Loading...
HomeMy WebLinkAbout22081_PE Valve_Phase I ESA_08.29.2019FORMER P.E. VALVE PROPERTY 1140 SWEETEN CREEK ROAD ASHEVILLE,BUNCOMBE COUNTY,NORTH CAROLINA 28803 ECS PROJECT NO.49:7572-A AUGUST 29, 2019 August 29, 2019 Mr. Peter Hall 63 Mountain View Drive Arden, North Carolina 28704 ECS Project No. 49: 7572-A Reference:Phase I Environmental Site Assessment Report,Former P.E.Valve Property,1140 Sweeten Creek Road, Asheville, Buncombe County, North Carolina 28803 Dear Mr. Hall: ECS Southeast,LLP (ECS)is pleased to provide you with the results of our Phase I Environmental Site Assessment (ESA)for the referenced site.ECS services were provided in general accordance with ECS Proposal No.49:14874-P authorized on July 11,2019 and generally meet the requirements of ASTM E1527-13,Standard Practice for Environmental Site Assessments:Phase I Environmental Site Assessment Process and EPA Standards and Practices for All Appropriate Inquiries contained in 40 CFR Part 312. If there are questions regarding this report,or a need for further information,please contact the undersigned. ECS Southeast, LLP Don Randall Marlor Justin Roth, CHMM Environmental Technician Environmental Principal jbevers@ecslimited.com jroth@ecslimited.com (828) 785-4183 (843) 284-7213 ECS Southeast, LLP 1900 Hendersonville Road,Suite 10,Asheville,North Carolina 28803 •T:828-665-2307 •F:828-665-8128 •ecslimited.com Project Summary Former P.E. Valve Property 1140 Sweeten Creek Road Asheville, North Carolina 28803 Report Section No Further Action REC CREC HREC BER Comment 4.0 User Provided Information  5.1 Federal ASTM Databases  Subject property is identified on the RCRIS database and was formerly utilized as an industrial manufacturing facility. 5.2 State ASTM Databases  5.3 Additional Environmental Record Sources  The subject property was identified on the Brownfields database. Prior reports indicate the subject property has been historically utilized as an industrial manufacturing facility and elevated concentrations of TCE and chromium have been identified on the subject property. 6.0 Historical Use Information  The historical use of the subject property as an industrial manufacturing facility. A Soil and Groundwater Assessment conducted by ECS identifying TCE in the groundwater at concentrations above regulations and VISLs and arsenic and hexavalent chromium in the soil at concentrations above PSRG standards. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-A Report Section No Further Action REC CREC HREC BER Comment 7.0 Site and Area Reconnaissance  8.0 Additional Services  9.0 Interviews  August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-A ENVIRONMENTAL PROFESSIONAL STATEMENT We declare that,to the best of our professional knowledge and belief,we meet the definition of Environmental Professional as defined in §312.10 of 40 CFR 312.We have the specific qualifications based on education,training,and experience to assess a property of the nature,history,and setting of the subject property.We have developed and performed the all appropriate inquiries in conformance with the standards and practices set forth in 40 CFR Part 312. Justin Roth, CHMM Environmental Principal August 29, 2019 August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-A PAGETABLE OF CONTENTS 1.0 EXECUTIVE SUMMARY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 2.0 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 2.1 Purpose and Reason for Performing Phase I ESA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 2.2 Scope of Services . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 2.3 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 2.4 Limitations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 2.5 Data Gaps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 2.6 Limiting Conditions/Deviations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 3.0 SUBJECT PROPERTY DESCRIPTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 3.1 Subject Property Location and Legal Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 3.2 Physical Setting and Hydrogeology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 3.3 Current Use and Description of the Site . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 4.0 USER PROVIDED INFORMATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 4.1 Title Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 4.2 Environmental Liens or Activity and Use Limitations . . . . . . . . . . . . . . . . . . . . . . . . . . 9 4.3 Specialized Knowledge . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 4.4 Commonly Known or Reasonably Ascertainable Information . . . . . . . . . . . . . . . . . . 9 4.5 Valuation Reduction for Environmental Issues . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 4.6 Owner, Property Manager, and Occupant Information . . . . . . . . . . . . . . . . . . . . . . . . 9 4.7 Degree of Obviousness . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10 5.0 RECORDS REVIEW . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 5.1 Federal ASTM Databases . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 5.1.1 Federal RCRIS - Generators . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 5.2 State ASTM Databases . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 5.2.1 State Hazardous Waste Sites (SHWS) Inventory . . . . . . . . . . . . . . . . . . . . . . 13 5.2.2 State LAST . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 5.2.3 Leaking Underground Storage Tank (LUST) List . . . . . . . . . . . . . . . . . . . . . . 13 5.2.4 Registered Underground Storage Tank (UST) List . . . . . . . . . . . . . . . . . . . . 14 5.3 Additional Environmental Record Sources . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 5.3.1 Additional Non-ASTM Federal Databases . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 5.3.1.1 US Brownfields . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-A 5.3.1.2 FINDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 5.3.2 Additional Non-ASTM State Databases . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 5.3.2.1 Leaking Underground Storage Tanks (LUST TRUST). . . . . . . . . . 16 5.3.2.2 Incident Management Database (IMD). . . . . . . . . . . . . . . . . . . . . . 16 5.3.3 Other Proprietary Databases . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 5.3.3.1 EDR Historical Auto Stations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 5.3.4 Unmapped (Orphan) Facilities and Sites . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 5.4 Regulatory Review Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 6.0 HISTORICAL USE INFORMATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 6.1 Aerial Photograph Review . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 6.2 Sanborn Fire Insurance Map Review . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20 6.3 Property Tax Files . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21 6.4 Recorded Land Title Records . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21 6.5 Historical USGS Topographic Maps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22 6.6 City Directory Review . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23 6.7 Building Department Records . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 6.8 Zoning/Land Use Records . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 6.9 Other Historical Sources . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 6.10 Previous Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 6.11 Historical Use Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 7.0 SITE AND AREA RECONNAISSANCE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28 7.1 Methodology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28 7.2 On-Site Features . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28 7.3 Adjoining and Nearby Properties . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29 7.4 Site and Area Reconnaissance Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30 8.0 ADDITIONAL SERVICES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31 9.0 INTERVIEWS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 10.0 FINDINGS AND CONCLUSIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33 11.0 REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36 August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-A TABLE OF APPENDICES Appendix I:Figures Appendix II:Correspondence and User Questionnaire Appendix III:Regulatory Records Documentation Appendix IV:Historical Research Documentation Appendix V:Site Photographs Appendix VI:Statement of Qualifications Appendix VII:Acronyms August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-A 1.0 EXECUTIVE SUMMARY ECS Southeast,LLP (ECS)was contracted by Mr.Peter Hall to perform an ASTM E1527-13,Phase I Environmental Site Assessment (ESA)of the Former P.E.Valve Property located at 1140 Sweeten Creek Road in Asheville,Buncombe County,North Carolina (i.e.subject property).This Executive Summary is an integral part of the Phase I ESA report.ECS recommends that the report be read in its entirety. The subject property is identified by the Buncombe County GIS website as Parcel Identification Number (PIN)965721823600000 and owned by Mr.Peter Hall.The approximately 1.63-acre subject property is currently vacant.Water and sewer services are available in the vicinity of the subject property through the City of Asheville and the Metropolitan Sewerage District.The subject property gently slopes from east to west.A road affords access to the subject property.Scattered debris consisting of bottles,cans,scrap metal,and discarded wood was observed scattered across the subject property.Several pole-mounted transformers were observed at the subject property.The transformers are owned and maintained by Duke Energy.We did not observe evidence of leakage or staining in the vicinity of the transformers. ECS conducted a Soil and Groundwater Assessment at the subject property (ECS project number 49-7572,dated October 11,2018).Approximately six soil test borings were drilled to depths ranging between 5 and 8 feet below the ground surface (bgs).The soil borings were located in the vicinity of a former floor drain in the former loading dock (S-1),in the vicinity of former floor drains in the former assembly room (S-2),in the former machining room (S-3),in the vicinity of the former waste oil and ASTs (S-4),in the vicinity of a former floor drain outside former tool room (S-5),and in the vicinity of the former AST located on the southern side of the former building. Laboratory analysis of soil samples S-1,S-3,S-4,S-5,and S-6 detected arsenic at concentrations above the Residential Health Based Preliminary Soil Remediation Goal (PSRG)standard;however, the concentrations do not exceed the Industrial/Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard.Laboratory analysis of soil sample S-2 detected arsenic at a concentration (3.1 mg/kg)above the Industrial/Commercial Health Based PSRG standard;however, the concentrations do not exceed the Protection of Groundwater PSRG standard.According to the Elements in North American Soils (Second Edition),the mean concentration of arsenic in North Carolina is 4.8 mg/kg,which is above the concentrations identified in the samples.Laboratory analysis of soil samples S-1 through S-6 detected hexavalent chromium at concentrations above the Residential Health Based PSRG standard;however,the concentrations do not exceed the Industrial/ Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard. Four groundwater borings were advanced at the subject property.The groundwater borings were located in the vicinity of former floor drains in the former assembly room (GW-1),in the vicinity of the former waste oil and ASTs (GW-2),in the vicinity of a former AST located on the southern side of the former building (GW-3),and downgradient of the former building (GW-4).Groundwater was identified at depths ranging from 7 to 10 feet bgs.Laboratory analysis of groundwater sample GW-3 detected trichloroethene (TCE)at a concentration above its NC2LGWQS,Residential VISL,and Non-Residential VISL. The locations of the soil and groundwater samples are approximate due the building no longer August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage1 being present.ECS considers the identified soil and groundwater impacts to represent a recognized environmental condition (REC) for the subject property. The subject property is located in a commercial/residential area of Asheville,North Carolina. The subject property is bound on the north by West Chapel Road followed by Sunset Cemetery;on the east by wooded land and an oped field;on the south by a residence;and on the west by Sweeten Creek Road followed by the Car Dr,a residence,and Crossroads Towing.ECS did not identify environmental issues at adjoining or nearby properties that are believed to present a REC at the subject property. Based on the records search,site reconnaissance and interviews,it appears that the subject property was developed with an industrial facility since approximately the mid 1930s.The onsite building was demolished prior to 2012 and the subject property has remained vacant since.Historical records prior to 1936 were not reasonably ascertainable for the subject property.Our review of historical information for adjoining or nearby properties identified the area as originally the surrounding area has developed from agricultural land to commercial/residential area. Historical aerial photographs depict structures on the subject property that were not located on the subject property during our site reconnaissance.ECS does not have technical evidence how these structures were heated,or if the structures utilized septic tanks or water supply wells.Based on the age,it is possible that the structures were heated with oil stored in USTs.ECS did not observe evidence of USTs,septic tanks,or water supply wells during our site reconnaissance.While not considered a REC,if encountered during site development,USTs,septic systems,and water supply wells should be closed in accordance with applicable laws. A regulatory database search report was provided by Environmental Data Resources,Inc.(EDR). The database search involves researching a series of Federal,State,Local,and other databases for facilities and properties that are located within specified minimum search distances from the subject property. The report did identify the subject property on the databases researched. The subject property was identified on the Brownfields and RCRIS databases.Prior reports indicate the subject property has been historically utilized as an industrial manufacturing facility and elevated concentrations of TCE and chromium have been identified on the subject property.ECS considers the use of the subject property as an industrial manufacturing facility and existing contamination on subject property to be a REC for the subject property. The EDR report identified several off-site properties within the minimum ASTM search distances. Based on our review of available public records,none of the listings are believed to represent a REC for the subject property. ASTM E1527-13 defines a “data gap”as:“a lack of or inability to obtain information required by this practice despite good faith efforts by the environmental professional to gather such information.” Data gaps which would be expected to impact our ability to render a professional opinion concerning the subject property were not identified. We have performed a Phase I Environmental Site Assessment in general conformance with the scope and limitations of ASTM E1527-13 of the Former P.E.Valve Property located at 1140 Sweeten Creek August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage2 Road,in Asheville,Buncombe County,North Carolina.Exceptions to,or deletions from,this practice are described in Section 2.6 of this report.This assessment has revealed no evidence of recognized environmental conditions in connection with the property except for the following: •Due to the historical use of the subject property as an industrial manufacturing facility and confirmed groundwater contamination at concentrations above regulatory limits,ECS considers the prior use to be a REC. ECS recommends soil gas sampling be conducted to determine if the groundwater concentrations identified are causing a vapor concern at the subject property. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage3 2.0 INTRODUCTION 2.1 Purpose and Reason for Performing Phase I ESA The purpose of the ESA was to: •evaluate the probability of impact to the surface water,groundwater and/or soils within the property boundaries through a review of regulatory information and a reconnaissance of the subject property and vicinity; •evaluate historical land usage to identify previous conditions that could potentially impact the environmental condition of the subject property; •conduct all appropriate inquiry as defined by ASTM E1527-13 and 40 CFR Part 312; •evaluate the potential for on-site and off-site contamination; and, •provide a professional opinion regarding the potential for environmental impact at the site and a list of Recognized Environmental Conditions (RECs). The ESA should allow the Users the opportunity to qualify for landowner liability protection under the Comprehensive Environmental Response,Compensation and Liability Act (CERCLA)provided certain stipulations are met.The landowner liability protections are:an innocent landowner,a contiguous property owner,or a bona fide prospective purchaser.The User must meet the protection stipulations detailed in CERCLA to qualify as well as meet the User Obligations contained within the ASTM E1527- 13 standard. The reason for conducting this ESA is to perform all appropriate inquiries into the uses and prior ownership of the subject property as requested by the North Carolina Department of Environmental Quality (NCDEQ) Brownfields Program. 2.2 Scope of Services The environmental assessment was conducted in general accordance with ASTM E1527-13 and EPA Standards and Practices for All Appropriate Inquiry (40 CFR §312.10).The environmental assessment was conducted under the supervision or responsible charge of an individual that qualifies as an environmental professional, as defined in 40 CFR §312.10. ECS was contracted by Mr.Peter Hall to perform an ASTM E1527-13,Phase I Environmental Site Assessment (ESA)of the Former P.E.Valve Property located at 1140 Sweeten Creek Road in Asheville, Buncombe County, North Carolina. ECS was not contracted to address non-scope considerations. 2.3 Definitions ASTM E1527-13 defines a "recognized environmental condition (REC)"as "the presence or likely presence of any hazardous substances or petroleum products in,on or at a property:1)due to release to the environment,2)under conditions indicative of a release to the environment;or 3)under conditions that pose a material threat of a future release to the environment.”For the purposes of this practice,“migrate"and “migration”refer to the movement of hazardous substances or petroleum products in any form including solid and liquid at the surface or subsurface and vapor in the subsurface. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage4 ASTM E1527-13 defines a “business environmental risk”(BER)as "a risk which can have a material environmental or environmentally-driven impact on the business associated with the current or planned use of a parcel of commercial real estate,not necessarily limited to those environmental issues required to be investigated in this practice".ECS also uses the term "Other Environmental Considerations"to discuss BERs and environmental concerns outside of the ASTM E1527-13 requirements (radon,asbestos,lead,wetlands,etc.).Client-imposed limitations and site condition limitations, if encountered, are detailed in Section 7.1 Methodology and Limiting Conditions. ASTM E1527-13 defines a “de minimis condition”as a condition that generally does not represent a threat to human health or the environment and that generally would not be the subject of an enforcement action if brought to the attention of appropriate governmental agencies.De minimis conditions are not recognized environmental conditions nor controlled recognized environmental conditions. ASTM E1527-13 defines a "controlled recognized environmental condition (CREC)"as a recognized environmental condition resulting from a past release of hazardous substances or petroleum products that has been addressed to the satisfaction of the applicable regulatory authority (for example,as evidenced by the issuance of a no further action letter or equivalent,or meeting risk-based criteria established by regulatory authority),with hazardous substances or petroleum products allowed to remain in place subject to the implementation of required controls (for example property use restrictions,activity and use limitations,institutional controls,or engineering controls). A condition identified as a controlled recognized environmental condition does not imply that the Environmental Professional has evaluated or confirmed the adequacy,implementation or continued effectiveness of the required control that has been, or is intended to be, implemented. ASTM E1527-13 defines a "historical recognized environmental condition (HREC)"as a past release of any hazardous substances or petroleum products that has occurred in connection with the property and has been addressed to the satisfaction of the applicable regulatory authority or meeting unrestricted residential use criteria established by a regulatory authority,without subjecting the property to any required controls (for example property use restrictions,activity and use limitations, institutional controls,or engineering controls).Before calling the past release a historical recognized environmental condition,the Environmental Professional must determine whether the past release is a recognized environmental condition at the time the Phase I Environmental Site Assessment is conducted (for example, if there has been a change in the regulatory criteria). 2.4 Limitations The ESA involved a reconnaissance of the subject property and contiguous properties and a review of regulatory and historical information in general accordance with the ASTM standard and EPA regulation referenced herein.No non-scope considerations or additional issues such as asbestos, radon, wetlands or mold were investigated, unless otherwise described in Section 8.0 of this report. Note:vapor migration in the subsurface is described in Guide E2600 published by ASTM.ECS has not conducted a Vapor Encroachment Screen in accordance with the E2600 guide. The conclusions and/or recommendations presented within this report are based upon a level of investigation consistent with the standard of care and skill exercised by members of the same August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage5 profession currently practicing in the same locality under similar conditions.The intent of this assessment is to identify the potential for recognized environmental conditions in connection with the subject property;however,no environmental site assessment can completely eliminate uncertainty regarding the potential for recognized environmental conditions in connection with the subject property.The findings of this ESA are not intended to serve as an audit for health and safety compliance issues pertaining to improvements or activities at the subject property.ECS is not liable for the discovery or elimination of hazards that may potentially cause damage, accidents or injury. Observations,conclusions and/or recommendations pertaining to environmental conditions at the subject property are necessarily limited to conditions observed,and or materials reviewed at the time this study was undertaken.It was not the purpose of this study to determine the actual presence, degree or extent of contamination,if any,at this subject property.This could require additional exploratory work,including sampling and laboratory analysis.No warranty,expressed or implied,is made with regard to the conclusions and/or recommendations presented within this report. This report is provided for the exclusive use of Mr.Peter Hall.This report is not intended to be used or relied upon in connection with other projects or by other unidentified third parties.The use of this report by any undesignated third party or parties will be at such party’s sole risk and ECS disclaims liability for any such third party use or reliance. 2.5 Data Gaps Data failures (historical data gaps)were identified during the historical research of this subject property.Use of the subject property was generally documented back to 1894.Historical information was missing for various periods.However,due to the apparent former use as an industrial facility and the information obtained associated with that use;the historical data gaps are not expected to impact our ability to render a professional opinion regarding the subject property. 2.6 Limiting Conditions/Deviations ASTM E1527-13 requires that the Environmental Professional identify limiting conditions,deletions, and deviations from the ASTM E1527-13 standard,if any,including client-imposed constraints. Limiting conditions and/or deviations from the standard practice that would be expected to impact our ability to provide a professional opinion concerning the subject property were not encountered during the performance of this Phase I ESA. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage6 3.0 SUBJECT PROPERTY DESCRIPTION 3.1 Subject Property Location and Legal Description Site Name Former P.E. Valve Property Property Address 1140 Sweeten Creek Road Property City, State Asheville,North Carolina Property County Buncombe County Number of Parcels One Property ID Number(s)965721823600000 Property Size 1.63 Acres Property Owner of Record Mr. Peter Hall 3.2 Physical Setting and Hydrogeology USGS Topographic Map Quad Designation TP, Asheville and E, Oteen Date 2013 Subject Property Settings Average Subject Property Elevation (in ft or meters) Approximately 2,125 feet above mean sea level (AMSL) General Sloping Direction West Bodies of Water None General Directions of Surface Flow West Presumed Direction of Groundwater Flow West Geologic Province Blue Ridge Up-gradient Property Direction East Nearby Properties' Setting General Sloping Direction East to west August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage7 Bodies of Water Stream located approximately 200 feet west General Directions of Surface Flow West Presumed Direction of Groundwater Flow West Regional influences may have an impact on groundwater flow.The actual groundwater flow direction cannot be determined without site-specific information obtained through the gauging of groundwater monitoring wells. 3.3 Current Use and Description of the Site The subject property consists of an approximately 1.63-acre parcel of land that is currently utilized as as a vacant parcel of land.The subject property is located in an area that can generally be described as commercial/residential. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage8 4.0 USER PROVIDED INFORMATION The ASTM standard includes disclosure and obligations of the User to help the Environmental Professional identify the potential for Recognized Environmental Conditions associated with the subject property.The ASTM E1527-13 User Questionnaire was submitted to and completed by Mr. Peter Hall (User of the report).Section 4.0 is based on the completed User Questionnaire.A copy of the completed User Questionnaire is included in Appendix II. 4.1 Title Information ECS was not provided with title information by the User.If this information is provided following issuance of this report and information contained therein materially changes the outcome of this report, ECS will issue an addendum to this report. 4.2 Environmental Liens or Activity and Use Limitations ECS was neither contracted to obtain information on environmental liens or activity and use limitations,nor have we been provided with information on environmental liens or activity and use limitations for our review.It should be noted by the User of this report that if the User does not obtain activity and use limitation information,the User that is seeking to qualify for an innocent landowner, a contiguous property owner,or a bona fide prospective purchaser liability defense may lose these rights to qualify under CERCLA.If the activity and use information is provided following issuance of this report and information contained therein materially changes the outcome of this report,ECS will issue an addendum to this report.The User stated they were not aware of any AULs associated with the subject property. 4.3 Specialized Knowledge The User indicated that they did not possess specialized knowledge of the subject property. 4.4 Commonly Known or Reasonably Ascertainable Information The User indicated that the facility previously present at the subject property made socks and textiles prior to the purchase in the early 1970s.The User indicated that the previous industry used trichloroethene (TCE) and perchloroethylene (PCE). 4.5 Valuation Reduction for Environmental Issues The subject property is not currently being soid.However,the User indicated that it is anticipated that if environmental concerns were not present,the User would get more money for the property.The User had an offer above current purchase price before environmental concerns were discovered. 4.6 Owner, Property Manager, and Occupant Information The current property owner is Mr. Peter Hall. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage9 4.7 Degree of Obviousness Assessments were conducted on the property to identify contamination. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage10 5.0 RECORDS REVIEW A regulatory records search of ASTM standard and supplemental databases was conducted for the subject property and is included in Appendix III.The regulatory search report in the appendix includes additional details about the regulatory databases that were reviewed.The regulatory records search involves searching a series of databases for facilities that are located within a specified distance from the subject property.The ASTM standard specifies an approximate minimum search distance from the subject property for each database.Pursuant to ASTM,the approximate minimum search distance may be reduced for each standard environmental record except for Federal NPL site list,and Federal RCRA TSD list.According to ASTM,government information obtained from nongovernmental sources may be considered current if the source updates the information at least every 90 days or, for information that is updated less frequently than quarterly by the government agency,within 90 days of the date the government agency makes the information available to the public.The following table indicates the standard environmental record sources and the approximate minimum search distances for each record. Standard Environmental Record Sources Approximate Minimum Search Distance Per ASTM (miles) Subject Property Off-Site Properties Federal NPL 1.0 No 0 Federal Delisted NPL 0.5 No 0 Federal CERCLIS 0.5 No 0 Federal CERCLIS NFRAP 0.5 No 0 Federal RCRA CORRACTS 1.0 No 0 Federal RCRA non-CORRACTS TSD 0.5 No 0 Federal RCRA Generators Subject Site and Adjoining Properties Yes 3 Federal IC/EC Subject Site Only No N/A Federal ERNS Subject Site Only No N/A State and Tribal Hazardous Waste Sites (NPL Equivalent) 1.0 No 0 State and Tribal Hazardous Waste Sites (CERCLIS Equivalent) 0.5 No 1 State and Tribal Landfill and/or solid waste disposal sites 0.5 No 0 August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage11 Standard Environmental Record Sources Approximate Minimum Search Distance Per ASTM (miles) Subject Property Off-Site Properties State and Tribal Leaking Tanks 0.5 No 14 State and Tribal Registered UST and AST Subject Site and Adjoining Properties No 3 State and Tribal IC/EC Subject Site Only No N/A State and Tribal Voluntary Cleanup (VCP) 0.5 No 0 State and Tribal Brownfield Sites 0.5 Yes 0 Based on our knowledge of the subject property and the surrounding area,ECS attempts to verify and interpret this data.While this attempt at verification is made with due diligence,ECS cannot guarantee the accuracy of the record(s)search beyond that of information provided by the regulatory report(s).ECS makes no warranty regarding the accuracy of the database report information included within the regulatory report(s). The regulatory database search was performed by EDR,dated July 15,2019.ECS did not reduce the minimum ASTM search distances stipulated in the standard.The regulatory databases reviewed by ECS included supplemental databases researched by EDR. 5.1 Federal ASTM Databases 5.1.1 Federal RCRIS - Generators RCRIS identifies facilities that generate hazardous wastes as defined by the RCRA.Conditionally exempt small quantity generators (CESQGs)generate less than 100 kilograms of hazardous waste, or less than 1 kilogram of acutely hazardous waste,per month.Small quantity generators (SQGs) generate between 100 and 1,000 kilograms of hazardous waste per month.Large quantity generators (LQGs)generate more than 1,000 kilograms of hazardous waste or more than 1 kilogram of acutely hazardous waste per month. The subject property was identified on the RCRIS Generator database.The subject property was listed as the PE Valve Co,located at 1140 Sweeten Creek Rd.According to the EDR report, the facility was listed as a CESQG of ignitable waste.No violations were reported at the facility.Additional information associated with this listing is located in section 5.3.1.1 of this report.ECS considers this to be a REC for the subject property. One or more off-site properties within the minimum search distance of inquiry were reported as being on the Federal RCRIS Generators database. Core &Main LP,1129 Sweeten Creek Road -This address is located approximately 500 feet August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage12 southwest and topographically downgradient of the subject property.According to the EDR report,this facility is listed as a CESQG of ignitable waste,corrosive waste,mercury,benzene, and methyl enthyl ketone.No violations have been reported at the facility.Due to the distance and topographic downgradient position from the subject property,ECS does not consider this an REC for the subject property. United Parcel Service-Asheville,301 Sweeten Creek Road -This address is located approximately 750 feet north northeast and topographically downgradient of the subject property.According to the EDR report,this facility is listed as a CESQG of ignitable waste, benzene,nonhalogenated solvents,tetrachloroethylene,nicotine,and salts.Due to the distance and topographic downgradient location from the subject property,ECS does not consider this a REC for the subject property. The EDR report lists an additional 1 facilities within the search radius for the database.These facilities are located greater than 1,000 feet from the subject property.Based on the distance from the subject property,ECS does not consider these listings to be RECs for the subject property.Additional information pertaining to these listings can be viewed in the regulatory report included in Appendix III. 5.2 State ASTM Databases 5.2.1 State Hazardous Waste Sites (SHWS) Inventory State hazardous waste site records are the states’equivalent to CERCLIS.These sites may or may not be already listed on the federal CERCLIS database. One or more off-site properties within the minimum search distance of inquiry was reported as being on the SHWS database. Smith's Aerospace,401 Sweeten Creek Industrial Park -This address is located approximately 850 feet northeast and topographically downgradient from the subject property. According to the EDR report,the Environmental Protection Agency Identification Number is NONCD0001163.Due the distance and downgradient location from the subject property,ECS does not consider this a REC for the subject property. 5.2.2 State LAST The LAST list is a record of reported leaking aboveground storage tank incidents. The EDR report lists one facility within the search radius for the database.This facility is located greater than 1,000 feet from the subject property.Based on the distance from the subject property, ECS does not consider this listing to be a REC for the subject property.Additional information pertaining to this listing can be viewed in the regulatory report included in Appendix III. 5.2.3 Leaking Underground Storage Tank (LUST) List The LUST list is a record of reported leaking underground storage tank incidents.The LUST list may also identify properties that have had soil and/or groundwater contamination associated with August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage13 documented releases from aboveground storage tanks, surface spills, and other sources. One or more off-site properties within the minimum search distance of inquiry was reported as being on the LUST database. Robert Ted Young (The Appliance Hut),1085 Sweeten Creek Road -This address is located approximately 70 feet northwest and topographically downgradient from the subject property. According to the EDR report,an underground leak occurred in December of 1997.The incident has been closed and a letter of No Further Action (NFA)has been issued.Due to the topographic downgradient location from the subject property,ECS does not consider this a REC for the subject property. Hot Spot #2003,1069 Sweeten Creek Road -This address is located approximately 470 feet northwest and topographically downgradient of the subject property.According to the EDR report,an underground lead occurred in March of 2013.Due to the distance and topographic downgradient location from the subject property,ECS does not consider this a REC for the subject property. United Parcel Service,301 Sweeten Creek Industrial Park -This address is located approximately 750 feet north northeast and topographically downgradient of the subject property.According to documentation the tanks are located over a 1,000 feet from the subject property property.Due to the distance from the subject property,ECS does not consider this a REC for the subject property. The EDR report lists an additional seven facilities within the search radius for the database. These facilities are located greater than 1,000 feet from the subject property.Based on the distance from the subject property,ECS does not consider these listings to be RECs for the subject property.Additional information pertaining to these listings can be viewed in the regulatory report included in Appendix III. 5.2.4 Registered Underground Storage Tank (UST) List The Registered UST List inventories underground storage tanks registered with the state.This list does not identify USTs that have not been registered or are exempt,such as home heating oil tanks and other unregulated tanks. One or more off-site properties within the minimum search distance of inquiry was reported as being on the UST database. Hot Spot 2003,1069 Sweeten Creek Road -This address is located approximately 470 feet northwest and topographically downgradient of the subject property.According to the EDR report,three 10,000-gallon USTs containing gasoline were installed in 1964 and are still current. One 4,000-gallon UST containing kerosene was installed in 1964 and is still current.Due to the distance and topographic downgradient location from the subject property,ECS does not consider this a REC for the subject property. Sweeten Creek Quality Plus,Address -This address is located approximately 680 feet northwest and topographically downgradient of the subject property.According to the EDR August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage14 report,one 20,000-gallon UST and one 12,000-gallon UST both containing gasoline were installed in 2010 and are still current.One 12,000-gallon UST containing diesel was installed in 2010 and is still current.One 3,000-gallon UST containing gasoline was installed in 2010 and is still current. Due to the distance from the subject property,ECS does not consider this a REC for the subject property. The EDR report lists one additional facility within the search radius for the database. This facility is located greater than 1,000 feet from the subject property.Based on the distance from the subject property,ECS does not consider this listing to be a REC for the subject property.Additional information pertaining to this listing can be viewed in the regulatory report included in Appendix III. 5.3 Additional Environmental Record Sources 5.3.1 Additional Non-ASTM Federal Databases 5.3.1.1 US Brownfields The US Brownfields identifies brownfields properties inventoried with the USEPA.The properties in the listing are addressed by Cooperative Agreement Recipients and Targeted Brownfields Assessments. The subject property was identified on the US Brownfields database.According to the EDR report,the subject property is listed as a pending brownfield site (Project ID 22081-18-011). A Report of Limited Phase II ESA conducted by Bunnell-Lammons Engineering,Inc.(BLE) indicated that BLE conducted a Phase I ESA prior to the Phase II ESA.The Phase I ESA identified the following information.The subject property was developed as a textile manufacturing facility as early as the 1930s.Then utilized as a valve manufacturing facility (P.E.Valve Company,Inc.)after approximately 1968.During the Phase I ESA site walk several RECs were identified at the subject property.The RECs included rusted 55-gallon drums,an AST,staining along the norther wall of the building,a loading dock with floor drains and two ASTs on the interior of the building.Multiple 55-gallon drums and 5-gallon buckets of waste oil,coolant, and unidentified liquids inside of the building.Lastly,heavy staining on the floor of the building with a network of floor drains located inside the building. The Phase II ESA conducted by BLE advanced four borings (BL-1 through BL-4)to refusal to obtain groundwater samples at the subject property.At four locations within the building soil samples (HAB-1 through HAB -4)were collected underneath the concrete slab utilizing a hand auger.Groundwater samples identified TCE in BL-2,BL-3 and BL-4 above North Carolina 15A NCAC 2L standards for groundwater.Soil Samples identified selenium in HAB-4 and chromium in HAB-1, HAB-2, and HAB-4 above the North Carolina IHSB Soil Remediation Goals. ECS conducted a Soil and Groundwater Assessment at the subject property.Information associated with the Soil and Groundwater Assessment is located in section 6.10 of this report. After review of the information,it is ECS'opinion that based upon the historic use of the subject property,RECs identified in prior Phase I ESA,the findings of BLE's Phase II ESA,and August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage15 the findings of ECS's Soil and Groundwater Assessment this listing is considered a REC for the subject property. 5.3.1.2 FINDS Facility Index System.FINDS contains both facility information and ’pointers’to other sources that contain more detail.EDR includes the following FINDS databases in this report:PCS (Permit Compliance System),AIRS (Aerometric Information Retrieval System),Integrated Compliance Information System (ICIS),DOCKET (Enforcement Docket used to manage and track information on civil judicial enforcement cases for all environmental statutes),FURS (Federal Underground Injection Control),C-DOCKET (Criminal Docket System used to track criminal enforcement actions for all environmental statutes),FFIS (Federal Facilities Information System),STATE (State Environmental Laws and Statutes), and PADS (PCB Activity Data System). The subject property was identified on the FINDS database.The subject property was listed as the PE Valve Co,located at 1140 Sweeten Creek Rd.Information associated with this listing is located in section 5.3.1.1 of this report. ECS considers this a REC for the subject property. 5.3.2 Additional Non-ASTM State Databases 5.3.2.1 Leaking Underground Storage Tanks (LUST TRUST) The LUST TRUST database contains information about claims against the State Trust Funds for reimbursements for expenses incurred while remediating Leaking USTs. The EDR report lists two facilities within the search radius for the database.These facilities are located greater than 1,000 feet from the subject property.Based on the distance from the subject property,ECS does not consider these listings to be RECs for the subject property.Additional information pertaining to these listings can be viewed in the regulatory report included in Appendix III. 5.3.2.2 Incident Management Database (IMD) The IMD is a database of groundwater and soil contamination incidents. One or more off-site properties within the minimum search distance of inquiry was reported as being on the IMS database. Robert Ted Young (The Appliance Hut),1085 Sweeten Creek Road -This address is located approximately 70 feet northwest and topographically downgradient from the subject property. Information associated with this listing is located in section 5.2.3 of this report.ECS does not consider this a REC for the subject property. United Parcel Service-Asheville,301 Sweeten Creek Road -This address is located approximately 750 feet north northeast and topographically downgradient of the subject property.Information associated with this listing is located in section 5.1.1 of this report.ECS does not consider this a REC for the subject property. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage16 The EDR report lists an additional three facilities within the search radius for the database.These facilities are located greater than 1,000 feet from the subject property.Based on the distance from the subject property,ECS does not consider these listings to be RECs for the subject property.Additional information pertaining to these listings can be viewed in the regulatory report included in Appendix III. 5.3.3 Other Proprietary Databases 5.3.3.1 EDR Historical Auto Stations EDR has searched selected national collections of business directories and has collected listings of potential gas station/filling station/service station sites that were available to EDR researchers.EDR's review was limited to those categories of sources that might,in EDR's opinion,include gas station/ filling station/service station establishments.The categories reviewed included,but were not limited to gas,gas station,gasoline station,filling station,auto,automobile repair,auto service station, service station, etc. One or more off-site properties within the minimum search distance of inquiry was reported as being on the EDR Historical Auto Stations database. Jordan R L Oil CO of NC,1069 Sweeten Creek Road -This address is located approximately 470 feet northwest and topographically downgradient of the subject property.According to the EDR report,this facility was listed as a Jordan R L Oil CO of NC (Gasoline Service Station)from 2000 until 2014.Due to the distance and topographic downgradient location from the subject property, ECS does not consider this a REC for the subject property. 5.3.4 Unmapped (Orphan) Facilities and Sites Several properties were identified on the Orphan Summary List.These facilities are considered as unmappable because the facility information in the database is insufficient and does not report accurate facility location. 5.4 Regulatory Review Summary A regulatory database search report was provided by EDR.The database search involves researching a series of Federal,State,Local,and other databases for facilities and properties that are located within specified minimum search distances from the subject property.The report did identify the subject property on the databases researched. The subject property was identified on the Brownfields and RCRIS databases.Prior reports indicate the subject property has been historically utilized as an industrial manufacturing facility and elevated concentrations of trichloroethene and chromium have been identified on the subject property. ECS considers the use of the subject property as an industrial manufacturing facility and existing contamination on subject property to be a REC for the subject property. The EDR report identified several off-site properties within the minimum ASTM search distances. Based on our review of available public records,ECS does not consider the listings to be potential August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage17 sources of soil, groundwater or vapor impact to the subject property. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage18 6.0 HISTORICAL USE INFORMATION 6.1 Aerial Photograph Review ECS reviewed aerial photographs of the subject property and immediately surrounding properties for evidence of former usage which may indicate potential environmental issues.The aerial photographs were obtained from EDR.The aerial photographs reviewed were dated 1951,1964,1975,1984,1988, 1994,1998,2006,2009,2012,and 2016.Aerial photographs dated prior to 1951 were not available for review.The ECS review is dependent on the quality and scale of the photographs.The following is a description of relevant information from the aerial photographs: Year(s)Subject Property Adjoining Properties REC? (yes or no) 1951 Apparent industrial/ commercial buildings and agricultural land North - Road followed by agricultural land East - Apparent residence and agricultural land South - Apparent buildings and agricultural land West - Road followed by apparent buildings Yes 1964 Apparent industrial/ commercial buildings North - Road followed by an apparent cemetery East - Apparent residences and agricultural land South - Apparent residence followed by commercial buildings West - Road followed by apparent buildings Yes 1975 Aerial poor quality Aerial poor quality No 1984, 1988,1994, 1998, 2006, and 2009 Apparent industrial/ commercial buildings North - Road followed by an apparent cemetery East - Apparent residences South - Apparent residence followed by commercial buildings West - Road followed by apparent commercial buildings Yes August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage19 Year(s)Subject Property Adjoining Properties REC? (yes or no) 2012 and 2016 Vacant land North - Road followed by an apparent cemetery East - Apparent residences South - Apparent residence followed by commercial buildings West - Road followed by apparent commercial buildings No 6.2 Sanborn Fire Insurance Map Review In an effort to identify past uses,ECS reviewed historical fire insurance maps obtained from EDR for information regarding the subject property and surrounding area.Historical SanbornTM Fire Insurance Maps (Sanborns)dated 1950,1954,1957,1961,1963,and 1972 provided coverage of the subject property area.A copy of the EDR report is included in Appendix IV.The following is a description of relevant information from the Sanborns: Year(s)Subject Property Adjoining Properties REC? (yes or no) 1950 Appalachian Textile Corp'n (weaving room, and dye room),dwellings and storage building North - West Chapel Road East - Cold storage building South - Dwelling West - Sweeten Creek Road followed by a store and a dwelling Yes 1954 Appalachian Textile Corp'n (weaving room, and dye room),dwelling, and storage building North - West Chapel Road East - Cold storage building South - Dwelling West - Sweeten Creek Road followed by a store and multiple dwellings Yes August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage20 Year(s)Subject Property Adjoining Properties REC? (yes or no) 1957 Chakales & CO MFG Hosiery, office building, and storage building North - West Chapel Road followed by Sunset Cemetery East - Cold storage building South - Dwelling West - Sweeten Creek Road followed by a store and multiple dwellings Yes 1961 Vacant industrial building, office building, and vacant storage building North - West Chapel Road followed by Sunset Cemetery East - Cold storage building South - Dwelling West - Sweeten Creek Road followed by a store and multiple dwellings Yes 1963 Industrial building, office building, and vacant storage building North - West Chapel Road followed by Sunset Cemetery East - Cold storage building South - Dwelling West - Sweeten Creek Road followed by a store and multiple dwellings Yes 1972 Vacant industrial building, office building, and vacant storage building North - West Chapel Road followed by Sunset Cemetery East - Cold storage building South - Dwelling West - Sweeten Creek Road followed by a store and multiple dwellings Yes 6.3 Property Tax Files Property tax files may include records of past ownership,appraisals,maps,sketches,photos or other information kept by the local jurisdiction for property tax assessment purposes.According to the Buncombe County tax assessor on-line information,the subject property is owned by Mr. Peter Hall.The subject property is listed as a 1.63-acre parcel with an identification number of 965721823600000. 6.4 Recorded Land Title Records Recorded land title records may include leases,land contracts,and AULs recorded by the local August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage21 jurisdiction.Land title records may provide only a list of the names of previous owners and may be of limited use;however,they may provide useful information about uses or occupancy of the property when employed in combination with other sources. ECS was not provided with Land Title Records. 6.5 Historical USGS Topographic Maps Topographic maps are produced by the United States Geological Survey (USGS)for various time periods.ECS reviewed topographic maps of the subject property and immediately surrounding properties for evidence of former usage which may indicate potential environmental issues.The topographic maps were obtained from EDR and were dated 1894,1901,1936,1943,1961,1988,1990, and 2013.Topographic maps dated prior to 1894 were not available for review.The following is a description of relevant information from the topographic maps: Year(s)Subject Property Adjoining Properties REC? (yes or no) 1894 Undeveloped North - Undeveloped East - Undeveloped South - Udeveloped West - Fosters Mill Creek No 1901 Undeveloped North - Road East - Undeveloped South - Undeveloped West - Stream No 1936 Depicted industrial/commercial building North - Road followed by depicted building East - Depicted building South - Depicted smaller buildings and larger industrial/ commercial building West - Road followed by Sweeten Creek Yes 1943 Depicted industrial/commercial building and a smaller building North - Road East - Depicted building South - Depicted smaller buildings and larger industrial/ commercial building West - Road followed by depicted buildings beyond of which Sweeten Creek Yes August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage22 Year(s)Subject Property Adjoining Properties REC? (yes or no) 1961 Depicted industrial/commercial building and a smaller building North - Road East - Depicted buildings South - Depicted smaller buildings and larger industrial/ commercial building West - Road followed by depicted buildings beyond of which Sweeten Creek Yes 1988 Depicted industrial/commercial building and two smaller buildings North - Road East - Depicted buildings South - Depicted smaller buildings and larger industrial/ commercial building West - Road followed by depicted buildings beyond of which Sweeten Creek Yes 1990 Vacant North - Road East - Depicted buildings South - Depicted smaller buildings and larger industrial/ commercial building West - Road followed by Sweeten Creek No 2013 Building layer not depicted North - Road East - Nothing depicted South - Nothing depicted West - Road followed by Sweeten Creek No 6.6 City Directory Review One of the ASTM standard historical sources to be reviewed for previous subject property uses is local street directories,commonly known as City Directories.The purpose of the directory review is to identify past occupants of the subject property,adjoining properties,or nearby properties.In some rural areas, street directories information is limited. ECS reviewed city directories obtained from EDR.The directories reviewed were dated 1975,1981, 1985,1987,1992,1995,2000,2005,2010,and 2014.The directories reviewed prior to 1992 did not provide listings for the subject property or surrounding area.Directories dated prior to 1975 were not available for review.The subject property address utilized for the research was 1140 Sweeten Creek August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage23 Road.A copy of the city directory report is included in Appendix IV.The following is a description of relevant information from the city directories: Year(s)Subject Property Adjoining Properties REC? (yes or no) 1981 No listings North - No listings East - No listings South - No listings West - B & S Auto Sales No 1985 and 1987 No listings North - No listings East - No listings Southwest - Myers Sports Car Service West - Residence, Ted's Welding, B & S Auto Sales No 1992 P E Product Engineering Corp North - No listings East - No listings Southwest - Residence West - Residence Yes 1995 P E Product Engineering Corp North - No listings East - Residence Southwest - Residence West - Appliance Shop, Dunhams TV Service Yes 2000 P E Valve Company Inc North - No listings East - Residence Southwest - Residence West - Extreme Digital Planet, B & S Auto Sales Yes 2005 P E Valve Company Inc North - No listings East - Residences Southwest - Residence West - No listings Yes 2010 No listings North - No listings East - Residences Southwest - Residence West - No listings No August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage24 Year(s)Subject Property Adjoining Properties REC? (yes or no) 2014 No listings North - No listings East - Residences Southwest - Myers Motorcycles Inc West - Senor Clean, Pavone LLC, Carolina Dental Lab No 6.7 Building Department Records The term building department records means those records of the local government indicating permissions of the local government to construct, alter or demolish improvements on the property. ECS personnel searched the Buncombe County Development,Permit,and License Portal website on July 19,2019 to determine if there were any permits associated with subject property that had historical information regarding construction dates,inspections,or other information regarding the subject property.No documentation was found associated with the subject property. 6.8 Zoning/Land Use Records The term zoning/land use records refers to records of the local government indicating the uses permitted by the government in particular zones within its jurisdictions. ECS reviewed zoning/land use records obtained from the Buncombe County GIS website.The subject property is currently zoned for commercial industrial (CI)use. 6.9 Other Historical Sources Other credible historical sources may be reviewed to identify past uses of the subject property.These sources may include websites,county or state road maps,historical society documents,or local library information. ECS personnel searched the Buncombe County Development,Permit,and License Portal website on July 19,2019 to determine if there were any permits associated with the subject property that had historical information regarding environmental issues or responses.No documentation was found associated with the subject property. ECS personnel attempted to contact the City of Asheville Fire Department to determine if they had historical information regarding environmental issues or responses at the subject property.No information has been received at the time of the report completion.If information is received that changes the conclusions or recommendations of this report,ECS will forward the information to the Client. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage25 6.10 Previous Reports We have conducted the following environmental and/or engineering assessment(s)for the subject property: ECS conducted a Soil and Groundwater Assessment at the subject property (ECS project number 49-7572).Approximately six soil test borings were drilled to depths of ranging between 5 and 8 feet below the ground surface (bgs).The soil borings were located in the vicinity of a former floor drain in the former loading dock (S-1),in the vicinity of former floor drains in the former assembly room (S-2), in the former machining room (S-3),in the vicinity of the former waste oil and ASTs (S-4),in the vicinity of a former floor drain outside former tool room (S-5),and in the vicinity of the former AST located on the southern side of the former building. Four groundwater borings were advanced at the subject property.The groundwater borings were located in the vicinity of former floor drains in the former assembly room (GW-1),in the vicinity of the former waste oil and ASTs (GW-2),in the vicinity of a former AST located on the southern side of the former building (GW-3),and downgradient of the former building (GW-4).Groundwater was identified at depths ranging from 7 to 10 feet bgs. Laboratory analysis of groundwater sample GW-3 detected TCE at a concentration above its NC2LGWQS, Residential VISL, and Non-Residential VISL. Laboratory analysis of soil samples S-1,S-3,S-4,S-5,and S-6 detected arsenic at concentrations above the Residential Health Based PSRG standard;however,the concentrations do not exceed the Industrial/Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard.Laboratory analysis of soil sample S-2 detected arsenic at a concentration (3.1 mg/kg) above the Industrial/Commercial Health Based PSRG standard;however,the concentrations do not exceed the Protection of Groundwater PSRG standard.According to the Elements in North American Soils (Second Edition),the mean concentration of arsenic in North Carolina is 4.8 mg/kg,which is above the concentrations identified in the samples.Laboratory analysis of soil samples S-1 through S-6 detected hexavalent chromium at concentrations above the Residential Health Based PSRG standard;however,the concentrations do not exceed the Industrial/Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard. The extent of impact to the site has not been fully delineated.Additional assessment would be necessary to fully delineate the extent of impact to the site. ECS considers the identified soil and groundwater impacts to represent a REC for the subject property. 6.11 Historical Use Summary According to historical records research and other sources,the site has historically been utilized as an industrial facility since approximately the mid 1930s.The onsite building was demolished prior to 2012 and the subject property has remained vacant since.The surrounding area has developed from agricultural land to commercial/residential area.Indications of recognized environmental conditions were identified in the historical data review.The following recognized environmental conditions were identified through a review of available historical records: August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage26 •The historical use of the subject property as an industrial manufacturing facility apparent in aerials from 1951 until 2009,identified on Sanborn Maps from 1950 until 1972,depicted in topographic maps from 1936 until 1988,and identified on City directories from 1992 until 2005. •A Soil and Groundwater Assessment conducted by ECS identifying TCE at a concentrations above its NC2LGWQS,Residential VISL,and Non-Residential VISL.Soil samples identifying arsenic and hexavalent chromium above the Residential Health Based PSRG standard.One soil sample detected arsenic at a concentration above the Industrial/Commercial Health Based PSRG standard. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage27 7.0 SITE AND AREA RECONNAISSANCE 7.1 Methodology Don Randall Marlor of ECS conducted the field reconnaissance on July 25,2019.The weather at the time of the reconnaissance was 74 degrees Fahrenheit and cloudy.Observations were made from a walking reconnaissance around the perimeter and along several transects across the subject property.Access or visibility limitations,if any,are discussed in Section 2.6.Subject property photographs are included in Appendix V. 7.2 On-Site Features The subject property is approximately 1.63 acres in size and consists of a vacant,heavily vegetated lot.Water and sewer services are available in the vicinity of the subject property through the City of Asheville and the Metropolitan Sewerage District.The subject property gently slopes from east to west. A road affords access to the subject property.Scattered debris consisting of bottles,cans,scrap metal, and discarded wood was observed scattered across the subject property. Several pole-mounted transformers were observed at the subject property.The transformers are owned and maintained by Duke Energy.We did not observe evidence of leakage or staining in the vicinity of the transformers. The table below lists pertinent features of interest that were assessed for the subject property. Relevant information regarding pertinent features is discussed further in this section. Feature Yes No Underground or aboveground storage tanks  Strong, pungent or noxious odors  Surface waters  Standing pools of liquid likely containing petroleum or hazardous substances  Drums or containers of petroleum or hazardous substances greater than five-gallons  Drums or containers of petroleum or hazardous substances less than or equal to five-gallons  Unidentified opened or damaged containers of hazardous substances or petroleum products  Known or suspect PCB-containing equipment (excluding light ballasts) Stains or corrosion to floors, walls or ceilings  August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage28 Feature Yes No Floor drains and sump pumps  Pits, ponds or lagoons  Stained soil or pavement  Stressed vegetation  Solid waste mounds or non-natural fill materials  Wastewater discharges into drains, ditches or streams  Groundwater wells including potable, monitoring, dry, irrigation, injections and/or abandoned  Septic systems or cesspools  Elevators  Dry cleaning  Onsite emergency electrical generators  Specialized industrial equipment (paint booths, bag houses, etc.,) on-site  Hydraulic lifts  Oil-water separators  Compressors on-site  Grease traps  Known or suspect PCB-containing equipment (excluding light ballasts) Three pole-mounted transformer are located across the subject property.The transformer is owned and maintained by Duke Energy.Staining,which could be indicative of leakage,was not observed on the transformer or surfaces in the vicinity of the transformer. 7.3 Adjoining and Nearby Properties Contiguous and nearby properties were observed during a walking and vehicular reconnaissance of the subject property boundary and public places.The subject property is located in a commercial/ residential area of Asheville, Buncombe County, North Carolina. Direction Description Relative Gradient REC North West Chapel Road followed by Sunset Cemetery Cross-gradient No East Wooded land and an oped field Up-gradient No August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage29 Direction Description Relative Gradient REC South Residence Cross-gradient No West Sweeten Creek Road followed by the Car Dr, a residence, and Crossroads Towing Down-gradient No 7.4 Site and Area Reconnaissance Summary According to our site observations and a review of adjoining and nearby properties,the subject property is used as a vacant lot.The subject property is located in a commercial/residential area. Details pertaining to our on-site and off-site observations are referenced previously.We did not identify RECs associated with the subject property or neighboring properties and businesses during the reconnaissance. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage30 8.0 ADDITIONAL SERVICES ASTM guidelines identify non-scope issues,which are beyond the scope of this practice.Non-scope issues have the potential to be business environmental risks.Some of these non-scope issues include; asbestos-containing building materials,radon,lead-based paint,lead in drinking water,wetlands and mold. ECS was not authorized to assess non-scope issues in conjunction with this assessment. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage31 9.0 INTERVIEWS On August 24,2019,Mr.Peter Hall completed an ECS provided property owner survey.Mr.Hall has over 45 years of knowledge related to the subject property and associated activities.Mr.Hall indicated that he purchased the property from Mr.Jimmy Shackles around 1972.The subject property was developed with a sock and textile manufacturing facility when the property was purchased.The subject was originally developed with a chicken farm in the 1920s.Since the purchase of the subject property by Mr.Hall,a valve manufacturing company operated in the former on-site facility.The building was demolished and there are currently no structures on the subject property.According to Mr.Hall,the building was heated by natural gas.Floor drains were associated with the facility. However,it was unknown where the drains discharged.A Phase I ESA and soil and groundwater assessment was previously completed by others in 2010.Mr.Hall indicated that he is not aware of 1)environmental concerns associated with the subject property;2)any pending,past,or threatened administrative litigation or administrative proceedings relevant to hazardous substances or petroleum products in,on,or from the subject property;or 3)any government notices regarding any possible violation of environmental laws or possible liability related to hazardous substances or petroleum products. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage32 10.0 FINDINGS AND CONCLUSIONS The subject property is identified by the Buncombe County GIS website as PIN 965721823600000 and owned by Mr.Peter Hall.The approximately 1.63-acre subject property is currently vacant.Water and sewer services are available in the vicinity of the subject property through the City of Asheville and the Metropolitan Sewerage District.The subject property gently slopes from east to west.A road affords access to the subject property.Scattered debris consisting of bottles,cans,scrap metal, and discarded wood was observed scattered across the subject property.Several pole-mounted transformers were observed at the subject property.The transformers are owned and maintained by Duke Energy.We did not observe evidence of leakage or staining in the vicinity of the transformers. ECS conducted a Soil and Groundwater Assessment at the subject property (ECS project number 49-7572,dated October 11,2018).Approximately six soil test borings were drilled to depths ranging between 5 and 8 feet bgs.The soil borings were located in the vicinity of a former floor drain in the former loading dock (S-1),in the vicinity of former floor drains in the former assembly room (S-2),in the former machining room (S-3),in the vicinity of the former waste oil and ASTs (S-4),in the vicinity of a former floor drain outside former tool room (S-5),and in the vicinity of the former AST located on the southern side of the former building. Laboratory analysis of soil samples S-1,S-3,S-4,S-5,and S-6 detected arsenic at concentrations above the Residential Health Based PSRG standard;however,the concentrations do not exceed the Industrial/Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard.Laboratory analysis of soil sample S-2 detected arsenic at a concentration (3.1 mg/kg) above the Industrial/Commercial Health Based PSRG standard;however,the concentrations do not exceed the Protection of Groundwater PSRG standard.According to the Elements in North American Soils (Second Edition),the mean concentration of arsenic in North Carolina is 4.8 mg/kg,which is above the concentrations identified in the samples.Laboratory analysis of soil samples S-1 through S-6 detected hexavalent chromium at concentrations above the Residential Health Based PSRG standard;however,the concentrations do not exceed the Industrial/Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard. Four groundwater borings were advanced at the subject property.The groundwater borings were located in the vicinity of former floor drains in the former assembly room (GW-1),in the vicinity of the former waste oil and ASTs (GW-2),in the vicinity of a former AST located on the southern side of the former building (GW-3),and downgradient of the former building (GW-4).Groundwater was identified at depths ranging from 7 to 10 feet bgs.Laboratory analysis of groundwater sample GW-3 detected TCE at a concentration above its NC2LGWQS, Residential VISL, and Non-Residential VISL. The locations of the soil and groundwater samples are approximate due the building no longer being present.ECS considers the identified soil and groundwater impacts to represent a REC for the subject property. The subject property is located in a commercial/residential area of Asheville,North Carolina. The subject property is bound on the north by West Chapel Road followed by Sunset Cemetery;on the east by wooded land and an oped field;on the south by a residence;and on the west by Sweeten Creek Road followed by the Car Dr,a residence,and Crossroads Towing.ECS did not identify August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage33 environmental issues at adjoining or nearby properties that are believed to present a REC at the subject property. Based on the records search,site reconnaissance and interviews,it appears that the subject property was developed with an industrial facility since approximately the mid 1930s.The onsite building was demolished prior to 2012 and the subject property has remained vacant since.Historical records prior to 1936 were not reasonably ascertainable for the subject property.Our review of historical information for adjoining or nearby properties identified the area as originally the surrounding area has developed from agricultural land to commercial/residential area. Historical aerial photographs depict structures on the subject property that were not located on the subject property during our site reconnaissance.ECS does not have technical evidence how these structures were heated,or if the structures utilized septic tanks or water supply wells.Based on the age,it is possible that the structures were heated with oil stored in USTs.ECS did not observe evidence of USTs,septic tanks,or water supply wells during our site reconnaissance.While not considered a REC,if encountered during site development,USTs,septic systems,and water supply wells should be closed in accordance with applicable laws. A regulatory database search report was provided by EDR.The database search involves researching a series of Federal,State,Local,and other databases for facilities and properties that are located within specified minimum search distances from the subject property.The report did identify the subject property on the databases researched. The subject property was identified on the Brownfields and RCRIS databases.Prior reports indicate the subject property has been historically utilized as an industrial manufacturing facility and elevated concentrations of TCE and chromium have been identified on the subject property.ECS considers the use of the subject property as an industrial manufacturing facility and existing contamination on subject property to be a REC for the subject property. The EDR report identified several off-site properties within the minimum ASTM search distances. Based on our review of available public records,none of the listings are believed to represent a REC for the subject property. ASTM E1527-13 defines a “data gap”as:“a lack of or inability to obtain information required by this practice despite good faith efforts by the environmental professional to gather such information.” Data gaps which would be expected to impact our ability to render a professional opinion concerning the subject property were not identified. We have performed a Phase I Environmental Site Assessment in general conformance with the scope and limitations of ASTM E1527-13 of the Former P.E.Valve Property located at 1140 Sweeten Creek Road,in Asheville,Buncombe County,North Carolina.Exceptions to,or deletions from,this practice are described in Section 2.6 of this report.This assessment has revealed no evidence of recognized environmental conditions in connection with the property except for the following: •Due to the historical use of the subject property as an industrial manufacturing facility and confirmed groundwater contamination at concentrations above regulatory limits,ECS considers the prior use to be a REC. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage34 ECS recommends soil gas sampling be conducted to determine if the groundwater concentrations identified are causing a vapor concern at the subject property. