22074_Gathing Motors_Final BR Foundation Soil (East Office Tower) Report

‘Wood’ is a trading name for John Wood Group PLC and its subsidiaries
REPORT OF SOIL CHARACTERIZATION FOR BENEFICIAL REUSE
FOUNDATION SOIL (EAST OFFICE BUILDING)
FORMER GATHINGS MOTOR COMPANY
1100 and 1200 South Tryon Street
Charlotte, North Carolina
Brownfields Project Number 22074-18-060
PREPARED FOR:
TRYON STREET INVESTORS, LLC
Care of Spectrum Development Company, LLC
300 South Tryon Street, Ste. 200
Charlotte, North Carolina 28202
PREPARED BY:
WOOD ENVIRONMENT & INFRASTRUCTURE SOLUTIONS,INC.
2801 Yorkmont Road, Suite 100
Charlotte, North Carolina 28208
February 10, 2020
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number:6228-18-0495
ii
TABLE OF CONTENTS
1.0 PROJECT INFORMATION AND PURPOSE...........................................................................................................................1
2.0 ASSESSMENT ACTIVITIES..........................................................................................................................................................2
2.1 Boring Layout and Underground Utility Survey............................................................................2
2.2 Soil Sampling and Analyses...........................................................................................................2
3.0 RESULTS...........................................................................................................................................................................................4
3.1 Volatile Organic Compounds ........................................................................................................4
3.2 Semi-Volatile Organic Compounds ...............................................................................................5
3.3 Total Metals ..................................................................................................................................5
4.0 CONCLUSIONS AND RECOMMENDATIONS.....................................................................................................................6
LIST OF TABLES
Table 1 Summary of Field Screening Results
Table 2 Summary of Detected Volatile Organic Compounds (VOC) Analytical Results
Table 3 Summary of Detected Semi-Volatile Organic Compounds (SVOCs) and Total Metals
Analytical Results
LIST OF FIGURES
Figure 1 Site Topo
Figure 2 Beneficial Reuse Characterization-Foundation Soil (East Office Tower)
Figure 3 Summary of Analytical Results
Figure 4 Proposed Soil Borings
LIST OF APPENDICES
Appendix Laboratory Analytical Reports and Chain-of-Custody Forms
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number:6228-18-0495
1
1.0 PROJECT INFORMATION AND PURPOSE
The subject site consists of four parcels encompassing approximately 4.9 acres situated at the intersection
of South Tryon Street and West Carson Boulevard in Charlotte, North Carolina (Figure 1). Under separate
work plans, Wood previously performed shallow and deep soil characterization of soil that was to be
generated during the construction of the proposed West Office Tower and Parking Garage on the western
and southern portions of the site, respectively, and soil characterization of shallow soil that will be
disturbed during planned grading activities of the proposed East Office Tower on the eastern portion of
the site.
Historical information reviewed by Wood indicates that the land area to be redeveloped as the East Office
Tower was formerly occupied by a gasoline station (Top Gas &Oil, 1100 and 1120 South Tryon Street)
from at least 1960 to 1986. Review of a regulatory database report revealed that the site was identified on
the leaking underground storage tank (LUST) and underground storage tank (UST) lists. The site was also
identified on the Historical Auto Stations list as Tops of Charlotte (1100 & 1120 South Tryon Street) for
the years 1959, 1964, 1969, 1974, 1979 and 1984.
The Prospective Developer (PD) recently provided information regarding the location and diameter of
piles that will be drilled during the proposed East Office Tower which will eventually be constructed on the
eastern portion of the site.The approximate 2-foot diameter shafts will be filled with cement. During
drilling of the boreholes for the piles, it is estimated that 5,000 cubic yards of soil, weathered rock and
possibly bedrock will be removed. Wood prepared an Environmental Management Plan (EMP), which was
approved by the North Carolina Department of Environmental Quality (NCDEQ), Division of Waste
Management (DWM), Brownfields Program (BFP) on April 25, 2019. The EMP specified a plan for field
screening and analytical characterization of the material to be generated during foundation drilling. The
EMP was based on the soil generated during foundation drilling being field screened. Based on the field
screening, samples of soil would be retained for analysis of Volatile Organic Compounds (VOCs).
Subsequently, the soil “cuttings” would be stockpiled at the site and one composite samples of soil was to
be collected per every 1,000 cubic yards for analysis of Semi-Volatile Organic Compounds (SVOCs) and
metals.
Later, Wood personnel were provided with information from the construction team that suggested field
screening and analytical characterization during foundation drilling would not be feasible due to space
and time constraints. Therefore, Wood prepared a work plan for soil characterization to be performed
prior to the start of foundation drilling. The NCDEQ BFP approved the work plan in a letter (dated
December 20, 2019)
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte,North Carolina
Wood Project Number: 6228-18-0495
2
The assessment activities were performed in general accordance with the most recent Inactive Hazardous
Sites Branch (IHSB) Program Guidelines for Assessment and Cleanup
(https://files.nc.gov/ncdeq/Waste%20Management/DWM/SF/IHS/guidance/IHSB_RemediationGuidance01
2720.pdf) dated January 2020 and the most recent versions of the U.S. Environmental Protection Agency
(EPA) Region IV Science and Ecosystem Support Division (SESD) Field Branches Quality System and
Technical Procedures guidance.
2.0 ASSESSMENT ACTIVITIES
2.1 Boring Layout and Underground Utility Survey
In the work plan, Wood proposed to advance ten soil borings at locations shown on Figure 2 on the
eastern portion of the site.The boring locations were approved by the BFP and were marked in the field
and recorded on a Trimble GeoExplorer XH 6000 Series hand-held Global Positioning System (GPS) unit
for future reference. The purpose of advancing the borings was to collect representative samples of in-situ
soil beginning at the existing grade to the approximate depths planned for the pile shafts. The locations
selected by Wood for the 10 borings are generally within proposed “pile caps” where three or more pile
shafts will be drilled since those areas represent areas from which larger volumes of “cuttings” will be
generated.The selected areas were also “biased” toward the north-northeastern portion of the proposed
building area since previous exploration in this area identified petroleum-affected soil and groundwater
related to the former Top Gas & Oil (Incident #40460).The purpose of the soil characterization is to
evaluate if concentrations of contaminants are identified in the soil to be exported that exceed the
Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) for Residential or
Protection of Groundwater (PoG).
Prior to conducting the soil assessment activities, Wood contacted the North Carolina 811 public
underground utility location service. Furthermore,on December 5, 2019, Wood personnel visited the site
to perform Ground-Penetrating Radar (GPR) and Electromagnetic (EM) surveys to attempt to detect
metallic objects such as pipes, tanks or underground utility lines. The purpose of this effort was to
minimize the potential for probing into underground utilities buried at the properties.
2.2 Soil Sampling and Analyses
On December 26 and 27, 2019, Wood personnel and Geologic Exploration (GEX), our probing
subcontractor licensed in the State of North Carolina, mobilized to the site to advance eight of the ten soil
borings approved by the BFP.Two of the ten soil borings (PG-24 and PG-28)were not advanced due to
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte,North Carolina
Wood Project Number: 6228-18-0495
3
equipment issues and time restraints.GEX advanced a MacroCore®soil sampler at five-foot intervals to
depths ranging from 33 to 46 feet below existing grade, at which depths probe refusal was encountered
using a Geoprobe®8040DT direct-push rig.To minimize the potential for cross-contamination between
samples, a new polyvinyl chloride (PVC) sleeve (liner) was inserted into the sampler for each five-foot
interval.Wood field personnel collected soil cores from the disposable liners and recorded visual and
olfactory observations relative to the soil. The soil types encountered in the borings were recorded as field
soil boring logs.
To select “discrete” samples retained for analysis of VOCs, Wood personnel donned a new pair of nitrile
gloves and split the soil core longitudinally. A representative portion of one-half of the sample was placed
directly in VOC sample containers and a representative portion of the remaining half was placed in a re-
sealable plastic bag and screened in the field using an Organic Vapor Analyzer (OVA) equipped with a
flame ionization detector (FID). Wood’s environmental professionals performed the field screening of the
headspace vapors in each bag to evaluate the presence of VOCs. The purpose of the screening was to
assist with selection of a depth interval to collect one “discrete” soil sample for laboratory analysis of
VOCs from each boring. The field screening results for each depth interval from each of the eight borings
were recorded on the field boring logs and were tabulated for this report (Table 1).The results of the field
screening ranged from 0.07 to 15,600 parts per million (ppm).For each soil boring,a “discrete”soil sample
was collected from the depth interval that exhibited the highest FID reading,placed in laboratory
provided containers, placed in a cooler with ice and shipped to Con-Test Analytical Laboratory (Con-Test)
in East Longmeadow, Massachusetts for analysis of VOCs using EPA Method 8260D. A total of eight soil
samples were retained for VOCs analysis.Selected “discrete” sample depths and screening data for each
boring are also included in Table 1.
Regarding the samples that were retained for analysis of SVOCs, total metals and hexavalent chromium
[Cr(VI)], the remaining portions of each five-foot soil core were collected from each boring and placed
into laboratory containers by Wood personnel. Wood personnel labeled and grouped the “discrete” soil
samples from each boring. These “discrete” samples were placed in a cooler with ice and shipped to Con-
Test with instructions for preparing one “composite” sample per boring. Con-Test laboratory personnel
combined the “discrete” samples in the laboratory and placed the “composite” soil samples into
laboratory containers for analysis of SVOCs by EPA Method 8270E, Resource Conservation and Recovery
Act (RCRA) Metals (total) by EPA Method 6020/7471 and Cr(VI)by Method 7199 to speciate the identified
chromium as hexavalent, if present. The VOC, SVOC and metals soil samples were maintained under a
chain-of-custody protocol. One soil field duplicate QA/QC sample was collected for analysis of VOCs
(Dup-122719) and one QA/QC sample was collected for analysis of SVOCs and RCRA metals (DUP-COMP).
One trip blank for VOC analysis was also analyzed for VOCs.
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte,North Carolina
Wood Project Number: 6228-18-0495
4
Following the completion of the soil sampling activities, the borings were backfilled with the soil cores
and/or bentonite to the ground surface.
3.0 RESULTS
The results of the laboratory analysis are summarized on Tables 2 and 3. The laboratory reports and
chain-of-custody forms are included as an Appendix to this report. The following subsections include
discussion of the findings.
3.1 Volatile Organic Compounds
The results of the laboratory analysis for VOCs are summarized on Table 2 and shown on Figure 3.No
detectable concentrations of VOCs were identified in the “discrete” samples collected from borings PG-21,
PG-22 and PG-23. Several VOC concentrations were identified in the samples collected from borings PG-
25,PG-26 and PG-27. However, none of the concentrations exceeded their respective IHSB PSRGs.
Furthermore,five of the concentrations were J-flagged, indicating the concentrations were identified at a
level above the method detection limit (MDL), but below the reporting limit (RL) and is considered an
estimate.
Concentrations of VOCs were identified in the samples collected from borings PG-29 and PG-30 that
exceeded the applicable PSRGs. These findings are summarized as follows:
The concentration of ethylbenzene identified in the soil sample collected from boring PG-29
exceeded the IHSB Residential Health-Based, Industrial/Commercial Health-Based and PoG
PSRGs.
The concentrations of naphthalene and 1,2,4-trimethylbenzene identified in the soil sample
collected from boring PG-29 exceeded their respective IHSB Residential Health-Based and PoG
PSRGs.
The concentrations of benzene, n-butylbenzene, isopropylbenzene, p-isopropyltoluene, n-
propylbenzene, 1,3,5-trimethylbenzene, m&p xylene, and o-xylene identified in the soil sample
collected from boring PG-29 exceeded their respective IHSB PoG PSRGs.
The concentrations of ethylbenzene and naphthalene identified in the soil sample collected from
boring PG-30 exceeded their respective IHSB Residential Health-Based and PoG PSRGs.
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte,North Carolina
Wood Project Number: 6228-18-0495
5
The concentrations of n-butylbenzene, isopropylbenzene, n-propylbenzene, 1,2,4-
trimethylbenzene,1,3,5-trimethylbenzene and m&p xylene identified in the soil sample collected
from boring PG-30 exceeded their respective IHSB PoG PSRGs.
3.2 Semi-Volatile Organic Compounds
The results of the laboratory analysis for SVOCs are summarized on Table 3 and shown on Figure 3.No
detectable concentrations of SVOCs were identified in the “composite” samples collected from borings
PG-21,PG-22,PG-23,PG-25,PG-26 and PG-27. Several SVOC concentrations were identified in the
“composite” samples collected from borings PG-29 and PG-30.However,with the exception of 1-
methylnaphthalene,none of the concentrations identified in the samples collected from borings PG-29
and PG-30 exceeded their respective IHSB PSRGs.The concentration of 1-methylnaphthalene identified in
samples COMP-PG29 and COMP-PG30 was J-flagged and exceeded the IHSB PoG PSRG.
3.3 Total Metals
The results of the laboratory analysis for total metals are summarized on Table 3 and shown on Figure 3.
The analysis identified the following:
Varying concentrations of total barium, cadmium, lead, mercury, selenium and silver were
identified in the “composite”soil samples collected for this assessment. None of the
concentrations exceeded their respective the IHSB PSRGs.
Detectable concentrations of total arsenic ranging from 0.24 milligrams per kilogram (mg/kg)to
0.94 mg/kg were identified in the “composite” soil samples collected for this assessment.The
concentrations detected in soil samples collected from borings PG-27 and PG-29 exceeded the
IHSB Residential Health-Based PSRG of 0.68 mg/kg, but did not exceed the IHSB
Industrial/Commercial Health-Based or PoG PSRGs. According to published literature, these
concentrations are within or below the typical range of “naturally-occurring” arsenic levels in soil
in the Piedmont of North Carolina.
Detectable concentrations of total chromium ranging from 4.7 to 82 mg/kg were identified in the
“composite” soil samples collected for this assessment.In addition,detectable concentrations of
Cr(VI)were identified in the “composite” samples collected from borings PG-27 and PG-29.
Furthermore, the concentration of Cr(VI)identified in the sample collected from boring PG-29
exceeded the IHSB Residential Health-Based PSRG.Please note, the concentrations of Cr(VI)
identified were J-flagged, indicating the concentrations were identified at a level above the MDL,
but below the RL and are considered estimates.According to published literature, the
concentrations of total chromium identified in the “composite” samples are within the typical
range of “naturally-occurring”chromium levels in soil in the Piedmont of North Carolina.
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte,North Carolina
Wood Project Number: 6228-18-0495
6
4.0 CONCLUSIONS AND RECOMMENDATIONS
Based on the findings of this assessment, Wood offers the following conclusions and recommendations:
Geoprobe®refusal was encountered at depths ranging from 33 to 46 feet bgs in the eight borings
advanced during this assessment.The borings did not encounter areas of debris fill that should
not be considered soil.Based on field screening data, eight “discrete” soil samples (one from each
boring) were retained for laboratory analysis of VOCs.
Concentrations of ethylbenzene, naphthalene, and 1,2,4-trimethylbenzene were identified in the
“discrete”sample collected from boring PG-29 which exceeded their respective IHSB Residential
Health-Based PSRGs. In addition, the concentration of ethylbenzene exceeded the IHSB
Industrial/Commercial Health-Based PSRG. Furthermore, the concentrations of naphthalene and
ethylbenzene identified in the “discrete”sample collected from boring PG-30 exceeded their
respective IHSB Residential Health-Based PSRGs. Based on the results of the VOC analysis,
additional borings should be advanced to collect soil samples from pile group locations
surrounding borings PG-29 and PG-30 to further delineate pile groups in which VOC-affected soil
may be encountered. The proposed boring locations are shown on Figure 4.
“Discrete”soil samples from the eight borings were used to prepare eight “composite”soil
samples for analysis of SVOCs and total metals.Concentrations of 1-methylnaphthalene were
identified in two of the soil samples that exceed the IHSB PoG PSRG.The total metals analysis
identified detectable metal concentrations in the “composite” soil samples collected for this
assessment.However, these concentrations are within are within the typical range of “naturally-
occurring”metal levels in soil in the Piedmont of North Carolina.
A detectable concentration of Cr(VI)was identified in the “composite”sample collected from
boring PG-29 which exceeded the IHSB Residential Health-Based PSRG.The valence states for
chromium range from -2 to +6, but in natural environments, it is generally found as trivalent
chromium [Cr (III)]or Cr(VI).Cr(VI)is often associated with industrial processes. No information is
available that suggests Cr(VI)was used or generated at the site.It is Wood’s opinion that the
Cr(VI)identified in the soil samples represent naturally-occurring chromium of the +6 valence
state.
Based on the results of this assessment,the foundation soil in the area of the proposed East
Office Tower could be used as fill material at the site or transported to another Brownfields
property (contingent on approval of the BFP and property owner/recipient) if the use of the
affected soil as beneficial fill will not increase the potential for risk to human health at that site.
Furthermore, the BFP may approve relocation of material that meets the Beneficial Fill Rule to
non-Brownfields properties.
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte,North Carolina
Wood Project Number: 6228-18-0495
TABLES
Boring ID "Discrete" Soil
Sample ID
Date
Collected
Time
Collected
Depth
Collected
OVA
Readings Notes
PG-21-5 9:40 5 2.40
PG-21-10 9:45 10 2.61 PG-21 VOC sample collected at 9:45
PG-21-15 9:50 15 2.15
PG-21-20 9:55 20 1.87
PG-21-25 10:00 25 2.36
PG-21-30 10:05 30 2.07
PG-21-35 10:10 35 1.37
PG-21-40 10:15 40 0.65
PG-21-42 10:20 42 2.06
PG-22-5 16:10 5 5.72
PG-22-10 16:15 10 6.18 PG-22 VOC sample collected at 16:15
PG-22-15 16:20 15 3.71
PG-22-20 16:25 20 2.98
PG-22-25 16:30 25 0.85
PG-22-30 16:35 30 1.27
PG-22-35 16:40 35 1.39
PG-22-40 16:45 40 1.64
PG-22-43 16:50 43 0.96
PG-23-5 11:00 5 3.84
PG-23-10 11:05 10 4.06 PG-23 VOC sample collected at 11:05
PG-23-15 11:10 15 2.12
PG-23-20 11:15 20 1.96
PG-23-25 11:20 25 1.65
PG-23-30 11:25 30 2.17
PG-23-35 11:30 35 1.11
PG-23-36 11:35 36 0.57
PG-25-5 9:55 5 1.10
PG-25-10 10:00 10 1.10
PG-25-15 10:05 15 1.12
PG-25-20 10:10 20 1.11
PG-25-25 10:15 25 1.26 PG-25 VOC sample collected at 10:15;
PG-25-30 10:20 30 1.03 DUP-122719 collected at 10:15
PG-25-35 10:25 35 0.86
PG-25-40 10:30 40 1.20
PG-25-45 10:35 45 1.01
PG-25-46 10:40 46 0.79
PG-26-5 13:35 5 1.43
PG-26-10 13:40 10 1.15
PG-26-15 13:45 15 1.27
PG-26-20 13:50 20 1.21
PG-26-25 13:55 25 1.79 PG-26 VOC sample collected at 13:55
PG-26-30 14:00 30 0.51
PG-26-35 14:05 35 1.41
PG-26-37 14:10 37 1.23
PG-27-5 14:55 5 0.07
PG-27-10 15:00 10 1.86
PG-27-15 15:05 15 1.85
PG-27-20 15:10 20 2.01
PG-27-25 15:15 25 1.07
PG-27-30 15:20 30 4.07
PG-27-33 15:25 33 6.35 PG-27 VOC sample collected at 15:25
PG-29-5 12:55 5 7.50
PG-29-10 13:00 10 63.22
PG-29-15 13:05 15 60.11
PG-29-20 13:10 20 219
PG-29-25 13:15 25 15,600 PG-29 VOC sample collected at 13:15
PG-29-30 13:20 30 79.63
PG-29-34 13:25 34 59.86
PG-30-5 13:50 5 14.55
PG-30-10 13:55 10 23.22
PG-30-15 14:00 15 46.33
PG-30-20 14:05 20 76.67
PG-30-25 14:10 25 8,967 PG-30 VOC sample collected at 14:10
PG-30-30 14:15 30 545
PG-30-34 14:20 34 73.50
Notes:
1. Depths shown in feet below ground surface (bgs)Prepared By/Date:MAS 1/8/2020
2. OVA readings shown in parts per million (ppm)Checked By/Date:AJF 1/30/2020
3. OVA = Organic Vapor Analyzer (Field screening performed using a Foxboro Thermo TVA 1000 with Flame Ionization Detector)
4. VOC = Volatile organic compound
PG-29 12/27/2019
PG-30 12/27/2019
Table 1: Summary of Field Screening Results - Foundation Soil (East Office Tower)
Former Gathings Motor Company
Charlotte, North Carolina
Brownfields Project Number: 22074-18-060
Wood Project Number: 6228-18-0495
PG-25 12/27/2019
PG-26 12/26/2019
PG-27 12/26/2019
PG-21 12/26/2019
PG-22 12/26/2019
PG-23 12/26/2019
Sample ID PG-21-10 PG-22-10 PG-23-10 PG-25-25 PG-26-25 PG-27-33 PG-29-25 PG-30-25 DUP-122719
Sample Depth 5-10 5-10 5-10 20-25 20-25 28-33 20-25 20-25 20-25
Date Sampled 12/26/2019 12/26/2019 12/26/2019 12/27/2019 12/26/2019 12/26/2019 12/27/2019 12/27/2019 12/27/2019
Benzene <0.0026 <0.0025 <0.0025 <0.0031 <0.0027 0.0093 0.62 J <0.70 <0.0028 1.2 5.4 0.01
n-Butylbenzene <0.0026 <0.0025 <0.0025 <0.0031 <0.0027 <0.0029 9.4 4.6 <0.0028 780 12,000 4.5
sec-Butylbenzene <0.0026 <0.0025 <0.0025 <0.0031 <0.0027 <0.0029 1.7 J 0.97 <0.0028 1,600 23,000 4.1
Chloroform <0.0053 <0.0051 <0.0051 0.0022 J <0.0055 <0.0058 <4.1 <1.4 0.0022 J 0.34 1.5 0.39
Ethylbenzene <0.0026 <0.0025 <0.0025 <0.0031 <0.0027 <0.0029 66 26 <0.0028 6.1 27 13
Isopropylbenzene (Cumene)<0.0026 <0.0025 <0.0025 <0.0031 <0.0027 0.0015 J 4.7 2.4 <0.0028 410 2,100 2.3
p-Isopropyltoluene (p-Cymene)<0.0026 <0.0025 <0.0025 <0.0031 <0.0027 <0.0029 1.4 J 0.60 J <0.0028 NE NE 1.24
Naphthalene <0.0053 <0.0051 <0.0051 <0.0062 <0.0055 0.0070 9.0 4.1 <0.0057 4.1 18 0.39
n-Propylbenzene <0.0026 <0.0025 <0.0025 <0.0031 <0.0027 <0.0029 19 9.5 <0.0028 780 5,100 2.6
1,2,4-Trimethylbenzene <0.0026 <0.0025 <0.0025 <0.0031 0.0016 J 0.021 120 56 <0.0028 63 370 12
1,3,5-Trimethylbenzene <0.0026 <0.0025 <0.0025 <0.0031 <0.0027 0.0028 J 33 16 <0.0028 56 320 11
m&p Xylene <0.0053 <0.0051 <0.0051 <0.0062 0.0026 J 0.023 82 34 <0.0057 240 1,020 19.6
o-Xylene <0.0026 <0.0025 <0.0025 <0.0031 <0.0027 <0.0029 68 5.3 <0.0028 140 590 9.8
Notes:
1. Concentrations shown in milligrams per kilogram (mg/kg)Prepared By/Date:MAS 1/15/2020
2. Depths shown in feet below ground surface (bgs)Checked By/Date:AJF 1/30/2020
3. Constituents detected above Reporting Limit and J-flagged results are shown, see laboratory analytical report for full constituent list
4. PSRGs = North Carolina Department of Environmental Quality, Inactive Hazardous Sites Branch, Preliminary Soil Remediation Goals, dated December 2019
5. NE = Not established
6. J = Indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate
7.Bold font indicates identified concentration exceeded Protection of Groundwater PSRG
8.Bold font and shaded GOLD indicates identified concentration exceeded Protection of Groundwater and Residential PSRGs
9.Bold font and shaded BLUE indicates identified concentration exceeded Protection of Groundwater, Residential, and Industrial/Commercial PSRGs
10. DUP-122719 collected from parent sample PG-25-25
Brownfields Project Number: 22074-18-060
Charlotte, North Carolina
Former Gathings Motor Company
Table 2: Summary of Detected Volatile Organic Compounds (VOCs) Analytical Results - Foundation Soil (East Office Tower)
Residential
Health-Based
PSRGs
Industrial/
Commercial
Health-Based
PSRGs
Protection of
Groundwater
PSRGs
Wood Project Number: 6228-18-0495
Sample ID COMP-PG21 COMP-PG22 COMP-PG23 COMP-PG25 COMP-PG26 COMP-PG27 COMP-PG29 COMP-PG30 DUP-COMP
Sample Depth 0-42 0-40 0-36 0-46 0-37 0-33 0-34 0-34 0-42
Date Sampled 12/26/2019 12/26/2019 12/26/2019 12/27/2019 12/26/2019 12/26/2019 12/27/2019 12/27/2019 12/26/2019 Range Mean
1-Methylnaphthalene <0.24 <0.23 <0.23 <0.24 <0.21 <0.24 0.15 J 0.14 J <0.24 18 73 0.11
2-Methylnaphthalene <0.24 <0.23 <0.23 <0.24 <0.21 <0.24 0.34 0.34 <0.24 48 600 3.1
Naphthalene <0.24 <0.23 <0.23 <0.24 <0.21 <0.24 0.21 J 0.25 <0.24 4.1 18 0.39
Arsenic 0.28 0.36 0.34 0.34 0.24 0.94 0.70 0.50 0.25 0.68 3.0 5.8 1.0-40**NS
Barium 180 200 150 180 68 88 120 78 300 3,100 47,000 580 50-1000 356
Cadmium 0.029 J 0.075 J 0.047 J 0.035 J <0.42 <0.47 <0.46 <0.42 0.052 J 14 200 3.0 0.01-7.0**NS
Chromium 9.2 9.8 6.9 4.7 J 4.9 J 82 65 14 7.7 23,000 350,000 360,000 7-300 65
Lead 7.2 8.9 7.6 9.0 6.5 9.7 7.2 6.5 5.9 400 800 270 2-200**NS
Mercury <0.034 0.012 J <0.034 0.011 J 0.078 0.015 J 0.015 J 0.027 J <0.037 2.3 9.7 1.0 0.03-0.52 0.121
Selenium <1.9 <1.8 <1.8 <1.9 <1.7 <1.9 <1.8 <1.7 <1.9 78 1,200 2.1 <0.1-0.8 0.42
Silver 0.042 J 0.034 J 0.033 J 0.030 J <0.10 0.065 J 0.032 J 0.039 J 0.032 J 78 1,200 3.4 NS NS
Hexavalent Chromium <0.255 <0.255 <0.255 <0.255 <0.255 0.298 J 0.684 J <0.255 <0.255 0.31 6.5 3.8 NS NS
Notes:
1. Concentrations shown in milligrams per kilogram (mg/kg)Prepared By/Date:MAS 1/16/2020
2. Depths shown in feet below ground surface (bgs)Checked By/Date:AJF 1/30/2020
3. Constituents detected above Reporting Limit and J-flagged results are shown, see laboratory analytical report for full constituent list
4. PSRGs = North Carolina Department of Environmental Quality, Inactive Hazardous Sites Branch, Preliminary Soil Remediation Goals, dated December 2019
5. NS = Not specified
6. J = Indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate
7.Bold font indicates identified concentration exceeded Protection of Groundwater PSRG
8.Bold font and shaded GREEN indicates identified concentration exceeded Residential PSRG, these concentrations reflect "naturally occurring" metals in soil
9. DUP-COMP collected from parent sample COMP-PG21
* Range and mean values for "Background Metals for North Carolina Soils" taken from Elements in North American Soils by Dragun and Chekiri, 2005
** Typical Range of "Native Soil Concentrations of Various Elements" as taken from The Soil Chemistry of Hazardous Materials, Dragun, James, 1988
Not Applicable
Metals (Total)
SVOCs
Table 3: Summary of Detected Semi-Volatile Organic Compounds (SVOCs) and Total Metals Analytical Results - Foundation Soil (East Office Tower)
Protection of
Groundwater
PSRGs
Industrial/
Commercial
Health-Based
PSRGs
Residential
Health-Based
PSRGs
Regional Background Metals in Soil*
Wood Project Number: 6228-18-0495
Brownfields Project Number: 22074-18-060
Charlotte, North Carolina
Former Gathings Motor Company
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte,North Carolina
Wood Project Number: 6228-18-0495
FIGURES
USGS The National Map: National Boundaries Dataset, National ElevationDataset, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; U.S. Census Bureau - TIGER/Line; HERERoad Data. Data Refreshed July, 2017.
