22016 Supplemental BF Assessment Report_Quality Products Company 20191216

Via Email

December 16, 2019

NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646

Attention: Mr. Bill Schmithorst, PG

Re: Supplemental Brownfields Assessment Report
Quality Products Company
S. Mint Street and Westwood Avenue
Charlotte, North Carolina
Brownfields Project No. 22016-18-060
H&H Job No. LEH-004

Dear Bill:

1.0 Introduction

On behalf of LEH NC Mint, LLC (the Prospective Developer or PD), Hart & Hickman, PC
(H&H) is providing this Supplemental Brownfields Assessment Report to document additional
soil and groundwater assessment activities completed at the Quality Products Company
Brownfields property (Brownfields Project No. 22016-18-060) located at 1513-1537 S. Mint
Street (odd addresses only) and 404 Westwood Avenue in Charlotte, Mecklenburg County,
North Carolina (Site or subject Site). A Site location map is provided as Figure 1, and the Site
and surrounding area are shown in Figure 2.

In July 2019, H&H collected soil, groundwater, and sub-slab soil gas samples for laboratory
analysis to evaluate the potential for impact associated with historical uses on the 1525, 1529,
1537 S. Mint Street and 404 Westwood Avenue portions of the Brownfields property. The July
2019 assessment activities are documented in our Phase I and II Environmental Site Assessment
(ESA) report dated August 26, 2019. Locations of previous environmental samples collected at
the Brownfields property including the recent July 2019 Phase II ESA sample locations are
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shown in Figure 2. A brief summary of the July 2019 soil, groundwater, and sub-slab soil gas
assessment results is provided below.

 Soil sample laboratory analytical results indicated several volatile organic compounds
(VOCs) and metals were detected at concentrations exceeding the North Carolina
Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB)
Preliminary Soil Remediation Goals (PSRGs) in shallow soil samples collected below the
slab of the 1525 S. Mint Street building and at the base of an out-of-use underground
storage tank (UST) located beneath the western portion of the 1525 S. Mint Street
building. No compounds were detected above the DEQ IHSB PSRGs in soil samples
collected on the 1529 S. Mint Street, 1537 S. Mint Street, or 404 Westwood Avenue
portions of the Brownfields property.

 Trace levels of VOCs and metals were detected in groundwater samples collected on the
1525, 1529, 1537 S. Mint Street and 404 Westwood Avenue portions of the Brownfields
property. Laboratory analytical results of a groundwater sample collected in a
downgradient (northwestern) portion of the 1537 S. Mint Street property indicated that
1,2-dichloroethane was detected at a concentration slightly exceeded the DEQ 15A
NCAC 2L Groundwater Quality Standard (2L Standard). No other compounds were
detected at concentrations above the 2L Standards in other groundwater samples
collected in the 1525, 1529, 1537 S. Mint Street and 404 Westwood Avenue portions of
the Brownfields property and no compounds were detected at concentrations above the
DEQ Division of Waste Management (DWM) Vapor Intrusion Groundwater Screening
Levels (GWSLs).

 H&H collected two sub-slab soil gas samples for laboratory analysis in each of the three
buildings (a total of 6 sub-slab soil gas samples) located in the 1525, 1529, and 1537 S.
Mint Street portions of the Brownfields property. Sub-slab soil gas sample results
indicated that benzene, naphthalene, 1,2,4-trimethylbenzene, and 1,3,5-trimethylbenzene
were detected at concentrations exceeding the DEQ DWM Vapor Intrusion Sub-slab and
Exterior Soil Gas Screening Levels (SGSLs) in a sample collected within the 1525 S.
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Mint Street building. No compounds were detected at concentrations above the DEQ
DWM SGSLs in the sub-slab soil gas samples collected within the 1529 or 1537 S. Mint
Street buildings.

In an email dated November 4, 2019, the DEQ Brownfields Program requested additional soil
and groundwater assessment to further evaluate the potential for impacts in the 1537 S. Mint
Street and 404 Westwood Avenue portions of the Brownfields property based on results of the
July 2019 Phase II ESA soil, groundwater, and sub-slab soil gas sampling results. H&H
prepared a Supplemental Brownfields Assessment Work Plan dated December 6, 2019 to address
DEQ Brownfields requests for additional assessment. A summary of the supplemental
Brownfields soil and groundwater assessment activities is provided in the following sections.

2.0 Supplemental Brownfields Assessment Activities

On November 9, 2019, H&H completed soil and groundwater sampling activities to further
evaluate the potential for impacts in the 1537 S. Mint Street and 404 Westwood Avenue portions
of the Brownfields property. The assessment activities were performed in general accordance
with the DEQ IHSB Guidelines for Assessment and Cleanup (Guidelines) dated October 2015,
the most recent versions of the U.S. Environmental Protection Agency (EPA) Region IV Science
and Ecosystem Support Division (SESD) Field Branches Quality System and Technical
Procedure, the DEQ-approved November 2018 Brownfields Assessment Work Plan (Revision
1), and the Supplemental Brownfields Assessment Work Plan dated December 6, 2019.

Prior to completed the sampling activities, H&H contacted North Carolina 811, the public utility
locator, to mark subsurface utilities at the Site. In accordance with Mecklenburg County rules,
H&H updated the existing Subsurface Investigation Permit (SIP No. 70002650) following
completion of the groundwater sampling activities.

A summary of the supplemental soil assessment activities is provided in Section 3.0, the
supplemental groundwater assessment activities are discussed in Section 4.0, and summary and
conclusions based on the assessment results is provided in Section 5.0.
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3.0 Soil Assessment Activities

On November 9, 2019, H&H provided oversight during advancement of two shallow soil borings
(SB-11 and SB-12) south of the 1537 S. Mint Street building in the southwestern portion of the
Brownfields property. One soil sample was collected from each boring for laboratory analysis to
evaluate the potential for impacts in shallow soil in an area historically used for storage of
equipment and materials associated with automotive repair operations. The soil boring locations
(denoted by SB nomenclature) are shown in Figure 2, and a brief summary of the soil sampling
activities and results is provided below.

3.1 Soil Sampling Methodology

H&H teamed with Midsouth Environmental to advance soil borings SB-11 and SB-12 (Figure 2)
to approximately 5 ft below ground surface (ft bgs) using decontaminated stainless-steel hand
augers. Continuous soil samples were collected from the center of the hand auger bucket at each
boring. The soil samples were logged for lithologic description and screened using visual and
olfactory methods for obvious evidence of staining, unusual odors, and for the presence of
volatile organic vapors using a calibrated photoionization detector (PID). Field screening results
did not identify obvious indications of potential impact in soil. Therefore, soil samples were
collected from shallow soil at a depth of approximately 1 to 3 feet (ft) below ground surface
(bgs). Boring logs, including lithologic descriptions and field screening results are provided in
Appendix A.

Following field screening, the soil samples selected for laboratory analysis were collected
directly into dedicated laboratory supplied sample containers, labeled with the sample
identification, date, time, and requested analyses and placed in a laboratory supplied cooler with
ice. The samples were submitted under standard chain of custody protocols to Pace Analytical
(Pace) for analysis of VOCs by EPA Method 8260, semi-VOCs (SVOCs) by EPA Method 8270,
and Resource Conservation and Recovery Act (RCRA) metals plus hexavalent chromium by
EPA Methods 6020/7471/7199. In addition, H&H instructed Pace to analyze soil sample (SB-8)
previously collected in July 2019 for polychlorinated biphenyls (PCBs) by EPA Method 8082.
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Soil sample SB-8 was collected adjacent to an in-ground hydraulic lift located in the 1537 S.
Mint Street building during Phase II ESA activities to evaluate the potential for impact
associated with an undocumented release from assumed underground hydraulic oil reservoirs.

Upon completion of the sampling activities, the soil borings were abandoned and the surfaces
were repaired similar to pre-drilling conditions. In addition, the soil boring locations were
estimated using a hand-held global positioning system (GPS) unit.

3.2 Soil Sampling Analytical Results

A tabular summary of the soil sample analytical results is presented in Table 1 along with
historical soil sample analytical results from previous assessment activities completed on the
Brownfields property. The laboratory analytical report and chain of custody records are
provided as Appendix B. The laboratory analytical results were compared to the DEQ IHSB
Residential and Industrial/Commercial PSRGs dated May 2019. In addition to the PSRGs,
metals results were compared to published concentrations for naturally occurring metals in North
Carolina soil and Site-specific background concentrations.

Laboratory analytical results indicate that trace levels of acetone (up to 0.0393J milligram per
kilogram [mg/kg]) were detected in both samples at concentrations well below the DEQ IHSB
Residential PSRG of 12,000 mg/kg. Please note that the “J-Flag” designation indicates that the
concentration was detected above the laboratory method detection level, but below the laboratory
reporting limits resulting in a laboratory estimated value. No other VOCs or SVOCs were
detected in the November 2019 soil samples.

Low levels of several metals including arsenic (up to 2.07 mg/kg), barium (up to 48.6 mg/kg),
trivalent chromium (up to 44.1 mg/kg), lead (up to 12.9 mg/kg), mercury (up to 0.167 mg/kg),
and selenium (up to 0.896 mg/kg) were detected above the laboratory method detection limits in
both soil samples. The detected metals concentrations are consistent with naturally occurring
levels in North Carolina soil and are considered to be background levels.

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As noted above, soil sample SB-8 collected in July 2019 near an in-ground hydraulic lift in the
1537 S. Mint Street building was submitted for analysis of PCBs. Laboratory analytical results
indicate that PCBs were not detected at concentrations above the laboratory method detection
limits. A copy of the laboratory analytical report updated to include the SB-8 soil sample PCB
results is included in Appendix B.

4.0 Groundwater Assessment Activities

On November 9, 2019, H&H provided oversight during installation of two temporary
groundwater monitoring wells in southwestern portions of the Brownfields property and
collected groundwater samples for laboratory analysis from each location to further evaluate
subsurface conditions at the Site. The temporary groundwater monitoring well locations
(denoted by TMW nomenclature) are shown in Figure 2, and a brief summary of the
groundwater sampling activities and results is provided below.

4.1 Groundwater Sampling Activities

H&H teamed with Midsouth Environmental to advance two soil borings for installation of
temporary groundwater monitoring wells TMW-5 and TMW-6. Temporary monitoring well
TMW-5 was installed cross-gradient and southeast of the 1525 S. Mint Street building, and
temporary monitoring well TMW-6 was installed cross-gradient and southeast of the 1537 S.
Mint Street building (Figure 2). The temporary well borings were advanced using a track-
mounted drill rig capable of utilizing direct push technology (DPT) drilling techniques.
Continuous soil samples were collected from each soil boring using acetate lined macrocore
sleeves. The soil samples were logged for lithologic description and field screened for the
presence of obvious staining, unusual odors, and volatile organic vapors using a calibrated PID.
Field screening results did not identify obvious evidence of impacts in the temporary well boring
soil samples.

Temporary monitoring wells were constructed of 1-inch diameter PVC with 10 ft of well screen
set to bracket the water table and 1-inch diameter PVC well casing to the ground surface. A
filter sand pack was placed from the bottom of each temporary well boring to approximately 2 ft
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above each well screen, and a minimum of an approximately 2 ft hydrated bentonite seal was
then installed above the filter sand pack. Temporary monitoring well boring logs and
construction details are provided in Appendix A.

Upon completion of temporary monitoring well installation activities, the wells were allowed to
equilibrate to static conditions and a decontaminated electronic water level indicator was used to
measure the depth to the water table relative to the ground surface and the tops of the well
casings. Depth to groundwater in the southwestern portions of the Brownfields property was
measured at depths between approximately 17 and 18 ft bgs.

Each temporary well was then developed by removing a minimum of 3 to 5 well volumes and
field parameters stabilized (pH ± 0.1 Standard Units [SU] and conductivity varied no more than
5%). After development, a groundwater sample was collected from temporary monitoring wells
TMW-5 and TMW-6 utilizing low flow/low stress purging techniques using a peristaltic pump
and dedicated polyethylene tubing. The intake point of the pump tubing was placed in the
approximate mid-portion of the screened interval of the well and groundwater was removed at a
rate no greater than 200 milliliters per minute. H&H utilized a water quality meter to collect
measurements of pH, temperature, dissolved oxygen, oxidation reduction potential, turbidity, and
specific conductivity during the purging process. Purging was considered complete when the
parameters had stabilized (pH ± 0.1 SU, conductivity varied no more than 5%, and turbidity was
less than 10 Nephelometric Turbidity Units [NTUs]). Groundwater sampling forms completed
by sampling personnel are provided in Appendix C.

Once groundwater parameters stabilized, the groundwater samples for VOC analysis were
collected directly into laboratory supplied sample containers using the “soda straw” method to
minimize volatile loss through the peristaltic pump head. Groundwater samples for the
remaining analyses were collected directly into laboratory supplied glassware directly from the
sample tubing discharge. The sample containers were labeled with the sample identification,
date, and requested analysis, and placed in a laboratory supplied cooler with ice. The samples
were delivered to Pace under standard chain of custody protocols for analysis of VOCs by EPA
Method 8260, SVOCs by EPA Method 8270 and RCRA metals by EPA Methods 6020/7471.
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4.2 Groundwater Sampling Analytical Results

A tabular summary of the groundwater samples analytical results is presented in Table 2 along
with historical groundwater analytical data for sample collected during previous assessment
activities completed at the Brownfields property. The laboratory analytical report and chain of
custody records are provided in Appendix B. Groundwater data was compared to the 2L
Standards dated April 2013 and the DEQ DWM Residential and Non-Residential Vapor
Intrusion GWSLs dated February 2018.

Laboratory analytical results indicated no VOCs or SVOCs were detected above the laboratory
method detection limits in groundwater samples TMW-5 and TMW-6. Trace levels of metals
were detected in at least one of the two groundwater samples including arsenic (up to 0.452J
µg/L), barium (up to 88 µg/L), total chromium (up to 4.14 µg/L), lead (up to 0.790J µg/L), and
selenium (up to 1.94J µg/L). No metals were detected at concentrations above the 2L Standards.

5.0 Summary and Conclusions

H&H completed supplemental Brownfields assessment activities in southwestern portions of the
Quality Products Company Brownfields property located in Charlotte, Mecklenburg County.
The assessment activities were conducted in accordance with the DEQ Brownfields approved
Work Plan (Revision 1) dated November 28, 2018 and the Supplemental Brownfields
Assessment Work Plan dated December 6, 2019. Supplemental Brownfields assessment
activities included collection of soil and groundwater samples for laboratory analysis further
evaluate the potential for impacts in areas of potential concern at the Site identified by DEQ
Brownfields. A brief summary of the Brownfields assessment results is provided below.

 H&H collected two shallow soil samples on the southern side of the 1537 S. Mint Street
building from shallow soil depths. No organic compounds were detected above the DEQ
IHSB PSRGs in either soil sample. In addition, detected metals concentrations appear to
be consistent with naturally occurring levels in North Carolina soil.
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Attachments:

Table 1 – Summary of Soil Analytical Data
Table 2 – Summary of Groundwater Analytical Data

Figure 1 – Site Location Map
Figure 2 –Sample Location Map

Appendix A – Boring Logs
Appendix B – Laboratory Analytical Reports
Appendix C – Groundwater Sampling Forms
Table 1Summary of Soil Analytical DataQuality Products ComapnyS. Mint Street and Westwood AvenueCharlotte, North CarolinaH&H Job No. LEH-004Sample ID SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-7 SB-8 SB-9 SB-10 SB-11 SB-12Date Sample Collected 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 11/9/2019 11/9/2019Sample LocationUST - 1525 S. Mint StreetCentral floor drain - 1525 S. Mint StreetSoutheastern floor drain - 1525 S. Mint StreetMechanical pit -1537 S. Mint StreetDepth (ft bgs)8-10 3-4 0-2 0-2 0-2 2-3 0-2 7-10 7-10 7-10 1-3 1-3 Range MeanUnitsVOCs (8260D)Acetone<0.460.33<0.00850.021J 0.033J 0.024J<0.0092 NA NA NA0.0185J 0.0393J 12,000 140,000-- -- --Benzene<0.0740.0045J<0.0014 <0.0015 <0.0015 <0.0015 <0.0015 NA NA NA <0.0011 <0.00111.2 5.4-- -- --2-Butanone (MEK)<0.130.028J<0.0025 <0.0027 <0.0027 <0.0028 <0.0027 NA NA NA <0.0151 <0.01435,500 40,000-- -- --n-Butylbenzene 1.6<0.0018 <0.0015 <0.0017 <0.0017 <0.0017 <0.0017 NA NA NA <0.0036 <0.0034780 12,000-- -- --sec-Butylbenzene 0.71<1.9 <0.0014 <0.0015 <0.0015 <0.0015 <0.0015 NA NA NA <0.0027 <0.00251,600 23,000-- -- --tert-Butylbenzene 0.14J<0.0020 <0.0017 <0.0018 <0.0019 <0.0019 <0.0018 NA NA NA <0.0021 <0.00201,600 23,000-- -- --Chlorobenzene<0.088145<0.00160.0022J<0.0018 <0.0018 <0.0017 NA NA NA <0.0012 <0.001258 280-- --1,2-Dichlorobenzene<0.088159<0.00160.0056<0.0018 <0.0018 <0.0017 NA NA NA <0.0022 <0.0021380 2,000-- -- --1,3-Dichlorobenzene<0.0933.9J<0.0017 <0.0018 <0.0019 <0.0019 <0.0018 NA NA NA <0.0023 <0.0021NS NS-- -- --1,4-Dichlorobenzene<0.07923.6<0.0014 <0.0016 <0.0016 <0.0016 <0.0016 NA NA NA <0.0022 <0.00212.8 12-- -- --Ethylbenzene 1.1 2.9J<0.0015 <0.0017 <0.0017 <0.0017 <0.0017 NA NA NA <0.0013 <0.00136.1 27-- -- --Isopropylbenzene (Cumene) 1.3 3.4J<0.0016 <0.0017 <0.0018 <0.0018 <0.0017 NA NA NA <0.0018 <0.0017410 2,100-- -- --p-Isopropyltoluene (p-Cymene)<0.07918.3<0.0014 <0.0016 <0.0016 <0.0016 <0.0016 NA NA NA <0.0031 <0.0029NE NE-- -- --Naphthalene5.9 42.0<0.0010 <0.00110.0028J<0.0014 <0.0011 NA NA NA <0.0054 <0.00514.1 18-- -- --n-Propylbenzene 3.4<2.0 <0.0014 <0.0016 <0.0016 <0.0016 <0.0016 NA NA NA <0.0021 <0.0020780 5,100-- --Toluene<0.0830.13<0.0015 <0.0017 <0.0017 <0.0017 <0.0017 NA NA NA <0.0021 <0.0019990 9,700-- -- --1,2,4-Trichlorobenzene<0.0740.0075<0.0017 <0.0015 <0.0015 <0.0015 <0.0015 NA NA NA <0.0034 <0.003212 55-- -- --1,2,4-Trimethylbenzene<0.093127<0.00170.0025J<0.0019 <0.0019 <0.0018 NA NA NA <0.0025 <0.002363 370-- -- --1,3,5-Trimethylbenzene<0.08341.6<0.0015 <0.0017 <0.0017 <0.0017 <0.0017 NA NA NA <0.0021 <0.002056 320-- -- --m&p-Xylene<0.178.2J<0.0030 <0.0033 <0.0034 <0.0034 <0.0033 NA NA NA <0.0030 <0.0028240 1,040-- -- --SVOCs (8270E)1,2-Dichlorobenzene<0.08718.5<0.083 <0.091 <0.093 <0.090 <0.090 NA NA NA <0.0931 <0.0913380 2,000-- -- --1,4-Dichlorobenzene<0.0892.8J<0.085 <0.093 <0.095 <0.091 <0.092 NA NA NA <0.0946 <0.09282.8 12-- -- --1-Methylnaphthalene0.20J4.8<0.10 <0.11 <0.11 <0.11 <0.11 NA NA NA <0.115 <0.11218 73-- -- --2-Methylnaphthalene0.36J7.0<0.098 <0.11 <0.11 <0.11 <0.11 NA NA NA <0.109 <0.10748 600-- -- --Naphthalene0.505.1<0.092 <0.10 <0.10 <0.10 <0.10 NA NA NA <0.103 <0.1014.1 18-- -- --PCBs (8082A)NA NA NA NA NA NA NAALL BDL NA NA NA NA -- ---- -- --Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (May 2019) or NC DEQ Underground Storage Tank (UST) Section Maximum Soil Contaminant Concentration (MSCCs)2) North Carolina DEQ UST Section Action Levels (2019) 3) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.4) Background values reported for soils of the southeastern United States.Compound concentrations reported in milligrams per kilogram (mg/kg)Trivalent chromium calculated as total chromium minus hexavalent chromium.Aside from metals, only constituents detected in at least one sample are shown.Compound concentrations are reported to the laboratory method detection limits.Bold indicates concentration exceeds DEQ Action Level or DEQ IHSB Residential PSRG and are above the mean background metals in North Carolina soils for metals as preliminary comparison Underlined indicates concentration exceeds DEQ IHSB Industrial/Commercial PSRGs and are above the mean background metals in North Carolina soils for metals as preliminary comparisonVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; GRO = gasoline range organics; DRO = diesel range organics; ORO = oil range organics; PCBs = polychlorinated biphenylsVPH = volatile petroleum hydrocarbons; EPH = extractable petroleum hydrocarbons; MADEP = Massachusetts Department of Environmental ProetectionPSRGs are listed for comparison to VOCs, SVOCs, and metals. MSCCs are listed for comparison to EPH and VPH. DEQ action levels are listed for comparison to GRO and DRO.ft bgs= feet below ground surface; NA= Not Analyzed; -- = Not Applicable; NE = Not Established; NS = Not Specified; BDL = Below Laboratory Method Detection LimitJ indicates a detection above the laboratory method detection limit (MDL), but below the laboratory reporting limit resulting in a laboratory estimated concentrationPaint booth - 1525 S. Mint Street In-ground hydraulic lifts - 1537 S. Mint StreetResidential PSRGs or MSCCs(1)Industrial/ Commercial PSRGs or MSCCs (1)DEQ Action Levels (2)1525, 1529, & 1537 S. Mint Street and 404 Westwood Avenuemg/kgPublished Background Metals Concentrations for North Carolina Soils (3)Southeast of 1537 S. Mint Street Building\\HARTHICKMAN.LOCAL\Shares\MasterFiles\AAA-Master Projects\Lischerong Enterprises and Holdings (LEH)\S. Mint Street\1525-1537 Phase I, II (LEH-005)\Supplemental BF Assessment\Tables\LEH_Data Tables12/13/2019Table 1 (Page 1 of 2)Hart & Hickman, PC
Table 1Summary of Soil Analytical DataQuality Products ComapnyS. Mint Street and Westwood AvenueCharlotte, North CarolinaH&H Job No. LEH-004Sample ID SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-7 SB-8 SB-9 SB-10 SB-11 SB-12Date Sample Collected 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 7/27/2019 11/9/2019 11/9/2019Sample LocationUST - 1525 S. Mint StreetCentral floor drain - 1525 S. Mint StreetSoutheastern floor drain - 1525 S. Mint StreetMechanical pit -1537 S. Mint StreetDepth (ft bgs)8-10 3-4 0-2 0-2 0-2 2-3 0-2 7-10 7-10 7-10 1-3 1-3 Range MeanUnitsEPH (MADEP)Aliphatic (C9-C18)12.5NA NA NA NA NA NA NA NA NA NA NA1,500 40,000-- -- --VPH (MADEP)Aliphatic (C5-C8)253NA NA NA NA NA NA NA NA NA NA NA939 24,528-- -- --Aliphatic (C9-C12)327NA NA NA NA NA NA NA NA NA NA NA1,500 40,000-- -- --Aromatic (C9-C10)126NA NA NA NA NA NA NA NA NA NA NA469 12,264-- -- --GRO (8015C)C6-C10799NA NA NA NA NA NA NA NA NA NA NA----50-- --DRO (8015C)C10-C28106NA NA NA NA NA NA <3.2 <3.1 <3.5 NA NA----100-- --ORO (8015C)C28-C40NA NA NA NA NA NA NA <9.4 <9.0 <9.8 NA NA----NE-- --Metals (6020B/7471B/7199)Arsenic2.45 1.88 2.2968.22.26 3.73 3.93NA NA NA1.36 2.070.68 3.0--1.0 - 18 4.8Barium195 27.8 44.8 46.3 55.7 294 75.3NA NA NA35.3 48.63,100 47,000--50 - 1,000 356Cadmium0.280J 0.584J 0.316J 0.257J<1.07 <0.105 <0.104 NA NA NA <0.104 <0.10914 200--1.0 - 10 (5)4.3 (4)Trivalent Chromium43.0 33.1 35.2 40.8 41.5 75.6 35.4NA NA NA30.6 44.123,000 350,000--7.0 - 300 65Hexavalent Chromium0.533J 0.372J<0.307 <0.3600.386J 0.451J 0.339JNA NA NA <0.333 <0.3460.31 6.5--NS NSTotal Chromium43.5 33.5 35.2 40.8 41.9 76.1 35.7NA NA NA30.6 44.1-- ---- -- --Lead12.3 21.5 25.6 24.6 14.7 20.1 22.0NA NA NA7.51 12.9400 800--ND - 50 16Mercury10.530.24.090.207 0.768 0.4565.88NA NA NA0.0692 0.1672.3 9.7--0.03 - 0.52 0.12Selenium1.31 1.17 1.01 0.954 0.83 1.31 0.843NA NA NA0.781 0.89678 1,200--<0.1 - 0.8 0.42Silver<0.6710.421J<0.187 <0.219 <0.208 <0.204 <0.201 NA NA NA <0.202 <0.21078 1,200--ND - 5.0 (5)NSNotes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (May 2019) or NC DEQ Underground Storage Tank (UST) Section Maximum Soil Contaminant Concentration (MSCCs)2) North Carolina DEQ UST Section Action Levels (2019) 3) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.4) Background values reported for soils of the southeastern United States.Compound concentrations reported in milligrams per kilogram (mg/kg)Trivalent chromium calculated as total chromium minus hexavalent chromium.Aside from metals, only constituents detected in at least one sample are shown.Compound concentrations are reported to the laboratory method detection limits.Bold indicates concentration exceeds DEQ Action Level, DEQ Soil to Water MSCC, or DEQ IHSB Residential PSRG and are above the mean background metals in North Carolina soils for metals as preliminary comparison Underlined indicates concentration exceeds DEQ IHSB Industrial/Commercial PSRGs and are above the mean background metals in North Carolina soils for metals as preliminary comparisonVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; GRO = gasoline range organics; DRO = diesel range organics; ORO = oil range organics; PCBs = polychlorinated biphenylsVPH = volatile petroleum hydrocarbons; EPH = extractable petroleum hydrocarbons; MADEP = Massachusetts Department of Environmental ProetectionPSRGs are listed for comparison to VOCs, SVOCs, and metals. MSCCs are listed for comparison to EPH and VPH. DEQ Action Levels are listed for comparison to GRO and DRO.ft bgs= feet below ground surface; NA= Not Analyzed; -- = Not Applicable; NE = Not Established; NS = Not Specified; BDL = Below Laboratory Method Detection LimitJ indicates a detection above the laboratory method detection limit (MDL), but below the laboratory reporting limit resulting in a laboratory estimated concentrationDEQ Action Levels (2)Residential PSRGs or MSCCs(1)Industrial/ Commercial PSRGs or MSCCs (1)Published Background Metals Concentrations for North Carolina Soils (3)Paint booth - 1525 S. Mint Street In-ground hydraulic lifts - 1537 S. Mint Street1525, 1529, & 1537 S. Mint Street and 404 Westwood Avenuemg/kgSoutheast of 1537 S. Mint Street\\HARTHICKMAN.LOCAL\Shares\MasterFiles\AAA-Master Projects\Lischerong Enterprises and Holdings (LEH)\S. Mint Street\1525-1537 Phase I, II (LEH-005)\Supplemental BF Assessment\Tables\LEH_Data Tables12/13/2019Table 1 (Page 2 of 2)Hart & Hickman, PC
Table 2Summary of Groundwater Analytical DataQuality Products CompanyS. Mint Street and Westwood AvenueCharlotte, North CarolinaH&H Job No. LEH-004Sample ID TMW-1 TMW-2 TMW-3 TMW-4 TMW-5 TMW-6Date Sample Collected 7/27/2019 7/27/2019 7/27/2019 7/27/2019 11/9/2019 11/9/2019Location DescriptionUpgradient - 404 Westwood Ave.East of 1529 S. Mint StreetNorthwest of 1529 S. Mint StreetNorthwest of 1537 S. Mint StreetSoutheast of 1525 S. Mint Street BuildingSoutheast of 1537 S. Mint Street BuildingUnitsVOCs (8260D)1,2-Dichloroethane<0.34 <0.34 <0.340.55J<0.34 <0.340.4 22 981,1-Dichloroethylene0.80J<0.24 <0.24 <0.24 <0.24 <0.24350 39 160Toluene0.44J<0.24 <0.24 <0.24 <0.24 <0.24600 3,800 16,000SVOCs (8270E)All BDLAll BDLAll BDL All BDL All BDL All BDL-- -- --Metals (6020A-B, 7470A)Arsenic0.323JNA NA <0.2500.452J<0.25010-- --Barium30.7NA NA102 88 38 700-- --Cadmium0.404JNA NA <0.160 <0.160 <0.1602-- --Chromium2.58NA NA0.761J 4.14 1.94J 10-- --Lead1.13JNA NA0.356J 0.790J<0.24015-- --Mercury<0.0490 NA NA <0.0490 <0.0490 <0.04901 0.18 0.75Selenium<0.380 NA NA <0.3801.94J<0.38020-- --Silver<0.310 NA NA <0.310 <0.310 <0.31020-- --Notes:1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) (April 2013)2) NC DEQ Division of Waste Management (DWM) Residential Vapor Intrusion Groundwater Screening Level (GWSLs) (February 2018)3) NC DEQ DWM Non-Residential Vapor Intrusion Groundwater Screening Level (GWSLs) (February 2018)Compound concentrations reported in micrograms per liter (µg/L)Aside from metals, only constituents detected in at least one sample are shownCompound concentrations are reported to the laboratory method detection limitsBold indicates concentration exceeds DEQ 2L StandardVOCs = volatile organic compounds; SVOCs = semi-volatile organic compoundsNA = Not Analyzed; -- = Not Applicable; BDL = Below Laboratory Method Detection LimitJ indicates a detection above the laboratory method detection limit (MDL), but below the laboratory reporting limit resulting in a laboratory estimated concentrationµg/LNon-Residential GWSL(3) 2L Standards (1) Residential GWSL(2)1525, 1529, & 1537 S. Mint Street and 404 Westwood Avenue\\HARTHICKMAN.LOCAL\Shares\MasterFiles\AAA-Master Projects\Lischerong Enterprises and Holdings (LEH)\S. Mint Street\1525-1537 Phase I, II (LEH-005)\Supplemental BF Assessment\Tables\LEH_Data Tables12/13/2019Table 2 (Page 1 of 1)Hart & Hickman, PC
TITLE
PROJECT
SITE LOCATION MAP
QUALITY PRODUCTS COMPANYSOUTH MINT STREET AND WESTWOOD AVENUECHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
12-3-19 0
1LEH-004
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NORTH CAROLINA, 1991
IAS-3
IAS-4
IAS-2
IAS-1BG-1
BG-2
TMW-2
BKG-1
PIRTEK
SOUTHEND
SSV-1
SSV-4
SSV-2
SB-1RCI DEMOL
I
T
IONVACANT
SB-5
SB-6
TMW-1
SB-2
SB-4
SB-5
SB-3
SB-6
SB-8
SB-9
SB-10
SB-7
SSV-5
SSV-6
TMW-4
TMW-1
TMW-2
TMW-3
S. MI
N
T
S
T
R
E
E
T
WESTWOOD AVENUE
SB-4
SB-2
SB-1
SB-3
SB-1
TMW-3/DUP-1
SSV-3
SSV-4
SSV-3
SSV-2
SSV-1
TMW-6/SB-12
SB-11
TMW-5
REVISION NO. 0DATE: 11-19-19
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
JOB NO. LEH-004 FIGURE NO. 2
QUALITY PRODUCTS COMPANY
S. MINT STREET AND WESTWOOD AVENUE
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
NOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG CO. GIS
(2019).
2.JANUARY 2018 PHASE II SAMPLES COLLECTED BY H&H ON
JANUARY 26, 2018.
3.DECEMBER 2018 BROWNFIELDS ASSESSMENT SAMPLES
COLLECTED BY H&H ON DECEMBER 19-20, 2018.
4.JULY 2019 PHASE II ESA SAMPLES COLLECTED BY H&H ON
JULY 27, 2019.
5. NOVEMBER 2019 SUPPLEMENTAL BROWNFIELDS ASSESSMENT SAMPLES COLLECTED BY H&H ON NOVEMBER 9, 2019.
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
FORMER BUILDING FOOTPRINT
SOIL BORING (JANUARY 2018)
SUB-SLAB SOIL GAS MONITORING POINT
(JANUARY 2018)
SOIL BORING (DECEMBER 2018)
CO-LOCATED SOIL BORING/TEMPORARY
GROUNDWATER MONITORING WELL
(DECEMBER 2018)
INDOOR AIR SAMPLE LOCATION
(DECEMBER 2018)
SOIL BORING (JULY 2019)
TEMPORARY GROUNDWATER MONITORING
WELL (JULY 2019)
SUB-SLAB SOIL GAS MONITORING POINT
(JULY 2019)
SOIL BORING (NOVEMBER 2019)
TEMPORARY GROUNDWATER MONITORING
WELL (NOVEMBER 2019)
CO-LOCATED SOIL
BORING/TEMPORARY GROUNDWATER
MONITORING WELL (NOVEMBER 2019)S:\AAA-Master Projects\Lischerong Enterprises and Holdings (LEH)\S. Mint Street\Figures\Brownfields Assessment Maps.dwg, 11/19/2019 9:45:05 AM, amckenzie

Appendix A
Boring Logs
NOTES: Boring installed to 3.0' on 11/9/19 using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Lisherong Enterprise and Holdings
LEH.004
1515-1537 S. Mint Street, 404Westwood Avenue, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-11
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/9/19
Midsouth Environmental
Don Warren
Alexis McKenzie
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') Concrete
(0.5') Lean CLAY (CL); medium plasticity, stiff, moist, reddish-brown
(3') Boring terminated
9.1
SB-11
0
1
2
3
4
5
11/9/19
Hand Auger
NOTES: Hole precleared to 5.0' on 11/9/19 using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Lisherong Enterprise and Holdings
LEH.004
1515-1537 S. Mint Street, 404Westwood Avenue, Charlotte, NC
WELL LOG
Well No.
Page:
TMW-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/9/19
11/9/19
Midsouth Environmental
Direct Push
54DT
Don Warren
Alexis McKenzie
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
20.0 Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
20.0
1.0
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Pellets
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Silty CLAY (CL); medium plasticity, medium stiff, moist, reddish-brown
(4') As Above: orange-brown
(5') Clayey SILT (ML); soft, moist, light
brown, tan
(11') As Above: wet
(12') Silty SAND (SP); loose, wet, white, tan
1.2
2.4
1.0
7.1
2.7
6.1
5.6
4.6
4.2
5.1
0
5
10
15
20
NOTES: Hole precleared to 5.0' on 11/9/19 using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Lisherong Enterprise and Holdings
LEH.004
1515-1537 S. Mint Street & 404
Westwood Avenue, Charlotte, NC
WELL LOG
Well No.
Page:
TMW-6/SB-12
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/9/19
11/9/19
Midsouth Environmental
Direct Push
54DT
Don Warren
Alexis McKenzie
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
24.0 Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
24.0
1.0
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Pellets
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
(0') Concrete
(0.5') Silty CLAY (CL); medium plasticity, medium stiff, moist, reddish-brown
(3') Clayey SILT (ML); medium stiff, moist, reddish-brown
(10') As Above: trace sand
(15') Sandy SILT (ML); soft, wet, light brown, tan, black mottling
(24') Boring terminated
8.5
6.2
3.2
4.7
3.6
SB-12
0
5
10
15
20
25