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage35 11.0 REFERENCES ASTM E1527-13.Standard Practice for Environmental Site Assessment,Phase I Environmental Site Assessment Process. Environmental Data Resources,Inc.,The EDR Aerial Photo Decade Package (years 1951,1964,1975, 1984, 1988, 1994, 1998, 2006, 2009, 2012, and 2016), dated July 16, 2019. Environmental Data Resources, Inc., The EDR Radius Map Report, dated July 15, 2019. Environmental Data Resources,Inc.,Certified Sanborn Map Report (years 1950,1954,1957,1961, 1963, and 1972), dated July 15, 2019. Buncombe County County GIS website, accessed on July 18, 2019. Report of Limited Phase II Environmental Site Assessment,Bunnell-Lammons Engineering,Inc.,dated March 8, 2010. Soil and Groundwater Assessment,Former PE Valve Facility,ECS Southeast,LLP,dated October 11, 2018. Property Owner Survey completed by Mr. Peter Hall, dated August 24, 2019. User Questionnaire completed by Mr. Peter Hall, dated August 22, 2019. Environmental Data Resources,Inc.,EDR City Directory Image Report (no coverage),dated July 16, 2019. Environmental Data Resources,Inc.,Historical Topo Map Report (years 1894,1901,1936,1943,1961, 1988, 1990, and 2013), dated July 15, 2019. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-APage36 Appendix I:Figures Appendix II:Correspondence and User Questionnaire Appendix III:Regulatory Records Documentation FORM-LBC-GON ®kcehCoeG htiw tropeR ™paM suidaR RDE ehT 6 Armstrong Road, 4th floor Shelton, CT 06484 Toll Free: 800.352.0050 www.edrnet.com Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 Inquiry Number: 5716013.2s July 15, 2019 SECTION PAGE Executive Summary ES1 Overview Map 2 Detail Map 3 Map Findings Summary 4 Map Findings 8 Orphan Summary 56 Government Records Searched/Data Currency Tracking GR-1 GEOCHECK ADDENDUM Physical Setting Source Addendum A-1 Physical Setting Source Summary A-2 Physical Setting Source Map A-7 Physical Setting Source Map Findings A-8 Physical Setting Source Records Searched PSGR-1 TC5716013.2s Page 1 Thank you for your business. Please contact EDR at 1-800-352-0050 with any questions or comments. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2019 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. TABLE OF CONTENTS EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 1 A search of available environmental records was conducted by Environmental Data Resources, Inc (EDR). The report was designed to assist parties seeking to meet the search requirements of EPA’s Standards and Practices for All Appropriate Inquiries (40 CFR Part 312), the ASTM Standard Practice for Environmental Site Assessments (E 1527-13), the ASTM Standard Practice for Environmental Site Assessments for Forestland or Rural Property (E 2247-16), the ASTM Standard Practice for Limited Environmental Due Diligence: Transaction Screen Process (E 1528-14) or custom requirements developed for the evaluation of environmental risk associated with a parcel of real estate. TARGET PROPERTY INFORMATION ADDRESS 1140 SWEETEN CREEK RD ASHEVILLE, NC 28803 COORDINATES 35.5435130 - 35˚ 32’ 36.64’’Latitude (North): 82.5209360 - 82˚ 31’ 15.36’’Longitude (West): Zone 17Universal Tranverse Mercator: 362127.5UTM X (Meters): 3934184.0UTM Y (Meters): 2119 ft. above sea levelElevation: USGS TOPOGRAPHIC MAP ASSOCIATED WITH TARGET PROPERTY 5948460 ASHEVILLE, NCTarget Property Map: 2013Version Date: AERIAL PHOTOGRAPHY IN THIS REPORT 20141009Portions of Photo from: USDASource: 5716013.2s Page 2 24 BRUNNER AND LAY 150 SWEETEN CREEK RD LUST Lower 2556, 0.484, North 23 WEST CHAPEL BALL FIE WEST CHAPEL BALL FIE LAST, IMD Higher 2437, 0.462, East 22 TUSKEEGEE CLEANERS F 20 ROBERSON AVE. LAST, IMD Higher 2097, 0.397, NNW 21 FRANCES SUBER RESIDE 74 TAFT AVENUE LUST, LUST TRUST, INST CONTROL Higher 2024, 0.383, WNW 20 FREDRICKSON MOTOR EX 502 SWEETEN CREEK IN LUST, IMD Lower 1828, 0.346, NNE 19 SMITH’S AEROSPACE 401 SWEETEN CREEK IN SHWS Lower 1714, 0.325, NNE 18 MARCY PROPERTY (LISA 60 IMPERIAL COURT LUST Higher 1696, 0.321, WSW 17 PEPSI WAREHOUSE 601 SWEETEN CREEK IN LUST Lower 1584, 0.300, NE 16 FRESHWATER PROPERTY 523 CARIBOU ROAD LUST, LUST TRUST Higher 1456, 0.276, NW C15 UNITED PARCEL SERVIC 301 SWEETEN CREEK IN LUST Lower 1422, 0.269, NNE C14 UNITED PARCEL SERVIC 301 SWEETEN CREEK RD RCRA-CESQG, IMD Lower 1422, 0.269, NNE 13 PEPSI COLA CO P.O. BOX 5315 LUST, IMD Higher 1396, 0.264, NE 12 MACKS USED CAR & TRU 1191 SWEETEN CREEK R RCRA NonGen / NLR Higher 1311, 0.248, South 11 FORMER PEPSI-COLA BU 601 SWEETEN CRK INDU UST Higher 987, 0.187, West 10 STANLEY A BRIGGS INC 1026 SWEETEN CREEK R RCRA NonGen / NLR Lower 801, 0.152, NNW 9 SWEETEN CREEK QUALIT 1133 SWEETEN CREEK R UST, Financial Assurance Higher 622, 0.118, South B8 HOT SPOT 2003 1069 SWEETEN CREEK R UST Lower 520, 0.098, NNW B7 HOT SPOT #2003 1069 SWEETEN CREEK R LUST Lower 520, 0.098, NNW B6 JORDAN R L OIL CO OF 1069 SWEETEN CREEK R EDR Hist Auto Lower 520, 0.098, NNW 5 CORE & MAIN, LP 1129 SWEETEN CREEK R RCRA-CESQG Higher 250, 0.047, South A4 ROBERT TED YOUNG (TH 1085 SWEETEN CREEK R LUST, IMD Lower 83, 0.016, WSW A3 PE VALVE CO 1140 SWEETEN CREEK R FINDS, ECHO TP A2 PE VALVE CO 1140 SWEETEN CREEK R RCRA-CESQG TP A1 FORMER PE VALVE MANU 1140 SWEETEN CREEK R BROWNFIELDS TP MAPPED SITES SUMMARY Target Property Address: 1140 SWEETEN CREEK RD ASHEVILLE, NC 28803 Click on Map ID to see full detail. MAP RELATIVE DIST (ft. & mi.) ID DATABASE ACRONYMS ELEVATION DIRECTIONSITE NAME ADDRESS EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 3 TARGET PROPERTY SEARCH RESULTS The target property was identified in the following records. For more information on this property see page 8 of the attached EDR Radius Map report: EPA IDDatabase(s)Site FORMER PE VALVE MANU 1140 SWEETEN CREEK R ASHEVILLE, NC N/ABROWNFIELDS Project ID: 22081-18-011 PE VALVE CO 1140 SWEETEN CREEK R ASHEVILLE, NC 28803 NCD982130825RCRA-CESQG EPA ID:: NCD982130825 PE VALVE CO 1140 SWEETEN CREEK R ASHEVILLE, NC 28803 N/AFINDS Registry ID:: 110004034152 ECHO Registry ID: 110004034152 DATABASES WITH NO MAPPED SITES No mapped sites were found in EDR’s search of available ("reasonably ascertainable ") government records either on the target property or within the search radius around the target property for the following databases: STANDARD ENVIRONMENTAL RECORDS Federal NPL site list NPL National Priority List Proposed NPL Proposed National Priority List Sites NPL LIENS Federal Superfund Liens Federal Delisted NPL site list Delisted NPL National Priority List Deletions Federal CERCLIS list FEDERAL FACILITY Federal Facility Site Information listing SEMS Superfund Enterprise Management System Federal CERCLIS NFRAP site list SEMS-ARCHIVE Superfund Enterprise Management System Archive EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 4 Federal RCRA CORRACTS facilities list CORRACTS Corrective Action Report Federal RCRA non-CORRACTS TSD facilities list RCRA-TSDF RCRA - Treatment, Storage and Disposal Federal RCRA generators list RCRA-LQG RCRA - Large Quantity Generators RCRA-SQG RCRA - Small Quantity Generators Federal institutional controls / engineering controls registries LUCIS Land Use Control Information System US ENG CONTROLS Engineering Controls Sites List US INST CONTROL Sites with Institutional Controls Federal ERNS list ERNS Emergency Response Notification System State- and tribal - equivalent NPL NC HSDS Hazardous Substance Disposal Site State and tribal landfill and/or solid waste disposal site lists SWF/LF List of Solid Waste Facilities OLI Old Landfill Inventory DEBRIS Solid Waste Active Disaster Debris Sites Listing LCID Land-Clearing and Inert Debris (LCID) Landfill Notifications State and tribal leaking storage tank lists INDIAN LUST Leaking Underground Storage Tanks on Indian Land State and tribal registered storage tank lists FEMA UST Underground Storage Tank Listing AST AST Database INDIAN UST Underground Storage Tanks on Indian Land State and tribal voluntary cleanup sites VCP Responsible Party Voluntary Action Sites INDIAN VCP Voluntary Cleanup Priority Listing ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists US BROWNFIELDS A Listing of Brownfields Sites EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 5 Local Lists of Landfill / Solid Waste Disposal Sites SWRCY Recycling Center Listing HIST LF Solid Waste Facility Listing INDIAN ODI Report on the Status of Open Dumps on Indian Lands DEBRIS REGION 9 Torres Martinez Reservation Illegal Dump Site Locations ODI Open Dump Inventory IHS OPEN DUMPS Open Dumps on Indian Land Local Lists of Hazardous waste / Contaminated Sites US HIST CDL Delisted National Clandestine Laboratory Register US CDL National Clandestine Laboratory Register Local Land Records LIENS 2 CERCLA Lien Information Records of Emergency Release Reports HMIRS Hazardous Materials Information Reporting System SPILLS Spills Incident Listing SPILLS 90 SPILLS 90 data from FirstSearch SPILLS 80 SPILLS 80 data from FirstSearch Other Ascertainable Records FUDS Formerly Used Defense Sites DOD Department of Defense Sites SCRD DRYCLEANERS State Coalition for Remediation of Drycleaners Listing US FIN ASSUR Financial Assurance Information EPA WATCH LIST EPA WATCH LIST 2020 COR ACTION 2020 Corrective Action Program List TSCA Toxic Substances Control Act TRIS Toxic Chemical Release Inventory System SSTS Section 7 Tracking Systems ROD Records Of Decision RMP Risk Management Plans RAATS RCRA Administrative Action Tracking System PRP Potentially Responsible Parties PADS PCB Activity Database System ICIS Integrated Compliance Information System FTTS FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) MLTS Material Licensing Tracking System COAL ASH DOE Steam-Electric Plant Operation Data COAL ASH EPA Coal Combustion Residues Surface Impoundments List PCB TRANSFORMER PCB Transformer Registration Database RADINFO Radiation Information Database HIST FTTS FIFRA/TSCA Tracking System Administrative Case Listing DOT OPS Incident and Accident Data CONSENT Superfund (CERCLA) Consent Decrees INDIAN RESERV Indian Reservations FUSRAP Formerly Utilized Sites Remedial Action Program EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 6 UMTRA Uranium Mill Tailings Sites LEAD SMELTERS Lead Smelter Sites US AIRS Aerometric Information Retrieval System Facility Subsystem US MINES Mines Master Index File ABANDONED MINES Abandoned Mines UXO Unexploded Ordnance Sites DOCKET HWC Hazardous Waste Compliance Docket Listing FUELS PROGRAM EPA Fuels Program Registered Listing AIRS Air Quality Permit Listing ASBESTOS ASBESTOS COAL ASH Coal Ash Disposal Sites DRYCLEANERS Drycleaning Sites Financial Assurance Financial Assurance Information Listing NPDES NPDES Facility Location Listing UIC Underground Injection Wells Listing AOP Animal Operation Permits Listing PCSRP Petroleum-Contaminated Soil Remediation Permits SEPT HAULERS Permitted Septage Haulers Listing CCB Coal Ash Structural Fills (CCB) Listing EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR MGP EDR Proprietary Manufactured Gas Plants EDR Hist Cleaner EDR Exclusive Historical Cleaners EDR RECOVERED GOVERNMENT ARCHIVES Exclusive Recovered Govt. Archives RGA HWS Recovered Government Archive State Hazardous Waste Facilities List RGA LF Recovered Government Archive Solid Waste Facilities List RGA LUST Recovered Government Archive Leaking Underground Storage Tank SURROUNDING SITES: SEARCH RESULTS Surrounding sites were identified in the following databases. Elevations have been determined from the USGS Digital Elevation Model and should be evaluated on a relative (not an absolute) basis. Relative elevation information between sites of close proximity should be field verified. Sites with an elevation equal to or higher than the target property have been differentiated below from sites with an elevation lower than the target property. Page numbers and map identification numbers refer to the EDR Radius Map report where detailed data on individual sites can be reviewed. Sites listed in bold italics are in multiple databases. Unmappable (orphan) sites are not considered in the foregoing analysis. EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 7 STANDARD ENVIRONMENTAL RECORDS Federal RCRA generators list RCRA-CESQG: RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Conditionally exempt small quantity generators (CESQGs) generate less than 100 kg of hazardous waste, or less than 1 kg of acutely hazardous waste per month. A review of the RCRA-CESQG list, as provided by EDR, and dated 03/25/2019 has revealed that there is 1 RCRA-CESQG site within approximately 0.25 miles of the target property. PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____ CORE & MAIN, LP 1129 SWEETEN CREEK R S 0 - 1/8 (0.047 mi.) 5 13 EPA ID:: NC0991302874 State- and tribal - equivalent CERCLIS SHWS: The State Hazardous Waste Sites records are the states’ equivalent to CERCLIS. These sites may or may not already be listed on the federal CERCLIS list. Priority sites planned for cleanup using state funds (state equivalent of Superfund) are identified along with sites where cleanup will be paid for by potentially responsible parties. The data come from the Department of Environment & Natural Resources’ Inactive Hazardous Sites Program. A review of the SHWS list, as provided by EDR, and dated 02/08/2019 has revealed that there is 1 SHWS site within approximately 1 mile of the target property. PageMap IDDirection / Distance Address Lower Elevation ____________________ ________ ___________________ _____ _____ SMITH’S AEROSPACE 401 SWEETEN CREEK IN NNE 1/4 - 1/2 (0.325 mi.) 19 42 Facility Id: NONCD0001163 State and tribal leaking storage tank lists LAST: A listing of leaking aboveground storage tank site locations. A review of the LAST list, as provided by EDR, and dated 05/03/2019 has revealed that there are 2 LAST sites within approximately 0.5 miles of the target property. PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____ TUSKEEGEE CLEANERS F 20 ROBERSON AVE. NNW 1/4 - 1/2 (0.397 mi.) 22 48 Incident Number: 85893 Current Status: C WEST CHAPEL BALL FIE WEST CHAPEL BALL FIE E 1/4 - 1/2 (0.462 mi.) 23 51 Close Out: 02/23/1996 Incident Number: 12778 EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 8 Current Status: A LUST: The Leaking Underground Storage Tank Incidents Management Database contains an inventory of reported leaking underground storage tank incidents. The data come from the Department of Environment, & Natural Resources’ Incidents by Address. A review of the LUST list, as provided by EDR, and dated 05/03/2019 has revealed that there are 10 LUST sites within approximately 0.5 miles of the target property. PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____ PEPSI COLA CO P.O. BOX 5315 NE 1/4 - 1/2 (0.264 mi.) 13 28 Incident Number: 28101 Current Status: File Located in Archives FRESHWATER PROPERTY 523 CARIBOU ROAD NW 1/4 - 1/2 (0.276 mi.) 16 36 Incident Number: 28613 Current Status: File Located in House MARCY PROPERTY (LISA 60 IMPERIAL COURT WSW 1/4 - 1/2 (0.321 mi.) 18 41 Incident Phase: Closed Out Incident Number: 41485 Current Status: File Located in Archives FRANCES SUBER RESIDE 74 TAFT AVENUE WNW 1/4 - 1/2 (0.383 mi.) 21 46 Incident Phase: Closed Out Incident Number: 41090 Current Status: File Located in Archives PageMap IDDirection / Distance Address Lower Elevation ____________________ ________ ___________________ _____ _____ ROBERT TED YOUNG (TH 1085 SWEETEN CREEK R WSW 0 - 1/8 (0.016 mi.) A4 10 Incident Phase: Closed Out Incident Number: 22039 Current Status: File Located in House HOT SPOT #2003 1069 SWEETEN CREEK R NNW 0 - 1/8 (0.098 mi.) B7 15 Incident Phase: Closed Out Incident Number: 41100 Current Status: File Located in House UNITED PARCEL SERVIC 301 SWEETEN CREEK IN NNE 1/4 - 1/2 (0.269 mi.) C15 35 Incident Phase: Closed Out Incident Number: 11492 Current Status: File Located in House PEPSI WAREHOUSE 601 SWEETEN CREEK IN NE 1/4 - 1/2 (0.300 mi.) 17 38 Incident Phase: Closed Out Incident Number: 28537 Current Status: File Located in Archives FREDRICKSON MOTOR EX 502 SWEETEN CREEK IN NNE 1/4 - 1/2 (0.346 mi.) 20 43 Incident Phase: Closed Out Incident Number: 19012 Current Status: File Located in Archives BRUNNER AND LAY 150 SWEETEN CREEK RD N 1/4 - 1/2 (0.484 mi.) 24 54 Incident Phase: Closed Out Incident Number: 41172 EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 9 Current Status: File Located in Archives LUST TRUST: This database contains information about claims against the State Trust Funds for reimbursements for expenses incurred while remediating Leaking USTs. A review of the LUST TRUST list, as provided by EDR, and dated 04/05/2019 has revealed that there are 2 LUST TRUST sites within approximately 0.5 miles of the target property. PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____ FRESHWATER PROPERTY 523 CARIBOU ROAD NW 1/4 - 1/2 (0.276 mi.) 16 36 Site ID: 28613 FRANCES SUBER RESIDE 74 TAFT AVENUE WNW 1/4 - 1/2 (0.383 mi.) 21 46 Site ID: 41090 State and tribal registered storage tank lists UST: The Underground Storage Tank database contains registered USTs. USTs are regulated under Subtitle I of the Resource Conservation and Recovery Act (RCRA). The data come from the Department of Environment & Natural Resources’ Petroleum Underground Storage Tank Database. A review of the UST list, as provided by EDR, and dated 05/03/2019 has revealed that there are 3 UST sites within approximately 0.25 miles of the target property. PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____ SWEETEN CREEK QUALIT 1133 SWEETEN CREEK R S 0 - 1/8 (0.118 mi.) 9 19 Tank Status: Current Facility Id: 00-0-0000037117 FORMER PEPSI-COLA BU 601 SWEETEN CRK INDU W 1/8 - 1/4 (0.187 mi.) 11 24 Tank Status: Removed Facility Id: 00-0-0000021422 PageMap IDDirection / Distance Address Lower Elevation ____________________ ________ ___________________ _____ _____ HOT SPOT 2003 1069 SWEETEN CREEK R NNW 0 - 1/8 (0.098 mi.) B8 17 Tank Status: Current Facility Id: 00-0-0000007647 State and tribal institutional control / engineering control registries INST CONTROL: No Further Action Sites With Land Use Restrictions Monitoring. A review of the INST CONTROL list, as provided by EDR, and dated 12/19/2018 has revealed that there is 1 INST CONTROL site within approximately 0.5 miles of the target property. PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____ FRANCES SUBER RESIDE 74 TAFT AVENUE WNW 1/4 - 1/2 (0.383 mi.) 21 46 EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 10 ADDITIONAL ENVIRONMENTAL RECORDS Records of Emergency Release Reports IMD: Incident Management Database. A review of the IMD list, as provided by EDR, and dated 07/21/2006 has revealed that there are 6 IMD sites within approximately 0.5 miles of the target property. PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____ PEPSI COLA CO P.O. BOX 5315 NE 1/4 - 1/2 (0.264 mi.) 13 28 Facility Id: 28101 TUSKEEGEE CLEANERS F 20 ROBERSON AVE. NNW 1/4 - 1/2 (0.397 mi.) 22 48 Facility Id: 85893 WEST CHAPEL BALL FIE WEST CHAPEL BALL FIE E 1/4 - 1/2 (0.462 mi.) 23 51 Facility Id: 12778 PageMap IDDirection / Distance Address Lower Elevation ____________________ ________ ___________________ _____ _____ ROBERT TED YOUNG (TH 1085 SWEETEN CREEK R WSW 0 - 1/8 (0.016 mi.) A4 10 Facility Id: 22039 UNITED PARCEL SERVIC 301 SWEETEN CREEK RD NNE 1/4 - 1/2 (0.269 mi.) C14 31 Facility Id: 11492 Facility Id: 8255 FREDRICKSON MOTOR EX 502 SWEETEN CREEK IN NNE 1/4 - 1/2 (0.346 mi.) 20 43 Facility Id: 19012 Other Ascertainable Records RCRA NonGen / NLR: RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Non-Generators do not presently generate hazardous waste. A review of the RCRA NonGen / NLR list, as provided by EDR, and dated 03/25/2019 has revealed that there are 2 RCRA NonGen / NLR sites within approximately 0.25 miles of the target property. PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____ MACKS USED CAR & TRU 1191 SWEETEN CREEK R S 1/8 - 1/4 (0.248 mi.) 12 27 EPA ID:: NCS000001020 PageMap IDDirection / Distance Address Lower Elevation ____________________ ________ ___________________ _____ _____ STANLEY A BRIGGS INC 1026 SWEETEN CREEK R NNW 1/8 - 1/4 (0.152 mi.) 10 21 EPA ID:: NCD986229300 EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 11 EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR Hist Auto: EDR has searched selected national collections of business directories and has collected listings of potential gas station/filling station/service station sites that were available to EDR researchers. EDR’s review was limited to those categories of sources that might, in EDR’s opinion, include gas station/filling station/service station establishments. The categories reviewed included, but were not limited to gas, gas station, gasoline station, filling station, auto, automobile repair, auto service station, service station, etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR’s HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. A review of the EDR Hist Auto list, as provided by EDR, has revealed that there is 1 EDR Hist Auto site within approximately 0.125 miles of the target property. PageMap IDDirection / Distance Address Lower Elevation ____________________ ________ ___________________ _____ _____ JORDAN R L OIL CO OF 1069 SWEETEN CREEK R NNW 0 - 1/8 (0.098 mi.) B6 15 EXECUTIVE SUMMARY TC5716013.2s EXECUTIVE SUMMARY 12 There were no unmapped sites in this report. EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.212021602200 22002 160 22402 160 2280 2 20022002200 22402 0802080220023 20224022 80228028 0 22 4 0 2240276 2720224024332440 3 3 22400 03131 2 0 3 080304030002960 2920288028402800276027202680020802 0 80208 02080 2 080 2122120 2120 21202 1202120212021 202120 2 1202 12 0 21202120212021 20 2 1 602 1 6 0 2 1 6 0 21602160 2160216021602160 21 6021602 1 6 0 21 602 16 0216021602160 2160216022002 200 2200220022 00 220 02200220022002200220022002200220022002200 2 20 02 200 2240 224 0 2 2 4 022 40 2240 224022 40224 022402240 22 4 0 2240 228 0 22802 2 8 0 2282280 23202320 2320 236 02360 240 00 24 4024 8 2 52025602600264 EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc. 2 2002200208021202120 21602160 2160 2200 MAP FINDINGS SUMMARY Search TargetDistance Total Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted STANDARD ENVIRONMENTAL RECORDS Federal NPL site list 0 NR 0 0 0 0 1.000NPL 0 NR 0 0 0 0 1.000Proposed NPL 0 NR 0 0 0 0 1.000NPL LIENS Federal Delisted NPL site list 0 NR 0 0 0 0 1.000Delisted NPL Federal CERCLIS list 0 NR NR 0 0 0 0.500FEDERAL FACILITY 0 NR NR 0 0 0 0.500SEMS Federal CERCLIS NFRAP site list 0 NR NR 0 0 0 0.500SEMS-ARCHIVE Federal RCRA CORRACTS facilities list 0 NR 0 0 0 0 1.000CORRACTS Federal RCRA non-CORRACTS TSD facilities list 0 NR NR 0 0 0 0.500RCRA-TSDF Federal RCRA generators list 0 NR NR NR 0 0 0.250RCRA-LQG 0 NR NR NR 0 0 0.250RCRA-SQG 2 NR NR NR 0 1 0.250 1RCRA-CESQG Federal institutional controls / engineering controls registries 0 NR NR 0 0 0 0.500LUCIS 0 NR NR 0 0 0 0.500US ENG CONTROLS 0 NR NR 0 0 0 0.500US INST CONTROL Federal ERNS list 0 NR NR NR NR NR TPERNS State- and tribal - equivalent NPL 0 NR 0 0 0 0 1.000NC HSDS State- and tribal - equivalent CERCLIS 1 NR 0 1 0 0 1.000SHWS State and tribal landfill and/or solid waste disposal site lists 0 NR NR 0 0 0 0.500SWF/LF 0 NR NR 0 0 0 0.500OLI 0 NR NR 0 0 0 0.500DEBRIS 0 NR NR 0 0 0 0.500LCID TC5716013.2s Page 4 MAP FINDINGS SUMMARY Search TargetDistance Total Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted State and tribal leaking storage tank lists 2 NR NR 2 0 0 0.500LAST 10 NR NR 8 0 2 0.500LUST 0 NR NR 0 0 0 0.500INDIAN LUST 2 NR NR 2 0 0 0.500LUST TRUST State and tribal registered storage tank lists 0 NR NR NR 0 0 0.250FEMA UST 3 NR NR NR 1 2 0.250UST 0 NR NR NR 0 0 0.250AST 0 NR NR NR 0 0 0.250INDIAN UST State and tribal institutional control / engineering control registries 1 NR NR 1 0 0 0.500INST CONTROL State and tribal voluntary cleanup sites 0 NR NR 0 0 0 0.500VCP 0 NR NR 0 0 0 0.500INDIAN VCP State and tribal Brownfields sites 1 NR NR 0 0 0 0.500 1BROWNFIELDS ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists 0 NR NR 0 0 0 0.500US BROWNFIELDS Local Lists of Landfill / Solid Waste Disposal Sites 0 NR NR 0 0 0 0.500SWRCY 0 NR NR 0 0 0 0.500HIST LF 0 NR NR 0 0 0 0.500INDIAN ODI 0 NR NR 0 0 0 0.500DEBRIS REGION 9 0 NR NR 0 0 0 0.500ODI 0 NR NR 0 0 0 0.500IHS OPEN DUMPS Local Lists of Hazardous waste / Contaminated Sites 0 NR NR NR NR NR TPUS HIST CDL 0 NR NR NR NR NR TPUS CDL Local Land Records 0 NR NR NR NR NR TPLIENS 2 Records of Emergency Release Reports 0 NR NR NR NR NR TPHMIRS 0 NR NR NR NR NR TPSPILLS 6 NR NR 5 0 1 0.500IMD TC5716013.2s Page 5 MAP FINDINGS SUMMARY Search TargetDistance Total Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted 0 NR NR NR NR NR TPSPILLS 90 0 NR NR NR NR NR TPSPILLS 80 Other Ascertainable Records 2 NR NR NR 2 0 0.250RCRA NonGen / NLR 0 NR 0 0 0 0 1.000FUDS 0 NR 0 0 0 0 1.000DOD 0 NR NR 0 0 0 0.500SCRD DRYCLEANERS 0 NR NR NR NR NR TPUS FIN ASSUR 0 NR NR NR NR NR TPEPA WATCH LIST 0 NR NR NR 0 0 0.2502020 COR ACTION 0 NR NR NR NR NR TPTSCA 0 NR NR NR NR NR TPTRIS 0 NR NR NR NR NR TPSSTS 0 NR 0 0 0 0 1.000ROD 0 NR NR NR NR NR TPRMP 0 NR NR NR NR NR TPRAATS 0 NR NR NR NR NR TPPRP 0 NR NR NR NR NR TPPADS 0 NR NR NR NR NR TPICIS 0 NR NR NR NR NR TPFTTS 0 NR NR NR NR NR TPMLTS 0 NR NR NR NR NR TPCOAL ASH DOE 0 NR NR 0 0 0 0.500COAL ASH EPA 0 NR NR NR NR NR TPPCB TRANSFORMER 0 NR NR NR NR NR TPRADINFO 0 NR NR NR NR NR TPHIST FTTS 0 NR NR NR NR NR TPDOT OPS 0 NR 0 0 0 0 1.000CONSENT 0 NR 0 0 0 0 1.000INDIAN RESERV 0 NR 0 0 0 0 1.000FUSRAP 0 NR NR 0 0 0 0.500UMTRA 0 NR NR NR NR NR TPLEAD SMELTERS 0 NR NR NR NR NR TPUS AIRS 0 NR NR NR 0 0 0.250US MINES 0 NR NR NR 0 0 0.250ABANDONED MINES 1 NR NR NR NR NR TP 1FINDS 1 NR NR NR NR NR TP 1ECHO 0 NR 0 0 0 0 1.000UXO 0 NR NR NR NR NR TPDOCKET HWC 0 NR NR NR 0 0 0.250FUELS PROGRAM 0 NR NR NR NR NR TPAIRS 0 NR NR NR NR NR TPASBESTOS 0 NR NR 0 0 0 0.500COAL ASH 0 NR NR NR 0 0 0.250DRYCLEANERS 0 NR NR NR NR NR TPFinancial Assurance 0 NR NR NR NR NR TPNPDES 0 NR NR NR NR NR TPUIC 0 NR NR NR NR NR TPAOP 0 NR NR 0 0 0 0.500PCSRP 0 NR NR NR NR NR TPSEPT HAULERS TC5716013.2s Page 6 MAP FINDINGS SUMMARY Search TargetDistance Total Database Property(Miles) < 1/8 1/8 - 1/4 1/4 - 1/2 1/2 - 1 > 1 Plotted 0 NR NR 0 0 0 0.500CCB EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records 0 NR 0 0 0 0 1.000EDR MGP 1 NR NR NR NR 1 0.125EDR Hist Auto 0 NR NR NR NR 0 0.125EDR Hist Cleaner EDR RECOVERED GOVERNMENT ARCHIVES Exclusive Recovered Govt. Archives 0 NR NR NR NR NR TPRGA HWS 0 NR NR NR NR NR TPRGA LF 0 NR NR NR NR NR TPRGA LUST 33 0 0 19 3 7 4- Totals -- NOTES: TP = Target Property NR = Not Requested at this Search Distance Sites may be listed in more than one database TC5716013.2s Page 7 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 671356.94619Y Coord: 952822.79359X Coord: 12/26/2018Status Date: 1.63BF Acreage: Cody CannonBF Manager: 22081-18-011Project ID: PendingProject Type: BROWNFIELDS: Site 1 of 4 in cluster A Actual: 2119 ft. Property ASHEVILLE, NC Target 1140 SWEETEN CREEK ROAD N/A A1 BROWNFIELDSFORMER PE VALVE MANUFACTURING S123565579 Not reportedOwner/operator email: 828-684-1234Owner/operator telephone: Not reportedOwner/operator country: ARDEN, NC 28704 100 AIRPORT RDOwner/operator address: PETER HALLOwner/operator name: Owner/Operator Summary: hazardous waste the cleanup of a spill, into or on any land or water, of acutely any residue or contaminated soil, waste or other debris resulting from time: 1 kg or less of acutely hazardous waste; or 100 kg or less of hazardous waste during any calendar month, and accumulates at any from the cleanup of a spill, into or on any land or water, of acutely of any residue or contaminated soil, waste or other debris resulting land or water, of acutely hazardous waste; or generates 100 kg or less other debris resulting from the cleanup of a spill, into or on any waste; or 100 kg or less of any residue or contaminated soil, waste or month, and accumulates at any time: 1 kg or less of acutely hazardous or generates 1 kg or less of acutely hazardous waste per calendar month, and accumulates 1000 kg or less of hazardous waste at any time; Handler: generates 100 kg or less of hazardous waste per calendarDescription: Conditionally Exempt Small Quantity GeneratorClassification: 04EPA Region: Not reportedContact email: 828-274-1286Contact telephone: USContact country: ASHEVILLE, NC 28813 PO BOX 15369Contact address: DEAN DIXONContact: ASHEVILLE, NC 28813 PO BOX 15369Mailing address: NCD982130825EPA ID: ASHEVILLE, NC 28803 1140 SWEETEN CREEK RDFacility address: PE VALVE COFacility name: 01/11/2000Date form received by agency: RCRA-CESQG: Site 2 of 4 in cluster A Actual: 2119 ft. Property ASHEVILLE, NC 28803 Target 1140 SWEETEN CREEK RD NCD982130825 A2 RCRA-CESQGPE VALVE CO 1004745516 TC5716013.2s Page 8 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation No violations foundViolation Status: IGNITABLE WASTE. Waste name: D001. Waste code: Hazardous Waste Summary: NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste: Handler Activities Summary: Not reportedOwner/Op end date: Not reportedOwner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator extension: Not reportedOwner/operator fax: PE VALVE CO (Continued)1004745516 http://echo.epa.gov/detailed-facility-report?fid=110004034152DFR URL: 110004034152Registry ID: 1016606643Envid: ECHO: additional FINDS: detail in the EDR Site Report. Click this hyperlink while viewing on your computer to access corrective action activities required under RCRA. program staff to track the notification, permit, compliance, and and treat, store, or dispose of hazardous waste. RCRAInfo allows RCRA events and activities related to facilities that generate, transport, Conservation and Recovery Act (RCRA) program through the tracking of RCRAInfo is a national information system that supports the Resource Environmental Interest/Information System 110004034152Registry ID: FINDS: Site 3 of 4 in cluster A Actual: 2119 ft. Property ASHEVILLE, NC 28803 Target ECHO1140 SWEETEN CREEK RD N/A A3 FINDSPE VALVE CO 1016606643 TC5716013.2s Page 9 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedRP Address: Not reportedTelephone: Not reportedContact Person: Not reportedCompany: ASHRegion: DPMRegional Officer Project Mgr: Not reportedTestlat: 35.5439 -82.5217Lat/Long Decimal: FalseValid: Not reportedError Code: 0Error Flag: FalseRPOP: FalseRPOW: 0Reel Num: 0CD Num: FalseRPL: 3PETOPT: Not reportedRBCA GW: File Located in HouseCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: YesFlag: UnknownMTBE1: NoMTBE: ResidentialLand Use: Not reportedSite Risk Reason: Not reportedPhase Of LSA Req: Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: COMMERCIALCommercial/NonCommercial UST Site: 0# Of Supply Wells: RTank Regulated Status: Industrial/CommercialLevel Of Soil Cleanup Achieved: 01/14/2019Close Out: Not reportedClosure Request: 02/23/2001Cleanup: 12/10/1997Date Occur: 01/29/1998Date Reported: PProduct Type: Leak-undergroundSource Type: GWContamination Type: 22039Incident Number: AS-1873UST Number: Not reportedFacility ID: ASHEVILLE, NC 28803-City,State,Zip: 1085 SWEETEN CREEK ROADAddress: ROBERT TED YOUNG (THE APPLIANCE HUT)Name: LUST: 83 ft. Site 4 of 4 in cluster A 0.016 mi. Relative: Lower Actual: 2115 ft. < 1/8 ASHEVILLE, NC 28803 WSW IMD1085 SWEETEN CREEK ROAD N/A A4 LUSTROBERT TED YOUNG (THE APPLIANCE HUT) S104914218 TC5716013.2s Page 10 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 2019-01-14 00:00:00Last Modified: Not reportedUst Number: Not reportedSource: Not reportedCause: Not reportedErr Type: MIN_SOILSource Code: N86L5PRelease Code: ASHEVILPirf/Min Soil: 25 Minute Quad: 47#5 Minute Quad: Not reportedSamples Include: NWells Affected Y/N: 2000-08-03 00:00:00Priority Update: LSite Priority: 1Location: 3Type: 6Operation Type: 4Ownership: ROBERT TED YOUNG/ RUBY YOUNGOwner/Operator: MG/KG : 3550 IDENTIFIED. SOIL SAMP INDICATED TPH-GRO 18MG/KG: 5030, TPH-DRO 125 DURING GEOPHYSICAL ASSESS CONDUCTED BY RUST. UST POSSIBLY WASDescription Of Incident: 2000-07-11 00:00:00Date Reported: 1997-12-10 00:00:00Date Occurred: 22039Facility Id: PIRF: Not reported5 Min Quad: with a note to the file on 01/14/2019. specific information, NFA status was assigned and the incident closed DOT roadway expansion. No wells in the area. Due to this site 1/14/2019. Incident closed. Low level soil contamination exists under Site changed to "low" on 03/29/2005 following site visit DPM. determiend to be > TPH (Y-1 = DRO @ 22 mg/kg, Y-2= GRO @130 mg/kg). along ROW. Soils along ROW/along front of building were excavated and identified. Soil excataion and test pits conducted (34.36 tons total) following GPR. Possibly a former gas station as 2 product lines 03/27/01- Pre-liminary Site Assessment: Possible UST identified 1,3,5-trimethylbenzene @380 ug/L and total xylenes @14400 ug/L. @530 ug/L, toluene @ 4200 ug/L, 1,2,4-trimethylbenzene @2400 ug/L, p-isopropyltoluene @430 ug/L, naphthalene @ 200 ug/L, n-propylbenzene diisopropylether @ 220 ug/L, Ethylbenzene @3000 ug/L, mg/kg in C-4. TW installed in boring C-1 > 2L (benzene @120 ug/L, at 12’ bls. TPH GRO @ 18 mg/kg in C-2A, DRO @ 92 mg/kg (C-1) and 125 registered. 6 borings advanced from 1.5’ to 16’ bls. GW envountered identified in the SW corner of the building. Tanks were not USTs were identified in the front of the building. Fill port was Assessment for NCDOT. Two vent pipes and 2 anomalies consistent with CONDUCTED SITE VISIT 7/10/2000. 01/20/98: Pre-liminary Site ****ALL FILES UPLOADED TO G&S Laserfiche for processing**** DEWComments: Not reportedRP County: Not reportedRP City,St,Zip: ROBERT TED YOUNG (THE APPLIANCE HUT) (Continued) S104914218 TC5716013.2s Page 11 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedLast Modified: 22039Facility ID: DWMAgency: NODGPS: 82.5225Longitude Decimal: 35.5436111111111Latitude Decimal: 823121Longitude Number: 353237Latitude Number: -82.5225Longitude: 35.54361111Latitude: N86L5P5 Min Quad: ASHEVIL7.5 Min Quad: Soil SamplesSamples Include: OtherSampled By: Not reportedWells Contam: Not reportedNum Affected: NoWells Affected: DPMDem Contact: 8/3/2000Priority Update: LPriority Code: LSite Priority: LRisk Site: UrbanSetting: FacilityLocation: Gasoline/dieselType: Leak-undergroundSource: Not reportedQty Recovered: UNKNOWNQty Lost: DIESELMaterial: Not reportedQty Recovered 1: Not reportedQty Lost 1: GASOLINEMaterial: CommercialOperation: PrivateOwnership: Not reportedOper City,St,Zip: Not reportedOperator City: Not reportedOperator Address: Not reportedOwner Company: Not reportedContact Phone: Not reportedOperator: MG/KG : 3550 IDENTIFIED. SOIL SAMP INDICATED TPH-GRO 18MG/KG: 5030, TPH-DRO 125 DURING GEOPHYSICAL ASSESS CONDUCTED BY RUST. UST POSSIBLY WASIncident Desc: YesSoil Contam: No Groundwater Contamination detectedGW Contam: 7/11/2000Submit Date: 12/10/1997Date Occurred: 22039Facility ID: ASHRegion: IMD: Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: ROBERT TED YOUNG (THE APPLIANCE HUT) (Continued) S104914218 TC5716013.2s Page 12 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Sighned: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: REIncident Phase: ROBERT TED YOUNG (THE APPLIANCE HUT) (Continued) S104914218 Not reportedOwner/operator email: 828-274-4111Owner/operator telephone: USOwner/operator country: ASHEVILLE, NC 28803 HENDERSONVILLE ROAD SUITE 201Owner/operator address: M REALTYOwner/operator name: Owner/Operator Summary: hazardous waste the cleanup of a spill, into or on any land or water, of acutely any residue or contaminated soil, waste or other debris resulting from time: 1 kg or less of acutely hazardous waste; or 100 kg or less of hazardous waste during any calendar month, and accumulates at any from the cleanup of a spill, into or on any land or water, of acutely of any residue or contaminated soil, waste or other debris resulting land or water, of acutely hazardous waste; or generates 100 kg or less other debris resulting from the cleanup of a spill, into or on any waste; or 100 kg or less of any residue or contaminated soil, waste or month, and accumulates at any time: 1 kg or less of acutely hazardous or generates 1 kg or less of acutely hazardous waste per calendar month, and accumulates 1000 kg or less of hazardous waste at any time; Handler: generates 100 kg or less of hazardous waste per calendarDescription: Conditionally Exempt Small Quantity GeneratorClassification: 04EPA Region: KAREN.KERN@COREANDMAIN.COMContact email: 215-651-2960Contact telephone: USContact country: ST. LOUIS, MO 63146 CRAIG PARK COURTContact address: KAREN KERNContact: ST. LOUIS, MO 63146 CRAIG PARK COURTMailing address: NC0991302874EPA ID: ASHEVILLE, NC 28803 1129 SWEETEN CREEK RDFacility address: CORE & MAIN, LPFacility name: 09/27/2017Date form received by agency: RCRA-CESQG: 250 ft. 0.047 mi. Relative: Higher Actual: 2128 ft. < 1/8 ASHEVILLE, NC 28803 South 1129 SWEETEN CREEK RD NC0991302874 5 RCRA-CESQGCORE & MAIN, LP 1010323089 TC5716013.2s Page 13 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation D002. Waste code: IGNITABLE WASTE. Waste name: D001. Waste code: Hazardous Waste Summary: Conditionally Exempt Small Quantity GeneratorClassification: HD SUPPLY WATER WORKS - WW 0170Site name: 01/19/2007Date form received by agency: Conditionally Exempt Small Quantity GeneratorClassification: HD SUPPLY WATER WORKS - WW 0170Site name: 10/04/2007Date form received by agency: Not a generator, verifiedClassification: HD SUPPLY WATERWORKS LTD (WW0170)Site name: 07/28/2008Date form received by agency: Historical Generators: NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste: Handler Activities Summary: Not reportedOwner/Op end date: 09/27/2017Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator extension: Not reportedOwner/operator fax: Not reportedOwner/operator email: Not reportedOwner/operator telephone: Not reportedOwner/operator country: Not reported Not reportedOwner/operator address: CORE & MAIN, LPOwner/operator name: Not reportedOwner/Op end date: 04/28/2006Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator extension: Not reportedOwner/operator fax: CORE & MAIN, LP (Continued)1010323089 TC5716013.2s Page 14 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation No violations foundViolation Status: METHYL ETHYL KETONE. Waste name: D035. Waste code: BENZENE. Waste name: D018. Waste code: MERCURY. Waste name: D009. Waste code: CORROSIVE WASTE. Waste name: CORE & MAIN, LP (Continued)1010323089 Gasoline Service Stations2014 JORDAN R L OIL CO OF NC Gasoline Service Stations2013 JORDAN R L OIL CO OF NC Gasoline Service Stations2012 JORDAN R L OIL CO OF NC Gasoline Service Stations2011 JORDAN R L OIL CO OF NC Gasoline Service Stations2010 JORDAN R L OIL CO OF NC Gasoline Service Stations2009 JORDAN R L OIL CO OF NC Gasoline Service Stations2008 JORDAN R L OIL CO OF NC INC Gasoline Service Stations2007 JORDAN R L OIL CO OF NC INC Gasoline Service Stations2006 JORDAN R L OIL CO OF NC Gasoline Service Stations2005 JORDAN R L OIL CO OF NC Gasoline Service Stations2004 JORDAN R L OIL CO OF NC Gasoline Service Stations2003 JORDAN R L OIL CO OF NC Gasoline Service Stations2002 JORDAN R L OIL CO OF NC Gasoline Service Stations2001 JORDAN R L OIL CO OF NC Gasoline Service Stations2000 JORDAN R L OIL CO OF NC Type:Year: Name: EDR Hist Auto 520 ft. Site 1 of 3 in cluster B 0.098 mi. Relative: Lower Actual: 2101 ft. < 1/8 ASHEVILLE, NC 28803 NNW 1069 SWEETEN CREEK RD N/A B6 EDR Hist AutoJORDAN R L OIL CO OF NC 1020206850 04/10/2013Cleanup: 03/29/2013Date Occur: 04/11/2013Date Reported: PProduct Type: Leak-undergroundSource Type: SLContamination Type: 41100Incident Number: AS-3991UST Number: 00-0-000Facility ID: ASHEVILLE, NC 28803City,State,Zip: 1069 SWEETEN CREEK ROADAddress: HOT SPOT #2003Name: LUST: 520 ft. Site 2 of 3 in cluster B 0.098 mi. Relative: Lower Actual: 2101 ft. < 1/8 ASHEVILLE, NC 28803 NNW 1069 SWEETEN CREEK ROAD N/A B7 LUSTHOT SPOT #2003 S113486672 TC5716013.2s Page 15 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedPriority Update: Not reportedSite Priority: 1Location: 3Type: 6Operation Type: 4Ownership: Not reportedOwner/Operator: Soil samples collected adj to sumps. Soils > TPH DRO (7.6 mg/kg).Description Of Incident: 2013-04-11 00:00:00Date Reported: 2013-03-29 00:00:00Date Occurred: 41100Facility Id: PIRF: Not reported5 Min Quad: > TPH DRO (7.6 mg/kg). Recommends NFA. 04/11/13 - Site Check Rpt: Soil samples collected adj to sumps. SoilsComments: Not reportedRP County: Spartanburg, SC 29304RP City,St,Zip: P. O. Box 2527RP Address: Not reportedTelephone: Cyndi SuttlesContact Person: Jordan Oil Company of NC, IncCompany: ASHRegion: CELRegional Officer Project Mgr: Not reportedTestlat: 35.5453 -82.5222Lat/Long Decimal: FalseValid: NError Code: 0Error Flag: TrueRPOP: TrueRPOW: 0Reel Num: 655CD Num: FalseRPL: 3PETOPT: Not reportedRBCA GW: File Located in HouseCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: YesFlag: UnknownMTBE1: NoMTBE: ResidentialLand Use: Not reportedSite Risk Reason: 1Phase Of LSA Req: Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: COMMERCIALCommercial/NonCommercial UST Site: 0# Of Supply Wells: RTank Regulated Status: Soil to GroundwaterLevel Of Soil Cleanup Achieved: 05/08/2013Close Out: Not reportedClosure Request: HOT SPOT #2003 (Continued)S113486672 TC5716013.2s Page 16 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 2013-05-08 00:00:00Last Modified: PUst Number: ASource: 7Cause: 1Err Type: Not reportedSource Code: Not reportedRelease Code: Not reportedPirf/Min Soil: Not reported5 Minute Quad: Y7#5 Minute Quad: Not reportedSamples Include: NWells Affected Y/N: HOT SPOT #2003 (Continued)S113486672 Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: 0Manifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 10000Tank Capacity: Gasoline, Gas MixProduct Name: Not reportedPerm Close Date: 04/26/1964Installed Date: CurrentTank Status: 1Tank Id: -82.52225Longitude: 35.54539Latitude: BuncombeFIPS County Desc: SPARTANBURG, SC 29304-2527Contact City/State/Zip: Not reportedContact Address2: P O BOX 2527Contact Address1: R.L. JORDAN OIL COMPANY OF NORTH CAROLINA, INC.Contact: 00-0-0000007647Facility Id: ASHEVILLE, NC 28803City,State,Zip: 1069 SWEETEN CREEK ROADAddress: HOT SPOT 2003Name: UST: 520 ft. Site 3 of 3 in cluster B 0.098 mi. Relative: Lower Actual: 2101 ft. < 1/8 ASHEVILLE, NC 28803 NNW 1069 SWEETEN CREEK ROAD N/A B8 USTHOT SPOT 2003 U000824024 TC5716013.2s Page 17 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation NoMain Tank: Not reportedRoot Tank Id: 4000Tank Capacity: Kerosene, Kero MixProduct Name: Not reportedPerm Close Date: 04/26/1964Installed Date: CurrentTank Status: 4Tank Id: UnknownDecode for PSYS_KEY: OtherDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: Not reportedLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: 0Manifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 10000Tank Capacity: Gasoline, Gas MixProduct Name: Not reportedPerm Close Date: 04/26/1964Installed Date: CurrentTank Status: 3Tank Id: UnknownDecode for PSYS_KEY: OtherDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: Not reportedLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: 0Manifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 10000Tank Capacity: Gasoline, Gas MixProduct Name: Not reportedPerm Close Date: 04/26/1964Installed Date: CurrentTank Status: 2Tank Id: UnknownDecode for PSYS_KEY: OtherDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: Not reportedLeak Detection Name: Catchment BasinSpill Protection Name: HOT SPOT 2003 (Continued)U000824024 TC5716013.2s Page 18 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation UnknownDecode for PSYS_KEY: OtherDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: Not reportedLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: 0Manifold Tank: NoCompartment Tank: HOT SPOT 2003 (Continued)U000824024 12000Tank Capacity: Gasoline, Gas MixProduct Name: Not reportedPerm Close Date: 11/11/2010Installed Date: CurrentTank Status: 2Tank Id: Pressurized SystemDecode for PSYS_KEY: Double Wall FRPDecode for PCONS_KEY: Double Wall FRPDecode for TCONS_KEY: Not reportedLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: 0Manifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 20000Tank Capacity: Gasoline, Gas MixProduct Name: Not reportedPerm Close Date: 11/11/2010Installed Date: CurrentTank Status: 1Tank Id: -82.52127Longitude: 35.54148Latitude: BuncombeFIPS County Desc: WINSTON SALEM, NC 27102-2736Contact City/State/Zip: Not reportedContact Address2: PO BOX 2736/1540 SILAS CREEK PKYContact Address1: QUALITY OIL COMPANY, LLCContact: 00-0-0000037117Facility Id: ASHEVILLE, NC 28803City,State,Zip: 1133 SWEETEN CREEK ROADAddress: SWEETEN CREEK QUALITY PLUSName: UST: 622 ft. 0.118 mi. Relative: Higher Actual: 2124 ft. < 1/8 ASHEVILLE, NC 28803 South Financial Assurance1133 SWEETEN CREEK ROAD N/A 9 USTSWEETEN CREEK QUALITY PLUS U004158470 TC5716013.2s Page 19 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Pressurized SystemDecode for PSYS_KEY: Double Wall FRPDecode for PCONS_KEY: Double Wall FRPDecode for TCONS_KEY: Not reportedLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: 0Manifold Tank: YesCompartment Tank: NoMain Tank: 248454Root Tank Id: 3000Tank Capacity: Kerosene, Kero MixProduct Name: Not reportedPerm Close Date: 11/11/2010Installed Date: CurrentTank Status: 3BTank Id: Pressurized SystemDecode for PSYS_KEY: Double Wall FRPDecode for PCONS_KEY: Double Wall FRPDecode for TCONS_KEY: Not reportedLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: 0Manifold Tank: YesCompartment Tank: YesMain Tank: 248454Root Tank Id: 12000Tank Capacity: DieselProduct Name: Not reportedPerm Close Date: 11/11/2010Installed Date: CurrentTank Status: 3ATank Id: Pressurized SystemDecode for PSYS_KEY: Double Wall FRPDecode for PCONS_KEY: Double Wall FRPDecode for TCONS_KEY: Not reportedLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: 0Manifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: SWEETEN CREEK QUALITY PLUS (Continued) U004158470 TC5716013.2s Page 20 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 04/30/2013Ended Date: 05/01/2012Started Date: Quality Oil Company, LLCFinancial Responsibility Name: Self-InsuranceFinancial Responsibility Desc: 1Region: 00-0-0000037117Facility ID: ASHEVILLE, NC 28803City,State,Zip: 1133 SWEETEN CREEK ROADAddress: SWEETEN CREEK QUALITY PLUSName: NC Financial Assurance 1: SWEETEN CREEK QUALITY PLUS (Continued) U004158470 NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste: Handler Activities Summary: Not reportedOwner/Op end date: Not reportedOwner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator extension: Not reportedOwner/operator fax: Not reportedOwner/operator email: 828-274-0441Owner/operator telephone: Not reportedOwner/operator country: ASHEVILLE, NC 28803 1026 SWEETEN CREEK RDOwner/operator address: STANLEY A BRIGGSOwner/operator name: Owner/Operator Summary: Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: PrivateLand type: 04EPA Region: Not reportedContact email: 828-274-0441Contact telephone: USContact country: ASHEVILLE, NC 28803 SWEETEN CREEK RDContact address: STANLEY BRIGGSContact: ASHEVILLE, NC 28803 SWEETEN CREEK RDMailing address: NCD986229300EPA ID: ASHEVILLE, NC 28803 1026 SWEETEN CREEK RDFacility address: STANLEY A BRIGGS INCFacility name: 06/23/2015Date form received by agency: RCRA NonGen / NLR: 801 ft. 0.152 mi. Relative: Lower Actual: 2106 ft. 1/8-1/4 ASHEVILLE, NC 28803 NNW 1026 SWEETEN CREEK RD NCD986229300 10 RCRA NonGen / NLRSTANLEY A BRIGGS INC 1000832123 TC5716013.2s Page 21 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation SR - 130A-294-1Regulation violated: Facility Has Received Notices of Violations: THESE SPENT SOLVENTS AND SPENT SOLVENT MIXTURES. LISTED IN F001, F002, OR F004; AND STILL BOTTOMS FROM THE RECOVERY OF ONE OR MORE OF THE ABOVE NONHALOGENATED SOLVENTS OR THOSE SOLVENTS CONTAINING, BEFORE USE, A TOTAL OF TEN PERCENT OR MORE (BY VOLUME) OF 2-ETHOXYETHANOL, AND 2-NITROPROPANE; ALL SPENT SOLVENT MIXTURES/BLENDS KETONE, CARBON DISULFIDE, ISOBUTANOL, PYRIDINE, BENZENE, THE FOLLOWING SPENT NONHALOGENATED SOLVENTS: TOLUENE, METHYL ETHYL. Waste name: F005. Waste code: MIXTURES. BOTTOMS FROM THE RECOVERY OF THESE SPENT SOLVENTS AND SPENT SOLVENT MORE OF THOSE SOLVENTS LISTED IN F001, F002, F004, AND F005; AND STILL SOLVENTS, AND A TOTAL OF TEN PERCENT OR MORE (BY VOLUME) OF ONE OR CONTAINING, BEFORE USE, ONE OR MORE OF THE ABOVE NONHALOGENATED NONHALOGENATED SOLVENTS; AND ALL SPENT SOLVENT MIXTURES/BLENDS MIXTURES/BLENDS CONTAINING, BEFORE USE, ONLY THE ABOVE SPENT ALCOHOL, CYCLOHEXANONE, AND METHANOL; ALL SPENT SOLVENT ACETATE, ETHYL BENZENE, ETHYL ETHER, METHYL ISOBUTYL KETONE, N-BUTYL THE FOLLOWING SPENT NONHALOGENATED SOLVENTS: XYLENE, ACETONE, ETHYL. Waste name: F003. Waste code: SPENT SOLVENT MIXTURES. F005; AND STILL BOTTOMS FROM THE RECOVERY OF THESE SPENT SOLVENTS AND ABOVE HALOGENATED SOLVENTS OR THOSE SOLVENTS LISTED IN F001, F004, AND USE, A TOTAL OF TEN PERCENT OR MORE (BY VOLUME) OF ONE OR MORE OF THE TRICHLOROETHANE; ALL SPENT SOLVENT MIXTURES/BLENDS CONTAINING, BEFORE ORTHO-DICHLOROBENZENE, TRICHLOROFLUOROMETHANE, AND 1,1,2, CHLOROBENZENE, 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE, METHYLENE CHLORIDE, TRICHLOROETHYLENE, 1,1,1-TRICHLOROETHANE, THE FOLLOWING SPENT HALOGENATED SOLVENTS: TETRACHLOROETHYLENE,. Waste name: F002. Waste code: Hazardous Waste Summary: Small Quantity GeneratorClassification: STANLEY A BRIGGS INCSite name: 11/23/1992Date form received by agency: Small Quantity GeneratorClassification: STANLEY A BRIGGS INCSite name: 12/12/2000Date form received by agency: Historical Generators: NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: STANLEY A BRIGGS INC (Continued) 1000832123 TC5716013.2s Page 22 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Generators - GeneralArea of violation: FOLLOW-UP INSPECTIONEvaluation: 11/23/1994Evaluation date: StateEvaluation lead agency: Not reportedDate achieved compliance: Not reportedArea of violation: COMPLIANCE SCHEDULE EVALUATIONEvaluation: 12/02/1994Evaluation date: StateEvaluation lead agency: Not reportedDate achieved compliance: Not reportedArea of violation: COMPLIANCE EVALUATION INSPECTION ON-SITEEvaluation: 07/14/2004Evaluation date: Evaluation Action Summary: Not reported Paid penalty amount: Not reported Final penalty amount: Not reported Proposed penalty amount: State Enforcement lead agency: Not reported Enf. disp. status date: Not reported Enf. disposition status: 07/28/1992 Enforcement action date: WRITTEN INFORMAL Enforcement action: StateViolation lead agency: 12/16/1992Date achieved compliance: 07/28/1992Date violation determined: Generators - GeneralArea of violation: SR - 262.11,262.12Regulation violated: Not reported Paid penalty amount: Not reported Final penalty amount: Not reported Proposed penalty amount: State Enforcement lead agency: Not reported Enf. disp. status date: Not reported Enf. disposition status: 07/28/1992 Enforcement action date: WRITTEN INFORMAL Enforcement action: StateViolation lead agency: 12/16/1992Date achieved compliance: 07/28/1992Date violation determined: Generators - GeneralArea of violation: SR - 15A NCAC 13A .0009(a)Regulation violated: Not reported Paid penalty amount: Not reported Final penalty amount: Not reported Proposed penalty amount: State Enforcement lead agency: Not reported Enf. disp. status date: Not reported Enf. disposition status: 11/23/1994 Enforcement action date: VERBAL INFORMAL Enforcement action: StateViolation lead agency: 12/02/1994Date achieved compliance: 11/23/1994Date violation determined: Generators - GeneralArea of violation: STANLEY A BRIGGS INC (Continued) 1000832123 TC5716013.2s Page 23 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation StateEvaluation lead agency: Not reportedDate achieved compliance: Not reportedArea of violation: COMPLIANCE EVALUATION INSPECTION ON-SITEEvaluation: 07/28/1992Evaluation date: StateEvaluation lead agency: 12/16/1992Date achieved compliance: Generators - GeneralArea of violation: COMPLIANCE SCHEDULE EVALUATIONEvaluation: 01/05/1993Evaluation date: StateEvaluation lead agency: 12/02/1994Date achieved compliance: STANLEY A BRIGGS INC (Continued) 1000832123 11/04/1991Perm Close Date: 12/20/1976Installed Date: RemovedTank Status: 2Tank Id: UnknownDecode for PSYS_KEY: UnknownDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: UnknownSpill Protection Name: UnknownOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 8000Tank Capacity: DieselProduct Name: 11/30/1991Perm Close Date: 12/20/1976Installed Date: RemovedTank Status: 1Tank Id: -82.51756Longitude: 35.54689Latitude: BuncombeFIPS County Desc: ASHEVILLE, NC 28803-1733Contact City/State/Zip: Not reportedContact Address2: 932 HENDERSONVILLE ROADContact Address1: M REALTY LLCContact: 00-0-0000021422Facility Id: ASHEVILLE, NC 28813City,State,Zip: 601 SWEETEN CRK INDUSTRIAL PARKAddress: FORMER PEPSI-COLA BUILDINGName: UST: 987 ft. 0.187 mi. Relative: Higher Actual: 2182 ft. 1/8-1/4 ASHEVILLE, NC 28813 West 601 SWEETEN CRK INDUSTRIAL PARK N/A 11 USTFORMER PEPSI-COLA BUILDING U001199836 TC5716013.2s Page 24 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation UnknownDecode for PSYS_KEY: OtherDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: Catchment BasinSpill Protection Name: Overfill AlarmOverfill Protection Name: Not reportedOther CP Tank: NoRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 5000Tank Capacity: Heating Oil/FuelProduct Name: 08/16/2001Perm Close Date: 01/01/1987Installed Date: RemovedTank Status: 4Tank Id: European SuctionDecode for PSYS_KEY: OtherDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 3000Tank Capacity: Gasoline, Gas MixProduct Name: 10/25/2006Perm Close Date: 01/01/1987Installed Date: RemovedTank Status: 3Tank Id: UnknownDecode for PSYS_KEY: UnknownDecode for PCONS_KEY: Single Wall SteelDecode for TCONS_KEY: UnknownLeak Detection Name: UnknownSpill Protection Name: UnknownOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 3000Tank Capacity: Gasoline, Gas MixProduct Name: FORMER PEPSI-COLA BUILDING (Continued) U001199836 TC5716013.2s Page 25 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: NoRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 6000Tank Capacity: Heating Oil/FuelProduct Name: 11/02/2010Perm Close Date: 10/01/2001Installed Date: RemovedTank Status: A2Tank Id: Pressurized SystemDecode for PSYS_KEY: Single Wall FRPDecode for PCONS_KEY: Single Wall Steel/FRPDecode for TCONS_KEY: MLLDLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 10000Tank Capacity: DieselProduct Name: 10/25/2006Perm Close Date: 10/01/2001Installed Date: RemovedTank Status: A1Tank Id: UnknownDecode for PSYS_KEY: Single Wall FRPDecode for PCONS_KEY: Single Wall FRPDecode for TCONS_KEY: UnknownLeak Detection Name: Catchment BasinSpill Protection Name: Ball Float ValveOverfill Protection Name: Not reportedOther CP Tank: YesRegulated: YesCommercial: Not reportedManifold Tank: NoCompartment Tank: NoMain Tank: Not reportedRoot Tank Id: 10000Tank Capacity: DieselProduct Name: 08/16/2001Perm Close Date: 11/01/1991Installed Date: RemovedTank Status: 5Tank Id: FORMER PEPSI-COLA BUILDING (Continued) U001199836 TC5716013.2s Page 26 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Suction SystemDecode for PSYS_KEY: OtherDecode for PCONS_KEY: Single Wall Steel/FRPDecode for TCONS_KEY: UnknownLeak Detection Name: FORMER PEPSI-COLA BUILDING (Continued) U001199836 06/15/2006Evaluation date: StateEvaluation lead agency: Not reportedDate achieved compliance: Not reportedArea of violation: FOCUSED COMPLIANCE INSPECTIONEvaluation: 03/19/2014Evaluation date: Evaluation Action Summary: No violations foundViolation Status: NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste: Handler Activities Summary: Handler: Non-Generators do not presently generate hazardous wasteDescription: Non-GeneratorClassification: PrivateLand type: 04EPA Region: Not reportedContact email: 828-274-3569Contact telephone: USContact country: ASHEVILLE, NC 28803 SWEETEN CREEK ROADContact address: HUBERT JONESContact: ASHEVILLE, NC 28803 SWEETEN CREEK ROADMailing address: NCS000001020EPA ID: ASHEVILLE, NC 28803 1191 SWEETEN CREEK ROADFacility address: MACKS USED CAR & TRUCK PARTSFacility name: 06/15/2006Date form received by agency: RCRA NonGen / NLR: 1311 ft. 0.248 mi. Relative: Higher Actual: 2146 ft. 1/8-1/4 ASHEVILLE, NC 28803 South 1191 SWEETEN CREEK ROAD NCS000001020 12 RCRA NonGen / NLRMACKS USED CAR & TRUCK PARTS 1010786921 TC5716013.2s Page 27 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation StateEvaluation lead agency: Not reportedDate achieved compliance: Not reportedArea of violation: FOCUSED COMPLIANCE INSPECTIONEvaluation: MACKS USED CAR & TRUCK PARTS (Continued) 1010786921 JCARegional Officer Project Mgr: Not reportedTestlat: 35.5468 -82.5175Lat/Long Decimal: FalseValid: Not reportedError Code: 0Error Flag: FalseRPOP: TrueRPOW: 0Reel Num: 237CD Num: FalseRPL: 3PETOPT: Not reportedRBCA GW: File Located in ArchivesCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: NoFlag: UnknownMTBE1: NoMTBE: Not reportedLand Use: Not reportedSite Risk Reason: Not reportedPhase Of LSA Req: Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: COMMERCIALCommercial/NonCommercial UST Site: 0# Of Supply Wells: RTank Regulated Status: Not reportedLevel Of Soil Cleanup Achieved: 03/29/2003Close Out: Not reportedClosure Request: 08/16/2001Cleanup: 08/16/2001Date Occur: 11/13/2001Date Reported: PProduct Type: Leak-undergroundSource Type: SLContamination Type: 28101Incident Number: AS-2804UST Number: 00-0-000Facility ID: ASHEVILLE, NC 28813City,State,Zip: P.O. BOX 5315Address: PEPSI COLA COName: LUST: 1396 ft. 0.264 mi. Relative: Higher Actual: 2128 ft. 1/4-1/2 ASHEVILLE, NC 28813 NE IMDP.O. BOX 5315 N/A 13 LUSTPEPSI COLA CO S105893417 TC5716013.2s Page 28 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation MINOR SOIL CONTAMINATION REVEALED DURING CLOSURE OF 1-5-K HEATING OILIncident Desc: YesSoil Contam: No Groundwater Contamination detectedGW Contam: 11/13/2001Submit Date: 8/16/2001Date Occurred: 28101Facility ID: ASHRegion: IMD: Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Not reportedIncident Phase: Not reportedLast Modified: EUst Number: Not reportedSource: Not reportedCause: 2Err Type: Not reportedSource Code: Not reportedRelease Code: Not reportedPirf/Min Soil: Not reported5 Minute Quad: Y7#5 Minute Quad: Not reportedSamples Include: NWells Affected Y/N: Not reportedPriority Update: Not reportedSite Priority: 1Location: 3Type: 6Operation Type: 4Ownership: Not reportedOwner/Operator: LTR 3/29/2003 AND 1-10-K DIESEL UST; BOTTOM OF EXCAVATION BELOW ACTION LEVELS;NFA MINOR SOIL CONTAMINATION REVEALED DURING CLOSURE OF 1-5-K HEATING OILDescription Of Incident: 2001-11-13 00:00:00Date Reported: 2001-08-16 00:00:00Date Occurred: 28101Facility Id: PIRF: Not reported5 Min Quad: Not reportedComments: Not reportedRP County: ASHEVILLE, NCRP City,St,Zip: P.O. BOX 5315RP Address: Not reportedTelephone: CLIFF REDMONContact Person: PEPSI COLA COCompany: ASHRegion: PEPSI COLA CO (Continued)S105893417 TC5716013.2s Page 29 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Sighned: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Not reportedIncident Phase: Not reportedLast Modified: Not reportedFacility ID: DWMAgency: 7GPS: Not reportedLongitude Decimal: Not reportedLatitude Decimal: Not reportedLongitude Number: Not reportedLatitude Number: Not reportedLongitude: Not reportedLatitude: Not reported5 Min Quad: Not reported7.5 Min Quad: Not reportedSamples Include: YSampled By: Not reportedWells Contam: Not reportedNum Affected: NoWells Affected: JCADem Contact: Not reportedPriority Update: Not reportedPriority Code: Not reportedSite Priority: LRisk Site: Not reportedSetting: FacilityLocation: Gasoline/dieselType: Leak-undergroundSource: Not reportedQty Recovered 1: Not reportedQty Lost 1: Not reportedMaterial: CommercialOperation: PrivateOwnership: ASHEVILLE, NCOper City,St,Zip: ASHEVILLEOperator City: P.O. BOX 5315Operator Address: PEPSI COLA COOwner Company: Not reportedContact Phone: CLIFF REDMONOperator: LTR 3/29/2003 AND 1-10-K DIESEL UST; BOTTOM OF EXCAVATION BELOW ACTION LEVELS;NFA PEPSI COLA CO (Continued)S105893417 TC5716013.2s Page 30 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedOwner/operator extension: Not reportedOwner/operator fax: Not reportedOwner/operator email: 336-370-3822Owner/operator telephone: USOwner/operator country: GREENSBORO, NC 27406 FLAGSTONE DROwner/operator address: UNITED PARCEL SERVICE IN AN OHIO CORPOwner/operator name: Not reportedOwner/Op end date: 07/01/1975Owner/Op start date: OperatorOwner/Operator Type: PrivateLegal status: Not reportedOwner/operator extension: Not reportedOwner/operator fax: Not reportedOwner/operator email: Not reportedOwner/operator telephone: USOwner/operator country: Not reported Not reportedOwner/operator address: UNITED PARCEL SERVICEOwner/operator name: Owner/Operator Summary: hazardous waste the cleanup of a spill, into or on any land or water, of acutely any residue or contaminated soil, waste or other debris resulting from time: 1 kg or less of acutely hazardous waste; or 100 kg or less of hazardous waste during any calendar month, and accumulates at any from the cleanup of a spill, into or on any land or water, of acutely of any residue or contaminated soil, waste or other debris resulting land or water, of acutely hazardous waste; or generates 100 kg or less other debris resulting from the cleanup of a spill, into or on any waste; or 100 kg or less of any residue or contaminated soil, waste or month, and accumulates at any time: 1 kg or less of acutely hazardous or generates 1 kg or less of acutely hazardous waste per calendar month, and accumulates 1000 kg or less of hazardous waste at any time; Handler: generates 100 kg or less of hazardous waste per calendarDescription: Conditionally Exempt Small Quantity GeneratorClassification: 04EPA Region: DWILKINS@UPS.COMContact email: 919-796-6115Contact telephone: USContact country: GREENSBORO, NC 27406 FLAGSTONE DRContact address: DEMETRIUS WILKINSContact: GREENSBORO, NC 27406 FLAGSTONE DRMailing address: NCD089154322EPA ID: ASHEVILLE, NC 28803 301 SWEETEN CREEK RDFacility address: UNITED PARCEL SERVICE-ASHEVILLEFacility name: 11/15/2016Date form received by agency: RCRA-CESQG: 1422 ft. Site 1 of 2 in cluster C 0.269 mi. Relative: Lower Actual: 2075 ft. 1/4-1/2 ASHEVILLE, NC 28803 NNE IMD301 SWEETEN CREEK RD NCD089154322 C14 RCRA-CESQGUNITED PARCEL SERVICE-ASHEVILLE 1004744813 TC5716013.2s Page 31 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation No violations foundViolation Status: SALTS NICOTINE, & SALTS (OR) PYRIDINE, 3-(1-METHYL-2-PYRROLIDINYL)-,(S)-, &. Waste name: P075. Waste code: SPENT SOLVENT MIXTURES. F005; AND STILL BOTTOMS FROM THE RECOVERY OF THESE SPENT SOLVENTS AND NONHALOGENATED SOLVENTS OR THOSE SOLVENTS LISTED IN F001, F002, AND TOTAL OF TEN PERCENT OR MORE (BY VOLUME) OF ONE OR MORE OF THE ABOVE SOLVENTS; ALL SPENT SOLVENT MIXTURES/BLENDS CONTAINING, BEFORE USE, A AND NITROBENZENE; AND THE STILL BOTTOMS FROM THE RECOVERY OF THESE THE FOLLOWING SPENT NONHALOGENATED SOLVENTS: CRESOLS, CRESYLIC ACID,. Waste name: F004. Waste code: TETRACHLOROETHYLENE. Waste name: D039. Waste code: BENZENE. Waste name: D018. Waste code: IGNITABLE WASTE. Waste name: D001. Waste code: Hazardous Waste Summary: Conditionally Exempt Small Quantity GeneratorClassification: UNITED PARCEL SERVICESite name: 12/08/1993Date form received by agency: Large Quantity GeneratorClassification: UNITED PARCEL SERVICE-ASHEVILLESite name: 10/18/2016Date form received by agency: Historical Generators: NoUsed oil transporter: NoUsed oil transfer facility: NoUsed oil Specification marketer: NoUsed oil fuel marketer to burner: NoUser oil refiner: NoUsed oil processor: NoUsed oil fuel burner: NoFurnace exemption: NoOn-site burner exemption: NoUnderground injection activity: NoTreater, storer or disposer of HW: NoTransporter of hazardous waste: NoRecycler of hazardous waste: NoMixed waste (haz. and radioactive): NoU.S. importer of hazardous waste: Handler Activities Summary: Not reportedOwner/Op end date: 07/01/1975Owner/Op start date: OwnerOwner/Operator Type: PrivateLegal status: UNITED PARCEL SERVICE-ASHEVILLE (Continued) 1004744813 TC5716013.2s Page 32 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Sighned: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: REIncident Phase: Not reportedLast Modified: 11492Facility ID: DWMAgency: 7GPS: 82.5211111111111Longitude Decimal: 35.5469444444444Latitude Decimal: 823116Longitude Number: 353249Latitude Number: -82.52111111Longitude: 35.54694444Latitude: N86L5 Min Quad: Not reported7.5 Min Quad: Groundwater SamplesSamples Include: OtherSampled By: Not reportedWells Contam: 0Num Affected: NoWells Affected: DPMDem Contact: Not reportedPriority Update: EPriority Code: 60 ESite Priority: LRisk Site: IndustrialSetting: FacilityLocation: Gasoline/dieselType: Leak-undergroundSource: Not reportedQty Recovered 1: Not reportedQty Lost 1: GASOLINEMaterial: CommercialOperation: PrivateOwnership: CHARLOTTE, NC 28217-Oper City,St,Zip: CHARLOTTEOperator City: 4335 STUART ANDREW BLVD.Operator Address: KERMIT NABORSOwner Company: 704-561-5377Contact Phone: UNITED PARCEL SERVICEOperator: CONTAMINATION. RESULT OF CSA CONDUCTED BY NCI, INC. CONFIRMED SOIL AND GWIncident Desc: YesSoil Contam: No Groundwater Contamination detectedGW Contam: 1/13/1994Submit Date: 11/9/1993Date Occurred: 11492Facility ID: ASHRegion: IMD: UNITED PARCEL SERVICE-ASHEVILLE (Continued) 1004744813 TC5716013.2s Page 33 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 8/5/1992Close-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Sighned: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 2/3/1993Last Modified: 8255Facility ID: DWMAgency: NODGPS: Not reportedLongitude Decimal: Not reportedLatitude Decimal: Not reportedLongitude Number: Not reportedLatitude Number: Not reportedLongitude: Not reportedLatitude: Not reported5 Min Quad: Not reported7.5 Min Quad: Not reportedSamples Include: Not reportedSampled By: Not reportedWells Contam: 0Num Affected: Not reportedWells Affected: MESDem Contact: Not reportedPriority Update: Not reportedPriority Code: Not reportedSite Priority: Not reportedRisk Site: Not reportedSetting: Not reportedLocation: Gasoline/dieselType: Leak-undergroundSource: Not reportedQty Recovered 1: Not reportedQty Lost 1: Not reportedMaterial: Not reportedOperation: Not reportedOwnership: Not reportedOper City,St,Zip: Not reportedOperator City: Not reportedOperator Address: Not reportedOwner Company: Not reportedContact Phone: Not reportedOperator: Not reportedIncident Desc: YesSoil Contam: No Groundwater Contamination detectedGW Contam: 2/6/1992Submit Date: Not reportedDate Occurred: 8255Facility ID: ASHRegion: UNITED PARCEL SERVICE-ASHEVILLE (Continued) 1004744813 TC5716013.2s Page 34 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 4335 STUART ANDREW BLVD.RP Address: 704-561-5377Telephone: UNITED PARCEL SERVICEContact Person: KERMIT NABORSCompany: ASHRegion: DPMRegional Officer Project Mgr: Not reportedTestlat: 35.5469 -82.5211Lat/Long Decimal: FalseValid: Not reportedError Code: 0Error Flag: FalseRPOP: FalseRPOW: 0Reel Num: 0CD Num: FalseRPL: Not reportedPETOPT: Not reportedRBCA GW: File Located in HouseCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: YesFlag: UnknownMTBE1: Not reportedMTBE: Not reportedLand Use: Not reportedSite Risk Reason: Not reportedPhase Of LSA Req: 60 ESite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: COMMERCIALCommercial/NonCommercial UST Site: Not reported# Of Supply Wells: RTank Regulated Status: Not reportedLevel Of Soil Cleanup Achieved: 10/10/2016Close Out: Not reportedClosure Request: 11/09/1993Cleanup: 11/09/1993Date Occur: 11/09/1993Date Reported: PProduct Type: Leak-undergroundSource Type: SLContamination Type: 11492Incident Number: AS-1072UST Number: 00-0-000Facility ID: ASHEVILLE, NC 28803City,State,Zip: 301 SWEETEN CREEK IND. PARKAddress: UNITED PARCEL SERVICEName: LUST: 1422 ft. Site 2 of 2 in cluster C 0.269 mi. Relative: Lower Actual: 2075 ft. 1/4-1/2 ASHEVILLE, NC 28803 NNE 301 SWEETEN CREEK IND. PARK N/A C15 LUSTUNITED PARCEL SERVICE S118755595 TC5716013.2s Page 35 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 2016-10-10 00:00:00Last Modified: Not reportedUst Number: Not reportedSource: Not reportedCause: Not reportedErr Type: PirfSource Code: N86LRelease Code: Not reportedPirf/Min Soil: 15 Minute Quad: 47#5 Minute Quad: 0Samples Include: NWells Affected Y/N: Not reportedPriority Update: 60 ESite Priority: 1Location: 3Type: 6Operation Type: 4Ownership: KERMIT NABORSOwner/Operator: CONTAMINATION. RESULT OF CSA CONDUCTED BY NCI, INC. CONFIRMED SOIL AND GWDescription Of Incident: 1994-01-13 00:00:00Date Reported: 1993-11-09 00:00:00Date Occurred: 11492Facility Id: PIRF: Not reported5 Min Quad: Closed incident on 10/10./2016. See note to fileComments: Not reportedRP County: CHARLOTTE, NC 28217-RP City,St,Zip: UNITED PARCEL SERVICE (Continued) S118755595 Leak-undergroundSource Type: SLContamination Type: 28613Incident Number: AS-3464UST Number: Not reportedFacility ID: ASHEVILLE, NC 28803City,State,Zip: 523 CARIBOU ROADAddress: FRESHWATER PROPERTYName: LUST: 1456 ft. 0.276 mi. Relative: Higher Actual: 2192 ft. 1/4-1/2 ASHEVILLE, NC 28803 NW LUST TRUST523 CARIBOU ROAD N/A 16 LUSTFRESHWATER PROPERTY S109034155 TC5716013.2s Page 36 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedOwner/Operator: UST Soil contamination confirmed during removal of 275 gallon heating oilDescription Of Incident: 2008-05-28 00:00:00Date Reported: 2008-04-15 00:00:00Date Occurred: 28613Facility Id: PIRF: Not reported5 Min Quad: required. LSA received 7-29-08. Low risk site. UST. Initial Abatement & Actions Report received June 16, 2008. LSA Soil contamination confirmed during removal of 275 gallon heating oilComments: Not reportedRP County: Hendersonville, NC 28792RP City,St,Zip: 117 W. Barnwell St., Ste. 5RP Address: 8286980191Telephone: Scott FreshwaterContact Person: Freshwater Affiliated HoldingsCompany: ASHRegion: mesRegional Officer Project Mgr: Not reportedTestlat: 35.5461 -82.5255Lat/Long Decimal: FalseValid: NError Code: 0Error Flag: FalseRPOP: TrueRPOW: 0Reel Num: 0CD Num: TrueRPL: 4PETOPT: Not reportedRBCA GW: File Located in HouseCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: NoFlag: NoMTBE1: NoMTBE: Not reportedLand Use: Not reportedSite Risk Reason: 2Phase Of LSA Req: Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: NON COMMERCIALCommercial/NonCommercial UST Site: 0# Of Supply Wells: NTank Regulated Status: Not reportedLevel Of Soil Cleanup Achieved: Not reportedClose Out: Not reportedClosure Request: 05/28/2008Cleanup: 04/15/2008Date Occur: 05/28/2008Date Reported: PProduct Type: FRESHWATER PROPERTY (Continued) S109034155 TC5716013.2s Page 37 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 0Sum 3rd Party Amt Applied: 03rd Party Deductable Amt: 0Deductable Amount: Not reportedPriority Rank: 100% Non-CommercialCommercial Find: TrueSite Eligible?: Noncommercial; 100% eligible; $0 deductible.[CGS 8/25/08]Site Note: 28613Site ID: Not reportedFacility ID: LUST TRUST: Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Not reportedIncident Phase: Not reportedLast Modified: PUst Number: ASource: 3Cause: 2Err Type: Not reportedSource Code: Not reportedRelease Code: Not reportedPirf/Min Soil: Not reported5 Minute Quad: Y7#5 Minute Quad: Not reportedSamples Include: NWells Affected Y/N: Not reportedPriority Update: Not reportedSite Priority: 7Location: 4Type: 3Operation Type: 4Ownership: FRESHWATER PROPERTY (Continued) S109034155 Leak-undergroundSource Type: SLContamination Type: 28537Incident Number: AS-3379UST Number: 00-0-000Facility ID: ASHEVILLE, NC 28803City,State,Zip: 601 SWEETEN CREEK INDUSTRIAL PAddress: PEPSI WAREHOUSEName: LUST: 1584 ft. 0.300 mi. Relative: Lower Actual: 2086 ft. 1/4-1/2 ASHEVILLE, NC 28803 NE 601 SWEETEN CREEK INDUSTRIAL P N/A 17 LUSTPEPSI WAREHOUSE S108664805 TC5716013.2s Page 38 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation identified until 07/17/07. Therefore M. Realty is RP. Re-issued NORR arisen. Pepsi sold property to M. Realty on 04/27/06 - contam was not over all responsibilities including any env issues that may have attorney about how they sold property "As Is" and that M. Realty took closure. LSA NORR Issued. 12/30/09 - Received letter from Pepsi’s 12/16/09 - Consultant called trying to find out what’s needed for 08/17/07 - NORR Issued for IAA based on 24-Hour reporting form. JCA conducted site visit on 08/20/07 - Appears low risk site. previously removed (pre-1990’s and 1991). NFA was issued for these?. 05/07/07 as part of property transfer. Soils > TPH. USTs were 07/17/07 - 24-Hour reporting form submitted: Phase II conducted onComments: Not reportedRP County: Fletcher, NC 28732RP City,St,Zip: P O Box 1207RP Address: 8282744600Telephone: Cliff RedmondContact Person: Pepsi-Cola CoCompany: ASHRegion: CELRegional Officer Project Mgr: Not reportedTestlat: 35.5472 -82.5163Lat/Long Decimal: FalseValid: NError Code: 0Error Flag: TrueRPOP: TrueRPOW: 0Reel Num: 484CD Num: FalseRPL: 3PETOPT: Not reportedRBCA GW: File Located in ArchivesCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: NoFlag: UnknownMTBE1: NoMTBE: ResidentialLand Use: Not reportedSite Risk Reason: Not reportedPhase Of LSA Req: Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: COMMERCIALCommercial/NonCommercial UST Site: 0# Of Supply Wells: RTank Regulated Status: Soil to GroundwaterLevel Of Soil Cleanup Achieved: 01/15/2010Close Out: Not reportedClosure Request: 07/17/2007Cleanup: 05/07/2007Date Occur: 07/17/2007Date Reported: PProduct Type: PEPSI WAREHOUSE (Continued)S108664805 TC5716013.2s Page 39 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 2010-01-14 00:00:00Last Modified: PUst Number: Not reportedSource: Not reportedCause: 3Err Type: Not reportedSource Code: Not reportedRelease Code: Not reportedPirf/Min Soil: Not reported5 Minute Quad: Y7#5 Minute Quad: Not reportedSamples Include: NWells Affected Y/N: Not reportedPriority Update: Not reportedSite Priority: 1Location: 3Type: 6Operation Type: 4Ownership: Not reportedOwner/Operator: SOIL CONTAMINATION DISCOVERED DURING PHASE II FOR PROPERTY REANSACTIONDescription Of Incident: 2007-07-17 00:00:00Date Reported: 2007-05-07 00:00:00Date Occurred: 28537Facility Id: PIRF: Not reported5 Min Quad: data was from previous tanks that were removed). Issuing NFA. most recent UST closure there is no incident at the site (all TPH contam soil was removed and that incident was closed out. Based on herein.". Previous samples indicated Soils > TPH in one sample, but hold Buyer harmless from any breach of the representations contained any of same to remain on the Property. Seller shall indemnify and or state laws, ordinances, regulations, etc., nor has Seller allowed would be deemed hazardous or dangerous under any applicable federal nor is aware of the dumping of any chemicals or other wastes which dumped, has not caused the dumping of, has not allowed dumping of, property from Pepsi based on "Seller represents that Seller has not documenting UST closure and Phase I ESA. They said they bought to M. Realty on 12/30/09. 