PREPARED BY: LM DATE: 3/12/2019 DATE: 3/12/2019CHECKED BY: RCF
Site Boundary
Document Path: F:\AMEC_Projects\2018\6228-18-0495\MXD\Topo.mxd¯
PROJECT NO: 6228-18-0495 FIGURE NO: 1
SITE TOPOFormer Gathings Motor Company1100-1200 South Tryon StreetCharlotte, North CarolinaBrownfields Project #: 22074-18-060
0 1,000 2,000500Feet
PG-22
PG-25
PG-26 PG-27
PG-29
PG-30
PG-23
PG-21
Beneficial Reuse Characterization Foundation Soil(East Office Tower)Former Gathings Motor Company1100-1200 South Tryon StreetCharlotte, North CarolinaBrownfields Project #: 22074-18-060
PROJECT NO.:FIGURE NO.:6228-18-0495 2Reference: Adapted from Foundation Plan S101 Drawing by Moore Linder Engineering, Inc. dated 4/12/2019Document Path: F:\AMEC_Projects\2018\6228-18-0495\MXD\EastOffice.mxd Prepared By: LMM 6/26/19; Checked by JRM 12/30/19
0 20 40 60Feet
TW-1
LEGEND
TW-2
PG-21
Approximate Proposed Building Footprint
Boring Location Boring not drilled at time of report
Approximate former location of temporary monitoring well (others, 2014)
Potential former fuel dispenser island (others)
PG-24 PG-28
PG-24
!
!
!
!
!
!!
!
!
!
PG-22
PG-25
PG-26 PG-27
PG-29
PG-30
PG-23
PG-21
Summary of Analytical Results
Beneficial Reuse Characterization
(East Office Tower)
Former Gathings Motor Company
1100-1200 South Tryon Street
Charlotte, North Carolina
Brownfields Project #: 22074-18-060
PROJECT NO.:FIGURE NO.:6228-18-0495 3Reference: Adapted from Foundation Plan S101 Drawing by Moore Linder Engineering, Inc. dated 4/12/2019
Document Path: F:\AMEC_Projects\2018\6228-18-0495\MXD\Chemboxfig\Chemboxfig.aprx Prepared By: LMM 1/29/2020; Checked
¯
P
!
!A
!A
P
!!
TW-1
)B
P
B)
!A
!A
TW-2
!
Approximate Proposed Building Footprint
!A Approximate former location of temporary monitoring well (others, 2014)
Potential former fuel dispenser island (others)
Boring Location!PG-21 PG-24Boring not drilled at time of report
Service Layer Credits: Mecklenburg County Aerial Imagery Dated 2019
PG-24 PG-28
Notes:VOCs = Volatile Organic CompoundsSVOCs = Semi-Volatile Organic CompoundsDepths shown in feet below ground surface (bgs)Concentrations shown in milligrams per kilogram (mg/kg)Analytes detected above PSRGs are shown, see laboratory analytical report for full analyte list PSRGs = North Carolina Department of Environmental Quality,Inactive Hazardous Sites Branch, Preliminary Soil Remediation Goals, dated December 2019
* Range and mean values for "Background Metals for North Carolina Soils" taken from Elements in North American Soils by Dragun and Chekiri, 2005** Typical Range of "Native Soil Concentrations of Various Elements" as taken from The Soil Chemistry of Hazardous Materials, Dragun, James, 1988NE = Not exceedances
NS = Not specified-- = Not establishedBold font indicates identified concentration exceeded Protection of Groundwater PSRG
Bold font and shaded GREEN indicates identified concentration exceeded Residential PSRG, these concentrations reflect "naturally occurring" metals in soilBold font and shaded GOLD indicates identified concentration exceeded Protection of Groundwater and Residential PSRGsBold font and shaded BLUE indicates identified concentration exceeded Protection of Groundwater, Residential, and Industrial/Commercial PSRGs
J = Indicates that compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate
0 30 6015
Feet
Boring PG-21
Date Sampled 12/26/2019
"Discrete" Sample Depth
(VOCs)5-10
"Composite" Sample Depth
(SVOCs and Metals)0-42
Analyzed Analytes NE
Analyzed Analytes NE
Analyzed Analytes NE
VOCs
SVOCs
Metals (Total)
Boring PG-22
Date Sampled 12/26/2019
"Discrete" Sample Depth
(VOCs)5-10
"Composite" Sample Depth
(SVOCs and Metals)0-40
Analyzed Analytes NE
Analyzed Analytes NE
Analyzed Analytes NE
VOCs
SVOCs
Metals (Total)
Boring PG-23
Date Sampled 12/26/2019
"Discrete" Sample Depth
(VOCs)5-10
"Composite" Sample Depth
(SVOCs and Metals)0-36
Analyzed Analytes NE
Analyzed Analytes NE
Analyzed Analytes NE
VOCs
SVOCs
Metals (Total)
Boring PG-25
Date Sampled 12/27/2019
"Discrete" Sample Depth
(VOCs)20-25
"Composite" Sample Depth
(SVOCs and Metals)0-46
Analyzed Analytes NE
Analyzed Analytes NE
Analyzed Analytes NE
VOCs
SVOCs
Metals (Total)
Boring PG-26
Date Sampled 12/26/2019
"Discrete" Sample Depth
(VOCs)20-25
"Composite" Sample Depth
(SVOCs and Metals)0-37
Analyzed Analytes NE
Analyzed Analytes NE
Analyzed Analytes NE
VOCs
SVOCs
Metals (Total)
Boring PG-27
Date Sampled 12/26/2019
"Discrete" Sample Depth
(VOCs)28-33
"Composite" Sample Depth
(SVOCs and Metals)0-33
Analyzed Analytes NE
Analyzed Analytes NE
Arsenic 0.94
VOCs
SVOCs
Metals (Total)
Boring PG-29
Date Sampled 12/27/2019
"Discrete" Sample Depth
(VOCs)20-25
"Composite" Sample Depth
(SVOCs and Metals)0-34
VOCs
Benzene 0.62 J
n-Butylbenzene 9.4
Ethylbenzene 66
Isopropylbenzene (Cumene)4.7
p-Isopropyltoluene (p-Cymene)1.4 J
Naphthalene 9.0
n-Propylbenzene 19
1,2,4-Trimethylbenzene 120
1,3,5-Trimethylbenzene 33
m&p Xylene 82
o-Xylene 68
SVOCs
1-Methylnaphthalene 0.15 J
Metals (Total)
Arsenic 0.70
Hexavalent Chromium 0.684 J
Boring PG-30
Date Sampled 12/27/2019
"Discrete" Sample Depth
(VOCs)20-25
"Composite" Sample Depth
(SVOCs and Metals)0-34
n-Butylbenzene 4.6
Ethylbenzene 26
Isopropylbenzene (Cumene)2.4
Naphthalene 4.1
n-Propylbenzene 9.5
1,2,4-Trimethylbenzene 56
1,3,5-Trimethylbenzene 16
m&p Xylene 34
1-Methylnaphthalene 0.14 J
Analyzed Analytes NE
VOCs
SVOCs
Metals (Total)
Range Mean
Benzene 1.2 5.4 0.01
n-Butylbenzene 780 12,000 4.5
sec-Butylbenzene 1,600 23,000 4.1
Chloroform 0.34 1.5 0.39
Ethylbenzene 6.1 27 13
Isopropylbenzene (Cumene)410 2,100 2.3
p-Isopropyltoluene (p-Cymene)----1.24
Naphthalene 4.1 18 0.39
n-Propylbenzene 780 5,100 2.6
1,2,4-Trimethylbenzene 63 370 12
1,3,5-Trimethylbenzene 56 320 11
m&p Xylene 240 1,020 19.6
o-Xylene 140 590 9.8
1-Methylnaphthalene 18 73 0.11
2-Methylnaphthalene 48 600 3.1
Naphthalene 4.1 18 0.39
Arsenic 0.68 3.0 5.8 1.0-40**NS
Barium 3,100 47,000 580 50-1000 356
Cadmium 14 200 3.0 0.01-7.0**NS
Chromium 23,000 350,000 360,000 7-300 65
Lead 400 800 270 2-200**NS
Mercury 2.3 9.7 1.0 0.03-0.52 0.121
Selenium 78 1,200 2.1 <0.1-0.8 0.42
Silver 78 1,200 3.4 NS NS
Hexavalent Chromium 0.31 6.5 3.8 NS NS
Not Applicable
SVOCs
Not Applicable
Metals (Total)
Residential
Health-Based
PSRGs
Industrial/
Commercial
Health-Based
PSRGs
Protection of
Groundwater
PSRGs
Regional Background
Metals in Soil*
VOCs
b: AJFy1/31/2020
PG-34PG-33
PG-32
PG-31
PG-28PG-24
PG-29
PG-30
Proposed Soil Borings Beneficial Reuse Characterization(East Office Tower)Former Gathings Motor Company 1100-1200 South Tryon Street Charlotte, North Carolina Brownfields Project #: 22074-18-060
PROJECT NO.:FIGURE NO.:6228-18-0495 4Reference: Adapted from Foundation Plan S101 Drawing by Moore Linder Engineering, Inc. dated 4/12/2019Document Path: F:\AMEC_Projects\2018\6228-18-0495\MXD\ProposedBorings.mxd Prepared By: LMM 1/31/2020; Checked by AJF 1/31/2020
0 20 40 60Feet
TW-1
LEGEND
TW-2
Approximate Proposed Building Footprint
Approximate former location of temporary monitoring well (others, 2014)
Potential former fuel dispenser island (others)
Former Boring LocationPG-21 Proposed Soil BoringPG-24
Report of Soil Characterization for Beneficial Reuse –Foundation Soil (East Office Tower)February 10, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte,North Carolina
Wood Project Number: 6228-18-0495
APPENDIX
LABORATORY ANALYTICAL REPORTS AND CHAIN-OF-CUSTODY FORMS
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
January 15, 2020
Rob Foster
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: Charlotte, NC
Client Job Number:
Project Number: 6228-18-0495
Laboratory Work Order Number: 19L1171
Enclosed are results of analyses for samples received by the laboratory on December 30, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 145
Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 6
Sample Results 10
19L1171-02 10
19L1171-11 13
19L1171-22 16
19L1171-32 19
19L1171-34 22
19L1171-46 25
19L1171-56 28
19L1171-63 31
19L1171-66 34
19L1171-67 37
19L1171-68 42
19L1171-69 44
19L1171-70 49
19L1171-71 54
19L1171-72 59
19L1171-73 64
19L1171-74 69
19L1171-75 74
19L1171-76 79
Sample Preparation Information 84
QC Data 86
Volatile Organic Compounds by GC/MS 86
Page 2 of 145
Table of Contents
Table of Contents (continued)
B249284 86
B249440 90
Semivolatile Organic Compounds by GC/MS 96
B249356 96
Metals Analyses (Total) 101
B249454 101
B249488 101
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 103
B249433 103
Flag/Qualifier Summary 104
Certifications 105
Chain of Custody/Sample Receipt 111
Page 3 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
1/15/2020
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228-18-0495
19L1171
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
PG-21-10 19L1171-02 Soil SM 2540G
SW-846 8260D
PG-23-10 19L1171-11 Soil SM 2540G
SW-846 8260D
PG-26-25 19L1171-22 Soil SM 2540G
SW-846 8260D
PG-27-33 19L1171-32 Soil SM 2540G
SW-846 8260D
PG-22-10 19L1171-34 Soil SM 2540G
SW-846 8260D
PG-25-25 19L1171-46 Soil SM 2540G
SW-846 8260D
PG-29-25 19L1171-56 Soil SM 2540G
SW-846 8260D
PG-30-25 19L1171-63 Soil SM 2540G
SW-846 8260D
DUP-122719 19L1171-66 Soil SM 2540G
SW-846 8260D
DUP-COMP 19L1171-67 Soil -CT PH-0197/NY11742
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
TRIP BLANK 19L1171-68 Trip Blank Soil SW-846 8260D
COMP-PG21 19L1171-69 Soil -CT PH-0197/NY11742
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
COMP-PG22 19L1171-70 Soil -CT PH-0197/NY11742
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
COMP-PG23 19L1171-71 Soil -CT PH-0197/NY11742
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
[TOC_1]Sample Summary[TOC]
Page 4 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
1/15/2020
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228-18-0495
19L1171
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
COMP-PG25 19L1171-72 Soil -CT PH-0197/NY11742
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
COMP-PG26 19L1171-73 Soil -CT PH-0197/NY11742
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
COMP-PG27 19L1171-74 Soil -CT PH-0197/NY11742
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
COMP-PG29 19L1171-75 Soil -CT PH-0197/NY11742
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
COMP-PG30 19L1171-76 Soil -CT PH-0197/NY11742
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
Page 5 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6020, all dilutions were performed as per standard operating procedure.
[TOC_1]Case Narrative[TOC]
Page 6 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SW-846 6020B
Qualifications:
Sample to spike ratio is greater than or equal to 4:1. Spiked amount is not representative of the native amount in the sample. Appropriate or
meaningful recoveries cannot be calculated.
