ID:FA68836-3 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:92.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006768.D 1 10/15/19 17:10 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.5 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 0.88 0.18 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.18 0.020 mg/kg
95-57-8 2-Chlorophenol ND 0.18 0.022 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.18 0.020 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.18 0.047 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.88 0.18 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.35 0.071 mg/kg
95-48-7 2-Methylphenol ND 0.18 0.021 mg/kg
3&4-Methylphenol ND 0.18 0.029 mg/kg
88-75-5 2-Nitrophenol ND 0.18 0.019 mg/kg
100-02-7 4-Nitrophenol ND 0.88 0.18 mg/kg
87-86-5 Pentachlorophenol ND 0.88 0.18 mg/kg
108-95-2 Phenol ND 0.18 0.018 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.18 0.020 mg/kg
83-32-9 Acenaphthene ND 0.18 0.019 mg/kg
208-96-8 Acenaphthylene ND 0.18 0.018 mg/kg
120-12-7 Anthracene ND 0.18 0.020 mg/kg
56-55-3 Benzo(a)anthracene ND 0.18 0.018 mg/kg
50-32-8 Benzo(a)pyrene ND 0.18 0.021 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.18 0.019 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.18 0.018 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.18 0.023 mg/kg
100-51-6 Benzyl Alcohol ND 0.18 0.018 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.18 0.018 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.18 0.035 mg/kg
106-47-8 4-Chloroaniline ND 0.18 0.044 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.18 0.018 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.18 0.020 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.18 0.022 mg/kg
91-58-7 2-Chloronaphthalene ND 0.18 0.018 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.18 0.018 mg/kg
218-01-9 Chrysene ND 0.18 0.018 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 189
FA6883633.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-3 (2')
Lab Sample ID:FA68836-3 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:92.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.18 0.022 mg/kg
132-64-9 Dibenzofuran ND 0.18 0.018 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.18 0.018 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.18 0.019 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.18 0.024 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.18 0.042 mg/kg
84-66-2 Diethyl Phthalate ND 0.35 0.035 mg/kg
131-11-3 Dimethyl Phthalate ND 0.18 0.035 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.18 0.035 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.35 0.071 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 0.18 0.018 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.35 0.035 mg/kg
206-44-0 Fluoranthene ND 0.18 0.018 mg/kg
86-73-7 Fluorene ND 0.18 0.019 mg/kg
118-74-1 Hexachlorobenzene ND 0.18 0.018 mg/kg
87-68-3 Hexachlorobutadiene ND 0.18 0.018 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.18 0.035 mg/kg
67-72-1 Hexachloroethane ND 0.18 0.021 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.18 0.021 mg/kg
78-59-1 Isophorone ND 0.18 0.018 mg/kg
90-12-0 1-Methylnaphthalene ND 0.18 0.018 mg/kg
91-57-6 2-Methylnaphthalene ND 0.18 0.018 mg/kg
91-20-3 Naphthalene ND 0.18 0.018 mg/kg
98-95-3 Nitrobenzene ND 0.18 0.018 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.18 0.018 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.18 0.019 mg/kg
85-01-8 Phenanthrene ND 0.18 0.018 mg/kg
129-00-0 Pyrene ND 0.18 0.020 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.18 0.021 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 65%40-102%
4165-62-2 Phenol-d5 70%41-100%
118-79-6 2,4,6-Tribromophenol 77%42-108%
4165-60-0 Nitrobenzene-d5 65%40-105%
321-60-8 2-Fluorobiphenyl 71%43-107%
1718-51-0 Terphenyl-d14 75%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 189
FA6883633.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-3 (2')
Lab Sample ID:FA68836-3 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:92.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 2.4 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 25.0 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <1.0 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 8.9 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 6.9 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.038 0.038 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a <1.0 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <1.0 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36236
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
29 of 189
FA6883633.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-4 (2')
Lab Sample ID:FA68836-4 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:83.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13569.D 1 10/10/19 17:00 SP n/a n/a V2B517
Run #2 b 2B13600.D 1 10/11/19 17:05 SP n/a n/a V2B518
Initial Weight Final Volume
Run #1 3.77 g 5.0 ml
Run #2 3.78 g 5.0 ml
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.536 c 0.32 0.16 mg/kg
71-43-2 Benzene ND 0.0079 0.0019 mg/kg
108-86-1 Bromobenzene ND 0.0079 0.0016 mg/kg
74-97-5 Bromochloromethane ND 0.0079 0.0023 mg/kg
75-27-4 Bromodichloromethane d ND 0.0079 0.0016 mg/kg
75-25-2 Bromoform ND 0.0079 0.0016 mg/kg
78-93-3 2-Butanone (MEK)ND 0.040 0.012 mg/kg
104-51-8 n-Butylbenzene ND 0.0079 0.0016 mg/kg
135-98-8 sec-Butylbenzene ND 0.0079 0.0016 mg/kg
98-06-6 tert-Butylbenzene ND 0.0079 0.0016 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0079 0.0016 mg/kg
108-90-7 Chlorobenzene ND 0.0079 0.0016 mg/kg
75-00-3 Chloroethane e ND 0.0079 0.0032 mg/kg
67-66-3 Chloroform ND 0.0079 0.0021 mg/kg
95-49-8 o-Chlorotoluene ND 0.0079 0.0016 mg/kg
106-43-4 p-Chlorotoluene ND 0.0079 0.0016 mg/kg
124-48-1 Dibromochloromethane ND 0.0079 0.0016 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0079 0.0016 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0079 0.0032 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0079 0.0016 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0079 0.0016 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0079 0.0018 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0079 0.0028 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0079 0.0016 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0079 0.0016 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0079 0.0022 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0079 0.0016 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0079 0.0016 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0079 0.0016 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0079 0.0016 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0079 0.0016 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0079 0.0016 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 189
FA6883633.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-4 (2')
Lab Sample ID:FA68836-4 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:83.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0079 0.0016 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0079 0.0037 mg/kg
64-17-5 Ethyl Alcohol f ND 0.63 0.12 mg/kg
100-41-4 Ethylbenzene ND 0.0079 0.0016 mg/kg
591-78-6 2-Hexanone ND 0.040 0.012 mg/kg
98-82-8 Isopropylbenzene ND 0.0079 0.0016 mg/kg
99-87-6 p-Isopropyltoluene 0.0161 0.0079 0.0016 mg/kg
74-83-9 Methyl Bromide ND 0.0079 0.0032 mg/kg
74-87-3 Methyl Chloride ND 0.0079 0.0032 mg/kg
75-09-2 Methylene Chloride g ND 0.032 0.017 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.040 0.012 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0079 0.0016 mg/kg
91-20-3 Naphthalene ND 0.0079 0.0032 mg/kg
103-65-1 n-Propylbenzene ND 0.0079 0.0016 mg/kg
100-42-5 Styrene ND 0.0079 0.0016 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0079 0.0016 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0079 0.0016 mg/kg
127-18-4 Tetrachloroethylene ND 0.0079 0.0020 mg/kg
108-88-3 Toluene ND 0.032 0.016 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0079 0.0022 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0079 0.0016 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0079 0.0016 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0079 0.0016 mg/kg
79-01-6 Trichloroethylene ND 0.0079 0.0016 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0079 0.0032 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0079 0.0020 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0079 0.0016 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0079 0.0016 mg/kg
108-05-4 Vinyl Acetate ND 0.040 0.026 mg/kg
75-01-4 Vinyl Chloride ND 0.0079 0.0016 mg/kg
m,p-Xylene ND 0.016 0.0017 mg/kg
95-47-6 o-Xylene ND 0.0079 0.0016 mg/kg
1330-20-7 Xylene (total)ND 0.024 0.0033 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%102%75-124%
17060-07-0 1,2-Dichloroethane-D4 114%120%72-135%
2037-26-5 Toluene-D8 101%103%75-126%
460-00-4 4-Bromofluorobenzene 94%87%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 189
FA6883633.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-4 (2')
Lab Sample ID:FA68836-4 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:83.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample. Internal standard response outside control limits. Confirmed
by MS/MSD.
(b) Results reported from Bisulfate preserved sample.
(c) Result is from Run# 2
(d) Initial calibration response factors not 8260D compliant.
(e) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(f) Associated BS recovery outside control limits high; however sample is ND. Associated CCV outside of control
limits high, sample was ND.
(g) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 189
FA6883633.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-4 (2')
Lab Sample ID:FA68836-4 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:83.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006769.D 1 10/15/19 17:37 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 0.99 0.20 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.20 0.022 mg/kg
95-57-8 2-Chlorophenol ND 0.20 0.024 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.20 0.023 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.20 0.053 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.99 0.20 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.40 0.080 mg/kg
95-48-7 2-Methylphenol ND 0.20 0.024 mg/kg
3&4-Methylphenol ND 0.20 0.033 mg/kg
88-75-5 2-Nitrophenol ND 0.20 0.022 mg/kg
100-02-7 4-Nitrophenol ND 0.99 0.20 mg/kg
87-86-5 Pentachlorophenol ND 0.99 0.20 mg/kg
108-95-2 Phenol ND 0.20 0.020 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.20 0.023 mg/kg
83-32-9 Acenaphthene ND 0.20 0.021 mg/kg
208-96-8 Acenaphthylene ND 0.20 0.020 mg/kg
120-12-7 Anthracene ND 0.20 0.022 mg/kg
56-55-3 Benzo(a)anthracene ND 0.20 0.020 mg/kg
50-32-8 Benzo(a)pyrene ND 0.20 0.023 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.20 0.022 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.20 0.021 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.20 0.026 mg/kg
100-51-6 Benzyl Alcohol ND 0.20 0.020 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.20 0.021 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.20 0.040 mg/kg
106-47-8 4-Chloroaniline ND 0.20 0.050 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.20 0.020 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.20 0.023 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.20 0.025 mg/kg
91-58-7 2-Chloronaphthalene ND 0.20 0.020 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.20 0.020 mg/kg
218-01-9 Chrysene ND 0.20 0.020 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 189
FA6883633.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-4 (2')
Lab Sample ID:FA68836-4 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:83.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.20 0.025 mg/kg
132-64-9 Dibenzofuran ND 0.20 0.020 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.20 0.020 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.20 0.021 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.20 0.026 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.20 0.047 mg/kg
84-66-2 Diethyl Phthalate ND 0.40 0.040 mg/kg
131-11-3 Dimethyl Phthalate ND 0.20 0.040 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.20 0.040 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.40 0.080 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 0.20 0.020 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate 0.0516 0.40 0.040 mg/kg J
206-44-0 Fluoranthene ND 0.20 0.020 mg/kg
86-73-7 Fluorene ND 0.20 0.021 mg/kg
118-74-1 Hexachlorobenzene ND 0.20 0.020 mg/kg
87-68-3 Hexachlorobutadiene ND 0.20 0.020 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.20 0.040 mg/kg
67-72-1 Hexachloroethane ND 0.20 0.023 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.20 0.024 mg/kg
78-59-1 Isophorone ND 0.20 0.020 mg/kg
90-12-0 1-Methylnaphthalene ND 0.20 0.020 mg/kg
91-57-6 2-Methylnaphthalene ND 0.20 0.020 mg/kg
91-20-3 Naphthalene ND 0.20 0.020 mg/kg
98-95-3 Nitrobenzene ND 0.20 0.020 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.20 0.020 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.20 0.021 mg/kg
85-01-8 Phenanthrene ND 0.20 0.020 mg/kg
129-00-0 Pyrene ND 0.20 0.023 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.023 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 68%40-102%
4165-62-2 Phenol-d5 72%41-100%
118-79-6 2,4,6-Tribromophenol 83%42-108%
4165-60-0 Nitrobenzene-d5 69%40-105%
321-60-8 2-Fluorobiphenyl 74%43-107%
1718-51-0 Terphenyl-d14 79%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 189
FA6883633.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-4 (2')
Lab Sample ID:FA68836-4 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:83.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 7.3 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 36.0 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 32.5 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 6.5 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.045 0.045 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36236
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
35 of 189
FA6883633.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-5 (2')
Lab Sample ID:FA68836-5 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:81.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13601.D 1 10/11/19 17:31 SP n/a n/a V2B518
Run #2 b 2B13570.D 1 10/10/19 17:25 SP n/a n/a V2B517
Initial Weight Final Volume
Run #1 3.20 g 5.0 ml
Run #2 3.97 g 5.0 ml
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.199 0.38 0.19 mg/kg J
71-43-2 Benzene ND 0.0096 0.0023 mg/kg
108-86-1 Bromobenzene ND 0.0096 0.0019 mg/kg
74-97-5 Bromochloromethane ND 0.0096 0.0028 mg/kg
75-27-4 Bromodichloromethane c ND 0.0096 0.0019 mg/kg
75-25-2 Bromoform ND 0.0096 0.0019 mg/kg
78-93-3 2-Butanone (MEK)ND 0.048 0.014 mg/kg
104-51-8 n-Butylbenzene ND 0.0096 0.0019 mg/kg
135-98-8 sec-Butylbenzene ND 0.0096 0.0019 mg/kg
98-06-6 tert-Butylbenzene ND 0.0096 0.0019 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0096 0.0019 mg/kg
108-90-7 Chlorobenzene ND 0.0096 0.0019 mg/kg
75-00-3 Chloroethane d ND 0.0096 0.0038 mg/kg
67-66-3 Chloroform ND 0.0096 0.0025 mg/kg
95-49-8 o-Chlorotoluene ND 0.0096 0.0019 mg/kg
106-43-4 p-Chlorotoluene ND 0.0096 0.0019 mg/kg
124-48-1 Dibromochloromethane ND 0.0096 0.0019 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0096 0.0019 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0096 0.0038 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0096 0.0019 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0096 0.0019 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0096 0.0022 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0096 0.0034 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0096 0.0019 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0096 0.0019 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0096 0.0026 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0096 0.0019 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0096 0.0019 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0096 0.0019 mg/kg
594-20-7 2,2-Dichloropropane e ND 0.0096 0.0019 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0096 0.0019 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0096 0.0019 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 189
FA6883633.5
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-5 (2')
Lab Sample ID:FA68836-5 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:81.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0096 0.0019 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0096 0.0044 mg/kg
64-17-5 Ethyl Alcohol e ND 0.76 0.14 mg/kg
100-41-4 Ethylbenzene ND 0.0096 0.0019 mg/kg
591-78-6 2-Hexanone ND 0.048 0.014 mg/kg
98-82-8 Isopropylbenzene ND 0.0096 0.0019 mg/kg
99-87-6 p-Isopropyltoluene 0.0058 0.0096 0.0019 mg/kg J
74-83-9 Methyl Bromide ND 0.0096 0.0038 mg/kg
74-87-3 Methyl Chloride ND 0.0096 0.0038 mg/kg
75-09-2 Methylene Chloride e ND 0.038 0.021 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.048 0.014 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0096 0.0019 mg/kg
91-20-3 Naphthalene ND 0.0096 0.0038 mg/kg
103-65-1 n-Propylbenzene ND 0.0096 0.0019 mg/kg
100-42-5 Styrene ND 0.0096 0.0019 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0096 0.0020 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0096 0.0019 mg/kg
127-18-4 Tetrachloroethylene ND 0.0096 0.0024 mg/kg
108-88-3 Toluene ND 0.038 0.019 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0096 0.0027 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0096 0.0019 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0096 0.0019 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0096 0.0019 mg/kg
79-01-6 Trichloroethylene ND 0.0096 0.0019 mg/kg
75-69-4 Trichlorofluoromethane e ND 0.0096 0.0038 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0096 0.0024 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0096 0.0019 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0096 0.0019 mg/kg
108-05-4 Vinyl Acetate ND 0.048 0.031 mg/kg
75-01-4 Vinyl Chloride ND 0.0096 0.0019 mg/kg
m,p-Xylene ND 0.019 0.0021 mg/kg
95-47-6 o-Xylene ND 0.0096 0.0019 mg/kg
1330-20-7 Xylene (total)ND 0.029 0.0040 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%100%75-124%
17060-07-0 1,2-Dichloroethane-D4 120%115%72-135%
2037-26-5 Toluene-D8 104%100%75-126%
460-00-4 4-Bromofluorobenzene 85%91%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 189
FA6883633.5
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-5 (2')
Lab Sample ID:FA68836-5 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:81.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Results reported from Bisulfate preserved sample. Confirmation run for internal standard areas.
(c) Initial calibration response factors not 8260D compliant.
(d) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(e) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 189
FA6883633.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-5 (2')
Lab Sample ID:FA68836-5 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:81.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006770.D 1 10/15/19 18:04 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1.0 0.20 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.20 0.023 mg/kg
95-57-8 2-Chlorophenol ND 0.20 0.025 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.20 0.023 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.20 0.054 mg/kg
51-28-5 2,4-Dinitrophenol ND 1.0 0.20 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.40 0.081 mg/kg
95-48-7 2-Methylphenol ND 0.20 0.024 mg/kg
3&4-Methylphenol ND 0.20 0.033 mg/kg
88-75-5 2-Nitrophenol ND 0.20 0.022 mg/kg
100-02-7 4-Nitrophenol ND 1.0 0.20 mg/kg
87-86-5 Pentachlorophenol ND 1.0 0.20 mg/kg
108-95-2 Phenol ND 0.20 0.020 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.20 0.023 mg/kg
83-32-9 Acenaphthene ND 0.20 0.021 mg/kg
208-96-8 Acenaphthylene ND 0.20 0.020 mg/kg
120-12-7 Anthracene ND 0.20 0.023 mg/kg
56-55-3 Benzo(a)anthracene ND 0.20 0.020 mg/kg
50-32-8 Benzo(a)pyrene ND 0.20 0.024 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.20 0.022 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.20 0.021 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.20 0.026 mg/kg
100-51-6 Benzyl Alcohol ND 0.20 0.020 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.20 0.021 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.20 0.040 mg/kg
106-47-8 4-Chloroaniline ND 0.20 0.051 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.20 0.020 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.20 0.023 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.20 0.025 mg/kg
91-58-7 2-Chloronaphthalene ND 0.20 0.020 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.20 0.020 mg/kg
218-01-9 Chrysene ND 0.20 0.021 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 189
FA6883633.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-5 (2')
Lab Sample ID:FA68836-5 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:81.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.20 0.025 mg/kg
132-64-9 Dibenzofuran ND 0.20 0.020 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.20 0.020 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.20 0.022 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.20 0.027 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.20 0.048 mg/kg
84-66-2 Diethyl Phthalate ND 0.40 0.040 mg/kg
131-11-3 Dimethyl Phthalate ND 0.20 0.040 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.20 0.040 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.40 0.081 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 0.20 0.020 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.40 0.040 mg/kg
206-44-0 Fluoranthene ND 0.20 0.020 mg/kg
86-73-7 Fluorene ND 0.20 0.022 mg/kg
118-74-1 Hexachlorobenzene ND 0.20 0.021 mg/kg
87-68-3 Hexachlorobutadiene ND 0.20 0.020 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.20 0.040 mg/kg
67-72-1 Hexachloroethane ND 0.20 0.024 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.20 0.025 mg/kg
78-59-1 Isophorone ND 0.20 0.020 mg/kg
90-12-0 1-Methylnaphthalene ND 0.20 0.020 mg/kg
91-57-6 2-Methylnaphthalene ND 0.20 0.020 mg/kg
91-20-3 Naphthalene ND 0.20 0.020 mg/kg
98-95-3 Nitrobenzene ND 0.20 0.020 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.20 0.020 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.20 0.022 mg/kg
85-01-8 Phenanthrene ND 0.20 0.020 mg/kg
129-00-0 Pyrene ND 0.20 0.023 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.024 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 68%40-102%
4165-62-2 Phenol-d5 72%41-100%
118-79-6 2,4,6-Tribromophenol 78%42-108%
4165-60-0 Nitrobenzene-d5 68%40-105%
321-60-8 2-Fluorobiphenyl 72%43-107%
1718-51-0 Terphenyl-d14 75%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 189
FA6883633.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-5 (2')
Lab Sample ID:FA68836-5 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:81.8
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 4.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 57.6 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 39.6 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 16.0 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury 0.074 0.044 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36236
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
41 of 189
FA6883633.5
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-6 (2')
Lab Sample ID:FA68836-6 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:93.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13571.D 1 10/10/19 17:50 SP n/a n/a V2B517
Run #2 a 2B13602.D 1 10/11/19 17:57 SP n/a n/a V2B518
Initial Weight Final Volume
Run #1 4.69 g 5.0 ml
Run #2 4.69 g 5.0 ml
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.376 b 0.23 0.11 mg/kg
71-43-2 Benzene ND 0.0057 0.0014 mg/kg
108-86-1 Bromobenzene ND 0.0057 0.0011 mg/kg
74-97-5 Bromochloromethane ND 0.0057 0.0017 mg/kg
75-27-4 Bromodichloromethane c ND 0.0057 0.0011 mg/kg
75-25-2 Bromoform ND 0.0057 0.0011 mg/kg
78-93-3 2-Butanone (MEK)ND 0.029 0.0083 mg/kg
104-51-8 n-Butylbenzene ND 0.0057 0.0011 mg/kg
135-98-8 sec-Butylbenzene ND 0.0057 0.0011 mg/kg
98-06-6 tert-Butylbenzene ND 0.0057 0.0011 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0057 0.0012 mg/kg
108-90-7 Chlorobenzene ND 0.0057 0.0011 mg/kg
75-00-3 Chloroethane d ND 0.0057 0.0023 mg/kg
67-66-3 Chloroform ND 0.0057 0.0015 mg/kg
95-49-8 o-Chlorotoluene ND 0.0057 0.0011 mg/kg
106-43-4 p-Chlorotoluene ND 0.0057 0.0011 mg/kg
124-48-1 Dibromochloromethane ND 0.0057 0.0011 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0057 0.0011 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0057 0.0023 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0057 0.0011 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0057 0.0011 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0057 0.0013 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0057 0.0020 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0057 0.0011 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0057 0.0011 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0057 0.0016 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0057 0.0011 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0057 0.0011 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0057 0.0011 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0057 0.0011 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0057 0.0012 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0057 0.0011 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 189
FA6883633.6
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-6 (2')
Lab Sample ID:FA68836-6 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:93.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0057 0.0011 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0057 0.0027 mg/kg
64-17-5 Ethyl Alcohol e ND 0.46 0.086 mg/kg
100-41-4 Ethylbenzene ND 0.0057 0.0011 mg/kg
591-78-6 2-Hexanone ND 0.029 0.0086 mg/kg
98-82-8 Isopropylbenzene ND 0.0057 0.0011 mg/kg
99-87-6 p-Isopropyltoluene 0.0121 0.0057 0.0011 mg/kg
74-83-9 Methyl Bromide ND 0.0057 0.0023 mg/kg
74-87-3 Methyl Chloride ND 0.0057 0.0023 mg/kg
75-09-2 Methylene Chloride f ND 0.023 0.013 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.029 0.0086 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0057 0.0011 mg/kg
91-20-3 Naphthalene ND 0.0057 0.0023 mg/kg
103-65-1 n-Propylbenzene ND 0.0057 0.0011 mg/kg
100-42-5 Styrene ND 0.0057 0.0011 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0057 0.0012 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0057 0.0011 mg/kg
127-18-4 Tetrachloroethylene ND 0.0057 0.0015 mg/kg
108-88-3 Toluene ND 0.023 0.011 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0057 0.0016 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0057 0.0011 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0057 0.0011 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0057 0.0011 mg/kg
79-01-6 Trichloroethylene ND 0.0057 0.0011 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0057 0.0023 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0057 0.0014 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0057 0.0011 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0057 0.0011 mg/kg
108-05-4 Vinyl Acetate ND 0.029 0.019 mg/kg
75-01-4 Vinyl Chloride ND 0.0057 0.0011 mg/kg
m,p-Xylene ND 0.011 0.0013 mg/kg
95-47-6 o-Xylene ND 0.0057 0.0011 mg/kg
1330-20-7 Xylene (total)ND 0.017 0.0024 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%103%75-124%
17060-07-0 1,2-Dichloroethane-D4 115%120%72-135%
2037-26-5 Toluene-D8 101%99%75-126%
460-00-4 4-Bromofluorobenzene 95%92%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 189
FA6883633.6
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-6 (2')
Lab Sample ID:FA68836-6 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:93.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Result is from Run# 2
(c) Initial calibration response factors not 8260D compliant.
(d) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(e) Associated BS recovery outside control limits high; however sample is ND. Associated CCV outside of control
limits high, sample was ND.
(f) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 189
FA6883633.6
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-6 (2')
Lab Sample ID:FA68836-6 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:93.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006771.D 1 10/15/19 18:31 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid 1.49 0.90 0.18 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.18 0.020 mg/kg
95-57-8 2-Chlorophenol ND 0.18 0.022 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.18 0.021 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.18 0.048 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.90 0.18 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.36 0.072 mg/kg
95-48-7 2-Methylphenol ND 0.18 0.022 mg/kg
3&4-Methylphenol ND 0.18 0.029 mg/kg
88-75-5 2-Nitrophenol ND 0.18 0.019 mg/kg
100-02-7 4-Nitrophenol ND 0.90 0.18 mg/kg
87-86-5 Pentachlorophenol ND 0.90 0.18 mg/kg
108-95-2 Phenol ND 0.18 0.018 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.18 0.021 mg/kg
83-32-9 Acenaphthene ND 0.18 0.019 mg/kg
208-96-8 Acenaphthylene ND 0.18 0.018 mg/kg
120-12-7 Anthracene ND 0.18 0.020 mg/kg
56-55-3 Benzo(a)anthracene ND 0.18 0.018 mg/kg
50-32-8 Benzo(a)pyrene ND 0.18 0.021 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.18 0.020 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.18 0.019 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.18 0.023 mg/kg
100-51-6 Benzyl Alcohol ND 0.18 0.018 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.18 0.019 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.18 0.036 mg/kg
106-47-8 4-Chloroaniline ND 0.18 0.045 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.18 0.018 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.18 0.021 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.18 0.023 mg/kg
91-58-7 2-Chloronaphthalene ND 0.18 0.018 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.18 0.018 mg/kg
218-01-9 Chrysene ND 0.18 0.018 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 189
FA6883633.6
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-6 (2')
Lab Sample ID:FA68836-6 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:93.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.18 0.022 mg/kg
132-64-9 Dibenzofuran ND 0.18 0.018 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.18 0.018 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.18 0.019 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.18 0.024 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.18 0.043 mg/kg
84-66-2 Diethyl Phthalate ND 0.36 0.036 mg/kg
131-11-3 Dimethyl Phthalate ND 0.18 0.036 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.18 0.036 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.36 0.072 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 0.18 0.018 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.36 0.036 mg/kg
206-44-0 Fluoranthene ND 0.18 0.018 mg/kg
86-73-7 Fluorene ND 0.18 0.019 mg/kg
118-74-1 Hexachlorobenzene ND 0.18 0.018 mg/kg
87-68-3 Hexachlorobutadiene ND 0.18 0.018 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.18 0.036 mg/kg
67-72-1 Hexachloroethane ND 0.18 0.021 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.18 0.022 mg/kg
78-59-1 Isophorone ND 0.18 0.018 mg/kg
90-12-0 1-Methylnaphthalene ND 0.18 0.018 mg/kg
91-57-6 2-Methylnaphthalene ND 0.18 0.018 mg/kg
91-20-3 Naphthalene ND 0.18 0.018 mg/kg
98-95-3 Nitrobenzene ND 0.18 0.018 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.18 0.018 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.18 0.019 mg/kg
85-01-8 Phenanthrene ND 0.18 0.018 mg/kg
129-00-0 Pyrene ND 0.18 0.021 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.18 0.021 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 63%40-102%
4165-62-2 Phenol-d5 68%41-100%
118-79-6 2,4,6-Tribromophenol 77%42-108%
4165-60-0 Nitrobenzene-d5 65%40-105%
321-60-8 2-Fluorobiphenyl 71%43-107%
1718-51-0 Terphenyl-d14 76%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 189
FA6883633.6
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-6 (2')
Lab Sample ID:FA68836-6 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:93.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 3.2 0.83 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 11.8 0.83 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <0.83 0.83 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 31.4 0.83 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 7.2 0.83 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.042 0.042 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a 0.93 0.83 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <0.83 0.83 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36236
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
47 of 189
FA6883633.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SB-7 (2')
Lab Sample ID:FA68836-7 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13572.D 1 10/10/19 18:16 SP n/a n/a V2B517
Run #2 a 2B13603.D 1 10/11/19 18:22 SP n/a n/a V2B518
Initial Weight Final Volume
Run #1 4.49 g 5.0 ml
Run #2 3.67 g 5.0 ml
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.414 b 0.30 0.15 mg/kg
71-43-2 Benzene ND 0.0061 0.0015 mg/kg
108-86-1 Bromobenzene ND 0.0061 0.0012 mg/kg
74-97-5 Bromochloromethane ND 0.0061 0.0018 mg/kg
75-27-4 Bromodichloromethane c ND 0.0061 0.0012 mg/kg
75-25-2 Bromoform ND 0.0061 0.0012 mg/kg
78-93-3 2-Butanone (MEK)0.0128 0.030 0.0088 mg/kg J
104-51-8 n-Butylbenzene ND 0.0061 0.0012 mg/kg
135-98-8 sec-Butylbenzene ND 0.0061 0.0012 mg/kg
98-06-6 tert-Butylbenzene ND 0.0061 0.0012 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0061 0.0012 mg/kg
108-90-7 Chlorobenzene ND 0.0061 0.0012 mg/kg
75-00-3 Chloroethane d ND 0.0061 0.0024 mg/kg
67-66-3 Chloroform ND 0.0061 0.0016 mg/kg
95-49-8 o-Chlorotoluene ND 0.0061 0.0012 mg/kg
106-43-4 p-Chlorotoluene ND 0.0061 0.0012 mg/kg
124-48-1 Dibromochloromethane ND 0.0061 0.0012 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0061 0.0012 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0061 0.0024 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0061 0.0012 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0061 0.0012 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0061 0.0014 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0061 0.0021 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0061 0.0012 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0061 0.0012 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0061 0.0017 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0061 0.0012 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0061 0.0012 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0061 0.0012 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0061 0.0012 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0061 0.0012 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0061 0.0012 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 189
FA6883633.7
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SB-7 (2')
Lab Sample ID:FA68836-7 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0061 0.0012 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0061 0.0028 mg/kg
64-17-5 Ethyl Alcohol e 0.120 0.48 0.091 mg/kg J
100-41-4 Ethylbenzene ND 0.0061 0.0012 mg/kg
591-78-6 2-Hexanone ND 0.030 0.0091 mg/kg
98-82-8 Isopropylbenzene ND 0.0061 0.0012 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0061 0.0012 mg/kg
74-83-9 Methyl Bromide ND 0.0061 0.0024 mg/kg
74-87-3 Methyl Chloride ND 0.0061 0.0024 mg/kg
75-09-2 Methylene Chloride f ND 0.024 0.013 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.030 0.0091 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0061 0.0012 mg/kg
91-20-3 Naphthalene ND 0.0061 0.0024 mg/kg
103-65-1 n-Propylbenzene ND 0.0061 0.0012 mg/kg
100-42-5 Styrene ND 0.0061 0.0012 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0061 0.0012 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0061 0.0012 mg/kg
127-18-4 Tetrachloroethylene ND 0.0061 0.0016 mg/kg
108-88-3 Toluene ND 0.024 0.012 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0061 0.0017 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0061 0.0012 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0061 0.0012 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0061 0.0012 mg/kg
79-01-6 Trichloroethylene ND 0.0061 0.0012 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0061 0.0024 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0061 0.0015 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0061 0.0012 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0061 0.0012 mg/kg
108-05-4 Vinyl Acetate ND 0.030 0.020 mg/kg
75-01-4 Vinyl Chloride ND 0.0061 0.0012 mg/kg
m,p-Xylene ND 0.012 0.0013 mg/kg
95-47-6 o-Xylene ND 0.0061 0.0012 mg/kg
1330-20-7 Xylene (total)ND 0.018 0.0025 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%104%75-124%
17060-07-0 1,2-Dichloroethane-D4 115%122%72-135%
2037-26-5 Toluene-D8 102%101%75-126%
460-00-4 4-Bromofluorobenzene 101%98%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
49 of 189
FA6883633.7
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SB-7 (2')
Lab Sample ID:FA68836-7 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Result is from Run# 2
(c) Initial calibration response factors not 8260D compliant.
(d) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(e) Associated BS recovery outside control limits high. Associated CCV outside of control limits high. Results
from different vials are not consistent; higher results were reported.