01/07/10 - Received email from M. Realty PEPSI WAREHOUSE (Continued)S108664805 TC5716013.2s Page 40 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedRP Address: Not reportedTelephone: Not reportedContact Person: Not reportedCompany: ASHRegion: JCARegional Officer Project Mgr: Not reportedTestlat: 35.5407 -82.5261Lat/Long Decimal: FalseValid: NError Code: 0Error Flag: FalseRPOP: FalseRPOW: 0Reel Num: 0CD Num: FalseRPL: 4PETOPT: Not reportedRBCA GW: File Located in ArchivesCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: NoFlag: UnknownMTBE1: NoMTBE: Not reportedLand Use: Not reportedSite Risk Reason: Not reportedPhase Of LSA Req: Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: NON COMMERCIALCommercial/NonCommercial UST Site: 0# Of Supply Wells: NTank Regulated Status: Soil to GroundwaterLevel Of Soil Cleanup Achieved: 08/09/2016Close Out: Not reportedClosure Request: 07/26/2016Cleanup: 07/25/2016Date Occur: 08/03/2016Date Reported: PProduct Type: Leak-undergroundSource Type: SLContamination Type: 41485Incident Number: AS-4427UST Number: Not reportedFacility ID: ASHEVILLE, NC 28803City,State,Zip: 60 IMPERIAL COURTAddress: MARCY PROPERTY (LISA)Name: LUST: 1696 ft. 0.321 mi. Relative: Higher Actual: 2244 ft. 1/4-1/2 ASHEVILLE, NC 28803 WSW 60 IMPERIAL COURT N/A 18 LUSTMARCY PROPERTY (LISA)S119104784 TC5716013.2s Page 41 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 2016-08-09 00:00:00Last Modified: PUst Number: ASource: 3Cause: 2Err Type: Not reportedSource Code: Not reportedRelease Code: Not reportedPirf/Min Soil: Not reported5 Minute Quad: N7#5 Minute Quad: Not reportedSamples Include: NWells Affected Y/N: Not reportedPriority Update: Not reportedSite Priority: 7Location: 4Type: 3Operation Type: 4Ownership: Not reportedOwner/Operator: A LEAKING 275 GALLON HEATING OIL UST CAUSED A RELEASEDescription Of Incident: 2016-08-03 00:00:00Date Reported: 2016-07-25 00:00:00Date Occurred: 41485Facility Id: PIRF: Not reported5 Min Quad: *** ALL FILES ON LASERFICHE. ***Comments: Not reportedRP County: NCRP City,St,Zip: MARCY PROPERTY (LISA) (Continued) S119104784 On Screen Placement On Georeferenced MapGeolocation Method: 35.548752 / -82.518101Lat/Longitude: NONCD0001163EPAID: SHWS: 1714 ft. 0.325 mi. Relative: Lower Actual: 2083 ft. 1/4-1/2 ASHEVILLE, NC NNE 401 SWEETEN CREEK IND. PK. N/A 19 SHWSSMITH’S AEROSPACE S108631702 TC5716013.2s Page 42 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedRP Address: Not reportedTelephone: Not reportedContact Person: Not reportedCompany: ASHRegion: MESRegional Officer Project Mgr: Not reportedTestlat: 35.5487 -82.5164Lat/Long Decimal: FalseValid: Not reportedError Code: 0Error Flag: FalseRPOP: FalseRPOW: 0Reel Num: 236CD Num: FalseRPL: Not reportedPETOPT: Not reportedRBCA GW: File Located in ArchivesCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: NoFlag: UnknownMTBE1: Not reportedMTBE: Not reportedLand Use: Not reportedSite Risk Reason: Not reportedPhase Of LSA Req: Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: COMMERCIALCommercial/NonCommercial UST Site: Not reported# Of Supply Wells: RTank Regulated Status: Not reportedLevel Of Soil Cleanup Achieved: 09/15/1998Close Out: Not reportedClosure Request: 08/15/1998Cleanup: 05/06/1998Date Occur: 06/15/1998Date Reported: PProduct Type: Leak-undergroundSource Type: SLContamination Type: 19012Incident Number: AS-1705UST Number: Not reportedFacility ID: ASHEVILLE, NC 288031530City,State,Zip: 502 SWEETEN CREEK IND. DRAddress: FREDRICKSON MOTOR EXPRESSName: LUST: 1828 ft. 0.346 mi. Relative: Lower Actual: 2075 ft. 1/4-1/2 ASHEVILLE, NC 28803 NNE IMD502 SWEETEN CREEK IND. DR N/A 20 LUSTFREDRICKSON MOTOR EXPRESS S106349139 TC5716013.2s Page 43 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedOwner Company: Not reportedContact Phone: Not reportedOperator: INDICATED NO DETECTABLE HYD ADDITIONAL EXCAVATION AND SOIL REMOVAL PERFORMED; FINAL SOIL SAMPLE PETRO HYDROCARBON CONTAM. SOIL DETECTED DURING REMOVAL OF TANKS;Incident Desc: YesSoil Contam: No Groundwater Contamination detectedGW Contam: 9/15/1998Submit Date: 5/6/1998Date Occurred: 19012Facility ID: ASHRegion: IMD: 1998-05-06 00:00:00Close-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 1998-10-06 00:00:00Last Modified: EUst Number: Not reportedSource: Not reportedCause: 2Err Type: Min_SoilSource Code: Not reportedRelease Code: Not reportedPirf/Min Soil: Not reported5 Minute Quad: Not reported7#5 Minute Quad: Not reportedSamples Include: Not reportedWells Affected Y/N: 1998-09-28 00:00:00Priority Update: Not reportedSite Priority: 1Location: 3Type: 5Operation Type: 4Ownership: ALAN SMITH, CFOOwner/Operator: INDICATED NO DETECTABLE HYD ADDITIONAL EXCAVATION AND SOIL REMOVAL PERFORMED; FINAL SOIL SAMPLE PETRO HYDROCARBON CONTAM. SOIL DETECTED DURING REMOVAL OF TANKS;Description Of Incident: 1998-09-15 00:00:00Date Reported: 1998-05-06 00:00:00Date Occurred: 19012Facility Id: PIRF: Not reported5 Min Quad: CLOSED 9/15/98Comments: Not reportedRP County: Not reportedRP City,St,Zip: FREDRICKSON MOTOR EXPRESS (Continued) S106349139 TC5716013.2s Page 44 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 5/6/1998Close-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Sighned: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 10/6/1998Last Modified: 19012Facility ID: DWMAgency: NODGPS: Not reportedLongitude Decimal: Not reportedLatitude Decimal: Not reportedLongitude Number: Not reportedLatitude Number: Not reportedLongitude: Not reportedLatitude: Not reported5 Min Quad: Not reported7.5 Min Quad: Not reportedSamples Include: Not reportedSampled By: Not reportedWells Contam: Not reportedNum Affected: Not reportedWells Affected: MESDem Contact: 9/28/1998Priority Update: Not reportedPriority Code: Not reportedSite Priority: LRisk Site: Not reportedSetting: FacilityLocation: Gasoline/dieselType: Leak-undergroundSource: Not reportedQty Recovered 3: Not reportedQty Lost: USED OILMaterial: Not reportedQty Recovered: Not reportedQty Lost: DIESELMaterial: Not reportedQty Recovered 1: Not reportedQty Lost 1: GASOLINEMaterial: IndustrialOperation: PrivateOwnership: Not reportedOper City,St,Zip: Not reportedOperator City: Not reportedOperator Address: FREDRICKSON MOTOR EXPRESS (Continued) S106349139 TC5716013.2s Page 45 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 74 taft avenueRP Address: 8280000000Telephone: frances suberContact Person: frances suber residenceCompany: ASHRegion: DpmRegional Officer Project Mgr: Not reportedTestlat: 35.5460 -82.5277Lat/Long Decimal: FalseValid: NError Code: 0Error Flag: FalseRPOP: FalseRPOW: 0Reel Num: 654CD Num: FalseRPL: 4PETOPT: Cleanups to 2L.0202 standardsRBCA GW: File Located in ArchivesCurrent Status: 0Release Detection: 08/26/2013LUR Filed: NoFlag1: YesFlag: UnknownMTBE1: NoMTBE: ResidentialLand Use: Not reportedSite Risk Reason: 1Phase Of LSA Req: Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: NON COMMERCIALCommercial/NonCommercial UST Site: 0# Of Supply Wells: NTank Regulated Status: ResidentialLevel Of Soil Cleanup Achieved: 05/06/2013Close Out: Not reportedClosure Request: 03/08/2013Cleanup: 02/14/2013Date Occur: 03/08/2013Date Reported: PProduct Type: Leak-undergroundSource Type: SLContamination Type: 41090Incident Number: AS-3981UST Number: Not reportedFacility ID: ASHEVILLE, NC 28803City,State,Zip: 74 TAFT AVENUEAddress: FRANCES SUBER RESIDENCEName: LUST: 2024 ft. 0.383 mi. Relative: Higher Actual: 2171 ft. 1/4-1/2 INST CONTROLASHEVILLE, NC 28803 WNW LUST TRUST74 TAFT AVENUE N/A 21 LUSTFRANCES SUBER RESIDENCE S113193336 TC5716013.2s Page 46 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 0Sum 3rd Party Amt Applied: 03rd Party Deductable Amt: 0Deductable Amount: Not reportedPriority Rank: 100% Non-CommercialCommercial Find: TrueSite Eligible?: Law 2010-154. [CGS 9/18/13] would have been 5K + 10% as this is receiving 100% because of Session Noncommercial; 100% eligible; $0 deductible. Track this as a site thatSite Note: 41090Site ID: Not reportedFacility ID: LUST TRUST: Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 2013-05-06 00:00:00Last Modified: PUst Number: ASource: 7Cause: 2Err Type: Not reportedSource Code: Not reportedRelease Code: Not reportedPirf/Min Soil: Not reported5 Minute Quad: Y7#5 Minute Quad: Not reportedSamples Include: NWells Affected Y/N: Not reportedPriority Update: Not reportedSite Priority: 1Location: 4Type: 3Operation Type: 4Ownership: Not reportedOwner/Operator: Release from heating oil tank to soilDescription Of Incident: 2013-03-08 00:00:00Date Reported: 2013-02-14 00:00:00Date Occurred: 41090Facility Id: PIRF: Not reported5 Min Quad: on 5/6/2013.Soil only restriction, Book, 5138, Pages, 107-111 as "low risk", NFA letter for closure with no further action issued heating oil release from residential ust, LSA received, site rankedComments: Not reportedRP County: asheville, NC 28803RP City,St,Zip: FRANCES SUBER RESIDENCE (Continued) S113193336 TC5716013.2s Page 47 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 672294.06177Y Coord: 950832.72671X Coord: Not reportedPlat Date: Not reportedPlat: Recorded 8-25-2013Deed Date: Not reportedDeed: Notice and RestrictionInstrument: Not reportedPlat PG: Not reportedPlat BK: Not reportedDeed PG: Not reportedDeed BK: EffectiveInstrument Status: Not reportedPlant Reception Date: NoneCertification: Media Restrictions OnlyAllowed Use: Soil OnlyRestricted Media: 8/25/2013Received Date: UST SystemContamination Source: Multi COCCOC: No Further ActionProject Status: Underground Storage Tank SectionDWM Program: Asheville Regional Office (828) 296-4500DWM Contact: 6447Object ID: AS-3981Project Number: INST CONTROL: FRANCES SUBER RESIDENCE (Continued) S113193336 Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: LRisk Classification: Not reportedCommercial/NonCommercial UST Site: 0# Of Supply Wells: Not reportedTank Regulated Status: Not reportedLevel Of Soil Cleanup Achieved: Not reportedClose Out: Not reportedClosure Request: Not reportedCleanup: 08/10/2001Date Occur: 08/10/2001Date Reported: PProduct Type: Not reportedSource Type: SLContamination Type: 85893Incident Number: AS-88142UST Number: Not reportedFacility ID: ASHEVILLE, NC 28803City,State,Zip: 20 ROBERSON AVE.Address: TUSKEEGEE CLEANERS FORMERName: LAST: 2097 ft. 0.397 mi. Relative: Higher Actual: 2183 ft. 1/4-1/2 ASHEVILLE, NC 28803 NNW IMD20 ROBERSON AVE. N/A 22 LASTTUSKEEGEE CLEANERS FORMER S105120610 TC5716013.2s Page 48 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation SOIL CONTAMINATION DETECTED IN THE DRAIN FIELD (FLOOR DRAIN FROM AIncident Desc: Not reportedSoil Contam: No data entered (data entry person submitted a blank fieldGW Contam: 8/30/2001Submit Date: 8/10/2001Date Occurred: 85893Facility ID: ASHRegion: IMD: Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: 8/30/2001NOV Issued: REIncident Phase: Not reportedLast Modified: Not reported5 Min Quad: CLEAN-UP. JEFF BROOKS: 275-0019. BOUGHT THE PROPERTY AND WILL BE DOING THE SITE ASSESSMENT AND CLEANER OPERATION - MINERAL OIL ONLY). TOP DOG PROPERTIES, INC. SOIL CONTAMINATION DETECTED IN THE DRAIN FIELD (FLOOR DRAIN FROM AComments: Not reportedRP County: NCRP City,St,Zip: Not reportedRP Address: Not reportedTelephone: Not reportedContact Person: Not reportedCompany: ASHRegion: MESRegional Officer Project Mgr: Not reportedTestlat: 35.54944 -82.52333Lat/Long Decimal: 35 32 57.96 82 31 23.94Lat/Long: FalseValid: NError Code: 0Error Flag: FalseRPOP: FalseRPOW: 0Reel Num: 0CD Num: FalseRPL: 5PETOPT: Not reportedRBCA GW: CCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: NoFlag: UnknownMTBE1: NoMTBE: Not reportedLand Use: Not reportedSite Risk Reason: Not reportedPhase Of LSA Req: TUSKEEGEE CLEANERS FORMER (Continued) S105120610 TC5716013.2s Page 49 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Sighned: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: 8/30/2001NOV Issued: AssessmentIncident Phase: 8/30/2001Last Modified: 85893Facility ID: DWQAgency: GPSGPS: Not reportedLongitude Decimal: Not reportedLatitude Decimal: Not reportedLongitude Number: Not reportedLatitude Number: -82.523333Longitude: 35.549444Latitude: Not reported5 Min Quad: Not reported7.5 Min Quad: Not reportedSamples Include: Not reportedSampled By: Not reportedWells Contam: 0Num Affected: NoWells Affected: QQDem Contact: Not reportedPriority Update: EPriority Code: 20Site Priority: Not reportedRisk Site: Not reportedSetting: Not reportedLocation: Other petroleum productType: Pit, pond, lagoonSource: Not reportedQty Recovered 1: Not reportedQty Lost 1: Not reportedMaterial: 8Operation: FederalOwnership: ASEVILLE 828-274-2648Oper City,St,Zip: ASEVILLEOperator City: 20 ROBINSON AVENUEOperator Address: Not reportedOwner Company: 828-274-2648Contact Phone: B. DENNISON, W.Operator: THE PROPERTY AND WILL CLEANER OPERATION - MINERAL OIL ONLY). TOP DOG PROPERTIES, INC. BOUGHT TUSKEEGEE CLEANERS FORMER (Continued) S105120610 TC5716013.2s Page 50 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedTelephone: Not reportedContact Person: CITY OF ASHEVILLECompany: ASHRegion: Not reportedRegional Officer Project Mgr: Not reportedTestlat: 35.54466 -82.51242Lat/Long Decimal: 35 32 40.74 82 30 44.7Lat/Long: FalseValid: Not reportedError Code: 0Error Flag: FalseRPOP: FalseRPOW: 0Reel Num: 302CD Num: FalseRPL: Not reportedPETOPT: Not reportedRBCA GW: ACurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: NoFlag: UnknownMTBE1: NoMTBE: Not reportedLand Use: Not reportedSite Risk Reason: Not reportedPhase Of LSA Req: 0Site Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: Not reportedRisk Classification: Not reportedCommercial/NonCommercial UST Site: 0# Of Supply Wells: Not reportedTank Regulated Status: Not reportedLevel Of Soil Cleanup Achieved: 02/23/1996Close Out: Not reportedClosure Request: 07/19/1994Cleanup: 04/26/1994Date Occur: 07/19/1994Date Reported: NProduct Type: 19Source Type: SLContamination Type: 12778Incident Number: AS-12778UST Number: Not reportedFacility ID: ASHVILLE, NC 28803City,State,Zip: WEST CHAPEL BALL FIELDAddress: WEST CHAPEL BALL FIELDName: LAST: 2437 ft. 0.462 mi. Relative: Higher Actual: 2123 ft. 1/4-1/2 ASHVILLE, NC 28803 East IMDWEST CHAPEL BALL FIELD N/A 23 LASTWEST CHAPEL BALL FIELD S103131348 TC5716013.2s Page 51 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation ,Operator: WAS EXCAVATED TO GRO EQUIPMENT AND TANK WAS PIERCED AND SPILLED ONTO THE GROUND. SITE AREA RELEASE DURING GRADING AT NEW BALLPARK. UST WAS STRUCK BY EARTHMOVINGIncident Desc: Not reportedSoil Contam: No data entered (data entry person submitted a blank fieldGW Contam: 9/27/1994Submit Date: 4/26/1994Date Occurred: 12778Facility ID: ASHRegion: IMD: 2/23/1996Close-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: COIncident Phase: 1/22/2001Last Modified: 0Source Type: Not reportedSource: Not reportedCause: Not reportedRelease Code: Not reportedPirf/Min Soil: Not reported5 Min Quad: Not reported7#5 Min Quad: Not reportedSamples Include: Not reportedSamples Taken By: 0Wells Affected Number: NWells Affected Y/N: Not reportedPriority Update: 0NODSite Priority: Not reportedLocation: Not reportedType: 3Operation Type: 3Ownership: Not reportedOwner/Operator: Not reportedDescription Of Incident: Not reportedDate Reported: Not reportedDate Occurred: 12778Facility Id: PIRF: Not reported5 Min Quad: INDICATED NO CONTAMINATION OF GROUNDWATER. WAS EXCAVATED TO GROUNDWATER TABLE. MW INSTALLED AND SAMPLING EQUIPMENT AND TANK WAS PIERCED AND SPILLED ONTO THE GROUND. SITE AREA RELEASE DURING GRADING AT NEW BALLPARK. UST WAS STRUCK BY EARTHMOVINGComments: Not reportedRP County: ASHEVILLE, NCRP City,St,Zip: COURT HOUSERP Address: WEST CHAPEL BALL FIELD (Continued) S103131348 TC5716013.2s Page 52 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 2/23/1996Close-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Sighned: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 1/22/2001Last Modified: 12778Facility ID: DWQAgency: NODGPS: Not reportedLongitude Decimal: Not reportedLatitude Decimal: Not reportedLongitude Number: Not reportedLatitude Number: Not reportedLongitude: Not reportedLatitude: Not reported5 Min Quad: Not reported7.5 Min Quad: Not reportedSamples Include: Not reportedSampled By: Not reportedWells Contam: 0Num Affected: NoWells Affected: JCADem Contact: Not reportedPriority Update: NODPriority Code: Not reportedSite Priority: Not reportedRisk Site: Not reportedSetting: Not reportedLocation: Gasoline/dieselType: Spill-surfaceSource: Not reportedQty Recovered 1: Not reportedQty Lost 1: Not reportedMaterial: ResidentialOperation: UnknownOwnership: ASHEVILLE, NCOper City,St,Zip: ASHEVILLEOperator City: COURT HOUSEOperator Address: CITY OF ASHEVILLEOwner Company: Not reportedContact Phone: WEST CHAPEL BALL FIELD (Continued) S103131348 TC5716013.2s Page 53 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation 1510 OLD MISSOURI RDRP Address: Not reportedTelephone: JOE FANCHERContact Person: BRUNNER AND LAYCompany: ASHRegion: JCARegional Officer Project Mgr: Not reportedTestlat: 35.5512 -82.5195Lat/Long Decimal: FalseValid: NError Code: 0Error Flag: TrueRPOP: TrueRPOW: 0Reel Num: 657CD Num: FalseRPL: 4PETOPT: Cleanups to 2L.0202 standardsRBCA GW: File Located in ArchivesCurrent Status: 0Release Detection: Not reportedLUR Filed: NoFlag1: NoFlag: UnknownMTBE1: NoMTBE: Not reportedLand Use: Not reportedSite Risk Reason: Not reportedPhase Of LSA Req: Not reportedSite Priority: Not reportedNORR Issue Date: Not reportedNOV Issue Date: Not reportedCorrective Action Plan Type: LRisk Class Based On Review: URisk Classification: COMMERCIALCommercial/NonCommercial UST Site: 0# Of Supply Wells: NTank Regulated Status: Soil to GroundwaterLevel Of Soil Cleanup Achieved: 02/27/2014Close Out: Not reportedClosure Request: 11/25/2013Cleanup: 11/25/2013Date Occur: 11/25/2013Date Reported: PProduct Type: Leak-undergroundSource Type: SLContamination Type: 41172Incident Number: AS-4073UST Number: Not reportedFacility ID: ASHEVILLE, NC 28803City,State,Zip: 150 SWEETEN CREEK RDAddress: BRUNNER AND LAYName: LUST: 2556 ft. 0.484 mi. Relative: Lower Actual: 2093 ft. 1/4-1/2 ASHEVILLE, NC 28803 North 150 SWEETEN CREEK RD N/A 24 LUSTBRUNNER AND LAY S115705402 TC5716013.2s Page 54 MAP FINDINGSMap ID Direction EDR ID NumberDistance EPA ID NumberDatabase(s)SiteElevation Not reportedClose-out Report: Not reportedClosure Request Date: Not reportedRS Designation: Not reportedReclassification Report: Not reportedSOC Signed: Not reportedCorrective Action Planned: Not reportedPublic Meeting Held: Not reported45 Day Report: Not reportedNORR Issued: Not reportedNOV Issued: Closed OutIncident Phase: 2014-02-27 00:00:00Last Modified: PUst Number: GSource: 7Cause: 2Err Type: Not reportedSource Code: Not reportedRelease Code: Not reportedPirf/Min Soil: Not reported5 Minute Quad: N7#5 Minute Quad: Not reportedSamples Include: NWells Affected Y/N: Not reportedPriority Update: Not reportedSite Priority: 1Location: 4Type: 6Operation Type: 4Ownership: Not reportedOwner/Operator: OIL UST DRO ABOVE ACTION LEVEL DISCOVERED DURING THE REMOVAL OF A 10K HEATINGDescription Of Incident: 2013-11-25 00:00:00Date Reported: 2013-11-25 00:00:00Date Occurred: 41172Facility Id: PIRF: Not reported5 Min Quad: established in Title 15A NCAC 2L .0202.PN not required. contamination did not exceed the groundwater quality standards (MSCCs), established in Title 15A NCAC 2L .0411 and that groundwater exceed the residential maximum soil contaminant concentrations Letter 2/27/2014 LSA review indicated that soil contamination did not Closure of a 10K heating oil UST LSA required NFA 2/27/2014. NFAComments: Not reportedRP County: SPRINGDALE, AR 72765RP City,St,Zip: BRUNNER AND LAY (Continued)S115705402 TC5716013.2s Page 55 ORPHAN SUMMARYCityEDR IDSite NameSite AddressZipDatabase(s)Count: 0 records.NO SITES FOUNDTC5716013.2s Page 56 To maintain currency of the following federal and state databases, EDR contacts the appropriate governmental agency on a monthly or quarterly basis, as required. Number of Days to Update:Provides confirmation that EDR is reporting records that have been updated within 90 days from the date the government agency made the information available to the public. STANDARD ENVIRONMENTAL RECORDS Federal NPL site list NPL: National Priority List National Priorities List (Superfund). The NPL is a subset of CERCLIS and identifies over 1,200 sites for priority cleanup under the Superfund Program. NPL sites may encompass relatively large areas. As such, EDR provides polygon coverage for over 1,000 NPL site boundaries produced by EPA’s Environmental Photographic Interpretation Center (EPIC) and regional EPA offices. Date of Government Version: 04/11/2019 Date Data Arrived at EDR: 04/18/2019 Date Made Active in Reports: 05/14/2019 Number of Days to Update: 26 Source: EPA Telephone: N/A Last EDR Contact: 07/02/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Quarterly NPL Site Boundaries Sources: EPA’s Environmental Photographic Interpretation Center (EPIC) Telephone: 202-564-7333 EPA Region 1 EPA Region 6 Telephone 617-918-1143 Telephone: 214-655-6659 EPA Region 3 EPA Region 7 Telephone 215-814-5418 Telephone: 913-551-7247 EPA Region 4 EPA Region 8 Telephone 404-562-8033 Telephone: 303-312-6774 EPA Region 5 EPA Region 9 Telephone 312-886-6686 Telephone: 415-947-4246 EPA Region 10 Telephone 206-553-8665 Proposed NPL: Proposed National Priority List Sites A site that has been proposed for listing on the National Priorities List through the issuance of a proposed rule in the Federal Register. EPA then accepts public comments on the site, responds to the comments, and places on the NPL those sites that continue to meet the requirements for listing. Date of Government Version: 04/11/2019 Date Data Arrived at EDR: 04/18/2019 Date Made Active in Reports: 05/14/2019 Number of Days to Update: 26 Source: EPA Telephone: N/A Last EDR Contact: 07/02/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Quarterly NPL LIENS: Federal Superfund Liens Federal Superfund Liens. Under the authority granted the USEPA by CERCLA of 1980, the USEPA has the authority to file liens against real property in order to recover remedial action expenditures or when the property owner received notification of potential liability. USEPA compiles a listing of filed notices of Superfund Liens. TC5716013.2s Page GR-1 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 10/15/1991 Date Data Arrived at EDR: 02/02/1994 Date Made Active in Reports: 03/30/1994 Number of Days to Update: 56 Source: EPA Telephone: 202-564-4267 Last EDR Contact: 08/15/2011 Next Scheduled EDR Contact: 11/28/2011 Data Release Frequency: No Update Planned Federal Delisted NPL site list Delisted NPL: National Priority List Deletions The National Oil and Hazardous Substances Pollution Contingency Plan (NCP) establishes the criteria that the EPA uses to delete sites from the NPL. In accordance with 40 CFR 300.425.(e), sites may be deleted from the NPL where no further response is appropriate. Date of Government Version: 04/11/2019 Date Data Arrived at EDR: 04/18/2019 Date Made Active in Reports: 05/14/2019 Number of Days to Update: 26 Source: EPA Telephone: N/A Last EDR Contact: 07/02/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Quarterly Federal CERCLIS list FEDERAL FACILITY: Federal Facility Site Information listing A listing of National Priority List (NPL) and Base Realignment and Closure (BRAC) sites found in the Comprehensive Environmental Response, Compensation and Liability Information System (CERCLIS) Database where EPA Federal Facilities Restoration and Reuse Office is involved in cleanup activities. Date of Government Version: 04/03/2019 Date Data Arrived at EDR: 04/05/2019 Date Made Active in Reports: 05/14/2019 Number of Days to Update: 39 Source: Environmental Protection Agency Telephone: 703-603-8704 Last EDR Contact: 07/03/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Varies SEMS: Superfund Enterprise Management System SEMS (Superfund Enterprise Management System) tracks hazardous waste sites, potentially hazardous waste sites, and remedial activities performed in support of EPA’s Superfund Program across the United States. The list was formerly know as CERCLIS, renamed to SEMS by the EPA in 2015. The list contains data on potentially hazardous waste sites that have been reported to the USEPA by states, municipalities, private companies and private persons, pursuant to Section 103 of the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA). This dataset also contains sites which are either proposed to or on the National Priorities List (NPL) and the sites which are in the screening and assessment phase for possible inclusion on the NPL. Date of Government Version: 04/11/2019 Date Data Arrived at EDR: 04/18/2019 Date Made Active in Reports: 05/23/2019 Number of Days to Update: 35 Source: EPA Telephone: 800-424-9346 Last EDR Contact: 07/02/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Quarterly Federal CERCLIS NFRAP site list SEMS-ARCHIVE: Superfund Enterprise Management System Archive TC5716013.2s Page GR-2 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING SEMS-ARCHIVE (Superfund Enterprise Management System Archive) tracks sites that have no further interest under the Federal Superfund Program based on available information. The list was formerly known as the CERCLIS-NFRAP, renamed to SEMS ARCHIVE by the EPA in 2015. EPA may perform a minimal level of assessment work at a site while it is archived if site conditions change and/or new information becomes available. Archived sites have been removed and archived from the inventory of SEMS sites. Archived status indicates that, to the best of EPA’s knowledge, assessment at a site has been completed and that EPA has determined no further steps will be taken to list the site on the National Priorities List (NPL), unless information indicates this decision was not appropriate or other considerations require a recommendation for listing at a later time. The decision does not necessarily mean that there is no hazard associated with a given site; it only means that. based upon available information, the location is not judged to be potential NPL site. Date of Government Version: 04/11/2019 Date Data Arrived at EDR: 04/18/2019 Date Made Active in Reports: 05/23/2019 Number of Days to Update: 35 Source: EPA Telephone: 800-424-9346 Last EDR Contact: 07/02/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Quarterly Federal RCRA CORRACTS facilities list CORRACTS: Corrective Action Report CORRACTS identifies hazardous waste handlers with RCRA corrective action activity. Date of Government Version: 03/25/2019 Date Data Arrived at EDR: 03/27/2019 Date Made Active in Reports: 04/17/2019 Number of Days to Update: 21 Source: EPA Telephone: 800-424-9346 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Quarterly Federal RCRA non-CORRACTS TSD facilities list RCRA-TSDF: RCRA - Treatment, Storage and Disposal RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Transporters are individuals or entities that move hazardous waste from the generator offsite to a facility that can recycle, treat, store, or dispose of the waste. TSDFs treat, store, or dispose of the waste. Date of Government Version: 03/25/2019 Date Data Arrived at EDR: 03/27/2019 Date Made Active in Reports: 04/17/2019 Number of Days to Update: 21 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Quarterly Federal RCRA generators list RCRA-LQG: RCRA - Large Quantity Generators RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Large quantity generators (LQGs) generate over 1,000 kilograms (kg) of hazardous waste, or over 1 kg of acutely hazardous waste per month. Date of Government Version: 03/25/2019 Date Data Arrived at EDR: 03/27/2019 Date Made Active in Reports: 04/17/2019 Number of Days to Update: 21 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Quarterly TC5716013.2s Page GR-3 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING RCRA-SQG: RCRA - Small Quantity Generators RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Small quantity generators (SQGs) generate between 100 kg and 1,000 kg of hazardous waste per month. Date of Government Version: 03/25/2019 Date Data Arrived at EDR: 03/27/2019 Date Made Active in Reports: 04/17/2019 Number of Days to Update: 21 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Quarterly RCRA-CESQG: RCRA - Conditionally Exempt Small Quantity Generators RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Conditionally exempt small quantity generators (CESQGs) generate less than 100 kg of hazardous waste, or less than 1 kg of acutely hazardous waste per month. Date of Government Version: 03/25/2019 Date Data Arrived at EDR: 03/27/2019 Date Made Active in Reports: 04/17/2019 Number of Days to Update: 21 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Quarterly Federal institutional controls / engineering controls registries LUCIS: Land Use Control Information System LUCIS contains records of land use control information pertaining to the former Navy Base Realignment and Closure properties. Date of Government Version: 02/22/2019 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 04/17/2019 Number of Days to Update: 41 Source: Department of the Navy Telephone: 843-820-7326 Last EDR Contact: 05/10/2019 Next Scheduled EDR Contact: 08/26/2019 Data Release Frequency: Varies US ENG CONTROLS: Engineering Controls Sites List A listing of sites with engineering controls in place. Engineering controls include various forms of caps, building foundations, liners, and treatment methods to create pathway elimination for regulated substances to enter environmental media or effect human health. Date of Government Version: 01/31/2019 Date Data Arrived at EDR: 02/04/2019 Date Made Active in Reports: 03/08/2019 Number of Days to Update: 32 Source: Environmental Protection Agency Telephone: 703-603-0695 Last EDR Contact: 05/29/2019 Next Scheduled EDR Contact: 09/09/2019 Data Release Frequency: Varies US INST CONTROL: Sites with Institutional Controls A listing of sites with institutional controls in place. Institutional controls include administrative measures, such as groundwater use restrictions, construction restrictions, property use restrictions, and post remediation care requirements intended to prevent exposure to contaminants remaining on site. Deed restrictions are generally required as part of the institutional controls. Date of Government Version: 01/31/2019 Date Data Arrived at EDR: 02/04/2019 Date Made Active in Reports: 03/08/2019 Number of Days to Update: 32 Source: Environmental Protection Agency Telephone: 703-603-0695 Last EDR Contact: 05/29/2019 Next Scheduled EDR Contact: 09/09/2019 Data Release Frequency: Varies TC5716013.2s Page GR-4 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Federal ERNS list ERNS: Emergency Response Notification System Emergency Response Notification System. ERNS records and stores information on reported releases of oil and hazardous substances. Date of Government Version: 03/25/2019 Date Data Arrived at EDR: 03/26/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 36 Source: National Response Center, United States Coast Guard Telephone: 202-267-2180 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Quarterly State- and tribal - equivalent NPL HSDS: Hazardous Substance Disposal Site Locations of uncontrolled and unregulated hazardous waste sites. The file includes sites on the National Priority List as well as those on the state priority list. Date of Government Version: 08/09/2011 Date Data Arrived at EDR: 11/08/2011 Date Made Active in Reports: 12/05/2011 Number of Days to Update: 27 Source: North Carolina Center for Geographic Information and Analysis Telephone: 919-754-6580 Last EDR Contact: 04/22/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Biennially State- and tribal - equivalent CERCLIS SHWS: Inactive Hazardous Sites Inventory State Hazardous Waste Sites. State hazardous waste site records are the states’ equivalent to CERCLIS. These sites may or may not already be listed on the federal CERCLIS list. Priority sites planned for cleanup using state funds (state equivalent of Superfund) are identified along with sites where cleanup will be paid for by potentially responsible parties. Available information varies by state. Date of Government Version: 02/08/2019 Date Data Arrived at EDR: 03/13/2019 Date Made Active in Reports: 05/17/2019 Number of Days to Update: 65 Source: Department of Environment, Health and Natural Resources Telephone: 919-508-8400 Last EDR Contact: 06/12/2019 Next Scheduled EDR Contact: 09/23/2019 Data Release Frequency: Quarterly State and tribal landfill and/or solid waste disposal site lists SWF/LF: List of Solid Waste Facilities Solid Waste Facilities/Landfill Sites. SWF/LF type records typically contain an inventory of solid waste disposal facilities or landfills in a particular state. Depending on the state, these may be active or inactive facilities or open dumps that failed to meet RCRA Subtitle D Section 4004 criteria for solid waste landfills or disposal sites. Date of Government Version: 10/05/2018 Date Data Arrived at EDR: 12/26/2018 Date Made Active in Reports: 02/05/2019 Number of Days to Update: 41 Source: Department of Environment and Natural Resources Telephone: 919-733-0692 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Varies OLI: Old Landfill Inventory Old landfill inventory location information. (Does not include no further action sites and other agency lead sites). Date of Government Version: 10/09/2018 Date Data Arrived at EDR: 01/15/2019 Date Made Active in Reports: 03/26/2019 Number of Days to Update: 70 Source: Department of Environment & Natural Resources Telephone: 919-733-4996 Last EDR Contact: 07/12/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Varies TC5716013.2s Page GR-5 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING DEBRIS: Solid Waste Active Disaster Debris Sites Listing NCDEQ Division of Waste Management Solid Waste Section Temporary Disaster Debris Staging Site (TDDSS) Locations which are available to be activated in a disaster or emergency.. Disaster Debris Sites can only be used for temporary disaster debris storage if the site’s responsible party activates the site for use by notifying the NCDEQ DWM Solid Waste Section staff during an emergency Date of Government Version: 03/19/2019 Date Data Arrived at EDR: 03/20/2019 Date Made Active in Reports: 05/16/2019 Number of Days to Update: 57 Source: Department of Environmental Quality Telephone: 919-707-8247 Last EDR Contact: 06/19/2019 Next Scheduled EDR Contact: 09/30/2019 Data Release Frequency: Varies LCID: Land-Clearing and Inert Debris (LCID) Landfill Notifications A list all of the Land-Clearing and Inert Debris (LCID) Landfill Notification facilities (under 2 acres in size) in North Carolina. Date of Government Version: 09/06/2018 Date Data Arrived at EDR: 01/09/2019 Date Made Active in Reports: 03/25/2019 Number of Days to Update: 75 Source: Department of Environmental Quality Telephone: 919-707-8248 Last EDR Contact: 07/12/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Varies State and tribal leaking storage tank lists LAST: Leaking Aboveground Storage Tanks A listing of leaking aboveground storage tank site locations. Date of Government Version: 05/03/2019 Date Data Arrived at EDR: 05/08/2019 Date Made Active in Reports: 07/11/2019 Number of Days to Update: 64 Source: Department of Environment & Natural Resources Telephone: 877-623-6748 Last EDR Contact: 05/08/2019 Next Scheduled EDR Contact: 08/19/2019 Data Release Frequency: Quarterly LUST: Regional UST Database This database contains information obtained from the Regional Offices. It provides a more detailed explanation of current and historic activity for individual sites, as well as what was previously found in the Incident Management Database. Sites in this database with Incident Numbers are considered LUSTs. Date of Government Version: 05/03/2019 Date Data Arrived at EDR: 05/08/2019 Date Made Active in Reports: 07/11/2019 Number of Days to Update: 64 Source: Department of Environment and Natural Resources Telephone: 919-707-8200 Last EDR Contact: 05/08/2019 Next Scheduled EDR Contact: 08/19/2019 Data Release Frequency: Quarterly INDIAN LUST R5: Leaking Underground Storage Tanks on Indian Land Leaking underground storage tanks located on Indian Land in Michigan, Minnesota and Wisconsin. Date of Government Version: 10/12/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA, Region 5 Telephone: 312-886-7439 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN LUST R7: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Iowa, Kansas, and Nebraska Date of Government Version: 02/19/2019 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 7 Telephone: 913-551-7003 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies TC5716013.2s Page GR-6 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING INDIAN LUST R10: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Alaska, Idaho, Oregon and Washington. Date of Government Version: 10/17/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 10 Telephone: 206-553-2857 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN LUST R9: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Arizona, California, New Mexico and Nevada Date of Government Version: 10/10/2018 Date Data Arrived at EDR: 03/08/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 54 Source: Environmental Protection Agency Telephone: 415-972-3372 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN LUST R8: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Colorado, Montana, North Dakota, South Dakota, Utah and Wyoming. Date of Government Version: 10/16/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 8 Telephone: 303-312-6271 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN LUST R6: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in New Mexico and Oklahoma. Date of Government Version: 11/01/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 6 Telephone: 214-665-6597 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN LUST R4: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Florida, Mississippi and North Carolina. Date of Government Version: 09/24/2018 Date Data Arrived at EDR: 03/12/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 50 Source: EPA Region 4 Telephone: 404-562-8677 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN LUST R1: Leaking Underground Storage Tanks on Indian Land A listing of leaking underground storage tank locations on Indian Land. Date of Government Version: 10/13/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 1 Telephone: 617-918-1313 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies LUST TRUST: State Trust Fund Database This database contains information about claims against the State Trust Funds for reimbursements for expenses incurred while remediating Leaking USTs. Date of Government Version: 04/05/2019 Date Data Arrived at EDR: 04/10/2019 Date Made Active in Reports: 05/17/2019 Number of Days to Update: 37 Source: Department of Environment and Natural Resources Telephone: 919-733-1315 Last EDR Contact: 07/09/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Quarterly TC5716013.2s Page GR-7 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING State and tribal registered storage tank lists FEMA UST: Underground Storage Tank Listing A listing of all FEMA owned underground storage tanks. Date of Government Version: 05/15/2017 Date Data Arrived at EDR: 05/30/2017 Date Made Active in Reports: 10/13/2017 Number of Days to Update: 136 Source: FEMA Telephone: 202-646-5797 Last EDR Contact: 07/10/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Varies UST: Petroleum Underground Storage Tank Database Registered Underground Storage Tanks. UST’s are regulated under Subtitle I of the Resource Conservation and Recovery Act (RCRA) and must be registered with the state department responsible for administering the UST program. Available information varies by state program. Date of Government Version: 05/03/2019 Date Data Arrived at EDR: 05/08/2019 Date Made Active in Reports: 07/11/2019 Number of Days to Update: 64 Source: Department of Environment and Natural Resources Telephone: 919-733-1308 Last EDR Contact: 05/09/2019 Next Scheduled EDR Contact: 08/19/2019 Data Release Frequency: Quarterly AST: AST Database Facilities with aboveground storage tanks that have a capacity greater than 21,000 gallons. Date of Government Version: 03/08/2019 Date Data Arrived at EDR: 03/21/2019 Date Made Active in Reports: 05/16/2019 Number of Days to Update: 56 Source: Department of Environment and Natural Resources Telephone: 919-715-6183 Last EDR Contact: 06/17/2019 Next Scheduled EDR Contact: 09/30/2019 Data Release Frequency: Semi-Annually INDIAN UST R7: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 7 (Iowa, Kansas, Missouri, Nebraska, and 9 Tribal Nations). Date of Government Version: 11/07/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 7 Telephone: 913-551-7003 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN UST R5: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 5 (Michigan, Minnesota and Wisconsin and Tribal Nations). Date of Government Version: 10/12/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 5 Telephone: 312-886-6136 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN UST R4: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 4 (Alabama, Florida, Georgia, Kentucky, Mississippi, North Carolina, South Carolina, Tennessee and Tribal Nations) Date of Government Version: 09/24/2018 Date Data Arrived at EDR: 03/12/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 50 Source: EPA Region 4 Telephone: 404-562-9424 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies TC5716013.2s Page GR-8 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING INDIAN UST R1: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 1 (Connecticut, Maine, Massachusetts, New Hampshire, Rhode Island, Vermont and ten Tribal Nations). Date of Government Version: 10/03/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA, Region 1 Telephone: 617-918-1313 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN UST R9: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 9 (Arizona, California, Hawaii, Nevada, the Pacific Islands, and Tribal Nations). Date of Government Version: 10/10/2018 Date Data Arrived at EDR: 03/08/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 54 Source: EPA Region 9 Telephone: 415-972-3368 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN UST R6: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 6 (Louisiana, Arkansas, Oklahoma, New Mexico, Texas and 65 Tribes). Date of Government Version: 11/01/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 6 Telephone: 214-665-7591 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN UST R8: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 8 (Colorado, Montana, North Dakota, South Dakota, Utah, Wyoming and 27 Tribal Nations). Date of Government Version: 10/16/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 8 Telephone: 303-312-6137 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies INDIAN UST R10: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 10 (Alaska, Idaho, Oregon, Washington, and Tribal Nations). Date of Government Version: 10/17/2018 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 55 Source: EPA Region 10 Telephone: 206-553-2857 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies State and tribal institutional control / engineering control registries INST CONTROL: No Further Action Sites With Land Use Restrictions Monitoring A land use restricted site is a property where there are limits or requirements on future use of the property due to varying levels of cleanup possible, practical, or necessary at the site. Date of Government Version: 12/19/2018 Date Data Arrived at EDR: 03/13/2019 Date Made Active in Reports: 05/17/2019 Number of Days to Update: 65 Source: Department of Environment, Health and Natural Resources Telephone: 919-508-8400 Last EDR Contact: 06/12/2019 Next Scheduled EDR Contact: 09/23/2019 Data Release Frequency: Quarterly TC5716013.2s Page GR-9 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING State and tribal voluntary cleanup sites VCP: Responsible Party Voluntary Action Sites Responsible Party Voluntary Action site locations. Date of Government Version: 02/08/2019 Date Data Arrived at EDR: 03/13/2019 Date Made Active in Reports: 05/17/2019 Number of Days to Update: 65 Source: Department of Environment and Natural Resources Telephone: 919-508-8400 Last EDR Contact: 06/12/2019 Next Scheduled EDR Contact: 09/23/2019 Data Release Frequency: Quarterly INDIAN VCP R7: Voluntary Cleanup Priority Lisitng A listing of voluntary cleanup priority sites located on Indian Land located in Region 7. Date of Government Version: 03/20/2008 Date Data Arrived at EDR: 04/22/2008 Date Made Active in Reports: 05/19/2008 Number of Days to Update: 27 Source: EPA, Region 7 Telephone: 913-551-7365 Last EDR Contact: 04/20/2009 Next Scheduled EDR Contact: 07/20/2009 Data Release Frequency: Varies INDIAN VCP R1: Voluntary Cleanup Priority Listing A listing of voluntary cleanup priority sites located on Indian Land located in Region 1. Date of Government Version: 07/27/2015 Date Data Arrived at EDR: 09/29/2015 Date Made Active in Reports: 02/18/2016 Number of Days to Update: 142 Source: EPA, Region 1 Telephone: 617-918-1102 Last EDR Contact: 06/20/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Varies State and tribal Brownfields sites BROWNFIELDS: Brownfields Projects Inventory A brownfield site is an abandoned, idled, or underused property where the threat of environmental contamination has hindered its redevelopment. All of the sites in the inventory are working toward a brownfield agreement for cleanup and liabitliy control. Date of Government Version: 04/01/2019 Date Data Arrived at EDR: 04/03/2019 Date Made Active in Reports: 05/16/2019 Number of Days to Update: 43 Source: Department of Environment and Natural Resources Telephone: 919-733-4996 Last EDR Contact: 07/01/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Quarterly ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists US BROWNFIELDS: A Listing of Brownfields Sites Brownfields are real property, the expansion, redevelopment, or reuse of which may be complicated by the presence or potential presence of a hazardous substance, pollutant, or contaminant. Cleaning up and reinvesting in these properties takes development pressures off of undeveloped, open land, and both improves and protects the environment. Assessment, Cleanup and Redevelopment Exchange System (ACRES) stores information reported by EPA Brownfields grant recipients on brownfields properties assessed or cleaned up with grant funding as well as information on Targeted Brownfields Assessments performed by EPA Regions. A listing of ACRES Brownfield sites is obtained from Cleanups in My Community. Cleanups in My Community provides information on Brownfields properties for which information is reported back to EPA, as well as areas served by Brownfields grant programs. Date of Government Version: 12/17/2018 Date Data Arrived at EDR: 12/18/2018 Date Made Active in Reports: 01/11/2019 Number of Days to Update: 24 Source: Environmental Protection Agency Telephone: 202-566-2777 Last EDR Contact: 06/04/2019 Next Scheduled EDR Contact: 09/30/2019 Data Release Frequency: Semi-Annually TC5716013.2s Page GR-10 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Local Lists of Landfill / Solid Waste Disposal Sites SWRCY: Recycling Center Listing A listing of recycling center locations. Date of Government Version: 05/06/2019 Date Data Arrived at EDR: 05/07/2019 Date Made Active in Reports: 07/11/2019 Number of Days to Update: 65 Source: Department of Environment & Natural Resources Telephone: 919-707-8137 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/12/2019 Data Release Frequency: Varies HIST LF: Solid Waste Facility Listing A listing of solid waste facilities. Date of Government Version: 11/06/2006 Date Data Arrived at EDR: 02/13/2007 Date Made Active in Reports: 03/02/2007 Number of Days to Update: 17 Source: Department of Environment & Natural Resources Telephone: 919-733-0692 Last EDR Contact: 01/19/2009 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned INDIAN ODI: Report on the Status of Open Dumps on Indian Lands Location of open dumps on Indian land. Date of Government Version: 12/31/1998 Date Data Arrived at EDR: 12/03/2007 Date Made Active in Reports: 01/24/2008 Number of Days to Update: 52 Source: Environmental Protection Agency Telephone: 703-308-8245 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/12/2019 Data Release Frequency: Varies ODI: Open Dump Inventory An open dump is defined as a disposal facility that does not comply with one or more of the Part 257 or Part 258 Subtitle D Criteria. Date of Government Version: 06/30/1985 Date Data Arrived at EDR: 08/09/2004 Date Made Active in Reports: 09/17/2004 Number of Days to Update: 39 Source: Environmental Protection Agency Telephone: 800-424-9346 Last EDR Contact: 06/09/2004 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned DEBRIS REGION 9: Torres Martinez Reservation Illegal Dump Site Locations A listing of illegal dump sites location on the Torres Martinez Indian Reservation located in eastern Riverside County and northern Imperial County, California. Date of Government Version: 01/12/2009 Date Data Arrived at EDR: 05/07/2009 Date Made Active in Reports: 09/21/2009 Number of Days to Update: 137 Source: EPA, Region 9 Telephone: 415-947-4219 Last EDR Contact: 04/22/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: No Update Planned IHS OPEN DUMPS: Open Dumps on Indian Land A listing of all open dumps located on Indian Land in the United States. Date of Government Version: 04/01/2014 Date Data Arrived at EDR: 08/06/2014 Date Made Active in Reports: 01/29/2015 Number of Days to Update: 176 Source: Department of Health & Human Serivces, Indian Health Service Telephone: 301-443-1452 Last EDR Contact: 04/23/2019 Next Scheduled EDR Contact: 08/12/2019 Data Release Frequency: Varies Local Lists of Hazardous waste / Contaminated Sites TC5716013.2s Page GR-11 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING US HIST CDL: National Clandestine Laboratory Register A listing of clandestine drug lab locations that have been removed from the DEAs National Clandestine Laboratory Register. Date of Government Version: 02/24/2019 Date Data Arrived at EDR: 02/26/2019 Date Made Active in Reports: 04/17/2019 Number of Days to Update: 50 Source: Drug Enforcement Administration Telephone: 202-307-1000 Last EDR Contact: 05/24/2019 Next Scheduled EDR Contact: 09/09/2019 Data Release Frequency: No Update Planned US CDL: Clandestine Drug Labs A listing of clandestine drug lab locations. The U.S. Department of Justice ("the Department") provides this web site as a public service. It contains addresses of some locations where law enforcement agencies reported they found chemicals or other items that indicated the presence of either clandestine drug laboratories or dumpsites. In most cases, the source of the entries is not the Department, and the Department has not verified the entry and does not guarantee its accuracy. Members of the public must verify the accuracy of all entries by, for example, contacting local law enforcement and local health departments. Date of Government Version: 02/24/2019 Date Data Arrived at EDR: 02/26/2019 Date Made Active in Reports: 04/17/2019 Number of Days to Update: 50 Source: Drug Enforcement Administration Telephone: 202-307-1000 Last EDR Contact: 05/24/2019 Next Scheduled EDR Contact: 09/09/2019 Data Release Frequency: Quarterly Local Land Records LIENS 2: CERCLA Lien Information A Federal CERCLA (’Superfund’) lien can exist by operation of law at any site or property at which EPA has spent Superfund monies. These monies are spent to investigate and address releases and threatened releases of contamination. CERCLIS provides information as to the identity of these sites and properties. Date of Government Version: 04/11/2019 Date Data Arrived at EDR: 04/18/2019 Date Made Active in Reports: 05/23/2019 Number of Days to Update: 35 Source: Environmental Protection Agency Telephone: 202-564-6023 Last EDR Contact: 07/02/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Semi-Annually Records of Emergency Release Reports HMIRS: Hazardous Materials Information Reporting System Hazardous Materials Incident Report System. HMIRS contains hazardous material spill incidents reported to DOT. Date of Government Version: 03/25/2019 Date Data Arrived at EDR: 03/26/2019 Date Made Active in Reports: 05/14/2019 Number of Days to Update: 49 Source: U.S. Department of Transportation Telephone: 202-366-4555 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Quarterly SPILLS: Spills Incident Listing A listing spills, hazardous material releases, sanitary sewer overflows, wastewater treatment plant bypasses and upsets, citizen complaints, and any other environmental emergency calls reported to the agency. Date of Government Version: 12/12/2018 Date Data Arrived at EDR: 12/17/2018 Date Made Active in Reports: 12/18/2018 Number of Days to Update: 1 Source: Department of Environment & Natural Resources Telephone: 919-807-6308 Last EDR Contact: 07/08/2019 Next Scheduled EDR Contact: 09/23/2019 Data Release Frequency: Quarterly IMD: Incident Management Database Groundwater and/or soil contamination incidents TC5716013.2s Page GR-12 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 07/21/2006 Date Data Arrived at EDR: 08/01/2006 Date Made Active in Reports: 08/23/2006 Number of Days to Update: 22 Source: Department of Environment and Natural Resources Telephone: 877-623-6748 Last EDR Contact: 07/01/2011 Next Scheduled EDR Contact: 10/17/2011 Data Release Frequency: No Update Planned SPILLS 90: SPILLS90 data from FirstSearch Spills 90 includes those spill and release records available exclusively from FirstSearch databases. Typically, they may include chemical, oil and/or hazardous substance spills recorded after 1990. Duplicate records that are already included in EDR incident and release records are not included in Spills 90. Date of Government Version: 09/27/2012 Date Data Arrived at EDR: 01/03/2013 Date Made Active in Reports: 03/06/2013 Number of Days to Update: 62 Source: FirstSearch Telephone: N/A Last EDR Contact: 01/03/2013 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned SPILLS 80: SPILLS80 data from FirstSearch Spills 80 includes those spill and release records available from FirstSearch databases prior to 1990. Typically, they may include chemical, oil and/or hazardous substance spills recorded before 1990. Duplicate records that are already included in EDR incident and release records are not included in Spills 80. Date of Government Version: 06/14/2001 Date Data Arrived at EDR: 01/03/2013 Date Made Active in Reports: 03/06/2013 Number of Days to Update: 62 Source: FirstSearch Telephone: N/A Last EDR Contact: 01/03/2013 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned Other Ascertainable Records RCRA NonGen / NLR: RCRA - Non Generators / No Longer Regulated RCRAInfo is EPA’s comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Non-Generators do not presently generate hazardous waste. Date of Government Version: 03/25/2019 Date Data Arrived at EDR: 03/27/2019 Date Made Active in Reports: 04/17/2019 Number of Days to Update: 21 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Quarterly FUDS: Formerly Used Defense Sites The listing includes locations of Formerly Used Defense Sites properties where the US Army Corps of Engineers is actively working or will take necessary cleanup actions. Date of Government Version: 03/07/2019 Date Data Arrived at EDR: 04/03/2019 Date Made Active in Reports: 05/23/2019 Number of Days to Update: 50 Source: U.S. Army Corps of Engineers Telephone: 202-528-4285 Last EDR Contact: 05/21/2019 Next Scheduled EDR Contact: 09/02/2019 Data Release Frequency: Varies DOD: Department of Defense Sites This data set consists of federally owned or administered lands, administered by the Department of Defense, that have any area equal to or greater than 640 acres of the United States, Puerto Rico, and the U.S. Virgin Islands. Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 11/10/2006 Date Made Active in Reports: 01/11/2007 Number of Days to Update: 62 Source: USGS Telephone: 888-275-8747 Last EDR Contact: 07/09/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Semi-Annually TC5716013.2s Page GR-13 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING FEDLAND: Federal and Indian Lands Federally and Indian administrated lands of the United States. Lands included are administrated by: Army Corps of Engineers, Bureau of Reclamation, National Wild and Scenic River, National Wildlife Refuge, Public Domain Land, Wilderness, Wilderness Study Area, Wildlife Management Area, Bureau of Indian Affairs, Bureau of Land Management, Department of Justice, Forest Service, Fish and Wildlife Service, National Park Service. Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 02/06/2006 Date Made Active in Reports: 01/11/2007 Number of Days to Update: 339 Source: U.S. Geological Survey Telephone: 888-275-8747 Last EDR Contact: 07/10/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: N/A SCRD DRYCLEANERS: State Coalition for Remediation of Drycleaners Listing The State Coalition for Remediation of Drycleaners was established in 1998, with support from the U.S. EPA Office of Superfund Remediation and Technology Innovation. It is comprised of representatives of states with established drycleaner remediation programs. Currently the member states are Alabama, Connecticut, Florida, Illinois, Kansas, Minnesota, Missouri, North Carolina, Oregon, South Carolina, Tennessee, Texas, and Wisconsin. Date of Government Version: 01/01/2017 Date Data Arrived at EDR: 02/03/2017 Date Made Active in Reports: 04/07/2017 Number of Days to Update: 63 Source: Environmental Protection Agency Telephone: 615-532-8599 Last EDR Contact: 05/13/2019 Next Scheduled EDR Contact: 08/26/2019 Data Release Frequency: Varies US FIN ASSUR: Financial Assurance Information All owners and operators of facilities that treat, store, or dispose of hazardous waste are required to provide proof that they will have sufficient funds to pay for the clean up, closure, and post-closure care of their facilities. Date of Government Version: 03/25/2019 Date Data Arrived at EDR: 03/26/2019 Date Made Active in Reports: 05/07/2019 Number of Days to Update: 42 Source: Environmental Protection Agency Telephone: 202-566-1917 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Quarterly EPA WATCH LIST: EPA WATCH LIST EPA maintains a "Watch List" to facilitate dialogue between EPA, state and local environmental agencies on enforcement matters relating to facilities with alleged violations identified as either significant or high priority. Being on the Watch List does not mean that the facility has actually violated the law only that an investigation by EPA or a state or local environmental agency has led those organizations to allege that an unproven violation has in fact occurred. Being on the Watch List does not represent a higher level of concern regarding the alleged violations that were detected, but instead indicates cases requiring additional dialogue between EPA, state and local agencies - primarily because of the length of time the alleged violation has gone unaddressed or unresolved. Date of Government Version: 08/30/2013 Date Data Arrived at EDR: 03/21/2014 Date Made Active in Reports: 06/17/2014 Number of Days to Update: 88 Source: Environmental Protection Agency Telephone: 617-520-3000 Last EDR Contact: 05/06/2019 Next Scheduled EDR Contact: 08/19/2019 Data Release Frequency: Quarterly 2020 COR ACTION: 2020 Corrective Action Program List The EPA has set ambitious goals for the RCRA Corrective Action program by creating the 2020 Corrective Action Universe. This RCRA cleanup baseline includes facilities expected to need corrective action. The 2020 universe contains a wide variety of sites. Some properties are heavily contaminated while others were contaminated but have since been cleaned up. Still others have not been fully investigated yet, and may require little or no remediation. Inclusion in the 2020 Universe does not necessarily imply failure on the part of a facility to meet its RCRA obligations. Date of Government Version: 09/30/2017 Date Data Arrived at EDR: 05/08/2018 Date Made Active in Reports: 07/20/2018 Number of Days to Update: 73 Source: Environmental Protection Agency Telephone: 703-308-4044 Last EDR Contact: 05/10/2019 Next Scheduled EDR Contact: 08/19/2019 Data Release Frequency: Varies TC5716013.2s Page GR-14 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING TSCA: Toxic Substances Control Act Toxic Substances Control Act. TSCA identifies manufacturers and importers of chemical substances included on the TSCA Chemical Substance Inventory list. It includes data on the production volume of these substances by plant site. Date of Government Version: 12/31/2016 Date Data Arrived at EDR: 06/21/2017 Date Made Active in Reports: 01/05/2018 Number of Days to Update: 198 Source: EPA Telephone: 202-260-5521 Last EDR Contact: 06/18/2019 Next Scheduled EDR Contact: 09/30/2019 Data Release Frequency: Every 4 Years TRIS: Toxic Chemical Release Inventory System Toxic Release Inventory System. TRIS identifies facilities which release toxic chemicals to the air, water and land in reportable quantities under SARA Title III Section 313. Date of Government Version: 12/31/2016 Date Data Arrived at EDR: 01/10/2018 Date Made Active in Reports: 01/12/2018 Number of Days to Update: 2 Source: EPA Telephone: 202-566-0250 Last EDR Contact: 05/24/2019 Next Scheduled EDR Contact: 09/02/2019 Data Release Frequency: Annually SSTS: Section 7 Tracking Systems Section 7 of the Federal Insecticide, Fungicide and Rodenticide Act, as amended (92 Stat. 829) requires all registered pesticide-producing establishments to submit a report to the Environmental Protection Agency by March 1st each year. Each establishment must report the types and amounts of pesticides, active ingredients and devices being produced, and those having been produced and sold or distributed in the past year. Date of Government Version: 12/31/2009 Date Data Arrived at EDR: 12/10/2010 Date Made Active in Reports: 02/25/2011 Number of Days to Update: 77 Source: EPA Telephone: 202-564-4203 Last EDR Contact: 04/24/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Annually ROD: Records Of Decision Record of Decision. ROD documents mandate a permanent remedy at an NPL (Superfund) site containing technical and health information to aid in the cleanup. Date of Government Version: 04/11/2019 Date Data Arrived at EDR: 04/18/2019 Date Made Active in Reports: 05/23/2019 Number of Days to Update: 35 Source: EPA Telephone: 703-416-0223 Last EDR Contact: 07/01/2019 Next Scheduled EDR Contact: 09/16/2019 Data Release Frequency: Annually RMP: Risk Management Plans TC5716013.2s Page GR-15 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING When Congress passed the Clean Air Act Amendments of 1990, it required EPA to publish regulations and guidance for chemical accident prevention at facilities using extremely hazardous substances. The Risk Management Program Rule (RMP Rule) was written to implement Section 112(r) of these amendments. The rule, which built upon existing industry codes and standards, requires companies of all sizes that use certain flammable and toxic substances to develop a Risk Management Program, which includes a(n): Hazard assessment that details the potential effects of an accidental release, an accident history of the last five years, and an evaluation of worst-case and alternative accidental releases; Prevention program that includes safety precautions and maintenance, monitoring, and employee training measures; and Emergency response program that spells out emergency health care, employee training measures and procedures for informing the public and response agencies (e.g the fire department) should an accident occur. Date of Government Version: 04/25/2019 Date Data Arrived at EDR: 05/02/2019 Date Made Active in Reports: 05/23/2019 Number of Days to Update: 21 Source: Environmental Protection Agency Telephone: 202-564-8600 Last EDR Contact: 04/22/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies RAATS: RCRA Administrative Action Tracking System RCRA Administration Action Tracking System. RAATS contains records based on enforcement actions issued under RCRA pertaining to major violators and includes administrative and civil actions brought by the EPA. For administration actions after September 30, 1995, data entry in the RAATS database was discontinued. EPA will retain a copy of the database for historical records. It was necessary to terminate RAATS because a decrease in agency resources made it impossible to continue to update the information contained in the database. Date of Government Version: 04/17/1995 Date Data Arrived at EDR: 07/03/1995 Date Made Active in Reports: 08/07/1995 Number of Days to Update: 35 Source: EPA Telephone: 202-564-4104 Last EDR Contact: 06/02/2008 Next Scheduled EDR Contact: 09/01/2008 Data Release Frequency: No Update Planned PRP: Potentially Responsible Parties A listing of verified Potentially Responsible Parties Date of Government Version: 04/11/2019 Date Data Arrived at EDR: 04/18/2019 Date Made Active in Reports: 05/23/2019 Number of Days to Update: 35 Source: EPA Telephone: 202-564-6023 Last EDR Contact: 07/01/2019 Next Scheduled EDR Contact: 08/19/2019 Data Release Frequency: Quarterly PADS: PCB Activity Database System PCB Activity Database. PADS Identifies generators, transporters, commercial storers and/or brokers and disposers of PCB’s who are required to notify the EPA of such activities. Date of Government Version: 03/20/2019 Date Data Arrived at EDR: 04/10/2019 Date Made Active in Reports: 05/14/2019 Number of Days to Update: 34 Source: EPA Telephone: 202-566-0500 Last EDR Contact: 07/12/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Annually ICIS: Integrated Compliance Information System The Integrated Compliance Information System (ICIS) supports the information needs of the national enforcement and compliance program as well as the unique needs of the National Pollutant Discharge Elimination System (NPDES) program. Date of Government Version: 11/18/2016 Date Data Arrived at EDR: 11/23/2016 Date Made Active in Reports: 02/10/2017 Number of Days to Update: 79 Source: Environmental Protection Agency Telephone: 202-564-2501 Last EDR Contact: 07/03/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Quarterly TC5716013.2s Page GR-16 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING FTTS: FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) FTTS tracks administrative cases and pesticide enforcement actions and compliance activities related to FIFRA, TSCA and EPCRA (Emergency Planning and Community Right-to-Know Act). To maintain currency, EDR contacts the Agency on a quarterly basis. Date of Government Version: 04/09/2009 Date Data Arrived at EDR: 04/16/2009 Date Made Active in Reports: 05/11/2009 Number of Days to Update: 25 Source: EPA/Office of Prevention, Pesticides and Toxic Substances Telephone: 202-566-1667 Last EDR Contact: 08/18/2017 Next Scheduled EDR Contact: 12/04/2017 Data Release Frequency: No Update Planned FTTS INSP: FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) A listing of FIFRA/TSCA Tracking System (FTTS) inspections and enforcements. Date of Government Version: 04/09/2009 Date Data Arrived at EDR: 04/16/2009 Date Made Active in Reports: 05/11/2009 Number of Days to Update: 25 Source: EPA Telephone: 202-566-1667 Last EDR Contact: 08/18/2017 Next Scheduled EDR Contact: 12/04/2017 Data Release Frequency: No Update Planned MLTS: Material Licensing Tracking System MLTS is maintained by the Nuclear Regulatory Commission and contains a list of approximately 8,100 sites which possess or use radioactive materials and which are subject to NRC licensing requirements. To maintain currency, EDR contacts the Agency on a quarterly basis. Date of Government Version: 08/30/2016 Date Data Arrived at EDR: 09/08/2016 Date Made Active in Reports: 10/21/2016 Number of Days to Update: 43 Source: Nuclear Regulatory Commission Telephone: 301-415-7169 Last EDR Contact: 04/22/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Quarterly COAL ASH DOE: Steam-Electric Plant Operation Data A listing of power plants that store ash in surface ponds. Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 08/07/2009 Date Made Active in Reports: 10/22/2009 Number of Days to Update: 76 Source: Department of Energy Telephone: 202-586-8719 Last EDR Contact: 06/07/2019 Next Scheduled EDR Contact: 09/16/2019 Data Release Frequency: Varies COAL ASH EPA: Coal Combustion Residues Surface Impoundments List A listing of coal combustion residues surface impoundments with high hazard potential ratings. Date of Government Version: 07/01/2014 Date Data Arrived at EDR: 09/10/2014 Date Made Active in Reports: 10/20/2014 Number of Days to Update: 40 Source: Environmental Protection Agency Telephone: N/A Last EDR Contact: 06/07/2019 Next Scheduled EDR Contact: 09/16/2019 Data Release Frequency: Varies PCB TRANSFORMER: PCB Transformer Registration Database The database of PCB transformer registrations that includes all PCB registration submittals. Date of Government Version: 05/24/2017 Date Data Arrived at EDR: 11/30/2017 Date Made Active in Reports: 12/15/2017 Number of Days to Update: 15 Source: Environmental Protection Agency Telephone: 202-566-0517 Last EDR Contact: 04/26/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies RADINFO: Radiation Information Database The Radiation Information Database (RADINFO) contains information about facilities that are regulated by U.S. Environmental Protection Agency (EPA) regulations for radiation and radioactivity. TC5716013.2s Page GR-17 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 04/02/2019 Date Data Arrived at EDR: 04/02/2019 Date Made Active in Reports: 05/14/2019 Number of Days to Update: 42 Source: Environmental Protection Agency Telephone: 202-343-9775 Last EDR Contact: 07/01/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Quarterly HIST FTTS: FIFRA/TSCA Tracking System Administrative Case Listing A complete administrative case listing from the FIFRA/TSCA Tracking System (FTTS) for all ten EPA regions. The information was obtained from the National Compliance Database (NCDB). NCDB supports the implementation of FIFRA (Federal Insecticide, Fungicide, and Rodenticide Act) and TSCA (Toxic Substances Control Act). Some EPA regions are now closing out records. Because of that, and the fact that some EPA regions are not providing EPA Headquarters with updated records, it was decided to create a HIST FTTS database. It included records that may not be included in the newer FTTS database updates. This database is no longer updated. Date of Government Version: 10/19/2006 Date Data Arrived at EDR: 03/01/2007 Date Made Active in Reports: 04/10/2007 Number of Days to Update: 40 Source: Environmental Protection Agency Telephone: 202-564-2501 Last EDR Contact: 12/17/2007 Next Scheduled EDR Contact: 03/17/2008 Data Release Frequency: No Update Planned HIST FTTS INSP: FIFRA/TSCA Tracking System Inspection & Enforcement Case Listing A complete inspection and enforcement case listing from the FIFRA/TSCA Tracking System (FTTS) for all ten EPA regions. The information was obtained from the National Compliance Database (NCDB). NCDB supports the implementation of FIFRA (Federal Insecticide, Fungicide, and Rodenticide Act) and TSCA (Toxic Substances Control Act). Some EPA regions are now closing out records. Because of that, and the fact that some EPA regions are not providing EPA Headquarters with updated records, it was decided to create a HIST FTTS database. It included records that may not be included in the newer FTTS database updates. This database is no longer updated. Date of Government Version: 10/19/2006 Date Data Arrived at EDR: 03/01/2007 Date Made Active in Reports: 04/10/2007 Number of Days to Update: 40 Source: Environmental Protection Agency Telephone: 202-564-2501 Last EDR Contact: 12/17/2008 Next Scheduled EDR Contact: 03/17/2008 Data Release Frequency: No Update Planned DOT OPS: Incident and Accident Data Department of Transporation, Office of Pipeline Safety Incident and Accident data. Date of Government Version: 12/03/2018 Date Data Arrived at EDR: 01/29/2019 Date Made Active in Reports: 03/21/2019 Number of Days to Update: 51 Source: Department of Transporation, Office of Pipeline Safety Telephone: 202-366-4595 Last EDR Contact: 04/30/2019 Next Scheduled EDR Contact: 08/12/2019 Data Release Frequency: Quarterly CONSENT: Superfund (CERCLA) Consent Decrees Major legal settlements that establish responsibility and standards for cleanup at NPL (Superfund) sites. Released periodically by United States District Courts after settlement by parties to litigation matters. Date of Government Version: 03/31/2019 Date Data Arrived at EDR: 04/23/2019 Date Made Active in Reports: 05/23/2019 Number of Days to Update: 30 Source: Department of Justice, Consent Decree Library Telephone: Varies Last EDR Contact: 07/08/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Varies BRS: Biennial Reporting System The Biennial Reporting System is a national system administered by the EPA that collects data on the generation and management of hazardous waste. BRS captures detailed data from two groups: Large Quantity Generators (LQG) and Treatment, Storage, and Disposal Facilities. Date of Government Version: 12/31/2015 Date Data Arrived at EDR: 02/22/2017 Date Made Active in Reports: 09/28/2017 Number of Days to Update: 218 Source: EPA/NTIS Telephone: 800-424-9346 Last EDR Contact: 06/26/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Biennially TC5716013.2s Page GR-18 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING INDIAN RESERV: Indian Reservations This map layer portrays Indian administered lands of the United States that have any area equal to or greater than 640 acres. Date of Government Version: 12/31/2014 Date Data Arrived at EDR: 07/14/2015 Date Made Active in Reports: 01/10/2017 Number of Days to Update: 546 Source: USGS Telephone: 202-208-3710 Last EDR Contact: 07/10/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Semi-Annually FUSRAP: Formerly Utilized Sites Remedial Action Program DOE established the Formerly Utilized Sites Remedial Action Program (FUSRAP) in 1974 to remediate sites where radioactive contamination remained from Manhattan Project and early U.S. Atomic Energy Commission (AEC) operations. Date of Government Version: 08/08/2017 Date Data Arrived at EDR: 09/11/2018 Date Made Active in Reports: 09/14/2018 Number of Days to Update: 3 Source: Department of Energy Telephone: 202-586-3559 Last EDR Contact: 05/02/2019 Next Scheduled EDR Contact: 08/19/2019 Data Release Frequency: Varies UMTRA: Uranium Mill Tailings Sites Uranium ore was mined by private companies for federal government use in national defense programs. When the mills shut down, large piles of the sand-like material (mill tailings) remain after uranium has been extracted from the ore. Levels of human exposure to radioactive materials from the piles are low; however, in some cases tailings were used as construction materials before the potential health hazards of the tailings were recognized. Date of Government Version: 06/23/2017 Date Data Arrived at EDR: 10/11/2017 Date Made Active in Reports: 11/03/2017 Number of Days to Update: 23 Source: Department of Energy Telephone: 505-845-0011 Last EDR Contact: 05/24/2019 Next Scheduled EDR Contact: 09/02/2019 Data Release Frequency: Varies LEAD SMELTER 1: Lead Smelter Sites A listing of former lead smelter site locations. Date of Government Version: 04/11/2019 Date Data Arrived at EDR: 04/18/2019 Date Made Active in Reports: 05/14/2019 Number of Days to Update: 26 Source: Environmental Protection Agency Telephone: 703-603-8787 Last EDR Contact: 07/01/2019 Next Scheduled EDR Contact: 10/14/2019 Data Release Frequency: Varies LEAD SMELTER 2: Lead Smelter Sites A list of several hundred sites in the U.S. where secondary lead smelting was done from 1931and 1964. These sites may pose a threat to public health through ingestion or inhalation of contaminated soil or dust Date of Government Version: 04/05/2001 Date Data Arrived at EDR: 10/27/2010 Date Made Active in Reports: 12/02/2010 Number of Days to Update: 36 Source: American Journal of Public Health Telephone: 703-305-6451 Last EDR Contact: 12/02/2009 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned US AIRS (AFS): Aerometric Information Retrieval System Facility Subsystem (AFS) The database is a sub-system of Aerometric Information Retrieval System (AIRS). AFS contains compliance data on air pollution point sources regulated by the U.S. EPA and/or state and local air regulatory agencies. This information comes from source reports by various stationary sources of air pollution, such as electric power plants, steel mills, factories, and universities, and provides information about the air pollutants they produce. Action, air program, air program pollutant, and general level plant data. It is used to track emissions and compliance data from industrial plants. TC5716013.2s Page GR-19 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 10/12/2016 Date Data Arrived at EDR: 10/26/2016 Date Made Active in Reports: 02/03/2017 Number of Days to Update: 100 Source: EPA Telephone: 202-564-2496 Last EDR Contact: 09/26/2017 Next Scheduled EDR Contact: 01/08/2018 Data Release Frequency: Annually US AIRS MINOR: Air Facility System Data A listing of minor source facilities. Date of Government Version: 10/12/2016 Date Data Arrived at EDR: 10/26/2016 Date Made Active in Reports: 02/03/2017 Number of Days to Update: 100 Source: EPA Telephone: 202-564-2496 Last EDR Contact: 09/26/2017 Next Scheduled EDR Contact: 01/08/2018 Data Release Frequency: Annually US MINES: Mines Master Index File Contains all mine identification numbers issued for mines active or opened since 1971. The data also includes violation information. Date of Government Version: 11/27/2018 Date Data Arrived at EDR: 02/27/2019 Date Made Active in Reports: 04/01/2019 Number of Days to Update: 33 Source: Department of Labor, Mine Safety and Health Administration Telephone: 303-231-5959 Last EDR Contact: 05/29/2019 Next Scheduled EDR Contact: 09/09/2019 Data Release Frequency: Semi-Annually US MINES 2: Ferrous and Nonferrous Metal Mines Database Listing This map layer includes ferrous (ferrous metal mines are facilities that extract ferrous metals, such as iron ore or molybdenum) and nonferrous (Nonferrous metal mines are facilities that extract nonferrous metals, such as gold, silver, copper, zinc, and lead) metal mines in the United States. Date of Government Version: 12/05/2005 Date Data Arrived at EDR: 02/29/2008 Date Made Active in Reports: 04/18/2008 Number of Days to Update: 49 Source: USGS Telephone: 703-648-7709 Last EDR Contact: 05/31/2019 Next Scheduled EDR Contact: 09/09/2019 Data Release Frequency: Varies US MINES 3: Active Mines & Mineral Plants Database Listing Active Mines and Mineral Processing Plant operations for commodities monitored by the Minerals Information Team of the USGS. Date of Government Version: 04/14/2011 Date Data Arrived at EDR: 06/08/2011 Date Made Active in Reports: 09/13/2011 Number of Days to Update: 97 Source: USGS Telephone: 703-648-7709 Last EDR Contact: 05/31/2019 Next Scheduled EDR Contact: 09/09/2019 Data Release Frequency: Varies ABANDONED MINES: Abandoned Mines An inventory of land and water impacted by past mining (primarily coal mining) is maintained by OSMRE to provide information needed to implement the Surface Mining Control and Reclamation Act of 1977 (SMCRA). The inventory contains information on the location, type, and extent of AML impacts, as well as, information on the cost associated with the reclamation of those problems. The inventory is based upon field surveys by State, Tribal, and OSMRE program officials. It is dynamic to the extent that it is modified as new problems are identified and existing problems are reclaimed. Date of Government Version: 03/27/2019 Date Data Arrived at EDR: 03/28/2019 Date Made Active in Reports: 05/01/2019 Number of Days to Update: 34 Source: Department of Interior Telephone: 202-208-2609 Last EDR Contact: 06/19/2019 Next Scheduled EDR Contact: 09/23/2019 Data Release Frequency: Quarterly TC5716013.2s Page GR-20 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING FINDS: Facility Index System/Facility Registry System Facility Index System. FINDS contains both facility information and ’pointers’ to other sources that contain more detail. EDR includes the following FINDS databases in this report: PCS (Permit Compliance System), AIRS (Aerometric Information Retrieval System), DOCKET (Enforcement Docket used to manage and track information on civil judicial enforcement cases for all environmental statutes), FURS (Federal Underground Injection Control), C-DOCKET (Criminal Docket System used to track criminal enforcement actions for all environmental statutes), FFIS (Federal Facilities Information System), STATE (State Environmental Laws and Statutes), and PADS (PCB Activity Data System). Date of Government Version: 02/15/2019 Date Data Arrived at EDR: 03/05/2019 Date Made Active in Reports: 03/15/2019 Number of Days to Update: 10 Source: EPA Telephone: (404) 562-9900 Last EDR Contact: 06/05/2019 Next Scheduled EDR Contact: 09/16/2019 Data Release Frequency: Quarterly UXO: Unexploded Ordnance Sites A listing of unexploded ordnance site locations Date of Government Version: 12/31/2017 Date Data Arrived at EDR: 01/17/2019 Date Made Active in Reports: 04/01/2019 Number of Days to Update: 74 Source: Department of Defense Telephone: 703-704-1564 Last EDR Contact: 04/15/2019 Next Scheduled EDR Contact: 07/29/2019 Data Release Frequency: Varies DOCKET HWC: Hazardous Waste Compliance Docket Listing A complete list of the Federal Agency Hazardous Waste Compliance Docket Facilities. Date of Government Version: 05/31/2018 Date Data Arrived at EDR: 07/26/2018 Date Made Active in Reports: 10/05/2018 Number of Days to Update: 71 Source: Environmental Protection Agency Telephone: 202-564-0527 Last EDR Contact: 05/24/2019 Next Scheduled EDR Contact: 09/09/2019 Data Release Frequency: Varies ECHO: Enforcement & Compliance History Information ECHO provides integrated compliance and enforcement information for about 800,000 regulated facilities nationwide. Date of Government Version: 04/07/2019 Date Data Arrived at EDR: 04/09/2019 Date Made Active in Reports: 05/23/2019 Number of Days to Update: 44 Source: Environmental Protection Agency Telephone: 202-564-2280 Last EDR Contact: 07/09/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Quarterly FUELS PROGRAM: EPA Fuels Program Registered Listing This listing includes facilities that are registered under the Part 80 (Code of Federal Regulations) EPA Fuels Programs. All companies now are required to submit new and updated registrations. Date of Government Version: 02/19/2019 Date Data Arrived at EDR: 02/21/2019 Date Made Active in Reports: 04/01/2019 Number of Days to Update: 39 Source: EPA Telephone: 800-385-6164 Last EDR Contact: 05/21/2019 Next Scheduled EDR Contact: 09/02/2019 Data Release Frequency: Quarterly AIRS: Air Quality Permit Listing A listing of facilities with air quality permits. Date of Government Version: 03/11/2019 Date Data Arrived at EDR: 03/13/2019 Date Made Active in Reports: 05/16/2019 Number of Days to Update: 64 Source: Department of Environmental Quality Telephone: 919-707-8726 Last EDR Contact: 06/12/2019 Next Scheduled EDR Contact: 09/23/2019 Data Release Frequency: Varies TC5716013.2s Page GR-21 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING ASBESTOS: ASBESTOS Asbestos notification sites Date of Government Version: 01/31/2019 Date Data Arrived at EDR: 02/08/2019 Date Made Active in Reports: 03/25/2019 Number of Days to Update: 45 Source: Department of Health & Human Services Telephone: 919-707-5973 Last EDR Contact: 06/03/2019 Next Scheduled EDR Contact: 08/05/2019 Data Release Frequency: Varies COAL ASH: Coal Ash Disposal Sites A listing of coal combustion products distribution permits issued by the Division for the treatment, storage, transportation, use and disposal of coal combustion products. Date of Government Version: 02/25/2019 Date Data Arrived at EDR: 02/28/2019 Date Made Active in Reports: 05/16/2019 Number of Days to Update: 77 Source: Department of Environment & Natural Resources Telephone: 919-807-6359 Last EDR Contact: 06/24/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Varies DRYCLEANERS: Drycleaning Sites Potential and known drycleaning sites, active and abandoned, that the Drycleaning Solvent Cleanup Program has knowledge of and entered into this database. Date of Government Version: 10/24/2018 Date Data Arrived at EDR: 03/20/2019 Date Made Active in Reports: 05/17/2019 Number of Days to Update: 58 Source: Department of Environment & Natural Resources Telephone: 919-508-8400 Last EDR Contact: 06/21/2019 Next Scheduled EDR Contact: 09/30/2019 Data Release Frequency: Varies Financial Assurance 1: Financial Assurance Information Listing A listing of financial assurance information for underground storage tank facilities. Financial assurance is intended to ensure that resources are available to pay for the cost of closure, post-closure care, and corrective measures if the owner or operator of a regulated facility is unable or unwilling to pay. Date of Government Version: 05/03/2019 Date Data Arrived at EDR: 05/08/2019 Date Made Active in Reports: 07/11/2019 Number of Days to Update: 64 Source: Department of Environment & Natural Resources Telephone: 919-733-1322 Last EDR Contact: 05/08/2019 Next Scheduled EDR Contact: 08/19/2019 Data Release Frequency: Quarterly Financial Assurance 2: Financial Assurance Information Listing Information for solid waste facilities. Financial assurance is intended to ensure that resources are available to pay for the cost of closure, post-closure care, and corrective measures if the owner or operator of a regulated facility is unable or unwilling to pay. Date of Government Version: 10/02/2012 Date Data Arrived at EDR: 10/03/2012 Date Made Active in Reports: 10/26/2012 Number of Days to Update: 23 Source: Department of Environmental & Natural Resources Telephone: 919-508-8496 Last EDR Contact: 06/20/2019 Next Scheduled EDR Contact: 10/07/2019 Data Release Frequency: Varies Financial Assurance 3: Financial Assurance Information Hazardous waste financial assurance information. Date of Government Version: 06/11/2018 Date Data Arrived at EDR: 06/12/2018 Date Made Active in Reports: 07/25/2018 Number of Days to Update: 43 Source: Department of Environment & Natural Resources Telephone: 919-707-8222 Last EDR Contact: 06/10/2019 Next Scheduled EDR Contact: 09/23/2019 Data Release Frequency: Varies TC5716013.2s Page GR-22 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING NPDES: NPDES Facility Location Listing General information regarding NPDES(National Pollutant Discharge Elimination System) permits. Date of Government Version: 02/01/2019 Date Data Arrived at EDR: 05/01/2019 Date Made Active in Reports: 07/10/2019 Number of Days to Update: 70 Source: Department of Environment & Natural Resources Telephone: 919-733-7015 Last EDR Contact: 05/01/2019 Next Scheduled EDR Contact: 08/12/2019 Data Release Frequency: Varies UIC: Underground Injection Wells Listing A listing of uncerground injection wells locations. Date of Government Version: 03/05/2019 Date Data Arrived at EDR: 03/07/2019 Date Made Active in Reports: 05/17/2019 Number of Days to Update: 71 Source: Department of Environment & Natural Resources Telephone: 919-807-6412 Last EDR Contact: 06/03/2019 Next Scheduled EDR Contact: 09/16/2019 Data Release Frequency: Quarterly AOP: Animal Operation Permits Listing This listing includes animal operations that are required to be permitted by the state. Date of Government Version: 02/12/2019 Date Data Arrived at EDR: 03/15/2019 Date Made Active in Reports: 05/16/2019 Number of Days to Update: 62 Source: Department of Environmental Quality Telephone: 919-707-9129 Last EDR Contact: 06/14/2019 Next Scheduled EDR Contact: 09/23/2019 Data Release Frequency: Varies SEPT HAULERS: Permitted Septage Haulers Listing This list of all active and permitted Septage Land Application Site (SLAS) and Septage Detention and Treatment Facility (SDTF) sites in North Carolina. The purpose of this map is to provide the public and government entities a visual overview of the businesses that manage septage and septage facilities throughout the state. Date of Government Version: 07/23/2018 Date Data Arrived at EDR: 10/19/2018 Date Made Active in Reports: 01/04/2019 Number of Days to Update: 77 Source: Department of Environmental Quality Telephone: 919-707-8248 Last EDR Contact: 07/12/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Varies PCSRP: Petroleum-Contaminated Soil Remediation Permits To treat petroleum-contaminated soil in order to protect North Carolinaa??s environment and the health of the citizens of North Carolina. Date of Government Version: 01/08/2019 Date Data Arrived at EDR: 01/09/2019 Date Made Active in Reports: 03/26/2019 Number of Days to Update: 76 Source: Department of Environmental Quality Telephone: 919-707-8248 Last EDR Contact: 07/09/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Varies CCB: Coal Ash Structural Fills (CCB) Listing These are not permitted Coal Ash landfills A list all of the now closed Coal Ash Structural Fills (CCB) in North Carolina, in point data form. The purpose is to provide the public and other government entities a visual overview of coal ash structural fills throughout the state and increase public awareness of their current locations. Date of Government Version: 09/06/2018 Date Data Arrived at EDR: 01/09/2019 Date Made Active in Reports: 03/25/2019 Number of Days to Update: 75 Source: Department of Environmental Quality Telephone: 919-707-8248 Last EDR Contact: 07/12/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Varies TC5716013.2s Page GR-23 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR MGP: EDR Proprietary Manufactured Gas Plants The EDR Proprietary Manufactured Gas Plant Database includes records of coal gas plants (manufactured gas plants) compiled by EDR’s researchers. Manufactured gas sites were used in the United States from the 1800’s to 1950’s to produce a gas that could be distributed and used as fuel. These plants used whale oil, rosin, coal, or a mixture of coal, oil, and water that also produced a significant amount of waste. Many of the byproducts of the gas production, such as coal tar (oily waste containing volatile and non-volatile chemicals), sludges, oils and other compounds are potentially hazardous to human health and the environment. The byproduct from this process was frequently disposed of directly at the plant site and can remain or spread slowly, serving as a continuous source of soil and groundwater contamination. Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A Source: EDR, Inc. Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned EDR Hist Auto: EDR Exclusive Historical Auto Stations EDR has searched selected national collections of business directories and has collected listings of potential gas station/filling station/service station sites that were available to EDR researchers. EDR’s review was limited to those categories of sources that might, in EDR’s opinion, include gas station/filling station/service station establishments. The categories reviewed included, but were not limited to gas, gas station, gasoline station, filling station, auto, automobile repair, auto service station, service station, etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR’s HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A Source: EDR, Inc. Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: Varies EDR Hist Cleaner: EDR Exclusive Historical Cleaners EDR has searched selected national collections of business directories and has collected listings of potential dry cleaner sites that were available to EDR researchers. EDR’s review was limited to those categories of sources that might, in EDR’s opinion, include dry cleaning establishments. The categories reviewed included, but were not limited to dry cleaners, cleaners, laundry, laundromat, cleaning/laundry, wash & dry etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR’s HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A Source: EDR, Inc. Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: Varies EDR RECOVERED GOVERNMENT ARCHIVES Exclusive Recovered Govt. Archives RGA HWS: Recovered Government Archive State Hazardous Waste Facilities List The EDR Recovered Government Archive State Hazardous Waste database provides a list of SHWS incidents derived from historical databases and includes many records that no longer appear in current government lists. Compiled from Records formerly available from the Department of Environment, Health and Natural Resources in North Carolina. TC5716013.2s Page GR-24 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: N/A Date Data Arrived at EDR: 07/01/2013 Date Made Active in Reports: 12/24/2013 Number of Days to Update: 176 Source: Department of Environment, Health and Natural Resources Telephone: N/A Last EDR Contact: 06/01/2012 Next Scheduled EDR Contact: N/A Data Release Frequency: Varies RGA LF: Recovered Government Archive Solid Waste Facilities List The EDR Recovered Government Archive Landfill database provides a list of landfills derived from historical databases and includes many records that no longer appear in current government lists. Compiled from Records formerly available from the Department of Environment, Health and Natural Resources in North Carolina. Date of Government Version: N/A Date Data Arrived at EDR: 07/01/2013 Date Made Active in Reports: 01/13/2014 Number of Days to Update: 196 Source: Department of Environment, Health and Natural Resources Telephone: N/A Last EDR Contact: 06/01/2012 Next Scheduled EDR Contact: N/A Data Release Frequency: Varies RGA LUST: Recovered Government Archive Leaking Underground Storage Tank The EDR Recovered Government Archive Leaking Underground Storage Tank database provides a list of LUST incidents derived from historical databases and includes many records that no longer appear in current government lists. Compiled from Records formerly available from the Department of Environment, Health and Natural Resources in North Carolina. Date of Government Version: N/A Date Data Arrived at EDR: 07/01/2013 Date Made Active in Reports: 12/20/2013 Number of Days to Update: 172 Source: Department of Environment, Health and Natural Resources Telephone: N/A Last EDR Contact: 06/01/2012 Next Scheduled EDR Contact: N/A Data Release Frequency: Varies OTHER DATABASE(S) Depending on the geographic area covered by this report, the data provided in these specialty databases may or may not be complete. For example, the existence of wetlands information data in a specific report does not mean that all wetlands in the area covered by the report are included. Moreover, the absence of any reported wetlands information does not necessarily mean that wetlands do not exist in the area covered by the report. CT MANIFEST: Hazardous Waste Manifest Data Facility and manifest data. Manifest is a document that lists and tracks hazardous waste from the generator through transporters to a tsd facility. Date of Government Version: 02/11/2019 Date Data Arrived at EDR: 02/12/2019 Date Made Active in Reports: 03/04/2019 Number of Days to Update: 20 Source: Department of Energy & Environmental Protection Telephone: 860-424-3375 Last EDR Contact: 05/14/2019 Next Scheduled EDR Contact: 08/26/2019 Data Release Frequency: No Update Planned NJ MANIFEST: Manifest Information Hazardous waste manifest information. Date of Government Version: 12/31/2018 Date Data Arrived at EDR: 04/10/2019 Date Made Active in Reports: 05/16/2019 Number of Days to Update: 36 Source: Department of Environmental Protection Telephone: N/A Last EDR Contact: 07/09/2019 Next Scheduled EDR Contact: 10/21/2019 Data Release Frequency: Annually NY MANIFEST: Facility and Manifest Data Manifest is a document that lists and tracks hazardous waste from the generator through transporters to a TSD facility. TC5716013.2s Page GR-25 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Date of Government Version: 01/01/2019 Date Data Arrived at EDR: 05/01/2019 Date Made Active in Reports: 06/21/2019 Number of Days to Update: 51 Source: Department of Environmental Conservation Telephone: 518-402-8651 Last EDR Contact: 05/01/2019 Next Scheduled EDR Contact: 08/12/2019 Data Release Frequency: Quarterly PA MANIFEST: Manifest Information Hazardous waste manifest information. Date of Government Version: 12/31/2017 Date Data Arrived at EDR: 10/23/2018 Date Made Active in Reports: 11/27/2018 Number of Days to Update: 35 Source: Department of Environmental Protection Telephone: 717-783-8990 Last EDR Contact: 04/15/2019 Next Scheduled EDR Contact: 07/29/2019 Data Release Frequency: Annually RI MANIFEST: Manifest information Hazardous waste manifest information Date of Government Version: 12/31/2017 Date Data Arrived at EDR: 02/23/2018 Date Made Active in Reports: 04/09/2018 Number of Days to Update: 45 Source: Department of Environmental Management Telephone: 401-222-2797 Last EDR Contact: 05/17/2019 Next Scheduled EDR Contact: 09/02/2019 Data Release Frequency: Annually WI MANIFEST: Manifest Information Hazardous waste manifest information. Date of Government Version: 12/31/2017 Date Data Arrived at EDR: 06/15/2018 Date Made Active in Reports: 07/09/2018 Number of Days to Update: 24 Source: Department of Natural Resources Telephone: N/A Last EDR Contact: 06/10/2019 Next Scheduled EDR Contact: 09/23/2019 Data Release Frequency: Annually Oil/Gas Pipelines Source: PennWell Corporation Petroleum Bundle (Crude Oil, Refined Products, Petrochemicals, Gas Liquids (LPG/NGL), and Specialty Gases (Miscellaneous)) N = Natural Gas Bundle (Natural Gas, Gas Liquids (LPG/NGL), and Specialty Gases (Miscellaneous)). This map includes information copyrighted by PennWell Corporation. This information is provided on a best effort basis and PennWell Corporation does not guarantee its accuracy nor warrant its fitness for any particular purpose. Such information has been reprinted with the permission of PennWell. Electric Power Transmission Line Data Source: PennWell Corporation This map includes information copyrighted by PennWell Corporation. This information is provided on a best effort basis and PennWell Corporation does not guarantee its accuracy nor warrant its fitness for any particular purpose. Such information has been reprinted with the permission of PennWell. Sensitive Receptors: There are individuals deemed sensitive receptors due to their fragile immune systems and special sensitivity to environmental discharges. These sensitive receptors typically include the elderly, the sick, and children. While the location of all sensitive receptors cannot be determined, EDR indicates those buildings and facilities - schools, daycares, hospitals, medical centers, and nursing homes - where individuals who are sensitive receptors are likely to be located. AHA Hospitals: Source: American Hospital Association, Inc. Telephone: 312-280-5991 The database includes a listing of hospitals based on the American Hospital Association’s annual survey of hospitals. Medical Centers: Provider of Services Listing Source: Centers for Medicare & Medicaid Services Telephone: 410-786-3000 A listing of hospitals with Medicare provider number, produced by Centers of Medicare & Medicaid Services, a federal agency within the U.S. Department of Health and Human Services. Nursing Homes Source: National Institutes of Health Telephone: 301-594-6248 Information on Medicare and Medicaid certified nursing homes in the United States. TC5716013.2s Page GR-26 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING Public Schools Source: National Center for Education Statistics Telephone: 202-502-7300 The National Center for Education Statistics’ primary database on elementary and secondary public education in the United States. It is a comprehensive, annual, national statistical database of all public elementary and secondary schools and school districts, which contains data that are comparable across all states. Private Schools Source: National Center for Education Statistics Telephone: 202-502-7300 The National Center for Education Statistics’ primary database on private school locations in the United States. Daycare Centers: Child Care Facility List Source: Department of Health & Human Services Telephone: 919-662-4499 Flood Zone Data: This data was obtained from the Federal Emergency Management Agency (FEMA). It depicts 100-year and 500-year flood zones as defined by FEMA. It includes the National Flood Hazard Layer (NFHL) which incorporates Flood Insurance Rate Map (FIRM) data and Q3 data from FEMA in areas not covered by NFHL. Source: FEMA Telephone: 877-336-2627 Date of Government Version: 2003, 2015 NWI: National Wetlands Inventory. This data, available in select counties across the country, was obtained by EDR in 2002, 2005 and 2010 from the U.S. Fish and Wildlife Service. State Wetlands Data: Wetland Inventory Source: US Fish & Wildlife Service Telephone: 703-358-2171 Current USGS 7.5 Minute Topographic Map Source: U.S. Geological Survey STREET AND ADDRESS INFORMATION © 2015 TomTom North America, Inc. All rights reserved. This material is proprietary and the subject of copyright protection and other intellectual property rights owned by or licensed to Tele Atlas North America, Inc. The use of this material is subject to the terms of a license agreement. You will be held liable for any unauthorized copying or disclosure of this material. TC5716013.2s Page GR-27 GOVERNMENT RECORDS SEARCHED / DATA CURRENCY TRACKING TC5716013.2s Page A-1 geologic strata. of the soil, and nearby wells. Groundwater flow velocity is generally impacted by the nature of the Groundwater flow direction may be impacted by surface topography, hydrology, hydrogeology, characteristics 2. Groundwater flow velocity. 1. Groundwater flow direction, and Assessment of the impact of contaminant migration generally has two principle investigative components: forming an opinion about the impact of potential contaminant migration. EDR’s GeoCheck Physical Setting Source Addendum is provided to assist the environmental professional in 2013Version Date: 5948460 ASHEVILLE, NCTarget Property Map: USGS TOPOGRAPHIC MAP 2119 ft. above sea levelElevation: 3934184.0UTM Y (Meters): 362127.5UTM X (Meters): Zone 17Universal Tranverse Mercator: 82.520936 - 82˚ 31’ 15.37’’Longitude (West): 35.543513 - 35˚ 32’ 36.65’’Latitude (North): TARGET PROPERTY COORDINATES ASHEVILLE, NC 28803 1140 SWEETEN CREEK RD FORMER P.E. VALVE PROPERTY TARGET PROPERTY ADDRESS ®GEOCHECK - PHYSICAL SETTING SOURCE ADDENDUM® TC5716013.2s Page A-2 should be field verified. on a relative (not an absolute) basis. Relative elevation information between sites of close proximity Source: Topography has been determined from the USGS 7.5’ Digital Elevation Model and should be evaluated SURROUNDING TOPOGRAPHY: ELEVATION PROFILES Elevation (ft)Elevation (ft)TP TP 0 1/2 1 Miles✩Target Property Elevation: 2119 ft. North South West East23522241225321982195215921432119212921192149211621092129213021492079204120472222222022242179215822122210215521432119216721512141210221392140215121752206General NNWGeneral Topographic Gradient: TARGET PROPERTY TOPOGRAPHY should contamination exist on the target property, what downgradient sites might be impacted. assist the environmental professional in forming an opinion about the impact of nearby contaminated properties or, Surface topography may be indicative of the direction of surficial groundwater flow. This information can be used to TOPOGRAPHIC INFORMATION collected on nearby properties, and regional groundwater flow information (from deep aquifers). sources of information, such as surface topographic information, hydrologic information, hydrogeologic data using site-specific well data. If such data is not reasonably ascertainable, it may be necessary to rely on other Groundwater flow direction for a particular site is best determined by a qualified environmental professional GROUNDWATER FLOW DIRECTION INFORMATION ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC5716013.2s Page A-3 Not Reported GENERAL DIRECTIONLOCATION GROUNDWATER FLOWFROM TPMAP ID hydrogeologically, and the depth to water table. authorities at select sites and has extracted the date of the report, groundwater flow direction as determined flow at specific points. EDR has reviewed reports submitted by environmental professionals to regulatory EDR has developed the AQUIFLOW Information System to provide data on the general direction of groundwater AQUIFLOW® Search Radius: 1.000 Mile. contamination exist on the target property, what downgradient sites might be impacted. environmental professional in forming an opinion about the impact of nearby contaminated properties or, should of groundwater flow direction in the immediate area. Such hydrogeologic information can be used to assist the Hydrogeologic information obtained by installation of wells on a specific site can often be an indicator HYDROGEOLOGIC INFORMATION YES - refer to the Overview Map and Detail MapASHEVILLE NATIONAL WETLAND INVENTORY NWI Electronic Data CoverageNWI Quad at Target Property FEMA FIRM Flood data3700964600J FEMA FIRM Flood data3700965600J FEMA FIRM Flood data3700964700J Additional Panels in search area:FEMA Source Type FEMA FIRM Flood data3700965700J Flood Plain Panel at Target Property FEMA Source Type FEMA FLOOD ZONE and bodies of water). Refer to the Physical Setting Source Map following this summary for hydrologic information (major waterways contamination exist on the target property, what downgradient sites might be impacted. the environmental professional in forming an opinion about the impact of nearby contaminated properties or, should Surface water can act as a hydrologic barrier to groundwater flow. Such hydrologic information can be used to assist HYDROLOGIC INFORMATION ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC5716013.2s Page A-4 > 60 inchesDepth to Bedrock Max: > 60 inchesDepth to Bedrock Min: MODERATECorrosion Potential - Uncoated Steel: Hydric Status: Soil does not meet the requirements for a hydric soil. water table is more than 6 feet. Well drained. Soils have intermediate water holding capacity. Depth toSoil Drainage Class: textures. moderately well and well drained soils with moderately coarse Class B - Moderate infiltration rates. Deep and moderately deep,Hydrologic Group: loamSoil Surface Texture: HAYESVILLE Soil Component Name: The following information is based on Soil Conservation Service STATSGO data. in a landscape. Soil maps for STATSGO are compiled by generalizing more detailed (SSURGO) soil survey maps. for privately owned lands in the United States. A soil map in a soil survey is a representation of soil patterns Survey (NCSS) and is responsible for collecting, storing, maintaining and distributing soil survey information The U.S. Department of Agriculture’s (USDA) Soil Conservation Service (SCS) leads the National Cooperative Soil DOMINANT SOIL COMPOSITION IN GENERAL AREA OF TARGET PROPERTY Map, USGS Digital Data Series DDS - 11 (1994). of the Conterminous U.S. at 1:2,500,000 Scale - a digital representation of the 1974 P.B. King and H.M. Beikman Geologic Age and Rock Stratigraphic Unit Source: P.G. Schruben, R.E. Arndt and W.J. Bawiec, Geology ROCK STRATIGRAPHIC UNIT GEOLOGIC AGE IDENTIFICATION Stratified SequenceCategory:PrecambrianEra: PrecambrianSystem: Z Sedimentary rocksSeries: ZCode: (decoded above as Era, System & Series) at which contaminant migration may be occurring. Geologic information can be used by the environmental professional in forming an opinion about the relative speed GEOLOGIC INFORMATION IN GENERAL AREA OF TARGET PROPERTY move more quickly through sandy-gravelly types of soils than silty-clayey types of soils. characteristics data collected on nearby properties and regional soil information. In general, contaminant plumes to rely on other sources of information, including geologic age identification, rock stratigraphic unit and soil using site specific geologic and soil strata data. If such data are not reasonably ascertainable, it may be necessary Groundwater flow velocity information for a particular site is best determined by a qualified environmental professional GROUNDWATER FLOW VELOCITY INFORMATION ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC5716013.2s Page A-5 clay loam gravelly - sand sandy loam stratified loamDeeper Soil Types: silt loam sandy clay loamShallow Soil Types: silt loam fine sandy loam sandy loam gravelly - loamSurficial Soil Types: silt loam fine sandy loam sandy loam gravelly - loamSoil Surface Textures: appear within the general area of target property. Based on Soil Conservation Service STATSGO data, the following additional subordinant soil types may OTHER SOIL TYPES IN AREA Min: 3.60 Max: 6.00 Min: 2.00 Max: 6.00 Silty Sand. Sands with fines, SOILS, Sands, COARSE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clayfine sandy loam60 inches48 inches 4 Min: 3.60 Max: 6.00 Min: 0.60 Max: 2.00 Silty Sand. Sands with fines, SOILS, Sands, COARSE-GRAINED Soils. 200), Clayey passing No. than 35 pct. Materials (more Silt-Claysandy clay loam48 inches38 inches 3 Min: 3.60 Max: 6.00 Min: 0.60 Max: 2.00 50%), silt. limit less than Clays (liquid SOILS, Silts and FINE-GRAINED Soils. 200), Clayey passing No. than 35 pct. Materials (more Silt-Clayclay loam38 inches 5 inches 2 Min: 3.60 Max: 6.50 Min: 2.00 Max: 6.00 Silty Sand. Sands with fines, SOILS, Sands, COARSE-GRAINED Soils. 200), Silty passing No. than 35 pct. Materials (more Silt-Clayloam 5 inches 0 inches 1 Soil Layer Information Boundary Classification Permeability Rate (in/hr) Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil Soil Reaction (pH) ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® TC5716013.2s Page A-6 No Wells Found STATE DATABASE WELL INFORMATION LOCATION FROM TPWELL IDMAP ID Note: PWS System location is not always the same as well location. 1/2 - 1 Mile SSWNC0111401 1 FEDERAL FRDS PUBLIC WATER SUPPLY SYSTEM INFORMATION LOCATION FROM TPWELL IDMAP ID 1/2 - 1 Mile SEUSGS40000888326 2 FEDERAL USGS WELL INFORMATION LOCATION FROM TPWELL IDMAP ID 1.000State Database Nearest PWS within 1 mileFederal FRDS PWS 1.000Federal USGS WELL SEARCH DISTANCE INFORMATION SEARCH DISTANCE (miles)DATABASE opinion about the impact of contaminant migration on nearby drinking water wells. professional in assessing sources that may impact ground water flow direction, and in forming an EDR Local/Regional Water Agency records provide water well information to assist the environmental LOCAL / REGIONAL WATER AGENCY RECORDS ®GEOCHECK - PHYSICAL SETTING SOURCE SUMMARY® EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc.EDR Inc. 20 8020802 2 00212021602 2002200216022402 1 6 022 80 2 200 2200 22402 08020802320224022802 4 40 2 400236023202320 2 28022 80280022 402240 276027202240248033 602 4 40 3 3 2 0 2400 23602 36032803280403200316031 2 0 31 2 0 3 080 08 03 0 4030002960 2920288028402840 28002 8 00 2760272027 20 26802680 2040 20402 040204020402080020 8 0 208020 80208020802080 208020802080 2082080 21 20021202120 2120 21202 1202120212021 202120212021202120212021202120212 0 21 20 2 120 21 2 0212021 2 1 602 1 6 0 2 1 6 0 21602160 2 160 216021602160 21 60216 02160 2 16021 6 0216021602160 21602 1 6021 6 0 2160 21602160 216 022002 20 0 22002200220 0 2 20 0 220022 0022002 2002 2002200220022002200 2200 2200 2 20022 0 0 22 00 2240 22402240 2 2 40 2240 224022402 24022402240 2 2 40 2240 2 240 228 0 22802 2 802280228022 80 23202320 2320 2320 2 3 20 236 02360 236 0 2400 2400 24 4 02 4402480 2480 25 202520 2 56025 60 26002600 26402640 2080 208021602120212021602 1602522200220023202240224022802320236023602400 2720276024402440 2 8002 8402480248025203 3 203 2 803 2403 2003 2 0 0316313080 3080 30402 96 02 9 6 0 29 202 2 8 8028 402276 2 7 60 2 7 202680264026002560NC TC5716013.2s Page A-8 2002Violation Year: NCState: SOrig code: 202Violation id: 0824200Longitude: 353925Latitude: 0823142Longitude: 353200Latitude: 0824200Longitude: 353925Latitude: UntreatedTreatment: 101 - 500 PersonsPopulation served: ASHEVILLECity served: 011County FIPS: 28803System zip: NCSystem state: ASHEVILLESystem city: Not ReportedSystem address: LEICESTER ELEM SCHOOLSystem name: 00000474Retail population: Not ReportedDate system deactivated: 7706Date system activated: ActiveActivity status: NC0111401PWS ID: Not ReportedContact telephone: 828-232-42Contact zip: 28Contact state: NCContact city: ASHEVILLEContact address: 175 BINGHAM RDContact address: HALL, BELVINContact: 650Retail population served: NTNCPWS type code: LEICESTER ELEM SCHOOLPWS name: 28803PWS zip: NCPWS state: ASHEVILLEPWS city: Not ReportedPWS address: BUNCOMBE CO. BOARD OF EDUCATPWS name: System Owner/Responsible PartyPWS type: NC0111401PWS ID: 28803PWS zip: NCPWS state: ASHEVILLEPWS city: Not ReportedPWS address: MR JAMES WARREN OR MAINT SUPERPWS name: System Owner/Responsible PartyPWS type: NC0111401PWS ID: TPFactypecode: hypochlorination, postTrtprocess: disinfectionTrtobjective: AFacactivitycode: Treatment_plantFactype: TREATMENT_PLT_WELL #1Facname: 7413Facid: NC0111401Pwsid: TPFactypecode: ph adjustmentTrtprocess: corrosion controlTrtobjective: AFacactivitycode: Treatment_plantFactype: TREATMENT_PLT_WELL #1Facname: 7413Facid: NC0111401Pwsid: APwsactivitycode: 28806Contactzip: NCContactstate: ASHEVILLEContactcity: Not ReportedContactaddress2: 175 BINGHAM RDContactaddress1: 828-232-4244Contactphone: HALL, BELVINContactorgname: HALL, BELVINContact: Local_GovtOwner: NTNCWSPwstype: GroundwaterPsource longname: 1Pwssvcconn: 679Retpopsrvd: ActiveStatus: 37021Fipscounty: Not ReportedZipserved: NCStateserved: Not ReportedCityserved: LEICESTER ELEM SCHOOLPwsname: NC0111401Pwsid: NCState: 04Epa region: 1 SSW 1/2 - 1 Mile Higher NC0111401FRDS PWS Map ID Direction Distance Elevation EDR ID NumberDatabase ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-9 SOrig code: 610Violation id: Not ReportedCmp edt: 10/01/2010Cmp bdt: Not ReportedState mcl: Not ReportedUnit of measure: Not ReportedViolation measur: LCRRule name: 350Rule code: Follow-up Or Routine LCR Tap M/RViolation name: 52Violation code: Lead and Copper RuleContamination Name: 5000Contamination code: 2010Violation Year: NCState: SOrig code: 609Violation id: Not ReportedCmp edt: 10/01/2007Cmp bdt: Not ReportedState mcl: Not ReportedUnit of measure: Not ReportedViolation measur: LCRRule name: 350Rule code: Follow-up Or Routine LCR Tap M/RViolation name: 52Violation code: Lead and Copper RuleContamination Name: 5000Contamination code: 2007Violation Year: NCState: SOrig code: 607Violation id: 03/31/2005Cmp edt: 01/01/2005Cmp bdt: Not ReportedState mcl: Not ReportedUnit of measure: Not ReportedViolation measur: NitratesRule name: 331Rule code: Monitoring, RegularViolation name: 03Violation code: NitrateContamination Name: 1040Contamination code: 2005Violation Year: NCState: SOrig code: 605Violation id: 09/30/2004Cmp edt: 07/01/2004Cmp bdt: Not ReportedState mcl: Not ReportedUnit of measure: Not ReportedViolation measur: NitratesRule name: 331Rule code: Monitoring, RegularViolation name: 03Violation code: NitrateContamination Name: 1040Contamination code: 2004Violation Year: NCState: SOrig code: 505Violation id: 09/30/2003Cmp edt: 07/01/2003Cmp bdt: 10State mcl: MG/LUnit of measure: 11Violation measur: NitratesRule name: 331Rule code: MCL, AverageViolation name: 02Violation code: NitrateContamination Name: 1040Contamination code: 2003Violation Year: NCState: SOrig code: 403Violation id: 12/31/2002Cmp edt: 10/01/2002Cmp bdt: Not ReportedState mcl: Not ReportedUnit of measure: Not ReportedViolation measur: NitratesRule name: 331Rule code: Monitoring, RegularViolation name: 03Violation code: NitrateContamination Name: 1040Contamination code: 2002Violation Year: NCState: SOrig code: 303Violation id: 06/30/2002Cmp edt: 04/01/2002Cmp bdt: Not ReportedState mcl: Not ReportedUnit of measure: Not ReportedViolation measur: NitratesRule name: 331Rule code: Monitoring, RegularViolation name: 03Violation code: NitrateContamination Name: 1040Contamination code: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-10 SIEEnforcement Action: 2/18/2003 0:00:00Enforcement Date: 303Violation ID: 12/31/2002 0:00:00Compliance End: 10/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 4/15/2004 0:00:00Enforcement Date: 303Violation ID: 12/31/2002 0:00:00Compliance End: 10/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 2/18/2003 0:00:00Enforcement Date: 303Violation ID: 12/31/2002 0:00:00Compliance End: 10/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 2/18/2003 0:00:00Enforcement Date: 303Violation ID: 12/31/2002 0:00:00Compliance End: 10/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 2/18/2003 0:00:00Enforcement Date: 303Violation ID: 12/31/2002 0:00:00Compliance End: 10/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 8/16/2002 0:00:00Enforcement Date: 202Violation ID: 6/30/2002 0:00:00Compliance End: 4/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 8/16/2002 0:00:00Enforcement Date: 202Violation ID: 6/30/2002 0:00:00Compliance End: 4/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 4/15/2004 0:00:00Enforcement Date: 202Violation ID: 6/30/2002 0:00:00Compliance End: 4/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 8/16/2002 0:00:00Enforcement Date: 202Violation ID: 6/30/2002 0:00:00Compliance End: 4/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 8/16/2002 0:00:00Enforcement Date: 202Violation ID: 6/30/2002 0:00:00Compliance End: 4/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 4/15/2004 0:00:00Enforcement Date: 202Violation ID: 6/30/2002 0:00:00Compliance End: 4/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: Not ReportedCmp edt: 04/11/2012Cmp bdt: Not ReportedState mcl: Not ReportedUnit of measure: Not ReportedViolation measur: PN ruleRule name: 410Rule code: PN Violation for NPDWR ViolationViolation name: 75Violation code: Public NoticeContamination Name: 7500Contamination code: 2012Violation Year: NCState: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-11 7/1/2004 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 12/9/2004 0:00:00Enforcement Date: 505Violation ID: 9/30/2004 0:00:00Compliance End: 7/1/2004 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 12/9/2004 0:00:00Enforcement Date: 505Violation ID: 9/30/2004 0:00:00Compliance End: 7/1/2004 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 12/22/2004 0:00:00Enforcement Date: 505Violation ID: 9/30/2004 0:00:00Compliance End: 7/1/2004 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 7/25/2003 0:00:00Enforcement Date: 403Violation ID: 9/30/2003 0:00:00Compliance End: 7/1/2003 0:00:00Compliance Begin: 1040Contaminant: 2Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIFEnforcement Action: 7/30/2003 0:00:00Enforcement Date: 403Violation ID: 9/30/2003 0:00:00Compliance End: 7/1/2003 0:00:00Compliance Begin: 1040Contaminant: 2Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIFEnforcement Action: 7/30/2003 0:00:00Enforcement Date: 403Violation ID: 9/30/2003 0:00:00Compliance End: 7/1/2003 0:00:00Compliance Begin: 1040Contaminant: 2Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 7/25/2003 0:00:00Enforcement Date: 403Violation ID: 9/30/2003 0:00:00Compliance End: 7/1/2003 0:00:00Compliance Begin: 1040Contaminant: 2Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 11/6/2003 0:00:00Enforcement Date: 403Violation ID: 9/30/2003 0:00:00Compliance End: 7/1/2003 0:00:00Compliance Begin: 1040Contaminant: 2Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 7/25/2003 0:00:00Enforcement Date: 403Violation ID: 9/30/2003 0:00:00Compliance End: 7/1/2003 0:00:00Compliance Begin: 1040Contaminant: 2Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 7/25/2003 0:00:00Enforcement Date: 403Violation ID: 9/30/2003 0:00:00Compliance End: 7/1/2003 0:00:00Compliance Begin: 1040Contaminant: 2Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 11/6/2003 0:00:00Enforcement Date: 403Violation ID: 9/30/2003 0:00:00Compliance End: 7/1/2003 0:00:00Compliance Begin: 1040Contaminant: 2Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 4/15/2004 0:00:00Enforcement Date: 303Violation ID: 12/31/2002 0:00:00Compliance End: 10/1/2002 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-12 SFJEnforcement Action: 1995-09-29Enforcement Date: 9546079Violation ID: 2015-12-31Compliance End: 1994-07-01Compliance Begin: 5000Contaminant: 57Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 1995-09-29Enforcement Date: 9546079Violation ID: 1994-12-31Compliance End: 1994-07-01Compliance Begin: 5000Contaminant: 57Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 5/12/2005 0:00:00Enforcement Date: 605Violation ID: 3/31/2005 0:00:00Compliance End: 1/1/2005 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 5/12/2005 0:00:00Enforcement Date: 605Violation ID: 3/31/2005 0:00:00Compliance End: 1/1/2005 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 4/29/2005 0:00:00Enforcement Date: 605Violation ID: 3/31/2005 0:00:00Compliance End: 1/1/2005 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 4/29/2005 0:00:00Enforcement Date: 605Violation ID: 3/31/2005 0:00:00Compliance End: 1/1/2005 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 5/12/2005 0:00:00Enforcement Date: 605Violation ID: 3/31/2005 0:00:00Compliance End: 1/1/2005 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 5/12/2005 0:00:00Enforcement Date: 605Violation ID: 3/31/2005 0:00:00Compliance End: 1/1/2005 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 12/22/2004 0:00:00Enforcement Date: 505Violation ID: 9/30/2004 0:00:00Compliance End: 7/1/2004 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SFJEnforcement Action: 12/9/2004 0:00:00Enforcement Date: 505Violation ID: 9/30/2004 0:00:00Compliance End: 7/1/2004 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 12/9/2004 0:00:00Enforcement Date: 505Violation ID: 9/30/2004 0:00:00Compliance End: 7/1/2004 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIFEnforcement Action: 1/3/2005 0:00:00Enforcement Date: 505Violation ID: 9/30/2004 0:00:00Compliance End: 7/1/2004 0:00:00Compliance Begin: 1040Contaminant: 3Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIFEnforcement Action: 1/3/2005 0:00:00Enforcement Date: 505Violation ID: 9/30/2004 0:00:00Compliance End: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-13 ResolvingEnforcement Category: St Compliance achievedEnforcement Detail: 11/06/2003Enforcement Action: 2004Enforcemnt FY: SOrig Code: 403Violation ID: InformalEnforcement Category: St Public Notif requestedEnforcement Detail: 07/25/2003Enforcement Action: 2003Enforcemnt FY: SOrig Code: 403Violation ID: ResolvingEnforcement Category: St Compliance achievedEnforcement Detail: 04/15/2004Enforcement Action: 2004Enforcemnt FY: SOrig Code: 303Violation ID: InformalEnforcement Category: St Public Notif requestedEnforcement Detail: 02/18/2003Enforcement Action: 2003Enforcemnt FY: SOrig Code: 303Violation ID: InformalEnforcement Category: St Formal NOV issuedEnforcement Detail: 02/18/2003Enforcement Action: 2003Enforcemnt FY: SOrig Code: 303Violation ID: InformalEnforcement Category: St Formal NOV issuedEnforcement Detail: 08/16/2002Enforcement Action: 2002Enforcemnt FY: SOrig Code: 202Violation ID: InformalEnforcement Category: St Public Notif requestedEnforcement Detail: 08/16/2002Enforcement Action: 2002Enforcemnt FY: SOrig Code: 202Violation ID: ResolvingEnforcement Category: St Compliance achievedEnforcement Detail: 04/15/2004Enforcement Action: 2004Enforcemnt FY: SOrig Code: 202Violation ID: SOXEnforcement Action: 1995-10-30Enforcement Date: 9546079Violation ID: 2015-12-31Compliance End: 1994-07-01Compliance Begin: 5000Contaminant: 57Violation Type: LEICESTER ELEM SCHOOLSystem Name: SOXEnforcement Action: 1995-10-30Enforcement Date: 9546079Violation ID: 1994-12-31Compliance End: 1994-07-01Compliance Begin: 5000Contaminant: 57Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIFEnforcement Action: 1995-10-30Enforcement Date: 9546079Violation ID: 2015-12-31Compliance End: 1994-07-01Compliance Begin: 5000Contaminant: 57Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIFEnforcement Action: 1995-10-30Enforcement Date: 9546079Violation ID: 1994-12-31Compliance End: 1994-07-01Compliance Begin: 5000Contaminant: 57Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 1995-09-29Enforcement Date: 9546079Violation ID: 2015-12-31Compliance End: 1994-07-01Compliance Begin: 5000Contaminant: 57Violation Type: LEICESTER ELEM SCHOOLSystem Name: SIEEnforcement Action: 1995-09-29Enforcement Date: 9546079Violation ID: 1994-12-31Compliance End: 1994-07-01Compliance Begin: 5000Contaminant: 57Violation Type: LEICESTER ELEM SCHOOLSystem Name: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-14 04/04/2011Enforcement Action: 2011Enforcemnt FY: SOrig Code: 609Violation ID: InformalEnforcement Category: St Public Notif receivedEnforcement Detail: 01/09/2013Enforcement Action: 2013Enforcemnt FY: SOrig Code: 609Violation ID: InformalEnforcement Category: St Formal NOV issuedEnforcement Detail: 05/29/2008Enforcement Action: 2008Enforcemnt FY: SOrig Code: 607Violation ID: FormalEnforcement Category: St AO (w/penalty) issuedEnforcement Detail: 06/26/2008Enforcement Action: 2008Enforcemnt FY: SOrig Code: 607Violation ID: InformalEnforcement Category: St Public Notif requestedEnforcement Detail: 05/29/2008Enforcement Action: 2008Enforcemnt FY: SOrig Code: 607Violation ID: InformalEnforcement Category: St Public Notif receivedEnforcement Detail: 05/11/2009Enforcement Action: 2009Enforcemnt FY: SOrig Code: 607Violation ID: ResolvingEnforcement Category: St Compliance achievedEnforcement Detail: 08/21/2008Enforcement Action: 2008Enforcemnt FY: SOrig Code: 607Violation ID: InformalEnforcement Category: St Formal NOV issuedEnforcement Detail: 05/12/2005Enforcement Action: 2005Enforcemnt FY: SOrig Code: 605Violation ID: InformalEnforcement Category: St Public Notif requestedEnforcement Detail: 05/12/2005Enforcement Action: 2005Enforcemnt FY: SOrig Code: 605Violation ID: ResolvingEnforcement Category: St Compliance achievedEnforcement Detail: 04/29/2005Enforcement Action: 2005Enforcemnt FY: SOrig Code: 605Violation ID: InformalEnforcement Category: St Public Notif receivedEnforcement Detail: 01/03/2005Enforcement Action: 2005Enforcemnt FY: SOrig Code: 505Violation ID: InformalEnforcement Category: St Public Notif requestedEnforcement Detail: 12/09/2004Enforcement Action: 2005Enforcemnt FY: SOrig Code: 505Violation ID: InformalEnforcement Category: St Formal NOV issuedEnforcement Detail: 12/09/2004Enforcement Action: 2005Enforcemnt FY: SOrig Code: 505Violation ID: ResolvingEnforcement Category: St Compliance achievedEnforcement Detail: 12/22/2004Enforcement Action: 2005Enforcemnt FY: SOrig Code: 505Violation ID: InformalEnforcement Category: St Formal NOV issuedEnforcement Detail: 07/25/2003Enforcement Action: 2003Enforcemnt FY: SOrig Code: 403Violation ID: InformalEnforcement Category: St Public Notif receivedEnforcement Detail: 07/30/2003Enforcement Action: 2003Enforcemnt FY: SOrig Code: 403Violation ID: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-15 Not ReportedViolation measurement: State Public Notif RequestedEnforcement action: 2/18/2003 0:00:00Enforcement date: 12/31/2002 0:00:00Compliance end date: 10/1/2002 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 303Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Formal NOV IssuedEnforcement action: 2/18/2003 0:00:00Enforcement date: 12/31/2002 0:00:00Compliance end date: 10/1/2002 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 303Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Public Notif RequestedEnforcement action: 8/16/2002 0:00:00Enforcement date: 6/30/2002 0:00:00Compliance end date: 4/1/2002 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 202Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Formal NOV IssuedEnforcement action: 8/16/2002 0:00:00Enforcement date: 6/30/2002 0:00:00Compliance end date: 4/1/2002 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 202Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Compliance AchievedEnforcement action: 4/15/2004 0:00:00Enforcement date: 6/30/2002 0:00:00Compliance end date: 4/1/2002 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 202Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: InformalEnforcement Category: St Formal NOV issuedEnforcement Detail: 11/22/2012Enforcement Action: 2013Enforcemnt FY: SOrig Code: 610Violation ID: FormalEnforcement Category: St AO (w/o penalty) issuedEnforcement Detail: 11/22/2012Enforcement Action: 2013Enforcemnt FY: SOrig Code: 610Violation ID: ResolvingEnforcement Category: St Compliance achievedEnforcement Detail: 12/17/2012Enforcement Action: 2013Enforcemnt FY: SOrig Code: 610Violation ID: ResolvingEnforcement Category: St Compliance achievedEnforcement Detail: 07/17/2013Enforcement Action: 2013Enforcemnt FY: SOrig Code: 609Violation ID: InformalEnforcement Category: St Formal NOV issuedEnforcement Detail: 04/04/2011Enforcement Action: 2011Enforcemnt FY: SOrig Code: 609Violation ID: InformalEnforcement Category: St Public Notif requestedEnforcement Detail: 04/04/2011Enforcement Action: 2011Enforcemnt FY: SOrig Code: 609Violation ID: FormalEnforcement Category: St AO (w/o penalty) issuedEnforcement Detail: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-16 Not ReportedViolation measurement: State Public Notif RequestedEnforcement action: 12/9/2004 0:00:00Enforcement date: 9/30/2004 0:00:00Compliance end date: 7/1/2004 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 505Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Formal NOV IssuedEnforcement action: 12/9/2004 0:00:00Enforcement date: 9/30/2004 0:00:00Compliance end date: 7/1/2004 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 505Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Compliance AchievedEnforcement action: 12/22/2004 0:00:00Enforcement date: 9/30/2004 0:00:00Compliance end date: 7/1/2004 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 505Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Public Notif ReceivedEnforcement action: 1/3/2005 0:00:00Enforcement date: 9/30/2004 0:00:00Compliance end date: 7/1/2004 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 505Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: 11Violation measurement: State Public Notif ReceivedEnforcement action: 7/30/2003 0:00:00Enforcement date: 9/30/2003 0:00:00Compliance end date: 7/1/2003 0:00:00Compliance start date: 2Violation type: NITRATEContaminant: 403Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: 11Violation measurement: State Public Notif RequestedEnforcement action: 7/25/2003 0:00:00Enforcement date: 9/30/2003 0:00:00Compliance end date: 7/1/2003 0:00:00Compliance start date: 2Violation type: NITRATEContaminant: 403Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: 11Violation measurement: State Formal NOV IssuedEnforcement action: 7/25/2003 0:00:00Enforcement date: 9/30/2003 0:00:00Compliance end date: 7/1/2003 0:00:00Compliance start date: 2Violation type: NITRATEContaminant: 403Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: 11Violation measurement: State Compliance AchievedEnforcement action: 11/6/2003 0:00:00Enforcement date: 9/30/2003 0:00:00Compliance end date: 7/1/2003 0:00:00Compliance start date: 2Violation type: NITRATEContaminant: 403Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Compliance AchievedEnforcement action: 4/15/2004 0:00:00Enforcement date: 12/31/2002 0:00:00Compliance end date: 10/1/2002 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 303Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-17 1970Level reading date: 1Ground water levels,Number of Measurements: Not ReportedWell Hole Depth Units: Not ReportedWell Hole Depth: ftWell Depth Units: 163Well Depth: Not ReportedConstruction Date: Not ReportedAquifer Type: QuartziteFormation Type: Piedmont and Blue Ridge crystalline-rock aquifersAquifer: Not ReportedContrib Drainage Area Unts: Not ReportedContrib Drainage Area: Not ReportedDrainage Area Units: Not ReportedDrainage Area: Not ReportedHUC: Not ReportedDescription: WellType: BU-039Monitor Location: USGS North Carolina Water Science CenterOrganization Name: USGS-NCOrganization ID: 2 SE 1/2 - 1 Mile Higher USGS40000888326FED USGS Not ReportedViolation measurement: State AO (w/penalty) IssuedEnforcement action: 6/26/2008 0:00:00Enforcement date: 12/31/2025 0:00:00Compliance end date: 10/1/2007 0:00:00Compliance start date: Follow-up and Routine Tap SamplingViolation type: LEAD & COPPER RULEContaminant: 607Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Public Notif RequestedEnforcement action: 5/29/2008 0:00:00Enforcement date: 12/31/2025 0:00:00Compliance end date: 10/1/2007 0:00:00Compliance start date: Follow-up and Routine Tap SamplingViolation type: LEAD & COPPER RULEContaminant: 607Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Formal NOV IssuedEnforcement action: 5/29/2008 0:00:00Enforcement date: 12/31/2025 0:00:00Compliance end date: 10/1/2007 0:00:00Compliance start date: Follow-up and Routine Tap SamplingViolation type: LEAD & COPPER RULEContaminant: 607Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Public Notif RequestedEnforcement action: 5/12/2005 0:00:00Enforcement date: 3/31/2005 0:00:00Compliance end date: 1/1/2005 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 605Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Formal NOV IssuedEnforcement action: 5/12/2005 0:00:00Enforcement date: 3/31/2005 0:00:00Compliance end date: 1/1/2005 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 605Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: Not ReportedViolation measurement: State Compliance AchievedEnforcement action: 4/29/2005 0:00:00Enforcement date: 3/31/2005 0:00:00Compliance end date: 1/1/2005 0:00:00Compliance start date: 3Violation type: NITRATEContaminant: 605Violation ID: NTNCPWS type code: 650Population served: LEICESTER ELEM SCHOOLPWS name: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-18 Not ReportedNote: Not ReportedFeet to sea level: 94Feet below surface: ®GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS® TC5716013.2s Page A-19 0%67%33%6.000 pCi/LBasement Not ReportedNot ReportedNot ReportedNot ReportedLiving Area - 2nd Floor 0%0%100%1.343 pCi/LLiving Area - 1st Floor % >20 pCi/L% 4-20 pCi/L% <4 pCi/LAverage ActivityArea Number of sites tested: 7 Federal Area Radon Information for Zip Code: 28803 : Zone 3 indoor average level < 2 pCi/L. : Zone 2 indoor average level >= 2 pCi/L and <= 4 pCi/L. Note: Zone 1 indoor average level > 4 pCi/L. Federal EPA Radon Zone for BUNCOMBE County: 1 999.001 7.57.57.501 90.35.5839 9.80.33.59297 __________________________________ Max pCi/LMin pCi/LAvg pCi/LNum Results Radon Test Results State Database: NC Radon AREA RADON INFORMATION GEOCHECK - PHYSICAL SETTING SOURCE MAP FINDINGS RADON ® TOPOGRAPHIC INFORMATION USGS 7.5’ Digital Elevation Model (DEM) Source: United States Geologic Survey EDR acquired the USGS 7.5’ Digital Elevation Model in 2002 and updated it in 2006. The 7.5 minute DEM corresponds to the USGS 1:24,000- and 1:25,000-scale topographic quadrangle maps. The DEM provides elevation data with consistent elevation units and projection. Current USGS 7.5 Minute Topographic Map Source: U.S. Geological Survey HYDROLOGIC INFORMATION Flood Zone Data: This data was obtained from the Federal Emergency Management Agency (FEMA). It depicts 100-year and 500-year flood zones as defined by FEMA. It includes the National Flood Hazard Layer (NFHL) which incorporates Flood Insurance Rate Map (FIRM) data and Q3 data from FEMA in areas not covered by NFHL. Source: FEMA Telephone: 877-336-2627 Date of Government Version: 2003, 2015 NWI: National Wetlands Inventory. This data, available in select counties across the country, was obtained by EDR in 2002, 2005 and 2010 from the U.S. Fish and Wildlife Service. State Wetlands Data: Wetland Inventory Source: US Fish & Wildlife Service Telephone: 703-358-2171 HYDROGEOLOGIC INFORMATION AQUIFLOW Information SystemR Source: EDR proprietary database of groundwater flow information EDR has developed the AQUIFLOW Information System (AIS) to provide data on the general direction of groundwater flow at specific points. EDR has reviewed reports submitted to regulatory authorities at select sites and has extracted the date of the report, hydrogeologically determined groundwater flow direction and depth to water table information. GEOLOGIC INFORMATION Geologic Age and Rock Stratigraphic Unit Source: P.G. Schruben, R.E. Arndt and W.J. Bawiec, Geology of the Conterminous U.S. at 1:2,500,000 Scale - A digital representation of the 1974 P.B. King and H.M. Beikman Map, USGS Digital Data Series DDS - 11 (1994). STATSGO: State Soil Geographic Database Source: Department of Agriculture, Natural Resources Conservation Service (NRCS) The U.S. Department of Agriculture’s (USDA) Natural Resources Conservation Service (NRCS) leads the national Conservation Soil Survey (NCSS) and is responsible for collecting, storing, maintaining and distributing soil survey information for privately owned lands in the United States. A soil map in a soil survey is a representation of soil patterns in a landscape. Soil maps for STATSGO are compiled by generalizing more detailed (SSURGO) soil survey maps. SSURGO: Soil Survey Geographic Database Source: Department of Agriculture, Natural Resources Conservation Service (NRCS) Telephone: 800-672-5559 SSURGO is the most detailed level of mapping done by the Natural Resources Conservation Service, mapping scales generally range from 1:12,000 to 1:63,360. Field mapping methods using national standards are used to construct the soil maps in the Soil Survey Geographic (SSURGO) database. SSURGO digitizing duplicates the original soil survey maps. This level of mapping is designed for use by landowners, townships and county natural resource planning and management. TC5716013.2s Page PSGR-1 PHYSICAL SETTING SOURCE RECORDS SEARCHED LOCAL / REGIONAL WATER AGENCY RECORDS FEDERAL WATER WELLS PWS: Public Water Systems Source: EPA/Office of Drinking Water Telephone: 202-564-3750 Public Water System data from the Federal Reporting Data System. A PWS is any water system which provides water to at least 25 people for at least 60 days annually. PWSs provide water from wells, rivers and other sources. PWS ENF: Public Water Systems Violation and Enforcement Data Source: EPA/Office of Drinking Water Telephone: 202-564-3750 Violation and Enforcement data for Public Water Systems from the Safe Drinking Water Information System (SDWIS) after August 1995. Prior to August 1995, the data came from the Federal Reporting Data System (FRDS). USGS Water Wells: USGS National Water Inventory System (NWIS) This database contains descriptive information on sites where the USGS collects or has collected data on surface water and/or groundwater. The groundwater data includes information on wells, springs, and other sources of groundwater. STATE RECORDS North Carolina Public Water Supply Wells Source: Department of Environmental Health Telephone: 919-715-3243 OTHER STATE DATABASE INFORMATION North Carolina Wildlife Resources/Game Lands Source: Center for Geographic Information and Analysis Telephone: 919-733-2090 All publicly owned game lands managed by the North Carolina Wildlife Resources Commission and as listed in Hunting and Fishing Maps. NC Natural Heritage Sites: Natural Heritage Element Occurrence Sites Source: Natural Heritage Occurrence Sites Center for Geographic Information and Analysis Telephone: 919-733-2090 A point coverage identifying locations of rare and endangered species, occurrences of exemplary or unique natural ecosystems (terrestrial or aquatic), and special animal habitats (e.g., colonial waterbird nesting sites). NC Natural Areas: Significant Natural Heritage Areas Source: Center for Geographic Information and Analysis Telephone: 919-733-2090 A polygon converage identifying sites (terrestrial or aquatic) that have particular biodiversity significance. A site’s significance may be due to the presenceof rare species, rare or high quality natural communities, or other important ecological features. RADON State Database: NC Radon Source: Department of Environment & Natural Resources Telephone: 919-733-4984 Radon Statistical and Non Statiscal Data Area Radon Information Source: USGS Telephone: 703-356-4020 The National Radon Database has been developed by the U.S. Environmental Protection Agency (USEPA) and is a compilation of the EPA/State Residential Radon Survey and the National Residential Radon Survey. The study covers the years 1986 - 1992. Where necessary data has been supplemented by information collected at private sources such as universities and research institutions. TC5716013.2s Page PSGR-2 PHYSICAL SETTING SOURCE RECORDS SEARCHED EPA Radon Zones Source: EPA Telephone: 703-356-4020 Sections 307 & 309 of IRAA directed EPA to list and identify areas of U.S. with the potential for elevated indoor radon levels. OTHER Airport Landing Facilities: Private and public use landing facilities Source: Federal Aviation Administration, 800-457-6656 Epicenters: World earthquake epicenters, Richter 5 or greater Source: Department of Commerce, National Oceanic and Atmospheric Administration Earthquake Fault Lines: The fault lines displayed on EDR’s Topographic map are digitized quaternary faultlines, prepared in 1975 by the United State Geological Survey STREET AND ADDRESS INFORMATION © 2015 TomTom North America, Inc. All rights reserved. This material is proprietary and the subject of copyright protection and other intellectual property rights owned by or licensed to Tele Atlas North America, Inc. The use of this material is subject to the terms of a license agreement. You will be held liable for any unauthorized copying or disclosure of this material. TC5716013.2s Page PSGR-3 PHYSICAL SETTING SOURCE RECORDS SEARCHED ISLEINC. EUNNELL-LAMMONS ENGINEERING, INC. GEOTECHNick ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS REPORT OF LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT FORMER P.E. VALVE PROPERTY 1140 SWEETEN CREEK ROAD ASHEVILLE, NORTH CAROLINA Prepared For Mr. Tom Dolan Colonial Oil Group P.O. Box 576 Savannah, Georgia 31402 Prepared By Bunnell-Lammons Engineering, Inc. 6004 Ponders Court Greenville, South Carolina 29615 March 8, 2010 BLE Project No. J10-6875-02 T INC. BUNNELL•LAMMONS ENGINEERING, INC. GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS roup ,rgia 31402 Report of Limited Phase H Environmental Site Assessment Former P.E. Valve Property 1140 Sweeten Creek Road Asheville, North Carolina BLE Job Number J10-6875-02 F11 Ions Engineering, Inc. (BLE) is pleased to submit this report of our Limited Phase II Site Assessment (ESA) for the subject property. Our services were performed as .E Proposal No. P10-0107. The purpose of this assessment was to investigate vironmental Conditions (RECs) identified during a Phase I ESA performed by BLE 110. From these results, the objective was to determine if the subject property has Etted by on-site environmental conditions. id recommendations contained herein are based upon the data that was reviewed and this report along with our experience on similar projects. The discovery of any oration concerning the environmental conditions at the site should be reported to us v so that we can reassess potential environmental impacts and modify our ,ns, if necessary. the opportunity to work with you on this project. Please call us if you have any ,ve may be of further service. 1 m IMONS ENGINEERING, INC. ® Sf,AL 1.264 01) Thomas L. Lammons, P.G.`'-Pg®°°®° eologist Principal Geologist Registered, North Carolina No. 1264 PHONE (864) 288-1265 FAX (864) 288-4430 Limited Phase HESA March 8, 2010 Former P.E. Valve Property BLE Project No. J10-6875-02 Asheville, North Carolina 1.0 PROJECT INFORMATION The following project information was obtained from site reconnaissance, regulatory database search, and interviews with knowledgeable persons during a Phase I ESA conducted at the subject site. Details of the assessment can be found in Report of Phase I Environmental Site Assessment, by BLE dated March 4, 2010. The approximate 1.63-acre site, located at 1140 Sweeten Creek Road in Asheville, South Carolina (Figure 1) is currently occupied by a vacant 30,302 square foot industrial manufacturing building. The site was first developed during the 1930s as a textile manufacturing facility, but was later (circa 1968) used as a valve manufacturing facility by P.E. Valve Company, Inc. During the Phase I ESA site walk, several recognized environmental conditions (REQ) were identified at the site. RECs included, but were not limited to: 1) rusted 55-gallon drums located on the southern side of the manufacturing building, of which the historic contents are unknown; 2) an above ground storage tank (AST) located on the southern side of the building; 3) staining along the northern wall of the building and a loading dock with floor drains; 4) two ASTs located on the interior of the building; 4) multiple 55-gallon drums and 5-gallon buckets of waste oil, waste coolant, and unidentified liquids inside the building; 5) heavy staining on the floor of the building; and 6) a network of floor drains located inside the building. As a result of the historical site usage and above listed RECs, Colonial Oil Group requested that a limited Phase II ESA be performed. pill Wlfo 1912 to] _a I Ll 10~woIG 1 a -9 -W M 011 In accordance with our Proposal for Phase II Environmental Site Assessment dated January 29, 2010, BLE was authorized to perform a Limited Phase II ESA of the 1.63-acre property. The objectives of this assessment were to assess the soil and groundwater quality at selected locations that were potentially impacted by RECs. On February 3, 2010 four borings (BL-1 through BL-4) were advanced to depths of refusal (which is generally interpreted as bedrock) using a Geoprobe 6600 Truck Mounted Direct Push Technology drill rig to obtain groundwater samples. A groundwater sample from each location was submitted for laboratory analysis of volatile organic compounds (VOCs), polycyclic aromatic hydrocarbons (PAHs), and 8-RCRA metals. Three additional geoprobe borings (BR-1, BR-2, and BR-3) were advanced to depths of refusal in order to provide a bedrock surface profile. Continuous macrocore soil samples were collected from BR-2 and BR-3. At four locations within the industrial manufacturing building (HAB-1 through HAB-4), soil samples were obtained from beneath the concrete slab and scanned using a MiniRAE® 2000 Photo-Ionization Detector (PID). Soil samples from HAB-1, HAB-2, and HAB-4 were submitted for laboratory analysis of VOCs, PAHs, and 8-RCRA metals. Boring locations are shown on Figures 2 and 3. Limited Phase II ESA March 8, 2010 Former P.E. Valve Property BLE Project No. J] 0-6875-02 Asheville, North Carolina 3.0 FIELD ACTIVITIES Groundwater Sample Collection Boring locations were determined based upon historical information, recognized potential sources of contamination identified during the Phase I ESA, and drill rig accessibility. Boring locations are indicated on Figures 2 and 3 and described below. Boring ID Description BL-1 Located downgradient and west of the manufacturing building BL-2 Located at the downgradient, northwest corner of site BL-3 Located at the southwest corner of the manufacturing building, downgradient of an AST BL-4 Adjacent to loading dock and 40-inch by 24-inch hinged door used to access the storm water drain sum Four geoprobe borings were advanced to refusal to collect groundwater samples. A groundwater sample was collected from each location and submitted to Pace Analytical Services, Inc. in Huntersville, North Carolina for laboratory analysis. Upon completion of sampling activities, the open boreholes were abandoned by backfilling with a bentonite cement- grout to the land surface. Hand Auger Boring Soil Sample Collection Soil samples were obtained from beneath the manufacturing building foundation at four locations. A core machine was used to core through the concrete foundation, and a hand auger was advanced up to three feet below the foundation. Soil samples were visually examined in the field by a geologist and screened at 1-foot intervals using a PID. Soil sample locations were determined based upon historical information and recognized potential sources of contamination identified inside the manufacturing building. Hand auger boring locations are indicated on Figure 2 and described below. Boring ID Description HAB-1 Adjacent to the location of 55-gallon drums, ASTs, and 5-gallon buckets containing waste oil, coolant, and unidentified liquids. Boring was performed in a low spot in the foundation where cracks in the concrete and heavy staining were observed. HAB-2 Located inside the machining room where heavy staining and absorbent socks and kitty litter were observed. Adjacent to the 40-inch by 24-inch hinged door used to access the storm water drain sump. HAB-3 Located inside the paint room HAB-4 Adjacent to a floor drain located in the southern portion of the manufacturing building. A soil sample was collected from three of the four hand auger boring locations (HAB-1, HAB-2, and HAB-4) and submitted to Pace Analytical Services, Inc. in Huntersville, North Carolina for U Limited Phase II ESA March 8, 2010 Former P.E. Valve Property BLE Project No. JI0-6875-02 Asheville, North Carolina laboratory analysis of VOCs, PAHs, and 8-RCRA metals. Upon completion of sampling activities, the open boreholes were abandoned by backfilling with a cement-grout to the foundation surface. Subsurface Exploratory Borings Three geoprobe borings (BR-1, BR-2, and BR-3) were advanced to refusal which ranged from 23 to 26 feet below ground surface (bgs) to explore the bedrock surface. A continuous soil sample was collected from two of the three borings using a macrotube soil sampling system. Representative portions of the soil samples were visually examined and classified in the field by a geologist and screened at 1-foot intervals using a PID. Geoprobe drilling procedures are included in Appendix A. Lithologic descriptions are provided in Appendix B. Laboratory Analysis Methodology Sample analysis methods were selected based on potential sources of contaminants as determined from the Phase I ESA. Groundwater and soil samples were analyzed for VOCs by Environmental Protection Agency (EPA) Method 8260B, PAHs by EPA Method 8270C, and 8-RCRA metals by EPA Method 6010 and 7470. The groundwater samples were filtered in the lab prior to analysis. Groundwater Sample BL-1 Boring BL-1 was conducted downgradient and west of the manufacturing building. Geoprobe refusal (bedrock) was encountered at 36 feet bgs and a groundwater sample was collected from the screened interval at 32 to 36 feet bgs. Contaminants of concern (CoC) detected above the laboratory method detection limit included bromodichloromethane (0.21J µg/1), arsenic (3.OJ µg/1), barium (82.4 µg/1), lead (5.9 µg/1), silver (0.18J µg/1), and mercury (0.187 µg/1). No CoC in BL-1 exceeded the 15A NCAC 2L .0202 groundwater standards'. Laboratory analytical results are included in Appendix C and summarized on Tables 1 through 3. Groundwater Sample BL-2 Boring BL-2 was conducted downgradient of and at the northwest corner of the subject property. Geoprobe refusal (bedrock) was encountered at 35 feet bgs and a groundwater sample was collected from the screened interval at 31 to 35 feet bgs. CoC detected above the laboratory method detection limit included cis-1,2-dichloroethene (22.3 µg/1), trichloroethene (4.5 µg/1), arsenic (3.8J µg/1), barium (167 µg/1), silver (0.26J µg/1), and mercury (0.12J µg/1). Trichloroethene (4.5 µg/1) in BL-2 exceeded the 15A NCAC 2L .0202 groundwater standard of 3 µg/1. Laboratory analytical results are included in Appendix C and summarized on Tables 1 through 3. ' North Carolina Groundwater Quality Standards as established in the North Carolina Administrative Code Title 15A, Subchapter 2L-Groundwater Classifications and Standards, dated January 2010. Limited Phase II ESA March 8, 2010 Former P.E. Valve Property BLE Project No. J10-6875-02 Asheville, North Carolina Groundwater Sample BL-3 Boring BL-3 was conducted at the southwest corner of the manufacturing building, downgradient of the AST located on the exterior of the building. Geoprobe refusal (bedrock) was encountered at 37 feet bgs and a groundwater sample was collected from the screened interval at 33 to 37 feet bgs. CoC detected above the laboratory method detection limit included bromodichloromethane (0.23J µg/1), cis-1,2-dichloroethene (0.58J µg/1), trichloroethene (30.2 µg/1), barium (62.6 µg/1), and mercury (0.20 µg/1). Trichloroethene (30.2 µg/1) in BL-3 exceeded the 15A NCAC 2L .0202 groundwater standard of 3 µg/l. Laboratory analytical results are included in Appendix C and summarized on Tables 1 through 3. Groundwater Sample BL-4 Boring BL-4 was conducted adjacent to the loading dock and 40" by 24" metal hinged door used to access the storm water drain sump. Geoprobe refusal (bedrock) was encountered at 26 feet bgs and a groundwater sample was collected from the screened interval at 22 to 26 feet bgs. CoC detected above the laboratory method detection limit included bromodichloromethane (0.24J µg/1), 2-butanone (2.2J µg/1), chloroform (0.16J µg/1), 4-methyl-2-pentanone (0.95J µg/1), toluene (1.2 µg/1), trichloroethene (4.4 µg/1), barium (78.4 µg/1), silver (0.11J µg/1), and mercury (0.28 µg/1). Trichloroethene (4.4 µg/1) in BL-4 exceeded the 15A NCAC 2L .0202 groundwater standard of 3 µg/1. Laboratory analytical results are included in Appendix C and summarized on Tables 1 through 3. Hand Auger Boring Soil Samples Four soil samples (HAB-1 through HAB-4) were collected from beneath the concrete slab in the manufacturing building. Soils encountered were primarily silty clay and gravel fill materials. Soil samples from HAB-1, HAB-2, and HAB-4 were submitted for laboratory analysis. Concentrations of acetone, 2-butanone, chloroform, cis-1,2-dichloroethene, trans-1,2-dichloroethene, toluene, trichloroethene, arsenic, barium, chromium, lead, selenium, silver, and mercury were detected in the soils. Selenium was detected in HAB-4 (4.6 mg/kg) above the North Carolina Inactive Hazardous Sites Branch (IHSB) Soil Remediation Goa12 of 0.29 mg/kg and chromium was detected in HAB-1, HAB-2, and HAB-4 above the IHSB Soil Remediation Goal of 0.29 mg/kg. It should be noted that the IHSB Soil Remediation Goal of 0.29 mg/kg is based on the soil remediation goal for chromium (VI) and not total chromium. Further laboratory testing must be performed to speciate the soil total chromium laboratory results. Laboratory analytical results are included in Appendix C and summarized on Tables 1 through 3. Subsurface Exploration A total of seven geoprobe borings (BL-1 through BL-4 and BR-1 through BR-3) were advanced to refusal, which is generally interpreted as bedrock, during this scope of work. Depths to refusal ranged from 23 to 36 bgs. Soils encountered were primarily silty clays and clayey silts 2 North Carolina Inactive Hazardous Sites Branch (IHSB) Soil Remediation Goals dated January 2010. Both the "Preliminary Health-Based Preliminary Soil Remediation Goals (PSRGs)" and "Protection of Groundwater Preliminary Soil Remediation Goals (PSRGs)" must be met to satisfy the requirements set forth in the IHSB Soil Remediation Goals guidance document. Therefore, IHSB Soil Remediation Goals for individual constituents used during this project are based upon the lower of the two PSRGs. Limited Phase HESA March 8, 2010 Former P.E. Valve Property BLE Project No. J10-6875-02 Asheville, North Carolina grading to saprolite and partially weathered rock at depth. Approximate ground surface elevations and depths to refusal are summarized on Figure 3. 