Analyte & Samples(s) Qualified:
MS-19
Barium
19L1171-67[DUP-COMP], B249488-MS1
SW-846 8260D
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Bromomethane
B249440-BS1, B249440-BSD1
Chloromethane
B249440-BS1, B249440-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
1,2,3-Trichlorobenzene
19L1171-56[PG-29-25], 19L1171-63[PG-30-25], B249440-BLK1, B249440-BS1, B249440-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
1,2,4-Trichlorobenzene
B249440-BS1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
19L1171-56[PG-29-25], 19L1171-63[PG-30-25]
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
1,2,3-Trichlorobenzene
19L1171-56[PG-29-25], 19L1171-63[PG-30-25], B249440-BLK1, B249440-BS1, B249440-BSD1, S044397-CCV1
1,2,4-Trichlorobenzene
19L1171-56[PG-29-25], 19L1171-63[PG-30-25], B249440-BLK1, B249440-BS1, B249440-BSD1, S044397-CCV1
Chloromethane
19L1171-02[PG-21-10], 19L1171-11[PG-23-10], 19L1171-22[PG-26-25], 19L1171-32[PG-27-33], 19L1171-34[PG-22-10], 19L1171-46[PG-25-25],
19L1171-66[DUP-122719], 19L1171-68[TRIP BLANK], B249284-BLK1, B249284-BS1, B249284-BSD1, S044295-CCV1
Naphthalene
19L1171-56[PG-29-25], 19L1171-63[PG-30-25], B249440-BLK1, B249440-BS1, B249440-BSD1, S044397-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
Bromomethane
B249440-BS1, B249440-BSD1, S044397-CCV1
Chloromethane
B249440-BS1, B249440-BSD1, S044397-CCV1
Page 7 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
Bromomethane
19L1171-02[PG-21-10], 19L1171-11[PG-23-10], 19L1171-22[PG-26-25], 19L1171-32[PG-27-33], 19L1171-34[PG-22-10], 19L1171-46[PG-25-25],
19L1171-66[DUP-122719], 19L1171-68[TRIP BLANK], B249284-BLK1, B249284-BS1, B249284-BSD1, S044295-CCV1
SW-846 8270E
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Hexachlorocyclopentadiene
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1, B249356-BS1, B249356-BSD1
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-04
Benzidine
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1, B249356-BS1, B249356-BSD1, S044354-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Benzidine
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1, B249356-BS1, B249356-BSD1, S044354-CCV1
Hexachlorobutadiene
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1, B249356-BS1, B249356-BSD1, S044354-CCV1
Hexachlorocyclopentadiene
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1, B249356-BS1, B249356-BSD1, S044354-CCV1
Pentachlorophenol
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1, B249356-BS1, B249356-BSD1, S044354-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
V-06
2,4-Dinitrotoluene
B249356-BS1, B249356-BSD1, S044354-CCV1
2-Nitroaniline
B249356-BS1, B249356-BSD1, S044354-CCV1
3-Nitroaniline
B249356-BS1, B249356-BSD1, S044354-CCV1
Phenol
B249356-BS1, B249356-BSD1, S044354-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
2,4-Dinitrotoluene
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1
Phenol
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1
Page 8 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
4-Chloroaniline
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1, B249356-BS1, B249356-BSD1, S044354-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-35
Benzidine
19L1171-67[DUP-COMP], 19L1171-69[COMP-PG21], 19L1171-70[COMP-PG22], 19L1171-71[COMP-PG23], 19L1171-72[COMP-PG25], 19L1171-73[COMP-PG26],
19L1171-74[COMP-PG27], 19L1171-75[COMP-PG29], 19L1171-76[COMP-PG30], B249356-BLK1, B249356-BS1, B249356-BSD1, S044354-CCV1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 9 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-02
Field Sample #: PG-21-10
Sample Matrix: Soil
Sampled: 12/26/2019 09:45
[TOC_2]19L1171-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 1/2/20 7:43 MFFmg/Kg dry0.031 1/2/20SW-846 8260D1Acetone
ND 0.0079 1/2/20 7:43 MFFmg/Kg dry0.0033 1/2/20SW-846 8260D1Acrylonitrile
ND 0.0013 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Benzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Bromobenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D1Bromochloromethane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00079 1/2/20SW-846 8260D1Bromodichloromethane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D1Bromoform
ND 0.013 1/2/20 7:43 MFFmg/Kg dry0.0056 1/2/20SW-846 8260D1V-34Bromomethane
ND 0.053 1/2/20 7:43 MFFmg/Kg dry0.023 1/2/20SW-846 8260D12-Butanone (MEK)
ND 0.053 1/2/20 7:43 MFFmg/Kg dry0.028 1/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1n-Butylbenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1sec-Butylbenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1tert-Butylbenzene
ND 0.0013 1/2/20 7:43 MFFmg/Kg dry0.00079 1/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0079 1/2/20 7:43 MFFmg/Kg dry0.0057 1/2/20SW-846 8260D1Carbon Disulfide
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Chlorobenzene
ND 0.0013 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Chlorodibromomethane
ND 0.026 1/2/20 7:43 MFFmg/Kg dry0.0020 1/2/20SW-846 8260D1Chloroethane
ND 0.0053 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Chloroform
ND 0.013 1/2/20 7:43 MFFmg/Kg dry0.0085 1/2/20SW-846 8260D1V-05Chloromethane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D12-Chlorotoluene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D14-Chlorotoluene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 1/2/20 7:43 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00079 1/2/20SW-846 8260D1Dibromomethane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0053 1/2/20 7:43 MFFmg/Kg dry0.0028 1/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.026 1/2/20 7:43 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0053 1/2/20 7:43 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D11,2-Dichloropropane
ND 0.0013 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,1-Dichloropropene
ND 0.0013 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0013 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.026 1/2/20 7:43 MFFmg/Kg dry0.0024 1/2/20SW-846 8260D1Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 10 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-02
Field Sample #: PG-21-10
Sample Matrix: Soil
Sampled: 12/26/2019 09:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 1/2/20 7:43 MFFmg/Kg dry0.00079 1/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.13 1/2/20 7:43 MFFmg/Kg dry0.076 1/2/20SW-846 8260D11,4-Dioxane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Ethylbenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.026 1/2/20 7:43 MFFmg/Kg dry0.014 1/2/20SW-846 8260D12-Hexanone (MBK)
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0053 1/2/20 7:43 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.026 1/2/20 7:43 MFFmg/Kg dry0.0094 1/2/20SW-846 8260D1Methylene Chloride
ND 0.026 1/2/20 7:43 MFFmg/Kg dry0.010 1/2/20SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0053 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Naphthalene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1n-Propylbenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00079 1/2/20SW-846 8260D1Styrene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0024 1/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0013 1/2/20 7:43 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D1Tetrachloroethylene
ND 0.013 1/2/20 7:43 MFFmg/Kg dry0.0029 1/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Toluene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00079 1/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1Trichloroethylene
ND 0.013 1/2/20 7:43 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.013 1/2/20 7:43 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00079 1/2/20SW-846 8260D11,3,5-Trimethylbenzene
ND 0.013 1/2/20 7:43 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1Vinyl Chloride
ND 0.0053 1/2/20 7:43 MFFmg/Kg dry0.0023 1/2/20SW-846 8260D1m+p Xylene
ND 0.0026 1/2/20 7:43 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 92.6 1/2/20 7:4370-130
Toluene-d8 97.8 1/2/20 7:4370-130
4-Bromofluorobenzene 102 1/2/20 7:4370-130
Page 11 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-02
Field Sample #: PG-21-10
Sample Matrix: Soil
Sampled: 12/26/2019 09:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
73.9 1/5/20 16:03 JS% Wt 1/5/20SM 2540G1% Solids
Page 12 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-11
Field Sample #: PG-23-10
Sample Matrix: Soil
Sampled: 12/26/2019 11:05
[TOC_2]19L1171-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 1/2/20 8:10 MFFmg/Kg dry0.030 1/2/20SW-846 8260D1Acetone
ND 0.0076 1/2/20 8:10 MFFmg/Kg dry0.0032 1/2/20SW-846 8260D1Acrylonitrile
ND 0.0013 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Benzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Bromobenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D1Bromochloromethane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1Bromodichloromethane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D1Bromoform
ND 0.013 1/2/20 8:10 MFFmg/Kg dry0.0053 1/2/20SW-846 8260D1V-34Bromomethane
ND 0.051 1/2/20 8:10 MFFmg/Kg dry0.022 1/2/20SW-846 8260D12-Butanone (MEK)
ND 0.051 1/2/20 8:10 MFFmg/Kg dry0.027 1/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1n-Butylbenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1sec-Butylbenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1tert-Butylbenzene
ND 0.0013 1/2/20 8:10 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0076 1/2/20 8:10 MFFmg/Kg dry0.0055 1/2/20SW-846 8260D1Carbon Disulfide
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Chlorobenzene
ND 0.0013 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Chlorodibromomethane
ND 0.025 1/2/20 8:10 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D1Chloroethane
ND 0.0051 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Chloroform
ND 0.013 1/2/20 8:10 MFFmg/Kg dry0.0081 1/2/20SW-846 8260D1V-05Chloromethane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D12-Chlorotoluene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D14-Chlorotoluene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 1/2/20 8:10 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1Dibromomethane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0051 1/2/20 8:10 MFFmg/Kg dry0.0027 1/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.025 1/2/20 8:10 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0051 1/2/20 8:10 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D11,2-Dichloropropane
ND 0.0013 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,1-Dichloropropene
ND 0.0013 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0013 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.025 1/2/20 8:10 MFFmg/Kg dry0.0023 1/2/20SW-846 8260D1Diethyl Ether
Page 13 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-11
Field Sample #: PG-23-10
Sample Matrix: Soil
Sampled: 12/26/2019 11:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 1/2/20 8:10 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.13 1/2/20 8:10 MFFmg/Kg dry0.073 1/2/20SW-846 8260D11,4-Dioxane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Ethylbenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.025 1/2/20 8:10 MFFmg/Kg dry0.014 1/2/20SW-846 8260D12-Hexanone (MBK)
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0051 1/2/20 8:10 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.025 1/2/20 8:10 MFFmg/Kg dry0.0090 1/2/20SW-846 8260D1Methylene Chloride
ND 0.025 1/2/20 8:10 MFFmg/Kg dry0.0097 1/2/20SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0051 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Naphthalene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1n-Propylbenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1Styrene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0023 1/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0013 1/2/20 8:10 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D1Tetrachloroethylene
ND 0.013 1/2/20 8:10 MFFmg/Kg dry0.0028 1/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Toluene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1Trichloroethylene
ND 0.013 1/2/20 8:10 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.013 1/2/20 8:10 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D11,3,5-Trimethylbenzene
ND 0.013 1/2/20 8:10 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1Vinyl Chloride
ND 0.0051 1/2/20 8:10 MFFmg/Kg dry0.0022 1/2/20SW-846 8260D1m+p Xylene
ND 0.0025 1/2/20 8:10 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 96.6 1/2/20 8:1070-130
Toluene-d8 97.8 1/2/20 8:1070-130
4-Bromofluorobenzene 102 1/2/20 8:1070-130
Page 14 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-11
Field Sample #: PG-23-10
Sample Matrix: Soil
Sampled: 12/26/2019 11:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
76.4 1/5/20 16:03 JS% Wt 1/5/20SM 2540G1% Solids
Page 15 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-22
Field Sample #: PG-26-25
Sample Matrix: Soil
Sampled: 12/26/2019 13:55
[TOC_2]19L1171-22[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.14 1/2/20 8:38 MFFmg/Kg dry0.032 1/2/20SW-846 8260D1Acetone
ND 0.0082 1/2/20 8:38 MFFmg/Kg dry0.0034 1/2/20SW-846 8260D1Acrylonitrile
ND 0.0014 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1Benzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Bromobenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D1Bromochloromethane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00082 1/2/20SW-846 8260D1Bromodichloromethane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D1Bromoform
ND 0.014 1/2/20 8:38 MFFmg/Kg dry0.0058 1/2/20SW-846 8260D1V-34Bromomethane
ND 0.055 1/2/20 8:38 MFFmg/Kg dry0.024 1/2/20SW-846 8260D12-Butanone (MEK)
ND 0.055 1/2/20 8:38 MFFmg/Kg dry0.029 1/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1n-Butylbenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1sec-Butylbenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1tert-Butylbenzene
ND 0.0014 1/2/20 8:38 MFFmg/Kg dry0.00082 1/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0082 1/2/20 8:38 MFFmg/Kg dry0.0059 1/2/20SW-846 8260D1Carbon Disulfide
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1Chlorobenzene
ND 0.0014 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1Chlorodibromomethane
ND 0.027 1/2/20 8:38 MFFmg/Kg dry0.0021 1/2/20SW-846 8260D1Chloroethane
ND 0.0055 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1Chloroform
ND 0.014 1/2/20 8:38 MFFmg/Kg dry0.0088 1/2/20SW-846 8260D1V-05Chloromethane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D12-Chlorotoluene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D14-Chlorotoluene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0014 1/2/20 8:38 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00082 1/2/20SW-846 8260D1Dibromomethane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0055 1/2/20 8:38 MFFmg/Kg dry0.0029 1/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.027 1/2/20 8:38 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0055 1/2/20 8:38 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D11,2-Dichloropropane
ND 0.0014 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,1-Dichloropropene
ND 0.0014 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0014 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.027 1/2/20 8:38 MFFmg/Kg dry0.0025 1/2/20SW-846 8260D1Diethyl Ether
Page 16 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-22
Field Sample #: PG-26-25
Sample Matrix: Soil
Sampled: 12/26/2019 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0014 1/2/20 8:38 MFFmg/Kg dry0.00082 1/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.14 1/2/20 8:38 MFFmg/Kg dry0.079 1/2/20SW-846 8260D11,4-Dioxane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Ethylbenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.027 1/2/20 8:38 MFFmg/Kg dry0.015 1/2/20SW-846 8260D12-Hexanone (MBK)
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0055 1/2/20 8:38 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.027 1/2/20 8:38 MFFmg/Kg dry0.0097 1/2/20SW-846 8260D1Methylene Chloride
ND 0.027 1/2/20 8:38 MFFmg/Kg dry0.010 1/2/20SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0055 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1Naphthalene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1n-Propylbenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00082 1/2/20SW-846 8260D1Styrene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0025 1/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0014 1/2/20 8:38 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D1Tetrachloroethylene
ND 0.014 1/2/20 8:38 MFFmg/Kg dry0.0030 1/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Toluene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00082 1/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1Trichloroethylene
ND 0.014 1/2/20 8:38 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.014 1/2/20 8:38 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
0.0016 0.0027 1/2/20 8:38 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1J1,2,4-Trimethylbenzene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00082 1/2/20SW-846 8260D11,3,5-Trimethylbenzene
ND 0.014 1/2/20 8:38 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1Vinyl Chloride
0.0026 0.0055 1/2/20 8:38 MFFmg/Kg dry0.0023 1/2/20SW-846 8260D1Jm+p Xylene
ND 0.0027 1/2/20 8:38 MFFmg/Kg dry0.00096 1/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.2 1/2/20 8:3870-130
Toluene-d8 98.2 1/2/20 8:3870-130
4-Bromofluorobenzene 101 1/2/20 8:3870-130
Page 17 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-22
Field Sample #: PG-26-25
Sample Matrix: Soil
Sampled: 12/26/2019 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
72.3 1/5/20 16:04 JS% Wt 1/5/20SM 2540G1% Solids
Page 18 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-32
Field Sample #: PG-27-33
Sample Matrix: Soil
Sampled: 12/26/2019 15:25
[TOC_2]19L1171-32[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.15 1/2/20 9:05 MFFmg/Kg dry0.034 1/2/20SW-846 8260D1Acetone
ND 0.0087 1/2/20 9:05 MFFmg/Kg dry0.0036 1/2/20SW-846 8260D1Acrylonitrile
ND 0.0015 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
0.0093 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Benzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Bromobenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0020 1/2/20SW-846 8260D1Bromochloromethane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.00087 1/2/20SW-846 8260D1Bromodichloromethane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0020 1/2/20SW-846 8260D1Bromoform
ND 0.015 1/2/20 9:05 MFFmg/Kg dry0.0061 1/2/20SW-846 8260D1V-34Bromomethane
ND 0.058 1/2/20 9:05 MFFmg/Kg dry0.025 1/2/20SW-846 8260D12-Butanone (MEK)
ND 0.058 1/2/20 9:05 MFFmg/Kg dry0.030 1/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1n-Butylbenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1sec-Butylbenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1tert-Butylbenzene
ND 0.0015 1/2/20 9:05 MFFmg/Kg dry0.00087 1/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0087 1/2/20 9:05 MFFmg/Kg dry0.0063 1/2/20SW-846 8260D1Carbon Disulfide
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Chlorobenzene
ND 0.0015 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Chlorodibromomethane
ND 0.029 1/2/20 9:05 MFFmg/Kg dry0.0022 1/2/20SW-846 8260D1Chloroethane
ND 0.0058 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Chloroform
ND 0.015 1/2/20 9:05 MFFmg/Kg dry0.0093 1/2/20SW-846 8260D1V-05Chloromethane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D12-Chlorotoluene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D14-Chlorotoluene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0015 1/2/20 9:05 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.00087 1/2/20SW-846 8260D1Dibromomethane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0058 1/2/20 9:05 MFFmg/Kg dry0.0031 1/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.029 1/2/20 9:05 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0058 1/2/20 9:05 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D11,2-Dichloropropane
ND 0.0015 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,1-Dichloropropene
ND 0.0015 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0015 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.029 1/2/20 9:05 MFFmg/Kg dry0.0026 1/2/20SW-846 8260D1Diethyl Ether
Page 19 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-32
Field Sample #: PG-27-33
Sample Matrix: Soil
Sampled: 12/26/2019 15:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0015 1/2/20 9:05 MFFmg/Kg dry0.00087 1/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.15 1/2/20 9:05 MFFmg/Kg dry0.084 1/2/20SW-846 8260D11,4-Dioxane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Ethylbenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.029 1/2/20 9:05 MFFmg/Kg dry0.016 1/2/20SW-846 8260D12-Hexanone (MBK)
0.0015 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1JIsopropylbenzene (Cumene)
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0058 1/2/20 9:05 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.029 1/2/20 9:05 MFFmg/Kg dry0.010 1/2/20SW-846 8260D1Methylene Chloride
ND 0.029 1/2/20 9:05 MFFmg/Kg dry0.011 1/2/20SW-846 8260D14-Methyl-2-pentanone (MIBK)
0.0070 0.0058 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Naphthalene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1n-Propylbenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.00087 1/2/20SW-846 8260D1Styrene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0026 1/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0015 1/2/20 9:05 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D1Tetrachloroethylene
ND 0.015 1/2/20 9:05 MFFmg/Kg dry0.0032 1/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Toluene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.00087 1/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1Trichloroethylene
ND 0.015 1/2/20 9:05 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.015 1/2/20 9:05 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
0.021 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,2,4-Trimethylbenzene
0.0028 0.0029 1/2/20 9:05 MFFmg/Kg dry0.00087 1/2/20SW-846 8260D1J1,3,5-Trimethylbenzene
ND 0.015 1/2/20 9:05 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D1Vinyl Chloride
0.023 0.0058 1/2/20 9:05 MFFmg/Kg dry0.0025 1/2/20SW-846 8260D1m+p Xylene
ND 0.0029 1/2/20 9:05 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.7 1/2/20 9:0570-130
Toluene-d8 98.0 1/2/20 9:0570-130
4-Bromofluorobenzene 104 1/2/20 9:0570-130
Page 20 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-32
Field Sample #: PG-27-33
Sample Matrix: Soil
Sampled: 12/26/2019 15:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
74.9 1/5/20 16:04 JS% Wt 1/5/20SM 2540G1% Solids
Page 21 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-34
Field Sample #: PG-22-10
Sample Matrix: Soil
Sampled: 12/26/2019 16:15
[TOC_2]19L1171-34[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 1/2/20 9:32 MFFmg/Kg dry0.030 1/2/20SW-846 8260D1Acetone
ND 0.0076 1/2/20 9:32 MFFmg/Kg dry0.0032 1/2/20SW-846 8260D1Acrylonitrile
ND 0.0013 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Benzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Bromobenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D1Bromochloromethane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1Bromodichloromethane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D1Bromoform
ND 0.013 1/2/20 9:32 MFFmg/Kg dry0.0053 1/2/20SW-846 8260D1V-34Bromomethane
ND 0.051 1/2/20 9:32 MFFmg/Kg dry0.022 1/2/20SW-846 8260D12-Butanone (MEK)
ND 0.051 1/2/20 9:32 MFFmg/Kg dry0.026 1/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1n-Butylbenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1sec-Butylbenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1tert-Butylbenzene
ND 0.0013 1/2/20 9:32 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0076 1/2/20 9:32 MFFmg/Kg dry0.0054 1/2/20SW-846 8260D1Carbon Disulfide
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Chlorobenzene
ND 0.0013 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Chlorodibromomethane
ND 0.025 1/2/20 9:32 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D1Chloroethane
ND 0.0051 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Chloroform
ND 0.013 1/2/20 9:32 MFFmg/Kg dry0.0081 1/2/20SW-846 8260D1V-05Chloromethane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D12-Chlorotoluene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D14-Chlorotoluene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 1/2/20 9:32 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1Dibromomethane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0051 1/2/20 9:32 MFFmg/Kg dry0.0027 1/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.025 1/2/20 9:32 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0051 1/2/20 9:32 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,2-Dichloropropane
ND 0.0013 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,1-Dichloropropene
ND 0.0013 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0013 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.025 1/2/20 9:32 MFFmg/Kg dry0.0023 1/2/20SW-846 8260D1Diethyl Ether
Page 22 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-34
Field Sample #: PG-22-10
Sample Matrix: Soil
Sampled: 12/26/2019 16:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 1/2/20 9:32 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.13 1/2/20 9:32 MFFmg/Kg dry0.073 1/2/20SW-846 8260D11,4-Dioxane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Ethylbenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.025 1/2/20 9:32 MFFmg/Kg dry0.014 1/2/20SW-846 8260D12-Hexanone (MBK)
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0051 1/2/20 9:32 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.025 1/2/20 9:32 MFFmg/Kg dry0.0090 1/2/20SW-846 8260D1Methylene Chloride
ND 0.025 1/2/20 9:32 MFFmg/Kg dry0.0096 1/2/20SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0051 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1Naphthalene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1n-Propylbenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D1Styrene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0023 1/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0013 1/2/20 9:32 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D1Tetrachloroethylene
ND 0.013 1/2/20 9:32 MFFmg/Kg dry0.0028 1/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D1Toluene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1Trichloroethylene
ND 0.013 1/2/20 9:32 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.013 1/2/20 9:32 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.0010 1/2/20SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00076 1/2/20SW-846 8260D11,3,5-Trimethylbenzene
ND 0.013 1/2/20 9:32 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1Vinyl Chloride
ND 0.0051 1/2/20 9:32 MFFmg/Kg dry0.0022 1/2/20SW-846 8260D1m+p Xylene
ND 0.0025 1/2/20 9:32 MFFmg/Kg dry0.00089 1/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.5 1/2/20 9:3270-130
Toluene-d8 98.2 1/2/20 9:3270-130
4-Bromofluorobenzene 101 1/2/20 9:3270-130
Page 23 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-34
Field Sample #: PG-22-10
Sample Matrix: Soil
Sampled: 12/26/2019 16:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
76.6 1/5/20 16:04 JS% Wt 1/5/20SM 2540G1% Solids
Page 24 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-46
Field Sample #: PG-25-25
Sample Matrix: Soil
Sampled: 12/27/2019 10:15
[TOC_2]19L1171-46[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.15 1/2/20 10:00 MFFmg/Kg dry0.036 1/2/20SW-846 8260D1Acetone
ND 0.0093 1/2/20 10:00 MFFmg/Kg dry0.0039 1/2/20SW-846 8260D1Acrylonitrile
ND 0.0015 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Benzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Bromobenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0022 1/2/20SW-846 8260D1Bromochloromethane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Bromodichloromethane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0022 1/2/20SW-846 8260D1Bromoform