Appendix B
Laboratory Analytical Reports
#=CL#
November 19, 2019
LIMS USE: FR - RALPH MCGEE
LIMS OBJECT ID: 92453170
92453170
Project:
Pace Project No.:
RE:
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
LEH-004
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on November 11, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
cc:Alexis McKenzie, Hart & Hickman
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92453170
LEH-004
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 32
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92453170
LEH-004
Lab ID Sample ID Matrix Date Collected Date Received
92453170001 SB-11 Solid 11/09/19 13:00 11/11/19 13:43
92453170002 SB-12 Solid 11/09/19 12:50 11/11/19 13:43
92453170003 DUP-3 Solid 11/09/19 00:00 11/11/19 13:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 32
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92453170
LEH-004
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92453170001 SB-11 EPA 6020B 7 PANJPD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92453170002 SB-12 EPA 6020B 7 PANJPD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453170
LEH-004
Sample:SB-11 Lab ID:92453170001 Collected:11/09/19 13:00 Received:11/11/19 13:43 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 1.36 mg/kg 11/15/19 20:50 7440-38-211/14/19 15:310.653 0.163 5
Barium 35.3 mg/kg 11/15/19 20:50 7440-39-311/14/19 15:311.31 0.209 5
Cadmium ND mg/kg 11/15/19 20:50 7440-43-911/14/19 15:310.653 0.104 5
Chromium 30.6 mg/kg 11/15/19 20:50 7440-47-311/14/19 15:311.31 0.353 5
Lead 7.51 mg/kg 11/15/19 20:50 7439-92-111/14/19 15:310.653 0.157 5
Selenium 0.781 mg/kg 11/15/19 20:50 7782-49-211/14/19 15:310.653 0.248 5
Silver ND mg/kg 11/15/19 20:50 7440-22-411/14/19 15:310.653 0.202 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.0692 mg/kg 11/14/19 12:31 7439-97-611/13/19 21:480.0392 0.00366 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 11/14/19 17:47 83-32-911/12/19 11:344301111
Acenaphthylene ND ug/kg 11/14/19 17:47 208-96-811/12/19 11:344301021
Aniline ND ug/kg 11/14/19 17:47 62-53-311/12/19 11:3443096.6 1
Anthracene ND ug/kg 11/14/19 17:47 120-12-711/12/19 11:344301121
Benzo(a)anthracene ND ug/kg 11/14/19 17:47 56-55-311/12/19 11:344301371
Benzo(a)pyrene ND ug/kg 11/14/19 17:47 50-32-811/12/19 11:344301861
Benzo(b)fluoranthene ND ug/kg 11/14/19 17:47 205-99-211/12/19 11:344301731
Benzo(g,h,i)perylene ND ug/kg 11/14/19 17:47 191-24-211/12/19 11:344301681
Benzo(k)fluoranthene ND ug/kg 11/14/19 17:47 207-08-911/12/19 11:344301811
Benzoic Acid ND ug/kg 11/14/19 17:47 65-85-011/12/19 11:3421504641
Benzyl alcohol ND ug/kg 11/14/19 17:47 100-51-611/12/19 11:348602281
4-Bromophenylphenyl ether ND ug/kg 11/14/19 17:47 101-55-311/12/19 11:344301131
Butylbenzylphthalate ND ug/kg 11/14/19 17:47 85-68-711/12/19 11:344301151
4-Chloro-3-methylphenol ND ug/kg 11/14/19 17:47 59-50-711/12/19 11:348602621
4-Chloroaniline ND ug/kg 11/14/19 17:47 106-47-811/12/19 11:3421502631
bis(2-Chloroethoxy)methane ND ug/kg 11/14/19 17:47 111-91-111/12/19 11:344301151
bis(2-Chloroethyl) ether ND ug/kg 11/14/19 17:47 111-44-411/12/19 11:3443091.4 1
2-Chloronaphthalene ND ug/kg 11/14/19 17:47 91-58-711/12/19 11:3443095.8 1
2-Chlorophenol ND ug/kg 11/14/19 17:47 95-57-811/12/19 11:344301001
4-Chlorophenylphenyl ether ND ug/kg 11/14/19 17:47 7005-72-311/12/19 11:344301121
Chrysene ND ug/kg 11/14/19 17:47 218-01-911/12/19 11:344301251
Dibenz(a,h)anthracene ND ug/kg 11/14/19 17:47 53-70-311/12/19 11:344301721
Dibenzofuran ND ug/kg 11/14/19 17:47 132-64-911/12/19 11:344301081
1,2-Dichlorobenzene ND ug/kg 11/14/19 17:47 95-50-111/12/19 11:3443093.1 1
1,3-Dichlorobenzene ND ug/kg 11/14/19 17:47 541-73-111/12/19 11:3443096.8 1
1,4-Dichlorobenzene ND ug/kg 11/14/19 17:47 106-46-711/12/19 11:3443094.6 1
3,3'-Dichlorobenzidine ND ug/kg 11/14/19 17:47 91-94-111/12/19 11:3421503001
2,4-Dichlorophenol ND ug/kg 11/14/19 17:47 120-83-211/12/19 11:344301421
Diethylphthalate ND ug/kg 11/14/19 17:47 84-66-211/12/19 11:3443093.3 1
2,4-Dimethylphenol ND ug/kg 11/14/19 17:47 105-67-911/12/19 11:344301071
Dimethylphthalate ND ug/kg 11/14/19 17:47 131-11-311/12/19 11:3443097.2 1
Di-n-butylphthalate ND ug/kg 11/14/19 17:47 84-74-211/12/19 11:344301061
4,6-Dinitro-2-methylphenol ND ug/kg 11/14/19 17:47 534-52-111/12/19 11:348606931
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453170
LEH-004
Sample:SB-11 Lab ID:92453170001 Collected:11/09/19 13:00 Received:11/11/19 13:43 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 11/14/19 17:47 51-28-511/12/19 11:34215013701
2,4-Dinitrotoluene ND ug/kg 11/14/19 17:47 121-14-211/12/19 11:344301141
2,6-Dinitrotoluene ND ug/kg 11/14/19 17:47 606-20-211/12/19 11:344301121
Di-n-octylphthalate ND ug/kg 11/14/19 17:47 117-84-011/12/19 11:344302451
bis(2-Ethylhexyl)phthalate ND ug/kg 11/14/19 17:47 117-81-711/12/19 11:344301411
Fluoranthene ND ug/kg 11/14/19 17:47 206-44-011/12/19 11:344301301
Fluorene ND ug/kg 11/14/19 17:47 86-73-711/12/19 11:344301151
Hexachloro-1,3-butadiene ND ug/kg 11/14/19 17:47 87-68-311/12/19 11:344301051
Hexachlorobenzene ND ug/kg 11/14/19 17:47 118-74-111/12/19 11:344301091
Hexachlorocyclopentadiene ND ug/kg 11/14/19 17:47 77-47-411/12/19 11:344301721
Hexachloroethane ND ug/kg 11/14/19 17:47 67-72-111/12/19 11:3443098.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 11/14/19 17:47 193-39-511/12/19 11:344301971
Isophorone ND ug/kg 11/14/19 17:47 78-59-111/12/19 11:3443093.5 1
1-Methylnaphthalene ND ug/kg 11/14/19 17:47 90-12-011/12/19 11:344301151
2-Methylnaphthalene ND ug/kg 11/14/19 17:47 91-57-611/12/19 11:344301091
2-Methylphenol(o-Cresol)ND ug/kg 11/14/19 17:47 95-48-711/12/19 11:3443095.3 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/14/19 17:47 15831-10-411/12/19 11:344301081
Naphthalene ND ug/kg 11/14/19 17:47 91-20-311/12/19 11:344301031
2-Nitroaniline ND ug/kg 11/14/19 17:47 88-74-411/12/19 11:3421502161
3-Nitroaniline ND ug/kg 11/14/19 17:47 99-09-211/12/19 11:3421502281
4-Nitroaniline ND ug/kg 11/14/19 17:47 100-01-611/12/19 11:348602121
Nitrobenzene ND ug/kg 11/14/19 17:47 98-95-311/12/19 11:344301031
2-Nitrophenol ND ug/kg 11/14/19 17:47 88-75-511/12/19 11:344301331
4-Nitrophenol ND ug/kg 11/14/19 17:47 100-02-711/12/19 11:3421506861
N-Nitrosodimethylamine ND ug/kg 11/14/19 17:47 62-75-911/12/19 11:344301211
N-Nitroso-di-n-propylamine ND ug/kg 11/14/19 17:47 621-64-711/12/19 11:344301201
N-Nitrosodiphenylamine ND ug/kg 11/14/19 17:47 86-30-611/12/19 11:344301101
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/14/19 17:47 108-60-111/12/19 11:344301201
Pentachlorophenol ND ug/kg 11/14/19 17:47 87-86-511/12/19 11:3421501971
Phenanthrene ND ug/kg 11/14/19 17:47 85-01-811/12/19 11:344301081
Phenol ND ug/kg 11/14/19 17:47 108-95-211/12/19 11:344301031
Pyrene ND ug/kg 11/14/19 17:47 129-00-011/12/19 11:344301181
Pyridine ND ug/kg 11/14/19 17:47 110-86-111/12/19 11:344301091
1,2,4-Trichlorobenzene ND ug/kg 11/14/19 17:47 120-82-111/12/19 11:3443098.5 1
2,4,5-Trichlorophenol ND ug/kg 11/14/19 17:47 95-95-411/12/19 11:344301121
2,4,6-Trichlorophenol ND ug/kg 11/14/19 17:47 88-06-211/12/19 11:344301081
Surrogates
Nitrobenzene-d5 (S)69 %11/14/19 17:47 4165-60-011/12/19 11:3423-110 1
2-Fluorobiphenyl (S)68 %11/14/19 17:47 321-60-811/12/19 11:3430-110 1
Terphenyl-d14 (S)78 %11/14/19 17:47 1718-51-011/12/19 11:3428-110 1
Phenol-d6 (S)64 %11/14/19 17:47 13127-88-311/12/19 11:3422-110 1
2-Fluorophenol (S)65 %11/14/19 17:47 367-12-411/12/19 11:3413-110 1
2,4,6-Tribromophenol (S)84 %11/14/19 17:47 118-79-611/12/19 11:3427-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453170
LEH-004
Sample:SB-11 Lab ID:92453170001 Collected:11/09/19 13:00 Received:11/11/19 13:43 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 18.5J ug/kg 11/15/19 14:02 67-64-111/15/19 11:4712712.0 1
Benzene ND ug/kg 11/15/19 14:02 71-43-211/15/19 11:476.4 1.1 1
Bromobenzene ND ug/kg 11/15/19 14:02 108-86-111/15/19 11:476.4 1.7 1
Bromochloromethane ND ug/kg 11/15/19 14:02 74-97-511/15/19 11:476.4 1.6 1
Bromodichloromethane ND ug/kg 11/15/19 14:02 75-27-411/15/19 11:476.4 1.2 1
Bromoform ND ug/kg 11/15/19 14:02 75-25-211/15/19 11:476.4 3.1 1
Bromomethane ND ug/kg 11/15/19 14:02 74-83-911/15/19 11:4712.7 3.0 1
2-Butanone (MEK)ND ug/kg 11/15/19 14:02 78-93-311/15/19 11:4712715.1 1
n-Butylbenzene ND ug/kg 11/15/19 14:02 104-51-811/15/19 11:476.4 3.6 1
sec-Butylbenzene ND ug/kg 11/15/19 14:02 135-98-811/15/19 11:476.4 2.7 1
tert-Butylbenzene ND ug/kg 11/15/19 14:02 98-06-611/15/19 11:476.4 2.1 1
Carbon tetrachloride ND ug/kg 11/15/19 14:02 56-23-511/15/19 11:476.4 1.2 1
Chlorobenzene ND ug/kg 11/15/19 14:02 108-90-711/15/19 11:476.4 1.2 1
Chloroethane ND ug/kg 11/15/19 14:02 75-00-311/15/19 11:4712.7 2.7 1
Chloroform ND ug/kg 11/15/19 14:02 67-66-311/15/19 11:476.4 1.3 1
Chloromethane ND ug/kg 11/15/19 14:02 74-87-311/15/19 11:4712.7 4.2 1
2-Chlorotoluene ND ug/kg 11/15/19 14:02 95-49-811/15/19 11:476.4 1.9 1
4-Chlorotoluene ND ug/kg 11/15/19 14:02 106-43-411/15/19 11:476.4 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/15/19 14:02 96-12-811/15/19 11:476.4 3.2 1
Dibromochloromethane ND ug/kg 11/15/19 14:02 124-48-111/15/19 11:476.4 3.2 1
1,2-Dibromoethane (EDB)ND ug/kg 11/15/19 14:02 106-93-411/15/19 11:476.4 1.4 1
Dibromomethane ND ug/kg 11/15/19 14:02 74-95-311/15/19 11:476.4 1.9 1
1,2-Dichlorobenzene ND ug/kg 11/15/19 14:02 95-50-111/15/19 11:476.4 2.2 1
1,3-Dichlorobenzene ND ug/kg 11/15/19 14:02 541-73-111/15/19 11:476.4 2.3 1
1,4-Dichlorobenzene ND ug/kg 11/15/19 14:02 106-46-711/15/19 11:476.4 2.2 1
Dichlorodifluoromethane ND ug/kg 11/15/19 14:02 75-71-811/15/19 11:4712.7 5.2 1
1,1-Dichloroethane ND ug/kg 11/15/19 14:02 75-34-311/15/19 11:476.4 0.93 1
1,2-Dichloroethane ND ug/kg 11/15/19 14:02 107-06-211/15/19 11:476.4 1.3 1
1,1-Dichloroethene ND ug/kg 11/15/19 14:02 75-35-411/15/19 11:476.4 1.5 1
cis-1,2-Dichloroethene ND ug/kg 11/15/19 14:02 156-59-211/15/19 11:476.4 1.1 1
trans-1,2-Dichloroethene ND ug/kg 11/15/19 14:02 156-60-511/15/19 11:476.4 1.2 1
1,2-Dichloropropane ND ug/kg 11/15/19 14:02 78-87-511/15/19 11:476.4 2.4 1
1,3-Dichloropropane ND ug/kg 11/15/19 14:02 142-28-911/15/19 11:476.4 2.4 1
2,2-Dichloropropane ND ug/kg 11/15/19 14:02 594-20-711/15/19 11:476.4 0.63 1
1,1-Dichloropropene ND ug/kg 11/15/19 14:02 563-58-611/15/19 11:476.4 2.7 1
cis-1,3-Dichloropropene ND ug/kg 11/15/19 14:02 10061-01-511/15/19 11:476.4 2.9 1
trans-1,3-Dichloropropene ND ug/kg 11/15/19 14:02 10061-02-611/15/19 11:476.4 1.1 1
Diisopropyl ether ND ug/kg 11/15/19 14:02 108-20-311/15/19 11:476.4 3.6 1
Ethylbenzene ND ug/kg 11/15/19 14:02 100-41-411/15/19 11:476.4 1.3 1
Hexachloro-1,3-butadiene ND ug/kg 11/15/19 14:02 87-68-311/15/19 11:476.4 3.1 1
2-Hexanone ND ug/kg 11/15/19 14:02 591-78-611/15/19 11:4763.6 6.6 1
Isopropylbenzene (Cumene)ND ug/kg 11/15/19 14:02 98-82-811/15/19 11:476.4 1.8 1
p-Isopropyltoluene ND ug/kg 11/15/19 14:02 99-87-611/15/19 11:476.4 3.1 1
Methylene Chloride ND ug/kg 11/15/19 14:02 75-09-211/15/19 11:4725.4 7.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/15/19 14:02 108-10-111/15/19 11:4763.6 4.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453170
LEH-004
Sample:SB-11 Lab ID:92453170001 Collected:11/09/19 13:00 Received:11/11/19 13:43 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 11/15/19 14:02 1634-04-411/15/19 11:476.4 3.6 1
Naphthalene ND ug/kg 11/15/19 14:02 91-20-311/15/19 11:476.4 5.4 1
n-Propylbenzene ND ug/kg 11/15/19 14:02 103-65-111/15/19 11:476.4 2.1 1
Styrene ND ug/kg 11/15/19 14:02 100-42-511/15/19 11:476.4 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/15/19 14:02 630-20-611/15/19 11:476.4 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/15/19 14:02 79-34-511/15/19 11:476.4 2.2 1
Tetrachloroethene ND ug/kg 11/15/19 14:02 127-18-411/15/19 11:476.4 2.0 1
Toluene ND ug/kg 11/15/19 14:02 108-88-311/15/19 11:476.4 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 11/15/19 14:02 87-61-611/15/19 11:476.4 4.5 1
1,2,4-Trichlorobenzene ND ug/kg 11/15/19 14:02 120-82-111/15/19 11:476.4 3.4 1
1,1,1-Trichloroethane ND ug/kg 11/15/19 14:02 71-55-611/15/19 11:476.4 1.1 1
1,1,2-Trichloroethane ND ug/kg 11/15/19 14:02 79-00-511/15/19 11:476.4 1.4 1
Trichloroethene ND ug/kg 11/15/19 14:02 79-01-611/15/19 11:476.4 1.7 1
Trichlorofluoromethane ND ug/kg 11/15/19 14:02 75-69-411/15/19 11:476.4 1.5 1
1,2,3-Trichloropropane ND ug/kg 11/15/19 14:02 96-18-411/15/19 11:476.4 2.1 1
1,2,4-Trimethylbenzene ND ug/kg 11/15/19 14:02 95-63-611/15/19 11:476.4 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 11/15/19 14:02 108-67-811/15/19 11:476.4 2.1 1
Vinyl acetate ND ug/kg 11/15/19 14:02 108-05-411/15/19 11:4763.6 20.7 1
Vinyl chloride ND ug/kg 11/15/19 14:02 75-01-411/15/19 11:4712.7 2.4 1
Xylene (Total)ND ug/kg 11/15/19 14:02 1330-20-711/15/19 11:4712.7 4.5 1
m&p-Xylene ND ug/kg 11/15/19 14:02 179601-23-111/15/19 11:4712.7 3.0 1
o-Xylene ND ug/kg 11/15/19 14:02 95-47-611/15/19 11:476.4 1.5 1
Surrogates
Toluene-d8 (S)111 %11/15/19 14:02 2037-26-511/15/19 11:4770-130 1
4-Bromofluorobenzene (S)104 %11/15/19 14:02 460-00-411/15/19 11:4770-130 1
1,2-Dichloroethane-d4 (S)88 %11/15/19 14:02 17060-07-011/15/19 11:4770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.5 %11/12/19 15:020.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 76.6 %11/16/19 13:0111/16/19 12:511
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 11/15/19 18:40 18540-29-911/15/19 13:401.31 0.333 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453170
LEH-004
Sample:SB-12 Lab ID:92453170002 Collected:11/09/19 12:50 Received:11/11/19 13:43 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 2.07 mg/kg 11/15/19 20:54 7440-38-211/14/19 15:310.679 0.170 5
Barium 48.6 mg/kg 11/15/19 20:54 7440-39-311/14/19 15:311.36 0.217 5
Cadmium ND mg/kg 11/15/19 20:54 7440-43-911/14/19 15:310.679 0.109 5
Chromium 44.1 mg/kg 11/15/19 20:54 7440-47-311/14/19 15:311.36 0.367 5
Lead 12.9 mg/kg 11/15/19 20:54 7439-92-111/14/19 15:310.679 0.163 5
Selenium 0.896 mg/kg 11/15/19 20:54 7782-49-211/14/19 15:310.679 0.258 5
Silver ND mg/kg 11/15/19 20:54 7440-22-411/14/19 15:310.679 0.210 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.167 mg/kg 11/14/19 12:34 7439-97-611/13/19 21:480.0407 0.00380 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 11/14/19 18:21 83-32-911/12/19 11:344221091
Acenaphthylene ND ug/kg 11/14/19 18:21 208-96-811/12/19 11:3442299.9 1
Aniline ND ug/kg 11/14/19 18:21 62-53-311/12/19 11:3442294.7 1
Anthracene ND ug/kg 11/14/19 18:21 120-12-711/12/19 11:344221091
Benzo(a)anthracene ND ug/kg 11/14/19 18:21 56-55-311/12/19 11:344221341
Benzo(a)pyrene ND ug/kg 11/14/19 18:21 50-32-811/12/19 11:344221831
Benzo(b)fluoranthene ND ug/kg 11/14/19 18:21 205-99-211/12/19 11:344221701
Benzo(g,h,i)perylene ND ug/kg 11/14/19 18:21 191-24-211/12/19 11:344221651
Benzo(k)fluoranthene ND ug/kg 11/14/19 18:21 207-08-911/12/19 11:344221781
Benzoic Acid ND ug/kg 11/14/19 18:21 65-85-011/12/19 11:3421104551
Benzyl alcohol ND ug/kg 11/14/19 18:21 100-51-611/12/19 11:348442241
4-Bromophenylphenyl ether ND ug/kg 11/14/19 18:21 101-55-311/12/19 11:344221111
Butylbenzylphthalate ND ug/kg 11/14/19 18:21 85-68-711/12/19 11:344221121
4-Chloro-3-methylphenol ND ug/kg 11/14/19 18:21 59-50-711/12/19 11:348442571
4-Chloroaniline ND ug/kg 11/14/19 18:21 106-47-811/12/19 11:3421102581
bis(2-Chloroethoxy)methane ND ug/kg 11/14/19 18:21 111-91-111/12/19 11:344221131
bis(2-Chloroethyl) ether ND ug/kg 11/14/19 18:21 111-44-411/12/19 11:3442289.6 1
2-Chloronaphthalene ND ug/kg 11/14/19 18:21 91-58-711/12/19 11:3442294.0 1
2-Chlorophenol ND ug/kg 11/14/19 18:21 95-57-811/12/19 11:3442298.2 1
4-Chlorophenylphenyl ether ND ug/kg 11/14/19 18:21 7005-72-311/12/19 11:344221101
Chrysene ND ug/kg 11/14/19 18:21 218-01-911/12/19 11:344221221
Dibenz(a,h)anthracene ND ug/kg 11/14/19 18:21 53-70-311/12/19 11:344221691
Dibenzofuran ND ug/kg 11/14/19 18:21 132-64-911/12/19 11:344221051
1,2-Dichlorobenzene ND ug/kg 11/14/19 18:21 95-50-111/12/19 11:3442291.3 1
1,3-Dichlorobenzene ND ug/kg 11/14/19 18:21 541-73-111/12/19 11:3442295.0 1
1,4-Dichlorobenzene ND ug/kg 11/14/19 18:21 106-46-711/12/19 11:3442292.8 1
3,3'-Dichlorobenzidine ND ug/kg 11/14/19 18:21 91-94-111/12/19 11:3421102941
2,4-Dichlorophenol ND ug/kg 11/14/19 18:21 120-83-211/12/19 11:344221391
Diethylphthalate ND ug/kg 11/14/19 18:21 84-66-211/12/19 11:3442291.5 1
2,4-Dimethylphenol ND ug/kg 11/14/19 18:21 105-67-911/12/19 11:344221051
Dimethylphthalate ND ug/kg 11/14/19 18:21 131-11-311/12/19 11:3442295.4 1
Di-n-butylphthalate ND ug/kg 11/14/19 18:21 84-74-211/12/19 11:344221041
4,6-Dinitro-2-methylphenol ND ug/kg 11/14/19 18:21 534-52-111/12/19 11:348446801
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453170
LEH-004
Sample:SB-12 Lab ID:92453170002 Collected:11/09/19 12:50 Received:11/11/19 13:43 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 11/14/19 18:21 51-28-511/12/19 11:34211013501
2,4-Dinitrotoluene ND ug/kg 11/14/19 18:21 121-14-211/12/19 11:344221121
2,6-Dinitrotoluene ND ug/kg 11/14/19 18:21 606-20-211/12/19 11:344221101
Di-n-octylphthalate ND ug/kg 11/14/19 18:21 117-84-011/12/19 11:344222401
bis(2-Ethylhexyl)phthalate ND ug/kg 11/14/19 18:21 117-81-711/12/19 11:344221381
Fluoranthene ND ug/kg 11/14/19 18:21 206-44-011/12/19 11:344221271
Fluorene ND ug/kg 11/14/19 18:21 86-73-711/12/19 11:344221131
Hexachloro-1,3-butadiene ND ug/kg 11/14/19 18:21 87-68-311/12/19 11:344221031
Hexachlorobenzene ND ug/kg 11/14/19 18:21 118-74-111/12/19 11:344221071
Hexachlorocyclopentadiene ND ug/kg 11/14/19 18:21 77-47-411/12/19 11:344221691
Hexachloroethane ND ug/kg 11/14/19 18:21 67-72-111/12/19 11:3442296.1 1
Indeno(1,2,3-cd)pyrene ND ug/kg 11/14/19 18:21 193-39-511/12/19 11:344221931
Isophorone ND ug/kg 11/14/19 18:21 78-59-111/12/19 11:3442291.7 1
1-Methylnaphthalene ND ug/kg 11/14/19 18:21 90-12-011/12/19 11:344221121
2-Methylnaphthalene ND ug/kg 11/14/19 18:21 91-57-611/12/19 11:344221071
2-Methylphenol(o-Cresol)ND ug/kg 11/14/19 18:21 95-48-711/12/19 11:3442293.5 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 11/14/19 18:21 15831-10-411/12/19 11:344221061
Naphthalene ND ug/kg 11/14/19 18:21 91-20-311/12/19 11:344221011
2-Nitroaniline ND ug/kg 11/14/19 18:21 88-74-411/12/19 11:3421102121
3-Nitroaniline ND ug/kg 11/14/19 18:21 99-09-211/12/19 11:3421102241
4-Nitroaniline ND ug/kg 11/14/19 18:21 100-01-611/12/19 11:348442081
Nitrobenzene ND ug/kg 11/14/19 18:21 98-95-311/12/19 11:344221011
2-Nitrophenol ND ug/kg 11/14/19 18:21 88-75-511/12/19 11:344221301
4-Nitrophenol ND ug/kg 11/14/19 18:21 100-02-711/12/19 11:3421106721
N-Nitrosodimethylamine ND ug/kg 11/14/19 18:21 62-75-911/12/19 11:344221191
N-Nitroso-di-n-propylamine ND ug/kg 11/14/19 18:21 621-64-711/12/19 11:344221181
N-Nitrosodiphenylamine ND ug/kg 11/14/19 18:21 86-30-611/12/19 11:344221081
2,2'-Oxybis(1-chloropropane)ND ug/kg 11/14/19 18:21 108-60-111/12/19 11:344221171
Pentachlorophenol ND ug/kg 11/14/19 18:21 87-86-511/12/19 11:3421101931
Phenanthrene ND ug/kg 11/14/19 18:21 85-01-811/12/19 11:344221061
Phenol ND ug/kg 11/14/19 18:21 108-95-211/12/19 11:344221011
Pyrene ND ug/kg 11/14/19 18:21 129-00-011/12/19 11:344221161
Pyridine ND ug/kg 11/14/19 18:21 110-86-111/12/19 11:344221071
1,2,4-Trichlorobenzene ND ug/kg 11/14/19 18:21 120-82-111/12/19 11:3442296.7 1
2,4,5-Trichlorophenol ND ug/kg 11/14/19 18:21 95-95-411/12/19 11:344221101
2,4,6-Trichlorophenol ND ug/kg 11/14/19 18:21 88-06-211/12/19 11:344221061
Surrogates
Nitrobenzene-d5 (S)75 %11/14/19 18:21 4165-60-011/12/19 11:3423-110 1
2-Fluorobiphenyl (S)73 %11/14/19 18:21 321-60-811/12/19 11:3430-110 1
Terphenyl-d14 (S)81 %11/14/19 18:21 1718-51-011/12/19 11:3428-110 1
Phenol-d6 (S)71 %11/14/19 18:21 13127-88-311/12/19 11:3422-110 1
2-Fluorophenol (S)70 %11/14/19 18:21 367-12-411/12/19 11:3413-110 1
2,4,6-Tribromophenol (S)85 %11/14/19 18:21 118-79-611/12/19 11:3427-110 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
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Page 10 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453170
LEH-004
Sample:SB-12 Lab ID:92453170002 Collected:11/09/19 12:50 Received:11/11/19 13:43 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 39.3J ug/kg 11/15/19 14:28 67-64-111/15/19 11:4712011.3 1
Benzene ND ug/kg 11/15/19 14:28 71-43-211/15/19 11:476.0 1.1 1
Bromobenzene ND ug/kg 11/15/19 14:28 108-86-111/15/19 11:476.0 1.6 1
Bromochloromethane ND ug/kg 11/15/19 14:28 74-97-511/15/19 11:476.0 1.5 1
Bromodichloromethane ND ug/kg 11/15/19 14:28 75-27-411/15/19 11:476.0 1.2 1
Bromoform ND ug/kg 11/15/19 14:28 75-25-211/15/19 11:476.0 2.9 1
Bromomethane ND ug/kg 11/15/19 14:28 74-83-911/15/19 11:4712.0 2.8 1
2-Butanone (MEK)ND ug/kg 11/15/19 14:28 78-93-311/15/19 11:4712014.3 1
n-Butylbenzene ND ug/kg 11/15/19 14:28 104-51-811/15/19 11:476.0 3.4 1
sec-Butylbenzene ND ug/kg 11/15/19 14:28 135-98-811/15/19 11:476.0 2.5 1
tert-Butylbenzene ND ug/kg 11/15/19 14:28 98-06-611/15/19 11:476.0 2.0 1
Carbon tetrachloride ND ug/kg 11/15/19 14:28 56-23-511/15/19 11:476.0 1.1 1
Chlorobenzene ND ug/kg 11/15/19 14:28 108-90-711/15/19 11:476.0 1.2 1
Chloroethane ND ug/kg 11/15/19 14:28 75-00-311/15/19 11:4712.0 2.5 1
Chloroform ND ug/kg 11/15/19 14:28 67-66-311/15/19 11:476.0 1.3 1
Chloromethane ND ug/kg 11/15/19 14:28 74-87-311/15/19 11:4712.0 3.9 1
2-Chlorotoluene ND ug/kg 11/15/19 14:28 95-49-811/15/19 11:476.0 1.8 1
4-Chlorotoluene ND ug/kg 11/15/19 14:28 106-43-411/15/19 11:476.0 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 11/15/19 14:28 96-12-811/15/19 11:476.0 3.0 1
Dibromochloromethane ND ug/kg 11/15/19 14:28 124-48-111/15/19 11:476.0 3.0 1
1,2-Dibromoethane (EDB)ND ug/kg 11/15/19 14:28 106-93-411/15/19 11:476.0 1.3 1
Dibromomethane ND ug/kg 11/15/19 14:28 74-95-311/15/19 11:476.0 1.8 1
1,2-Dichlorobenzene ND ug/kg 11/15/19 14:28 95-50-111/15/19 11:476.0 2.1 1
1,3-Dichlorobenzene ND ug/kg 11/15/19 14:28 541-73-111/15/19 11:476.0 2.1 1
1,4-Dichlorobenzene ND ug/kg 11/15/19 14:28 106-46-711/15/19 11:476.0 2.1 1
Dichlorodifluoromethane ND ug/kg 11/15/19 14:28 75-71-811/15/19 11:4712.0 4.9 1
1,1-Dichloroethane ND ug/kg 11/15/19 14:28 75-34-311/15/19 11:476.0 0.88 1
1,2-Dichloroethane ND ug/kg 11/15/19 14:28 107-06-211/15/19 11:476.0 1.2 1
1,1-Dichloroethene ND ug/kg 11/15/19 14:28 75-35-411/15/19 11:476.0 1.4 1
cis-1,2-Dichloroethene ND ug/kg 11/15/19 14:28 156-59-211/15/19 11:476.0 1.0 1
trans-1,2-Dichloroethene ND ug/kg 11/15/19 14:28 156-60-511/15/19 11:476.0 1.2 1
1,2-Dichloropropane ND ug/kg 11/15/19 14:28 78-87-511/15/19 11:476.0 2.3 1
1,3-Dichloropropane ND ug/kg 11/15/19 14:28 142-28-911/15/19 11:476.0 2.3 1
2,2-Dichloropropane ND ug/kg 11/15/19 14:28 594-20-711/15/19 11:476.0 0.59 1
1,1-Dichloropropene ND ug/kg 11/15/19 14:28 563-58-611/15/19 11:476.0 2.5 1
cis-1,3-Dichloropropene ND ug/kg 11/15/19 14:28 10061-01-511/15/19 11:476.0 2.7 1
trans-1,3-Dichloropropene ND ug/kg 11/15/19 14:28 10061-02-611/15/19 11:476.0 1.0 1
Diisopropyl ether ND ug/kg 11/15/19 14:28 108-20-311/15/19 11:476.0 3.4 1
Ethylbenzene ND ug/kg 11/15/19 14:28 100-41-411/15/19 11:476.0 1.3 1
Hexachloro-1,3-butadiene ND ug/kg 11/15/19 14:28 87-68-311/15/19 11:476.0 3.0 1
2-Hexanone ND ug/kg 11/15/19 14:28 591-78-611/15/19 11:4760.0 6.2 1
Isopropylbenzene (Cumene)ND ug/kg 11/15/19 14:28 98-82-811/15/19 11:476.0 1.7 1
p-Isopropyltoluene ND ug/kg 11/15/19 14:28 99-87-611/15/19 11:476.0 2.9 1
Methylene Chloride ND ug/kg 11/15/19 14:28 75-09-211/15/19 11:4724.0 7.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 11/15/19 14:28 108-10-111/15/19 11:4760.0 4.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 11 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453170
LEH-004
Sample:SB-12 Lab ID:92453170002 Collected:11/09/19 12:50 Received:11/11/19 13:43 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 11/15/19 14:28 1634-04-411/15/19 11:476.0 3.4 1
Naphthalene ND ug/kg 11/15/19 14:28 91-20-311/15/19 11:476.0 5.1 1
n-Propylbenzene ND ug/kg 11/15/19 14:28 103-65-111/15/19 11:476.0 2.0 1
Styrene ND ug/kg 11/15/19 14:28 100-42-511/15/19 11:476.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 11/15/19 14:28 630-20-611/15/19 11:476.0 1.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 11/15/19 14:28 79-34-511/15/19 11:476.0 2.1 1
Tetrachloroethene ND ug/kg 11/15/19 14:28 127-18-411/15/19 11:476.0 1.9 1
Toluene ND ug/kg 11/15/19 14:28 108-88-311/15/19 11:476.0 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 11/15/19 14:28 87-61-611/15/19 11:476.0 4.3 1
1,2,4-Trichlorobenzene ND ug/kg 11/15/19 14:28 120-82-111/15/19 11:476.0 3.2 1
1,1,1-Trichloroethane ND ug/kg 11/15/19 14:28 71-55-611/15/19 11:476.0 1.0 1
1,1,2-Trichloroethane ND ug/kg 11/15/19 14:28 79-00-511/15/19 11:476.0 1.4 1
Trichloroethene ND ug/kg 11/15/19 14:28 79-01-611/15/19 11:476.0 1.6 1
Trichlorofluoromethane ND ug/kg 11/15/19 14:28 75-69-411/15/19 11:476.0 1.4 1
1,2,3-Trichloropropane ND ug/kg 11/15/19 14:28 96-18-411/15/19 11:476.0 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 11/15/19 14:28 95-63-611/15/19 11:476.0 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 11/15/19 14:28 108-67-811/15/19 11:476.0 2.0 1
Vinyl acetate ND ug/kg 11/15/19 14:28 108-05-411/15/19 11:4760.0 19.5 1
Vinyl chloride ND ug/kg 11/15/19 14:28 75-01-411/15/19 11:4712.0 2.3 1
Xylene (Total)ND ug/kg 11/15/19 14:28 1330-20-711/15/19 11:4712.0 4.2 1
m&p-Xylene ND ug/kg 11/15/19 14:28 179601-23-111/15/19 11:4712.0 2.8 1
o-Xylene ND ug/kg 11/15/19 14:28 95-47-611/15/19 11:476.0 1.4 1
Surrogates
Toluene-d8 (S)108 %11/15/19 14:28 2037-26-511/15/19 11:4770-130 1
4-Bromofluorobenzene (S)104 %11/15/19 14:28 460-00-411/15/19 11:4770-130 1
1,2-Dichloroethane-d4 (S)88 %11/15/19 14:28 17060-07-011/15/19 11:4770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.1 %11/12/19 15:020.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 73.7 %11/16/19 13:0111/16/19 12:511
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 11/15/19 18:45 18540-29-911/15/19 13:401.36 0.346 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1380473
3050B
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples:92453170001, 92453170002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3472556-1
Associated Lab Samples:92453170001, 92453170002
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 0.500 11/15/19 19:340.125
Barium mg/kg 0.227J 1.00 J11/15/19 19:340.160
Cadmium mg/kg ND 0.500 11/15/19 19:340.0800
Chromium mg/kg ND 1.00 11/15/19 19:340.270
Lead mg/kg 0.152J 0.500 J11/15/19 19:340.120
Selenium mg/kg ND 0.500 11/15/19 19:340.190
Silver mg/kg ND 0.500 11/15/19 19:340.155
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3472556-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3472556-3
Arsenic mg/kg 96.0100 96.0 80.0-12093.093.0 3.19 20
Barium mg/kg 98.2100 98.2 80.0-12096.096.0 2.32 20
Cadmium mg/kg 101100 101 80.0-12099.599.5 1.95 20
Chromium mg/kg 103100 103 80.0-12098.098.0 4.50 20
Lead mg/kg 99.2100 99.2 80.0-12097.497.4 1.90 20
Selenium mg/kg 99.8100 99.8 80.0-12098.698.6 1.18 20
Silver mg/kg 20.020.0 99.9 80.0-12098.019.6 1.91 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3472556-6MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1159327-18
R3472556-7
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 20.0 88.8 75.0-12585.7 3.36 2020.05.73 94.5 91.4
Barium mg/kg 20.0 108 75.0-12584.4 7.71 2020.0206 314 291
Cadmium mg/kg 20.0 103 75.0-12598.3 5.07 2020.0ND 103 98.4
Chromium mg/kg 20.0 98.6 75.0-12595.3 2.63 2020.027.9 126 123
Lead mg/kg ML20.0 16.4 75.0-12560.3 12.1 2020.0325 341 385
Selenium mg/kg 20.0 101 75.0-12593.9 6.87 2020.00.525 101 94.5
Silver mg/kg 4.00 101 75.0-12593.3 7.80 204.00ND 20.3 18.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1380193
7471A
EPA 7471B
Mercury 7471B
Associated Lab Samples:92453170001, 92453170002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3471945-1
Associated Lab Samples:92453170001, 92453170002
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0300 11/14/19 11:460.00280
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3471945-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3471945-3
Mercury mg/kg 0.5420.500 108 80.0-1201060.529 2.43 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3471945-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1159312-01
R3471945-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg MH0.500 122 75.0-125129 3.54 200.5000.279 0.890 0.922
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
509780
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92453170001, 92453170002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2735758
Associated Lab Samples:92453170001, 92453170002
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 11/15/19 12:461.2
1,1,1-Trichloroethane ug/kg ND 5.0 11/15/19 12:460.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 11/15/19 12:461.7
1,1,2-Trichloroethane ug/kg ND 5.0 11/15/19 12:461.1
1,1-Dichloroethane ug/kg ND 5.0 11/15/19 12:460.74
1,1-Dichloroethene ug/kg ND 5.0 11/15/19 12:461.2
1,1-Dichloropropene ug/kg ND 5.0 11/15/19 12:462.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 11/15/19 12:463.6
1,2,3-Trichloropropane ug/kg ND 5.0 11/15/19 12:461.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 11/15/19 12:462.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 11/15/19 12:462.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 11/15/19 12:462.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 11/15/19 12:461.1
1,2-Dichlorobenzene ug/kg ND 5.0 11/15/19 12:461.8
1,2-Dichloroethane ug/kg ND 5.0 11/15/19 12:461.0
1,2-Dichloropropane ug/kg ND 5.0 11/15/19 12:461.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 11/15/19 12:461.7
1,3-Dichlorobenzene ug/kg ND 5.0 11/15/19 12:461.8
1,3-Dichloropropane ug/kg ND 5.0 11/15/19 12:461.9
1,4-Dichlorobenzene ug/kg ND 5.0 11/15/19 12:461.7
2,2-Dichloropropane ug/kg ND 5.0 11/15/19 12:460.49
2-Butanone (MEK)ug/kg ND 100 11/15/19 12:4611.9
2-Chlorotoluene ug/kg ND 5.0 11/15/19 12:461.5
2-Hexanone ug/kg ND 50.0 11/15/19 12:465.2
4-Chlorotoluene ug/kg ND 5.0 11/15/19 12:461.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 11/15/19 12:463.7
Acetone ug/kg ND 100 11/15/19 12:469.4
Benzene ug/kg ND 5.0 11/15/19 12:460.90
Bromobenzene ug/kg ND 5.0 11/15/19 12:461.4
Bromochloromethane ug/kg ND 5.0 11/15/19 12:461.2
Bromodichloromethane ug/kg ND 5.0 11/15/19 12:460.98
Bromoform ug/kg ND 5.0 11/15/19 12:462.4
Bromomethane ug/kg ND 10.0 11/15/19 12:462.4
Carbon tetrachloride ug/kg ND 5.0 11/15/19 12:460.96
Chlorobenzene ug/kg ND 5.0 11/15/19 12:460.97
Chloroethane ug/kg ND 10.0 11/15/19 12:462.1
Chloroform ug/kg ND 5.0 11/15/19 12:461.1
Chloromethane ug/kg ND 10.0 11/15/19 12:463.3
cis-1,2-Dichloroethene ug/kg ND 5.0 11/15/19 12:460.87
cis-1,3-Dichloropropene ug/kg ND 5.0 11/15/19 12:462.3
Dibromochloromethane ug/kg ND 5.0 11/15/19 12:462.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2735758
Associated Lab Samples:92453170001, 92453170002
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.0 11/15/19 12:461.5
Dichlorodifluoromethane ug/kg ND 10.0 11/15/19 12:464.1
Diisopropyl ether ug/kg ND 5.0 11/15/19 12:462.9
Ethylbenzene ug/kg ND 5.0 11/15/19 12:461.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 11/15/19 12:462.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 11/15/19 12:461.4
m&p-Xylene ug/kg ND 10.0 11/15/19 12:462.4
Methyl-tert-butyl ether ug/kg ND 5.0 11/15/19 12:462.9
Methylene Chloride ug/kg ND 20.0 11/15/19 12:465.9
n-Butylbenzene ug/kg ND 5.0 11/15/19 12:462.8
n-Propylbenzene ug/kg ND 5.0 11/15/19 12:461.7
Naphthalene ug/kg ND 5.0 11/15/19 12:464.2
o-Xylene ug/kg ND 5.0 11/15/19 12:461.2
p-Isopropyltoluene ug/kg ND 5.0 11/15/19 12:462.4
sec-Butylbenzene ug/kg ND 5.0 11/15/19 12:462.1
Styrene ug/kg ND 5.0 11/15/19 12:461.5
tert-Butylbenzene ug/kg ND 5.0 11/15/19 12:461.7
Tetrachloroethene ug/kg ND 5.0 11/15/19 12:461.6
Toluene ug/kg ND 5.0 11/15/19 12:461.6
trans-1,2-Dichloroethene ug/kg ND 5.0 11/15/19 12:460.98
trans-1,3-Dichloropropene ug/kg ND 5.0 11/15/19 12:460.88
Trichloroethene ug/kg ND 5.0 11/15/19 12:461.3
Trichlorofluoromethane ug/kg ND 5.0 11/15/19 12:461.2
Vinyl acetate ug/kg ND 50.0 11/15/19 12:4616.3
Vinyl chloride ug/kg ND 10.0 11/15/19 12:461.9
Xylene (Total)ug/kg ND 10.0 11/15/19 12:463.5
1,2-Dichloroethane-d4 (S)%89 70-132 11/15/19 12:46
4-Bromofluorobenzene (S)%100 70-130 11/15/19 12:46
Toluene-d8 (S)%113 70-130 11/15/19 12:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2735759LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2735760
1,1,1,2-Tetrachloroethane ug/kg 56.750 113 70-13011155.6 2 30
1,1,1-Trichloroethane ug/kg 54.550 109 70-13011356.4 3 30
1,1,2,2-Tetrachloroethane ug/kg 55.550 111 55-13010954.4 2 30
1,1,2-Trichloroethane ug/kg 53.650 107 70-13010954.3 1 30
1,1-Dichloroethane ug/kg 53.850 108 68-13010753.7 0 30
1,1-Dichloroethene ug/kg 54.050 108 70-13011155.6 3 30
1,1-Dichloropropene ug/kg 58.450 117 70-13012260.9 4 30
1,2,3-Trichlorobenzene ug/kg 57.650 115 70-13010451.8 11 30
1,2,3-Trichloropropane ug/kg 54.050 108 70-13010854.0 0 30
1,2,4-Trichlorobenzene ug/kg 53.750 107 70-13010049.9 7 30
1,2,4-Trimethylbenzene ug/kg 54.850 110 69-13010251.0 7 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
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Page 16 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2735759LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2735760
1,2-Dibromo-3-chloropropane ug/kg 58.850 118 57-14111155.7 5 30
1,2-Dibromoethane (EDB)ug/kg 57.350 115 70-13011255.9 2 30
1,2-Dichlorobenzene ug/kg 53.350 107 70-13010251.2 4 30
1,2-Dichloroethane ug/kg 51.550 103 70-13011055.2 7 30
1,2-Dichloropropane ug/kg 54.550 109 70-13011055.0 1 30
1,3,5-Trimethylbenzene ug/kg 53.950 108 70-13010351.4 5 30
1,3-Dichlorobenzene ug/kg 53.250 106 70-13010150.7 5 30
1,3-Dichloropropane ug/kg 56.650 113 70-13011356.3 1 30
1,4-Dichlorobenzene ug/kg 53.150 106 70-1309949.5 7 30
2,2-Dichloropropane ug/kg 53.750 107 70-13011055.1 3 30
2-Butanone (MEK)ug/kg 108100 108 60-130111111 2 30
2-Chlorotoluene ug/kg 54.150 108 70-13010552.3 3 30
2-Hexanone ug/kg 113100 113 70-132108108 4 30
4-Chlorotoluene ug/kg 53.750 107 70-13010351.5 4 30
4-Methyl-2-pentanone (MIBK)ug/kg 104100 104 69-130103103 1 30
Acetone ug/kg 101100 101 49-148101101 0 30
Benzene ug/kg 53.750 107 70-13010853.9 0 30
Bromobenzene ug/kg 57.250 114 70-13010753.7 6 30
Bromochloromethane ug/kg 52.050 104 70-13011356.4 8 30
Bromodichloromethane ug/kg 52.750 105 70-13010954.4 3 30
Bromoform ug/kg 56.650 113 68-13611457.2 1 30
Bromomethane ug/kg 61.450 123 60-14012964.7 5 30
Carbon tetrachloride ug/kg 55.050 110 70-13011356.6 3 30
Chlorobenzene ug/kg 52.850 106 70-13010451.8 2 30
Chloroethane ug/kg 57.550 115 51-14712261.2 6 30
Chloroform ug/kg 52.850 106 70-13011657.9 9 30
Chloromethane ug/kg 54.950 110 48-13010854.2 1 30
cis-1,2-Dichloroethene ug/kg 51.950 104 70-13010753.4 3 30
cis-1,3-Dichloropropene ug/kg 55.450 111 70-13011356.6 2 30
Dibromochloromethane ug/kg 55.550 111 70-13011155.5 0 30
Dibromomethane ug/kg 49.550 99 70-13010351.4 4 30
Dichlorodifluoromethane ug/kg 48.450 97 49-1309949.4 2 30
Diisopropyl ether ug/kg 56.250 112 66-13011456.8 1 30
Ethylbenzene ug/kg 51.750 103 70-13010251.2 1 30
Hexachloro-1,3-butadiene ug/kg 54.850 110 70-13010150.7 8 30
Isopropylbenzene (Cumene)ug/kg 53.650 107 70-13010753.3 1 30
m&p-Xylene ug/kg 104100 104 70-130104104 0 30
Methyl-tert-butyl ether ug/kg 57.850 116 70-13011758.6 1 30
Methylene Chloride ug/kg 47.950 96 50-1379949.7 4 30
n-Butylbenzene ug/kg 52.850 106 70-1309949.3 7 30
n-Propylbenzene ug/kg 52.850 106 70-13010150.3 5 30
Naphthalene ug/kg 59.050 118 70-13110552.3 12 30
o-Xylene ug/kg 52.450 105 70-13010753.5 2 30
p-Isopropyltoluene ug/kg 52.750 105 70-13010050.1 5 30
sec-Butylbenzene ug/kg 53.450 107 70-13010150.4 6 30
Styrene ug/kg 53.350 107 70-13010653.1 0 30
tert-Butylbenzene ug/kg 48.150 96 69-1309145.6 5 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
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Page 17 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2735759LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2735760
Tetrachloroethene ug/kg 53.350 107 56-13010150.5 5 30
Toluene ug/kg 49.750 99 70-1309949.5 0 30
trans-1,2-Dichloroethene ug/kg 53.550 107 70-13011155.7 4 30
trans-1,3-Dichloropropene ug/kg 54.850 110 70-13011155.4 1 30
Trichloroethene ug/kg 54.350 109 70-14110854.2 0 30
Trichlorofluoromethane ug/kg 50.750 101 67-13010351.3 1 30
Vinyl acetate ug/kg 109100 109 10-136102102 7 30
Vinyl chloride ug/kg 54.250 108 67-13011356.5 4 30
Xylene (Total)ug/kg 157150 104 70-130105157 0 30
1,2-Dichloroethane-d4 (S)%99 70-132100
4-Bromofluorobenzene (S)%100 70-130103
Toluene-d8 (S)%94 70-13095
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
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[phone]
Page 18 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
508980
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples:92453170001, 92453170002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2731859
Associated Lab Samples:92453170001, 92453170002
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 330 11/14/19 10:3375.6
1,2-Dichlorobenzene ug/kg ND 330 11/14/19 10:3371.4
1,3-Dichlorobenzene ug/kg ND 330 11/14/19 10:3374.3
1,4-Dichlorobenzene ug/kg ND 330 11/14/19 10:3372.6
1-Methylnaphthalene ug/kg ND 330 11/14/19 10:3387.9
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 11/14/19 10:3391.7
2,4,5-Trichlorophenol ug/kg ND 330 11/14/19 10:3385.7
2,4,6-Trichlorophenol ug/kg ND 330 11/14/19 10:3382.9
2,4-Dichlorophenol ug/kg ND 330 11/14/19 10:33109
2,4-Dimethylphenol ug/kg ND 330 11/14/19 10:3382.2
2,4-Dinitrophenol ug/kg ND 1650 11/14/19 10:331050
2,4-Dinitrotoluene ug/kg ND 330 11/14/19 10:3387.4
2,6-Dinitrotoluene ug/kg ND 330 11/14/19 10:3386.3
2-Chloronaphthalene ug/kg ND 330 11/14/19 10:3373.5
2-Chlorophenol ug/kg ND 330 11/14/19 10:3376.8
2-Methylnaphthalene ug/kg ND 330 11/14/19 10:3384.0
2-Methylphenol(o-Cresol)ug/kg ND 330 11/14/19 10:3373.1
2-Nitroaniline ug/kg ND 1650 11/14/19 10:33166
2-Nitrophenol ug/kg ND 330 11/14/19 10:33102
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 11/14/19 10:3383.0
3,3'-Dichlorobenzidine ug/kg ND 1650 11/14/19 10:33230
3-Nitroaniline ug/kg ND 1650 11/14/19 10:33175
4,6-Dinitro-2-methylphenol ug/kg ND 660 11/14/19 10:33532
4-Bromophenylphenyl ether ug/kg ND 330 11/14/19 10:3386.6
4-Chloro-3-methylphenol ug/kg ND 660 11/14/19 10:33201
4-Chloroaniline ug/kg ND 1650 11/14/19 10:33202
4-Chlorophenylphenyl ether ug/kg ND 330 11/14/19 10:3385.7
4-Nitroaniline ug/kg ND 660 11/14/19 10:33163
4-Nitrophenol ug/kg ND 1650 11/14/19 10:33526
Acenaphthene ug/kg ND 330 11/14/19 10:3384.9
Acenaphthylene ug/kg ND 330 11/14/19 10:3378.1
Aniline ug/kg ND 330 11/14/19 10:3374.1
Anthracene ug/kg ND 330 11/14/19 10:3385.6
Benzo(a)anthracene ug/kg ND 330 11/14/19 10:33105
Benzo(a)pyrene ug/kg ND 330 11/14/19 10:33143
Benzo(b)fluoranthene ug/kg ND 330 11/14/19 10:33133
Benzo(g,h,i)perylene ug/kg ND 330 11/14/19 10:33129
Benzo(k)fluoranthene ug/kg ND 330 11/14/19 10:33139
Benzoic Acid ug/kg ND 1650 11/14/19 10:33356
Benzyl alcohol ug/kg ND 660 11/14/19 10:33175
bis(2-Chloroethoxy)methane ug/kg ND 330 11/14/19 10:3388.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2731859
Associated Lab Samples:92453170001, 92453170002
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 330 11/14/19 10:3370.1
bis(2-Ethylhexyl)phthalate ug/kg ND 330 11/14/19 10:33108
Butylbenzylphthalate ug/kg ND 330 11/14/19 10:3387.9
Chrysene ug/kg ND 330 11/14/19 10:3395.8
Di-n-butylphthalate ug/kg ND 330 11/14/19 10:3381.4
Di-n-octylphthalate ug/kg ND 330 11/14/19 10:33188
Dibenz(a,h)anthracene ug/kg ND 330 11/14/19 10:33132
Dibenzofuran ug/kg ND 330 11/14/19 10:3382.5