4.0 CONCLUSIONS Four groundwater samples were collected on-site to assess the potential environmental impact of RECs on the property. The samples were analyzed for VOCs, PAHs, and 8-RCRA metals. Trichloroethene was detected in BL-2, BL-3, and BL-4 above the North Carolina 15A NCAC 2L .0202 groundwater standard of 3µg/1. Three soil samples were collected from beneath the concrete slab in the manufacturing building and submitted for laboratory analysis of VOCs, PAHs, and 8-RCRA metals. Selenium in HAB-4 and chromium_ in HAB-1, HAB-2, and HAB-4 were detected above the North Carolina IHSB Soil Remediation Goals. Additionally, a kerosene/heating oil odor was noted in the upper four feet of the continuous macrocore soil sample collected from boring location BR-2. 5.0 QUALIFICATIONS OF REPORT The activities and evaluative approaches used in this assessment are consistent with those normally employed in projects of this type. Our evaluation of site conditions has been based on our understanding of the site and project information, and the data obtained in our exploration. Regardless of the thoroughness of an environmental site assessment, there is always the possibility that conditions between borings will be different from that at the specific boring location due to the variability of subsurface conditions. Therefore, it was not possible to identify all conceivable forms of contamination at this site. The primary objective was to perform sufficient work to assess specific areas of concern that were identified during a review of historical records and site reconnaissance. It was not the purpose of this evaluation to fully define the degree or extent of all forms of contamination. 6 TABLES TABLE 1 ANALYTICAL DATA VOLATILE ORGANIC COMPOUNDS - DETECTED COMPOUNDS ONLY Former P.E. Valve - 1140 Sweeten Creek Road Asheville, North Carolina BLE Project No. J10-6875-02 Analysis Groundwater _ Soil 15A NCAC 2L.0202 (ug/1) BL-1 (ug/1) BL-2 (u9/1) BL.-3 (ug/1) BL-4 (ug/1) IHSB Cone. (mg/kg) HAB-1 (mg/kg) HAB-2 (-g/kg)„ HAB4 (-g/kg) Acetone 6,000 ND _ND ND ND 24 0.0799J 0.123 0.0624) bromodichloromethane 0.6 0.21J ND 023J 0.24J 0.0029 ND ND ND 2-butanone (NIEK) 4,000 ND ND ND 2.2J 16 0.0101 0.01447 ND Chloroform 70 ND ND ND 0.16J 0.30 0.00191 0.0014J 0.00227 Cis-1,2-dichloroethene 70 ND 22.3 0.58J ND 0.36 0.104 0.0013) ND 4-methyl-2-pentanone NE ND ND ND 0.957 NE ND ND ND trans-1,2-dichloroethene 100 ND ND ND ND 0.51 0.0029) ND ND toluene 600 ND ND ND 30.2 1.2 5.5 0.0037J ND ND trichloroethene 3 ND 4.5 4.4 0.018 0.0027) 0.0046 0.0073 Notes: ND = Not Detected at the laboratory method detection limit NE = Not Established J = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit ug/1 = micrograms per liter = parts per billion mg/kg = miligrams per kilogram = parts per million 15A NCAC 2L.0202 = North Carolina Groundwater Quality Standards as established in the North Carolina Administrative Code Title 15A, Subchapter 2L - Groundwater Classifications and standards, dated January 2010 IHSB Cone. = North Carolina Inactive Hazardous Sites Branch (IHSB) Soil Remediation Goals dated January 2010. Both the "Preliminary Health-Based Preliminary Soil Remediation Goals (PSRGs)" and "Protection of Groundwater PSRGs" must be met to satisfy the requirements set forth in the IHSB Soil Remediation Goals guidance document. Therefore, IHSB soil Remediation Goals for individual constituents used during this project are based upon the lower of the two PSRGs. Prepared By: US Checked By: IAI TABLE 2 ANALYTICAL DATA RCRA METALS Former P.E. Valve -1140 Sweeten Creek Road Asheville, North Carolina BLE Project No. J10-6875-02 Analysis Groundwater Soil 15A NCAC 2L.0202 (ug/1) BL-1 (ug/1) BLr2 (ug/1) BL-3 (ug/1) BL-4 (ug/1) lHSB Cone. (mg/kg) HAB-1 (mg/kg) HAB-2 (mg/kg) HAB-4 (mg/kg) Arsenic 10 3.0J 3.8J ND ND 4.4 2.3 3.0 2.6 Barium 700 82.4 167 62.6 78.4 580 77.7 89.3 94.9 Cadmium 2 ND ND ND ND 3.0 ND ND _ND_ Chromium 10 ND ND ND ND 0.29* 14.5 15.6 32.2 Lead 15 5.9 ND ND ND 270 12.0 13.7 11.9 Selenium 20 ND ND ND ND 2.1 1.8J ND -.4.6 Silver 20 0.187 0.127 TO.20 j 0.111 3.4 ND ND ND Mercury 1 0.187 0.28 1.1 0.018 1 0.027 0.088 Notes: ND = Not Detected at the laboratory method detection limit NE = Not Established J = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit ug/1= micrograms per liter = parts per billion mg/kg = miligrams per kilogram = parts per million 15A NCAC 2L.0202 = North Carolina Groundwater Quality Standards as established in the North Carolina Administrative Code Title 15A, Subchapter 2L- Groundwater Classifications and standards, dated January 2010 LHSB Cone. = North Carolina Inactive Hazardous Sites Branch (IHSB) Soil Remediation Goals dated January 2010. Both the "Preliminary Health-Based Preliminary Soil Remediation Goals (PSRGs)" and 'Protection of Groundwater PSRGs" must be met to satisfy the requirements set forth in the IHSB Soil Remediation Goals guidance document. Therefore,1HSB soil Remediation Goals for individual constituents used during this project are based upon the lower of the two PSRGs. Prepared By: TZS Checked By:IAI TABLE 3 ANALYTICAL DATA PAHs - DETECTED COMPOUNDS ONLY Former P.E. Valve - 1140 Sweeten Creek Road Asheville, North Carolina BLE Project No. J10-6875-02 Analysis Groundwater Soil 15ANCAC 2L.0202 11 (ugn) BL -I (ugn) I BL-2 (ugn) I BL-1 (ugn) I BL-4 I IHSB Conc. 11 (mg/kg) HAB-1 (-g/kg) I HAB-2 (mg/kg) I HAB-4 (mg/kg) No PAM were detected above Laboratory Method Detection Limits Notes: ND = Not Detected at the laboratory method detection limit NE = Not Established J = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit ug/l = micrograms per liter = parts per billion mg/kg = miligrams per kilogram = parts per million 15A NCAC 2L.0202 = North Carolina Groundwater Quality Standards as established in the North Carolina Administrative Code Title 15A, Subchapter 2L - Groundwater Classifications and standards, dated January 2010 IHSB Cone. =North Carolina Inactive Hazardous Sites Branch (IHSB) Soil Remediation Goals dated January 2010. Both the "Preliminary Health-Based Preliminary Soil Remediation Goals (PSRGs)" and "Protection of Groundwater PSRGs" must be met to satisfy the requirements set forth in the IHSB Soil Remediation Goals guidance document. Therefore, IHSB soil Remediation Goals for individual constituents used during this project are based upon the lower of the two PSRGs. Prepared By: US Checked By: IAI FIGUIIIJS LOCATION OF WASTE - - _ OIL AND ASTs _ ~} f '°f Ma p. Jam. ka ,j."~1'.~t Y _ _ ~.~'.. !/'. •. 4 r s a r BAY DOOR MACHINING ROOM F, m a~ t 1 ~;_ .{ s. .~.~ 1 d d ' .k ;. 1 • LOCATION OF 40" X 24" METAL •;, "~` r -. "' +-,s` 3 =r HAB2 DOOR USED TO ACCESS r s ~I STORM WATER DRAIN SUMP x r. BR-1 ' BAY DOOR LOADING DOCK BR-3 # + _ PAINT BOOTH ` • p~p— .•1-,X''w`R0-+CJ..i.:`^'4ta`.<.it:. s'f^-.~ks'=~.J.._a ,s'..}. ~ ~i. n'{'.,.J'~'#..f.x I E ~. /M.fT'. --. O HA83 TOOL ROOM BR ►~ - r "'"' ASSEMBLY . " STORAGE O O ROOM BL-2 A w.. 6 . ROOM HAB4 i _ BL-3 OFFICE BL-1 ALT ALT ,d 25 25 BUILDING FLOOR PLAN SCALE. 1 40 BATHROOM LEGEND LEGEND Q FLOOR DRAIN ® APPROXIMATE LOCATION OF GROUNDWATER APPROXIMATE LOCATION OF SCREENING POINT ® SOIL SCREENING POINT ® APPROXIMATE LOCATION OF BORING TO REFUSAL (BEDROCK) ONLY 60 30 0 60 120 REFERENCE: APPROXIMATE SCALE IN FEET BING MAPS. DRAWN BY: ACE DATE: 02-17-10 REVISIONS BLE ELL-LAIwIpNg ENG~EERNq NC, 8004 PONDERS COURT NC. PHONE 4~2t8-5IX6s FAXa(864~zse-44M BORING LOCATION PLAN 1140 SWEETEN CREEK ROAD ASHEVILLE, NORTH CAROLINA FIGURE No. DESCRIPTION BY CHECKED BY: TZS FILE: 1140SWCRKRD-02SM APPROVED BY: TLL JOB NO: J10-6875-02 ~ ,. to k, .' . ,,. • ,.. - . ~ ~ , '11L _~- ILI ~r BR-1 Jw ; = Ti BL-4 BR-3 n y BR-2m m, e o BL-3 r -10 ,~"~ ~ r .. •L ~' tea.' -1 BORING ID# DEPTH TO REFUSAL BELOW GROUND SURFACE APPROXIMATE GROUND SURFACE ELEVATION APPROXIMATE BEDROCK ELEVATION BL-1 36 FEET 2,120 2,084 BL-2 35 FEET 2,122 2,087 BL-3 37 FEET 2,126 2,089 BL-4 26 FEET 2,125 2,099 BR-1 26 FEET 2,130 2,104 BR-2 23 FEET 2,129 2,106 BR-3 25 FEET 2,125 2,100 a - ! 'F.~ —~ ~ '"•~ ' mix_. 9 tP ~. ~ _ F_..s .r ,4 ,~F s -- IF, ip I ru T SOL or 4 .r * fix T r 100 50 0 100 200 APPROXIMATE SCALE IN FEET LEGEND ® APPROXIMATE LOCATION OF GROUNDWATER SCREENING POINT n APPROXIMATE LOCATION OF BORING TO REFUSAL (BEDROCK) ONLY NOTES: 1. CONTOUR INTERVAL = 5 FEET 2. ELEVATION DATA ESTIMATED FROM INSPECTION OF 5—FEET ELEVATION CONTOUR DATA PROVIDED BY THE BUNCOMBE COUNTY, NORTH CAROLINA GIS DATABASE. REFERENCE: BUNCOMBE COUNTY N.C. GIS. DRAWN BY: ACE DATE: 03-04-10 REVISIONS 1131INESEM-LAMMM plpMEpNp, W. 6004 PONDERS COURT NIL NCo PHON~ 4'ff —1265 FA (N6s4~z6 443D BORING LOCATION PLAN WITH TOPOGRAPHY 1140 SWEETEN CREEK ROAD ASHEVILLE, NORTH CAROLINA FIGURE ~p 3 No. DESCRIPTION BY CHECKED BY: TZS FILE: 1140SWCRKRD-02BLP APPROVED BY. TILL JOB NO: J10-6875-02 a: APPENDIX A Geoprobe® Groundwater Screening and Sampling Procedures A groundwater sample was collected using a Geoprobe Systems Screen Point Groundwater Sampler. The assembled sampler had a 1.5-inch outside diameter (OD) and was 48-inches long. The sampler consisted of a 48-inch sealed stainless steel screen encased in a perforated stainless steel sleeve. The sampler was advanced to the desired sampling depth using 5-foot long sections of alloy steel probe rods driven with a portable automatic hammer. At the desired sampling depth, an extension ramrod was attached to extension rods and inserted inside the probe rods. The screen was enclosed in a sampling sheath until it was advanced into the formation at the desired sampling depth. A. General The samples were marked with identifying numbers, placed immediately in sample coolers, secured, and maintained at < 4° C. Preservatives were added to the samples as required. Samples were shipped to Pace Analytical Services, Inc., in Huntersville, NC for analysis. Appropriate chain-of-custody records were maintained. Geoprobe® Soil Screening Procedures Soil samples were collected using a Geoprobe Systems® Sampler. The sampler consisted of a nickel-plated sample tube, replaceable hardened cutting shoe, and a removable acetate liner. The sample tube was capable of recovering cores of soil for laboratory analysis. The sampler was sealed by a piston tip at the end of the sample tube while it was being advanced to the desired sampling depth using sections of alloy steel probe rods driven with a portable automatic hammer. At the desired sampling depth, a piston stop pin at the opposite end of the sampler was removed by means of stainless steel extension rods. The extension rods were inserted down the inside of the probe rods, which enabled the piston to retract into the sample tube while the sample was being taken. The sampler was then driven with the hammer to collect the sample. The sample tube and probe rods were then extracted from the ground. Post extraction, the sample tubes were sealed on each end with vinyl end caps. At 1-foot intervals the sample tube was opened and the resulting soil was scanned using a PID. ~''_J\1 0 a 0 N O N } J Z I ~ CL J J 0 z z z W ,ILIBINC. GEOPROEE BORING NO. ER-2 PROJECT: Former P.E. Valve Property/1140 Sweeten Creek Road PROJECT NO.: J10-6875-02 CLIENT: Colonial Oil START: 2-3-10 END: 2-3-10 BUNNELL-CANNONS ENGINEERING, INCa LOCATION: Asheville, North Carolina ELEVATION: 2129 approximate GEoTECHHIGALAI+®ENvRomms?mL DRILLER: Landprobe, T. Coon LOGGED BY: T. Slack CONSULTANTS DRILLING METHOD: Geoprobe 6600 Truck mount; direct push DEPTH TO - WATER> INITIAL: 21.0 AFTER 24 HOURS: T CAVING> ELEVATION/ DEPTH (FT) DESCRIPTION SOIL TYPE U) EZ a 0— a o W Dark yellowish-orange (10YR6/6), slightly moist to moist CLAY fill with cobbles <2 0.0 centimeters 2 Slight kerosene odor noted from 1.0 to 4.0 feet o'$ 1.6 Moderate red (5R4/6), slightly moist, slightly silty CLAY - (fill) 1.1 4 fill 0.0 Moderate yellowish-brown (10YR5/4) to pale reddish-brown (10R5/4), slightly moist, slightly fine sandy, clayey SILT 0.0 6 0.0 0.0 8 I I 111 0.0 Dark yellowish-brown (10YR4/2), slightly moist, clayey, fine SAND with extremely 0.0 10 weathered saprolitic foliation of light brown (5YR5/6) and dusky yellowish-brown (10114/2) 0.0 0.0 12 Dark yellowish-orange (10YR6/6) and moderate yellowish-brown (10YR5/4), slightly moist 0.1 to moist, clayey, medium to fine SAND with moderately weathered saprolitic foliation of 14 varying degrees of brown, bluish-white (569/1), and olive-black (5Y2/1) 0.0 0.3 0.2 16 0.1 0.3 18 0.2 0.4 20 0.5 22 24 Geoprobe refusal at 23 feet. Groundwater encountered at 21.0 feet at time of drilling. Elevation values obtained from approximate locations on Buncombe County N.C. GIS 26 topographic map. 28 30 32 34 36 38 GEOPROBE BORING NO. BR-2 Sheet 1 of 1 1`LIHiING. GEOPROPE PORING NO. PR-3 PROJECT: Former P.E. Valve Property/1140 Sweeten Creek Road PROJECT NO.: J10-6875-02 [UINELL-LAMMONS CLIENT: Colonial Oil START: 2-3-10 END: 2-3-10 ENGINEERING, INC. LOCATION: Asheville, North Carolina ELEVATION: 2125 approximate GEOTECHNICALANDENvRoNmia AL DRILLER: Landprobe, T. Coon LOGGED BY: T. Slack CONSULTAIM DRILLING METHOD: Geoprobe 6600 Truck mount; direct push DEPTH TO - WATER> INITIAL: 19.0 AFTER 24 HOURS: T CAVING>3M ELEVATION/ DEPTH (FT) DESCRIPTION SOIL TYPE Ul a 2 z_ o w GRAVEL FILL 0.4 2 Moderate yellowish-brown (10YR5/4), slightly moist, fine to medium SAND - (fill) 01 Moderate brown (5YR4/4), slightly moist to moist, fine sandy, silty CLAY with cobbles <2 0.2 centimeters flu 4 0.1 Light brown 5YR5/6) to dark yellowish-orange(10YR6/6 , slightly moist to moist fine 0.4 sandy, clayey SILT with cobbles <2 centimeters 0.1 s Moderate yellowish-brown (10YR5/4) to dark yellowish-brown (10YR4/2), slightly moist to moist, slightly micaceous, clayey, silty, fine SAND 0.0 $ 0.0 0.0 10 0.0 0.3 12 0.0 0.0 14 0.2 0.4 1s 0.1 Dark yellowish-orange (10YR6/6) to moderate yellowish-brown (10YR5/4), moist to wet, 0.2 moderately micaceous, clayey, silty, fine SAND with saprolitic foliation of yellowish-gray 18 (5Y8/1) and dark greenish-gray (5GY4/1) with very weathered feldspar and quartz vein 0.1 about 6-inches thick located at 19.5 to 20.0 feet 0.1 20 0.5 Paleyellowish-brown (10YR6/2) to dark yellowish-orange (10YR6/6)> moist to wet 0.7 moderately micaceous, clayey, medium to coarse SAND with cobbles and slightly 22 weathered saprolitic foliation of mica, feldspar and quartz o.4 0.8 24 0.4 26 Geoprobe refusal at 25 feet. Groundwater encountered at 19.0 feet at time of drilling. Elevation values obtained from approximate locations on Buncombe County N.C. GIS 28 topographic map. 30 32 34 36 38 GEOPROBE BORING NO. BR-3 Sheet 1 of 1 KEY TO SOIL CLASSIFLCL TLZAS AL-~D CONSISTENCY DESCRIPTIONS BUNNELL-LAMMONS ENGINEERING, INC. GREENVILLE, SOUTH CAROLINA Penetration Resistance* Relative Blows per Foot Density Particle Size Identification SANDS Boulder: Greater than 300 mm Cobble: 75 to 300 mm 0 to 4 Very Loose Gravel: 5 to 10 Loose Coarse -19 to 75 mm 11 to 20 Firm Fine - 4.75 to 19 mm 21 to 30 Very Firm Sand: 31 to 50 Dense Coarse - 2 to 4.75 mm over 50 Very Dense Medium - 0.425 to 2 mm Fine - 0.075 to 0.425 mm Silt & Clay: Less than 0.075 mm Penetration Resistance* Consistency Blows per Foot SILTS and CLAYS 0 to 2 Very Soft 3 to 4 Soft 5 to 8 Firm 9 to 15 Stiff 16 to 30 Very Stiff 31 to 50 Hard over 50 Very Hard *ASTM D1586 KEY TO DRILLING SYM30LS ® Grab Sample ® Split Spoon Sample Undisturbed Sample NR = No reaction to HCL NA = Not applicable NS = No sample 1 Groundwater Table at Time of Drilling ® Groundwater Table 24 Hours after Completion of Drilling KEY TO SOIL CLASSIFICATIONS Well-graded Gravel Low Plasticity Clay Clayey Silt M1 Silty Sand GW CL MH SM P30o Poorly-graded Gravel GP Sandy Clay Sandy Silt CLS MLS Topsoil TOPSOIL Partially Weathered Rock Silty Clay Sand Trash BLDRCBBL CL-ML SW MUCKPEAT High Plasticity Clay CH Poorly Graded Sand SP Clayey Sand Fill Sc FILL Limestone LIMESTONE APPENDIX C aeeAnaly~ical ivs»vpacetatis,com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 February 18, 2010 Mr. Trever Slack Bunnell-Lammons Engineering 6004 Ponders Ct Greenville, SC 29615 RE: Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Dear Mr. Slack: Enclosed are the analytical results for sample(s) received by the laboratory on February 06, 2010. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS Page 1 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ~Ll i~.lYbY.,z aceAnalytical www.pace7a'ts,c4m Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Charlotte Certification IDs 9800 Kincey Ave. - Ste 100 Huntersville, NC 28078 West Virginia Certification M 357 Connecticut Certification #: PH-0104 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana/LELAP Certification #: 04034 New Jersey Certification #: NC012 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pennsylvania Certification #: 68-00784 South Carolina Certification #: 990060001 South Carolina Drinking Water Cert. #: 990060003 Tennessee Certification #: 04010 Virginia Certification #: 00213 Asheville Certification IDs Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Louisiana/LELAP Certification #: 03095 Tennessee Certification #: 2980 New Jersey Certification #: NC011 Virginia Certification #: 00072 North Carolina Bioassay Certification #: 9 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 2225 Riverside Dr. Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Connecticut Certification #: PH-0106 Pennsylvania Certification #: 68-03578 Massachusetts Certification #: M-NC030 South Carolina Bioassay Certification #: 99030002 REPORT OF LABORATORY ANALYSIS Page 2 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Former PE Valve/Sweeten Creek Pace Project No,: 9262746 Lab ID Sample ID Matrix Date Collected Date Received 9262746001 BL-1 Water 02/03/10 11:54 02/06/10 09:15 9262746002 BL-2 Water 02/03/10 10:58 02/06/10 09:15 9262746003 BL-3 Water 02/03/10 12:45 02/06/10 09:15 9262746004 BL-4 Water 02/03/10 15:35 02/06/10 09:15 9262746005 HAB-1 Solid 02/03/10 11:10 02/06/10 09:15 9262746006 HAB-2 Solid 02/03/10 11:30 02/06/10 09:15 9262746007 HAB-4 Solid 02/03/10 12:10 02/06/10 09:15 REPORT OF LABORATORY ANALYSIS Page 3 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. ?t+e~''~ lXX cq f 2225 Riverside Dr. UV pacelabs,crim Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported 9262746001 BL-1 EPA 6010 EWS 7 EPA 7470 JMW 1 EPA 8270 PPM 21 EPA 8260 AW 63 9262746002 BL-2 EPA 6010 EWS 7 EPA 7470 JMW 1 EPA 8270 PPM 21 EPA 8260 AW 63 9262746003 BL-3 EPA 6010 EWS 7 EPA 7470 JMW 1 EPA 8270 PPM 21 EPA 8260 AW 63 9262746004 BL-4 EPA 6010 EWS 7 EPA 7470 JMW 1 EPA 8270 PPM 21 EPA 8260 AW 63 9262746005 HAB-1 EPA 6010 EWS 7 EPA 7471 JMW 1 EPA 8270 PPM 24 EPA 8260 DLK 71 ASTM D2974-87 KDF 1 9262746006 HAB-2 EPA 6010 EWS 7 EPA 7471 JMW 1 EPA 8270 PPM 24 EPA 8260 DLK 71 ASTM D2974-87 KDF 1 9262746007 HAB-4 EPA 6010 EWS 7 EPA 7471 JMW 1 EPA 8270 PPM 24 EPA 8260 DLK 71 ASTM D2974-87 KDF 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 44 aceftlytical ivww.pacehtis;com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BL-1 Lab ID: 9262746001 Collected: 02/03/10 11:54 Received: 02/06/10 09:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved 3.OJ ug/L 5.0 2.7 1 02/12/10 11:20 02/16/10 13:44 7440-38-2 Barium, Dissolved 82.4 ug/L 5.0 0.20 1 02/12/10 11:20 02/16/10 13:44 7440-39-3 Cadmium, Dissolved ND ug/L 1.0 0.50 1 02/12/10 11:20 02/16/10 13:44 7440-43-9 Chromium, Dissolved ND ug/L 5.0 0.40 1 02/12/10 11:20 02/16/10 13:44 7440-47-3 Lead, Dissolved 5.9 ug/L 5.0 4.0 1 02/12/10 11:20 02/16/10 13:44 7439-92-1 Selenium, Dissolved ND ug/L 10.0 3.8 1 02/12/10 11:20 02/16/10 13:44 7782-49-2 Silver, Dissolved 0.18J ug/L 5.0 0.10 1 02/12/10 11:20 02/16/10 13:44 7440-22-4 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved 0.18J ug/L 0.20 0.090 1 02/15/10 11:15 02/16/10 14:04 7439-97-6 Z2 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 28.6 8.0 1 02/09/10 08:30 02/11/10 17:09 83-32-9 Acenaphthylene ND ug/L 28.6 8.0 1 02/09/10 08:30 02/11/10 17:09 208-96-8 Anthracene ND ug/L 28.6 8.3 1 02/09/10 08:30 02/11/10 17:09 120-12-7 Benzo(a)anthracene ND ug/L 28.6 8.0 1 02/09/10 08:30 02/11/10 17:09 56-55-3 Benzo(a)pyrene ND ug/L 28.6 8.9 1 02/09/10 08:30 02/11/10 17:09 50-32-8 Benzo(b)fluoranthene ND ug/L 28.6 10.3 1 02/09/10 08:30 02/11/10 17:09 205-99-2 Benzo(g,h,i)perylene ND ug/L 28.6 8.9 1 02/09/10 08:30 02/11/10 17:09 191-24-2 Benzo(k)fluoranthene ND ug/L 28.6 8.6 1 02/09/10 08:30 02/11/10 17:09 207-08-9 Chrysene ND ug/L 28.6 7.7 1 02/09/10 08:30 02/11/10 17:09 218-01-9 Dibenz(a,h)anthracene ND ug/L 28.6 8.3 1 02/09/10 08:30 02/11/10 17:09 53-70-3 Fluoranthene ND ug/L 28.6 8.3 1 02/09/10 08:30 02/11/10 17:09 206-44-0 Fluorene ND ug/L 28.6 7.4 1 02/09/10 08:30 02/11/10 17:09 86-73-7 Indeno(1,2,3-cd)pyrene ND ug/L 28.6 8.6 1 02/09/10 08:30 02/11/10 17:09 193-39-5 1-Methylnaphthalene ND ug/L 28.6 10.3 1 02/09/10 08:30 02/11/10 17:09 90-12-0 2-Methylnaphthalene NO ug/L 28.6 9.7 1 02/09/10 08:30 02/11/10 17:09 91-57-6 Naphthalene ND ug/L 28.6 10.9 1 02/09/10 08:30 02/11/10 17:09 91-20-3 Phenanthrene ND ug/L 28.6 7.7 1 02/09/10 08:30 02/11/10 17:09 85-01-8 Pyrene ND ug/L 28.6 8.3 1 02/09/10 08:30 02/11/10 17:09 129-00-0 Nitrobenzene-d5 (S) 59 % 30-150 1 02/09/10 08:30 02/11/10 17:09 4165-60-0 2-Fiuorobiphenyl (S) 57 % 30-150 1 02/09/10 08:30 02/11/10 17:09 321-60-8 Terphenyl-d14 (S) 62 % 30-150 1 02/09/10 08:30 02/11/10 17:09 1718-51-0 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NO ug/L 25.0 2.2 1 02/10/10 10:08 67-64-1 Benzene ND ug/L 1.0 0.25 1 02/10/10 10:08 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 02/10/10 10:08 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 02/10/10 10:08 74-97-5 Bromodichloromethane 0.21J ug/L 1.0 0.18 1 02/10/1010:08 75-27-4 Bromoform ND ug/L 1.0 0.26 1 02/10/10 10:08 75-25-2 Bromomethane ND ug/L 5.0 0.29 1 02/10/10 10:08 74-83-9 2-Butanone (MEK) NO ug/L 5.0 0.96 1 02/10/10 10:08 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 02/10/10 10:08 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 02/10/10 10:08 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 02/10/10 10:08 75-00-3 Date: 02/18/2010 06:28 PM I REPORT OF LABORATORY ANALYSIS Page 5 of 44 This report shall not be reproduced, except in full, without the written conseentt of Pace Analytical Services, Inc.. JI_I_GiL].4~ Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 - ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BL-1 Lab ID: 9262746001 Collected: 02/03/10 11:54 Received: 02/06/10 09:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Chloroform ND ug/L 1.0 0.14 1 02/10/10 10:08 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 02/10/10 10:08 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 02/10/10 10:08 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 02/10/10 10:08 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 3.0 2.5 1 02/10/1010:08 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 02/10/1010:08 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 02/10/10 10:08 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 02/10/10 10:08 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 02/10/10 10:08 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 02/10/1010:08 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 02/10/1010:08 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 02/10/1010:08 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 02/10/10 10:08 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 02/10/10 10:08 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 02/10/1010:08 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 02/10/1010:08 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 02/10/1010:08 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 02/10/10 10:08 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 02/10/10 10:08 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 02/10/10 10:08 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 02/10/10 10:08 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 0.13 1 02/10/1010:08 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 0.26 1 02/10/10 10:08 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 02/10/10 10:08 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 02/10/10 10:08 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 02/10/10 10:08 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 02/10/10 10:08 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 02/10/10 10:08 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 02/10/10 10:08 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 02/10/10 10:08 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 02/10/10 10:08 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 02/10/10 10:08 91-20-3 Styrene ND ug/L 1.0 0.26 1 02/10/10 10:08 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 02/10/10 10:08 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 02/10/1010:08 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 02/10/10 10:08 127-18-4 Toluene ND ug/L 1.0 0.26 1 02/10/10 10:08 108-88-3 1,2,3-Trchlorobenzene ND ug/L 1.0 0.33 1 02/10/10 10:08 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 02/10/1010:08 120-82-1 1,1,1-Trchloroethane ND ug/L 1.0 0.48 1 02/10/1010:08 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 02/10/1010:08 79-00-5 Trchloroethene ND ug/L 1.0 0.47 1 02/10/10 10:08 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 02/10/10 10:08 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 02/10/1010:08 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 02/10/10 10:08 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 02/10/10 10:08 75-01-4 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 6 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BLA Parameters 8260 MSV Low Level m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofluoromethane (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Lab ID: 9262746001 Collected: 02/03/10 11:54 Received: 02/06/10 09:15 Matrix: Water Report Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[ Analytical Method: EPA 8260 ND ug/L 2.0 0.66 1 02/10/10 10:08 1330-20-7 ND ug/L 1.0 0.23 1 02/10/10 10:08 95-47-6 95 % 87-109 1 02/10/10 10:08 460-00-4 104 % 85-115 1 02/10/10 10:08 1868-53-7 96 % 79-120 1 02/10/10 10:08 17060-07-0 99 % 70-120 1 02/10/10 10:08 2037-26-5 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent ooff Pace Analytical A , nalytical Services, Inc.. Page 7 of 44 aceAnalytiloal wmrpacelatis:com I Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BL-2 Lab ID: 9262746002 Collected: 02/03/1010:58 Received: 02/06/10 09:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 3.8J ug/L 5.0 2.7 1 02/12/10 11:20 02/16/10 13:51 7440-38-2 167 ug/L 5.0 0.20 1 02/12/10 11:20 02/16/1013:51 7440-39-3 ND ug/L 1.0 0.50 1 02/12/10 11:20 02/16/10 13:51 7440-43-9 ND ug/L 5.0 0.40 1 02/12/10 11:20 02/16/1013:51 7440-47-3 ND ug/L 5.0 4.0 1 02/12/10 11:20 02/16/10 13:51 7439-92-1 ND ug/L 10.0 3.8 1 02/12/10 11:20 02/16/10 13:51 7782-49-2 0.26J ug/L 5.0 0.10 1 02/12/10 11:20 02/16/10 13:51 7440-22-4 Analytical Method: EPA 7470 Preparation Method: EPA 7470 0.12J ug/L 0.20 0.090 1 02/15/10 11:15 02/16/1014:09 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 14.3 4.0 1 02/09/10 08:30 02/11/10 17:34 83-32-9 ND ug/L 14,3 4.0 1 02/09/10 08:30 02/11/10 17:34 208-96-8 ND ug/L 14.3 4.1 1 02/09/10 08:30 02/11/10 17:34 120-12-7 ND ug/L 14.3 4.0 1 02/09/10 08:30 02/11/10 17:34 56-55-3 ND ug/L 14.3 4.4 1 02/09/10 08:30 02/11/10 17:34 50-32-8 ND ug/L 14.3 5.1 1 02/09/10 08:30 02/11/1017:34 205-99-2 ND ug/L 14.3 4.4 1 02/09/10 08:30 02/11/10 17:34 191-24-2 ND ug/L 14.3 4.3 1 02/09/10 08:30 02/11/10 17:34 207-08-9 ND ug/L 14.3 3.9 1 02/09/10 08:30 02/11/10 17:34 218-01-9 ND ug/L 14.3 4.1 1 02/09/10 08:30 02/11/10 17:34 53-70-3 ND ug/L 14.3 4.1 1 02/09/10 08:30 02/11/10 17:34 206-44-0 ND ug/L 14.3 3.7 1 02/09/10 08:30 02/11/10 17:34 86-73-7 NO ug/L 14.3 4.3 1 02/09/10 08:30 02/11/10 17:34 193-39-5 ND ug/L 14.3 5.1 1 02/09/10 08:30 02/11/10 17:34 90-12-0 ND ug/L 14.3 4.9 1 02/09/10 08:30 02/11/10 17:34 91-57-6 ND ug/L 14.3 5.4 1 02/09/10 08:30 02/11/10 17:34 91-20-3 ND ug/L 14.3 3.9 1 02/09/10 08:30 02/11/10 17:34 85-01-8 ND ug/L 14.3 4.1 1 02/09/10 08:30 02/11/10 17:34 129-00-0 46 % 30-150 1 02/09/10 08:30 02/11/10 17:34 4165-60-0 49 % 30-150 1 02/09/10 08:30 02/11/10 17:34 321-60-8 57 % 30-150 1 02/09/10 08:30 02/11/10 17:34 1718-51-0 Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 02/10/10 10:32 67-64-1 ND ug/L 1.0 0.25 1 02/10/10 10:32 71-43-2 ND ug/L 1.0 0.30 1 02/10/10 10:32 108-86-1 ND ug/L 1.0 0.17 1 02/10/10 10:32 74-97-5 ND ug/L 1.0 0.18 1 02/10/10 10:32 75-27-4 ND ug/L 1.0 0.26 1 02/10/1010:32 75-25-2 ND ug/L 5.0 0.29 1 02/10/10 10:32 74-83-9 ND ug/L 5.0 0.96 1 02/10/10 10:32 78-93-3 ND ug/L 1.0 0.25 1 02/10/10 10:32 56-23-5 ND ug/L 1.0 0.23 1 02/10/10 10:32 108-90-7 ND ug/L 1.0 0.54 1 02/10/10 10:32 75-00-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Chromium, Dissolved Lead, Dissolved Selenium, Dissolved Silver, Dissolved 7470 Mercury, Lab Filtered Mercury, Dissolved 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenz(a,h )anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Date: 02/18/2010 06:28 PM Page 8 of 44 r7 ) ~+ / Pace Analytical Services, Inc. Pace Analytical Services, Inc. aeeAt al jf ca 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pocefabt.corn Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BL-2 Lab ID: 9262746002 Collected: 02/03/1010:58 Received: 02/06/1009:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Chloroform ND ug/L 1.0 0.14 1 02/10/10 10:32 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 02/10/1010:32 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 02/10/1010:32 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 02/10/1010:32 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 3.0 2.5 1 02/10/1010:32 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 02/10/10 10:32 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 02/10/10 10:32 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 02/10/10 10:32 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 02/10/1010:32 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 02/10/1010:32 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 02/10/1010:32 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 02/10/1010:32 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 02/10/1010:32 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 02/10/1010:32 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 02/10/10 10:32 75-35-4 I cis-1,2-Dichloroethene 22.3 ug/L 1.0 0.19 1 02/10/1010:32 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 02/10/10 10:32 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 02/10/10 10:32 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 02/10/1010:32 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 02/10/10 10:32 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 02/10/10 10:32 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 0.13 1 02/10/1010:32 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 02/10/1010:32 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 02/10/10 10:32 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 02/10/1010:32 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 02/10/1010:32 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 02/10/1010:32 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 02/10/10 10:32 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 02/10/10 10:32 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 02/10/10 10:32 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 02/10/10 10:32 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 02/10/1010:32 91-20-3 Styrene ND ug/L 1.0 0.26 1 02/10/10 10:32 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 02/10/10 10:32 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 02/10/1010:32 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 02/10/1010:32 127-18-4 Toluene ND ug/L 1.0 0.26 1 02/10/1010:32 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 02/10/1010:32 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 02/10/1010:32 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 02/10/1010:32 71-55-6 1,1,2-Trchloroethane ND ug/L 1.0 0.29 1 02/10/1010:32 79-00-5 Trichloroethene 4.5 ug/L 1.0 0.47 1 02/10/1010:32 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 02/10/10 10:32 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 02/10/10 10:32 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 02/10/10 10:32 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 02/10/10 10:32 75-01-4 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 9 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ~lJLl'~elgL~ Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BL-2 Lab ID: 9262746002 Collected: 02/03/10 10:58 Received: 02/06/10 09:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 m&p-Xylene ND ug/L 2.0 0.66 1 02/10/10 10:32 1330-20-7 o-Xylene ND ug/L 1.0 0.23 1 02/10/1010:32 95-47-6 4-Bromofluorobenzene (S) 97 % 87-109 1 02/10/10 10:32 460-00-4 Dibromofluoromethane (S) 103 % 85-115 1 02/10/10 10:32 1868-53-7 1,2-Dichloroethane-d4 (S) 96 % 79-120 1 02/10/10 10:32 17060-07-0 Toluene-d8 (S) 98 % 70-120 1 02/10/10 10:32 2037-26-5 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 10 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. /l_LLlS67ai z aceAnalytical wzrw.paeslatis,cpm Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BL-3 Lab ID: 9262746003 Collected: 02/03/10 12:45 Received: 02/06/10 09:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved NO ug/L 5.0 2.7 1 02/12/10 11:20 02/16/10 13:58 7440-38-2 Barium, Dissolved 62.6 ug/L 5.0 0.20 1 02/12/10 11:20 02/16/10 13:58 7440-39-3 Cadmium, Dissolved ND ug/L 1.0 0.50 1 02/12/10 11:20 02/16/10 13:58 7440-43-9 Chromium, Dissolved ND ug/L 5.0 0.40 1 02/12/10 11:20 02/16/10 13:58 7440-47-3 Lead, Dissolved NO ug/L 5.0 4.0 1 02/12/10 11:20 02/16/10 13:58 7439-92-1 Selenium, Dissolved NO ug/L 10.0 3.8 1 02/12/10 11:20 02/16/10 13:58 7782-49-2 Silver, Dissolved NO ug/L 5.0 0.10 1 02/12/10 11:20 02/16/10 13:58 7440-22-4 7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury, Dissolved 0.20 ug/L 0.20 0.090 1 02/15/10 11:15 02/16/10 14:19 7439-97-6 Z2 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene NO ug/L 14.3 4.0 1 02/09/10 08:30 02/11/1017:59 83-32-9 Acenaphthylene NO ug/L 14.3 4.0 1 02/09/10 08:30 02/11/10 17:59 208-96-8 Anthracene ND ug/L 14.3 4.1 1 02/09/10 08:30 02/11/10 17:59 120-12-7 Benzo(a)anthracene ND ug/L 14.3 4.0 1 02/09/10 08:30 02/11/10 17:59 56-55-3 Benzo(a)pyrene ND ug/L 14.3 4.4 1 02/09/10 08:30 02/11/1017:59 50-32-8 Benzo(b)fluoranthene ND ug/L 14.3 5.1 1 02/09/10 08:30 02/11/1017:59 205-99-2 Benzo(g,h,i)perylene ND ug/L 14.3 4.4 1 02/09/10 08:30 02/11/10 17:59 191-24-2 Benzo(k)fluoranthene NO ug/L 14.3 4.3 1 02/09/10 08:30 02/11/10 17:59 207-08-9 Chrysene NO ug/L 14.3 3.9 1 02/09/10 08:30 02/11/10 17:59 218-01-9 Dibenz(a,h)anthracene ND ug/L 14.3 4.1 1 02/09/10 08:30 02/11/10 17:59 53-70-3 Fluoranthene ND ug/L 14.3 4.1 1 02/09/10 08:30 02/11/10 17:59 206-44-0 Fluorene ND ug/L 14.3 3.7 1 02/09/10 08:30 02/11/10 17:59 86-73-7 Indeno(1,2,3-cd)pyrene ND ug/L 14.3 4.3 1 02/09/10 08:30 02/11/10 17:59 193-39-5 1-Methyinaphthalene ND ug/L 14.3 5.1 1 02/09/10 08:30 02/11/10 17:59 90-12-0 2-Methyinaphthalene ND ug/L 14.3 4.9 1 02/09/10 08:30 02/11/10 17:59 91-57-6 Naphthalene NO ug/L 14.3 5.4 1 02/09/10 08:30 02/11/10 17:59 91-20-3 Phenanthrene ND ug/L 14.3 3.9 1 02/09/10 08:30 02/11/1017:59 85-01-8 Pyrene ND ug/L 14.3 4.1 1 02/09/10 08:30 02/11/10 17:59 129-00-0 Nitrobenzene-d5 (S) 60 % 30-150 1 02/09/10 08:30 02/11/10 17:59 4165-60-0 2-Fluorobiphenyl (S) 59 % 30-150 1 02/09/10 08:30 02/11/10 17:59 321-60-8 Terphenyl-d14 (S) 67 % 30-150 1 02/09/10 08:30 02/11/10 17:59 1718-51-0 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 02/10/10 10:56 67-64-1 Benzene NO ug/L 1.0 0.25 1 02/10/10 10:56 71-43-2 Bromobenzene NO ug/L 1.0 0.30 1 02/10/10 10:56 108-86-1 Bromochloromethane NO ug/L 1.0 0.17 1 02/10/10 10:56 74-97-5 Bromodichloromethane 0.23J ug/L 1.0 0.18 1 02/10/10 10:56 75-27-4 Bromoform ND ug/L 1.0 0.26 1 02/10/10 10:56 75-25-2 Bromomethane NO ug/L 5.0 0.29 1 02/10/10 10:56 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 02/10/10 10:56 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 02/10/10 10:56 56-23-5 Chlorobenzene NO ug/L 1.0 0.23 1 02/10/10 10:56 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 02/10/1010:56 75-00-3 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 11 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. oo~ aCeAnalyioal wmvpacelabs,mm Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 •••r•~• ~~ Lao iv: 9ZU14tiUO3 Collected: 02/03/10 12:45 Received: 02/06/10 09:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Chloroform Chloromethane ND ug/L 1.0 0.14 1 02/10/1010:56 67-66-3 2-Chlorotoluene ND ug/L ND ug/L 1.0 1.0 0.11 1 02/10/10 10:56 74-87-3 4-Chlorotoluene ND ug/L 1.0 0.35 0.31 1 1 02/10/10 10:56 95-49-8 1,2-Dibromo-3-chloropropane ND ug/L 3.0 2.5 1 02/10/10 10:56 106-43-4 Dibromochloromethane ND ug/L 1.0 0.21 1 02/10/1010:56 96-12-8 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 02/10/10 10:56 124-48-1 Dibromomethane ND ug/L 1.0 0.21 1 02/10/10 10:56 106-93-4 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 02/10/10 10:56 74-95-3 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 02/10/1010:56 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 02/10/10 10:56 541-73-1 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 02/10/1010:56 106-46-7 1,1-Dichloroethane ND ug/L 1.0 0.32 1 02/10/1010:56 75-71-8 1,2-Dichloroethane ND ug/L 1.0 0.12 1 02/10/1010:56 75-34-3 1,1-Dichloroethene ND ug/L 1.0 0.56 1 02/10/10 10:56 107-06-2 cis-1,2-Dichloroethene 0.58J ug/L 1.0 0.19 1 02/10/10 10:56 75-35-4 02/10/1010:56 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 02/10/1010:56 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 02/10/1010:56 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 02/10/10 10:56 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 02/10/10 10:56 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 02/10/1010:56 563-58-6 cis- 1, 3-Dichloropropene ND ug/L 1.0 0.13 1 02/10/1010:56 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 0.26 1 02/10/10 10:56 10061-02-6 Diisopropyl ether Ethylbenzene ND ug/L 1.0 0.12 1 02/10/10 10:56 108-20-3 Hexachloro-1,3-butadiene ND ug/L ND ug/L 1.0 1.0 0.30 0.71 1 1 02/10/1010:56 100-41-4 2-Hexanone ND ug/L 5.0 0.46 1 02/10/1010:56 87-68-3 p-Isopropyltoluene ND ug/L 1.0 0.31 1 02/10/1010:56 591-7 02/10/1010:56 99-87-6-6 Methylene Chloride ND ug/L 2.0 0.97 1 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 02/10/10 10:56 75-09-2 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 02/10/10 10:56 108-10-1 Naphthalene ND ug/L 1.0 0.24 1 02/10/10 10:56 1634-04-4 Styrene ND ug/L 1.0 0.26 1 02/10/1010:56 91-20-3 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 02/10/10 10:56 100-42-5 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 02/10/1010:56 630-20-6 Tetrachloroethene ND ug/L 1.0 0.46 1 02/10/1010:56 79-34-5 Toluene ND ug/L 1.0 0.26 1 02/10/1010:56 127-18-4 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 02/10/10 10:56 108-88-3 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 02/10/10 10:56 87-61-6 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 02/10/10 10:56 120-82-1 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 02/10/10 10:56 71-55-6 Trichloroethene 30.2 ug/L 1.0 0.47 1 02/10/10 10:56 79-00-5 Trichlorofluoromethane ND ug/L 1.0 0.20 1 02/10/1010:56 79-01-6 1,2,3-Trichooropropane ND ug/L 1.0 0.41 1 02/10/10 10:56 75-69-4 Vinyl acetate ND ug/L 2.0 0.35 1 02/10/1010:56 96-18-4 Vinyl chloride ND ug/L 1.0 0.62 02/10/10 10:56 108-05-4 1 02/10/10 10:56 75-01-4 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 12 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. N Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BL-3 Lab ID: 9262746003 Collected: 02/03/10 12:45 Received: 02/06/10 09:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 m&p-Xylene ND ug/L 2.0 0.66 1 02/10/10 10:56 1330-20-7 o-Xylene ND ug/L 1.0 0.23 1 02/10/1010:56 95-47-6 4-Bromofluorobenzene (S) 96 % 87-109 1 02/10/10 10:56 460-00-4 Dibromofluoromethane (S) 103 % 85-115 1 02/10/10 10:56 1868-53-7 1,2-Dichloroethane-d4 (S) 98 % 79-120 1 02/10/10 10:56 17060-07-0 Toluene-d8 (S) 97 % 70-120 1 02/10/10 10:56 2037-26-5 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 13 of 44 This report shall not be reproduced, except in full, without the written consent c of Pace C Analytical Services, Inc.. aeeAna~yficai www.pacelabs.corn Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BL-4 Lab ID: 9262746004 Collected: 02/03/10 15:35 Received: 02/06/1009:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 5.0 2.7 1 02/12/10 11:20 02/16/10 14:01 7440-38-2 78.4 ug/L 5.0 0.20 1 02/12/10 11:20 02/16/10 14:01 7440-39-3 ND ug/L 1.0 0.50 1 02/12/10 11:20 02/16/10 14:01 7440-43-9 ND ug/L 5.0 0.40 1 02/12/10 11:20 02/16/1014:01 7440-47-3 ND ug/L 5.0 4.0 1 02/12/10 11:20 02/16/10 14:01 7439-92-1 ND ug/L 10.0 3.8 1 02/12/10 11:20 02/16/10 14:01 7782-49-2 0.11J ug/L 5.0 0.10 1 02/12/1011:20 02/16/1014:01 7440-22-4 Analytical Method: EPA 7470 Preparation Method: EPA 7470 0.28 ug/L 0.20 0.090 1 02/15/10 11:15 02/16/10 14:22 7439-97-6 Z2 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 16.7 4.7 1 02/09/10 08:30 02/11/10 18:24 83-32-9 ND ug/L 16.7 4.7 1 02/09/10 08:30 02/11/10 18:24 208-96-8 ND ug/L 16.7 4.8 1 02/09/10 08:30 02/11/10 18:24 120-12-7 ND ug/L 16.7 4.7 1 02/09/10 08:30 02/11/10 18:24 56-55-3 ND ug/L 16.7 5.2 1 02/09/10 08:30 02/11/10 18:24 50-32-8 ND ug/L 16.7 6.0 1 02/09/10 08:30 02/11/10 18:24 205-99-2 ND ug/L 16.7 5.2 1 02/09/10 08:30 02/11/10 18:24 191-24-2 ND ug/L 16.7 5.0 1 02/09/10 08:30 02/11/10 18:24 207-08-9 ND ug/L 16.7 4.5 1 02/09/10 08:30 02/11/10 18:24 218-01-9 ND ug/L 16.7 4.8 1 02/09/10 08:30 02/11/10 18:24 53-70-3 ND ug/L 16.7 4.8 1 02/09/10 08:30 02/11/10 18:24 206-44-0 ND ug/L 16.7 4.3 1 02/09/10 08:30 02/11/10 18:24 86-73-7 ND ug/L 16.7 5.0 1 02/09/10 08:30 02/11/10 18:24 193-39-5 ND ug/L 16.7 6.0 1 02/09/10 08:30 02/11/10 18:24 90-12-0 ND ug/L 16.7 5.7 1 02/09/10 08:30 02/11/10 18:24 91-57-6 ND ug/L 16.7 6.3 1 02/09/10 08:30 02/11/10 18:24 91-20-3 ND ug/L 16.7 4.5 1 02/09/10 08:30 02/11/10 18:24 85-01-8 ND ug/L 16.7 4.8 1 02/09/10 08:30 02/11/10 18:24 129-00-0 58 % 30-150 1 02/09/10 08:30 02/11/10 18:24 4165-60-0 56 % 30-150 1 02/09/10 08:30 02/11/10 18:24 321-60-8 56 % 30-150 1 02/09/10 08:30 02/11/10 18:24 1718-51-0 6010 MET ICP, Lab Filtered Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Chromium, Dissolved Lead, Dissolved Selenium, Dissolved Silver, Dissolved 7470 Mercury, Lab Filtered Mercury, Dissolved 8270 MSSV Semivolatile Organic Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Di benz(a, h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 02/10/10 11:20 67-64-1 Benzene ND ug/L 1.0 0.25 1 02/10/1011:20 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 02/10/10 11:20 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 02/10/10 11:20 74-97-5 Bromodichloromethane 0.24J ug/L 1.0 0.18 1 02/10/1011:20 75-27-4 Bromoform ND ug/L 1.0 0.26 1 02/10/10 11:20 75-25-2 Bromomethane ND ug/L 5.0 0.29 1 02/10/10 11:20 74-83-9 2-Butanone (MEK) 2.2J ug/L 5.0 0.96 1 02/10/10 11:20 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 02/10/10 11:20 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 02/10/10 11:20 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 02/10/10 11:20 75-00-3 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 44 Pace Analytical Services, Inc. Pace Analytical Services, Inc. a ( f +~ V'(rAn Ij~~C~' t 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 ymw.pacelsbs.cbm Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: BL-4 Lab ID: 9262746004 Collected: 02/03/10 15:35 Received: 02/06/10 09:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Chloroform 0.16J ug/L 1.0 0.14 1 02/10/1011:20 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 02/10/10 11:20 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 02/10/10 11:20 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 02/10/10 11:20 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 3.0 2.5 1 02/10/1011:20 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 02/10/10 11:20 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 02/10/10 11:20 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 02/10/10 11:20 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 02/10/10 11:20 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 02/10/1011:20 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 02/10/1011:20 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 02/10/1011:20 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 02/10/1011:20 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 02/10/1011:20 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 02/10/1011:20 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 02/10/1011:20 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 02/10/1011:20 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 02/10/1011:20 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 02/10/1011:20 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 02/10/1011:20 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 02/1011011:20 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 02/10/1011:20 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 02/10/1011:20 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 02/10/10 11:20 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 02/10/1011:20 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 02/10/1011:20 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 02/10/1011:20 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 02/10/1011:20 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 02/10/10 11:20 75-09-2 4-Methyl-2-pentanone (MIBK) 0.95J ug/L 5.0 0.33 1 02/10/10 11:20 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 02/10/10 11:20 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 02/10/10 11:20 91-20-3 Styrene ND ug/L 1.0 0.26 1 02/10/1011:20 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 02/10/1011:20 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 02/10/10 11:20 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 02/10/10 11:20 127-18-4 Toluene 1.2 ug/L 1.0 0.26 1 02/10/10 11:20 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 02/10/1011:20 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 02/10/10 11:20 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 02/10/1011:20 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 02/10/1011:20 79-00-5 Trichloroethene 4.4 ug/L 1.0 0.47 1 02/10/10 11:20 79-01-6 Tdchlorofluoromethane ND ug/L 1.0 0.20 1 02/10/10 11:20 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 02/10/1011:20 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 02/10/10 11:20 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 02/10/10 11:20 75-01-4 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 15 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnal~ical wsvw.pacelabs,ctlm i i Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BL-4 Lab ID: 9262746004 Collected: 02103/1015-435 Received: 02/06/1009:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 m&p-Xylene ND ug/L 2.0 0.66 1 02/10/10 11:20 1330-20-7 o-Xylene ND ug/L 1.0 0.23 1 02/10/1011:20 95-47-6 4-Bromofluorobenzene (S) 96 % 87-109 1 02/10/10 11:20 460-00-4 Dibromofluoromethane (S) 104 % 85-115 1 02/10/10 11:20 1868-53-7 1,2-Dichloroethane-d4 (S) 96 % 79-120 1 02/10/10 11:20 17060-07-0 Toluene-d8 (S) 98 % 70-120 1 02/10/10 11:20 2037-26-5 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Q`4E°` _°°XC NC~ Page 16 of 44 i aceAnalytical www.p~celabs,cpm Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: HAB-1 Lab ID: 9262746005 Collected: 02/03/1011:10 Received: 02/06/1009:15 Matrix: Solid Results reported on a "dry-weight' basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[ 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 2.3 mg/kg 1.6 1.0 5 02/16/10 12:00 02/18/1010:42 7440-38-2 Barium 77.7 mg/kg 1.6 0.063 5 02/16/1012:00 02/18/1010:42 7440-39-3 Cadmium ND mg/kg 0.32 0.19 5 02/16/1012:00 02/18/1010:42 7440-43-9 Chromium 14.5 mg/kg 1.6 0.095 5 02/16/1012:00 02/18/1010:42 7440-47-3 Lead 12.0 mg/kg 1.6 1.5 5 02/16/1012:00 02/18/1010:42 7439-92-1 Selenium 1.8J mg/kg 3.2 1.2 5 02/16/10 12:00 02/18/10 10:42 7782-49-2 Silver ND mg/kg 1.6 0.095 5 02/16/10 12:00 02/18/10 10:42 7440-22-4 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.018 mg/kg 0.0051 0.00010 1 02/09/10 17:30 02/10/10 13:28 7439-97-6 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 413 95.1 1 02/08/10 10:30 02/10/10 20:44 83-32-9 Acenaphthylene ND ug/kg 413 97.6 1 02/08/10 10:30 02/10/10 20:44 208-96-8 Anthracene ND ug/kg 413 92.6 1 02/08/10 10:30 02/10/10 20:44 120-12-7 Benzo(a)anthracene ND ug/kg 413 76.3 1 02/08/10 10:30 02/10/10 20:44 56-55-3 Benzo(a)pyrene ND ug/kg 413 78.8 1 02/08/10 10:30 02/10/10 20:44 50-32-8 Benzo(b)fluoranthene ND ug/kg 413 71.3 1 02/08/10 10:30 02/10/10 20:44 205-99-2 Benzo(g,h,i)perylene ND ug/kg 413 105 1 02/08/10 10:30 02/10/10 20:44 191-24-2 Benzo(k)fluoranthene ND ug/kg 413 81.3 1 02/08/10 10:30 02/10/10 20:44 207-08-9 Chrysene ND ug/kg 413 55.1 1 02/08/10 10:30 02/10/10 20:44 218-01-9 Dibenz(a,h)anthracene ND ug/kg 413 87.6 1 02/08/10 10:30 02/10/10 20:44 53-70-3 Fluoranthene ND ug/kg 413 60.1 1 02/08/10 10:30 02/10/10 20:44 206-44-0 Fluorene ND ug/kg 413 85.1 1 02/08/10 10:30 02/10/10 20:44 86-73-7 Indeno(1,2,3-cd)pyrene ND ug/kg 413 85.1 1 02/08/10 10:30 02/10/10 20:44 193-39-5 1-Methylnaphthalene ND ug/kg 413 108 1 02/08/10 10:30 02/10/10 20:44 90-12-0 2-Methy1naphthalene ND ug/kg 413 88.8 1 02/08/10 10:30 02/10/10 20:44 91-57-6 Naphthalene ND ug/kg 413 101 1 02/08/10 10:30 02/10/10 20:44 91-20-3 Phenanthrene ND ug/kg 413 68.8 1 02/08/10 10:30 02/10/10 20:44 85-01-8 Pyrene ND ug/kg 413 70.1 1 02/08/10 10:30 02/10/10 20:44 129-00-0 Nitrobenzene-d5 (S) 38 % 30-150 1 02/08/10 10:30 02/10/10 20:44 4165-60-0 2-Fluorobiphenyl (S) 43 % 46-120 1 02/08/10 10:30 02/10/10 20:44 321-60-8 SO Terphenyl-d14 (S) 52 % 38-108 1 02/08/10 10:30 02/10/10 20:44 1718-51-0 Phenol-d6 (S) 49 % 35-120 1 02/08/10 10:30 02/10/10 20:44 13127-88-3 2-Fluorophenol (S) 49 % 24-120 1 02/08/10 10:30 02/10/10 20:44 367-12-4 2,4,6-Tribromophenol (S) 62 % 44-136 1 02/08/10 10:30 02/10/10 20:44 118-79-6 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone 79.9J ug/kg 89.8 9.0 1 02/07/10 12:37 67-64-1 Benzene ND ug/kg 4.5 1.4 1 02/07/1012:37 71-43-2 Bromobenzene ND ug/kg 4.5 1.8 1 02/07/10 12:37 108-86-1 Bromochloromethane ND ug/kg 4.5 1.5 1 02/07/10 12:37 74-97-5 Bromodichloromethane ND ug/kg 4.5 1.7 1 02/07/1012:37 75-27-4 Bromoform ND ug/kg 4.5 2.1 1 02/07/1012:37 75-25-2 Bromomethane ND ug/kg 9.0 2.2 1 02/07/10 12:37 74-83-9 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 17 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. - .~ aeeAnalyticai www.pacelatiscom Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: HAB-1 Lab ID: 9262746005 Collected: 02/03/10 11:10 Received: 02/06/10 09:15 Matrix: Solid Results reported on a "dry-weight' basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 826015035A Volatile Organics Analytical Method: EPA 8260 2-Butanone (MEK) 10.OJ ug/kg 89.8 2.6 1 02/07/10 12:37 78-93-3 n-Butylbenzene ND ug/kg 4.5 1.6 1 02/07/1012:37 104-51-8 sec-Butylbenzene ND ug/kg 4.5 1.4 1 02/07/10 12:37 135-98-8 tert-Butylbenzene ND ug/kg 4.5 1.8 1 02107/1012:37 98-06-6 Carbon tetrachloride ND ug/kg 4.5 2.3 1 02/07/10 12:37 56-23-5 Chlorobenzene ND ug/kg 4.5 1.7 1 02/07/10 12:37 108-90-7 Chloroethane ND ug/kg 9.0 2.2 1 02/07/1012:37 75-00-3 Chloroform 1.9J ug/kg 4.5 1.4 1 02/07/1012:37 67-66-3 Chloromethane ND ug/kg 9.0 2.2 1 02/07/1012:37 74-87-3 2-Chlorotoluene ND ug/kg 4.5 1.5 1 02/07/1012:37 95-49-8 4-Chlorotoluene ND ug/kg 4.5 1.6 1 02107/1012:37 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 4.5 3.2 1 02/07/1012:37 96-12-8 Dibromochloromethane ND ug/kg 4.5 1.6 1 02/07/1012:37 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 4.5 1.6 1 02/07/10 12:37 106-93-4 Dibromomethane ND ug/kg 4.5 2.2 1 02/07/1012:37 74-95-3 1,2-Dichlorobenzene ND ug/kg 4.5 1.7 1 02/07/1012:37 95-50-1 1,3-Dichlorobenzene ND ug/kg 4.5 1.8 1 02/07/1012:37 541-73-1 1,4-Dichlorobenzene ND ug/kg 4.5 1.5 1 02/07/1012:37 106-46-7 Dichlorodifluoromethane ND ug/kg 9.0 3.2 1 02/07/1012:37 75-71-8 1,1-Dichloroethane ND ug/kg 4.5 1.3 1 02/07/1012:37 75-34.3 1,2-Dichloroethane ND ug/kg 4.5 2.0 1 02/07/1012:37 107-06-2 1,1-Dichloroethene ND ug/kg 4.5 1.6 1 02/07/1012:37 75-35-4 cis-1,2-Dichloroethene 104 ug/kg 4.5 1.3 1 02/07/10 12:37 156-59-2 trans-1,2-Dichloroethene 2.9J ug/kg 4.5 1.7 1 02/07/1012:37 156-60-5 1,2-Dichloropropane ND ug/kg 4.5 1.5 1 02/07/1012:37 78-87-5 1,3-Dichloropropane ND ug/kg 4.5 1.7 1 02/07/1012:37 142-28-9 2,2-Dichloropropane ND ug/kg 4.5 1.5 1 02/07/1012:37 594-20-7 1,1-Dichloropropene ND ug/kg 4.5 1.3 1 02/07/1012:37 563-58-6 cis-1,3-Dichloropropene ND ug/kg 4.5 1.6 1 02/07/10 12:37 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 4.5 1.3 1 02/07/10 12:37 10061-02-6 Diisopropyl ether ND ug/kg 4.5 1.5 1 02/07/10 12:37 108-20-3 Ethylbenzene ND ug/kg 4.5 1.6 1 02/07/10 12:37 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 4.5 1.8 1 02/07/10 12:37 87-68-3 2-Hexanone ND ug/kg 44.9 3.5 1 02/07/1012:37 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 4.5 1.7 1 02/07/10 12:37 98-82-8 p-Isopropyltoluene ND ug/kg 4.5 1.5 1 02/07/1012:37 99-87-6 Methylene Chloride ND ug/kg 18.0 2.7 1 02/07/10 12:37 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 44.9 3.3 1 02/07/10 12:37 108-10-1 Methyl-tert-butyl ether ND ug/kg 4.5 1.3 1 02/07/10 12:37 1634-04-4 Naphthalene NO ug/kg 4.5 1.1 1 02/0711012:37 91-20-3 n-Propylbenzene NO ug/kg 4.5 1.5 1 02/07/10 12:37 103-65-1 Styrene NO ug/kg 4.5 1.6 1 02/07/10 12:37 100-42-5 1,1,1,2-Tetrachloroethane NO ug/kg 4.5 1.9 1 02/07/1012:37 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 4.5 1.7 1 02/07/1012:37 79-34-5 Tetrachloroethene ND ug/kg 4.5 1.5 1 02/07/10 12:37 127-18-4 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 18 of 44 This report shall not be reproduced, except in full, without the written consee~ntt of Pace Analytical Services, Inc.. JI_IGI~t.I r n /(n ~ Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnal /f'Kcal 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 c a ! .. Asheville, NC 28804 Huntersville, NC 28078 www.pacelabs.com (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: HAB-1 Lab ID: 9262746005 Collected: 02/03/10 11:10 Received: 02/06/10 09:15 Matrix: Solid Results reported on a "dry-weight' basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 826015035A Volatile Organics Analytical Method: EPA 8260 Toluene 3.7J ug/kg 4.5 1.6 1 02/07/10 12:37 108-88-3 1,2,3-Trichiorobenzene NO ug/kg 4.5 2.0 1 02/07/10 12:37 87-61-6 1,2,4-Trichlorobenzene NO ug/kg 4.5 1.4 1 02/07/10 12:37 120-82-1 1,1,1-Trichloroethane NO ug/kg 4.5 1.6 1 02/07/10 12:37 71-55-6 1,1,2-Trichloroethane ND ug/kg 4.5 1.9 1 02/07/1012:37 79-00-5 Trichloroethene 2.7J ug/kg 4.5 1.9 1 02/07/1012:37 79-01-6 Trichlorofluoromethane ND ug/kg 4.5 2.0 1 02/07/1012:37 75-69-4 1,2,3-Trichloropropane ND ug/kg 4.5 1.4 1 02/07/10 12:37 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 4.5 1.8 1 02/07/10 12:37 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 4.5 1.6 1 02/07/10 12:37 108-67-8 Vinyl acetate ND ug/kg 44.9 7.9 1 02/07/10 12:37 108-05-4 Vinyl chloride ND ug/kg 9.0 1.6 1 02/07/10 12:37 75-01-4 Xylene (Total) ND ug/kg 9.0 3.2 1 02/07/10 12:37 1330-20-7 m&p-Xylene ND ug/kg 9.0 3.2 1 02/07/10 12:37 1330-20-7 o-Xylene ND ug/kg 4.5 1.7 1 02/07/10 12:37 95-47-6 Dibromofluoromethane (S) 109 % 79-116 1 02/07/10 12:37 1868-53-7 Toluene-d8 (S) 100% 88-110 1 02/07/10 12:37 2037-26-5 4-Bromofluorobenzene (S) 83 % 74-115 1 02/07/10 12:37 460-00-4 1,2-Dichloroethane-d4 (S) 115 % 69-121 1 02/07/10 12:37 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 20.1 % 0.10 0.10 1 02/08/10 14:22 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 19 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. K Report Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 6010 Preparation Method: EPA 3050 3.0 mg/kg 1.7 1.1 5 02/16/10 12:00 02/18/1010:46 7440-38-2 89.3 mg/kg 1.7 0.069 5 02/16/10 12:00 02/18/10 10:46 7440-39-3 ND mg/kg 0.35 0.21 5 02/16/10 12:00 02/18/10 10:46 7440-43-9 15.6 mg/kg 1.7 0.10 5 02/16/10 12:00 02/18/10 10:46 7440-47-3 13.7 mg/kg 1.7 1.7 5 02/16/10 12:00 02/18/10 10:46 7439-92-1 NO mg/kg 3.5 1.3 5 02/16/10 12:00 02/18/1010:46 778249-2 NO mg/kg 1.7 0.10 5 02/16/10 12:00 02/18/1010:46 7440-22-4 Analytical Method: EPA 7471 Preparation Method: EPA 7471 0.027 mg/kg 0.0048 0.000097 1 02/09/10 17:30 02/10/10 13:31 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ug/kg 361 83.1 1 02/08/10 10:30 02/10/10 21:09 83-32-9 ND ug/kg 361 85.3 1 02/08/10 10:30 02/10/10 21:09 208-96-8 NO ug/kg 361 81.0 1 02/08/10 10:30 02/10/10 21:09 120-12-7 ND ug/kg 361 66.7 1 02/08/10 10:30 02/10/10 21:09 56-55-3 ND ug/kg 361 68.9 1 02/08/10 10:30 02/10/10 21:09 50-32-8 ND ug/kg 361 62.4 1 02/08/10 10:30 02/10/10 21:09 205-99-2 ND ug/kg 361 91.9 1 02/08/10 10:30 02/10/10 21:09 191-24-2 ND ug/kg 361 71.1 1 02/08/10 10:30 02/10/10 21:09 207-08-9 ND ug/kg 361 48.1 1 02/08/10 10:30 02/10/10 21:09 218-01-9 ND ug/kg 361 76.6 1 02/08/10 10:30 02/10/10 21:09 53-70-3 ND ug/kg 361 52.5 1 02/08/10 10:30 02/10/10 21:09 206-44-0 NO ug/kg 361 74.4 1 02/08/10 10:30 02/10/10 21:09 86-73-7 NO ug/kg 361 74.4 1 02/08/10 10:30 02/10/10 21:09 193-39-5 ND ug/kg 361 94.1 1 02/08/10 10:30 02/10/10 21:09 90-12-0 ND ug/kg 361 77.7 1 02/08/10 10:30 02/10/10 21:09 91-57-6 ND ug/kg 361 88.6 1 02/08/10 10:30 02/10/10 21:09 91-20-3 NO ug/kg 361 60.2 1 02/08/10 10:30 02/10/10 21:09 85-01-8 NO ug/kg 361 61.3 1 02/08/10 10:30 02/10/10 21:09 129-00-0 44 % 30-150 1 02/08/10 10:30 02/10/10 21:09 4165-60-0 43 % 46-120 1 02/08/10 10:30 02/10/10 21:09 321-60-8 52 % 38-108 1 02/08/10 10:30 02/10/10 21:09 1718-51-0 42 % 35-120 1 02/08/10 10:30 02/10/10 21:09 13127-88-3 43 % 24-120 1 02/08/10 10:30 02/10/10 21:09 367-12-4 54 % 44-136 1 02/08/10 10:30 02/10/10 21:09 118-79-6 Analytical Method: EPA 8260 123 ug/kg 82.0 8.2 1 02/07/1010:16 67-64-1 ND ug/kg 4.1 1.3 1 02/07/10 10:16 71-43-2 ND ug/kg 4.1 1.6 1 02/07/10 10:16 108-86-1 ND ug/kg 4.1 1.4 1 02/07/10 10:16 74-97-5 NO ug/kg 4.1 1.6 1 02/07/10 10:16 75-27-4 ND ug/kg 4.1 1.9 1 02/07/1010:16 75-25-2 ND ug/kg 8.2 2.1 1 02/07/1010:16 74-83-9 REPORT OF LABORATORY ANALYSIS Page 20 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc- JLL~.eltdt.; SO C9 aceAnalytical` w-..pacela6s.cnm Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace. Project No.: 9262746 Sample: HAB-2 Lab ID: 9262746006 Collected: 02/03/10 11:30 Received: 02/06/10 09:15 Matrix: Solid Results reported on a "dry-weight' basis Parameters 6010 MET lCP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV Microwave Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenz(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terpheny1-d14 (S) Phenol-d6(S) 2-Fluorophenol (S) 2,4,6-Thbromophenol (S) 826015035A Volatile Organics Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Date: 02/18/2010 06:28 PM aceAnalytical 1vww.pacelals,com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: HAB-2 Lab ID: 9262746006 Collected: 02/03/10 11:30 Received: 02/06/10 09:15 Matrix: Solid Results reported on a "dry-weight' basis Report Results Units Limit MDL Analytical Method: EPA 8260 14.4J ug/kg 82.0 2.4 ND ug/kg 4.1 1.5 ND ug/kg 4.1 1.3 ND ug/kg 4.1 1.6 NO ug/kg 4.1 2.1 ND ug/kg 4.1 1.6 ND ug/kg 8.2 2.0 1.4J ug/kg 4.1 1.3 ND ug/kg 8.2 2.0 ND ug/kg 4.1 1.4 ND ug/kg 4.1 1.5 ND ug/kg 4.1 3.0 ND ug/kg 4.1 1.5 ND ug/kg 4.1 1.5 ND ug/kg 4.1 2.1 ND ug/kg 4.1 1.6 ND ug/kg 4.1 1.6 ND ug/kg 4.1 1.4 ND ug/kg 8.2 3.0 NO ug/kg 4.1 1.2 ND ug/kg 4.1 1.8 ND ug/kg 4.1 1.5 1.3J ug/kg 4.1 1.1 ND ug/kg 4.1 1.6 ND ug/kg 4.1 1.4 ND ug/kg 4.1 1.6 ND ug/kg 4.1 1.4 ND ug/kg 4.1 1.2 ND ug/kg 4.1 1.5 ND ug/kg 4.1 1.2 NO ug/kg 4.1 1.4 ND ug/kg 4.1 1.5 ND ug/kg 4.1 1.6 ND ug/kg 41.0 3.2 ND ug/kg 4.1 1.6 ND ug/kg 4.1 1.4 ND ug/kg 16.4 2.5 ND ug/kg 41.0 3.0 ND ug/kg 4.1 1.2 ND ug/kg 4.1 0.98 ND ug/kg 4.1 1.4 ND ug/kg 4.1 1.5 ND ug/kg 4.1 1.7 ND ug/kg 4.1 1.6 ND ug/kg 4.1 1.4 Parameters 8260/5035A Volatile Organics 2-Butanone (MEK) n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1, 3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1, 3-butadiene 2-Hexanone Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene DF Prepared Analyzed CAS No. Qual 1 02/07/1010:16 78-93-3 1 02/07/10 10:16 104-51-8 1 02/07/10 10:16 135-98-8 1 02/07/1010:16 98-06-6 1 02/07/1010:16 56-23-5 1 02/07/10 10:16 108-90-7 1 02/07/1010:16 75-00-3 1 02/07/1010:16 67-66-3 1 02/07/1010:16 74-87-3 1 02/07/1010:16 95-49-8 1 02/07/10 10:16 106-43-4 1 02/07/1010:16 96-12-8 1 02/07/10 10:16 124-48-1 1 02/07/10 10:16 106-93-4 1 02107/1010:16 74-95-3 1 02/07/1010:16 95-50-1 1 02/07/1010:16 541-73-1 1 02/07/10 10:16 106-46-7 1 02/07/1010:16 75-71-8 1 02/07/1010:16 75-34-3 1 02/07/10 10:16 107-06-2 1 02/07/1010:16 75-35-4 1 02/07/10 10:16 156-59-2 1 02/07/10 10:16 156-60-5 1 02/07/1010:16 78-87-5 1 02/07/10 10:16 142-28-9 1 02/07/1010:16 594-20-7 1 02/07/1010:16 563-58-6 1 02/07/10 10:16 10061-01-5 1 02/07/10 10:16 10061-02-6 1 02/07/10 10:16 108-20-3 1 02/07/10 10:16 100-41-4 1 02/0711010:16 87-68-3 1 02107/1010:16 591-78-6 1 02/07/1010:16 98-82-8 1 02/07/1010:16 99-87-6 1 02/0711010:16 75-09-2 1 02/07/10 10:16 108-10-1 1 02/07/10 10:16 1634-04-4 1 02/07/1010:16 91-20-3 1 02/07/10 10:16 103-65-1 1 02/07/10 10:16 100-42-5 1 02/07/1010:16 630-20-6 1 02/07/1010:16 79-34-5 1 02/07/10 10:16 127-18-4 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. n iJl_I.GI~.t,.l Page 21 of 44 aceAnalytical itiww.pace]a6scprn Pace Analytical Services,.lnc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 I Sample: HAB-2 Lab ID: 9262746006 Collected: 02/03/10 11:30 Received: 02/06/1.0 09:15 Matrix: Solid Results reported on a "dry-weight' basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260/5035A Volatile Organics Analytical Method: EPA 8260 Toluene ND ug/kg 4.1 1.5 1 1,2,3-Trichlorobenzene ND ug/kg 4.1 1.8 1 1,2,4-Trchlorobenzene ND ug/kg 4.1 1.3 1 1, 1, 1 -Trich loroethane ND ug/kg 4.1 1.5 1 1,1,2-Trichloroethane ND ug/kg 4.1 1.7 1 Trichloroethene 4.6 ug/kg 4.1 1.7 1 Trichlorofluoromethane ND ug/kg 4.1 1.8 1 1,2,3-Trichloropropane ND ug/kg 4.1 1.3 1 1,2,4-Trimethylbenzene ND ug/kg 4.1 1.6 1 1,3,5-Trmethylbenzene ND ug/kg 4.1 1.5 1 Vinyl acetate ND ug/kg 41.0 7.2 1 Vinyl chloride ND ug/kg 8.2 1.5 1 Xylene (Total) ND ug/kg 8.2 3.0 1 m&p-Xylene ND ug/kg 8.2 3.0 1 o-Xylene ND ug/kg 4.1 1.6 1 Dibromofluoromethane (S) 107 % 79-116 1 Toluene-d8 (S) 100 % 88-110 1 4-Bromofluorobenzene(S) 82 % 74-115 1 1,2-Dichloroethane-d4 (S) 113 % 69-121 1 02/07/10 10:16 108-88-3 02/07/1010:16 87-61-6 02/07/10 10:16 120-82-1 02/07/1010:16 71-55-6 02/07/1010:16 79-00-5 02/07/1010:16 79-01-6 02/07/1010:16 75-69-4 02/07/1010:16 96-18-4 02/07/1010:16 95-63-6 02/07/10 10:16 108-67-8 02/07/10 10:16 108-05-4 02/07/1010:16 75-01-4 02/07/10 10:16 1330-20-7 02/07/10 10:16 1330-20-7 02/07/1010:16 95-47-6 02/07/10 10:16 1868-53-7 02/07/1010:16 2037-26-5 02/07/1010:16 460-00-4 02/07/10 10:16 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.6 % 0.10 0.10 1 02/08/10 14:23 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 22 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalytical www.pacela'tiscnm Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: HAB-4 Lab ID: 9262746007 Collected: 02/03/10 12:10 Received: 02/06/10 09:15 Matrix: Solid Results reported on a "dry-weight' basis Report Results Units Limit MDL DF Prepared Analyzed CAS No. Analytical Method: EPA 6010 Preparation Method: EPA 3050 2.6 mg/kg 2.2 1.4 5 02/16/10 12:00 02/18/10 10:49 7440-38-2 94.9 mg/kg 2.2 0.087 5 02/16/10 12:00 02/18/10 10:49 7440-39-3 ND mg/kg 0.44 0.26 5 02/16/1012:00 02/18/1010:49 7440-43-9 32.2 mg/kg 2.2 0.13 5 02/16/10 12:00 02/18/10 10:49 7440-47-3 11.9 mg/kg 2.2 2.1 5 02/16/1012:00 02/18/1010:49 7439-92-1 4.6 mg/kg 4.4 1.7 5 02/16/10 12:00 02/18/10 10:49 7782-49-2 ND mg/kg 2.2 0.13 5 02/16/10 12:00 02/18/1010:49 7440-22-4 Analytical Method: EPA 7471 Preparation Method: EPA 7471 0.088 mg/kg 0.0066 0.00013 1 02/09/1017:30 02/10/10 13:33 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3546 ND ug/kg 437 101 1 02/08/10 10:30 02/10/10 21:34 83-32-9 ND ug/kg 437 103 1 02/08/10 10:30 02/10/10 21:34 208-96-8 ND ug/kg 437 98.0 1 02/08/10 10:30 02/10/10 21:34 120-12-7 ND ug/kg 437 80.8 1 02/08/10 10:30 02/10/10 21:34 56-55-3 ND ug/kg 437 83.4 1 02/08/10 10:30 02/10/10 21:34 50-32-8 ND ug/kg 437 75.5 1 02/08/10 10:30 02/10/10 21:34 205-99-2 ND ug/kg 437 111 1 02/08/10 10:30 02/10/10 21:34 191-24-2 ND ug/kg 437 86.1 1 02/08/10 10:30 02/10/10 21:34 207-08-9 ND ug/kg 437 58.3 1 02/08/10 10:30 02/10/10 21:34 218-01-9 ND ug/kg 437 92.7 1 02/08/10 10:30 02/10/10 21:34 53-70-3 ND ug/kg 437 63.6 1 02/08/10 10:30 02/10/10 21:34 206-44-0 ND ug/kg 437 90.0 1 02/08/10 10:30 02/10/10 21:34 86-73-7 ND ug/kg 437 90.0 1 02/08/10 10:30 02/10/10 21:34 193-39-5 ND ug/kg 437 114 1 02/08/10 10:30 02/10/10 21:34 90-12-0 ND ug/kg 437 94.0 1 02/08/1010:30 02/10/1021:34 91-57-6 ND ug/kg 437 107 1 02/08/10 10:30 02/10/10 21:34 91-20-3 ND ug/kg 437 72.8 1 02/08/10 10:30 02/10/10 21:34 85-01-8 ND ug/kg 437 74.1 1 02/08/10 10:30 02/10/10 21:34 129-00-0 46 % 30-150 1 02/08/10 10:30 02/10/10 21:34 4165-60-0 53 % 46-120 1 02/08/10 10:30 02/10/10 21:34 321-60-8 62 % 38-108 1 02/08/10 10:30 02/10/10 21:34 1718-51-0 51 % 35-120 1 02/08/10 10:30 02/10/10 21:34 13127-88-3 39 % 24-120 1 02/08/10 10:30 02/10/10 21:34 367-12-4 72 % 44-136 1 02/08/10 10:30 02/10/10 21:34 118-79-6 Analytical Method: EPA 8260 62AJ ug/kg 119 11.9 1 02/07/1010:35 67-64-1 ND ug/kg 6.0 1.9 1 02/07/1010:35 71-43-2 ND ug/kg 6.0 2.4 1 02/07/10 10:35 108-86-1 ND ug/kg 6.0 2.0 1 02/07/1010:35 74-97-5 NO ug/kg 6.0 2.3 1 02/07/10 10:35 75-27-4 ND ug/kg 6.0 2.7 1 02/07/1010:35 75-25-2 ND ug/kg 11.9 3.0 1 02/07/10 10:35 74-83-9 REPORT OF LABORATORY ANALYSIS Page 23 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. M Parameters 6010 MET ICP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7471 Mercury Mercury 8270 MSSV Microwave Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Di benz(a, h )a nth racen e Fluoranthene Fluorene Indeno(1,2,3-ed)pyrene 1-Methylnaphthalene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-dl4 (S) Phenol-d6(S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260/5035A Volatile Organics Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Date: 02/18/2010 06:28 PM Qual ® aeeAnaytical wxw.pad"$,corh j Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Sample: HAB-4 Lab ID: 9262746007 Collected: 02/03/10 12:10 Received: 02/06/10 09:15 Matrix: Solid Results reported on a "dry-weight' basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 826015035A Volatile Organics Analytical Method: EPA 8260 2-Butanone (MEK) ND ug/kg 119 3.5 1 02/07/10 10:35 78-93-3 n-Butylbenzene ND ug/kg 6.0 2.1 1 02/07/10 10:35 104-51-8 sec-Butylbenzene ND ug/kg 6.0 1.9 1 02/07/10 10:35 135-98-8 tert-Butylbenzene ND ug/kg 6.0 2.4 1 02/07/10 10:35 98-06-6 Carbon tetrachloride ND ug/kg 6.0 3.1 1 02/07/10 10:35 56-23-5 Chlorobenzene ND ug/kg 6.0 2.3 1 02/07/1010:35 108-90-7 Chloroethane ND ug/kg 11.9 2.9 1 02/07/1010:35 75-00-3 Chloroform 2.2J ug/kg 6.0 1.9 1 02/07/1010:35 67-66-3 Chloromethane ND ug/kg 11.9 2.9 1 02/07/10 10:35 74-87-3 2-Chlorotoluene ND ug/kg 6.0 2.0 1 02/07/10 10:35 95-49-8 4-Chlorotoluene ND ug/kg 6.0 2.1 1 02/07/10 10:35 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 6.0 4.3 1 02/07/10 10:35 96-12-8 Dibromochloromethane ND ug/kg 6.0 2.1 1 02/07/10 10:35 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 6.0 2.1 1 02/07/10 10:35 106-93-4 Dibromomethane ND ug/kg 6.0 3.0 1 02/07/10 10:35 74-95-3 1,2-Dichlorobenzene ND ug/kg 6.0 2.3 1 02/07/10 10:35 95-50-1 1,3-Dichlorobenzene ND ug/kg 6.0 2.4 1 02/07/10 10:35 541-73-1 1,4-Dichlorobenzene ND ug/kg 6.0 2.0 1 02/07/1010:35 106-46-7 Dichlorodifluoromethane ND ug/kg 11.9 4.3 1 02/07/10 10:35 75-71-8 1,1-Dichloroethane ND ug/kg 6.0 1.8 1 02/07/1010:35 75-34-3 1,2-Dichloroethane ND ug/kg 6.0 2.6 1 02/07/1010:35 107-06-2 1,1-Dichloroethene ND ug/kg 6.0 2.1 1 02/07/10 10:35 75-35-4 cis-1,2-Dichloroethene ND ug/kg 6.0 1.7 1 02/07/1010:35 156-59-2 trans-1,2-Dichloroethene ND ug/kg 6.0 2.3 1 02/07/1010:35 156-60-5 1,2-Dichloropropane ND ug/kg 6.0 2.0 1 02/07/1010:35 78-87-5 1,3-Dichloropropane ND ug/kg 6.0 2.3 1 02/07/1010:35 142-28-9 2,2-Dichloropropane ND ug/kg 6.0 2.0 1 02/07/10 10:35 594-20-7 1,1-Dichloropropene NO ug/kg 6.0 1.8 1 02/07/10 10:35 563-58-6 cis-1,3-Dichloropropene ND ug/kg 6.0 2.1 1 02/07/10 10:35 10061-01-5 trans-1,3-Dichloropropene ND ug/kg 6.0 1.8 1 02/07/10 10:35 10061-02-6 Diisopropyl ether ND ug/kg 6.0 2.0 1 02/07/10 10:35 108-20-3 Ethylbenzene ND ug/kg 6.0 2.1 1 02/07/10 10:35 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 6.0 2.4 1 02/07/10 10:35 87-68-3 2-Hexanone ND ug/kg 59.6 4.7 1 02/07/10 10:35 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 6.0 2.3 1 02/07/10 10:35 98-82-8 p-Isopropyltoluene ND ug/kg 6.0 2.0 1 02/07/1010:35 99-87-6 Methylene Chloride ND ug/kg 23.9 3.6 1 02/07/10 10:35 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 59.6 4.4 1 02/07/10 10:35 108-10-1 Methyl-tert-butyl ether NO ug/kg 6.0 1.8 1 02/07/10 10:35 1634-04-4 Naphthalene NO ug/kg 6.0 1.4 1 02/07/10 10:35 91-20-3 n-Propylbenzene NO ug/kg 6.0 2.0 1 02/07/10 10:35 103-65-1 Styrene ND ug/kg 6.0 2.1 1 02/07/10 10:35 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 6.0 2.5 1 02/07/1010:35 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 6.0 2.3 1 02/07/1010:35 79-34-5 Tetrachloroethene ND ug/kg 6.0 2.0 1 02/07/10 10:35 127-18-4 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 24 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.paeelabscgm Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Sample: HAB-4 Lab ID: 9262746007 Collected: 02/03/10 12:10 Received: 02/06/10 09:15 Matrix: Solid Results reported on a "dry-weight' basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260/5035A Volatile Organics Analytical Method: EPA 8260 Toluene ND ug/kg 6.0 2.1 1 02/07/1010:35 108-88-3 1,2,3-Trchlorobenzene ND ug/kg 6.0 2.6 1 02/07/1010:35 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 6.0 1.9 1 02/07/1010:35 120-82-1 1,1,1-Trichloroethane ND ug/kg 6.0 2.1 1 02/07/1010:35 71-55-6 1,1,2-Trichloroethane ND ug/kg 6.0 2.5 1 02/07/1010:35 79-00-5 Trichloroethene 7.3 ug/kg 6.0 2.5 1 02/07/1010:35 79-01-6 Trichlorofluoromethane ND ug/kg 6.0 2.6 1 02/07/10 10:35 75-69-4 1,2,3-Trichloropropane ND ug/kg 6.0 1.9 1 02/07/1010:35 96-18-4 1,2,4-Trimethylbenzene ND ug/kg 6.0 2.4 1 02/07/1010:35 95-63-6 1,3,5-Trimethylbenzene ND ug/kg 6.0 2.1 1 02/07/1010:35 108-67-8 Vinyl acetate ND ug/kg 59.6 10.5 1 02/07/10 10:35 108-05-4 Vinyl chloride ND ug/kg 11.9 2.1 1 02/07/10 10:35 75-01-4 Xylene (Total) ND ug/kg 11.9 4.3 1 02/07/1010:35 1330-20-7 m&p-Xylene ND ug/kg 11.9 4.3 1 02/07/10 10:35 1330-20-7 o-Xylene ND ug/kg 6.0 2.3 1 02/07/1010:35 95-47-6 Dibromofluoromethane (S) 107 % 79-116 1 02/07/10 10:35 1868-53-7 Toluene-d8 (S) 102 % 88-110 1 02/07/10 10:35 2037-26-5 4-Bromofluorobenzene (S) 87 % 74-115 1 02/07/10 10:35 460-00-4 1,2-Dichloroethane-d4 (S) 115 % 69-121 1 02/07/10 10:35 17060-07-0 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 24.5 % 0.10 0.10 1 02/08/10 14:23 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 25 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 QC Batch: MPRP/5823 Analysis Method: EPA 6010 QC Batch Method: EPA 3050 Analysis Description: 6010 MET Associated Lab Samples: 9262746005, 9262746006, 9262746007 METHOD BLANK: 401985 Matrix: Solid Associated Lab Samples: 9262746005, 9262746006, 9262746007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Arsenic mg/kg NO 0.50 02/16/1017:31 Barium mg/kg NO 0.50 02/16/1017:31 Cadmium mg/kg ND 0.10 02/16/1017:31 Chromium mg/kg NO 0.50 02/16/1017:31 Lead mg/kg ND 0.50 02/16/1017:31 Selenium mg/kg ND 1.0 02/16/1017:31 Silver mg/kg NO 0.50 02/16/1017:31 LABORATORY CONTROL SAMPLE: 401986 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Arsenic mg/kg 50 47.0 94 80-120 Barium mg/kg 50 48.2 96 80-120 Cadmium mg/kg 50 47.0 94 80-120 Chromium mg/kg 50 47.1 94 80-120 Lead mg/kg 50 47.2 94 80-120 Selenium mg/kg 50 47.7 95 80-120 Silver i mg/kg 25 22.9 92 80-120 MATRIX SPIKE SAMPLE: 401987 ! 9263193001 Spike MS MS % Rec i Parameter Units Result Conc. Result % Rec Limits Qualifiers Arsenic mg/kg ND 34.2 37.0 108 75-125 Barium mg/kg ND 34.2 33.6 98 75-125 Cadmium mg/kg ND 34.2 31.3 91 75-125 Chromium mg/kg 9.38 ug/g 34.2 44.4 102 75-125 Lead mg/kg ND 34.2 28.2 81 75-125 Selenium mg/kg 1.14 ug/g 34.2 45.0 128 75-125 MO Silver mg/kg ND 17.1 15.3 90 75-125 SAMPLE DUPLICATE: 401988 9262867003 Dup Max Parameter Units Result Result RPD RPD Qualifiers Arsenic mg/kg 1.7 1.9 7 20 Barium mg/kg 33.5 27.4 20 20 Cadmium mg/kg 5.0 5.6 13 20 Chromium mg/kg 33.5 31.9 5 20 Lead mg/kg 15.4 17.3 12 20 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 26 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. iJCl~el~].1. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 aceAnaJytical wsnvpace48,com Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA SAMPLE DUPLICATE: 401988 9262867003 Dup Max Parameter Units Result Result RPD RPD Qualifiers Selenium mg/kg 1.5 1.8 21 20 R1 Silver mg/kg ND 0.032J 20 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 27 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. t r ~ Pace Analytical Services, Inc. Pace Analytical Services, Inc. a4+eAt /alX~ca1 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 wwwpacelatis com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 QC Batch: MPRP/5809 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Filtered Associated Lab Samples: 9262746001, 9262746002, 9262746003, 9262746004 METHOD BLANK: 401129 Matrix: Water Associated Lab Samples: 9262746001, 9262746002, 9262746003, 9262746004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Arsenic, Dissolved ug/L ND 5.0 02/16/10 13:28 Barium, Dissolved ug/L ND 5.0 02/16/10 13:28 Cadmium, Dissolved ug/L ND 1.0 02/16/10 13:28 Chromium, Dissolved ug/L ND 5.0 02/16/10 13:28 Lead, Dissolved ug/L ND 5.0 02/16/10 13:28 Selenium, Dissolved ug/L ND 10.0 02/16/10 13:28 Silver, Dissolved ug/L ND 5.0 02/16/10 13:28 LABORATORY CONTROL SAMPLE: 401130 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Arsenic, Dissolved ug/L 500 459 92 80-120 Barium, Dissolved ug/L 500 454 91 80-120 Cadmium, Dissolved ug/L 500 466 93 80-120 Chromium, Dissolved ug/L 500 449 90 80-120 Lead, Dissolved ug/L 500 465 93 80-120 Selenium, Dissolved ug/L 500 465 93 80-120 Silver, Dissolved ug/L 250 233 93 80-120 MATRIX SPIKE SAMPLE: 401131 9262746001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Arsenic, Dissolved ug/L 3.OJ 500 464 92 75-125 Barium, Dissolved ug/L 82.4 500 541 92 75-125 Cadmium, Dissolved ug/L ND 500 464 93 75-125 Chromium, Dissolved ug/L ND 500 465 93 75-125 Lead, Dissolved ug/L 5.9 500 459 91 75-125 Selenium, Dissolved ug/L ND 500 464 92 75-125 Silver, Dissolved ug/L 0.181 250 224 90 75-125 SAMPLE DUPLICATE: 401132 9262746002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Arsenic, Dissolved ug/L 3.8J ND 20 Barium, Dissolved ug/L 167 167 0 20 Cadmium, Dissolved ug/L ND ND 20 Chromium, Dissolved ug/L ND ND 20 Lead, Dissolved ug/L ND ND 20 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 28 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc aeeAnalytical vn+w.paceJatis,com Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 SAMPLE DUPLICATE: 401132 Parameter Units Selenium, Dissolved ug/L Silver, Dissolved ug/L Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA 9262746002 Dup Max Result Result RPD RPD Qualifiers ND ND 20 0.26J 0.32J 20 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 29 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. G~ JI_l_V!lfAr.Yai s ac6AnalyticaI wmvpaeePa'bs,c4m i Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 Pace Analytical Services,. Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 I QC Batch: MERP/2660 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Dissolved Associated Lab Samples: 9262746001, 9262746002, 9262746003, 9262746004 i METHOD BLANK: 402506 Matrix: Water Associated Lab Samples: 9262746001, 9262746002, 9262746003, 9262746004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury, Dissolved ug/L 0.0901 0.20 02/16/10 14:27 I LABORATORY CONTROL SAMPLE: 402507 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Mercury, Dissolved ug/L 2.5 2.4 97 80-120 MATRIX SPIKE SAMPLE: 402508 i 9262746001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Mercury, Dissolved ug/L 0.18J 2.5 2.6 95 75-125 SAMPLE DUPLICATE: 402509 9262746002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Mercury, Dissolved ug/L 0.12J 0.151 25 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 30 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. uL~L~ z pr n ~7 I ) Pace Analytical Services, Inc. Pace Analytical Services, Inc. acoA[ lat )j~~Cal 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 annvpacela'tis com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 QC Batch: MERP/2647 Analysis Method: EPA 7471 QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury Associated Lab Samples: 9262746005, 9262746006, 9262746007 METHOD BLANK: 399900 Matrix: Solid Associated Lab Samples: 9262746005, 9262746006, 9262746007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury mg/kg ND 0.0050 02/10/1012:23 LABORATORY CONTROL SAMPLE: 399901 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury mg/kg .067 0.063 95 80-120 MATRIX SPIKE SAMPLE: i Parameter Mercury SAMPLE DUPLICATE: 399903 I j Parameter Mercury 399902 9262341001 Spike MS MS % Rec Units Result Conc. Result % Rec Limits Qualifiers mg/kg 0.0048 .072 0.074 97 75-125 9262341002 Dup Max Units Result Result RPD RPD Qualifiers mg/kg 0.12 0.14 11 20 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 31 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalytical wmvpacelabs;com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 QC Batch: 0EXT/9218 Analysis Method: EPA 8270 QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave Associated Lab Samples: 9262746005, 9262746006, 9262746007 METHOD BLANK: 399710 Matrix: Solid Associated Lab Samples: 9262746005, 9262746006, 9262746007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1-Methylnaphthalene ug/kg ND 2-Methylnaphthalene ug/kg ND Acenaphthene ug/kg ND Acenaphthylene ug/kg ND Anthracene ug/kg ND Benzo(a)anthracene ug/kg ND Benzo(a)pyrene ug/kg ND Benzo(b)fluoranthene ug/kg ND Benzo(g,h,i)perylene ug/kg ND Benzo(k)fluoranthene ug/kg ND Chrysene ug/kg ND Dibenz(a,h)anthracene ug/kg ND Fluoranthene ug/kg ND Fluorene ug/kg ND Indeno(1,2,3-cd)pyrene ug/kg ND Naphthalene ug/kg ND Phenanthrene ug/kg ND Pyrene ug/kg ND 2,4,6-Tribromophenol (S) % 76 2-Fluorobiphenyl (S) % 63 2-Fluorophenol (S) % 82 Nitrobenzene-d5 (S) % 62 Phenol-d6 (S) % 64 Terphenyl-d14 (S) % 71 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 330 02/09/1018:22 44-136 02/09/1018:22 46-120 02/09/1018:22 24-120 02/09/1018:22 30-150 02/09/1018:22 35-120 02/09/1018:22 38-108 02/09/1018:22 LABORATORY CONTROL SAMPLE & LCSD: 399711 Parameter Units Spike Conc. 399712 LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Limits RPD Max RPD Qualifiers 1-Methylnaphthalene ug/kg 1670 1310 1160 79 70 50-150 12 30 2-Methylnaphthalene ug/kg 1670 1310 1130 79 68 50-150 15 30 Acenaphthene ug/kg 1670 1360 1290 82 77 50-150 5 30 Acenaphthylene ug/kg 1670 1350 1290 81 77 50-150 4 30 Anthracene ug/kg 1670 1370 1400 82 84 50-150 2 30 Benzo(a)anthracene ug/kg 1670 1530 1540 92 92 50-150 0 30 Benzo(a)pyrene ug/kg 1670 1390 1360 83 81 50-150 2 30 Benzo(b)fluoranthene ug/kg 1670 1430 1350 86 81 50-150 5 30 Benzo(g,h,i)perylene ug/kg 1670 1550 1520 93 91 24-117 2 30 Benzo(k)fluoranthene ug/kg 1670 1320 1320 79 79 50-150 0 30 Chrysene ug/kg 1670 1330 1370 80 82 50-150 3 30 Dibenz(a,h)anthracene ug/kg 1670 1600 1550 96 93 17-128 3 30 Fluoranthene ug/kg 1670 1410 1410 85 84 50-150 1 30 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 32 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. rr+qq f f ;~ Pace Analytical Services, Inc. Pace Analytical Services, Inc. aC, Ai al ~G' ! 2225 Riverside Dc 9800 Kincey Ave. Suite 100 —..pacelabsxom Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 LABORATORY CONTROL SAMPLE & LCSD: 399711 399712 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Cone. Result Result % Rec % Rec Limits RPD RPD Qualifiers Fluorene ug/kg 1670 1400 1340 84 80 50-150 4 30 Indeno(1,2,3-cd)pyrene ug/kg 1670 1560 1510 94 91 19-128 3 30 Naphthalene ug/kg 1670 1290 982 78 59 50-150 27 30 Phenanthrene ug/kg 1670 1380 1460 83 88 50-150 5 30 Pyrene ug/kg 1670 1290 1310 78 78 50-150 1 30 2,4,6-Tribromophenol (S) % 90 90 44-136 2-Fluorobiphenyl (S) % 79 71 46-120 2-Fluorophenol (S) % 85 59 24-120 Nitrobenzene-d5 (S) % 78 60 30-150 Phenol-d6(S) % 86 65 35-120 Terphenyl-d14 (S) % 79 79 38-108 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 399713 399714 MS MSD 9262638001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual 1-Methylnaphthalene ug/kg NO 2220 2220 1490 1150 64 48 50-150 26 30 MO 2-Methylnaphthalene ug/kg ND 2220 2220 1440 1100 63 47 50-150 27 30 MO Acenaphthene ug/kg ND 2220 2220 1420 1190 64 54 50-150 17 30 Acenaphthylene ug/kg ND 2220 2220 1410 1180 64 53 50-150 18 30 Anthracene ug/kg NO 2220 2220 1480 1310 67 59 50-150 12 30 Benzo(a)anthracene ug/kg NO 2220 2220 1470 1360 67 61 50-150 8 30 Benzo(a)pyrene ug/kg ND 2220 2220 1370 1250 62 57 50-150 9 30 Benzo(b)fluoranthene ug/kg NO 2220 2220 1350 1240 61 56 50-150 8 30 Benzo(g,h,i)perylene ug/kg ND 2220 2220 1540 1390 70 63 50-150 11 30 Benzo(k)fluoranthene ug/kg NO 2220 2220 1290 1230 58 55 50-150 5 30 Chrysene ug/kg NO 2220 2220 1420 1290 64 58 50-150 9 30 Dibenz(a,h)anthracene ug/kg NO 2220 2220 1570 1420 71 64 50-150 10 30 Fluoranthene ug/kg ND 2220 2220 1470 1340 67 60 50-150 10 30 Fluorene ug/kg NO 2220 2220 1480 1300 67 59 50-150 13 30 Indeno(1,2,3-cd)pyrene ug/kg ND 2220 2220 1530 1380 69 62 50-150 10 30 Naphthalene ug/kg NO 2220 2220 1290 998 58 45 50-150 26 30 MO Phenanthrene ug/kg NO 2220 2220 1480 1350 67 61 50-150 9 30 Pyrene ug/kg NO 2220 2220 1400 1270 63 57 50-150 10 30 2,4,6-Tribromophenol (S) % 69 64 44-136 2-Fluorobiphenyl (S) % 57 47 46-120 2-Fluorophenol (S) % 50 38 24-120 Nitrobenzene-d5 (S) % 53 42 30-150 Phenol-d6 (S) % 57 43 35-120 Terphenyl-d14 (S) % 56 54 38-108 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 33 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalytical www.p~cela'bs,cpm i Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 QC Batch: 0EXT/9221 Analysis Method: EPA 8270 QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV Associated Lab Samples: 9262746001, 9262746002, 9262746003, 9262746004 METHOD BLANK: 399863 Matrix: Water Associated Lab Samples: 9262746001, 9262746002, 9262746003, 9262746004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1-Methylnaphthalene ug/L ND 10.0 02/11/10 02:53 2-Methylnaphthalene ug/L ND 10.0 02/11/10 02:53 Acenaphthene ug/L ND 10.0 02/11/10 02:53 Acenaphthylene ug/L ND 10.0 02/11/10 02:53 Anthracene ug/L ND 10.0 02/11/10 02:53 Benzo(a)anthracene ug/L ND 10.0 02/11/10 02:53 Benzo(a)pyrene ug/L ND 10.0 02/11/10 02:53 Benzo(b)fluoranthene ug/L ND 10.0 02/11/10 02:53 Benzo(g,h,i)perylene ug/L ND 10.0 02/11/10 02:53 Benzo(k)fluoranthene ug/L ND 10.0 02/11/10 02:53 Chrysene ug/L ND 10.0 02/11/10 02:53 Dibenz(a,h)anthracene ug/L ND 10.0 02/11/10 02:53 Fluoranthene ug/L ND 10.0 02/11/10 02:53 Fluorene ug/L ND 10.0 02/11/10 02:53 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 02/11/10 02:53 Naphthalene ug/L ND 10.0 02/11/10 02:53 Phenanthrene ug/L ND 10.0 02/11/10 02:53 Pyrene ug/L ND 10.0 02/11/10 02:53 2,4,6-Tribromophenol (S) % 67 25-150 02/11/10 02:53 2-Fluorobiphenyl (S) % 57 30-150 02/11/10 02:53 2-Fluorophenol (S) % 36 25-150 02/11/10 02:53 Nitrobenzene-d5 (S) % 58 30-150 02/11/10 02:53 Phenol-d6(S) % 22 25-150 02/11/10 02:53 SO Terphenyl-d14 (S) % 65 30-150 02/11/10 02:53 LABORATORY CONTROL SAMPLE & LCSD: Parameter 399864 Spike Units Conc. 399865 LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Limits RPD Max RPD Qualifiers 1-Methylnaphthalene ug/L 50 24.6 26.8 49 54 21-120 9 30 2-Methylnaphthalene ug/L 50 23.4 25.8 47 52 19-120 10 30 Acenaphthene ug/L 50 35.6 31.1 71 62 27-102 14 30 Acenaphthylene ug/L 50 37.6 32.4 75 65 25-105 15 30 Anthracene ug/L 50 36.4 36.3 73 73 30-113 0 30 Benzo(a)anthracene ug/L 50 40.4 40.9 81 82 27-113 1 30 Benzo(a)pyrene ug/L 50 36.2 35.8 72 72 27-119 1 30 Benzo(b)fluoranthene ug/L 50 37.0 36.6 74 73 22-114 1 30 Benzo(g,h,i)perylene ug/L 50 36.8 36.6 74 73 10-129 1 30 Benzo(k)fluoranthene ug/L 50 33.4 34.2 67 68 24-111 2 30 Chrysene ug/L 50 35.6 35.4 71 71 23-112 0 30 Dibenz(a,h)anthracene ug/L 50 39.3 39.2 79 78 10-129 0 30 Fluoranthene ug/L 50 41.0 38.4 82 77 27-112 7 30 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 34 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc i lJl_~.vflfdV.i i i 0 aceAnalytical www.pacelaos, oin I Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 LABORATORY CONTROL SAMPLE & LCSD: 399864 Parameter Units Fluorene ug/L Indeno(1,2,3-cd)pyrene ug/L Naphthalene ug/L Phenanthrene ug/L Pyrene ug/L 2,4,6-Tribromophenol (S) % 2-Fluorobiphenyl (S) % 2-Fluorophenol (S) % Nitrobenzene-d5 (S) % Phenol-d6 (S) % Terpheny1-d14 (S) % QUALITY CONTROL DATA 399865 Spike LCS LCSD LCS LCSD % Rec Conc. Result Result % Rec % Rec Limits RPD 50 40.6 34.5 81 69 29-107 - 16 50 38.3 37.7 77 75 14-123 1 50 24.6 27.3 49 55 17-120 10 50 38.4 35.9 77 72 28-111 7 50 34.5 34.6 69 69 27-113 0 83 75 25-150 75 63 30-150 32 39 25-150 59 63 30-150 24 26 25-150 67 66 30-150 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 Max RPD Qualifiers 30 30 30 30 30 SO Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 35 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 3.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 5.0 02/10/10 02:09 1.0 02/10/10 02:09 5.0 02/10/10 02:09 1.0 02/10/10 02:09 5.0 02/10/10 02:09 25.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 5.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 1.0 02/10/10 02:09 C9 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.36J ND ND ND ND ND 2.0 ND ND ND ND ND ND ND ND ffi aceAnalj4pal ww.pacelags com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 QC Batch: MSV/9899 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 9262746001, 9262746002, 9262746003, 9262746004 METHOD BLANK: 400376 Matrix: Water Associated Lab Samples: 9262746001, 9262746002, 9262746003, 9262746004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2, 3-Trich loropropane 1,2,4-Trichlorobenzene 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dick loroethene cis-1,3-Dich loropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diisopropyl ether Ethylbenzene Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 11y 11%1I' q0 ~ Page 36 of 44 Pace Analytical Services, Inc. Pace Analytical Services, Inc. !ice na jl/1'''cgl 2225 Riverside Dr. 9800 KinceyAve. Suite 100 lss[[n ~ . p cea s. co Asheville, NC 28804 Huntersville, NC 28078 »nvp~ci:/atis,cnm (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 METHOD BLANK: 400376 Matrix: Water Associated Lab Samples: 9262746001, 9262746002, 9262746003, 9262746004 Blank Reporting Parameter i Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L ND 1.0 02/10/10 02:09 m&p-Xylene ug/L ND 2.0 02/10/10 02:09 Methyl-tert-butyl ether ug/L ND 1.0 02/10/10 02:09 Methylene Chloride ug/L ND 2.0 02/10/10 02:09 Naphthalene ug/L ND 1.0 02/10/10 02:09 o-Xylene ug/L ND 1.0 02/10/10 02:09 p-lsopropyltoluene ug/L NO 1.0 02/10/10 02:09 Styrene ug/L ND 1.0 02/10/10 02:09 Tetrachloroethene ug/L NO 1.0 02/10/10 02:09 Toluene ug/L NO 1.0 02/10/10 02:09 trans-1,2-Dichloroethene ug/L ND 1.0 02/10/10 02:09 trans-1,3-Dichloropropene ug/L ND 1.0 02/10/10 02:09 Trichloroethene ug/L ND 1.0 02/10/10 02:09 Trichlorofluoromethane ug/L ND 1.0 02/10/10 02:09 j Vinyl acetate ug/L ND 2.0 02/10/10 02:09 Vinyl chloride ug/L NO 1.0 02/10/10 02:09 1,2-Dichloroethane-d4 (S) % 89 79-120 02/10/10 02:09 4-Bromofluorobenzene (S) % 96 87-109 02/10/10 02:09 Dibromofluoromethane (S) % 100 85-115 02/10/10 02:09 Toluene-d8 (S) % 98 70-120 02/10/10 02:09 LABORATORY CONTROL SAMPLE: Parameter 400377 Units Spike Cone. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 51.2 102 83-125 1,1,1-Trichloroethane ug/L 50 44.9 90 80-129 1,1,2,2-Tetrachloroethane ug/L 50 49.2 98 73-127 1,1,2-Trichloroethane ug/L 50 50.3 101 77-123 1,1-Dichloroethane ug/L 50 50.7 101 76-129 1,1-Dichloroethene ug/L 50 43.7 87 78-146 1,1-Dichloropropene ug/L 50 44.8 90 79-134 1,2,3-Tdchlorobenzene ug/L 50 55.0 110 70-150 i 1,2,3-Trichloropropane ug/L 50 49.0 98 72-125 1,2,4-Trichlorobenzene ug/L 50 55.0 110 68-127 1,2-Dibromo-3-chloropropane ug/L 50 45.5 91 65-128 1,2-Dibromoethane (EDB) ug/L 50 53.2 106 81-125 1,2-Dichlorobenzene ug/L 50 54.0 108 82-126 1,2-Dichloroethane ug/L 50 40.5 81 72-126 1,2-Dichloropropane ug/L 50 50.4 101 80-127 1,3-Dichlorobenzene ug/L 50 53.5 107 82-124 1,3-Dichloropropane ug/L 50 52.1 104 79-124 1,4-Dichlorobenzene ug/L 50 52.7 105 79-125 2,2-Dichloropropane ug/L 50 40.3 81 58-140 2-Butanone (MEK) ug/L 100 86.1 86 50-134 2-Chlorotoluene ug/L 50 52.8 106 81-126 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 37 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ~4C a~ 1~= ace Analytical wmvpacelatis,com I Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 LABORATORY CONTROL SAMPLE: Parameter 400377 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2-Hexanone ug/L 100 106 106 58-138 4-Chlorotoluene ug/L 50 55.2 110 82-126 4-Methyl-2-pentanone (MIBK) ug/L 100 98.7 99 70-131 Acetone ug/L 100 27.6 28 50-146 LO Benzene ug/L 50 49.6 99 78-128 Bromobenzene ug/L 50 53.7 107 81-127 Bromochloromethane ug/L 50 47.8 96 73-124 Bromodichloromethane ug/L 50 42.4 85 81-125 Bromoform ug/L 50 52.7 105 71-125 Bromomethane ug/L 50 40.6 81 50-150 Carbon tetrachloride ug/L 50 44.8 90 81-137 Chlorobenzene ug/L 50 52.8 106 82-126 Chloroethane ug/L 50 42.1 84 69-140 Chloroform ug/L 50 45.8 92 77-129 Chloromethane ug/L 50 33.1 66 54-139 cis-1,2-Dichloroethene ug/L 50 47.9 96 76-133 cis-1,3-Dichloropropene ug/L 50 49.2 98 76-127 Dibromochloromethane ug/L 50 48.5 97 77-125 Dibromomethane ug/L 50 52.6 105 77-125 Dichlorodifluoromethane ug/L 50 27.5 55 50-150 Diisopropyl ether ug/L 50 46.4 93 74-131 Ethylbenzene ug/L 50 51.9 104 80-127 Hexachloro-1,3-butadiene ug/L 50 48.3 97 78-145 m&p-Xylene ug/L 100 106 106 82-127 Methyl-tert-butyl ether ug/L 50 48.6 97 71-130 Methylene Chloride ug/L 50 41.9 84 67-133 Naphthalene ug/L 50 53.4 107 52-136 o-Xylene ug/L 50 52.1 104 83-124 p-Isopropyltoluene ug/L 50 55.2 110 73-122 Styrene ug/L 50 54.5 109 80-130 Tetrachloroethene ug/L 50 51.0 102 78-128 Toluene ug/L 50 48.0 96 76-126 trans-1,2-Dichloroethene ug/L 50 44.5 89 78-134 trans-1,3-Dichloropropene ug/L 50 47.9 96 75-125 Trichloroethene ug/L 50 47.4 95 79-127 Trichlorofluoromethane ug/L 50 34.8 70 76-148 LO Vinyl acetate ug/L 100 106 106 50-150 Vinyl chloride ug/L 50 35.3 71 67-143 1,2-Dichloroethane-d4 (S) % 84 79-120 4-Bromofluorobenzene (S) % 97 87-109 Dibromocuoromethane (S) % 95 85-115 Toluene-d8 (S) % 97 70-120 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 38 of 44 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.91 ND ND ND ND ND ND i ace Analytical www.pacelabs,cnm Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 QC Batch: MSV/9889 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics Associated Lab Samples: 9262746005, 9262746006, 9262746007 METHOD BLANK: 399644 Matrix: Solid Associated Lab Samples: 9262746005,9262746006,9262746007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1, 1, 1,2-Tetrachloroethane 1, 1, 1 -Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1, 2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2, 3-Trichlorobenzene 1,2, 3-Trichooropropane 1,24-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-chioropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1, 2-Dichloroethene cis-1, 3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 100 02/07/10 07:54 5.0 02/07/10 07:54 50.0 02/07/10 07:54 5.0 02/07/10 07:54 50.0 02/07/10 07:54 100 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 10.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 10.0 02/07/10 07:54 5.0 02/07/10 07:54 10.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 5.0 02/07/10 07:54 10.0 02/07/10 07:54 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 39 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. An 2225 Riverside Dr. www.pacekbs,com Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ECG QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 METHOD BLANK: 399644 Matrix: Solid Associated Lab Samples: 9262746005, 9262746006, 9262746007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diisopropyl ether ug/kg NO 5.0 02/07/10 07:54 Ethylbenzene ug/kg ND 5.0 02/07/10 07:54 Hexachloro-1,3-butadiene ug/kg ND 5.0 02/07/10 07:54 Isopropylbenzene (Cumene) ug/kg NO 5.0 02/07/10 07:54 m&p-Xylene ug/kg ND 10.0 02/07/10 07:54 Methyl-tert-butyl ether ug/kg NO 5.0 02/07/10 07:54 Methylene Chloride ug/kg NO 20.0 02/07/10 07:54 n-Butylbenzene ug/kg NO 5.0 02/07/10 07:54 n-Propylbenzene ug/kg NO 5.0 02/07/10 07:54 Naphthalene ug/kg NO 5.0 02/07/10 07:54 o-Xylene ug/kg NO 5.0 02/07/10 07:54 p-Isopropyltoluene ug/kg NO 5.0 02/07/10 07:54 sec-Butylbenzene ug/kg NO 5.0 02/07/10 07:54 Styrene ug/kg ND 5.0 02/07/10 07:54 tert-Butylbenzene ug/kg NO 5.0 02/07/10 07:54 Tetrachloroethene ug/kg NO 5.0 02/07/10 07:54 Toluene ug/kg NO 5.0 02/07/10 07:54 traris-1,2-Dichloroethene ug/kg ND 5.0 02/07/10 07:54 trans-1,3-Dichloropropene ug/kg NO 5.0 02/07/10 07:54 Trichloroethene ug/kg NO 5.0 02/07/10 07:54 Trichlorofluoromethane ug/kg NO 5.0 02/07/10 07:54 Vinyl acetate ug/kg NO 50.0 02/07/10 07:54 Vinyl chloride ug/kg NO 10.0 02/07/10 07:54 Xylene (Total) ug/kg NO 10.0 02/07/10 07:54 1,2-Dichloroethane-d4 (S) % 113 69-121 02/07/10 07:54 4-Bromofluorobenzene (S) % 85 74-115 02/07/10 07:54 Dibromofluoromethane (S) % 108 79-116 02/07/10 07:54 Toluene-d8 (S) % 100 88-110 02/07/10 07:54 LABORATORY CONTROL SAMPLE: Parameter 399645 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/kg 50 52.1 104 75-137 1,1,1-Trichloroethane ug/kg 50 61.2 122 70-140 1,1,2,2-Tetrachloroethane ug/kg 50 52.8 106 74-133 1,1,2-Trichloroethane ug/kg 50 56.8 114 79-129 1,1-Dichloroethane ug/kg 50 64.8 130 72-139 1,1-Dichloroethene ug/kg 50 55.8 112 69-154 1,1-Dichloropropene ug/kg 50 57.6 115 74-138 1,2,3-Trchlorobenzene ug/kg 50 54.3 109 71-150 1,2,3-Trichloropropane ug/kg 50 51.0 102 74-135 1,2,4-Trichlorobenzene ug/kg 50 56.6 113 68-150 1,2,4-Trimethylbenzene ug/kg 50 62.3 125 70-130 1,2-Dibromo-3-chloropropane ug/kg 50 59.4 119 65-146 1,2-Dibromoethane (EDB) ug/kg 50 53.6 107 77-136 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Page 40 of 44 aWnaljd cal www.pamlabs.ccm Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 LAt3UKAI URY GUNTROL SAMPLE: Parameter 399645 Spike Units Conc. LCS Result LCS % Rec % Rec Limits 1,2-Dichlorobenzene ug/kg 50 58.5 117 75-141 1,2-Dichloroethane ug/kg 50 58.5 117 74-134 1,2-Dichloropropane ug/kg 50 59.7 119 77-138 1,3,5-Trimethylbenzene ug/kg 50 61.2 122 65-128 1,3-Dichlorobenzene ug/kg 50 58.5 117 76-133 1,3-Dichloropropane ug/kg 50 56.5 113 79-132 1,4-Dichlorobenzene ug/kg 50 58.2 116 75-137 2,2-Dichloropropane ug/kg 50 65.1 130 73-137 2-Butanone (MEK) ug/kg 100 135 135 61-138 2-Chlorotoluene ug/kg 50 62.6 125 73-138 2-Hexanone ug/kg 100 135 135 58-159 4-Chlorotoluene ug/kg 50 63.8 128 75-136 4-Methyl-2-pentanone (MIBK) ug/kg 100 135 135 74-139 Acetone ug/kg 100 128 128 58-150 Benzene ug/kg 50 56.4 113 71-140 Bromobenzene ug/kg 50 63.4 127 72-144 Bromochloromethane ug/kg 50 56.2 112 78-133 Bromodichloromethane ug/kg 50 56.0 112 78-133 Bromoform ug/kg 50 50.1 100 74-132 Bromomethane ug/kg 50 37.9 76 63-184 Carbon tetrachloride ug/kg 50 61.0 122 73-143 Chlorobenzene ug/kg 50 55.2 110 77-137 Chloroethane ug/kg 50 46.1 92 68-146 Chloroform ug/kg 50 53.8 108 75-137 Chloromethane ug/kg 50 41.4 83 54-143 cis-1,2-Dichloroethene ug/kg 50 62.4 125 71-143 cis-1,3-Dichloropropene ug/kg 50 61.0 122 76-133 Dibromochloromethane ug/kg 50 51.3 103 77-131 Dibromomethane ug/kg 50 53.2 106 63-184 Dichlorodifluoromethane ug/kg 50 35.7 71 36-173 Diisopropyl ether ug/kg 50 62.2 124 68-144 Ethylbenzene ug/kg 50 55.8 112 69-141 Hexachloro-1,3-butadiene ug/kg 50 53.6 107 70-152 Isopropylbenzene (Cumene) ug/kg 50 55.4 111 77-143 m&p-Xylene ug/kg 100 112 112 72-138 Methyl-tert-butyl ether ug/kg 50 58.1 116 2-138 Methylene Chloride ug/kg 50 57.4 115 69-136 n-Butylbenzene ug/kg 50 62.5 125 65-128 n-Propylbenzene ug/kg 50 62.3 125 72-139 Naphthalene ug/kg 50 59.8 120 61-138 o-Xylene ug/kg 50 57.0 114 74-137 p-Isopropyltoluene ug/kg 50 61.2 122 66-128 sec-Butylbenzene ug/kg 50 59.0 118 72-140 Styrene ug/kg 50 57.2 114 76-137 tert-Butylbenzene ug/kg 50 60.3 121 68-141 Tetrachloroethene ug/kg 50 50.6 101 72-136 Toluene ug/kg 50 55.9 112 69-139 trans-1,2-Dichloroethene ug/kg 50 55.6 111 72-144 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. `~,~/(!r~y~~ ~ L1S.Igti.l Qualifiers Page 41 of 44 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 LABORATORY CONTROL SAMPLE: 399645 Parameter Units trans- 1, 3-Dichloropropene ug/kg Trichloroethene ug/kg Tdchlorofluoromethane ug/kg Vinyl acetate ug/kg Vinyl chloride ug/kg Xylene (Total) ug/kg 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromethane (S) % Toluene-d8 (S) % Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 50 61.5 123 73-135 50 54.0 108 75-136 50 41.5 83 69-144 100 153 153 50-150 LO 50 39.2 78 61-145 150 169 113 73-138 110 69-121 89 74-115 109 79-116 102 88-110 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 42 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ~jo~ Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 QC Batch: PMST/3008 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 9262746005, 9262746006, 9262746007 SAMPLE DUPLICATE: 399687 9262417001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 12.9 12.9 0 25 SAMPLE DUPLICATE: 399688 9262746007 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 24.5 24.9 2 25 Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 43 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ItEo aceAnalytical svwwo laftcom Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Former PE Valve/Sweeten Creek Pace Project No.: 9262746 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. U - Indicates the compound was analyzed for, but not detected. ANALYTE QUALIFIERS C9 Common Laboratory Contaminant. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. R1 RPD value was outside control limits. SO Surrogate recovery outside laboratory control limits. Z2 Analyte present in the associated method blank above the detection limit. Date: 02/18/2010 06:28 PM REPORT OF LABORATORY ANALYSIS Page 44 of 44 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. CHAIN-OF-CUSTODY / Analytical Request Document The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section c Invoice Information: Page : 1 Of 1 Attention: Trever Slack Section A_ Section B ~ C0C3 October 11, 2018 Mr. Peter Hall c/o Mr. Bill Burgin Reference: Soil and Groundwater Assessment Former P.E. Valve Property 1140 Sweeten Creek Road Asheville, Buncombe County, North Carolina ECS Project 49:7572 Dear Mr. Hall: ECS Southeast, LLP (ECS) is pleased to provide the results of our Soil and Groundwater Assessment for the above referenced property. ECS’ services were conducted in accordance with the services outlined in ECS Proposal 49:8953-P dated March 15, 2018 and authorized on August 13, 2018. ECS appreciates the opportunity to provide our services to you. If there are questions regarding this report, or a need for further information, please contact us. Respectfully submitted, ECS Southeast, LLP James C. Bevers, PE jbevers@ecslimited.com 828-785-4179 Matthew H. McDuffie, PG mmcduffie@ecslimited.com 704-378-9003 Former P.E. Valve Property Ashville, Buncombe County, North Carolina ECS Project No. 49:7572 October 11, 2018 2 TABLE OF CONTENTS 1. PROJECT INFORMATION ............................................................................................... 1 2. SCOPE OF SERVICES .................................................................................................... 2 3. RESULTS ......................................................................................................................... 4 4. CONCLUSIONS & RECOMMENDATIONS ...................................................................... 5 5. QUALIFICATIONS OF REPORT ...................................................................................... 6 FIGURES Figure 1 Site Topographic Map Figure 2 Soil Sample Location Map Figure 3 Groundwater Sample Location Map TABLES Table 1 – Summary of PID Readings Table 2 – Well Construction Data Table 3 - Summary of Soil Analytical Results Table 4 – Summary of Groundwater Analytical Results APPENDICIES Appendix A – Health and Safety Plan Appendix B – Photographic Log Appendix C – Boring Logs Appendix D – Analytical Results and Chain-of-Custodies Former P.E. Valve Property Ashville, Buncombe County, North Carolina ECS Project No. 49:7572 October 11, 2018 1 1. PROJECT INFORMATION The site is the former P.E. Valve Property located at 1140 Sweeten Creek Road in Ashville, Buncombe County, North Carolina, Figure 1. The property is approximately 1.63 acres in size and is currently vacant. A prior Limited Phase II Environmental Site Assessment (ESA) was completed at the subject property by Bunnell-Lammons Engineering, Inc. (BLE) dated March 8, 2010. According to the Limited Phase II ESA, BLE completed a Phase I ESA dated March 4, 2010 for the subject property. The Phase I ESA indicated that a 30,302 square foot industrial manufacturing building was developed on the subject property which was used for textile manufacturing. In 1968, the building was used as a valve manufacturing facility. During the completion of the Phase I ESA, the building was vacant. The Phase I ESA identified the following recognized environmental conditions (RECs) with respect to the subject site:  Rusted 55-gallon drums located on the southern side of the building, of which the historic contents are unknown;  an above ground storage tank (AST) located on the southern side of the building;  staining along the northern wall of the building;  a loading dock with floor drains;  two ASTs located on the interior of the building;  multiple 55-gallon drums and 5-gallon buckets of waste oil, waste coolant, and unidentified liquids inside the building;  heavy staining on the floor of the building; and  a network of floor drains located inside the building. As part of the scope associated with the scope of the Limited Phase II ESA, four borings were advanced for the purposes of collecting groundwater samples. The borings were located downgradient and west of the building (BL-1), downgradient and near the northwest corner of the subject property (BL-2), downgradient of an AST and near the southwest corner of the building (BL-3), and adjacent to the loading dock (BL-4). The borings were advanced with a Geoprobe drill rig to refusal, which was approximately 25 feet below the ground surface (bgs). Groundwater was identified at approximately 20 feet bgs. Four hand auger borings were advanced within the building for the purposes of collecting soil samples. The borings were located adjacent to 55-gallon drums, ASTs, and 5-gallon buckets (HAB-1), inside the machining room where heavy staining was observed (HAB-2), inside the paint room (HAB-3), and adjacent to a floor drain in the southern portion of the building (HAB-4). Trichloroethene (TCE) was identified at concentrations above the North Carolina 2L Groundwater Quality Standard (NC2LGWQS) in groundwater samples BL-2, BL-3, and BL-4. Chromium was identified at concentrations above the Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goal (PSRG) in soil samples HAB-1, HAB-2, and HAB-2. Selenium was identified at a concentration above the IHSB PSRG in soil sample HAB-4. According to Mr. William Clarke with Roberts & Stevens, P.A., the building is no longer present at the subject property. Former P.E. Valve Property Ashville, Buncombe County, North Carolina ECS Project No. 49:7572 October 11, 2018 2 Based on a potential real estate transaction and determine the current contamination at the site, ECS was contracted to conduct an assessment of the site. Project information is based on correspondence between Mr. Clarke with Roberts & Stevens, P.A. and Mr. Matthew Fogleman with ECS and the aforementioned Limited Phase II ESA. 2. SCOPE OF SERVICES 2.1 – Introduction to Scope of Work The Phase II ESA soil and groundwater assessment consisted of collecting soil and groundwater samples using a Geoprobe® drill rig equipped to drill with direct push drilling techniques. The subcontractor used for this project was Mountain Environmental Services (NC Well Contractor Certification Number: 4179-B). 2.2 – Public Utility Clearance Prior to commencing with field activities, ECS contacted North Carolina One Call (ULOCO) to locate/mark public utilities at the site. Required separation distances between subsurface activities and marked utilities (typically 30-inches) were maintained during the field activities. 2.3 – Health and Safety Plan As part of this assessment, ECS prepared a site-specific health and safety plan (HASP) for the site. The HASP documented the known or suspected hazards, applicable personal protective equipment (PPE) of site personnel, and emergency response procedures. Prior to commencing with field activities, ECS and its subcontractors and applicable site personnel reviewed the site- specific HASP. A copy of the HASP review confirmation sheet is included in Appendix A. 2.4 – Geoprobe® Drilling Services The Geoprobe® consists of a hydraulic jack mounted on an all-terrain vehicle (ATV). The Geoprobe® is capable of driving various forms of groundwater, soil, and soil-gas sampling probes into the ground to depths equivalent of auger refusal. Photographs of the sampling activities are provided in Appendix B. 2.5 – Geoprobe® Soil Borings A total of six soil borings were advanced at the site. The soil borings were located in the vicinity of a former floor drain in the former loading dock (S-1), in the vicinity of former floor drains in the former assembly room (S-2), in the former machining room (S-3), in the vicinity of the former waste oil and ASTs (S-4), in the vicinity of a former floor drain outside former tool room (S-5), and in the vicinity of the former AST located on the southern side of the former building. The soil borings were advanced to depths ranging from 5 and 8 feet below the ground surface (bgs). Each soil boring was advanced by hydraulically driving a four-foot long, 1.5-inch soil sampling probe into the soil. Prior to advancing each boring, the down hole equipment and Geoprobe® Former P.E. Valve Property Ashville, Buncombe County, North Carolina ECS Project No. 49:7572 October 11, 2018 3 drill rig were decontaminated utilizing a high pressure steam cleaner that utilized municipal water. The down hole equipment and drill rig were decontaminated to prevent cross- contamination between boring locations. The soil sampling probe is lined with a disposable clear plastic tube, which is replaced with each four-foot interval. After the probe is driven, the clear plastic tube filled with soil is removed from the probe. The clear plastic tube is then cut open to remove the soil. ECS visually classified the soils collected from each boring. Boring logs, which include descriptions of the soils encountered, were prepared for each boring and are included in Appendix C. Upon completion, each boring was properly abandoned. 2.6 – Photoionization Detector (PID) Each soil samples collected in the field were transferred into a new, clean resealable bag (half full), and the bag placed in a warm location. Approximately ten minutes after the time of collection, the bag was opened slightly and the probe of a Rae Systems Mini Rae 3000 photoionization detector (PID) was inserted, and the bag immediately resealed using finger pressure. The meter of the PID was monitored and the reading recorded. Elevated PID readings were not observed during the assessment. Due to the lack of elevated PID readings, the shallow sample (0 to 4 feet bgs) from each boring was selected for analysis. The recorded PID responses are presented on the boring logs in Appendix C and included in Table 1. 2.7 – Geoprobe® Groundwater Borings A total of four groundwater borings were advanced at the site. The groundwater borings were located in the vicinity of former floor drains in the former assembly room (GW-1), in the vicinity of the former waste oil and ASTs (GW-2), in the vicinity of a former AST located on the southern side of the former building (GW-3), and downgradient of the former building (GW-4). Each groundwater boring was advanced by hydraulically driving a four-foot long, 1.5-inch diameter probe into the soil to an approximate depth of five feet beneath the water table as estimated during drilling. Prior to advancing each boring, the down hole equipment and Geoprobe® drill rig were decontaminated utilizing a high pressure steam cleaner that utilized municipal water. 2.8 – Temporary Monitoring Well Installation Temporary monitoring wells were installed in each of the groundwater borings. The temporary monitoring wells were installed to depths ranging from 15 to 20 feet bgs. The temporary wells were constructed with one-inch I.D. Schedule 40 PVC flush-threaded casing and screen. The PVC screen and casing was lowered into the open borehole. A ten-foot length of slotted well screen with machined 0.010-inch slot widths and a threaded bottom plug were installed at the bottom of wells GW-1, GW-2, and GW-4. A five-foot length of slotted will screen was installed at the bottom of well GW-3. A solid section of PVC casing was placed above the screened interval and extended to a point just above the ground surface. A temporary monitoring well construction diagram was prepared for each temporary monitoring well, which are included on the boring logs in Appendix C and well construction data is provided on Table 2. Former P.E. Valve Property Ashville, Buncombe County, North Carolina ECS Project No. 49:7572 October 11, 2018 4 2.9 – Monitoring Well Development The temporary groundwater monitoring wells were developed by evacuating at least three well volumes or until dryness twice using a peristaltic pump and tubing dedicated to each well. The wells were developed to remove sand, silt, and other fine sediments that may have entered the wells during their construction. 2.10 – Groundwater from Monitoring Wells After development, groundwater samples were collected from the wells. The groundwater samples were collected using a peristaltic pump with a new section of plastic tubing lowered into the groundwater. The groundwater was pumped directly into the laboratory prepared containers. 2.11 – Sample Preparation and Submittal The soil and groundwater samples were placed into laboratory prepared containers. The sample containers were labeled with ECS project number, sample identification, sample date and time, and requested analytical analysis. The containers were placed into protective packaging material and placed into a cooler with ice to maintain the samples at approximately 4 Celsius (C). The samples were submitted to Prism Laboratories located in Charlotte, North Carolina (North Carolina Certification #402 for chemical analysis. The soil samples were submitted for analysis for volatile organic compounds (VOCs) using EPA Method 8260, semi- volatile organic compounds (SVOCs) using EPA Method 8270, total RCRA metals using EPA Method 6010, and hexavalent chromium using EPA Method 7196. The groundwater samples were submitted for analysis for VOCs using EPA Method 8260, SVOCs using EPA Method 8270, and total RCRA metals using EPA Method 6010. ECS maintained proper chain-of-custody (COC) procedures throughout the sample collection and transportation process. Copies of the COCs are included in Appendix D. 3. RESULTS 3.1 – Summary of Soil Sample Results Laboratory analysis of soil samples S-1, S-3, S-4, S-5, and S-6 detected arsenic at concentrations above the Residential Health Based Preliminary Soil Remediation Goal (PSRG) standard; however, the concentrations do not exceed the Industrial/Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard. Laboratory analysis of soil sample S-2 detected arsenic at a concentration (3.1 mg/kg) above the Industrial/Commercial Health Based PSRG standard; however, the concentrations do not exceed the Protection of Groundwater PSRG standard. According to the Elements in North American Soils (Second Edition), the mean concentration of arsenic in North Carolina is 4.8 mg/kg, which is above the concentrations identified in the samples. Laboratory analysis of soil samples S-1 through S-6 detected hexavalent chromium at concentrations above the Residential Health Based PSRG standard; however, the concentrations do not exceed the Industrial/Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard. Former P.E. Valve Property Ashville, Buncombe County, North Carolina ECS Project No. 49:7572 October 11, 2018 5 Laboratory analysis of soil samples S-1 through S-6 detected several VOCs, SVOCs, and other metals at concentrations above laboratory detection limits, but the concentrations do not exceed their respective PSRG standards. 3.2 – Summary of Groundwater Sample Results Laboratory analysis of groundwater sample GW-3 detected TCE at a concentration above its NC2LGWQS, Residential Vapor Intrusion Screening Level (VISL), and Non-Residential VISL. VOCs, SVOCs, and metals were detected at concentrations above laboratory detection limits; however, the concentrations do not exceed the NC2LGWQS. A summary of the laboratory analytical results is included in Tables 3 and 4. The laboratory data sheets are included in the Appendix. 4. CONCLUSIONS & RECOMMENDATIONS 4.1 – Conclusions Based on the results of the soil and groundwater assessment, ECS concludes the following:  Evidence of a release including petroleum or chemical odors, staining, sheens, or elevated readings on the PID was not identified at the locations sampled during assessment activities.  Groundwater was identified at depths ranging from 7 to 11 feet below the ground surface at the locations sampled during assessment activities.  Laboratory analysis of soil samples S-1, S-3, S-4, S-5, and S-6 detected arsenic at concentrations above the Residential Health Based PSRG standard; however, the concentrations do not exceed the Industrial/Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard. Laboratory analysis of soil sample S-2 detected arsenic at a concentration (3.1 mg/kg) above the Industrial/Commercial Health Based PSRG standard; however, the concentrations do not exceed the Protection of Groundwater PSRG standard. According to the Elements in North American Soils (Second Edition), the mean concentration of arsenic in North Carolina is 4.8 mg/kg, which is above the concentrations identified in the samples. Laboratory analysis of soil samples S-1 through S-6 detected hexavalent chromium at concentrations above the Residential Health Based PSRG standard; however, the concentrations do not exceed the Industrial/Commercial Health Based PSRG standard or the Protection of Groundwater PSRG standard.  Laboratory analysis of groundwater sample GW-3 detected TCE at a concentration above its NC2LGWQS, Residential VISL, and Non-Residential VISL.  TCE concentrations in groundwater have reduced when compared to the concentrations of TCE identified in an assessment conducted in March 2010. Former P.E. Valve Property Ashville, Buncombe County, North Carolina ECS Project No. 49:7572 October 11, 2018 6  The extent of impact to the site has not been fully delineated. Additional assessment would be necessary to fully delineate the extent of impact to the site. 4.2 – Recommendations Based on the results of the soil and groundwater assessment, ECS recommends the following:  Arsenic and hexavalent chromium were identified at concentrations exceeding the PSRG standards. Soil disturbed and/or removed from the property during future development activities may require management and/or proper disposal in accordance with applicable regulations.  TCE was identified at a concentration exceeding the NC2LGWQS as well as the Residential and Non-Residential VISLs in one groundwater sample. A soil gas assessment is recommended to evaluate vapor intrusion concerns prior to development of the property.  ECS recommends that you (as the property owner) seek legal counsel regarding your reporting obligation.  Prior to the acquisition of the property, ECS recommends that the proposed buyer consult legal counsel. The site appears to be a candidate for eligibility into the North Carolina Brownfields Program. 5. QUALIFICATIONS OF REPORT The activities and evaluative approaches used in this assessment are consistent with those normally employed in soil and groundwater assessment projects of this type. Our evaluation of site conditions has been based on our understanding of the site project information and the data obtained during our field activities. This report was prepared for the express use of the Client. Use of this report by other individuals or companies implies their acceptance of the General Conditions of Service of the original contract. FIGURES FIGURE 1 SITE TOPOGRAPHIC MAP FORMER PE VALVE 1140 SWEETEN CREEK ROAD ASHEVILLE, BUNCOMBE COUNTY, NORTH CAROLINA ECS PROJECT NO. 49-7572 SOURCE: USGS TOPOGRAPHIC MAP ASHEVILLE, NORTH CAROLINA QUADRANGLE DATED 1961, PHOTOREVISED 1991 SITE FIGURE 2 SOIL SAMPLE LOCATION MAP FORMER PE VALVE FACILITY 1140 SWEETEN CREEK ROAD ASHEVILLE, BUNCOMBE COUNTY, NORTH CAROLINA ECS PROJECT NO. 49-7572 SOURCE: GOOGLE EARTH, DATED 2015 SCALE: PROPOSED SOIL SAMPLE LOCATION BOLD exceeds Residential Use Health Based PSRG UNDERLINE exceeds Industrial/Commercial Health Based PSRG Concentrations in mg/kgAPPROXIMATE SITE BOUNDARY LEGEND = 100 FEET S-6 Arsenic 2.5 Hexavalent Chromium 1.1 S-5 Arsenic 2.9 Hexavalent Chromium 0.86 S-4 Arsenic 2.7 Hexavalent Chromium 0.31J S-3 Arsenic 2.5 Hexavalent Chromium 0.62 S-1 Arsenic 2.3 Hexavalent Chromium 0.62 S-2 Arsenic 3.1 Hexavalent Chromium 0.67 FIGURE 3 GROUNDWATER SAMPLE LOCATION MAP FORMER PE VALVE FACILITY 1140 SWEETEN CREEK ROAD ASHEVILLE, BUNCOMBE COUNTY, NORTH CAROLINA ECS PROJECT NO. 49-7572 SOURCE: GOOGLE EARTH, DATED 2015 SCALE: PROPOSED GROUNDWATER SAMPLE LOCATION BOLD exceeds NC2LGWQS Concentrations in ug/L APPROXIMATE SITE BOUNDARY LEGEND = 100 FEET GW-3 TCE 16.9 GW-1 GW-2 GW-4 TABLES Sample ID Sample Depth (ft bgs) PID Reading (ppm) 0-2 0.0 2-4 0.0 4-5 0.0 5-6 0.0 0-2 0.0 2-4 0.0 4-5 0.0 5-6 0.0 0-4 0.0 4-5 0.0 5-6 0.0 0-2 0.0 2-4 0.0 4-6 0.0 6-8 0.0 0-2 0.0 2-4 0.0 4-6 0.0 6-8 0.0 0-2 0.0 2-4 0.0 4-5 0.0 PID = photoionization detector ppm = parts per million ft bgs = feet below the ground surface Readings taken on September 4, 2018 BOLD = Sample submitted for analysis Table 1 Summary of PID Readings Former P.E. Valve Property 1140 Sweeten Creek Road Asheville, Buncombe County, North Carolina ECS Project 49-7572 S-5 S-4 S-3 S-2 S-6 S-1 Well ID Installation Date Well Diameter (in) Total Depth (ft BTOC) Screen Interval (ft BTOC) Depth to Groundwater (ft BTOC) GW-1 9/4/2018 2 20 10-20 9 GW-2 9/4/2018 2 20 10-20 7 GW-3 9/4/2018 2 15 10-15 11 GW-4 9/4/2018 2 20 10-20 11 BTOC = Below top of casing ft = feet in = inches Table 2 Well Construction Data Former P.E. Valve Property 1140 Sweeten Creek Road Asheville, Buncombe County, North Carolina ECS Project 49-7572 Parameter Sample ID S-1 S-2 S-3 S-4 S-5 S-6 Sample Depth (ft bgs)0-2 0-2 0-4 0-2 0-2 0-2 Sample Date VOCs using EPA Method 8260 (mg/kg) Acetone 0.057 J*0.090 0.12 0.054 0.11 0.14 12,000 140,000 25 Bromomethane BRL BRL 0.0028 J*BRL BRL BRL 1.4 6.4 0.05 Toluene BRL BRL 0.011 BRL BRL BRL 990 9700 8.3 1,1,1-Trichloroethane BRL BRL BRL 0.0047 J*BRL BRL 1,700 7,600 1.4 Trichloroethylene 0.0060 BRL BRL 0.010 0.012 BRL 0.87 4.0 0.021 Trichlorofluoromethane 0.036 BRL BRL BRL BRL BRL 4,700 70,000 25 All other VOCs BRL BRL BRL BRL BRL BRL ------ SVOCs using EPA Method 8270 (mg/kg) 1-Methylnaphthalene BRL BRL BRL 0.19 J*BRL BRL 18 73 0.11 2-Methylnaphthalene BRL BRL BRL 0.24 J*0.13 J*BRL 48 600 3.1 Naphthalene BRL BRL BRL 0.18 J*BRL BRL 4.1 18 0.39 Phenanthrene BRL BRL BRL 0.11 J*BRL BRL NS NS 134 All other SVOCs BRL BRL BRL BRL BRL BRL ------ RCRA Metals using EPA Method 6010 (mg/kg) Arsenic 2.3 3.1 2.5 2.7 2.9 2.5 0.68 3.0 5.8 Barium 180 130 120 160 190 100 3,100 47,000 580 Cadmium 0.032 J*0.047 J*0.72 0.087 J*BRL 0.061 J*14 200 3.0 Chromium 30 31 41 13 28 28 23,000 350,000 360,000 Lead 14 18 18 16 15 16 400 800 270 Selenium BRL 0.32 J*0.48 J*1.0 0.40 J*0.72 78 1,200 2.1 Silver BRL BRL 0.56 BRL BRL BRL 78 1,200 3.4 Mercury using EPA Method 7471 (mg/kg) Mercury 0.082 0.031 0.049 0.017 J*0.018 J*0.097 2.3 9.7 1.0 Hexavalent Chromium using EPA Method 7168 (mg/kg) Hexavalent Chromium 0.62 0.67 0.62 0.31 J*0.86 1.1 0.31 6.5 3.8 ft bgs = feet below the ground surface PSRG = Preliminary Soil Remediation Goals mg/kg = Milligrams/kilogram VOCs = volatile organic compounds BOLD = Exceeds Unrestricted Use Health Based PSRG underline = Exceeds Industrial/Commercial Health Based PSRG italicized = Exceeds Protection of Groundwater PSRG J* = Detected but below the Reporting Limit; therefore, result is an estimated concentration NS = No Standard Asheville, Buncombe County, North Carolina Table 3 Summary of Soil Analytical Results Former P.E. Valve Property 1140 Sweeten Creek Road ECS Project 49-7572 Residential Health Based PSRG (mg/kg) Analytical Results 9/4/18 Industrial/ Commercial Health Based PSRG (mg/kg) Protection of Groundwater PSRG (mg/kg) Parameter Sample ID GW-1 GW-2 GW-3 GW-4 Sample Date Residential Non-Residential VOCs using EPA Method 8260 (µg/L) Acetone 13.3 BRL 5.93 BRL 6,000 4,500,000 19,000,000 Carbon disulfide 0.602 J*BRL BRL BRL 700 250 1,000 Chloromethane 0.972 J*0.793 J*1.59 J*0.921 J*3 52 220 cis-1,2-Dichloroethene BRL BRL 2.71 J*BRL 70 NS NS Trichloroethene BRL BRL 16.9 BRL 3 1 4.4 All VOCs BRL BRL BRL BRL ------ SVOCs using EPA Method 8270 (mg/kg) Benzoic Acid 630 BRL BRL BRL 30,000 NS NS Diethyl phthalate BRL BRL 8.1 J*BRL 6,000 NS NS All other SVOCs BRL BRL BRL BRL ------ RCRA Metals plus Manganese using EPA Method 6010 (µg/L) Arsenic BRL 0.013 J*0.070 0.011 J*10 NS NS Barium 0.24 1.1 6.9 0.92 700 NS NS Cadmium BRL 0.00022 J*BRL BRL 2 NS NS Chromium 0.0073 0.082 0.57 0.050 10 NS NS Lead 0.0049 J*0.058 0.22 0.031 15 NS NS All other metals BRL BRL BRL BRL ------ Mercury using EPA Method 7470 (µg/L) Mercury BRL BRL 0.00037 BRL 1 0.18 0.75 NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013 VOCs = Volatile Organic Compounds SVOCs = Semivolatile Organic CompoundsBOLD = Above NC2LGWQS underline = exceeds Residential Vapor Intrusion Screening Level Shaded = exceeds Non-Residential Vapor Intrusion Screening Level µg/L = Micrograms/LiterBRL = Below Reporting Limit J* = Detected but below the Reporting Limit; therefore, result is an estimated concentration 9/4/18 Analytical Results NC2LGWQS (µg/L) Vapor Intrusion Screening Levels Table 4 Summary of Groundwater Analytical Results Former P.E. Valve Property 1140 Sweeten Creek Road Asheville, Buncombe County, North Carolina ECS Project 49-7572 APPENDIX A APPENDIX B PHOTOGRAPH LOG FORMER P.E. VALVE ASHEVILLE, BUNCOMBE COUNTY, NORTH CAROLINA Photo 1: View of the Geoprobe drill rig. Photo 2: View of temporary well GW-1. PHOTOGRAPH LOG FORMER P.E. VALVE ASHEVILLE, BUNCOMBE COUNTY, NORTH CAROLINA Photo 3: View of temporary well GW-2. Photo 4: View of temporary well GW-3. PHOTOGRAPH LOG FORMER P.E. VALVE ASHEVILLE, BUNCOMBE COUNTY, NORTH CAROLINA Photo 5: View of temporary well GW-4. APPENDIX C 2127 2124 2121 2118 2115 2112 2109 0 3 6 9 12 15 18 21 0.0 0.0 0.0 0.0 S-1 Gravel CH CH-MH Gravel Tan clay Tan orange clayey silt End of boring PROJECT:Former PE Valve BORING NUM.S-1 CLIENT:Peter Hall PROJECT NO.49-7572 LOCATION: Former Loading Dock ELEVATION: 2,128 feet msl DRILLER: Mountain Environmental DATE DRILLED: 9/4/2018 LOGGED BY: JCB DRILL RIG: Geoprobe DEPTH TO WATER: Elevation/ Depth (Ft)PIDReadingSampleNumberSampleRecovery(in/in)Graphic LogSoilClassificationSOIL DESCRIPTION This information pertains only to this boring and should not beinterpreted as being indicative of the site.Page 1 of 1 2127 2124 2121 2118 2115 2112 2109 0 3 6 9 12 15 18 21 0.0 0.0 0.0 0.0 S-2 Gravel CH MH/SM Gravel Tan orange clay Tan silty sand End of boring PROJECT:Former PE Valve BORING NO.S-2/GW-1 CLIENT:Peter Hall PROJECT NO.49-7572 LOCATION: Assembly Room ELEVATION: 2,128 feet msl DRILLER: Mountain Environmental DATE DRILLED: 9/4/2018 LOGGED BY: JCB DRILL RIG: Geoprobe DEPTH TO WATER: 9 Elevation/ Depth (Ft)PIDReadingSampleNumberSampleRecovery(in/in)Graphic LogSoilClassificationSOIL DESCRIPTION WELL CONSTRUCTION This information pertains only to this boring and should not be interpreted as being indicative of the site.Figure Page 1 of 1 2127 2124 2121 2118 2115 2112 2109 0 3 6 9 12 15 18 21 0.0 0.0 0.0 S-3 Gravel CH CH-MH Gravel Brown clay Tan silty clay End of boring PROJECT:Former PE Valve BORING NUM.S-3 CLIENT:Peter Hall PROJECT NO.49-7572 LOCATION: Machining Room ELEVATION: 2,129 feet msl DRILLER: Mountain Environmental DATE DRILLED: 9/4/2018 LOGGED BY: JCB DRILL RIG: Geoprobe DEPTH TO WATER: Elevation/ Depth (Ft)PIDReadingSampleNumberSampleRecovery(in/in)Graphic LogSoilClassificationSOIL DESCRIPTION This information pertains only to this boring and should not beinterpreted as being indicative of the site.Page 1 of 1 2130 2127 2124 2121 2118 2115 2112 2109 0 3 6 9 12 15 18 21 0.0 0.0 0.0 0.0 S-4 Gravel SC CH-MH Gravel Brown sandy clay Tan silty clay End of boring PROJECT:Former PE Valve BORING NO.S-4/GW-2 CLIENT:Peter Hall PROJECT NO.49-7572 LOCATION: Near Bay Door ELEVATION: 2,130 feet msl DRILLER: Mountain Environmental DATE DRILLED: 9/4/2018 LOGGED BY: JCB DRILL RIG: Geoprobe DEPTH TO WATER: Elevation/ Depth (Ft)PIDReadingSampleNumberSampleRecovery(in/in)Graphic LogSoilClassificationSOIL DESCRIPTION WELL CONSTRUCTION This information pertains only to this boring and should not be interpreted as being indicative of the site.Figure Page 1 of 1 2127 2124 2121 2118 2115 2112 2109 0 3 6 9 12 15 18 21 0.0 0.0 0.0 0.0 S-5 Gravel CH CH-MH Gravel Tan orange clay Tan silty clay End of boring PROJECT:Former PE Valve BORING NUM.S-5 CLIENT:Peter Hall PROJECT NO.49-7572 LOCATION: Adjacent to Tool Room ELEVATION: 2,129 feet msl DRILLER: Mountain Environmental DATE DRILLED: 9/4/2018 LOGGED BY: JCB DRILL RIG: Geoprobe DEPTH TO WATER: Elevation/ Depth (Ft)PIDReadingSampleNumberSampleRecovery(in/in)Graphic LogSoilClassificationSOIL DESCRIPTION This information pertains only to this boring and should not beinterpreted as being indicative of the site.Page 1 of 1 2127 2124 2121 2118 2115 2112 2109 0 3 6 9 12 15 18 21 0.0 0.0 0.0 S-6 Gravel CH Gravel Brown clay End of boring PROJECT:Former PE Valve BORING NO.S-6/GW-3 CLIENT:Peter Hall PROJECT NO.49-7572 LOCATION: AST ELEVATION: 2,128 feet msl DRILLER: Mountain Environmental DATE DRILLED: 9/4/2018 LOGGED BY: JCB DRILL RIG: Geoprobe DEPTH TO WATER: Elevation/ Depth (Ft)PIDReadingSampleNumberSampleRecovery(in/in)Graphic LogSoilClassificationSOIL DESCRIPTION WELL CONSTRUCTION This information pertains only to this boring and should not be interpreted as being indicative of the site.Figure Page 1 of 1 APPENDIX D This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Case Narrative 09/20/2018 ECS Carolinas, LLP (Asheville) James Bevers 1900 Hendersonville Road, Suite 10 Asheville, NC 28803 Project: PE Valve Lab Submittal Date: 09/06/2018 Prism Work Order: 8090062 Method 8260 water analysis was subcontracted to GCAL. Laboratory report is attached. Narrative Notes: Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. VP Laboratory Services Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash President/Project Manager This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 95 Data Qualifiers Key Reference: A CCV result is below range. Analyte is not detected in sample. No further action taken. Aa The CCV result is below the established QC limits. This compound was not detected in the sample down to the MDL. No further action was taken. D RPD value outside of the control limits. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken. M Matrix spike outside of the control limits. PS Post Spike recovery is outside of the control limits. SE Surrogate recovery outside the QC limits due to emulsion. SR Surrogate recovery outside the QC limits. Method Detection LimitMDL Below Reporting LimitBRL Relative Percent DifferenceRPD *Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 95 Sample Receipt Summary 09/20/2018 Prism Work Order: 8090062 Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received 8090062-01 09/04/18 9:45S-1 09/06/18 8:30Solid 8090062-02 09/04/18 10:00S-2 09/06/18 8:30Solid 8090062-03 09/04/18 10:15S-3 09/06/18 8:30Solid 8090062-04 09/04/18 10:45S-4 09/06/18 8:30Solid 8090062-05 09/04/18 11:00S-5 09/06/18 8:30Solid 8090062-06 09/04/18 11:15S-6 09/06/18 8:30Solid 8090062-07 09/04/18 18:45GW-1 09/06/18 8:30Water 8090062-08 09/04/18 17:30GW-2 09/06/18 8:30Water 8090062-09 09/04/18 16:00GW-3 09/06/18 8:30Water 8090062-10 09/04/18 17:30GW-4 09/06/18 8:30Water 8090062-11 09/04/18 0:00Trip Blank 09/06/18 8:30Water Samples were received in good condition at 5.1 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-01 Prism Work Order: 8090062 Time Collected: 09/04/18 09:45 Time Submitted: 09/06/18 08:30 S-1 General Chemistry Parameters 84.0 SM2540 G P8I014010.100 9/11/18 8:00 SLS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0611,2,4-Trichlorobenzene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0601,2-Dichlorobenzene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0551,3-Dichlorobenzene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0571,4-Dichlorobenzene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0761-Methylnaphthalene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0742,4,6-Trichlorophenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0762,4-Dichlorophenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0602,4-Dimethylphenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0552,4-Dinitrophenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0482,4-Dinitrotoluene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0522,6-Dinitrotoluene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0572-Chloronaphthalene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0562-Chlorophenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0632-Methylnaphthalene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0502-Methylphenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0712-Nitrophenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0773,3’-Dichlorobenzidine BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0483/4-Methylphenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0594,6-Dinitro-2-methylphenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0674-Bromophenyl phenyl ether BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0554-Chloro-3-methylphenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0474-Chloroaniline BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.0604-Nitrophenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.053Acenaphthene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.057Acenaphthylene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.063Anthracene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.052Azobenzene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.051Benzo(a)anthracene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.042Benzo(a)pyrene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.046Benzo(b)fluoranthene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.043Benzo(g,h,i)perylene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.051Benzo(k)fluoranthene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.033Benzoic Acid BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.052Benzyl alcohol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.068bis(2-Chloroethoxy)methane BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.055Bis(2-Chloroethyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-01 Prism Work Order: 8090062 Time Collected: 09/04/18 09:45 Time Submitted: 09/06/18 08:30 S-1 BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.067Bis(2-chloroisopropyl)ether BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.058Bis(2-Ethylhexyl)phthalate BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.056Butyl benzyl phthalate BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.049Chrysene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.060Dibenzofuran BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.054Diethyl phthalate BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.052Dimethyl phthalate BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.056Di-n-butyl phthalate BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.048Di-n-octyl phthalate BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.050Fluoranthene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.056Fluorene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.062Hexachlorobenzene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.070Hexachlorobutadiene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.070Hexachlorocyclopentadiene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.066Hexachloroethane BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.053Isophorone BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.063Naphthalene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.056Nitrobenzene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.062N-Nitroso-di-n-propylamine BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.060N-Nitrosodiphenylamine BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.046Pentachlorophenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.051Phenanthrene BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.058Phenol BRL 8270D P8I012110.39 9/11/18 17:47 JMVmg/kg dry 0.052Pyrene Surrogate Recovery Control Limits 39-13255 %2,4,6-Tribromophenol 44-11585 %2-Fluorobiphenyl 35-11580 %2-Fluorophenol 37-12274 %Nitrobenzene-d5 34-12177 %Phenol-d5 54-12776 %Terphenyl-d14 Total Metals 0.62 7196A P8I014410.48 9/11/18 15:30 BMSmg/kg dry 0.11Hexavalent Chromium 0.082 7471B P8I006310.024 9/7/18 11:20 MMRmg/kg dry 0.0023Mercury 2.3 6010D P8I006410.60 9/7/18 14:57 JABmg/kg dry 0.036Arsenic 180 6010D P8I006453.0 9/11/18 12:18 JABmg/kg dry 0.43Barium 0.032 6010D P8I006410.30 9/7/18 14:57 JABJmg/kg dry 0.0080Cadmium 30 6010D P8I006410.30 9/7/18 14:57 JABmg/kg dry 0.050Chromium 14 6010D P8I006410.30 9/7/18 14:57 JABmg/kg dry 0.055Lead This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-01 Prism Work Order: 8090062 Time Collected: 09/04/18 09:45 Time Submitted: 09/06/18 08:30 S-1 BRL 6010D P8I006410.60 9/7/18 14:57 JABmg/kg dry 0.14Selenium BRL 6010D P8I006410.30 9/7/18 14:57 JABmg/kg dry 0.0074Silver Volatile Organic Compounds by GC/MS BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000491,1,1,2-Tetrachloroethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000291,1,1-Trichloroethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000401,1,2,2-Tetrachloroethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000531,1,2-Trichloroethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000161,1-Dichloroethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000261,1-Dichloroethylene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000331,1-Dichloropropylene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000341,2,3-Trichlorobenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000761,2,3-Trichloropropane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000441,2,4-Trichlorobenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000451,2,4-Trimethylbenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000241,2-Dibromoethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000281,2-Dichlorobenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000351,2-Dichloroethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000371,2-Dichloropropane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000451,3,5-Trimethylbenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000391,3-Dichlorobenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000301,3-Dichloropropane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000231,4-Dichlorobenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000282,2-Dichloropropane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000312-Chlorotoluene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000354-Chlorotoluene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.000294-Isopropyltoluene 0.057 8260B P8I010610.059 9/10/18 15:06 ANGJmg/kg dry 0.0014Acetone BRL 8260B P8I010610.0036 9/10/18 15:06 ANGmg/kg dry 0.00035Benzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00049Bromobenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00033Bromochloromethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00033Bromodichloromethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00067Bromoform BRL 8260B P8I010610.012 9/10/18 15:06 ANGmg/kg dry 0.00073Bromomethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00030Carbon Tetrachloride BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00031Chlorobenzene BRL 8260B P8I010610.012 9/10/18 15:06 ANGmg/kg dry 0.00049Chloroethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00043Chloroform BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00040Chloromethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00025cis-1,2-Dichloroethylene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00024Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-01 Prism Work Order: 8090062 Time Collected: 09/04/18 09:45 Time Submitted: 09/06/18 08:30 S-1 BRL 8260B P8I010610.0059 9/10/18 15:06 ANGAamg/kg dry 0.00027Dichlorodifluoromethane BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00023Ethylbenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00024Isopropyl Ether BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00035Isopropylbenzene (Cumene) BRL 8260B P8I010610.012 9/10/18 15:06 ANGmg/kg dry 0.00055m,p-Xylenes BRL 8260B P8I010610.059 9/10/18 15:06 ANGmg/kg dry 0.00054Methyl Butyl Ketone (2-Hexanone) BRL 8260B P8I010610.12 9/10/18 15:06 ANGmg/kg dry 0.00054Methyl Ethyl Ketone (2-Butanone) BRL 8260B P8I010610.059 9/10/18 15:06 ANGmg/kg dry 0.00051Methyl Isobutyl Ketone BRL 8260B P8I010610.012 9/10/18 15:06 ANGmg/kg dry 0.00033Methylene Chloride BRL 8260B P8I010610.012 9/10/18 15:06 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether BRL 8260B P8I010610.012 9/10/18 15:06 ANGmg/kg dry 0.00019Naphthalene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00030n-Butylbenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00035n-Propylbenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00024o-Xylene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00029sec-Butylbenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00036Styrene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00020tert-Butylbenzene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00028Tetrachloroethylene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00034Toluene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00035trans-1,2-Dichloroethylene BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00031trans-1,3-Dichloropropylene 0.0060 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00038Trichloroethylene 0.036 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00038Trichlorofluoromethane BRL 8260B P8I010610.030 9/10/18 15:06 ANGmg/kg dry 0.00081Vinyl acetate BRL 8260B P8I010610.0059 9/10/18 15:06 ANGmg/kg dry 0.00029Vinyl chloride BRL 8260B P8I010610.018 9/10/18 15:06 ANGmg/kg dry 0.0011Xylenes, total Surrogate Recovery Control Limits 70-13098 %4-Bromofluorobenzene 84-123107 %Dibromofluoromethane 76-12989 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-02 Prism Work Order: 8090062 Time Collected: 09/04/18 10:00 Time Submitted: 09/06/18 08:30 S-2 General Chemistry Parameters 78.2 SM2540 G P8I014010.100 9/11/18 8:00 SLS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0661,2,4-Trichlorobenzene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0641,2-Dichlorobenzene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0591,3-Dichlorobenzene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0621,4-Dichlorobenzene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0811-Methylnaphthalene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0792,4,6-Trichlorophenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0812,4-Dichlorophenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0652,4-Dimethylphenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0592,4-Dinitrophenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0512,4-Dinitrotoluene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0562,6-Dinitrotoluene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0612-Chloronaphthalene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0602-Chlorophenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0672-Methylnaphthalene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0542-Methylphenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0772-Nitrophenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0833,3’-Dichlorobenzidine BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0523/4-Methylphenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0634,6-Dinitro-2-methylphenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0724-Bromophenyl phenyl ether BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0594-Chloro-3-methylphenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0514-Chloroaniline BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0554-Chlorophenyl phenyl ether BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.0654-Nitrophenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.057Acenaphthene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.061Acenaphthylene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.068Anthracene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.056Azobenzene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.055Benzo(a)anthracene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.046Benzo(a)pyrene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.049Benzo(b)fluoranthene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.046Benzo(g,h,i)perylene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.055Benzo(k)fluoranthene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.035Benzoic Acid BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.056Benzyl alcohol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.073bis(2-Chloroethoxy)methane BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.059Bis(2-Chloroethyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-02 Prism Work Order: 8090062 Time Collected: 09/04/18 10:00 Time Submitted: 09/06/18 08:30 S-2 BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.060Butyl benzyl phthalate BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.053Chrysene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.064Dibenzofuran BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.058Diethyl phthalate BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.056Dimethyl phthalate BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.060Di-n-butyl phthalate BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.052Di-n-octyl phthalate BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.054Fluoranthene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.060Fluorene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.067Hexachlorobenzene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.076Hexachlorobutadiene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.075Hexachlorocyclopentadiene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.071Hexachloroethane BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.048Indeno(1,2,3-cd)pyrene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.057Isophorone BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.068Naphthalene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.060Nitrobenzene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.066N-Nitroso-di-n-propylamine BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.064N-Nitrosodiphenylamine BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.050Pentachlorophenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.055Phenanthrene BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.062Phenol BRL 8270D P8I012110.42 9/11/18 18:09 JMVmg/kg dry 0.056Pyrene Surrogate Recovery Control Limits 39-13283 %2,4,6-Tribromophenol 44-11578 %2-Fluorobiphenyl 35-11580 %2-Fluorophenol 37-12268 %Nitrobenzene-d5 34-12177 %Phenol-d5 54-12776 %Terphenyl-d14 Total Metals 0.67 7196A P8I014410.51 9/11/18 15:30 BMSmg/kg dry 0.11Hexavalent Chromium 0.031 7471B P8I006310.025 9/7/18 11:34 MMRmg/kg dry 0.0024Mercury 3.1 6010D P8I006410.64 9/7/18 15:26 JABmg/kg dry 0.039Arsenic 130 6010D P8I006410.64 9/7/18 15:26 JABmg/kg dry 0.093Barium 0.047 6010D P8I006410.32 9/7/18 15:26 JABJmg/kg dry 0.0086Cadmium 31 6010D P8I006410.32 9/7/18 15:26 JABmg/kg dry 0.053Chromium 18 6010D P8I006410.32 9/7/18 15:26 JABmg/kg dry 0.059Lead This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-02 Prism Work Order: 8090062 Time Collected: 09/04/18 10:00 Time Submitted: 09/06/18 08:30 S-2 0.32 6010D P8I006410.64 9/7/18 15:26 JABJmg/kg dry 0.15Selenium BRL 6010D P8I006410.32 9/7/18 15:26 JABmg/kg dry 0.0079Silver Volatile Organic Compounds by GC/MS BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000431,1,1,2-Tetrachloroethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000261,1,1-Trichloroethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000361,1,2,2-Tetrachloroethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000471,1,2-Trichloroethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000151,1-Dichloroethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000231,1-Dichloroethylene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000291,1-Dichloropropylene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000301,2,3-Trichlorobenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000671,2,3-Trichloropropane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000391,2,4-Trichlorobenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000401,2,4-Trimethylbenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000211,2-Dibromoethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000251,2-Dichlorobenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000311,2-Dichloroethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000331,2-Dichloropropane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000401,3,5-Trimethylbenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000351,3-Dichlorobenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000271,3-Dichloropropane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000211,4-Dichlorobenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000252,2-Dichloropropane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000272-Chlorotoluene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000314-Chlorotoluene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.000254-Isopropyltoluene 0.090 8260B P8I010610.053 9/10/18 15:34 ANGmg/kg dry 0.0013Acetone BRL 8260B P8I010610.0032 9/10/18 15:34 ANGmg/kg dry 0.00031Benzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00044Bromobenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00029Bromochloromethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00029Bromodichloromethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00060Bromoform BRL 8260B P8I010610.011 9/10/18 15:34 ANGmg/kg dry 0.00065Bromomethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00026Carbon Tetrachloride BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00028Chlorobenzene BRL 8260B P8I010610.011 9/10/18 15:34 ANGmg/kg dry 0.00044Chloroethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00038Chloroform BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00036Chloromethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00023cis-1,2-Dichloroethylene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00018cis-1,3-Dichloropropylene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00022Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-02 Prism Work Order: 8090062 Time Collected: 09/04/18 10:00 Time Submitted: 09/06/18 08:30 S-2 BRL 8260B P8I010610.0053 9/10/18 15:34 ANGAamg/kg dry 0.00024Dichlorodifluoromethane BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00020Ethylbenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00022Isopropyl Ether BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00031Isopropylbenzene (Cumene) BRL 8260B P8I010610.011 9/10/18 15:34 ANGmg/kg dry 0.00049m,p-Xylenes BRL 8260B P8I010610.053 9/10/18 15:34 ANGmg/kg dry 0.00048Methyl Butyl Ketone (2-Hexanone) BRL 8260B P8I010610.11 9/10/18 15:34 ANGmg/kg dry 0.00048Methyl Ethyl Ketone (2-Butanone) BRL 8260B P8I010610.053 9/10/18 15:34 ANGmg/kg dry 0.00045Methyl Isobutyl Ketone BRL 8260B P8I010610.011 9/10/18 15:34 ANGmg/kg dry 0.00030Methylene Chloride BRL 8260B P8I010610.011 9/10/18 15:34 ANGmg/kg dry 0.00017Methyl-tert-Butyl Ether BRL 8260B P8I010610.011 9/10/18 15:34 ANGmg/kg dry 0.00017Naphthalene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00027n-Butylbenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00031n-Propylbenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00022o-Xylene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00026sec-Butylbenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00032Styrene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00018tert-Butylbenzene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00025Tetrachloroethylene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00030Toluene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00032trans-1,2-Dichloroethylene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00028trans-1,3-Dichloropropylene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00034Trichloroethylene BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00034Trichlorofluoromethane BRL 8260B P8I010610.026 9/10/18 15:34 ANGmg/kg dry 0.00072Vinyl acetate BRL 8260B P8I010610.0053 9/10/18 15:34 ANGmg/kg dry 0.00026Vinyl chloride BRL 8260B P8I010610.016 9/10/18 15:34 ANGmg/kg dry 0.00099Xylenes, total Surrogate Recovery Control Limits 70-13097 %4-Bromofluorobenzene 84-123105 %Dibromofluoromethane 76-12989 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-03 Prism Work Order: 8090062 Time Collected: 09/04/18 10:15 Time Submitted: 09/06/18 08:30 S-3 General Chemistry Parameters 82.6 SM2540 G P8I014010.100 9/11/18 8:00 SLS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0621,2,4-Trichlorobenzene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0601,2-Dichlorobenzene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0561,3-Dichlorobenzene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0581,4-Dichlorobenzene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0771-Methylnaphthalene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0752,4,6-Trichlorophenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0772,4-Dichlorophenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0612,4-Dimethylphenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0562,4-Dinitrophenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0482,4-Dinitrotoluene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0532,6-Dinitrotoluene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0582-Chloronaphthalene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0572-Chlorophenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0642-Methylnaphthalene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0512-Methylphenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0732-Nitrophenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0793,3’-Dichlorobenzidine BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0493/4-Methylphenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0604,6-Dinitro-2-methylphenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0684-Bromophenyl phenyl ether BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0564-Chloro-3-methylphenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0484-Chloroaniline BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.0614-Nitrophenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.054Acenaphthene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.058Acenaphthylene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.064Anthracene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.053Azobenzene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.052Benzo(a)anthracene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.043Benzo(a)pyrene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.046Benzo(b)fluoranthene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.044Benzo(g,h,i)perylene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.052Benzo(k)fluoranthene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.034Benzoic