ND 0.015 1/2/20 10:00 MFFmg/Kg dry0.0065 1/2/20SW-846 8260D1V-34Bromomethane
ND 0.062 1/2/20 10:00 MFFmg/Kg dry0.027 1/2/20SW-846 8260D12-Butanone (MEK)
ND 0.062 1/2/20 10:00 MFFmg/Kg dry0.032 1/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1n-Butylbenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1sec-Butylbenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1tert-Butylbenzene
ND 0.0015 1/2/20 10:00 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0093 1/2/20 10:00 MFFmg/Kg dry0.0067 1/2/20SW-846 8260D1Carbon Disulfide
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Chlorobenzene
ND 0.0015 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Chlorodibromomethane
ND 0.031 1/2/20 10:00 MFFmg/Kg dry0.0023 1/2/20SW-846 8260D1Chloroethane
0.0022 0.0062 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1JChloroform
ND 0.015 1/2/20 10:00 MFFmg/Kg dry0.0099 1/2/20SW-846 8260D1V-05Chloromethane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D12-Chlorotoluene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D14-Chlorotoluene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0015 1/2/20 10:00 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Dibromomethane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0062 1/2/20 10:00 MFFmg/Kg dry0.0033 1/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.031 1/2/20 10:00 MFFmg/Kg dry0.0020 1/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0020 1/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0062 1/2/20 10:00 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0020 1/2/20SW-846 8260D11,2-Dichloropropane
ND 0.0015 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,1-Dichloropropene
ND 0.0015 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0015 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.031 1/2/20 10:00 MFFmg/Kg dry0.0028 1/2/20SW-846 8260D1Diethyl Ether
Page 25 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-46
Field Sample #: PG-25-25
Sample Matrix: Soil
Sampled: 12/27/2019 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0015 1/2/20 10:00 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.15 1/2/20 10:00 MFFmg/Kg dry0.089 1/2/20SW-846 8260D11,4-Dioxane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Ethylbenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.031 1/2/20 10:00 MFFmg/Kg dry0.017 1/2/20SW-846 8260D12-Hexanone (MBK)
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0062 1/2/20 10:00 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.031 1/2/20 10:00 MFFmg/Kg dry0.011 1/2/20SW-846 8260D1Methylene Chloride
ND 0.031 1/2/20 10:00 MFFmg/Kg dry0.012 1/2/20SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0062 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Naphthalene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1n-Propylbenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D1Styrene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0028 1/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0015 1/2/20 10:00 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0020 1/2/20SW-846 8260D1Tetrachloroethylene
ND 0.015 1/2/20 10:00 MFFmg/Kg dry0.0034 1/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D1Toluene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0019 1/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0015 1/2/20SW-846 8260D1Trichloroethylene
ND 0.015 1/2/20 10:00 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.015 1/2/20 10:00 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0012 1/2/20SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.00093 1/2/20SW-846 8260D11,3,5-Trimethylbenzene
ND 0.015 1/2/20 10:00 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D1Vinyl Chloride
ND 0.0062 1/2/20 10:00 MFFmg/Kg dry0.0026 1/2/20SW-846 8260D1m+p Xylene
ND 0.0031 1/2/20 10:00 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.7 1/2/20 10:0070-130
Toluene-d8 98.9 1/2/20 10:0070-130
4-Bromofluorobenzene 99.9 1/2/20 10:0070-130
Page 26 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-46
Field Sample #: PG-25-25
Sample Matrix: Soil
Sampled: 12/27/2019 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
68.4 1/5/20 16:04 JS% Wt 1/5/20SM 2540G1% Solids
Page 27 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-56
Field Sample #: PG-29-25
Sample Matrix: Soil
Sampled: 12/27/2019 13:15
[TOC_2]19L1171-56[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 100 1/6/20 20:59 MFFmg/Kg dry7.8 1/2/20SW-846 8260D20Acetone
ND 10 1/6/20 20:59 MFFmg/Kg dry1.1 1/2/20SW-846 8260D20Acrylonitrile
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.29 1/2/20SW-846 8260D20tert-Amyl Methyl Ether (TAME)
0.62 2.1 1/6/20 20:59 MFFmg/Kg dry0.37 1/2/20SW-846 8260D20JBenzene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.31 1/2/20SW-846 8260D20Bromobenzene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.66 1/2/20SW-846 8260D20Bromochloromethane
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.33 1/2/20SW-846 8260D20Bromodichloromethane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.94 1/2/20SW-846 8260D20Bromoform
ND 4.1 1/6/20 20:59 MFFmg/Kg dry1.6 1/2/20SW-846 8260D20Bromomethane
ND 41 1/6/20 20:59 MFFmg/Kg dry4.0 1/2/20SW-846 8260D202-Butanone (MEK)
ND 41 1/6/20 20:59 MFFmg/Kg dry8.6 1/2/20SW-846 8260D20tert-Butyl Alcohol (TBA)
9.4 2.1 1/6/20 20:59 MFFmg/Kg dry0.43 1/2/20SW-846 8260D20n-Butylbenzene
1.7 2.1 1/6/20 20:59 MFFmg/Kg dry0.33 1/2/20SW-846 8260D20Jsec-Butylbenzene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.35 1/2/20SW-846 8260D20tert-Butylbenzene
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.33 1/2/20SW-846 8260D20tert-Butyl Ethyl Ether (TBEE)
ND 10 1/6/20 20:59 MFFmg/Kg dry9.1 1/2/20SW-846 8260D20Carbon Disulfide
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.23 1/2/20SW-846 8260D20Carbon Tetrachloride
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.31 1/2/20SW-846 8260D20Chlorobenzene
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.43 1/2/20SW-846 8260D20Chlorodibromomethane
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.72 1/2/20SW-846 8260D20Chloroethane
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.35 1/2/20SW-846 8260D20Chloroform
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.92 1/2/20SW-846 8260D20Chloromethane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.25 1/2/20SW-846 8260D202-Chlorotoluene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.29 1/2/20SW-846 8260D204-Chlorotoluene
ND 10 1/6/20 20:59 MFFmg/Kg dry1.1 1/2/20SW-846 8260D201,2-Dibromo-3-chloropropane (DBCP)
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.39 1/2/20SW-846 8260D201,2-Dibromoethane (EDB)
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.76 1/2/20SW-846 8260D20Dibromomethane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.33 1/2/20SW-846 8260D201,2-Dichlorobenzene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.25 1/2/20SW-846 8260D201,3-Dichlorobenzene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.27 1/2/20SW-846 8260D201,4-Dichlorobenzene
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.64 1/2/20SW-846 8260D20trans-1,4-Dichloro-2-butene
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.53 1/2/20SW-846 8260D20Dichlorodifluoromethane (Freon 12)
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.33 1/2/20SW-846 8260D201,1-Dichloroethane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.84 1/2/20SW-846 8260D201,2-Dichloroethane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.66 1/2/20SW-846 8260D201,1-Dichloroethylene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.27 1/2/20SW-846 8260D20cis-1,2-Dichloroethylene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.64 1/2/20SW-846 8260D20trans-1,2-Dichloroethylene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.41 1/2/20SW-846 8260D201,2-Dichloropropane
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.23 1/2/20SW-846 8260D201,3-Dichloropropane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.41 1/2/20SW-846 8260D202,2-Dichloropropane
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.33 1/2/20SW-846 8260D201,1-Dichloropropene
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.27 1/2/20SW-846 8260D20cis-1,3-Dichloropropene
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.47 1/2/20SW-846 8260D20trans-1,3-Dichloropropene
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.70 1/2/20SW-846 8260D20Diethyl Ether
Page 28 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-56
Field Sample #: PG-29-25
Sample Matrix: Soil
Sampled: 12/27/2019 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.35 1/2/20SW-846 8260D20Diisopropyl Ether (DIPE)
ND 100 1/6/20 20:59 MFFmg/Kg dry46 1/2/20SW-846 8260D201,4-Dioxane
66 2.1 1/6/20 20:59 MFFmg/Kg dry0.27 1/2/20SW-846 8260D20Ethylbenzene
ND 1.2 1/6/20 20:59 MFFmg/Kg dry0.96 1/2/20SW-846 8260D20Hexachlorobutadiene
ND 21 1/6/20 20:59 MFFmg/Kg dry3.1 1/2/20SW-846 8260D202-Hexanone (MBK)
4.7 2.1 1/6/20 20:59 MFFmg/Kg dry0.35 1/2/20SW-846 8260D20Isopropylbenzene (Cumene)
1.4 2.1 1/6/20 20:59 MFFmg/Kg dry0.41 1/2/20SW-846 8260D20Jp-Isopropyltoluene (p-Cymene)
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.51 1/2/20SW-846 8260D20Methyl tert-Butyl Ether (MTBE)
ND 10 1/6/20 20:59 MFFmg/Kg dry0.70 1/2/20SW-846 8260D20Methylene Chloride
ND 21 1/6/20 20:59 MFFmg/Kg dry3.4 1/2/20SW-846 8260D204-Methyl-2-pentanone (MIBK)
9.0 4.1 1/6/20 20:59 MFFmg/Kg dry0.64 1/2/20SW-846 8260D20V-05Naphthalene
19 2.1 1/6/20 20:59 MFFmg/Kg dry0.27 1/2/20SW-846 8260D20n-Propylbenzene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.23 1/2/20SW-846 8260D20Styrene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.55 1/2/20SW-846 8260D201,1,1,2-Tetrachloroethane
ND 1.0 1/6/20 20:59 MFFmg/Kg dry0.45 1/2/20SW-846 8260D201,1,2,2-Tetrachloroethane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.37 1/2/20SW-846 8260D20Tetrachloroethylene
ND 21 1/6/20 20:59 MFFmg/Kg dry1.0 1/2/20SW-846 8260D20Tetrahydrofuran
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.29 1/2/20SW-846 8260D20Toluene
ND 10 1/6/20 20:59 MFFmg/Kg dry1.2 1/2/20SW-846 8260D20L-04, V-051,2,3-Trichlorobenzene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.82 1/2/20SW-846 8260D20V-051,2,4-Trichlorobenzene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.62 1/2/20SW-846 8260D201,3,5-Trichlorobenzene
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.41 1/2/20SW-846 8260D201,1,1-Trichloroethane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.33 1/2/20SW-846 8260D201,1,2-Trichloroethane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.49 1/2/20SW-846 8260D20Trichloroethylene
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.68 1/2/20SW-846 8260D20Trichlorofluoromethane (Freon 11)
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.51 1/2/20SW-846 8260D201,2,3-Trichloropropane
ND 2.1 1/6/20 20:59 MFFmg/Kg dry0.66 1/2/20SW-846 8260D201,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
120 2.1 1/6/20 20:59 MFFmg/Kg dry0.37 1/2/20SW-846 8260D201,2,4-Trimethylbenzene
33 2.1 1/6/20 20:59 MFFmg/Kg dry0.29 1/2/20SW-846 8260D201,3,5-Trimethylbenzene
ND 4.1 1/6/20 20:59 MFFmg/Kg dry0.92 1/2/20SW-846 8260D20Vinyl Chloride
82 4.1 1/6/20 20:59 MFFmg/Kg dry0.62 1/2/20SW-846 8260D20m+p Xylene
68 2.1 1/6/20 20:59 MFFmg/Kg dry0.35 1/2/20SW-846 8260D20o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 1/6/20 20:5970-130
Toluene-d8 97.0 1/6/20 20:5970-130
4-Bromofluorobenzene 95.6 1/6/20 20:5970-130
Page 29 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-56
Field Sample #: PG-29-25
Sample Matrix: Soil
Sampled: 12/27/2019 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
65.6 1/5/20 16:04 JS% Wt 1/5/20SM 2540G1% Solids
Page 30 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-63
Field Sample #: PG-30-25
Sample Matrix: Soil
Sampled: 12/27/2019 14:10
[TOC_2]19L1171-63[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 35 1/6/20 21:26 MFFmg/Kg dry2.7 1/2/20SW-846 8260D10Acetone
ND 3.5 1/6/20 21:26 MFFmg/Kg dry0.37 1/2/20SW-846 8260D10Acrylonitrile
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.098 1/2/20SW-846 8260D10tert-Amyl Methyl Ether (TAME)
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.13 1/2/20SW-846 8260D10Benzene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.11 1/2/20SW-846 8260D10Bromobenzene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.22 1/2/20SW-846 8260D10Bromochloromethane
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.11 1/2/20SW-846 8260D10Bromodichloromethane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.32 1/2/20SW-846 8260D10Bromoform
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.55 1/2/20SW-846 8260D10Bromomethane
ND 14 1/6/20 21:26 MFFmg/Kg dry1.4 1/2/20SW-846 8260D102-Butanone (MEK)
ND 14 1/6/20 21:26 MFFmg/Kg dry2.9 1/2/20SW-846 8260D10tert-Butyl Alcohol (TBA)
4.6 0.70 1/6/20 21:26 MFFmg/Kg dry0.15 1/2/20SW-846 8260D10n-Butylbenzene
0.97 0.70 1/6/20 21:26 MFFmg/Kg dry0.11 1/2/20SW-846 8260D10sec-Butylbenzene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.12 1/2/20SW-846 8260D10tert-Butylbenzene
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.11 1/2/20SW-846 8260D10tert-Butyl Ethyl Ether (TBEE)
ND 3.5 1/6/20 21:26 MFFmg/Kg dry3.1 1/2/20SW-846 8260D10Carbon Disulfide
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.077 1/2/20SW-846 8260D10Carbon Tetrachloride
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.11 1/2/20SW-846 8260D10Chlorobenzene
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.15 1/2/20SW-846 8260D10Chlorodibromomethane
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.25 1/2/20SW-846 8260D10Chloroethane
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.12 1/2/20SW-846 8260D10Chloroform
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.32 1/2/20SW-846 8260D10Chloromethane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.084 1/2/20SW-846 8260D102-Chlorotoluene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.098 1/2/20SW-846 8260D104-Chlorotoluene
ND 3.5 1/6/20 21:26 MFFmg/Kg dry0.37 1/2/20SW-846 8260D101,2-Dibromo-3-chloropropane (DBCP)
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.13 1/2/20SW-846 8260D101,2-Dibromoethane (EDB)
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.26 1/2/20SW-846 8260D10Dibromomethane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.11 1/2/20SW-846 8260D101,2-Dichlorobenzene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.084 1/2/20SW-846 8260D101,3-Dichlorobenzene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.091 1/2/20SW-846 8260D101,4-Dichlorobenzene
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.22 1/2/20SW-846 8260D10trans-1,4-Dichloro-2-butene
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.18 1/2/20SW-846 8260D10Dichlorodifluoromethane (Freon 12)
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.11 1/2/20SW-846 8260D101,1-Dichloroethane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.29 1/2/20SW-846 8260D101,2-Dichloroethane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.22 1/2/20SW-846 8260D101,1-Dichloroethylene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.091 1/2/20SW-846 8260D10cis-1,2-Dichloroethylene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.22 1/2/20SW-846 8260D10trans-1,2-Dichloroethylene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.14 1/2/20SW-846 8260D101,2-Dichloropropane
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.077 1/2/20SW-846 8260D101,3-Dichloropropane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.14 1/2/20SW-846 8260D102,2-Dichloropropane
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.11 1/2/20SW-846 8260D101,1-Dichloropropene
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.091 1/2/20SW-846 8260D10cis-1,3-Dichloropropene
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.16 1/2/20SW-846 8260D10trans-1,3-Dichloropropene
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.24 1/2/20SW-846 8260D10Diethyl Ether
Page 31 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-63
Field Sample #: PG-30-25
Sample Matrix: Soil
Sampled: 12/27/2019 14:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.12 1/2/20SW-846 8260D10Diisopropyl Ether (DIPE)
ND 35 1/6/20 21:26 MFFmg/Kg dry16 1/2/20SW-846 8260D101,4-Dioxane
26 0.70 1/6/20 21:26 MFFmg/Kg dry0.091 1/2/20SW-846 8260D10Ethylbenzene
ND 0.42 1/6/20 21:26 MFFmg/Kg dry0.33 1/2/20SW-846 8260D10Hexachlorobutadiene
ND 7.0 1/6/20 21:26 MFFmg/Kg dry1.1 1/2/20SW-846 8260D102-Hexanone (MBK)
2.4 0.70 1/6/20 21:26 MFFmg/Kg dry0.12 1/2/20SW-846 8260D10Isopropylbenzene (Cumene)
0.60 0.70 1/6/20 21:26 MFFmg/Kg dry0.14 1/2/20SW-846 8260D10Jp-Isopropyltoluene (p-Cymene)
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.18 1/2/20SW-846 8260D10Methyl tert-Butyl Ether (MTBE)
ND 3.5 1/6/20 21:26 MFFmg/Kg dry0.24 1/2/20SW-846 8260D10Methylene Chloride
ND 7.0 1/6/20 21:26 MFFmg/Kg dry1.2 1/2/20SW-846 8260D104-Methyl-2-pentanone (MIBK)
4.1 1.4 1/6/20 21:26 MFFmg/Kg dry0.22 1/2/20SW-846 8260D10V-05Naphthalene
9.5 0.70 1/6/20 21:26 MFFmg/Kg dry0.091 1/2/20SW-846 8260D10n-Propylbenzene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.077 1/2/20SW-846 8260D10Styrene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.19 1/2/20SW-846 8260D101,1,1,2-Tetrachloroethane
ND 0.35 1/6/20 21:26 MFFmg/Kg dry0.15 1/2/20SW-846 8260D101,1,2,2-Tetrachloroethane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.13 1/2/20SW-846 8260D10Tetrachloroethylene
ND 7.0 1/6/20 21:26 MFFmg/Kg dry0.36 1/2/20SW-846 8260D10Tetrahydrofuran
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.098 1/2/20SW-846 8260D10Toluene
ND 3.5 1/6/20 21:26 MFFmg/Kg dry0.40 1/2/20SW-846 8260D10L-04, V-051,2,3-Trichlorobenzene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.28 1/2/20SW-846 8260D10V-051,2,4-Trichlorobenzene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.21 1/2/20SW-846 8260D101,3,5-Trichlorobenzene
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.14 1/2/20SW-846 8260D101,1,1-Trichloroethane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.11 1/2/20SW-846 8260D101,1,2-Trichloroethane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.17 1/2/20SW-846 8260D10Trichloroethylene
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.23 1/2/20SW-846 8260D10Trichlorofluoromethane (Freon 11)
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.18 1/2/20SW-846 8260D101,2,3-Trichloropropane
ND 0.70 1/6/20 21:26 MFFmg/Kg dry0.22 1/2/20SW-846 8260D101,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
56 0.70 1/6/20 21:26 MFFmg/Kg dry0.13 1/2/20SW-846 8260D101,2,4-Trimethylbenzene
16 0.70 1/6/20 21:26 MFFmg/Kg dry0.098 1/2/20SW-846 8260D101,3,5-Trimethylbenzene
ND 1.4 1/6/20 21:26 MFFmg/Kg dry0.32 1/2/20SW-846 8260D10Vinyl Chloride
34 1.4 1/6/20 21:26 MFFmg/Kg dry0.21 1/2/20SW-846 8260D10m+p Xylene
5.3 0.70 1/6/20 21:26 MFFmg/Kg dry0.12 1/2/20SW-846 8260D10o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 1/6/20 21:2670-130
Toluene-d8 99.1 1/6/20 21:2670-130
4-Bromofluorobenzene 97.0 1/6/20 21:2670-130
Page 32 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-63
Field Sample #: PG-30-25
Sample Matrix: Soil
Sampled: 12/27/2019 14:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
77.2 1/5/20 16:04 JS% Wt 1/5/20SM 2540G1% Solids
Page 33 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-66
Field Sample #: DUP-122719
Sample Matrix: Soil
Sampled: 12/27/2019 00:00
[TOC_2]19L1171-66[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.14 1/2/20 10:27 MFFmg/Kg dry0.033 1/2/20SW-846 8260D1Acetone
ND 0.0085 1/2/20 10:27 MFFmg/Kg dry0.0036 1/2/20SW-846 8260D1Acrylonitrile
ND 0.0014 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1Benzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Bromobenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0020 1/2/20SW-846 8260D1Bromochloromethane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00085 1/2/20SW-846 8260D1Bromodichloromethane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0020 1/2/20SW-846 8260D1Bromoform
ND 0.014 1/2/20 10:27 MFFmg/Kg dry0.0060 1/2/20SW-846 8260D1V-34Bromomethane
ND 0.057 1/2/20 10:27 MFFmg/Kg dry0.025 1/2/20SW-846 8260D12-Butanone (MEK)
ND 0.057 1/2/20 10:27 MFFmg/Kg dry0.030 1/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1n-Butylbenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1sec-Butylbenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1tert-Butylbenzene
ND 0.0014 1/2/20 10:27 MFFmg/Kg dry0.00085 1/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0085 1/2/20 10:27 MFFmg/Kg dry0.0061 1/2/20SW-846 8260D1Carbon Disulfide
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1Chlorobenzene
ND 0.0014 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1Chlorodibromomethane
ND 0.028 1/2/20 10:27 MFFmg/Kg dry0.0021 1/2/20SW-846 8260D1Chloroethane
0.0022 0.0057 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1JChloroform
ND 0.014 1/2/20 10:27 MFFmg/Kg dry0.0091 1/2/20SW-846 8260D1V-05Chloromethane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D12-Chlorotoluene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D14-Chlorotoluene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0014 1/2/20 10:27 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00085 1/2/20SW-846 8260D1Dibromomethane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0057 1/2/20 10:27 MFFmg/Kg dry0.0030 1/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.028 1/2/20 10:27 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0057 1/2/20 10:27 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D11,2-Dichloropropane
ND 0.0014 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,1-Dichloropropene
ND 0.0014 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0014 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.028 1/2/20 10:27 MFFmg/Kg dry0.0026 1/2/20SW-846 8260D1Diethyl Ether
Page 34 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-66
Field Sample #: DUP-122719
Sample Matrix: Soil
Sampled: 12/27/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0014 1/2/20 10:27 MFFmg/Kg dry0.00085 1/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.14 1/2/20 10:27 MFFmg/Kg dry0.082 1/2/20SW-846 8260D11,4-Dioxane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Ethylbenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.028 1/2/20 10:27 MFFmg/Kg dry0.015 1/2/20SW-846 8260D12-Hexanone (MBK)
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0057 1/2/20 10:27 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.028 1/2/20 10:27 MFFmg/Kg dry0.010 1/2/20SW-846 8260D1Methylene Chloride
ND 0.028 1/2/20 10:27 MFFmg/Kg dry0.011 1/2/20SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0057 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1Naphthalene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1n-Propylbenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00085 1/2/20SW-846 8260D1Styrene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0026 1/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0014 1/2/20 10:27 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0018 1/2/20SW-846 8260D1Tetrachloroethylene
ND 0.014 1/2/20 10:27 MFFmg/Kg dry0.0031 1/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D1Toluene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00085 1/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0017 1/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0014 1/2/20SW-846 8260D1Trichloroethylene
ND 0.014 1/2/20 10:27 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.014 1/2/20 10:27 MFFmg/Kg dry0.0013 1/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.0011 1/2/20SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00085 1/2/20SW-846 8260D11,3,5-Trimethylbenzene
ND 0.014 1/2/20 10:27 MFFmg/Kg dry0.0016 1/2/20SW-846 8260D1Vinyl Chloride
ND 0.0057 1/2/20 10:27 MFFmg/Kg dry0.0024 1/2/20SW-846 8260D1m+p Xylene
ND 0.0028 1/2/20 10:27 MFFmg/Kg dry0.00099 1/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 92.6 1/2/20 10:2770-130
Toluene-d8 98.7 1/2/20 10:2770-130
4-Bromofluorobenzene 98.4 1/2/20 10:2770-130
Page 35 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-66
Field Sample #: DUP-122719
Sample Matrix: Soil
Sampled: 12/27/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
67.9 1/5/20 16:05 JS% Wt 1/5/20SM 2540G1% Solids
Page 36 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-67
Field Sample #: DUP-COMP
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
[TOC_2]19L1171-67[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Acenaphthene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Acenaphthylene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Acetophenone
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Aniline
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Anthracene
ND 0.94 1/4/20 12:27 KLBmg/Kg dry0.26 1/3/20SW-846 8270E1V-04, V-05, V-35Benzidine
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Benzo(a)anthracene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Benzo(a)pyrene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.4 1/4/20 12:27 KLBmg/Kg dry0.84 1/3/20SW-846 8270E1Benzoic Acid
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.24 1/3/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.33 1/3/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E14-Bromophenylphenylether
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Butylbenzylphthalate
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Carbazole
ND 0.94 1/4/20 12:27 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1V-344-Chloroaniline
ND 0.94 1/4/20 12:27 KLBmg/Kg dry0.20 1/3/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12-Chloronaphthalene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12-Chlorophenol
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E14-Chlorophenylphenylether
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Chrysene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Dibenzofuran
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Di-n-butylphthalate
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Dichlorobenzene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,3-Dichlorobenzene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11,4-Dichlorobenzene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.19 1/3/20SW-846 8270E13,3-Dichlorobenzidine
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12,4-Dichlorophenol
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Diethylphthalate
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4-Dimethylphenol
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Dimethylphthalate
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.43 1/3/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.94 1/4/20 12:27 KLBmg/Kg dry0.66 1/3/20SW-846 8270E12,4-Dinitrophenol
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.23 1/3/20SW-846 8270E1V-202,4-Dinitrotoluene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.23 1/3/20SW-846 8270E12,6-Dinitrotoluene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1Di-n-octylphthalate
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Fluoranthene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Fluorene
Page 37 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-67
Field Sample #: DUP-COMP
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Hexachlorobenzene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1V-05Hexachlorobutadiene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.40 1/3/20SW-846 8270E1L-04, V-05Hexachlorocyclopentadiene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Hexachloroethane
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Isophorone
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11-Methylnaphthalene
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E12-Methylnaphthalene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.19 1/3/20SW-846 8270E12-Methylphenol
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E13/4-Methylphenol
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Naphthalene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.29 1/3/20SW-846 8270E12-Nitroaniline
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.20 1/3/20SW-846 8270E13-Nitroaniline