Diethylphthalate ug/kg ND 330 11/14/19 10:3371.6
Dimethylphthalate ug/kg ND 330 11/14/19 10:3374.6
Fluoranthene ug/kg ND 330 11/14/19 10:3399.7
Fluorene ug/kg ND 330 11/14/19 10:3388.3
Hexachloro-1,3-butadiene ug/kg ND 330 11/14/19 10:3380.2
Hexachlorobenzene ug/kg ND 330 11/14/19 10:3383.8
Hexachlorocyclopentadiene ug/kg ND 330 11/14/19 10:33132
Hexachloroethane ug/kg ND 330 11/14/19 10:3375.2
Indeno(1,2,3-cd)pyrene ug/kg ND 330 11/14/19 10:33151
Isophorone ug/kg ND 330 11/14/19 10:3371.7
N-Nitroso-di-n-propylamine ug/kg ND 330 11/14/19 10:3392.4
N-Nitrosodimethylamine ug/kg ND 330 11/14/19 10:3392.8
N-Nitrosodiphenylamine ug/kg ND 330 11/14/19 10:3384.2
Naphthalene ug/kg ND 330 11/14/19 10:3379.0
Nitrobenzene ug/kg ND 330 11/14/19 10:3378.8
Pentachlorophenol ug/kg ND 1650 11/14/19 10:33151
Phenanthrene ug/kg ND 330 11/14/19 10:3383.1
Phenol ug/kg ND 330 11/14/19 10:3378.8
Pyrene ug/kg ND 330 11/14/19 10:3390.8
Pyridine ug/kg ND 330 11/14/19 10:3383.5
2,4,6-Tribromophenol (S)%75 27-110 11/14/19 10:33
2-Fluorobiphenyl (S)%77 30-110 11/14/19 10:33
2-Fluorophenol (S)%71 13-110 11/14/19 10:33
Nitrobenzene-d5 (S)%73 23-110 11/14/19 10:33
Phenol-d6 (S)%70 22-110 11/14/19 10:33
Terphenyl-d14 (S)%84 28-110 11/14/19 10:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2731860LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13501680 81 52-130
1,2-Dichlorobenzene ug/kg 12901680 77 51-130
1,3-Dichlorobenzene ug/kg 13001680 78 50-130
1,4-Dichlorobenzene ug/kg 12701680 76 49-130
1-Methylnaphthalene ug/kg 13701680 82 55-130
2,2'-Oxybis(1-chloropropane)ug/kg 12301680 73 30-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2731860LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/kg 13101680 78 55-130
2,4,6-Trichlorophenol ug/kg 13301680 79 57-130
2,4-Dichlorophenol ug/kg 13501680 80 56-130
2,4-Dimethylphenol ug/kg 13501680 81 51-130
2,4-Dinitrophenol ug/kg 67208390 80 27-133
2,4-Dinitrotoluene ug/kg 14701680 88 61-130
2,6-Dinitrotoluene ug/kg 14201680 85 60-130
2-Chloronaphthalene ug/kg 13501680 80 52-130
2-Chlorophenol ug/kg 13501680 80 54-130
2-Methylnaphthalene ug/kg 13501680 80 54-130
2-Methylphenol(o-Cresol)ug/kg 13101680 78 51-130
2-Nitroaniline ug/kg 30103360 90 51-130
2-Nitrophenol ug/kg 13301680 79 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 12801680 76 11-163
3,3'-Dichlorobenzidine ug/kg 21203360 63 10-132
3-Nitroaniline ug/kg 25503360 76 55-130
4,6-Dinitro-2-methylphenol ug/kg 30603360 91 47-142
4-Bromophenylphenyl ether ug/kg 13601680 81 59-130
4-Chloro-3-methylphenol ug/kg 27103360 81 55-130
4-Chloroaniline ug/kg 27203360 81 54-130
4-Chlorophenylphenyl ether ug/kg 14001680 83 58-130
4-Nitroaniline ug/kg 27503360 82 54-130
4-Nitrophenol ug/kg 71608390 85 48-130
Acenaphthene ug/kg 14301680 85 60-130
Acenaphthylene ug/kg 14901680 89 60-130
Aniline ug/kg 12201680 73 43-130
Anthracene ug/kg 15201680 91 63-130
Benzo(a)anthracene ug/kg 15101680 90 59-130
Benzo(a)pyrene ug/kg 15201680 90 57-130
Benzo(b)fluoranthene ug/kg 14901680 89 54-130
Benzo(g,h,i)perylene ug/kg 15401680 92 59-130
Benzo(k)fluoranthene ug/kg 14601680 87 54-130
Benzoic Acid ug/kg 46008390 55 19-130
Benzyl alcohol ug/kg 23703360 71 50-130
bis(2-Chloroethoxy)methane ug/kg 13201680 78 54-130
bis(2-Chloroethyl) ether ug/kg 13301680 79 48-130
bis(2-Ethylhexyl)phthalate ug/kg 14101680 84 45-134
Butylbenzylphthalate ug/kg 13901680 83 46-138
Chrysene ug/kg 14201680 84 58-130
Di-n-butylphthalate ug/kg 13601680 81 60-130
Di-n-octylphthalate ug/kg 14701680 88 53-130
Dibenz(a,h)anthracene ug/kg 15601680 93 59-130
Dibenzofuran ug/kg 13901680 83 60-130
Diethylphthalate ug/kg 14001680 83 60-130
Dimethylphthalate ug/kg 13701680 82 60-130
Fluoranthene ug/kg 14501680 87 65-130
Fluorene ug/kg 14601680 87 63-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2731860LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/kg 13501680 80 46-130
Hexachlorobenzene ug/kg 13501680 81 58-130
Hexachlorocyclopentadiene ug/kg 13901680 83 23-130
Hexachloroethane ug/kg 13001680 78 47-130
Indeno(1,2,3-cd)pyrene ug/kg 15101680 90 60-130
Isophorone ug/kg 13901680 83 49-130
N-Nitroso-di-n-propylamine ug/kg 13701680 82 47-130
N-Nitrosodimethylamine ug/kg 13601680 81 45-130
N-Nitrosodiphenylamine ug/kg 13601680 81 59-130
Naphthalene ug/kg 13901680 83 55-130
Nitrobenzene ug/kg 14001680 84 49-130
Pentachlorophenol ug/kg 22803360 68 10-132
Phenanthrene ug/kg 14401680 86 62-130
Phenol ug/kg 13701680 81 46-130
Pyrene ug/kg 14901680 89 53-130
Pyridine ug/kg 9911680 59 37-130
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%84 30-110
2-Fluorophenol (S)%84 13-110
Nitrobenzene-d5 (S)%86 23-110
Phenol-d6 (S)%83 22-110
Terphenyl-d14 (S)%84 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2731861MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92453160005
2731862
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1850 69 18-13064 8 301850ND12801180
1,2-Dichlorobenzene ug/kg 1850 66 14-13059 11 301850ND12201090
1,3-Dichlorobenzene ug/kg 1850 63 12-13059 8 301850ND11801090
1,4-Dichlorobenzene ug/kg 1850 65 10-13058 11 301850ND12001080
1-Methylnaphthalene ug/kg 1850 69 12-13067 3 301850ND12801240
2,2'-Oxybis(1-
chloropropane)ug/kg 1850 65 10-13063 4 301850ND12101160
2,4,5-Trichlorophenol ug/kg 1850 71 13-13075 6 301850ND13201400
2,4,6-Trichlorophenol ug/kg 1850 67 17-13068 1 301850ND12501260
2,4-Dichlorophenol ug/kg 1850 71 10-13072 1 301850ND13101330
2,4-Dimethylphenol ug/kg 1850 72 10-13071 2 301850ND13401310
2,4-Dinitrophenol ug/kg M19280010-1300 309280NDNDND
2,4-Dinitrotoluene ug/kg 1850 72 24-13078 7 301850ND13401440
2,6-Dinitrotoluene ug/kg 1850 74 23-13079 7 301850ND13801470
2-Chloronaphthalene ug/kg 1850 70 19-13073 4 301850ND13101360
2-Chlorophenol ug/kg 1850 74 10-13069 8 301850ND13701270
2-Methylnaphthalene ug/kg 1850 66 18-13065 2 301850ND12301210
2-Methylphenol(o-Cresol)ug/kg 1850 73 10-13070 4 301850ND13601300
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 05:03 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2731861MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92453160005
2731862
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitroaniline ug/kg 3710 80 17-13085 7 303710ND29503170
2-Nitrophenol ug/kg 1850 69 10-13065 5 301850ND12801210
3&4-Methylphenol(m&p
Cresol)ug/kg 1850 74 10-13074 0 301850ND13801380
3,3'-Dichlorobenzidine ug/kg 3710 56 10-13067 19 303710ND20702500
3-Nitroaniline ug/kg 3710 71 24-13078 9 303710ND26402900
4,6-Dinitro-2-methylphenol ug/kg M137101210-1528 303710NDNDND
4-Bromophenylphenyl ether ug/kg 1850 65 29-13071 10 301850ND12001320
4-Chloro-3-methylphenol ug/kg 3710 71 17-13075 6 303710ND26302800
4-Chloroaniline ug/kg 3710 65 14-13065 0 303710ND24302430
4-Chlorophenylphenyl ether ug/kg 1850 68 25-13074 8 301850ND12701380
4-Nitroaniline ug/kg 3710 76 22-13082 7 303710ND28303040
4-Nitrophenol ug/kg 9280 50 10-13047 7 309280ND46304330
Acenaphthene ug/kg 1850 73 20-13076 4 301850ND13501410
Acenaphthylene ug/kg 1850 78 25-13082 4 301850ND14501510
Aniline ug/kg 1850 63 10-13057 9 301850ND11601060
Anthracene ug/kg 1850 75 29-13082 9 301850ND14001530
Benzo(a)anthracene ug/kg 1850 68 19-13077 12 301850ND13101470
Benzo(a)pyrene ug/kg 1850 70 12-13078 12 301850ND12901460
Benzo(b)fluoranthene ug/kg 1850 71 14-13079 9 301850ND13301460
Benzo(g,h,i)perylene ug/kg 1850 67 10-13074 9 301850ND12501370
Benzo(k)fluoranthene ug/kg 1850 67 14-13074 10 301850ND12501380
Benzoic Acid ug/kg M19280010-1300 309280NDNDND
Benzyl alcohol ug/kg 3710 72 13-13066 8 303710ND26802470
bis(2-
Chloroethoxy)methane ug/kg 1850 69 16-13064 8 301850ND12801190
bis(2-Chloroethyl) ether ug/kg 1850 69 11-13064 7 301850ND12801190
bis(2-Ethylhexyl)phthalate ug/kg 1850 62 21-13067 7 301850ND11601240
Butylbenzylphthalate ug/kg 1850 64 23-13067 4 301850ND11901250
Chrysene ug/kg 1850 68 22-13075 11 301850ND12601400
Di-n-butylphthalate ug/kg 1850 61 30-13067 10 301850ND11301240
Di-n-octylphthalate ug/kg 1850 62 23-14268 9 301850ND11601270
Dibenz(a,h)anthracene ug/kg 1850 66 10-13075 13 301850ND12301400
Dibenzofuran ug/kg 1850 70 24-13073 4 301850ND13001350
Diethylphthalate ug/kg 1850 70 26-13076 8 301850ND13001400
Dimethylphthalate ug/kg 1850 72 22-13076 6 301850ND13301410
Fluoranthene ug/kg 1850 68 33-13083 19 301850ND13401620
Fluorene ug/kg 1850 73 22-13077 5 301850ND13601430
Hexachloro-1,3-butadiene ug/kg 1850 64 13-13059 8 301850ND11901100
Hexachlorobenzene ug/kg 1850 66 29-13071 8 301850ND12201320
Hexachlorocyclopentadiene ug/kg 1850 61 10-13056 10 301850ND11401030
Hexachloroethane ug/kg 1850 66 10-13064 3 301850ND12201180
Indeno(1,2,3-cd)pyrene ug/kg 1850 68 10-13075 9 301850ND12601390
Isophorone ug/kg 1850 69 13-13067 2 301850ND12801250
N-Nitroso-di-n-propylamine ug/kg 1850 74 12-13070 5 301850ND13701300
N-Nitrosodimethylamine ug/kg 1850 63 11-13057 11 301850ND11701060
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Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2731861MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92453160005
2731862
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodiphenylamine ug/kg 1850 72 15-13079 9 301850ND13401480
Naphthalene ug/kg 1850 73 15-13068 7 301850ND13501260
Nitrobenzene ug/kg 1850 69 12-13066 4 301850ND12801230
Pentachlorophenol ug/kg 3710 36 10-13032 303710ND1340J1170J
Phenanthrene ug/kg 1850 70 27-13083 16 301850ND13501580
Phenol ug/kg 1850 79 10-13078 1 301850ND14701450
Pyrene ug/kg 1850 72 19-13084 14 301850ND14001620
Pyridine ug/kg 1850 53 10-13047 12 301850ND989874
2,4,6-Tribromophenol (S)%79 27-11082
2-Fluorobiphenyl (S)%67 30-11065
2-Fluorophenol (S)%70 13-11061
Nitrobenzene-d5 (S)%69 23-11062
Phenol-d6 (S)%75 22-11068
Terphenyl-d14 (S)%58 28-11060
REPORT OF LABORATORY ANALYSIS
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Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
509034
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92453170001, 92453170002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92453160001
2732187SAMPLE DUPLICATE:
Percent Moisture %8.1 3 257.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92453270006
2732246SAMPLE DUPLICATE:
Percent Moisture %13.9 8 2512.8
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1381344
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92453170001, 92453170002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3473050-1
Associated Lab Samples:92453170001, 92453170002
Matrix:Solid
AnalyzedMDL
Total Solids %0.00200 11/16/19 13:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3473050-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1159973-01
R3473050-3SAMPLE DUPLICATE:
Total Solids %93.0 0.125 1092.9
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Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453170
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1380647
3060A
EPA 7199
Wet Chemistry 7199
Associated Lab Samples:92453170001, 92453170002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3472547-1
Associated Lab Samples:92453170001, 92453170002
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 11/15/19 16:300.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3472547-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.8410.0 98.4 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3472547-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1159154-02
R3472547-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg ML20.0 49.4 75.0-12549.3 0.187 2020.0ND 9.88 9.86
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3472547-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1159154-02
Chromium, Hexavalent mg/kg 9391030 91.1 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1159081-01
R3472547-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1160648-02
R3472547-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
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Page 27 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92453170
LEH-004
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
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Page 28 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92453170
LEH-004
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92453170001 1380473 1380473SB-11 3050B EPA 6020B
92453170002 1380473 1380473SB-12 3050B EPA 6020B
92453170001 1380193 1380193SB-11 7471A EPA 7471B
92453170002 1380193 1380193SB-12 7471A EPA 7471B
92453170001 508980 509509SB-11 EPA 3546 EPA 8270E
92453170002 508980 509509SB-12 EPA 3546 EPA 8270E
92453170001 509780 509784SB-11 EPA 5035A EPA 8260D
92453170002 509780 509784SB-12 EPA 5035A EPA 8260D
92453170001 509034SB-11 ASTM D2974-87
92453170002 509034SB-12 ASTM D2974-87
92453170001 1381344 1381344SB-11 SM 2540 G SM 2540G
92453170002 1381344 1381344SB-12 SM 2540 G SM 2540G
92453170001 1380647 1380647SB-11 3060A EPA 7199
92453170002 1380647 1380647SB-12 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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Page 29 of 32
Page 30 of 32
Page 31 of 32
Page 32 of 32
#=CL#
November 19, 2019
LIMS USE: FR - RALPH MCGEE
LIMS OBJECT ID: 92453168
92453168
Project:
Pace Project No.:
RE:
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
LEH-004
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on November 11, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
cc:Alexis McKenzie, Hart & Hickman
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Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92453168
LEH-004
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
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Canada Certification #: 1461.01
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DOD Certification: #1461.01
EPA# TN00003
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South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
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USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
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Pace Analytical Services Charlotte
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Virginia/VELAP Certification #: 460221
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92453168
LEH-004
Lab ID Sample ID Matrix Date Collected Date Received
92453168001 TMW-5 Water 11/09/19 14:45 11/11/19 13:43
92453168002 TMW-6 Water 11/09/19 15:20 11/11/19 13:43
92453168003 DUP-4 Water 11/09/19 00:00 11/11/19 13:43
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92453168
LEH-004
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92453168001 TMW-5 EPA 6020B 7 PANJPD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92453168002 TMW-6 EPA 6020B 7 PANJPD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92453168003 DUP-4 EPA 8270E 74 PASI-CPKS
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Page 4 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:TMW-5 Lab ID:92453168001 Collected:11/09/19 14:45 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Arsenic 0.452J ug/L 11/16/19 12:26 7440-38-2 J11/15/19 12:022.00 0.250 1
Barium 87.6 ug/L 11/16/19 12:26 7440-39-311/15/19 12:025.00 0.360 1
Cadmium ND ug/L 11/16/19 12:26 7440-43-911/15/19 12:021.00 0.160 1
Chromium 4.14 ug/L 11/16/19 12:26 7440-47-311/15/19 12:022.00 0.540 1
Lead 0.790J ug/L 11/16/19 12:26 7439-92-1 B,J11/15/19 12:022.00 0.240 1
Selenium 1.94J ug/L 11/16/19 12:26 7782-49-2 J11/15/19 12:022.00 0.380 1
Silver ND ug/L 11/16/19 12:26 7440-22-411/15/19 12:022.00 0.310 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 11/14/19 13:57 7439-97-611/13/19 22:000.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 11/15/19 23:30 83-32-911/14/19 16:4510.0 1.6 1
Acenaphthylene ND ug/L 11/15/19 23:30 208-96-811/14/19 16:4510.0 1.6 1
Aniline ND ug/L 11/15/19 23:30 62-53-311/14/19 16:4510.0 1.9 1
Anthracene ND ug/L 11/15/19 23:30 120-12-711/14/19 16:4510.0 1.7 1
Benzo(a)anthracene ND ug/L 11/15/19 23:30 56-55-311/14/19 16:4510.0 1.8 1
Benzo(a)pyrene ND ug/L 11/15/19 23:30 50-32-811/14/19 16:4510.0 2.1 1
Benzo(b)fluoranthene ND ug/L 11/15/19 23:30 205-99-211/14/19 16:4510.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 11/15/19 23:30 191-24-211/14/19 16:4510.0 1.4 1
Benzo(k)fluoranthene ND ug/L 11/15/19 23:30 207-08-911/14/19 16:4510.0 1.9 1
Benzoic Acid ND ug/L 11/15/19 23:30 65-85-011/14/19 16:4550.0 43.0 1
Benzyl alcohol ND ug/L 11/15/19 23:30 100-51-611/14/19 16:4520.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 11/15/19 23:30 101-55-311/14/19 16:4510.0 1.6 1
Butylbenzylphthalate ND ug/L 11/15/19 23:30 85-68-711/14/19 16:4510.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 11/15/19 23:30 59-50-711/14/19 16:4520.0 2.8 1
4-Chloroaniline ND ug/L 11/15/19 23:30 106-47-811/14/19 16:4520.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 11/15/19 23:30 111-91-111/14/19 16:4510.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 11/15/19 23:30 111-44-411/14/19 16:4510.0 1.8 1
2-Chloronaphthalene ND ug/L 11/15/19 23:30 91-58-711/14/19 16:4510.0 1.5 1
2-Chlorophenol ND ug/L 11/15/19 23:30 95-57-811/14/19 16:4510.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 11/15/19 23:30 7005-72-311/14/19 16:4510.0 1.6 1
Chrysene ND ug/L 11/15/19 23:30 218-01-911/14/19 16:4510.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 11/15/19 23:30 53-70-311/14/19 16:4510.0 1.6 1
Dibenzofuran ND ug/L 11/15/19 23:30 132-64-911/14/19 16:4510.0 1.5 1
1,2-Dichlorobenzene ND ug/L 11/15/19 23:30 95-50-111/14/19 16:4510.0 1.3 1
1,3-Dichlorobenzene ND ug/L 11/15/19 23:30 541-73-111/14/19 16:4510.0 1.5 1
1,4-Dichlorobenzene ND ug/L 11/15/19 23:30 106-46-711/14/19 16:4510.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 11/15/19 23:30 91-94-111/14/19 16:4520.0 3.0 1
2,4-Dichlorophenol ND ug/L 11/15/19 23:30 120-83-211/14/19 16:4510.0 1.4 1
Diethylphthalate ND ug/L 11/15/19 23:30 84-66-211/14/19 16:4510.0 2.4 1
2,4-Dimethylphenol ND ug/L 11/15/19 23:30 105-67-911/14/19 16:4510.0 1.4 1
Dimethylphthalate ND ug/L 11/15/19 23:30 131-11-311/14/19 16:4510.0 1.6 1
Di-n-butylphthalate ND ug/L 11/15/19 23:30 84-74-211/14/19 16:4510.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 11/15/19 23:30 534-52-111/14/19 16:4520.0 15.2 1
2,4-Dinitrophenol ND ug/L 11/15/19 23:30 51-28-511/14/19 16:4550.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:TMW-5 Lab ID:92453168001 Collected:11/09/19 14:45 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 11/15/19 23:30 121-14-211/14/19 16:4510.0 1.2 1
2,6-Dinitrotoluene ND ug/L 11/15/19 23:30 606-20-211/14/19 16:4510.0 1.4 1
Di-n-octylphthalate ND ug/L 11/15/19 23:30 117-84-011/14/19 16:4510.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/15/19 23:30 117-81-711/14/19 16:456.0 2.1 1
Fluoranthene ND ug/L 11/15/19 23:30 206-44-011/14/19 16:4510.0 1.7 1
Fluorene ND ug/L 11/15/19 23:30 86-73-711/14/19 16:4510.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 11/15/19 23:30 87-68-311/14/19 16:4510.0 2.0 1
Hexachlorobenzene ND ug/L 11/15/19 23:30 118-74-111/14/19 16:4510.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 11/15/19 23:30 77-47-411/14/19 16:4510.0 1.7 1
Hexachloroethane ND ug/L 11/15/19 23:30 67-72-111/14/19 16:4510.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/15/19 23:30 193-39-511/14/19 16:4510.0 1.6 1
Isophorone ND ug/L 11/15/19 23:30 78-59-111/14/19 16:4510.0 1.6 1
1-Methylnaphthalene ND ug/L 11/15/19 23:30 90-12-011/14/19 16:4510.0 1.4 1
2-Methylnaphthalene ND ug/L 11/15/19 23:30 91-57-611/14/19 16:4510.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 11/15/19 23:30 95-48-711/14/19 16:4510.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/15/19 23:30 15831-10-411/14/19 16:4510.0 1.2 1
Naphthalene ND ug/L 11/15/19 23:30 91-20-311/14/19 16:4510.0 1.4 1
2-Nitroaniline ND ug/L 11/15/19 23:30 88-74-411/14/19 16:4520.0 4.2 1
3-Nitroaniline ND ug/L 11/15/19 23:30 99-09-211/14/19 16:4520.0 2.3 1
4-Nitroaniline ND ug/L 11/15/19 23:30 100-01-611/14/19 16:4520.0 2.2 1
Nitrobenzene ND ug/L 11/15/19 23:30 98-95-311/14/19 16:4510.0 2.1 1
2-Nitrophenol ND ug/L 11/15/19 23:30 88-75-511/14/19 16:4510.0 1.4 1
4-Nitrophenol ND ug/L 11/15/19 23:30 100-02-711/14/19 16:4550.0 3.5 1
N-Nitrosodimethylamine ND ug/L 11/15/19 23:30 62-75-911/14/19 16:4510.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 11/15/19 23:30 621-64-711/14/19 16:4510.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 11/15/19 23:30 86-30-611/14/19 16:4510.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/15/19 23:30 108-60-111/14/19 16:4510.0 2.8 1
Pentachlorophenol ND ug/L 11/15/19 23:30 87-86-511/14/19 16:4525.0 2.2 1
Phenanthrene ND ug/L 11/15/19 23:30 85-01-811/14/19 16:4510.0 1.7 1
Phenol ND ug/L 11/15/19 23:30 108-95-211/14/19 16:4510.0 0.92 1
Pyrene ND ug/L 11/15/19 23:30 129-00-011/14/19 16:4510.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 11/15/19 23:30 120-82-111/14/19 16:4510.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 11/15/19 23:30 95-95-411/14/19 16:4510.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 11/15/19 23:30 88-06-211/14/19 16:4510.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)68 %11/15/19 23:30 4165-60-011/14/19 16:4513-130 1
2-Fluorobiphenyl (S)61 %11/15/19 23:30 321-60-811/14/19 16:4513-130 1
Terphenyl-d14 (S)66 %11/15/19 23:30 1718-51-011/14/19 16:4525-130 1
Phenol-d6 (S)41 %11/15/19 23:30 13127-88-311/14/19 16:4510-130 1
2-Fluorophenol (S)52 %11/15/19 23:30 367-12-411/14/19 16:4510-130 1
2,4,6-Tribromophenol (S)69 %11/15/19 23:30 118-79-611/14/19 16:4510-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 11/15/19 09:21 67-64-125.0 6.2 1
Benzene ND ug/L 11/15/19 09:21 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/15/19 09:21 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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[phone]
Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:TMW-5 Lab ID:92453168001 Collected:11/09/19 14:45 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 11/15/19 09:21 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/15/19 09:21 75-27-41.0 0.26 1
Bromoform ND ug/L 11/15/19 09:21 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/15/19 09:21 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 11/15/19 09:21 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/15/19 09:21 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/15/19 09:21 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/15/19 09:21 75-00-31.0 0.49 1
Chloroform ND ug/L 11/15/19 09:21 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/15/19 09:21 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/15/19 09:21 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/15/19 09:21 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/15/19 09:21 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/15/19 09:21 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/15/19 09:21 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/15/19 09:21 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/15/19 09:21 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/15/19 09:21 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/15/19 09:21 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/15/19 09:21 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/15/19 09:21 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/15/19 09:21 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/15/19 09:21 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 11/15/19 09:21 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/15/19 09:21 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/15/19 09:21 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/15/19 09:21 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/15/19 09:21 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/15/19 09:21 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/15/19 09:21 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/15/19 09:21 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/15/19 09:21 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/15/19 09:21 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/15/19 09:21 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/15/19 09:21 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/15/19 09:21 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/15/19 09:21 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/15/19 09:21 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/15/19 09:21 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/15/19 09:21 91-20-31.0 0.35 1
Styrene ND ug/L 11/15/19 09:21 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/15/19 09:21 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 11/15/19 09:21 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/15/19 09:21 127-18-41.0 0.16 1
Toluene ND ug/L 11/15/19 09:21 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/15/19 09:21 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:TMW-5 Lab ID:92453168001 Collected:11/09/19 14:45 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 11/15/19 09:21 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/15/19 09:21 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/15/19 09:21 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/15/19 09:21 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/15/19 09:21 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/15/19 09:21 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/15/19 09:21 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/15/19 09:21 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/15/19 09:21 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/15/19 09:21 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/15/19 09:21 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)102 %11/15/19 09:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %11/15/19 09:21 17060-07-070-130 1
Toluene-d8 (S)95 %11/15/19 09:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:TMW-6 Lab ID:92453168002 Collected:11/09/19 15:20 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Arsenic ND ug/L 11/16/19 12:30 7440-38-211/15/19 12:022.00 0.250 1
Barium 37.5 ug/L 11/16/19 12:30 7440-39-311/15/19 12:025.00 0.360 1
Cadmium ND ug/L 11/16/19 12:30 7440-43-911/15/19 12:021.00 0.160 1
Chromium 1.94J ug/L 11/16/19 12:30 7440-47-3 J11/15/19 12:022.00 0.540 1
Lead ND ug/L 11/16/19 12:30 7439-92-111/15/19 12:022.00 0.240 1
Selenium ND ug/L 11/16/19 12:30 7782-49-211/15/19 12:022.00 0.380 1
Silver ND ug/L 11/16/19 12:30 7440-22-411/15/19 12:022.00 0.310 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 11/14/19 13:59 7439-97-611/13/19 22:000.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 11/15/19 23:56 83-32-911/14/19 16:4510.0 1.6 1
Acenaphthylene ND ug/L 11/15/19 23:56 208-96-811/14/19 16:4510.0 1.6 1
Aniline ND ug/L 11/15/19 23:56 62-53-311/14/19 16:4510.0 1.9 1
Anthracene ND ug/L 11/15/19 23:56 120-12-711/14/19 16:4510.0 1.7 1
Benzo(a)anthracene ND ug/L 11/15/19 23:56 56-55-311/14/19 16:4510.0 1.8 1
Benzo(a)pyrene ND ug/L 11/15/19 23:56 50-32-811/14/19 16:4510.0 2.1 1
Benzo(b)fluoranthene ND ug/L 11/15/19 23:56 205-99-211/14/19 16:4510.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 11/15/19 23:56 191-24-211/14/19 16:4510.0 1.4 1
Benzo(k)fluoranthene ND ug/L 11/15/19 23:56 207-08-911/14/19 16:4510.0 1.9 1
Benzoic Acid ND ug/L 11/15/19 23:56 65-85-011/14/19 16:4550.0 43.0 1
Benzyl alcohol ND ug/L 11/15/19 23:56 100-51-611/14/19 16:4520.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 11/15/19 23:56 101-55-311/14/19 16:4510.0 1.6 1
Butylbenzylphthalate ND ug/L 11/15/19 23:56 85-68-711/14/19 16:4510.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 11/15/19 23:56 59-50-711/14/19 16:4520.0 2.8 1
4-Chloroaniline ND ug/L 11/15/19 23:56 106-47-811/14/19 16:4520.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 11/15/19 23:56 111-91-111/14/19 16:4510.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 11/15/19 23:56 111-44-411/14/19 16:4510.0 1.8 1
2-Chloronaphthalene ND ug/L 11/15/19 23:56 91-58-711/14/19 16:4510.0 1.5 1
2-Chlorophenol ND ug/L 11/15/19 23:56 95-57-811/14/19 16:4510.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 11/15/19 23:56 7005-72-311/14/19 16:4510.0 1.6 1
Chrysene ND ug/L 11/15/19 23:56 218-01-911/14/19 16:4510.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 11/15/19 23:56 53-70-311/14/19 16:4510.0 1.6 1
Dibenzofuran ND ug/L 11/15/19 23:56 132-64-911/14/19 16:4510.0 1.5 1
1,2-Dichlorobenzene ND ug/L 11/15/19 23:56 95-50-111/14/19 16:4510.0 1.3 1
1,3-Dichlorobenzene ND ug/L 11/15/19 23:56 541-73-111/14/19 16:4510.0 1.5 1
1,4-Dichlorobenzene ND ug/L 11/15/19 23:56 106-46-711/14/19 16:4510.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 11/15/19 23:56 91-94-111/14/19 16:4520.0 3.0 1
2,4-Dichlorophenol ND ug/L 11/15/19 23:56 120-83-211/14/19 16:4510.0 1.4 1
Diethylphthalate ND ug/L 11/15/19 23:56 84-66-211/14/19 16:4510.0 2.4 1
2,4-Dimethylphenol ND ug/L 11/15/19 23:56 105-67-911/14/19 16:4510.0 1.4 1
Dimethylphthalate ND ug/L 11/15/19 23:56 131-11-311/14/19 16:4510.0 1.6 1
Di-n-butylphthalate ND ug/L 11/15/19 23:56 84-74-211/14/19 16:4510.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 11/15/19 23:56 534-52-111/14/19 16:4520.0 15.2 1
2,4-Dinitrophenol ND ug/L 11/15/19 23:56 51-28-511/14/19 16:4550.0 40.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
Pace Analytical Services, LLC
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[phone]
Page 9 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:TMW-6 Lab ID:92453168002 Collected:11/09/19 15:20 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 11/15/19 23:56 121-14-211/14/19 16:4510.0 1.2 1
2,6-Dinitrotoluene ND ug/L 11/15/19 23:56 606-20-211/14/19 16:4510.0 1.4 1
Di-n-octylphthalate ND ug/L 11/15/19 23:56 117-84-011/14/19 16:4510.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/15/19 23:56 117-81-711/14/19 16:456.0 2.1 1
Fluoranthene ND ug/L 11/15/19 23:56 206-44-011/14/19 16:4510.0 1.7 1
Fluorene ND ug/L 11/15/19 23:56 86-73-711/14/19 16:4510.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 11/15/19 23:56 87-68-311/14/19 16:4510.0 2.0 1
Hexachlorobenzene ND ug/L 11/15/19 23:56 118-74-111/14/19 16:4510.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 11/15/19 23:56 77-47-411/14/19 16:4510.0 1.7 1
Hexachloroethane ND ug/L 11/15/19 23:56 67-72-111/14/19 16:4510.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/15/19 23:56 193-39-511/14/19 16:4510.0 1.6 1
Isophorone ND ug/L 11/15/19 23:56 78-59-111/14/19 16:4510.0 1.6 1
1-Methylnaphthalene ND ug/L 11/15/19 23:56 90-12-011/14/19 16:4510.0 1.4 1
2-Methylnaphthalene ND ug/L 11/15/19 23:56 91-57-611/14/19 16:4510.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 11/15/19 23:56 95-48-711/14/19 16:4510.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/15/19 23:56 15831-10-411/14/19 16:4510.0 1.2 1
Naphthalene ND ug/L 11/15/19 23:56 91-20-311/14/19 16:4510.0 1.4 1
2-Nitroaniline ND ug/L 11/15/19 23:56 88-74-411/14/19 16:4520.0 4.2 1
3-Nitroaniline ND ug/L 11/15/19 23:56 99-09-211/14/19 16:4520.0 2.3 1
4-Nitroaniline ND ug/L 11/15/19 23:56 100-01-611/14/19 16:4520.0 2.2 1
Nitrobenzene ND ug/L 11/15/19 23:56 98-95-311/14/19 16:4510.0 2.1 1
2-Nitrophenol ND ug/L 11/15/19 23:56 88-75-511/14/19 16:4510.0 1.4 1
4-Nitrophenol ND ug/L 11/15/19 23:56 100-02-711/14/19 16:4550.0 3.5 1
N-Nitrosodimethylamine ND ug/L 11/15/19 23:56 62-75-911/14/19 16:4510.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 11/15/19 23:56 621-64-711/14/19 16:4510.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 11/15/19 23:56 86-30-611/14/19 16:4510.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/15/19 23:56 108-60-111/14/19 16:4510.0 2.8 1
Pentachlorophenol ND ug/L 11/15/19 23:56 87-86-511/14/19 16:4525.0 2.2 1
Phenanthrene ND ug/L 11/15/19 23:56 85-01-811/14/19 16:4510.0 1.7 1
Phenol ND ug/L 11/15/19 23:56 108-95-211/14/19 16:4510.0 0.92 1
Pyrene ND ug/L 11/15/19 23:56 129-00-011/14/19 16:4510.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 11/15/19 23:56 120-82-111/14/19 16:4510.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 11/15/19 23:56 95-95-411/14/19 16:4510.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 11/15/19 23:56 88-06-211/14/19 16:4510.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)84 %11/15/19 23:56 4165-60-011/14/19 16:4513-130 1
2-Fluorobiphenyl (S)74 %11/15/19 23:56 321-60-811/14/19 16:4513-130 1
Terphenyl-d14 (S)79 %11/15/19 23:56 1718-51-011/14/19 16:4525-130 1
Phenol-d6 (S)54 %11/15/19 23:56 13127-88-311/14/19 16:4510-130 1
2-Fluorophenol (S)68 %11/15/19 23:56 367-12-411/14/19 16:4510-130 1
2,4,6-Tribromophenol (S)91 %11/15/19 23:56 118-79-611/14/19 16:4510-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 11/15/19 09:38 67-64-125.0 6.2 1
Benzene ND ug/L 11/15/19 09:38 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/15/19 09:38 108-86-11.0 0.22 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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Page 10 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:TMW-6 Lab ID:92453168002 Collected:11/09/19 15:20 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Bromochloromethane ND ug/L 11/15/19 09:38 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/15/19 09:38 75-27-41.0 0.26 1
Bromoform ND ug/L 11/15/19 09:38 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/15/19 09:38 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 11/15/19 09:38 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/15/19 09:38 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/15/19 09:38 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/15/19 09:38 75-00-31.0 0.49 1
Chloroform ND ug/L 11/15/19 09:38 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/15/19 09:38 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/15/19 09:38 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/15/19 09:38 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/15/19 09:38 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/15/19 09:38 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/15/19 09:38 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/15/19 09:38 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/15/19 09:38 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/15/19 09:38 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/15/19 09:38 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/15/19 09:38 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/15/19 09:38 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/15/19 09:38 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/15/19 09:38 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 11/15/19 09:38 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/15/19 09:38 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/15/19 09:38 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/15/19 09:38 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/15/19 09:38 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/15/19 09:38 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/15/19 09:38 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/15/19 09:38 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/15/19 09:38 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/15/19 09:38 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/15/19 09:38 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/15/19 09:38 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/15/19 09:38 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/15/19 09:38 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/15/19 09:38 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/15/19 09:38 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/15/19 09:38 91-20-31.0 0.35 1
Styrene ND ug/L 11/15/19 09:38 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/15/19 09:38 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 11/15/19 09:38 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/15/19 09:38 127-18-41.0 0.16 1
Toluene ND ug/L 11/15/19 09:38 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/15/19 09:38 87-61-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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Page 11 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:TMW-6 Lab ID:92453168002 Collected:11/09/19 15:20 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
1,2,4-Trichlorobenzene ND ug/L 11/15/19 09:38 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/15/19 09:38 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/15/19 09:38 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/15/19 09:38 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/15/19 09:38 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/15/19 09:38 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/15/19 09:38 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/15/19 09:38 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/15/19 09:38 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/15/19 09:38 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/15/19 09:38 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %11/15/19 09:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %11/15/19 09:38 17060-07-070-130 1
Toluene-d8 (S)103 %11/15/19 09:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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Page 12 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:DUP-4 Lab ID:92453168003 Collected:11/09/19 00:00 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 11/16/19 00:21 83-32-911/14/19 16:4510.0 1.6 1
Acenaphthylene ND ug/L 11/16/19 00:21 208-96-811/14/19 16:4510.0 1.6 1
Aniline ND ug/L 11/16/19 00:21 62-53-311/14/19 16:4510.0 1.9 1
Anthracene ND ug/L 11/16/19 00:21 120-12-711/14/19 16:4510.0 1.7 1
Benzo(a)anthracene ND ug/L 11/16/19 00:21 56-55-311/14/19 16:4510.0 1.8 1
Benzo(a)pyrene ND ug/L 11/16/19 00:21 50-32-811/14/19 16:4510.0 2.1 1
Benzo(b)fluoranthene ND ug/L 11/16/19 00:21 205-99-211/14/19 16:4510.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 11/16/19 00:21 191-24-211/14/19 16:4510.0 1.4 1
Benzo(k)fluoranthene ND ug/L 11/16/19 00:21 207-08-911/14/19 16:4510.0 1.9 1
Benzoic Acid ND ug/L 11/16/19 00:21 65-85-011/14/19 16:4550.0 43.0 1
Benzyl alcohol ND ug/L 11/16/19 00:21 100-51-611/14/19 16:4520.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 11/16/19 00:21 101-55-311/14/19 16:4510.0 1.6 1
Butylbenzylphthalate ND ug/L 11/16/19 00:21 85-68-711/14/19 16:4510.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 11/16/19 00:21 59-50-711/14/19 16:4520.0 2.8 1
4-Chloroaniline ND ug/L 11/16/19 00:21 106-47-811/14/19 16:4520.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 11/16/19 00:21 111-91-111/14/19 16:4510.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 11/16/19 00:21 111-44-411/14/19 16:4510.0 1.8 1
2-Chloronaphthalene ND ug/L 11/16/19 00:21 91-58-711/14/19 16:4510.0 1.5 1
2-Chlorophenol ND ug/L 11/16/19 00:21 95-57-811/14/19 16:4510.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 11/16/19 00:21 7005-72-311/14/19 16:4510.0 1.6 1
Chrysene ND ug/L 11/16/19 00:21 218-01-911/14/19 16:4510.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 11/16/19 00:21 53-70-311/14/19 16:4510.0 1.6 1
Dibenzofuran ND ug/L 11/16/19 00:21 132-64-911/14/19 16:4510.0 1.5 1
1,2-Dichlorobenzene ND ug/L 11/16/19 00:21 95-50-111/14/19 16:4510.0 1.3 1
1,3-Dichlorobenzene ND ug/L 11/16/19 00:21 541-73-111/14/19 16:4510.0 1.5 1
1,4-Dichlorobenzene ND ug/L 11/16/19 00:21 106-46-711/14/19 16:4510.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 11/16/19 00:21 91-94-111/14/19 16:4520.0 3.0 1
2,4-Dichlorophenol ND ug/L 11/16/19 00:21 120-83-211/14/19 16:4510.0 1.4 1
Diethylphthalate ND ug/L 11/16/19 00:21 84-66-211/14/19 16:4510.0 2.4 1
2,4-Dimethylphenol ND ug/L 11/16/19 00:21 105-67-911/14/19 16:4510.0 1.4 1