Acid BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.053Benzyl alcohol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.069bis(2-Chloroethoxy)methane BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.056Bis(2-Chloroethyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-03 Prism Work Order: 8090062 Time Collected: 09/04/18 10:15 Time Submitted: 09/06/18 08:30 S-3 BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.068Bis(2-chloroisopropyl)ether BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.059Bis(2-Ethylhexyl)phthalate BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.057Butyl benzyl phthalate BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.050Chrysene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.061Dibenzofuran BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.055Diethyl phthalate BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.053Dimethyl phthalate BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.057Di-n-butyl phthalate BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.049Di-n-octyl phthalate BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.051Fluoranthene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.057Fluorene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.063Hexachlorobenzene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.072Hexachlorobutadiene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.071Hexachlorocyclopentadiene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.067Hexachloroethane BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.054Isophorone BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.064Naphthalene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.057Nitrobenzene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.061N-Nitrosodiphenylamine BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.047Pentachlorophenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.052Phenanthrene BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.059Phenol BRL 8270D P8I012110.40 9/11/18 18:31 JMVmg/kg dry 0.053Pyrene Surrogate Recovery Control Limits 39-13270 %2,4,6-Tribromophenol 44-11590 %2-Fluorobiphenyl 35-11591 %2-Fluorophenol 37-12280 %Nitrobenzene-d5 34-12189 %Phenol-d5 54-12781 %Terphenyl-d14 Total Metals 0.62 7196A P8I014410.48 9/11/18 15:30 BMSmg/kg dry 0.11Hexavalent Chromium 0.049 7471B P8I006310.024 9/7/18 11:38 MMRmg/kg dry 0.0023Mercury 2.5 6010D P8I006410.60 9/7/18 15:34 JABmg/kg dry 0.037Arsenic 120 6010D P8I006410.60 9/7/18 15:34 JABmg/kg dry 0.087Barium 0.72 6010D P8I006410.30 9/7/18 15:34 JABmg/kg dry 0.0080Cadmium 41 6010D P8I006410.30 9/7/18 15:34 JABmg/kg dry 0.050Chromium 18 6010D P8I006410.30 9/7/18 15:34 JABmg/kg dry 0.056Lead This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-03 Prism Work Order: 8090062 Time Collected: 09/04/18 10:15 Time Submitted: 09/06/18 08:30 S-3 0.48 6010D P8I006410.60 9/11/18 18:48 JABJmg/kg dry 0.14Selenium 0.56 6010D P8I006410.30 9/7/18 15:34 JABmg/kg dry 0.0074Silver Volatile Organic Compounds by GC/MS BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000441,1,1,2-Tetrachloroethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000261,1,1-Trichloroethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000361,1,2,2-Tetrachloroethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000471,1,2-Trichloroethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000151,1-Dichloroethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000241,1-Dichloroethylene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000291,1-Dichloropropylene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000301,2,3-Trichlorobenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000681,2,3-Trichloropropane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000401,2,4-Trichlorobenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000411,2,4-Trimethylbenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000221,2-Dibromoethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000251,2-Dichlorobenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000321,2-Dichloroethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000331,2-Dichloropropane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000401,3,5-Trimethylbenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000351,3-Dichlorobenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000271,3-Dichloropropane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000211,4-Dichlorobenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000252,2-Dichloropropane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000282-Chlorotoluene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000324-Chlorotoluene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.000264-Isopropyltoluene 0.12 8260B P8I010610.054 9/10/18 16:02 ANGmg/kg dry 0.0013Acetone BRL 8260B P8I010610.0032 9/10/18 16:02 ANGmg/kg dry 0.00031Benzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00045Bromobenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00029Bromochloromethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00030Bromodichloromethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00061Bromoform 0.0028 8260B P8I010610.011 9/10/18 16:02 ANGJmg/kg dry 0.00066Bromomethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00027Carbon Tetrachloride BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00028Chlorobenzene BRL 8260B P8I010610.011 9/10/18 16:02 ANGmg/kg dry 0.00045Chloroethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00039Chloroform BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00036Chloromethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00023cis-1,2-Dichloroethylene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00018cis-1,3-Dichloropropylene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00022Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-03 Prism Work Order: 8090062 Time Collected: 09/04/18 10:15 Time Submitted: 09/06/18 08:30 S-3 BRL 8260B P8I010610.0054 9/10/18 16:02 ANGAamg/kg dry 0.00024Dichlorodifluoromethane BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00021Ethylbenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00022Isopropyl Ether BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00032Isopropylbenzene (Cumene) BRL 8260B P8I010610.011 9/10/18 16:02 ANGmg/kg dry 0.00049m,p-Xylenes BRL 8260B P8I010610.054 9/10/18 16:02 ANGmg/kg dry 0.00048Methyl Butyl Ketone (2-Hexanone) BRL 8260B P8I010610.11 9/10/18 16:02 ANGmg/kg dry 0.00048Methyl Ethyl Ketone (2-Butanone) BRL 8260B P8I010610.054 9/10/18 16:02 ANGmg/kg dry 0.00046Methyl Isobutyl Ketone BRL 8260B P8I010610.011 9/10/18 16:02 ANGmg/kg dry 0.00030Methylene Chloride BRL 8260B P8I010610.011 9/10/18 16:02 ANGmg/kg dry 0.00017Methyl-tert-Butyl Ether BRL 8260B P8I010610.011 9/10/18 16:02 ANGmg/kg dry 0.00017Naphthalene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00027n-Butylbenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00032n-Propylbenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00022o-Xylene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00026sec-Butylbenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00032Styrene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00018tert-Butylbenzene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00025Tetrachloroethylene 0.011 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00031Toluene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00032trans-1,2-Dichloroethylene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00028trans-1,3-Dichloropropylene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00035Trichloroethylene BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00035Trichlorofluoromethane BRL 8260B P8I010610.027 9/10/18 16:02 ANGmg/kg dry 0.00073Vinyl acetate BRL 8260B P8I010610.0054 9/10/18 16:02 ANGmg/kg dry 0.00026Vinyl chloride BRL 8260B P8I010610.016 9/10/18 16:02 ANGmg/kg dry 0.0010Xylenes, total Surrogate Recovery Control Limits 70-13097 %4-Bromofluorobenzene 84-123105 %Dibromofluoromethane 76-12990 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-04 Prism Work Order: 8090062 Time Collected: 09/04/18 10:45 Time Submitted: 09/06/18 08:30 S-4 General Chemistry Parameters 89.1 SM2540 G P8I014010.100 9/11/18 8:00 SLS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0581,2,4-Trichlorobenzene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0561,2-Dichlorobenzene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0521,3-Dichlorobenzene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0541,4-Dichlorobenzene 0.19 8270D P8I012110.37 9/11/18 18:54 JMVJmg/kg dry 0.0711-Methylnaphthalene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0692,4,6-Trichlorophenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0712,4-Dichlorophenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0572,4-Dimethylphenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0522,4-Dinitrophenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0452,4-Dinitrotoluene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0492,6-Dinitrotoluene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0542-Chloronaphthalene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0522-Chlorophenol 0.24 8270D P8I012110.37 9/11/18 18:54 JMVJmg/kg dry 0.0592-Methylnaphthalene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0472-Methylphenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0672-Nitrophenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0733,3’-Dichlorobenzidine BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0463/4-Methylphenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0564,6-Dinitro-2-methylphenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0644-Bromophenyl phenyl ether BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0524-Chloro-3-methylphenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0444-Chloroaniline BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0484-Chlorophenyl phenyl ether BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.0574-Nitrophenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.050Acenaphthene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.054Acenaphthylene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.060Anthracene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.049Azobenzene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.048Benzo(a)anthracene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.040Benzo(a)pyrene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.043Benzo(b)fluoranthene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.041Benzo(g,h,i)perylene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.049Benzo(k)fluoranthene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.031Benzoic Acid BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.049Benzyl alcohol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.064bis(2-Chloroethoxy)methane BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.052Bis(2-Chloroethyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-04 Prism Work Order: 8090062 Time Collected: 09/04/18 10:45 Time Submitted: 09/06/18 08:30 S-4 BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.063Bis(2-chloroisopropyl)ether BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.055Bis(2-Ethylhexyl)phthalate BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.053Butyl benzyl phthalate BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.047Chrysene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.045Dibenzo(a,h)anthracene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.056Dibenzofuran BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.051Diethyl phthalate BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.049Dimethyl phthalate BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.053Di-n-butyl phthalate BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.045Di-n-octyl phthalate BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.047Fluoranthene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.053Fluorene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.059Hexachlorobenzene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.066Hexachlorobutadiene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.066Hexachlorocyclopentadiene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.062Hexachloroethane BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.042Indeno(1,2,3-cd)pyrene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.050Isophorone 0.18 8270D P8I012110.37 9/11/18 18:54 JMVJmg/kg dry 0.059Naphthalene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.053Nitrobenzene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.058N-Nitroso-di-n-propylamine BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.056N-Nitrosodiphenylamine BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.044Pentachlorophenol 0.11 8270D P8I012110.37 9/11/18 18:54 JMVJmg/kg dry 0.048Phenanthrene BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.055Phenol BRL 8270D P8I012110.37 9/11/18 18:54 JMVmg/kg dry 0.049Pyrene Surrogate Recovery Control Limits 39-13279 %2,4,6-Tribromophenol 44-11579 %2-Fluorobiphenyl 35-11582 %2-Fluorophenol 37-12275 %Nitrobenzene-d5 34-12183 %Phenol-d5 54-12782 %Terphenyl-d14 Total Metals 0.31 7196A P8I014410.45 9/11/18 15:30 BMSJmg/kg dry 0.10Hexavalent Chromium 0.017 7471B P8I006310.022 9/7/18 11:43 MMRJmg/kg dry 0.0021Mercury 2.7 6010D P8I006410.56 9/7/18 15:43 JABmg/kg dry 0.034Arsenic 160 6010D P8I006452.8 9/11/18 12:25 JABmg/kg dry 0.41Barium 0.087 6010D P8I006410.28 9/7/18 15:43 JABJmg/kg dry 0.0075Cadmium 13 6010D P8I006410.28 9/7/18 15:43 JABmg/kg dry 0.047Chromium 16 6010D P8I006410.28 9/7/18 15:43 JABmg/kg dry 0.052Lead This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-04 Prism Work Order: 8090062 Time Collected: 09/04/18 10:45 Time Submitted: 09/06/18 08:30 S-4 1.0 6010D P8I006410.56 9/11/18 18:58 JABmg/kg dry 0.13Selenium BRL 6010D P8I006410.28 9/7/18 15:43 JABmg/kg dry 0.0070Silver Volatile Organic Compounds by GC/MS BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000411,1,1,2-Tetrachloroethane 0.0047 8260B P8I010610.0050 9/10/18 16:29 ANGJmg/kg dry 0.000241,1,1-Trichloroethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000341,1,2,2-Tetrachloroethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000441,1,2-Trichloroethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000141,1-Dichloroethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000221,1-Dichloroethylene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000271,1-Dichloropropylene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000281,2,3-Trichlorobenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000641,2,3-Trichloropropane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000371,2,4-Trichlorobenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000381,2,4-Trimethylbenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000201,2-Dibromoethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000231,2-Dichlorobenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000301,2-Dichloroethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000311,2-Dichloropropane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000381,3,5-Trimethylbenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000331,3-Dichlorobenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000251,3-Dichloropropane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000201,4-Dichlorobenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000242,2-Dichloropropane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000262-Chlorotoluene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000304-Chlorotoluene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.000244-Isopropyltoluene 0.054 8260B P8I010610.050 9/10/18 16:29 ANGmg/kg dry 0.0012Acetone BRL 8260B P8I010610.0030 9/10/18 16:29 ANGmg/kg dry 0.00029Benzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00042Bromobenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00027Bromochloromethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00028Bromodichloromethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00057Bromoform BRL 8260B P8I010610.010 9/10/18 16:29 ANGmg/kg dry 0.00061Bromomethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00025Carbon Tetrachloride BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00026Chlorobenzene BRL 8260B P8I010610.010 9/10/18 16:29 ANGmg/kg dry 0.00042Chloroethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00036Chloroform BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00033Chloromethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00021cis-1,2-Dichloroethylene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00017cis-1,3-Dichloropropylene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00021Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-04 Prism Work Order: 8090062 Time Collected: 09/04/18 10:45 Time Submitted: 09/06/18 08:30 S-4 BRL 8260B P8I010610.0050 9/10/18 16:29 ANGAamg/kg dry 0.00023Dichlorodifluoromethane BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00019Ethylbenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00020Isopropyl Ether BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00030Isopropylbenzene (Cumene) BRL 8260B P8I010610.010 9/10/18 16:29 ANGmg/kg dry 0.00046m,p-Xylenes BRL 8260B P8I010610.050 9/10/18 16:29 ANGmg/kg dry 0.00045Methyl Butyl Ketone (2-Hexanone) BRL 8260B P8I010610.10 9/10/18 16:29 ANGmg/kg dry 0.00045Methyl Ethyl Ketone (2-Butanone) BRL 8260B P8I010610.050 9/10/18 16:29 ANGmg/kg dry 0.00042Methyl Isobutyl Ketone BRL 8260B P8I010610.010 9/10/18 16:29 ANGmg/kg dry 0.00028Methylene Chloride BRL 8260B P8I010610.010 9/10/18 16:29 ANGmg/kg dry 0.00016Methyl-tert-Butyl Ether BRL 8260B P8I010610.010 9/10/18 16:29 ANGmg/kg dry 0.00016Naphthalene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00025n-Butylbenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00030n-Propylbenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00020o-Xylene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00024sec-Butylbenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00030Styrene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00017tert-Butylbenzene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00024Tetrachloroethylene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00029Toluene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00030trans-1,2-Dichloroethylene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00026trans-1,3-Dichloropropylene 0.010 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00032Trichloroethylene BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00032Trichlorofluoromethane BRL 8260B P8I010610.025 9/10/18 16:29 ANGmg/kg dry 0.00068Vinyl acetate BRL 8260B P8I010610.0050 9/10/18 16:29 ANGmg/kg dry 0.00024Vinyl chloride BRL 8260B P8I010610.015 9/10/18 16:29 ANGmg/kg dry 0.00093Xylenes, total Surrogate Recovery Control Limits 70-13097 %4-Bromofluorobenzene 84-123108 %Dibromofluoromethane 76-12988 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-05 Prism Work Order: 8090062 Time Collected: 09/04/18 11:00 Time Submitted: 09/06/18 08:30 S-5 General Chemistry Parameters 79.5 SM2540 G P8I014010.100 9/11/18 8:00 SLS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0651,2,4-Trichlorobenzene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0631,2-Dichlorobenzene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0581,3-Dichlorobenzene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0611,4-Dichlorobenzene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0801-Methylnaphthalene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0782,4,6-Trichlorophenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0802,4-Dichlorophenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0632,4-Dimethylphenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0582,4-Dinitrophenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0502,4-Dinitrotoluene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0552,6-Dinitrotoluene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0602-Chloronaphthalene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0592-Chlorophenol 0.13 8270D P8I012110.41 9/11/18 19:16 JMVJmg/kg dry 0.0662-Methylnaphthalene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0532-Methylphenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0752-Nitrophenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0823,3’-Dichlorobenzidine BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0513/4-Methylphenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0714-Bromophenyl phenyl ether BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0584-Chloro-3-methylphenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0504-Chloroaniline BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.0644-Nitrophenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.056Acenaphthene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.060Acenaphthylene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.067Anthracene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.055Azobenzene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.054Benzo(a)anthracene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.045Benzo(a)pyrene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.048Benzo(b)fluoranthene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.045Benzo(g,h,i)perylene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.054Benzo(k)fluoranthene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.035Benzoic Acid BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.055Benzyl alcohol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.072bis(2-Chloroethoxy)methane BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-05 Prism Work Order: 8090062 Time Collected: 09/04/18 11:00 Time Submitted: 09/06/18 08:30 S-5 BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.071Bis(2-chloroisopropyl)ether BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.059Butyl benzyl phthalate BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.052Chrysene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.063Dibenzofuran BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.057Diethyl phthalate BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.055Dimethyl phthalate BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.059Di-n-butyl phthalate BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.051Di-n-octyl phthalate BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.053Fluoranthene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.059Fluorene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.066Hexachlorobenzene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.074Hexachlorobutadiene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.074Hexachlorocyclopentadiene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.069Hexachloroethane BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.048Indeno(1,2,3-cd)pyrene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.056Isophorone BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.067Naphthalene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.059Nitrobenzene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.063N-Nitrosodiphenylamine BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.049Pentachlorophenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.054Phenanthrene BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.061Phenol BRL 8270D P8I012110.41 9/11/18 19:16 JMVmg/kg dry 0.055Pyrene Surrogate Recovery Control Limits 39-13282 %2,4,6-Tribromophenol 44-11581 %2-Fluorobiphenyl 35-11578 %2-Fluorophenol 37-12271 %Nitrobenzene-d5 34-12175 %Phenol-d5 54-12777 %Terphenyl-d14 Total Metals 0.86 7196A P8I014410.50 9/11/18 15:30 BMSmg/kg dry 0.11Hexavalent Chromium 0.018 7471B P8I006310.024 9/7/18 11:48 MMRJmg/kg dry 0.0023Mercury 2.9 6010D P8I006410.62 9/7/18 15:52 JABmg/kg dry 0.038Arsenic 190 6010D P8I006453.1 9/11/18 12:33 JABmg/kg dry 0.45Barium BRL 6010D P8I006410.31 9/7/18 15:52 JABmg/kg dry 0.0083Cadmium 28 6010D P8I006410.31 9/7/18 15:52 JABmg/kg dry 0.052Chromium 15 6010D P8I006410.31 9/7/18 15:52 JABmg/kg dry 0.058Lead This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-05 Prism Work Order: 8090062 Time Collected: 09/04/18 11:00 Time Submitted: 09/06/18 08:30 S-5 0.40 6010D P8I006410.62 9/11/18 19:03 JABJmg/kg dry 0.15Selenium BRL 6010D P8I006410.31 9/7/18 15:52 JABmg/kg dry 0.0077Silver Volatile Organic Compounds by GC/MS BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000421,1,1,2-Tetrachloroethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000251,1,1-Trichloroethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000351,1,2,2-Tetrachloroethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000461,1,2-Trichloroethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000141,1-Dichloroethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000231,1-Dichloroethylene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000281,1-Dichloropropylene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000291,2,3-Trichlorobenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000661,2,3-Trichloropropane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000381,2,4-Trichlorobenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000391,2,4-Trimethylbenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000211,2-Dibromoethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000241,2-Dichlorobenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000311,2-Dichloroethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000321,2-Dichloropropane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000391,3,5-Trimethylbenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000341,3-Dichlorobenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000261,3-Dichloropropane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000201,4-Dichlorobenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000242,2-Dichloropropane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000272-Chlorotoluene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000314-Chlorotoluene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.000254-Isopropyltoluene 0.11 8260B P8I010610.051 9/10/18 16:57 ANGmg/kg dry 0.0013Acetone BRL 8260B P8I010610.0031 9/10/18 16:57 ANGmg/kg dry 0.00030Benzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00043Bromobenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00028Bromochloromethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00029Bromodichloromethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00058Bromoform BRL 8260B P8I010610.010 9/10/18 16:57 ANGmg/kg dry 0.00063Bromomethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00026Carbon Tetrachloride BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00027Chlorobenzene BRL 8260B P8I010610.010 9/10/18 16:57 ANGmg/kg dry 0.00043Chloroethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00037Chloroform BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00035Chloromethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00022cis-1,2-Dichloroethylene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00017cis-1,3-Dichloropropylene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00021Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-05 Prism Work Order: 8090062 Time Collected: 09/04/18 11:00 Time Submitted: 09/06/18 08:30 S-5 BRL 8260B P8I010610.0051 9/10/18 16:57 ANGAamg/kg dry 0.00023Dichlorodifluoromethane BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00020Ethylbenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00021Isopropyl Ether BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00030Isopropylbenzene (Cumene) BRL 8260B P8I010610.010 9/10/18 16:57 ANGmg/kg dry 0.00047m,p-Xylenes BRL 8260B P8I010610.051 9/10/18 16:57 ANGmg/kg dry 0.00047Methyl Butyl Ketone (2-Hexanone) BRL 8260B P8I010610.10 9/10/18 16:57 ANGmg/kg dry 0.00047Methyl Ethyl Ketone (2-Butanone) BRL 8260B P8I010610.051 9/10/18 16:57 ANGmg/kg dry 0.00044Methyl Isobutyl Ketone BRL 8260B P8I010610.010 9/10/18 16:57 ANGmg/kg dry 0.00029Methylene Chloride BRL 8260B P8I010610.010 9/10/18 16:57 ANGmg/kg dry 0.00016Methyl-tert-Butyl Ether BRL 8260B P8I010610.010 9/10/18 16:57 ANGmg/kg dry 0.00016Naphthalene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00026n-Butylbenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00031n-Propylbenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00021o-Xylene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00025sec-Butylbenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00031Styrene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00017tert-Butylbenzene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00024Tetrachloroethylene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00030Toluene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00031trans-1,2-Dichloroethylene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00027trans-1,3-Dichloropropylene 0.012 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00033Trichloroethylene BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00033Trichlorofluoromethane BRL 8260B P8I010610.026 9/10/18 16:57 ANGmg/kg dry 0.00070Vinyl acetate BRL 8260B P8I010610.0051 9/10/18 16:57 ANGmg/kg dry 0.00025Vinyl chloride BRL 8260B P8I010610.015 9/10/18 16:57 ANGmg/kg dry 0.00096Xylenes, total Surrogate Recovery Control Limits 70-13095 %4-Bromofluorobenzene 84-123107 %Dibromofluoromethane 76-12990 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-06 Prism Work Order: 8090062 Time Collected: 09/04/18 11:15 Time Submitted: 09/06/18 08:30 S-6 General Chemistry Parameters 77.2 SM2540 G P8I014010.100 9/11/18 8:00 SLS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0671,2,4-Trichlorobenzene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0651,2-Dichlorobenzene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0601,3-Dichlorobenzene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0631,4-Dichlorobenzene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0821-Methylnaphthalene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0802,4,6-Trichlorophenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0832,4-Dichlorophenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0662,4-Dimethylphenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0602,4-Dinitrophenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0522,4-Dinitrotoluene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0572,6-Dinitrotoluene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0622-Chloronaphthalene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0612-Chlorophenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0682-Methylnaphthalene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0552-Methylphenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0782-Nitrophenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0843,3’-Dichlorobenzidine BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0533/4-Methylphenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0644,6-Dinitro-2-methylphenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0734-Bromophenyl phenyl ether BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0604-Chloro-3-methylphenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0514-Chloroaniline BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.0664-Nitrophenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.058Acenaphthene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.062Acenaphthylene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.069Anthracene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.056Azobenzene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.056Benzo(a)anthracene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.046Benzo(a)pyrene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.050Benzo(b)fluoranthene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.047Benzo(g,h,i)perylene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.056Benzo(k)fluoranthene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.036Benzoic Acid BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.056Benzyl alcohol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.074bis(2-Chloroethoxy)methane BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.060Bis(2-Chloroethyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-06 Prism Work Order: 8090062 Time Collected: 09/04/18 11:15 Time Submitted: 09/06/18 08:30 S-6 BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.073Bis(2-chloroisopropyl)ether BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.061Butyl benzyl phthalate BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.054Chrysene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.065Dibenzofuran BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.059Diethyl phthalate BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.056Dimethyl phthalate BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.061Di-n-butyl phthalate BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.053Di-n-octyl phthalate BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.055Fluoranthene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.061Fluorene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.068Hexachlorobenzene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.077Hexachlorobutadiene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.076Hexachlorocyclopentadiene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.072Hexachloroethane BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.058Isophorone BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.069Naphthalene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.061Nitrobenzene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.067N-Nitroso-di-n-propylamine BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.065N-Nitrosodiphenylamine BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.051Pentachlorophenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.056Phenanthrene BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.063Phenol BRL 8270D P8I012110.43 9/11/18 19:38 JMVmg/kg dry 0.057Pyrene Surrogate Recovery Control Limits 39-13287 %2,4,6-Tribromophenol 44-11583 %2-Fluorobiphenyl 35-11591 %2-Fluorophenol 37-12273 %Nitrobenzene-d5 34-12186 %Phenol-d5 54-12781 %Terphenyl-d14 Total Metals 1.1 7196A P8I014410.52 9/11/18 15:30 BMSmg/kg dry 0.12Hexavalent Chromium 0.097 7471B P8I006310.026 9/7/18 11:52 MMRmg/kg dry 0.0025Mercury 2.5 6010D P8I006410.64 9/7/18 16:00 JABmg/kg dry 0.039Arsenic 100 6010D P8I006410.64 9/7/18 16:00 JABmg/kg dry 0.094Barium 0.061 6010D P8I006410.32 9/7/18 16:00 JABJmg/kg dry 0.0086Cadmium 28 6010D P8I006410.32 9/7/18 16:00 JABmg/kg dry 0.054Chromium 16 6010D P8I006410.32 9/7/18 16:00 JABmg/kg dry 0.060Lead This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-06 Prism Work Order: 8090062 Time Collected: 09/04/18 11:15 Time Submitted: 09/06/18 08:30 S-6 0.72 6010D P8I006410.64 9/11/18 19:15 JABmg/kg dry 0.15Selenium BRL 6010D P8I006410.32 9/7/18 16:00 JABmg/kg dry 0.0080Silver Volatile Organic Compounds by GC/MS BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000491,1,1,2-Tetrachloroethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000291,1,1-Trichloroethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000401,1,2,2-Tetrachloroethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000531,1,2-Trichloroethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000171,1-Dichloroethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000261,1-Dichloroethylene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000331,1-Dichloropropylene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000341,2,3-Trichlorobenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000761,2,3-Trichloropropane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000441,2,4-Trichlorobenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000461,2,4-Trimethylbenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000241,2-Dibromoethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000281,2-Dichlorobenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000361,2-Dichloroethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000371,2-Dichloropropane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000451,3,5-Trimethylbenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000391,3-Dichlorobenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000301,3-Dichloropropane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000241,4-Dichlorobenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000282,2-Dichloropropane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000312-Chlorotoluene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000364-Chlorotoluene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.000294-Isopropyltoluene 0.14 8260B P8I010610.060 9/10/18 17:24 ANGmg/kg dry 0.0015Acetone BRL 8260B P8I010610.0036 9/10/18 17:24 ANGmg/kg dry 0.00035Benzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00050Bromobenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00033Bromochloromethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00033Bromodichloromethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00068Bromoform BRL 8260B P8I010610.012 9/10/18 17:24 ANGmg/kg dry 0.00074Bromomethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00030Carbon Tetrachloride BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00032Chlorobenzene BRL 8260B P8I010610.012 9/10/18 17:24 ANGmg/kg dry 0.00050Chloroethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00043Chloroform BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00040Chloromethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00025cis-1,2-Dichloroethylene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00025Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Solid Client Sample ID: Prism Sample ID: 8090062-06 Prism Work Order: 8090062 Time Collected: 09/04/18 11:15 Time Submitted: 09/06/18 08:30 S-6 BRL 8260B P8I010610.0060 9/10/18 17:24 ANGAamg/kg dry 0.00027Dichlorodifluoromethane BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00023Ethylbenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00024Isopropyl Ether BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00035Isopropylbenzene (Cumene) BRL 8260B P8I010610.012 9/10/18 17:24 ANGmg/kg dry 0.00055m,p-Xylenes BRL 8260B P8I010610.060 9/10/18 17:24 ANGmg/kg dry 0.00054Methyl Butyl Ketone (2-Hexanone) BRL 8260B P8I010610.12 9/10/18 17:24 ANGmg/kg dry 0.00054Methyl Ethyl Ketone (2-Butanone) BRL 8260B P8I010610.060 9/10/18 17:24 ANGmg/kg dry 0.00051Methyl Isobutyl Ketone BRL 8260B P8I010610.012 9/10/18 17:24 ANGmg/kg dry 0.00034Methylene Chloride BRL 8260B P8I010610.012 9/10/18 17:24 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether BRL 8260B P8I010610.012 9/10/18 17:24 ANGmg/kg dry 0.00019Naphthalene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00030n-Butylbenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00035n-Propylbenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00024o-Xylene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00029sec-Butylbenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00036Styrene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00020tert-Butylbenzene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00028Tetrachloroethylene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00034Toluene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00036trans-1,2-Dichloroethylene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00031trans-1,3-Dichloropropylene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00039Trichloroethylene BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00039Trichlorofluoromethane BRL 8260B P8I010610.030 9/10/18 17:24 ANGmg/kg dry 0.00082Vinyl acetate BRL 8260B P8I010610.0060 9/10/18 17:24 ANGmg/kg dry 0.00029Vinyl chloride BRL 8260B P8I010610.018 9/10/18 17:24 ANGmg/kg dry 0.0011Xylenes, total Surrogate Recovery Control Limits 70-13096 %4-Bromofluorobenzene 84-123105 %Dibromofluoromethane 76-12988 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-07 Prism Work Order: 8090062 Time Collected: 09/04/18 18:45 Time Submitted: 09/06/18 08:30 GW-1 Semivolatile Organic Compounds by GC/MS BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.81,2,4-Trichlorobenzene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.61,2-Dichlorobenzene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.91,3-Dichlorobenzene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.61,4-Dichlorobenzene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.61-Methylnaphthalene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.62,4,5-Trichlorophenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.82,4,6-Trichlorophenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.62,4-Dichlorophenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 3.42,4-Dimethylphenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.72,4-Dinitrophenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.42,4-Dinitrotoluene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.12,6-Dinitrotoluene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.72-Chloronaphthalene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.92-Chlorophenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.42-Methylnaphthalene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.82-Methylphenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.42-Nitroaniline BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.42-Nitrophenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.43,3’-Dichlorobenzidine BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.53/4-Methylphenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.43-Nitroaniline BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.44,6-Dinitro-2-methylphenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.34-Bromophenyl phenyl ether BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.44-Chloro-3-methylphenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.44-Chloroaniline BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.34-Chlorophenyl phenyl ether BRL 8270D P8I00571109/10/18 16:02 JMVug/L 0.934-Nitroaniline BRL 8270D P8I00571109/10/18 16:02 JMVug/L 0.604-Nitrophenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.8Acenaphthene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.0Acenaphthylene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.4Aniline BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.4Anthracene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.8Azobenzene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.4Benzo(a)anthracene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.4Benzo(a)pyrene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.1Benzo(b)fluoranthene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.4Benzo(g,h,i)perylene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.4Benzo(k)fluoranthene 630 8270D P8I005755009/11/18 11:31 JMVug/L 23Benzoic Acid BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.1Benzyl alcohol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-07 Prism Work Order: 8090062 Time Collected: 09/04/18 18:45 Time Submitted: 09/06/18 08:30 GW-1 BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.6bis(2-Chloroethoxy)methane BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.3Bis(2-Chloroethyl)ether BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.0Bis(2-chloroisopropyl)ether BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.3Bis(2-Ethylhexyl)phthalate BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.4Butyl benzyl phthalate BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.4Chrysene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.2Dibenzo(a,h)anthracene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.8Dibenzofuran BRL 8270D P8I00571109/10/18 16:02 JMVug/L 3.3Diethyl phthalate BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.4Dimethyl phthalate BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.7Di-n-butyl phthalate BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.3Di-n-octyl phthalate BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.7Fluoranthene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.7Fluorene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.3Hexachlorobenzene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.1Hexachlorobutadiene BRL 8270D P8I00571109/10/18 16:02 JMVAug/L 1.7Hexachlorocyclopentadiene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.7Hexachloroethane BRL 8270D P8I00571109/10/18 16:02 JMVug/L 3.9Indeno(1,2,3-cd)pyrene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.5Isophorone BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.6Naphthalene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.6Nitrobenzene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 2.2N-Nitroso-di-n-propylamine BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.3N-Nitrosodiphenylamine BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.2Pentachlorophenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.5Phenanthrene BRL 8270D P8I00571109/10/18 16:02 JMVug/L 0.98Phenol BRL 8270D P8I00571109/10/18 16:02 JMVug/L 1.4Pyrene Surrogate Recovery Control Limits 43-14040 %2,4,6-Tribromophenol SE 44-11935 %2-Fluorobiphenyl SE 19-11936 %2-Fluorophenol 44-12032 %Nitrobenzene-d5 SE 11-5226 %Phenol-d5 50-13442 %Terphenyl-d14 SE Total Metals BRL 7470A P8I011710.00020 9/11/18 13:56 MMRmg/L 0.000036Mercury BRL 6010D P8I006510.020 9/11/18 13:07 JABmg/L 0.0031Arsenic 0.24 6010D P8I006510.010 9/11/18 13:07 JABmg/L 0.00080Barium BRL 6010D P8I006510.0010 9/11/18 18:18 JABmg/L 0.00015Cadmium 0.0073 6010D P8I006510.0050 9/11/18 13:07 JABmg/L 0.00036Chromium This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-07 Prism Work Order: 8090062 Time Collected: 09/04/18 18:45 Time Submitted: 09/06/18 08:30 GW-1 0.0049 6010D P8I006510.0050 9/13/18 12:19 JABJmg/L 0.00080Lead BRL 6010D P8I006510.020 9/11/18 13:07 JABmg/L 0.0056Selenium BRL 6010D P8I006510.0050 9/11/18 13:07 JABmg/L 0.00039Silver This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-08 Prism Work Order: 8090062 Time Collected: 09/04/18 17:30 Time Submitted: 09/06/18 08:30 GW-2 Semivolatile Organic Compounds by GC/MS BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.81,2,4-Trichlorobenzene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.71,2-Dichlorobenzene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.91,3-Dichlorobenzene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.71,4-Dichlorobenzene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.71-Methylnaphthalene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.62,4,5-Trichlorophenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.92,4,6-Trichlorophenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.62,4-Dichlorophenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 3.52,4-Dimethylphenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.82,4-Dinitrophenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.52,4-Dinitrotoluene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.22,6-Dinitrotoluene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.82-Chloronaphthalene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.92-Chlorophenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.42-Methylnaphthalene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.92-Methylphenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.42-Nitroaniline BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.42-Nitrophenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.53,3’-Dichlorobenzidine BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.63/4-Methylphenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.43-Nitroaniline BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.44,6-Dinitro-2-methylphenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.34-Bromophenyl phenyl ether BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.44-Chloro-3-methylphenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.54-Chloroaniline BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.34-Chlorophenyl phenyl ether BRL 8270D P8I00571109/10/18 16:24 JMVug/L 0.954-Nitroaniline BRL 8270D P8I00571109/10/18 16:24 JMVug/L 0.614-Nitrophenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.8Acenaphthene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.1Acenaphthylene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.4Aniline BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.5Anthracene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.8Azobenzene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.5Benzo(a)anthracene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.5Benzo(a)pyrene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.2Benzo(b)fluoranthene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.4Benzo(g,h,i)perylene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.4Benzo(k)fluoranthene BRL 8270D P8I005711009/10/18 16:24 JMVug/L 4.8Benzoic Acid BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.2Benzyl alcohol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-08 Prism Work Order: 8090062 Time Collected: 09/04/18 17:30 Time Submitted: 09/06/18 08:30 GW-2 BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.6bis(2-Chloroethoxy)methane BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.4Bis(2-Chloroethyl)ether BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.0Bis(2-chloroisopropyl)ether BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.3Bis(2-Ethylhexyl)phthalate BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.4Butyl benzyl phthalate BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.5Chrysene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.2Dibenzo(a,h)anthracene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.8Dibenzofuran BRL 8270D P8I00571109/10/18 16:24 JMVug/L 3.4Diethyl phthalate BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.4Dimethyl phthalate BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.7Di-n-butyl phthalate BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.3Di-n-octyl phthalate BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.7Fluoranthene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.7Fluorene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.3Hexachlorobenzene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.2Hexachlorobutadiene BRL 8270D P8I00571109/10/18 16:24 JMVAug/L 1.8Hexachlorocyclopentadiene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.8Hexachloroethane BRL 8270D P8I00571109/10/18 16:24 JMVug/L 4.0Indeno(1,2,3-cd)pyrene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.6Isophorone BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.6Naphthalene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.6Nitrobenzene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 2.2N-Nitroso-di-n-propylamine BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.3N-Nitrosodiphenylamine BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.3Pentachlorophenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.5Phenanthrene BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.0Phenol BRL 8270D P8I00571109/10/18 16:24 JMVug/L 1.5Pyrene Surrogate Recovery Control Limits 43-14097 %2,4,6-Tribromophenol 44-11995 %2-Fluorobiphenyl 19-11956 %2-Fluorophenol 44-12089 %Nitrobenzene-d5 11-5236 %Phenol-d5 50-134101 %Terphenyl-d14 Total Metals BRL 7470A P8I011710.00020 9/11/18 13:44 MMRmg/L 0.000036Mercury 0.013 6010D P8I006510.020 9/11/18 13:29 JABJmg/L 0.0031Arsenic 1.1 6010D P8I006510.010 9/11/18 13:29 JABmg/L 0.00080Barium 0.00022 6010D P8I006510.0010 9/11/18 18:27 JABJmg/L 0.00015Cadmium 0.082 6010D P8I006510.0050 9/11/18 13:29 JABmg/L 0.00036Chromium This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-08 Prism Work Order: 8090062 Time Collected: 09/04/18 17:30 Time Submitted: 09/06/18 08:30 GW-2 0.058 6010D P8I006510.0050 9/13/18 12:27 JABmg/L 0.00080Lead BRL 6010D P8I006510.020 9/11/18 13:29 JABmg/L 0.0056Selenium BRL 6010D P8I006510.0050 9/11/18 18:27 JABmg/L 0.00039Silver This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-09 Prism Work Order: 8090062 Time Collected: 09/04/18 16:00 Time Submitted: 09/06/18 08:30 GW-3 Semivolatile Organic Compounds by GC/MS BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.91,2,4-Trichlorobenzene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.81,2-Dichlorobenzene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.01,3-Dichlorobenzene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.81,4-Dichlorobenzene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.81-Methylnaphthalene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.72,4,5-Trichlorophenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.02,4,6-Trichlorophenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.82,4-Dichlorophenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 3.82,4-Dimethylphenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.92,4-Dinitrophenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.62,4-Dinitrotoluene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.22,6-Dinitrotoluene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.92-Chloronaphthalene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.02-Chlorophenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.62-Methylnaphthalene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.02-Methylphenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.52-Nitroaniline BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.62-Nitrophenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.63,3’-Dichlorobenzidine BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.73/4-Methylphenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.53-Nitroaniline BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.54,6-Dinitro-2-methylphenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.44-Bromophenyl phenyl ether BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.64-Chloro-3-methylphenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.74-Chloroaniline BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.44-Chlorophenyl phenyl ether BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.04-Nitroaniline BRL 8270D P8I00571119/10/18 16:46 JMVug/L 0.654-Nitrophenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.0Acenaphthene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.2Acenaphthylene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.6Aniline BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.6Anthracene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.9Azobenzene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.6Benzo(a)anthracene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.6Benzo(a)pyrene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.2Benzo(b)fluoranthene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.5Benzo(g,h,i)perylene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.5Benzo(k)fluoranthene BRL 8270D P8I005711109/10/18 16:46 JMVug/L 5.1Benzoic Acid BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.3Benzyl alcohol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-09 Prism Work Order: 8090062 Time Collected: 09/04/18 16:00 Time Submitted: 09/06/18 08:30 GW-3 BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.8bis(2-Chloroethoxy)methane BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.5Bis(2-Chloroethyl)ether BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.1Bis(2-chloroisopropyl)ether BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.4Bis(2-Ethylhexyl)phthalate BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.5Butyl benzyl phthalate BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.6Chrysene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.3Dibenzo(a,h)anthracene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.9Dibenzofuran 8.1 8270D P8I00571119/10/18 16:46 JMVJug/L 3.6Diethyl phthalate BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.5Dimethyl phthalate BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.8Di-n-butyl phthalate BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.4Di-n-octyl phthalate BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.8Fluoranthene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.8Fluorene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.4Hexachlorobenzene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.3Hexachlorobutadiene BRL 8270D P8I00571119/10/18 16:46 JMVAug/L 1.9Hexachlorocyclopentadiene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.9Hexachloroethane BRL 8270D P8I00571119/10/18 16:46 JMVug/L 4.2Indeno(1,2,3-cd)pyrene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.7Isophorone BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.8Naphthalene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.8Nitrobenzene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 2.4N-Nitroso-di-n-propylamine BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.4N-Nitrosodiphenylamine BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.3Pentachlorophenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.6Phenanthrene BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.1Phenol BRL 8270D P8I00571119/10/18 16:46 JMVug/L 1.6Pyrene Surrogate Recovery Control Limits 43-14083 %2,4,6-Tribromophenol 44-11988 %2-Fluorobiphenyl 19-11949 %2-Fluorophenol 44-12082 %Nitrobenzene-d5 11-5236 %Phenol-d5 50-13496 %Terphenyl-d14 Total Metals 0.00037 7470A P8I011710.00020 9/11/18 13:48 MMRmg/L 0.000036Mercury 0.070 6010D P8I006510.020 9/11/18 13:38 JABmg/L 0.0031Arsenic 6.9 6010D P8I0065100.10 9/12/18 12:24 JABmg/L 0.0080Barium BRL 6010D P8I006510.0010 9/11/18 13:38 JABmg/L 0.00015Cadmium 0.57 6010D P8I006510.0050 9/11/18 13:38 JABmg/L 0.00036Chromium This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 35 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-09 Prism Work Order: 8090062 Time Collected: 09/04/18 16:00 Time Submitted: 09/06/18 08:30 GW-3 0.22 6010D P8I006510.0050 9/11/18 13:38 JABmg/L 0.00080Lead BRL 6010D P8I006510.020 9/11/18 13:38 JABmg/L 0.0056Selenium BRL 6010D P8I006510.0050 9/11/18 13:38 JABmg/L 0.00039Silver This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 36 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-10 Prism Work Order: 8090062 Time Collected: 09/04/18 17:30 Time Submitted: 09/06/18 08:30 GW-4 Semivolatile Organic Compounds by GC/MS BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.81,2,4-Trichlorobenzene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.61,2-Dichlorobenzene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.91,3-Dichlorobenzene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.61,4-Dichlorobenzene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.61-Methylnaphthalene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.62,4,5-Trichlorophenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.82,4,6-Trichlorophenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.62,4-Dichlorophenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 3.42,4-Dimethylphenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.72,4-Dinitrophenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.42,4-Dinitrotoluene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.12,6-Dinitrotoluene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.72-Chloronaphthalene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.92-Chlorophenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.42-Methylnaphthalene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.82-Methylphenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.42-Nitroaniline BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.42-Nitrophenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.43,3’-Dichlorobenzidine BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.53/4-Methylphenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.43-Nitroaniline BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.44,6-Dinitro-2-methylphenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.34-Bromophenyl phenyl ether BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.44-Chloro-3-methylphenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.44-Chloroaniline BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.34-Chlorophenyl phenyl ether BRL 8270D P8I00571109/10/18 17:08 JMVug/L 0.934-Nitroaniline BRL 8270D P8I00571109/10/18 17:08 JMVug/L 0.604-Nitrophenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.8Acenaphthene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.0Acenaphthylene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.4Aniline BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.4Anthracene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.8Azobenzene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.4Benzo(a)anthracene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.4Benzo(a)pyrene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.1Benzo(b)fluoranthene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.4Benzo(g,h,i)perylene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.4Benzo(k)fluoranthene BRL 8270D P8I005711009/10/18 17:08 JMVug/L 4.7Benzoic Acid BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.1Benzyl alcohol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-10 Prism Work Order: 8090062 Time Collected: 09/04/18 17:30 Time Submitted: 09/06/18 08:30 GW-4 BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.6bis(2-Chloroethoxy)methane BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.3Bis(2-Chloroethyl)ether BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.0Bis(2-chloroisopropyl)ether BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.3Bis(2-Ethylhexyl)phthalate BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.4Butyl benzyl phthalate BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.4Chrysene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.2Dibenzo(a,h)anthracene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.8Dibenzofuran BRL 8270D P8I00571109/10/18 17:08 JMVug/L 3.3Diethyl phthalate BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.4Dimethyl phthalate BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.7Di-n-butyl phthalate BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.3Di-n-octyl phthalate BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.7Fluoranthene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.7Fluorene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.3Hexachlorobenzene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.1Hexachlorobutadiene BRL 8270D P8I00571109/10/18 17:08 JMVAug/L 1.7Hexachlorocyclopentadiene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.7Hexachloroethane BRL 8270D P8I00571109/10/18 17:08 JMVug/L 3.9Indeno(1,2,3-cd)pyrene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.5Isophorone BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.6Naphthalene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.6Nitrobenzene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 2.2N-Nitroso-di-n-propylamine BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.3N-Nitrosodiphenylamine BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.2Pentachlorophenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.5Phenanthrene BRL 8270D P8I00571109/10/18 17:08 JMVug/L 0.98Phenol BRL 8270D P8I00571109/10/18 17:08 JMVug/L 1.4Pyrene Surrogate Recovery Control Limits 43-14084 %2,4,6-Tribromophenol 44-11993 %2-Fluorobiphenyl 19-11953 %2-Fluorophenol 44-12085 %Nitrobenzene-d5 11-5234 %Phenol-d5 50-13497 %Terphenyl-d14 Total Metals BRL 7470A P8I011710.00020 9/11/18 13:52 MMRmg/L 0.000036Mercury 0.011 6010D P8I006510.020 9/11/18 13:54 JABJmg/L 0.0031Arsenic 0.92 6010D P8I006510.010 9/11/18 13:54 JABmg/L 0.00080Barium BRL 6010D P8I006510.0010 9/11/18 13:54 JABmg/L 0.00015Cadmium 0.050 6010D P8I006510.0050 9/11/18 13:54 JABmg/L 0.00036Chromium This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 of 95 Laboratory Report 09/20/2018 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Sample Matrix: Water Client Sample ID: Prism Sample ID: 8090062-10 Prism Work Order: 8090062 Time Collected: 09/04/18 17:30 Time Submitted: 09/06/18 08:30 GW-4 0.031 6010D P8I006510.0050 9/11/18 13:54 JABmg/L 0.00080Lead BRL 6010D P8I006510.020 9/11/18 13:54 JABmg/L 0.0056Selenium BRL 6010D P8I006510.0050 9/11/18 13:54 JABmg/L 0.00039Silver This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 39 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P8I0106 - 5035 Blank (P8I0106-BLK1)Prepared & Analyzed: 09/10/18 1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050 1,1,1-Trichloroethane mg/kg wetBRL0.0050 1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050 1,1,2-Trichloroethane mg/kg wetBRL0.0050 1,1-Dichloroethane mg/kg wetBRL0.0050 1,1-Dichloroethylene mg/kg wetBRL0.0050 1,1-Dichloropropylene mg/kg wetBRL0.0050 1,2,3-Trichlorobenzene mg/kg wetBRL0.0050 1,2,3-Trichloropropane mg/kg wetBRL0.0050 1,2,4-Trichlorobenzene mg/kg wetBRL0.0050 1,2,4-Trimethylbenzene mg/kg wetBRL0.0050 1,2-Dibromoethane mg/kg wetBRL0.0050 1,2-Dichlorobenzene mg/kg wetBRL0.0050 1,2-Dichloroethane mg/kg wetBRL0.0050 1,2-Dichloropropane mg/kg wetBRL0.0050 1,3,5-Trimethylbenzene mg/kg wetBRL0.0050 1,3-Dichlorobenzene mg/kg wetBRL0.0050 1,3-Dichloropropane mg/kg wetBRL0.0050 1,4-Dichlorobenzene mg/kg wetBRL0.0050 2,2-Dichloropropane mg/kg wetBRL0.0050 2-Chlorotoluene mg/kg wetBRL0.0050 4-Chlorotoluene mg/kg wetBRL0.0050 4-Isopropyltoluene mg/kg wetBRL0.0050 Acetone mg/kg wetBRL0.050 Benzene mg/kg wetBRL0.0030 Bromobenzene mg/kg wetBRL0.0050 Bromochloromethane mg/kg wetBRL0.0050 Bromodichloromethane mg/kg wetBRL0.0050 Bromoform mg/kg wetBRL0.0050 Bromomethane mg/kg wetBRL0.010 Carbon Tetrachloride mg/kg wetBRL0.0050 Chlorobenzene mg/kg wetBRL0.0050 Chloroethane mg/kg wetBRL0.010 Chloroform mg/kg wetBRL0.0050 Chloromethane mg/kg wetBRL0.0050 cis-1,2-Dichloroethylene mg/kg wetBRL0.0050 cis-1,3-Dichloropropylene mg/kg wetBRL0.0050 Dibromochloromethane mg/kg wetBRL0.0050 Dichlorodifluoromethane mg/kg wetBRL0.0050 Ethylbenzene mg/kg wetBRL0.0050 Isopropyl Ether mg/kg wetBRL0.0050 Isopropylbenzene (Cumene)mg/kg wetBRL0.0050 m,p-Xylenes mg/kg wetBRL0.010 Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050 Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10 Methyl Isobutyl Ketone mg/kg wetBRL0.050 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P8I0106 - 5035 Blank (P8I0106-BLK1)Prepared & Analyzed: 09/10/18 Methylene Chloride mg/kg wetBRL0.010 Methyl-tert-Butyl Ether mg/kg wetBRL0.010 Naphthalene mg/kg wetBRL0.010 n-Butylbenzene mg/kg wetBRL0.0050 n-Propylbenzene mg/kg wetBRL0.0050 o-Xylene mg/kg wetBRL0.0050 sec-Butylbenzene mg/kg wetBRL0.0050 Styrene mg/kg wetBRL0.0050 tert-Butylbenzene mg/kg wetBRL0.0050 Tetrachloroethylene mg/kg wetBRL0.0050 Toluene mg/kg wetBRL0.0050 trans-1,2-Dichloroethylene mg/kg wetBRL0.0050 trans-1,3-Dichloropropylene mg/kg wetBRL0.0050 Trichloroethylene mg/kg wetBRL0.0050 Trichlorofluoromethane mg/kg wetBRL0.0050 Vinyl acetate mg/kg wetBRL0.025 Vinyl chloride mg/kg wetBRL0.0050 Xylenes, total mg/kg wetBRL0.015 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.6 ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10452.1 ug/L 50.00 76-129Surrogate: Toluene-d8 8944.7 LCS (P8I0106-BS1)Prepared & Analyzed: 09/10/18 1,1,1,2-Tetrachloroethane mg/kg wet0.0520 0.0050 0.05000 72-115104 1,1,1-Trichloroethane mg/kg wet0.0506 0.0050 0.05000 67-131101 1,1,2,2-Tetrachloroethane mg/kg wet0.0463 0.0050 0.05000 56-12693 1,1,2-Trichloroethane mg/kg wet0.0502 0.0050 0.05000 70-133100 1,1-Dichloroethane mg/kg wet0.0488 0.0050 0.05000 74-12798 1,1-Dichloroethylene mg/kg wet0.0526 0.0050 0.05000 67-149105 1,1-Dichloropropylene mg/kg wet0.0529 0.0050 0.05000 71-130106 1,2,3-Trichlorobenzene mg/kg wet0.0450 0.0050 0.05000 68-13090 1,2,3-Trichloropropane mg/kg wet0.0442 0.0050 0.05000 60-13788 1,2,4-Trichlorobenzene mg/kg wet0.0456 0.0050 0.05000 66-12591 1,2,4-Trimethylbenzene mg/kg wet0.0439 0.0050 0.05000 69-12988 1,2-Dibromoethane mg/kg wet0.0487 0.0050 0.05000 70-13297 1,2-Dichlorobenzene mg/kg wet0.0439 0.0050 0.05000 72-12388 1,2-Dichloroethane mg/kg wet0.0543 0.0050 0.05000 68-128109 1,2-Dichloropropane mg/kg wet0.0543 0.0050 0.05000 73-130109 1,3,5-Trimethylbenzene mg/kg wet0.0425 0.0050 0.05000 69-12885 1,3-Dichlorobenzene mg/kg wet0.0431 0.0050 0.05000 71-12086 1,3-Dichloropropane mg/kg wet0.0502 0.0050 0.05000 75-124100 1,4-Dichlorobenzene mg/kg wet0.0438 0.0050 0.05000 71-12388 2,2-Dichloropropane mg/kg wet0.0510 0.0050 0.05000 50-142102 2-Chlorotoluene mg/kg wet0.0418 0.0050 0.05000 67-12484 4-Chlorotoluene mg/kg wet0.0432 0.0050 0.05000 71-12686 4-Isopropyltoluene mg/kg wet0.0422 0.0050 0.05000 68-12984 Acetone mg/kg wet0.102 0.050 0.1000 29-198102 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 41 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P8I0106 - 5035 LCS (P8I0106-BS1)Prepared & Analyzed: 09/10/18 Benzene mg/kg wet0.0536 0.0030 0.05000 74-127107 Bromobenzene mg/kg wet0.0420 0.0050 0.05000 73-12584 Bromochloromethane mg/kg wet0.0556 0.0050 0.05000 72-134111 Bromodichloromethane mg/kg wet0.0574 0.0050 0.05000 75-122115 Bromoform mg/kg wet0.0616 0.0050 0.05000 66-135123 Bromomethane mg/kg wet0.0428 0.010 0.05000 20-18086 Carbon Tetrachloride mg/kg wet0.0541 0.0050 0.05000 64-143108 Chlorobenzene mg/kg wet0.0482 0.0050 0.05000 74-11896 Chloroethane mg/kg wet0.0402 0.010 0.05000 33-14980 Chloroform mg/kg wet0.0527 0.0050 0.05000 73-127105 Chloromethane mg/kg wet0.0437 0.0050 0.05000 45-14387 cis-1,2-Dichloroethylene mg/kg wet0.0517 0.0050 0.05000 76-134103 cis-1,3-Dichloropropylene mg/kg wet0.0553 0.0050 0.05000 71-125111 Dibromochloromethane mg/kg wet0.0561 0.0050 0.05000 73-122112 Dichlorodifluoromethane mg/kg wet0.0300 0.0050 0.05000 Aa26-14660 Ethylbenzene mg/kg wet0.0487 0.0050 0.05000 74-12897 Isopropyl Ether mg/kg wet0.0547 0.0050 0.05000 59-159109 Isopropylbenzene (Cumene)mg/kg wet0.0428 0.0050 0.05000 68-12686 m,p-Xylenes mg/kg wet0.0979 0.010 0.1000 75-12498 Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0503 0.050 0.05000 61-157101 Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0528 0.10 0.05000 J63-149106 Methyl Isobutyl Ketone mg/kg wet0.0556 0.050 0.05000 57-162111 Methylene Chloride mg/kg wet0.0513 0.010 0.05000 74-129103 Methyl-tert-Butyl Ether mg/kg wet0.0524 0.010 0.05000 70-130105 Naphthalene mg/kg wet0.0449 0.010 0.05000 57-15790 n-Butylbenzene mg/kg wet0.0432 0.0050 0.05000 65-13586 n-Propylbenzene mg/kg wet0.0434 0.0050 0.05000 67-13087 o-Xylene mg/kg wet0.0485 0.0050 0.05000 74-12697 sec-Butylbenzene mg/kg wet0.0431 0.0050 0.05000 66-13186 Styrene mg/kg wet0.0490 0.0050 0.05000 77-12198 tert-Butylbenzene mg/kg wet0.0427 0.0050 0.05000 67-13285 Tetrachloroethylene mg/kg wet0.0505 0.0050 0.05000 68-130101 Toluene mg/kg wet0.0530 0.0050 0.05000 71-129106 trans-1,2-Dichloroethylene mg/kg wet0.0523 0.0050 0.05000 73-132105 trans-1,3-Dichloropropylene mg/kg wet0.0557 0.0050 0.05000 68-123111 Trichloroethylene mg/kg wet0.0538 0.0050 0.05000 75-133108 Trichlorofluoromethane mg/kg wet0.0425 0.0050 0.05000 44-14685 Vinyl acetate mg/kg wet0.0483 0.025 0.05000 85-16197 Vinyl chloride mg/kg wet0.0448 0.0050 0.05000 48-14790 Xylenes, total mg/kg wet0.146 0.015 0.1500 74-12698 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9446.8 ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9949.3 ug/L 50.00 76-129Surrogate: Toluene-d8 8843.9 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 42 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P8I0106 - 5035 LCS Dup (P8I0106-BSD1)Prepared & Analyzed: 09/10/18 1,1,1,2-Tetrachloroethane mg/kg wet0.0525 0.0050 0.05000 2072-115105 0.9 1,1,1-Trichloroethane mg/kg wet0.0494 0.0050 0.05000 2067-13199 2 1,1,2,2-Tetrachloroethane mg/kg wet0.0478 0.0050 0.05000 2056-12696 3 1,1,2-Trichloroethane mg/kg wet0.0516 0.0050 0.05000 2070-133103 3 1,1-Dichloroethane mg/kg wet0.0479 0.0050 0.05000 2074-12796 2 1,1-Dichloroethylene mg/kg wet0.0503 0.0050 0.05000 2067-149101 4 1,1-Dichloropropylene mg/kg wet0.0512 0.0050 0.05000 2071-130102 3 1,2,3-Trichlorobenzene mg/kg wet0.0449 0.0050 0.05000 2068-13090 0.09 1,2,3-Trichloropropane mg/kg wet0.0458 0.0050 0.05000 2060-13792 4 1,2,4-Trichlorobenzene mg/kg wet0.0446 0.0050 0.05000 2066-12589 2 1,2,4-Trimethylbenzene mg/kg wet0.0432 0.0050 0.05000 2069-12986 2 1,2-Dibromoethane mg/kg wet0.0501 0.0050 0.05000 2070-132100 3 1,2-Dichlorobenzene mg/kg wet0.0432 0.0050 0.05000 2072-12386 2 1,2-Dichloroethane mg/kg wet0.0542 0.0050 0.05000 2068-128108 0.2 1,2-Dichloropropane mg/kg wet0.0540 0.0050 0.05000 2073-130108 0.6 1,3,5-Trimethylbenzene mg/kg wet0.0417 0.0050 0.05000 2069-12883 2 1,3-Dichlorobenzene mg/kg wet0.0422 0.0050 0.05000 2071-12084 2 1,3-Dichloropropane mg/kg wet0.0512 0.0050 0.05000 2075-124102 2 1,4-Dichlorobenzene mg/kg wet0.0432 0.0050 0.05000 2071-12386 1 2,2-Dichloropropane mg/kg wet0.0494 0.0050 0.05000 2050-14299 3 2-Chlorotoluene mg/kg wet0.0407 0.0050 0.05000 2067-12481 3 4-Chlorotoluene mg/kg wet0.0425 0.0050 0.05000 2071-12685 2 4-Isopropyltoluene mg/kg wet0.0413 0.0050 0.05000 2068-12983 2 Acetone mg/kg wet0.109 0.050 0.1000 2029-198109 7 Benzene mg/kg wet0.0527 0.0030 0.05000 2074-127105 2 Bromobenzene mg/kg wet0.0413 0.0050 0.05000 2073-12583 2 Bromochloromethane mg/kg wet0.0557 0.0050 0.05000 2072-134111 0.2 Bromodichloromethane mg/kg wet0.0569 0.0050 0.05000 2075-122114 0.9 Bromoform mg/kg wet0.0631 0.0050 0.05000 2066-135126 2 Bromomethane mg/kg wet0.0425 0.010 0.05000 2020-18085 0.8 Carbon Tetrachloride mg/kg wet0.0526 0.0050 0.05000 2064-143105 3 Chlorobenzene mg/kg wet0.0482 0.0050 0.05000 2074-11896 0.04 Chloroethane mg/kg wet0.0391 0.010 0.05000 2033-14978 3 Chloroform mg/kg wet0.0521 0.0050 0.05000 2073-127104 1 Chloromethane mg/kg wet0.0410 0.0050 0.05000 2045-14382 6 cis-1,2-Dichloroethylene mg/kg wet0.0510 0.0050 0.05000 2076-134102 1 cis-1,3-Dichloropropylene mg/kg wet0.0550 0.0050 0.05000 2071-125110 0.4 Dibromochloromethane mg/kg wet0.0571 0.0050 0.05000 2073-122114 2 Dichlorodifluoromethane mg/kg wet0.0292 0.0050 0.05000 20 Aa26-14658 3 Ethylbenzene mg/kg wet0.0484 0.0050 0.05000 2074-12897 0.6 Isopropyl Ether mg/kg wet0.0544 0.0050 0.05000 2059-159109 0.5 Isopropylbenzene (Cumene)mg/kg wet0.0420 0.0050 0.05000 2068-12684 2 m,p-Xylenes mg/kg wet0.0976 0.010 0.1000 2075-12498 0.3 Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0547 0.050 0.05000 2061-157109 8 Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0566 0.10 0.05000 20 J63-149113 7 Methyl Isobutyl Ketone mg/kg wet0.0588 0.050 0.05000 2057-162118 6 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 43 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P8I0106 - 5035 LCS Dup (P8I0106-BSD1)Prepared & Analyzed: 09/10/18 Methylene Chloride mg/kg wet0.0508 0.010 0.05000 2074-129102 0.9 Methyl-tert-Butyl Ether mg/kg wet0.0583 0.010 0.05000 2070-130117 11 Naphthalene mg/kg wet0.0456 0.010 0.05000 2057-15791 2 n-Butylbenzene mg/kg wet0.0422 0.0050 0.05000 2065-13584 2 n-Propylbenzene mg/kg wet0.0425 0.0050 0.05000 2067-13085 2 o-Xylene mg/kg wet0.0485 0.0050 0.05000 2074-12697 0.1 sec-Butylbenzene mg/kg wet0.0421 0.0050 0.05000 2066-13184 2 Styrene mg/kg wet0.0491 0.0050 0.05000 2077-12198 0.1 tert-Butylbenzene mg/kg wet0.0417 0.0050 0.05000 2067-13283 2 Tetrachloroethylene mg/kg wet0.0494 0.0050 0.05000 2068-13099 2 Toluene mg/kg wet0.0523 0.0050 0.05000 2071-129105 1 trans-1,2-Dichloroethylene mg/kg wet0.0514 0.0050 0.05000 2073-132103 2 trans-1,3-Dichloropropylene mg/kg wet0.0560 0.0050 0.05000 2068-123112 0.5 Trichloroethylene mg/kg wet0.0530 0.0050 0.05000 2075-133106 2 Trichlorofluoromethane mg/kg wet0.0408 0.0050 0.05000 2044-14682 4 Vinyl acetate mg/kg wet0.0507 0.025 0.05000 2085-161101 5 Vinyl chloride mg/kg wet0.0434 0.0050 0.05000 2048-14787 3 Xylenes, total mg/kg wet0.146 0.015 0.1500 2074-12697 0.2 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9346.4 ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10049.9 ug/L 50.00 76-129Surrogate: Toluene-d8 8944.7 Matrix Spike (P8I0106-MS1)Prepared & Analyzed: 09/10/18 Source: 8090062-01 1,1,1,2-Tetrachloroethane mg/kg dry0.0381 0.0057 0.05662 BRL 60-12067 1,1,1-Trichloroethane mg/kg dry0.0380 0.0057 0.05662 BRL 52-13967 1,1,2,2-Tetrachloroethane mg/kg dry0.0345 0.0057 0.05662 BRL 39-13561 1,1,2-Trichloroethane mg/kg dry0.0377 0.0057 0.05662 BRL 44-14067 1,1-Dichloroethane mg/kg dry0.0369 0.0057 0.05662 BRL 59-13765 1,1-Dichloroethylene mg/kg dry0.0393 0.0057 0.05662 BRL 54-16269 1,1-Dichloropropylene mg/kg dry0.0389 0.0057 0.05662 BRL 55-13769 1,2,3-Trichlorobenzene mg/kg dry0.0275 0.0057 0.05662 BRL 34-12049 1,2,3-Trichloropropane mg/kg dry0.0341 0.0057 0.05662 BRL 45-13960 1,2,4-Trichlorobenzene mg/kg dry0.0271 0.0057 0.05662 BRL 35-11648 1,2,4-Trimethylbenzene