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.19 1/3/20SW-846 8270E14-Nitroaniline
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Nitrobenzene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.20 1/3/20SW-846 8270E12-Nitrophenol
ND 0.94 1/4/20 12:27 KLBmg/Kg dry0.34 1/3/20SW-846 8270E14-Nitrophenol
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.26 1/3/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Pentachloronitrobenzene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.33 1/3/20SW-846 8270E1V-05Pentachlorophenol
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Phenanthrene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1V-20Phenol
ND 0.24 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Pyrene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Pyridine
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.19 1/3/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.16 1/3/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.49 1/4/20 12:27 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 77.5 1/4/20 12:2730-130
Phenol-d6 82.9 1/4/20 12:2730-130
Nitrobenzene-d5 73.0 1/4/20 12:2730-130
2-Fluorobiphenyl 84.3 1/4/20 12:2730-130
2,4,6-Tribromophenol 78.2 1/4/20 12:2730-130
p-Terphenyl-d14 70.0 1/4/20 12:2730-130
Page 38 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-67
Field Sample #: DUP-COMP
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.25 0.24 1/7/20 12:07 MJHmg/Kg dry0.044 1/6/20SW-846 6020B5Arsenic
7.7 6.0 1/7/20 12:07 MJHmg/Kg dry0.17 1/6/20SW-846 6020B5Chromium
5.9 2.4 1/7/20 12:07 MJHmg/Kg dry0.031 1/6/20SW-846 6020B5Lead
ND 0.037 1/7/20 10:25 CJVmg/Kg dry0.011 1/6/20SW-846 7471B1Mercury
ND 1.9 1/7/20 12:07 MJHmg/Kg dry0.14 1/6/20SW-846 6020B5Selenium
0.032 0.12 1/7/20 12:07 MJHmg/Kg dry0.021 1/6/20SW-846 6020B5JSilver
300 12 1/7/20 12:07 MJHmg/Kg dry0.11 1/6/20SW-846 6020B5MS-19Barium
0.052 0.48 1/7/20 12:07 MJHmg/Kg dry0.021 1/6/20SW-846 6020B5JCadmium
Page 39 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-67
Field Sample #: DUP-COMP
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
69.2 1/5/20 16:05 JS% Wt 1/5/20SM 2540G1% Solids
Page 40 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-67
Field Sample #: DUP-COMP
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Method 7199
Attached Attached 1/6/20 23:35 PALmg/KgAttached Method 71991Hexavalent Chromium
Page 41 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-68
Field Sample #: TRIP BLANK
Sample Matrix: Trip Blank Soil
Sampled: 12/26/2019 00:00
[TOC_2]19L1171-68[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.10 1/2/20 10:54 MFFmg/Kg wet0.023 1/2/20SW-846 8260D1Acetone
ND 0.0060 1/2/20 10:54 MFFmg/Kg wet0.0025 1/2/20SW-846 8260D1Acrylonitrile
ND 0.0010 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1Benzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D1Bromobenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0014 1/2/20SW-846 8260D1Bromochloromethane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00060 1/2/20SW-846 8260D1Bromodichloromethane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0014 1/2/20SW-846 8260D1Bromoform
ND 0.010 1/2/20 10:54 MFFmg/Kg wet0.0042 1/2/20SW-846 8260D1V-34Bromomethane
ND 0.040 1/2/20 10:54 MFFmg/Kg wet0.018 1/2/20SW-846 8260D12-Butanone (MEK)
ND 0.040 1/2/20 10:54 MFFmg/Kg wet0.021 1/2/20SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1n-Butylbenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0010 1/2/20SW-846 8260D1sec-Butylbenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00090 1/2/20SW-846 8260D1tert-Butylbenzene
ND 0.0010 1/2/20 10:54 MFFmg/Kg wet0.00060 1/2/20SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0060 1/2/20 10:54 MFFmg/Kg wet0.0043 1/2/20SW-846 8260D1Carbon Disulfide
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D1Carbon Tetrachloride
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1Chlorobenzene
ND 0.0010 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1Chlorodibromomethane
ND 0.020 1/2/20 10:54 MFFmg/Kg wet0.0015 1/2/20SW-846 8260D1Chloroethane
ND 0.0040 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1Chloroform
ND 0.010 1/2/20 10:54 MFFmg/Kg wet0.0064 1/2/20SW-846 8260D1V-05Chloromethane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D12-Chlorotoluene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D14-Chlorotoluene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0011 1/2/20SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0010 1/2/20 10:54 MFFmg/Kg wet0.0010 1/2/20SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00060 1/2/20SW-846 8260D1Dibromomethane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D11,2-Dichlorobenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D11,3-Dichlorobenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D11,4-Dichlorobenzene
ND 0.0040 1/2/20 10:54 MFFmg/Kg wet0.0021 1/2/20SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.020 1/2/20 10:54 MFFmg/Kg wet0.0013 1/2/20SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D11,1-Dichloroethane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0013 1/2/20SW-846 8260D11,2-Dichloroethane
ND 0.0040 1/2/20 10:54 MFFmg/Kg wet0.0011 1/2/20SW-846 8260D11,1-Dichloroethylene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00090 1/2/20SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0013 1/2/20SW-846 8260D11,2-Dichloropropane
ND 0.0010 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D11,3-Dichloropropane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00090 1/2/20SW-846 8260D12,2-Dichloropropane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00090 1/2/20SW-846 8260D11,1-Dichloropropene
ND 0.0010 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0010 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1trans-1,3-Dichloropropene
ND 0.020 1/2/20 10:54 MFFmg/Kg wet0.0018 1/2/20SW-846 8260D1Diethyl Ether
Page 42 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-68
Field Sample #: TRIP BLANK
Sample Matrix: Trip Blank Soil
Sampled: 12/26/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0010 1/2/20 10:54 MFFmg/Kg wet0.00060 1/2/20SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.10 1/2/20 10:54 MFFmg/Kg wet0.058 1/2/20SW-846 8260D11,4-Dioxane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D1Ethylbenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0010 1/2/20SW-846 8260D1Hexachlorobutadiene
ND 0.020 1/2/20 10:54 MFFmg/Kg wet0.011 1/2/20SW-846 8260D12-Hexanone (MBK)
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0040 1/2/20 10:54 MFFmg/Kg wet0.00090 1/2/20SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.020 1/2/20 10:54 MFFmg/Kg wet0.0071 1/2/20SW-846 8260D1Methylene Chloride
ND 0.020 1/2/20 10:54 MFFmg/Kg wet0.0076 1/2/20SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0040 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1Naphthalene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1n-Propylbenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00060 1/2/20SW-846 8260D1Styrene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0018 1/2/20SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0010 1/2/20 10:54 MFFmg/Kg wet0.00090 1/2/20SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0013 1/2/20SW-846 8260D1Tetrachloroethylene
ND 0.010 1/2/20 10:54 MFFmg/Kg wet0.0022 1/2/20SW-846 8260D1Tetrahydrofuran
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D1Toluene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00060 1/2/20SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0010 1/2/20SW-846 8260D11,1,1-Trichloroethane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0012 1/2/20SW-846 8260D11,1,2-Trichloroethane
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0010 1/2/20SW-846 8260D1Trichloroethylene
ND 0.010 1/2/20 10:54 MFFmg/Kg wet0.0011 1/2/20SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.0011 1/2/20SW-846 8260D11,2,3-Trichloropropane
ND 0.010 1/2/20 10:54 MFFmg/Kg wet0.00090 1/2/20SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00080 1/2/20SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00060 1/2/20SW-846 8260D11,3,5-Trimethylbenzene
ND 0.010 1/2/20 10:54 MFFmg/Kg wet0.0011 1/2/20SW-846 8260D1Vinyl Chloride
ND 0.0040 1/2/20 10:54 MFFmg/Kg wet0.0017 1/2/20SW-846 8260D1m+p Xylene
ND 0.0020 1/2/20 10:54 MFFmg/Kg wet0.00070 1/2/20SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.1 1/2/20 10:5470-130
Toluene-d8 97.1 1/2/20 10:5470-130
4-Bromofluorobenzene 98.8 1/2/20 10:5470-130
Page 43 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-69
Field Sample #: COMP-PG21
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
[TOC_2]19L1171-69[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Acenaphthene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Acenaphthylene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Acetophenone
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Aniline
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Anthracene
ND 0.94 1/4/20 12:56 KLBmg/Kg dry0.26 1/3/20SW-846 8270E1V-04, V-05, V-35Benzidine
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Benzo(a)anthracene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Benzo(a)pyrene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.4 1/4/20 12:56 KLBmg/Kg dry0.84 1/3/20SW-846 8270E1Benzoic Acid
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.24 1/3/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.33 1/3/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E14-Bromophenylphenylether
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Butylbenzylphthalate
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Carbazole
ND 0.94 1/4/20 12:56 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1V-344-Chloroaniline
ND 0.94 1/4/20 12:56 KLBmg/Kg dry0.20 1/3/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12-Chloronaphthalene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12-Chlorophenol
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E14-Chlorophenylphenylether
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Chrysene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Dibenzofuran
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Di-n-butylphthalate
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Dichlorobenzene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,3-Dichlorobenzene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11,4-Dichlorobenzene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.18 1/3/20SW-846 8270E13,3-Dichlorobenzidine
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12,4-Dichlorophenol
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Diethylphthalate
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4-Dimethylphenol
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Dimethylphthalate
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.43 1/3/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.94 1/4/20 12:56 KLBmg/Kg dry0.65 1/3/20SW-846 8270E12,4-Dinitrophenol
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.23 1/3/20SW-846 8270E1V-202,4-Dinitrotoluene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.23 1/3/20SW-846 8270E12,6-Dinitrotoluene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1Di-n-octylphthalate
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Fluoranthene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Fluorene
Page 44 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-69
Field Sample #: COMP-PG21
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Hexachlorobenzene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1V-05Hexachlorobutadiene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.40 1/3/20SW-846 8270E1L-04, V-05Hexachlorocyclopentadiene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Hexachloroethane
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Isophorone
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11-Methylnaphthalene
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E12-Methylnaphthalene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.18 1/3/20SW-846 8270E12-Methylphenol
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E13/4-Methylphenol
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Naphthalene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.28 1/3/20SW-846 8270E12-Nitroaniline
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.20 1/3/20SW-846 8270E13-Nitroaniline
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.18 1/3/20SW-846 8270E14-Nitroaniline
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Nitrobenzene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.20 1/3/20SW-846 8270E12-Nitrophenol
ND 0.94 1/4/20 12:56 KLBmg/Kg dry0.34 1/3/20SW-846 8270E14-Nitrophenol
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.26 1/3/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Pentachloronitrobenzene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.33 1/3/20SW-846 8270E1V-05Pentachlorophenol
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Phenanthrene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1V-20Phenol
ND 0.24 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Pyrene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Pyridine
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.18 1/3/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.16 1/3/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.48 1/4/20 12:56 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 64.8 1/4/20 12:5630-130
Phenol-d6 70.2 1/4/20 12:5630-130
Nitrobenzene-d5 61.9 1/4/20 12:5630-130
2-Fluorobiphenyl 72.1 1/4/20 12:5630-130
2,4,6-Tribromophenol 68.4 1/4/20 12:5630-130
p-Terphenyl-d14 60.7 1/4/20 12:5630-130
Page 45 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-69
Field Sample #: COMP-PG21
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.28 0.23 1/7/20 12:11 MJHmg/Kg dry0.044 1/6/20SW-846 6020B5Arsenic
9.2 5.9 1/7/20 12:11 MJHmg/Kg dry0.17 1/6/20SW-846 6020B5Chromium
7.2 2.3 1/7/20 12:11 MJHmg/Kg dry0.030 1/6/20SW-846 6020B5Lead
ND 0.034 1/7/20 10:27 CJVmg/Kg dry0.010 1/6/20SW-846 7471B1Mercury
ND 1.9 1/7/20 12:11 MJHmg/Kg dry0.14 1/6/20SW-846 6020B5Selenium
0.042 0.12 1/7/20 12:11 MJHmg/Kg dry0.021 1/6/20SW-846 6020B5JSilver
180 12 1/7/20 12:11 MJHmg/Kg dry0.10 1/6/20SW-846 6020B5Barium
0.029 0.47 1/7/20 12:11 MJHmg/Kg dry0.021 1/6/20SW-846 6020B5JCadmium
Page 46 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-69
Field Sample #: COMP-PG21
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
69.4 1/5/20 16:05 JS% Wt 1/5/20SM 2540G1% Solids
Page 47 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-69
Field Sample #: COMP-PG21
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:40:00AM
Stop Date/Time: 12/26/2019 10:20:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Method 7199
Attached Attached 1/6/20 23:48 PALmg/KgAttached Method 71991Hexavalent Chromium
Page 48 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-70
Field Sample #: COMP-PG22
Sample Matrix: Soil
Start Date/Time: 12/26/2019 4:10:00PM
Stop Date/Time: 12/26/2019 4:45:00PM
[TOC_2]19L1171-70[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Acenaphthene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Acenaphthylene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Acetophenone
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Aniline
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Anthracene
ND 0.91 1/4/20 13:25 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1V-04, V-05, V-35Benzidine
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)anthracene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)pyrene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.4 1/4/20 13:25 KLBmg/Kg dry0.82 1/3/20SW-846 8270E1Benzoic Acid
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.23 1/3/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E14-Bromophenylphenylether
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Butylbenzylphthalate
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Carbazole
ND 0.91 1/4/20 13:25 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1V-344-Chloroaniline
ND 0.91 1/4/20 13:25 KLBmg/Kg dry0.19 1/3/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12-Chloronaphthalene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12-Chlorophenol
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E14-Chlorophenylphenylether
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Chrysene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Dibenzofuran
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Di-n-butylphthalate
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Dichlorobenzene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,3-Dichlorobenzene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.12 1/3/20SW-846 8270E11,4-Dichlorobenzene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E13,3-Dichlorobenzidine
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12,4-Dichlorophenol
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Diethylphthalate
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4-Dimethylphenol
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Dimethylphthalate
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.41 1/3/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.91 1/4/20 13:25 KLBmg/Kg dry0.64 1/3/20SW-846 8270E12,4-Dinitrophenol
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.22 1/3/20SW-846 8270E1V-202,4-Dinitrotoluene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.22 1/3/20SW-846 8270E12,6-Dinitrotoluene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1Di-n-octylphthalate
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Fluoranthene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Fluorene
Page 49 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-70
Field Sample #: COMP-PG22
Sample Matrix: Soil
Start Date/Time: 12/26/2019 4:10:00PM
Stop Date/Time: 12/26/2019 4:45:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Hexachlorobenzene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1V-05Hexachlorobutadiene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.39 1/3/20SW-846 8270E1L-04, V-05Hexachlorocyclopentadiene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Hexachloroethane
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Isophorone
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.12 1/3/20SW-846 8270E11-Methylnaphthalene
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12-Methylnaphthalene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E12-Methylphenol
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E13/4-Methylphenol
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Naphthalene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.28 1/3/20SW-846 8270E12-Nitroaniline
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.19 1/3/20SW-846 8270E13-Nitroaniline
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E14-Nitroaniline
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Nitrobenzene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.19 1/3/20SW-846 8270E12-Nitrophenol
ND 0.91 1/4/20 13:25 KLBmg/Kg dry0.33 1/3/20SW-846 8270E14-Nitrophenol
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Pentachloronitrobenzene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1V-05Pentachlorophenol
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Phenanthrene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1V-20Phenol
ND 0.23 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Pyrene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Pyridine
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.47 1/4/20 13:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 62.8 1/4/20 13:2530-130
Phenol-d6 66.4 1/4/20 13:2530-130
Nitrobenzene-d5 58.4 1/4/20 13:2530-130
2-Fluorobiphenyl 70.5 1/4/20 13:2530-130
2,4,6-Tribromophenol 67.8 1/4/20 13:2530-130
p-Terphenyl-d14 58.2 1/4/20 13:2530-130
Page 50 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-70
Field Sample #: COMP-PG22
Sample Matrix: Soil
Start Date/Time: 12/26/2019 4:10:00PM
Stop Date/Time: 12/26/2019 4:45:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.36 0.22 1/7/20 12:14 MJHmg/Kg dry0.042 1/6/20SW-846 6020B5Arsenic
9.8 5.6 1/7/20 12:14 MJHmg/Kg dry0.16 1/6/20SW-846 6020B5Chromium
8.9 2.2 1/7/20 12:14 MJHmg/Kg dry0.029 1/6/20SW-846 6020B5Lead
0.012 0.033 1/7/20 10:23 CJVmg/Kg dry0.010 1/6/20SW-846 7471B1JMercury
ND 1.8 1/7/20 12:14 MJHmg/Kg dry0.13 1/6/20SW-846 6020B5Selenium
0.034 0.11 1/7/20 12:14 MJHmg/Kg dry0.020 1/6/20SW-846 6020B5JSilver
200 11 1/7/20 12:14 MJHmg/Kg dry0.099 1/6/20SW-846 6020B5Barium
0.075 0.45 1/7/20 12:14 MJHmg/Kg dry0.020 1/6/20SW-846 6020B5JCadmium
Page 51 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-70
Field Sample #: COMP-PG22
Sample Matrix: Soil
Start Date/Time: 12/26/2019 4:10:00PM
Stop Date/Time: 12/26/2019 4:45:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
71.7 1/5/20 16:05 JS% Wt 1/5/20SM 2540G1% Solids
Page 52 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-70
Field Sample #: COMP-PG22
Sample Matrix: Soil
Start Date/Time: 12/26/2019 4:10:00PM
Stop Date/Time: 12/26/2019 4:45:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Method 7199
Attached Attached 1/6/20 23:54 PALmg/KgAttached Method 71991Hexavalent Chromium
Page 53 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-71
Field Sample #: COMP-PG23
Sample Matrix: Soil
Start Date/Time: 12/26/2019 11:00:00AM
Stop Date/Time: 12/26/2019 11:35:00AM
[TOC_2]19L1171-71[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Acenaphthene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Acenaphthylene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Acetophenone
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Aniline
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Anthracene
ND 0.91 1/4/20 13:54 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1V-04, V-05, V-35Benzidine
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)anthracene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)pyrene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.4 1/4/20 13:54 KLBmg/Kg dry0.81 1/3/20SW-846 8270E1Benzoic Acid
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.23 1/3/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E14-Bromophenylphenylether
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Butylbenzylphthalate
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Carbazole
ND 0.91 1/4/20 13:54 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1V-344-Chloroaniline
ND 0.91 1/4/20 13:54 KLBmg/Kg dry0.19 1/3/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12-Chloronaphthalene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E12-Chlorophenol
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E14-Chlorophenylphenylether
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Chrysene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Dibenzofuran
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Di-n-butylphthalate
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Dichlorobenzene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,3-Dichlorobenzene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E11,4-Dichlorobenzene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.18 1/3/20SW-846 8270E13,3-Dichlorobenzidine
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12,4-Dichlorophenol
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Diethylphthalate
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E12,4-Dimethylphenol
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Dimethylphthalate
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.41 1/3/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.91 1/4/20 13:54 KLBmg/Kg dry0.63 1/3/20SW-846 8270E12,4-Dinitrophenol
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.22 1/3/20SW-846 8270E1V-202,4-Dinitrotoluene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.22 1/3/20SW-846 8270E12,6-Dinitrotoluene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1Di-n-octylphthalate
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Fluoranthene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Fluorene
Page 54 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-71
Field Sample #: COMP-PG23
Sample Matrix: Soil
Start Date/Time: 12/26/2019 11:00:00AM
Stop Date/Time: 12/26/2019 11:35:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Hexachlorobenzene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1V-05Hexachlorobutadiene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.38 1/3/20SW-846 8270E1L-04, V-05Hexachlorocyclopentadiene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Hexachloroethane
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Isophorone
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E11-Methylnaphthalene
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12-Methylnaphthalene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.18 1/3/20SW-846 8270E12-Methylphenol
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E13/4-Methylphenol
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Naphthalene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.27 1/3/20SW-846 8270E12-Nitroaniline
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.19 1/3/20SW-846 8270E13-Nitroaniline
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.18 1/3/20SW-846 8270E14-Nitroaniline
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Nitrobenzene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.19 1/3/20SW-846 8270E12-Nitrophenol
ND 0.91 1/4/20 13:54 KLBmg/Kg dry0.33 1/3/20SW-846 8270E14-Nitrophenol
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Pentachloronitrobenzene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1V-05Pentachlorophenol
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Phenanthrene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1V-20Phenol
ND 0.23 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Pyrene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Pyridine
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.18 1/3/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.47 1/4/20 13:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 66.6 1/4/20 13:5430-130
Phenol-d6 70.5 1/4/20 13:5430-130
Nitrobenzene-d5 63.1 1/4/20 13:5430-130
2-Fluorobiphenyl 74.0 1/4/20 13:5430-130
2,4,6-Tribromophenol 68.7 1/4/20 13:5430-130
p-Terphenyl-d14 61.6 1/4/20 13:5430-130
Page 55 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-71
Field Sample #: COMP-PG23
Sample Matrix: Soil
Start Date/Time: 12/26/2019 11:00:00AM
Stop Date/Time: 12/26/2019 11:35:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.34 0.23 1/7/20 12:24 MJHmg/Kg dry0.042 1/6/20SW-846 6020B5Arsenic
6.9 5.7 1/7/20 12:24 MJHmg/Kg dry0.16 1/6/20SW-846 6020B5Chromium
7.6 2.3 1/7/20 12:24 MJHmg/Kg dry0.030 1/6/20SW-846 6020B5Lead
ND 0.034 1/7/20 10:28 CJVmg/Kg dry0.010 1/6/20SW-846 7471B1Mercury
ND 1.8 1/7/20 12:24 MJHmg/Kg dry0.13 1/6/20SW-846 6020B5Selenium
0.033 0.11 1/7/20 12:24 MJHmg/Kg dry0.020 1/6/20SW-846 6020B5JSilver
150 11 1/7/20 12:24 MJHmg/Kg dry0.10 1/6/20SW-846 6020B5Barium
0.047 0.45 1/7/20 12:24 MJHmg/Kg dry0.020 1/6/20SW-846 6020B5JCadmium
Page 56 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-71
Field Sample #: COMP-PG23
Sample Matrix: Soil
Start Date/Time: 12/26/2019 11:00:00AM
Stop Date/Time: 12/26/2019 11:35:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
72.7 1/5/20 16:05 JS% Wt 1/5/20SM 2540G1% Solids
Page 57 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-71
Field Sample #: COMP-PG23
Sample Matrix: Soil
Start Date/Time: 12/26/2019 11:00:00AM
Stop Date/Time: 12/26/2019 11:35:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Method 7199
Attached Attached 1/6/20 23:59 PALmg/KgAttached Method 71991Hexavalent Chromium
Page 58 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-72
Field Sample #: COMP-PG25
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:55:00AM
Stop Date/Time: 12/26/2019 10:40:00AM
[TOC_2]19L1171-72[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Acenaphthene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Acenaphthylene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Acetophenone