Dimethylphthalate ND ug/L 11/16/19 00:21 131-11-311/14/19 16:4510.0 1.6 1
Di-n-butylphthalate ND ug/L 11/16/19 00:21 84-74-211/14/19 16:4510.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 11/16/19 00:21 534-52-111/14/19 16:4520.0 15.2 1
2,4-Dinitrophenol ND ug/L 11/16/19 00:21 51-28-511/14/19 16:4550.0 40.5 1
2,4-Dinitrotoluene ND ug/L 11/16/19 00:21 121-14-211/14/19 16:4510.0 1.2 1
2,6-Dinitrotoluene ND ug/L 11/16/19 00:21 606-20-211/14/19 16:4510.0 1.4 1
Di-n-octylphthalate ND ug/L 11/16/19 00:21 117-84-011/14/19 16:4510.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/16/19 00:21 117-81-711/14/19 16:456.0 2.1 1
Fluoranthene ND ug/L 11/16/19 00:21 206-44-011/14/19 16:4510.0 1.7 1
Fluorene ND ug/L 11/16/19 00:21 86-73-711/14/19 16:4510.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 11/16/19 00:21 87-68-311/14/19 16:4510.0 2.0 1
Hexachlorobenzene ND ug/L 11/16/19 00:21 118-74-111/14/19 16:4510.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 11/16/19 00:21 77-47-411/14/19 16:4510.0 1.7 1
Hexachloroethane ND ug/L 11/16/19 00:21 67-72-111/14/19 16:4510.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/16/19 00:21 193-39-511/14/19 16:4510.0 1.6 1
Isophorone ND ug/L 11/16/19 00:21 78-59-111/14/19 16:4510.0 1.6 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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Page 13 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92453168
LEH-004
Sample:DUP-4 Lab ID:92453168003 Collected:11/09/19 00:00 Received:11/11/19 13:43 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
1-Methylnaphthalene ND ug/L 11/16/19 00:21 90-12-011/14/19 16:4510.0 1.4 1
2-Methylnaphthalene ND ug/L 11/16/19 00:21 91-57-611/14/19 16:4510.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 11/16/19 00:21 95-48-711/14/19 16:4510.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 11/16/19 00:21 15831-10-411/14/19 16:4510.0 1.2 1
Naphthalene ND ug/L 11/16/19 00:21 91-20-311/14/19 16:4510.0 1.4 1
2-Nitroaniline ND ug/L 11/16/19 00:21 88-74-411/14/19 16:4520.0 4.2 1
3-Nitroaniline ND ug/L 11/16/19 00:21 99-09-211/14/19 16:4520.0 2.3 1
4-Nitroaniline ND ug/L 11/16/19 00:21 100-01-611/14/19 16:4520.0 2.2 1
Nitrobenzene ND ug/L 11/16/19 00:21 98-95-311/14/19 16:4510.0 2.1 1
2-Nitrophenol ND ug/L 11/16/19 00:21 88-75-511/14/19 16:4510.0 1.4 1
4-Nitrophenol ND ug/L 11/16/19 00:21 100-02-711/14/19 16:4550.0 3.5 1
N-Nitrosodimethylamine ND ug/L 11/16/19 00:21 62-75-911/14/19 16:4510.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 11/16/19 00:21 621-64-711/14/19 16:4510.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 11/16/19 00:21 86-30-611/14/19 16:4510.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 11/16/19 00:21 108-60-111/14/19 16:4510.0 2.8 1
Pentachlorophenol ND ug/L 11/16/19 00:21 87-86-511/14/19 16:4525.0 2.2 1
Phenanthrene ND ug/L 11/16/19 00:21 85-01-811/14/19 16:4510.0 1.7 1
Phenol ND ug/L 11/16/19 00:21 108-95-211/14/19 16:4510.0 0.92 1
Pyrene ND ug/L 11/16/19 00:21 129-00-011/14/19 16:4510.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 11/16/19 00:21 120-82-111/14/19 16:4510.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 11/16/19 00:21 95-95-411/14/19 16:4510.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 11/16/19 00:21 88-06-211/14/19 16:4510.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)72 %11/16/19 00:21 4165-60-011/14/19 16:4513-130 1
2-Fluorobiphenyl (S)63 %11/16/19 00:21 321-60-811/14/19 16:4513-130 1
Terphenyl-d14 (S)81 %11/16/19 00:21 1718-51-011/14/19 16:4525-130 1
Phenol-d6 (S)46 %11/16/19 00:21 13127-88-311/14/19 16:4510-130 1
2-Fluorophenol (S)58 %11/16/19 00:21 367-12-411/14/19 16:4510-130 1
2,4,6-Tribromophenol (S)78 %11/16/19 00:21 118-79-611/14/19 16:4510-137 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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Page 14 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1380949
3015
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples:92453168001, 92453168002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3472683-1
Associated Lab Samples:92453168001, 92453168002
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 2.00 11/16/19 11:450.250
Barium ug/L ND 5.00 11/16/19 11:450.360
Cadmium ug/L ND 1.00 11/16/19 11:450.160
Chromium ug/L ND 2.00 11/16/19 11:450.540
Lead ug/L 0.895J 2.00 J11/16/19 11:450.240
Selenium ug/L ND 2.00 11/16/19 11:450.380
Silver ug/L ND 2.00 11/16/19 11:450.310
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3472683-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3472683-3
Arsenic ug/L 49.050.0 98.0 80.0-12010150.5 3.06 20
Barium ug/L 47.950.0 95.7 80.0-12092.546.2 3.45 20
Cadmium ug/L 47.450.0 94.8 80.0-12098.749.4 4.07 20
Chromium ug/L 49.250.0 98.4 80.0-12010351.4 4.39 20
Lead ug/L 48.150.0 96.2 80.0-12097.148.5 0.958 20
Selenium ug/L 47.750.0 95.5 80.0-12098.549.3 3.15 20
Silver ug/L 50.050.0 100 80.0-12010351.5 2.94 20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1380155
7470A
EPA 7470A
Mercury 7470A
Associated Lab Samples:92453168001, 92453168002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3472009-1
Associated Lab Samples:92453168001, 92453168002
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.200 11/14/19 13:440.0490
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3472009-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3472009-3
Mercury ug/L 3.223.00 107 80.0-1201013.03 5.87 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3472009-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1160439-11
R3472009-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 3.00 113 75.0-125113 0.485 203.00ND 3.39 3.38
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
509616
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples:92453168001, 92453168002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2734999
Associated Lab Samples:92453168001, 92453168002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/15/19 02:100.34
1,1,1-Trichloroethane ug/L ND 1.0 11/15/19 02:100.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/15/19 02:100.22
1,1,2-Trichloroethane ug/L ND 1.0 11/15/19 02:100.24
1,1-Dichloroethane ug/L ND 1.0 11/15/19 02:100.27
1,1-Dichloroethene ug/L ND 1.0 11/15/19 02:100.24
1,1-Dichloropropene ug/L ND 1.0 11/15/19 02:100.21
1,2,3-Trichlorobenzene ug/L ND 1.0 11/15/19 02:100.34
1,2,3-Trichloropropane ug/L ND 1.0 11/15/19 02:100.35
1,2,4-Trichlorobenzene ug/L ND 1.0 11/15/19 02:100.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 11/15/19 02:100.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/15/19 02:100.26
1,2-Dichlorobenzene ug/L ND 1.0 11/15/19 02:100.29
1,2-Dichloroethane ug/L ND 1.0 11/15/19 02:100.34
1,2-Dichloropropane ug/L ND 1.0 11/15/19 02:100.19
1,3-Dichlorobenzene ug/L ND 1.0 11/15/19 02:100.22
1,3-Dichloropropane ug/L ND 1.0 11/15/19 02:100.16
1,4-Dichlorobenzene ug/L ND 1.0 11/15/19 02:100.26
2,2-Dichloropropane ug/L ND 1.0 11/15/19 02:100.27
2-Butanone (MEK)ug/L ND 5.0 11/15/19 02:103.3
2-Chlorotoluene ug/L ND 1.0 11/15/19 02:100.20
2-Hexanone ug/L ND 5.0 11/15/19 02:100.57
4-Chlorotoluene ug/L ND 1.0 11/15/19 02:100.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/15/19 02:104.5
Acetone ug/L ND 25.0 11/15/19 02:106.2
Benzene ug/L ND 1.0 11/15/19 02:100.15
Bromobenzene ug/L ND 1.0 11/15/19 02:100.22
Bromochloromethane ug/L ND 1.0 11/15/19 02:100.34
Bromodichloromethane ug/L ND 1.0 11/15/19 02:100.26
Bromoform ug/L ND 1.0 11/15/19 02:100.62
Bromomethane ug/L ND 2.0 v211/15/19 02:100.62
Carbon tetrachloride ug/L ND 1.0 11/15/19 02:100.22
Chlorobenzene ug/L ND 1.0 11/15/19 02:100.23
Chloroethane ug/L ND 1.0 11/15/19 02:100.49
Chloroform ug/L ND 5.0 11/15/19 02:102.3
Chloromethane ug/L ND 1.0 11/15/19 02:100.39
cis-1,2-Dichloroethene ug/L ND 1.0 11/15/19 02:100.29
cis-1,3-Dichloropropene ug/L ND 1.0 11/15/19 02:100.30
Dibromochloromethane ug/L ND 1.0 11/15/19 02:100.41
Dibromomethane ug/L ND 1.0 11/15/19 02:100.46
Dichlorodifluoromethane ug/L ND 1.0 11/15/19 02:100.23
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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Page 17 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2734999
Associated Lab Samples:92453168001, 92453168002
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 11/15/19 02:100.22
Ethylbenzene ug/L ND 1.0 11/15/19 02:100.26
Hexachloro-1,3-butadiene ug/L ND 1.0 11/15/19 02:100.44
m&p-Xylene ug/L ND 2.0 11/15/19 02:100.41
Methyl-tert-butyl ether ug/L ND 1.0 11/15/19 02:100.28
Methylene Chloride ug/L ND 5.0 11/15/19 02:103.7
Naphthalene ug/L ND 1.0 11/15/19 02:100.35
o-Xylene ug/L ND 1.0 11/15/19 02:100.22
p-Isopropyltoluene ug/L ND 1.0 11/15/19 02:100.21
Styrene ug/L ND 1.0 11/15/19 02:100.27
Tetrachloroethene ug/L ND 1.0 11/15/19 02:100.16
Toluene ug/L ND 1.0 11/15/19 02:100.24
trans-1,2-Dichloroethene ug/L ND 1.0 11/15/19 02:100.25
trans-1,3-Dichloropropene ug/L ND 1.0 11/15/19 02:100.31
Trichloroethene ug/L ND 1.0 11/15/19 02:100.22
Trichlorofluoromethane ug/L ND 1.0 11/15/19 02:100.31
Vinyl acetate ug/L ND 2.0 11/15/19 02:101.4
Vinyl chloride ug/L ND 1.0 11/15/19 02:100.24
Xylene (Total)ug/L ND 1.0 11/15/19 02:100.63
1,2-Dichloroethane-d4 (S)%102 70-130 11/15/19 02:10
4-Bromofluorobenzene (S)%101 70-130 11/15/19 02:10
Toluene-d8 (S)%100 70-130 11/15/19 02:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2735000LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.550 109 70-130
1,1,1-Trichloroethane ug/L 52.450 105 70-130
1,1,2,2-Tetrachloroethane ug/L 51.550 103 70-130
1,1,2-Trichloroethane ug/L 52.850 106 70-130
1,1-Dichloroethane ug/L 53.150 106 70-130
1,1-Dichloroethene ug/L 53.050 106 70-130
1,1-Dichloropropene ug/L 56.650 113 70-130
1,2,3-Trichlorobenzene ug/L 53.750 107 70-130
1,2,3-Trichloropropane ug/L 53.550 107 70-130
1,2,4-Trichlorobenzene ug/L 53.650 107 70-130
1,2-Dibromo-3-chloropropane ug/L 55.950 112 70-130
1,2-Dibromoethane (EDB)ug/L 53.450 107 70-130
1,2-Dichlorobenzene ug/L 50.950 102 70-130
1,2-Dichloroethane ug/L 49.350 99 70-130
1,2-Dichloropropane ug/L 52.350 105 70-130
1,3-Dichlorobenzene ug/L 50.950 102 70-130
1,3-Dichloropropane ug/L 52.950 106 70-131
1,4-Dichlorobenzene ug/L 50.450 101 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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Page 18 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2735000LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 52.550 105 69-130
2-Butanone (MEK)ug/L 107100 107 64-135
2-Chlorotoluene ug/L 50.250 100 70-130
2-Hexanone ug/L 105100 105 66-135
4-Chlorotoluene ug/L 50.550 101 70-130
4-Methyl-2-pentanone (MIBK)ug/L 105100 105 70-130
Acetone ug/L 108100 108 61-157
Benzene ug/L 51.250 102 70-130
Bromobenzene ug/L 52.250 104 70-130
Bromochloromethane ug/L 54.450 109 70-130
Bromodichloromethane ug/L 52.250 104 70-130
Bromoform ug/L 55.850 112 70-130
Bromomethane ug/L 45.9 v3509238-130
Carbon tetrachloride ug/L 51.950 104 70-130
Chlorobenzene ug/L 50.650 101 70-130
Chloroethane ug/L 42.550 85 37-142
Chloroform ug/L 52.750 105 70-130
Chloromethane ug/L 48.050 96 48-130
cis-1,2-Dichloroethene ug/L 52.550 105 70-130
cis-1,3-Dichloropropene ug/L 56.150 112 70-130
Dibromochloromethane ug/L 53.650 107 70-130
Dibromomethane ug/L 53.150 106 70-130
Dichlorodifluoromethane ug/L 48.850 98 53-134
Diisopropyl ether ug/L 54.050 108 70-135
Ethylbenzene ug/L 51.150 102 70-130
Hexachloro-1,3-butadiene ug/L 52.150 104 68-132
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 52.150 104 70-130
Methylene Chloride ug/L 50.850 102 67-132
Naphthalene ug/L 54.150 108 70-130
o-Xylene ug/L 52.250 104 70-131
p-Isopropyltoluene ug/L 52.750 105 70-130
Styrene ug/L 53.850 108 70-130
Tetrachloroethene ug/L 53.050 106 69-130
Toluene ug/L 51.150 102 70-130
trans-1,2-Dichloroethene ug/L 52.850 106 70-130
trans-1,3-Dichloropropene ug/L 54.650 109 70-130
Trichloroethene ug/L 52.050 104 70-130
Trichlorofluoromethane ug/L 48.850 98 63-130
Vinyl acetate ug/L 113100 113 55-143
Vinyl chloride ug/L 56.450 113 70-131
Xylene (Total)ug/L 153150 102 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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Page 19 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2735676MATRIX SPIKE SAMPLE:
MSSpike
Result
92453163003
1,1,1,2-Tetrachloroethane ug/L 22.120 111 73-134ND
1,1,1-Trichloroethane ug/L 24.520 122 82-143ND
1,1,2,2-Tetrachloroethane ug/L 19.920 99 70-136ND
1,1,2-Trichloroethane ug/L 22.820 114 70-135ND
1,1-Dichloroethane ug/L 24.520 122 70-139ND
1,1-Dichloroethene ug/L 24.320 122 70-154ND
1,1-Dichloropropene ug/L 26.520 132 70-149ND
1,2,3-Trichlorobenzene ug/L 21.020 105 70-135ND
1,2,3-Trichloropropane ug/L 20.420 102 71-137ND
1,2,4-Trichlorobenzene ug/L 20.320 102 73-140ND
1,2-Dibromo-3-chloropropane ug/L 21.320 106 65-134ND
1,2-Dibromoethane (EDB)ug/L 21.920 109 70-137ND
1,2-Dichlorobenzene ug/L 21.420 107 70-133ND
1,2-Dichloroethane ug/L 23.220 116 70-137ND
1,2-Dichloropropane ug/L 23.720 118 70-140ND
1,3-Dichlorobenzene ug/L 21.220 106 70-135ND
1,3-Dichloropropane ug/L 22.620 113 70-143ND
1,4-Dichlorobenzene ug/L 21.120 106 70-133ND
2,2-Dichloropropane ug/L 22.520 113 61-148ND
2-Butanone (MEK)ug/L 47.540 119 60-139ND
2-Chlorotoluene ug/L 20.420 102 70-144ND
2-Hexanone ug/L 39.940 100 65-138ND
4-Chlorotoluene ug/L 20.720 103 70-137ND
4-Methyl-2-pentanone (MIBK)ug/L 40.940 102 65-135ND
Acetone ug/L 44.440 111 60-148ND
Benzene ug/L 23.720 118 70-151ND
Bromobenzene ug/L 22.420 112 70-136ND
Bromochloromethane ug/L 24.720 123 70-141ND
Bromodichloromethane ug/L 23.120 115 70-138ND
Bromoform ug/L 21.320 107 63-130ND
Bromomethane ug/L 24.020 120 15-152ND
Carbon tetrachloride ug/L 23.420 117 70-143ND
Chlorobenzene ug/L 21.920 110 70-138ND
Chloroethane ug/L 21.720 109 52-163ND
Chloroform ug/L 24.920 124 70-139ND
Chloromethane ug/L 21.820 109 41-139ND
cis-1,2-Dichloroethene ug/L 23.720 118 70-141ND
cis-1,3-Dichloropropene ug/L 23.420 117 70-137ND
Dibromochloromethane ug/L 21.220 106 70-134ND
Dibromomethane ug/L 23.420 117 70-138ND
Dichlorodifluoromethane ug/L 24.220 121 47-155ND
Diisopropyl ether ug/L 23.820 119 63-144ND
Ethylbenzene ug/L 22.120 110 66-153ND
Hexachloro-1,3-butadiene ug/L 19.320 96 65-149ND
m&p-Xylene ug/L 43.940 110 69-152ND
Methyl-tert-butyl ether ug/L 23.520 117 54-156ND
Methylene Chloride ug/L 24.720 123 42-159ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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9800 Kincey Ave. Suite 100
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Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2735676MATRIX SPIKE SAMPLE:
MSSpike
Result
92453163003
Naphthalene ug/L 19.420 97 61-148ND
o-Xylene ug/L 22.020 110 70-148ND
p-Isopropyltoluene ug/L 21.620 108 70-146ND
Styrene ug/L 22.020 110 70-135ND
Tetrachloroethene ug/L 21.620 108 59-143ND
Toluene ug/L 22.720 114 59-148ND
trans-1,2-Dichloroethene ug/L 25.220 126 70-146ND
trans-1,3-Dichloropropene ug/L 22.620 113 70-135ND
Trichloroethene ug/L 22.820 114 70-147ND
Trichlorofluoromethane ug/L 22.420 111 70-148ND
Vinyl acetate ug/L 46.340 116 49-151ND
Vinyl chloride ug/L 25.620 128 70-156ND
Xylene (Total)ug/L 65.860 110 63-158ND
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92453163005
2735677SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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[phone]
Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92453163005
2735677SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%106107
4-Bromofluorobenzene (S)%91101
Toluene-d8 (S)%101100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
Pace Analytical Services, LLC
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Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
509556
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Associated Lab Samples:92453168001, 92453168002, 92453168003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2734531
Associated Lab Samples:92453168001, 92453168002, 92453168003
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 11/15/19 17:111.5
1,2-Dichlorobenzene ug/L ND 10.0 11/15/19 17:111.3
1,3-Dichlorobenzene ug/L ND 10.0 11/15/19 17:111.5
1,4-Dichlorobenzene ug/L ND 10.0 11/15/19 17:112.1
1-Methylnaphthalene ug/L ND 10.0 11/15/19 17:111.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 11/15/19 17:112.8
2,4,5-Trichlorophenol ug/L ND 10.0 11/15/19 17:111.4
2,4,6-Trichlorophenol ug/L ND 10.0 11/15/19 17:111.5
2,4-Dichlorophenol ug/L ND 10.0 11/15/19 17:111.4
2,4-Dimethylphenol ug/L ND 10.0 11/15/19 17:111.4
2,4-Dinitrophenol ug/L ND 50.0 11/15/19 17:1140.5
2,4-Dinitrotoluene ug/L ND 10.0 11/15/19 17:111.2
2,6-Dinitrotoluene ug/L ND 10.0 11/15/19 17:111.4
2-Chloronaphthalene ug/L ND 10.0 11/15/19 17:111.5
2-Chlorophenol ug/L ND 10.0 11/15/19 17:111.2
2-Methylnaphthalene ug/L ND 10.0 11/15/19 17:111.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 11/15/19 17:111.2
2-Nitroaniline ug/L ND 20.0 11/15/19 17:114.2
2-Nitrophenol ug/L ND 10.0 11/15/19 17:111.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 11/15/19 17:111.2
3,3'-Dichlorobenzidine ug/L ND 20.0 11/15/19 17:113.0
3-Nitroaniline ug/L ND 20.0 11/15/19 17:112.3
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/15/19 17:1115.2
4-Bromophenylphenyl ether ug/L ND 10.0 11/15/19 17:111.6
4-Chloro-3-methylphenol ug/L ND 20.0 11/15/19 17:112.8
4-Chloroaniline ug/L ND 20.0 11/15/19 17:112.8
4-Chlorophenylphenyl ether ug/L ND 10.0 11/15/19 17:111.6
4-Nitroaniline ug/L ND 20.0 11/15/19 17:112.2
4-Nitrophenol ug/L ND 50.0 11/15/19 17:113.5
Acenaphthene ug/L ND 10.0 11/15/19 17:111.6
Acenaphthylene ug/L ND 10.0 11/15/19 17:111.6
Aniline ug/L ND 10.0 11/15/19 17:111.9
Anthracene ug/L ND 10.0 11/15/19 17:111.7
Benzo(a)anthracene ug/L ND 10.0 11/15/19 17:111.8
Benzo(a)pyrene ug/L ND 10.0 11/15/19 17:112.1
Benzo(b)fluoranthene ug/L ND 10.0 11/15/19 17:111.9
Benzo(g,h,i)perylene ug/L ND 10.0 11/15/19 17:111.4
Benzo(k)fluoranthene ug/L ND 10.0 11/15/19 17:111.9
Benzoic Acid ug/L ND 50.0 11/15/19 17:1143.0
Benzyl alcohol ug/L ND 20.0 11/15/19 17:112.6
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/15/19 17:111.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/19/2019 04:24 PM
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[phone]
Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2734531
Associated Lab Samples:92453168001, 92453168002, 92453168003
Matrix:Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 11/15/19 17:111.8
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/15/19 17:112.1
Butylbenzylphthalate ug/L ND 10.0 11/15/19 17:111.6
Chrysene ug/L ND 10.0 11/15/19 17:111.7
Di-n-butylphthalate ug/L ND 10.0 11/15/19 17:111.8
Di-n-octylphthalate ug/L ND 10.0 11/15/19 17:111.8
Dibenz(a,h)anthracene ug/L ND 10.0 11/15/19 17:111.6
Dibenzofuran ug/L ND 10.0 11/15/19 17:111.5
Diethylphthalate ug/L ND 10.0 11/15/19 17:112.4
Dimethylphthalate ug/L ND 10.0 11/15/19 17:111.6
Fluoranthene ug/L ND 10.0 11/15/19 17:111.7
Fluorene ug/L ND 10.0 11/15/19 17:111.6
Hexachloro-1,3-butadiene ug/L ND 10.0 11/15/19 17:112.0
Hexachlorobenzene ug/L ND 10.0 11/15/19 17:111.7
Hexachlorocyclopentadiene ug/L ND 10.0 11/15/19 17:111.7
Hexachloroethane ug/L ND 10.0 11/15/19 17:112.0
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/15/19 17:111.6
Isophorone ug/L ND 10.0 11/15/19 17:111.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 11/15/19 17:112.2
N-Nitrosodimethylamine ug/L ND 10.0 11/15/19 17:111.2
N-Nitrosodiphenylamine ug/L ND 10.0 11/15/19 17:111.7
Naphthalene ug/L ND 10.0 11/15/19 17:111.4
Nitrobenzene ug/L ND 10.0 11/15/19 17:112.1
Pentachlorophenol ug/L ND 25.0 11/15/19 17:112.2
Phenanthrene ug/L ND 10.0 11/15/19 17:111.7
Phenol ug/L ND 10.0 11/15/19 17:110.92
Pyrene ug/L ND 10.0 11/15/19 17:112.1
2,4,6-Tribromophenol (S)%76 10-137 11/15/19 17:11
2-Fluorobiphenyl (S)%70 13-130 11/15/19 17:11
2-Fluorophenol (S)%67 10-130 11/15/19 17:11
Nitrobenzene-d5 (S)%70 13-130 11/15/19 17:11
Phenol-d6 (S)%53 10-130 11/15/19 17:11
Terphenyl-d14 (S)%85 25-130 11/15/19 17:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2734532LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 28.050 56 30-130
1,2-Dichlorobenzene ug/L 29.550 59 30-130
1,3-Dichlorobenzene ug/L 29.450 59 20-130
1,4-Dichlorobenzene ug/L 29.450 59 30-130
1-Methylnaphthalene ug/L 30.850 62 30-130
2,2'-Oxybis(1-chloropropane)ug/L 31.150 62 20-130
2,4,5-Trichlorophenol ug/L 29.850 60 40-130
REPORT OF LABORATORY ANALYSIS
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Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2734532LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 31.250 62 40-130
2,4-Dichlorophenol ug/L 29.750 59 31-130
2,4-Dimethylphenol ug/L 31.450 63 30-130
2,4-Dinitrophenol ug/L 168250 67 30-130
2,4-Dinitrotoluene ug/L 34.550 69 49-130
2,6-Dinitrotoluene ug/L 33.550 67 50-130
2-Chloronaphthalene ug/L 30.050 60 30-130
2-Chlorophenol ug/L 31.650 63 30-130
2-Methylnaphthalene ug/L 30.350 61 30-130
2-Methylphenol(o-Cresol)ug/L 29.650 59 30-130
2-Nitroaniline ug/L 71.1100 71 40-130
2-Nitrophenol ug/L 31.450 63 20-130
3&4-Methylphenol(m&p Cresol)ug/L 29.550 59 20-130
3,3'-Dichlorobenzidine ug/L 54.0100 54 10-150
3-Nitroaniline ug/L 67.8100 68 40-130
4,6-Dinitro-2-methylphenol ug/L 73.9100 74 40-130
4-Bromophenylphenyl ether ug/L 29.050 58 30-130
4-Chloro-3-methylphenol ug/L 66.2100 66 30-130
4-Chloroaniline ug/L 65.7100 66 20-130
4-Chlorophenylphenyl ether ug/L 29.650 59 20-130
4-Nitroaniline ug/L 66.1100 66 40-130
4-Nitrophenol ug/L 122250 49 10-130
Acenaphthene ug/L 31.850 64 30-130
Acenaphthylene ug/L 34.150 68 30-130
Aniline ug/L 30.050 60 20-130
Anthracene ug/L 34.250 68 50-130
Benzo(a)anthracene ug/L 34.650 69 50-130
Benzo(a)pyrene ug/L 36.750 73 50-130
Benzo(b)fluoranthene ug/L 35.250 70 50-130
Benzo(g,h,i)perylene ug/L 35.450 71 50-130
Benzo(k)fluoranthene ug/L 35.250 70 50-130
Benzoic Acid ug/L 94.3250 38 10-130
Benzyl alcohol ug/L 63.7100 64 20-130
bis(2-Chloroethoxy)methane ug/L 31.250 62 30-130
bis(2-Chloroethyl) ether ug/L 32.150 64 30-130
bis(2-Ethylhexyl)phthalate ug/L 38.150 76 50-130
Butylbenzylphthalate ug/L 36.850 74 50-150
Chrysene ug/L 33.050 66 50-130
Di-n-butylphthalate ug/L 34.950 70 50-130
Di-n-octylphthalate ug/L 39.150 78 50-130
Dibenz(a,h)anthracene ug/L 34.750 69 40-130
Dibenzofuran ug/L 30.550 61 40-130
Diethylphthalate ug/L 33.250 66 40-130
Dimethylphthalate ug/L 31.750 63 40-130
Fluoranthene ug/L 34.050 68 30-130
Fluorene ug/L 32.450 65 20-130
Hexachloro-1,3-butadiene ug/L 26.950 54 10-130
REPORT OF LABORATORY ANALYSIS
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Page 25 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2734532LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 29.350 59 30-130
Hexachlorocyclopentadiene ug/L 32.550 65 10-150
Hexachloroethane ug/L 30.750 61 10-130
Indeno(1,2,3-cd)pyrene ug/L 34.850 70 40-130
Isophorone ug/L 32.750 65 30-130
N-Nitroso-di-n-propylamine ug/L 32.950 66 30-130
N-Nitrosodimethylamine ug/L 31.950 64 10-130
N-Nitrosodiphenylamine ug/L 31.250 62 30-130
Naphthalene ug/L 30.850 62 20-130
Nitrobenzene ug/L 31.650 63 20-130
Pentachlorophenol ug/L 62.6100 63 10-140
Phenanthrene ug/L 32.250 64 50-130
Phenol ug/L 22.150 44 10-130
Pyrene ug/L 33.850 68 50-130
2,4,6-Tribromophenol (S)%63 10-137
2-Fluorobiphenyl (S)%56 13-130
2-Fluorophenol (S)%57 10-130
Nitrobenzene-d5 (S)%58 13-130
Phenol-d6 (S)%45 10-130
Terphenyl-d14 (S)%61 25-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2734533MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92453160011
2734534
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 82 30-13078 6 3050ND41.2 38.9
1,2-Dichlorobenzene ug/L 50 86 30-13081 6 3050ND43.1 40.6
1,3-Dichlorobenzene ug/L 50 84 20-13080 6 3050ND42.2 39.8
1,4-Dichlorobenzene ug/L 50 85 30-13080 6 3050ND42.5 39.8
1-Methylnaphthalene ug/L 50 92 30-13089 3 3050ND45.9 44.6
2,2'-Oxybis(1-
chloropropane)ug/L 50 89 20-13087 3 3050ND44.7 43.5
2,4,5-Trichlorophenol ug/L 50 86 40-13085 2 3050ND43.1 42.3
2,4,6-Trichlorophenol ug/L 50 91 40-13088 3 3050ND45.5 44.1
2,4-Dichlorophenol ug/L 50 87 31-13084 4 3050ND43.4 41.8
2,4-Dimethylphenol ug/L 50 93 30-13088 5 3050ND46.4 44.0
2,4-Dinitrophenol ug/L 250 102 30-130100 2 30250ND255251
2,4-Dinitrotoluene ug/L 50 103 49-130103 0 3050ND51.3 51.3
2,6-Dinitrotoluene ug/L 50 102 50-130100 2 3050ND50.9 49.9
2-Chloronaphthalene ug/L 50 89 30-13086 3 3050ND44.4 42.9
2-Chlorophenol ug/L 50 88 30-13087 1 3050ND43.9 43.4
2-Methylnaphthalene ug/L 50 90 30-13088 3 3050ND45.1 44.0
2-Methylphenol(o-Cresol)ug/L 50 87 30-13081 7 3050ND43.3 40.4
2-Nitroaniline ug/L 100 106 40-130104 2 30100ND106104
2-Nitrophenol ug/L 50 92 20-13089 3 3050ND46.1 44.6
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2734533MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92453160011
2734534
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/L 50 85 20-13080 6 3050ND42.6 40.1
3,3'-Dichlorobenzidine ug/L 100 93 10-15084 9 30100ND92.5 84.2
3-Nitroaniline ug/L 100 102 40-130101 1 30100ND102101
4,6-Dinitro-2-methylphenol ug/L 100 115 40-130109 6 30100ND115109
4-Bromophenylphenyl ether ug/L 50 87 30-13084 4 3050ND43.5 41.8
4-Chloro-3-methylphenol ug/L 100 96 30-13093 4 30100ND96.2 92.5
4-Chloroaniline ug/L 100 91 20-13087 5 30100ND90.7 86.5
4-Chlorophenylphenyl ether ug/L 50 88 20-13086 3 3050ND44.1 42.8
4-Nitroaniline ug/L 100 101 40-13099 2 30100ND10199.4
4-Nitrophenol ug/L 250 78 10-13072 7 30250ND195181
Acenaphthene ug/L 50 93 30-13091 2 3050ND46.4 45.7
Acenaphthylene ug/L 50 102 30-130100 2 3050ND51.0 49.9
Aniline ug/L 50 74 20-13073 2 3050ND37.1 36.3
Anthracene ug/L 50 105 50-130102 3 3050ND52.6 50.8
Benzo(a)anthracene ug/L 50 105 50-130102 3 3050ND52.4 51.0
Benzo(a)pyrene ug/L 50 110 50-130108 1 3050ND55.0 54.2
Benzo(b)fluoranthene ug/L 50 105 50-130101 5 3050ND52.7 50.3
Benzo(g,h,i)perylene ug/L 50 101 50-130100 1 3050ND50.5 50.2
Benzo(k)fluoranthene ug/L 50 104 50-130103 2 3050ND52.1 51.3
Benzoic Acid ug/L 250 65 10-13065 1 30250ND163164
Benzyl alcohol ug/L 100 91 20-13089 2 30100ND91.5 89.5
bis(2-
Chloroethoxy)methane ug/L 50 90 30-13089 2 3050ND45.1 44.3
bis(2-Chloroethyl) ether ug/L 50 90 30-13090 1 3050ND45.2 44.9
bis(2-Ethylhexyl)phthalate ug/L 50 120 50-130112 7 3050ND60.2 56.0
Butylbenzylphthalate ug/L 50 117 50-150111 5 3050ND58.3 55.6
Chrysene ug/L 50 98 50-13095 3 3050ND49.2 47.6
Di-n-butylphthalate ug/L 50 108 50-130103 5 3050ND54.2 51.6
Di-n-octylphthalate ug/L 50 127 50-130119 6 3050ND63.6 59.7
Dibenz(a,h)anthracene ug/L 50 102 40-130100 2 3050ND50.9 50.0
Dibenzofuran ug/L 50 89 40-13087 2 3050ND44.6 43.7
Diethylphthalate ug/L 50 99 40-13097 2 3050ND49.7 48.7
Dimethylphthalate ug/L 50 93 40-13092 1 3050ND46.5 46.0
Fluoranthene ug/L 50 104 30-130101 3 3050ND51.9 50.4
Fluorene ug/L 50 97 20-13095 2 3050ND48.4 47.4
Hexachloro-1,3-butadiene ug/L 50 79 10-13072 8 3050ND39.3 36.2
Hexachlorobenzene ug/L 50 88 30-13084 5 3050ND44.2 42.1
Hexachlorocyclopentadiene ug/L 50 97 10-15092 5 3050ND48.5 46.1
Hexachloroethane ug/L 50 87 10-13081 7 3050ND43.5 40.6
Indeno(1,2,3-cd)pyrene ug/L 50 103 40-130101 2 3050ND51.5 50.6
Isophorone ug/L 50 98 30-13095 2 3050ND48.9 47.7
N-Nitroso-di-n-propylamine ug/L 50 98 30-13097 1 3050ND49.0 48.5
N-Nitrosodimethylamine ug/L 50 93 10-13089 5 3050ND46.6 44.5
N-Nitrosodiphenylamine ug/L 50 96 30-13091 5 3050ND47.8 45.6
Naphthalene ug/L 50 90 20-13087 4 3050ND45.1 43.4
REPORT OF LABORATORY ANALYSIS
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Page 27 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92453168
LEH-004
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2734533MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92453160011
2734534
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrobenzene ug/L 50 93 20-13091 2 3050ND46.6 45.7
Pentachlorophenol ug/L 100 98 10-14093 5 30100ND98.0 93.5
Phenanthrene ug/L 50 98 50-13095 3 3050ND49.1 47.6
Phenol ug/L 50 72 10-13064 11 3050ND35.8 32.1
Pyrene ug/L 50 104 50-130100 4 3050ND52.1 50.1
2,4,6-Tribromophenol (S)%104 10-13762
2-Fluorobiphenyl (S)%88 13-13054
2-Fluorophenol (S)%87 10-13052
Nitrobenzene-d5 (S)%90 13-13057
Phenol-d6 (S)%79 10-13046
Terphenyl-d14 (S)%101 25-13061
REPORT OF LABORATORY ANALYSIS
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Page 28 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92453168
LEH-004
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 29 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92453168
LEH-004
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92453168001 1380949 1380949TMW-5 3015 EPA 6020B
92453168002 1380949 1380949TMW-6 3015 EPA 6020B
92453168001 1380155 1380155TMW-5 7470A EPA 7470A
92453168002 1380155 1380155TMW-6 7470A EPA 7470A
92453168001 509556 509826TMW-5 EPA 3510C EPA 8270E
92453168002 509556 509826TMW-6 EPA 3510C EPA 8270E
92453168003 509556 509826DUP-4 EPA 3510C EPA 8270E
92453168001 509616TMW-5 EPA 8260D
92453168002 509616TMW-6 EPA 8260D
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Page 30 of 33
Page 31 of 33
Page 32 of 33
Page 33 of 33
#=CL#
November 05, 2019
LIMS USE: FR - ROBERT SORGEL
LIMS OBJECT ID: 92438947
92438947
Project:
Pace Project No.:
RE:
Robert Sorgel
Hart & Hickman
2923 S Tryon Street
Suite 100
Charlotte, NC 28203
LEH-005
Dear Robert Sorgel:
Enclosed are the analytical results for sample(s) received by the laboratory on July 29, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
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Page 1 of 99
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92438947
LEH-005
Pace Analytical National Certification IDs
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92438947
LEH-005
Lab ID Sample ID Matrix Date Collected Date Received
92438947001 SB-1 (8-10)Solid 07/27/19 13:35 07/29/19 06:30
92438947002 SB-2 (3-4)Solid 07/27/19 12:50 07/29/19 06:30
92438947003 SB-3 (0-2)Solid 07/27/19 13:45 07/29/19 06:30
92438947004 SB-4 (0-2)Solid 07/27/19 13:05 07/29/19 06:30
92438947005 SB-5 (0-2)Solid 07/27/19 13:55 07/29/19 06:30
92438947006 SB-6 (2-3)Solid 07/27/19 14:00 07/29/19 06:30
92438947007 SB-7 (0-2)Solid 07/27/19 14:35 07/29/19 06:30
92438947008 SB-8 (7-10)Solid 07/27/19 12:10 07/29/19 06:30
92438947009 SB-9 (7-10)Solid 07/27/19 11:45 07/29/19 06:30
92438947010 SP-10 (7-10)Solid 07/27/19 11:20 07/29/19 06:30
REPORT OF LABORATORY ANALYSIS
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Page 3 of 99
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92438947
LEH-005
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92438947001 SB-1 (8-10)EPA 8015C Modified 2 PASI-CBAJ
MADEP EPH 7 PASI-CSEM
EPA 8015C Modified 2 PASI-CLMB
MADEP VPH 6 PASI-CLMB
EPA 6020B 7 PANJPD
EPA 7471B 1 PANABL
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92438947002 SB-2 (3-4)EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92438947003 SB-3 (0-2)EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92438947004 SB-4 (0-2)EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92438947005 SB-5 (0-2)EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 99
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92438947
LEH-005
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92438947006 SB-6 (2-3)EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92438947007 SB-7 (0-2)EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANLEB
92438947008 SB-8 (7-10)EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CBAJ
EPA 8082A 8 PASI-CSEM
ASTM D2974-87 1 PASI-CKDF
92438947009 SB-9 (7-10)EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CBAJ
ASTM D2974-87 1 PASI-CKDF
92438947010 SP-10 (7-10)EPA 8015C Modified 2 PASI-CBAJ
EPA 8015C Modified 2 PASI-CBAJ
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-1 (8-10)Lab ID:92438947001 Collected:07/27/19 13:35 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)106 mg/kg 08/02/19 10:4808/01/19 12:326.3 2.9 1
Surrogates
n-Pentacosane (S)73 %08/02/19 10:48 629-99-208/01/19 12:3233-129 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)12.5 mg/kg 08/12/19 13:18 N208/07/19 18:3612.4 12.4 1
Aliphatic (C19-C36)ND mg/kg 08/12/19 13:18 N208/07/19 18:3612.4 12.4 1
Aromatic (C11-C22)ND mg/kg 08/12/19 13:18 N208/07/19 18:3612.4 12.4 1
Surrogates
Nonatriacontane (S)71 %08/12/19 13:18 7194-86-708/07/19 18:3640-140 1
o-Terphenyl (S)87 %08/12/19 13:18 84-15-108/07/19 18:3640-140 1
2-Fluorobiphenyl (S)101 %08/12/19 13:18 321-60-808/07/19 18:3640-140 1
2-Bromonaphthalene (S)101 %08/12/19 13:18 580-13-208/07/19 18:3640-140 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030BGasoline Range Organics
Gas Range Organics (C6-C10)799 mg/kg 07/29/19 19:4107/29/19 17:3522.9 4.3 4
Surrogates
4-Bromofluorobenzene (S)248 %07/29/19 19:41 460-00-4 S507/29/19 17:3563-130 4
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)253 mg/kg 08/07/19 14:50 N208/07/19 13:423.0 3.0 1
Aliphatic (C09-C12)327 mg/kg 08/07/19 14:50 N208/07/19 13:423.0 3.0 1
Aliphatic(C09-C12) Adjusted 200 mg/kg 08/07/19 14:50 N208/07/19 13:423.0 3.0 1
Aromatic (C09-C10)126 mg/kg 08/07/19 14:50 N208/07/19 13:423.0 3.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)404 %08/07/19 14:50 460-00-4 S508/07/19 13:4270-130 1
4-Bromofluorobenzene (PID) (S)171 %08/07/19 14:50 460-00-4 S508/07/19 13:4270-130 1
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 2.45 mg/kg 08/08/19 08:36 7440-38-2 PH08/08/19 00:060.671 0.168 5
Barium 195 mg/kg 08/08/19 08:56 7440-39-308/08/19 00:062.68 0.430 10
Cadmium 0.280J mg/kg 08/08/19 08:36 7440-43-9 J08/08/19 00:060.671 0.107 5
Chromium 43.5 mg/kg 08/08/19 08:36 7440-47-308/08/19 00:061.34 0.362 5
Lead 12.3 mg/kg 08/08/19 08:36 7439-92-108/08/19 00:060.671 0.161 5
Selenium 1.31 mg/kg 08/08/19 08:36 7782-49-208/08/19 00:060.671 0.255 5
Silver ND mg/kg 08/08/19 08:36 7440-22-408/08/19 00:060.671 0.208 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 10.5 mg/kg 08/08/19 12:39 7439-97-608/07/19 23:320.201 0.0188 5
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/11/19 17:41 83-32-908/09/19 17:460.40 0.10 1
Acenaphthylene ND mg/kg 08/11/19 17:41 208-96-808/09/19 17:460.40 0.096 1
Aniline ND mg/kg 08/11/19 17:41 62-53-308/09/19 17:460.40 0.091 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-1 (8-10)Lab ID:92438947001 Collected:07/27/19 13:35 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Anthracene ND mg/kg 08/11/19 17:41 120-12-708/09/19 17:460.40 0.10 1
Benzo(a)anthracene ND mg/kg 08/11/19 17:41 56-55-308/09/19 17:460.40 0.13 1
Benzo(a)pyrene ND mg/kg 08/11/19 17:41 50-32-808/09/19 17:460.40 0.17 1
Benzo(b)fluoranthene ND mg/kg 08/11/19 17:41 205-99-208/09/19 17:460.40 0.16 1
Benzo(g,h,i)perylene ND mg/kg 08/11/19 17:41 191-24-208/09/19 17:460.40 0.16 1
Benzo(k)fluoranthene ND mg/kg 08/11/19 17:41 207-08-908/09/19 17:460.40 0.17 1
Benzoic Acid ND mg/kg 08/11/19 17:41 65-85-008/09/19 17:462.0 0.44 1
Benzyl alcohol ND mg/kg 08/11/19 17:41 100-51-608/09/19 17:460.81 0.21 1
4-Bromophenylphenyl ether ND mg/kg 08/11/19 17:41 101-55-308/09/19 17:460.40 0.11 1
Butylbenzylphthalate ND mg/kg 08/11/19 17:41 85-68-708/09/19 17:460.40 0.11 1
4-Chloro-3-methylphenol ND mg/kg 08/11/19 17:41 59-50-708/09/19 17:460.81 0.25 1
4-Chloroaniline ND mg/kg 08/11/19 17:41 106-47-808/09/19 17:462.0 0.25 1
bis(2-Chloroethoxy)methane ND mg/kg 08/11/19 17:41 111-91-108/09/19 17:460.40 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 08/11/19 17:41 111-44-408/09/19 17:460.40 0.086 1
2-Chloronaphthalene ND mg/kg 08/11/19 17:41 91-58-708/09/19 17:460.40 0.090 1
2-Chlorophenol ND mg/kg 08/11/19 17:41 95-57-808/09/19 17:460.40 0.094 1
4-Chlorophenylphenyl ether ND mg/kg 08/11/19 17:41 7005-72-308/09/19 17:460.40 0.10 1
Chrysene ND mg/kg 08/11/19 17:41 218-01-908/09/19 17:460.40 0.12 1
Dibenz(a,h)anthracene ND mg/kg 08/11/19 17:41 53-70-308/09/19 17:460.40 0.16 1
Dibenzofuran ND mg/kg 08/11/19 17:41 132-64-908/09/19 17:460.40 0.10 1
1,2-Dichlorobenzene ND mg/kg 08/11/19 17:41 95-50-108/09/19 17:460.40 0.087 1
1,3-Dichlorobenzene ND mg/kg 08/11/19 17:41 541-73-108/09/19 17:460.40 0.091 1
1,4-Dichlorobenzene ND mg/kg 08/11/19 17:41 106-46-708/09/19 17:460.40 0.089 1
3,3'-Dichlorobenzidine ND mg/kg 08/11/19 17:41 91-94-108/09/19 17:462.0 0.28 1
2,4-Dichlorophenol ND mg/kg 08/11/19 17:41 120-83-208/09/19 17:460.40 0.13 1
Diethylphthalate ND mg/kg 08/11/19 17:41 84-66-208/09/19 17:460.40 0.088 1
2,4-Dimethylphenol ND mg/kg 08/11/19 17:41 105-67-908/09/19 17:460.40 0.10 1
Dimethylphthalate ND mg/kg 08/11/19 17:41 131-11-308/09/19 17:460.40 0.091 1
Di-n-butylphthalate ND mg/kg 08/11/19 17:41 84-74-208/09/19 17:460.40 0.10 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/11/19 17:41 534-52-108/09/19 17:460.81 0.65 1
2,4-Dinitrophenol ND mg/kg 08/11/19 17:41 51-28-508/09/19 17:462.0 1.3 1
2,4-Dinitrotoluene ND mg/kg 08/11/19 17:41 121-14-208/09/19 17:460.40 0.11 1
2,6-Dinitrotoluene ND mg/kg 08/11/19 17:41 606-20-208/09/19 17:460.40 0.11 1
Di-n-octylphthalate ND mg/kg 08/11/19 17:41 117-84-0 v108/09/19 17:460.40 0.23 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/11/19 17:41 117-81-708/09/19 17:460.40 0.13 1
Fluoranthene ND mg/kg 08/11/19 17:41 206-44-008/09/19 17:460.40 0.12 1
Fluorene ND mg/kg 08/11/19 17:41 86-73-708/09/19 17:460.40 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 08/11/19 17:41 87-68-308/09/19 17:460.40 0.098 1
Hexachlorobenzene ND mg/kg 08/11/19 17:41 118-74-108/09/19 17:460.40 0.10 1
Hexachlorocyclopentadiene ND mg/kg 08/11/19 17:41 77-47-408/09/19 17:460.40 0.16 1
Hexachloroethane ND mg/kg 08/11/19 17:41 67-72-108/09/19 17:460.40 0.092 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/11/19 17:41 193-39-508/09/19 17:460.40 0.18 1
Isophorone ND mg/kg 08/11/19 17:41 78-59-108/09/19 17:460.40 0.088 1
1-Methylnaphthalene 0.20J mg/kg 08/11/19 17:41 90-12-008/09/19 17:460.40 0.11 1
2-Methylnaphthalene 0.36J mg/kg 08/11/19 17:41 91-57-608/09/19 17:460.40 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-1 (8-10)Lab ID:92438947001 Collected:07/27/19 13:35 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2-Methylphenol(o-Cresol)ND mg/kg 08/11/19 17:41 95-48-708/09/19 17:460.40 0.089 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/11/19 17:41 15831-10-408/09/19 17:460.40 0.10 1
Naphthalene 0.50 mg/kg 08/11/19 17:41 91-20-308/09/19 17:460.40 0.097 1
2-Nitroaniline ND mg/kg 08/11/19 17:41 88-74-408/09/19 17:462.0 0.20 1
3-Nitroaniline ND mg/kg 08/11/19 17:41 99-09-208/09/19 17:462.0 0.21 1
4-Nitroaniline ND mg/kg 08/11/19 17:41 100-01-608/09/19 17:460.81 0.20 1
Nitrobenzene ND mg/kg 08/11/19 17:41 98-95-308/09/19 17:460.40 0.096 1
2-Nitrophenol ND mg/kg 08/11/19 17:41 88-75-508/09/19 17:460.40 0.12 1
4-Nitrophenol ND mg/kg 08/11/19 17:41 100-02-708/09/19 17:462.0 0.64 1
N-Nitrosodimethylamine ND mg/kg 08/11/19 17:41 62-75-908/09/19 17:460.40 0.11 1
N-Nitroso-di-n-propylamine ND mg/kg 08/11/19 17:41 621-64-708/09/19 17:460.40 0.11 1
N-Nitrosodiphenylamine ND mg/kg 08/11/19 17:41 86-30-608/09/19 17:460.40 0.10 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/11/19 17:41 108-60-1 v108/09/19 17:460.40 0.11 1
Pentachlorophenol ND mg/kg 08/11/19 17:41 87-86-508/09/19 17:462.0 0.18 1
Phenanthrene ND mg/kg 08/11/19 17:41 85-01-808/09/19 17:460.40 0.10 1
Phenol ND mg/kg 08/11/19 17:41 108-95-208/09/19 17:460.40 0.096 1
Pyrene ND mg/kg 08/11/19 17:41 129-00-008/09/19 17:460.40 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 08/11/19 17:41 120-82-108/09/19 17:460.40 0.092 1
2,4,5-Trichlorophenol ND mg/kg 08/11/19 17:41 95-95-408/09/19 17:460.40 0.10 1
2,4,6-Trichlorophenol ND mg/kg 08/11/19 17:41 88-06-208/09/19 17:460.40 0.10 1
Surrogates
Nitrobenzene-d5 (S)56 %08/11/19 17:41 4165-60-008/09/19 17:4623-110 1
2-Fluorobiphenyl (S)48 %08/11/19 17:41 321-60-808/09/19 17:4630-110 1
Terphenyl-d14 (S)68 %08/11/19 17:41 1718-51-008/09/19 17:4628-110 1
Phenol-d6 (S)58 %08/11/19 17:41 13127-88-308/09/19 17:4622-110 1
2-Fluorophenol (S)60 %08/11/19 17:41 367-12-408/09/19 17:4613-110 1