(f) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
50 of 189
FA6883633.7
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-7 (2')
Lab Sample ID:FA68836-7 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006772.D 1 10/15/19 18:57 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 0.90 0.18 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.18 0.020 mg/kg
95-57-8 2-Chlorophenol ND 0.18 0.022 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.18 0.021 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.18 0.048 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.90 0.18 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.36 0.072 mg/kg
95-48-7 2-Methylphenol ND 0.18 0.022 mg/kg
3&4-Methylphenol ND 0.18 0.030 mg/kg
88-75-5 2-Nitrophenol ND 0.18 0.020 mg/kg
100-02-7 4-Nitrophenol ND 0.90 0.18 mg/kg
87-86-5 Pentachlorophenol ND 0.90 0.18 mg/kg
108-95-2 Phenol ND 0.18 0.018 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.18 0.021 mg/kg
83-32-9 Acenaphthene ND 0.18 0.019 mg/kg
208-96-8 Acenaphthylene ND 0.18 0.018 mg/kg
120-12-7 Anthracene ND 0.18 0.020 mg/kg
56-55-3 Benzo(a)anthracene ND 0.18 0.018 mg/kg
50-32-8 Benzo(a)pyrene ND 0.18 0.021 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.18 0.020 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.18 0.019 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.18 0.024 mg/kg
100-51-6 Benzyl Alcohol ND 0.18 0.018 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.18 0.019 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.18 0.036 mg/kg
106-47-8 4-Chloroaniline ND 0.18 0.046 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.18 0.018 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.18 0.021 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.18 0.023 mg/kg
91-58-7 2-Chloronaphthalene ND 0.18 0.018 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.18 0.018 mg/kg
218-01-9 Chrysene ND 0.18 0.018 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
51 of 189
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SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-7 (2')
Lab Sample ID:FA68836-7 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.18 0.023 mg/kg
132-64-9 Dibenzofuran ND 0.18 0.018 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.18 0.018 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.18 0.020 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.18 0.024 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.18 0.043 mg/kg
84-66-2 Diethyl Phthalate ND 0.36 0.036 mg/kg
131-11-3 Dimethyl Phthalate ND 0.18 0.036 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.18 0.036 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.36 0.072 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 0.18 0.018 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate 0.0403 0.36 0.036 mg/kg J
206-44-0 Fluoranthene ND 0.18 0.018 mg/kg
86-73-7 Fluorene ND 0.18 0.019 mg/kg
118-74-1 Hexachlorobenzene ND 0.18 0.018 mg/kg
87-68-3 Hexachlorobutadiene ND 0.18 0.018 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.18 0.036 mg/kg
67-72-1 Hexachloroethane ND 0.18 0.021 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.18 0.022 mg/kg
78-59-1 Isophorone ND 0.18 0.018 mg/kg
90-12-0 1-Methylnaphthalene ND 0.18 0.018 mg/kg
91-57-6 2-Methylnaphthalene ND 0.18 0.018 mg/kg
91-20-3 Naphthalene ND 0.18 0.018 mg/kg
98-95-3 Nitrobenzene ND 0.18 0.018 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.18 0.018 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.18 0.019 mg/kg
85-01-8 Phenanthrene ND 0.18 0.018 mg/kg
129-00-0 Pyrene ND 0.18 0.021 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.18 0.021 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 66%40-102%
4165-62-2 Phenol-d5 69%41-100%
118-79-6 2,4,6-Tribromophenol 77%42-108%
4165-60-0 Nitrobenzene-d5 67%40-105%
321-60-8 2-Fluorobiphenyl 71%43-107%
1718-51-0 Terphenyl-d14 75%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
52 of 189
FA6883633.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-7 (2')
Lab Sample ID:FA68836-7 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 1.8 0.98 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 35.9 0.98 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <0.98 0.98 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 14.0 0.98 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 10.3 0.98 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.042 0.042 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a 1.2 0.98 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <0.98 0.98 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36236
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
53 of 189
FA6883633.7
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SOIL-DUP-A
Lab Sample ID:FA68836-8 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:87.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13573.D 1 10/10/19 18:42 SP n/a n/a V2B517
Run #2 b 2B13604.D 1 10/11/19 18:48 SP n/a n/a V2B518
Initial Weight Final Volume
Run #1 5.60 g 5.0 ml
Run #2 4.84 g 5.0 ml
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone c 0.157 0.20 0.10 mg/kg J
71-43-2 Benzene ND 0.0051 0.0012 mg/kg
108-86-1 Bromobenzene ND 0.0051 0.0010 mg/kg
74-97-5 Bromochloromethane ND 0.0051 0.0015 mg/kg
75-27-4 Bromodichloromethane d ND 0.0051 0.0010 mg/kg
75-25-2 Bromoform ND 0.0051 0.0010 mg/kg
78-93-3 2-Butanone (MEK)ND 0.026 0.0074 mg/kg
104-51-8 n-Butylbenzene ND 0.0051 0.0010 mg/kg
135-98-8 sec-Butylbenzene ND 0.0051 0.0010 mg/kg
98-06-6 tert-Butylbenzene ND 0.0051 0.0010 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0051 0.0010 mg/kg
108-90-7 Chlorobenzene ND 0.0051 0.0010 mg/kg
75-00-3 Chloroethane e ND 0.0051 0.0020 mg/kg
67-66-3 Chloroform ND 0.0051 0.0014 mg/kg
95-49-8 o-Chlorotoluene ND 0.0051 0.0010 mg/kg
106-43-4 p-Chlorotoluene ND 0.0051 0.0010 mg/kg
124-48-1 Dibromochloromethane ND 0.0051 0.0010 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0051 0.0010 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0051 0.0020 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0051 0.0010 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0051 0.0010 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0051 0.0012 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0051 0.0018 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0051 0.0010 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0051 0.0010 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0051 0.0014 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0051 0.0010 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0051 0.0010 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0051 0.0010 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0051 0.0010 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0051 0.0010 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0051 0.0010 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
54 of 189
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SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SOIL-DUP-A
Lab Sample ID:FA68836-8 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:87.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0051 0.0010 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0051 0.0024 mg/kg
64-17-5 Ethyl Alcohol f 0.355 0.41 0.077 mg/kg J
100-41-4 Ethylbenzene ND 0.0051 0.0010 mg/kg
591-78-6 2-Hexanone ND 0.026 0.0077 mg/kg
98-82-8 Isopropylbenzene ND 0.0051 0.0010 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0051 0.0010 mg/kg
74-83-9 Methyl Bromide ND 0.0051 0.0020 mg/kg
74-87-3 Methyl Chloride ND 0.0051 0.0020 mg/kg
75-09-2 Methylene Chloride g ND 0.020 0.011 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.026 0.0077 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0051 0.0010 mg/kg
91-20-3 Naphthalene ND 0.0051 0.0020 mg/kg
103-65-1 n-Propylbenzene ND 0.0051 0.0010 mg/kg
100-42-5 Styrene ND 0.0051 0.0010 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0051 0.0011 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0051 0.0010 mg/kg
127-18-4 Tetrachloroethylene ND 0.0051 0.0013 mg/kg
108-88-3 Toluene ND 0.020 0.010 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0051 0.0014 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0051 0.0010 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0051 0.0010 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0051 0.0010 mg/kg
79-01-6 Trichloroethylene ND 0.0051 0.0010 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0051 0.0020 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0051 0.0013 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0051 0.0010 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0051 0.0010 mg/kg
108-05-4 Vinyl Acetate ND 0.026 0.017 mg/kg
75-01-4 Vinyl Chloride ND 0.0051 0.0010 mg/kg
m,p-Xylene ND 0.010 0.0011 mg/kg
95-47-6 o-Xylene ND 0.0051 0.0010 mg/kg
1330-20-7 Xylene (total)ND 0.015 0.0021 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%102%75-124%
17060-07-0 1,2-Dichloroethane-D4 116%120%72-135%
2037-26-5 Toluene-D8 98%100%75-126%
460-00-4 4-Bromofluorobenzene 91%92%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
55 of 189
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SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SOIL-DUP-A
Lab Sample ID:FA68836-8 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:87.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Results reported from Bisulfate preserved sample. Confirmation run.
(c) Associated CCV outside of control limits high.
(d) Initial calibration response factors not 8260D compliant.
(e) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(f) Associated BS recovery outside control limits high. Associated CCV outside of control limits high.
(g) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
56 of 189
FA6883633.8
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SOIL-DUP-A
Lab Sample ID:FA68836-8 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:87.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006773.D 1 10/15/19 19:24 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 0.94 0.19 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.19 0.021 mg/kg
95-57-8 2-Chlorophenol ND 0.19 0.023 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.19 0.022 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.19 0.050 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.94 0.19 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.38 0.075 mg/kg
95-48-7 2-Methylphenol ND 0.19 0.023 mg/kg
3&4-Methylphenol ND 0.19 0.031 mg/kg
88-75-5 2-Nitrophenol ND 0.19 0.020 mg/kg
100-02-7 4-Nitrophenol ND 0.94 0.19 mg/kg
87-86-5 Pentachlorophenol ND 0.94 0.19 mg/kg
108-95-2 Phenol ND 0.19 0.019 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.19 0.022 mg/kg
83-32-9 Acenaphthene ND 0.19 0.020 mg/kg
208-96-8 Acenaphthylene ND 0.19 0.019 mg/kg
120-12-7 Anthracene ND 0.19 0.021 mg/kg
56-55-3 Benzo(a)anthracene ND 0.19 0.019 mg/kg
50-32-8 Benzo(a)pyrene ND 0.19 0.022 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.19 0.021 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.19 0.019 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.19 0.025 mg/kg
100-51-6 Benzyl Alcohol ND 0.19 0.019 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.19 0.020 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.19 0.038 mg/kg
106-47-8 4-Chloroaniline ND 0.19 0.047 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.19 0.019 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.19 0.022 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.19 0.024 mg/kg
91-58-7 2-Chloronaphthalene ND 0.19 0.019 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.19 0.019 mg/kg
218-01-9 Chrysene ND 0.19 0.019 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
57 of 189
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SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SOIL-DUP-A
Lab Sample ID:FA68836-8 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:87.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.19 0.024 mg/kg
132-64-9 Dibenzofuran ND 0.19 0.019 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.19 0.019 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.19 0.020 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.19 0.025 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.19 0.045 mg/kg
84-66-2 Diethyl Phthalate ND 0.38 0.038 mg/kg
131-11-3 Dimethyl Phthalate ND 0.19 0.038 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.19 0.038 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.38 0.075 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 0.19 0.019 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.38 0.038 mg/kg
206-44-0 Fluoranthene ND 0.19 0.019 mg/kg
86-73-7 Fluorene ND 0.19 0.020 mg/kg
118-74-1 Hexachlorobenzene ND 0.19 0.019 mg/kg
87-68-3 Hexachlorobutadiene ND 0.19 0.019 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.19 0.038 mg/kg
67-72-1 Hexachloroethane ND 0.19 0.022 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.19 0.023 mg/kg
78-59-1 Isophorone ND 0.19 0.019 mg/kg
90-12-0 1-Methylnaphthalene ND 0.19 0.019 mg/kg
91-57-6 2-Methylnaphthalene ND 0.19 0.019 mg/kg
91-20-3 Naphthalene ND 0.19 0.019 mg/kg
98-95-3 Nitrobenzene ND 0.19 0.019 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.19 0.019 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.19 0.020 mg/kg
85-01-8 Phenanthrene ND 0.19 0.019 mg/kg
129-00-0 Pyrene ND 0.19 0.022 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.19 0.022 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 64%40-102%
4165-62-2 Phenol-d5 68%41-100%
118-79-6 2,4,6-Tribromophenol 71%42-108%
4165-60-0 Nitrobenzene-d5 64%40-105%
321-60-8 2-Fluorobiphenyl 69%43-107%
1718-51-0 Terphenyl-d14 72%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
58 of 189
FA6883633.8
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SOIL-DUP-A
Lab Sample ID:FA68836-8 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:87.5
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 20.8 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 12.5 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 14.3 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 7.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury 0.065 0.046 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a 2.5 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36237
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
59 of 189
FA6883633.8
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-8 (2')
Lab Sample ID:FA68836-9 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8081B SW846 3546 Percent Solids:90.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ST144718.D 1 10/15/19 18:23 WH 10/15/19 08:10 OP77280 GST3465
Run #2
Initial Weight Final Volume
Run #1 15.3 g 5.0 ml
Run #2
Pesticide TCL List
CAS No.Compound Result RL MDL Units Q
309-00-2 Aldrin a ND 0.0018 0.00057 mg/kg
319-84-6 alpha-BHC a ND 0.0018 0.00057 mg/kg
319-85-7 beta-BHC a ND 0.0018 0.00053 mg/kg
319-86-8 delta-BHC a ND 0.0018 0.00051 mg/kg
58-89-9 gamma-BHC (Lindane) a ND 0.0018 0.00054 mg/kg
5103-71-9 alpha-Chlordane a ND 0.0018 0.00056 mg/kg
5103-74-2 gamma-Chlordane a ND 0.0018 0.00052 mg/kg
60-57-1 Dieldrin a ND 0.0018 0.00050 mg/kg
72-54-8 4,4'-DDD a ND 0.0036 0.00050 mg/kg
72-55-9 4,4'-DDE a ND 0.0036 0.00066 mg/kg
50-29-3 4,4'-DDT a ND 0.0036 0.00055 mg/kg
72-20-8 Endrin a ND 0.0036 0.00091 mg/kg
1031-07-8 Endosulfan sulfate ND 0.0036 0.00048 mg/kg
7421-93-4 Endrin aldehyde ND 0.0036 0.00042 mg/kg
53494-70-5 Endrin ketone ND 0.0036 0.00057 mg/kg
959-98-8 Endosulfan-I a ND 0.0018 0.00041 mg/kg
33213-65-9 Endosulfan-II ND 0.0018 0.00043 mg/kg
76-44-8 Heptachlor a ND 0.0018 0.00053 mg/kg
1024-57-3 Heptachlor epoxide a ND 0.0018 0.00053 mg/kg
72-43-5 Methoxychlor a ND 0.0036 0.00072 mg/kg
8001-35-2 Toxaphene ND 0.090 0.027 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 122%50-122%
2051-24-3 Decachlorobiphenyl 85%50-133%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
60 of 189
FA6883633.9
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-8 (2')
Lab Sample ID:FA68836-9 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8141B SW846 3546 Percent Solids:90.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZZ33612.D 1 10/11/19 18:29 NJ 10/11/19 12:30 OP77244 GZZ1370
Run #2
Initial Weight Final Volume
Run #1 10.4 g 2.0 ml
Run #2
Organophosphorus Pesticides
CAS No.Compound Result RL MDL Units Q
35400-43-2 Bolstar ND 0.042 0.011 mg/kg
2921-88-2 Chlorpyrifos ND 0.042 0.011 mg/kg
56-72-4 Coumaphos ND 0.042 0.011 mg/kg
8065-48-3 Demeton ND 0.085 0.026 mg/kg
333-41-5 Diazinon ND 0.042 0.011 mg/kg
62-73-7 Dichlorvos ND 0.042 0.011 mg/kg
60-51-5 Dimethoate a ND 0.042 0.011 mg/kg
298-04-4 Disulfoton ND 0.042 0.011 mg/kg
2104-64-5 EPN ND 0.042 0.011 mg/kg
13194-48-4 Ethoprop ND 0.042 0.011 mg/kg
56-38-2 Ethyl Parathion ND 0.042 0.011 mg/kg
115-90-2 Fensulfothion ND 0.085 0.014 mg/kg
55-38-9 Fenthion ND 0.042 0.011 mg/kg
121-75-5 Malathion ND 0.042 0.011 mg/kg
86-50-0 Methyl Azinphos (Guthion)ND 0.042 0.011 mg/kg
298-00-0 Methyl Parathion ND 0.042 0.011 mg/kg
150-50-5 Merphos a ND 0.11 0.057 mg/kg
7786-34-7 Mevinphos ND 0.042 0.011 mg/kg
6923-22-4 Monocrotophos a ND 0.11 0.032 mg/kg
300-76-5 Naled b ND 0.042 0.011 mg/kg
298-02-2 Phorate ND 0.042 0.011 mg/kg
299-84-3 Ronnel ND 0.042 0.011 mg/kg
3689-24-5 Sulfotep a ND 0.042 0.011 mg/kg
22248-79-9 Stirophos ND 0.042 0.011 mg/kg
107-49-3 TEPP a ND 0.17 0.084 mg/kg
34643-46-4 Tokuthion ND 0.042 0.011 mg/kg
327-98-0 Trichloronate ND 0.042 0.011 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
126-73-8 Tributyl phosphate 73%47-136%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
61 of 189
FA6883633.9
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-8 (2')
Lab Sample ID:FA68836-9 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8141B SW846 3546 Percent Solids:90.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Organophosphorus Pesticides
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated BS outside of control limits high, sample was ND. Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
62 of 189
FA6883633.9
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-8 (2')
Lab Sample ID:FA68836-9 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:90.6
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 3.9 0.96 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 42.8 0.96 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <0.96 0.96 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 26.1 0.96 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 13.5 0.96 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.042 0.042 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a 2.0 0.96 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <0.96 0.96 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36237
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
63 of 189
FA6883633.9
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-9 (2')
Lab Sample ID:FA68836-10 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8081B SW846 3546 Percent Solids:84.7
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ST144721.D 1 10/15/19 19:08 WH 10/15/19 08:10 OP77280 GST3465
Run #2
Initial Weight Final Volume
Run #1 15.0 g 5.0 ml
Run #2
Pesticide TCL List
CAS No.Compound Result RL MDL Units Q
309-00-2 Aldrin a ND 0.0020 0.00062 mg/kg
319-84-6 alpha-BHC a ND 0.0020 0.00062 mg/kg
319-85-7 beta-BHC a ND 0.0020 0.00058 mg/kg
319-86-8 delta-BHC a ND 0.0020 0.00056 mg/kg
58-89-9 gamma-BHC (Lindane) a ND 0.0020 0.00059 mg/kg
5103-71-9 alpha-Chlordane a ND 0.0020 0.00061 mg/kg
5103-74-2 gamma-Chlordane a ND 0.0020 0.00057 mg/kg
60-57-1 Dieldrin a ND 0.0020 0.00055 mg/kg
72-54-8 4,4'-DDD a ND 0.0039 0.00054 mg/kg
72-55-9 4,4'-DDE a ND 0.0039 0.00072 mg/kg
50-29-3 4,4'-DDT a ND 0.0039 0.00060 mg/kg
72-20-8 Endrin a ND 0.0039 0.0010 mg/kg
1031-07-8 Endosulfan sulfate ND 0.0039 0.00052 mg/kg
7421-93-4 Endrin aldehyde ND 0.0039 0.00046 mg/kg
53494-70-5 Endrin ketone ND 0.0039 0.00062 mg/kg
959-98-8 Endosulfan-I a ND 0.0020 0.00045 mg/kg
33213-65-9 Endosulfan-II ND 0.0020 0.00046 mg/kg
76-44-8 Heptachlor a ND 0.0020 0.00058 mg/kg
1024-57-3 Heptachlor epoxide a ND 0.0020 0.00058 mg/kg
72-43-5 Methoxychlor a ND 0.0039 0.00079 mg/kg
8001-35-2 Toxaphene ND 0.098 0.030 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 143%50-122%
2051-24-3 Decachlorobiphenyl 94%50-133%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
64 of 189
FA6883633.10
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-9 (2')
Lab Sample ID:FA68836-10 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8141B SW846 3546 Percent Solids:84.7
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZZ33615.D 1 10/11/19 19:49 NJ 10/11/19 12:30 OP77244 GZZ1370
Run #2
Initial Weight Final Volume
Run #1 10.2 g 2.0 ml
Run #2
Organophosphorus Pesticides
CAS No.Compound Result RL MDL Units Q
35400-43-2 Bolstar ND 0.046 0.012 mg/kg
2921-88-2 Chlorpyrifos ND 0.046 0.012 mg/kg
56-72-4 Coumaphos ND 0.046 0.012 mg/kg
8065-48-3 Demeton ND 0.093 0.028 mg/kg
333-41-5 Diazinon ND 0.046 0.012 mg/kg
62-73-7 Dichlorvos ND 0.046 0.012 mg/kg
60-51-5 Dimethoate a ND 0.046 0.012 mg/kg
298-04-4 Disulfoton ND 0.046 0.012 mg/kg
2104-64-5 EPN ND 0.046 0.012 mg/kg
13194-48-4 Ethoprop ND 0.046 0.012 mg/kg
56-38-2 Ethyl Parathion ND 0.046 0.012 mg/kg
115-90-2 Fensulfothion ND 0.093 0.015 mg/kg
55-38-9 Fenthion ND 0.046 0.012 mg/kg
121-75-5 Malathion ND 0.046 0.012 mg/kg
86-50-0 Methyl Azinphos (Guthion)ND 0.046 0.012 mg/kg
298-00-0 Methyl Parathion ND 0.046 0.012 mg/kg
150-50-5 Merphos a ND 0.12 0.062 mg/kg
7786-34-7 Mevinphos ND 0.046 0.012 mg/kg
6923-22-4 Monocrotophos a ND 0.12 0.035 mg/kg
300-76-5 Naled b ND 0.046 0.012 mg/kg
298-02-2 Phorate ND 0.046 0.012 mg/kg
299-84-3 Ronnel ND 0.046 0.012 mg/kg
3689-24-5 Sulfotep a ND 0.046 0.012 mg/kg
22248-79-9 Stirophos ND 0.046 0.012 mg/kg
107-49-3 TEPP a ND 0.19 0.092 mg/kg
34643-46-4 Tokuthion ND 0.046 0.012 mg/kg
327-98-0 Trichloronate ND 0.046 0.012 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
126-73-8 Tributyl phosphate 75%47-136%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
65 of 189
FA6883633.10
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-9 (2')
Lab Sample ID:FA68836-10 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8141B SW846 3546 Percent Solids:84.7
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Organophosphorus Pesticides
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated BS outside of control limits high, sample was ND. Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
66 of 189
FA6883633.10
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-9 (2')
Lab Sample ID:FA68836-10 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:84.7
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 6.7 0.94 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 51.8 0.94 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <0.94 0.94 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 26.8 0.94 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 8.7 0.94 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury 0.091 0.047 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a 1.6 0.94 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <0.94 0.94 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36237
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
67 of 189
FA6883633.10
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-10 (2')
Lab Sample ID:FA68836-11 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8081B SW846 3546 Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ST144722.D 1 10/15/19 19:25 WH 10/15/19 08:10 OP77280 GST3465
Run #2 a ST144769.D 1 10/16/19 22:58 WH 10/16/19 08:06 OP77303 GST3466
Initial Weight Final Volume
Run #1 15.1 g 5.0 ml
Run #2 15.2 g 5.0 ml
Pesticide TCL List
CAS No.Compound Result RL MDL Units Q
309-00-2 Aldrin b ND 0.0018 0.00057 mg/kg
319-84-6 alpha-BHC b ND 0.0018 0.00057 mg/kg
319-85-7 beta-BHC b ND 0.0018 0.00053 mg/kg
319-86-8 delta-BHC b ND 0.0018 0.00051 mg/kg
58-89-9 gamma-BHC (Lindane) b ND 0.0018 0.00054 mg/kg
5103-71-9 alpha-Chlordane b ND 0.0018 0.00056 mg/kg
5103-74-2 gamma-Chlordane b ND 0.0018 0.00052 mg/kg
60-57-1 Dieldrin b ND 0.0018 0.00050 mg/kg
72-54-8 4,4'-DDD b ND 0.0036 0.00050 mg/kg
72-55-9 4,4'-DDE b ND 0.0036 0.00066 mg/kg
50-29-3 4,4'-DDT b ND 0.0036 0.00055 mg/kg
72-20-8 Endrin b ND 0.0036 0.00091 mg/kg
1031-07-8 Endosulfan sulfate ND 0.0036 0.00048 mg/kg
7421-93-4 Endrin aldehyde ND 0.0036 0.00042 mg/kg
53494-70-5 Endrin ketone ND 0.0036 0.00057 mg/kg
959-98-8 Endosulfan-I b ND 0.0018 0.00041 mg/kg
33213-65-9 Endosulfan-II ND 0.0018 0.00043 mg/kg
76-44-8 Heptachlor b ND 0.0018 0.00053 mg/kg
1024-57-3 Heptachlor epoxide b ND 0.0018 0.00053 mg/kg
72-43-5 Methoxychlor b ND 0.0036 0.00072 mg/kg
8001-35-2 Toxaphene ND 0.090 0.027 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 101%135%50-122%
2051-24-3 Decachlorobiphenyl 98%117%50-133%
(a) Confirmation run.
(b) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
68 of 189
FA6883633.11
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SB-10 (2')
Lab Sample ID:FA68836-11 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8141B SW846 3546 Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZZ33616.D 1 10/11/19 20:15 NJ 10/11/19 12:30 OP77244 GZZ1370
Run #2
Initial Weight Final Volume
Run #1 10.5 g 2.0 ml
Run #2
Organophosphorus Pesticides
CAS No.Compound Result RL MDL Units Q
35400-43-2 Bolstar ND 0.041 0.010 mg/kg
2921-88-2 Chlorpyrifos ND 0.041 0.010 mg/kg
56-72-4 Coumaphos ND 0.041 0.010 mg/kg
8065-48-3 Demeton ND 0.083 0.025 mg/kg
333-41-5 Diazinon ND 0.041 0.010 mg/kg
62-73-7 Dichlorvos ND 0.041 0.010 mg/kg
60-51-5 Dimethoate a ND 0.041 0.011 mg/kg
298-04-4 Disulfoton ND 0.041 0.010 mg/kg
2104-64-5 EPN ND 0.041 0.010 mg/kg
13194-48-4 Ethoprop ND 0.041 0.010 mg/kg
56-38-2 Ethyl Parathion ND 0.041 0.010 mg/kg
115-90-2 Fensulfothion ND 0.083 0.013 mg/kg
55-38-9 Fenthion ND 0.041 0.010 mg/kg
121-75-5 Malathion ND 0.041 0.010 mg/kg
86-50-0 Methyl Azinphos (Guthion)ND 0.041 0.010 mg/kg
298-00-0 Methyl Parathion ND 0.041 0.010 mg/kg
150-50-5 Merphos a ND 0.10 0.055 mg/kg
7786-34-7 Mevinphos ND 0.041 0.010 mg/kg
6923-22-4 Monocrotophos a ND 0.10 0.031 mg/kg
300-76-5 Naled b ND 0.041 0.010 mg/kg
298-02-2 Phorate ND 0.041 0.010 mg/kg
299-84-3 Ronnel ND 0.041 0.010 mg/kg
3689-24-5 Sulfotep a ND 0.041 0.010 mg/kg
22248-79-9 Stirophos ND 0.041 0.010 mg/kg
107-49-3 TEPP a ND 0.17 0.082 mg/kg
34643-46-4 Tokuthion ND 0.041 0.010 mg/kg
327-98-0 Trichloronate ND 0.041 0.010 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
126-73-8 Tributyl phosphate 76%47-136%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
69 of 189
FA6883633.11
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SB-10 (2')
Lab Sample ID:FA68836-11 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8141B SW846 3546 Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Organophosphorus Pesticides
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated BS outside of control limits high, sample was ND. Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
70 of 189
FA6883633.11
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SB-10 (2')
Lab Sample ID:FA68836-11 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:91.9
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 2.0 0.84 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 33.7 0.84 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <0.84 0.84 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 9.9 0.84 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 18.6 0.84 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.041 0.041 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a <0.84 0.84 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <0.84 0.84 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36237
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
71 of 189
FA6883633.11
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SOIL DUP-B
Lab Sample ID:FA68836-12 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8081B SW846 3546 Percent Solids:92.3
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ST144723.D 1 10/15/19 19:42 WH 10/15/19 08:10 OP77280 GST3465
Run #2
Initial Weight Final Volume
Run #1 15.0 g 5.0 ml
Run #2
Pesticide TCL List
CAS No.Compound Result RL MDL Units Q
309-00-2 Aldrin a ND 0.0018 0.00057 mg/kg
319-84-6 alpha-BHC a ND 0.0018 0.00057 mg/kg
319-85-7 beta-BHC a ND 0.0018 0.00053 mg/kg
319-86-8 delta-BHC a ND 0.0018 0.00051 mg/kg
58-89-9 gamma-BHC (Lindane) a ND 0.0018 0.00054 mg/kg
5103-71-9 alpha-Chlordane a ND 0.0018 0.00056 mg/kg
5103-74-2 gamma-Chlordane a ND 0.0018 0.00052 mg/kg
60-57-1 Dieldrin a ND 0.0018 0.00051 mg/kg
72-54-8 4,4'-DDD a ND 0.0036 0.00050 mg/kg
72-55-9 4,4'-DDE a ND 0.0036 0.00066 mg/kg
50-29-3 4,4'-DDT a ND 0.0036 0.00055 mg/kg
72-20-8 Endrin a ND 0.0036 0.00091 mg/kg
1031-07-8 Endosulfan sulfate ND 0.0036 0.00048 mg/kg
7421-93-4 Endrin aldehyde ND 0.0036 0.00042 mg/kg
53494-70-5 Endrin ketone ND 0.0036 0.00057 mg/kg
959-98-8 Endosulfan-I a ND 0.0018 0.00042 mg/kg
33213-65-9 Endosulfan-II ND 0.0018 0.00043 mg/kg
76-44-8 Heptachlor a ND 0.0018 0.00053 mg/kg
1024-57-3 Heptachlor epoxide a ND 0.0018 0.00053 mg/kg
72-43-5 Methoxychlor a ND 0.0036 0.00072 mg/kg
8001-35-2 Toxaphene ND 0.090 0.027 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 113%50-122%
2051-24-3 Decachlorobiphenyl 95%50-133%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
72 of 189
FA6883633.12
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SOIL DUP-B
Lab Sample ID:FA68836-12 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8141B SW846 3546 Percent Solids:92.3
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 ZZ33617.D 1 10/11/19 20:41 NJ 10/11/19 12:30 OP77244 GZZ1370
Run #2
Initial Weight Final Volume
Run #1 10.0 g 2.0 ml
Run #2
Organophosphorus Pesticides
CAS No.Compound Result RL MDL Units Q
35400-43-2 Bolstar ND 0.043 0.011 mg/kg
2921-88-2 Chlorpyrifos ND 0.043 0.011 mg/kg
56-72-4 Coumaphos ND 0.043 0.011 mg/kg
8065-48-3 Demeton ND 0.087 0.026 mg/kg
333-41-5 Diazinon ND 0.043 0.011 mg/kg
62-73-7 Dichlorvos ND 0.043 0.011 mg/kg
60-51-5 Dimethoate a ND 0.043 0.011 mg/kg
298-04-4 Disulfoton ND 0.043 0.011 mg/kg
2104-64-5 EPN ND 0.043 0.011 mg/kg
13194-48-4 Ethoprop ND 0.043 0.011 mg/kg
56-38-2 Ethyl Parathion ND 0.043 0.011 mg/kg
115-90-2 Fensulfothion ND 0.087 0.014 mg/kg
55-38-9 Fenthion ND 0.043 0.011 mg/kg
121-75-5 Malathion ND 0.043 0.011 mg/kg
86-50-0 Methyl Azinphos (Guthion)ND 0.043 0.011 mg/kg
298-00-0 Methyl Parathion ND 0.043 0.011 mg/kg
150-50-5 Merphos a ND 0.11 0.058 mg/kg
7786-34-7 Mevinphos ND 0.043 0.011 mg/kg
6923-22-4 Monocrotophos a ND 0.11 0.033 mg/kg
300-76-5 Naled b ND 0.043 0.011 mg/kg
298-02-2 Phorate ND 0.043 0.011 mg/kg
299-84-3 Ronnel ND 0.043 0.011 mg/kg
3689-24-5 Sulfotep a ND 0.043 0.011 mg/kg
22248-79-9 Stirophos ND 0.043 0.011 mg/kg
107-49-3 TEPP a ND 0.17 0.086 mg/kg
34643-46-4 Tokuthion ND 0.043 0.011 mg/kg
327-98-0 Trichloronate ND 0.043 0.011 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
126-73-8 Tributyl phosphate 69%47-136%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
73 of 189
FA6883633.12
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SOIL DUP-B
Lab Sample ID:FA68836-12 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8141B SW846 3546 Percent Solids:92.3
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Organophosphorus Pesticides
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated BS outside of control limits high, sample was ND. Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
74 of 189
FA6883633.12
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SOIL DUP-B
Lab Sample ID:FA68836-12 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:92.3
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 2.5 0.93 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 33.3 0.93 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <0.93 0.93 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 10.1 0.93 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 15.5 0.93 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.042 0.042 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a <0.93 0.93 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <0.93 0.93 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36237
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
75 of 189
FA6883633.12
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SW-EFF
Lab Sample ID:FA68836-13 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0136283.D 1 10/12/19 12:34 AB n/a n/a VC5431
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 20.4 25 10 ug/l J
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
76 of 189
FA6883633.13
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SW-EFF
Lab Sample ID:FA68836-13 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene 1.1 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene 1.7 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%83-118%
17060-07-0 1,2-Dichloroethane-D4 105%79-125%
2037-26-5 Toluene-D8 97%85-112%
460-00-4 4-Bromofluorobenzene 101%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
77 of 189
FA6883633.13
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SW-EFF
Lab Sample ID:FA68836-13 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X067488.D 1 10/14/19 17:53 MV 10/12/19 08:00 OP77241 SX2779
Run #2
Initial Volume Final Volume
Run #1 100 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 500 100 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 50 5.9 ug/l
95-57-8 2-Chlorophenol ND 50 6.3 ug/l
120-83-2 2,4-Dichlorophenol ND 50 8.4 ug/l
105-67-9 2,4-Dimethylphenol ND 50 7.4 ug/l
51-28-5 2,4-Dinitrophenol ND 250 50 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 100 20 ug/l
95-48-7 2-Methylphenol ND 50 5.6 ug/l
3&4-Methylphenol 18.0 50 9.8 ug/l J
88-75-5 2-Nitrophenol ND 50 8.5 ug/l
100-02-7 4-Nitrophenol ND 250 50 ug/l
87-86-5 Pentachlorophenol ND 250 50 ug/l
108-95-2 Phenol 7.5 50 5.0 ug/l J
88-06-2 2,4,6-Trichlorophenol ND 50 7.5 ug/l
83-32-9 Acenaphthene ND 50 6.3 ug/l
208-96-8 Acenaphthylene ND 50 6.4 ug/l
120-12-7 Anthracene ND 50 8.0 ug/l
56-55-3 Benzo(a)anthracene ND 50 7.6 ug/l
50-32-8 Benzo(a)pyrene ND 50 7.8 ug/l
205-99-2 Benzo(b)fluoranthene ND 50 7.8 ug/l
191-24-2 Benzo(g,h,i)perylene ND 50 8.2 ug/l
207-08-9 Benzo(k)fluoranthene ND 50 8.6 ug/l
100-51-6 Benzyl Alcohol ND 50 6.1 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 50 8.5 ug/l
85-68-7 Butyl Benzyl Phthalate ND 50 10 ug/l
106-47-8 4-Chloroaniline ND 50 6.3 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 50 8.1 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 50 7.3 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 50 7.6 ug/l
91-58-7 2-Chloronaphthalene ND 50 5.0 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 50 5.4 ug/l
218-01-9 Chrysene ND 50 8.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
78 of 189
FA6883633.13
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SW-EFF
Lab Sample ID:FA68836-13 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 50 8.0 ug/l
132-64-9 Dibenzofuran ND 50 6.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 5.0 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 5.0 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 5.0 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 50 6.4 ug/l
84-66-2 Diethyl Phthalate ND 50 10 ug/l
131-11-3 Dimethyl Phthalate ND 50 10 ug/l
84-74-2 Di-n-butyl Phthalate ND 50 10 ug/l
117-84-0 Di-n-octyl Phthalate ND 50 10 ug/l
122-66-7 1,2-Diphenylhydrazine ND 50 7.6 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 50 10 ug/l
206-44-0 Fluoranthene ND 50 5.5 ug/l
86-73-7 Fluorene ND 50 7.0 ug/l
118-74-1 Hexachlorobenzene ND 50 6.9 ug/l
87-68-3 Hexachlorobutadiene ND 50 5.0 ug/l
77-47-4 Hexachlorocyclopentadiene ND 50 18 ug/l
67-72-1 Hexachloroethane ND 50 16 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene a ND 50 7.1 ug/l
78-59-1 Isophorone ND 50 7.8 ug/l
90-12-0 1-Methylnaphthalene ND 50 5.3 ug/l
91-57-6 2-Methylnaphthalene ND 50 6.0 ug/l
91-20-3 Naphthalene ND 50 5.0 ug/l
98-95-3 Nitrobenzene ND 50 9.3 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 50 6.7 ug/l
86-30-6 N-Nitrosodiphenylamine ND 50 8.1 ug/l
85-01-8 Phenanthrene ND 50 8.6 ug/l
129-00-0 Pyrene ND 50 6.8 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 11 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 18%14-67%
4165-62-2 Phenol-d5 13%10-50%
118-79-6 2,4,6-Tribromophenol 58%33-118%
4165-60-0 Nitrobenzene-d5 55%42-108%
321-60-8 2-Fluorobiphenyl 61%40-106%
1718-51-0 Terphenyl-d14 49%39-121%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
79 of 189
FA6883633.13
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SW-EFF
Lab Sample ID:FA68836-13 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 23.3 20 ug/l 20 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Barium a 1630 20 ug/l 20 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Cadmium a <20 20 ug/l 20 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Chromium a 277 20 ug/l 20 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Lead a 194 20 ug/l 20 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Mercury <0.50 0.50 ug/l 1 10/11/19 10/11/19 JC SW846 7470A 1 SW846 7470A 3
Selenium a <20 20 ug/l 20 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Silver a <20 20 ug/l 20 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
(1) Instrument QC Batch: MA16246
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36244
(4) Prep QC Batch: MP36255
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
80 of 189
FA6883633.13
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SED-EFF
Lab Sample ID:FA68836-14 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:79.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13574.D 1 10/10/19 19:07 SP n/a n/a V2B517
Run #2
Initial Weight Final Volume
Run #1 6.00 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone b ND 0.21 0.11 mg/kg
71-43-2 Benzene ND 0.0053 0.0013 mg/kg
108-86-1 Bromobenzene ND 0.0053 0.0011 mg/kg
74-97-5 Bromochloromethane ND 0.0053 0.0016 mg/kg
75-27-4 Bromodichloromethane c ND 0.0053 0.0011 mg/kg
75-25-2 Bromoform ND 0.0053 0.0011 mg/kg
78-93-3 2-Butanone (MEK)ND 0.026 0.0077 mg/kg
104-51-8 n-Butylbenzene ND 0.0053 0.0011 mg/kg
135-98-8 sec-Butylbenzene ND 0.0053 0.0011 mg/kg
98-06-6 tert-Butylbenzene ND 0.0053 0.0011 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0053 0.0011 mg/kg
108-90-7 Chlorobenzene ND 0.0053 0.0011 mg/kg
75-00-3 Chloroethane d ND 0.0053 0.0021 mg/kg
67-66-3 Chloroform ND 0.0053 0.0014 mg/kg
95-49-8 o-Chlorotoluene ND 0.0053 0.0011 mg/kg
106-43-4 p-Chlorotoluene ND 0.0053 0.0011 mg/kg
124-48-1 Dibromochloromethane ND 0.0053 0.0011 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0053 0.0011 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0053 0.0021 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0053 0.0011 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0053 0.0011 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0053 0.0012 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0053 0.0019 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0053 0.0011 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0053 0.0011 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0053 0.0015 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0053 0.0011 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0053 0.0011 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0053 0.0011 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0053 0.0011 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0053 0.0011 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0053 0.0011 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
81 of 189
FA6883633.14
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SED-EFF
Lab Sample ID:FA68836-14 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:79.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0053 0.0011 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0053 0.0024 mg/kg
64-17-5 Ethyl Alcohol e ND 0.42 0.079 mg/kg
100-41-4 Ethylbenzene ND 0.0053 0.0011 mg/kg
591-78-6 2-Hexanone ND 0.026 0.0079 mg/kg
98-82-8 Isopropylbenzene ND 0.0053 0.0011 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0053 0.0011 mg/kg
74-83-9 Methyl Bromide ND 0.0053 0.0021 mg/kg
74-87-3 Methyl Chloride ND 0.0053 0.0021 mg/kg
75-09-2 Methylene Chloride b ND 0.021 0.012 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.026 0.0079 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0053 0.0011 mg/kg
91-20-3 Naphthalene ND 0.0053 0.0021 mg/kg
103-65-1 n-Propylbenzene ND 0.0053 0.0011 mg/kg
100-42-5 Styrene ND 0.0053 0.0011 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0053 0.0011 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0053 0.0011 mg/kg
127-18-4 Tetrachloroethylene ND 0.0053 0.0013 mg/kg
108-88-3 Toluene ND 0.021 0.011 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0053 0.0015 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0053 0.0011 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0053 0.0011 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0053 0.0011 mg/kg
79-01-6 Trichloroethylene ND 0.0053 0.0011 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0053 0.0021 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0053 0.0013 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0053 0.0011 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0053 0.0011 mg/kg
108-05-4 Vinyl Acetate ND 0.026 0.017 mg/kg
75-01-4 Vinyl Chloride ND 0.0053 0.0011 mg/kg
m,p-Xylene ND 0.011 0.0012 mg/kg
95-47-6 o-Xylene ND 0.0053 0.0011 mg/kg
1330-20-7 Xylene (total)ND 0.016 0.0022 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 117%72-135%
2037-26-5 Toluene-D8 109%75-126%
460-00-4 4-Bromofluorobenzene 113%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
82 of 189
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Report of Analysis Page 3 of 3
Client Sample ID:SED-EFF
Lab Sample ID:FA68836-14 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:79.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Associated CCV outside of control limits high, sample was ND.