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Aniline
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Anthracene
ND 0.93 1/4/20 14:25 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1V-04, V-05, V-35Benzidine
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)anthracene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)pyrene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.4 1/4/20 14:25 KLBmg/Kg dry0.83 1/3/20SW-846 8270E1Benzoic Acid
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.24 1/3/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E14-Bromophenylphenylether
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Butylbenzylphthalate
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Carbazole
ND 0.93 1/4/20 14:25 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1V-344-Chloroaniline
ND 0.93 1/4/20 14:25 KLBmg/Kg dry0.20 1/3/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12-Chloronaphthalene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12-Chlorophenol
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E14-Chlorophenylphenylether
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Chrysene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Dibenzofuran
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Di-n-butylphthalate
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Dichlorobenzene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,3-Dichlorobenzene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11,4-Dichlorobenzene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E13,3-Dichlorobenzidine
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12,4-Dichlorophenol
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Diethylphthalate
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4-Dimethylphenol
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Dimethylphthalate
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.42 1/3/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.93 1/4/20 14:25 KLBmg/Kg dry0.65 1/3/20SW-846 8270E12,4-Dinitrophenol
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.22 1/3/20SW-846 8270E1V-202,4-Dinitrotoluene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.22 1/3/20SW-846 8270E12,6-Dinitrotoluene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1Di-n-octylphthalate
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Fluoranthene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Fluorene
Page 59 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-72
Field Sample #: COMP-PG25
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:55:00AM
Stop Date/Time: 12/26/2019 10:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Hexachlorobenzene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1V-05Hexachlorobutadiene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.39 1/3/20SW-846 8270E1L-04, V-05Hexachlorocyclopentadiene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Hexachloroethane
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Isophorone
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11-Methylnaphthalene
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12-Methylnaphthalene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E12-Methylphenol
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E13/4-Methylphenol
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Naphthalene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.28 1/3/20SW-846 8270E12-Nitroaniline
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.20 1/3/20SW-846 8270E13-Nitroaniline
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E14-Nitroaniline
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Nitrobenzene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.20 1/3/20SW-846 8270E12-Nitrophenol
ND 0.93 1/4/20 14:25 KLBmg/Kg dry0.34 1/3/20SW-846 8270E14-Nitrophenol
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Pentachloronitrobenzene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1V-05Pentachlorophenol
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Phenanthrene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1V-20Phenol
ND 0.24 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Pyrene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Pyridine
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.18 1/3/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.15 1/3/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.48 1/4/20 14:25 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 69.3 1/4/20 14:2530-130
Phenol-d6 74.4 1/4/20 14:2530-130
Nitrobenzene-d5 65.5 1/4/20 14:2530-130
2-Fluorobiphenyl 76.9 1/4/20 14:2530-130
2,4,6-Tribromophenol 74.1 1/4/20 14:2530-130
p-Terphenyl-d14 61.5 1/4/20 14:2530-130
Page 60 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-72
Field Sample #: COMP-PG25
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:55:00AM
Stop Date/Time: 12/26/2019 10:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.34 0.23 1/7/20 12:27 MJHmg/Kg dry0.043 1/6/20SW-846 6020B5Arsenic
4.7 5.8 1/7/20 12:27 MJHmg/Kg dry0.17 1/6/20SW-846 6020B5JChromium
9.0 2.3 1/7/20 12:27 MJHmg/Kg dry0.030 1/6/20SW-846 6020B5Lead
0.011 0.035 1/7/20 10:30 CJVmg/Kg dry0.010 1/6/20SW-846 7471B1JMercury
ND 1.9 1/7/20 12:27 MJHmg/Kg dry0.14 1/6/20SW-846 6020B5Selenium
0.030 0.12 1/7/20 12:27 MJHmg/Kg dry0.021 1/6/20SW-846 6020B5JSilver
180 12 1/7/20 12:27 MJHmg/Kg dry0.10 1/6/20SW-846 6020B5Barium
0.035 0.47 1/7/20 12:27 MJHmg/Kg dry0.021 1/6/20SW-846 6020B5JCadmium
Page 61 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-72
Field Sample #: COMP-PG25
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:55:00AM
Stop Date/Time: 12/26/2019 10:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
70.8 1/5/20 16:05 JS% Wt 1/5/20SM 2540G1% Solids
Page 62 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-72
Field Sample #: COMP-PG25
Sample Matrix: Soil
Start Date/Time: 12/26/2019 9:55:00AM
Stop Date/Time: 12/26/2019 10:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Method 7199
Attached Attached 1/7/20 0:35 PALmg/KgAttached Method 71991Hexavalent Chromium
Page 63 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-73
Field Sample #: COMP-PG26
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:35:00PM
Stop Date/Time: 12/26/2019 2:10:00PM
[TOC_2]19L1171-73[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Acenaphthene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Acenaphthylene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Acetophenone
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.10 1/3/20SW-846 8270E1Aniline
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Anthracene
ND 0.82 1/4/20 14:54 KLBmg/Kg dry0.22 1/3/20SW-846 8270E1V-04, V-05, V-35Benzidine
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(a)anthracene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(a)pyrene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.2 1/4/20 14:54 KLBmg/Kg dry0.74 1/3/20SW-846 8270E1Benzoic Acid
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.29 1/3/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E14-Bromophenylphenylether
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Butylbenzylphthalate
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Carbazole
ND 0.82 1/4/20 14:54 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1V-344-Chloroaniline
ND 0.82 1/4/20 14:54 KLBmg/Kg dry0.17 1/3/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E12-Chloronaphthalene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12-Chlorophenol
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E14-Chlorophenylphenylether
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Chrysene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Dibenzofuran
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Di-n-butylphthalate
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E11,2-Dichlorobenzene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E11,3-Dichlorobenzene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.11 1/3/20SW-846 8270E11,4-Dichlorobenzene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E13,3-Dichlorobenzidine
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E12,4-Dichlorophenol
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Diethylphthalate
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12,4-Dimethylphenol
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Dimethylphthalate
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.37 1/3/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.82 1/4/20 14:54 KLBmg/Kg dry0.57 1/3/20SW-846 8270E12,4-Dinitrophenol
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1V-202,4-Dinitrotoluene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.20 1/3/20SW-846 8270E12,6-Dinitrotoluene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Di-n-octylphthalate
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Fluoranthene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Fluorene
Page 64 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-73
Field Sample #: COMP-PG26
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:35:00PM
Stop Date/Time: 12/26/2019 2:10:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Hexachlorobenzene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1V-05Hexachlorobutadiene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.35 1/3/20SW-846 8270E1L-04, V-05Hexachlorocyclopentadiene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Hexachloroethane
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Isophorone
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.11 1/3/20SW-846 8270E11-Methylnaphthalene
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12-Methylnaphthalene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E12-Methylphenol
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E13/4-Methylphenol
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Naphthalene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.25 1/3/20SW-846 8270E12-Nitroaniline
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.17 1/3/20SW-846 8270E13-Nitroaniline
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E14-Nitroaniline
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Nitrobenzene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12-Nitrophenol
ND 0.82 1/4/20 14:54 KLBmg/Kg dry0.30 1/3/20SW-846 8270E14-Nitrophenol
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.22 1/3/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Pentachloronitrobenzene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.29 1/3/20SW-846 8270E1V-05Pentachlorophenol
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Phenanthrene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1V-20Phenol
ND 0.21 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Pyrene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.12 1/3/20SW-846 8270E1Pyridine
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.16 1/3/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.42 1/4/20 14:54 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 72.0 1/4/20 14:5430-130
Phenol-d6 76.6 1/4/20 14:5430-130
Nitrobenzene-d5 67.8 1/4/20 14:5430-130
2-Fluorobiphenyl 78.6 1/4/20 14:5430-130
2,4,6-Tribromophenol 79.6 1/4/20 14:5430-130
p-Terphenyl-d14 67.8 1/4/20 14:5430-130
Page 65 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-73
Field Sample #: COMP-PG26
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:35:00PM
Stop Date/Time: 12/26/2019 2:10:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.24 0.21 1/7/20 12:30 MJHmg/Kg dry0.039 1/6/20SW-846 6020B5Arsenic
4.9 5.2 1/7/20 12:30 MJHmg/Kg dry0.15 1/6/20SW-846 6020B5JChromium
6.5 2.1 1/7/20 12:30 MJHmg/Kg dry0.027 1/6/20SW-846 6020B5Lead
0.078 0.033 1/7/20 10:36 CJVmg/Kg dry0.0099 1/6/20SW-846 7471B1Mercury
ND 1.7 1/7/20 12:30 MJHmg/Kg dry0.12 1/6/20SW-846 6020B5Selenium
ND 0.10 1/7/20 12:30 MJHmg/Kg dry0.019 1/6/20SW-846 6020B5Silver
68 10 1/7/20 12:30 MJHmg/Kg dry0.092 1/6/20SW-846 6020B5Barium
ND 0.42 1/7/20 12:30 MJHmg/Kg dry0.018 1/6/20SW-846 6020B5Cadmium
Page 66 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-73
Field Sample #: COMP-PG26
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:35:00PM
Stop Date/Time: 12/26/2019 2:10:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
79.2 1/5/20 16:05 JS% Wt 1/5/20SM 2540G1% Solids
Page 67 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-73
Field Sample #: COMP-PG26
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:35:00PM
Stop Date/Time: 12/26/2019 2:10:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Method 7199
Attached Attached 1/7/20 0:40 PALmg/KgAttached Method 71991Hexavalent Chromium
Page 68 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-74
Field Sample #: COMP-PG27
Sample Matrix: Soil
Start Date/Time: 12/26/2019 2:55:00PM
Stop Date/Time: 12/26/2019 3:25:00PM
[TOC_2]19L1171-74[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Acenaphthene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Acenaphthylene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Acetophenone
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Aniline
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Anthracene
ND 0.92 1/4/20 15:23 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1V-04, V-05, V-35Benzidine
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)anthracene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)pyrene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.4 1/4/20 15:23 KLBmg/Kg dry0.82 1/3/20SW-846 8270E1Benzoic Acid
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.24 1/3/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E14-Bromophenylphenylether
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Butylbenzylphthalate
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Carbazole
ND 0.92 1/4/20 15:23 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1V-344-Chloroaniline
ND 0.92 1/4/20 15:23 KLBmg/Kg dry0.20 1/3/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12-Chloronaphthalene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12-Chlorophenol
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E14-Chlorophenylphenylether
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Chrysene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Dibenzofuran
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Di-n-butylphthalate
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Dichlorobenzene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,3-Dichlorobenzene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11,4-Dichlorobenzene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.18 1/3/20SW-846 8270E13,3-Dichlorobenzidine
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12,4-Dichlorophenol
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Diethylphthalate
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4-Dimethylphenol
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Dimethylphthalate
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.42 1/3/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.92 1/4/20 15:23 KLBmg/Kg dry0.64 1/3/20SW-846 8270E12,4-Dinitrophenol
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.22 1/3/20SW-846 8270E1V-202,4-Dinitrotoluene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.22 1/3/20SW-846 8270E12,6-Dinitrotoluene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1Di-n-octylphthalate
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Fluoranthene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Fluorene
Page 69 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-74
Field Sample #: COMP-PG27
Sample Matrix: Soil
Start Date/Time: 12/26/2019 2:55:00PM
Stop Date/Time: 12/26/2019 3:25:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Hexachlorobenzene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1V-05Hexachlorobutadiene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.39 1/3/20SW-846 8270E1L-04, V-05Hexachlorocyclopentadiene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Hexachloroethane
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Isophorone
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11-Methylnaphthalene
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12-Methylnaphthalene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.18 1/3/20SW-846 8270E12-Methylphenol
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E13/4-Methylphenol
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Naphthalene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.28 1/3/20SW-846 8270E12-Nitroaniline
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.20 1/3/20SW-846 8270E13-Nitroaniline
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.18 1/3/20SW-846 8270E14-Nitroaniline
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Nitrobenzene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.20 1/3/20SW-846 8270E12-Nitrophenol
ND 0.92 1/4/20 15:23 KLBmg/Kg dry0.33 1/3/20SW-846 8270E14-Nitrophenol
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Pentachloronitrobenzene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1V-05Pentachlorophenol
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Phenanthrene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1V-20Phenol
ND 0.24 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Pyrene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Pyridine
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.18 1/3/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.15 1/3/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.47 1/4/20 15:23 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 71.7 1/4/20 15:2330-130
Phenol-d6 77.3 1/4/20 15:2330-130
Nitrobenzene-d5 70.9 1/4/20 15:2330-130
2-Fluorobiphenyl 80.0 1/4/20 15:2330-130
2,4,6-Tribromophenol 73.9 1/4/20 15:2330-130
p-Terphenyl-d14 64.8 1/4/20 15:2330-130
Page 70 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-74
Field Sample #: COMP-PG27
Sample Matrix: Soil
Start Date/Time: 12/26/2019 2:55:00PM
Stop Date/Time: 12/26/2019 3:25:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.94 0.24 1/7/20 12:34 MJHmg/Kg dry0.044 1/6/20SW-846 6020B5Arsenic
82 5.9 1/7/20 12:34 MJHmg/Kg dry0.17 1/6/20SW-846 6020B5Chromium
9.7 2.4 1/7/20 12:34 MJHmg/Kg dry0.031 1/6/20SW-846 6020B5Lead
0.015 0.036 1/7/20 10:37 CJVmg/Kg dry0.011 1/6/20SW-846 7471B1JMercury
ND 1.9 1/7/20 12:34 MJHmg/Kg dry0.14 1/6/20SW-846 6020B5Selenium
0.065 0.12 1/7/20 12:34 MJHmg/Kg dry0.021 1/6/20SW-846 6020B5JSilver
88 12 1/7/20 12:34 MJHmg/Kg dry0.10 1/6/20SW-846 6020B5Barium
ND 0.47 1/7/20 12:34 MJHmg/Kg dry0.021 1/6/20SW-846 6020B5Cadmium
Page 71 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-74
Field Sample #: COMP-PG27
Sample Matrix: Soil
Start Date/Time: 12/26/2019 2:55:00PM
Stop Date/Time: 12/26/2019 3:25:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
70.3 1/5/20 16:05 JS% Wt 1/5/20SM 2540G1% Solids
Page 72 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-74
Field Sample #: COMP-PG27
Sample Matrix: Soil
Start Date/Time: 12/26/2019 2:55:00PM
Stop Date/Time: 12/26/2019 3:25:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Method 7199
Attached Attached 1/7/20 0:45 PALmg/KgAttached Method 71991Hexavalent Chromium
Page 73 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-75
Field Sample #: COMP-PG29
Sample Matrix: Soil
Start Date/Time: 12/26/2019 12:55:00PM
Stop Date/Time: 12/26/2019 1:25:00PM
[TOC_2]19L1171-75[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Acenaphthene
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Acenaphthylene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Acetophenone
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Aniline
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Anthracene
ND 0.93 1/4/20 15:52 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1V-04, V-05, V-35Benzidine
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)anthracene
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(a)pyrene
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.4 1/4/20 15:52 KLBmg/Kg dry0.83 1/3/20SW-846 8270E1Benzoic Acid
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.24 1/3/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E14-Bromophenylphenylether
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Butylbenzylphthalate
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Carbazole
ND 0.93 1/4/20 15:52 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1V-344-Chloroaniline
ND 0.93 1/4/20 15:52 KLBmg/Kg dry0.20 1/3/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12-Chloronaphthalene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12-Chlorophenol
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E14-Chlorophenylphenylether
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Chrysene
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Dibenzofuran
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Di-n-butylphthalate
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Dichlorobenzene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,3-Dichlorobenzene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11,4-Dichlorobenzene
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.18 1/3/20SW-846 8270E13,3-Dichlorobenzidine
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12,4-Dichlorophenol
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Diethylphthalate
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4-Dimethylphenol
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Dimethylphthalate
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.42 1/3/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.93 1/4/20 15:52 KLBmg/Kg dry0.65 1/3/20SW-846 8270E12,4-Dinitrophenol
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.22 1/3/20SW-846 8270E1V-202,4-Dinitrotoluene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.22 1/3/20SW-846 8270E12,6-Dinitrotoluene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1Di-n-octylphthalate
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Fluoranthene
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Fluorene
Page 74 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-75
Field Sample #: COMP-PG29
Sample Matrix: Soil
Start Date/Time: 12/26/2019 12:55:00PM
Stop Date/Time: 12/26/2019 1:25:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Hexachlorobenzene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1V-05Hexachlorobutadiene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.39 1/3/20SW-846 8270E1L-04, V-05Hexachlorocyclopentadiene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Hexachloroethane
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Isophorone
0.15 0.24 1/4/20 15:52 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1J1-Methylnaphthalene
0.34 0.24 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12-Methylnaphthalene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.18 1/3/20SW-846 8270E12-Methylphenol
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E13/4-Methylphenol
0.21 0.24 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1JNaphthalene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.28 1/3/20SW-846 8270E12-Nitroaniline
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.20 1/3/20SW-846 8270E13-Nitroaniline
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.18 1/3/20SW-846 8270E14-Nitroaniline
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1Nitrobenzene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.20 1/3/20SW-846 8270E12-Nitrophenol
ND 0.93 1/4/20 15:52 KLBmg/Kg dry0.34 1/3/20SW-846 8270E14-Nitrophenol
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.25 1/3/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1Pentachloronitrobenzene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.32 1/3/20SW-846 8270E1V-05Pentachlorophenol
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Phenanthrene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E1V-20Phenol
ND 0.24 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Pyrene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Pyridine
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.18 1/3/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.15 1/3/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.48 1/4/20 15:52 KLBmg/Kg dry0.17 1/3/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 59.6 1/4/20 15:5230-130
Phenol-d6 63.4 1/4/20 15:5230-130
Nitrobenzene-d5 56.4 1/4/20 15:5230-130
2-Fluorobiphenyl 63.1 1/4/20 15:5230-130
2,4,6-Tribromophenol 58.3 1/4/20 15:5230-130
p-Terphenyl-d14 48.7 1/4/20 15:5230-130
Page 75 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-75
Field Sample #: COMP-PG29
Sample Matrix: Soil
Start Date/Time: 12/26/2019 12:55:00PM
Stop Date/Time: 12/26/2019 1:25:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.70 0.23 1/7/20 12:37 MJHmg/Kg dry0.043 1/6/20SW-846 6020B5Arsenic
65 5.8 1/7/20 12:37 MJHmg/Kg dry0.17 1/6/20SW-846 6020B5Chromium
7.2 2.3 1/7/20 12:37 MJHmg/Kg dry0.030 1/6/20SW-846 6020B5Lead
0.015 0.035 1/7/20 10:39 CJVmg/Kg dry0.011 1/6/20SW-846 7471B1JMercury
ND 1.8 1/7/20 12:37 MJHmg/Kg dry0.14 1/6/20SW-846 6020B5Selenium
0.032 0.12 1/7/20 12:37 MJHmg/Kg dry0.021 1/6/20SW-846 6020B5JSilver
120 12 1/7/20 12:37 MJHmg/Kg dry0.10 1/6/20SW-846 6020B5Barium
ND 0.46 1/7/20 12:37 MJHmg/Kg dry0.020 1/6/20SW-846 6020B5Cadmium
Page 76 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-75
Field Sample #: COMP-PG29
Sample Matrix: Soil
Start Date/Time: 12/26/2019 12:55:00PM
Stop Date/Time: 12/26/2019 1:25:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
71.3 1/5/20 16:06 JS% Wt 1/5/20SM 2540G1% Solids
Page 77 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-75
Field Sample #: COMP-PG29
Sample Matrix: Soil
Start Date/Time: 12/26/2019 12:55:00PM
Stop Date/Time: 12/26/2019 1:25:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Method 7199
Attached Attached 1/7/20 0:51 PALmg/KgAttached Method 71991Hexavalent Chromium
Page 78 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-76
Field Sample #: COMP-PG30
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:50:00PM
Stop Date/Time: 12/26/2019 2:20:00PM
[TOC_2]19L1171-76[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Acenaphthene
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Acenaphthylene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Acetophenone
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.10 1/3/20SW-846 8270E1Aniline
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Anthracene
ND 0.83 1/4/20 16:21 KLBmg/Kg dry0.23 1/3/20SW-846 8270E1V-04, V-05, V-35Benzidine
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(a)anthracene
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(a)pyrene
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(b)fluoranthene
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Benzo(g,h,i)perylene
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Benzo(k)fluoranthene
ND 1.3 1/4/20 16:21 KLBmg/Kg dry0.74 1/3/20SW-846 8270E1Benzoic Acid
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.21 1/3/20SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.29 1/3/20SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E14-Bromophenylphenylether
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Butylbenzylphthalate
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Carbazole
ND 0.83 1/4/20 16:21 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1V-344-Chloroaniline
ND 0.83 1/4/20 16:21 KLBmg/Kg dry0.18 1/3/20SW-846 8270E14-Chloro-3-methylphenol
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E12-Chloronaphthalene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12-Chlorophenol
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E14-Chlorophenylphenylether
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Chrysene
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Dibenz(a,h)anthracene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Dibenzofuran
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Di-n-butylphthalate