2,4,6-Tribromophenol (S)67 %08/11/19 17:41 118-79-608/09/19 17:4627-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 08/07/19 20:46 67-64-108/07/19 16:104.6 0.46 50
Benzene ND mg/kg 08/07/19 20:46 71-43-208/07/19 16:100.23 0.074 50
Bromobenzene ND mg/kg 08/07/19 20:46 108-86-108/07/19 16:100.23 0.093 50
Bromochloromethane ND mg/kg 08/07/19 20:46 74-97-508/07/19 16:100.23 0.079 50
Bromodichloromethane ND mg/kg 08/07/19 20:46 75-27-408/07/19 16:100.23 0.088 50
Bromoform ND mg/kg 08/07/19 20:46 75-25-208/07/19 16:100.23 0.11 50
Bromomethane ND mg/kg 08/07/19 20:46 74-83-908/07/19 16:100.46 0.12 50
2-Butanone (MEK)ND mg/kg 08/07/19 20:46 78-93-308/07/19 16:104.6 0.13 50
n-Butylbenzene 1.6 mg/kg 08/07/19 20:46 104-51-808/07/19 16:100.23 0.083 50
sec-Butylbenzene 0.71 mg/kg 08/07/19 20:46 135-98-808/07/19 16:100.23 0.074 50
tert-Butylbenzene 0.14J mg/kg 08/07/19 20:46 98-06-608/07/19 16:100.23 0.093 50
Carbon tetrachloride ND mg/kg 08/07/19 20:46 56-23-508/07/19 16:100.23 0.12 50
Chlorobenzene ND mg/kg 08/07/19 20:46 108-90-708/07/19 16:100.23 0.088 50
Chloroethane ND mg/kg 08/07/19 20:46 75-00-3 v108/07/19 16:100.46 0.11 50
Chloroform ND mg/kg 08/07/19 20:46 67-66-308/07/19 16:100.23 0.074 50
Chloromethane ND mg/kg 08/07/19 20:46 74-87-308/07/19 16:100.46 0.11 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-1 (8-10)Lab ID:92438947001 Collected:07/27/19 13:35 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
2-Chlorotoluene ND mg/kg 08/07/19 20:46 95-49-808/07/19 16:100.23 0.079 50
4-Chlorotoluene ND mg/kg 08/07/19 20:46 106-43-408/07/19 16:100.23 0.083 50
1,2-Dibromo-3-chloropropane ND mg/kg 08/07/19 20:46 96-12-808/07/19 16:100.23 0.17 50
Dibromochloromethane ND mg/kg 08/07/19 20:46 124-48-108/07/19 16:100.23 0.083 50
1,2-Dibromoethane (EDB)ND mg/kg 08/07/19 20:46 106-93-408/07/19 16:100.23 0.083 50
Dibromomethane ND mg/kg 08/07/19 20:46 74-95-308/07/19 16:100.23 0.12 50
1,2-Dichlorobenzene ND mg/kg 08/07/19 20:46 95-50-108/07/19 16:100.23 0.088 50
1,3-Dichlorobenzene ND mg/kg 08/07/19 20:46 541-73-108/07/19 16:100.23 0.093 50
1,4-Dichlorobenzene ND mg/kg 08/07/19 20:46 106-46-708/07/19 16:100.23 0.079 50
Dichlorodifluoromethane ND mg/kg 08/07/19 20:46 75-71-808/07/19 16:100.46 0.17 50
1,1-Dichloroethane ND mg/kg 08/07/19 20:46 75-34-308/07/19 16:100.23 0.069 50
1,2-Dichloroethane ND mg/kg 08/07/19 20:46 107-06-208/07/19 16:100.23 0.10 50
1,1-Dichloroethene ND mg/kg 08/07/19 20:46 75-35-408/07/19 16:100.23 0.083 50
cis-1,2-Dichloroethene ND mg/kg 08/07/19 20:46 156-59-208/07/19 16:100.23 0.065 50
trans-1,2-Dichloroethene ND mg/kg 08/07/19 20:46 156-60-508/07/19 16:100.23 0.088 50
1,2-Dichloropropane ND mg/kg 08/07/19 20:46 78-87-508/07/19 16:100.23 0.079 50
1,3-Dichloropropane ND mg/kg 08/07/19 20:46 142-28-908/07/19 16:100.23 0.088 50
2,2-Dichloropropane ND mg/kg 08/07/19 20:46 594-20-708/07/19 16:100.23 0.079 50
1,1-Dichloropropene ND mg/kg 08/07/19 20:46 563-58-608/07/19 16:100.23 0.069 50
cis-1,3-Dichloropropene ND mg/kg 08/07/19 20:46 10061-01-508/07/19 16:100.23 0.083 50
trans-1,3-Dichloropropene ND mg/kg 08/07/19 20:46 10061-02-608/07/19 16:100.23 0.069 50
Diisopropyl ether ND mg/kg 08/07/19 20:46 108-20-308/07/19 16:100.23 0.079 50
Ethylbenzene 1.1 mg/kg 08/07/19 20:46 100-41-408/07/19 16:100.23 0.083 50
Hexachloro-1,3-butadiene ND mg/kg 08/07/19 20:46 87-68-308/07/19 16:100.23 0.093 50
2-Hexanone ND mg/kg 08/07/19 20:46 591-78-608/07/19 16:102.3 0.18 50
Isopropylbenzene (Cumene)1.3 mg/kg 08/07/19 20:46 98-82-808/07/19 16:100.23 0.088 50
p-Isopropyltoluene ND mg/kg 08/07/19 20:46 99-87-608/07/19 16:100.23 0.079 50
Methylene Chloride ND mg/kg 08/07/19 20:46 75-09-208/07/19 16:100.93 0.14 50
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/07/19 20:46 108-10-1 M108/07/19 16:102.3 0.17 50
Methyl-tert-butyl ether ND mg/kg 08/07/19 20:46 1634-04-408/07/19 16:100.23 0.069 50
Naphthalene 5.9 mg/kg 08/07/19 20:46 91-20-308/07/19 16:100.23 0.056 50
n-Propylbenzene 3.4 mg/kg 08/07/19 20:46 103-65-1 M108/07/19 16:100.23 0.079 50
Styrene ND mg/kg 08/07/19 20:46 100-42-508/07/19 16:100.23 0.083 50
1,1,1,2-Tetrachloroethane ND mg/kg 08/07/19 20:46 630-20-608/07/19 16:100.23 0.097 50
1,1,2,2-Tetrachloroethane ND mg/kg 08/07/19 20:46 79-34-508/07/19 16:100.23 0.088 50
Tetrachloroethene ND mg/kg 08/07/19 20:46 127-18-408/07/19 16:100.23 0.079 50
Toluene ND mg/kg 08/07/19 20:46 108-88-308/07/19 16:100.23 0.083 50
1,2,3-Trichlorobenzene ND mg/kg 08/07/19 20:46 87-61-608/07/19 16:100.23 0.10 50
1,2,4-Trichlorobenzene ND mg/kg 08/07/19 20:46 120-82-108/07/19 16:100.23 0.074 50
1,1,1-Trichloroethane ND mg/kg 08/07/19 20:46 71-55-608/07/19 16:100.23 0.083 50
1,1,2-Trichloroethane ND mg/kg 08/07/19 20:46 79-00-508/07/19 16:100.23 0.097 50
Trichloroethene ND mg/kg 08/07/19 20:46 79-01-608/07/19 16:100.23 0.097 50
Trichlorofluoromethane ND mg/kg 08/07/19 20:46 75-69-408/07/19 16:100.23 0.10 50
1,2,3-Trichloropropane ND mg/kg 08/07/19 20:46 96-18-408/07/19 16:100.23 0.074 50
1,2,4-Trimethylbenzene ND mg/kg 08/07/19 20:46 95-63-608/07/19 16:100.23 0.093 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-1 (8-10)Lab ID:92438947001 Collected:07/27/19 13:35 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
1,3,5-Trimethylbenzene ND mg/kg 08/07/19 20:46 108-67-808/07/19 16:100.23 0.083 50
Vinyl acetate ND mg/kg 08/07/19 20:46 108-05-408/07/19 16:102.3 0.41 50
Vinyl chloride ND mg/kg 08/07/19 20:46 75-01-408/07/19 16:100.46 0.083 50
Xylene (Total)ND mg/kg 08/07/19 20:46 1330-20-708/07/19 16:100.46 0.17 50
m&p-Xylene ND mg/kg 08/07/19 20:46 179601-23-108/07/19 16:100.46 0.17 50
o-Xylene ND mg/kg 08/07/19 20:46 95-47-608/07/19 16:100.23 0.088 50
Surrogates
Toluene-d8 (S)101 %08/07/19 20:46 2037-26-508/07/19 16:1070-130 50
4-Bromofluorobenzene (S)117 %08/07/19 20:46 460-00-408/07/19 16:1070-130 50
1,2-Dichloroethane-d4 (S)92 %08/07/19 20:46 17060-07-008/07/19 16:1070-132 50
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.6 %07/29/19 16:170.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 74.5 %08/12/19 14:5908/12/19 14:511
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.533J mg/kg 08/09/19 18:07 18540-29-9 J08/09/19 11:251.34 0.342 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-2 (3-4)Lab ID:92438947002 Collected:07/27/19 12:50 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 1.88 mg/kg 08/02/19 13:49 7440-38-2 PH08/01/19 20:160.644 0.161 5
Barium 27.8 mg/kg 08/02/19 13:49 7440-39-308/01/19 20:161.29 0.206 5
Cadmium 0.584J mg/kg 08/02/19 13:49 7440-43-9 J08/01/19 20:160.644 0.103 5
Chromium 33.5 mg/kg 08/02/19 13:49 7440-47-308/01/19 20:161.29 0.348 5
Lead 21.5 mg/kg 08/02/19 13:49 7439-92-108/01/19 20:160.644 0.155 5
Selenium 1.17 mg/kg 08/02/19 13:49 7782-49-208/01/19 20:160.644 0.245 5
Silver 0.421J mg/kg 08/02/19 13:49 7440-22-4 J08/01/19 20:160.644 0.200 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 30.2 mg/kg 08/04/19 16:09 7439-97-608/02/19 10:193.87 0.361 100
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/02/19 14:30 83-32-907/31/19 10:434.0 1.0 10
Acenaphthylene ND mg/kg 08/02/19 14:30 208-96-807/31/19 10:434.0 0.95 10
Aniline ND mg/kg 08/02/19 14:30 62-53-307/31/19 10:434.0 0.90 10
Anthracene ND mg/kg 08/02/19 14:30 120-12-707/31/19 10:434.0 1.0 10
Benzo(a)anthracene ND mg/kg 08/02/19 14:30 56-55-307/31/19 10:434.0 1.3 10
Benzo(a)pyrene ND mg/kg 08/02/19 14:30 50-32-807/31/19 10:434.0 1.7 10
Benzo(b)fluoranthene ND mg/kg 08/02/19 14:30 205-99-207/31/19 10:434.0 1.6 10
Benzo(g,h,i)perylene ND mg/kg 08/02/19 14:30 191-24-207/31/19 10:434.0 1.6 10
Benzo(k)fluoranthene ND mg/kg 08/02/19 14:30 207-08-907/31/19 10:434.0 1.7 10
Benzoic Acid ND mg/kg 08/02/19 14:30 65-85-007/31/19 10:4320.1 4.3 10
Benzyl alcohol ND mg/kg 08/02/19 14:30 100-51-607/31/19 10:438.0 2.1 10
4-Bromophenylphenyl ether ND mg/kg 08/02/19 14:30 101-55-307/31/19 10:434.0 1.1 10
Butylbenzylphthalate ND mg/kg 08/02/19 14:30 85-68-707/31/19 10:434.0 1.1 10
4-Chloro-3-methylphenol ND mg/kg 08/02/19 14:30 59-50-707/31/19 10:438.0 2.5 10
4-Chloroaniline ND mg/kg 08/02/19 14:30 106-47-807/31/19 10:4320.1 2.5 10
bis(2-Chloroethoxy)methane ND mg/kg 08/02/19 14:30 111-91-107/31/19 10:434.0 1.1 10
bis(2-Chloroethyl) ether ND mg/kg 08/02/19 14:30 111-44-4 v107/31/19 10:434.0 0.85 10
2-Chloronaphthalene ND mg/kg 08/02/19 14:30 91-58-707/31/19 10:434.0 0.90 10
2-Chlorophenol ND mg/kg 08/02/19 14:30 95-57-807/31/19 10:434.0 0.94 10
4-Chlorophenylphenyl ether ND mg/kg 08/02/19 14:30 7005-72-307/31/19 10:434.0 1.0 10
Chrysene ND mg/kg 08/02/19 14:30 218-01-907/31/19 10:434.0 1.2 10
Dibenz(a,h)anthracene ND mg/kg 08/02/19 14:30 53-70-307/31/19 10:434.0 1.6 10
Dibenzofuran ND mg/kg 08/02/19 14:30 132-64-907/31/19 10:434.0 1.0 10
1,2-Dichlorobenzene 18.5 mg/kg 08/02/19 14:30 95-50-107/31/19 10:434.0 0.87 10
1,3-Dichlorobenzene ND mg/kg 08/02/19 14:30 541-73-107/31/19 10:434.0 0.91 10
1,4-Dichlorobenzene 2.8J mg/kg 08/02/19 14:30 106-46-707/31/19 10:434.0 0.89 10
3,3'-Dichlorobenzidine ND mg/kg 08/02/19 14:30 91-94-107/31/19 10:4320.1 2.8 10
2,4-Dichlorophenol ND mg/kg 08/02/19 14:30 120-83-207/31/19 10:434.0 1.3 10
Diethylphthalate ND mg/kg 08/02/19 14:30 84-66-207/31/19 10:434.0 0.87 10
2,4-Dimethylphenol ND mg/kg 08/02/19 14:30 105-67-907/31/19 10:434.0 1.0 10
Dimethylphthalate ND mg/kg 08/02/19 14:30 131-11-307/31/19 10:434.0 0.91 10
Di-n-butylphthalate ND mg/kg 08/02/19 14:30 84-74-207/31/19 10:434.0 0.99 10
4,6-Dinitro-2-methylphenol ND mg/kg 08/02/19 14:30 534-52-1 v107/31/19 10:438.0 6.5 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-2 (3-4)Lab ID:92438947002 Collected:07/27/19 12:50 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 08/02/19 14:30 51-28-507/31/19 10:4320.1 12.8 10
2,4-Dinitrotoluene ND mg/kg 08/02/19 14:30 121-14-207/31/19 10:434.0 1.1 10
2,6-Dinitrotoluene ND mg/kg 08/02/19 14:30 606-20-207/31/19 10:434.0 1.1 10
Di-n-octylphthalate ND mg/kg 08/02/19 14:30 117-84-0 v107/31/19 10:434.0 2.3 10
bis(2-Ethylhexyl)phthalate ND mg/kg 08/02/19 14:30 117-81-707/31/19 10:434.0 1.3 10
Fluoranthene ND mg/kg 08/02/19 14:30 206-44-007/31/19 10:434.0 1.2 10
Fluorene ND mg/kg 08/02/19 14:30 86-73-707/31/19 10:434.0 1.1 10
Hexachloro-1,3-butadiene ND mg/kg 08/02/19 14:30 87-68-307/31/19 10:434.0 0.98 10
Hexachlorobenzene ND mg/kg 08/02/19 14:30 118-74-107/31/19 10:434.0 1.0 10
Hexachlorocyclopentadiene ND mg/kg 08/02/19 14:30 77-47-4 v107/31/19 10:434.0 1.6 10
Hexachloroethane ND mg/kg 08/02/19 14:30 67-72-107/31/19 10:434.0 0.92 10
Indeno(1,2,3-cd)pyrene ND mg/kg 08/02/19 14:30 193-39-507/31/19 10:434.0 1.8 10
Isophorone ND mg/kg 08/02/19 14:30 78-59-107/31/19 10:434.0 0.87 10
1-Methylnaphthalene 4.8 mg/kg 08/02/19 14:30 90-12-007/31/19 10:434.0 1.1 10
2-Methylnaphthalene 7.0 mg/kg 08/02/19 14:30 91-57-607/31/19 10:434.0 1.0 10
2-Methylphenol(o-Cresol)ND mg/kg 08/02/19 14:30 95-48-707/31/19 10:434.0 0.89 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/02/19 14:30 15831-10-4 v107/31/19 10:434.0 1.0 10
Naphthalene 5.1 mg/kg 08/02/19 14:30 91-20-307/31/19 10:434.0 0.96 10
2-Nitroaniline ND mg/kg 08/02/19 14:30 88-74-4 v107/31/19 10:4320.1 2.0 10
3-Nitroaniline ND mg/kg 08/02/19 14:30 99-09-207/31/19 10:4320.1 2.1 10
4-Nitroaniline ND mg/kg 08/02/19 14:30 100-01-607/31/19 10:438.0 2.0 10
Nitrobenzene ND mg/kg 08/02/19 14:30 98-95-307/31/19 10:434.0 0.96 10
2-Nitrophenol ND mg/kg 08/02/19 14:30 88-75-507/31/19 10:434.0 1.2 10
4-Nitrophenol ND mg/kg 08/02/19 14:30 100-02-707/31/19 10:4320.1 6.4 10
N-Nitrosodimethylamine ND mg/kg 08/02/19 14:30 62-75-9 v107/31/19 10:434.0 1.1 10
N-Nitroso-di-n-propylamine ND mg/kg 08/02/19 14:30 621-64-707/31/19 10:434.0 1.1 10
N-Nitrosodiphenylamine ND mg/kg 08/02/19 14:30 86-30-607/31/19 10:434.0 1.0 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/02/19 14:30 108-60-1 v107/31/19 10:434.0 1.1 10
Pentachlorophenol ND mg/kg 08/02/19 14:30 87-86-507/31/19 10:4320.1 1.8 10
Phenanthrene ND mg/kg 08/02/19 14:30 85-01-807/31/19 10:434.0 1.0 10
Phenol ND mg/kg 08/02/19 14:30 108-95-207/31/19 10:434.0 0.96 10
Pyrene ND mg/kg 08/02/19 14:30 129-00-007/31/19 10:434.0 1.1 10
1,2,4-Trichlorobenzene ND mg/kg 08/02/19 14:30 120-82-107/31/19 10:434.0 0.92 10
2,4,5-Trichlorophenol ND mg/kg 08/02/19 14:30 95-95-407/31/19 10:434.0 1.0 10
2,4,6-Trichlorophenol ND mg/kg 08/02/19 14:30 88-06-207/31/19 10:434.0 1.0 10
Surrogates
Nitrobenzene-d5 (S)0 %08/02/19 14:30 4165-60-0 D3,S407/31/19 10:4323-110 10
2-Fluorobiphenyl (S)0 %08/02/19 14:30 321-60-8 S407/31/19 10:4330-110 10
Terphenyl-d14 (S)0 %08/02/19 14:30 1718-51-0 S407/31/19 10:4328-110 10
Phenol-d6 (S)0 %08/02/19 14:30 13127-88-3 S407/31/19 10:4322-110 10
2-Fluorophenol (S)0 %08/02/19 14:30 367-12-4 S407/31/19 10:4313-110 10
2,4,6-Tribromophenol (S)0 %08/02/19 14:30 118-79-6 S407/31/19 10:4327-110 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 0.33 mg/kg 07/30/19 20:18 67-64-107/30/19 13:100.098 0.0098 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-2 (3-4)Lab ID:92438947002 Collected:07/27/19 12:50 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Benzene 0.0045J mg/kg 07/30/19 20:18 71-43-207/30/19 13:100.0049 0.0016 1
Bromobenzene ND mg/kg 07/30/19 20:18 108-86-107/30/19 13:100.0049 0.0020 1
Bromochloromethane ND mg/kg 07/30/19 20:18 74-97-507/30/19 13:100.0049 0.0017 1
Bromodichloromethane ND mg/kg 07/30/19 20:18 75-27-407/30/19 13:100.0049 0.0019 1
Bromoform ND mg/kg 07/30/19 20:18 75-25-207/30/19 13:100.0049 0.0022 1
Bromomethane ND mg/kg 07/30/19 20:18 74-83-907/30/19 13:100.0098 0.0024 1
2-Butanone (MEK)0.028J mg/kg 07/30/19 20:18 78-93-307/30/19 13:100.098 0.0028 1
n-Butylbenzene ND mg/kg 07/30/19 20:18 104-51-807/30/19 13:100.0049 0.0018 1
sec-Butylbenzene ND mg/kg 08/01/19 15:26 135-98-807/31/19 12:285.9 1.9 1000
tert-Butylbenzene ND mg/kg 07/30/19 20:18 98-06-607/30/19 13:100.0049 0.0020 1
Carbon tetrachloride ND mg/kg 07/30/19 20:18 56-23-507/30/19 13:100.0049 0.0025 1
Chlorobenzene 145 mg/kg 08/01/19 15:26 108-90-707/31/19 12:285.9 2.2 1000
Chloroethane ND mg/kg 07/30/19 20:18 75-00-307/30/19 13:100.0098 0.0023 1
Chloroform ND mg/kg 07/30/19 20:18 67-66-307/30/19 13:100.0049 0.0016 1
Chloromethane ND mg/kg 07/30/19 20:18 74-87-307/30/19 13:100.0098 0.0023 1
2-Chlorotoluene ND mg/kg 07/30/19 20:18 95-49-807/30/19 13:100.0049 0.0017 1
4-Chlorotoluene ND mg/kg 07/30/19 20:18 106-43-407/30/19 13:100.0049 0.0018 1
1,2-Dibromo-3-chloropropane ND mg/kg 07/30/19 20:18 96-12-807/30/19 13:100.0049 0.0035 1
Dibromochloromethane ND mg/kg 07/30/19 20:18 124-48-107/30/19 13:100.0049 0.0018 1
1,2-Dibromoethane (EDB)ND mg/kg 07/30/19 20:18 106-93-407/30/19 13:100.0049 0.0018 1
Dibromomethane ND mg/kg 07/30/19 20:18 74-95-307/30/19 13:100.0049 0.0024 1
1,2-Dichlorobenzene 159 mg/kg 08/01/19 15:26 95-50-107/31/19 12:285.9 2.2 1000
1,3-Dichlorobenzene 3.9J mg/kg 08/01/19 15:26 541-73-107/31/19 12:285.9 2.3 1000
1,4-Dichlorobenzene 23.6 mg/kg 08/01/19 15:26 106-46-707/31/19 12:285.9 2.0 1000
Dichlorodifluoromethane ND mg/kg 07/30/19 20:18 75-71-807/30/19 13:100.0098 0.0035 1
1,1-Dichloroethane ND mg/kg 07/30/19 20:18 75-34-307/30/19 13:100.0049 0.0015 1
1,2-Dichloroethane ND mg/kg 07/30/19 20:18 107-06-207/30/19 13:100.0049 0.0021 1
1,1-Dichloroethene ND mg/kg 07/30/19 20:18 75-35-407/30/19 13:100.0049 0.0018 1
cis-1,2-Dichloroethene ND mg/kg 07/30/19 20:18 156-59-207/30/19 13:100.0049 0.0014 1
trans-1,2-Dichloroethene ND mg/kg 07/30/19 20:18 156-60-507/30/19 13:100.0049 0.0019 1
1,2-Dichloropropane ND mg/kg 07/30/19 20:18 78-87-507/30/19 13:100.0049 0.0017 1
1,3-Dichloropropane ND mg/kg 07/30/19 20:18 142-28-907/30/19 13:100.0049 0.0019 1
2,2-Dichloropropane ND mg/kg 07/30/19 20:18 594-20-707/30/19 13:100.0049 0.0017 1
1,1-Dichloropropene ND mg/kg 07/30/19 20:18 563-58-607/30/19 13:100.0049 0.0015 1
cis-1,3-Dichloropropene ND mg/kg 07/30/19 20:18 10061-01-507/30/19 13:100.0049 0.0018 1
trans-1,3-Dichloropropene ND mg/kg 07/30/19 20:18 10061-02-607/30/19 13:100.0049 0.0015 1
Diisopropyl ether ND mg/kg 07/30/19 20:18 108-20-307/30/19 13:100.0049 0.0017 1
Ethylbenzene 2.9J mg/kg 08/01/19 15:26 100-41-407/31/19 12:285.9 2.1 1000
Hexachloro-1,3-butadiene ND mg/kg 07/30/19 20:18 87-68-307/30/19 13:100.0049 0.0020 1
2-Hexanone ND mg/kg 07/30/19 20:18 591-78-607/30/19 13:100.049 0.0038 1
Isopropylbenzene (Cumene)3.4J mg/kg 08/01/19 15:26 98-82-807/31/19 12:285.9 2.2 1000
p-Isopropyltoluene 18.3 mg/kg 08/01/19 15:26 99-87-607/31/19 12:285.9 2.0 1000
Methylene Chloride ND mg/kg 07/30/19 20:18 75-09-207/30/19 13:100.020 0.0029 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 07/30/19 20:18 108-10-107/30/19 13:100.049 0.0036 1
Methyl-tert-butyl ether ND mg/kg 07/30/19 20:18 1634-04-407/30/19 13:100.0049 0.0015 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-2 (3-4)Lab ID:92438947002 Collected:07/27/19 12:50 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene 42.0 mg/kg 08/01/19 15:26 91-20-307/31/19 12:285.9 1.4 1000
n-Propylbenzene ND mg/kg 08/01/19 15:26 103-65-107/31/19 12:285.9 2.0 1000
Styrene ND mg/kg 07/30/19 20:18 100-42-507/30/19 13:100.0049 0.0018 1
1,1,1,2-Tetrachloroethane ND mg/kg 07/30/19 20:18 630-20-607/30/19 13:100.0049 0.0020 1
1,1,2,2-Tetrachloroethane ND mg/kg 07/30/19 20:18 79-34-507/30/19 13:100.0049 0.0019 1
Tetrachloroethene ND mg/kg 07/30/19 20:18 127-18-407/30/19 13:100.0049 0.0017 1
Toluene 0.013 mg/kg 07/30/19 20:18 108-88-307/30/19 13:100.0049 0.0018 1
1,2,3-Trichlorobenzene ND mg/kg 07/30/19 20:18 87-61-607/30/19 13:100.0049 0.0021 1
1,2,4-Trichlorobenzene 0.0075 mg/kg 07/30/19 20:18 120-82-107/30/19 13:100.0049 0.0016 1
1,1,1-Trichloroethane ND mg/kg 07/30/19 20:18 71-55-607/30/19 13:100.0049 0.0018 1
1,1,2-Trichloroethane ND mg/kg 07/30/19 20:18 79-00-507/30/19 13:100.0049 0.0020 1
Trichloroethene ND mg/kg 07/30/19 20:18 79-01-607/30/19 13:100.0049 0.0020 1
Trichlorofluoromethane ND mg/kg 07/30/19 20:18 75-69-407/30/19 13:100.0049 0.0021 1
1,2,3-Trichloropropane ND mg/kg 07/30/19 20:18 96-18-407/30/19 13:100.0049 0.0016 1
1,2,4-Trimethylbenzene 127 mg/kg 08/01/19 15:26 95-63-607/31/19 12:285.9 2.3 1000
1,3,5-Trimethylbenzene 41.6 mg/kg 08/01/19 15:26 108-67-807/31/19 12:285.9 2.1 1000
Vinyl acetate ND mg/kg 07/30/19 20:18 108-05-407/30/19 13:100.049 0.0086 1
Vinyl chloride ND mg/kg 07/30/19 20:18 75-01-407/30/19 13:100.0098 0.0018 1
Xylene (Total)ND mg/kg 08/01/19 15:26 1330-20-707/31/19 12:2811.7 4.2 1000
m&p-Xylene 8.2J mg/kg 08/01/19 15:26 179601-23-107/31/19 12:2811.7 4.2 1000
o-Xylene ND mg/kg 08/01/19 15:26 95-47-607/31/19 12:285.9 2.2 1000
Surrogates
Toluene-d8 (S)102 %07/30/19 20:18 2037-26-5 IO07/30/19 13:1070-130 1
4-Bromofluorobenzene (S)456 %07/30/19 20:18 460-00-4 S107/30/19 13:1070-130 1
1,2-Dichloroethane-d4 (S)122 %07/30/19 20:18 17060-07-007/30/19 13:1070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.4 %07/29/19 16:170.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 77.6 %08/03/19 16:3308/03/19 16:221
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.372J mg/kg 08/05/19 14:57 18540-29-9 J08/05/19 11:321.29 0.329 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-3 (0-2)Lab ID:92438947003 Collected:07/27/19 13:45 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 2.29 mg/kg 08/02/19 14:12 7440-38-208/01/19 20:160.602 0.150 5
Barium 44.8 mg/kg 08/02/19 14:12 7440-39-308/01/19 20:161.20 0.193 5
Cadmium 0.316J mg/kg 08/02/19 14:12 7440-43-9 J08/01/19 20:160.602 0.0963 5
Chromium 35.2 mg/kg 08/02/19 14:12 7440-47-308/01/19 20:161.20 0.325 5
Lead 25.6 mg/kg 08/02/19 14:12 7439-92-108/01/19 20:160.602 0.144 5
Selenium 1.01 mg/kg 08/02/19 14:12 7782-49-208/01/19 20:160.602 0.229 5
Silver ND mg/kg 08/02/19 14:12 7440-22-408/01/19 20:160.602 0.187 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 4.09 mg/kg 08/04/19 16:11 7439-97-608/02/19 10:190.181 0.0169 5
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/01/19 19:29 83-32-907/31/19 10:430.38 0.099 1
Acenaphthylene ND mg/kg 08/01/19 19:29 208-96-807/31/19 10:430.38 0.091 1
Aniline ND mg/kg 08/01/19 19:29 62-53-307/31/19 10:430.38 0.086 1
Anthracene ND mg/kg 08/01/19 19:29 120-12-707/31/19 10:430.38 0.10 1
Benzo(a)anthracene ND mg/kg 08/01/19 19:29 56-55-307/31/19 10:430.38 0.12 1
Benzo(a)pyrene ND mg/kg 08/01/19 19:29 50-32-807/31/19 10:430.38 0.17 1
Benzo(b)fluoranthene ND mg/kg 08/01/19 19:29 205-99-207/31/19 10:430.38 0.15 1
Benzo(g,h,i)perylene ND mg/kg 08/01/19 19:29 191-24-207/31/19 10:430.38 0.15 1
Benzo(k)fluoranthene ND mg/kg 08/01/19 19:29 207-08-907/31/19 10:430.38 0.16 1
Benzoic Acid ND mg/kg 08/01/19 19:29 65-85-007/31/19 10:431.9 0.41 1
Benzyl alcohol ND mg/kg 08/01/19 19:29 100-51-607/31/19 10:430.77 0.20 1
4-Bromophenylphenyl ether ND mg/kg 08/01/19 19:29 101-55-307/31/19 10:430.38 0.10 1
Butylbenzylphthalate ND mg/kg 08/01/19 19:29 85-68-707/31/19 10:430.38 0.10 1
4-Chloro-3-methylphenol ND mg/kg 08/01/19 19:29 59-50-707/31/19 10:430.77 0.23 1
4-Chloroaniline ND mg/kg 08/01/19 19:29 106-47-807/31/19 10:431.9 0.24 1
bis(2-Chloroethoxy)methane ND mg/kg 08/01/19 19:29 111-91-107/31/19 10:430.38 0.10 1
bis(2-Chloroethyl) ether ND mg/kg 08/01/19 19:29 111-44-407/31/19 10:430.38 0.082 1
2-Chloronaphthalene ND mg/kg 08/01/19 19:29 91-58-707/31/19 10:430.38 0.086 1
2-Chlorophenol ND mg/kg 08/01/19 19:29 95-57-807/31/19 10:430.38 0.090 1
4-Chlorophenylphenyl ether ND mg/kg 08/01/19 19:29 7005-72-307/31/19 10:430.38 0.10 1
Chrysene ND mg/kg 08/01/19 19:29 218-01-907/31/19 10:430.38 0.11 1
Dibenz(a,h)anthracene ND mg/kg 08/01/19 19:29 53-70-307/31/19 10:430.38 0.15 1
Dibenzofuran ND mg/kg 08/01/19 19:29 132-64-907/31/19 10:430.38 0.096 1
1,2-Dichlorobenzene ND mg/kg 08/01/19 19:29 95-50-107/31/19 10:430.38 0.083 1
1,3-Dichlorobenzene ND mg/kg 08/01/19 19:29 541-73-107/31/19 10:430.38 0.087 1
1,4-Dichlorobenzene ND mg/kg 08/01/19 19:29 106-46-707/31/19 10:430.38 0.085 1
3,3'-Dichlorobenzidine ND mg/kg 08/01/19 19:29 91-94-107/31/19 10:431.9 0.27 1
2,4-Dichlorophenol ND mg/kg 08/01/19 19:29 120-83-207/31/19 10:430.38 0.13 1
Diethylphthalate ND mg/kg 08/01/19 19:29 84-66-207/31/19 10:430.38 0.083 1
2,4-Dimethylphenol ND mg/kg 08/01/19 19:29 105-67-907/31/19 10:430.38 0.096 1
Dimethylphthalate ND mg/kg 08/01/19 19:29 131-11-307/31/19 10:430.38 0.087 1
Di-n-butylphthalate ND mg/kg 08/01/19 19:29 84-74-207/31/19 10:430.38 0.095 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/01/19 19:29 534-52-107/31/19 10:430.77 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
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Page 15 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-3 (0-2)Lab ID:92438947003 Collected:07/27/19 13:45 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 08/01/19 19:29 51-28-507/31/19 10:431.9 1.2 1
2,4-Dinitrotoluene ND mg/kg 08/01/19 19:29 121-14-207/31/19 10:430.38 0.10 1
2,6-Dinitrotoluene ND mg/kg 08/01/19 19:29 606-20-207/31/19 10:430.38 0.10 1
Di-n-octylphthalate ND mg/kg 08/01/19 19:29 117-84-007/31/19 10:430.38 0.22 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/01/19 19:29 117-81-707/31/19 10:430.38 0.13 1
Fluoranthene ND mg/kg 08/01/19 19:29 206-44-007/31/19 10:430.38 0.12 1
Fluorene ND mg/kg 08/01/19 19:29 86-73-707/31/19 10:430.38 0.10 1
Hexachloro-1,3-butadiene ND mg/kg 08/01/19 19:29 87-68-307/31/19 10:430.38 0.093 1
Hexachlorobenzene ND mg/kg 08/01/19 19:29 118-74-107/31/19 10:430.38 0.098 1
Hexachlorocyclopentadiene ND mg/kg 08/01/19 19:29 77-47-407/31/19 10:430.38 0.15 1
Hexachloroethane ND mg/kg 08/01/19 19:29 67-72-107/31/19 10:430.38 0.088 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/01/19 19:29 193-39-507/31/19 10:430.38 0.18 1
Isophorone ND mg/kg 08/01/19 19:29 78-59-107/31/19 10:430.38 0.084 1
1-Methylnaphthalene ND mg/kg 08/01/19 19:29 90-12-007/31/19 10:430.38 0.10 1
2-Methylnaphthalene ND mg/kg 08/01/19 19:29 91-57-607/31/19 10:430.38 0.098 1
2-Methylphenol(o-Cresol)ND mg/kg 08/01/19 19:29 95-48-707/31/19 10:430.38 0.085 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/01/19 19:29 15831-10-407/31/19 10:430.38 0.097 1
Naphthalene ND mg/kg 08/01/19 19:29 91-20-307/31/19 10:430.38 0.092 1
2-Nitroaniline ND mg/kg 08/01/19 19:29 88-74-407/31/19 10:431.9 0.19 1
3-Nitroaniline ND mg/kg 08/01/19 19:29 99-09-207/31/19 10:431.9 0.20 1
4-Nitroaniline ND mg/kg 08/01/19 19:29 100-01-607/31/19 10:430.77 0.19 1
Nitrobenzene ND mg/kg 08/01/19 19:29 98-95-307/31/19 10:430.38 0.092 1
2-Nitrophenol ND mg/kg 08/01/19 19:29 88-75-507/31/19 10:430.38 0.12 1
4-Nitrophenol ND mg/kg 08/01/19 19:29 100-02-707/31/19 10:431.9 0.61 1
N-Nitrosodimethylamine ND mg/kg 08/01/19 19:29 62-75-907/31/19 10:430.38 0.11 1
N-Nitroso-di-n-propylamine ND mg/kg 08/01/19 19:29 621-64-707/31/19 10:430.38 0.11 1
N-Nitrosodiphenylamine ND mg/kg 08/01/19 19:29 86-30-607/31/19 10:430.38 0.098 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/01/19 19:29 108-60-1 v107/31/19 10:430.38 0.11 1
Pentachlorophenol ND mg/kg 08/01/19 19:29 87-86-507/31/19 10:431.9 0.18 1
Phenanthrene ND mg/kg 08/01/19 19:29 85-01-807/31/19 10:430.38 0.097 1
Phenol ND mg/kg 08/01/19 19:29 108-95-207/31/19 10:430.38 0.092 1
Pyrene ND mg/kg 08/01/19 19:29 129-00-007/31/19 10:430.38 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 08/01/19 19:29 120-82-107/31/19 10:430.38 0.088 1
2,4,5-Trichlorophenol ND mg/kg 08/01/19 19:29 95-95-407/31/19 10:430.38 0.10 1
2,4,6-Trichlorophenol ND mg/kg 08/01/19 19:29 88-06-207/31/19 10:430.38 0.097 1
Surrogates
Nitrobenzene-d5 (S)77 %08/01/19 19:29 4165-60-007/31/19 10:4323-110 1
2-Fluorobiphenyl (S)79 %08/01/19 19:29 321-60-807/31/19 10:4330-110 1
Terphenyl-d14 (S)98 %08/01/19 19:29 1718-51-007/31/19 10:4328-110 1
Phenol-d6 (S)70 %08/01/19 19:29 13127-88-307/31/19 10:4322-110 1
2-Fluorophenol (S)72 %08/01/19 19:29 367-12-407/31/19 10:4313-110 1
2,4,6-Tribromophenol (S)89 %08/01/19 19:29 118-79-607/31/19 10:4327-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 07/31/19 15:27 67-64-107/31/19 12:070.085 0.0085 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-3 (0-2)Lab ID:92438947003 Collected:07/27/19 13:45 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Benzene ND mg/kg 07/31/19 15:27 71-43-207/31/19 12:070.0042 0.0014 1
Bromobenzene ND mg/kg 07/31/19 15:27 108-86-107/31/19 12:070.0042 0.0017 1
Bromochloromethane ND mg/kg 07/31/19 15:27 74-97-507/31/19 12:070.0042 0.0014 1
Bromodichloromethane ND mg/kg 07/31/19 15:27 75-27-407/31/19 12:070.0042 0.0016 1
Bromoform ND mg/kg 07/31/19 15:27 75-25-207/31/19 12:070.0042 0.0019 1
Bromomethane ND mg/kg 07/31/19 15:27 74-83-907/31/19 12:070.0085 0.0021 1
2-Butanone (MEK)ND mg/kg 07/31/19 15:27 78-93-307/31/19 12:070.085 0.0025 1
n-Butylbenzene ND mg/kg 07/31/19 15:27 104-51-807/31/19 12:070.0042 0.0015 1
sec-Butylbenzene ND mg/kg 07/31/19 15:27 135-98-807/31/19 12:070.0042 0.0014 1
tert-Butylbenzene ND mg/kg 07/31/19 15:27 98-06-607/31/19 12:070.0042 0.0017 1
Carbon tetrachloride ND mg/kg 07/31/19 15:27 56-23-507/31/19 12:070.0042 0.0022 1
Chlorobenzene ND mg/kg 07/31/19 15:27 108-90-707/31/19 12:070.0042 0.0016 1
Chloroethane ND mg/kg 07/31/19 15:27 75-00-307/31/19 12:070.0085 0.0020 1
Chloroform ND mg/kg 07/31/19 15:27 67-66-307/31/19 12:070.0042 0.0014 1
Chloromethane ND mg/kg 07/31/19 15:27 74-87-307/31/19 12:070.0085 0.0020 1
2-Chlorotoluene ND mg/kg 07/31/19 15:27 95-49-807/31/19 12:070.0042 0.0014 1
4-Chlorotoluene ND mg/kg 07/31/19 15:27 106-43-407/31/19 12:070.0042 0.0015 1
1,2-Dibromo-3-chloropropane ND mg/kg 07/31/19 15:27 96-12-807/31/19 12:070.0042 0.0030 1
Dibromochloromethane ND mg/kg 07/31/19 15:27 124-48-107/31/19 12:070.0042 0.0015 1
1,2-Dibromoethane (EDB)ND mg/kg 07/31/19 15:27 106-93-407/31/19 12:070.0042 0.0015 1
Dibromomethane ND mg/kg 07/31/19 15:27 74-95-307/31/19 12:070.0042 0.0021 1
1,2-Dichlorobenzene ND mg/kg 07/31/19 15:27 95-50-107/31/19 12:070.0042 0.0016 1
1,3-Dichlorobenzene ND mg/kg 07/31/19 15:27 541-73-107/31/19 12:070.0042 0.0017 1
1,4-Dichlorobenzene ND mg/kg 07/31/19 15:27 106-46-707/31/19 12:070.0042 0.0014 1
Dichlorodifluoromethane ND mg/kg 07/31/19 15:27 75-71-807/31/19 12:070.0085 0.0030 1
1,1-Dichloroethane ND mg/kg 07/31/19 15:27 75-34-307/31/19 12:070.0042 0.0013 1
1,2-Dichloroethane ND mg/kg 07/31/19 15:27 107-06-207/31/19 12:070.0042 0.0019 1
1,1-Dichloroethene ND mg/kg 07/31/19 15:27 75-35-407/31/19 12:070.0042 0.0015 1
cis-1,2-Dichloroethene ND mg/kg 07/31/19 15:27 156-59-207/31/19 12:070.0042 0.0012 1
trans-1,2-Dichloroethene ND mg/kg 07/31/19 15:27 156-60-507/31/19 12:070.0042 0.0016 1
1,2-Dichloropropane ND mg/kg 07/31/19 15:27 78-87-507/31/19 12:070.0042 0.0014 1
1,3-Dichloropropane ND mg/kg 07/31/19 15:27 142-28-907/31/19 12:070.0042 0.0016 1
2,2-Dichloropropane ND mg/kg 07/31/19 15:27 594-20-707/31/19 12:070.0042 0.0014 1
1,1-Dichloropropene ND mg/kg 07/31/19 15:27 563-58-607/31/19 12:070.0042 0.0013 1
cis-1,3-Dichloropropene ND mg/kg 07/31/19 15:27 10061-01-507/31/19 12:070.0042 0.0015 1
trans-1,3-Dichloropropene ND mg/kg 07/31/19 15:27 10061-02-607/31/19 12:070.0042 0.0013 1
Diisopropyl ether ND mg/kg 07/31/19 15:27 108-20-307/31/19 12:070.0042 0.0014 1
Ethylbenzene ND mg/kg 07/31/19 15:27 100-41-407/31/19 12:070.0042 0.0015 1
Hexachloro-1,3-butadiene ND mg/kg 07/31/19 15:27 87-68-307/31/19 12:070.0042 0.0017 1
2-Hexanone ND mg/kg 07/31/19 15:27 591-78-607/31/19 12:070.042 0.0033 1
Isopropylbenzene (Cumene)ND mg/kg 07/31/19 15:27 98-82-807/31/19 12:070.0042 0.0016 1
p-Isopropyltoluene ND mg/kg 07/31/19 15:27 99-87-607/31/19 12:070.0042 0.0014 1
Methylene Chloride ND mg/kg 07/31/19 15:27 75-09-2 v207/31/19 12:070.017 0.0025 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 07/31/19 15:27 108-10-107/31/19 12:070.042 0.0031 1
Methyl-tert-butyl ether ND mg/kg 07/31/19 15:27 1634-04-407/31/19 12:070.0042 0.0013 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-3 (0-2)Lab ID:92438947003 Collected:07/27/19 13:45 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND mg/kg 07/31/19 15:27 91-20-307/31/19 12:070.0042 0.0010 1
n-Propylbenzene ND mg/kg 07/31/19 15:27 103-65-107/31/19 12:070.0042 0.0014 1
Styrene ND mg/kg 07/31/19 15:27 100-42-507/31/19 12:070.0042 0.0015 1
1,1,1,2-Tetrachloroethane ND mg/kg 07/31/19 15:27 630-20-607/31/19 12:070.0042 0.0018 1
1,1,2,2-Tetrachloroethane ND mg/kg 07/31/19 15:27 79-34-507/31/19 12:070.0042 0.0016 1
Tetrachloroethene ND mg/kg 07/31/19 15:27 127-18-407/31/19 12:070.0042 0.0014 1
Toluene ND mg/kg 07/31/19 15:27 108-88-307/31/19 12:070.0042 0.0015 1
1,2,3-Trichlorobenzene ND mg/kg 07/31/19 15:27 87-61-607/31/19 12:070.0042 0.0019 1
1,2,4-Trichlorobenzene ND mg/kg 07/31/19 15:27 120-82-107/31/19 12:070.0042 0.0014 1
1,1,1-Trichloroethane ND mg/kg 07/31/19 15:27 71-55-607/31/19 12:070.0042 0.0015 1
1,1,2-Trichloroethane ND mg/kg 07/31/19 15:27 79-00-507/31/19 12:070.0042 0.0018 1
Trichloroethene ND mg/kg 07/31/19 15:27 79-01-607/31/19 12:070.0042 0.0018 1
Trichlorofluoromethane ND mg/kg 07/31/19 15:27 75-69-407/31/19 12:070.0042 0.0019 1
1,2,3-Trichloropropane ND mg/kg 07/31/19 15:27 96-18-407/31/19 12:070.0042 0.0014 1
1,2,4-Trimethylbenzene ND mg/kg 07/31/19 15:27 95-63-607/31/19 12:070.0042 0.0017 1
1,3,5-Trimethylbenzene ND mg/kg 07/31/19 15:27 108-67-807/31/19 12:070.0042 0.0015 1
Vinyl acetate ND mg/kg 07/31/19 15:27 108-05-407/31/19 12:070.042 0.0075 1
Vinyl chloride ND mg/kg 07/31/19 15:27 75-01-407/31/19 12:070.0085 0.0015 1
Xylene (Total)ND mg/kg 07/31/19 15:27 1330-20-707/31/19 12:070.0085 0.0030 1
m&p-Xylene ND mg/kg 07/31/19 15:27 179601-23-107/31/19 12:070.0085 0.0030 1
o-Xylene ND mg/kg 07/31/19 15:27 95-47-607/31/19 12:070.0042 0.0016 1
Surrogates
Toluene-d8 (S)101 %07/31/19 15:27 2037-26-507/31/19 12:0770-130 1
4-Bromofluorobenzene (S)101 %07/31/19 15:27 460-00-407/31/19 12:0770-130 1
1,2-Dichloroethane-d4 (S)85 %07/31/19 15:27 17060-07-007/31/19 12:0770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.2 %07/29/19 16:170.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 83.1 %08/03/19 16:3308/03/19 16:221
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/05/19 15:09 18540-29-908/05/19 11:321.20 0.307 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-4 (0-2)Lab ID:92438947004 Collected:07/27/19 13:05 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 68.2 mg/kg 08/02/19 14:16 7440-38-208/01/19 20:160.705 0.176 5
Barium 46.3 mg/kg 08/02/19 14:16 7440-39-308/01/19 20:161.41 0.226 5
Cadmium 0.257J mg/kg 08/02/19 14:16 7440-43-9 J08/01/19 20:160.705 0.113 5
Chromium 40.8 mg/kg 08/02/19 14:16 7440-47-308/01/19 20:161.41 0.381 5
Lead 24.6 mg/kg 08/02/19 14:16 7439-92-108/01/19 20:160.705 0.169 5
Selenium 0.954 mg/kg 08/02/19 14:16 7782-49-208/01/19 20:160.705 0.268 5
Silver ND mg/kg 08/02/19 14:16 7440-22-408/01/19 20:160.705 0.219 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.207 mg/kg 08/04/19 12:17 7439-97-608/02/19 10:190.0423 0.00395 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/01/19 20:03 83-32-907/31/19 10:430.42 0.11 1
Acenaphthylene ND mg/kg 08/01/19 20:03 208-96-807/31/19 10:430.42 0.10 1
Aniline ND mg/kg 08/01/19 20:03 62-53-307/31/19 10:430.42 0.095 1
Anthracene ND mg/kg 08/01/19 20:03 120-12-707/31/19 10:430.42 0.11 1
Benzo(a)anthracene ND mg/kg 08/01/19 20:03 56-55-307/31/19 10:430.42 0.13 1
Benzo(a)pyrene ND mg/kg 08/01/19 20:03 50-32-807/31/19 10:430.42 0.18 1
Benzo(b)fluoranthene ND mg/kg 08/01/19 20:03 205-99-207/31/19 10:430.42 0.17 1
Benzo(g,h,i)perylene ND mg/kg 08/01/19 20:03 191-24-207/31/19 10:430.42 0.17 1
Benzo(k)fluoranthene ND mg/kg 08/01/19 20:03 207-08-907/31/19 10:430.42 0.18 1
Benzoic Acid ND mg/kg 08/01/19 20:03 65-85-007/31/19 10:432.1 0.46 1
Benzyl alcohol ND mg/kg 08/01/19 20:03 100-51-607/31/19 10:430.84 0.22 1
4-Bromophenylphenyl ether ND mg/kg 08/01/19 20:03 101-55-307/31/19 10:430.42 0.11 1
Butylbenzylphthalate ND mg/kg 08/01/19 20:03 85-68-707/31/19 10:430.42 0.11 1
4-Chloro-3-methylphenol ND mg/kg 08/01/19 20:03 59-50-707/31/19 10:430.84 0.26 1
4-Chloroaniline ND mg/kg 08/01/19 20:03 106-47-807/31/19 10:432.1 0.26 1
bis(2-Chloroethoxy)methane ND mg/kg 08/01/19 20:03 111-91-107/31/19 10:430.42 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 08/01/19 20:03 111-44-407/31/19 10:430.42 0.090 1
2-Chloronaphthalene ND mg/kg 08/01/19 20:03 91-58-707/31/19 10:430.42 0.094 1
2-Chlorophenol ND mg/kg 08/01/19 20:03 95-57-807/31/19 10:430.42 0.098 1
4-Chlorophenylphenyl ether ND mg/kg 08/01/19 20:03 7005-72-307/31/19 10:430.42 0.11 1
Chrysene ND mg/kg 08/01/19 20:03 218-01-907/31/19 10:430.42 0.12 1
Dibenz(a,h)anthracene ND mg/kg 08/01/19 20:03 53-70-307/31/19 10:430.42 0.17 1
Dibenzofuran ND mg/kg 08/01/19 20:03 132-64-907/31/19 10:430.42 0.11 1
1,2-Dichlorobenzene ND mg/kg 08/01/19 20:03 95-50-107/31/19 10:430.42 0.091 1
1,3-Dichlorobenzene ND mg/kg 08/01/19 20:03 541-73-107/31/19 10:430.42 0.095 1
1,4-Dichlorobenzene ND mg/kg 08/01/19 20:03 106-46-707/31/19 10:430.42 0.093 1
3,3'-Dichlorobenzidine ND mg/kg 08/01/19 20:03 91-94-107/31/19 10:432.1 0.29 1
2,4-Dichlorophenol ND mg/kg 08/01/19 20:03 120-83-207/31/19 10:430.42 0.14 1
Diethylphthalate ND mg/kg 08/01/19 20:03 84-66-207/31/19 10:430.42 0.092 1
2,4-Dimethylphenol ND mg/kg 08/01/19 20:03 105-67-907/31/19 10:430.42 0.11 1
Dimethylphthalate ND mg/kg 08/01/19 20:03 131-11-307/31/19 10:430.42 0.095 1
Di-n-butylphthalate ND mg/kg 08/01/19 20:03 84-74-207/31/19 10:430.42 0.10 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/01/19 20:03 534-52-107/31/19 10:430.84 0.68 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 19 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-4 (0-2)Lab ID:92438947004 Collected:07/27/19 13:05 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 08/01/19 20:03 51-28-507/31/19 10:432.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 08/01/19 20:03 121-14-207/31/19 10:430.42 0.11 1
2,6-Dinitrotoluene ND mg/kg 08/01/19 20:03 606-20-207/31/19 10:430.42 0.11 1
Di-n-octylphthalate ND mg/kg 08/01/19 20:03 117-84-007/31/19 10:430.42 0.24 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/01/19 20:03 117-81-707/31/19 10:430.42 0.14 1
Fluoranthene ND mg/kg 08/01/19 20:03 206-44-007/31/19 10:430.42 0.13 1
Fluorene ND mg/kg 08/01/19 20:03 86-73-707/31/19 10:430.42 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 08/01/19 20:03 87-68-307/31/19 10:430.42 0.10 1
Hexachlorobenzene ND mg/kg 08/01/19 20:03 118-74-107/31/19 10:430.42 0.11 1
Hexachlorocyclopentadiene ND mg/kg 08/01/19 20:03 77-47-407/31/19 10:430.42 0.17 1
Hexachloroethane ND mg/kg 08/01/19 20:03 67-72-107/31/19 10:430.42 0.096 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/01/19 20:03 193-39-507/31/19 10:430.42 0.19 1
Isophorone ND mg/kg 08/01/19 20:03 78-59-107/31/19 10:430.42 0.092 1
1-Methylnaphthalene ND mg/kg 08/01/19 20:03 90-12-007/31/19 10:430.42 0.11 1
2-Methylnaphthalene ND mg/kg 08/01/19 20:03 91-57-607/31/19 10:430.42 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 08/01/19 20:03 95-48-707/31/19 10:430.42 0.094 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/01/19 20:03 15831-10-407/31/19 10:430.42 0.11 1
Naphthalene ND mg/kg 08/01/19 20:03 91-20-307/31/19 10:430.42 0.10 1
2-Nitroaniline ND mg/kg 08/01/19 20:03 88-74-407/31/19 10:432.1 0.21 1
3-Nitroaniline ND mg/kg 08/01/19 20:03 99-09-207/31/19 10:432.1 0.22 1
4-Nitroaniline ND mg/kg 08/01/19 20:03 100-01-607/31/19 10:430.84 0.21 1
Nitrobenzene ND mg/kg 08/01/19 20:03 98-95-307/31/19 10:430.42 0.10 1
2-Nitrophenol ND mg/kg 08/01/19 20:03 88-75-507/31/19 10:430.42 0.13 1
4-Nitrophenol ND mg/kg 08/01/19 20:03 100-02-707/31/19 10:432.1 0.67 1
N-Nitrosodimethylamine ND mg/kg 08/01/19 20:03 62-75-907/31/19 10:430.42 0.12 1
N-Nitroso-di-n-propylamine ND mg/kg 08/01/19 20:03 621-64-707/31/19 10:430.42 0.12 1
N-Nitrosodiphenylamine ND mg/kg 08/01/19 20:03 86-30-607/31/19 10:430.42 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/01/19 20:03 108-60-1 v107/31/19 10:430.42 0.12 1
Pentachlorophenol ND mg/kg 08/01/19 20:03 87-86-507/31/19 10:432.1 0.19 1
Phenanthrene ND mg/kg 08/01/19 20:03 85-01-807/31/19 10:430.42 0.11 1
Phenol ND mg/kg 08/01/19 20:03 108-95-207/31/19 10:430.42 0.10 1
Pyrene ND mg/kg 08/01/19 20:03 129-00-007/31/19 10:430.42 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 08/01/19 20:03 120-82-107/31/19 10:430.42 0.097 1
2,4,5-Trichlorophenol ND mg/kg 08/01/19 20:03 95-95-407/31/19 10:430.42 0.11 1
2,4,6-Trichlorophenol ND mg/kg 08/01/19 20:03 88-06-207/31/19 10:430.42 0.11 1
Surrogates
Nitrobenzene-d5 (S)46 %08/01/19 20:03 4165-60-007/31/19 10:4323-110 1
2-Fluorobiphenyl (S)52 %08/01/19 20:03 321-60-807/31/19 10:4330-110 1
Terphenyl-d14 (S)62 %08/01/19 20:03 1718-51-007/31/19 10:4328-110 1
Phenol-d6 (S)50 %08/01/19 20:03 13127-88-307/31/19 10:4322-110 1
2-Fluorophenol (S)52 %08/01/19 20:03 367-12-407/31/19 10:4313-110 1
2,4,6-Tribromophenol (S)86 %08/01/19 20:03 118-79-607/31/19 10:4327-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 0.021J mg/kg 07/30/19 21:33 67-64-107/30/19 13:100.092 0.0092 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-4 (0-2)Lab ID:92438947004 Collected:07/27/19 13:05 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Benzene ND mg/kg 07/30/19 21:33 71-43-207/30/19 13:100.0046 0.0015 1
Bromobenzene ND mg/kg 07/30/19 21:33 108-86-107/30/19 13:100.0046 0.0018 1
Bromochloromethane ND mg/kg 07/30/19 21:33 74-97-507/30/19 13:100.0046 0.0016 1
Bromodichloromethane ND mg/kg 07/30/19 21:33 75-27-407/30/19 13:100.0046 0.0017 1
Bromoform ND mg/kg 07/30/19 21:33 75-25-207/30/19 13:100.0046 0.0021 1
Bromomethane ND mg/kg 07/30/19 21:33 74-83-907/30/19 13:100.0092 0.0023 1
2-Butanone (MEK)ND mg/kg 07/30/19 21:33 78-93-307/30/19 13:100.092 0.0027 1
n-Butylbenzene ND mg/kg 07/30/19 21:33 104-51-807/30/19 13:100.0046 0.0017 1
sec-Butylbenzene ND mg/kg 07/30/19 21:33 135-98-807/30/19 13:100.0046 0.0015 1
tert-Butylbenzene ND mg/kg 07/30/19 21:33 98-06-607/30/19 13:100.0046 0.0018 1
Carbon tetrachloride ND mg/kg 07/30/19 21:33 56-23-507/30/19 13:100.0046 0.0024 1
Chlorobenzene 0.0022J mg/kg 07/30/19 21:33 108-90-707/30/19 13:100.0046 0.0017 1