(c) Initial calibration response factors not 8260D compliant.
(d) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(e) Associated BS recovery outside control limits high; however sample is ND. Associated CCV outside of control
limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
83 of 189
FA6883633.14
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SED-EFF
Lab Sample ID:FA68836-14 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:79.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006774.D 1 10/15/19 19:50 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.5 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1.0 0.21 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.21 0.023 mg/kg
95-57-8 2-Chlorophenol ND 0.21 0.025 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.21 0.024 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.21 0.055 mg/kg
51-28-5 2,4-Dinitrophenol ND 1.0 0.21 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.41 0.083 mg/kg
95-48-7 2-Methylphenol ND 0.21 0.025 mg/kg
3&4-Methylphenol ND 0.21 0.034 mg/kg
88-75-5 2-Nitrophenol ND 0.21 0.023 mg/kg
100-02-7 4-Nitrophenol ND 1.0 0.21 mg/kg
87-86-5 Pentachlorophenol ND 1.0 0.21 mg/kg
108-95-2 Phenol ND 0.21 0.021 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.21 0.024 mg/kg
83-32-9 Acenaphthene ND 0.21 0.022 mg/kg
208-96-8 Acenaphthylene ND 0.21 0.021 mg/kg
120-12-7 Anthracene ND 0.21 0.023 mg/kg
56-55-3 Benzo(a)anthracene ND 0.21 0.021 mg/kg
50-32-8 Benzo(a)pyrene ND 0.21 0.024 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.21 0.023 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.21 0.021 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.21 0.027 mg/kg
100-51-6 Benzyl Alcohol ND 0.21 0.021 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.21 0.022 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.21 0.041 mg/kg
106-47-8 4-Chloroaniline ND 0.21 0.052 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.21 0.021 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.21 0.024 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.21 0.026 mg/kg
91-58-7 2-Chloronaphthalene ND 0.21 0.021 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.21 0.021 mg/kg
218-01-9 Chrysene ND 0.21 0.021 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
84 of 189
FA6883633.14
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SED-EFF
Lab Sample ID:FA68836-14 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:79.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.21 0.026 mg/kg
132-64-9 Dibenzofuran ND 0.21 0.021 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.21 0.021 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.21 0.022 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.21 0.028 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.21 0.049 mg/kg
84-66-2 Diethyl Phthalate ND 0.41 0.041 mg/kg
131-11-3 Dimethyl Phthalate ND 0.21 0.041 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.21 0.041 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.41 0.083 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 0.21 0.021 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.41 0.041 mg/kg
206-44-0 Fluoranthene ND 0.21 0.021 mg/kg
86-73-7 Fluorene ND 0.21 0.022 mg/kg
118-74-1 Hexachlorobenzene ND 0.21 0.021 mg/kg
87-68-3 Hexachlorobutadiene ND 0.21 0.021 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.21 0.041 mg/kg
67-72-1 Hexachloroethane ND 0.21 0.024 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.21 0.025 mg/kg
78-59-1 Isophorone ND 0.21 0.021 mg/kg
90-12-0 1-Methylnaphthalene ND 0.21 0.021 mg/kg
91-57-6 2-Methylnaphthalene ND 0.21 0.021 mg/kg
91-20-3 Naphthalene ND 0.21 0.021 mg/kg
98-95-3 Nitrobenzene ND 0.21 0.021 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.21 0.021 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.21 0.022 mg/kg
85-01-8 Phenanthrene ND 0.21 0.021 mg/kg
129-00-0 Pyrene ND 0.21 0.024 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.21 0.024 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 67%40-102%
4165-62-2 Phenol-d5 72%41-100%
118-79-6 2,4,6-Tribromophenol 80%42-108%
4165-60-0 Nitrobenzene-d5 68%40-105%
321-60-8 2-Fluorobiphenyl 75%43-107%
1718-51-0 Terphenyl-d14 75%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
85 of 189
FA6883633.14
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SED-EFF
Lab Sample ID:FA68836-14 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:79.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 2.7 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 26.2 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <1.0 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 10.1 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 10.6 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.049 0.049 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a <1.0 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <1.0 1.0 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36237
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
86 of 189
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SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SW-INF
Lab Sample ID:FA68836-15 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0136284.D 1 10/12/19 13:01 AB n/a n/a VC5431
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
87 of 189
FA6883633.15
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SW-INF
Lab Sample ID:FA68836-15 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%83-118%
17060-07-0 1,2-Dichloroethane-D4 105%79-125%
2037-26-5 Toluene-D8 95%85-112%
460-00-4 4-Bromofluorobenzene 99%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
88 of 189
FA6883633.15
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SW-INF
Lab Sample ID:FA68836-15 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X067489.D 1 10/14/19 18:19 MV 10/12/19 08:00 OP77241 SX2779
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 48 9.5 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l
95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l
105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.8 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.5 1.9 ug/l
95-48-7 2-Methylphenol ND 4.8 0.53 ug/l
3&4-Methylphenol ND 4.8 0.93 ug/l
88-75-5 2-Nitrophenol ND 4.8 0.81 ug/l
100-02-7 4-Nitrophenol ND 24 4.8 ug/l
87-86-5 Pentachlorophenol ND 24 4.8 ug/l
108-95-2 Phenol ND 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l
83-32-9 Acenaphthene ND 4.8 0.60 ug/l
208-96-8 Acenaphthylene ND 4.8 0.61 ug/l
120-12-7 Anthracene ND 4.8 0.76 ug/l
56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l
100-51-6 Benzyl Alcohol ND 4.8 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/l
106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.8 0.72 ug/l
91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l
218-01-9 Chrysene ND 4.8 0.81 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
89 of 189
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SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SW-INF
Lab Sample ID:FA68836-15 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l
132-64-9 Dibenzofuran ND 4.8 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.8 0.48 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.8 0.48 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.8 0.48 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/l
131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.8 0.95 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.8 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l
206-44-0 Fluoranthene ND 4.8 0.53 ug/l
86-73-7 Fluorene ND 4.8 0.67 ug/l
118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l
87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.8 1.7 ug/l
67-72-1 Hexachloroethane ND 4.8 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene a ND 4.8 0.68 ug/l
78-59-1 Isophorone ND 4.8 0.74 ug/l
90-12-0 1-Methylnaphthalene ND 4.8 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.8 0.57 ug/l
91-20-3 Naphthalene ND 4.8 0.48 ug/l
98-95-3 Nitrobenzene ND 4.8 0.89 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.8 0.77 ug/l
85-01-8 Phenanthrene ND 4.8 0.82 ug/l
129-00-0 Pyrene ND 4.8 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.8 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 20%14-67%
4165-62-2 Phenol-d5 13%10-50%
118-79-6 2,4,6-Tribromophenol 77%33-118%
4165-60-0 Nitrobenzene-d5 62%42-108%
321-60-8 2-Fluorobiphenyl 70%40-106%
1718-51-0 Terphenyl-d14 57%39-121%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
90 of 189
FA6883633.15
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SW-INF
Lab Sample ID:FA68836-15 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic 2.3 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Barium 177 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Cadmium <2.0 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Chromium 7.6 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Lead 6.2 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Mercury <0.50 0.50 ug/l 1 10/11/19 10/11/19 JC SW846 7470A 1 SW846 7470A 3
Selenium <2.0 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Silver <2.0 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
(1) Instrument QC Batch: MA16246
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36244
(4) Prep QC Batch: MP36255
RL = Reporting Limit
91 of 189
FA6883633.15
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:SED-INF
Lab Sample ID:FA68836-16 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:81.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13575.D 1 10/10/19 19:33 SP n/a n/a V2B517
Run #2
Initial Weight Final Volume
Run #1 5.58 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone b 0.269 0.22 0.11 mg/kg
71-43-2 Benzene ND 0.0055 0.0013 mg/kg
108-86-1 Bromobenzene ND 0.0055 0.0011 mg/kg
74-97-5 Bromochloromethane ND 0.0055 0.0016 mg/kg
75-27-4 Bromodichloromethane c ND 0.0055 0.0011 mg/kg
75-25-2 Bromoform ND 0.0055 0.0011 mg/kg
78-93-3 2-Butanone (MEK)0.0093 0.028 0.0080 mg/kg J
104-51-8 n-Butylbenzene ND 0.0055 0.0011 mg/kg
135-98-8 sec-Butylbenzene ND 0.0055 0.0011 mg/kg
98-06-6 tert-Butylbenzene ND 0.0055 0.0011 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0055 0.0011 mg/kg
108-90-7 Chlorobenzene ND 0.0055 0.0011 mg/kg
75-00-3 Chloroethane d ND 0.0055 0.0022 mg/kg
67-66-3 Chloroform ND 0.0055 0.0015 mg/kg
95-49-8 o-Chlorotoluene ND 0.0055 0.0011 mg/kg
106-43-4 p-Chlorotoluene ND 0.0055 0.0011 mg/kg
124-48-1 Dibromochloromethane ND 0.0055 0.0011 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0055 0.0011 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0055 0.0022 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0055 0.0011 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0055 0.0011 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0055 0.0013 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0055 0.0020 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0055 0.0011 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0055 0.0011 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0055 0.0015 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0055 0.0011 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0055 0.0011 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0055 0.0011 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0055 0.0011 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0055 0.0011 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0055 0.0011 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
92 of 189
FA6883633.16
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:SED-INF
Lab Sample ID:FA68836-16 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:81.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0055 0.0011 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0055 0.0026 mg/kg
64-17-5 Ethyl Alcohol e 0.255 0.44 0.083 mg/kg J
100-41-4 Ethylbenzene ND 0.0055 0.0011 mg/kg
591-78-6 2-Hexanone ND 0.028 0.0083 mg/kg
98-82-8 Isopropylbenzene ND 0.0055 0.0011 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0055 0.0011 mg/kg
74-83-9 Methyl Bromide ND 0.0055 0.0022 mg/kg
74-87-3 Methyl Chloride ND 0.0055 0.0022 mg/kg
75-09-2 Methylene Chloride f ND 0.022 0.012 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.028 0.0083 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0055 0.0011 mg/kg
91-20-3 Naphthalene ND 0.0055 0.0022 mg/kg
103-65-1 n-Propylbenzene ND 0.0055 0.0011 mg/kg
100-42-5 Styrene ND 0.0055 0.0011 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0055 0.0011 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0055 0.0011 mg/kg
127-18-4 Tetrachloroethylene ND 0.0055 0.0014 mg/kg
108-88-3 Toluene ND 0.022 0.011 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0055 0.0015 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0055 0.0011 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0055 0.0011 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0055 0.0011 mg/kg
79-01-6 Trichloroethylene ND 0.0055 0.0011 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0055 0.0022 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0055 0.0014 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0055 0.0011 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0055 0.0011 mg/kg
108-05-4 Vinyl Acetate ND 0.028 0.018 mg/kg
75-01-4 Vinyl Chloride ND 0.0055 0.0011 mg/kg
m,p-Xylene ND 0.011 0.0012 mg/kg
95-47-6 o-Xylene ND 0.0055 0.0011 mg/kg
1330-20-7 Xylene (total)ND 0.017 0.0023 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%75-124%
17060-07-0 1,2-Dichloroethane-D4 119%72-135%
2037-26-5 Toluene-D8 103%75-126%
460-00-4 4-Bromofluorobenzene 107%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
93 of 189
FA6883633.16
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:SED-INF
Lab Sample ID:FA68836-16 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:81.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Associated CCV outside of control limits high.
(c) Initial calibration response factors not 8260D compliant.
(d) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(e) Associated BS recovery outside control limits, high. Associated CCV outside of control limits high.
(f) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
94 of 189
FA6883633.16
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SED-INF
Lab Sample ID:FA68836-16 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:81.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I006775.D 1 10/15/19 20:16 MV 10/11/19 12:40 OP77248 S9I250
Run #2
Initial Weight Final Volume
Run #1 30.3 g 5.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 5.1 1.0 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 1.0 0.11 mg/kg
95-57-8 2-Chlorophenol ND 1.0 0.12 mg/kg
120-83-2 2,4-Dichlorophenol ND 1.0 0.12 mg/kg
105-67-9 2,4-Dimethylphenol ND 1.0 0.27 mg/kg
51-28-5 2,4-Dinitrophenol ND 5.1 1.0 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 2.0 0.41 mg/kg
95-48-7 2-Methylphenol ND 1.0 0.12 mg/kg
3&4-Methylphenol ND 1.0 0.17 mg/kg
88-75-5 2-Nitrophenol ND 1.0 0.11 mg/kg
100-02-7 4-Nitrophenol ND 5.1 1.0 mg/kg
87-86-5 Pentachlorophenol ND 5.1 1.0 mg/kg
108-95-2 Phenol ND 1.0 0.10 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 1.0 0.12 mg/kg
83-32-9 Acenaphthene ND 1.0 0.11 mg/kg
208-96-8 Acenaphthylene ND 1.0 0.10 mg/kg
120-12-7 Anthracene ND 1.0 0.11 mg/kg
56-55-3 Benzo(a)anthracene ND 1.0 0.10 mg/kg
50-32-8 Benzo(a)pyrene ND 1.0 0.12 mg/kg
205-99-2 Benzo(b)fluoranthene ND 1.0 0.11 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 1.0 0.11 mg/kg
207-08-9 Benzo(k)fluoranthene ND 1.0 0.13 mg/kg
100-51-6 Benzyl Alcohol ND 1.0 0.10 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 1.0 0.11 mg/kg
85-68-7 Butyl benzyl phthalate ND 1.0 0.20 mg/kg
106-47-8 4-Chloroaniline ND 1.0 0.26 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 1.0 0.10 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 1.0 0.12 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1.0 0.13 mg/kg
91-58-7 2-Chloronaphthalene ND 1.0 0.10 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 1.0 0.10 mg/kg
218-01-9 Chrysene ND 1.0 0.10 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
95 of 189
FA6883633.16
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SED-INF
Lab Sample ID:FA68836-16 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:81.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 1.0 0.13 mg/kg
132-64-9 Dibenzofuran ND 1.0 0.10 mg/kg
95-50-1 1,2-Dichlorobenzene ND 1.0 0.10 mg/kg
541-73-1 1,3-Dichlorobenzene ND 1.0 0.11 mg/kg
106-46-7 1,4-Dichlorobenzene ND 1.0 0.14 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 1.0 0.24 mg/kg
84-66-2 Diethyl Phthalate ND 2.0 0.20 mg/kg
131-11-3 Dimethyl Phthalate ND 1.0 0.20 mg/kg
117-84-0 Di-n-octyl Phthalate ND 1.0 0.20 mg/kg
84-74-2 Di-n-butyl Phthalate ND 2.0 0.41 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 1.0 0.10 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 2.0 0.20 mg/kg
206-44-0 Fluoranthene ND 1.0 0.10 mg/kg
86-73-7 Fluorene ND 1.0 0.11 mg/kg
118-74-1 Hexachlorobenzene ND 1.0 0.10 mg/kg
87-68-3 Hexachlorobutadiene ND 1.0 0.10 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 1.0 0.20 mg/kg
67-72-1 Hexachloroethane ND 1.0 0.12 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 1.0 0.12 mg/kg
78-59-1 Isophorone ND 1.0 0.10 mg/kg
90-12-0 1-Methylnaphthalene ND 1.0 0.10 mg/kg
91-57-6 2-Methylnaphthalene ND 1.0 0.10 mg/kg
91-20-3 Naphthalene ND 1.0 0.10 mg/kg
98-95-3 Nitrobenzene ND 1.0 0.10 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 1.0 0.10 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 1.0 0.11 mg/kg
85-01-8 Phenanthrene ND 1.0 0.10 mg/kg
129-00-0 Pyrene ND 1.0 0.12 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.12 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 68%40-102%
4165-62-2 Phenol-d5 74%41-100%
118-79-6 2,4,6-Tribromophenol 74%42-108%
4165-60-0 Nitrobenzene-d5 68%40-105%
321-60-8 2-Fluorobiphenyl 74%43-107%
1718-51-0 Terphenyl-d14 69%45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
96 of 189
FA6883633.16
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SED-INF
Lab Sample ID:FA68836-16 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:81.1
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a 1.7 0.78 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 27.3 0.78 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <0.78 0.78 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 8.5 0.78 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 3.5 0.78 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.042 0.042 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a 1.5 0.78 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <0.78 0.78 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36237
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
97 of 189
FA6883633.16
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SW DUP-C
Lab Sample ID:FA68836-17 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0136285.D 1 10/12/19 13:27 AB n/a n/a VC5431
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
98 of 189
FA6883633.17
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:SW DUP-C
Lab Sample ID:FA68836-17 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%83-118%
17060-07-0 1,2-Dichloroethane-D4 105%79-125%
2037-26-5 Toluene-D8 97%85-112%
460-00-4 4-Bromofluorobenzene 98%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
99 of 189
FA6883633.17
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SW DUP-C
Lab Sample ID:FA68836-17 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X067490.D 1 10/14/19 18:45 MV 10/12/19 08:00 OP77241 SX2779
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 48 9.5 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l
95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l
105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.8 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.5 1.9 ug/l
95-48-7 2-Methylphenol ND 4.8 0.53 ug/l
3&4-Methylphenol ND 4.8 0.93 ug/l
88-75-5 2-Nitrophenol ND 4.8 0.81 ug/l
100-02-7 4-Nitrophenol ND 24 4.8 ug/l
87-86-5 Pentachlorophenol ND 24 4.8 ug/l
108-95-2 Phenol ND 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l
83-32-9 Acenaphthene ND 4.8 0.60 ug/l
208-96-8 Acenaphthylene ND 4.8 0.61 ug/l
120-12-7 Anthracene ND 4.8 0.76 ug/l
56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l
100-51-6 Benzyl Alcohol ND 4.8 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/l
106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.8 0.72 ug/l
91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l
218-01-9 Chrysene ND 4.8 0.81 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
100 of 189
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Report of Analysis Page 2 of 2
Client Sample ID:SW DUP-C
Lab Sample ID:FA68836-17 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l
132-64-9 Dibenzofuran ND 4.8 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.8 0.48 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.8 0.48 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.8 0.48 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/l
131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.8 0.95 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.8 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l
206-44-0 Fluoranthene ND 4.8 0.53 ug/l
86-73-7 Fluorene ND 4.8 0.67 ug/l
118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l
87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.8 1.7 ug/l
67-72-1 Hexachloroethane ND 4.8 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene a ND 4.8 0.68 ug/l
78-59-1 Isophorone ND 4.8 0.74 ug/l
90-12-0 1-Methylnaphthalene ND 4.8 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.8 0.57 ug/l
91-20-3 Naphthalene ND 4.8 0.48 ug/l
98-95-3 Nitrobenzene ND 4.8 0.89 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.8 0.77 ug/l
85-01-8 Phenanthrene ND 4.8 0.82 ug/l
129-00-0 Pyrene ND 4.8 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.8 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 18%14-67%
4165-62-2 Phenol-d5 12%10-50%
118-79-6 2,4,6-Tribromophenol 72%33-118%
4165-60-0 Nitrobenzene-d5 59%42-108%
321-60-8 2-Fluorobiphenyl 68%40-106%
1718-51-0 Terphenyl-d14 64%39-121%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
101 of 189
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SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SW DUP-C
Lab Sample ID:FA68836-17 Date Sampled:10/05/19
Matrix:AQ - Surface Water Date Received:10/09/19
Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic <2.0 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Barium 99.7 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Cadmium <2.0 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Chromium 2.5 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Lead <2.0 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Mercury <0.50 0.50 ug/l 1 10/11/19 10/11/19 JC SW846 7470A 1 SW846 7470A 3
Selenium <2.0 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
Silver <2.0 2.0 ug/l 2 10/14/19 10/15/19 DM SW846 6020B 2 SW846 3010A 4
(1) Instrument QC Batch: MA16246
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36244
(4) Prep QC Batch: MP36255
RL = Reporting Limit
102 of 189
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Report of Analysis Page 1 of 3
Client Sample ID:SED DUP-D
Lab Sample ID:FA68836-18 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:81.0
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2B13576.D 1 10/10/19 19:58 SP n/a n/a V2B517
Run #2
Initial Weight Final Volume
Run #1 3.59 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone b 0.230 0.34 0.17 mg/kg J
71-43-2 Benzene 0.0040 0.0086 0.0021 mg/kg J
108-86-1 Bromobenzene ND 0.0086 0.0017 mg/kg
74-97-5 Bromochloromethane ND 0.0086 0.0025 mg/kg
75-27-4 Bromodichloromethane c ND 0.0086 0.0017 mg/kg
75-25-2 Bromoform ND 0.0086 0.0017 mg/kg
78-93-3 2-Butanone (MEK)0.0268 0.043 0.013 mg/kg J
104-51-8 n-Butylbenzene ND 0.0086 0.0017 mg/kg
135-98-8 sec-Butylbenzene ND 0.0086 0.0017 mg/kg
98-06-6 tert-Butylbenzene ND 0.0086 0.0017 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0086 0.0018 mg/kg
108-90-7 Chlorobenzene ND 0.0086 0.0017 mg/kg
75-00-3 Chloroethane d ND 0.0086 0.0034 mg/kg
67-66-3 Chloroform ND 0.0086 0.0023 mg/kg
95-49-8 o-Chlorotoluene ND 0.0086 0.0017 mg/kg
106-43-4 p-Chlorotoluene ND 0.0086 0.0017 mg/kg
124-48-1 Dibromochloromethane ND 0.0086 0.0017 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0086 0.0017 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0086 0.0034 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0086 0.0017 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0086 0.0017 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0086 0.0020 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0086 0.0030 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0086 0.0017 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0086 0.0017 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0086 0.0024 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0086 0.0017 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0086 0.0017 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0086 0.0017 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0086 0.0017 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0086 0.0018 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0086 0.0017 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:SED DUP-D
Lab Sample ID:FA68836-18 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:81.0
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0086 0.0017 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0086 0.0040 mg/kg
64-17-5 Ethyl Alcohol e 0.935 0.69 0.13 mg/kg
100-41-4 Ethylbenzene ND 0.0086 0.0017 mg/kg
591-78-6 2-Hexanone ND 0.043 0.013 mg/kg
98-82-8 Isopropylbenzene ND 0.0086 0.0017 mg/kg
99-87-6 p-Isopropyltoluene ND 0.0086 0.0017 mg/kg
74-83-9 Methyl Bromide ND 0.0086 0.0034 mg/kg
74-87-3 Methyl Chloride ND 0.0086 0.0034 mg/kg
75-09-2 Methylene Chloride f ND 0.034 0.019 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.043 0.013 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0086 0.0017 mg/kg
91-20-3 Naphthalene ND 0.0086 0.0034 mg/kg
103-65-1 n-Propylbenzene ND 0.0086 0.0017 mg/kg
100-42-5 Styrene ND 0.0086 0.0017 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0086 0.0018 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0086 0.0017 mg/kg
127-18-4 Tetrachloroethylene ND 0.0086 0.0022 mg/kg
108-88-3 Toluene 0.0346 0.034 0.017 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0086 0.0024 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0086 0.0017 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0086 0.0017 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0086 0.0017 mg/kg
79-01-6 Trichloroethylene ND 0.0086 0.0017 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0086 0.0034 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0086 0.0021 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0086 0.0017 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0086 0.0017 mg/kg
108-05-4 Vinyl Acetate ND 0.043 0.028 mg/kg
75-01-4 Vinyl Chloride ND 0.0086 0.0017 mg/kg
m,p-Xylene ND 0.017 0.0019 mg/kg
95-47-6 o-Xylene ND 0.0086 0.0017 mg/kg
1330-20-7 Xylene (total)ND 0.026 0.0036 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%75-124%
17060-07-0 1,2-Dichloroethane-D4 122%72-135%
2037-26-5 Toluene-D8 113%75-126%
460-00-4 4-Bromofluorobenzene 117%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
104 of 189
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Report of Analysis Page 3 of 3
Client Sample ID:SED DUP-D
Lab Sample ID:FA68836-18 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8260D Percent Solids:81.0
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Results reported from Bisulfate preserved sample.
(b) Associated CCV outside of control limits high.
(c) Initial calibration response factors not 8260D compliant.
(d) Associated ICV and BS outside control limits high, however sample ND. Associated CCV outside of control limits
high, sample was ND.
(e) Associated BS recovery outside control limits, high. Associated CCV outside of control limits high.