mg/kg dry0.0302 0.0057 0.05662 BRL 38-14253 1,2-Dibromoethane mg/kg dry0.0365 0.0057 0.05662 BRL 49-13264 1,2-Dichlorobenzene mg/kg dry0.0303 0.0057 0.05662 BRL 42-13053 1,2-Dichloroethane mg/kg dry0.0409 0.0057 0.05662 BRL 51-13172 1,2-Dichloropropane mg/kg dry0.0401 0.0057 0.05662 BRL 55-13871 1,3,5-Trimethylbenzene mg/kg dry0.0294 0.0057 0.05662 BRL 44-14052 1,3-Dichlorobenzene mg/kg dry0.0295 0.0057 0.05662 BRL 41-12952 1,3-Dichloropropane mg/kg dry0.0369 0.0057 0.05662 BRL 53-12965 1,4-Dichlorobenzene mg/kg dry0.0299 0.0057 0.05662 BRL 44-13453 2,2-Dichloropropane mg/kg dry0.0371 0.0057 0.05662 BRL 30-14766 2-Chlorotoluene mg/kg dry0.0288 0.0057 0.05662 BRL 46-13251 4-Chlorotoluene mg/kg dry0.0295 0.0057 0.05662 BRL 44-13552 4-Isopropyltoluene mg/kg dry0.0284 0.0057 0.05662 BRL 32-14450 Acetone mg/kg dry0.0885 0.057 0.1132 0.0570 M34-14328 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 44 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P8I0106 - 5035 Matrix Spike (P8I0106-MS1)Prepared & Analyzed: 09/10/18 Source: 8090062-01 Benzene mg/kg dry0.0400 0.0034 0.05662 BRL 60-13571 Bromobenzene mg/kg dry0.0294 0.0057 0.05662 BRL 45-13552 Bromochloromethane mg/kg dry0.0422 0.0057 0.05662 BRL 55-13675 Bromodichloromethane mg/kg dry0.0428 0.0057 0.05662 BRL 55-12776 Bromoform mg/kg dry0.0457 0.0057 0.05662 BRL 40-13681 Bromomethane mg/kg dry0.0329 0.011 0.05662 BRL 30-13758 Carbon Tetrachloride mg/kg dry0.0412 0.0057 0.05662 BRL 48-15373 Chlorobenzene mg/kg dry0.0348 0.0057 0.05662 BRL 57-12561 Chloroethane mg/kg dry0.0398 0.011 0.05662 BRL 16-17770 Chloroform mg/kg dry0.0392 0.0057 0.05662 BRL 56-13769 Chloromethane mg/kg dry0.0401 0.0057 0.05662 BRL 40-14571 cis-1,2-Dichloroethylene mg/kg dry0.0386 0.0057 0.05662 BRL 58-14068 cis-1,3-Dichloropropylene mg/kg dry0.0384 0.0057 0.05662 BRL 42-13568 Dibromochloromethane mg/kg dry0.0411 0.0057 0.05662 BRL 49-12773 Dichlorodifluoromethane mg/kg dry0.0399 0.0057 0.05662 BRL 25-15170 Ethylbenzene mg/kg dry0.0349 0.0057 0.05662 BRL 44-14462 Isopropyl Ether mg/kg dry0.0390 0.0057 0.05662 BRL 51-15569 Isopropylbenzene (Cumene)mg/kg dry0.0299 0.0057 0.05662 BRL 41-14053 m,p-Xylenes mg/kg dry0.0703 0.011 0.1132 BRL 36-14862 Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0375 0.057 0.05662 BRL J30-14766 Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0430 0.11 0.05662 BRL J24-16076 Methyl Isobutyl Ketone mg/kg dry0.0424 0.057 0.05662 BRL J25-16375 Methylene Chloride mg/kg dry0.0423 0.011 0.05662 BRL 53-14475 Methyl-tert-Butyl Ether mg/kg dry0.0392 0.011 0.05662 BRL 49-13569 Naphthalene mg/kg dry0.0294 0.011 0.05662 BRL 32-12752 n-Butylbenzene mg/kg dry0.0279 0.0057 0.05662 BRL 23-14849 n-Propylbenzene mg/kg dry0.0299 0.0057 0.05662 BRL 35-14453 o-Xylene mg/kg dry0.0347 0.0057 0.05662 BRL 43-14361 sec-Butylbenzene mg/kg dry0.0296 0.0057 0.05662 BRL 34-14452 Styrene mg/kg dry0.0344 0.0057 0.05662 BRL 42-13261 tert-Butylbenzene mg/kg dry0.0297 0.0057 0.05662 BRL 36-15053 Tetrachloroethylene mg/kg dry0.0365 0.0057 0.05662 BRL 47-14264 Toluene mg/kg dry0.0391 0.0057 0.05662 BRL 57-13569 trans-1,2-Dichloroethylene mg/kg dry0.0394 0.0057 0.05662 BRL 58-14170 trans-1,3-Dichloropropylene mg/kg dry0.0396 0.0057 0.05662 BRL 41-12470 Trichloroethylene mg/kg dry0.0410 0.0057 0.05662 0.00603 38-16462 Trichlorofluoromethane mg/kg dry0.0434 0.0057 0.05662 0.0359 M30-15713 Vinyl acetate mg/kg dry0.0113 0.028 0.05662 BRL M, J61-15420 Vinyl chloride mg/kg dry0.0465 0.0057 0.05662 BRL 40-15682 Xylenes, total mg/kg dry0.105 0.017 0.1698 BRL 36-14862 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9547.6 ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10250.9 ug/L 50.00 76-129Surrogate: Toluene-d8 8944.6 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 45 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P8I0106 - 5035 Matrix Spike Dup (P8I0106-MSD1)Prepared & Analyzed: 09/10/18 Source: 8090062-01 1,1,1,2-Tetrachloroethane mg/kg dry0.0417 0.0058 0.05794 BRL 1560-12072 9 1,1,1-Trichloroethane mg/kg dry0.0436 0.0058 0.05794 BRL 2152-13975 14 1,1,2,2-Tetrachloroethane mg/kg dry0.0357 0.0058 0.05794 BRL 2239-13562 3 1,1,2-Trichloroethane mg/kg dry0.0401 0.0058 0.05794 BRL 2144-14069 6 1,1-Dichloroethane mg/kg dry0.0411 0.0058 0.05794 BRL 2159-13771 11 1,1-Dichloroethylene mg/kg dry0.0453 0.0058 0.05794 BRL 2254-16278 14 1,1-Dichloropropylene mg/kg dry0.0444 0.0058 0.05794 BRL 1955-13777 13 1,2,3-Trichlorobenzene mg/kg dry0.0294 0.0058 0.05794 BRL 4134-12051 7 1,2,3-Trichloropropane mg/kg dry0.0348 0.0058 0.05794 BRL 2545-13960 2 1,2,4-Trichlorobenzene mg/kg dry0.0291 0.0058 0.05794 BRL 6235-11650 7 1,2,4-Trimethylbenzene mg/kg dry0.0340 0.0058 0.05794 BRL 2438-14259 12 1,2-Dibromoethane mg/kg dry0.0377 0.0058 0.05794 BRL 1549-13265 3 1,2-Dichlorobenzene mg/kg dry0.0330 0.0058 0.05794 BRL 2142-13057 9 1,2-Dichloroethane mg/kg dry0.0432 0.0058 0.05794 BRL 1351-13175 5 1,2-Dichloropropane mg/kg dry0.0440 0.0058 0.05794 BRL 1655-13876 9 1,3,5-Trimethylbenzene mg/kg dry0.0336 0.0058 0.05794 BRL 2944-14058 13 1,3-Dichlorobenzene mg/kg dry0.0324 0.0058 0.05794 BRL 2441-12956 9 1,3-Dichloropropane mg/kg dry0.0392 0.0058 0.05794 BRL 1553-12968 6 1,4-Dichlorobenzene mg/kg dry0.0324 0.0058 0.05794 BRL 2144-13456 8 2,2-Dichloropropane mg/kg dry0.0424 0.0058 0.05794 BRL 2030-14773 13 2-Chlorotoluene mg/kg dry0.0326 0.0058 0.05794 BRL 2946-13256 12 4-Chlorotoluene mg/kg dry0.0330 0.0058 0.05794 BRL 2344-13557 11 4-Isopropyltoluene mg/kg dry0.0324 0.0058 0.05794 BRL 2232-14456 13 Acetone mg/kg dry0.0821 0.058 0.1159 0.0570 49 M34-14322 7 Benzene mg/kg dry0.0447 0.0035 0.05794 BRL 2060-13577 11 Bromobenzene mg/kg dry0.0325 0.0058 0.05794 BRL 2545-13556 10 Bromochloromethane mg/kg dry0.0448 0.0058 0.05794 BRL 1855-13677 6 Bromodichloromethane mg/kg dry0.0464 0.0058 0.05794 BRL 1755-12780 8 Bromoform mg/kg dry0.0482 0.0058 0.05794 BRL 3540-13683 5 Bromomethane mg/kg dry0.0420 0.012 0.05794 BRL 3030-13772 24 Carbon Tetrachloride mg/kg dry0.0469 0.0058 0.05794 BRL 2348-15381 13 Chlorobenzene mg/kg dry0.0388 0.0058 0.05794 BRL 1457-12567 11 Chloroethane mg/kg dry0.0443 0.012 0.05794 BRL 4716-17776 11 Chloroform mg/kg dry0.0436 0.0058 0.05794 BRL 1856-13775 11 Chloromethane mg/kg dry0.0454 0.0058 0.05794 BRL 2640-14578 12 cis-1,2-Dichloroethylene mg/kg dry0.0426 0.0058 0.05794 BRL 2858-14074 10 cis-1,3-Dichloropropylene mg/kg dry0.0424 0.0058 0.05794 BRL 3242-13573 10 Dibromochloromethane mg/kg dry0.0444 0.0058 0.05794 BRL 2449-12777 8 Dichlorodifluoromethane mg/kg dry0.0456 0.0058 0.05794 BRL 3725-15179 13 Ethylbenzene mg/kg dry0.0395 0.0058 0.05794 BRL 1944-14468 12 Isopropyl Ether mg/kg dry0.0433 0.0058 0.05794 BRL 1351-15575 10 Isopropylbenzene (Cumene)mg/kg dry0.0345 0.0058 0.05794 BRL 2741-14059 14 m,p-Xylenes mg/kg dry0.0788 0.012 0.1159 BRL 2036-14868 11 Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0374 0.058 0.05794 BRL 42 J30-14765 0.4 Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0417 0.12 0.05794 BRL 42 J24-16072 3 Methyl Isobutyl Ketone mg/kg dry0.0422 0.058 0.05794 BRL 44 J25-16373 0.3 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 46 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P8I0106 - 5035 Matrix Spike Dup (P8I0106-MSD1)Prepared & Analyzed: 09/10/18 Source: 8090062-01 Methylene Chloride mg/kg dry0.0457 0.012 0.05794 BRL 1453-14479 8 Methyl-tert-Butyl Ether mg/kg dry0.0380 0.012 0.05794 BRL 2249-13566 3 Naphthalene mg/kg dry0.0304 0.012 0.05794 BRL 4432-12753 3 n-Butylbenzene mg/kg dry0.0317 0.0058 0.05794 BRL 3923-14855 13 n-Propylbenzene mg/kg dry0.0342 0.0058 0.05794 BRL 2735-14459 13 o-Xylene mg/kg dry0.0388 0.0058 0.05794 BRL 1743-14367 11 sec-Butylbenzene mg/kg dry0.0339 0.0058 0.05794 BRL 2834-14458 14 Styrene mg/kg dry0.0383 0.0058 0.05794 BRL 2842-13266 11 tert-Butylbenzene mg/kg dry0.0341 0.0058 0.05794 BRL 2936-15059 14 Tetrachloroethylene mg/kg dry0.0424 0.0058 0.05794 BRL 2647-14273 15 Toluene mg/kg dry0.0437 0.0058 0.05794 BRL 2257-13575 11 trans-1,2-Dichloroethylene mg/kg dry0.0446 0.0058 0.05794 BRL 1858-14177 12 trans-1,3-Dichloropropylene mg/kg dry0.0418 0.0058 0.05794 BRL 2041-12472 6 Trichloroethylene mg/kg dry0.0460 0.0058 0.05794 0.00603 1838-16469 11 Trichlorofluoromethane mg/kg dry0.0487 0.0058 0.05794 0.0359 27 M30-15722 12 Vinyl acetate mg/kg dry0.0127 0.029 0.05794 BRL 35 M, J61-15422 12 Vinyl chloride mg/kg dry0.0524 0.0058 0.05794 BRL 3540-15691 12 Xylenes, total mg/kg dry0.118 0.017 0.1738 BRL 2036-14868 11 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9547.6 ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10150.6 ug/L 50.00 76-129Surrogate: Toluene-d8 9045.0 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 47 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS Blank (P8I0057-BLK1)Prepared: 09/06/18 Analyzed: 09/11/18 1,2,4-Trichlorobenzene ug/LBRL10 1,2-Dichlorobenzene ug/LBRL10 1,3-Dichlorobenzene ug/LBRL10 1,4-Dichlorobenzene ug/LBRL10 1-Methylnaphthalene ug/LBRL10 2,4,5-Trichlorophenol ug/LBRL10 2,4,6-Trichlorophenol ug/LBRL10 2,4-Dichlorophenol ug/LBRL10 2,4-Dimethylphenol ug/LBRL10 2,4-Dinitrophenol ug/LBRL10 2,4-Dinitrotoluene ug/LBRL10 2,6-Dinitrotoluene ug/LBRL10 2-Chloronaphthalene ug/LBRL10 2-Chlorophenol ug/LBRL10 2-Methylnaphthalene ug/LBRL10 2-Methylphenol ug/LBRL10 2-Nitroaniline ug/LBRL10 2-Nitrophenol ug/LBRL10 3,3’-Dichlorobenzidine ug/LBRL10 3/4-Methylphenol ug/LBRL10 3-Nitroaniline ug/LBRL10 4,6-Dinitro-2-methylphenol ug/LBRL10 4-Bromophenyl phenyl ether ug/LBRL10 4-Chloro-3-methylphenol ug/LBRL10 4-Chloroaniline ug/LBRL10 4-Chlorophenyl phenyl ether ug/LBRL10 4-Nitroaniline ug/LBRL10 4-Nitrophenol ug/LBRL10 Acenaphthene ug/LBRL10 Acenaphthylene ug/LBRL10 Aniline ug/LBRL10 Anthracene ug/LBRL10 Azobenzene ug/LBRL10 Benzo(a)anthracene ug/LBRL10 Benzo(a)pyrene ug/LBRL10 Benzo(b)fluoranthene ug/LBRL10 Benzo(g,h,i)perylene ug/LBRL10 Benzo(k)fluoranthene ug/LBRL10 Benzoic Acid ug/LBRL100 Benzyl alcohol ug/LBRL10 bis(2-Chloroethoxy)methane ug/LBRL10 Bis(2-Chloroethyl)ether ug/LBRL10 Bis(2-chloroisopropyl)ether ug/LBRL10 Bis(2-Ethylhexyl)phthalate ug/LBRL10 Butyl benzyl phthalate ug/LBRL10 Chrysene ug/LBRL10 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 48 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS Blank (P8I0057-BLK1)Prepared: 09/06/18 Analyzed: 09/11/18 Dibenzo(a,h)anthracene ug/LBRL10 Dibenzofuran ug/LBRL10 Diethyl phthalate ug/LBRL10 Dimethyl phthalate ug/LBRL10 Di-n-butyl phthalate ug/LBRL10 Di-n-octyl phthalate ug/LBRL10 Fluoranthene ug/LBRL10 Fluorene ug/LBRL10 Hexachlorobenzene ug/LBRL10 Hexachlorobutadiene ug/LBRL10 Hexachlorocyclopentadiene ug/LBRL10 Hexachloroethane ug/LBRL10 Indeno(1,2,3-cd)pyrene ug/LBRL10 Isophorone ug/LBRL10 Naphthalene ug/LBRL10 Nitrobenzene ug/LBRL10 N-Nitroso-di-n-propylamine ug/LBRL10 N-Nitrosodiphenylamine ug/LBRL10 Pentachlorophenol ug/LBRL10 Phenanthrene ug/LBRL10 Phenol ug/LBRL10 Pyrene ug/LBRL10 ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 8383.4 ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8441.9 ug/L 100.0 19-119Surrogate: 2-Fluorophenol 8787.4 ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7336.6 ug/L 100.0 SR11-52Surrogate: Phenol-d5 8281.8 ug/L 50.00 50-134Surrogate: Terphenyl-d14 8040.1 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 49 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS LCS (P8I0057-BS1)Prepared: 09/06/18 Analyzed: 09/10/18 1,2,4-Trichlorobenzene ug/L28.2 10 50.00 29-12656 1,2-Dichlorobenzene ug/L27.5 10 50.00 32-11155 1,3-Dichlorobenzene ug/L25.0 10 50.00 28-11050 1,4-Dichlorobenzene ug/L26.2 10 50.00 29-11252 1-Methylnaphthalene ug/L34.8 10 50.00 41-11970 2,4,5-Trichlorophenol ug/L40.9 10 50.00 53-12382 2,4,6-Trichlorophenol ug/L37.5 10 50.00 50-12575 2,4-Dichlorophenol ug/L34.6 10 50.00 47-12169 2,4-Dimethylphenol ug/L25.8 10 50.00 31-12452 2,4-Dinitrophenol ug/L22.1 10 50.00 23-14344 2,4-Dinitrotoluene ug/L41.5 10 50.00 57-12883 2,6-Dinitrotoluene ug/L41.5 10 50.00 57-12483 2-Chloronaphthalene ug/L35.6 10 50.00 40-11671 2-Chlorophenol ug/L31.8 10 50.00 38-11764 2-Methylnaphthalene ug/L32.9 10 50.00 40-12166 2-Methylphenol ug/L29.3 10 50.00 30-11759 2-Nitroaniline ug/L41.3 10 50.00 55-12783 2-Nitrophenol ug/L34.8 10 50.00 47-12370 3,3’-Dichlorobenzidine ug/L40.8 10 50.00 27-12982 3/4-Methylphenol ug/L24.8 10 50.00 29-11050 3-Nitroaniline ug/L41.4 10 50.00 41-12883 4,6-Dinitro-2-methylphenol ug/L15.4 10 50.00 L44-13731 4-Bromophenyl phenyl ether ug/L40.3 10 50.00 55-12481 4-Chloro-3-methylphenol ug/L36.4 10 50.00 52-11973 4-Chloroaniline ug/L41.6 10 50.00 33-11783 4-Chlorophenyl phenyl ether ug/L39.6 10 50.00 53-12179 4-Nitroaniline ug/L41.0 10 50.00 45-13582 4-Nitrophenol ug/L15.8 10 50.00 10-7732 Acenaphthene ug/L38.2 10 50.00 47-12276 Acenaphthylene ug/L41.4 10 50.00 41-13083 Aniline ug/L59.6 10 50.00 12-197119 Anthracene ug/L43.4 10 50.00 57-12387 Azobenzene ug/L38.0 10 50.00 61-11676 Benzo(a)anthracene ug/L42.2 10 50.00 58-12584 Benzo(a)pyrene ug/L42.2 10 50.00 54-12884 Benzo(b)fluoranthene ug/L42.5 10 50.00 53-13185 Benzo(g,h,i)perylene ug/L41.9 10 50.00 50-13484 Benzo(k)fluoranthene ug/L39.9 10 50.00 57-12980 Benzoic Acid ug/L16.8 100 50.00 J10-12534 Benzyl alcohol ug/L32.3 10 50.00 31-11265 bis(2-Chloroethoxy)methane ug/L39.4 10 50.00 48-12079 Bis(2-Chloroethyl)ether ug/L29.4 10 50.00 43-11859 Bis(2-chloroisopropyl)ether ug/L33.8 10 50.00 37-13068 Bis(2-Ethylhexyl)phthalate ug/L42.8 10 50.00 55-13586 Butyl benzyl phthalate ug/L41.6 10 50.00 53-13483 Chrysene ug/L41.2 10 50.00 59-12382 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 50 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS LCS (P8I0057-BS1)Prepared: 09/06/18 Analyzed: 09/10/18 Dibenzo(a,h)anthracene ug/L42.9 10 50.00 51-13486 Dibenzofuran ug/L39.9 10 50.00 53-11880 Diethyl phthalate ug/L42.3 10 50.00 56-12585 Dimethyl phthalate ug/L41.3 10 50.00 45-12783 Di-n-butyl phthalate ug/L42.1 10 50.00 59-12784 Di-n-octyl phthalate ug/L44.4 10 50.00 51-14089 Fluoranthene ug/L41.7 10 50.00 57-12883 Fluorene ug/L41.8 10 50.00 52-12484 Hexachlorobenzene ug/L39.7 10 50.00 53-12579 Hexachlorobutadiene ug/L28.2 10 50.00 22-12456 Hexachlorocyclopentadiene ug/L17.0 10 50.00 32-11734 Hexachloroethane ug/L23.8 10 50.00 21-11548 Indeno(1,2,3-cd)pyrene ug/L47.8 10 50.00 52-13496 Isophorone ug/L41.8 10 50.00 42-12484 Naphthalene ug/L33.5 10 50.00 40-12167 Nitrobenzene ug/L35.9 10 50.00 45-12172 N-Nitroso-di-n-propylamine ug/L34.2 10 50.00 49-11968 N-Nitrosodiphenylamine ug/L47.8 10 50.00 51-12396 Pentachlorophenol ug/L39.1 10 50.00 35-13878 Phenanthrene ug/L42.7 10 50.00 59-12085 Phenol ug/L18.0 10 50.00 12-5836 Pyrene ug/L41.5 10 50.00 57-12683 ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 7675.8 ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7336.7 ug/L 100.0 19-119Surrogate: 2-Fluorophenol 4746.9 ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7034.8 ug/L 100.0 11-52Surrogate: Phenol-d5 2828.1 ug/L 50.00 50-134Surrogate: Terphenyl-d14 7738.3 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 51 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS LCS Dup (P8I0057-BSD1)Prepared: 09/06/18 Analyzed: 09/10/18 1,2,4-Trichlorobenzene ug/L35.9 10 50.00 20 D29-12672 24 1,2-Dichlorobenzene ug/L32.4 10 50.00 2032-11165 16 1,3-Dichlorobenzene ug/L30.2 10 50.00 2028-11060 19 1,4-Dichlorobenzene ug/L31.6 10 50.00 2029-11263 19 1-Methylnaphthalene ug/L42.4 10 50.00 2041-11985 20 2,4,5-Trichlorophenol ug/L50.7 10 50.00 20 D53-123101 22 2,4,6-Trichlorophenol ug/L49.1 10 50.00 20 D50-12598 27 2,4-Dichlorophenol ug/L44.0 10 50.00 20 D47-12188 24 2,4-Dimethylphenol ug/L30.0 10 50.00 2031-12460 15 2,4-Dinitrophenol ug/L24.4 10 50.00 2023-14349 10 2,4-Dinitrotoluene ug/L50.3 10 50.00 2057-128101 19 2,6-Dinitrotoluene ug/L50.3 10 50.00 2057-124101 19 2-Chloronaphthalene ug/L44.9 10 50.00 20 D40-11690 23 2-Chlorophenol ug/L40.9 10 50.00 20 D38-11782 25 2-Methylnaphthalene ug/L40.3 10 50.00 2040-12181 20 2-Methylphenol ug/L36.8 10 50.00 20 D30-11774 23 2-Nitroaniline ug/L51.2 10 50.00 20 D55-127102 21 2-Nitrophenol ug/L44.3 10 50.00 20 D47-12389 24 3,3’-Dichlorobenzidine ug/L50.8 10 50.00 20 D27-129102 22 3/4-Methylphenol ug/L31.1 10 50.00 20 D29-11062 22 3-Nitroaniline ug/L51.1 10 50.00 20 D41-128102 21 4,6-Dinitro-2-methylphenol ug/L21.1 10 50.00 20 D, L44-13742 31 4-Bromophenyl phenyl ether ug/L50.1 10 50.00 20 D55-124100 22 4-Chloro-3-methylphenol ug/L44.4 10 50.00 2052-11989 20 4-Chloroaniline ug/L50.3 10 50.00 2033-117101 19 4-Chlorophenyl phenyl ether ug/L48.4 10 50.00 2053-12197 20 4-Nitroaniline ug/L49.2 10 50.00 2045-13598 18 4-Nitrophenol ug/L20.7 10 50.00 20 D10-7741 27 Acenaphthene ug/L48.2 10 50.00 20 D47-12296 23 Acenaphthylene ug/L50.4 10 50.00 2041-130101 19 Aniline ug/L79.2 10 50.00 20 D12-197158 28 Anthracene ug/L52.5 10 50.00 2057-123105 19 Azobenzene ug/L46.8 10 50.00 20 D61-11694 21 Benzo(a)anthracene ug/L49.5 10 50.00 2058-12599 16 Benzo(a)pyrene ug/L52.0 10 50.00 20 D54-128104 21 Benzo(b)fluoranthene ug/L49.0 10 50.00 2053-13198 14 Benzo(g,h,i)perylene ug/L51.2 10 50.00 2050-134102 20 Benzo(k)fluoranthene ug/L51.2 10 50.00 20 D57-129102 25 Benzoic Acid ug/L17.7 100 50.00 20 J10-12535 5 Benzyl alcohol ug/L42.4 10 50.00 20 D31-11285 27 bis(2-Chloroethoxy)methane ug/L49.3 10 50.00 20 D48-12099 22 Bis(2-Chloroethyl)ether ug/L38.6 10 50.00 20 D43-11877 27 Bis(2-chloroisopropyl)ether ug/L42.8 10 50.00 20 D37-13086 23 Bis(2-Ethylhexyl)phthalate ug/L50.8 10 50.00 2055-135102 17 Butyl benzyl phthalate ug/L49.1 10 50.00 2053-13498 17 Chrysene ug/L49.3 10 50.00 2059-12399 18 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 52 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS LCS Dup (P8I0057-BSD1)Prepared: 09/06/18 Analyzed: 09/10/18 Dibenzo(a,h)anthracene ug/L52.1 10 50.00 2051-134104 19 Dibenzofuran ug/L48.5 10 50.00 2053-11897 19 Diethyl phthalate ug/L51.6 10 50.00 2056-125103 20 Dimethyl phthalate ug/L51.0 10 50.00 20 D45-127102 21 Di-n-butyl phthalate ug/L50.8 10 50.00 2059-127102 19 Di-n-octyl phthalate ug/L53.8 10 50.00 2051-140108 19 Fluoranthene ug/L49.8 10 50.00 2057-128100 18 Fluorene ug/L51.6 10 50.00 20 D52-124103 21 Hexachlorobenzene ug/L49.1 10 50.00 20 D53-12598 21 Hexachlorobutadiene ug/L34.2 10 50.00 2022-12468 19 Hexachlorocyclopentadiene ug/L18.6 10 50.00 2032-11737 9 Hexachloroethane ug/L28.2 10 50.00 2021-11556 17 Indeno(1,2,3-cd)pyrene ug/L58.2 10 50.00 2052-134116 20 Isophorone ug/L51.3 10 50.00 2042-124103 20 Naphthalene ug/L40.7 10 50.00 2040-12181 20 Nitrobenzene ug/L44.0 10 50.00 20 D45-12188 20 N-Nitroso-di-n-propylamine ug/L44.6 10 50.00 2049-11989 26 N-Nitrosodiphenylamine ug/L58.1 10 50.00 2051-123116 19 Pentachlorophenol ug/L45.6 10 50.00 2035-13891 15 Phenanthrene ug/L51.5 10 50.00 2059-120103 19 Phenol ug/L21.6 10 50.00 2012-5843 18 Pyrene ug/L50.3 10 50.00 2057-126101 19 ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 9796.8 ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8944.4 ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5958.7 ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 8743.3 ug/L 100.0 11-52Surrogate: Phenol-d5 3535.4 ug/L 50.00 50-134Surrogate: Terphenyl-d14 9145.3 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 53 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS Matrix Spike (P8I0057-MS1)Prepared: 09/07/18 Analyzed: 09/10/18 Source: 8090062-10 1,2,4-Trichlorobenzene ug/L36.9 10 50.00 BRL 29-11674 1,2-Dichlorobenzene ug/L33.4 10 50.00 BRL 32-11167 1,3-Dichlorobenzene ug/L32.1 10 50.00 BRL 28-11064 1,4-Dichlorobenzene ug/L33.0 10 50.00 BRL 29-11266 1-Methylnaphthalene ug/L44.6 10 50.00 BRL 41-11989 2,4,5-Trichlorophenol ug/L50.0 10 50.00 BRL 53-123100 2,4,6-Trichlorophenol ug/L48.5 10 50.00 BRL 50-12597 2,4-Dichlorophenol ug/L44.9 10 50.00 BRL 47-12190 2,4-Dimethylphenol ug/L29.9 10 50.00 BRL 31-12460 2,4-Dinitrophenol ug/L27.3 10 50.00 BRL 23-14355 2,4-Dinitrotoluene ug/L52.0 10 50.00 BRL 57-128104 2,6-Dinitrotoluene ug/L52.0 10 50.00 BRL 57-124104 2-Chloronaphthalene ug/L44.8 10 50.00 BRL 40-11690 2-Chlorophenol ug/L42.6 10 50.00 BRL 38-11785 2-Methylnaphthalene ug/L42.4 10 50.00 BRL 40-12185 2-Methylphenol ug/L41.8 10 50.00 BRL 30-11784 2-Nitroaniline ug/L49.4 10 50.00 BRL 55-12799 2-Nitrophenol ug/L46.1 10 50.00 BRL 47-12392 3,3’-Dichlorobenzidine ug/L50.5 10 50.00 BRL 27-129101 3/4-Methylphenol ug/L36.8 10 50.00 BRL 29-11074 3-Nitroaniline ug/L51.1 10 50.00 BRL 41-128102 4,6-Dinitro-2-methylphenol ug/L23.6 10 50.00 BRL 44-13747 4-Bromophenyl phenyl ether ug/L50.2 10 50.00 BRL 55-124100 4-Chloro-3-methylphenol ug/L45.6 10 50.00 BRL 52-11991 4-Chloroaniline ug/L48.8 10 50.00 BRL 33-11798 4-Chlorophenyl phenyl ether ug/L49.3 10 50.00 BRL 53-12199 4-Nitroaniline ug/L49.1 10 50.00 BRL 45-13598 4-Nitrophenol ug/L30.1 10 50.00 BRL 10-10560 Acenaphthene ug/L48.0 10 50.00 BRL 47-12296 Acenaphthylene ug/L50.8 10 50.00 BRL 41-130102 Aniline ug/L72.2 10 50.00 BRL M11-124144 Anthracene ug/L53.3 10 50.00 BRL 57-123107 Azobenzene ug/L47.5 10 50.00 BRL 61-11695 Benzo(a)anthracene ug/L51.8 10 50.00 BRL 58-125104 Benzo(a)pyrene ug/L53.8 10 50.00 BRL 54-128108 Benzo(b)fluoranthene ug/L50.0 10 50.00 BRL 53-131100 Benzo(g,h,i)perylene ug/L49.9 10 50.00 BRL 50-134100 Benzo(k)fluoranthene ug/L53.4 10 50.00 BRL 57-129107 Benzoic Acid ug/L29.8 100 50.00 BRL J10-12560 Benzyl alcohol ug/L46.2 10 50.00 BRL 31-11292 bis(2-Chloroethoxy)methane ug/L52.1 10 50.00 BRL 48-120104 Bis(2-Chloroethyl)ether ug/L39.3 10 50.00 BRL 43-11879 Bis(2-chloroisopropyl)ether ug/L42.8 10 50.00 BRL 37-13086 Bis(2-Ethylhexyl)phthalate ug/L52.3 10 50.00 BRL 55-135105 Butyl benzyl phthalate ug/L52.6 10 50.00 BRL 53-134105 Chrysene ug/L50.4 10 50.00 BRL 59-123101 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 54 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS Matrix Spike (P8I0057-MS1)Prepared: 09/07/18 Analyzed: 09/10/18 Source: 8090062-10 Dibenzo(a,h)anthracene ug/L53.4 10 50.00 BRL 51-134107 Dibenzofuran ug/L49.3 10 50.00 BRL 53-11899 Diethyl phthalate ug/L51.4 10 50.00 BRL 56-125103 Dimethyl phthalate ug/L50.4 10 50.00 BRL 45-127101 Di-n-butyl phthalate ug/L50.8 10 50.00 BRL 59-127102 Di-n-octyl phthalate ug/L55.0 10 50.00 BRL 51-140110 Fluoranthene ug/L50.7 10 50.00 BRL 57-128101 Fluorene ug/L51.1 10 50.00 BRL 52-124102 Hexachlorobenzene ug/L48.7 10 50.00 BRL 53-12597 Hexachlorobutadiene ug/L38.2 10 50.00 BRL 22-12476 Hexachlorocyclopentadiene ug/L20.0 10 50.00 BRL 26-12240 Hexachloroethane ug/L30.4 10 50.00 BRL 21-11561 Indeno(1,2,3-cd)pyrene ug/L57.7 10 50.00 BRL 52-134115 Isophorone ug/L52.2 10 50.00 BRL 42-124104 Naphthalene ug/L41.5 10 50.00 BRL 40-12183 Nitrobenzene ug/L45.5 10 50.00 BRL 45-12191 N-Nitroso-di-n-propylamine ug/L45.2 10 50.00 BRL 49-11990 N-Nitrosodiphenylamine ug/L59.7 10 50.00 BRL 51-123119 Pentachlorophenol ug/L47.1 10 50.00 BRL 35-13894 Phenanthrene ug/L51.8 10 50.00 BRL 59-120104 Phenol ug/L30.6 10 50.00 BRL 10-6861 Pyrene ug/L51.8 10 50.00 BRL 57-126104 ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 9898.4 ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8944.4 ug/L 100.0 19-119Surrogate: 2-Fluorophenol 7676.5 ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 8844.0 ug/L 100.0 SR11-52Surrogate: Phenol-d5 5857.6 ug/L 50.00 50-134Surrogate: Terphenyl-d14 9446.8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 55 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS Matrix Spike Dup (P8I0057-MSD1)Prepared: 09/07/18 Analyzed: 09/10/18 Source: 8090062-10 1,2,4-Trichlorobenzene ug/L39.1 10 50.00 BRL 3029-11678 6 1,2-Dichlorobenzene ug/L33.7 10 50.00 BRL 5032-11167 0.7 1,3-Dichlorobenzene ug/L32.3 10 50.00 BRL 5028-11065 0.7 1,4-Dichlorobenzene ug/L33.1 10 50.00 BRL 5029-11266 0.3 1-Methylnaphthalene ug/L46.8 10 50.00 BRL 5041-11994 5 2,4,5-Trichlorophenol ug/L51.9 10 50.00 BRL 5053-123104 4 2,4,6-Trichlorophenol ug/L48.6 10 50.00 BRL 5050-12597 0.2 2,4-Dichlorophenol ug/L45.7 10 50.00 BRL 5047-12191 2 2,4-Dimethylphenol ug/L36.9 10 50.00 BRL 5031-12474 21 2,4-Dinitrophenol ug/L26.8 10 50.00 BRL 5023-14354 2 2,4-Dinitrotoluene ug/L50.2 10 50.00 BRL 5057-128100 4 2,6-Dinitrotoluene ug/L50.2 10 50.00 BRL 5057-124100 4 2-Chloronaphthalene ug/L47.2 10 50.00 BRL 5040-11694 5 2-Chlorophenol ug/L39.3 10 50.00 BRL 5038-11779 8 2-Methylnaphthalene ug/L43.6 10 50.00 BRL 5040-12187 3 2-Methylphenol ug/L39.4 10 50.00 BRL 5030-11779 6 2-Nitroaniline ug/L52.4 10 50.00 BRL 5055-127105 6 2-Nitrophenol ug/L44.0 10 50.00 BRL 5047-12388 5 3,3’-Dichlorobenzidine ug/L44.3 10 50.00 BRL 5027-12989 13 3/4-Methylphenol ug/L34.3 10 50.00 BRL 5029-11069 7 3-Nitroaniline ug/L53.2 10 50.00 BRL 5041-128106 4 4,6-Dinitro-2-methylphenol ug/L23.2 10 50.00 BRL 5044-13746 1 4-Bromophenyl phenyl ether ug/L52.6 10 50.00 BRL 5055-124105 5 4-Chloro-3-methylphenol ug/L47.8 10 50.00 BRL 5052-11996 5 4-Chloroaniline ug/L42.3 10 50.00 BRL 5033-11785 14 4-Chlorophenyl phenyl ether ug/L49.7 10 50.00 BRL 5053-12199 0.8 4-Nitroaniline ug/L49.3 10 50.00 BRL 5045-13599 0.3 4-Nitrophenol ug/L30.6 10 50.00 BRL 5010-10561 2 Acenaphthene ug/L50.0 10 50.00 BRL 5047-122100 4 Acenaphthylene ug/L51.9 10 50.00 BRL 5041-130104 2 Aniline ug/L61.1 10 50.00 BRL 5011-124122 17 Anthracene ug/L55.6 10 50.00 BRL 5057-123111 4 Azobenzene ug/L49.8 10 50.00 BRL 5061-116100 5 Benzo(a)anthracene ug/L52.7 10 50.00 BRL 5058-125105 2 Benzo(a)pyrene ug/L55.0 10 50.00 BRL 5054-128110 2 Benzo(b)fluoranthene ug/L52.8 10 50.00 BRL 5053-131106 5 Benzo(g,h,i)perylene ug/L53.5 10 50.00 BRL 5050-134107 7 Benzo(k)fluoranthene ug/L54.4 10 50.00 BRL 5057-129109 2 Benzoic Acid ug/L28.2 100 50.00 BRL 50 J10-12556 5 Benzyl alcohol ug/L43.0 10 50.00 BRL 5031-11286 7 bis(2-Chloroethoxy)methane ug/L51.2 10 50.00 BRL 5048-120102 2 Bis(2-Chloroethyl)ether ug/L36.4 10 50.00 BRL 5043-11873 8 Bis(2-chloroisopropyl)ether ug/L40.8 10 50.00 BRL 5037-13082 5 Bis(2-Ethylhexyl)phthalate ug/L52.6 10 50.00 BRL 5055-135105 0.6 Butyl benzyl phthalate ug/L52.2 10 50.00 BRL 5053-134104 0.8 Chrysene ug/L50.8 10 50.00 BRL 5059-123102 0.8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 56 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0057 - 3510C MS Matrix Spike Dup (P8I0057-MSD1)Prepared: 09/07/18 Analyzed: 09/10/18 Source: 8090062-10 Dibenzo(a,h)anthracene ug/L55.3 10 50.00 BRL 5051-134111 4 Dibenzofuran ug/L51.3 10 50.00 BRL 5053-118103 4 Diethyl phthalate ug/L53.6 10 50.00 BRL 5056-125107 4 Dimethyl phthalate ug/L52.7 10 50.00 BRL 5045-127105 4 Di-n-butyl phthalate ug/L53.9 10 50.00 BRL 5059-127108 6 Di-n-octyl phthalate ug/L56.8 10 50.00 BRL 5051-140114 3 Fluoranthene ug/L53.0 10 50.00 BRL 5057-128106 5 Fluorene ug/L53.2 10 50.00 BRL 5052-124106 4 Hexachlorobenzene ug/L52.8 10 50.00 BRL 5053-125106 8 Hexachlorobutadiene ug/L39.5 10 50.00 BRL 5022-12479 3 Hexachlorocyclopentadiene ug/L21.6 10 50.00 BRL 5026-12243 8 Hexachloroethane ug/L30.7 10 50.00 BRL 5021-11561 0.8 Indeno(1,2,3-cd)pyrene ug/L61.2 10 50.00 BRL 5052-134122 6 Isophorone ug/L53.5 10 50.00 BRL 5042-124107 3 Naphthalene ug/L43.7 10 50.00 BRL 5040-12187 5 Nitrobenzene ug/L44.0 10 50.00 BRL 5045-12188 3 N-Nitroso-di-n-propylamine ug/L42.0 10 50.00 BRL 5049-11984 7 N-Nitrosodiphenylamine ug/L60.0 10 50.00 BRL 5051-123120 0.4 Pentachlorophenol ug/L48.1 10 50.00 BRL 5035-13896 2 Phenanthrene ug/L54.5 10 50.00 BRL 5059-120109 5 Phenol ug/L28.4 10 50.00 BRL 5010-6857 8 Pyrene ug/L52.6 10 50.00 BRL 5057-126105 1 ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 9999.4 ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 9145.3 ug/L 100.0 19-119Surrogate: 2-Fluorophenol 7271.7 ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 8643.2 ug/L 100.0 SR11-52Surrogate: Phenol-d5 5353.0 ug/L 50.00 50-134Surrogate: Terphenyl-d14 9447.1 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 57 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0121 - 3546 Blank (P8I0121-BLK1)Prepared & Analyzed: 09/11/18 1,2,4-Trichlorobenzene mg/kg wetBRL0.33 1,2-Dichlorobenzene mg/kg wetBRL0.33 1,3-Dichlorobenzene mg/kg wetBRL0.33 1,4-Dichlorobenzene mg/kg wetBRL0.33 1-Methylnaphthalene mg/kg wetBRL0.33 2,4,6-Trichlorophenol mg/kg wetBRL0.33 2,4-Dichlorophenol mg/kg wetBRL0.33 2,4-Dimethylphenol mg/kg wetBRL0.33 2,4-Dinitrophenol mg/kg wetBRL0.33 2,4-Dinitrotoluene mg/kg wetBRL0.33 2,6-Dinitrotoluene mg/kg wetBRL0.33 2-Chloronaphthalene mg/kg wetBRL0.33 2-Chlorophenol mg/kg wetBRL0.33 2-Methylnaphthalene mg/kg wetBRL0.33 2-Methylphenol mg/kg wetBRL0.33 2-Nitrophenol mg/kg wetBRL0.33 3,3’-Dichlorobenzidine mg/kg wetBRL0.33 3/4-Methylphenol mg/kg wetBRL0.33 4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33 4-Bromophenyl phenyl ether mg/kg wetBRL0.33 4-Chloro-3-methylphenol mg/kg wetBRL0.33 4-Chloroaniline mg/kg wetBRL0.33 4-Chlorophenyl phenyl ether mg/kg wetBRL0.33 4-Nitrophenol mg/kg wetBRL0.33 Acenaphthene mg/kg wetBRL0.33 Acenaphthylene mg/kg wetBRL0.33 Anthracene mg/kg wetBRL0.33 Azobenzene mg/kg wetBRL0.33 Benzo(a)anthracene mg/kg wetBRL0.33 Benzo(a)pyrene mg/kg wetBRL0.33 Benzo(b)fluoranthene mg/kg wetBRL0.33 Benzo(g,h,i)perylene mg/kg wetBRL0.33 Benzo(k)fluoranthene mg/kg wetBRL0.33 Benzoic Acid mg/kg wetBRL0.33 Benzyl alcohol mg/kg wetBRL0.33 bis(2-Chloroethoxy)methane mg/kg wetBRL0.33 Bis(2-Chloroethyl)ether mg/kg wetBRL0.33 Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33 Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33 Butyl benzyl phthalate mg/kg wetBRL0.33 Chrysene mg/kg wetBRL0.33 Dibenzo(a,h)anthracene mg/kg wetBRL0.33 Dibenzofuran mg/kg wetBRL0.33 Diethyl phthalate mg/kg wetBRL0.33 Dimethyl phthalate mg/kg wetBRL0.33 Di-n-butyl phthalate mg/kg wetBRL0.33 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 58 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0121 - 3546 Blank (P8I0121-BLK1)Prepared & Analyzed: 09/11/18 Di-n-octyl phthalate mg/kg wetBRL0.33 Fluoranthene mg/kg wetBRL0.33 Fluorene mg/kg wetBRL0.33 Hexachlorobenzene mg/kg wetBRL0.33 Hexachlorobutadiene mg/kg wetBRL0.33 Hexachlorocyclopentadiene mg/kg wetBRL0.33 Hexachloroethane mg/kg wetBRL0.33 Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33 Isophorone mg/kg wetBRL0.33 Naphthalene mg/kg wetBRL0.33 Nitrobenzene mg/kg wetBRL0.33 N-Nitroso-di-n-propylamine mg/kg wetBRL0.33 N-Nitrosodiphenylamine mg/kg wetBRL0.33 Pentachlorophenol mg/kg wetBRL0.33 Phenanthrene mg/kg wetBRL0.33 Phenol mg/kg wetBRL0.33 Pyrene mg/kg wetBRL0.33 mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 983.28 mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 891.48 mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 903.00 mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 811.35 mg/kg wet 3.333 34-121Surrogate: Phenol-d5 862.88 mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 851.41 LCS (P8I0121-BS1)Prepared & Analyzed: 09/11/18 1,2,4-Trichlorobenzene mg/kg wet1.10 0.33 1.667 34-11866 1,2-Dichlorobenzene mg/kg wet0.978 0.33 1.667 33-11759 1,3-Dichlorobenzene mg/kg wet0.952 0.33 1.667 30-11557 1,4-Dichlorobenzene mg/kg wet0.951 0.33 1.667 31-11557 1-Methylnaphthalene mg/kg wet1.34 0.33 1.667 40-11980 2,4,6-Trichlorophenol mg/kg wet1.29 0.33 1.667 39-12677 2,4-Dichlorophenol mg/kg wet1.28 0.33 1.667 40-12277 2,4-Dimethylphenol mg/kg wet1.67 0.33 1.667 30-127100 2,4-Dinitrophenol mg/kg wet1.11 0.33 1.667 27-12966 2,4-Dinitrotoluene mg/kg wet1.38 0.33 1.667 48-12683 2,6-Dinitrotoluene mg/kg wet1.38 0.33 1.667 46-12483 2-Chloronaphthalene mg/kg wet1.28 0.33 1.667 41-11477 2-Chlorophenol mg/kg wet1.19 0.33 1.667 34-12171 2-Methylnaphthalene mg/kg wet1.24 0.33 1.667 38-12275 2-Methylphenol mg/kg wet1.22 0.33 1.667 32-12273 2-Nitrophenol mg/kg wet1.15 0.33 1.667 36-12369 3,3’-Dichlorobenzidine mg/kg wet1.34 0.33 1.667 22-12180 3/4-Methylphenol mg/kg wet1.11 0.33 1.667 34-11967 4,6-Dinitro-2-methylphenol mg/kg wet1.15 0.33 1.667 29-13269 4-Bromophenyl phenyl ether mg/kg wet1.36 0.33 1.667 46-12482 4-Chloro-3-methylphenol mg/kg wet1.31 0.33 1.667 45-12278 4-Chloroaniline mg/kg wet1.44 0.33 1.667 17-10686 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 59 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0121 - 3546 LCS (P8I0121-BS1)Prepared & Analyzed: 09/11/18 4-Chlorophenyl phenyl ether mg/kg wet1.34 0.33 1.667 45-12181 4-Nitrophenol mg/kg wet1.22 0.33 1.667 30-13273 Acenaphthene mg/kg wet1.34 0.33 1.667 40-12381 Acenaphthylene mg/kg wet1.40 0.33 1.667 32-13284 Anthracene mg/kg wet1.45 0.33 1.667 47-12387 Azobenzene mg/kg wet1.28 0.33 1.667 39-12577 Benzo(a)anthracene mg/kg wet1.34 0.33 1.667 49-12680 Benzo(a)pyrene mg/kg wet1.47 0.33 1.667 45-12988 Benzo(b)fluoranthene mg/kg wet1.47 0.33 1.667 45-13288 Benzo(g,h,i)perylene mg/kg wet1.47 0.33 1.667 43-13488 Benzo(k)fluoranthene mg/kg wet1.36 0.33 1.667 47-13282 Benzoic Acid mg/kg wet0.950 0.33 1.667 10-8357 Benzyl alcohol mg/kg wet1.24 0.33 1.667 29-12274 bis(2-Chloroethoxy)methane mg/kg wet1.37 0.33 1.667 36-12182 Bis(2-Chloroethyl)ether mg/kg wet3.02 0.33 1.667 L131-120181 Bis(2-chloroisopropyl)ether mg/kg wet1.12 0.33 1.667 33-13167 Bis(2-Ethylhexyl)phthalate mg/kg wet1.35 0.33 1.667 51-13381 Butyl benzyl phthalate mg/kg wet1.35 0.33 1.667 48-13281 Chrysene mg/kg wet1.36 0.33 1.667 50-12481 Dibenzo(a,h)anthracene mg/kg wet1.46 0.33 1.667 45-13488 Dibenzofuran mg/kg wet1.35 0.33 1.667 44-12081 Diethyl phthalate mg/kg wet1.41 0.33 1.667 50-12485 Dimethyl phthalate mg/kg wet1.41 0.33 1.667 48-12484 Di-n-butyl phthalate mg/kg wet1.34 0.33 1.667 51-12881 Di-n-octyl phthalate mg/kg wet1.47 0.33 1.667 45-14088 Fluoranthene mg/kg wet1.40 0.33 1.667 50-12784 Fluorene mg/kg wet1.46 0.33 1.667 43-12588 Hexachlorobenzene mg/kg wet1.31 0.33 1.667 45-12279 Hexachlorobutadiene mg/kg wet1.12 0.33 1.667 32-12367 Hexachlorocyclopentadiene mg/kg wet1.23 0.33 1.667 32-11774 Hexachloroethane mg/kg wet0.946 0.33 1.667 28-11757 Indeno(1,2,3-cd)pyrene mg/kg wet1.61 0.33 1.667 45-13397 Isophorone mg/kg wet1.41 0.33 1.667 30-12284 Naphthalene mg/kg wet1.21 0.33 1.667 35-12372 Nitrobenzene mg/kg wet1.19 0.33 1.667 34-12271 N-Nitroso-di-n-propylamine mg/kg wet1.15 0.33 1.667 36-12069 N-Nitrosodiphenylamine mg/kg wet1.60 0.33 1.667 38-12796 Pentachlorophenol mg/kg wet1.13 0.33 1.667 25-13368 Phenanthrene mg/kg wet1.39 0.33 1.667 50-12183 Phenol mg/kg wet1.22 0.33 1.667 34-12173 Pyrene mg/kg wet1.33 0.33 1.667 47-12780 mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 802.67 mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 781.29 mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 772.58 mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 711.18 mg/kg wet 3.333 34-121Surrogate: Phenol-d5 752.51 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 60 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0121 - 3546 LCS (P8I0121-BS1)Prepared & Analyzed: 09/11/18 mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 731.22 LCS Dup (P8I0121-BSD1)Prepared & Analyzed: 09/11/18 1,2,4-Trichlorobenzene mg/kg wet1.40 0.33 1.667 20 D34-11884 24 1,2-Dichlorobenzene mg/kg wet1.30 0.33 1.667 20 D33-11778 28 1,3-Dichlorobenzene mg/kg wet1.21 0.33 1.667 20 D30-11572 23 1,4-Dichlorobenzene mg/kg wet1.26 0.33 1.667 20 D31-11576 28 1-Methylnaphthalene mg/kg wet1.69 0.33 1.667 20 D40-119101 23 2,4,6-Trichlorophenol mg/kg wet1.63 0.33 1.667 20 D39-12698 23 2,4-Dichlorophenol mg/kg wet1.68 0.33 1.667 20 D40-122100 27 2,4-Dimethylphenol mg/kg wet2.04 0.33 1.667 2030-127122 20 2,4-Dinitrophenol mg/kg wet1.40 0.33 1.667 20 D27-12984 24 2,4-Dinitrotoluene mg/kg wet1.65 0.33 1.667 2048-12699 17 2,6-Dinitrotoluene mg/kg wet1.65 0.33 1.667 2046-12499 17 2-Chloronaphthalene mg/kg wet1.55 0.33 1.667 2041-11493 19 2-Chlorophenol mg/kg wet1.52 0.33 1.667 20 D34-12191 24 2-Methylnaphthalene mg/kg wet1.58 0.33 1.667 20 D38-12295 24 2-Methylphenol mg/kg wet1.65 0.33 1.667 20 D32-12299 30 2-Nitrophenol mg/kg wet1.48 0.33 1.667 20 D36-12389 25 3,3’-Dichlorobenzidine mg/kg wet1.61 0.33 1.667 2022-12196 18 3/4-Methylphenol mg/kg wet1.52 0.33 1.667 20 D34-11991 31 4,6-Dinitro-2-methylphenol mg/kg wet1.44 0.33 1.667 20 D29-13286 23 4-Bromophenyl phenyl ether mg/kg wet1.56 0.33 1.667 2046-12494 14 4-Chloro-3-methylphenol mg/kg wet1.63 0.33 1.667 20 D45-12298 22 4-Chloroaniline mg/kg wet1.73 0.33 1.667 2017-106104 19 4-Chlorophenyl phenyl ether mg/kg wet1.59 0.33 1.667 2045-12196 17 4-Nitrophenol mg/kg wet1.46 0.33 1.667 2030-13288 18 Acenaphthene mg/kg wet1.61 0.33 1.667 2040-12397 18 Acenaphthylene mg/kg wet1.70 0.33 1.667 2032-132102 20 Anthracene mg/kg wet1.75 0.33 1.667 2047-123105 19 Azobenzene mg/kg wet1.59 0.33 1.667 20 D39-12596 22 Benzo(a)anthracene mg/kg wet1.71 0.33 1.667 20 D49-126103 24 Benzo(a)pyrene mg/kg wet1.75 0.33 1.667 2045-129105 18 Benzo(b)fluoranthene mg/kg wet1.71 0.33 1.667 2045-132103 15 Benzo(g,h,i)perylene mg/kg wet1.72 0.33 1.667 2043-134103 16 Benzo(k)fluoranthene mg/kg wet1.63 0.33 1.667 2047-13298 18 Benzoic Acid mg/kg wet1.03 0.33 1.667 2010-8362 8 Benzyl alcohol mg/kg wet1.64 0.33 1.667 20 D29-12298 28 bis(2-Chloroethoxy)methane mg/kg wet1.74 0.33 1.667 20 D36-121105 24 Bis(2-Chloroethyl)ether mg/kg wet1.48 0.33 1.667 20 D31-12089 69 Bis(2-chloroisopropyl)ether mg/kg wet1.48 0.33 1.667 20 D33-13189 28 Bis(2-Ethylhexyl)phthalate mg/kg wet1.65 0.33 1.667 2051-13399 20 Butyl benzyl phthalate mg/kg wet1.66 0.33 1.667 20 D48-13299 21 Chrysene mg/kg wet1.66 0.33 1.667 2050-12499 20 Dibenzo(a,h)anthracene mg/kg wet1.73 0.33 1.667 2045-134104 17 Dibenzofuran mg/kg wet1.66 0.33 1.667 20 D44-120100 21 Diethyl phthalate mg/kg wet1.71 0.33 1.667 2050-124102 19 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 61 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P8I0121 - 3546 LCS Dup (P8I0121-BSD1)Prepared & Analyzed: 09/11/18 Dimethyl phthalate mg/kg wet1.68 0.33 1.667 2048-124101 18 Di-n-butyl phthalate mg/kg wet1.70 0.33 1.667 20 D51-128102 23 Di-n-octyl phthalate mg/kg wet1.74 0.33 1.667 2045-140104 16 Fluoranthene mg/kg wet1.75 0.33 1.667 20 D50-127105 22 Fluorene mg/kg wet1.73 0.33 1.667 2043-125104 17 Hexachlorobenzene mg/kg wet1.59 0.33 1.667 2045-12295 19 Hexachlorobutadiene mg/kg wet1.46 0.33 1.667 20 D32-12388 27 Hexachlorocyclopentadiene mg/kg wet1.49 0.33 1.667 2032-11790 20 Hexachloroethane mg/kg wet1.30 0.33 1.667 20 D28-11778 31 Indeno(1,2,3-cd)pyrene mg/kg wet1.94 0.33 1.667 2045-133116 18 Isophorone mg/kg wet1.76 0.33 1.667 20 D30-122105 22 Naphthalene mg/kg wet1.56 0.33 1.667 20 D35-12394 26 Nitrobenzene mg/kg wet1.51 0.33 1.667 20 D34-12290 24 N-Nitroso-di-n-propylamine mg/kg wet1.51 0.33 1.667 20 D36-12091 27 N-Nitrosodiphenylamine mg/kg wet1.95 0.33 1.667 2038-127117 19 Pentachlorophenol mg/kg wet1.34 0.33 1.667 2025-13381 17 Phenanthrene mg/kg wet1.72 0.33 1.667 20 D50-121103 22 Phenol mg/kg wet1.64 0.33 1.667 20 D34-12198 29 Pyrene mg/kg wet1.68 0.33 1.667 20 D47-127101 23 mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 993.29 mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 931.55 mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 993.32 mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 891.48 mg/kg wet 3.333 34-121Surrogate: Phenol-d5 973.25 mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 891.48 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 62 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P8I0063 - 7471B Blank (P8I0063-BLK1)Prepared & Analyzed: 09/07/18 Mercury mg/kg wetBRL0.020 Matrix Spike (P8I0063-MS1)Prepared & Analyzed: 09/07/18 Source: 8090062-01 Mercury mg/kg dry0.673 0.024 0.4963 0.0825 80-120119 Matrix Spike Dup (P8I0063-MSD1)Prepared & Analyzed: 09/07/18 Source: 8090062-01 Mercury mg/kg dry0.556 0.023 0.4882 0.0825 2080-12097 19 Batch P8I0064 - 3050B Blank (P8I0064-BLK1)Prepared & Analyzed: 09/07/18 Arsenic mg/kg wetBRL0.50 Barium mg/kg wetBRL0.50 Cadmium mg/kg wetBRL0.25 Chromium mg/kg wetBRL0.25 Lead mg/kg wetBRL0.25 Selenium mg/kg wetBRL0.50 Silver mg/kg wetBRL0.25 LCS (P8I0064-BS1)Prepared & Analyzed: 09/07/18 Arsenic mg/kg wet12.3 0.50 12.50 80-12098 Barium mg/kg wet12.7 0.50 12.50 80-120101 Cadmium mg/kg wet12.5 0.25 12.50 80-120100 Chromium mg/kg wet13.0 0.25 12.50 80-120104 Lead mg/kg wet12.5 0.25 12.50 80-120100 Selenium mg/kg wet11.9 0.50 12.50 80-12095 Silver mg/kg wet4.93 0.25 5.000 80-12099 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 63 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P8I0064 - 3050B Matrix Spike (P8I0064-MS1)Prepared & Analyzed: 09/07/18 Source: 8090062-01 Arsenic mg/kg dry13.9 0.59 14.82 2.34 75-12578 Barium mg/kg dry2.96E10 0.59 14.82 177 M75-125NR Cadmium mg/kg dry11.4 0.30 14.82 0.0323 75-12577 Chromium mg/kg dry43.2 0.30 14.82 30.1 75-12588 Lead mg/kg dry25.5 0.30 14.82 14.1 75-12577 Selenium mg/kg dry12.0 0.59 14.81 BRL 75-12581 Silver mg/kg dry3.99 0.30 5.926 BRL M75-12567 Matrix Spike Dup (P8I0064-MSD1)Prepared & Analyzed: 09/07/18 Source: 8090062-01 Arsenic mg/kg dry13.7 0.60 14.89 2.34 2075-12576 1 Barium mg/kg dry2.98E10 0.60 14.89 177 20 M75-125NR 0.5 Cadmium mg/kg dry11.4 0.30 14.89 0.0323 2075-12576 0.1 Chromium mg/kg dry42.7 0.30 14.89 30.1 2075-12585 1 Lead mg/kg dry25.1 0.30 14.89 14.1 20 M75-12574 2 Selenium mg/kg dry12.7 0.60 14.89 BRL 2075-12585 6 Silver mg/kg dry4.02 0.30 5.956 BRL 20 M75-12568 0.9 Post Spike (P8I0064-PS1)Prepared & Analyzed: 09/07/18 Source: 8090062-01 Arsenic mg/L0.464 0.5001 0.0786 PS80-12077 Barium mg/L1.00E9 0.5000 5.95 PS80-120NR Cadmium mg/L0.366 0.5000 0.00108 PS80-12073 Chromium mg/L1.37 0.5001 1.01 PS80-12072 Lead mg/L0.803 0.5001 0.474 PS80-12066 Selenium mg/L0.376 0.4999 0.000215 PS80-12075 Silver mg/L0.131 0.2000 -0.0376 PS80-12066 Batch P8I0065 - 3010A Blank (P8I0065-BLK1)Prepared: 09/07/18 Analyzed: 09/11/18 Arsenic mg/LBRL0.020 Barium mg/L0.00111 0.010 J Cadmium mg/LBRL0.0010 Chromium mg/LBRL0.0050 Lead mg/LBRL0.0050 Selenium mg/LBRL0.020 Silver mg/LBRL0.0050 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 64 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P8I0065 - 3010A LCS (P8I0065-BS1)Prepared: 09/07/18 Analyzed: 09/11/18 Arsenic mg/L0.498 0.020 0.5001 80-12099 Barium mg/L0.502 0.010 0.5000 80-120100 Cadmium mg/L0.502 0.0010 0.5000 80-120100 Chromium mg/L0.518 0.0050 0.5001 80-120104 Lead mg/L0.501 0.0050 0.5001 80-120100 Selenium mg/L0.492 0.020 0.4999 80-12098 Silver mg/L0.199 0.0050 0.2000 80-120100 Matrix Spike (P8I0065-MS1)Prepared: 09/07/18 Analyzed: 09/11/18 Source: 8090062-07 Arsenic mg/L0.511 0.020 0.5001 BRL 75-125102 Barium mg/L0.767 0.010 0.5000 0.243 75-125105 Cadmium mg/L0.511 0.0010 0.5000 BRL 75-125102 Chromium mg/L0.516 0.0050 0.5001 0.00730 75-125102 Lead mg/L0.509 0.0050 0.5001 0.00488 75-125101 Selenium mg/L0.498 0.020 0.4999 BRL 75-125100 Silver mg/L0.201 0.0050 0.2000 BRL 75-125101 Matrix Spike Dup (P8I0065-MSD1)Prepared: 09/07/18 Analyzed: 09/11/18 Source: 8090062-07 Arsenic mg/L0.519 0.020 0.5001 BRL 2075-125104 2 Barium mg/L0.775 0.010 0.5000 0.243 2075-125107 1 Cadmium mg/L0.514 0.0010 0.5000 BRL 2075-125103 0.6 Chromium mg/L0.527 0.0050 0.5001 0.00730 2075-125104 2 Lead mg/L0.518 0.0050 0.5001 0.00488 2075-125103 2 Selenium mg/L0.513 0.020 0.4999 BRL 2075-125103 3 Silver mg/L0.202 0.0050 0.2000 BRL 2075-125101 0.6 Batch P8I0117 - 7470A Blank (P8I0117-BLK1)Prepared & Analyzed: 09/11/18 Mercury mg/LBRL0.00020 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 65 of 95 9/20/18 Level II QC Report 1900 Hendersonville Road, Suite 10 Project: PE ValveECS Carolinas, LLP (Asheville) Asheville, NC 28803 Attn: James Bevers Prism Work Order: 8090062 Time Submitted: 9/6/2018 8:30:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P8I0117 - 7470A LCS (P8I0117-BS1)Prepared & Analyzed: 09/11/18 Mercury mg/L0.00949 0.00020 0.009375 80-120101 Batch P8I0144 - 3060A Blank (P8I0144-BLK1)Prepared & Analyzed: 09/11/18 Hexavalent Chromium mg/kg wetBRL0.40 LCS (P8I0144-BS1)Prepared & Analyzed: 09/11/18 Hexavalent Chromium mg/kg wet16.1 0.40 16.00 80-120100 Matrix Spike (P8I0144-MS1)Prepared & Analyzed: 09/11/18 Source: 8090062-04 Hexavalent Chromium mg/kg dry14.5 0.45 17.96 0.308 75-12579 Matrix Spike Dup (P8I0144-MSD1)Prepared & Analyzed: 09/11/18 Source: 8090062-04 Hexavalent Chromium mg/kg dry14.3 0.45 17.96 0.308 2075-12578 1 Post Spike (P8I0144-PS1)Prepared & Analyzed: 09/11/18 Source: 8090062-04 Hexavalent Chromium mg/kg0.399 0.4000 0.00685 85-11598 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 66 of 95 Sample Extraction Data Prep Method: Solids, Dry Weight Lab Number Batch Date/TimeInitialFinal P8I01408090062-01 09/11/18 8:0030 30g g P8I01408090062-02 09/11/18 8:0030 30g g P8I01408090062-03 09/11/18 8:0030 30g g P8I01408090062-04 09/11/18 8:0030 30g g P8I01408090062-05 09/11/18 8:0030 30g g P8I01408090062-06 09/11/18 8:0030 30g g Prep Method: 3510C MS Lab Number Batch Date/TimeInitialFinal P8I00578090062-07 09/07/18 9:291000 1mL mL P8I00578090062-07 09/07/18 9:291000 1mL mL P8I00578090062-08 09/07/18 9:299801mL mL P8I00578090062-09 09/07/18 9:299201mL mL P8I00578090062-10 09/07/18 9:291000 1mL mL Prep Method: 3546 Lab Number Batch Date/TimeInitialFinal P8I01218090062-01 09/11/18 10:3030.07 1g mL P8I01218090062-02 09/11/18 10:3030.05 1g mL P8I01218090062-03 09/11/18 10:3030.07 1g mL P8I01218090062-04 09/11/18 10:3030.06 1g mL P8I01218090062-05 09/11/18 10:3030.09 1g mL P8I01218090062-06 09/11/18 10:3030.01 1g mL Prep Method: 3010A Lab Number Batch Date/TimeInitialFinal P8I00658090062-07 09/07/18 7:3550 50mL mL P8I00658090062-07 09/07/18 7:3550 50mL mL P8I00658090062-07 09/07/18 7:3550 50mL mL P8I00658090062-08 09/07/18 7:3550 50mL mL P8I00658090062-08 09/07/18 7:3550 50mL mL P8I00658090062-08 09/07/18 7:3550 50mL mL P8I00658090062-09 09/07/18 7:3550 50mL mL P8I00658090062-09 09/07/18 7:3550 50mL mL P8I00658090062-10 09/07/18 7:3550 50mL mL Prep Method: 3050B Lab Number Batch Date/TimeInitialFinal P8I00648090062-01 09/07/18 9:002 50g mL P8I00648090062-01 09/07/18 9:002 50g mL P8I00648090062-02 09/07/18 9:002 50g mL P8I00648090062-03 09/07/18 9:002.02 50g mL P8I00648090062-03 09/07/18 9:002.02 50g mL P8I00648090062-04 09/07/18 9:002 50g mL P8I00648090062-04 09/07/18 9:002 50g mL P8I00648090062-04 09/07/18 9:002 50g mL P8I00648090062-05 09/07/18 9:002.02 50g mL P8I00648090062-05 09/07/18 9:002.02 50g mL P8I00648090062-05 09/07/18 9:002.02 50g mL P8I00648090062-06 09/07/18 9:002.01 50g mL P8I00648090062-06 09/07/18 9:002.01 50g mL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 67 of 95 Sample Extraction Data Prep Method: 3060A Lab Number Batch Date/TimeInitialFinal P8I01448090062-01 09/11/18 9:052.5 100g mL P8I01448090062-02 09/11/18 9:052.5 100g mL P8I01448090062-03 09/11/18 9:052.5 100g mL P8I01448090062-04 09/11/18 9:052.5 100g mL P8I01448090062-05 09/11/18 9:052.5 100g mL P8I01448090062-06 09/11/18 9:052.5 100g mL Prep Method: 7470A Lab Number Batch Date/TimeInitialFinal P8I01178090062-07 09/11/18 8:1520 30mL mL P8I01178090062-08 09/11/18 8:1520 30mL mL P8I01178090062-09 09/11/18 8:1520 30mL mL P8I01178090062-10 09/11/18 8:1520 30mL mL Prep Method: 7471B Lab Number Batch Date/TimeInitialFinal P8I00638090062-01 09/07/18 9:000.6 50g mL P8I00638090062-02 09/07/18 9:000.62 50g mL P8I00638090062-03 09/07/18 9:000.6 50g mL P8I00638090062-04 09/07/18 9:000.6 50g mL P8I00638090062-05 09/07/18 9:000.62 50g mL P8I00638090062-06 09/07/18 9:000.6 50g mL Prep Method: 5035 Lab Number Batch Date/TimeInitialFinal P8I01068090062-01 09/10/18 9:475.02 5g mL P8I01068090062-02 09/10/18 9:476.05 5g mL P8I01068090062-03 09/10/18 9:475.65 5g mL P8I01068090062-04 09/10/18 9:475.63 5g mL P8I01068090062-05 09/10/18 9:476.11 5g mL P8I01068090062-06 09/10/18 9:475.43 5g mL Subcontracted Analyses Lab Number The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc. Analysis 8090062-07 8260 (Low) 8090062-08 8260 (Low) 8090062-09 8260 (Low) 8090062-10 8260 (Low) 8090062-11 8260 (Low) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 68 of 95 Page 69 of 95 Page 70 of 95 Page 71 of 95 Page 72 of 95 Page 73 of 95 Page 74 of 95 Page 75 of 95 Page 76 of 95 Page 77 of 95 Page 78 of 95 Page 79 of 95 Page 80 of 95 Page 81 of 95 Page 82 of 95 Page 83 of 95 Page 84 of 95 Page 85 of 95 Page 86 of 95 Page 87 of 95 Page 88 of 95 Page 89 of 95 Page 90 of 95 Page 91 of 95 Page 92 of 95 Page 93 of 95 Page 94 of 95 Page 95 of 95 Appendix IV:Historical Research Documentation The EDR Aerial Photo Decade Package Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 Inquiry Number: July 16, 2019 5716013.8 6 Armstrong Road, 4th floor Shelton, CT 06484 Toll Free: 800.352.0050 www.edrnet.com 2016 1"=500'Flight Year: 2016 USDA/NAIP 2012 1"=500'Flight Year: 2012 USDA/NAIP 2009 1"=500'Flight Year: 2009 USDA/NAIP 2006 1"=500'Flight Year: 2006 USDA/NAIP 1998 1"=750'Flight Date: March 15, 1998 USGS 1994 1"=500'Acquisition Date: March 22, 1994 USGS/DOQQ 1988 1"=1000'Flight Date: May 27, 1988 USGS 1984 1"=500'Flight Date: April 26, 1984 USGS 1975 1"=500'Flight Date: April 01, 1975 USGS 1964 1"=500'Flight Date: October 07, 1964 USGS 1951 1"=500'Flight Date: May 09, 1951 USDA EDR Aerial Photo Decade Package 07/16/19 Former P.E. Valve Property Site Name:Client Name: ECS Southeast, LLP 1140 Sweeten Creek RD 1900 Hendersonville Road Asheville, NC 28803 Ashville, NC 28803 EDR Inquiry #5716013.8 Contact:Don Marlor Environmental Data Resources, Inc. (EDR) Aerial Photo Decade Package is a screening tool designed to assist environmental professionals in evaluating potential liability on a target property resulting from past activities. EDR’s professional researchers provide digitally reproduced historical aerial photographs, and when available, provide one photo per decade. Search Results: Year Scale Details Source When delivered electronically by EDR, the aerial photo images included with this report are for ONE TIME USE ONLY. Further reproduction of these aerial photo images is prohibited without permission from EDR. For more information contact your EDR Account Executive. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2019 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. 5716013 8-page 2 5716013.8 2016 = 500' 5716013.8 2012 = 500' 5716013.8 2009 = 500' 5716013.8 2006 = 500' 5716013.8 1998 = 750' 5716013.8 1994 = 500' 5716013.8 1988 = 1000' 5716013.8 1984 = 500' 5716013.8 1975 = 500' 5716013.8 1964 = 500' 5716013.8 1951 = 500' Certified Sanborn® Map Report Inquiry Number: 6 Armstrong Road, 4th floor Shelton, CT 06484 Toll Free: 800.352.0050 www.edrnet.com Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 July 15, 2019 5716013.3 Certified Sanborn® Map Report Certified Sanborn Results: Disclaimer - Copyright and Trademark Notice EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. page- The Sanborn Library includes more than 1.2 million fire insurance maps from Sanborn, Bromley, Perris & Browne, Hopkins, Barlow and others which track historical property usage in approximately 12,000 American cities and towns. Collections searched: Library of Congress University Publications of America EDR Private Collection The Sanborn Library LLC Since 1866™ Limited Permission To Make Copies Sanborn® Library search results Contact:EDR Inquiry # Site Name: Client Name: Certification # PO # Project 1972 1963 1961 1957 1954 1950 07/15/19 1140 Sweeten Creek RD Former P.E. Valve Property ECS Southeast, LLP 1900 Hendersonville Road Asheville, NC 28803 5716013.3 Ashville, NC 28803 Don Marlor The Sanborn Library has been searched by EDR and maps covering the target property location as provided by ECS Southeast, LLP were identified for the years listed below. The Sanborn Library is the largest, most complete collection of fire insurance maps. The collection includes maps from Sanborn, Bromley, Perris & Browne, Hopkins, Barlow, and others. Only Environmental Data Resources Inc. (EDR) is authorized to grant rights for commercial reproduction of maps by the Sanborn Library LLC, the copyright holder for the collection. Results can be authenticated by visiting www.edrnet.com/sanborn. The Sanborn Library is continually enhanced with newly identified map archives. This report accesses all maps in the collection as of the day this report was generated. 1D3E-40C1-939F TBD Maps Provided: Former P.E. Valve Phase I ESA Certification #: 1D3E-40C1-939F ECS Southeast, LLP (the client) is permitted to make up to FIVE photocopies of this Sanborn Map transmittal and each fire insurance map accompanying this report solely for the limited use of its customer. No one other than the client is authorized to make copies. Upon request made directly to an EDR Account Executive, the client may be permitted to make a limited number of additional photocopies. This permission is conditioned upon compliance by the client, its customer and their agents with EDR's copyright policy; a copy of which is available upon request. This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2019 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. 5716013 3 2 page- Sanborn Sheet Key This Certified Sanborn Map Report is based upon the following Sanborn Fire Insurance map sheets. 1972 Source Sheets 1972 Volume 2, Sheet 208 1963 Source Sheets 1963 Volume 2, Sheet 208 1961 Source Sheets 1961 Volume 2, Sheet 208 1957 Source Sheets 1957 Volume 2, Sheet 208 5716013 3 3 page- Sanborn Sheet Key This Certified Sanborn Map Report is based upon the following Sanborn Fire Insurance map sheets. 1954 Source Sheets 1954 Volume 2, Sheet 87 1950 Source Sheets 1950 Volume 2, Sheet 87 5716013 3 4 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection.0 Feet 150 300 600 - page Certified Sanborn® Map Site Name: Address: City, ST, ZIP:Asheville, NC 28803 Client:ECS Southeast, LLP EDR Inquiry:5716013.3 Order Date:07/15/2019 Certification # Copyright 1972 1972 1D3E-40C1-939F 1D3E-40C1-939FFormer P.E. Valve Property 1140 Sweeten Creek RD Volume 2, Sheet 208 5716013 3 5 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection.0 Feet 150 300 600 - page Certified Sanborn® Map Site Name: Address: City, ST, ZIP:Asheville, NC 28803 Client:ECS Southeast, LLP EDR Inquiry:5716013.3 Order Date:07/15/2019 Certification # Copyright 1963 1963 1D3E-40C1-939F 1D3E-40C1-939FFormer P.E. Valve Property 1140 Sweeten Creek RD Volume 2, Sheet 208 5716013 3 6 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection.0 Feet 150 300 600 - page Certified Sanborn® Map Site Name: Address: City, ST, ZIP:Asheville, NC 28803 Client:ECS Southeast, LLP EDR Inquiry:5716013.3 Order Date:07/15/2019 Certification # Copyright 1961 1961 1D3E-40C1-939F 1D3E-40C1-939FFormer P.E. Valve Property 1140 Sweeten Creek RD Volume 2, Sheet 208 5716013 3 7 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection.0 Feet 150 300 600 - page Certified Sanborn® Map Site Name: Address: City, ST, ZIP:Asheville, NC 28803 Client:ECS Southeast, LLP EDR Inquiry:5716013.3 Order Date:07/15/2019 Certification # Copyright 1957 1957 1D3E-40C1-939F 1D3E-40C1-939FFormer P.E. Valve Property 1140 Sweeten Creek RD Volume 2, Sheet 208 5716013 3 8 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection.0 Feet 150 300 600 - page Certified Sanborn® Map Site Name: Address: City, ST, ZIP:Asheville, NC 28803 Client:ECS Southeast, LLP EDR Inquiry:5716013.3 Order Date:07/15/2019 Certification # Copyright 1954 1954 1D3E-40C1-939F 1D3E-40C1-939FFormer P.E. Valve Property 1140 Sweeten Creek RD Volume 2, Sheet 87 5716013 3 9 This Certified Sanborn Map combines the following sheets. Outlined areas indicate map sheets within the collection.0 Feet 150 300 600 - page Certified Sanborn® Map Site Name: Address: City, ST, ZIP:Asheville, NC 28803 Client:ECS Southeast, LLP EDR Inquiry:5716013.3 Order Date:07/15/2019 Certification # Copyright 1950 1950 1D3E-40C1-939F 1D3E-40C1-939FFormer P.E. Valve Property 1140 Sweeten Creek RD Volume 2, Sheet 87 5716013 3 10 EDR Historical Topo Map Report Inquiry Number: 6 Armstrong Road, 4th floor Shelton, CT 06484 Toll Free: 800.352.0050 www.edrnet.com with QuadMatch™ Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 July 15, 2019 5716013.4 EDR Historical Topo Map Report EDR Inquiry # Search Results: P.O.# Project: Maps Provided: Disclaimer - Copyright and Trademark Notice EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. page- Coordinates: Latitude: Longitude: UTM Zone: UTM X Meters: UTM Y Meters: Elevation: Contact: Site Name: Client Name: 2013 1990, 1991 1988 1961 1943 1936 1901 1894 07/15/19 Former P.E. Valve Property ECS Southeast, LLP 1140 Sweeten Creek RD 1900 Hendersonville Road Asheville, NC 28803 Ashville, NC 28803 5716013.4 Don Marlor EDR Topographic Map Library has been searched by EDR and maps covering the target property location as provided by ECS Southeast, LLP were identified for the years listed below. EDR’s Historical Topo Map Report is designed to assist professionals in evaluating potential liability on a target property resulting from past activities. EDRs Historical Topo Map Report includes a search of a collection of public and private color historical topographic maps, dating back to the late 1800s. TBD 35.543513 35° 32' 37" North Former P.E. Valve Phase I ESA -82.520936 -82° 31' 15" West Zone 17 North 362130.73 3934383.20 2119.94' above sea level This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2019 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. 5716013 4 2 page Topo Sheet Key This EDR Topo Map Report is based upon the following USGS topographic map sheets. - 2013 Source Sheets 2013 Oteen 7.5-minute, 24000 2013 Asheville 7.5-minute, 24000 1990, 1991 Source Sheets 1990 Oteen 7.5-minute, 24000 Aerial Photo Revised 1987 1991 Asheville 7.5-minute, 24000 Aerial Photo Revised 1987 1988 Source Sheets 1988 ASHEVILLE 15-minute, 50000 1961 Source Sheets 1961 Asheville 7.5-minute, 24000 Aerial Photo Revised 1960 5716013 4 3 page Topo Sheet Key This EDR Topo Map Report is based upon the following USGS topographic map sheets. - 1943 Source Sheets 1943 Asheville 7.5-minute, 24000 1936 Source Sheets 1936 Asheville 7.5-minute, 24000 1901 Source Sheets 1901 Asheville 30-minute, 125000 1894 Source Sheets 1894 Asheville 30-minute, 125000 5716013 4 4 Historical Topo Map page SITE NAME: ADDRESS: CLIENT: This report includes information from the following map sheet(s). - EW SW S SE NW N NE 2013 0 Miles 0.25 0.5 1 1.5 Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 ECS Southeast, LLP TP, Asheville, 2013, 7.5-minute E, Oteen, 2013, 7.5-minute 5716013 4 5 Historical Topo Map page SITE NAME: ADDRESS: CLIENT: This report includes information from the following map sheet(s). - EW SW S SE NW N NE 1990, 1991 0 Miles 0.25 0.5 1 1.5 Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 ECS Southeast, LLP TP, Asheville, 1991, 7.5-minute E, Oteen, 1990, 7.5-minute 5716013 4 6 Historical Topo Map page SITE NAME: ADDRESS: CLIENT: This report includes information from the following map sheet(s). - EW SW S SE NW N NE 1988 0 Miles 0.25 0.5 1 1.5 Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 ECS Southeast, LLP TP, ASHEVILLE, 1988, 15-minute 5716013 4 7 Historical Topo Map page SITE NAME: ADDRESS: CLIENT: This report includes information from the following map sheet(s). - EW SW S SE NW N NE 1961 0 Miles 0.25 0.5 1 1.5 Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 ECS Southeast, LLP TP, Asheville, 1961, 7.5-minute 5716013 4 8 Historical Topo Map page SITE NAME: ADDRESS: CLIENT: This report includes information from the following map sheet(s). - EW SW S SE NW N NE 1943 0 Miles 0.25 0.5 1 1.5 Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 ECS Southeast, LLP TP, Asheville, 1943, 7.5-minute 5716013 4 9 Historical Topo Map page SITE NAME: ADDRESS: CLIENT: This report includes information from the following map sheet(s). - EW SW S SE NW N NE 1936 0 Miles 0.25 0.5 1 1.5 Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 ECS Southeast, LLP TP, Asheville, 1936, 7.5-minute 5716013 4 10 Historical Topo Map page SITE NAME: ADDRESS: CLIENT: This report includes information from the following map sheet(s). - EW SW S SE NW N NE 1901 0 Miles 0.25 0.5 1 1.5 Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 ECS Southeast, LLP TP, Asheville, 1901, 30-minute 5716013 4 11 Historical Topo Map page SITE NAME: ADDRESS: CLIENT: This report includes information from the following map sheet(s). - EW SW S SE NW N NE 1894 0 Miles 0.25 0.5 1 1.5 Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 ECS Southeast, LLP TP, Asheville, 1894, 30-minute 5716013 4 12 Former P.E. Valve Property 1140 Sweeten Creek RD Asheville, NC 28803 Inquiry Number: 5716013.5 July 16, 2019 The EDR-City Directory Image Report 6 Armstrong Road Shelton, CT 06484 800.352.0050 www.edrnet.comEnvironmental Data Resources IncEnvironmental Data Resources IncEnvironmental Data Resources IncEnvironmental Data Resources Inc TABLE OF CONTENTS SECTION Executive Summary Findings City Directory Images Thank you for your business. Please contact EDR at 1-800-352-0050 with any questions or comments. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OR DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction orforecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2017 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc. or its affiliates is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. EXECUTIVE SUMMARY DESCRIPTION Environmental Data Resources, Inc.’s (EDR) City Directory Report is a screening tool designed to assist environmental professionals in evaluating potential liability on a target property resulting from past activities. EDR’s City Directory Report includes a search of available city directory data at 5 year intervals. RECORD SOURCES EDR's Digital Archive combines historical directory listings from sources such as Cole Information and Dun & Bradstreet. These standard sources of property information complement and enhance each other to provide a more comprehensive report. EDR is licensed to reproduce certain City Directory works by the copyright holders of those works. The purchaser of this EDR City Directory Report may include it in report(s) delivered to a customer. Reproduction of City Directories without permission of the publisher or licensed vendor may be a violation of copyright. RESEARCH SUMMARY The following research sources were consulted in the preparation of this report. A check mark indicates where information was identified in the source and provided in this report. Year Target Street Cross Street Source 2014 þ þ EDR Digital Archive 2010 þ þ EDR Digital Archive 2005 þ þ EDR Digital Archive 2000 þ þ EDR Digital Archive 1995 þ þ EDR Digital Archive 1992 þ þ EDR Digital Archive 1987 þ þ Polk's City Directory 1985 þ ¨Polk's City Directory 1981 þ ¨Polk's City Directory 1975 þ ¨HILLS DIRECTORY CO. 1970 ¨¨Polk's City Directory 1965 ¨¨HILLS DIRECTORY CO. 5716013-5 Page 1 FINDINGS TARGET PROPERTY STREET 1140 Sweeten Creek RD Asheville, NC 28803 Year CD Image Source SWEETEN CREEK RD 2014 pg A1 EDR Digital Archive 2010 pg A3 EDR Digital Archive 2005 pg A6 EDR Digital Archive 2000 pg A9 EDR Digital Archive 1995 pg A11 EDR Digital Archive 1992 pg A13 EDR Digital Archive 1987 pg A15 Polk's City Directory 1987 pg A16 Polk's City Directory 1985 pg A18 Polk's City Directory 1981 pg A19 Polk's City Directory 1975 pg A20 HILLS DIRECTORY CO. 1970 -Polk's City Directory Target and Adjoining not listed in Source 1965 -HILLS DIRECTORY CO.Target and Adjoining not listed in Source 5716013-5 Page 2 FINDINGS CROSS STREETS Year CD Image Source W CHAPEL RD 2014 pg. A2 EDR Digital Archive 2010 pg. A5 EDR Digital Archive 2005 pg. A8 EDR Digital Archive 2000 pg. A10 EDR Digital Archive 1995 pg. A12 EDR Digital Archive 1992 pg. A14 EDR Digital Archive 1987 pg. A17 Polk's City Directory 1985 -Polk's City Directory Target and Adjoining not listed in Source 1981 -Polk's City Directory Target and Adjoining not listed in Source 1975 -HILLS DIRECTORY CO.Target and Adjoining not listed in Source 1970 -Polk's City Directory Target and Adjoining not listed in Source 1965 -HILLS DIRECTORY CO.Target and Adjoining not listed in Source 5716013-5 Page 3 City Directory Images - SWEETEN CREEK RD EDR Digital Archive 5716013.5 Page: A1 SourceTarget Street Cross Street 2014 1026 BRIGGS STANLEY A CUSTOM FURN 1069 JORDAN R L OIL CO OF NC 1072 PEREZ, GUADALUPE 1075 ALAS, WILFREDO ARANA, ANDRES B&M DRYWALL CO CABANAS, NICOLAS A CARBAJAL, HILARIO FAMER, DIANNA GUTIERREZ, JOSUE HERNANDEZ, ISRAEL D HINOJOSA, MANUELA MATEOS, PATRICIA C MENDEZ, RICARDO MENDOZA, DOROTEO E MUNOZ, JUAN PARKER, WILLIAM PHYTHIAN, FREDERICK RUIZ, SERGIO SANTIAGO, GILBERTO SELLARS, CALVIN SPEER, WENDELL J WILSON, MICHAEL A WYATT, HERMAN J 1081 OCCUPANT UNKNOWN, 1116 OCCUPANT UNKNOWN, 1122 CAROLINA DENTAL LAB 1123 PAVONE LLC SENOR CLEAN 1125 MYERS JAMES F III MYERS MOTORCYCLES INC 1129 HD SUPPLY WATERWORKS LTD US FILTER 1130 GEORGES STOR-MOR REALTY LLC 1131 MINDFUL MANAGEMENT LLC NORTH CAROLINA WINE GIFTS LLC 1133 A L ODOM LOCKSMITHS INC DUTCH GIRL COIN LAUNDRY STUM, DARRIAN 1149 ARROWOOD, TIMOTHY W - W CHAPEL RD EDR Digital Archive 5716013.5 Page: A2 SourceTarget Street Cross Street 2014 11 OCCUPANT UNKNOWN, 19 REID, ROBERT J 21 HICKMAN MURRELL C HICKMAN, CHARLES M 23 OCCUPANT UNKNOWN, - SWEETEN CREEK RD EDR Digital Archive 5716013.5 Page: A3 SourceTarget Street Cross Street 2010 1026 BRIGGS STANLEY A CUSTOM FURN 1069 JORDAN R L OIL CO OF NC 1072 PEREZ, GUADALUPE 1075 A DRUG 24 HOUR A ABLE HELPLINE ALVAREZ, RAYMUNDO AQUILAR-BENITEZ, ALBERTO ARANA, ANDRES B&M DRYWALL CO BARCENAS, RICARDO F BENITEZ, ANDRES BENJARAN, LETICIA CABANAS, CONCEPCION CABANAS, NICOLAS A CALDERON-MATEOS, PATRICIA CARBAJAL, HILARIO CORDERO, ELEAZAR CORDOBA, ALEJANDRO CRUZ, GARCIA EWING, FRANCES FRANKLIN, LOU A GOMEZ, DEMETRIO HERNANDEZ ALEX HERNANDEZ, ANGEL HERNANDEZ, ANTONIO LARA, MARIA LOPEZ, ROSA G MARTINEZ, ADOLFO MEJIA, ENCARNACION MENDOZA, DOROTEO E MUNOZ, EDUARDO NAVARRETE, ALEJANOLRO L ORTIZ, LORENZO OSORIO, MARTIN PALESTINA, JUAN PEREZ, ROSARIO QUINONES, GERARDO RAFAEL FLORES RUIZ, SERGIO SANTIAGO, RAUL TIPTON, BARBARA J VAL PAK OF WESTERN NC VAZQUEZ, ALBINO WYATT, HERMAN J 1081 OCCUPANT UNKNOWN, 1083 OCCUPANT UNKNOWN, 1125 MYERS JAMES F III 1129 HD SUPPLY WATERWORKS LTD 1130 MINI STORAGE COMPANY A 1131 A L ODOM LOCKSMITH PRECISION TRUSS COMPANY (Cont'd) - SWEETEN CREEK RD EDR Digital Archive 5716013.5 Page: A4 SourceTarget Street Cross Street 2010 1133 DUTCH GIRL COIN LAUNDRY STUM, DARRIAN 1149 ARROWOOD, TIMOTHY W - W CHAPEL RD EDR Digital Archive 5716013.5 Page: A5 SourceTarget Street Cross Street 2010 11 LOWRY, ANNE 19 REID, ROBERT J 21 HICKMAN, CHARLES M 23 OCCUPANT UNKNOWN, 39 GACS INC 41 DAUGHTERS OF ISIS N & S AMERI - SWEETEN CREEK RD EDR Digital Archive 5716013.5 Page: A6 SourceTarget Street Cross Street 2005 1026 BRIGGS STANLEY A CUSTOM FURN 1069 JORDAN R L OIL CO OF NC 1072 PEREZ, GUADALUPE 1075 ACOSTA, SOFIA AGUIRRE, JOSE A ALAS, WILFREDO ALVAREZ, RAYMUNDO AQUILAR-BENITEZ, ALBERTO B&M DRYWALL CO BAXTER, JEFFREY BELLO, PEDRO A BINUELO, UBALDO A BOMAYE, CARLOS CABANAS, CONCEPCION CABANAS, NICOLAS A CALDERON-MATEOS, PATRICIA CANALES, MARIA CARBAJAL, HILARIO CORTEZ, GUILLERMO CRUZ, GOMEZ EWING, AARON FRANKLIN, LOU A GARCIA, MOISES S GOMEZ, DEMETRIO GUEVARRA, CARMEN GUITERREZ, FRANCISCO GUZMAN, LUIS HERNANDEZ, JOAQUIN L HUANAI, DANITZA LARA, MARIA LARIOS, FRANCISCO LAZARO, MONICA LETICIA, B LOPEZ, ARTURO A LOPEZ, FERMIN MACHADO, SANTOS MARQUEZ, RUBEN H MARTINEZ, ADOLFO MARTINEZ, JOSE L MARTINEZ, MARGARITA MEJIA, ENCARNACION MORALES, ALEJANDRO NAVA, SALVADOR ORTIZ, LUCILA OSORIO, MARTIN PEREZ, ROSARIO PINE VALLEY MOBILE HOME PARK PLANEPANTLA, MARCELINO RAMOS, RICARDO RESENDIZ, RAMIRO (Cont'd) - SWEETEN CREEK RD EDR Digital Archive 5716013.5 Page: A7 SourceTarget Street Cross Street 2005 1075 ROBINSON, DAVID W RODRIGUEZ, GERARDO ROJO, ALEJANDRO ROSAS, RITA RUIZ, ALICIA RUIZ, SERGIO SAAVEDRA, MOISES SERRANO, ROBERTO O SERVIN, AMADOR TIPTON, B J VAL PAK OF WESTERN NC VAZQUEZ, ALBINO VELASQUEZ, FELIPE P WYATT, HERMAN J 1125 MYERS JAMES F III 1129 NATIONAL WATERWORKS INC 1130 SWANN, LARRY R 1133 CENTURY MODIFICATION CORP DUTCH GIRL COIN LAUNDRY EL PROGRESO TIENDA MEXICANA MINIVER CREATIONS INC STUM, DARRIAN 1140 P E VALVE COMPANY INC 1141 FILTER SERVICES OF ASHEVILLE 1149 ARROWOOD, TIMOTHY W - W CHAPEL RD EDR Digital Archive 5716013.5 Page: A8 SourceTarget Street Cross Street 2005 1 MCQUEEN, JEAN B 7 OCCUPANT UNKNOWN, 9 OCCUPANT UNKNOWN, 11 ALLEN, NATASHA D 14 RICHARDSON, RENEE 19 CENTURY HEATING & COOLING OCCUPANT UNKNOWN, 21 OCCUPANT UNKNOWN, 23 PAYNE, JOHN - SWEETEN CREEK RD EDR Digital Archive 5716013.5 Page: A9 SourceTarget Street Cross Street 2000 1026 STANLEY A BRIGGS CUSTOM FURN 1069 JORDAN R L OIL CO OF NC 1075 BARBOZA, GILBERT FAUSTO, G FERNANDEZ, F KENNEDY, DAVID MARTINEZ, F PINE VALLEY MOBILE HOME PARK RAMOS, RICARDO ROBINSON ELECTRONICS ROBINSON, DAVID ROMERO, ELMER B TAYLOR, RICHARD TELLES, LEONOR TELLEZ, JUAN C TIPTON, B J TREJO, RUTH 1087 EXTREME DIGITAL PLANET 1123 B & S AUTO SALES 1125 MYERS JAMES F III 1129 US FILTER DIST GROUP INC 1130 CAROLINA DENTAL LAB 1133 ATWORK PERSONNEL SERVICES INC DIAMOND/TRIUMPH AUTO GLASS RBS GAS INC 1140 P E VALVE COMPANY INC - W CHAPEL RD EDR Digital Archive 5716013.5 Page: A10 SourceTarget Street Cross Street 2000 19 REID, ROBT J 21 HICKMAN, CHARLES - SWEETEN CREEK RD EDR Digital Archive 5716013.5 Page: A11 SourceTarget Street Cross Street 1995 1026 STANLEY A BRIGGS CUSTOM FURN 1061 PRESSLEY, WAYNE A 1065 OCCUPANT UNKNOWNN 1075 BANKS, DAWN BUCHANAN, J CLAYTON, ROBERT DUNCAN, BRENDA M DUZYK, SONYA ESTRADA, B GAGNE, GARY GRAHAM, SUSAN LAUGHTER, DORIS MASSEY, S A NORRIS, WAKINA PARKER, WAYNE PINE VALLEY MOBILE HOME PARK REESE, JACK SAPPENFIELD, RICHARD L JR SNYDER, KAREN STEPHEN, EDWARD L TIPTON, B J TOPPING, L N WORLEY, EARL D 1077 OCCUPANT UNKNOWNN 1085 APPLIANCE SHOP DUNHAMS TV SERVICE OCCUPANT UNKNOWNN 1125 MYERS JAMES F III MYERS, JAMES F III 1127 OCCUPANT UNKNOWNN 1129 WATERPRO SUPPLIES CORPORATION 1130 MINI STORAGE COMPANY A OCCUPANT UNKNOWNN 1131 TRAVELHOST MAGAZINE 1133 HACO LEASING CORPORATION PLUMBING STORE RBS GAS INC THREE BEARS INC 1135 OCCUPANT UNKNOWNN 1137 ALL AMERICAN HOME IMPRV CO SIMULA INC 1139 COCAMO TANNING SALON MYERS BILL FABRICS INC 1140 P E PRODUCT ENGINEERING CORP 1145 SAINT NICHOLAS ORTHODOX CHURCH 1149 ARROWOOD, TIMOTHY W 1151 OCCUPANT UNKNOWNN - W CHAPEL RD EDR Digital Archive 5716013.5 Page: A12 SourceTarget Street Cross Street 1995 11 DEAL, MELVIN 19 REID, ROBT J 20 RICE, GEORGE S 21 HICKMAN, CHARLES 23 PAYNE, WILLARD D - SWEETEN CREEK RD EDR Digital Archive 5716013.5 Page: A13 SourceTarget Street Cross Street 1992 1026 STANLEY A BRIGGS CUSTOM FURN 1061 PRESSLEY, WAYNE A 1065 PRESSLEY, ALMA M 1075 CLEMENTS, MELISSA DRYE, J A FERGUSON, CHERYL L GIPSON, DARREN GOSS, BEN KINNEY, P M PRICE, MARK ROBINSON, STACEY D SNYDER, KAREN SWAN, NELL TIPTON, B J WHITFIELD, RONALD J 1083 JARAMILLO, B V 1125 JAMES F MYERS III MYERS, JAMES F III 1127 LENTZ, B T 1130 MINI STORAGE COMPANY A 1137 CROWN ASSET RECOVERY CORP SHER PLEASER DISIGN 1139 MYERS BILL FABRICS INC 1140 P E PRODUCT ENGINEERING CORP 1147 CARNER, DELBERT WASHBURN, CHRIS 1149 ARROWOOD, TIMOTHY W - W CHAPEL RD EDR Digital Archive 5716013.5 Page: A14 SourceTarget Street Cross Street 1992 21 HICKMAN, CHARLES - SWEETEN CREEK RD Polk's City Directory 5716013.5 Page: A15 SourceTarget Street Cross Street 1987 - SWEETEN CREEK RD Polk's City Directory 5716013.5 Page: A16 SourceTarget Street Cross Street 1987 - W CHAPEL RD Polk's City Directory 5716013.5 Page: A17 SourceTarget Street Cross Street 1987 - SWEETEN CREEK RD Polk's City Directory 5716013.5 Page: A18 SourceTarget Street Cross Street 1985 - SWEETEN CREEK RD Polk's City Directory 5716013.5 Page: A19 SourceTarget Street Cross Street 1981 - SWEETEN CREEK RD HILLS DIRECTORY CO. 5716013.5 Page: A20 SourceTarget Street Cross Street 1975 Appendix V:Site Photographs 1 -A view of the subject property facing south. 2 -A view of a transformer located on the subject property. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-A 3 -A view of West Chapel Road followed by Sunset Cemetery located north, facing north. 4 -A view of an open field and wooded land located east, facing south. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-A 5 -A view of a residence located south, facing southeast. 6 -A view of Sweeten Creek Road followed by the Car Dr and Crossroads Towing located west, facing southwest. August 29, 2019 ECS Southeast, LLP ECS Project #49: 7572-A Appendix VI:Statement of Qualifications REGISTRATIONS Certified Hazardous Materials Manager: CHMM OSHA: 20 CFR 1910.146, Confined Space Entry, Attendant, 8-Hour; OSHA: 29 CFR 1910.120, HAZWOPER, 40-Hour; EPA Accredited Lead Inspector South Carolina Certified Lead-Based Paint Professional AHERA: Accredited Asbestos Building Inspector SC: Asbestos Building Inspector FEMA: National Incident Management Systems Awareness SKILLS Phase I Environmental Site Assessments Phase II Environmental Site Assessments Hazardous Material Surveys Asbestos and Lead-Based Paint Surveys Remediation EDUCATION Bachelor of Science, 2004, Ecology, West Chester University ENVIRONMENTAL PRINCIPAL/ ENVIRONMENTAL REGIONAL MANAGER JUSTIN ROTH, CHMM Mr. Roth started in 2005 with ECS as an Environmental Scientist and is currently a Regional Manager of Environmental Services for ECS. Responsibilities include profit & loss analysis, budget control, scheduling, resource allocation, client interaction and invoicing for environmental projects. He provides technical supervision, technical review and regulatory support, as well as, construction support from the field and office. Additional responsibilities include performing and managing Phase I, II & III Environmental Site Assessments, management and performance of hazardous and non-hazardous materials surveys to include asbestos and lead-based paint surveys, remediation, abatement monitoring, conducting underground storage tank investigations, National Environmental Policy Act surveys, State Historic Preservation Offices studies, site characterization, risk assessment, remedial design and implementation, rare species surveys and wetland delineations. PROFESSIONAL PROFILE • Proposed Meeting & Lee Street Redevelopment, Charleston, SC - This project consisted of the performance and coordination of Phase I & II Environmental Site Assessments associated with a half city block project area. The project site included several former residential dwellings, two former gasoline service stations, and an adjacent former drycleaning operation. Upon completion of the Phase I ESA, ECS assisted with the preparation and submittal of a South Carolina Department of Health and Environmental Control (SC DHEC) Voluntary Cleanup Contract (VCC) application. The application was approved and Work Plans were prepared in preparation of additional work necessary to fulfill the VCC. • Sumter Dialysis Tier I Assessment, SC - This project consisted of a Phase I & II Environmental Site Assessment, including soil and groundwater sampling associated with redevelopment of the site. A remnant heating oil underground storage tank was also discovered for which ECS completed removal & remediation activities as well as a Tier 1 Assessment associated with identified groundwater impact. • Proposed Retail Store IGWA - This project consisted of Phase I & II Environmental Site Assessments, hazardous materials surveys, and an Initial Groundwater Assessment (IGWA) associated with suspected groundwater impact from an underground storage tank release. PROJECT EXPERIENCE ™ Don Marlor ENVIRONMENTAL TECHNICIAN REGISTRATIONS PROFESSIONAL PROFILE Mr. Marlor is an Environmental Technician for ECS. He has over 5 years of experience in the construction field, and over 1.5 years of experience in the environmental consulting field. This includes a variety of project experience for environmental assessment. His present responsibilities include site assessment, reporting, and client development for the Asheville Branch Office of ECS. Additional experience includes field support and inspections on projects ranging from Brownfields Program to construction material and soil testing. PROJECT EXPERIENCE • Former Drexel Facility Brownfields Site, Marion, NC • McDowell Concrete Plant Site Phase I ESA, Marion, NC • Biltmore Iron & Metal Phase I ESA and Groundwater/Soil Assessment, Hendersonville, NC • FCE#1426 Shell Gasoline Station Groundwater Assessment, Hendersonville, NC • Camp Golden Valley Groundwater Assessment, Nebo, NC • Reynolds Mountain Landfill Groundwater Sampling, Woodfin, NC ™ ACI Concrete Testing M40-Hour HAZWOPER SKILLS Phase I Environmental Site Assessments Soil and Groundwater Assessments Field Support and Inspections EDUCATION Bachelor of Science, Geology, 2017 Western Carolina University Cullowhee, NC Appendix VII:Acronyms ACRONYMS AUL Activity and Use Limitations AST Aboveground Storage Tank ASTM American Society for Testing and Materials ACM Asbestos Containing Materials BER Business Environmental Risk CORRACTS CERCLA Corrective Action List NPL CERCLA National Priorities List NFRAP CERCLA No Further Remedial Action Planned CERCLA Comprehensive Environmental Response Cleanup Liability Act CESQG Conditionally Exempt Small Quantity Generator CREC Controlled Recognized Environmental Condition ERNS Emergency Response Notification System EC Engineering Controls HIST LF Historical Landfill HREC Historical Recognized Environmental Condition IC Institutional Controls LQG Large Quantity Generator LBP Lead Based Paint LTANKS Leaking Tanks LUST Leaking Underground Storage Tank REC Recognized Environmental Condition RCRA Resource Conservation and Recovery Act RCRIS Resource Conservation and Recovery Information System SQG Small Quantity Generator SWF/LF Solid Waste Facility/Landfill SHWS State Hazardous Waste Sites UST Underground Storage Tank USGS United States Geological Survey