Chloroethane ND mg/kg 07/30/19 21:33 75-00-307/30/19 13:100.0092 0.0022 1
Chloroform ND mg/kg 07/30/19 21:33 67-66-307/30/19 13:100.0046 0.0015 1
Chloromethane ND mg/kg 07/30/19 21:33 74-87-307/30/19 13:100.0092 0.0022 1
2-Chlorotoluene ND mg/kg 07/30/19 21:33 95-49-807/30/19 13:100.0046 0.0016 1
4-Chlorotoluene ND mg/kg 07/30/19 21:33 106-43-407/30/19 13:100.0046 0.0017 1
1,2-Dibromo-3-chloropropane ND mg/kg 07/30/19 21:33 96-12-807/30/19 13:100.0046 0.0033 1
Dibromochloromethane ND mg/kg 07/30/19 21:33 124-48-107/30/19 13:100.0046 0.0017 1
1,2-Dibromoethane (EDB)ND mg/kg 07/30/19 21:33 106-93-407/30/19 13:100.0046 0.0017 1
Dibromomethane ND mg/kg 07/30/19 21:33 74-95-307/30/19 13:100.0046 0.0023 1
1,2-Dichlorobenzene 0.0056 mg/kg 07/30/19 21:33 95-50-107/30/19 13:100.0046 0.0017 1
1,3-Dichlorobenzene ND mg/kg 07/30/19 21:33 541-73-107/30/19 13:100.0046 0.0018 1
1,4-Dichlorobenzene ND mg/kg 07/30/19 21:33 106-46-707/30/19 13:100.0046 0.0016 1
Dichlorodifluoromethane ND mg/kg 07/30/19 21:33 75-71-807/30/19 13:100.0092 0.0033 1
1,1-Dichloroethane ND mg/kg 07/30/19 21:33 75-34-307/30/19 13:100.0046 0.0014 1
1,2-Dichloroethane ND mg/kg 07/30/19 21:33 107-06-207/30/19 13:100.0046 0.0020 1
1,1-Dichloroethene ND mg/kg 07/30/19 21:33 75-35-407/30/19 13:100.0046 0.0017 1
cis-1,2-Dichloroethene ND mg/kg 07/30/19 21:33 156-59-207/30/19 13:100.0046 0.0013 1
trans-1,2-Dichloroethene ND mg/kg 07/30/19 21:33 156-60-507/30/19 13:100.0046 0.0017 1
1,2-Dichloropropane ND mg/kg 07/30/19 21:33 78-87-507/30/19 13:100.0046 0.0016 1
1,3-Dichloropropane ND mg/kg 07/30/19 21:33 142-28-907/30/19 13:100.0046 0.0017 1
2,2-Dichloropropane ND mg/kg 07/30/19 21:33 594-20-707/30/19 13:100.0046 0.0016 1
1,1-Dichloropropene ND mg/kg 07/30/19 21:33 563-58-607/30/19 13:100.0046 0.0014 1
cis-1,3-Dichloropropene ND mg/kg 07/30/19 21:33 10061-01-507/30/19 13:100.0046 0.0017 1
trans-1,3-Dichloropropene ND mg/kg 07/30/19 21:33 10061-02-607/30/19 13:100.0046 0.0014 1
Diisopropyl ether ND mg/kg 07/30/19 21:33 108-20-307/30/19 13:100.0046 0.0016 1
Ethylbenzene ND mg/kg 07/30/19 21:33 100-41-407/30/19 13:100.0046 0.0017 1
Hexachloro-1,3-butadiene ND mg/kg 07/30/19 21:33 87-68-307/30/19 13:100.0046 0.0018 1
2-Hexanone ND mg/kg 07/30/19 21:33 591-78-607/30/19 13:100.046 0.0036 1
Isopropylbenzene (Cumene)ND mg/kg 07/30/19 21:33 98-82-807/30/19 13:100.0046 0.0017 1
p-Isopropyltoluene ND mg/kg 07/30/19 21:33 99-87-607/30/19 13:100.0046 0.0016 1
Methylene Chloride ND mg/kg 07/30/19 21:33 75-09-207/30/19 13:100.018 0.0028 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 07/30/19 21:33 108-10-107/30/19 13:100.046 0.0034 1
Methyl-tert-butyl ether ND mg/kg 07/30/19 21:33 1634-04-407/30/19 13:100.0046 0.0014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-4 (0-2)Lab ID:92438947004 Collected:07/27/19 13:05 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND mg/kg 07/30/19 21:33 91-20-307/30/19 13:100.0046 0.0011 1
n-Propylbenzene ND mg/kg 07/30/19 21:33 103-65-107/30/19 13:100.0046 0.0016 1
Styrene ND mg/kg 07/30/19 21:33 100-42-507/30/19 13:100.0046 0.0017 1
1,1,1,2-Tetrachloroethane ND mg/kg 07/30/19 21:33 630-20-607/30/19 13:100.0046 0.0019 1
1,1,2,2-Tetrachloroethane ND mg/kg 07/30/19 21:33 79-34-507/30/19 13:100.0046 0.0017 1
Tetrachloroethene ND mg/kg 07/30/19 21:33 127-18-407/30/19 13:100.0046 0.0016 1
Toluene ND mg/kg 07/30/19 21:33 108-88-307/30/19 13:100.0046 0.0017 1
1,2,3-Trichlorobenzene ND mg/kg 07/30/19 21:33 87-61-607/30/19 13:100.0046 0.0020 1
1,2,4-Trichlorobenzene ND mg/kg 07/30/19 21:33 120-82-107/30/19 13:100.0046 0.0015 1
1,1,1-Trichloroethane ND mg/kg 07/30/19 21:33 71-55-607/30/19 13:100.0046 0.0017 1
1,1,2-Trichloroethane ND mg/kg 07/30/19 21:33 79-00-507/30/19 13:100.0046 0.0019 1
Trichloroethene ND mg/kg 07/30/19 21:33 79-01-607/30/19 13:100.0046 0.0019 1
Trichlorofluoromethane ND mg/kg 07/30/19 21:33 75-69-407/30/19 13:100.0046 0.0020 1
1,2,3-Trichloropropane ND mg/kg 07/30/19 21:33 96-18-407/30/19 13:100.0046 0.0015 1
1,2,4-Trimethylbenzene 0.0025J mg/kg 07/30/19 21:33 95-63-607/30/19 13:100.0046 0.0018 1
1,3,5-Trimethylbenzene ND mg/kg 07/30/19 21:33 108-67-807/30/19 13:100.0046 0.0017 1
Vinyl acetate ND mg/kg 07/30/19 21:33 108-05-407/30/19 13:100.046 0.0081 1
Vinyl chloride ND mg/kg 07/30/19 21:33 75-01-407/30/19 13:100.0092 0.0017 1
Xylene (Total)ND mg/kg 07/30/19 21:33 1330-20-707/30/19 13:100.0092 0.0033 1
m&p-Xylene ND mg/kg 07/30/19 21:33 179601-23-107/30/19 13:100.0092 0.0033 1
o-Xylene ND mg/kg 07/30/19 21:33 95-47-607/30/19 13:100.0046 0.0017 1
Surrogates
Toluene-d8 (S)103 %07/30/19 21:33 2037-26-507/30/19 13:1070-130 1
4-Bromofluorobenzene (S)100 %07/30/19 21:33 460-00-407/30/19 13:1070-130 1
1,2-Dichloroethane-d4 (S)81 %07/30/19 21:33 17060-07-007/30/19 13:1070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.4 %07/29/19 16:170.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 70.9 %08/03/19 16:3308/03/19 16:221
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/05/19 15:15 18540-29-908/05/19 11:321.41 0.360 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-5 (0-2)Lab ID:92438947005 Collected:07/27/19 13:55 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 2.26 mg/kg 08/02/19 14:47 7440-38-208/01/19 20:160.670 0.167 5
Barium 55.7 mg/kg 08/02/19 14:47 7440-39-308/01/19 20:161.34 0.214 5
Cadmium ND mg/kg 08/02/19 14:47 7440-43-908/01/19 20:160.670 0.107 5
Chromium 41.9 mg/kg 08/02/19 14:47 7440-47-308/01/19 20:161.34 0.362 5
Lead 14.7 mg/kg 08/02/19 14:47 7439-92-108/01/19 20:160.670 0.161 5
Selenium 0.830 mg/kg 08/02/19 14:47 7782-49-208/01/19 20:160.670 0.254 5
Silver ND mg/kg 08/02/19 14:47 7440-22-408/01/19 20:160.670 0.208 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.768 mg/kg 08/04/19 12:19 7439-97-608/02/19 10:190.0402 0.00375 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/02/19 13:55 83-32-907/31/19 10:430.43 0.11 1
Acenaphthylene ND mg/kg 08/02/19 13:55 208-96-807/31/19 10:430.43 0.10 1
Aniline ND mg/kg 08/02/19 13:55 62-53-307/31/19 10:430.43 0.097 1
Anthracene ND mg/kg 08/02/19 13:55 120-12-707/31/19 10:430.43 0.11 1
Benzo(a)anthracene ND mg/kg 08/02/19 13:55 56-55-307/31/19 10:430.43 0.14 1
Benzo(a)pyrene ND mg/kg 08/02/19 13:55 50-32-807/31/19 10:430.43 0.19 1
Benzo(b)fluoranthene ND mg/kg 08/02/19 13:55 205-99-207/31/19 10:430.43 0.17 1
Benzo(g,h,i)perylene ND mg/kg 08/02/19 13:55 191-24-207/31/19 10:430.43 0.17 1
Benzo(k)fluoranthene ND mg/kg 08/02/19 13:55 207-08-907/31/19 10:430.43 0.18 1
Benzoic Acid ND mg/kg 08/02/19 13:55 65-85-007/31/19 10:432.2 0.46 1
Benzyl alcohol ND mg/kg 08/02/19 13:55 100-51-607/31/19 10:430.86 0.23 1
4-Bromophenylphenyl ether ND mg/kg 08/02/19 13:55 101-55-307/31/19 10:430.43 0.11 1
Butylbenzylphthalate ND mg/kg 08/02/19 13:55 85-68-707/31/19 10:430.43 0.11 1
4-Chloro-3-methylphenol ND mg/kg 08/02/19 13:55 59-50-707/31/19 10:430.86 0.26 1
4-Chloroaniline ND mg/kg 08/02/19 13:55 106-47-807/31/19 10:432.2 0.26 1
bis(2-Chloroethoxy)methane ND mg/kg 08/02/19 13:55 111-91-107/31/19 10:430.43 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 08/02/19 13:55 111-44-4 v107/31/19 10:430.43 0.091 1
2-Chloronaphthalene ND mg/kg 08/02/19 13:55 91-58-707/31/19 10:430.43 0.096 1
2-Chlorophenol ND mg/kg 08/02/19 13:55 95-57-807/31/19 10:430.43 0.10 1
4-Chlorophenylphenyl ether ND mg/kg 08/02/19 13:55 7005-72-307/31/19 10:430.43 0.11 1
Chrysene ND mg/kg 08/02/19 13:55 218-01-907/31/19 10:430.43 0.13 1
Dibenz(a,h)anthracene ND mg/kg 08/02/19 13:55 53-70-307/31/19 10:430.43 0.17 1
Dibenzofuran ND mg/kg 08/02/19 13:55 132-64-907/31/19 10:430.43 0.11 1
1,2-Dichlorobenzene ND mg/kg 08/02/19 13:55 95-50-107/31/19 10:430.43 0.093 1
1,3-Dichlorobenzene ND mg/kg 08/02/19 13:55 541-73-107/31/19 10:430.43 0.097 1
1,4-Dichlorobenzene ND mg/kg 08/02/19 13:55 106-46-707/31/19 10:430.43 0.095 1
3,3'-Dichlorobenzidine ND mg/kg 08/02/19 13:55 91-94-107/31/19 10:432.2 0.30 1
2,4-Dichlorophenol ND mg/kg 08/02/19 13:55 120-83-207/31/19 10:430.43 0.14 1
Diethylphthalate ND mg/kg 08/02/19 13:55 84-66-207/31/19 10:430.43 0.093 1
2,4-Dimethylphenol ND mg/kg 08/02/19 13:55 105-67-907/31/19 10:430.43 0.11 1
Dimethylphthalate ND mg/kg 08/02/19 13:55 131-11-307/31/19 10:430.43 0.097 1
Di-n-butylphthalate ND mg/kg 08/02/19 13:55 84-74-207/31/19 10:430.43 0.11 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/02/19 13:55 534-52-1 v107/31/19 10:430.86 0.69 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-5 (0-2)Lab ID:92438947005 Collected:07/27/19 13:55 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 08/02/19 13:55 51-28-507/31/19 10:432.2 1.4 1
2,4-Dinitrotoluene ND mg/kg 08/02/19 13:55 121-14-207/31/19 10:430.43 0.11 1
2,6-Dinitrotoluene ND mg/kg 08/02/19 13:55 606-20-207/31/19 10:430.43 0.11 1
Di-n-octylphthalate ND mg/kg 08/02/19 13:55 117-84-007/31/19 10:430.43 0.25 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/02/19 13:55 117-81-707/31/19 10:430.43 0.14 1
Fluoranthene ND mg/kg 08/02/19 13:55 206-44-007/31/19 10:430.43 0.13 1
Fluorene ND mg/kg 08/02/19 13:55 86-73-707/31/19 10:430.43 0.12 1
Hexachloro-1,3-butadiene ND mg/kg 08/02/19 13:55 87-68-307/31/19 10:430.43 0.10 1
Hexachlorobenzene ND mg/kg 08/02/19 13:55 118-74-107/31/19 10:430.43 0.11 1
Hexachlorocyclopentadiene ND mg/kg 08/02/19 13:55 77-47-4 v107/31/19 10:430.43 0.17 1
Hexachloroethane ND mg/kg 08/02/19 13:55 67-72-107/31/19 10:430.43 0.098 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/02/19 13:55 193-39-507/31/19 10:430.43 0.20 1
Isophorone ND mg/kg 08/02/19 13:55 78-59-107/31/19 10:430.43 0.094 1
1-Methylnaphthalene ND mg/kg 08/02/19 13:55 90-12-007/31/19 10:430.43 0.11 1
2-Methylnaphthalene ND mg/kg 08/02/19 13:55 91-57-607/31/19 10:430.43 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 08/02/19 13:55 95-48-707/31/19 10:430.43 0.095 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/02/19 13:55 15831-10-4 v107/31/19 10:430.43 0.11 1
Naphthalene ND mg/kg 08/02/19 13:55 91-20-307/31/19 10:430.43 0.10 1
2-Nitroaniline ND mg/kg 08/02/19 13:55 88-74-4 v107/31/19 10:432.2 0.22 1
3-Nitroaniline ND mg/kg 08/02/19 13:55 99-09-207/31/19 10:432.2 0.23 1
4-Nitroaniline ND mg/kg 08/02/19 13:55 100-01-607/31/19 10:430.86 0.21 1
Nitrobenzene ND mg/kg 08/02/19 13:55 98-95-307/31/19 10:430.43 0.10 1
2-Nitrophenol ND mg/kg 08/02/19 13:55 88-75-507/31/19 10:430.43 0.13 1
4-Nitrophenol ND mg/kg 08/02/19 13:55 100-02-707/31/19 10:432.2 0.69 1
N-Nitrosodimethylamine ND mg/kg 08/02/19 13:55 62-75-9 v107/31/19 10:430.43 0.12 1
N-Nitroso-di-n-propylamine ND mg/kg 08/02/19 13:55 621-64-707/31/19 10:430.43 0.12 1
N-Nitrosodiphenylamine ND mg/kg 08/02/19 13:55 86-30-607/31/19 10:430.43 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/02/19 13:55 108-60-1 v107/31/19 10:430.43 0.12 1
Pentachlorophenol ND mg/kg 08/02/19 13:55 87-86-507/31/19 10:432.2 0.20 1
Phenanthrene ND mg/kg 08/02/19 13:55 85-01-807/31/19 10:430.43 0.11 1
Phenol ND mg/kg 08/02/19 13:55 108-95-207/31/19 10:430.43 0.10 1
Pyrene ND mg/kg 08/02/19 13:55 129-00-007/31/19 10:430.43 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 08/02/19 13:55 120-82-107/31/19 10:430.43 0.099 1
2,4,5-Trichlorophenol ND mg/kg 08/02/19 13:55 95-95-407/31/19 10:430.43 0.11 1
2,4,6-Trichlorophenol ND mg/kg 08/02/19 13:55 88-06-207/31/19 10:430.43 0.11 1
Surrogates
Nitrobenzene-d5 (S)67 %08/02/19 13:55 4165-60-007/31/19 10:4323-110 1
2-Fluorobiphenyl (S)56 %08/02/19 13:55 321-60-807/31/19 10:4330-110 1
Terphenyl-d14 (S)76 %08/02/19 13:55 1718-51-007/31/19 10:4328-110 1
Phenol-d6 (S)65 %08/02/19 13:55 13127-88-307/31/19 10:4322-110 1
2-Fluorophenol (S)69 %08/02/19 13:55 367-12-407/31/19 10:4313-110 1
2,4,6-Tribromophenol (S)75 %08/02/19 13:55 118-79-607/31/19 10:4327-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 0.033J mg/kg 07/31/19 12:35 67-64-107/31/19 11:380.094 0.0094 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-5 (0-2)Lab ID:92438947005 Collected:07/27/19 13:55 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Benzene ND mg/kg 07/31/19 12:35 71-43-207/31/19 11:380.0047 0.0015 1
Bromobenzene ND mg/kg 07/31/19 12:35 108-86-107/31/19 11:380.0047 0.0019 1
Bromochloromethane ND mg/kg 07/31/19 12:35 74-97-507/31/19 11:380.0047 0.0016 1
Bromodichloromethane ND mg/kg 07/31/19 12:35 75-27-407/31/19 11:380.0047 0.0018 1
Bromoform ND mg/kg 07/31/19 12:35 75-25-207/31/19 11:380.0047 0.0022 1
Bromomethane ND mg/kg 07/31/19 12:35 74-83-907/31/19 11:380.0094 0.0023 1
2-Butanone (MEK)ND mg/kg 07/31/19 12:35 78-93-307/31/19 11:380.094 0.0027 1
n-Butylbenzene ND mg/kg 07/31/19 12:35 104-51-807/31/19 11:380.0047 0.0017 1
sec-Butylbenzene ND mg/kg 07/31/19 12:35 135-98-807/31/19 11:380.0047 0.0015 1
tert-Butylbenzene ND mg/kg 07/31/19 12:35 98-06-607/31/19 11:380.0047 0.0019 1
Carbon tetrachloride ND mg/kg 07/31/19 12:35 56-23-507/31/19 11:380.0047 0.0024 1
Chlorobenzene ND mg/kg 07/31/19 12:35 108-90-707/31/19 11:380.0047 0.0018 1
Chloroethane ND mg/kg 07/31/19 12:35 75-00-307/31/19 11:380.0094 0.0022 1
Chloroform ND mg/kg 07/31/19 12:35 67-66-307/31/19 11:380.0047 0.0015 1
Chloromethane ND mg/kg 07/31/19 12:35 74-87-307/31/19 11:380.0094 0.0022 1
2-Chlorotoluene ND mg/kg 07/31/19 12:35 95-49-807/31/19 11:380.0047 0.0016 1
4-Chlorotoluene ND mg/kg 07/31/19 12:35 106-43-407/31/19 11:380.0047 0.0017 1
1,2-Dibromo-3-chloropropane ND mg/kg 07/31/19 12:35 96-12-807/31/19 11:380.0047 0.0034 1
Dibromochloromethane ND mg/kg 07/31/19 12:35 124-48-107/31/19 11:380.0047 0.0017 1
1,2-Dibromoethane (EDB)ND mg/kg 07/31/19 12:35 106-93-407/31/19 11:380.0047 0.0017 1
Dibromomethane ND mg/kg 07/31/19 12:35 74-95-307/31/19 11:380.0047 0.0023 1
1,2-Dichlorobenzene ND mg/kg 07/31/19 12:35 95-50-107/31/19 11:380.0047 0.0018 1
1,3-Dichlorobenzene ND mg/kg 07/31/19 12:35 541-73-107/31/19 11:380.0047 0.0019 1
1,4-Dichlorobenzene ND mg/kg 07/31/19 12:35 106-46-707/31/19 11:380.0047 0.0016 1
Dichlorodifluoromethane ND mg/kg 07/31/19 12:35 75-71-807/31/19 11:380.0094 0.0034 1
1,1-Dichloroethane ND mg/kg 07/31/19 12:35 75-34-307/31/19 11:380.0047 0.0014 1
1,2-Dichloroethane ND mg/kg 07/31/19 12:35 107-06-207/31/19 11:380.0047 0.0021 1
1,1-Dichloroethene ND mg/kg 07/31/19 12:35 75-35-407/31/19 11:380.0047 0.0017 1
cis-1,2-Dichloroethene ND mg/kg 07/31/19 12:35 156-59-207/31/19 11:380.0047 0.0013 1
trans-1,2-Dichloroethene ND mg/kg 07/31/19 12:35 156-60-507/31/19 11:380.0047 0.0018 1
1,2-Dichloropropane ND mg/kg 07/31/19 12:35 78-87-507/31/19 11:380.0047 0.0016 1
1,3-Dichloropropane ND mg/kg 07/31/19 12:35 142-28-907/31/19 11:380.0047 0.0018 1
2,2-Dichloropropane ND mg/kg 07/31/19 12:35 594-20-707/31/19 11:380.0047 0.0016 1
1,1-Dichloropropene ND mg/kg 07/31/19 12:35 563-58-607/31/19 11:380.0047 0.0014 1
cis-1,3-Dichloropropene ND mg/kg 07/31/19 12:35 10061-01-507/31/19 11:380.0047 0.0017 1
trans-1,3-Dichloropropene ND mg/kg 07/31/19 12:35 10061-02-607/31/19 11:380.0047 0.0014 1
Diisopropyl ether ND mg/kg 07/31/19 12:35 108-20-307/31/19 11:380.0047 0.0016 1
Ethylbenzene ND mg/kg 07/31/19 12:35 100-41-407/31/19 11:380.0047 0.0017 1
Hexachloro-1,3-butadiene ND mg/kg 07/31/19 12:35 87-68-307/31/19 11:380.0047 0.0019 1
2-Hexanone ND mg/kg 07/31/19 12:35 591-78-607/31/19 11:380.047 0.0037 1
Isopropylbenzene (Cumene)ND mg/kg 07/31/19 12:35 98-82-807/31/19 11:380.0047 0.0018 1
p-Isopropyltoluene ND mg/kg 07/31/19 12:35 99-87-607/31/19 11:380.0047 0.0016 1
Methylene Chloride ND mg/kg 07/31/19 12:35 75-09-207/31/19 11:380.019 0.0028 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 07/31/19 12:35 108-10-107/31/19 11:380.047 0.0035 1
Methyl-tert-butyl ether ND mg/kg 07/31/19 12:35 1634-04-407/31/19 11:380.0047 0.0014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-5 (0-2)Lab ID:92438947005 Collected:07/27/19 13:55 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene 0.0028J mg/kg 07/31/19 12:35 91-20-307/31/19 11:380.0047 0.0011 1
n-Propylbenzene ND mg/kg 07/31/19 12:35 103-65-107/31/19 11:380.0047 0.0016 1
Styrene ND mg/kg 07/31/19 12:35 100-42-507/31/19 11:380.0047 0.0017 1
1,1,1,2-Tetrachloroethane ND mg/kg 07/31/19 12:35 630-20-607/31/19 11:380.0047 0.0020 1
1,1,2,2-Tetrachloroethane ND mg/kg 07/31/19 12:35 79-34-507/31/19 11:380.0047 0.0018 1
Tetrachloroethene ND mg/kg 07/31/19 12:35 127-18-407/31/19 11:380.0047 0.0016 1
Toluene ND mg/kg 07/31/19 12:35 108-88-307/31/19 11:380.0047 0.0017 1
1,2,3-Trichlorobenzene ND mg/kg 07/31/19 12:35 87-61-607/31/19 11:380.0047 0.0021 1
1,2,4-Trichlorobenzene ND mg/kg 07/31/19 12:35 120-82-107/31/19 11:380.0047 0.0015 1
1,1,1-Trichloroethane ND mg/kg 07/31/19 12:35 71-55-607/31/19 11:380.0047 0.0017 1
1,1,2-Trichloroethane ND mg/kg 07/31/19 12:35 79-00-507/31/19 11:380.0047 0.0020 1
Trichloroethene ND mg/kg 07/31/19 12:35 79-01-607/31/19 11:380.0047 0.0020 1
Trichlorofluoromethane ND mg/kg 07/31/19 12:35 75-69-407/31/19 11:380.0047 0.0021 1
1,2,3-Trichloropropane ND mg/kg 07/31/19 12:35 96-18-407/31/19 11:380.0047 0.0015 1
1,2,4-Trimethylbenzene ND mg/kg 07/31/19 12:35 95-63-607/31/19 11:380.0047 0.0019 1
1,3,5-Trimethylbenzene ND mg/kg 07/31/19 12:35 108-67-807/31/19 11:380.0047 0.0017 1
Vinyl acetate ND mg/kg 07/31/19 12:35 108-05-4 v107/31/19 11:380.047 0.0082 1
Vinyl chloride ND mg/kg 07/31/19 12:35 75-01-407/31/19 11:380.0094 0.0017 1
Xylene (Total)ND mg/kg 07/31/19 12:35 1330-20-707/31/19 11:380.0094 0.0034 1
m&p-Xylene ND mg/kg 07/31/19 12:35 179601-23-107/31/19 11:380.0094 0.0034 1
o-Xylene ND mg/kg 07/31/19 12:35 95-47-607/31/19 11:380.0047 0.0018 1
Surrogates
Toluene-d8 (S)101 %07/31/19 12:35 2037-26-507/31/19 11:3870-130 1
4-Bromofluorobenzene (S)105 %07/31/19 12:35 460-00-407/31/19 11:3870-130 1
1,2-Dichloroethane-d4 (S)96 %07/31/19 12:35 17060-07-007/31/19 11:3870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.6 %07/29/19 16:170.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 74.7 %08/03/19 16:0508/03/19 15:541
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.386J mg/kg 08/05/19 15:35 18540-29-9 J08/05/19 11:321.34 0.341 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-6 (2-3)Lab ID:92438947006 Collected:07/27/19 14:00 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 3.73 mg/kg 08/02/19 14:52 7440-38-208/01/19 20:160.658 0.165 5
Barium 294 mg/kg 08/02/19 14:52 7440-39-308/01/19 20:161.32 0.211 5
Cadmium ND mg/kg 08/02/19 14:52 7440-43-908/01/19 20:160.658 0.105 5
Chromium 76.1 mg/kg 08/02/19 14:52 7440-47-308/01/19 20:161.32 0.355 5
Lead 20.1 mg/kg 08/02/19 14:52 7439-92-108/01/19 20:160.658 0.158 5
Selenium 1.31 mg/kg 08/02/19 14:52 7782-49-208/01/19 20:160.658 0.250 5
Silver ND mg/kg 08/02/19 14:52 7440-22-408/01/19 20:160.658 0.204 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.456 mg/kg 08/04/19 12:22 7439-97-608/02/19 10:190.0395 0.00369 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/01/19 18:47 83-32-907/31/19 10:430.42 0.11 1
Acenaphthylene ND mg/kg 08/01/19 18:47 208-96-807/31/19 10:430.42 0.098 1
Aniline ND mg/kg 08/01/19 18:47 62-53-307/31/19 10:430.42 0.093 1
Anthracene ND mg/kg 08/01/19 18:47 120-12-707/31/19 10:430.42 0.11 1
Benzo(a)anthracene ND mg/kg 08/01/19 18:47 56-55-307/31/19 10:430.42 0.13 1
Benzo(a)pyrene ND mg/kg 08/01/19 18:47 50-32-807/31/19 10:430.42 0.18 1
Benzo(b)fluoranthene ND mg/kg 08/01/19 18:47 205-99-207/31/19 10:430.42 0.17 1
Benzo(g,h,i)perylene ND mg/kg 08/01/19 18:47 191-24-207/31/19 10:430.42 0.16 1
Benzo(k)fluoranthene ND mg/kg 08/01/19 18:47 207-08-907/31/19 10:430.42 0.18 1
Benzoic Acid ND mg/kg 08/01/19 18:47 65-85-007/31/19 10:432.1 0.45 1
Benzyl alcohol ND mg/kg 08/01/19 18:47 100-51-607/31/19 10:430.83 0.22 1
4-Bromophenylphenyl ether ND mg/kg 08/01/19 18:47 101-55-307/31/19 10:430.42 0.11 1
Butylbenzylphthalate ND mg/kg 08/01/19 18:47 85-68-707/31/19 10:430.42 0.11 1
4-Chloro-3-methylphenol ND mg/kg 08/01/19 18:47 59-50-707/31/19 10:430.83 0.25 1
4-Chloroaniline ND mg/kg 08/01/19 18:47 106-47-807/31/19 10:432.1 0.25 1
bis(2-Chloroethoxy)methane ND mg/kg 08/01/19 18:47 111-91-107/31/19 10:430.42 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 08/01/19 18:47 111-44-407/31/19 10:430.42 0.088 1
2-Chloronaphthalene ND mg/kg 08/01/19 18:47 91-58-707/31/19 10:430.42 0.093 1
2-Chlorophenol ND mg/kg 08/01/19 18:47 95-57-807/31/19 10:430.42 0.097 1
4-Chlorophenylphenyl ether ND mg/kg 08/01/19 18:47 7005-72-307/31/19 10:430.42 0.11 1
Chrysene ND mg/kg 08/01/19 18:47 218-01-907/31/19 10:430.42 0.12 1
Dibenz(a,h)anthracene ND mg/kg 08/01/19 18:47 53-70-307/31/19 10:430.42 0.17 1
Dibenzofuran ND mg/kg 08/01/19 18:47 132-64-907/31/19 10:430.42 0.10 1
1,2-Dichlorobenzene ND mg/kg 08/01/19 18:47 95-50-107/31/19 10:430.42 0.090 1
1,3-Dichlorobenzene ND mg/kg 08/01/19 18:47 541-73-107/31/19 10:430.42 0.094 1
1,4-Dichlorobenzene ND mg/kg 08/01/19 18:47 106-46-707/31/19 10:430.42 0.091 1
3,3'-Dichlorobenzidine ND mg/kg 08/01/19 18:47 91-94-107/31/19 10:432.1 0.29 1
2,4-Dichlorophenol ND mg/kg 08/01/19 18:47 120-83-207/31/19 10:430.42 0.14 1
Diethylphthalate ND mg/kg 08/01/19 18:47 84-66-207/31/19 10:430.42 0.090 1
2,4-Dimethylphenol ND mg/kg 08/01/19 18:47 105-67-907/31/19 10:430.42 0.10 1
Dimethylphthalate ND mg/kg 08/01/19 18:47 131-11-307/31/19 10:430.42 0.094 1
Di-n-butylphthalate ND mg/kg 08/01/19 18:47 84-74-207/31/19 10:430.42 0.10 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/01/19 18:47 534-52-107/31/19 10:430.83 0.67 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-6 (2-3)Lab ID:92438947006 Collected:07/27/19 14:00 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 08/01/19 18:47 51-28-507/31/19 10:432.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 08/01/19 18:47 121-14-207/31/19 10:430.42 0.11 1
2,6-Dinitrotoluene ND mg/kg 08/01/19 18:47 606-20-207/31/19 10:430.42 0.11 1
Di-n-octylphthalate ND mg/kg 08/01/19 18:47 117-84-007/31/19 10:430.42 0.24 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/01/19 18:47 117-81-707/31/19 10:430.42 0.14 1
Fluoranthene ND mg/kg 08/01/19 18:47 206-44-007/31/19 10:430.42 0.13 1
Fluorene ND mg/kg 08/01/19 18:47 86-73-707/31/19 10:430.42 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 08/01/19 18:47 87-68-307/31/19 10:430.42 0.10 1
Hexachlorobenzene ND mg/kg 08/01/19 18:47 118-74-107/31/19 10:430.42 0.11 1
Hexachlorocyclopentadiene ND mg/kg 08/01/19 18:47 77-47-407/31/19 10:430.42 0.17 1
Hexachloroethane ND mg/kg 08/01/19 18:47 67-72-107/31/19 10:430.42 0.095 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/01/19 18:47 193-39-507/31/19 10:430.42 0.19 1
Isophorone ND mg/kg 08/01/19 18:47 78-59-107/31/19 10:430.42 0.090 1
1-Methylnaphthalene ND mg/kg 08/01/19 18:47 90-12-007/31/19 10:430.42 0.11 1
2-Methylnaphthalene ND mg/kg 08/01/19 18:47 91-57-607/31/19 10:430.42 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 08/01/19 18:47 95-48-707/31/19 10:430.42 0.092 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/01/19 18:47 15831-10-407/31/19 10:430.42 0.10 1
Naphthalene ND mg/kg 08/01/19 18:47 91-20-307/31/19 10:430.42 0.10 1
2-Nitroaniline ND mg/kg 08/01/19 18:47 88-74-407/31/19 10:432.1 0.21 1
3-Nitroaniline ND mg/kg 08/01/19 18:47 99-09-207/31/19 10:432.1 0.22 1
4-Nitroaniline ND mg/kg 08/01/19 18:47 100-01-607/31/19 10:430.83 0.21 1
Nitrobenzene ND mg/kg 08/01/19 18:47 98-95-307/31/19 10:430.42 0.099 1
2-Nitrophenol ND mg/kg 08/01/19 18:47 88-75-507/31/19 10:430.42 0.13 1
4-Nitrophenol ND mg/kg 08/01/19 18:47 100-02-707/31/19 10:432.1 0.66 1
N-Nitrosodimethylamine ND mg/kg 08/01/19 18:47 62-75-907/31/19 10:430.42 0.12 1
N-Nitroso-di-n-propylamine ND mg/kg 08/01/19 18:47 621-64-707/31/19 10:430.42 0.12 1
N-Nitrosodiphenylamine ND mg/kg 08/01/19 18:47 86-30-607/31/19 10:430.42 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/01/19 18:47 108-60-1 v107/31/19 10:430.42 0.12 1
Pentachlorophenol ND mg/kg 08/01/19 18:47 87-86-507/31/19 10:432.1 0.19 1
Phenanthrene ND mg/kg 08/01/19 18:47 85-01-807/31/19 10:430.42 0.10 1
Phenol ND mg/kg 08/01/19 18:47 108-95-207/31/19 10:430.42 0.099 1
Pyrene ND mg/kg 08/01/19 18:47 129-00-007/31/19 10:430.42 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 08/01/19 18:47 120-82-107/31/19 10:430.42 0.095 1
2,4,5-Trichlorophenol ND mg/kg 08/01/19 18:47 95-95-407/31/19 10:430.42 0.11 1
2,4,6-Trichlorophenol ND mg/kg 08/01/19 18:47 88-06-207/31/19 10:430.42 0.10 1
Surrogates
Nitrobenzene-d5 (S)70 %08/01/19 18:47 4165-60-007/31/19 10:4323-110 1
2-Fluorobiphenyl (S)60 %08/01/19 18:47 321-60-807/31/19 10:4330-110 1
Terphenyl-d14 (S)75 %08/01/19 18:47 1718-51-007/31/19 10:4328-110 1
Phenol-d6 (S)68 %08/01/19 18:47 13127-88-307/31/19 10:4322-110 1
2-Fluorophenol (S)69 %08/01/19 18:47 367-12-407/31/19 10:4313-110 1
2,4,6-Tribromophenol (S)61 %08/01/19 18:47 118-79-607/31/19 10:4327-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 0.024J mg/kg 07/31/19 15:52 67-64-107/31/19 12:070.096 0.0096 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-6 (2-3)Lab ID:92438947006 Collected:07/27/19 14:00 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Benzene ND mg/kg 07/31/19 15:52 71-43-207/31/19 12:070.0048 0.0015 1
Bromobenzene ND mg/kg 07/31/19 15:52 108-86-107/31/19 12:070.0048 0.0019 1
Bromochloromethane ND mg/kg 07/31/19 15:52 74-97-507/31/19 12:070.0048 0.0016 1
Bromodichloromethane ND mg/kg 07/31/19 15:52 75-27-407/31/19 12:070.0048 0.0018 1
Bromoform ND mg/kg 07/31/19 15:52 75-25-207/31/19 12:070.0048 0.0022 1
Bromomethane ND mg/kg 07/31/19 15:52 74-83-907/31/19 12:070.0096 0.0024 1
2-Butanone (MEK)ND mg/kg 07/31/19 15:52 78-93-307/31/19 12:070.096 0.0028 1
n-Butylbenzene ND mg/kg 07/31/19 15:52 104-51-807/31/19 12:070.0048 0.0017 1
sec-Butylbenzene ND mg/kg 07/31/19 15:52 135-98-807/31/19 12:070.0048 0.0015 1
tert-Butylbenzene ND mg/kg 07/31/19 15:52 98-06-607/31/19 12:070.0048 0.0019 1
Carbon tetrachloride ND mg/kg 07/31/19 15:52 56-23-507/31/19 12:070.0048 0.0025 1
Chlorobenzene ND mg/kg 07/31/19 15:52 108-90-707/31/19 12:070.0048 0.0018 1
Chloroethane ND mg/kg 07/31/19 15:52 75-00-307/31/19 12:070.0096 0.0023 1
Chloroform ND mg/kg 07/31/19 15:52 67-66-307/31/19 12:070.0048 0.0015 1
Chloromethane ND mg/kg 07/31/19 15:52 74-87-307/31/19 12:070.0096 0.0023 1
2-Chlorotoluene ND mg/kg 07/31/19 15:52 95-49-807/31/19 12:070.0048 0.0016 1
4-Chlorotoluene ND mg/kg 07/31/19 15:52 106-43-407/31/19 12:070.0048 0.0017 1
1,2-Dibromo-3-chloropropane ND mg/kg 07/31/19 15:52 96-12-807/31/19 12:070.0048 0.0034 1
Dibromochloromethane ND mg/kg 07/31/19 15:52 124-48-107/31/19 12:070.0048 0.0017 1
1,2-Dibromoethane (EDB)ND mg/kg 07/31/19 15:52 106-93-407/31/19 12:070.0048 0.0017 1
Dibromomethane ND mg/kg 07/31/19 15:52 74-95-307/31/19 12:070.0048 0.0024 1
1,2-Dichlorobenzene ND mg/kg 07/31/19 15:52 95-50-107/31/19 12:070.0048 0.0018 1
1,3-Dichlorobenzene ND mg/kg 07/31/19 15:52 541-73-107/31/19 12:070.0048 0.0019 1
1,4-Dichlorobenzene ND mg/kg 07/31/19 15:52 106-46-707/31/19 12:070.0048 0.0016 1
Dichlorodifluoromethane ND mg/kg 07/31/19 15:52 75-71-807/31/19 12:070.0096 0.0034 1
1,1-Dichloroethane ND mg/kg 07/31/19 15:52 75-34-307/31/19 12:070.0048 0.0014 1
1,2-Dichloroethane ND mg/kg 07/31/19 15:52 107-06-207/31/19 12:070.0048 0.0021 1
1,1-Dichloroethene ND mg/kg 07/31/19 15:52 75-35-407/31/19 12:070.0048 0.0017 1
cis-1,2-Dichloroethene ND mg/kg 07/31/19 15:52 156-59-207/31/19 12:070.0048 0.0013 1
trans-1,2-Dichloroethene ND mg/kg 07/31/19 15:52 156-60-507/31/19 12:070.0048 0.0018 1
1,2-Dichloropropane ND mg/kg 07/31/19 15:52 78-87-507/31/19 12:070.0048 0.0016 1
1,3-Dichloropropane ND mg/kg 07/31/19 15:52 142-28-907/31/19 12:070.0048 0.0018 1
2,2-Dichloropropane ND mg/kg 07/31/19 15:52 594-20-707/31/19 12:070.0048 0.0016 1
1,1-Dichloropropene ND mg/kg 07/31/19 15:52 563-58-607/31/19 12:070.0048 0.0014 1
cis-1,3-Dichloropropene ND mg/kg 07/31/19 15:52 10061-01-507/31/19 12:070.0048 0.0017 1
trans-1,3-Dichloropropene ND mg/kg 07/31/19 15:52 10061-02-607/31/19 12:070.0048 0.0014 1
Diisopropyl ether ND mg/kg 07/31/19 15:52 108-20-307/31/19 12:070.0048 0.0016 1
Ethylbenzene ND mg/kg 07/31/19 15:52 100-41-407/31/19 12:070.0048 0.0017 1
Hexachloro-1,3-butadiene ND mg/kg 07/31/19 15:52 87-68-307/31/19 12:070.0048 0.0019 1
2-Hexanone ND mg/kg 07/31/19 15:52 591-78-607/31/19 12:070.048 0.0037 1
Isopropylbenzene (Cumene)ND mg/kg 07/31/19 15:52 98-82-807/31/19 12:070.0048 0.0018 1
p-Isopropyltoluene ND mg/kg 07/31/19 15:52 99-87-607/31/19 12:070.0048 0.0016 1
Methylene Chloride ND mg/kg 07/31/19 15:52 75-09-2 v207/31/19 12:070.019 0.0029 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 07/31/19 15:52 108-10-107/31/19 12:070.048 0.0035 1
Methyl-tert-butyl ether ND mg/kg 07/31/19 15:52 1634-04-407/31/19 12:070.0048 0.0014 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-6 (2-3)Lab ID:92438947006 Collected:07/27/19 14:00 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND mg/kg 07/31/19 15:52 91-20-307/31/19 12:070.0048 0.0011 1
n-Propylbenzene ND mg/kg 07/31/19 15:52 103-65-107/31/19 12:070.0048 0.0016 1
Styrene ND mg/kg 07/31/19 15:52 100-42-507/31/19 12:070.0048 0.0017 1
1,1,1,2-Tetrachloroethane ND mg/kg 07/31/19 15:52 630-20-607/31/19 12:070.0048 0.0020 1
1,1,2,2-Tetrachloroethane ND mg/kg 07/31/19 15:52 79-34-507/31/19 12:070.0048 0.0018 1
Tetrachloroethene ND mg/kg 07/31/19 15:52 127-18-407/31/19 12:070.0048 0.0016 1
Toluene ND mg/kg 07/31/19 15:52 108-88-307/31/19 12:070.0048 0.0017 1
1,2,3-Trichlorobenzene ND mg/kg 07/31/19 15:52 87-61-607/31/19 12:070.0048 0.0021 1
1,2,4-Trichlorobenzene ND mg/kg 07/31/19 15:52 120-82-107/31/19 12:070.0048 0.0015 1
1,1,1-Trichloroethane ND mg/kg 07/31/19 15:52 71-55-607/31/19 12:070.0048 0.0017 1
1,1,2-Trichloroethane ND mg/kg 07/31/19 15:52 79-00-507/31/19 12:070.0048 0.0020 1
Trichloroethene ND mg/kg 07/31/19 15:52 79-01-607/31/19 12:070.0048 0.0020 1
Trichlorofluoromethane ND mg/kg 07/31/19 15:52 75-69-407/31/19 12:070.0048 0.0021 1
1,2,3-Trichloropropane ND mg/kg 07/31/19 15:52 96-18-407/31/19 12:070.0048 0.0015 1
1,2,4-Trimethylbenzene ND mg/kg 07/31/19 15:52 95-63-607/31/19 12:070.0048 0.0019 1
1,3,5-Trimethylbenzene ND mg/kg 07/31/19 15:52 108-67-807/31/19 12:070.0048 0.0017 1
Vinyl acetate ND mg/kg 07/31/19 15:52 108-05-407/31/19 12:070.048 0.0084 1
Vinyl chloride ND mg/kg 07/31/19 15:52 75-01-407/31/19 12:070.0096 0.0017 1
Xylene (Total)ND mg/kg 07/31/19 15:52 1330-20-707/31/19 12:070.0096 0.0034 1
m&p-Xylene ND mg/kg 07/31/19 15:52 179601-23-107/31/19 12:070.0096 0.0034 1
o-Xylene ND mg/kg 07/31/19 15:52 95-47-607/31/19 12:070.0048 0.0018 1
Surrogates
Toluene-d8 (S)101 %07/31/19 15:52 2037-26-507/31/19 12:0770-130 1
4-Bromofluorobenzene (S)101 %07/31/19 15:52 460-00-407/31/19 12:0770-130 1
1,2-Dichloroethane-d4 (S)84 %07/31/19 15:52 17060-07-007/31/19 12:0770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.9 %07/29/19 16:170.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 76.0 %08/03/19 16:0508/03/19 15:541
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.451J mg/kg 08/05/19 15:51 18540-29-9 J08/05/19 11:321.32 0.336 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-7 (0-2)Lab ID:92438947007 Collected:07/27/19 14:35 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050BMetals (ICPMS) 6020B
Arsenic 3.93 mg/kg 08/02/19 14:57 7440-38-208/01/19 20:160.648 0.162 5
Barium 75.3 mg/kg 08/02/19 14:57 7440-39-308/01/19 20:161.30 0.207 5
Cadmium ND mg/kg 08/02/19 14:57 7440-43-908/01/19 20:160.648 0.104 5
Chromium 35.7 mg/kg 08/02/19 14:57 7440-47-308/01/19 20:161.30 0.350 5
Lead 22.0 mg/kg 08/02/19 14:57 7439-92-108/01/19 20:160.648 0.156 5
Selenium 0.843 mg/kg 08/02/19 14:57 7782-49-208/01/19 20:160.648 0.246 5
Silver ND mg/kg 08/02/19 14:57 7440-22-408/01/19 20:160.648 0.201 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 5.88 mg/kg 08/04/19 16:13 7439-97-608/02/19 10:190.778 0.0726 20
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/02/19 13:21 83-32-907/31/19 10:430.42 0.11 1
Acenaphthylene ND mg/kg 08/02/19 13:21 208-96-807/31/19 10:430.42 0.099 1
Aniline ND mg/kg 08/02/19 13:21 62-53-307/31/19 10:430.42 0.094 1
Anthracene ND mg/kg 08/02/19 13:21 120-12-707/31/19 10:430.42 0.11 1
Benzo(a)anthracene ND mg/kg 08/02/19 13:21 56-55-307/31/19 10:430.42 0.13 1
Benzo(a)pyrene ND mg/kg 08/02/19 13:21 50-32-807/31/19 10:430.42 0.18 1
Benzo(b)fluoranthene ND mg/kg 08/02/19 13:21 205-99-207/31/19 10:430.42 0.17 1
Benzo(g,h,i)perylene ND mg/kg 08/02/19 13:21 191-24-207/31/19 10:430.42 0.16 1
Benzo(k)fluoranthene ND mg/kg 08/02/19 13:21 207-08-907/31/19 10:430.42 0.18 1
Benzoic Acid ND mg/kg 08/02/19 13:21 65-85-007/31/19 10:432.1 0.45 1
Benzyl alcohol ND mg/kg 08/02/19 13:21 100-51-607/31/19 10:430.83 0.22 1
4-Bromophenylphenyl ether ND mg/kg 08/02/19 13:21 101-55-307/31/19 10:430.42 0.11 1
Butylbenzylphthalate ND mg/kg 08/02/19 13:21 85-68-707/31/19 10:430.42 0.11 1
4-Chloro-3-methylphenol ND mg/kg 08/02/19 13:21 59-50-707/31/19 10:430.83 0.25 1
4-Chloroaniline ND mg/kg 08/02/19 13:21 106-47-807/31/19 10:432.1 0.26 1
bis(2-Chloroethoxy)methane ND mg/kg 08/02/19 13:21 111-91-107/31/19 10:430.42 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 08/02/19 13:21 111-44-4 v107/31/19 10:430.42 0.089 1
2-Chloronaphthalene ND mg/kg 08/02/19 13:21 91-58-707/31/19 10:430.42 0.093 1
2-Chlorophenol ND mg/kg 08/02/19 13:21 95-57-807/31/19 10:430.42 0.097 1
4-Chlorophenylphenyl ether ND mg/kg 08/02/19 13:21 7005-72-307/31/19 10:430.42 0.11 1
Chrysene ND mg/kg 08/02/19 13:21 218-01-907/31/19 10:430.42 0.12 1
Dibenz(a,h)anthracene ND mg/kg 08/02/19 13:21 53-70-307/31/19 10:430.42 0.17 1
Dibenzofuran ND mg/kg 08/02/19 13:21 132-64-907/31/19 10:430.42 0.10 1
1,2-Dichlorobenzene ND mg/kg 08/02/19 13:21 95-50-107/31/19 10:430.42 0.090 1
1,3-Dichlorobenzene ND mg/kg 08/02/19 13:21 541-73-107/31/19 10:430.42 0.094 1
1,4-Dichlorobenzene ND mg/kg 08/02/19 13:21 106-46-707/31/19 10:430.42 0.092 1
3,3'-Dichlorobenzidine ND mg/kg 08/02/19 13:21 91-94-107/31/19 10:432.1 0.29 1
2,4-Dichlorophenol ND mg/kg 08/02/19 13:21 120-83-207/31/19 10:430.42 0.14 1
Diethylphthalate ND mg/kg 08/02/19 13:21 84-66-207/31/19 10:430.42 0.090 1
2,4-Dimethylphenol ND mg/kg 08/02/19 13:21 105-67-907/31/19 10:430.42 0.10 1
Dimethylphthalate ND mg/kg 08/02/19 13:21 131-11-307/31/19 10:430.42 0.094 1
Di-n-butylphthalate ND mg/kg 08/02/19 13:21 84-74-207/31/19 10:430.42 0.10 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/02/19 13:21 534-52-1 v107/31/19 10:430.83 0.67 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-7 (0-2)Lab ID:92438947007 Collected:07/27/19 14:35 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 08/02/19 13:21 51-28-507/31/19 10:432.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 08/02/19 13:21 121-14-207/31/19 10:430.42 0.11 1
2,6-Dinitrotoluene ND mg/kg 08/02/19 13:21 606-20-207/31/19 10:430.42 0.11 1
Di-n-octylphthalate ND mg/kg 08/02/19 13:21 117-84-007/31/19 10:430.42 0.24 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/02/19 13:21 117-81-707/31/19 10:430.42 0.14 1
Fluoranthene ND mg/kg 08/02/19 13:21 206-44-007/31/19 10:430.42 0.13 1
Fluorene ND mg/kg 08/02/19 13:21 86-73-707/31/19 10:430.42 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 08/02/19 13:21 87-68-307/31/19 10:430.42 0.10 1
Hexachlorobenzene ND mg/kg 08/02/19 13:21 118-74-107/31/19 10:430.42 0.11 1
Hexachlorocyclopentadiene ND mg/kg 08/02/19 13:21 77-47-4 v107/31/19 10:430.42 0.17 1
Hexachloroethane ND mg/kg 08/02/19 13:21 67-72-107/31/19 10:430.42 0.095 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/02/19 13:21 193-39-507/31/19 10:430.42 0.19 1
Isophorone ND mg/kg 08/02/19 13:21 78-59-107/31/19 10:430.42 0.091 1
1-Methylnaphthalene ND mg/kg 08/02/19 13:21 90-12-007/31/19 10:430.42 0.11 1
2-Methylnaphthalene ND mg/kg 08/02/19 13:21 91-57-607/31/19 10:430.42 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 08/02/19 13:21 95-48-707/31/19 10:430.42 0.092 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/02/19 13:21 15831-10-4 v107/31/19 10:430.42 0.10 1
Naphthalene ND mg/kg 08/02/19 13:21 91-20-307/31/19 10:430.42 0.10 1
2-Nitroaniline ND mg/kg 08/02/19 13:21 88-74-4 v107/31/19 10:432.1 0.21 1
3-Nitroaniline ND mg/kg 08/02/19 13:21 99-09-207/31/19 10:432.1 0.22 1
4-Nitroaniline ND mg/kg 08/02/19 13:21 100-01-607/31/19 10:430.83 0.21 1
Nitrobenzene ND mg/kg 08/02/19 13:21 98-95-307/31/19 10:430.42 0.10 1
2-Nitrophenol ND mg/kg 08/02/19 13:21 88-75-507/31/19 10:430.42 0.13 1
4-Nitrophenol ND mg/kg 08/02/19 13:21 100-02-707/31/19 10:432.1 0.66 1
N-Nitrosodimethylamine ND mg/kg 08/02/19 13:21 62-75-9 v107/31/19 10:430.42 0.12 1
N-Nitroso-di-n-propylamine ND mg/kg 08/02/19 13:21 621-64-707/31/19 10:430.42 0.12 1
N-Nitrosodiphenylamine ND mg/kg 08/02/19 13:21 86-30-607/31/19 10:430.42 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/02/19 13:21 108-60-1 v107/31/19 10:430.42 0.12 1
Pentachlorophenol ND mg/kg 08/02/19 13:21 87-86-507/31/19 10:432.1 0.19 1
Phenanthrene ND mg/kg 08/02/19 13:21 85-01-807/31/19 10:430.42 0.10 1
Phenol ND mg/kg 08/02/19 13:21 108-95-207/31/19 10:430.42 0.10 1
Pyrene ND mg/kg 08/02/19 13:21 129-00-007/31/19 10:430.42 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 08/02/19 13:21 120-82-107/31/19 10:430.42 0.095 1
2,4,5-Trichlorophenol ND mg/kg 08/02/19 13:21 95-95-407/31/19 10:430.42 0.11 1
2,4,6-Trichlorophenol ND mg/kg 08/02/19 13:21 88-06-207/31/19 10:430.42 0.10 1
Surrogates
Nitrobenzene-d5 (S)64 %08/02/19 13:21 4165-60-007/31/19 10:4323-110 1
2-Fluorobiphenyl (S)53 %08/02/19 13:21 321-60-807/31/19 10:4330-110 1
Terphenyl-d14 (S)73 %08/02/19 13:21 1718-51-007/31/19 10:4328-110 1
Phenol-d6 (S)67 %08/02/19 13:21 13127-88-307/31/19 10:4322-110 1
2-Fluorophenol (S)68 %08/02/19 13:21 367-12-407/31/19 10:4313-110 1
2,4,6-Tribromophenol (S)77 %08/02/19 13:21 118-79-607/31/19 10:4327-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 07/30/19 22:48 67-64-107/30/19 13:100.092 0.0092 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
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Page 32 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-7 (0-2)Lab ID:92438947007 Collected:07/27/19 14:35 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Benzene ND mg/kg 07/30/19 22:48 71-43-207/30/19 13:100.0046 0.0015 1
Bromobenzene ND mg/kg 07/30/19 22:48 108-86-107/30/19 13:100.0046 0.0018 1
Bromochloromethane ND mg/kg 07/30/19 22:48 74-97-507/30/19 13:100.0046 0.0016 1
Bromodichloromethane ND mg/kg 07/30/19 22:48 75-27-407/30/19 13:100.0046 0.0017 1
Bromoform ND mg/kg 07/30/19 22:48 75-25-207/30/19 13:100.0046 0.0021 1
Bromomethane ND mg/kg 07/30/19 22:48 74-83-907/30/19 13:100.0092 0.0023 1
2-Butanone (MEK)ND mg/kg 07/30/19 22:48 78-93-307/30/19 13:100.092 0.0027 1
n-Butylbenzene ND mg/kg 07/30/19 22:48 104-51-807/30/19 13:100.0046 0.0017 1
sec-Butylbenzene ND mg/kg 07/30/19 22:48 135-98-807/30/19 13:100.0046 0.0015 1
tert-Butylbenzene ND mg/kg 07/30/19 22:48 98-06-607/30/19 13:100.0046 0.0018 1
Carbon tetrachloride ND mg/kg 07/30/19 22:48 56-23-507/30/19 13:100.0046 0.0024 1
Chlorobenzene ND mg/kg 07/30/19 22:48 108-90-707/30/19 13:100.0046 0.0017 1
Chloroethane ND mg/kg 07/30/19 22:48 75-00-307/30/19 13:100.0092 0.0022 1
Chloroform ND mg/kg 07/30/19 22:48 67-66-307/30/19 13:100.0046 0.0015 1
Chloromethane ND mg/kg 07/30/19 22:48 74-87-307/30/19 13:100.0092 0.0022 1
2-Chlorotoluene ND mg/kg 07/30/19 22:48 95-49-807/30/19 13:100.0046 0.0016 1
4-Chlorotoluene ND mg/kg 07/30/19 22:48 106-43-407/30/19 13:100.0046 0.0017 1
1,2-Dibromo-3-chloropropane ND mg/kg 07/30/19 22:48 96-12-807/30/19 13:100.0046 0.0033 1
Dibromochloromethane ND mg/kg 07/30/19 22:48 124-48-107/30/19 13:100.0046 0.0017 1
1,2-Dibromoethane (EDB)ND mg/kg 07/30/19 22:48 106-93-407/30/19 13:100.0046 0.0017 1
Dibromomethane ND mg/kg 07/30/19 22:48 74-95-307/30/19 13:100.0046 0.0023 1
1,2-Dichlorobenzene ND mg/kg 07/30/19 22:48 95-50-107/30/19 13:100.0046 0.0017 1
1,3-Dichlorobenzene ND mg/kg 07/30/19 22:48 541-73-107/30/19 13:100.0046 0.0018 1
1,4-Dichlorobenzene ND mg/kg 07/30/19 22:48 106-46-707/30/19 13:100.0046 0.0016 1