(f) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
105 of 189
FA6883633.18
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:SED DUP-D
Lab Sample ID:FA68836-18 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:81.0
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X067546.D 1 10/16/19 11:49 MV 10/11/19 12:40 OP77248 SX2781
Run #2
Initial Weight Final Volume
Run #1 30.5 g 10.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 10 2.0 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 2.0 0.23 mg/kg
95-57-8 2-Chlorophenol ND 2.0 0.25 mg/kg
120-83-2 2,4-Dichlorophenol ND 2.0 0.23 mg/kg
105-67-9 2,4-Dimethylphenol ND 2.0 0.54 mg/kg
51-28-5 2,4-Dinitrophenol ND 10 2.0 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 4.0 0.81 mg/kg
95-48-7 2-Methylphenol ND 2.0 0.24 mg/kg
3&4-Methylphenol ND 2.0 0.33 mg/kg
88-75-5 2-Nitrophenol ND 2.0 0.22 mg/kg
100-02-7 4-Nitrophenol ND 10 2.0 mg/kg
87-86-5 Pentachlorophenol ND 10 2.0 mg/kg
108-95-2 Phenol ND 2.0 0.20 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 2.0 0.23 mg/kg
83-32-9 Acenaphthene ND 2.0 0.21 mg/kg
208-96-8 Acenaphthylene ND 2.0 0.20 mg/kg
120-12-7 Anthracene ND 2.0 0.23 mg/kg
56-55-3 Benzo(a)anthracene ND 2.0 0.20 mg/kg
50-32-8 Benzo(a)pyrene ND 2.0 0.24 mg/kg
205-99-2 Benzo(b)fluoranthene ND 2.0 0.22 mg/kg
191-24-2 Benzo(g,h,i)perylene 0.273 2.0 0.21 mg/kg J
207-08-9 Benzo(k)fluoranthene ND 2.0 0.27 mg/kg
100-51-6 Benzyl Alcohol ND 2.0 0.20 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 2.0 0.21 mg/kg
85-68-7 Butyl benzyl phthalate ND 2.0 0.40 mg/kg
106-47-8 4-Chloroaniline ND 2.0 0.51 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 2.0 0.20 mg/kg
111-44-4 bis(2-Chloroethyl)ether a ND 2.0 0.23 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 2.0 0.25 mg/kg
91-58-7 2-Chloronaphthalene ND 2.0 0.20 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 2.0 0.20 mg/kg
218-01-9 Chrysene ND 2.0 0.21 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:SED DUP-D
Lab Sample ID:FA68836-18 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Method:SW846 8270E SW846 3546 Percent Solids:81.0
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 2.0 0.25 mg/kg
132-64-9 Dibenzofuran ND 2.0 0.20 mg/kg
95-50-1 1,2-Dichlorobenzene ND 2.0 0.20 mg/kg
541-73-1 1,3-Dichlorobenzene ND 2.0 0.22 mg/kg
106-46-7 1,4-Dichlorobenzene ND 2.0 0.27 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 2.0 0.48 mg/kg
84-66-2 Diethyl Phthalate ND 4.0 0.40 mg/kg
131-11-3 Dimethyl Phthalate ND 2.0 0.40 mg/kg
117-84-0 Di-n-octyl Phthalate ND 2.0 0.40 mg/kg
84-74-2 Di-n-butyl Phthalate ND 4.0 0.81 mg/kg
122-66-7 1,2-Diphenylhydrazine ND 2.0 0.20 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.0 0.40 mg/kg
206-44-0 Fluoranthene ND 2.0 0.20 mg/kg
86-73-7 Fluorene ND 2.0 0.22 mg/kg
118-74-1 Hexachlorobenzene ND 2.0 0.21 mg/kg
87-68-3 Hexachlorobutadiene ND 2.0 0.20 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 2.0 0.40 mg/kg
67-72-1 Hexachloroethane ND 2.0 0.24 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 2.0 0.25 mg/kg
78-59-1 Isophorone ND 2.0 0.20 mg/kg
90-12-0 1-Methylnaphthalene ND 2.0 0.20 mg/kg
91-57-6 2-Methylnaphthalene ND 2.0 0.20 mg/kg
91-20-3 Naphthalene ND 2.0 0.20 mg/kg
98-95-3 Nitrobenzene ND 2.0 0.20 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 2.0 0.20 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 2.0 0.22 mg/kg
85-01-8 Phenanthrene ND 2.0 0.20 mg/kg
129-00-0 Pyrene ND 2.0 0.23 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.24 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 59%40-102%
4165-62-2 Phenol-d5 70%41-100%
118-79-6 2,4,6-Tribromophenol 67%42-108%
4165-60-0 Nitrobenzene-d5 56%40-105%
321-60-8 2-Fluorobiphenyl 63%43-107%
1718-51-0 Terphenyl-d14 65%45-119%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
107 of 189
FA6883633.18
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:SED DUP-D
Lab Sample ID:FA68836-18 Date Sampled:10/05/19
Matrix:SO - Soil Date Received:10/09/19
Percent Solids:81.0
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Barium a 24.4 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Cadmium a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Chromium a 8.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Lead a 3.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Mercury <0.050 0.050 mg/kg 1 10/10/19 10/10/19 JC SW846 7471B 1 SW846 7471B 3
Selenium a 1.7 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
Silver a <1.1 1.1 mg/kg 20 10/12/19 10/15/19 DM SW846 6020B 2 SW846 3050B 4
(1) Instrument QC Batch: MA16239
(2) Instrument QC Batch: MA16253
(3) Prep QC Batch: MP36237
(4) Prep QC Batch: MP36254
(a) Sample dilution required due to difficult matrix.
RL = Reporting Limit
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Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA68836-19 Date Sampled:10/05/19
Matrix:AQ - Trip Blank Water Date Received:10/09/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0136294.D 1 10/12/19 17:22 AB n/a n/a VC5431
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA68836-19 Date Sampled:10/05/19
Matrix:AQ - Trip Blank Water Date Received:10/09/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%83-118%
17060-07-0 1,2-Dichloroethane-D4 104%79-125%
2037-26-5 Toluene-D8 96%85-112%
460-00-4 4-Bromofluorobenzene 100%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
111 of 189
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FA68836: Chain of Custody
Page 1 of 3
112 of 189
FA6883644.1
FA68836: Chain of Custody
Page 2 of 3
113 of 189
FA6883644.1
Job Number:FA68836 Client:RESOLVE ENV.
Date / Time Received:10/9/2019 9:00:00 AM Delivery Method:FX
Project:ELAN-INDIAN TRAIL
Airbill #'s:
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (0.9);
Cooler 1: (1.9);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:11Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:1; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:PETERH Date:Date:10/9/2019 9:00:00 AM
FA68836: Chain of Custody
Page 3 of 3
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SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
115 of 189
FA688365
Method Blank Summary Page 1 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B517-MB 2B13560.D 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-3, FA68836-4, FA68836-6, FA68836-7, FA68836-8, FA68836-14, FA68836-16, FA68836-18
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
108-86-1 Bromobenzene ND 5.0 1.0 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 2.3 ug/kg
64-17-5 Ethyl Alcohol ND 400 75 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
116 of 189
FA6883655.1.1
Method Blank Summary Page 2 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B517-MB 2B13560.D 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-3, FA68836-4, FA68836-6, FA68836-7, FA68836-8, FA68836-14, FA68836-16, FA68836-18
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone 7.6 25 7.5 ug/kg J
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene Chloride ND 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 16 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%75-124%
17060-07-0 1,2-Dichloroethane-D4 113%72-135%
2037-26-5 Toluene-D8 101%75-126%
117 of 189
FA6883655.1.1
Method Blank Summary Page 3 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B517-MB 2B13560.D 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-3, FA68836-4, FA68836-6, FA68836-7, FA68836-8, FA68836-14, FA68836-16, FA68836-18
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 92%71-133%
118 of 189
FA6883655.1.1
Method Blank Summary Page 1 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B518-MB 2B13597.D 1 10/11/19 SP n/a n/a V2B518
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-1, FA68836-2, FA68836-4, FA68836-5, FA68836-6, FA68836-7
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
108-86-1 Bromobenzene ND 5.0 1.0 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 2.3 ug/kg
64-17-5 Ethyl Alcohol ND 400 75 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
119 of 189
FA6883655.1.2
Method Blank Summary Page 2 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B518-MB 2B13597.D 1 10/11/19 SP n/a n/a V2B518
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-1, FA68836-2, FA68836-4, FA68836-5, FA68836-6, FA68836-7
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene Chloride ND 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 16 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%75-124%
17060-07-0 1,2-Dichloroethane-D4 116%72-135%
2037-26-5 Toluene-D8 101%75-126%
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FA6883655.1.2
Method Blank Summary Page 3 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B518-MB 2B13597.D 1 10/11/19 SP n/a n/a V2B518
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-1, FA68836-2, FA68836-4, FA68836-5, FA68836-6, FA68836-7
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 87%71-133%
121 of 189
FA6883655.1.2
Method Blank Summary Page 1 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5431-MB C0136281.D 1 10/12/19 AB n/a n/a VC5431
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-13, FA68836-15, FA68836-17, FA68836-19
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
122 of 189
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Method Blank Summary Page 2 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5431-MB C0136281.D 1 10/12/19 AB n/a n/a VC5431
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-13, FA68836-15, FA68836-17, FA68836-19
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%83-118%
17060-07-0 1,2-Dichloroethane-D4 105%79-125%
2037-26-5 Toluene-D8 97%85-112%
123 of 189
FA6883655.1.3
Method Blank Summary Page 3 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5431-MB C0136281.D 1 10/12/19 AB n/a n/a VC5431
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-13, FA68836-15, FA68836-17, FA68836-19
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 100%83-118%
124 of 189
FA6883655.1.3
Blank Spike Summary Page 1 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B517-BS 2B13561.D 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-3, FA68836-4, FA68836-6, FA68836-7, FA68836-8, FA68836-14, FA68836-16, FA68836-18
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 360 144 61-152
71-43-2 Benzene 50 52.9 106 76-126
108-86-1 Bromobenzene 50 48.9 98 76-122
74-97-5 Bromochloromethane 50 50.5 101 77-120
75-27-4 Bromodichloromethane 50 54.4 109 74-130
75-25-2 Bromoform 50 53.2 106 76-127
78-93-3 2-Butanone (MEK)250 315 126 75-137
104-51-8 n-Butylbenzene 50 54.7 109 71-128
135-98-8 sec-Butylbenzene 50 52.2 104 79-135
98-06-6 tert-Butylbenzene 50 50.7 101 77-133
56-23-5 Carbon Tetrachloride 50 58.2 116 78-133
108-90-7 Chlorobenzene 50 53.1 106 81-129
75-00-3 Chloroethane 50 69.9 140*68-133
67-66-3 Chloroform 50 57.7 115 72-123
95-49-8 o-Chlorotoluene 50 53.3 107 77-129
106-43-4 p-Chlorotoluene 50 52.0 104 80-134
124-48-1 Dibromochloromethane 50 52.6 105 76-127
106-93-4 1,2-Dibromoethane 50 50.8 102 77-126
75-71-8 Dichlorodifluoromethane 50 46.5 93 68-168
95-50-1 1,2-Dichlorobenzene 50 49.5 99 80-129
541-73-1 1,3-Dichlorobenzene 50 50.5 101 81-129
106-46-7 1,4-Dichlorobenzene 50 51.0 102 76-130
75-34-3 1,1-Dichloroethane 50 59.1 118 73-125
107-06-2 1,2-Dichloroethane 50 57.1 114 74-128
75-35-4 1,1-Dichloroethylene 50 59.1 118 81-136
156-59-2 cis-1,2-Dichloroethylene 50 54.5 109 74-126
156-60-5 trans-1,2-Dichloroethylene 50 57.8 116 70-127
78-87-5 1,2-Dichloropropane 50 52.5 105 74-125
142-28-9 1,3-Dichloropropane 50 49.6 99 76-122
594-20-7 2,2-Dichloropropane 50 65.4 131 77-133
563-58-6 1,1-Dichloropropene 50 55.9 112 75-130
10061-01-5 cis-1,3-Dichloropropene 50 48.3 97 80-123
10061-02-6 trans-1,3-Dichloropropene 50 54.0 108 75-131
108-20-3 Di-Isopropyl Ether 50 54.9 110 75-122
64-17-5 Ethyl Alcohol 1000 1620 162*53-154
100-41-4 Ethylbenzene 50 55.6 111 77-123
* = Outside of Control Limits.
125 of 189
FA6883655.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B517-BS 2B13561.D 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-3, FA68836-4, FA68836-6, FA68836-7, FA68836-8, FA68836-14, FA68836-16, FA68836-18
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 270 108 72-133
98-82-8 Isopropylbenzene 50 56.5 113 80-136
99-87-6 p-Isopropyltoluene 50 52.2 104 77-131
74-83-9 Methyl Bromide 50 57.8 116 65-139
74-87-3 Methyl Chloride 50 54.7 109 71-144
75-09-2 Methylene Chloride 50 63.0 126 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 280 112 76-132
1634-04-4 Methyl Tert Butyl Ether 50 47.1 94 77-120
91-20-3 Naphthalene 50 49.6 99 79-129
103-65-1 n-Propylbenzene 50 52.3 105 80-135
100-42-5 Styrene 50 51.4 103 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 55.2 110 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 54.5 109 71-126
127-18-4 Tetrachloroethylene 50 52.1 104 79-130
108-88-3 Toluene 50 51.5 103 76-124
87-61-6 1,2,3-Trichlorobenzene 50 47.2 94 77-128
120-82-1 1,2,4-Trichlorobenzene 50 47.4 95 78-130
71-55-6 1,1,1-Trichloroethane 50 57.5 115 70-129
79-00-5 1,1,2-Trichloroethane 50 51.2 102 74-124
79-01-6 Trichloroethylene 50 53.4 107 75-128
75-69-4 Trichlorofluoromethane 50 63.1 126 73-145
96-18-4 1,2,3-Trichloropropane 50 52.1 104 74-127
95-63-6 1,2,4-Trimethylbenzene 50 51.4 103 74-123
108-67-8 1,3,5-Trimethylbenzene 50 52.1 104 73-122
108-05-4 Vinyl Acetate 250 278 111 48-164
75-01-4 Vinyl Chloride 50 56.0 112 76-141
m,p-Xylene 100 111 111 80-128
95-47-6 o-Xylene 50 54.2 108 80-132
1330-20-7 Xylene (total)150 165 110 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 108%72-135%
2037-26-5 Toluene-D8 100%75-126%
* = Outside of Control Limits.
126 of 189
FA6883655.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B517-BS 2B13561.D 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-3, FA68836-4, FA68836-6, FA68836-7, FA68836-8, FA68836-14, FA68836-16, FA68836-18
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 89%71-133%
* = Outside of Control Limits.
127 of 189
FA6883655.2.1
Blank Spike Summary Page 1 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B518-BS 2B13596.D 1 10/11/19 SP n/a n/a V2B518
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-1, FA68836-2, FA68836-4, FA68836-5, FA68836-6, FA68836-7
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 339 136 61-152
71-43-2 Benzene 50 54.0 108 76-126
108-86-1 Bromobenzene 50 48.7 97 76-122
74-97-5 Bromochloromethane 50 51.8 104 77-120
75-27-4 Bromodichloromethane 50 58.4 117 74-130
75-25-2 Bromoform 50 54.8 110 76-127
78-93-3 2-Butanone (MEK)250 327 131 75-137
104-51-8 n-Butylbenzene 50 54.5 109 71-128
135-98-8 sec-Butylbenzene 50 52.9 106 79-135
98-06-6 tert-Butylbenzene 50 54.3 109 77-133
56-23-5 Carbon Tetrachloride 50 57.3 115 78-133
108-90-7 Chlorobenzene 50 53.3 107 81-129
75-00-3 Chloroethane 50 71.1 142*68-133
67-66-3 Chloroform 50 58.3 117 72-123
95-49-8 o-Chlorotoluene 50 53.4 107 77-129
106-43-4 p-Chlorotoluene 50 51.8 104 80-134
124-48-1 Dibromochloromethane 50 55.8 112 76-127
106-93-4 1,2-Dibromoethane 50 53.4 107 77-126
75-71-8 Dichlorodifluoromethane 50 40.4 81 68-168
95-50-1 1,2-Dichlorobenzene 50 49.8 100 80-129
541-73-1 1,3-Dichlorobenzene 50 50.4 101 81-129
106-46-7 1,4-Dichlorobenzene 50 51.4 103 76-130
75-34-3 1,1-Dichloroethane 50 59.2 118 73-125
107-06-2 1,2-Dichloroethane 50 61.2 122 74-128
75-35-4 1,1-Dichloroethylene 50 57.3 115 81-136
156-59-2 cis-1,2-Dichloroethylene 50 54.1 108 74-126
156-60-5 trans-1,2-Dichloroethylene 50 56.8 114 70-127
78-87-5 1,2-Dichloropropane 50 55.1 110 74-125
142-28-9 1,3-Dichloropropane 50 52.9 106 76-122
594-20-7 2,2-Dichloropropane 50 63.0 126 77-133
563-58-6 1,1-Dichloropropene 50 56.6 113 75-130
10061-01-5 cis-1,3-Dichloropropene 50 52.6 105 80-123
10061-02-6 trans-1,3-Dichloropropene 50 59.0 118 75-131
108-20-3 Di-Isopropyl Ether 50 58.1 116 75-122
64-17-5 Ethyl Alcohol 1000 1100 110 53-154
100-41-4 Ethylbenzene 50 55.7 111 77-123
* = Outside of Control Limits.
128 of 189
FA6883655.2.2
Blank Spike Summary Page 2 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B518-BS 2B13596.D 1 10/11/19 SP n/a n/a V2B518
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-1, FA68836-2, FA68836-4, FA68836-5, FA68836-6, FA68836-7
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 317 127 72-133
98-82-8 Isopropylbenzene 50 57.1 114 80-136
99-87-6 p-Isopropyltoluene 50 52.0 104 77-131
74-83-9 Methyl Bromide 50 52.5 105 65-139
74-87-3 Methyl Chloride 50 48.8 98 71-144
75-09-2 Methylene Chloride 50 67.6 135 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 327 131 76-132
1634-04-4 Methyl Tert Butyl Ether 50 55.1 110 77-120
91-20-3 Naphthalene 50 51.9 104 79-129
103-65-1 n-Propylbenzene 50 52.2 104 80-135
100-42-5 Styrene 50 51.9 104 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 57.4 115 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 57.2 114 71-126
127-18-4 Tetrachloroethylene 50 52.4 105 79-130
108-88-3 Toluene 50 52.7 105 76-124
87-61-6 1,2,3-Trichlorobenzene 50 48.7 97 77-128
120-82-1 1,2,4-Trichlorobenzene 50 47.5 95 78-130
71-55-6 1,1,1-Trichloroethane 50 55.9 112 70-129
79-00-5 1,1,2-Trichloroethane 50 55.1 110 74-124
79-01-6 Trichloroethylene 50 54.7 109 75-128
75-69-4 Trichlorofluoromethane 50 61.6 123 73-145
96-18-4 1,2,3-Trichloropropane 50 53.5 107 74-127
95-63-6 1,2,4-Trimethylbenzene 50 51.7 103 74-123
108-67-8 1,3,5-Trimethylbenzene 50 52.6 105 73-122
108-05-4 Vinyl Acetate 250 321 128 48-164
75-01-4 Vinyl Chloride 50 50.7 101 76-141
m,p-Xylene 100 112 112 80-128
95-47-6 o-Xylene 50 55.3 111 80-132
1330-20-7 Xylene (total)150 168 112 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%75-124%
17060-07-0 1,2-Dichloroethane-D4 114%72-135%
2037-26-5 Toluene-D8 101%75-126%
* = Outside of Control Limits.
129 of 189
FA6883655.2.2
Blank Spike Summary Page 3 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2B518-BS 2B13596.D 1 10/11/19 SP n/a n/a V2B518
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-1, FA68836-2, FA68836-4, FA68836-5, FA68836-6, FA68836-7
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 88%71-133%
* = Outside of Control Limits.
130 of 189
FA6883655.2.2
Blank Spike Summary Page 1 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5431-BS C0136280.D 1 10/12/19 AB n/a n/a VC5431
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-13, FA68836-15, FA68836-17, FA68836-19
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 125 119 95 50-147
71-43-2 Benzene 25 22.8 91 81-122
108-86-1 Bromobenzene 25 22.3 89 80-121
74-97-5 Bromochloromethane 25 21.9 88 76-123
75-27-4 Bromodichloromethane 25 24.3 97 79-123
75-25-2 Bromoform 25 21.8 87 66-123
78-93-3 2-Butanone (MEK)125 106 85 56-143
104-51-8 n-Butylbenzene 25 24.0 96 79-126
135-98-8 sec-Butylbenzene 25 23.7 95 83-133
98-06-6 tert-Butylbenzene 25 22.2 89 80-133
56-23-5 Carbon Tetrachloride 25 26.5 106 76-136
108-90-7 Chlorobenzene 25 21.9 88 82-124
75-00-3 Chloroethane 25 24.2 97 62-144
67-66-3 Chloroform 25 23.4 94 80-124
95-49-8 o-Chlorotoluene 25 22.5 90 81-127
106-43-4 p-Chlorotoluene 25 22.6 90 83-130
124-48-1 Dibromochloromethane 25 23.0 92 78-122
106-93-4 1,2-Dibromoethane 25 21.5 86 75-120
75-71-8 Dichlorodifluoromethane 25 26.2 105 42-167
95-50-1 1,2-Dichlorobenzene 25 21.9 88 82-124
541-73-1 1,3-Dichlorobenzene 25 22.6 90 84-125
106-46-7 1,4-Dichlorobenzene 25 22.3 89 78-120
75-34-3 1,1-Dichloroethane 25 23.9 96 81-122
107-06-2 1,2-Dichloroethane 25 22.5 90 75-125
75-35-4 1,1-Dichloroethylene 25 25.1 100 78-137
156-59-2 cis-1,2-Dichloroethylene 25 23.5 94 78-120
156-60-5 trans-1,2-Dichloroethylene 25 24.2 97 76-127
78-87-5 1,2-Dichloropropane 25 23.0 92 76-124
142-28-9 1,3-Dichloropropane 25 20.8 83 80-118
594-20-7 2,2-Dichloropropane 25 24.9 100 74-139
563-58-6 1,1-Dichloropropene 25 25.4 102 79-131
10061-01-5 cis-1,3-Dichloropropene 25 23.0 92 75-118
10061-02-6 trans-1,3-Dichloropropene 25 22.8 91 80-120
108-20-3 Di-Isopropyl Ether 25 21.7 87 68-123
64-17-5 Ethyl Alcohol 500 515 103 46-145
100-41-4 Ethylbenzene 25 22.7 91 81-121
* = Outside of Control Limits.
131 of 189
FA6883655.2.3
Blank Spike Summary Page 2 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5431-BS C0136280.D 1 10/12/19 AB n/a n/a VC5431
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-13, FA68836-15, FA68836-17, FA68836-19
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 125 99.1 79 61-129
98-82-8 Isopropylbenzene 25 24.1 96 83-132
99-87-6 p-Isopropyltoluene 25 23.3 93 79-130
74-83-9 Methyl Bromide 25 22.6 90 59-143
74-87-3 Methyl Chloride 25 22.1 88 50-159
75-09-2 Methylene Chloride 25 18.1 72 69-135
108-10-1 4-Methyl-2-pentanone (MIBK)125 101 81 66-122
1634-04-4 Methyl Tert Butyl Ether 25 21.4 86 72-117
91-20-3 Naphthalene 25 20.3 81 63-132
103-65-1 n-Propylbenzene 25 22.9 92 82-133
100-42-5 Styrene 25 22.0 88 78-119
630-20-6 1,1,1,2-Tetrachloroethane 25 23.9 96 77-122
79-34-5 1,1,2,2-Tetrachloroethane 25 21.1 84 72-120
127-18-4 Tetrachloroethylene 25 23.9 96 76-135
108-88-3 Toluene 25 22.7 91 80-120
87-61-6 1,2,3-Trichlorobenzene 25 21.3 85 68-131
120-82-1 1,2,4-Trichlorobenzene 25 22.4 90 73-129
71-55-6 1,1,1-Trichloroethane 25 24.5 98 75-130
79-00-5 1,1,2-Trichloroethane 25 21.1 84 76-119
79-01-6 Trichloroethylene 25 23.4 94 81-126
75-69-4 Trichlorofluoromethane 25 27.4 110 71-156
96-18-4 1,2,3-Trichloropropane 25 20.4 82 77-120
95-63-6 1,2,4-Trimethylbenzene 25 21.6 86 79-120
108-67-8 1,3,5-Trimethylbenzene 25 22.9 92 79-120
108-05-4 Vinyl Acetate 125 109 87 43-154
75-01-4 Vinyl Chloride 25 26.0 104 69-159
m,p-Xylene 50 46.1 92 79-126
95-47-6 o-Xylene 25 22.6 90 80-127
1330-20-7 Xylene (total)75 68.8 92 80-126
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%83-118%
17060-07-0 1,2-Dichloroethane-D4 102%79-125%
2037-26-5 Toluene-D8 98%85-112%
* = Outside of Control Limits.
132 of 189
FA6883655.2.3
Blank Spike Summary Page 3 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5431-BS C0136280.D 1 10/12/19 AB n/a n/a VC5431
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-13, FA68836-15, FA68836-17, FA68836-19
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 99%83-118%
* = Outside of Control Limits.
133 of 189
FA6883655.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68836-4MS a 2B13583.D 1 10/10/19 SP n/a n/a V2B517
FA68836-4MSD a 2B13584.D 1 10/10/19 SP n/a n/a V2B517
FA68836-4 b 2B13569.D 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-3, FA68836-4, FA68836-6, FA68836-7, FA68836-8, FA68836-14, FA68836-16, FA68836-18
FA68836-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 522 303 326 -65*300 461 -20*34*61-152/27
71-43-2 Benzene ND 60.6 63.7 105 59.9 61.4 102 4 76-126/26
108-86-1 Bromobenzene ND 60.6 42.7 70*59.9 44.7 75*5 76-122/32
74-97-5 Bromochloromethane ND 60.6 47.1 78 59.9 54.5 91 15 77-120/24
75-27-4 Bromodichloromethane ND 60.6 56.8 94 59.9 60.8 101 7 74-130/25
75-25-2 Bromoform ND 60.6 35.8 59*59.9 45.1 75*23 76-127/26
78-93-3 2-Butanone (MEK)ND 303 203 67*300 324 108 46*75-137/25
104-51-8 n-Butylbenzene ND 60.6 56.0 92 59.9 52.8 88 6 71-128/35
135-98-8 sec-Butylbenzene ND 60.6 60.3 99 59.9 57.8 96 4 79-135/34
98-06-6 tert-Butylbenzene ND 60.6 57.0 94 59.9 59.4 99 4 77-133/34
56-23-5 Carbon Tetrachloride ND 60.6 86.5 143*59.9 68.0 114 24 78-133/29
108-90-7 Chlorobenzene ND 60.6 55.5 92 59.9 54.3 91 2 81-129/29
75-00-3 Chloroethane ND 60.6 125 206*59.9 68.2 114 59*68-133/29
67-66-3 Chloroform ND 60.6 65.7 108 59.9 67.8 113 3 72-123/26
95-49-8 o-Chlorotoluene ND 60.6 54.4 90 59.9 53.4 89 2 77-129/33
106-43-4 p-Chlorotoluene ND 60.6 49.6 82 59.9 47.6 79*4 80-134/33
124-48-1 Dibromochloromethane ND 60.6 43.2 71*59.9 54.0 90 22 76-127/27
106-93-4 1,2-Dibromoethane ND 60.6 38.2 63*59.9 48.8 81 24 77-126/26
75-71-8 Dichlorodifluoromethane ND 60.6 73.2 121 59.9 52.7 88 33*68-168/29
95-50-1 1,2-Dichlorobenzene ND 60.6 34.1 56*59.9 37.4 62*9 80-129/32
541-73-1 1,3-Dichlorobenzene ND 60.6 39.3 65*59.9 40.6 68*3 81-129/33
106-46-7 1,4-Dichlorobenzene ND 60.6 38.9 64*59.9 40.3 67*4 76-130/32
75-34-3 1,1-Dichloroethane ND 60.6 71.5 118 59.9 70.4 118 2 73-125/27
107-06-2 1,2-Dichloroethane ND 60.6 51.1 84 59.9 62.7 105 20 74-128/23
75-35-4 1,1-Dichloroethylene ND 60.6 90.0 148*59.9 71.4 119 23 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 60.6 60.7 100 59.9 62.7 105 3 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 60.6 74.3 123 59.9 67.6 113 9 70-127/27
78-87-5 1,2-Dichloropropane ND 60.6 60.2 99 59.9 59.3 99 2 74-125/25
142-28-9 1,3-Dichloropropane ND 60.6 41.5 68*59.9 51.9 87 22 76-122/26
594-20-7 2,2-Dichloropropane ND 60.6 99.5 164*59.9 72.0 120 32*77-133/28
563-58-6 1,1-Dichloropropene ND 60.6 67.4 111 59.9 66.9 112 1 75-130/28
10061-01-5 cis-1,3-Dichloropropene ND 60.6 48.4 80 59.9 50.9 85 5 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 60.6 44.4 73*59.9 55.4 92 22 75-131/28
108-20-3 Di-Isopropyl Ether ND 60.6 74.2 122 59.9 67.2 112 10 75-122/25
64-17-5 Ethyl Alcohol ND 1210 12700 1047*1200 6490 542*65*53-154/42
100-41-4 Ethylbenzene ND 60.6 66.3 109 59.9 61.9 103 7 77-123/31
* = Outside of Control Limits.
134 of 189
FA6883655.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68836-4MS a 2B13583.D 1 10/10/19 SP n/a n/a V2B517
FA68836-4MSD a 2B13584.D 1 10/10/19 SP n/a n/a V2B517
FA68836-4 b 2B13569.D 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-3, FA68836-4, FA68836-6, FA68836-7, FA68836-8, FA68836-14, FA68836-16, FA68836-18
FA68836-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone ND 303 134 44*300 223 74 50*72-133/26
98-82-8 Isopropylbenzene ND 60.6 67.3 111 59.9 63.6 106 6 80-136/32
99-87-6 p-Isopropyltoluene 16.1 60.6 57.8 69*59.9 54.6 64*6 77-131/34
74-83-9 Methyl Bromide ND 60.6 86.6 143*59.9 63.9 107 30 65-139/31
74-87-3 Methyl Chloride ND 60.6 79.8 132 59.9 60.0 100 28*71-144/27
75-09-2 Methylene Chloride ND 60.6 81.2 134 59.9 78.5 131 3 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 303 176 58*300 303 101 53*76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 60.6 52.1 86 59.9 54.3 91 4 77-120/24
91-20-3 Naphthalene ND 60.6 14.0 23*59.9 20.5 34*38*79-129/33
103-65-1 n-Propylbenzene ND 60.6 60.3 99 59.9 56.7 95 6 80-135/33
100-42-5 Styrene ND 60.6 43.9 72*59.9 40.5 68*8 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 60.6 56.8 94 59.9 62.2 104 9 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane ND 60.6 36.4 60*59.9 48.8 81 29 71-126/30
127-18-4 Tetrachloroethylene ND 60.6 61.0 101 59.9 61.9 103 1 79-130/31
108-88-3 Toluene ND 60.6 57.7 95 59.9 60.7 101 5 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 60.6 16.4 27*59.9 22.0 37*29 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 60.6 20.1 33*59.9 25.3 42*23 78-130/34
71-55-6 1,1,1-Trichloroethane ND 60.6 86.1 142*59.9 67.2 112 25 70-129/27
79-00-5 1,1,2-Trichloroethane ND 60.6 42.3 70*59.9 53.9 90 24 74-124/28
79-01-6 Trichloroethylene ND 60.6 63.8 105 59.9 62.6 104 2 75-128/27
75-69-4 Trichlorofluoromethane ND 60.6 107 176*59.9 74.9 125 35*73-145/31
96-18-4 1,2,3-Trichloropropane ND 60.6 33.8 56*59.9 46.3 77 31*74-127/27
95-63-6 1,2,4-Trimethylbenzene ND 60.6 51.9 86 59.9 50.4 84 3 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 60.6 55.9 92 59.9 54.8 91 2 73-122/33
108-05-4 Vinyl Acetate ND 303 85.1 28*300 117 39*32 48-164/37
75-01-4 Vinyl Chloride ND 60.6 92.8 153*59.9 64.1 107 37*76-141/27
m,p-Xylene ND 121 130 107 120 122 102 6 80-128/30
95-47-6 o-Xylene ND 60.6 60.2 99 59.9 58.7 98 3 80-132/30
1330-20-7 Xylene (total)ND 182 191 105 180 180 100 6 80-129/30
CAS No.Surrogate Recoveries MS MSD FA68836-4 Limits
1868-53-7 Dibromofluoromethane 95%103%100%75-124%
17060-07-0 1,2-Dichloroethane-D4 94%111%114%72-135%
2037-26-5 Toluene-D8 96%105%101%75-126%
* = Outside of Control Limits.
135 of 189
FA6883655.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68836-4MS a 2B13583.D 1 10/10/19 SP n/a n/a V2B517
FA68836-4MSD a 2B13584.D 1 10/10/19 SP n/a n/a V2B517
FA68836-4 b 2B13569.D 1 10/10/19 SP n/a n/a V2B517
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-3, FA68836-4, FA68836-6, FA68836-7, FA68836-8, FA68836-14, FA68836-16, FA68836-18
CAS No.Surrogate Recoveries MS MSD FA68836-4 Limits
460-00-4 4-Bromofluorobenzene 87%89%94%71-133%
(a) Results reported from Bisulfate preserved sample.
(b) Results reported from Bisulfate preserved sample. Internal standard response outside control limits. Confirmed
by MS/MSD.
* = Outside of Control Limits.