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11,2-Dichlorobenzene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11,3-Dichlorobenzene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.11 1/3/20SW-846 8270E11,4-Dichlorobenzene
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.16 1/3/20SW-846 8270E13,3-Dichlorobenzidine
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E12,4-Dichlorophenol
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Diethylphthalate
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12,4-Dimethylphenol
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1Dimethylphthalate
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.38 1/3/20SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.83 1/4/20 16:21 KLBmg/Kg dry0.58 1/3/20SW-846 8270E12,4-Dinitrophenol
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.20 1/3/20SW-846 8270E1V-202,4-Dinitrotoluene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.20 1/3/20SW-846 8270E12,6-Dinitrotoluene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1Di-n-octylphthalate
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Fluoranthene
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Fluorene
Page 79 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-76
Field Sample #: COMP-PG30
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:50:00PM
Stop Date/Time: 12/26/2019 2:20:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Hexachlorobenzene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.16 1/3/20SW-846 8270E1V-05Hexachlorobutadiene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.35 1/3/20SW-846 8270E1L-04, V-05Hexachlorocyclopentadiene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Hexachloroethane
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Isophorone
0.14 0.21 1/4/20 16:21 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1J1-Methylnaphthalene
0.34 0.21 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E12-Methylnaphthalene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.16 1/3/20SW-846 8270E12-Methylphenol
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E13/4-Methylphenol
0.25 0.21 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Naphthalene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.25 1/3/20SW-846 8270E12-Nitroaniline
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.18 1/3/20SW-846 8270E13-Nitroaniline
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.16 1/3/20SW-846 8270E14-Nitroaniline
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.18 1/3/20SW-846 8270E1Nitrobenzene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.18 1/3/20SW-846 8270E12-Nitrophenol
ND 0.83 1/4/20 16:21 KLBmg/Kg dry0.30 1/3/20SW-846 8270E14-Nitrophenol
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.23 1/3/20SW-846 8270E1N-Nitrosodimethylamine
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.19 1/3/20SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1Pentachloronitrobenzene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.29 1/3/20SW-846 8270E1V-05Pentachlorophenol
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.11 1/3/20SW-846 8270E1Phenanthrene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E1V-20Phenol
ND 0.21 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E1Pyrene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.13 1/3/20SW-846 8270E1Pyridine
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.16 1/3/20SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.14 1/3/20SW-846 8270E11,2,4-Trichlorobenzene
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12,4,5-Trichlorophenol
ND 0.43 1/4/20 16:21 KLBmg/Kg dry0.15 1/3/20SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 63.6 1/4/20 16:2130-130
Phenol-d6 67.3 1/4/20 16:2130-130
Nitrobenzene-d5 60.8 1/4/20 16:2130-130
2-Fluorobiphenyl 68.3 1/4/20 16:2130-130
2,4,6-Tribromophenol 63.1 1/4/20 16:2130-130
p-Terphenyl-d14 56.2 1/4/20 16:2130-130
Page 80 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-76
Field Sample #: COMP-PG30
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:50:00PM
Stop Date/Time: 12/26/2019 2:20:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.50 0.21 1/7/20 12:40 MJHmg/Kg dry0.039 1/6/20SW-846 6020B5Arsenic
14 5.2 1/7/20 12:40 MJHmg/Kg dry0.15 1/6/20SW-846 6020B5Chromium
6.5 2.1 1/7/20 12:40 MJHmg/Kg dry0.027 1/6/20SW-846 6020B5Lead
0.027 0.033 1/7/20 10:41 CJVmg/Kg dry0.0098 1/6/20SW-846 7471B1JMercury
ND 1.7 1/7/20 12:40 MJHmg/Kg dry0.12 1/6/20SW-846 6020B5Selenium
0.039 0.10 1/7/20 12:40 MJHmg/Kg dry0.019 1/6/20SW-846 6020B5JSilver
78 10 1/7/20 12:40 MJHmg/Kg dry0.093 1/6/20SW-846 6020B5Barium
ND 0.42 1/7/20 12:40 MJHmg/Kg dry0.018 1/6/20SW-846 6020B5Cadmium
Page 81 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-76
Field Sample #: COMP-PG30
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:50:00PM
Stop Date/Time: 12/26/2019 2:20:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
79.2 1/5/20 16:06 JS% Wt 1/5/20SM 2540G1% Solids
Page 82 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/30/2019
Work Order: 19L1171Sample Description:Project Location: Charlotte, NC
Sample ID: 19L1171-76
Field Sample #: COMP-PG30
Sample Matrix: Soil
Start Date/Time: 12/26/2019 1:50:00PM
Stop Date/Time: 12/26/2019 2:20:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Method 7199
Attached Attached 1/7/20 0:56 PALmg/KgAttached Method 71991Hexavalent Chromium
Page 83 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B249433 01/05/2019L1171-02 [PG-21-10]
B249433 01/05/2019L1171-11 [PG-23-10]
B249433 01/05/2019L1171-22 [PG-26-25]
B249433 01/05/2019L1171-32 [PG-27-33]
B249433 01/05/2019L1171-34 [PG-22-10]
B249433 01/05/2019L1171-46 [PG-25-25]
B249433 01/05/2019L1171-56 [PG-29-25]
B249433 01/05/2019L1171-63 [PG-30-25]
B249433 01/05/2019L1171-66 [DUP-122719]
B249433 01/05/2019L1171-67 [DUP-COMP]
B249433 01/05/2019L1171-69 [COMP-PG21]
B249433 01/05/2019L1171-70 [COMP-PG22]
B249433 01/05/2019L1171-71 [COMP-PG23]
B249433 01/05/2019L1171-72 [COMP-PG25]
B249433 01/05/2019L1171-73 [COMP-PG26]
B249433 01/05/2019L1171-74 [COMP-PG27]
B249433 01/05/2019L1171-75 [COMP-PG29]
B249433 01/05/2019L1171-76 [COMP-PG30]
Prep Method: SW-846 3050B-SW-846 6020B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B249488 01/06/201.52 50.019L1171-67 [DUP-COMP]
B249488 01/06/201.54 50.019L1171-69 [COMP-PG21]
B249488 01/06/201.55 50.019L1171-70 [COMP-PG22]
B249488 01/06/201.51 50.019L1171-71 [COMP-PG23]
B249488 01/06/201.51 50.019L1171-72 [COMP-PG25]
B249488 01/06/201.51 50.019L1171-73 [COMP-PG26]
B249488 01/06/201.51 50.019L1171-74 [COMP-PG27]
B249488 01/06/201.52 50.019L1171-75 [COMP-PG29]
B249488 01/06/201.51 50.019L1171-76 [COMP-PG30]
Prep Method: SW-846 7471-SW-846 7471B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B249454 01/06/200.590 50.019L1171-67 [DUP-COMP]
B249454 01/06/200.628 50.019L1171-69 [COMP-PG21]
B249454 01/06/200.626 50.019L1171-70 [COMP-PG22]
B249454 01/06/200.603 50.019L1171-71 [COMP-PG23]
B249454 01/06/200.606 50.019L1171-72 [COMP-PG25]
B249454 01/06/200.573 50.019L1171-73 [COMP-PG26]
B249454 01/06/200.600 50.019L1171-74 [COMP-PG27]
B249454 01/06/200.598 50.019L1171-75 [COMP-PG29]
B249454 01/06/200.582 50.019L1171-76 [COMP-PG30]
Prep Method: SW-846 5035-SW-846 8260D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B249284 01/02/205.11 10.019L1171-02 [PG-21-10]
B249284 01/02/205.14 10.019L1171-11 [PG-23-10]
B249284 01/02/205.04 10.019L1171-22 [PG-26-25]
[TOC_1]Sample Preparation Information[TOC]
Page 84 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5035-SW-846 8260D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B249284 01/02/204.58 10.019L1171-32 [PG-27-33]
B249284 01/02/205.16 10.019L1171-34 [PG-22-10]
B249284 01/02/204.72 10.019L1171-46 [PG-25-25]
B249284 01/02/205.18 10.019L1171-66 [DUP-122719]
B249284 01/02/205.00 10.019L1171-68 [TRIP BLANK]
Prep Method: SW-846 5035-SW-846 8260D
Lab Number [Field ID]Batch
Sample
Amount(g)
Methanol
Volume(mL)
Methanol
Aliquot(mL)
Final
Volume(mL)Date
19L1171-56 [PG-29-25]B249440 4.99 6.72 0.05 50 01/02/20
19L1171-63 [PG-30-25]B249440 5.83 6.33 0.1 50 01/02/20
Prep Method: SW-846 3546-SW-846 8270E
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B249356 01/03/2030.3 1.0019L1171-67 [DUP-COMP]
B249356 01/03/2030.4 1.0019L1171-69 [COMP-PG21]
B249356 01/03/2030.3 1.0019L1171-70 [COMP-PG22]
B249356 01/03/2030.1 1.0019L1171-71 [COMP-PG23]
B249356 01/03/2030.2 1.0019L1171-72 [COMP-PG25]
B249356 01/03/2030.3 1.0019L1171-73 [COMP-PG26]
B249356 01/03/2030.6 1.0019L1171-74 [COMP-PG27]
B249356 01/03/2030.0 1.0019L1171-75 [COMP-PG29]
B249356 01/03/2030.1 1.0019L1171-76 [COMP-PG30]
Page 85 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B249284 - SW-846 5035
[TOC_3]B249284[TOC]
Blank (B249284-BLK1) Prepared & Analyzed: 01/02/20
Acetone mg/Kg wet0.10ND
Acrylonitrile mg/Kg wet0.0060ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010ND
Benzene mg/Kg wet0.0020ND
Bromobenzene mg/Kg wet0.0020ND
Bromochloromethane mg/Kg wet0.0020ND
Bromodichloromethane mg/Kg wet0.0020ND
Bromoform mg/Kg wet0.0020ND
Bromomethane mg/Kg wet0.010 V-34ND
2-Butanone (MEK)mg/Kg wet0.040ND
tert-Butyl Alcohol (TBA)mg/Kg wet0.040ND
n-Butylbenzene mg/Kg wet0.0020ND
sec-Butylbenzene mg/Kg wet0.0020ND
tert-Butylbenzene mg/Kg wet0.0020ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010ND
Carbon Disulfide mg/Kg wet0.0060ND
Carbon Tetrachloride mg/Kg wet0.0020ND
Chlorobenzene mg/Kg wet0.0020ND
Chlorodibromomethane mg/Kg wet0.0010ND
Chloroethane mg/Kg wet0.020ND
Chloroform mg/Kg wet0.0040ND
Chloromethane mg/Kg wet0.010 V-05ND
2-Chlorotoluene mg/Kg wet0.0020ND
4-Chlorotoluene mg/Kg wet0.0020ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020ND
1,2-Dibromoethane (EDB)mg/Kg wet0.0010ND
Dibromomethane mg/Kg wet0.0020ND
1,2-Dichlorobenzene mg/Kg wet0.0020ND
1,3-Dichlorobenzene mg/Kg wet0.0020ND
1,4-Dichlorobenzene mg/Kg wet0.0020ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020ND
1,1-Dichloroethane mg/Kg wet0.0020ND
1,2-Dichloroethane mg/Kg wet0.0020ND
1,1-Dichloroethylene mg/Kg wet0.0040ND
cis-1,2-Dichloroethylene mg/Kg wet0.0020ND
trans-1,2-Dichloroethylene mg/Kg wet0.0020ND
1,2-Dichloropropane mg/Kg wet0.0020ND
1,3-Dichloropropane mg/Kg wet0.0010ND
2,2-Dichloropropane mg/Kg wet0.0020ND
1,1-Dichloropropene mg/Kg wet0.0020ND
cis-1,3-Dichloropropene mg/Kg wet0.0010ND
trans-1,3-Dichloropropene mg/Kg wet0.0010ND
Diethyl Ether mg/Kg wet0.020ND
Diisopropyl Ether (DIPE)mg/Kg wet0.0010ND
1,4-Dioxane mg/Kg wet0.10ND
Ethylbenzene mg/Kg wet0.0020ND
Hexachlorobutadiene mg/Kg wet0.0020ND
2-Hexanone (MBK)mg/Kg wet0.020ND
Isopropylbenzene (Cumene)mg/Kg wet0.0020ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040ND
[TOC_1]QC Data[TOC]
Page 86 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249284 - SW-846 5035
Blank (B249284-BLK1) Prepared & Analyzed: 01/02/20
Methylene Chloride mg/Kg wet0.020ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020ND
Naphthalene mg/Kg wet0.0040ND
n-Propylbenzene mg/Kg wet0.0020ND
Styrene mg/Kg wet0.0020ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010ND
Tetrachloroethylene mg/Kg wet0.0020ND
Tetrahydrofuran mg/Kg wet0.010ND
Toluene mg/Kg wet0.0020ND
1,2,3-Trichlorobenzene mg/Kg wet0.0020ND
1,2,4-Trichlorobenzene mg/Kg wet0.0020ND
1,3,5-Trichlorobenzene mg/Kg wet0.0020ND
1,1,1-Trichloroethane mg/Kg wet0.0020ND
1,1,2-Trichloroethane mg/Kg wet0.0020ND
Trichloroethylene mg/Kg wet0.0020ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010ND
1,2,3-Trichloropropane mg/Kg wet0.0020ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010ND
1,2,4-Trimethylbenzene mg/Kg wet0.0020ND
1,3,5-Trimethylbenzene mg/Kg wet0.0020ND
Vinyl Chloride mg/Kg wet0.010ND
m+p Xylene mg/Kg wet0.0040ND
o-Xylene mg/Kg wet0.0020ND
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 87.90.0440
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 97.80.0489
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1010.0504
LCS (B249284-BS1) Prepared & Analyzed: 01/02/20
Acetone mg/Kg wet0.10 0.200 70-16086.20.172
Acrylonitrile mg/Kg wet0.0060 0.0200 70-13092.30.0185
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 70-13091.80.0184
Benzene mg/Kg wet0.0020 0.0200 70-13087.70.0175
Bromobenzene mg/Kg wet0.0020 0.0200 70-13099.10.0198
Bromochloromethane mg/Kg wet0.0020 0.0200 70-1301070.0213
Bromodichloromethane mg/Kg wet0.0020 0.0200 70-13089.30.0179
Bromoform mg/Kg wet0.0020 0.0200 70-1301160.0233
Bromomethane mg/Kg wet0.010 0.0200 V-3440-13079.00.0158
2-Butanone (MEK)mg/Kg wet0.040 0.200 70-16088.10.176
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 40-13089.90.180
n-Butylbenzene mg/Kg wet0.0020 0.0200 70-13085.70.0171
sec-Butylbenzene mg/Kg wet0.0020 0.0200 70-13098.10.0196
tert-Butylbenzene mg/Kg wet0.0020 0.0200 70-16096.00.0192
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 70-13091.40.0183
Carbon Disulfide mg/Kg wet0.0060 0.200 70-13086.50.173
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 70-13094.30.0189
Chlorobenzene mg/Kg wet0.0020 0.0200 70-1301060.0213
Chlorodibromomethane mg/Kg wet0.0010 0.0200 70-1301000.0201
Chloroethane mg/Kg wet0.020 0.0200 J70-13082.50.0165
Chloroform mg/Kg wet0.0040 0.0200 70-13087.80.0176
Chloromethane mg/Kg wet0.010 0.0200 V-0570-13077.40.0155
2-Chlorotoluene mg/Kg wet0.0020 0.0200 70-13098.10.0196
Page 87 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249284 - SW-846 5035
LCS (B249284-BS1) Prepared & Analyzed: 01/02/20
4-Chlorotoluene mg/Kg wet0.0020 0.0200 70-13093.50.0187
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 70-13098.60.0197
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 70-1301030.0206
Dibromomethane mg/Kg wet0.0020 0.0200 70-1301010.0203
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301000.0201
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13098.10.0196
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13098.80.0198
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 70-13094.50.0189
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 J40-16077.90.0156
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 70-13091.90.0184
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 70-13096.40.0193
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 70-13083.60.0167
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-13083.80.0168
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-13089.00.0178
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13097.70.0195
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 70-13099.50.0199
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13082.60.0165
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 70-13082.70.0165
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13096.50.0193
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13097.80.0196
Diethyl Ether mg/Kg wet0.020 0.0200 J70-13084.90.0170
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 70-13086.80.0174
1,4-Dioxane mg/Kg wet0.10 0.200 40-16086.20.172
Ethylbenzene mg/Kg wet0.0020 0.0200 70-13091.80.0184
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 70-1601020.0205
2-Hexanone (MBK)mg/Kg wet0.020 0.200 70-16088.50.177
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 70-1301030.0206
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 70-13095.40.0191
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 70-13090.50.0181
Methylene Chloride mg/Kg wet0.020 0.0200 J40-16089.30.0179
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 70-16088.40.177
Naphthalene mg/Kg wet0.0040 0.0200 40-13086.60.0173
n-Propylbenzene mg/Kg wet0.0020 0.0200 70-13093.40.0187
Styrene mg/Kg wet0.0020 0.0200 70-1301020.0204
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 70-1301080.0216
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 70-1301020.0204
Tetrachloroethylene mg/Kg wet0.0020 0.0200 70-1301010.0202
Tetrahydrofuran mg/Kg wet0.010 0.0200 70-13099.40.0199
Toluene mg/Kg wet0.0020 0.0200 70-13090.50.0181
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13097.50.0195
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13095.80.0192
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13097.20.0194
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 70-13082.80.0166
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 70-13094.20.0188
Trichloroethylene mg/Kg wet0.0020 0.0200 70-13091.80.0184
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 70-13089.10.0178
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 70-1301080.0216
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 70-13091.80.0184
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-13091.10.0182
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-13095.20.0190
Vinyl Chloride mg/Kg wet0.010 0.0200 40-13081.60.0163
Page 88 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249284 - SW-846 5035
LCS (B249284-BS1) Prepared & Analyzed: 01/02/20
m+p Xylene mg/Kg wet0.0040 0.0400 70-13093.40.0374
o-Xylene mg/Kg wet0.0020 0.0200 70-13092.80.0186
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 88.00.0440
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 98.10.0491
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1020.0508
LCS Dup (B249284-BSD1) Prepared & Analyzed: 01/02/20
Acetone mg/Kg wet0.10 0.200 2570-16083.4 3.300.167
Acrylonitrile mg/Kg wet0.0060 0.0200 2570-13093.2 0.9700.0186
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 2570-13092.0 0.2180.0184
Benzene mg/Kg wet0.0020 0.0200 2570-13088.0 0.3410.0176
Bromobenzene mg/Kg wet0.0020 0.0200 2570-13098.9 0.2020.0198
Bromochloromethane mg/Kg wet0.0020 0.0200 2570-130108 1.770.0217
Bromodichloromethane mg/Kg wet0.0020 0.0200 2570-13088.5 0.9000.0177
Bromoform mg/Kg wet0.0020 0.0200 2570-130111 4.300.0223
Bromomethane mg/Kg wet0.010 0.0200 25 V-3440-13082.9 4.820.0166
2-Butanone (MEK)mg/Kg wet0.040 0.200 2570-16090.0 2.120.180
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 2540-13097.6 8.300.195
n-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13082.8 3.440.0166
sec-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13099.4 1.320.0199
tert-Butylbenzene mg/Kg wet0.0020 0.0200 2570-16095.4 0.6270.0191
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 2570-13090.1 1.430.0180
Carbon Disulfide mg/Kg wet0.0060 0.200 2570-13084.3 2.520.169
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 2570-13092.3 2.140.0185
Chlorobenzene mg/Kg wet0.0020 0.0200 2570-130106 0.1880.0213
Chlorodibromomethane mg/Kg wet0.0010 0.0200 2570-130102 1.090.0203
Chloroethane mg/Kg wet0.020 0.0200 25 J70-13086.5 4.730.0173
Chloroform mg/Kg wet0.0040 0.0200 2570-13087.2 0.6860.0174
Chloromethane mg/Kg wet0.010 0.0200 25 V-0570-13075.1 3.020.0150
2-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13099.3 1.220.0199
4-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13092.3 1.290.0185
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 2570-130103 4.460.0206
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 2570-130102 1.660.0203
Dibromomethane mg/Kg wet0.0020 0.0200 2570-130103 1.470.0206
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130100 0.1990.0200
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130101 2.620.0201
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13096.9 1.940.0194
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 2570-13090.3 4.550.0181
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 25 J40-16075.7 2.860.0151
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 2570-13090.5 1.540.0181
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 2570-13095.8 0.6240.0192
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 2570-13081.1 3.040.0162
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13084.2 0.4760.0168
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13085.6 3.890.0171
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13095.1 2.700.0190
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 2570-13098.5 1.010.0197
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13081.1 1.830.0162
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 2570-13085.9 3.800.0172
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13095.9 0.6240.0192
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13095.2 2.690.0190
Diethyl Ether mg/Kg wet0.020 0.0200 25 J70-13088.6 4.270.0177
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 2570-13086.0 0.9260.0172
Page 89 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249284 - SW-846 5035
LCS Dup (B249284-BSD1) Prepared & Analyzed: 01/02/20
1,4-Dioxane mg/Kg wet0.10 0.200 5040-16089.8 4.130.180
Ethylbenzene mg/Kg wet0.0020 0.0200 2570-13088.6 3.550.0177
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 2570-160104 1.460.0208
2-Hexanone (MBK)mg/Kg wet0.020 0.200 2570-16085.7 3.220.171
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 2570-130105 1.920.0210
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 2570-13093.8 1.690.0188
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 2570-13090.6 0.1100.0181
Methylene Chloride mg/Kg wet0.020 0.0200 25 J40-16088.3 1.130.0177
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 2570-16087.2 1.480.174
Naphthalene mg/Kg wet0.0040 0.0200 2540-13087.4 0.9200.0175
n-Propylbenzene mg/Kg wet0.0020 0.0200 2570-13092.1 1.400.0184
Styrene mg/Kg wet0.0020 0.0200 2570-130100 1.680.0201
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 2570-130107 0.7440.0214
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 2570-130103 0.6840.0205
Tetrachloroethylene mg/Kg wet0.0020 0.0200 2570-130100 0.4970.0201
Tetrahydrofuran mg/Kg wet0.010 0.0200 2570-13096.9 2.550.0194
Toluene mg/Kg wet0.0020 0.0200 2570-13091.1 0.6610.0182
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-130101 3.130.0201
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13099.2 3.490.0198
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13097.7 0.5130.0195
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 2570-13084.9 2.500.0170
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 2570-13092.8 1.500.0186
Trichloroethylene mg/Kg wet0.0020 0.0200 2570-13091.2 0.6560.0182
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 2570-13084.3 5.540.0169
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 2570-130110 1.470.0219
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 2570-13089.3 2.760.0179
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13088.0 3.460.0176
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13093.5 1.800.0187
Vinyl Chloride mg/Kg wet0.010 0.0200 2540-13080.1 1.860.0160
m+p Xylene mg/Kg wet0.0040 0.0400 2570-13093.5 0.1070.0374
o-Xylene mg/Kg wet0.0020 0.0200 2570-13094.2 1.500.0188
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 87.50.0438
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 96.70.0484
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1020.0510
Batch B249440 - SW-846 5035
[TOC_3]B249440[TOC]
Blank (B249440-BLK1) Prepared & Analyzed: 01/06/20
Acetone mg/Kg wet2.5ND
Acrylonitrile mg/Kg wet0.25ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.025ND
Benzene mg/Kg wet0.050ND
Bromobenzene mg/Kg wet0.050ND
Bromochloromethane mg/Kg wet0.050ND
Bromodichloromethane mg/Kg wet0.025ND
Bromoform mg/Kg wet0.050ND
Bromomethane mg/Kg wet0.10ND
2-Butanone (MEK)mg/Kg wet1.0ND
tert-Butyl Alcohol (TBA)mg/Kg wet1.0ND
n-Butylbenzene mg/Kg wet0.050ND
sec-Butylbenzene mg/Kg wet0.050ND
tert-Butylbenzene mg/Kg wet0.050ND
Page 90 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249440 - SW-846 5035
Blank (B249440-BLK1) Prepared & Analyzed: 01/06/20
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.025ND
Carbon Disulfide mg/Kg wet0.25ND
Carbon Tetrachloride mg/Kg wet0.050ND
Chlorobenzene mg/Kg wet0.050ND
Chlorodibromomethane mg/Kg wet0.025ND
Chloroethane mg/Kg wet0.10ND
Chloroform mg/Kg wet0.10ND
Chloromethane mg/Kg wet0.10ND
2-Chlorotoluene mg/Kg wet0.050ND
4-Chlorotoluene mg/Kg wet0.050ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.25ND
1,2-Dibromoethane (EDB)mg/Kg wet0.025ND
Dibromomethane mg/Kg wet0.050ND
1,2-Dichlorobenzene mg/Kg wet0.050ND
1,3-Dichlorobenzene mg/Kg wet0.050ND
1,4-Dichlorobenzene mg/Kg wet0.050ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.10ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.10ND
1,1-Dichloroethane mg/Kg wet0.050ND
1,2-Dichloroethane mg/Kg wet0.050ND
1,1-Dichloroethylene mg/Kg wet0.050ND
cis-1,2-Dichloroethylene mg/Kg wet0.050ND
trans-1,2-Dichloroethylene mg/Kg wet0.050ND
1,2-Dichloropropane mg/Kg wet0.050ND
1,3-Dichloropropane mg/Kg wet0.025ND
2,2-Dichloropropane mg/Kg wet0.050ND
1,1-Dichloropropene mg/Kg wet0.10ND
cis-1,3-Dichloropropene mg/Kg wet0.025ND
trans-1,3-Dichloropropene mg/Kg wet0.025ND
Diethyl Ether mg/Kg wet0.10ND
Diisopropyl Ether (DIPE)mg/Kg wet0.025ND
1,4-Dioxane mg/Kg wet2.5ND
Ethylbenzene mg/Kg wet0.050ND
Hexachlorobutadiene mg/Kg wet0.030ND
2-Hexanone (MBK)mg/Kg wet0.50ND
Isopropylbenzene (Cumene)mg/Kg wet0.050ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
Methylene Chloride mg/Kg wet0.25ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.50ND
Naphthalene mg/Kg wet0.10 V-05ND
n-Propylbenzene mg/Kg wet0.050ND
Styrene mg/Kg wet0.050ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.050ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.025ND
Tetrachloroethylene mg/Kg wet0.050ND
Tetrahydrofuran mg/Kg wet0.50ND
Toluene mg/Kg wet0.050ND
1,2,3-Trichlorobenzene mg/Kg wet0.25 L-04, V-05ND
1,2,4-Trichlorobenzene mg/Kg wet0.050 V-05ND
1,3,5-Trichlorobenzene mg/Kg wet0.050ND
1,1,1-Trichloroethane mg/Kg wet0.050ND
Page 91 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249440 - SW-846 5035
Blank (B249440-BLK1) Prepared & Analyzed: 01/06/20
1,1,2-Trichloroethane mg/Kg wet0.050ND
Trichloroethylene mg/Kg wet0.050ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.10ND
1,2,3-Trichloropropane mg/Kg wet0.10ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
1,3,5-Trimethylbenzene mg/Kg wet0.050ND
Vinyl Chloride mg/Kg wet0.10ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
mg/Kg wet 0.0250 70-130Surrogate: 1,2-Dichloroethane-d4 1080.0269
mg/Kg wet 0.0250 70-130Surrogate: Toluene-d8 95.60.0239
mg/Kg wet 0.0250 70-130Surrogate: 4-Bromofluorobenzene 90.60.0226
LCS (B249440-BS1) Prepared & Analyzed: 01/06/20
Acetone mg/Kg wet0.057 0.113 70-16098.50.112
Acrylonitrile mg/Kg wet0.0057 0.0113 70-13093.70.0106
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.00057 0.0113 70-13084.20.00954
Benzene mg/Kg wet0.0011 0.0113 70-1301050.0119
Bromobenzene mg/Kg wet0.0011 0.0113 70-13098.00.0111
Bromochloromethane mg/Kg wet0.0011 0.0113 70-1301150.0130
Bromodichloromethane mg/Kg wet0.00057 0.0113 70-1301080.0122
Bromoform mg/Kg wet0.0011 0.0113 70-13096.10.0109
Bromomethane mg/Kg wet0.0023 0.0113 L-02, V-2040-130134*0.0152
2-Butanone (MEK)mg/Kg wet0.023 0.113 70-1601010.114
tert-Butyl Alcohol (TBA)mg/Kg wet0.023 0.113 40-1301040.118
n-Butylbenzene mg/Kg wet0.0011 0.0113 70-13096.40.0109
sec-Butylbenzene mg/Kg wet0.0011 0.0113 70-1301100.0125
tert-Butylbenzene mg/Kg wet0.0011 0.0113 70-1601080.0123
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.00057 0.0113 70-13091.90.0104
Carbon Disulfide mg/Kg wet0.0057 0.113 70-1301010.115
Carbon Tetrachloride mg/Kg wet0.0011 0.0113 70-1301100.0124
Chlorobenzene mg/Kg wet0.0011 0.0113 70-1301030.0116
Chlorodibromomethane mg/Kg wet0.00057 0.0113 70-1301040.0118
Chloroethane mg/Kg wet0.0023 0.0113 70-1301010.0115
Chloroform mg/Kg wet0.0023 0.0113 70-1301120.0127
Chloromethane mg/Kg wet0.0023 0.0113 L-02, V-2070-130134*0.0152
2-Chlorotoluene mg/Kg wet0.0011 0.0113 70-13097.10.0110
4-Chlorotoluene mg/Kg wet0.0011 0.0113 70-13096.60.0109
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0057 0.0113 70-13093.90.0106
1,2-Dibromoethane (EDB)mg/Kg wet0.00057 0.0113 70-1301090.0124
Dibromomethane mg/Kg wet0.0011 0.0113 70-1301030.0117
1,2-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-1301030.0117
1,3-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-1301080.0123
1,4-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-1301030.0116
trans-1,4-Dichloro-2-butene mg/Kg wet0.0023 0.0113 70-13089.50.0101
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.0023 0.0113 40-16096.40.0109
1,1-Dichloroethane mg/Kg wet0.0011 0.0113 70-1301100.0124
1,2-Dichloroethane mg/Kg wet0.0011 0.0113 70-1301080.0123
1,1-Dichloroethylene mg/Kg wet0.0011 0.0113 70-1301140.0129