Dichlorodifluoromethane ND mg/kg 07/30/19 22:48 75-71-807/30/19 13:100.0092 0.0033 1
1,1-Dichloroethane ND mg/kg 07/30/19 22:48 75-34-307/30/19 13:100.0046 0.0014 1
1,2-Dichloroethane ND mg/kg 07/30/19 22:48 107-06-207/30/19 13:100.0046 0.0020 1
1,1-Dichloroethene ND mg/kg 07/30/19 22:48 75-35-407/30/19 13:100.0046 0.0017 1
cis-1,2-Dichloroethene ND mg/kg 07/30/19 22:48 156-59-207/30/19 13:100.0046 0.0013 1
trans-1,2-Dichloroethene ND mg/kg 07/30/19 22:48 156-60-507/30/19 13:100.0046 0.0017 1
1,2-Dichloropropane ND mg/kg 07/30/19 22:48 78-87-507/30/19 13:100.0046 0.0016 1
1,3-Dichloropropane ND mg/kg 07/30/19 22:48 142-28-907/30/19 13:100.0046 0.0017 1
2,2-Dichloropropane ND mg/kg 07/30/19 22:48 594-20-707/30/19 13:100.0046 0.0016 1
1,1-Dichloropropene ND mg/kg 07/30/19 22:48 563-58-607/30/19 13:100.0046 0.0014 1
cis-1,3-Dichloropropene ND mg/kg 07/30/19 22:48 10061-01-507/30/19 13:100.0046 0.0017 1
trans-1,3-Dichloropropene ND mg/kg 07/30/19 22:48 10061-02-607/30/19 13:100.0046 0.0014 1
Diisopropyl ether ND mg/kg 07/30/19 22:48 108-20-307/30/19 13:100.0046 0.0016 1
Ethylbenzene ND mg/kg 07/30/19 22:48 100-41-407/30/19 13:100.0046 0.0017 1
Hexachloro-1,3-butadiene ND mg/kg 07/30/19 22:48 87-68-307/30/19 13:100.0046 0.0018 1
2-Hexanone ND mg/kg 07/30/19 22:48 591-78-607/30/19 13:100.046 0.0036 1
Isopropylbenzene (Cumene)ND mg/kg 07/30/19 22:48 98-82-807/30/19 13:100.0046 0.0017 1
p-Isopropyltoluene ND mg/kg 07/30/19 22:48 99-87-607/30/19 13:100.0046 0.0016 1
Methylene Chloride ND mg/kg 07/30/19 22:48 75-09-207/30/19 13:100.018 0.0028 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 07/30/19 22:48 108-10-107/30/19 13:100.046 0.0034 1
Methyl-tert-butyl ether ND mg/kg 07/30/19 22:48 1634-04-407/30/19 13:100.0046 0.0014 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-7 (0-2)Lab ID:92438947007 Collected:07/27/19 14:35 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND mg/kg 07/30/19 22:48 91-20-307/30/19 13:100.0046 0.0011 1
n-Propylbenzene ND mg/kg 07/30/19 22:48 103-65-107/30/19 13:100.0046 0.0016 1
Styrene ND mg/kg 07/30/19 22:48 100-42-507/30/19 13:100.0046 0.0017 1
1,1,1,2-Tetrachloroethane ND mg/kg 07/30/19 22:48 630-20-607/30/19 13:100.0046 0.0019 1
1,1,2,2-Tetrachloroethane ND mg/kg 07/30/19 22:48 79-34-507/30/19 13:100.0046 0.0017 1
Tetrachloroethene ND mg/kg 07/30/19 22:48 127-18-407/30/19 13:100.0046 0.0016 1
Toluene ND mg/kg 07/30/19 22:48 108-88-307/30/19 13:100.0046 0.0017 1
1,2,3-Trichlorobenzene ND mg/kg 07/30/19 22:48 87-61-607/30/19 13:100.0046 0.0020 1
1,2,4-Trichlorobenzene ND mg/kg 07/30/19 22:48 120-82-107/30/19 13:100.0046 0.0015 1
1,1,1-Trichloroethane ND mg/kg 07/30/19 22:48 71-55-607/30/19 13:100.0046 0.0017 1
1,1,2-Trichloroethane ND mg/kg 07/30/19 22:48 79-00-507/30/19 13:100.0046 0.0019 1
Trichloroethene ND mg/kg 07/30/19 22:48 79-01-607/30/19 13:100.0046 0.0019 1
Trichlorofluoromethane ND mg/kg 07/30/19 22:48 75-69-407/30/19 13:100.0046 0.0020 1
1,2,3-Trichloropropane ND mg/kg 07/30/19 22:48 96-18-407/30/19 13:100.0046 0.0015 1
1,2,4-Trimethylbenzene ND mg/kg 07/30/19 22:48 95-63-607/30/19 13:100.0046 0.0018 1
1,3,5-Trimethylbenzene ND mg/kg 07/30/19 22:48 108-67-807/30/19 13:100.0046 0.0017 1
Vinyl acetate ND mg/kg 07/30/19 22:48 108-05-407/30/19 13:100.046 0.0081 1
Vinyl chloride ND mg/kg 07/30/19 22:48 75-01-407/30/19 13:100.0092 0.0017 1
Xylene (Total)ND mg/kg 07/30/19 22:48 1330-20-707/30/19 13:100.0092 0.0033 1
m&p-Xylene ND mg/kg 07/30/19 22:48 179601-23-107/30/19 13:100.0092 0.0033 1
o-Xylene ND mg/kg 07/30/19 22:48 95-47-607/30/19 13:100.0046 0.0017 1
Surrogates
Toluene-d8 (S)113 %07/30/19 22:48 2037-26-5 1g07/30/19 13:1070-130 1
4-Bromofluorobenzene (S)106 %07/30/19 22:48 460-00-407/30/19 13:1070-130 1
1,2-Dichloroethane-d4 (S)100 %07/30/19 22:48 17060-07-007/30/19 13:1070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.1 %07/29/19 16:180.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 77.1 %08/03/19 16:0508/03/19 15:541
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 0.339J mg/kg 08/05/19 15:56 18540-29-9 J08/05/19 11:321.30 0.331 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
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Page 34 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-8 (7-10)Lab ID:92438947008 Collected:07/27/19 12:10 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/31/19 17:2107/31/19 12:027.0 3.2 1
Surrogates
n-Pentacosane (S)60 %07/31/19 17:21 629-99-207/31/19 12:0233-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 07/30/19 21:0207/30/19 13:1821.1 9.4 1
Surrogates
n-Pentacosane (S)59 %07/30/19 21:02 629-99-207/30/19 13:1833-129 1
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 11/04/19 14:06 12674-11-211/02/19 12:0746.5 12.5 1
PCB-1221 (Aroclor 1221)ND ug/kg 11/04/19 14:06 11104-28-211/02/19 12:0746.5 16.5 1
PCB-1232 (Aroclor 1232)ND ug/kg 11/04/19 14:06 11141-16-511/02/19 12:0746.5 11.7 1
PCB-1242 (Aroclor 1242)ND ug/kg 11/04/19 14:06 53469-21-911/02/19 12:0746.5 3.1 1
PCB-1248 (Aroclor 1248)ND ug/kg 11/04/19 14:06 12672-29-611/02/19 12:0746.5 8.2 1
PCB-1254 (Aroclor 1254)ND ug/kg 11/04/19 14:06 11097-69-111/02/19 12:0746.5 8.7 1
PCB-1260 (Aroclor 1260)ND ug/kg 11/04/19 14:06 11096-82-511/02/19 12:0746.5 10.7 1
Surrogates
Decachlorobiphenyl (S)100 %11/04/19 14:06 2051-24-311/02/19 12:0710-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 27.8 %07/29/19 16:180.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SB-9 (7-10)Lab ID:92438947009 Collected:07/27/19 11:45 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/30/19 19:4807/30/19 13:186.8 3.1 1
Surrogates
n-Pentacosane (S)68 %07/30/19 19:48 629-99-207/30/19 13:1833-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 07/30/19 19:4807/30/19 13:1820.1 9.0 1
Surrogates
n-Pentacosane (S)59 %07/30/19 19:48 629-99-207/30/19 13:1833-129 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 27.0 %07/29/19 16:180.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 99
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92438947
LEH-005
Sample:SP-10 (7-10)Lab ID:92438947010 Collected:07/27/19 11:20 Received:07/29/19 06:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/30/19 20:1307/30/19 13:187.7 3.5 1
Surrogates
n-Pentacosane (S)65 %07/30/19 20:13 629-99-207/30/19 13:1833-129 1
Analytical Method: EPA 8015C Modified Preparation Method: EPA 35468015 GCS THC-ORO
Oil Range Organics (C28-C40)ND mg/kg 07/30/19 20:1307/30/19 13:1822.0 9.8 1
Surrogates
n-Pentacosane (S)58 %07/30/19 20:13 629-99-207/30/19 13:1833-129 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 33.9 %07/29/19 16:180.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489013
EPA 5030B
EPA 8015C Modified
Gasoline Range Organics
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2639450
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg ND 6.0 07/29/19 13:031.1
4-Bromofluorobenzene (S)%86 63-130 07/29/19 13:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2639451LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 46.650 93 70-130
4-Bromofluorobenzene (S)%85 63-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2639452MATRIX SPIKE SAMPLE:
MSSpike
Result
92438729001
Gas Range Organics (C6-C10)mg/kg 21.821.1 102 40-155ND
4-Bromofluorobenzene (S)%93 63-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438729001
2639453SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%8887
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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[phone]
Page 38 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
490884
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2647690
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
Aliphatic (C05-C08)mg/kg ND 2.5 N208/07/19 14:212.5
Aliphatic (C09-C12)mg/kg ND 2.5 N208/07/19 14:212.5
Aromatic (C09-C10)mg/kg ND 2.5 N208/07/19 14:212.5
4-Bromofluorobenzene (FID) (S)%88 70-130 08/07/19 14:21
4-Bromofluorobenzene (PID) (S)%91 70-130 08/07/19 14:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2647691LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2647692
Aliphatic (C05-C08)mg/kg 14.6 N2159770-1309714.6 0 25
Aliphatic (C09-C12)mg/kg 15.3 N21510230-13010215.3 0 25
Aromatic (C09-C10)mg/kg 4.9 N259970-130984.9 0 25
4-Bromofluorobenzene (FID) (S)%93 70-13094
4-Bromofluorobenzene (PID) (S)%95 70-13097
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1321597
3050B
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples:92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3436906-2
Associated Lab Samples:92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 0.500 08/02/19 13:350.125
Barium mg/kg ND 1.00 08/02/19 13:350.160
Cadmium mg/kg ND 0.500 08/02/19 13:350.0800
Chromium mg/kg 0.382J 1.00 J08/02/19 13:350.270
Lead mg/kg ND 0.500 08/02/19 13:350.120
Selenium mg/kg ND 0.500 08/02/19 13:350.190
Silver mg/kg ND 0.500 08/02/19 13:350.155
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3436906-3LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3436906-4
Arsenic mg/kg 96.7100 96.7 80.0-12099.199.1 2.51 20
Barium mg/kg 88.7100 88.7 80.0-12094.794.7 6.61 20
Cadmium mg/kg 103100 103 80.0-120104104 1.02 20
Chromium mg/kg 101100 101 80.0-120105105 3.93 20
Lead mg/kg 93.7100 93.7 80.0-12099.299.2 5.70 20
Selenium mg/kg 102100 102 80.0-120105105 3.27 20
Silver mg/kg 20.220.0 101 80.0-12010521.0 3.58 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3436906-7MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92438947002
R3436906-8
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 25.8 91.8 75.0-12589.2 2.83 2025.81.88 120 117
Barium mg/kg 25.8 95.2 75.0-12582.8 11.2 2025.827.8 150 135
Cadmium mg/kg 25.8 106 75.0-125104 2.64 2025.80.584 138 134
Chromium mg/kg 25.8 98.5 75.0-12587.5 9.20 2025.833.5 160 146
Lead mg/kg 25.8 94.8 75.0-12594.2 0.518 2025.821.5 144 143
Selenium mg/kg 25.8 104 75.0-125102 2.36 2025.81.17 135 132
Silver mg/kg 5.15 103 75.0-125101 2.50 205.150.421 27.1 26.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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Huntersville, NC 28078
[phone]
Page 40 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1324994
3051
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3438479-1
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 0.500 08/08/19 08:260.125
Barium mg/kg ND 1.00 08/08/19 08:260.160
Cadmium mg/kg ND 0.500 08/08/19 08:260.0800
Chromium mg/kg ND 1.00 08/08/19 08:260.270
Lead mg/kg ND 0.500 08/08/19 08:260.120
Selenium mg/kg ND 0.500 08/08/19 08:260.190
Silver mg/kg ND 0.500 08/08/19 08:260.155
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3438479-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3438479-3
Arsenic mg/kg 96.4100 96.4 80.0-12094.994.9 1.55 20
Barium mg/kg 96.6100 96.6 80.0-12094.494.4 2.31 20
Cadmium mg/kg 102100 102 80.0-120102102 0.470 20
Chromium mg/kg 99.9100 99.9 80.0-12099.299.2 0.775 20
Lead mg/kg 96.5100 96.5 80.0-12096.196.1 0.429 20
Selenium mg/kg 99.7100 99.7 80.0-12096.796.7 3.07 20
Silver mg/kg 20.120.0 100 80.0-12097.819.6 2.71 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3438479-6MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92438947001
R3438479-7
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 26.8 84.0 75.0-12590.8 7.63 2026.82.45 115 124
Barium mg/kg MH,R126.8 112 75.0-125231 37.7 2026.8193 344 504
Cadmium mg/kg 26.8 104 75.0-125107 3.05 2026.80.280 140 144
Chromium mg/kg 26.8 100 75.0-125111 7.74 2026.843.5 178 193
Lead mg/kg 26.8 95.8 75.0-125103 6.72 2026.812.3 141 151
Selenium mg/kg 26.8 92.2 75.0-125100 8.42 2026.81.31 125 136
Silver mg/kg 5.37 101 75.0-125108 6.63 205.37ND 27.0 28.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1321702
7471A
EPA 7471B
Mercury 7471B
Associated Lab Samples:92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3437240-5
Associated Lab Samples:92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0300 08/04/19 16:060.00280
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3437240-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3437240-2
Mercury mg/kg 0.5160.500 103 80.0-1201050.524 1.54 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3437240-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1123664-01
R3437240-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.500 90.4 75.0-12597.7 6.27 200.5000.114 0.566 0.602
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1324990
7471A
EPA 7471B
Mercury 7471B
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3438575-1
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0300 08/08/19 11:580.00280
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3438575-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3438575-3
Mercury mg/kg 0.5200.500 104 80.0-1201030.517 0.643 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3438575-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1126081-03
R3438575-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.500 100 75.0-12592.7 7.59 200.500ND 0.509 0.471
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489263
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92438947002, 92438947004, 92438947007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2640402
Associated Lab Samples:92438947002, 92438947004, 92438947007
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 07/30/19 14:300.0021
1,1,1-Trichloroethane mg/kg ND 0.0050 07/30/19 14:300.0018
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 07/30/19 14:300.0019
1,1,2-Trichloroethane mg/kg ND 0.0050 07/30/19 14:300.0021
1,1-Dichloroethane mg/kg ND 0.0050 07/30/19 14:300.0015
1,1-Dichloroethene mg/kg ND 0.0050 07/30/19 14:300.0018
1,1-Dichloropropene mg/kg ND 0.0050 07/30/19 14:300.0015
1,2,3-Trichlorobenzene mg/kg ND 0.0050 07/30/19 14:300.0022
1,2,3-Trichloropropane mg/kg ND 0.0050 07/30/19 14:300.0016
1,2,4-Trichlorobenzene mg/kg ND 0.0050 07/30/19 14:300.0016
1,2,4-Trimethylbenzene mg/kg ND 0.0050 07/30/19 14:300.0020
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 07/30/19 14:300.0036
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 07/30/19 14:300.0018
1,2-Dichlorobenzene mg/kg ND 0.0050 07/30/19 14:300.0019
1,2-Dichloroethane mg/kg ND 0.0050 07/30/19 14:300.0022
1,2-Dichloropropane mg/kg ND 0.0050 07/30/19 14:300.0017
1,3,5-Trimethylbenzene mg/kg ND 0.0050 07/30/19 14:300.0018
1,3-Dichlorobenzene mg/kg ND 0.0050 07/30/19 14:300.0020
1,3-Dichloropropane mg/kg ND 0.0050 07/30/19 14:300.0019
1,4-Dichlorobenzene mg/kg ND 0.0050 07/30/19 14:300.0017
2,2-Dichloropropane mg/kg ND 0.0050 07/30/19 14:300.0017
2-Butanone (MEK)mg/kg ND 0.10 07/30/19 14:300.0029
2-Chlorotoluene mg/kg ND 0.0050 07/30/19 14:300.0017
2-Hexanone mg/kg ND 0.050 07/30/19 14:300.0039
4-Chlorotoluene mg/kg ND 0.0050 07/30/19 14:300.0018
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 07/30/19 14:300.0037
Acetone mg/kg ND 0.10 07/30/19 14:300.010
Benzene mg/kg ND 0.0050 07/30/19 14:300.0016
Bromobenzene mg/kg ND 0.0050 07/30/19 14:300.0020
Bromochloromethane mg/kg ND 0.0050 07/30/19 14:300.0017
Bromodichloromethane mg/kg ND 0.0050 07/30/19 14:300.0019
Bromoform mg/kg ND 0.0050 07/30/19 14:300.0023
Bromomethane mg/kg ND 0.010 07/30/19 14:300.0025
Carbon tetrachloride mg/kg ND 0.0050 07/30/19 14:300.0026
Chlorobenzene mg/kg ND 0.0050 07/30/19 14:300.0019
Chloroethane mg/kg ND 0.010 07/30/19 14:300.0024
Chloroform mg/kg ND 0.0050 07/30/19 14:300.0016
Chloromethane mg/kg ND 0.010 07/30/19 14:300.0024
cis-1,2-Dichloroethene mg/kg ND 0.0050 07/30/19 14:300.0014
cis-1,3-Dichloropropene mg/kg ND 0.0050 07/30/19 14:300.0018
Dibromochloromethane mg/kg ND 0.0050 07/30/19 14:300.0018
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2640402
Associated Lab Samples:92438947002, 92438947004, 92438947007
Matrix:Solid
AnalyzedMDL
Dibromomethane mg/kg ND 0.0050 07/30/19 14:300.0025
Dichlorodifluoromethane mg/kg ND 0.010 07/30/19 14:300.0036
Diisopropyl ether mg/kg ND 0.0050 07/30/19 14:300.0017
Ethylbenzene mg/kg ND 0.0050 07/30/19 14:300.0018
Hexachloro-1,3-butadiene mg/kg ND 0.0050 07/30/19 14:300.0020
Isopropylbenzene (Cumene)mg/kg ND 0.0050 07/30/19 14:300.0019
m&p-Xylene mg/kg ND 0.010 07/30/19 14:300.0036
Methyl-tert-butyl ether mg/kg ND 0.0050 07/30/19 14:300.0015
Methylene Chloride mg/kg ND 0.020 07/30/19 14:300.0030
n-Butylbenzene mg/kg ND 0.0050 07/30/19 14:300.0018
n-Propylbenzene mg/kg ND 0.0050 07/30/19 14:300.0017
Naphthalene mg/kg ND 0.0050 07/30/19 14:300.0012
o-Xylene mg/kg ND 0.0050 07/30/19 14:300.0019
p-Isopropyltoluene mg/kg ND 0.0050 07/30/19 14:300.0017
sec-Butylbenzene mg/kg ND 0.0050 07/30/19 14:300.0016
Styrene mg/kg ND 0.0050 07/30/19 14:300.0018
tert-Butylbenzene mg/kg ND 0.0050 07/30/19 14:300.0020
Tetrachloroethene mg/kg ND 0.0050 07/30/19 14:300.0017
Toluene mg/kg ND 0.0050 07/30/19 14:300.0018
trans-1,2-Dichloroethene mg/kg ND 0.0050 07/30/19 14:300.0019
trans-1,3-Dichloropropene mg/kg ND 0.0050 07/30/19 14:300.0015
Trichloroethene mg/kg ND 0.0050 07/30/19 14:300.0021
Trichlorofluoromethane mg/kg ND 0.0050 07/30/19 14:300.0022
Vinyl acetate mg/kg ND 0.050 07/30/19 14:300.0088
Vinyl chloride mg/kg ND 0.010 07/30/19 14:300.0018
Xylene (Total)mg/kg ND 0.010 07/30/19 14:300.0036
1,2-Dichloroethane-d4 (S)%82 70-132 07/30/19 14:30
4-Bromofluorobenzene (S)%101 70-130 07/30/19 14:30
Toluene-d8 (S)%102 70-130 07/30/19 14:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2640403LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.0480.05 95 70-130
1,1,1-Trichloroethane mg/kg 0.0450.05 89 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.0450.05 91 55-130
1,1,2-Trichloroethane mg/kg 0.0490.05 99 70-130
1,1-Dichloroethane mg/kg 0.0430.05 86 68-130
1,1-Dichloroethene mg/kg 0.0420.05 84 70-130
1,1-Dichloropropene mg/kg 0.0430.05 85 70-130
1,2,3-Trichlorobenzene mg/kg 0.0460.05 93 70-130
1,2,3-Trichloropropane mg/kg 0.0460.05 92 70-130
1,2,4-Trichlorobenzene mg/kg 0.0440.05 88 70-130
1,2,4-Trimethylbenzene mg/kg 0.0450.05 90 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2640403LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane mg/kg 0.0520.05 103 57-141
1,2-Dibromoethane (EDB)mg/kg 0.0500.05 100 70-130
1,2-Dichlorobenzene mg/kg 0.0450.05 89 70-130
1,2-Dichloroethane mg/kg 0.0440.05 88 70-130
1,2-Dichloropropane mg/kg 0.0470.05 95 70-130
1,3,5-Trimethylbenzene mg/kg 0.0450.05 90 70-130
1,3-Dichlorobenzene mg/kg 0.0450.05 89 70-130
1,3-Dichloropropane mg/kg 0.0520.05 104 70-130
1,4-Dichlorobenzene mg/kg 0.0430.05 85 70-130
2,2-Dichloropropane mg/kg 0.0450.05 90 70-130
2-Butanone (MEK)mg/kg 0.096J0.1 96 60-130
2-Chlorotoluene mg/kg 0.0490.05 97 70-130
2-Hexanone mg/kg 0.100.1 104 70-132
4-Chlorotoluene mg/kg 0.0440.05 88 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.0980.1 98 69-130
Acetone mg/kg 0.090J0.1 90 49-148
Benzene mg/kg 0.0480.05 96 70-130
Bromobenzene mg/kg 0.0460.05 93 70-130
Bromochloromethane mg/kg 0.0430.05 85 70-130
Bromodichloromethane mg/kg 0.0490.05 99 70-130
Bromoform mg/kg 0.0480.05 97 68-136
Bromomethane mg/kg 0.0430.05 86 60-140
Carbon tetrachloride mg/kg 0.0460.05 92 70-130
Chlorobenzene mg/kg 0.0450.05 89 70-130
Chloroethane mg/kg 0.0490.05 99 51-147
Chloroform mg/kg 0.0420.05 84 70-130
Chloromethane mg/kg 0.0450.05 89 48-130
cis-1,2-Dichloroethene mg/kg 0.0430.05 86 70-130
cis-1,3-Dichloropropene mg/kg 0.0530.05 106 70-130
Dibromochloromethane mg/kg 0.0500.05 100 70-130
Dibromomethane mg/kg 0.0470.05 93 70-130
Dichlorodifluoromethane mg/kg 0.0470.05 94 49-130
Diisopropyl ether mg/kg 0.0440.05 88 66-130
Ethylbenzene mg/kg 0.0450.05 90 70-130
Hexachloro-1,3-butadiene mg/kg 0.0430.05 87 70-130
Isopropylbenzene (Cumene)mg/kg 0.0450.05 90 70-130
m&p-Xylene mg/kg 0.0890.1 89 70-130
Methyl-tert-butyl ether mg/kg 0.0460.05 93 70-130
Methylene Chloride mg/kg 0.0420.05 83 50-137
n-Butylbenzene mg/kg 0.0440.05 89 70-130
n-Propylbenzene mg/kg 0.0430.05 86 70-130
Naphthalene mg/kg 0.0490.05 97 70-131
o-Xylene mg/kg 0.0450.05 89 70-130
p-Isopropyltoluene mg/kg 0.0450.05 89 70-130
sec-Butylbenzene mg/kg 0.0460.05 92 70-130
Styrene mg/kg 0.0450.05 89 70-130
tert-Butylbenzene mg/kg 0.0400.05 81 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2640403LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene mg/kg 0.0450.05 89 56-130
Toluene mg/kg 0.0430.05 86 70-130
trans-1,2-Dichloroethene mg/kg 0.0430.05 86 70-130
trans-1,3-Dichloropropene mg/kg 0.0510.05 101 70-130
Trichloroethene mg/kg 0.0500.05 99 70-141
Trichlorofluoromethane mg/kg 0.0430.05 85 67-130
Vinyl acetate mg/kg 0.0990.1 99 10-136
Vinyl chloride mg/kg 0.0460.05 92 67-130
Xylene (Total)mg/kg 0.130.15 89 70-130
1,2-Dichloroethane-d4 (S)%95 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2641312MATRIX SPIKE SAMPLE:
MSSpike
Result
92438995003
1,1,1,2-Tetrachloroethane mg/kg 20.422.5 90 52-133ND
1,1,1-Trichloroethane mg/kg 19.722.5 88 49-137ND
1,1,2,2-Tetrachloroethane mg/kg 21.322.5 95 39-150ND
1,1,2-Trichloroethane mg/kg 21.022.5 93 48-140ND
1,1-Dichloroethane mg/kg 19.622.5 87 46-135ND
1,1-Dichloroethene mg/kg 20.022.5 89 38-149ND
1,1-Dichloropropene mg/kg 18.522.5 82 41-140ND
1,2,3-Trichlorobenzene mg/kg 20.222.5 90 10-158ND
1,2,3-Trichloropropane mg/kg 22.522.5 100 33-157ND
1,2,4-Trichlorobenzene mg/kg 19.222.5 85 10-155ND
1,2,4-Trimethylbenzene mg/kg 20.422.5 91 24-154ND
1,2-Dibromo-3-chloropropane mg/kg 23.322.5 104 33-158ND
1,2-Dibromoethane (EDB)mg/kg 21.122.5 94 40-136ND
1,2-Dichlorobenzene mg/kg 21.422.5 95 27-146ND
1,2-Dichloroethane mg/kg 19.622.5 87 49-140ND
1,2-Dichloropropane mg/kg 20.722.5 92 44-143ND
1,3,5-Trimethylbenzene mg/kg 19.522.5 86 40-144ND
1,3-Dichlorobenzene mg/kg 19.722.5 88 33-140ND
1,3-Dichloropropane mg/kg 21.422.5 95 47-147ND
1,4-Dichlorobenzene mg/kg 19.622.5 87 35-139ND
2,2-Dichloropropane mg/kg 18.322.5 81 41-140ND
2-Butanone (MEK)mg/kg 43.2J45.1 96 10-181ND
2-Chlorotoluene mg/kg 19.622.5 87 38-147ND
2-Hexanone mg/kg 49.8J45.1 110 18-169ND
4-Chlorotoluene mg/kg 19.722.5 87 36-145ND
4-Methyl-2-pentanone (MIBK)mg/kg 48.0J45.1 107 16-175ND
Acetone mg/kg 38.1J45.1 85 10-200ND
Benzene mg/kg 21.022.5 93 46-136ND
Bromobenzene mg/kg 20.822.5 92 38-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2641312MATRIX SPIKE SAMPLE:
MSSpike
Result
92438995003
Bromochloromethane mg/kg 20.222.5 90 44-142ND
Bromodichloromethane mg/kg 20.722.5 92 41-140ND
Bromoform mg/kg 19.622.5 87 34-145ND
Bromomethane mg/kg 18.822.5 83 14-162ND
Carbon tetrachloride mg/kg 20.022.5 89 44-141ND
Chlorobenzene mg/kg 20.022.5 89 39-141ND
Chloroethane mg/kg 22.022.5 97 10-182ND
Chloroform mg/kg 19.422.5 86 45-140ND
Chloromethane mg/kg 20.022.5 89 19-149ND
cis-1,2-Dichloroethene mg/kg 19.122.5 85 38-150ND
cis-1,3-Dichloropropene mg/kg 21.422.5 95 30-144ND
Dibromochloromethane mg/kg 19.822.5 88 36-145ND
Dibromomethane mg/kg 21.522.5 95 41-145ND
Dichlorodifluoromethane mg/kg 20.722.5 92 16-146ND
Diisopropyl ether mg/kg 19.322.5 86 41-143ND
Ethylbenzene mg/kg 19.822.5 88 35-144ND
Hexachloro-1,3-butadiene mg/kg 18.822.5 83 10-160ND
Isopropylbenzene (Cumene)mg/kg 19.822.5 88 30-152ND
m&p-Xylene mg/kg 39.345.1 87 33-145ND
Methyl-tert-butyl ether mg/kg 20.022.5 89 49-140ND
Methylene Chloride mg/kg 9.5J v322.5 42 10-174116J ug/kg
n-Butylbenzene mg/kg 19.222.5 85 10-160ND
n-Propylbenzene mg/kg 19.722.5 87 24-159ND
Naphthalene mg/kg 31.622.5 101 10-1718800 ug/kg
o-Xylene mg/kg 19.722.5 88 31-150ND
p-Isopropyltoluene mg/kg 19.822.5 88 21-154ND
sec-Butylbenzene mg/kg 20.022.5 89 19-159ND
Styrene mg/kg 19.522.5 86 15-152ND
tert-Butylbenzene mg/kg 17.922.5 80 31-141ND
Tetrachloroethene mg/kg 17.822.5 79 19-141ND
Toluene mg/kg 20.222.5 90 31-146ND
trans-1,2-Dichloroethene mg/kg 19.322.5 86 28-157ND
trans-1,3-Dichloropropene mg/kg 20.322.5 90 25-146ND
Trichloroethene mg/kg 19.922.5 88 34-149ND
Trichlorofluoromethane mg/kg 19.222.5 85 10-167ND
Vinyl acetate mg/kg 42.4J45.1 94 10-200ND
Vinyl chloride mg/kg 20.222.5 90 36-155ND
Xylene (Total)mg/kg 59.067.6 87 29-148ND
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438729001
2641311SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg 0.024J 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND 30ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg 0.0022J 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438729001
2641311SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND v230ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%8682
4-Bromofluorobenzene (S)%102100
Toluene-d8 (S)%102101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489511
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92438947005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2641477
Associated Lab Samples:92438947005
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 07/31/19 12:100.0021
1,1,1-Trichloroethane mg/kg ND 0.0050 07/31/19 12:100.0018
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 07/31/19 12:100.0019
1,1,2-Trichloroethane mg/kg ND 0.0050 07/31/19 12:100.0021
1,1-Dichloroethane mg/kg ND 0.0050 07/31/19 12:100.0015
1,1-Dichloroethene mg/kg ND 0.0050 07/31/19 12:100.0018
1,1-Dichloropropene mg/kg ND 0.0050 07/31/19 12:100.0015
1,2,3-Trichlorobenzene mg/kg ND 0.0050 07/31/19 12:100.0022
1,2,3-Trichloropropane mg/kg ND 0.0050 07/31/19 12:100.0016
1,2,4-Trichlorobenzene mg/kg ND 0.0050 07/31/19 12:100.0016
1,2,4-Trimethylbenzene mg/kg ND 0.0050 07/31/19 12:100.0020
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 07/31/19 12:100.0036
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 07/31/19 12:100.0018
1,2-Dichlorobenzene mg/kg 0.0021J 0.0050 07/31/19 12:100.0019
1,2-Dichloroethane mg/kg ND 0.0050 07/31/19 12:100.0022
1,2-Dichloropropane mg/kg ND 0.0050 07/31/19 12:100.0017
1,3,5-Trimethylbenzene mg/kg ND 0.0050 07/31/19 12:100.0018
1,3-Dichlorobenzene mg/kg ND 0.0050 07/31/19 12:100.0020
1,3-Dichloropropane mg/kg ND 0.0050 07/31/19 12:100.0019
1,4-Dichlorobenzene mg/kg ND 0.0050 07/31/19 12:100.0017
2,2-Dichloropropane mg/kg ND 0.0050 07/31/19 12:100.0017
2-Butanone (MEK)mg/kg ND 0.10 07/31/19 12:100.0029
2-Chlorotoluene mg/kg ND 0.0050 07/31/19 12:100.0017
2-Hexanone mg/kg ND 0.050 07/31/19 12:100.0039
4-Chlorotoluene mg/kg ND 0.0050 07/31/19 12:100.0018
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 07/31/19 12:100.0037
Acetone mg/kg ND 0.10 07/31/19 12:100.010
Benzene mg/kg ND 0.0050 07/31/19 12:100.0016
Bromobenzene mg/kg ND 0.0050 07/31/19 12:100.0020
Bromochloromethane mg/kg ND 0.0050 07/31/19 12:100.0017
Bromodichloromethane mg/kg ND 0.0050 07/31/19 12:100.0019
Bromoform mg/kg ND 0.0050 07/31/19 12:100.0023
Bromomethane mg/kg ND 0.010 07/31/19 12:100.0025
Carbon tetrachloride mg/kg ND 0.0050 07/31/19 12:100.0026
Chlorobenzene mg/kg ND 0.0050 07/31/19 12:100.0019
Chloroethane mg/kg ND 0.010 07/31/19 12:100.0024
Chloroform mg/kg ND 0.0050 07/31/19 12:100.0016
Chloromethane mg/kg ND 0.010 07/31/19 12:100.0024
cis-1,2-Dichloroethene mg/kg ND 0.0050 07/31/19 12:100.0014
cis-1,3-Dichloropropene mg/kg ND 0.0050 07/31/19 12:100.0018
Dibromochloromethane mg/kg ND 0.0050 07/31/19 12:100.0018
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2641477
Associated Lab Samples:92438947005
Matrix:Solid
AnalyzedMDL
Dibromomethane mg/kg ND 0.0050 07/31/19 12:100.0025
Dichlorodifluoromethane mg/kg ND 0.010 07/31/19 12:100.0036
Diisopropyl ether mg/kg ND 0.0050 07/31/19 12:100.0017
Ethylbenzene mg/kg ND 0.0050 07/31/19 12:100.0018
Hexachloro-1,3-butadiene mg/kg ND 0.0050 07/31/19 12:100.0020
Isopropylbenzene (Cumene)mg/kg ND 0.0050 07/31/19 12:100.0019
m&p-Xylene mg/kg ND 0.010 07/31/19 12:100.0036
Methyl-tert-butyl ether mg/kg ND 0.0050 07/31/19 12:100.0015
Methylene Chloride mg/kg 0.0072J 0.020 07/31/19 12:100.0030
n-Butylbenzene mg/kg ND 0.0050 07/31/19 12:100.0018
n-Propylbenzene mg/kg ND 0.0050 07/31/19 12:100.0017
Naphthalene mg/kg ND 0.0050 07/31/19 12:100.0012
o-Xylene mg/kg ND 0.0050 07/31/19 12:100.0019
p-Isopropyltoluene mg/kg ND 0.0050 07/31/19 12:100.0017
sec-Butylbenzene mg/kg ND 0.0050 07/31/19 12:100.0016
Styrene mg/kg ND 0.0050 07/31/19 12:100.0018
tert-Butylbenzene mg/kg ND 0.0050 07/31/19 12:100.0020
Tetrachloroethene mg/kg ND 0.0050 07/31/19 12:100.0017
Toluene mg/kg ND 0.0050 07/31/19 12:100.0018
trans-1,2-Dichloroethene mg/kg ND 0.0050 07/31/19 12:100.0019
trans-1,3-Dichloropropene mg/kg ND 0.0050 07/31/19 12:100.0015
Trichloroethene mg/kg ND 0.0050 07/31/19 12:100.0021
Trichlorofluoromethane mg/kg ND 0.0050 07/31/19 12:100.0022
Vinyl acetate mg/kg ND 0.050 v107/31/19 12:100.0088
Vinyl chloride mg/kg ND 0.010 07/31/19 12:100.0018
Xylene (Total)mg/kg ND 0.010 07/31/19 12:100.0036
1,2-Dichloroethane-d4 (S)%101 70-132 07/31/19 12:10
4-Bromofluorobenzene (S)%108 70-130 07/31/19 12:10
Toluene-d8 (S)%102 70-130 07/31/19 12:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641478LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2641479
1,1,1,2-Tetrachloroethane mg/kg 0.0520.05 104 70-1301000.050 3 30
1,1,1-Trichloroethane mg/kg 0.0470.05 95 70-130950.048 0 30
1,1,2,2-Tetrachloroethane mg/kg 0.0520.05 104 55-1301030.052 1 30
1,1,2-Trichloroethane mg/kg 0.0490.05 98 70-1301000.050 2 30
1,1-Dichloroethane mg/kg 0.0480.05 96 68-130970.049 1 30
1,1-Dichloroethene mg/kg 0.0490.05 99 70-1301000.050 1 30
1,1-Dichloropropene mg/kg 0.0470.05 93 70-130930.046 1 30
1,2,3-Trichlorobenzene mg/kg 0.0490.05 97 70-130970.048 1 30
1,2,3-Trichloropropane mg/kg 0.0540.05 107 70-1301040.052 3 30
1,2,4-Trichlorobenzene mg/kg 0.0500.05 99 70-130960.048 4 30
1,2,4-Trimethylbenzene mg/kg 0.0480.05 96 69-130970.048 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641478LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2641479
1,2-Dibromo-3-chloropropane mg/kg 0.0490.05 98 57-141910.046 7 30
1,2-Dibromoethane (EDB)mg/kg 0.0500.05 100 70-130980.049 2 30
1,2-Dichlorobenzene mg/kg 0.0520.05 104 70-1301000.050 4 30
1,2-Dichloroethane mg/kg 0.0470.05 94 70-130940.047 0 30
1,2-Dichloropropane mg/kg 0.0490.05 99 70-130990.050 1 30
1,3,5-Trimethylbenzene mg/kg 0.0480.05 96 70-130960.048 0 30
1,3-Dichlorobenzene mg/kg 0.0470.05 93 70-130940.047 1 30
1,3-Dichloropropane mg/kg 0.0520.05 104 70-1301020.051 2 30
1,4-Dichlorobenzene mg/kg 0.0490.05 98 70-130950.048 2 30
2,2-Dichloropropane mg/kg 0.0490.05 98 70-130970.048 2 30
2-Butanone (MEK)mg/kg 0.090J0.1 90 60-130910.091J 30
2-Chlorotoluene mg/kg 0.0470.05 94 70-130920.046 3 30
2-Hexanone mg/kg 0.100.1 103 70-132990.099 3 30
4-Chlorotoluene mg/kg 0.0460.05 93 70-130960.048 3 30
4-Methyl-2-pentanone (MIBK)mg/kg 0.0980.1 98 69-130960.096 2 30
Acetone mg/kg 0.093J0.1 93 49-148890.089J 30
Benzene mg/kg 0.0500.05 100 70-130990.049 2 30
Bromobenzene mg/kg 0.0490.05 98 70-130960.048 2 30
Bromochloromethane mg/kg 0.0450.05 90 70-130870.044 3 30
Bromodichloromethane mg/kg 0.0500.05 100 70-1301000.050 0 30
Bromoform mg/kg 0.0540.05 109 68-1361060.053 3 30
Bromomethane mg/kg 0.0580.05 117 60-1401150.058 2 30
Carbon tetrachloride mg/kg 0.0470.05 94 70-130950.047 1 30
Chlorobenzene mg/kg 0.0480.05 96 70-130950.047 1 30
Chloroethane mg/kg 0.0530.05 107 51-1471100.055 3 30
Chloroform mg/kg 0.0470.05 95 70-130930.047 2 30
Chloromethane mg/kg 0.0500.05 101 48-1301010.050 0 30
cis-1,2-Dichloroethene mg/kg 0.0480.05 96 70-130960.048 1 30
cis-1,3-Dichloropropene mg/kg 0.0530.05 107 70-1301060.053 1 30
Dibromochloromethane mg/kg 0.0500.05 100 70-130980.049 2 30
Dibromomethane mg/kg 0.0490.05 97 70-130970.048 0 30
Dichlorodifluoromethane mg/kg 0.0500.05 100 49-130980.049 1 30
Diisopropyl ether mg/kg 0.0480.05 97 66-130960.048 0 30
Ethylbenzene mg/kg 0.0490.05 98 70-130950.047 3 30
Hexachloro-1,3-butadiene mg/kg 0.0470.05 94 70-130920.046 3 30
Isopropylbenzene (Cumene)mg/kg 0.0500.05 101 70-130980.049 2 30
m&p-Xylene mg/kg 0.0980.1 98 70-130960.096 3 30
Methyl-tert-butyl ether mg/kg 0.0520.05 104 70-1301030.051 1 30
Methylene Chloride mg/kg 0.0470.05 95 50-137950.047 0 30
n-Butylbenzene mg/kg 0.0450.05 91 70-130940.047 3 30
n-Propylbenzene mg/kg 0.0470.05 94 70-130930.046 1 30
Naphthalene mg/kg 0.0430.05 86 70-131850.042 2 30
o-Xylene mg/kg 0.0490.05 99 70-130970.048 2 30
p-Isopropyltoluene mg/kg 0.0480.05 96 70-130960.048 0 30
sec-Butylbenzene mg/kg 0.0500.05 99 70-130980.049 1 30
Styrene mg/kg 0.0490.05 99 70-130960.048 3 30
tert-Butylbenzene mg/kg 0.0430.05 87 69-130860.043 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641478LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2641479
Tetrachloroethene mg/kg 0.0480.05 97 56-130940.047 3 30
Toluene mg/kg 0.0470.05 94 70-130950.047 0 30
trans-1,2-Dichloroethene mg/kg 0.0480.05 96 70-130970.049 1 30
trans-1,3-Dichloropropene mg/kg 0.0510.05 102 70-1301020.051 0 30
Trichloroethene mg/kg 0.0490.05 98 70-141990.049 1 30
Trichlorofluoromethane mg/kg 0.0500.05 99 67-130970.049 2 30
Vinyl acetate mg/kg 0.13 v10.1 132 10-1361220.12 8 30
Vinyl chloride mg/kg 0.0530.05 106 67-1301050.052 1 30
Xylene (Total)mg/kg 0.150.15 98 70-130960.14 2 30
1,2-Dichloroethane-d4 (S)%90 70-13290
4-Bromofluorobenzene (S)%104 70-130105
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489527
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92438947003, 92438947006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2641536
Associated Lab Samples:92438947003, 92438947006
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 07/31/19 13:450.0021
1,1,1-Trichloroethane mg/kg ND 0.0050 07/31/19 13:450.0018
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 07/31/19 13:450.0019
1,1,2-Trichloroethane mg/kg ND 0.0050 07/31/19 13:450.0021
1,1-Dichloroethane mg/kg ND 0.0050 07/31/19 13:450.0015
1,1-Dichloroethene mg/kg ND 0.0050 07/31/19 13:450.0018
1,1-Dichloropropene mg/kg ND 0.0050 07/31/19 13:450.0015
1,2,3-Trichlorobenzene mg/kg ND 0.0050 07/31/19 13:450.0022
1,2,3-Trichloropropane mg/kg ND 0.0050 07/31/19 13:450.0016
1,2,4-Trichlorobenzene mg/kg ND 0.0050 07/31/19 13:450.0016
1,2,4-Trimethylbenzene mg/kg ND 0.0050 07/31/19 13:450.0020
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 07/31/19 13:450.0036
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 07/31/19 13:450.0018
1,2-Dichlorobenzene mg/kg ND 0.0050 07/31/19 13:450.0019
1,2-Dichloroethane mg/kg ND 0.0050 07/31/19 13:450.0022
1,2-Dichloropropane mg/kg ND 0.0050 07/31/19 13:450.0017
1,3,5-Trimethylbenzene mg/kg ND 0.0050 07/31/19 13:450.0018
1,3-Dichlorobenzene mg/kg ND 0.0050 07/31/19 13:450.0020
1,3-Dichloropropane mg/kg ND 0.0050 07/31/19 13:450.0019
1,4-Dichlorobenzene mg/kg ND 0.0050 07/31/19 13:450.0017
2,2-Dichloropropane mg/kg ND 0.0050 07/31/19 13:450.0017
2-Butanone (MEK)mg/kg ND 0.10 07/31/19 13:450.0029
2-Chlorotoluene mg/kg ND 0.0050 07/31/19 13:450.0017
2-Hexanone mg/kg ND 0.050 07/31/19 13:450.0039
4-Chlorotoluene mg/kg ND 0.0050 07/31/19 13:450.0018
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 07/31/19 13:450.0037
Acetone mg/kg ND 0.10 07/31/19 13:450.010
Benzene mg/kg ND 0.0050 07/31/19 13:450.0016
Bromobenzene mg/kg ND 0.0050 07/31/19 13:450.0020
Bromochloromethane mg/kg ND 0.0050 07/31/19 13:450.0017
Bromodichloromethane mg/kg ND 0.0050 07/31/19 13:450.0019
Bromoform mg/kg ND 0.0050 07/31/19 13:450.0023
Bromomethane mg/kg ND 0.010 07/31/19 13:450.0025
Carbon tetrachloride mg/kg ND 0.0050 07/31/19 13:450.0026
Chlorobenzene mg/kg ND 0.0050 07/31/19 13:450.0019
Chloroethane mg/kg ND 0.010 07/31/19 13:450.0024
Chloroform mg/kg ND 0.0050 07/31/19 13:450.0016
Chloromethane mg/kg ND 0.010 07/31/19 13:450.0024
cis-1,2-Dichloroethene mg/kg ND 0.0050 07/31/19 13:450.0014
cis-1,3-Dichloropropene mg/kg ND 0.0050 07/31/19 13:450.0018
Dibromochloromethane mg/kg ND 0.0050 07/31/19 13:450.0018
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2641536
Associated Lab Samples:92438947003, 92438947006
Matrix:Solid
AnalyzedMDL
Dibromomethane mg/kg ND 0.0050 07/31/19 13:450.0025
Dichlorodifluoromethane mg/kg ND 0.010 07/31/19 13:450.0036
Diisopropyl ether mg/kg ND 0.0050 07/31/19 13:450.0017
Ethylbenzene mg/kg ND 0.0050 07/31/19 13:450.0018
Hexachloro-1,3-butadiene mg/kg ND 0.0050 07/31/19 13:450.0020
Isopropylbenzene (Cumene)mg/kg ND 0.0050 07/31/19 13:450.0019
m&p-Xylene mg/kg ND 0.010 07/31/19 13:450.0036
Methyl-tert-butyl ether mg/kg ND 0.0050 07/31/19 13:450.0015
Methylene Chloride mg/kg ND 0.020 v207/31/19 13:450.0030
n-Butylbenzene mg/kg ND 0.0050 07/31/19 13:450.0018
n-Propylbenzene mg/kg ND 0.0050 07/31/19 13:450.0017
Naphthalene mg/kg ND 0.0050 07/31/19 13:450.0012
o-Xylene mg/kg ND 0.0050 07/31/19 13:450.0019
p-Isopropyltoluene mg/kg ND 0.0050 07/31/19 13:450.0017
sec-Butylbenzene mg/kg ND 0.0050 07/31/19 13:450.0016
Styrene mg/kg ND 0.0050 07/31/19 13:450.0018
tert-Butylbenzene mg/kg ND 0.0050 07/31/19 13:450.0020
Tetrachloroethene mg/kg ND 0.0050 07/31/19 13:450.0017
Toluene mg/kg ND 0.0050 07/31/19 13:450.0018
trans-1,2-Dichloroethene mg/kg ND 0.0050 07/31/19 13:450.0019
trans-1,3-Dichloropropene mg/kg ND 0.0050 07/31/19 13:450.0015
Trichloroethene mg/kg ND 0.0050 07/31/19 13:450.0021
Trichlorofluoromethane mg/kg ND 0.0050 07/31/19 13:450.0022
Vinyl acetate mg/kg ND 0.050 07/31/19 13:450.0088
Vinyl chloride mg/kg ND 0.010 07/31/19 13:450.0018
Xylene (Total)mg/kg ND 0.010 07/31/19 13:450.0036
1,2-Dichloroethane-d4 (S)%80 70-132 07/31/19 13:45
4-Bromofluorobenzene (S)%103 70-130 07/31/19 13:45
Toluene-d8 (S)%102 70-130 07/31/19 13:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641537LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.0500.05 101 70-130
1,1,1-Trichloroethane mg/kg 0.0480.05 96 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.0490.05 98 55-130
1,1,2-Trichloroethane mg/kg 0.0490.05 98 70-130
1,1-Dichloroethane mg/kg 0.0450.05 90 68-130
1,1-Dichloroethene mg/kg 0.0440.05 89 70-130
1,1-Dichloropropene mg/kg 0.0440.05 87 70-130
1,2,3-Trichlorobenzene mg/kg 0.0500.05 100 70-130
1,2,3-Trichloropropane mg/kg 0.0530.05 105 70-130
1,2,4-Trichlorobenzene mg/kg 0.0470.05 94 70-130
1,2,4-Trimethylbenzene mg/kg 0.0460.05 93 69-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641537LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane mg/kg 0.0550.05 109 57-141
1,2-Dibromoethane (EDB)mg/kg 0.0520.05 103 70-130
1,2-Dichlorobenzene mg/kg 0.0460.05 92 70-130
1,2-Dichloroethane mg/kg 0.0460.05 92 70-130
1,2-Dichloropropane mg/kg 0.0490.05 98 70-130
1,3,5-Trimethylbenzene mg/kg 0.0460.05 93 70-130
1,3-Dichlorobenzene mg/kg 0.0460.05 91 70-130
1,3-Dichloropropane mg/kg 0.0540.05 108 70-130
1,4-Dichlorobenzene mg/kg 0.0450.05 91 70-130
2,2-Dichloropropane mg/kg 0.0470.05 94 70-130
2-Butanone (MEK)mg/kg 0.110.1 106 60-130
2-Chlorotoluene mg/kg 0.0460.05 92 70-130
2-Hexanone mg/kg 0.120.1 116 70-132
4-Chlorotoluene mg/kg 0.0460.05 91 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.100.1 104 69-130
Acetone mg/kg 0.089J0.1 89 49-148
Benzene mg/kg 0.0490.05 99 70-130
Bromobenzene mg/kg 0.0490.05 98 70-130
Bromochloromethane mg/kg 0.0430.05 86 70-130
Bromodichloromethane mg/kg 0.0490.05 98 70-130
Bromoform mg/kg 0.0490.05 99 68-136
Bromomethane mg/kg 0.0450.05 90 60-140
Carbon tetrachloride mg/kg 0.0460.05 93 70-130
Chlorobenzene mg/kg 0.0470.05 94 70-130
Chloroethane mg/kg 0.0510.05 103 51-147
Chloroform mg/kg 0.0430.05 86 70-130
Chloromethane mg/kg 0.0460.05 93 48-130
cis-1,2-Dichloroethene mg/kg 0.0440.05 87 70-130
cis-1,3-Dichloropropene mg/kg 0.0540.05 107 70-130
Dibromochloromethane mg/kg 0.0510.05 102 70-130
Dibromomethane mg/kg 0.0480.05 96 70-130
Dichlorodifluoromethane mg/kg 0.0480.05 95 49-130
Diisopropyl ether mg/kg 0.0510.05 101 66-130
Ethylbenzene mg/kg 0.0470.05 94 70-130
Hexachloro-1,3-butadiene mg/kg 0.0460.05 93 70-130
Isopropylbenzene (Cumene)mg/kg 0.0470.05 95 70-130
m&p-Xylene mg/kg 0.0930.1 93 70-130
Methyl-tert-butyl ether mg/kg 0.0460.05 91 70-130
Methylene Chloride mg/kg 0.041 v30.05 82 50-137
n-Butylbenzene mg/kg 0.0460.05 93 70-130
n-Propylbenzene mg/kg 0.0470.05 94 70-130
Naphthalene mg/kg 0.0520.05 105 70-131
o-Xylene mg/kg 0.0480.05 96 70-130
p-Isopropyltoluene mg/kg 0.0470.05 95 70-130
sec-Butylbenzene mg/kg 0.0480.05 95 70-130
Styrene mg/kg 0.0470.05 93 70-130