136 of 189
FA6883655.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68904-9MS a 2B13618.D 1 10/12/19 SP n/a n/a V2B518
FA68904-9MSD a 2B13619.D 1 10/12/19 SP n/a n/a V2B518
FA68904-9 b 2B13617.D 1 10/12/19 SP n/a n/a V2B518
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-1, FA68836-2, FA68836-4, FA68836-5, FA68836-6, FA68836-7
FA68904-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone ND 313 526 168*309 560 181*6 61-152/27
71-43-2 Benzene ND 62.6 63.0 101 61.8 64.6 104 3 76-126/26
108-86-1 Bromobenzene ND 62.6 46.0 73*61.8 48.9 79 6 76-122/32
74-97-5 Bromochloromethane ND 62.6 55.5 89 61.8 58.4 94 5 77-120/24
75-27-4 Bromodichloromethane ND 62.6 64.3 103 61.8 67.4 109 5 74-130/25
75-25-2 Bromoform ND 62.6 54.3 87 61.8 58.7 95 8 76-127/26
78-93-3 2-Butanone (MEK)ND 313 418 134 309 465 150*11 75-137/25
104-51-8 n-Butylbenzene ND 62.6 50.6 81 61.8 54.4 88 7 71-128/35
135-98-8 sec-Butylbenzene ND 62.6 53.1 85 61.8 55.1 89 4 79-135/34
98-06-6 tert-Butylbenzene ND 62.6 55.6 89 61.8 57.3 93 3 77-133/34
56-23-5 Carbon Tetrachloride ND 62.6 68.6 110 61.8 69.4 112 1 78-133/29
108-90-7 Chlorobenzene ND 62.6 57.3 92 61.8 58.8 95 3 81-129/29
75-00-3 Chloroethane ND 62.6 72.9 116 61.8 74.0 120 1 68-133/29
67-66-3 Chloroform ND 62.6 70.2 112 61.8 71.2 115 1 72-123/26
95-49-8 o-Chlorotoluene ND 62.6 53.0 85 61.8 54.5 88 3 77-129/33
106-43-4 p-Chlorotoluene ND 62.6 49.8 80 61.8 52.4 85 5 80-134/33
124-48-1 Dibromochloromethane ND 62.6 56.6 90 61.8 60.5 98 7 76-127/27
106-93-4 1,2-Dibromoethane ND 62.6 53.0 85 61.8 57.7 93 8 77-126/26
75-71-8 Dichlorodifluoromethane ND 62.6 55.3 88 61.8 52.5 85 5 68-168/29
95-50-1 1,2-Dichlorobenzene ND 62.6 42.0 67*61.8 44.2 71*5 80-129/32
541-73-1 1,3-Dichlorobenzene ND 62.6 43.9 70*61.8 45.9 74*4 81-129/33
106-46-7 1,4-Dichlorobenzene ND 62.6 44.7 71*61.8 46.8 76 5 76-130/32
75-34-3 1,1-Dichloroethane ND 62.6 72.3 115 61.8 73.0 118 1 73-125/27
107-06-2 1,2-Dichloroethane ND 62.6 69.4 111 61.8 72.3 117 4 74-128/23
75-35-4 1,1-Dichloroethylene ND 62.6 72.8 116 61.8 72.0 116 1 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 62.6 62.4 100 61.8 64.2 104 3 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 62.6 68.0 109 61.8 68.4 111 1 70-127/27
78-87-5 1,2-Dichloropropane ND 62.6 61.6 98 61.8 64.7 105 5 74-125/25
142-28-9 1,3-Dichloropropane ND 62.6 54.3 87 61.8 58.6 95 8 76-122/26
594-20-7 2,2-Dichloropropane ND 62.6 69.3 111 61.8 70.7 114 2 77-133/28
563-58-6 1,1-Dichloropropene ND 62.6 69.1 110 61.8 69.7 113 1 75-130/28
10061-01-5 cis-1,3-Dichloropropene ND 62.6 54.2 87 61.8 57.7 93 6 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 62.6 58.2 93 61.8 62.8 102 8 75-131/28
108-20-3 Di-Isopropyl Ether ND 62.6 67.9 108 61.8 70.1 113 3 75-122/25
64-17-5 Ethyl Alcohol ND 1250 7570 604*1240 8340 674*10 53-154/42
100-41-4 Ethylbenzene ND 62.6 62.6 100 61.8 64.2 104 3 77-123/31
* = Outside of Control Limits.
137 of 189
FA6883655.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68904-9MS a 2B13618.D 1 10/12/19 SP n/a n/a V2B518
FA68904-9MSD a 2B13619.D 1 10/12/19 SP n/a n/a V2B518
FA68904-9 b 2B13617.D 1 10/12/19 SP n/a n/a V2B518
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-1, FA68836-2, FA68836-4, FA68836-5, FA68836-6, FA68836-7
FA68904-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone ND 313 265 85 309 409 132 43*72-133/26
98-82-8 Isopropylbenzene ND 62.6 62.9 100 61.8 64.1 104 2 80-136/32
99-87-6 p-Isopropyltoluene ND 62.6 50.9 81 61.8 53.5 87 5 77-131/34
74-83-9 Methyl Bromide ND 62.6 64.9 104 61.8 62.4 101 4 65-139/31
74-87-3 Methyl Chloride ND 62.6 61.2 98 61.8 60.5 98 1 71-144/27
75-09-2 Methylene Chloride ND 62.6 74.9 120 61.8 75.2 122 0 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 313 343 110 309 377 122 9 76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 62.6 55.4 88 61.8 57.3 93 3 77-120/24
91-20-3 Naphthalene ND 62.6 30.0 48*61.8 32.0 52*6 79-129/33
103-65-1 n-Propylbenzene ND 62.6 53.6 86 61.8 55.8 90 4 80-135/33
100-42-5 Styrene ND 62.6 42.1 67*61.8 43.2 70*3 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 62.6 62.4 100 61.8 63.7 103 2 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane ND 62.6 54.5 87 61.8 59.1 96 8 71-126/30
127-18-4 Tetrachloroethylene ND 62.6 58.5 93 61.8 60.6 98 4 79-130/31
108-88-3 Toluene ND 62.6 58.7 94 61.8 61.1 99 4 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 62.6 28.6 46*61.8 30.1 49*5 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 62.6 30.2 48*61.8 32.0 52*6 78-130/34
71-55-6 1,1,1-Trichloroethane ND 62.6 68.5 109 61.8 69.1 112 1 70-129/27
79-00-5 1,1,2-Trichloroethane ND 62.6 57.3 92 61.8 61.6 100 7 74-124/28
79-01-6 Trichloroethylene ND 62.6 64.2 103 61.8 65.4 106 2 75-128/27
75-69-4 Trichlorofluoromethane ND 62.6 81.3 130 61.8 77.1 125 5 73-145/31
96-18-4 1,2,3-Trichloropropane ND 62.6 52.0 83 61.8 56.5 91 8 74-127/27
95-63-6 1,2,4-Trimethylbenzene ND 62.6 49.6 79 61.8 51.5 83 4 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 62.6 51.6 82 61.8 53.7 87 4 73-122/33
108-05-4 Vinyl Acetate ND 313 132 42*309 146 47*10 48-164/37
75-01-4 Vinyl Chloride ND 62.6 65.3 104 61.8 63.6 103 3 76-141/27
m,p-Xylene ND 125 124 99 124 128 103 3 80-128/30
95-47-6 o-Xylene ND 62.6 59.4 95 61.8 61.0 99 3 80-132/30
1330-20-7 Xylene (total)ND 188 183 97 186 189 102 3 80-129/30
CAS No.Surrogate Recoveries MS MSD FA68904-9 Limits
1868-53-7 Dibromofluoromethane 107%106%109%75-124%
17060-07-0 1,2-Dichloroethane-D4 122%119%127%72-135%
2037-26-5 Toluene-D8 99%100%97%75-126%
* = Outside of Control Limits.
138 of 189
FA6883655.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68904-9MS a 2B13618.D 1 10/12/19 SP n/a n/a V2B518
FA68904-9MSD a 2B13619.D 1 10/12/19 SP n/a n/a V2B518
FA68904-9 b 2B13617.D 1 10/12/19 SP n/a n/a V2B518
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-1, FA68836-2, FA68836-4, FA68836-5, FA68836-6, FA68836-7
CAS No.Surrogate Recoveries MS MSD FA68904-9 Limits
460-00-4 4-Bromofluorobenzene 85%86%88%71-133%
(a) Results reported from Bisulfate preserved sample.
(b) Results reported from Bisulfate preserved sample. Internal standard response outside control limits. Confirmed
by MS/MSD.
* = Outside of Control Limits.
139 of 189
FA6883655.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68595-11MS C0136292.D 5 10/12/19 AB n/a n/a VC5431
FA68595-11MSD C0136293.D 5 10/12/19 AB n/a n/a VC5431
FA68595-11 a C0136282.D 1 10/12/19 AB n/a n/a VC5431
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-13, FA68836-15, FA68836-17, FA68836-19
FA68595-11 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 625 497 80 625 529 85 6 50-147/21
71-43-2 Benzene ND 125 114 91 125 115 92 1 81-122/14
108-86-1 Bromobenzene ND 125 110 88 125 110 88 0 80-121/14
74-97-5 Bromochloromethane ND 125 113 90 125 114 91 1 76-123/14
75-27-4 Bromodichloromethane ND 125 123 98 125 124 99 1 79-123/19
75-25-2 Bromoform ND 125 109 87 125 108 86 1 66-123/21
78-93-3 2-Butanone (MEK)ND 625 499 80 625 527 84 5 56-143/18
104-51-8 n-Butylbenzene ND 125 113 90 125 110 88 3 79-126/16
135-98-8 sec-Butylbenzene 0.38 J 125 113 90 125 111 88 2 83-133/16
98-06-6 tert-Butylbenzene 0.36 J 125 110 88 125 108 86 2 80-133/16
56-23-5 Carbon Tetrachloride ND 125 136 109 125 132 106 3 76-136/23
108-90-7 Chlorobenzene 2.9 125 114 89 125 112 87 2 82-124/14
75-00-3 Chloroethane ND 125 115 92 125 128 102 11 62-144/20
67-66-3 Chloroform ND 125 119 95 125 123 98 3 80-124/15
95-49-8 o-Chlorotoluene ND 125 110 88 125 108 86 2 81-127/15
106-43-4 p-Chlorotoluene ND 125 111 89 125 110 88 1 83-130/15
124-48-1 Dibromochloromethane ND 125 115 92 125 115 92 0 78-122/19
106-93-4 1,2-Dibromoethane ND 125 107 86 125 103 82 4 75-120/13
75-71-8 Dichlorodifluoromethane ND 125 128 102 125 137 110 7 42-167/19
95-50-1 1,2-Dichlorobenzene 0.60 J 125 108 86 125 109 87 1 82-124/14
541-73-1 1,3-Dichlorobenzene ND 125 111 89 125 109 87 2 84-125/14
106-46-7 1,4-Dichlorobenzene 0.51 J 125 111 88 125 107 85 4 78-120/15
75-34-3 1,1-Dichloroethane ND 125 121 97 125 121 97 0 81-122/15
107-06-2 1,2-Dichloroethane ND 125 116 93 125 114 91 2 75-125/14
75-35-4 1,1-Dichloroethylene ND 125 121 97 125 126 101 4 78-137/18
156-59-2 cis-1,2-Dichloroethylene ND 125 120 96 125 119 95 1 78-120/15
156-60-5 trans-1,2-Dichloroethylene ND 125 117 94 125 117 94 0 76-127/17
78-87-5 1,2-Dichloropropane ND 125 116 93 125 116 93 0 76-124/14
142-28-9 1,3-Dichloropropane ND 125 101 81 125 100 80 1 80-118/13
594-20-7 2,2-Dichloropropane ND 125 118 94 125 120 96 2 74-139/17
563-58-6 1,1-Dichloropropene ND 125 119 95 125 125 100 5 79-131/16
10061-01-5 cis-1,3-Dichloropropene ND 125 112 90 125 114 91 2 75-118/23
10061-02-6 trans-1,3-Dichloropropene ND 125 114 91 125 113 90 1 80-120/22
108-20-3 Di-Isopropyl Ether ND 125 106 85 125 108 86 2 68-123/16
64-17-5 Ethyl Alcohol ND 2500 2090 84 2500 2290 92 9 46-145/30
100-41-4 Ethylbenzene ND 125 112 90 125 111 89 1 81-121/14
* = Outside of Control Limits.
140 of 189
FA6883655.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68595-11MS C0136292.D 5 10/12/19 AB n/a n/a VC5431
FA68595-11MSD C0136293.D 5 10/12/19 AB n/a n/a VC5431
FA68595-11 a C0136282.D 1 10/12/19 AB n/a n/a VC5431
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-13, FA68836-15, FA68836-17, FA68836-19
FA68595-11 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 625 474 76 625 499 80 5 61-129/18
98-82-8 Isopropylbenzene ND 125 119 95 125 117 94 2 83-132/15
99-87-6 p-Isopropyltoluene ND 125 114 91 125 110 88 4 79-130/16
74-83-9 Methyl Bromide ND 125 91.3 73 125 111 89 19 59-143/19
74-87-3 Methyl Chloride ND 125 98.8 79 125 108 86 9 50-159/19
75-09-2 Methylene Chloride ND 125 89.7 72 125 91.6 73 2 69-135/16
108-10-1 4-Methyl-2-pentanone (MIBK)ND 625 501 80 625 508 81 1 66-122/16
1634-04-4 Methyl Tert Butyl Ether 4.2 125 113 87 125 115 89 2 72-117/14
91-20-3 Naphthalene ND 125 102 82 125 105 84 3 63-132/25
103-65-1 n-Propylbenzene ND 125 112 90 125 109 87 3 82-133/15
100-42-5 Styrene ND 125 111 89 125 107 86 4 78-119/23
630-20-6 1,1,1,2-Tetrachloroethane ND 125 118 94 125 120 96 2 77-122/19
79-34-5 1,1,2,2-Tetrachloroethane ND 125 105 84 125 104 83 1 72-120/14
127-18-4 Tetrachloroethylene ND 125 117 94 125 115 92 2 76-135/16
108-88-3 Toluene ND 125 112 90 125 112 90 0 80-120/14
87-61-6 1,2,3-Trichlorobenzene ND 125 104 83 125 103 82 1 68-131/25
120-82-1 1,2,4-Trichlorobenzene ND 125 108 86 125 109 87 1 73-129/20
71-55-6 1,1,1-Trichloroethane ND 125 123 98 125 126 101 2 75-130/16
79-00-5 1,1,2-Trichloroethane ND 125 104 83 125 106 85 2 76-119/14
79-01-6 Trichloroethylene ND 125 115 92 125 117 94 2 81-126/15
75-69-4 Trichlorofluoromethane ND 125 135 108 125 143 114 6 71-156/21
96-18-4 1,2,3-Trichloropropane ND 125 101 81 125 102 82 1 77-120/16
95-63-6 1,2,4-Trimethylbenzene ND 125 107 86 125 106 85 1 79-120/18
108-67-8 1,3,5-Trimethylbenzene ND 125 111 89 125 110 88 1 79-120/19
108-05-4 Vinyl Acetate ND 625 534 85 625 556 89 4 43-154/14
75-01-4 Vinyl Chloride ND 125 118 94 125 133 106 12 69-159/18
m,p-Xylene ND 250 230 92 250 222 89 4 79-126/15
95-47-6 o-Xylene ND 125 113 90 125 111 89 2 80-127/14
1330-20-7 Xylene (total)ND 375 343 91 375 334 89 3 80-126/15
CAS No.Surrogate Recoveries MS MSD FA68595-11 Limits
1868-53-7 Dibromofluoromethane 102%103%102%83-118%
17060-07-0 1,2-Dichloroethane-D4 104%104%103%79-125%
2037-26-5 Toluene-D8 98%97%97%85-112%
* = Outside of Control Limits.
141 of 189
FA6883655.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68595-11MS C0136292.D 5 10/12/19 AB n/a n/a VC5431
FA68595-11MSD C0136293.D 5 10/12/19 AB n/a n/a VC5431
FA68595-11 a C0136282.D 1 10/12/19 AB n/a n/a VC5431
The QC reported here applies to the following samples:Method: SW846 8260D
FA68836-13, FA68836-15, FA68836-17, FA68836-19
CAS No.Surrogate Recoveries MS MSD FA68595-11 Limits
460-00-4 4-Bromofluorobenzene 99%98%101%83-118%
(a) Sample was not preserved to a pH < 2; reported results are considered minimum values.
* = Outside of Control Limits.
142 of 189
FA6883655.3.3
SGS North America Inc.
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
143 of 189
FA688366
Method Blank Summary Page 1 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77248-MB 9I006761.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7, FA68836-8, FA68836-14,
FA68836-16, FA68836-18
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 830 170 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 19 ug/kg
95-57-8 2-Chlorophenol ND 170 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 44 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 20 ug/kg
3&4-Methylphenol ND 170 27 ug/kg
88-75-5 2-Nitrophenol ND 170 18 ug/kg
100-02-7 4-Nitrophenol ND 830 170 ug/kg
87-86-5 Pentachlorophenol ND 830 170 ug/kg
108-95-2 Phenol ND 170 17 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 19 ug/kg
83-32-9 Acenaphthene ND 170 18 ug/kg
208-96-8 Acenaphthylene ND 170 17 ug/kg
120-12-7 Anthracene ND 170 19 ug/kg
56-55-3 Benzo(a)anthracene ND 170 17 ug/kg
50-32-8 Benzo(a)pyrene ND 170 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 18 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 22 ug/kg
100-51-6 Benzyl Alcohol ND 170 17 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
106-47-8 4-Chloroaniline ND 170 42 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 19 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 170 21 ug/kg
91-58-7 2-Chloronaphthalene ND 170 17 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 170 17 ug/kg
218-01-9 Chrysene ND 170 17 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 21 ug/kg
132-64-9 Dibenzofuran ND 170 17 ug/kg
95-50-1 1,2-Dichlorobenzene ND 170 17 ug/kg
541-73-1 1,3-Dichlorobenzene ND 170 18 ug/kg
144 of 189
FA6883666.1.1
Method Blank Summary Page 2 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77248-MB 9I006761.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7, FA68836-8, FA68836-14,
FA68836-16, FA68836-18
CAS No.Compound Result RL MDL Units Q
106-46-7 1,4-Dichlorobenzene ND 170 22 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 40 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg
122-66-7 1,2-Diphenylhydrazine ND 170 17 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 17 ug/kg
86-73-7 Fluorene ND 170 18 ug/kg
118-74-1 Hexachlorobenzene ND 170 17 ug/kg
87-68-3 Hexachlorobutadiene ND 170 17 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 20 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 20 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
90-12-0 1-Methylnaphthalene ND 170 17 ug/kg
91-57-6 2-Methylnaphthalene ND 170 17 ug/kg
91-20-3 Naphthalene ND 170 17 ug/kg
98-95-3 Nitrobenzene ND 170 17 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 17 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 18 ug/kg
85-01-8 Phenanthrene ND 170 17 ug/kg
129-00-0 Pyrene ND 170 19 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 170 20 ug/kg
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 72%40-102%
4165-62-2 Phenol-d5 76%41-100%
118-79-6 2,4,6-Tribromophenol 79%42-108%
4165-60-0 Nitrobenzene-d5 72%40-105%
321-60-8 2-Fluorobiphenyl 77%43-107%
1718-51-0 Terphenyl-d14 77%45-119%
145 of 189
FA6883666.1.1
Method Blank Summary Page 1 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77241-MB X067487.D 1 10/14/19 MV 10/12/19 OP77241 SX2779
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-13, FA68836-15, FA68836-17
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 50 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l
95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l
120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l
105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l
51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.0 0.56 ug/l
3&4-Methylphenol ND 5.0 0.98 ug/l
88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l
100-02-7 4-Nitrophenol ND 25 5.0 ug/l
87-86-5 Pentachlorophenol ND 25 5.0 ug/l
108-95-2 Phenol ND 5.0 0.50 ug/l
88-06-2 2,4,6-Trichlorophenol ND 5.0 0.75 ug/l
83-32-9 Acenaphthene ND 5.0 0.63 ug/l
208-96-8 Acenaphthylene ND 5.0 0.64 ug/l
120-12-7 Anthracene ND 5.0 0.80 ug/l
56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l
50-32-8 Benzo(a)pyrene ND 5.0 0.78 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.0 0.78 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l
100-51-6 Benzyl Alcohol ND 5.0 0.61 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.81 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l
91-58-7 2-Chloronaphthalene ND 5.0 0.50 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l
218-01-9 Chrysene ND 5.0 0.85 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l
132-64-9 Dibenzofuran ND 5.0 0.60 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 0.50 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 0.50 ug/l
146 of 189
FA6883666.1.2
Method Blank Summary Page 2 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77241-MB X067487.D 1 10/14/19 MV 10/12/19 OP77241 SX2779
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-13, FA68836-15, FA68836-17
CAS No.Compound Result RL MDL Units Q
106-46-7 1,4-Dichlorobenzene ND 5.0 0.50 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l
84-66-2 Diethyl Phthalate ND 5.0 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.0 1.0 ug/l
84-74-2 Di-n-butyl Phthalate ND 5.0 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.0 1.0 ug/l
122-66-7 1,2-Diphenylhydrazine ND 5.0 0.76 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l
206-44-0 Fluoranthene ND 5.0 0.55 ug/l
86-73-7 Fluorene ND 5.0 0.70 ug/l
118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l
77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l
67-72-1 Hexachloroethane ND 5.0 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l
78-59-1 Isophorone ND 5.0 0.78 ug/l
90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l
91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l
91-20-3 Naphthalene ND 5.0 0.50 ug/l
98-95-3 Nitrobenzene ND 5.0 0.93 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l
86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l
85-01-8 Phenanthrene ND 5.0 0.86 ug/l
129-00-0 Pyrene ND 5.0 0.68 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.1 ug/l
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 34%14-67%
4165-62-2 Phenol-d5 24%10-50%
118-79-6 2,4,6-Tribromophenol 89%33-118%
4165-60-0 Nitrobenzene-d5 72%42-108%
321-60-8 2-Fluorobiphenyl 80%40-106%
1718-51-0 Terphenyl-d14 82%39-121%
147 of 189
FA6883666.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77248-BS 9I006760.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7, FA68836-8, FA68836-14,
FA68836-16, FA68836-18
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
65-85-0 Benzoic Acid 3330 2580 77 36-118
59-50-7 4-Chloro-3-methyl Phenol 1670 1400 84 52-108
95-57-8 2-Chlorophenol 1670 1340 80 48-104
120-83-2 2,4-Dichlorophenol 1670 1450 87 51-105
105-67-9 2,4-Dimethylphenol 1670 1300 78 43-96
51-28-5 2,4-Dinitrophenol 3330 2530 76 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 3000 90 64-121
95-48-7 2-Methylphenol 1670 1190 71 46-107
3&4-Methylphenol 3330 2400 72 44-111
88-75-5 2-Nitrophenol 1670 1390 83 49-104
100-02-7 4-Nitrophenol 3330 2590 78 56-116
87-86-5 Pentachlorophenol 3330 2560 77 61-114
108-95-2 Phenol 1670 1310 79 45-110
88-06-2 2,4,6-Trichlorophenol 1670 1550 93 56-109
83-32-9 Acenaphthene 1670 1330 80 56-109
208-96-8 Acenaphthylene 1670 1420 85 56-106
120-12-7 Anthracene 1670 1310 79 61-110
56-55-3 Benzo(a)anthracene 1670 1470 88 66-111
50-32-8 Benzo(a)pyrene 1670 1340 80 59-104
205-99-2 Benzo(b)fluoranthene 1670 1440 86 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1370 82 67-113
207-08-9 Benzo(k)fluoranthene 1670 1420 85 67-114
100-51-6 Benzyl Alcohol 1670 1170 70 53-108
101-55-3 4-Bromophenyl phenyl ether 1670 1520 91 62-110
85-68-7 Butyl benzyl phthalate 1670 1490 89 65-113
106-47-8 4-Chloroaniline 1670 1130 68 30-115
111-91-1 bis(2-Chloroethoxy)methane 1670 1430 86 48-105
111-44-4 bis(2-Chloroethyl)ether 1670 1220 73 46-103
108-60-1 2,2'-Oxybis(1-chloropropane)1670 1160 70 40-110
91-58-7 2-Chloronaphthalene 1670 1360 82 53-106
7005-72-3 4-Chlorophenyl phenyl ether 1670 1450 87 58-106
218-01-9 Chrysene 1670 1460 88 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1380 83 68-115
132-64-9 Dibenzofuran 1670 1400 84 57-108
95-50-1 1,2-Dichlorobenzene 1670 1190 71 44-102
541-73-1 1,3-Dichlorobenzene 1670 1160 70 42-100
* = Outside of Control Limits.
148 of 189
FA6883666.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77248-BS 9I006760.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7, FA68836-8, FA68836-14,
FA68836-16, FA68836-18
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
106-46-7 1,4-Dichlorobenzene 1670 1170 70 40-106
91-94-1 3,3'-Dichlorobenzidine 1670 1280 77 36-114
84-66-2 Diethyl Phthalate 1670 1430 86 61-109
131-11-3 Dimethyl Phthalate 1670 1430 86 59-108
117-84-0 Di-n-octyl Phthalate 1670 1500 90 64-119
84-74-2 Di-n-butyl Phthalate 1670 1390 83 63-108
122-66-7 1,2-Diphenylhydrazine 1670 1420 85 58-112
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1510 91 64-115
206-44-0 Fluoranthene 1670 1320 79 60-108
86-73-7 Fluorene 1670 1380 83 58-109
118-74-1 Hexachlorobenzene 1670 1380 83 59-111
87-68-3 Hexachlorobutadiene 1670 1240 74 41-108
77-47-4 Hexachlorocyclopentadiene 1670 1220 73 49-110
67-72-1 Hexachloroethane 1670 1160 70 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1350 81 66-116
78-59-1 Isophorone 1670 1210 73 42-89
90-12-0 1-Methylnaphthalene 1670 1250 75 49-106
91-57-6 2-Methylnaphthalene 1670 1170 70 47-106
91-20-3 Naphthalene 1670 1250 75 44-104
98-95-3 Nitrobenzene 1670 1270 76 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 1190 71 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1370 82 62-110
85-01-8 Phenanthrene 1670 1330 80 63-111
129-00-0 Pyrene 1670 1460 88 65-115
120-82-1 1,2,4-Trichlorobenzene 1670 1270 76 45-100
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 72%40-102%
4165-62-2 Phenol-d5 77%41-100%
118-79-6 2,4,6-Tribromophenol 81%42-108%
4165-60-0 Nitrobenzene-d5 72%40-105%
321-60-8 2-Fluorobiphenyl 77%43-107%
1718-51-0 Terphenyl-d14 77%45-119%
* = Outside of Control Limits.
149 of 189
FA6883666.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77241-BS X067486.D 1 10/14/19 MV 10/12/19 OP77241 SX2779
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-13, FA68836-15, FA68836-17
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
65-85-0 Benzoic Acid 100 22.3 22 10-69
59-50-7 4-Chloro-3-methyl Phenol 50 38.7 77 54-103
95-57-8 2-Chlorophenol 50 35.3 71 52-98
120-83-2 2,4-Dichlorophenol 50 42.6 85 53-103
105-67-9 2,4-Dimethylphenol 50 37.0 74 43-90
51-28-5 2,4-Dinitrophenol 100 67.5 68 44-112
534-52-1 4,6-Dinitro-o-cresol 100 86.3 86 66-121
95-48-7 2-Methylphenol 50 28.0 56 43-90
3&4-Methylphenol 100 49.9 50 36-88
88-75-5 2-Nitrophenol 50 44.6 89 53-102
100-02-7 4-Nitrophenol 100 31.1 31 18-62
87-86-5 Pentachlorophenol 100 80.0 80 61-115
108-95-2 Phenol 50 12.7 25 19-56
88-06-2 2,4,6-Trichlorophenol 50 48.1 96 59-107
83-32-9 Acenaphthene 50 42.6 85 61-107
208-96-8 Acenaphthylene 50 44.4 89 60-104
120-12-7 Anthracene 50 41.9 84 65-108
56-55-3 Benzo(a)anthracene 50 46.4 93 66-111
50-32-8 Benzo(a)pyrene 50 44.6 89 62-107
205-99-2 Benzo(b)fluoranthene 50 46.9 94 65-114
191-24-2 Benzo(g,h,i)perylene 50 49.6 99 66-116
207-08-9 Benzo(k)fluoranthene 50 44.2 88 65-114
100-51-6 Benzyl Alcohol 50 27.3 55 46-94
101-55-3 4-Bromophenyl Phenyl Ether 50 48.3 97 65-109
85-68-7 Butyl Benzyl Phthalate 50 43.5 87 65-112
106-47-8 4-Chloroaniline 50 38.9 78 49-105
111-91-1 bis(2-Chloroethoxy)methane 50 40.9 82 51-102
111-44-4 bis(2-Chloroethyl)ether 50 38.2 76 53-100
108-60-1 2,2'-Oxybis(1-chloropropane)50 34.2 68 45-106
91-58-7 2-Chloronaphthalene 50 42.3 85 57-103
7005-72-3 4-Chlorophenyl Phenyl Ether 50 46.6 93 62-105
218-01-9 Chrysene 50 44.6 89 66-111
53-70-3 Dibenzo(a,h)anthracene 50 51.1 102 66-119
132-64-9 Dibenzofuran 50 43.4 87 61-106
95-50-1 1,2-Dichlorobenzene 50 39.8 80 48-97
541-73-1 1,3-Dichlorobenzene 50 40.6 81 45-95
* = Outside of Control Limits.
150 of 189
FA6883666.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77241-BS X067486.D 1 10/14/19 MV 10/12/19 OP77241 SX2779
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-13, FA68836-15, FA68836-17
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
106-46-7 1,4-Dichlorobenzene 50 39.9 80 45-98
91-94-1 3,3'-Dichlorobenzidine 50 47.4 95 46-117
84-66-2 Diethyl Phthalate 50 45.1 90 64-108
131-11-3 Dimethyl Phthalate 50 44.8 90 63-106
84-74-2 Di-n-butyl Phthalate 50 44.8 90 65-107
117-84-0 Di-n-octyl Phthalate 50 46.8 94 62-118
122-66-7 1,2-Diphenylhydrazine 50 36.2 72 61-110
117-81-7 bis(2-Ethylhexyl)phthalate 50 46.6 93 61-117
206-44-0 Fluoranthene 50 43.9 88 63-106
86-73-7 Fluorene 50 44.6 89 62-108
118-74-1 Hexachlorobenzene 50 46.3 93 63-108
87-68-3 Hexachlorobutadiene 50 40.9 82 42-102
77-47-4 Hexachlorocyclopentadiene 50 43.1 86 39-102
67-72-1 Hexachloroethane 50 39.0 78 42-100
193-39-5 Indeno(1,2,3-cd)pyrene 50 56.2 112 64-119
78-59-1 Isophorone 50 36.8 74 43-87
90-12-0 1-Methylnaphthalene 50 40.4 81 53-102
91-57-6 2-Methylnaphthalene 50 41.9 84 51-102
91-20-3 Naphthalene 50 40.5 81 47-100
98-95-3 Nitrobenzene 50 36.3 73 50-104
621-64-7 N-Nitrosodi-n-propylamine 50 36.1 72 52-104
86-30-6 N-Nitrosodiphenylamine 50 41.2 82 64-108
85-01-8 Phenanthrene 50 42.4 85 66-110
129-00-0 Pyrene 50 43.5 87 64-113
120-82-1 1,2,4-Trichlorobenzene 50 42.7 85 45-97
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 36%14-67%
4165-62-2 Phenol-d5 25%10-50%
118-79-6 2,4,6-Tribromophenol 90%33-118%
4165-60-0 Nitrobenzene-d5 71%42-108%
321-60-8 2-Fluorobiphenyl 80%40-106%
1718-51-0 Terphenyl-d14 78%39-121%
* = Outside of Control Limits.