cis-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 70-1301120.0127
trans-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 70-1301060.0120
Page 92 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249440 - SW-846 5035
LCS (B249440-BS1) Prepared & Analyzed: 01/06/20
1,2-Dichloropropane mg/Kg wet0.0011 0.0113 70-1301100.0124
1,3-Dichloropropane mg/Kg wet0.00057 0.0113 70-1301080.0122
2,2-Dichloropropane mg/Kg wet0.0011 0.0113 70-1301070.0121
1,1-Dichloropropene mg/Kg wet0.0023 0.0113 70-1301080.0123
cis-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 70-1301090.0124
trans-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 70-13099.90.0113
Diethyl Ether mg/Kg wet0.0023 0.0113 70-1301030.0117
Diisopropyl Ether (DIPE)mg/Kg wet0.00057 0.0113 70-1301100.0124
1,4-Dioxane mg/Kg wet0.057 0.113 40-16093.80.106
Ethylbenzene mg/Kg wet0.0011 0.0113 70-1301010.0114
Hexachlorobutadiene mg/Kg wet0.00068 0.0113 70-16088.10.00998
2-Hexanone (MBK)mg/Kg wet0.011 0.113 70-16092.90.105
Isopropylbenzene (Cumene)mg/Kg wet0.0011 0.0113 70-13099.60.0113
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0011 0.0113 70-13099.90.0113
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0011 0.0113 70-1301010.0114
Methylene Chloride mg/Kg wet0.0057 0.0113 40-1601100.0125
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.011 0.113 70-16097.10.110
Naphthalene mg/Kg wet0.0023 0.0113 V-0540-13062.30.00706
n-Propylbenzene mg/Kg wet0.0011 0.0113 70-13098.40.0112
Styrene mg/Kg wet0.0011 0.0113 70-13096.40.0109
1,1,1,2-Tetrachloroethane mg/Kg wet0.0011 0.0113 70-1301060.0120
1,1,2,2-Tetrachloroethane mg/Kg wet0.00057 0.0113 70-1301100.0124
Tetrachloroethylene mg/Kg wet0.0011 0.0113 70-1301020.0116
Tetrahydrofuran mg/Kg wet0.011 0.0113 70-1301050.0119
Toluene mg/Kg wet0.0011 0.0113 70-1301020.0115
1,2,3-Trichlorobenzene mg/Kg wet0.0057 0.0113 V-05, L-0470-13058.9 *0.00668
1,2,4-Trichlorobenzene mg/Kg wet0.0011 0.0113 V-05, L-0770-13064.1 *0.00726
1,3,5-Trichlorobenzene mg/Kg wet0.0011 0.0113 70-13081.80.00927
1,1,1-Trichloroethane mg/Kg wet0.0011 0.0113 70-1301110.0126
1,1,2-Trichloroethane mg/Kg wet0.0011 0.0113 70-1301080.0122
Trichloroethylene mg/Kg wet0.0011 0.0113 70-1301080.0122
Trichlorofluoromethane (Freon 11)mg/Kg wet0.0023 0.0113 70-1301070.0121
1,2,3-Trichloropropane mg/Kg wet0.0023 0.0113 70-13098.80.0112
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.0011 0.0113 70-1301110.0126
1,2,4-Trimethylbenzene mg/Kg wet0.0011 0.0113 70-1301030.0117
1,3,5-Trimethylbenzene mg/Kg wet0.0011 0.0113 70-13092.30.0105
Vinyl Chloride mg/Kg wet0.0023 0.0113 40-1301090.0124
m+p Xylene mg/Kg wet0.0023 0.0227 70-13099.30.0225
o-Xylene mg/Kg wet0.0011 0.0113 70-13099.30.0113
mg/Kg wet 0.0283 70-130Surrogate: 1,2-Dichloroethane-d4 1060.0301
mg/Kg wet 0.0283 70-130Surrogate: Toluene-d8 1000.0283
mg/Kg wet 0.0283 70-130Surrogate: 4-Bromofluorobenzene 96.20.0273
Page 93 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249440 - SW-846 5035
LCS Dup (B249440-BSD1) Prepared & Analyzed: 01/06/20
Acetone mg/Kg wet0.057 0.113 2570-160107 8.140.121
Acrylonitrile mg/Kg wet0.0057 0.0113 2570-13094.6 0.9560.0107
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.00057 0.0113 2570-13091.3 8.090.0103
Benzene mg/Kg wet0.0011 0.0113 2570-130110 5.020.0125
Bromobenzene mg/Kg wet0.0011 0.0113 2570-130103 4.590.0116
Bromochloromethane mg/Kg wet0.0011 0.0113 2570-130124 8.130.0141
Bromodichloromethane mg/Kg wet0.00057 0.0113 2570-130110 2.200.0125
Bromoform mg/Kg wet0.0011 0.0113 2570-130104 8.280.0118
Bromomethane mg/Kg wet0.0023 0.0113 25 L-02, V-2040-130140 4.74*0.0159
2-Butanone (MEK)mg/Kg wet0.023 0.113 2570-160107 6.170.121
tert-Butyl Alcohol (TBA)mg/Kg wet0.023 0.113 2540-130112 7.340.127
n-Butylbenzene mg/Kg wet0.0011 0.0113 2570-130102 5.650.0116
sec-Butylbenzene mg/Kg wet0.0011 0.0113 2570-130115 3.740.0130
tert-Butylbenzene mg/Kg wet0.0011 0.0113 2570-160113 4.250.0128
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.00057 0.0113 2570-13096.4 4.780.0109
Carbon Disulfide mg/Kg wet0.0057 0.113 2570-130107 5.920.122
Carbon Tetrachloride mg/Kg wet0.0011 0.0113 2570-130116 5.930.0132
Chlorobenzene mg/Kg wet0.0011 0.0113 2570-130108 5.130.0122
Chlorodibromomethane mg/Kg wet0.00057 0.0113 2570-130107 3.130.0121
Chloroethane mg/Kg wet0.0023 0.0113 2570-130113 11.00.0128
Chloroform mg/Kg wet0.0023 0.0113 2570-130114 2.120.0129
Chloromethane mg/Kg wet0.0023 0.0113 25 L-02, V-2070-130142 6.08*0.0161
2-Chlorotoluene mg/Kg wet0.0011 0.0113 2570-130103 6.280.0117
4-Chlorotoluene mg/Kg wet0.0011 0.0113 2570-130102 4.950.0115
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0057 0.0113 2570-13098.8 5.090.0112
1,2-Dibromoethane (EDB)mg/Kg wet0.00057 0.0113 2570-130107 2.130.0121
Dibromomethane mg/Kg wet0.0011 0.0113 2570-130104 0.8710.0118
1,2-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-130110 6.370.0125
1,3-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-130110 2.010.0125
1,4-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-130107 4.570.0122
trans-1,4-Dichloro-2-butene mg/Kg wet0.0023 0.0113 2570-13090.7 1.330.0103
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.0023 0.0113 2540-160100 4.160.0114
1,1-Dichloroethane mg/Kg wet0.0011 0.0113 2570-130114 3.500.0129
1,2-Dichloroethane mg/Kg wet0.0011 0.0113 2570-130108 0.1850.0123
1,1-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-130115 0.9620.0130
cis-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-130117 3.670.0132
trans-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-130109 2.330.0123
1,2-Dichloropropane mg/Kg wet0.0011 0.0113 2570-130116 5.580.0132
1,3-Dichloropropane mg/Kg wet0.00057 0.0113 2570-130109 0.7390.0123
2,2-Dichloropropane mg/Kg wet0.0011 0.0113 2570-130109 1.760.0124
1,1-Dichloropropene mg/Kg wet0.0023 0.0113 2570-130114 5.040.0129
cis-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 2570-130111 1.820.0126
trans-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 2570-130101 0.8970.0114
Diethyl Ether mg/Kg wet0.0023 0.0113 2570-130103 0.6790.0116
Diisopropyl Ether (DIPE)mg/Kg wet0.00057 0.0113 2570-130115 5.160.0131
1,4-Dioxane mg/Kg wet0.057 0.113 5040-160103 8.950.116
Ethylbenzene mg/Kg wet0.0011 0.0113 2570-130104 2.940.0118
Hexachlorobutadiene mg/Kg wet0.00068 0.0113 2570-16095.7 8.270.0108
2-Hexanone (MBK)mg/Kg wet0.011 0.113 2570-160102 9.830.116
Isopropylbenzene (Cumene)mg/Kg wet0.0011 0.0113 2570-130106 6.510.0120
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0011 0.0113 2570-130106 6.210.0120
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0011 0.0113 2570-130100 0.3970.0114
Page 94 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249440 - SW-846 5035
LCS Dup (B249440-BSD1) Prepared & Analyzed: 01/06/20
Methylene Chloride mg/Kg wet0.0057 0.0113 2540-160119 7.780.0135
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.011 0.113 2570-160101 3.920.114
Naphthalene mg/Kg wet0.0023 0.0113 25 V-0540-13065.3 4.700.00740
n-Propylbenzene mg/Kg wet0.0011 0.0113 2570-130102 3.690.0116
Styrene mg/Kg wet0.0011 0.0113 2570-130103 6.910.0117
1,1,1,2-Tetrachloroethane mg/Kg wet0.0011 0.0113 2570-130113 6.510.0128
1,1,2,2-Tetrachloroethane mg/Kg wet0.00057 0.0113 2570-130118 7.470.0134
Tetrachloroethylene mg/Kg wet0.0011 0.0113 2570-130106 3.740.0120
Tetrahydrofuran mg/Kg wet0.011 0.0113 2570-130111 5.720.0126
Toluene mg/Kg wet0.0011 0.0113 2570-130105 3.680.0119
1,2,3-Trichlorobenzene mg/Kg wet0.0057 0.0113 25 L-04, V-0570-13064.5 9.08*0.00731
1,2,4-Trichlorobenzene mg/Kg wet0.0011 0.0113 25 V-0570-13072.1 11.70.00817
1,3,5-Trichlorobenzene mg/Kg wet0.0011 0.0113 2570-13089.0 8.430.0101
1,1,1-Trichloroethane mg/Kg wet0.0011 0.0113 2570-130118 5.780.0133
1,1,2-Trichloroethane mg/Kg wet0.0011 0.0113 2570-130112 3.820.0127
Trichloroethylene mg/Kg wet0.0011 0.0113 2570-130114 5.490.0129
Trichlorofluoromethane (Freon 11)mg/Kg wet0.0023 0.0113 2570-130114 6.170.0129
1,2,3-Trichloropropane mg/Kg wet0.0023 0.0113 2570-130105 6.270.0119
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.0011 0.0113 2570-130115 2.920.0130
1,2,4-Trimethylbenzene mg/Kg wet0.0011 0.0113 2570-130112 8.440.0127
1,3,5-Trimethylbenzene mg/Kg wet0.0011 0.0113 2570-13096.3 4.240.0109
Vinyl Chloride mg/Kg wet0.0023 0.0113 2540-130114 4.290.0129
m+p Xylene mg/Kg wet0.0023 0.0227 2570-130105 5.200.0237
o-Xylene mg/Kg wet0.0011 0.0113 2570-130109 9.680.0124
mg/Kg wet 0.0283 70-130Surrogate: 1,2-Dichloroethane-d4 1050.0298
mg/Kg wet 0.0283 70-130Surrogate: Toluene-d8 99.60.0282
mg/Kg wet 0.0283 70-130Surrogate: 4-Bromofluorobenzene 96.40.0273
Page 95 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B249356 - SW-846 3546
[TOC_3]B249356[TOC]
Blank (B249356-BLK1) Prepared: 01/03/20 Analyzed: 01/04/20
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-04, V-05, V-35ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66 V-34ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34 V-20ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34 V-05ND
Hexachlorocyclopentadiene mg/Kg wet0.34 L-04, V-05ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 96 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249356 - SW-846 3546
Blank (B249356-BLK1) Prepared: 01/03/20 Analyzed: 01/04/20
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34 V-05ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34 V-20ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 75.35.02
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 81.35.42
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 72.02.40
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 81.42.71
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 69.44.62
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 69.12.30
LCS (B249356-BS1) Prepared: 01/03/20 Analyzed: 01/04/20
Acenaphthene mg/Kg wet0.17 1.67 40-14065.11.09
Acenaphthylene mg/Kg wet0.17 1.67 40-14068.71.14
Acetophenone mg/Kg wet0.34 1.67 40-14070.31.17
Aniline mg/Kg wet0.34 1.67 10-14048.90.815
Anthracene mg/Kg wet0.17 1.67 40-14071.61.19
Benzidine mg/Kg wet0.66 1.67 V-35, V-04, V-0540-14071.81.20
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14066.61.11
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14064.81.08
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14063.71.06
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14069.01.15
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14066.21.10
Benzoic Acid mg/Kg wet1.0 1.67 J30-13033.30.555
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14067.11.12
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14070.21.17
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14077.31.29
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-14057.60.960
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14060.81.01
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14062.61.04
Carbazole mg/Kg wet0.17 1.67 40-14071.01.18
4-Chloroaniline mg/Kg wet0.66 1.67 V-3410-14046.60.776
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13070.61.18
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14061.11.02
Page 97 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249356 - SW-846 3546
LCS (B249356-BS1) Prepared: 01/03/20 Analyzed: 01/04/20
2-Chlorophenol mg/Kg wet0.34 1.67 30-13070.81.18
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14060.11.00
Chrysene mg/Kg wet0.17 1.67 40-14067.31.12
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14066.11.10
Dibenzofuran mg/Kg wet0.34 1.67 40-14068.41.14
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14062.11.03
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14060.11.00
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14057.60.960
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14058.90.982
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 20-14046.60.777
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-13060.21.00
Diethylphthalate mg/Kg wet0.34 1.67 40-14062.11.04
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13067.51.13
Dimethylphthalate mg/Kg wet0.34 1.67 40-14064.21.07
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30-13062.71.04
2,4-Dinitrophenol mg/Kg wet0.66 1.67 J30-13037.00.617
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 V-0640-14077.21.29
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 40-14075.21.25
Di-n-octylphthalate mg/Kg wet0.34 1.67 40-14051.60.861
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 40-14079.11.32
Fluoranthene mg/Kg wet0.17 1.67 40-14069.21.15
Fluorene mg/Kg wet0.17 1.67 40-14069.71.16
Hexachlorobenzene mg/Kg wet0.34 1.67 40-14064.01.07
Hexachlorobutadiene mg/Kg wet0.34 1.67 V-0540-14048.00.801
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 L-04, V-0540-14028.3 *0.471
Hexachloroethane mg/Kg wet0.34 1.67 40-14061.01.02
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14073.41.22
Isophorone mg/Kg wet0.34 1.67 40-14072.11.20
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14057.70.961
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14068.81.15
2-Methylphenol mg/Kg wet0.34 1.67 30-13075.11.25
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13073.21.22
Naphthalene mg/Kg wet0.17 1.67 40-14065.01.08
2-Nitroaniline mg/Kg wet0.34 1.67 V-0640-14091.41.52
3-Nitroaniline mg/Kg wet0.34 1.67 V-0630-14076.01.27
4-Nitroaniline mg/Kg wet0.34 1.67 40-14081.81.36
Nitrobenzene mg/Kg wet0.34 1.67 40-14075.51.26
2-Nitrophenol mg/Kg wet0.34 1.67 30-13073.11.22
4-Nitrophenol mg/Kg wet0.66 1.67 30-13079.91.33
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14067.41.12
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 40-14073.01.22
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14073.91.23
Pentachloronitrobenzene mg/Kg wet0.34 1.67 40-14066.41.11
Pentachlorophenol mg/Kg wet0.34 1.67 V-0530-13040.50.675
Phenanthrene mg/Kg wet0.17 1.67 40-14072.01.20
Phenol mg/Kg wet0.34 1.67 V-0630-13083.21.39
Pyrene mg/Kg wet0.17 1.67 40-14068.41.14
Pyridine mg/Kg wet0.34 1.67 30-14041.40.690
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14056.80.947
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14053.70.895
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13064.41.07
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13061.61.03
Page 98 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249356 - SW-846 3546
LCS (B249356-BS1) Prepared: 01/03/20 Analyzed: 01/04/20
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 80.45.36
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 88.05.87
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 76.42.55
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 82.72.76
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 83.05.53
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 73.22.44
LCS Dup (B249356-BSD1) Prepared: 01/03/20 Analyzed: 01/04/20
Acenaphthene mg/Kg wet0.17 1.67 3040-14066.6 2.221.11
Acenaphthylene mg/Kg wet0.17 1.67 3040-14071.5 3.991.19
Acetophenone mg/Kg wet0.34 1.67 3040-14067.3 4.391.12
Aniline mg/Kg wet0.34 1.67 5010-14046.8 4.430.780
Anthracene mg/Kg wet0.17 1.67 3040-14075.3 4.981.26
Benzidine mg/Kg wet0.66 1.67 30 V-04, V-05, V-3540-14074.6 3.821.24
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14069.3 3.891.15
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14068.5 5.491.14
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14067.5 5.891.13
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14073.4 6.181.22
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14068.1 2.801.13
Benzoic Acid mg/Kg wet1.0 1.67 50 J30-13034.4 3.190.573
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14066.0 1.771.10
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14062.7 11.41.04
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14068.3 12.41.14
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14060.5 4.811.01
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14063.9 4.941.06
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14063.5 1.431.06
Carbazole mg/Kg wet0.17 1.67 3040-14077.6 8.911.29
4-Chloroaniline mg/Kg wet0.66 1.67 30 V-3410-14046.7 0.2140.778
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13069.4 1.771.16
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14063.1 3.351.05
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13067.6 4.511.13
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14062.2 3.441.04
Chrysene mg/Kg wet0.17 1.67 3040-14067.9 0.8581.13
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14070.9 6.921.18
Dibenzofuran mg/Kg wet0.34 1.67 3040-14070.8 3.451.18
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14065.1 4.721.08
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14059.1 1.610.985
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14056.9 1.290.948
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14057.3 2.680.956
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 5020-14050.0 7.040.833
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13061.5 2.141.02
Diethylphthalate mg/Kg wet0.34 1.67 3040-14062.0 0.1611.03
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13067.6 0.05911.13
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14065.1 1.421.09
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 3030-13065.0 3.661.08
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30 J30-13034.8 6.240.579
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 30 V-0640-14077.1 0.05181.29
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14076.6 1.741.28
Di-n-octylphthalate mg/Kg wet0.34 1.67 3040-14056.9 9.760.949
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 3040-14076.1 3.921.27
Fluoranthene mg/Kg wet0.17 1.67 3040-14078.2 12.21.30
Fluorene mg/Kg wet0.17 1.67 3040-14070.6 1.311.18
Page 99 of 145
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249356 - SW-846 3546
LCS Dup (B249356-BSD1) Prepared: 01/03/20 Analyzed: 01/04/20
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14067.5 5.231.12
Hexachlorobutadiene mg/Kg wet0.34 1.67 30 V-0540-14051.9 7.720.865
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 30 L-04, V-0540-14032.5 13.8*0.541
Hexachloroethane mg/Kg wet0.34 1.67 3040-14058.4 4.320.973
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14077.1 4.891.29
Isophorone mg/Kg wet0.34 1.67 3040-14069.8 3.271.16
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14058.1 0.7600.969
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14069.6 1.161.16
2-Methylphenol mg/Kg wet0.34 1.67 3030-13071.4 5.131.19
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13070.1 4.411.17
Naphthalene mg/Kg wet0.17 1.67 3040-14066.5 2.311.11
2-Nitroaniline mg/Kg wet0.34 1.67 30 V-0640-14085.1 7.101.42
3-Nitroaniline mg/Kg wet0.34 1.67 30 V-0630-14076.2 0.2361.27
4-Nitroaniline mg/Kg wet0.34 1.67 3040-14086.4 5.491.44
Nitrobenzene mg/Kg wet0.34 1.67 3040-14072.5 4.051.21
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13073.8 0.8441.23
4-Nitrophenol mg/Kg wet0.66 1.67 5030-13081.6 2.181.36
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14059.1 13.20.985
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 3040-14075.1 2.861.25
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14067.8 8.581.13
Pentachloronitrobenzene mg/Kg wet0.34 1.67 3040-14070.4 5.761.17
Pentachlorophenol mg/Kg wet0.34 1.67 30 V-0530-13046.2 13.20.770
Phenanthrene mg/Kg wet0.17 1.67 3040-14074.8 3.761.25
Phenol mg/Kg wet0.34 1.67 30 V-0630-13078.2 6.201.30
Pyrene mg/Kg wet0.17 1.67 3040-14066.1 3.361.10
Pyridine mg/Kg wet0.34 1.67 3030-14038.1 8.250.635
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14061.9 8.561.03
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14055.9 4.090.932
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13068.1 5.651.14
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13064.2 4.131.07
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 75.75.05
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 82.45.50
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 72.32.41
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 86.32.88
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 86.15.74
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 70.42.35
Page 100 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Metals Analyses (Total)[TOC]
Batch B249454 - SW-846 7471
[TOC_3]B249454[TOC]
Blank (B249454-BLK1) Prepared: 01/06/20 Analyzed: 01/07/20
Mercury mg/Kg wet0.025ND
LCS (B249454-BS1) Prepared: 01/06/20 Analyzed: 01/07/20
Mercury mg/Kg wet0.38 7.61 72.7-127.398.17.46
LCS Dup (B249454-BSD1) Prepared: 01/06/20 Analyzed: 01/07/20
Mercury mg/Kg wet0.38 7.61 2072.7-127.3100 2.237.63
Duplicate (B249454-DUP1) Prepared: 01/06/20 Analyzed: 01/07/20 Source: 19L1171-70
Mercury mg/Kg dry0.035 35 J32.00.0161 0.0116
Matrix Spike (B249454-MS1) Prepared: 01/06/20 Analyzed: 01/07/20 Source: 19L1171-70
Mercury mg/Kg dry0.036 0.479 75-1251070.525 0.0116
Batch B249488 - SW-846 3050B
[TOC_3]B249488[TOC]
Blank (B249488-BLK1) Prepared: 01/06/20 Analyzed: 01/07/20
Arsenic mg/Kg wet0.17ND
Chromium mg/Kg wet4.2 J0.15
Lead mg/Kg wet1.7ND
Selenium mg/Kg wet1.3ND
Silver mg/Kg wet0.083ND
Barium mg/Kg wet8.3ND
Cadmium mg/Kg wet0.33ND
LCS (B249488-BS1) Prepared: 01/06/20 Analyzed: 01/07/20
Arsenic mg/Kg wet2.0 143 83.2-117.5104149
Chromium mg/Kg wet50 101 82.4-116.899.0100
Lead mg/Kg wet20 125 82.4-116.8101126
Selenium mg/Kg wet16 77.9 79.3-120.710783.4
Silver mg/Kg wet1.0 34.3 81-119.210034.4
Barium mg/Kg wet100 415 82.7-117.698.6409
Cadmium mg/Kg wet4.0 56.2 82.9-117.310961.0
LCS Dup (B249488-BSD1) Prepared: 01/06/20 Analyzed: 01/07/20
Arsenic mg/Kg wet2.0 143 3083.2-117.5108 3.79155
Chromium mg/Kg wet50 101 3082.4-116.8103 4.25104
Lead mg/Kg wet20 125 3082.4-116.8105 3.61131
Selenium mg/Kg wet16 77.9 3079.3-120.7112 4.2587.0
Silver mg/Kg wet1.0 34.3 3081-119.2104 4.1135.8
Barium mg/Kg wet100 415 2082.7-117.6105 5.84434
Cadmium mg/Kg wet4.0 56.2 2082.9-117.3109 0.23161.1
Page 101 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
Batch B249488 - SW-846 3050B
Duplicate (B249488-DUP1) Prepared: 01/06/20 Analyzed: 01/07/20 Source: 19L1171-67
Arsenic mg/Kg dry0.24 351.590.252 0.248
Chromium mg/Kg dry6.0 356.978.26 7.70
Lead mg/Kg dry2.4 354.455.63 5.89
Selenium mg/Kg dry1.9 35NCNDND
Silver mg/Kg dry0.12 35 J5.290.0307 0.0324
Barium mg/Kg dry12 353.08290300
Cadmium mg/Kg dry0.48 35 J9.470.0475 0.0522
Matrix Spike (B249488-MS1) Prepared: 01/06/20 Analyzed: 01/07/20 Source: 19L1171-67
Arsenic mg/Kg dry0.95 23.8 75-12583.720.2 0.248
Chromium mg/Kg dry24 23.8 75-12598.031.0 7.70
Lead mg/Kg dry9.5 23.8 75-12510430.6 5.89
Selenium mg/Kg dry7.6 23.8 75-12578.118.6 ND
Silver mg/Kg dry0.48 23.8 75-12597.423.2 ND
Barium mg/Kg dry48 23.8 MS-1975-125132*331 300
Cadmium mg/Kg dry1.9 23.8 75-12510625.2 ND
Page 102 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B249433 - % Solids
[TOC_3]B249433[TOC]
Duplicate (B249433-DUP1) Prepared & Analyzed: 01/05/20 Source: 19L1171-11
% Solids % Wt 200.22876.6 76.4
Duplicate (B249433-DUP2) Prepared & Analyzed: 01/05/20 Source: 19L1171-22
% Solids % Wt 202.2874.0 72.3
Duplicate (B249433-DUP3) Prepared & Analyzed: 01/05/20 Source: 19L1171-32
% Solids % Wt 200.90774.2 74.9
Duplicate (B249433-DUP4) Prepared & Analyzed: 01/05/20 Source: 19L1171-34
% Solids % Wt 201.0775.8 76.6
Page 103 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Sample to spike ratio is greater than or equal to 4:1. Spiked amount is not representative of the native amount in
the sample. Appropriate or meaningful recoveries cannot be calculated.
MS-19
Elevated reporting limit due to high concentration of target compounds.RL-11
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-04
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for
this compound.
V-06
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this
compound. Reported result is estimated.
V-35
[TOC_1]Flag/Qualifier Summary[TOC]
Page 104 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 6020B in Soil
NY,VA,NH,NC,MEArsenic
NY,NC,MEChromium
NY,NC,MELead
NY,VA,NH,NC,MESelenium
NY,NC,MESilver
NY,NCBarium
NY,NC,MECadmium
SW-846 7471B in Soil
CT,NH,NY,NC,ME,VAMercury
SW-846 8260D in Soil
NCAcetone
NCAcetone
NCAcrylonitrile
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBenzene
NCBromobenzene
NCBromobenzene
NCBromochloromethane
NCBromochloromethane
NCBromodichloromethane
NCBromodichloromethane
NCBromoform
NCBromoform
NCBromomethane
NCBromomethane
NC2-Butanone (MEK)
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
NCtert-Butyl Alcohol (TBA)
NCn-Butylbenzene
NCn-Butylbenzene
NCsec-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Disulfide
NCCarbon Tetrachloride
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorobenzene
[TOC_1]Certifications[TOC]
Page 105 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Soil
NCChlorodibromomethane
NCChlorodibromomethane
NCChloroethane
NCChloroethane
NCChloroform
NCChloroform
NCChloromethane
NCChloromethane
NC2-Chlorotoluene
NC2-Chlorotoluene
NC4-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
Page 106 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Soil
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NC1,4-Dioxane
NCEthylbenzene
NCEthylbenzene
NCHexachlorobutadiene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCNaphthalene
NCn-Propylbenzene
NCn-Propylbenzene
NCStyrene
NCStyrene
NC1,1,1,2-Tetrachloroethane
NC1,1,1,2-Tetrachloroethane
NC1,1,2,2-Tetrachloroethane
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrachloroethylene
NCTetrahydrofuran
NCTetrahydrofuran
NCToluene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,3,5-Trichlorobenzene
Page 107 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Soil
NC1,1,1-Trichloroethane
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCVinyl Chloride
NCm+p Xylene
NCm+p Xylene
NCo-Xylene
NCo-Xylene
SW-846 8270E in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
NY,NH,ME,NC,VAAcetophenone
NY,NH,ME,NC,VAAniline
CT,NY,NH,ME,NC,VAAnthracene
CT,NY,NH,ME,NC,VABenzidine
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
NY,NH,ME,NC,VABenzoic Acid
CT,NY,NH,ME,NC,VABis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VABis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VABis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VABis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA4-Bromophenylphenylether
CT,NY,NH,ME,NC,VAButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA4-Chloroaniline
CT,NY,NH,ME,NC,VA4-Chloro-3-methylphenol
CT,NY,NH,NC,VA2-Chloronaphthalene
CT,NY,NH,ME,NC,VA2-Chlorophenol
Page 108 of 145
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270E in Soil
CT,NY,NH,ME,NC,VA4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
CT,NY,NH,ME,NC,VADibenzofuran
CT,NY,NH,ME,NC,VADi-n-butylphthalate
NY,NH,ME,NC,VA1,2-Dichlorobenzene
NY,NH,ME,NC,VA1,3-Dichlorobenzene
NY,NH,ME,NC,VA1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA2,4-Dichlorophenol
CT,NY,NH,ME,NC,VADiethylphthalate
CT,NY,NH,ME,NC,VA2,4-Dimethylphenol
CT,NY,NH,ME,NC,VADimethylphthalate
CT,NY,NH,ME,NC,VA4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VADi-n-octylphthalate
NY,NH,ME,NC,VA1,2-Diphenylhydrazine/Azobenzene
CT,NY,NH,ME,NC,VAFluoranthene
NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAHexachlorobenzene
CT,NY,NH,ME,NC,VAHexachlorobutadiene
CT,NY,NH,ME,NC,VAHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VAHexachloroethane
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylphenol
CT,NY,NH,ME,NC,VA3/4-Methylphenol
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VA2-Nitroaniline
CT,NY,NH,ME,NC,VA3-Nitroaniline
CT,NY,NH,ME,NC,VA4-Nitroaniline
CT,NY,NH,ME,NC,VANitrobenzene
CT,NY,NH,ME,NC,VA2-Nitrophenol
CT,NY,NH,ME,NC,VA4-Nitrophenol
CT,NY,NH,ME,NC,VAN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VAN-Nitrosodi-n-propylamine
NY,NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VAPentachlorophenol
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPhenol
CT,NY,NH,ME,NC,VAPyrene
CT,NY,NH,ME,NC,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
Page 109 of 145
Table of Contents
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270E in Soil
CT,NY,NH,ME,NC,VA1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2020
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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Table of Contents