151 of 189
FA6883666.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77248-MS 9I006765.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
OP77248-MSD 9I006766.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
FA68836-1 9I006764.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7, FA68836-8, FA68836-14,
FA68836-16, FA68836-18
FA68836-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
65-85-0 Benzoic Acid ND 3770 2820 75 3720 2640 71 7 36-118/41
59-50-7 4-Chloro-3-methyl Phenol ND 1880 1530 81 1860 1460 79 5 52-108/21
95-57-8 2-Chlorophenol ND 1880 1400 74 1860 1370 74 2 48-104/26
120-83-2 2,4-Dichlorophenol ND 1880 1570 83 1860 1490 80 5 51-105/27
105-67-9 2,4-Dimethylphenol ND 1880 1440 76 1860 1360 73 6 43-96/23
51-28-5 2,4-Dinitrophenol ND 3770 2770 74 3720 2630 71 5 40-119/32
534-52-1 4,6-Dinitro-o-cresol ND 3770 3360 89 3720 3200 86 5 64-121/29
95-48-7 2-Methylphenol ND 1880 1300 69 1860 1250 67 4 46-107/24
3&4-Methylphenol ND 3770 2570 68 3720 2490 67 3 44-111/24
88-75-5 2-Nitrophenol ND 1880 1460 78 1860 1400 75 4 49-104/27
100-02-7 4-Nitrophenol ND 3770 2930 78 3720 2800 75 5 56-116/23
87-86-5 Pentachlorophenol ND 3770 3110 83 3720 2950 79 5 61-114/23
108-95-2 Phenol ND 1880 1370 73 1860 1330 72 3 45-110/24
88-06-2 2,4,6-Trichlorophenol ND 1880 1680 89 1860 1610 87 4 56-109/25
83-32-9 Acenaphthene ND 1880 1470 78 1860 1370 74 7 56-109/23
208-96-8 Acenaphthylene ND 1880 1520 81 1860 1440 77 5 56-106/23
120-12-7 Anthracene ND 1880 1500 80 1860 1400 75 7 61-110/21
56-55-3 Benzo(a)anthracene ND 1880 1680 89 1860 1610 87 4 66-111/23
50-32-8 Benzo(a)pyrene ND 1880 1530 81 1860 1470 79 4 59-104/23
205-99-2 Benzo(b)fluoranthene ND 1880 1630 87 1860 1560 84 4 67-113/24
191-24-2 Benzo(g,h,i)perylene ND 1880 1510 80 1860 1460 79 3 67-113/21
207-08-9 Benzo(k)fluoranthene ND 1880 1580 84 1860 1520 82 4 67-114/22
100-51-6 Benzyl Alcohol ND 1880 1240 66 1860 1220 66 2 53-108/24
101-55-3 4-Bromophenyl phenyl ether ND 1880 1700 90 1860 1590 86 7 62-110/21
85-68-7 Butyl benzyl phthalate ND 1880 1660 88 1860 1600 86 4 65-113/20
106-47-8 4-Chloroaniline ND 1880 1210 64 1860 1180 63 3 30-115/30
111-91-1 bis(2-Chloroethoxy)methane ND 1880 1480 79 1860 1400 75 6 48-105/24
111-44-4 bis(2-Chloroethyl)ether ND 1880 1240 66 1860 1210 65 2 46-103/27
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1880 1170 62 1860 1150 62 2 40-110/25
91-58-7 2-Chloronaphthalene ND 1880 1470 78 1860 1400 75 5 53-106/23
7005-72-3 4-Chlorophenyl phenyl ether ND 1880 1600 85 1860 1480 80 8 58-106/21
218-01-9 Chrysene ND 1880 1620 86 1860 1600 86 1 65-112/25
53-70-3 Dibenzo(a,h)anthracene ND 1880 1510 80 1860 1480 80 2 68-115/23
132-64-9 Dibenzofuran ND 1880 1520 81 1860 1440 77 5 57-108/22
95-50-1 1,2-Dichlorobenzene ND 1880 1240 66 1860 1210 65 2 44-102/28
541-73-1 1,3-Dichlorobenzene ND 1880 1200 64 1860 1180 63 2 42-100/30
* = Outside of Control Limits.
152 of 189
FA6883666.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77248-MS 9I006765.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
OP77248-MSD 9I006766.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
FA68836-1 9I006764.D 1 10/15/19 MV 10/11/19 OP77248 S9I250
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7, FA68836-8, FA68836-14,
FA68836-16, FA68836-18
FA68836-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
106-46-7 1,4-Dichlorobenzene ND 1880 1200 64 1860 1180 63 2 40-106/29
91-94-1 3,3'-Dichlorobenzidine ND 1880 1440 76 1860 1460 79 1 36-114/28
84-66-2 Diethyl Phthalate ND 1880 1580 84 1860 1480 80 7 61-109/20
131-11-3 Dimethyl Phthalate ND 1880 1600 85 1860 1490 80 7 59-108/20
117-84-0 Di-n-octyl Phthalate ND 1880 1710 91 1860 1630 88 5 64-119/21
84-74-2 Di-n-butyl Phthalate ND 1880 1580 84 1860 1510 81 5 63-108/19
122-66-7 1,2-Diphenylhydrazine ND 1880 1580 84 1860 1480 80 7 58-112/22
117-81-7 bis(2-Ethylhexyl)phthalate 81.8 J 1880 1740 88 1860 1690 87 3 64-115/23
206-44-0 Fluoranthene ND 1880 1510 80 1860 1420 76 6 60-108/25
86-73-7 Fluorene ND 1880 1540 82 1860 1440 77 7 58-109/21
118-74-1 Hexachlorobenzene ND 1880 1580 84 1860 1490 80 6 59-111/21
87-68-3 Hexachlorobutadiene ND 1880 1300 69 1860 1240 67 5 41-108/27
77-47-4 Hexachlorocyclopentadiene ND 1880 1310 70 1860 1230 66 6 49-110/31
67-72-1 Hexachloroethane ND 1880 1170 62 1860 1150 62 2 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene ND 1880 1500 80 1860 1470 79 2 66-116/22
78-59-1 Isophorone ND 1880 1310 70 1860 1240 67 5 42-89/22
90-12-0 1-Methylnaphthalene ND 1880 1350 72 1860 1260 68 7 49-106/26
91-57-6 2-Methylnaphthalene ND 1880 1270 67 1860 1210 65 5 47-106/27
91-20-3 Naphthalene ND 1880 1320 70 1860 1260 68 5 44-104/27
98-95-3 Nitrobenzene ND 1880 1320 70 1860 1260 68 5 43-108/25
621-64-7 N-Nitrosodi-n-propylamine ND 1880 1260 67 1860 1210 65 4 48-108/27
86-30-6 N-Nitrosodiphenylamine ND 1880 1530 81 1860 1460 79 5 62-110/21
85-01-8 Phenanthrene ND 1880 1520 81 1860 1440 77 5 63-111/22
129-00-0 Pyrene ND 1880 1640 87 1860 1590 86 3 65-115/25
120-82-1 1,2,4-Trichlorobenzene ND 1880 1360 72 1860 1300 70 5 45-100/26
CAS No.Surrogate Recoveries MS MSD FA68836-1 Limits
367-12-4 2-Fluorophenol 66%66%64%40-102%
4165-62-2 Phenol-d5 71%70%67%41-100%
118-79-6 2,4,6-Tribromophenol 82%78%74%42-108%
4165-60-0 Nitrobenzene-d5 67%66%63%40-105%
321-60-8 2-Fluorobiphenyl 75%72%69%43-107%
1718-51-0 Terphenyl-d14 76%75%71%45-119%
* = Outside of Control Limits.
153 of 189
FA6883666.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77241-MS X067511.D 40 10/15/19 MV 10/12/19 OP77241 SX2779
OP77241-MSD X067512.D 40 10/15/19 MV 10/12/19 OP77241 SX2779
FA68860-1 a X067510.D 40 10/15/19 MV 10/12/19 OP77241 SX2779
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-13, FA68836-15, FA68836-17
FA68860-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
59-50-7 4-Chloro-3-methyl Phenol ND 100 114 114*100 118 118*3 54-103/23
95-57-8 2-Chlorophenol ND 100 64.0 64 100 71.7 72 11 52-98/25
120-83-2 2,4-Dichlorophenol ND 100 78.6 79 100 88.9 89 12 53-103/26
105-67-9 2,4-Dimethylphenol ND 100 96.1 96*100 99.3 99*3 43-90/27
95-48-7 2-Methylphenol 33.4 J 100 102 69 100 116 83 13 43-90/28
3&4-Methylphenol ND 200 96.5 48 200 106 53 9 36-88/28
88-75-5 2-Nitrophenol ND 100 78.2 78 100 80.5 81 3 53-102/29
88-06-2 2,4,6-Trichlorophenol ND 100 93.7 94 100 101 101 7 59-107/23
83-32-9 Acenaphthene ND 100 80.4 80 100 85.7 86 6 61-107/22
208-96-8 Acenaphthylene ND 100 86.1 86 100 89.2 89 4 60-104/22
120-12-7 Anthracene ND 100 79.5 80 100 85.2 85 7 65-108/20
56-55-3 Benzo(a)anthracene ND 100 95.1 95 100 101 101 6 66-111/22
50-32-8 Benzo(a)pyrene ND 100 77.3 77 100 85.2 85 10 62-107/23
205-99-2 Benzo(b)fluoranthene ND 100 81.7 82 100 92.3 92 12 65-114/23
191-24-2 Benzo(g,h,i)perylene ND 100 77.2 77 100 87.1 87 12 66-116/23
207-08-9 Benzo(k)fluoranthene ND 100 78.7 79 100 78.8 79 0 65-114/24
101-55-3 4-Bromophenyl Phenyl Ether ND 100 84.9 85 100 92.3 92 8 65-109/23
85-68-7 Butyl Benzyl Phthalate ND 100 101 101 100 108 108 7 65-112/24
106-47-8 4-Chloroaniline ND 100 66.6 67 100 70.0 70 5 49-105/27
111-91-1 bis(2-Chloroethoxy)methane ND 100 78.2 78 100 82.7 83 6 51-102/28
111-44-4 bis(2-Chloroethyl)ether ND 100 74.1 74 100 74.8 75 1 53-100/27
108-60-1 2,2'-Oxybis(1-chloropropane)ND 100 64.7 65 200*45-106/26
91-58-7 2-Chloronaphthalene ND 100 80.3 80 100 86.0 86 7 57-103/23
7005-72-3 4-Chlorophenyl Phenyl Ether ND 100 85.1 85 100 86.2 86 1 62-105/20
218-01-9 Chrysene ND 100 82.4 82 100 95.4 95 15 66-111/22
53-70-3 Dibenzo(a,h)anthracene ND 100 77.3 77 100 81.6 82 5 66-119/24
132-64-9 Dibenzofuran ND 100 82.8 83 100 83.3 83 1 61-106/21
95-50-1 1,2-Dichlorobenzene ND 100 67.6 68 100 75.2 75 11 48-97/24
541-73-1 1,3-Dichlorobenzene ND 100 73.0 73 100 77.8 78 6 45-95/25
106-46-7 1,4-Dichlorobenzene ND 100 69.2 69 100 69.9 70 1 45-98/25
84-66-2 Diethyl Phthalate ND 100 83.5 84 100 90.7 91 8 64-108/21
131-11-3 Dimethyl Phthalate ND 100 82.8 83 100 88.9 89 7 63-106/22
84-74-2 Di-n-butyl Phthalate ND 100 91.7 92 100 95.6 96 4 65-107/21
117-84-0 Di-n-octyl Phthalate ND 100 104 104 100 113 113 8 62-118/24
122-66-7 1,2-Diphenylhydrazine ND 100 68.5 69 100 70.4 70 3 61-110/24
117-81-7 bis(2-Ethylhexyl)phthalate ND 100 89.1 89 100 97.3 97 9 61-117/23
* = Outside of Control Limits.
154 of 189
FA6883666.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77241-MS X067511.D 40 10/15/19 MV 10/12/19 OP77241 SX2779
OP77241-MSD X067512.D 40 10/15/19 MV 10/12/19 OP77241 SX2779
FA68860-1 a X067510.D 40 10/15/19 MV 10/12/19 OP77241 SX2779
The QC reported here applies to the following samples:Method: SW846 8270E
FA68836-13, FA68836-15, FA68836-17
FA68860-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
206-44-0 Fluoranthene ND 100 82.8 83 100 91.2 91 10 63-106/21
86-73-7 Fluorene ND 100 84.5 85 100 88.1 88 4 62-108/20
118-74-1 Hexachlorobenzene ND 100 80.9 81 100 89.3 89 10 63-108/22
87-68-3 Hexachlorobutadiene ND 100 77.3 77 100 83.1 83 7 42-102/28
193-39-5 Indeno(1,2,3-cd)pyrene ND 100 83.8 84 100 96.5 97 14 64-119/24
78-59-1 Isophorone ND 100 68.0 68 100 69.2 69 2 43-87/25
90-12-0 1-Methylnaphthalene ND 100 93.5 94 100 104 104*11 53-102/27
91-57-6 2-Methylnaphthalene ND 100 115 115*100 119 119*3 51-102/26
91-20-3 Naphthalene ND 100 78.2 78 100 83.4 83 6 47-100/29
621-64-7 N-Nitrosodi-n-propylamine ND 100 70.1 70 100 71.9 72 3 52-104/25
86-30-6 N-Nitrosodiphenylamine ND 100 72.0 72 100 80.0 80 11 64-108/23
85-01-8 Phenanthrene ND 100 78.9 79 100 87.5 88 10 66-110/21
129-00-0 Pyrene ND 100 84.2 84 100 89.7 90 6 64-113/23
CAS No.Surrogate Recoveries MS MSD FA68860-1 Limits
367-12-4 2-Fluorophenol 0%* b 0%* b 14-67%
4165-62-2 Phenol-d5 0%* b 0%* b 10-50%
118-79-6 2,4,6-Tribromophenol 0%* b 0%* b 33-118%
4165-60-0 Nitrobenzene-d5 0%* b 0%* b 0%* b 42-108%
321-60-8 2-Fluorobiphenyl 0%* b 0%* b 0%* b 40-106%
1718-51-0 Terphenyl-d14 0%* b 0%* b 0%* b 39-121%
(a) Dilution required due to matrix interference.
(b) Outside control limits due to dilution.
* = Outside of Control Limits.
155 of 189
FA6883666.3.2
SGS North America Inc.
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
156 of 189
FA688367
Method Blank Summary Page 1 of 1
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77280-MB ST144717.D 1 10/15/19 WH 10/15/19 OP77280 GST3465
The QC reported here applies to the following samples:Method: SW846 8081B
FA68836-9, FA68836-10, FA68836-11, FA68836-12
CAS No.Compound Result RL MDL Units Q
309-00-2 Aldrin ND 1.7 0.53 ug/kg
319-84-6 alpha-BHC ND 1.7 0.53 ug/kg
319-85-7 beta-BHC ND 1.7 0.49 ug/kg
319-86-8 delta-BHC ND 1.7 0.47 ug/kg
58-89-9 gamma-BHC (Lindane)ND 1.7 0.50 ug/kg
5103-71-9 alpha-Chlordane ND 1.7 0.52 ug/kg
5103-74-2 gamma-Chlordane ND 1.7 0.48 ug/kg
60-57-1 Dieldrin ND 1.7 0.47 ug/kg
72-54-8 4,4'-DDD ND 3.3 0.46 ug/kg
72-55-9 4,4'-DDE ND 3.3 0.61 ug/kg
50-29-3 4,4'-DDT ND 3.3 0.51 ug/kg
72-20-8 Endrin ND 3.3 0.84 ug/kg
1031-07-8 Endosulfan sulfate ND 3.3 0.44 ug/kg
7421-93-4 Endrin aldehyde ND 3.3 0.39 ug/kg
53494-70-5 Endrin ketone ND 3.3 0.52 ug/kg
959-98-8 Endosulfan-I ND 1.7 0.38 ug/kg
33213-65-9 Endosulfan-II ND 1.7 0.39 ug/kg
76-44-8 Heptachlor ND 1.7 0.49 ug/kg
1024-57-3 Heptachlor epoxide ND 1.7 0.49 ug/kg
72-43-5 Methoxychlor ND 3.3 0.67 ug/kg
8001-35-2 Toxaphene ND 83 25 ug/kg
CAS No.Surrogate Recoveries Limits
877-09-8 Tetrachloro-m-xylene 120%50-122%
2051-24-3 Decachlorobiphenyl 99%50-133%
157 of 189
FA6883677.1.1
Method Blank Summary Page 1 of 1
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77244-MB ZZ33611.D 1 10/11/19 NJ 10/11/19 OP77244 GZZ1370
The QC reported here applies to the following samples:Method: SW846 8141B
FA68836-9, FA68836-10, FA68836-11, FA68836-12
CAS No.Compound Result RL MDL Units Q
35400-43-2 Bolstar ND 40 10 ug/kg
2921-88-2 Chlorpyrifos ND 40 10 ug/kg
56-72-4 Coumaphos ND 40 10 ug/kg
8065-48-3 Demeton ND 80 24 ug/kg
333-41-5 Diazinon ND 40 10 ug/kg
62-73-7 Dichlorvos ND 40 10 ug/kg
60-51-5 Dimethoate ND 40 11 ug/kg
298-04-4 Disulfoton ND 40 10 ug/kg
2104-64-5 EPN ND 40 10 ug/kg
13194-48-4 Ethoprop ND 40 10 ug/kg
56-38-2 Ethyl Parathion ND 40 10 ug/kg
115-90-2 Fensulfothion ND 80 13 ug/kg
55-38-9 Fenthion ND 40 10 ug/kg
121-75-5 Malathion ND 40 10 ug/kg
86-50-0 Methyl Azinphos (Guthion)ND 40 10 ug/kg
298-00-0 Methyl Parathion ND 40 10 ug/kg
150-50-5 Merphos ND 100 53 ug/kg
7786-34-7 Mevinphos ND 40 10 ug/kg
6923-22-4 Monocrotophos ND 100 30 ug/kg
300-76-5 Naled ND 40 10 ug/kg
298-02-2 Phorate ND 40 10 ug/kg
299-84-3 Ronnel ND 40 10 ug/kg
3689-24-5 Sulfotep ND 40 10 ug/kg
22248-79-9 Stirophos ND 40 10 ug/kg
107-49-3 TEPP ND 160 79 ug/kg
34643-46-4 Tokuthion ND 40 10 ug/kg
327-98-0 Trichloronate ND 40 10 ug/kg
CAS No.Surrogate Recoveries Limits
126-73-8 Tributyl phosphate 70%47-136%
158 of 189
FA6883677.1.2
Blank Spike Summary Page 1 of 1
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77280-BS ST144715.D 1 10/15/19 WH 10/15/19 OP77280 GST3465
The QC reported here applies to the following samples:Method: SW846 8081B
FA68836-9, FA68836-10, FA68836-11, FA68836-12
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
309-00-2 Aldrin 16.7 18.7 112 57-120
319-84-6 alpha-BHC 16.7 19.1 115 60-117
319-85-7 beta-BHC 16.7 17.3 104 57-125
319-86-8 delta-BHC 16.7 17.4 104 42-126
58-89-9 gamma-BHC (Lindane)16.7 19.3 116 60-123
5103-71-9 alpha-Chlordane 16.7 16.6 100 61-122
5103-74-2 gamma-Chlordane 16.7 16.9 101 63-122
60-57-1 Dieldrin 16.7 17.7 106 63-125
72-54-8 4,4'-DDD 16.7 16.1 97 55-135
72-55-9 4,4'-DDE 16.7 17.5 105 61-129
50-29-3 4,4'-DDT 16.7 18.6 112 60-136
72-20-8 Endrin 16.7 17.3 104 67-138
1031-07-8 Endosulfan sulfate 16.7 15.7 94 59-119
7421-93-4 Endrin aldehyde 16.7 14.8 89 37-110
53494-70-5 Endrin ketone 16.7 15.7 94 60-128
959-98-8 Endosulfan-I 16.7 16.8 101 62-122
33213-65-9 Endosulfan-II 16.7 15.9 95 62-122
76-44-8 Heptachlor 16.7 19.6 118 58-123
1024-57-3 Heptachlor epoxide 16.7 18.1 109 60-122
72-43-5 Methoxychlor 16.7 18.5 111 57-133
CAS No.Surrogate Recoveries BSP Limits
877-09-8 Tetrachloro-m-xylene 113%50-122%
2051-24-3 Decachlorobiphenyl 94%50-133%
* = Outside of Control Limits.
159 of 189
FA6883677.2.1
Blank Spike Summary Page 1 of 1
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77280-BS2 ST144716.D 1 10/15/19 WH 10/15/19 OP77280 GST3465
The QC reported here applies to the following samples:Method: SW846 8081B
FA68836-9, FA68836-10, FA68836-11, FA68836-12
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
8001-35-2 Toxaphene 167 254 152 48-155
CAS No.Surrogate Recoveries BSP Limits
877-09-8 Tetrachloro-m-xylene 122%50-122%
2051-24-3 Decachlorobiphenyl 97%50-133%
* = Outside of Control Limits.
160 of 189
FA6883677.2.2
Blank Spike Summary Page 1 of 1
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77244-BS ZZ33610.D 1 10/11/19 NJ 10/11/19 OP77244 GZZ1370
The QC reported here applies to the following samples:Method: SW846 8141B
FA68836-9, FA68836-10, FA68836-11, FA68836-12
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
35400-43-2 Bolstar 100 98.0 98 45-149
2921-88-2 Chlorpyrifos 100 117 117 49-146
56-72-4 Coumaphos 100 88.5 89 19-176
8065-48-3 Demeton 200 136 68 45-124
333-41-5 Diazinon 100 95.8 96 50-146
62-73-7 Dichlorvos 100 79.0 79 43-142
60-51-5 Dimethoate 100 109 109 21-127
298-04-4 Disulfoton 100 90.8 91 52-151
2104-64-5 EPN 100 108 108 43-146
13194-48-4 Ethoprop 100 88.5 89 50-137
56-38-2 Ethyl Parathion 100 135 135 49-135
115-90-2 Fensulfothion 100 97.9 98 21-155
55-38-9 Fenthion 100 95.5 96 50-148
121-75-5 Malathion 100 107 107 48-135
86-50-0 Methyl Azinphos (Guthion)100 97.4 97 26-145
298-00-0 Methyl Parathion 100 101 101 48-149
150-50-5 Merphos 300 108 36 10-135
7786-34-7 Mevinphos 100 93.2 93 42-133
6923-22-4 Monocrotophos 300 213 71 10-91
300-76-5 Naled 100 123 123*10-108
298-02-2 Phorate 100 56.5 57 47-149
299-84-3 Ronnel 100 99.1 99 50-148
3689-24-5 Sulfotep 100 53.3 53 42-154
22248-79-9 Stirophos 100 105 105 46-144
107-49-3 TEPP 300 303 101 10-112
34643-46-4 Tokuthion 100 95.0 95 43-151
327-98-0 Trichloronate 100 90.9 91 51-142
CAS No.Surrogate Recoveries BSP Limits
126-73-8 Tributyl phosphate 94%47-136%
* = Outside of Control Limits.
161 of 189
FA6883677.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77280-MS ST144719.D 1 10/15/19 WH 10/15/19 OP77280 GST3465
OP77280-MSD ST144720.D 1 10/15/19 WH 10/15/19 OP77280 GST3465
FA68836-9 ST144718.D 1 10/15/19 WH 10/15/19 OP77280 GST3465
The QC reported here applies to the following samples:Method: SW846 8081B
FA68836-9, FA68836-10, FA68836-11, FA68836-12
FA68836-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
309-00-2 Aldrin ND 17.9 22.3 124*17.8 20.3 114 9 57-120/28
319-84-6 alpha-BHC ND 17.9 24.9 139*17.8 22.1 124*12 60-117/24
319-85-7 beta-BHC ND 17.9 21.1 118 17.8 19.4 109 8 57-125/26
319-86-8 delta-BHC ND 17.9 21.0 117 17.8 19.4 109 8 42-126/24
58-89-9 gamma-BHC (Lindane)ND 17.9 23.8 133*17.8 21.2 119 12 60-123/29
5103-71-9 alpha-Chlordane ND 17.9 17.9 100 17.8 16.8 94 6 61-122/26
5103-74-2 gamma-Chlordane ND 17.9 18.1 101 17.8 17.0 95 6 63-122/28
60-57-1 Dieldrin ND 17.9 19.1 107 17.8 17.8 100 7 63-125/29
72-54-8 4,4'-DDD ND 17.9 16.7 93 17.8 16.2 91 3 55-135/31
72-55-9 4,4'-DDE ND 17.9 19.9 111 17.8 18.4 103 8 61-129/31
50-29-3 4,4'-DDT ND 17.9 23.4 131 17.8 21.8 122 7 60-136/39
72-20-8 Endrin ND 17.9 20.2 113 17.8 19.0 107 6 67-138/28
1031-07-8 Endosulfan sulfate ND 17.9 16.6 93 17.8 16.1 90 3 59-119/28
7421-93-4 Endrin aldehyde ND 17.9 13.8 77 17.8 13.8 78 0 37-110/25
53494-70-5 Endrin ketone ND 17.9 15.1 84 17.8 14.8 83 2 60-128/24
959-98-8 Endosulfan-I ND 17.9 18.2 102 17.8 17.0 95 7 62-122/29
33213-65-9 Endosulfan-II ND 17.9 15.9 89 17.8 15.5 87 3 62-122/31
76-44-8 Heptachlor ND 17.9 23.1 129*17.8 20.8 117 10 58-123/30
1024-57-3 Heptachlor epoxide ND 17.9 21.0 117 17.8 18.9 106 11 60-122/33
72-43-5 Methoxychlor ND 17.9 20.9 117 17.8 20.3 114 3 57-133/31
CAS No.Surrogate Recoveries MS MSD FA68836-9 Limits
877-09-8 Tetrachloro-m-xylene 123%*107%122%50-122%
2051-24-3 Decachlorobiphenyl 81%79%85%50-133%
* = Outside of Control Limits.
162 of 189
FA6883677.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA68836
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77244-MS ZZ33613.D 1 10/11/19 NJ 10/11/19 OP77244 GZZ1370
OP77244-MSD ZZ33614.D 1 10/11/19 NJ 10/11/19 OP77244 GZZ1370
FA68836-9 ZZ33612.D 1 10/11/19 NJ 10/11/19 OP77244 GZZ1370
The QC reported here applies to the following samples:Method: SW846 8141B
FA68836-9, FA68836-10, FA68836-11, FA68836-12
FA68836-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
35400-43-2 Bolstar ND 110 111 101 110 105 95 6 45-149/33
2921-88-2 Chlorpyrifos ND 110 136 123 110 128 116 6 49-146/30
56-72-4 Coumaphos ND 110 108 98 110 102 92 6 19-176/40
8065-48-3 Demeton ND 221 156 71 221 150 68 4 45-124/32
333-41-5 Diazinon ND 110 109 99 110 104 94 5 50-146/30
62-73-7 Dichlorvos ND 110 90.1 82 110 88.0 80 2 43-142/34
60-51-5 Dimethoate ND 110 85.7 78 110 90.8 82 6 21-127/39
298-04-4 Disulfoton ND 110 104 94 110 98.9 90 5 52-151/39
2104-64-5 EPN ND 110 117 106 110 110 100 6 43-146/37
13194-48-4 Ethoprop ND 110 107 97 110 99.3 90 7 50-137/31
56-38-2 Ethyl Parathion ND 110 151 137*110 140 127 8 49-135/32
115-90-2 Fensulfothion ND 110 102 92 110 91.3 83 11 21-155/37
55-38-9 Fenthion ND 110 111 101 110 104 94 7 50-148/31
121-75-5 Malathion ND 110 126 114 110 114 103 10 48-135/31
86-50-0 Methyl Azinphos (Guthion)ND 110 116 105 110 116 105 0 26-145/41
298-00-0 Methyl Parathion ND 110 117 106 110 105 95 11 48-149/32
150-50-5 Merphos ND 331 101 31 331 83.3 25 19 10-135/35
7786-34-7 Mevinphos ND 110 95.1 86 110 82.6 75 14 42-133/39
6923-22-4 Monocrotophos ND 331 199 60 331 181 55 9 10-91/20
300-76-5 Naled ND 110 144 130*110 103 93 33 10-108/40
298-02-2 Phorate ND 110 53.0 48 110 50.0 45*6 47-149/30
299-84-3 Ronnel ND 110 115 104 110 108 98 6 50-148/31
3689-24-5 Sulfotep ND 110 49.8 45 110 45.2 41*10 42-154/31
22248-79-9 Stirophos ND 110 124 112 110 116 105 7 46-144/34
107-49-3 TEPP ND 331 296 89 331 273 82 8 10-112/31
34643-46-4 Tokuthion ND 110 110 100 110 106 96 4 43-151/31
327-98-0 Trichloronate ND 110 111 101 110 103 93 7 51-142/31
CAS No.Surrogate Recoveries MS MSD FA68836-9 Limits
126-73-8 Tributyl phosphate 93%88%73%47-136%
* = Outside of Control Limits.
163 of 189
FA6883677.3.2
SGS North America Inc.
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Orlando, FL
Section 8
164 of 189
FA688368
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36236 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/10/19
MB
Metal RL IDL MDL raw final
Mercury 0.042 .0025 .0042 0.0079 <0.042
Associated samples MP36236: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
165 of 189
FA6883688.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36236 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/10/19 10/10/19
FA68729-1 QC FA68729-1 Spikelot QC
Metal Original DUP RPD Limits Original MS HGFLWS1 % Rec Limits
Mercury 0.013 0.014 7.4 0-20 0.013 0.29 0.276 100.5 80-120
Associated samples MP36236: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
166 of 189
FA6883688.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36236 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/10/19
FA68729-1 Spikelot MSD QC
Metal Original MSD HGFLWS1 % Rec RPD Limit
Mercury 0.013 0.33 0.303 104.7 12.9 20
Associated samples MP36236: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
167 of 189
FA6883688.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36236 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/10/19
BSP Spikelot QC
Metal Result HGFLWS1 % Rec Limits
Mercury 0.26 0.25 104.0 80-120
Associated samples MP36236: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
168 of 189
FA6883688.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36236 Methods: SW846 7471B
Matrix Type: SOLID Units: ug/l
Prep Date: 10/10/19
FA68729-1 QC
Metal Original SDL 1:5 %DIF Limits
Mercury 0.141 0.00 100.0(a) 0-10
Associated samples MP36236: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
169 of 189
FA6883688.1.4
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36237 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/10/19
MB
Metal RL IDL MDL raw final
Mercury 0.042 .0025 .0042 -0.0016 <0.042
Associated samples MP36237: FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14,
FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
170 of 189
FA6883688.2.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36237 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/10/19 10/10/19
FA68836-8 QC FA68836-8 Spikelot QC
Metal Original DUP RPD Limits Original MS HGFLWS1 % Rec Limits
Mercury 0.065 0.061 6.3 0-20 0.065 0.34 0.268 102.7 80-120
Associated samples MP36237: FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14,
FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
171 of 189
FA6883688.2.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36237 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/10/19
FA68836-8 Spikelot MSD QC
Metal Original MSD HGFLWS1 % Rec RPD Limit
Mercury 0.065 0.30 0.272 86.4 12.5 20
Associated samples MP36237: FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14,
FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
172 of 189
FA6883688.2.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36237 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/10/19
BSP Spikelot QC
Metal Result HGFLWS1 % Rec Limits
Mercury 0.26 0.25 104.0 80-120
Associated samples MP36237: FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14,
FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
173 of 189
FA6883688.2.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36237 Methods: SW846 7471B
Matrix Type: SOLID Units: ug/l
Prep Date: 10/10/19
FA68836-8 QC
Metal Original SDL 1:5 %DIF Limits
Mercury 0.703 0.487 30.7 (a) 0-10
Associated samples MP36237: FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14,
FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
174 of 189
FA6883688.2.4
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36244 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/11/19
MB
Metal RL IDL MDL raw final
Mercury 0.50 .03 .03 -0.018 <0.50
Associated samples MP36244: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
175 of 189
FA6883688.3.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36244 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/11/19 10/11/19
FA68612-2 QC FA68612-2 Spikelot QC
Metal Original DUP RPD Limits Original MS HGFLWS1 % Rec Limits
Mercury 0.0 0.0 NC 0-20 0.0 2.6 3 86.7 80-120
Associated samples MP36244: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
176 of 189
FA6883688.3.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36244 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/11/19
FA68612-2 Spikelot MSD QC
Metal Original MSD HGFLWS1 % Rec RPD Limit
Mercury 0.0 2.7 3 90.0 3.8 20
Associated samples MP36244: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
177 of 189
FA6883688.3.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36244 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/11/19
BSP Spikelot QC
Metal Result HGFLWS1 % Rec Limits
Mercury 2.9 3 96.7 80-120
Associated samples MP36244: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
178 of 189
FA6883688.3.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36244 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/11/19 10/11/19
FA68612-2 QC FA68612-2F QC
Metal Original SDL 1:5 %DIF Limits Original SDL 1:5 %DIF Limits
Mercury 0.00 0.00 NC 0-10 0.149 0.00 100.0(a) 0-10
Associated samples MP36244: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
179 of 189
FA6883688.3.4
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36254 Methods: SW846 6020B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/12/19
MB
Metal RL IDL MDL raw final
Aluminum 25 1.1 1.1
Antimony 0.25 .025 .025
Arsenic 0.25 .025 .025 0.0089 <0.25
Barium 0.25 .025 .025 0.0046 <0.25
Beryllium 0.25 .025 .027
Cadmium 0.25 .025 .025 -0.00019 <0.25
Calcium 25 1.8 1.8
Chromium 0.25 .025 .025 0.063 <0.25
Cobalt 0.25 .025 .025
Copper 0.25 .025 .025
Iron 25 2 2
Lead 0.25 .025 .025 0.0020 <0.25
Magnesium 25 1.3 1.3
Manganese 0.25 .025 .025
Molybdenum 0.25 .025 .025
Nickel 0.25 .025 .025
Potassium 25 1.6 1.6
Selenium 0.25 .028 .045 0.012 <0.25
Silver 0.25 .025 .025 0.0011 <0.25
Sodium 25 1.2 1.2
Strontium 0.25 .025 .025
Thallium 0.25 .025 .025
Tin 0.25 .025 .025
Titanium 0.25 .076 .076
Vanadium 0.25 .025 .025
Zinc 0.25 .073 .073
Associated samples MP36254: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7,
FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14, FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
180 of 189
FA6883688.4.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36254 Methods: SW846 6020B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/12/19 10/12/19
FA68836-1 QC FA68836-1 Spikelot QC
Metal Original DUP RPD Limits Original MS MPICPMS1 % Rec Limits
Aluminum
Antimony
Arsenic 18.6 19.1 (a) 2.7 0-20 18.6 40.5 22.4 97.7 80-120
Barium 14.9 16.5 (a) 10.2 0-20 14.9 36.0 22.4 94.1 80-120
Beryllium
Cadmium 0.0 0.0 (a) NC 0-20 0.0 21.3 22.4 95.0 80-120
Calcium
Chromium 15.2 14.6 (a) 4.0 0-20 15.2 38.1 22.4 102.1 80-120
Cobalt
Copper
Iron
Lead 7.1 8.2 (a) 14.4 0-20 7.1 29.0 22.4 97.7 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 2.0 2.1 (a) 4.9 0-20 2.0 20.7 22.4 83.4 80-120
Silver 0.0 0.0 (a) NC 0-20 0.0 10.1 11.2 90.1 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36254: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7,
FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14, FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) Sample dilution required due to difficult matrix.
_________________________________________________________________________________________________________
Page 1
181 of 189
FA6883688.4.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36254 Methods: SW846 6020B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/12/19
FA68836-1 Spikelot MSD QC
Metal Original MSD MPICPMS1 % Rec RPD Limit
Aluminum
Antimony
Arsenic 18.6 42.8 26.4 91.7 5.5 20
Barium 14.9 42.5 26.4 104.5 16.6 20
Beryllium
Cadmium 0.0 25.7 26.4 97.3 18.7 20
Calcium
Chromium 15.2 41.0 26.4 97.7 7.3 20
Cobalt
Copper
Iron
Lead 7.1 33.9 26.4 101.5 15.6 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 2.0 23.3 26.4 80.7 11.8 20
Silver 0.0 11.9 13.2 90.1 16.4 20
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36254: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7,
FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14, FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
182 of 189
FA6883688.4.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36254 Methods: SW846 6020B
Matrix Type: SOLID Units: mg/kg
Prep Date: 10/12/19
BSP Spikelot QC
Metal Result MPICPMS1 % Rec Limits
Aluminum
Antimony
Arsenic 27.1 25 108.4 80-120
Barium 25.8 25 103.2 80-120
Beryllium
Cadmium 26.9 25 107.6 80-120
Calcium
Chromium 28.1 25 112.4 80-120
Cobalt
Copper
Iron
Lead 26.7 25 106.8 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 25.3 25 101.2 80-120
Silver 12.8 12.5 102.4 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36254: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7,
FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14, FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
183 of 189
FA6883688.4.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36254 Methods: SW846 6020B
Matrix Type: SOLID Units: ug/l
Prep Date: 10/12/19
FA68836-1 QC
Metal Original SDL 20:100%DIF Limits
Aluminum
Antimony
Arsenic 350 314 10.1*(a) 0-10
Barium 280 235 16.0*(a) 0-10
Beryllium
Cadmium 0.00 0.00 NC 0-10
Calcium
Chromium 286 282 1.4 0-10
Cobalt
Copper
Iron
Lead 133 116 12.8*(a) 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 37.6 35.0 6.8 0-10
Silver 0.00 0.00 NC 0-10
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36254: FA68836-1, FA68836-2, FA68836-3, FA68836-4, FA68836-5, FA68836-6, FA68836-7,
FA68836-8, FA68836-9, FA68836-10, FA68836-11, FA68836-12, FA68836-14, FA68836-16, FA68836-18
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Serial dilution indicates possible matrix interference.
_________________________________________________________________________________________________________
Page 1
184 of 189
FA6883688.4.4
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36255 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/14/19
MB
Metal RL IDL MDL raw final
Aluminum 200 8.7 22
Antimony 2.0 .2 .2
Arsenic 2.0 .2 .21 0.12 <2.0
Barium 2.0 .2 .2 0.0022 <2.0
Beryllium 2.0 .2 .2
Cadmium 2.0 .2 .2 0.023 <2.0
Calcium 200 14 36
Chromium 2.0 .2 .2 0.49 <2.0
Cobalt 2.0 .2 .2
Copper 2.0 .2 .2
Iron 200 16 23
Lead 2.0 .2 .2 0.015 <2.0
Magnesium 200 10 19
Manganese 2.0 .2 .2
Molybdenum 2.0 .2 .39
Nickel 2.0 .2 .2
Potassium 200 13 75
Selenium 2.0 .22 .22 -0.013 <2.0
Silver 2.0 .2 .2 0.026 <2.0
Sodium 200 9.6 24
Strontium 2.0 .2 .2
Thallium 2.0 .2 .2
Tin 2.0 .2 .2
Titanium 2.0 .61 .88
Vanadium 2.0 .2 .24
Zinc 4.0 .58 1.7
Associated samples MP36255: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
185 of 189
FA6883688.5.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36255 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/14/19
FA68836-17 Spikelot QC
Metal Original MS MPICPMS1 % Rec Limits
Aluminum
Antimony
Arsenic 1.5 202 200 100.3 80-120
Barium 99.7 292 200 96.2 80-120
Beryllium
Cadmium 0.0 199 200 99.5 80-120
Calcium
Chromium 2.5 210 200 103.8 80-120
Cobalt
Copper
Iron
Lead 1.9 201 200 99.6 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 0.75 184 200 91.6 80-120
Silver 0.0 119 100 119.0 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36255: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
186 of 189
FA6883688.5.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36255 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/14/19 10/14/19
FA68836-17 Spikelot MSD QC FA68836-17 QC
Metal Original MSD MPICPMS1 % Rec RPD Limit Original DUP RPD Limits
Aluminum
Antimony
Arsenic 1.5 198 200 98.3 2.0 20 1.5 1.5 0.0 0-20
Barium 99.7 288 200 94.2 1.4 20 99.7 99.7 0.0 0-20
Beryllium
Cadmium 0.0 197 200 98.5 1.0 20 0.0 0.0 NC 0-20
Calcium
Chromium 2.5 208 200 102.8 1.0 20 2.5 2.6 3.9 0-20
Cobalt
Copper
Iron
Lead 1.9 199 200 98.6 1.0 20 1.9 2.0 5.1 0-20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 0.75 181 200 90.1 1.6 20 0.75 0.82 8.9 0-20
Silver 0.0 100 100 100.0 17.4 20 0.0 0.0 NC 0-20
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36255: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
187 of 189
FA6883688.5.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36255 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/14/19
BSP Spikelot QC
Metal Result MPICPMS1 % Rec Limits
Aluminum
Antimony
Arsenic 211 200 105.5 80-120
Barium 202 200 101.0 80-120
Beryllium
Cadmium 210 200 105.0 80-120
Calcium
Chromium 223 200 111.5 80-120
Cobalt
Copper
Iron
Lead 206 200 103.0 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 194 200 97.0 80-120
Silver 103 100 103.0 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36255: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
188 of 189
FA6883688.5.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA68836
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36255 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/14/19
FA68836-17 QC
Metal Original SDL 2:10 %DIF Limits
Aluminum
Antimony
Arsenic 1.49 1.79 20.4 (a) 0-10
Barium 99.7 114 14.0*(b) 0-10
Beryllium
Cadmium 0.00 0.00 NC 0-10
Calcium
Chromium 2.46 2.64 7.5 0-10
Cobalt
Copper
Iron
Lead 1.94 1.98 2.4 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 0.745 0.00 100.0(a) 0-10
Silver 0.00 0.00 NC 0-10
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36255: FA68836-13, FA68836-15, FA68836-17
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
(b) Serial dilution indicates possible matrix interference.
_________________________________________________________________________________________________________
Page 1
189 of 189
FA6883688.5.4
10/22/19
Technical Report for
Resolve Environmental
Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
SGS Job Number: FA68979
Sampling Date: 10/14/19
Report to:
Resolve Environmental
500 Devonport Dr
Matthews, NC 28104
[e-mail]
ATTN: Laura Minor
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 10/22/19
e-Hardcopy 2.0
Automated Report
72
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 72
FA68979
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA68979-1: MW-1 ........................................................................................................6
3.2: FA68979-2: MW-2 ........................................................................................................13
3.3: FA68979-3: MW-3 ........................................................................................................20
3.4: FA68979-4: DW-1 ........................................................................................................27
3.5: FA68979-5: DUP ..........................................................................................................34
3.6: FA68979-6: TRIP BLANK ...........................................................................................41
Section 4: Misc. Forms ............................................................................................................44
4.1: Chain of Custody ...........................................................................................................45
Section 5: MS Volatiles - QC Data Summaries .....................................................................47
5.1: Method Blank Summary ................................................................................................48
5.2: Blank Spike Summary ...................................................................................................51
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................54
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................57
6.1: Method Blank Summary ................................................................................................58
6.2: Blank Spike Summary ...................................................................................................60
Section 7: Metals Analysis - QC Data Summaries ................................................................62
7.1: Prep QC MP36268: Hg ..................................................................................................63
7.2: Prep QC MP36272: As,Ba,Cd,Cr,Pb,Se,Ag ..................................................................68 12345672 of 72
FA68979
SGS North America Inc.
Sample Summary
Resolve Environmental
Job No:FA68979
Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA68979-1 10/14/19 13:27 TK 10/15/19 AQ Ground Water MW-1
FA68979-2 10/14/19 13:49 TK 10/15/19 AQ Ground Water MW-2
FA68979-3 10/14/19 11:50 TK 10/15/19 AQ Ground Water MW-3
FA68979-4 10/14/19 13:00 TK 10/15/19 AQ Ground Water DW-1
FA68979-5 10/14/19 08:00 TK 10/15/19 AQ Ground Water DUP
FA68979-6 10/14/19 00:00 TK 10/15/19 AQ Trip Blank Water TRIP BLANK
3 of 72
FA689791
Summary of Hits Page 1 of 1
Job Number:FA68979
Account:Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Collected:10/14/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA68979-1 MW-1
Barium 31.7 2.0 ug/l SW846 6020B
Chromium 6.4 2.0 ug/l SW846 6020B
Selenium 2.1 2.0 ug/l SW846 6020B
FA68979-2 MW-2
cis-1,2-Dichloroethylene 0.44 J 1.0 0.28 ug/l SW846 8260D
Di-Isopropyl Ether 0.52 J 1.0 0.24 ug/l SW846 8260D
Methyl Tert Butyl Ether 3.1 1.0 0.23 ug/l SW846 8260D
Barium 12.2 2.0 ug/l SW846 6020B
FA68979-3 MW-3
1,2-Diphenylhydrazine a 0.83 J 4.7 0.72 ug/l SW846 8270E
Barium 15.6 2.0 ug/l SW846 6020B
Chromium 4.2 2.0 ug/l SW846 6020B
FA68979-4 DW-1
Methyl Tert Butyl Ether 0.70 J 1.0 0.23 ug/l SW846 8260D
bis(2-Ethylhexyl)phthalate a 1.1 J 4.7 0.94 ug/l SW846 8270E
Barium 10.8 2.0 ug/l SW846 6020B
FA68979-5 DUP
Barium 14.8 2.0 ug/l SW846 6020B
Chromium 4.4 2.0 ug/l SW846 6020B
FA68979-6 TRIP BLANK
No hits reported in this sample.
(a) Insufficient sample for re-extraction.
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FA689792
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 72
FA689793
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FA68979-1 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1A22301.D 1 10/19/19 12:18 CV n/a n/a V1A904
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA6897933.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FA68979-1 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide a ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%83-118%
17060-07-0 1,2-Dichloroethane-D4 96%79-125%
2037-26-5 Toluene-D8 100%85-112%
460-00-4 4-Bromofluorobenzene 100%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA6897933.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FA68979-1 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA6897933.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FA68979-1 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 9I006788.D 1 10/18/19 14:19 MV 10/17/19 14:00 OP77327 S9I251
Run #2
Initial Volume Final Volume
Run #1 1060 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 47 9.4 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.7 0.56 ug/l
95-57-8 2-Chlorophenol b ND 4.7 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.7 0.79 ug/l
105-67-9 2,4-Dimethylphenol ND 4.7 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.7 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.4 1.9 ug/l
95-48-7 2-Methylphenol b ND 4.7 0.53 ug/l
3&4-Methylphenol b ND 4.7 0.92 ug/l
88-75-5 2-Nitrophenol ND 4.7 0.80 ug/l
100-02-7 4-Nitrophenol ND 24 4.7 ug/l
87-86-5 Pentachlorophenol ND 24 4.7 ug/l
108-95-2 Phenol b ND 4.7 0.47 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.7 0.71 ug/l
83-32-9 Acenaphthene ND 4.7 0.59 ug/l
208-96-8 Acenaphthylene ND 4.7 0.60 ug/l
120-12-7 Anthracene ND 4.7 0.75 ug/l
56-55-3 Benzo(a)anthracene ND 4.7 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.7 0.74 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.7 0.73 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.7 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.7 0.81 ug/l
100-51-6 Benzyl Alcohol b ND 4.7 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.7 0.80 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.7 0.94 ug/l
106-47-8 4-Chloroaniline ND 4.7 0.59 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.7 0.76 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.7 0.69 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.7 0.71 ug/l
91-58-7 2-Chloronaphthalene ND 4.7 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.7 0.51 ug/l
218-01-9 Chrysene ND 4.7 0.80 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FA68979-1 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.7 0.76 ug/l
132-64-9 Dibenzofuran ND 4.7 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.7 0.47 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.7 0.47 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.7 0.47 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.7 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.7 0.94 ug/l
131-11-3 Dimethyl Phthalate ND 4.7 0.94 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.7 0.94 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.7 0.94 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.7 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.7 0.94 ug/l
206-44-0 Fluoranthene ND 4.7 0.52 ug/l
86-73-7 Fluorene ND 4.7 0.66 ug/l
118-74-1 Hexachlorobenzene ND 4.7 0.65 ug/l
87-68-3 Hexachlorobutadiene ND 4.7 0.47 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.7 1.7 ug/l
67-72-1 Hexachloroethane ND 4.7 1.5 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.7 0.67 ug/l
78-59-1 Isophorone ND 4.7 0.73 ug/l
90-12-0 1-Methylnaphthalene ND 4.7 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.7 0.57 ug/l
91-20-3 Naphthalene ND 4.7 0.47 ug/l
98-95-3 Nitrobenzene ND 4.7 0.88 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.7 0.63 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.7 0.76 ug/l
85-01-8 Phenanthrene ND 4.7 0.82 ug/l
129-00-0 Pyrene ND 4.7 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.7 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 27%14-67%
4165-62-2 Phenol-d5 17%10-50%
118-79-6 2,4,6-Tribromophenol 65%33-118%
4165-60-0 Nitrobenzene-d5 64%42-108%
321-60-8 2-Fluorobiphenyl 63%40-106%
1718-51-0 Terphenyl-d14 64%39-121%
(a) Insufficient sample for re-extraction.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FA68979-1 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 72
FA6897933.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FA68979-1 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Barium 31.7 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Cadmium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Chromium 6.4 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Lead <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Mercury <0.50 0.50 ug/l 1 10/16/19 10/16/19 JC SW846 7470A 1 SW846 7470A 3
Selenium 2.1 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Silver <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
(1) Instrument QC Batch: MA16259
(2) Instrument QC Batch: MA16267
(3) Prep QC Batch: MP36268
(4) Prep QC Batch: MP36272
RL = Reporting Limit
12 of 72
FA6897933.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-2
Lab Sample ID:FA68979-2 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1A22316.D 1 10/19/19 18:47 CV n/a n/a V1A904
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.44 1.0 0.28 ug/l J
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 72
FA6897933.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-2
Lab Sample ID:FA68979-2 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether 0.52 1.0 0.24 ug/l J
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide a ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.1 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 95%83-118%
17060-07-0 1,2-Dichloroethane-D4 96%79-125%
2037-26-5 Toluene-D8 101%85-112%
460-00-4 4-Bromofluorobenzene 98%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 72
FA6897933.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-2
Lab Sample ID:FA68979-2 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 72
FA6897933.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-2
Lab Sample ID:FA68979-2 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 9I006789.D 1 10/18/19 14:45 MV 10/17/19 14:00 OP77327 S9I251
Run #2
Initial Volume Final Volume
Run #1 1060 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 47 9.4 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.7 0.56 ug/l
95-57-8 2-Chlorophenol b ND 4.7 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.7 0.79 ug/l
105-67-9 2,4-Dimethylphenol ND 4.7 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.7 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.4 1.9 ug/l
95-48-7 2-Methylphenol b ND 4.7 0.53 ug/l
3&4-Methylphenol b ND 4.7 0.92 ug/l
88-75-5 2-Nitrophenol ND 4.7 0.80 ug/l
100-02-7 4-Nitrophenol ND 24 4.7 ug/l
87-86-5 Pentachlorophenol ND 24 4.7 ug/l
108-95-2 Phenol b ND 4.7 0.47 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.7 0.71 ug/l
83-32-9 Acenaphthene ND 4.7 0.59 ug/l
208-96-8 Acenaphthylene ND 4.7 0.60 ug/l
120-12-7 Anthracene ND 4.7 0.75 ug/l
56-55-3 Benzo(a)anthracene ND 4.7 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.7 0.74 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.7 0.73 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.7 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.7 0.81 ug/l
100-51-6 Benzyl Alcohol b ND 4.7 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.7 0.80 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.7 0.94 ug/l
106-47-8 4-Chloroaniline ND 4.7 0.59 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.7 0.76 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.7 0.69 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.7 0.71 ug/l
91-58-7 2-Chloronaphthalene ND 4.7 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.7 0.51 ug/l
218-01-9 Chrysene ND 4.7 0.80 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 72
FA6897933.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-2
Lab Sample ID:FA68979-2 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.7 0.76 ug/l
132-64-9 Dibenzofuran ND 4.7 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.7 0.47 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.7 0.47 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.7 0.47 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.7 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.7 0.94 ug/l
131-11-3 Dimethyl Phthalate ND 4.7 0.94 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.7 0.94 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.7 0.94 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.7 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.7 0.94 ug/l
206-44-0 Fluoranthene ND 4.7 0.52 ug/l
86-73-7 Fluorene ND 4.7 0.66 ug/l
118-74-1 Hexachlorobenzene ND 4.7 0.65 ug/l
87-68-3 Hexachlorobutadiene ND 4.7 0.47 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.7 1.7 ug/l
67-72-1 Hexachloroethane ND 4.7 1.5 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.7 0.67 ug/l
78-59-1 Isophorone ND 4.7 0.73 ug/l
90-12-0 1-Methylnaphthalene ND 4.7 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.7 0.57 ug/l
91-20-3 Naphthalene ND 4.7 0.47 ug/l
98-95-3 Nitrobenzene ND 4.7 0.88 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.7 0.63 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.7 0.76 ug/l
85-01-8 Phenanthrene ND 4.7 0.82 ug/l
129-00-0 Pyrene ND 4.7 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.7 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 28%14-67%
4165-62-2 Phenol-d5 18%10-50%
118-79-6 2,4,6-Tribromophenol 69%33-118%
4165-60-0 Nitrobenzene-d5 68%42-108%
321-60-8 2-Fluorobiphenyl 69%40-106%
1718-51-0 Terphenyl-d14 68%39-121%
(a) Insufficient sample for re-extraction.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 72
FA6897933.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-2
Lab Sample ID:FA68979-2 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 72
FA6897933.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:FA68979-2 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Barium 12.2 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Cadmium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Chromium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Lead <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Mercury <0.50 0.50 ug/l 1 10/16/19 10/16/19 JC SW846 7470A 1 SW846 7470A 3
Selenium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Silver <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
(1) Instrument QC Batch: MA16259
(2) Instrument QC Batch: MA16267
(3) Prep QC Batch: MP36268
(4) Prep QC Batch: MP36272
RL = Reporting Limit
19 of 72
FA6897933.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA68979-3 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1A22317.D 1 10/19/19 19:13 CV n/a n/a V1A904
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 72
FA6897933.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA68979-3 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide a ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%83-118%
17060-07-0 1,2-Dichloroethane-D4 98%79-125%
2037-26-5 Toluene-D8 100%85-112%
460-00-4 4-Bromofluorobenzene 98%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 72
FA6897933.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:FA68979-3 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 72
FA6897933.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA68979-3 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 9I006790.D 1 10/18/19 15:11 MV 10/17/19 14:00 OP77327 S9I251
Run #2
Initial Volume Final Volume
Run #1 1060 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 47 9.4 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.7 0.56 ug/l
95-57-8 2-Chlorophenol b ND 4.7 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.7 0.79 ug/l
105-67-9 2,4-Dimethylphenol ND 4.7 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.7 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.4 1.9 ug/l
95-48-7 2-Methylphenol b ND 4.7 0.53 ug/l
3&4-Methylphenol b ND 4.7 0.92 ug/l
88-75-5 2-Nitrophenol ND 4.7 0.80 ug/l
100-02-7 4-Nitrophenol ND 24 4.7 ug/l
87-86-5 Pentachlorophenol ND 24 4.7 ug/l
108-95-2 Phenol b ND 4.7 0.47 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.7 0.71 ug/l
83-32-9 Acenaphthene ND 4.7 0.59 ug/l
208-96-8 Acenaphthylene ND 4.7 0.60 ug/l
120-12-7 Anthracene ND 4.7 0.75 ug/l
56-55-3 Benzo(a)anthracene ND 4.7 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.7 0.74 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.7 0.73 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.7 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.7 0.81 ug/l
100-51-6 Benzyl Alcohol b ND 4.7 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.7 0.80 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.7 0.94 ug/l
106-47-8 4-Chloroaniline ND 4.7 0.59 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.7 0.76 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.7 0.69 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.7 0.71 ug/l
91-58-7 2-Chloronaphthalene ND 4.7 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.7 0.51 ug/l
218-01-9 Chrysene ND 4.7 0.80 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 72
FA6897933.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA68979-3 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.7 0.76 ug/l
132-64-9 Dibenzofuran ND 4.7 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.7 0.47 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.7 0.47 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.7 0.47 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.7 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.7 0.94 ug/l
131-11-3 Dimethyl Phthalate ND 4.7 0.94 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.7 0.94 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.7 0.94 ug/l
122-66-7 1,2-Diphenylhydrazine 0.83 4.7 0.72 ug/l J
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.7 0.94 ug/l
206-44-0 Fluoranthene ND 4.7 0.52 ug/l
86-73-7 Fluorene ND 4.7 0.66 ug/l
118-74-1 Hexachlorobenzene ND 4.7 0.65 ug/l
87-68-3 Hexachlorobutadiene ND 4.7 0.47 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.7 1.7 ug/l
67-72-1 Hexachloroethane ND 4.7 1.5 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.7 0.67 ug/l
78-59-1 Isophorone ND 4.7 0.73 ug/l
90-12-0 1-Methylnaphthalene ND 4.7 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.7 0.57 ug/l
91-20-3 Naphthalene ND 4.7 0.47 ug/l
98-95-3 Nitrobenzene ND 4.7 0.88 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.7 0.63 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.7 0.76 ug/l
85-01-8 Phenanthrene ND 4.7 0.82 ug/l
129-00-0 Pyrene ND 4.7 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.7 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 19%14-67%
4165-62-2 Phenol-d5 12%10-50%
118-79-6 2,4,6-Tribromophenol 59%33-118%
4165-60-0 Nitrobenzene-d5 52%42-108%
321-60-8 2-Fluorobiphenyl 53%40-106%
1718-51-0 Terphenyl-d14 57%39-121%
(a) Insufficient sample for re-extraction.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 72
FA6897933.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:FA68979-3 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 72
FA6897933.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FA68979-3 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Barium 15.6 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Cadmium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Chromium 4.2 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Lead <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Mercury <0.50 0.50 ug/l 1 10/16/19 10/16/19 JC SW846 7470A 1 SW846 7470A 3
Selenium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Silver <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
(1) Instrument QC Batch: MA16259
(2) Instrument QC Batch: MA16267
(3) Prep QC Batch: MP36268
(4) Prep QC Batch: MP36272
RL = Reporting Limit
26 of 72
FA6897933.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:DW-1
Lab Sample ID:FA68979-4 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1A22318.D 1 10/19/19 19:39 CV n/a n/a V1A904
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 72
FA6897933.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:DW-1
Lab Sample ID:FA68979-4 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide a ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.70 1.0 0.23 ug/l J
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%83-118%
17060-07-0 1,2-Dichloroethane-D4 96%79-125%
2037-26-5 Toluene-D8 100%85-112%
460-00-4 4-Bromofluorobenzene 98%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 72
FA6897933.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:DW-1
Lab Sample ID:FA68979-4 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 72
FA6897933.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:DW-1
Lab Sample ID:FA68979-4 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 9I006791.D 1 10/18/19 15:38 MV 10/17/19 14:00 OP77327 S9I251
Run #2
Initial Volume Final Volume
Run #1 1060 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 47 9.4 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.7 0.56 ug/l
95-57-8 2-Chlorophenol b ND 4.7 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.7 0.79 ug/l
105-67-9 2,4-Dimethylphenol ND 4.7 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.7 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.4 1.9 ug/l
95-48-7 2-Methylphenol b ND 4.7 0.53 ug/l
3&4-Methylphenol b ND 4.7 0.92 ug/l
88-75-5 2-Nitrophenol ND 4.7 0.80 ug/l
100-02-7 4-Nitrophenol ND 24 4.7 ug/l
87-86-5 Pentachlorophenol ND 24 4.7 ug/l
108-95-2 Phenol b ND 4.7 0.47 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.7 0.71 ug/l
83-32-9 Acenaphthene ND 4.7 0.59 ug/l
208-96-8 Acenaphthylene ND 4.7 0.60 ug/l
120-12-7 Anthracene ND 4.7 0.75 ug/l
56-55-3 Benzo(a)anthracene ND 4.7 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.7 0.74 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.7 0.73 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.7 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.7 0.81 ug/l
100-51-6 Benzyl Alcohol b ND 4.7 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.7 0.80 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.7 0.94 ug/l
106-47-8 4-Chloroaniline ND 4.7 0.59 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.7 0.76 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.7 0.69 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.7 0.71 ug/l
91-58-7 2-Chloronaphthalene ND 4.7 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.7 0.51 ug/l
218-01-9 Chrysene ND 4.7 0.80 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 72
FA6897933.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:DW-1
Lab Sample ID:FA68979-4 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.7 0.76 ug/l
132-64-9 Dibenzofuran ND 4.7 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.7 0.47 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.7 0.47 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.7 0.47 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.7 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.7 0.94 ug/l
131-11-3 Dimethyl Phthalate ND 4.7 0.94 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.7 0.94 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.7 0.94 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.7 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate 1.1 4.7 0.94 ug/l J
206-44-0 Fluoranthene ND 4.7 0.52 ug/l
86-73-7 Fluorene ND 4.7 0.66 ug/l
118-74-1 Hexachlorobenzene ND 4.7 0.65 ug/l
87-68-3 Hexachlorobutadiene ND 4.7 0.47 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.7 1.7 ug/l
67-72-1 Hexachloroethane ND 4.7 1.5 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.7 0.67 ug/l
78-59-1 Isophorone ND 4.7 0.73 ug/l
90-12-0 1-Methylnaphthalene ND 4.7 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.7 0.57 ug/l
91-20-3 Naphthalene ND 4.7 0.47 ug/l
98-95-3 Nitrobenzene ND 4.7 0.88 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.7 0.63 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.7 0.76 ug/l
85-01-8 Phenanthrene ND 4.7 0.82 ug/l
129-00-0 Pyrene ND 4.7 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.7 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 16%14-67%
4165-62-2 Phenol-d5 11%10-50%
118-79-6 2,4,6-Tribromophenol 71%33-118%
4165-60-0 Nitrobenzene-d5 45%42-108%
321-60-8 2-Fluorobiphenyl 49%40-106%
1718-51-0 Terphenyl-d14 64%39-121%
(a) Insufficient sample for re-extraction.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 72
FA6897933.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:DW-1
Lab Sample ID:FA68979-4 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 72
FA6897933.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:DW-1
Lab Sample ID:FA68979-4 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Barium 10.8 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Cadmium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Chromium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Lead <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Mercury <0.50 0.50 ug/l 1 10/16/19 10/16/19 JC SW846 7470A 1 SW846 7470A 3
Selenium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Silver <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
(1) Instrument QC Batch: MA16259
(2) Instrument QC Batch: MA16267
(3) Prep QC Batch: MP36268
(4) Prep QC Batch: MP36272
RL = Reporting Limit
33 of 72
FA6897933.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:DUP
Lab Sample ID:FA68979-5 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1A22319.D 1 10/19/19 20:04 CV n/a n/a V1A904
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:DUP
Lab Sample ID:FA68979-5 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide a ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%83-118%
17060-07-0 1,2-Dichloroethane-D4 98%79-125%
2037-26-5 Toluene-D8 101%85-112%
460-00-4 4-Bromofluorobenzene 99%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:DUP
Lab Sample ID:FA68979-5 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:DUP
Lab Sample ID:FA68979-5 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 9I006792.D 1 10/18/19 16:04 MV 10/17/19 14:00 OP77327 S9I251
Run #2
Initial Volume Final Volume
Run #1 1060 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 47 9.4 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.7 0.56 ug/l
95-57-8 2-Chlorophenol b ND 4.7 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.7 0.79 ug/l
105-67-9 2,4-Dimethylphenol ND 4.7 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.7 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 9.4 1.9 ug/l
95-48-7 2-Methylphenol b ND 4.7 0.53 ug/l
3&4-Methylphenol b ND 4.7 0.92 ug/l
88-75-5 2-Nitrophenol ND 4.7 0.80 ug/l
100-02-7 4-Nitrophenol ND 24 4.7 ug/l
87-86-5 Pentachlorophenol ND 24 4.7 ug/l
108-95-2 Phenol b ND 4.7 0.47 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.7 0.71 ug/l
83-32-9 Acenaphthene ND 4.7 0.59 ug/l
208-96-8 Acenaphthylene ND 4.7 0.60 ug/l
120-12-7 Anthracene ND 4.7 0.75 ug/l
56-55-3 Benzo(a)anthracene ND 4.7 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.7 0.74 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.7 0.73 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.7 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.7 0.81 ug/l
100-51-6 Benzyl Alcohol b ND 4.7 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.7 0.80 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.7 0.94 ug/l
106-47-8 4-Chloroaniline ND 4.7 0.59 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.7 0.76 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.7 0.69 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.7 0.71 ug/l
91-58-7 2-Chloronaphthalene ND 4.7 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.7 0.51 ug/l
218-01-9 Chrysene ND 4.7 0.80 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:DUP
Lab Sample ID:FA68979-5 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.7 0.76 ug/l
132-64-9 Dibenzofuran ND 4.7 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.7 0.47 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.7 0.47 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.7 0.47 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.7 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.7 0.94 ug/l
131-11-3 Dimethyl Phthalate ND 4.7 0.94 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.7 0.94 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.7 0.94 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.7 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.7 0.94 ug/l
206-44-0 Fluoranthene ND 4.7 0.52 ug/l
86-73-7 Fluorene ND 4.7 0.66 ug/l
118-74-1 Hexachlorobenzene ND 4.7 0.65 ug/l
87-68-3 Hexachlorobutadiene ND 4.7 0.47 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.7 1.7 ug/l
67-72-1 Hexachloroethane ND 4.7 1.5 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.7 0.67 ug/l
78-59-1 Isophorone ND 4.7 0.73 ug/l
90-12-0 1-Methylnaphthalene ND 4.7 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.7 0.57 ug/l
91-20-3 Naphthalene ND 4.7 0.47 ug/l
98-95-3 Nitrobenzene ND 4.7 0.88 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.7 0.63 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.7 0.76 ug/l
85-01-8 Phenanthrene ND 4.7 0.82 ug/l
129-00-0 Pyrene ND 4.7 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.7 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 22%14-67%
4165-62-2 Phenol-d5 14%10-50%
118-79-6 2,4,6-Tribromophenol 59%33-118%
4165-60-0 Nitrobenzene-d5 57%42-108%
321-60-8 2-Fluorobiphenyl 57%40-106%
1718-51-0 Terphenyl-d14 52%39-121%
(a) Insufficient sample for re-extraction.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:DUP
Lab Sample ID:FA68979-5 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:DUP
Lab Sample ID:FA68979-5 Date Sampled:10/14/19
Matrix:AQ - Ground Water Date Received:10/15/19
Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Barium 14.8 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Cadmium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Chromium 4.4 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Lead <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Mercury <0.50 0.50 ug/l 1 10/16/19 10/16/19 JC SW846 7470A 1 SW846 7470A 3
Selenium <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
Silver <2.0 2.0 ug/l 2 10/17/19 10/21/19 DM SW846 6020B 2 SW846 3010A 4
(1) Instrument QC Batch: MA16259
(2) Instrument QC Batch: MA16267
(3) Prep QC Batch: MP36268
(4) Prep QC Batch: MP36272
RL = Reporting Limit
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Report of Analysis Page 1 of 3
Client Sample ID:TRIP BLANK
Lab Sample ID:FA68979-6 Date Sampled:10/14/19
Matrix:AQ - Trip Blank Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 1A22320.D 1 10/19/19 20:30 CV n/a n/a V1A904
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:TRIP BLANK
Lab Sample ID:FA68979-6 Date Sampled:10/14/19
Matrix:AQ - Trip Blank Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide b ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%83-118%
17060-07-0 1,2-Dichloroethane-D4 95%79-125%
2037-26-5 Toluene-D8 101%85-112%
460-00-4 4-Bromofluorobenzene 99%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:TRIP BLANK
Lab Sample ID:FA68979-6 Date Sampled:10/14/19
Matrix:AQ - Trip Blank Water Date Received:10/15/19
Method:SW846 8260D Percent Solids:n/a
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Sample vial(s) contained bubbles greater than 6mm.
(b) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
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FA689794
FA68979: Chain of Custody
Page 1 of 2
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FA6897944.1
Job Number:FA68979 Client:RESOLVE ENVIRONMENTAL
Date / Time Received:10/15/2019 10:00:00 AM Delivery Method:FX
Project:ELAN-INDIAN TRAIL
Airbill #'s:7761 5923 9725
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (0.4);
Cooler 1: (1.4);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:1; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:PETERH Date:Date:10/15/2019 10:00:00
FA68979: Chain of Custody
Page 2 of 2
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
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FA689795
Method Blank Summary Page 1 of 3
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V1A904-MB 1A22300.D 1 10/19/19 CV n/a n/a V1A904
The QC reported here applies to the following samples:Method: SW846 8260D
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5, FA68979-6
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
48 of 72
FA6897955.1.1
Method Blank Summary Page 2 of 3
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V1A904-MB 1A22300.D 1 10/19/19 CV n/a n/a V1A904
The QC reported here applies to the following samples:Method: SW846 8260D
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5, FA68979-6
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 96%83-118%
17060-07-0 1,2-Dichloroethane-D4 94%79-125%
2037-26-5 Toluene-D8 100%85-112%
49 of 72
FA6897955.1.1
Method Blank Summary Page 3 of 3
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V1A904-MB 1A22300.D 1 10/19/19 CV n/a n/a V1A904
The QC reported here applies to the following samples:Method: SW846 8260D
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5, FA68979-6
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 100%83-118%
50 of 72
FA6897955.1.1
Blank Spike Summary Page 1 of 3
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V1A904-BS 1A22299.D 1 10/19/19 CV n/a n/a V1A904
The QC reported here applies to the following samples:Method: SW846 8260D
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5, FA68979-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 125 113 90 50-147
71-43-2 Benzene 25 25.3 101 81-122
108-86-1 Bromobenzene 25 25.0 100 80-121
74-97-5 Bromochloromethane 25 25.0 100 76-123
75-27-4 Bromodichloromethane 25 24.6 98 79-123
75-25-2 Bromoform 25 23.8 95 66-123
78-93-3 2-Butanone (MEK)125 123 98 56-143
104-51-8 n-Butylbenzene 25 24.8 99 79-126
135-98-8 sec-Butylbenzene 25 24.8 99 83-133
98-06-6 tert-Butylbenzene 25 23.3 93 80-133
56-23-5 Carbon Tetrachloride 25 26.4 106 76-136
108-90-7 Chlorobenzene 25 25.1 100 82-124
75-00-3 Chloroethane 25 27.7 111 62-144
67-66-3 Chloroform 25 25.1 100 80-124
95-49-8 o-Chlorotoluene 25 23.8 95 81-127
106-43-4 p-Chlorotoluene 25 24.1 96 83-130
124-48-1 Dibromochloromethane 25 24.8 99 78-122
106-93-4 1,2-Dibromoethane 25 24.8 99 75-120
75-71-8 Dichlorodifluoromethane 25 22.3 89 42-167
95-50-1 1,2-Dichlorobenzene 25 24.8 99 82-124
541-73-1 1,3-Dichlorobenzene 25 25.5 102 84-125
106-46-7 1,4-Dichlorobenzene 25 24.8 99 78-120
75-34-3 1,1-Dichloroethane 25 25.7 103 81-122
107-06-2 1,2-Dichloroethane 25 24.8 99 75-125
75-35-4 1,1-Dichloroethylene 25 25.7 103 78-137
156-59-2 cis-1,2-Dichloroethylene 25 25.6 102 78-120
156-60-5 trans-1,2-Dichloroethylene 25 25.3 101 76-127
78-87-5 1,2-Dichloropropane 25 24.9 100 76-124
142-28-9 1,3-Dichloropropane 25 23.5 94 80-118
594-20-7 2,2-Dichloropropane 25 25.4 102 74-139
563-58-6 1,1-Dichloropropene 25 26.4 106 79-131
10061-01-5 cis-1,3-Dichloropropene 25 23.8 95 75-118
10061-02-6 trans-1,3-Dichloropropene 25 24.9 100 80-120
108-20-3 Di-Isopropyl Ether 25 23.6 94 68-123
64-17-5 Ethyl Alcohol 500 509 102 46-145
100-41-4 Ethylbenzene 25 24.9 100 81-121
* = Outside of Control Limits.
51 of 72
FA6897955.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V1A904-BS 1A22299.D 1 10/19/19 CV n/a n/a V1A904
The QC reported here applies to the following samples:Method: SW846 8260D
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5, FA68979-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 125 119 95 61-129
98-82-8 Isopropylbenzene 25 26.1 104 83-132
99-87-6 p-Isopropyltoluene 25 25.0 100 79-130
74-83-9 Methyl Bromide 25 32.3 129 59-143
74-87-3 Methyl Chloride 25 22.8 91 50-159
75-09-2 Methylene Chloride 25 21.5 86 69-135
108-10-1 4-Methyl-2-pentanone (MIBK)125 112 90 66-122
1634-04-4 Methyl Tert Butyl Ether 25 24.3 97 72-117
91-20-3 Naphthalene 25 21.8 87 63-132
103-65-1 n-Propylbenzene 25 24.1 96 82-133
100-42-5 Styrene 25 24.7 99 78-119
630-20-6 1,1,1,2-Tetrachloroethane 25 25.5 102 77-122
79-34-5 1,1,2,2-Tetrachloroethane 25 24.0 96 72-120
127-18-4 Tetrachloroethylene 25 26.8 107 76-135
108-88-3 Toluene 25 24.0 96 80-120
87-61-6 1,2,3-Trichlorobenzene 25 22.1 88 68-131
120-82-1 1,2,4-Trichlorobenzene 25 23.5 94 73-129
71-55-6 1,1,1-Trichloroethane 25 25.2 101 75-130
79-00-5 1,1,2-Trichloroethane 25 24.5 98 76-119
79-01-6 Trichloroethylene 25 25.2 101 81-126
75-69-4 Trichlorofluoromethane 25 26.8 107 71-156
96-18-4 1,2,3-Trichloropropane 25 23.4 94 77-120
95-63-6 1,2,4-Trimethylbenzene 25 22.9 92 79-120
108-67-8 1,3,5-Trimethylbenzene 25 24.0 96 79-120
108-05-4 Vinyl Acetate 125 128 102 43-154
75-01-4 Vinyl Chloride 25 25.1 100 69-159
m,p-Xylene 50 49.8 100 79-126
95-47-6 o-Xylene 25 23.8 95 80-127
1330-20-7 Xylene (total)75 73.6 98 80-126
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%83-118%
17060-07-0 1,2-Dichloroethane-D4 101%79-125%
2037-26-5 Toluene-D8 98%85-112%
* = Outside of Control Limits.
52 of 72
FA6897955.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V1A904-BS 1A22299.D 1 10/19/19 CV n/a n/a V1A904
The QC reported here applies to the following samples:Method: SW846 8260D
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5, FA68979-6
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 99%83-118%
* = Outside of Control Limits.
53 of 72
FA6897955.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68979-1MS 1A22321.D 5 10/19/19 CV n/a n/a V1A904
FA68979-1MSD 1A22322.D 5 10/19/19 CV n/a n/a V1A904
FA68979-1 1A22301.D 1 10/19/19 CV n/a n/a V1A904
The QC reported here applies to the following samples:Method: SW846 8260D
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5, FA68979-6
FA68979-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 625 534 85 625 552 88 3 50-147/21
71-43-2 Benzene ND 125 125 100 125 122 98 2 81-122/14
108-86-1 Bromobenzene ND 125 123 98 125 120 96 2 80-121/14
74-97-5 Bromochloromethane ND 125 119 95 125 120 96 1 76-123/14
75-27-4 Bromodichloromethane ND 125 117 94 125 116 93 1 79-123/19
75-25-2 Bromoform ND 125 108 86 125 111 89 3 66-123/21
78-93-3 2-Butanone (MEK)ND 625 550 88 625 574 92 4 56-143/18
104-51-8 n-Butylbenzene ND 125 114 91 125 111 89 3 79-126/16
135-98-8 sec-Butylbenzene ND 125 122 98 125 117 94 4 83-133/16
98-06-6 tert-Butylbenzene ND 125 114 91 125 110 88 4 80-133/16
56-23-5 Carbon Tetrachloride ND 125 127 102 125 125 100 2 76-136/23
108-90-7 Chlorobenzene ND 125 124 99 125 122 98 2 82-124/14
75-00-3 Chloroethane ND 125 142 114 125 138 110 3 62-144/20
67-66-3 Chloroform ND 125 124 99 125 122 98 2 80-124/15
95-49-8 o-Chlorotoluene ND 125 117 94 125 114 91 3 81-127/15
106-43-4 p-Chlorotoluene ND 125 116 93 125 113 90 3 83-130/15
124-48-1 Dibromochloromethane ND 125 115 92 125 117 94 2 78-122/19
106-93-4 1,2-Dibromoethane ND 125 117 94 125 118 94 1 75-120/13
75-71-8 Dichlorodifluoromethane ND 125 108 86 125 107 86 1 42-167/19
95-50-1 1,2-Dichlorobenzene ND 125 120 96 125 118 94 2 82-124/14
541-73-1 1,3-Dichlorobenzene ND 125 123 98 125 121 97 2 84-125/14
106-46-7 1,4-Dichlorobenzene ND 125 122 98 125 120 96 2 78-120/15
75-34-3 1,1-Dichloroethane ND 125 127 102 125 123 98 3 81-122/15
107-06-2 1,2-Dichloroethane ND 125 122 98 125 120 96 2 75-125/14
75-35-4 1,1-Dichloroethylene ND 125 123 98 125 121 97 2 78-137/18
156-59-2 cis-1,2-Dichloroethylene ND 125 124 99 125 122 98 2 78-120/15
156-60-5 trans-1,2-Dichloroethylene ND 125 121 97 125 119 95 2 76-127/17
78-87-5 1,2-Dichloropropane ND 125 121 97 125 119 95 2 76-124/14
142-28-9 1,3-Dichloropropane ND 125 113 90 125 113 90 0 80-118/13
594-20-7 2,2-Dichloropropane ND 125 107 86 125 104 83 3 74-139/17
563-58-6 1,1-Dichloropropene ND 125 128 102 125 123 98 4 79-131/16
10061-01-5 cis-1,3-Dichloropropene ND 125 107 86 125 105 84 2 75-118/23
10061-02-6 trans-1,3-Dichloropropene ND 125 113 90 125 113 90 0 80-120/22
108-20-3 Di-Isopropyl Ether ND 125 115 92 125 113 90 2 68-123/16
64-17-5 Ethyl Alcohol ND 2500 2440 98 2500 2350 94 4 46-145/30
100-41-4 Ethylbenzene ND 125 121 97 125 120 96 1 81-121/14
* = Outside of Control Limits.
54 of 72
FA6897955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68979-1MS 1A22321.D 5 10/19/19 CV n/a n/a V1A904
FA68979-1MSD 1A22322.D 5 10/19/19 CV n/a n/a V1A904
FA68979-1 1A22301.D 1 10/19/19 CV n/a n/a V1A904
The QC reported here applies to the following samples:Method: SW846 8260D
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5, FA68979-6
FA68979-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 625 527 84 625 574 92 9 61-129/18
98-82-8 Isopropylbenzene ND 125 128 102 125 125 100 2 83-132/15
99-87-6 p-Isopropyltoluene ND 125 121 97 125 118 94 3 79-130/16
74-83-9 Methyl Bromide ND 125 169 135 125 165 132 2 59-143/19
74-87-3 Methyl Chloride ND 125 109 87 125 112 90 3 50-159/19
75-09-2 Methylene Chloride ND 125 106 85 125 104 83 2 69-135/16
108-10-1 4-Methyl-2-pentanone (MIBK)ND 625 520 83 625 556 89 7 66-122/16
1634-04-4 Methyl Tert Butyl Ether ND 125 114 91 125 115 92 1 72-117/14
91-20-3 Naphthalene ND 125 92.9 74 125 98.3 79 6 63-132/25
103-65-1 n-Propylbenzene ND 125 118 94 125 114 91 3 82-133/15
100-42-5 Styrene ND 125 119 95 125 118 94 1 78-119/23
630-20-6 1,1,1,2-Tetrachloroethane ND 125 124 99 125 122 98 2 77-122/19
79-34-5 1,1,2,2-Tetrachloroethane ND 125 114 91 125 115 92 1 72-120/14
127-18-4 Tetrachloroethylene ND 125 127 102 125 126 101 1 76-135/16
108-88-3 Toluene ND 125 117 94 125 115 92 2 80-120/14
87-61-6 1,2,3-Trichlorobenzene ND 125 95.7 77 125 98.1 78 2 68-131/25
120-82-1 1,2,4-Trichlorobenzene ND 125 102 82 125 104 83 2 73-129/20
71-55-6 1,1,1-Trichloroethane ND 125 125 100 125 121 97 3 75-130/16
79-00-5 1,1,2-Trichloroethane ND 125 117 94 125 118 94 1 76-119/14
79-01-6 Trichloroethylene ND 125 123 98 125 120 96 2 81-126/15
75-69-4 Trichlorofluoromethane ND 125 133 106 125 130 104 2 71-156/21
96-18-4 1,2,3-Trichloropropane ND 125 113 90 125 115 92 2 77-120/16
95-63-6 1,2,4-Trimethylbenzene ND 125 112 90 125 109 87 3 79-120/18
108-67-8 1,3,5-Trimethylbenzene ND 125 118 94 125 114 91 3 79-120/19
108-05-4 Vinyl Acetate ND 625 583 93 625 588 94 1 43-154/14
75-01-4 Vinyl Chloride ND 125 123 98 125 121 97 2 69-159/18
m,p-Xylene ND 250 243 97 250 239 96 2 79-126/15
95-47-6 o-Xylene ND 125 116 93 125 115 92 1 80-127/14
1330-20-7 Xylene (total)ND 375 358 95 375 354 94 1 80-126/15
CAS No.Surrogate Recoveries MS MSD FA68979-1 Limits
1868-53-7 Dibromofluoromethane 101%101%96%83-118%
17060-07-0 1,2-Dichloroethane-D4 99%99%96%79-125%
2037-26-5 Toluene-D8 96%97%100%85-112%
* = Outside of Control Limits.
55 of 72
FA6897955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA68979-1MS 1A22321.D 5 10/19/19 CV n/a n/a V1A904
FA68979-1MSD 1A22322.D 5 10/19/19 CV n/a n/a V1A904
FA68979-1 1A22301.D 1 10/19/19 CV n/a n/a V1A904
The QC reported here applies to the following samples:Method: SW846 8260D
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5, FA68979-6
CAS No.Surrogate Recoveries MS MSD FA68979-1 Limits
460-00-4 4-Bromofluorobenzene 98%98%100%83-118%
* = Outside of Control Limits.
56 of 72
FA6897955.3.1
SGS North America Inc.
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
57 of 72
FA689796
Method Blank Summary Page 1 of 2
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77327-MB 9I006787.D 1 10/18/19 MV 10/17/19 OP77327 S9I251
The QC reported here applies to the following samples:Method: SW846 8270E
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 50 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l
95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l
120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l
105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l
51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.0 0.56 ug/l
3&4-Methylphenol ND 5.0 0.98 ug/l
88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l
100-02-7 4-Nitrophenol ND 25 5.0 ug/l
87-86-5 Pentachlorophenol ND 25 5.0 ug/l
108-95-2 Phenol ND 5.0 0.50 ug/l
88-06-2 2,4,6-Trichlorophenol ND 5.0 0.75 ug/l
83-32-9 Acenaphthene ND 5.0 0.63 ug/l
208-96-8 Acenaphthylene ND 5.0 0.64 ug/l
120-12-7 Anthracene ND 5.0 0.80 ug/l
56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l
50-32-8 Benzo(a)pyrene ND 5.0 0.78 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.0 0.78 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l
100-51-6 Benzyl Alcohol ND 5.0 0.61 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.81 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l
91-58-7 2-Chloronaphthalene ND 5.0 0.50 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l
218-01-9 Chrysene ND 5.0 0.85 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l
132-64-9 Dibenzofuran ND 5.0 0.60 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 0.50 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 0.50 ug/l
58 of 72
FA6897966.1.1
Method Blank Summary Page 2 of 2
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77327-MB 9I006787.D 1 10/18/19 MV 10/17/19 OP77327 S9I251
The QC reported here applies to the following samples:Method: SW846 8270E
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
CAS No.Compound Result RL MDL Units Q
106-46-7 1,4-Dichlorobenzene ND 5.0 0.50 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l
84-66-2 Diethyl Phthalate ND 5.0 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.0 1.0 ug/l
84-74-2 Di-n-butyl Phthalate ND 5.0 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.0 1.0 ug/l
122-66-7 1,2-Diphenylhydrazine ND 5.0 0.76 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l
206-44-0 Fluoranthene ND 5.0 0.55 ug/l
86-73-7 Fluorene ND 5.0 0.70 ug/l
118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l
77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l
67-72-1 Hexachloroethane ND 5.0 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l
78-59-1 Isophorone ND 5.0 0.78 ug/l
90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l
91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l
91-20-3 Naphthalene ND 5.0 0.50 ug/l
98-95-3 Nitrobenzene ND 5.0 0.93 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l
86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l
85-01-8 Phenanthrene ND 5.0 0.86 ug/l
129-00-0 Pyrene ND 5.0 0.68 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.1 ug/l
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 27%14-67%
4165-62-2 Phenol-d5 18%10-50%
118-79-6 2,4,6-Tribromophenol 65%33-118%
4165-60-0 Nitrobenzene-d5 63%42-108%
321-60-8 2-Fluorobiphenyl 63%40-106%
1718-51-0 Terphenyl-d14 67%39-121%
59 of 72
FA6897966.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77327-BS 9I006786.D 1 10/18/19 MV 10/17/19 OP77327 S9I251
The QC reported here applies to the following samples:Method: SW846 8270E
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
65-85-0 Benzoic Acid 100 16.7 17 10-69
59-50-7 4-Chloro-3-methyl Phenol 50 33.3 67 54-103
95-57-8 2-Chlorophenol 50 25.1 50*52-98
120-83-2 2,4-Dichlorophenol 50 31.2 62 53-103
105-67-9 2,4-Dimethylphenol 50 26.7 53 43-90
51-28-5 2,4-Dinitrophenol 100 71.1 71 44-112
534-52-1 4,6-Dinitro-o-cresol 100 81.9 82 66-121
95-48-7 2-Methylphenol 50 19.5 39*43-90
3&4-Methylphenol 100 34.8 35*36-88
88-75-5 2-Nitrophenol 50 30.5 61 53-102
100-02-7 4-Nitrophenol 100 23.1 23 18-62
87-86-5 Pentachlorophenol 100 70.0 70 61-115
108-95-2 Phenol 50 8.0 16*19-56
88-06-2 2,4,6-Trichlorophenol 50 35.8 72 59-107
83-32-9 Acenaphthene 50 32.2 64 61-107
208-96-8 Acenaphthylene 50 33.7 67 60-104
120-12-7 Anthracene 50 35.0 70 65-108
56-55-3 Benzo(a)anthracene 50 39.4 79 66-111
50-32-8 Benzo(a)pyrene 50 36.0 72 62-107
205-99-2 Benzo(b)fluoranthene 50 38.5 77 65-114
191-24-2 Benzo(g,h,i)perylene 50 37.4 75 66-116
207-08-9 Benzo(k)fluoranthene 50 36.3 73 65-114
100-51-6 Benzyl Alcohol 50 18.8 38*46-94
101-55-3 4-Bromophenyl Phenyl Ether 50 36.4 73 65-109
85-68-7 Butyl Benzyl Phthalate 50 38.6 77 65-112
106-47-8 4-Chloroaniline 50 28.6 57 49-105
111-91-1 bis(2-Chloroethoxy)methane 50 30.4 61 51-102
111-44-4 bis(2-Chloroethyl)ether 50 26.9 54 53-100
108-60-1 2,2'-Oxybis(1-chloropropane)50 26.1 52 45-106
91-58-7 2-Chloronaphthalene 50 30.2 60 57-103
7005-72-3 4-Chlorophenyl Phenyl Ether 50 36.6 73 62-105
218-01-9 Chrysene 50 39.5 79 66-111
53-70-3 Dibenzo(a,h)anthracene 50 36.8 74 66-119
132-64-9 Dibenzofuran 50 35.2 70 61-106
95-50-1 1,2-Dichlorobenzene 50 26.4 53 48-97
541-73-1 1,3-Dichlorobenzene 50 25.8 52 45-95
* = Outside of Control Limits.
60 of 72
FA6897966.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA68979
Account:RENCM Resolve Environmental
Project:Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP77327-BS 9I006786.D 1 10/18/19 MV 10/17/19 OP77327 S9I251
The QC reported here applies to the following samples:Method: SW846 8270E
FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
106-46-7 1,4-Dichlorobenzene 50 26.1 52 45-98
91-94-1 3,3'-Dichlorobenzidine 50 41.0 82 46-117
84-66-2 Diethyl Phthalate 50 39.6 79 64-108
131-11-3 Dimethyl Phthalate 50 38.2 76 63-106
84-74-2 Di-n-butyl Phthalate 50 37.9 76 65-107
117-84-0 Di-n-octyl Phthalate 50 38.3 77 62-118
122-66-7 1,2-Diphenylhydrazine 50 31.7 63 61-110
117-81-7 bis(2-Ethylhexyl)phthalate 50 39.6 79 61-117
206-44-0 Fluoranthene 50 36.4 73 63-106
86-73-7 Fluorene 50 35.8 72 62-108
118-74-1 Hexachlorobenzene 50 35.1 70 63-108
87-68-3 Hexachlorobutadiene 50 24.6 49 42-102
77-47-4 Hexachlorocyclopentadiene 50 23.0 46 39-102
67-72-1 Hexachloroethane 50 24.8 50 42-100
193-39-5 Indeno(1,2,3-cd)pyrene 50 37.0 74 64-119
78-59-1 Isophorone 50 28.2 56 43-87
90-12-0 1-Methylnaphthalene 50 28.9 58 53-102
91-57-6 2-Methylnaphthalene 50 30.3 61 51-102
91-20-3 Naphthalene 50 27.3 55 47-100
98-95-3 Nitrobenzene 50 27.9 56 50-104
621-64-7 N-Nitrosodi-n-propylamine 50 27.9 56 52-104
86-30-6 N-Nitrosodiphenylamine 50 34.7 69 64-108
85-01-8 Phenanthrene 50 35.6 71 66-110
129-00-0 Pyrene 50 37.3 75 64-113
120-82-1 1,2,4-Trichlorobenzene 50 27.2 54 45-97
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 23%14-67%
4165-62-2 Phenol-d5 15%10-50%
118-79-6 2,4,6-Tribromophenol 68%33-118%
4165-60-0 Nitrobenzene-d5 54%42-108%
321-60-8 2-Fluorobiphenyl 56%40-106%
1718-51-0 Terphenyl-d14 66%39-121%
* = Outside of Control Limits.
61 of 72
FA6897966.2.1
SGS North America Inc.
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Orlando, FL
Section 7
62 of 72
FA689797
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36268 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/16/19
MB
Metal RL IDL MDL raw final
Mercury 0.50 .03 .03 0.080 <0.50
Associated samples MP36268: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
63 of 72
FA6897977.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36268 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/16/19 10/16/19
FA68663-2 QC FA68663-2 Spikelot QC
Metal Original DUP RPD Limits Original MS HGFLWS1 % Rec Limits
Mercury 0.032 0.0 200.0(a) 0-20 0.032 2.9 3 95.6 80-120
Associated samples MP36268: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) RPD acceptable due to low duplicate and sample concentrations.
_________________________________________________________________________________________________________
Page 1
64 of 72
FA6897977.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36268 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/16/19
FA68663-2 Spikelot MSD QC
Metal Original MSD HGFLWS1 % Rec RPD Limit
Mercury 0.032 2.9 3 95.6 0.0 20
Associated samples MP36268: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
65 of 72
FA6897977.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36268 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/16/19
BSP Spikelot QC
Metal Result HGFLWS1 % Rec Limits
Mercury 3.2 3 106.7 80-120
Associated samples MP36268: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
66 of 72
FA6897977.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36268 Methods: SW846 7470A
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/16/19
FA68663-2 QC
Metal Original SDL 1:5 %DIF Limits
Mercury 0.0322 0.00 100.0(a) 0-10
Associated samples MP36268: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
67 of 72
FA6897977.1.4
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36272 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/17/19
MB
Metal RL IDL MDL raw final
Aluminum 200 8.7 22
Antimony 2.0 .2 .2
Arsenic 2.0 .2 .21 0.11 <2.0
Barium 2.0 .2 .2 0.13 <2.0
Beryllium 2.0 .2 .2
Cadmium 2.0 .2 .2 -0.0019 <2.0
Calcium 200 14 36
Chromium 2.0 .2 .2 0.78 <2.0
Cobalt 2.0 .2 .2
Copper 2.0 .2 .2
Iron 200 16 23
Lead 2.0 .2 .2 0.085 <2.0
Magnesium 200 10 19
Manganese 2.0 .2 .2
Molybdenum 2.0 .2 .39
Nickel 2.0 .2 .2
Potassium 200 13 75
Selenium 2.0 .22 .22 -0.074 <2.0
Silver 2.0 .2 .2 0.044 <2.0
Sodium 200 9.6 24
Strontium 2.0 .2 .2
Thallium 2.0 .2 .2
Tin 2.0 .2 .2
Titanium 2.0 .61 .88
Vanadium 2.0 .2 .24
Zinc 4.0 .58 1.7
Associated samples MP36272: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
68 of 72
FA6897977.2.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36272 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/17/19 10/17/19
FA68979-1 QC FA68979-1 Spikelot QC
Metal Original DUP RPD Limits Original MS MPICPMS1 % Rec Limits
Aluminum
Antimony
Arsenic 1.3 1.3 0.0 0-20 1.3 216 200 107.4 80-120
Barium 31.7 31.8 0.3 0-20 31.7 242 200 105.2 80-120
Beryllium
Cadmium 0.37 0.36 2.7 0-20 0.37 212 200 105.8 80-120
Calcium
Chromium 6.4 6.4 0.0 0-20 6.4 229 200 111.3 80-120
Cobalt
Copper
Iron
Lead 1.3 1.3 0.0 0-20 1.3 217 200 107.9 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 2.1 2.0 4.9 0-20 2.1 199 200 98.5 80-120
Silver 0.0 0.0 NC 0-20 0.0 104 100 104.0 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36272: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
69 of 72
FA6897977.2.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36272 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/17/19
FA68979-1 Spikelot MSD QC
Metal Original MSD MPICPMS1 % Rec RPD Limit
Aluminum
Antimony
Arsenic 1.3 223 200 110.9 3.2 20
Barium 31.7 252 200 110.2 4.0 20
Beryllium
Cadmium 0.37 222 200 110.8 4.6 20
Calcium
Chromium 6.4 239 200 116.3 4.3 20
Cobalt
Copper
Iron
Lead 1.3 227 200 112.9 4.5 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 2.1 209 200 103.5 4.9 20
Silver 0.0 110 100 110.0 5.6 20
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36272: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
70 of 72
FA6897977.2.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36272 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/17/19
BSP Spikelot QC
Metal Result MPICPMS1 % Rec Limits
Aluminum
Antimony
Arsenic 215 200 107.5 80-120
Barium 211 200 105.5 80-120
Beryllium
Cadmium 214 200 107.0 80-120
Calcium
Chromium 227 200 113.5 80-120
Cobalt
Copper
Iron
Lead 217 200 108.5 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 198 200 99.0 80-120
Silver 107 100 107.0 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36272: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
71 of 72
FA6897977.2.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA68979
Account: RENCM - Resolve Environmental
Project: Elan Indian Trail; Chestnut Pkwy & US Hwy 74, Indian Trail, NC
QC Batch ID: MP36272 Methods: SW846 6020B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 10/17/19
FA68979-1 QC
Metal Original SDL 2:10 %DIF Limits
Aluminum
Antimony
Arsenic 1.26 1.22 3.2 0-10
Barium 31.7 35.8 13.1*(a) 0-10
Beryllium
Cadmium 0.366 0.00 100.0(b) 0-10
Calcium
Chromium 6.38 7.20 12.8 (b) 0-10
Cobalt
Copper
Iron
Lead 1.33 1.68 26.4 (b) 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 2.12 1.38 34.9 (b) 0-10
Silver 0.00 0.00 NC 0-10
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP36272: FA68979-1, FA68979-2, FA68979-3, FA68979-4, FA68979-5
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Serial dilution indicates possible matrix interference.
(b) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
72 of 72
FA6897977.2.4

APPENDIX C

Brownfields Property Receptor Survey Form

North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:Elan Indian Trail
Address:US 74 East and Chestnut Parkway
City:Indian Trail
County:Union
Brownfields Project Number:23037-19-090
Property and Building Characteristics
a. Provide occupancy and use information.
Two unccupied structures are located on the property.
One building was previously used a residence and later used as a landscaping business office.
The other building is a small storge/building office.
Both buildings are single story wood structures. Each building has a wooden floor and a pitched,
shingled roof. Each building has a main doorway and typical housing windows; the larger building also
has a sliding glass door.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
Both buildings are elevated onto concrete blocks with no foundation, slab or footers.
Neither building has an operational HVAC system.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
No
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air
return, and design considerations (e.g. positive pressure?). NA
0%
0.4%
Current Usage Proposed Usage
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the
information requested below. Distances are measured from the site property boundary unless otherwise indicated
by the DEQ Brownfield’s Project Manager (PM).
32.4
95%
4.5%
0.1%
32.4
Surface Conditions
Size of Property (acres)
% of property that is wooded/brush
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets
as needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may
be needed.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings
(e.g. windows, bay doors), and height (number of stories).
% of property that is covered by buildings
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
Northesast
Southwest
N
Y 100 S
N
Utilities
Is there a septic system on-site? (Y or N) ___Y______
Please provide the utility providers for the subject property
a. Natural Gas Piedmont
b. Sewer
c. Electricity Duke Power
d. Water/Sewer
For surrounding properties, please complete the following table with available information.
Y 25 NW
Y 50 NE
Y 100 S
Y 10 N/E
Y 50 N
Y 10 N
N
Is there a residence within 1,000 ft of the Property?
Commercial (Taco Bell/Walgreens/Napa Auto)
For the subject property, please provide a map of known buried utilites. If available, include depth to top,
construction material, and diameter of the utilities. In addition, please provide the following information on utilty
providers. If additional assessment is required, the public utility locators should be contacted. This information can
then be added to a site map.
Y/N *
Is a school or daycare center within 1,000 ft of the
Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific
addresses.
Distance
(ft)
Union County
Union County
Please provide information on the following land uses in the vicinity of the subject site, including a map of the
surrounding areas. If specific receptors are present, please provide addresses of the facilities.
Chestnut Parkway and property being currently developed.
Indian Trail Road/Commercial/Bank/Wooded, Residences
Proposed Usage Current Use/Occupant
DirectionUtility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
Direction
Is there a basement within 1,000 ft of the Property
Distance
(ft)Address
Zoning/Land Use
108 Shady Bluff Rd
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with
the subject property.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
US 74/Commercial; (strip mall/restaurants)
Wooded/ Recreation Center
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public __X___ Private ______
N
N
N
Surface Water & Wetlands
Rocky/Sediment
Yes
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Are there any wetlands present on the
property? If no wetlands on-site, are wetlands
suspected on adjoining properties?
a. Is the water body naturally developed or
man-made?Natural
Animal Drinking Water
Natural Stream
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property
boundary?Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in
the vicinity of the Property.
Yes
Are there surface water features on the
property? (If yes, please complete a. to d.)
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public,
please include the water providers name.
Distance
(ft)Direction Address
Provide Information regarding Surface Water
and Wetlands
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a
minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if
water supply or irrigation wells may be present. Information from applicable databases can and should be utilized;
however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested
radius, please provide a map of the well locations. If needed, please attach a separate table to list all wells. Please
note, the PM may opt for a more extensive water supply well survey if needed.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
Rev. 09/2015 Page 3 of 3

APPENDIX D

Zoning Map – Indian Trail

GoMaps
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P,NRCan, Esri Japan, METI, Esri China (Hong Kong), Esri Korea,Esri (Thailand), NGCC, (c) OpenStreetMap contributors, and theGIS User Community
Parcels
CBD
NBD
GBD
RBD
L-I
H-I
EXP
I
CZ COM
CZ COM 09-003
CZ RES
CZ RES 09-001
RSF
SF-1
SF-2
SF-3
SF-4
SF-5
MFR
November 23, 2019 0 0.1 0.20.05 mi
0 0.15 0.30.075 km
1:6,971