tert-Butylbenzene mg/kg 0.0430.05 85 69-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641537LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene mg/kg 0.0470.05 95 56-130
Toluene mg/kg 0.0440.05 88 70-130
trans-1,2-Dichloroethene mg/kg 0.0450.05 89 70-130
trans-1,3-Dichloropropene mg/kg 0.0520.05 103 70-130
Trichloroethene mg/kg 0.0500.05 100 70-141
Trichlorofluoromethane mg/kg 0.0430.05 87 67-130
Vinyl acetate mg/kg 0.120.1 116 10-136
Vinyl chloride mg/kg 0.0480.05 97 67-130
Xylene (Total)mg/kg 0.140.15 94 70-130
1,2-Dichloroethane-d4 (S)%97 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2642019MATRIX SPIKE SAMPLE:
MSSpike
Result
92439114007
1,1,1,2-Tetrachloroethane mg/kg 0.0180.023 77 52-133ND
1,1,1-Trichloroethane mg/kg 0.0170.023 73 49-137ND
1,1,2,2-Tetrachloroethane mg/kg 0.0190.023 83 39-150ND
1,1,2-Trichloroethane mg/kg 0.0170.023 74 48-140ND
1,1-Dichloroethane mg/kg 0.0180.023 77 46-135ND
1,1-Dichloroethene mg/kg 0.0190.023 81 38-149ND
1,1-Dichloropropene mg/kg 0.0170.023 74 41-140ND
1,2,3-Trichlorobenzene mg/kg 0.0180.023 77 10-158ND
1,2,3-Trichloropropane mg/kg 0.0220.023 94 33-157ND
1,2,4-Trichlorobenzene mg/kg 0.0170.023 72 10-155ND
1,2,4-Trimethylbenzene mg/kg 0.0180.023 78 24-154ND
1,2-Dibromo-3-chloropropane mg/kg 0.0180.023 77 33-158ND
1,2-Dibromoethane (EDB)mg/kg 0.0180.023 79 40-136ND
1,2-Dichlorobenzene mg/kg 0.0180.023 79 27-146ND
1,2-Dichloroethane mg/kg 0.0170.023 72 49-140ND
1,2-Dichloropropane mg/kg 0.0180.023 77 44-143ND
1,3,5-Trimethylbenzene mg/kg 0.0180.023 79 40-144ND
1,3-Dichlorobenzene mg/kg 0.0170.023 75 33-140ND
1,3-Dichloropropane mg/kg 0.0190.023 82 47-147ND
1,4-Dichlorobenzene mg/kg 0.0180.023 78 35-139ND
2,2-Dichloropropane mg/kg 0.0170.023 72 41-140ND
2-Butanone (MEK)mg/kg 0.033J0.046 71 10-181ND
2-Chlorotoluene mg/kg 0.0180.023 80 38-147ND
2-Hexanone mg/kg 0.040J0.046 87 18-169ND
4-Chlorotoluene mg/kg 0.0180.023 79 36-145ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.039J0.046 84 16-175ND
Acetone mg/kg 0.047J0.046 32 10-200ND
Benzene mg/kg 0.0190.023 84 46-136ND
Bromobenzene mg/kg 0.0190.023 82 38-149ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2642019MATRIX SPIKE SAMPLE:
MSSpike
Result
92439114007
Bromochloromethane mg/kg 0.0170.023 74 44-142ND
Bromodichloromethane mg/kg 0.0190.023 83 41-140ND
Bromoform mg/kg 0.0170.023 75 34-145ND
Bromomethane mg/kg 0.0180.023 76 14-162ND
Carbon tetrachloride mg/kg 0.0190.023 84 44-141ND
Chlorobenzene mg/kg 0.0180.023 80 39-141ND
Chloroethane mg/kg 0.0220.023 96 10-182ND
Chloroform mg/kg 0.0170.023 73 45-140ND
Chloromethane mg/kg 0.0190.023 81 19-149ND
cis-1,2-Dichloroethene mg/kg 0.0170.023 73 38-150ND
cis-1,3-Dichloropropene mg/kg 0.0180.023 79 30-144ND
Dibromochloromethane mg/kg 0.0180.023 79 36-145ND
Dibromomethane mg/kg 0.0180.023 80 41-145ND
Dichlorodifluoromethane mg/kg 0.0210.023 90 16-146ND
Diisopropyl ether mg/kg 0.0170.023 72 41-143ND
Ethylbenzene mg/kg 0.0200.023 86 35-144ND
Hexachloro-1,3-butadiene mg/kg 0.0140.023 63 10-160ND
Isopropylbenzene (Cumene)mg/kg 0.0190.023 83 30-152ND
m&p-Xylene mg/kg 0.0390.046 84 33-145ND
Methyl-tert-butyl ether mg/kg 0.0160.023 69 49-140ND
Methylene Chloride mg/kg 0.0041J v30.023 18 10-174ND
n-Butylbenzene mg/kg 0.0170.023 75 10-160ND
n-Propylbenzene mg/kg 0.0190.023 82 24-159ND
Naphthalene mg/kg 0.0180.023 78 10-171ND
o-Xylene mg/kg 0.0190.023 82 31-150ND
p-Isopropyltoluene mg/kg 0.0180.023 77 21-154ND
sec-Butylbenzene mg/kg 0.0180.023 80 19-159ND
Styrene mg/kg 0.0190.023 81 15-152ND
tert-Butylbenzene mg/kg 0.0160.023 70 31-141ND
Tetrachloroethene mg/kg 0.0170.023 74 19-141ND
Toluene mg/kg 0.0190.023 82 31-146ND
trans-1,2-Dichloroethene mg/kg 0.0180.023 77 28-157ND
trans-1,3-Dichloropropene mg/kg 0.0180.023 80 25-146ND
Trichloroethene mg/kg 0.0190.023 81 34-149ND
Trichlorofluoromethane mg/kg 0.0180.023 80 10-167ND
Vinyl acetate mg/kg 0.036J0.046 79 10-200ND
Vinyl chloride mg/kg 0.0190.023 85 36-155ND
Xylene (Total)mg/kg 0.0570.069 83 29-148ND
1,2-Dichloroethane-d4 (S)%93 70-132
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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Page 59 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92439114005
2642018SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg 0.022J 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND 30ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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Huntersville, NC 28078
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Page 60 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92439114005
2642018SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND v230ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%8687
4-Bromofluorobenzene (S)%102102
Toluene-d8 (S)%10499
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 61 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
490929
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2647881
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/07/19 11:290.0021
1,1,1-Trichloroethane mg/kg ND 0.0050 08/07/19 11:290.0018
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/07/19 11:290.0019
1,1,2-Trichloroethane mg/kg ND 0.0050 08/07/19 11:290.0021
1,1-Dichloroethane mg/kg ND 0.0050 08/07/19 11:290.0015
1,1-Dichloroethene mg/kg ND 0.0050 08/07/19 11:290.0018
1,1-Dichloropropene mg/kg ND 0.0050 08/07/19 11:290.0015
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/07/19 11:290.0022
1,2,3-Trichloropropane mg/kg ND 0.0050 08/07/19 11:290.0016
1,2,4-Trichlorobenzene mg/kg ND 0.0050 08/07/19 11:290.0016
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/07/19 11:290.0020
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 08/07/19 11:290.0036
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/07/19 11:290.0018
1,2-Dichlorobenzene mg/kg ND 0.0050 08/07/19 11:290.0019
1,2-Dichloroethane mg/kg ND 0.0050 08/07/19 11:290.0022
1,2-Dichloropropane mg/kg ND 0.0050 08/07/19 11:290.0017
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/07/19 11:290.0018
1,3-Dichlorobenzene mg/kg ND 0.0050 08/07/19 11:290.0020
1,3-Dichloropropane mg/kg ND 0.0050 08/07/19 11:290.0019
1,4-Dichlorobenzene mg/kg ND 0.0050 08/07/19 11:290.0017
2,2-Dichloropropane mg/kg ND 0.0050 08/07/19 11:290.0017
2-Butanone (MEK)mg/kg ND 0.10 08/07/19 11:290.0029
2-Chlorotoluene mg/kg ND 0.0050 08/07/19 11:290.0017
2-Hexanone mg/kg ND 0.050 08/07/19 11:290.0039
4-Chlorotoluene mg/kg ND 0.0050 08/07/19 11:290.0018
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/07/19 11:290.0037
Acetone mg/kg ND 0.10 08/07/19 11:290.010
Benzene mg/kg ND 0.0050 08/07/19 11:290.0016
Bromobenzene mg/kg ND 0.0050 08/07/19 11:290.0020
Bromochloromethane mg/kg ND 0.0050 08/07/19 11:290.0017
Bromodichloromethane mg/kg ND 0.0050 08/07/19 11:290.0019
Bromoform mg/kg ND 0.0050 08/07/19 11:290.0023
Bromomethane mg/kg ND 0.010 08/07/19 11:290.0025
Carbon tetrachloride mg/kg ND 0.0050 08/07/19 11:290.0026
Chlorobenzene mg/kg ND 0.0050 08/07/19 11:290.0019
Chloroethane mg/kg ND 0.010 08/07/19 11:290.0024
Chloroform mg/kg ND 0.0050 08/07/19 11:290.0016
Chloromethane mg/kg ND 0.010 08/07/19 11:290.0024
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/07/19 11:290.0014
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/07/19 11:290.0018
Dibromochloromethane mg/kg ND 0.0050 08/07/19 11:290.0018
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 62 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2647881
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
Dibromomethane mg/kg ND 0.0050 08/07/19 11:290.0025
Dichlorodifluoromethane mg/kg ND 0.010 08/07/19 11:290.0036
Diisopropyl ether mg/kg ND 0.0050 08/07/19 11:290.0017
Ethylbenzene mg/kg ND 0.0050 08/07/19 11:290.0018
Hexachloro-1,3-butadiene mg/kg ND 0.0050 08/07/19 11:290.0020
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/07/19 11:290.0019
m&p-Xylene mg/kg ND 0.010 08/07/19 11:290.0036
Methyl-tert-butyl ether mg/kg ND 0.0050 08/07/19 11:290.0015
Methylene Chloride mg/kg ND 0.020 08/07/19 11:290.0030
n-Butylbenzene mg/kg ND 0.0050 08/07/19 11:290.0018
n-Propylbenzene mg/kg ND 0.0050 08/07/19 11:290.0017
Naphthalene mg/kg ND 0.0050 08/07/19 11:290.0012
o-Xylene mg/kg ND 0.0050 08/07/19 11:290.0019
p-Isopropyltoluene mg/kg ND 0.0050 08/07/19 11:290.0017
sec-Butylbenzene mg/kg ND 0.0050 08/07/19 11:290.0016
Styrene mg/kg ND 0.0050 08/07/19 11:290.0018
tert-Butylbenzene mg/kg ND 0.0050 08/07/19 11:290.0020
Tetrachloroethene mg/kg ND 0.0050 08/07/19 11:290.0017
Toluene mg/kg ND 0.0050 08/07/19 11:290.0018
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/07/19 11:290.0019
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/07/19 11:290.0015
Trichloroethene mg/kg ND 0.0050 08/07/19 11:290.0021
Trichlorofluoromethane mg/kg ND 0.0050 08/07/19 11:290.0022
Vinyl acetate mg/kg ND 0.050 08/07/19 11:290.0088
Vinyl chloride mg/kg ND 0.010 08/07/19 11:290.0018
Xylene (Total)mg/kg ND 0.010 08/07/19 11:290.0036
1,2-Dichloroethane-d4 (S)%84 70-132 08/07/19 11:29
4-Bromofluorobenzene (S)%101 70-130 08/07/19 11:29
Toluene-d8 (S)%112 70-130 08/07/19 11:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2647882LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.0500.05 100 70-130
1,1,1-Trichloroethane mg/kg 0.0490.05 98 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.0440.05 89 55-130
1,1,2-Trichloroethane mg/kg 0.0500.05 99 70-130
1,1-Dichloroethane mg/kg 0.0480.05 96 68-130
1,1-Dichloroethene mg/kg 0.0490.05 97 70-130
1,1-Dichloropropene mg/kg 0.0500.05 100 70-130
1,2,3-Trichlorobenzene mg/kg 0.0470.05 94 70-130
1,2,3-Trichloropropane mg/kg 0.0470.05 93 70-130
1,2,4-Trichlorobenzene mg/kg 0.0480.05 96 70-130
1,2,4-Trimethylbenzene mg/kg 0.0470.05 95 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2647882LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane mg/kg 0.0480.05 95 57-141
1,2-Dibromoethane (EDB)mg/kg 0.0480.05 96 70-130
1,2-Dichlorobenzene mg/kg 0.0460.05 93 70-130
1,2-Dichloroethane mg/kg 0.0460.05 91 70-130
1,2-Dichloropropane mg/kg 0.0510.05 103 70-130
1,3,5-Trimethylbenzene mg/kg 0.0470.05 94 70-130
1,3-Dichlorobenzene mg/kg 0.0470.05 95 70-130
1,3-Dichloropropane mg/kg 0.0500.05 100 70-130
1,4-Dichlorobenzene mg/kg 0.0470.05 93 70-130
2,2-Dichloropropane mg/kg 0.0490.05 98 70-130
2-Butanone (MEK)mg/kg 0.092J0.1 92 60-130
2-Chlorotoluene mg/kg 0.0460.05 92 70-130
2-Hexanone mg/kg 0.100.1 100 70-132
4-Chlorotoluene mg/kg 0.0470.05 94 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.0940.1 94 69-130
Acetone mg/kg 0.089J0.1 89 49-148
Benzene mg/kg 0.0500.05 101 70-130
Bromobenzene mg/kg 0.0480.05 96 70-130
Bromochloromethane mg/kg 0.0460.05 92 70-130
Bromodichloromethane mg/kg 0.0510.05 102 70-130
Bromoform mg/kg 0.0500.05 100 68-136
Bromomethane mg/kg 0.0470.05 94 60-140
Carbon tetrachloride mg/kg 0.0510.05 103 70-130
Chlorobenzene mg/kg 0.0470.05 94 70-130
Chloroethane mg/kg 0.0520.05 105 51-147
Chloroform mg/kg 0.0470.05 94 70-130
Chloromethane mg/kg 0.0460.05 93 48-130
cis-1,2-Dichloroethene mg/kg 0.0460.05 92 70-130
cis-1,3-Dichloropropene mg/kg 0.0550.05 110 70-130
Dibromochloromethane mg/kg 0.0500.05 101 70-130
Dibromomethane mg/kg 0.0460.05 91 70-130
Dichlorodifluoromethane mg/kg 0.0450.05 90 49-130
Diisopropyl ether mg/kg 0.0490.05 99 66-130
Ethylbenzene mg/kg 0.0480.05 96 70-130
Hexachloro-1,3-butadiene mg/kg 0.0470.05 94 70-130
Isopropylbenzene (Cumene)mg/kg 0.0480.05 95 70-130
m&p-Xylene mg/kg 0.0970.1 97 70-130
Methyl-tert-butyl ether mg/kg 0.0490.05 97 70-130
Methylene Chloride mg/kg 0.0510.05 103 50-137
n-Butylbenzene mg/kg 0.0470.05 94 70-130
n-Propylbenzene mg/kg 0.0490.05 98 70-130
Naphthalene mg/kg 0.0480.05 96 70-131
o-Xylene mg/kg 0.0500.05 99 70-130
p-Isopropyltoluene mg/kg 0.0480.05 96 70-130
sec-Butylbenzene mg/kg 0.0490.05 99 70-130
Styrene mg/kg 0.0490.05 98 70-130
tert-Butylbenzene mg/kg 0.0430.05 87 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2647882LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene mg/kg 0.0450.05 90 56-130
Toluene mg/kg 0.0470.05 94 70-130
trans-1,2-Dichloroethene mg/kg 0.0490.05 97 70-130
trans-1,3-Dichloropropene mg/kg 0.0520.05 103 70-130
Trichloroethene mg/kg 0.0530.05 106 70-141
Trichlorofluoromethane mg/kg 0.0460.05 92 67-130
Vinyl acetate mg/kg 0.100.1 101 10-136
Vinyl chloride mg/kg 0.0470.05 93 67-130
Xylene (Total)mg/kg 0.150.15 98 70-130
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2647883MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92438947001
2647884
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane mg/kg 0.95 99 52-133110 10 300.95ND 0.94 1.0
1,1,1-Trichloroethane mg/kg 0.95 88 49-13796 9 300.95ND 0.83 0.91
1,1,2,2-Tetrachloroethane mg/kg 0.95 126 39-150131 4 300.95ND 1.2 1.2
1,1,2-Trichloroethane mg/kg 0.95 103 48-140113 10 300.95ND 0.97 1.1
1,1-Dichloroethane mg/kg 0.95 93 46-135103 10 300.95ND 0.88 0.97
1,1-Dichloroethene mg/kg 0.95 95 38-149102 8 300.95ND 0.89 0.97
1,1-Dichloropropene mg/kg 0.95 89 41-14096 8 300.95ND 0.84 0.91
1,2,3-Trichlorobenzene mg/kg 0.95 95 10-158105 10 300.95ND 0.90 0.99
1,2,3-Trichloropropane mg/kg 0.95 108 33-157108 0 300.95ND 1.0 1.0
1,2,4-Trichlorobenzene mg/kg 0.95 93 10-15597 4 300.95ND 0.88 0.92
1,2,4-Trimethylbenzene mg/kg 0.95 95 24-15499 4 300.95ND 0.89 0.93
1,2-Dibromo-3-
chloropropane mg/kg 0.95 99 33-15899 0 300.95ND 0.93 0.93
1,2-Dibromoethane (EDB)mg/kg 0.95 103 40-136110 7 300.95ND 0.97 1.0
1,2-Dichlorobenzene mg/kg 0.95 92 27-14699 7 300.95ND 0.87 0.93
1,2-Dichloroethane mg/kg 0.95 94 49-140100 6 300.95ND 0.89 0.94
1,2-Dichloropropane mg/kg 0.95 104 44-143103 1 300.95ND 0.98 0.97
1,3,5-Trimethylbenzene mg/kg 0.95 93 40-14497 3 300.95ND 0.88 0.91
1,3-Dichlorobenzene mg/kg 0.95 89 33-14091 2 300.95ND 0.84 0.86
1,3-Dichloropropane mg/kg 0.95 100 47-147111 10 300.95ND 0.94 1.0
1,4-Dichlorobenzene mg/kg 0.95 90 35-13996 7 300.95ND 0.85 0.91
2,2-Dichloropropane mg/kg 0.95 85 41-14095 11 300.95ND 0.80 0.90
2-Butanone (MEK)mg/kg 1.9 147 10-181158 301.9ND 2.8J 3.0J
2-Chlorotoluene mg/kg 0.95 94 38-14796 3 300.95ND 0.89 0.91
2-Hexanone mg/kg 1.9 111 18-169116 301.9ND 2.1J 2.2J
4-Chlorotoluene mg/kg 0.95 87 36-14595 8 300.95ND 0.83 0.89
4-Methyl-2-pentanone
(MIBK)mg/kg M11.9 344 16-175348 1 301.9ND 6.5 6.6
Acetone mg/kg 1.9 83 10-20086 301.9ND 1.6J 1.6J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2647883MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92438947001
2647884
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene mg/kg 0.95 98 46-136103 5 300.95ND 0.93 0.97
Bromobenzene mg/kg 0.95 96 38-14999 3 300.95ND 0.91 0.93
Bromochloromethane mg/kg 0.95 86 44-14297 13 300.95ND 0.81 0.92
Bromodichloromethane mg/kg 0.95 91 41-14092 1 300.95ND 0.86 0.87
Bromoform mg/kg 0.95 94 34-145105 11 300.95ND 0.89 0.99
Bromomethane mg/kg 0.95 86 14-16297 11 300.95ND 0.82 0.91
Carbon tetrachloride mg/kg 0.95 91 44-14193 2 300.95ND 0.86 0.88
Chlorobenzene mg/kg 0.95 91 39-141101 10 300.95ND 0.86 0.95
Chloroethane mg/kg v10.95 69 10-18284 20 300.95ND 0.65 0.80
Chloroform mg/kg 0.95 88 45-140100 13 300.95ND 0.83 0.95
Chloromethane mg/kg 0.95 98 19-149106 8 300.95ND 0.92 1.0
cis-1,2-Dichloroethene mg/kg 0.95 96 38-150100 5 300.95ND 0.90 0.95
cis-1,3-Dichloropropene mg/kg 0.95 101 30-144107 5 300.95ND 0.96 1.0
Dibromochloromethane mg/kg 0.95 96 36-145100 5 300.95ND 0.90 0.95
Dibromomethane mg/kg 0.95 97 41-14598 1 300.95ND 0.92 0.93
Dichlorodifluoromethane mg/kg 0.95 85 16-14699 15 300.95ND 0.80 0.93
Diisopropyl ether mg/kg 0.95 101 41-143107 6 300.95ND 0.95 1.0
Ethylbenzene mg/kg 0.95 66 35-14478 6 300.951.1 1.7 1.8
Hexachloro-1,3-butadiene mg/kg 0.95 94 10-16098 5 300.95ND 0.89 0.93
Isopropylbenzene
(Cumene)
mg/kg 0.95 56 30-15263 4 300.951.3 1.8 1.9
m&p-Xylene mg/kg 1.9 92 33-145100 9 301.9ND 1.7 1.9
Methyl-tert-butyl ether mg/kg 0.95 96 49-140100 4 300.95ND 0.90 0.94
Methylene Chloride mg/kg 0.95 99 10-17486 300.95ND 0.93 0.81J
n-Butylbenzene mg/kg 0.95 31 10-16037 3 300.951.6 1.9 1.9
n-Propylbenzene mg/kg M10.95 -5 24-1592 2 300.953.4 3.4 3.4
Naphthalene mg/kg 0.95 45 10-17179 5 300.955.9 6.3 6.6
o-Xylene mg/kg 0.95 95 31-150101 6 300.95ND 0.90 0.96
p-Isopropyltoluene mg/kg 0.95 110 21-154121 9 300.95ND 1.0 1.1
sec-Butylbenzene mg/kg 0.95 69 19-15980 7 300.950.71 1.4 1.5
Styrene mg/kg 0.95 95 15-152101 6 300.95ND 0.90 0.95
tert-Butylbenzene mg/kg 0.95 82 31-14184 2 300.950.14J 0.91 0.93
Tetrachloroethene mg/kg 0.95 87 19-14193 7 300.95ND 0.82 0.88
Toluene mg/kg 0.95 96 31-146103 6 300.95ND 0.91 0.97
trans-1,2-Dichloroethene mg/kg 0.95 95 28-157103 8 300.95ND 0.90 0.97
trans-1,3-Dichloropropene mg/kg 0.95 100 25-146102 2 300.95ND 0.94 0.96
Trichloroethene mg/kg 0.95 95 34-149101 6 300.95ND 0.90 0.95
Trichlorofluoromethane mg/kg 0.95 49 10-16751 4 300.95ND 0.46 0.48
Vinyl acetate mg/kg 1.9 91 10-200100 301.9ND 1.7J 1.9J
Vinyl chloride mg/kg 0.95 96 36-155102 7 300.95ND 0.90 0.97
Xylene (Total)mg/kg 2.9 93 29-148101 8 302.9ND 2.6 2.8
1,2-Dichloroethane-d4 (S)%97 70-13298
4-Bromofluorobenzene (S)%112 70-130113
Toluene-d8 (S)%103 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489259
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Associated Lab Samples:92438947009, 92438947010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2640386
Associated Lab Samples:92438947009, 92438947010
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 5.0 07/30/19 17:202.3
n-Pentacosane (S)%68 33-129 07/30/19 17:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2640387LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 53.766.4 81 43-130
n-Pentacosane (S)%68 33-129
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2640388MATRIX SPIKE SAMPLE:
MSSpike
Result
92438567001
Diesel Range Organics(C10-C28)mg/kg 15600 M173.9 -11600 10-13024200
n-Pentacosane (S)%S043733-129
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438729001
2640389SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 5.5J 305.7
n-Pentacosane (S)%6462
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489516
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Associated Lab Samples:92438947008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2641499
Associated Lab Samples:92438947008
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 5.0 07/31/19 15:432.3
n-Pentacosane (S)%78 33-129 07/31/19 15:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641500LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 60.065.6 91 43-130
n-Pentacosane (S)%75 33-129
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438947008
2641502SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 6.5J 30ND
n-Pentacosane (S)%6960
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489792
EPA 3546
EPA 8015C Modified
8015 Solid GCSV
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2642720
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 5.1 08/02/19 10:232.3
n-Pentacosane (S)%75 33-129 08/02/19 10:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2642721LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 56.665.8 86 43-130
n-Pentacosane (S)%73 33-129
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2642722MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439355005
2642723
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Diesel Range
Organics(C10-C28)mg/kg 85.1 73 10-13082 13 3085.7ND 63.1 71.8
n-Pentacosane (S)%62 33-12966
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489260
EPA 3546
EPA 8015C Modified
8015 Solid GCSV ORO
Associated Lab Samples:92438947008, 92438947009, 92438947010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2640392
Associated Lab Samples:92438947008, 92438947009, 92438947010
Matrix:Solid
AnalyzedMDL
Oil Range Organics (C28-C40)mg/kg ND 14.9 07/30/19 17:206.7
n-Pentacosane (S)%61 33-129 07/30/19 17:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2640393LABORATORY CONTROL SAMPLE:
LCSSpike
Oil Range Organics (C28-C40)mg/kg 61.183.6 73 49-130
n-Pentacosane (S)%65 33-129
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2640394MATRIX SPIKE SAMPLE:
MSSpike
Result
92438947008
Oil Range Organics (C28-C40)mg/kg 89.8114 76 10-132ND
n-Pentacosane (S)%65 33-129
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438947009
2640395SAMPLE DUPLICATE:
Oil Range Organics (C28-C40)mg/kg ND 30ND
n-Pentacosane (S)%5659
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
507284
EPA 3546
EPA 8082A
8082 GCS PCB
Associated Lab Samples:92438947008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2723646
Associated Lab Samples:92438947008
Matrix:Solid
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/kg ND 32.9 11/04/19 16:108.9
PCB-1221 (Aroclor 1221)ug/kg ND 32.9 11/04/19 16:1011.7
PCB-1232 (Aroclor 1232)ug/kg ND 32.9 11/04/19 16:108.3
PCB-1242 (Aroclor 1242)ug/kg ND 32.9 11/04/19 16:102.2
PCB-1248 (Aroclor 1248)ug/kg ND 32.9 11/04/19 16:105.8
PCB-1254 (Aroclor 1254)ug/kg ND 32.9 11/04/19 16:106.2
PCB-1260 (Aroclor 1260)ug/kg ND 32.9 11/04/19 16:107.6
Decachlorobiphenyl (S)%114 10-130 11/04/19 16:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2723647LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/kg 142166 85 35-130
PCB-1260 (Aroclor 1260)ug/kg 169166 101 46-130
Decachlorobiphenyl (S)%103 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489492
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples:92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2641355
Associated Lab Samples:92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.32 07/31/19 15:020.074
1,2-Dichlorobenzene mg/kg ND 0.32 07/31/19 15:020.070
1,3-Dichlorobenzene mg/kg ND 0.32 07/31/19 15:020.073
1,4-Dichlorobenzene mg/kg ND 0.32 07/31/19 15:020.071
1-Methylnaphthalene mg/kg ND 0.32 07/31/19 15:020.086
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.32 07/31/19 15:020.090
2,4,5-Trichlorophenol mg/kg ND 0.32 07/31/19 15:020.084
2,4,6-Trichlorophenol mg/kg ND 0.32 07/31/19 15:020.082
2,4-Dichlorophenol mg/kg ND 0.32 07/31/19 15:020.11
2,4-Dimethylphenol mg/kg ND 0.32 07/31/19 15:020.081
2,4-Dinitrophenol mg/kg ND 1.6 07/31/19 15:021.0
2,4-Dinitrotoluene mg/kg ND 0.32 07/31/19 15:020.086
2,6-Dinitrotoluene mg/kg ND 0.32 07/31/19 15:020.085
2-Chloronaphthalene mg/kg ND 0.32 07/31/19 15:020.072
2-Chlorophenol mg/kg ND 0.32 07/31/19 15:020.076
2-Methylnaphthalene mg/kg ND 0.32 07/31/19 15:020.083
2-Methylphenol(o-Cresol)mg/kg ND 0.32 07/31/19 15:020.072
2-Nitroaniline mg/kg ND 1.6 07/31/19 15:020.16
2-Nitrophenol mg/kg ND 0.32 07/31/19 15:020.10
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.32 07/31/19 15:020.082
3,3'-Dichlorobenzidine mg/kg ND 1.6 07/31/19 15:020.23
3-Nitroaniline mg/kg ND 1.6 07/31/19 15:020.17
4,6-Dinitro-2-methylphenol mg/kg ND 0.65 07/31/19 15:020.52
4-Bromophenylphenyl ether mg/kg ND 0.32 07/31/19 15:020.085
4-Chloro-3-methylphenol mg/kg ND 0.65 07/31/19 15:020.20
4-Chloroaniline mg/kg ND 1.6 07/31/19 15:020.20
4-Chlorophenylphenyl ether mg/kg ND 0.32 07/31/19 15:020.084
4-Nitroaniline mg/kg ND 0.65 07/31/19 15:020.16
4-Nitrophenol mg/kg ND 1.6 07/31/19 15:020.52
Acenaphthene mg/kg ND 0.32 07/31/19 15:020.084
Acenaphthylene mg/kg ND 0.32 07/31/19 15:020.077
Aniline mg/kg ND 0.32 07/31/19 15:020.073
Anthracene mg/kg ND 0.32 07/31/19 15:020.084
Benzo(a)anthracene mg/kg ND 0.32 07/31/19 15:020.10
Benzo(a)pyrene mg/kg ND 0.32 07/31/19 15:020.14
Benzo(b)fluoranthene mg/kg ND 0.32 07/31/19 15:020.13
Benzo(g,h,i)perylene mg/kg ND 0.32 07/31/19 15:020.13
Benzo(k)fluoranthene mg/kg ND 0.32 07/31/19 15:020.14
Benzoic Acid mg/kg ND 1.6 v107/31/19 15:020.35
Benzyl alcohol mg/kg ND 0.65 v107/31/19 15:020.17
bis(2-Chloroethoxy)methane mg/kg ND 0.32 07/31/19 15:020.087
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 72 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2641355
Associated Lab Samples:92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethyl) ether mg/kg ND 0.32 07/31/19 15:020.069
bis(2-Ethylhexyl)phthalate mg/kg ND 0.32 07/31/19 15:020.11
Butylbenzylphthalate mg/kg ND 0.32 07/31/19 15:020.086
Chrysene mg/kg ND 0.32 07/31/19 15:020.094
Di-n-butylphthalate mg/kg ND 0.32 07/31/19 15:020.080
Di-n-octylphthalate mg/kg ND 0.32 07/31/19 15:020.18
Dibenz(a,h)anthracene mg/kg ND 0.32 07/31/19 15:020.13
Dibenzofuran mg/kg ND 0.32 07/31/19 15:020.081
Diethylphthalate mg/kg ND 0.32 07/31/19 15:020.070
Dimethylphthalate mg/kg ND 0.32 07/31/19 15:020.073
Fluoranthene mg/kg ND 0.32 07/31/19 15:020.098
Fluorene mg/kg ND 0.32 07/31/19 15:020.087
Hexachloro-1,3-butadiene mg/kg ND 0.32 07/31/19 15:020.079
Hexachlorobenzene mg/kg ND 0.32 07/31/19 15:020.082
Hexachlorocyclopentadiene mg/kg ND 0.32 v107/31/19 15:020.13
Hexachloroethane mg/kg ND 0.32 v107/31/19 15:020.074
Indeno(1,2,3-cd)pyrene mg/kg ND 0.32 07/31/19 15:020.15
Isophorone mg/kg ND 0.32 07/31/19 15:020.071
N-Nitroso-di-n-propylamine mg/kg ND 0.32 v107/31/19 15:020.091
N-Nitrosodimethylamine mg/kg ND 0.32 07/31/19 15:020.091
N-Nitrosodiphenylamine mg/kg ND 0.32 07/31/19 15:020.083
Naphthalene mg/kg ND 0.32 07/31/19 15:020.078
Nitrobenzene mg/kg ND 0.32 07/31/19 15:020.078
Pentachlorophenol mg/kg ND 1.6 07/31/19 15:020.15
Phenanthrene mg/kg ND 0.32 07/31/19 15:020.082
Phenol mg/kg ND 0.32 07/31/19 15:020.078
Pyrene mg/kg ND 0.32 07/31/19 15:020.089
2,4,6-Tribromophenol (S)%90 27-110 07/31/19 15:02
2-Fluorobiphenyl (S)%77 30-110 07/31/19 15:02
2-Fluorophenol (S)%88 13-110 07/31/19 15:02
Nitrobenzene-d5 (S)%78 23-110 07/31/19 15:02
Phenol-d6 (S)%87 22-110 07/31/19 15:02
Terphenyl-d14 (S)%94 28-110 07/31/19 15:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641356LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.21.7 71 52-130
1,2-Dichlorobenzene mg/kg 1.21.7 71 51-130
1,3-Dichlorobenzene mg/kg 1.11.7 64 50-130
1,4-Dichlorobenzene mg/kg 1.21.7 73 49-130
1-Methylnaphthalene mg/kg 1.31.7 79 55-130
2,2'-Oxybis(1-chloropropane)mg/kg 1.31.7 81 30-130
2,4,5-Trichlorophenol mg/kg 1.61.7 94 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 73 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641356LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol mg/kg 1.71.7 100 57-130
2,4-Dichlorophenol mg/kg 1.41.7 86 56-130
2,4-Dimethylphenol mg/kg 1.41.7 87 51-130
2,4-Dinitrophenol mg/kg 7.98.3 95 27-133
2,4-Dinitrotoluene mg/kg 1.51.7 91 61-130
2,6-Dinitrotoluene mg/kg 1.51.7 93 60-130
2-Chloronaphthalene mg/kg 1.41.7 86 52-130
2-Chlorophenol mg/kg 1.31.7 77 54-130
2-Methylnaphthalene mg/kg 1.41.7 82 54-130
2-Methylphenol(o-Cresol)mg/kg 1.31.7 79 51-130
2-Nitroaniline mg/kg 3.13.3 95 51-130
2-Nitrophenol mg/kg 1.31.7 79 49-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.61.7 96 11-163
3,3'-Dichlorobenzidine mg/kg 2.83.3 84 10-132
3-Nitroaniline mg/kg 2.93.3 86 55-130
4,6-Dinitro-2-methylphenol mg/kg 3.53.3 106 47-142
4-Bromophenylphenyl ether mg/kg 1.51.7 89 59-130
4-Chloro-3-methylphenol mg/kg 3.13.3 95 55-130
4-Chloroaniline mg/kg 2.63.3 78 54-130
4-Chlorophenylphenyl ether mg/kg 1.51.7 93 58-130
4-Nitroaniline mg/kg 3.13.3 93 54-130
4-Nitrophenol mg/kg 8.38.3 100 48-130
Acenaphthene mg/kg 1.51.7 92 60-130
Acenaphthylene mg/kg 1.61.7 95 60-130
Aniline mg/kg 1.11.7 66 43-130
Anthracene mg/kg 1.61.7 94 63-130
Benzo(a)anthracene mg/kg 1.51.7 91 59-130
Benzo(a)pyrene mg/kg 1.61.7 94 57-130
Benzo(b)fluoranthene mg/kg 1.61.7 96 54-130
Benzo(g,h,i)perylene mg/kg 1.61.7 95 59-130
Benzo(k)fluoranthene mg/kg 1.51.7 94 54-130
Benzoic Acid mg/kg 6.1 v18.3 74 19-130
Benzyl alcohol mg/kg 3.0 v13.3 92 50-130
bis(2-Chloroethoxy)methane mg/kg 1.41.7 83 54-130
bis(2-Chloroethyl) ether mg/kg 1.21.7 75 48-130
bis(2-Ethylhexyl)phthalate mg/kg 1.41.7 86 45-134
Butylbenzylphthalate mg/kg 1.41.7 85 46-138
Chrysene mg/kg 1.41.7 87 58-130
Di-n-butylphthalate mg/kg 1.41.7 87 60-130
Di-n-octylphthalate mg/kg 1.41.7 86 53-130
Dibenz(a,h)anthracene mg/kg 1.51.7 91 59-130
Dibenzofuran mg/kg 1.61.7 94 60-130
Diethylphthalate mg/kg 1.51.7 89 60-130
Dimethylphthalate mg/kg 1.61.7 94 60-130
Fluoranthene mg/kg 1.61.7 97 65-130
Fluorene mg/kg 1.61.7 94 63-130
Hexachloro-1,3-butadiene mg/kg 1.11.7 68 46-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2641356LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene mg/kg 1.41.7 86 58-130
Hexachlorocyclopentadiene mg/kg 1.2 v11.7 70 23-130
Hexachloroethane mg/kg 1.3 v11.7 76 47-130
Indeno(1,2,3-cd)pyrene mg/kg 1.61.7 94 60-130
Isophorone mg/kg 1.31.7 79 49-130
N-Nitroso-di-n-propylamine mg/kg 1.5 v11.7 90 47-130
N-Nitrosodimethylamine mg/kg 1.11.7 69 45-130
N-Nitrosodiphenylamine mg/kg 1.51.7 93 59-130
Naphthalene mg/kg 1.31.7 78 55-130
Nitrobenzene mg/kg 1.21.7 70 49-130
Pentachlorophenol mg/kg 3.13.3 95 10-132
Phenanthrene mg/kg 1.61.7 96 62-130
Phenol mg/kg 1.31.7 78 46-130
Pyrene mg/kg 1.51.7 92 53-130
2,4,6-Tribromophenol (S)%99 27-110
2-Fluorobiphenyl (S)%90 30-110
2-Fluorophenol (S)%78 13-110
Nitrobenzene-d5 (S)%78 23-110
Phenol-d6 (S)%79 22-110
Terphenyl-d14 (S)%93 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2641357MATRIX SPIKE SAMPLE:
MSSpike
Result
92438729001
1,2,4-Trichlorobenzene mg/kg 1.31.9 70 18-130ND
1,2-Dichlorobenzene mg/kg 1.41.9 75 14-130ND
1,3-Dichlorobenzene mg/kg 1.31.9 71 12-130ND
1,4-Dichlorobenzene mg/kg 1.41.9 75 10-130ND
1-Methylnaphthalene mg/kg 1.31.9 71 12-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.61.9 88 10-130ND
2,4,5-Trichlorophenol mg/kg 1.71.9 91 13-130ND
2,4,6-Trichlorophenol mg/kg 1.81.9 99 17-130ND
2,4-Dichlorophenol mg/kg 1.51.9 82 10-130ND
2,4-Dimethylphenol mg/kg 1.61.9 87 10-130ND
2,4-Dinitrophenol mg/kg 8.39.3 90 10-130ND
2,4-Dinitrotoluene mg/kg 1.41.9 75 24-130ND
2,6-Dinitrotoluene mg/kg 1.61.9 84 23-130ND
2-Chloronaphthalene mg/kg 1.51.9 80 19-130ND
2-Chlorophenol mg/kg 1.61.9 87 10-130ND
2-Methylnaphthalene mg/kg 1.31.9 73 18-130ND
2-Methylphenol(o-Cresol)mg/kg 1.61.9 86 10-130ND
2-Nitroaniline mg/kg 3.53.7 93 17-130ND
2-Nitrophenol mg/kg 1.51.9 79 10-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.61.9 88 10-130ND
3,3'-Dichlorobenzidine mg/kg 2.93.7 79 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
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Page 75 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2641357MATRIX SPIKE SAMPLE:
MSSpike
Result
92438729001
3-Nitroaniline mg/kg 2.93.7 79 24-130ND
4,6-Dinitro-2-methylphenol mg/kg 3.43.7 93 10-152ND
4-Bromophenylphenyl ether mg/kg 1.41.9 75 29-130ND
4-Chloro-3-methylphenol mg/kg 3.13.7 85 17-130ND
4-Chloroaniline mg/kg 2.73.7 74 14-130ND
4-Chlorophenylphenyl ether mg/kg 1.41.9 76 25-130ND
4-Nitroaniline mg/kg 2.93.7 78 22-130ND
4-Nitrophenol mg/kg 8.39.3 89 10-130ND
Acenaphthene mg/kg 1.41.9 78 20-130ND
Acenaphthylene mg/kg 1.61.9 86 25-130ND
Aniline mg/kg 1.31.9 72 10-130ND
Anthracene mg/kg 1.41.9 77 29-130ND
Benzo(a)anthracene mg/kg 1.41.9 74 19-130ND
Benzo(a)pyrene mg/kg 1.41.9 74 12-130ND
Benzo(b)fluoranthene mg/kg 1.51.9 81 14-130ND
Benzo(g,h,i)perylene mg/kg 1.31.9 72 10-130ND
Benzo(k)fluoranthene mg/kg 1.41.9 73 14-130ND
Benzoic Acid mg/kg 6.9 v19.3 74 10-130ND
Benzyl alcohol mg/kg 3.33.7 88 13-130ND
bis(2-Chloroethoxy)methane mg/kg 1.51.9 83 16-130ND
bis(2-Chloroethyl) ether mg/kg 1.61.9 86 11-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.31.9 69 21-130ND
Butylbenzylphthalate mg/kg 1.31.9 71 23-130ND
Chrysene mg/kg 1.31.9 68 22-130ND
Di-n-butylphthalate mg/kg 1.31.9 70 30-130ND
Di-n-octylphthalate mg/kg 1.31.9 70 23-142ND
Dibenz(a,h)anthracene mg/kg 1.31.9 71 10-130ND
Dibenzofuran mg/kg 1.51.9 79 24-130ND
Diethylphthalate mg/kg 1.41.9 76 26-130ND
Dimethylphthalate mg/kg 1.61.9 88 22-130ND
Fluoranthene mg/kg 1.31.9 71 33-130ND
Fluorene mg/kg 1.41.9 78 22-130ND
Hexachloro-1,3-butadiene mg/kg 1.21.9 64 13-130ND
Hexachlorobenzene mg/kg 1.31.9 72 29-130ND
Hexachlorocyclopentadiene mg/kg 1.2 v11.9 62 10-130ND
Hexachloroethane mg/kg 1.3 v11.9 70 10-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.51.9 79 10-130ND
Isophorone mg/kg 1.41.9 75 13-130ND
N-Nitroso-di-n-propylamine mg/kg 1.5 v11.9 81 12-130ND
N-Nitrosodimethylamine mg/kg 1.41.9 77 11-130ND
N-Nitrosodiphenylamine mg/kg 1.51.9 79 15-130ND
Naphthalene mg/kg 1.41.9 77 15-130ND
Nitrobenzene mg/kg 1.41.9 73 12-130ND
Pentachlorophenol mg/kg 3.03.7 81 10-130ND
Phenanthrene mg/kg 1.51.9 81 27-130ND
Phenol mg/kg 1.71.9 89 10-130ND
Pyrene mg/kg 1.41.9 75 19-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2641357MATRIX SPIKE SAMPLE:
MSSpike
Result
92438729001
2,4,6-Tribromophenol (S)%83 27-110
2-Fluorobiphenyl (S)%81 30-110
2-Fluorophenol (S)%85 13-110
Nitrobenzene-d5 (S)%78 23-110
Phenol-d6 (S)%86 22-110
Terphenyl-d14 (S)%72 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438729002
2641358SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg ND 30ND
2,2'-Oxybis(1-chloropropane)mg/kg ND 30ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
2-Chlorophenol mg/kg ND 30ND
2-Methylnaphthalene mg/kg ND 30ND
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Nitroaniline mg/kg ND 30ND
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND 30ND
3-Nitroaniline mg/kg ND 30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND 30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
Aniline mg/kg ND 30ND
Anthracene mg/kg ND 30ND
Benzo(a)anthracene mg/kg ND 30ND
Benzo(a)pyrene mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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Page 77 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438729002
2641358SAMPLE DUPLICATE:
Benzo(b)fluoranthene mg/kg ND 30ND
Benzo(g,h,i)perylene mg/kg ND 30ND
Benzo(k)fluoranthene mg/kg ND 30ND
Benzoic Acid mg/kg ND v130ND
Benzyl alcohol mg/kg ND v130ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg ND 30ND
Butylbenzylphthalate mg/kg ND 30ND
Chrysene mg/kg ND 30ND
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg ND 30ND
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzofuran mg/kg ND 30ND
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg ND 30ND
Fluorene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND v130ND
Hexachloroethane mg/kg ND v130ND
Indeno(1,2,3-cd)pyrene mg/kg ND 30ND
Isophorone mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND v130ND
N-Nitrosodimethylamine mg/kg ND 30ND
N-Nitrosodiphenylamine mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg ND 30ND
Phenanthrene mg/kg ND 30ND
Phenol mg/kg ND 30ND
Pyrene mg/kg ND 30ND
2,4,6-Tribromophenol (S)%8063
2-Fluorobiphenyl (S)%6161
2-Fluorophenol (S)%8168
Nitrobenzene-d5 (S)%7668
Phenol-d6 (S)%7481
Terphenyl-d14 (S)%6769
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
491465
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2650627
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 08/11/19 09:580.077
1,2-Dichlorobenzene mg/kg ND 0.33 08/11/19 09:580.072
1,3-Dichlorobenzene mg/kg ND 0.33 08/11/19 09:580.075
1,4-Dichlorobenzene mg/kg ND 0.33 08/11/19 09:580.074
1-Methylnaphthalene mg/kg ND 0.33 08/11/19 09:580.089
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 v108/11/19 09:580.093
2,4,5-Trichlorophenol mg/kg ND 0.33 08/11/19 09:580.087
2,4,6-Trichlorophenol mg/kg ND 0.33 08/11/19 09:580.084
2,4-Dichlorophenol mg/kg ND 0.33 08/11/19 09:580.11
2,4-Dimethylphenol mg/kg ND 0.33 08/11/19 09:580.083
2,4-Dinitrophenol mg/kg ND 1.7 08/11/19 09:581.1
2,4-Dinitrotoluene mg/kg ND 0.33 08/11/19 09:580.089
2,6-Dinitrotoluene mg/kg ND 0.33 08/11/19 09:580.087
2-Chloronaphthalene mg/kg ND 0.33 08/11/19 09:580.074
2-Chlorophenol mg/kg ND 0.33 08/11/19 09:580.078
2-Methylnaphthalene mg/kg ND 0.33 08/11/19 09:580.085
2-Methylphenol(o-Cresol)mg/kg ND 0.33 08/11/19 09:580.074
2-Nitroaniline mg/kg ND 1.7 08/11/19 09:580.17
2-Nitrophenol mg/kg ND 0.33 08/11/19 09:580.10
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 08/11/19 09:580.084
3,3'-Dichlorobenzidine mg/kg ND 1.7 08/11/19 09:580.23
3-Nitroaniline mg/kg ND 1.7 08/11/19 09:580.18
4,6-Dinitro-2-methylphenol mg/kg ND 0.67 08/11/19 09:580.54
4-Bromophenylphenyl ether mg/kg ND 0.33 08/11/19 09:580.088
4-Chloro-3-methylphenol mg/kg ND 0.67 08/11/19 09:580.20
4-Chloroaniline mg/kg ND 1.7 08/11/19 09:580.20
4-Chlorophenylphenyl ether mg/kg ND 0.33 08/11/19 09:580.087
4-Nitroaniline mg/kg ND 0.67 08/11/19 09:580.17
4-Nitrophenol mg/kg ND 1.7 08/11/19 09:580.53
Acenaphthene mg/kg ND 0.33 08/11/19 09:580.086
Acenaphthylene mg/kg ND 0.33 08/11/19 09:580.079
Aniline mg/kg ND 0.33 08/11/19 09:580.075
Anthracene mg/kg ND 0.33 08/11/19 09:580.087
Benzo(a)anthracene mg/kg ND 0.33 08/11/19 09:580.11
Benzo(a)pyrene mg/kg ND 0.33 08/11/19 09:580.14
Benzo(b)fluoranthene mg/kg ND 0.33 08/11/19 09:580.13
Benzo(g,h,i)perylene mg/kg ND 0.33 08/11/19 09:580.13
Benzo(k)fluoranthene mg/kg ND 0.33 08/11/19 09:580.14
Benzoic Acid mg/kg ND 1.7 08/11/19 09:580.36
Benzyl alcohol mg/kg ND 0.67 08/11/19 09:580.18
bis(2-Chloroethoxy)methane mg/kg ND 0.33 08/11/19 09:580.089
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2650627
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethyl) ether mg/kg ND 0.33 08/11/19 09:580.071
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 08/11/19 09:580.11
Butylbenzylphthalate mg/kg ND 0.33 08/11/19 09:580.089
Chrysene mg/kg ND 0.33 08/11/19 09:580.097
Di-n-butylphthalate mg/kg ND 0.33 08/11/19 09:580.082
Di-n-octylphthalate mg/kg ND 0.33 v108/11/19 09:580.19
Dibenz(a,h)anthracene mg/kg ND 0.33 08/11/19 09:580.13
Dibenzofuran mg/kg ND 0.33 08/11/19 09:580.084
Diethylphthalate mg/kg ND 0.33 08/11/19 09:580.073
Dimethylphthalate mg/kg ND 0.33 08/11/19 09:580.076
Fluoranthene mg/kg ND 0.33 08/11/19 09:580.10
Fluorene mg/kg ND 0.33 08/11/19 09:580.089
Hexachloro-1,3-butadiene mg/kg ND 0.33 08/11/19 09:580.081
Hexachlorobenzene mg/kg ND 0.33 08/11/19 09:580.085
Hexachlorocyclopentadiene mg/kg ND 0.33 08/11/19 09:580.13
Hexachloroethane mg/kg ND 0.33 08/11/19 09:580.076
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 08/11/19 09:580.15
Isophorone mg/kg ND 0.33 08/11/19 09:580.073
N-Nitroso-di-n-propylamine mg/kg ND 0.33 08/11/19 09:580.094
N-Nitrosodimethylamine mg/kg ND 0.33 08/11/19 09:580.094
N-Nitrosodiphenylamine mg/kg ND 0.33 08/11/19 09:580.085
Naphthalene mg/kg ND 0.33 08/11/19 09:580.080
Nitrobenzene mg/kg ND 0.33 08/11/19 09:580.080
Pentachlorophenol mg/kg ND 1.7 08/11/19 09:580.15
Phenanthrene mg/kg ND 0.33 08/11/19 09:580.084
Phenol mg/kg ND 0.33 08/11/19 09:580.080
Pyrene mg/kg ND 0.33 08/11/19 09:580.092
2,4,6-Tribromophenol (S)%70 27-110 08/11/19 09:58
2-Fluorobiphenyl (S)%71 30-110 08/11/19 09:58
2-Fluorophenol (S)%69 13-110 08/11/19 09:58
Nitrobenzene-d5 (S)%67 23-110 08/11/19 09:58
Phenol-d6 (S)%69 22-110 08/11/19 09:58
Terphenyl-d14 (S)%84 28-110 08/11/19 09:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2650628LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.11.7 65 52-130
1,2-Dichlorobenzene mg/kg 1.21.7 71 51-130
1,3-Dichlorobenzene mg/kg 1.21.7 70 50-130
1,4-Dichlorobenzene mg/kg 1.21.7 71 49-130
1-Methylnaphthalene mg/kg 1.31.7 76 55-130
2,2'-Oxybis(1-chloropropane)mg/kg 1.9 v11.7 113 30-130
2,4,5-Trichlorophenol mg/kg 1.21.7 70 55-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2650628LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol mg/kg 1.21.7 70 57-130
2,4-Dichlorophenol mg/kg 1.21.7 71 56-130
2,4-Dimethylphenol mg/kg 1.31.7 77 51-130
2,4-Dinitrophenol mg/kg 5.68.4 67 27-133
2,4-Dinitrotoluene mg/kg 1.21.7 71 61-130
2,6-Dinitrotoluene mg/kg 1.21.7 74 60-130
2-Chloronaphthalene mg/kg 1.21.7 71 52-130
2-Chlorophenol mg/kg 1.31.7 79 54-130
2-Methylnaphthalene mg/kg 1.31.7 80 54-130
2-Methylphenol(o-Cresol)mg/kg 1.31.7 75 51-130
2-Nitroaniline mg/kg 2.93.3 87 51-130
2-Nitrophenol mg/kg 1.21.7 70 49-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.31.7 77 11-163
3,3'-Dichlorobenzidine mg/kg 2.53.3 76 10-132
3-Nitroaniline mg/kg 2.73.3 81 55-130
4,6-Dinitro-2-methylphenol mg/kg 2.73.3 81 47-142
4-Bromophenylphenyl ether mg/kg 1.31.7 79 59-130
4-Chloro-3-methylphenol mg/kg 2.63.3 78 55-130
4-Chloroaniline mg/kg 2.73.3 82 54-130
4-Chlorophenylphenyl ether mg/kg 1.21.7 71 58-130
4-Nitroaniline mg/kg 2.83.3 85 54-130
4-Nitrophenol mg/kg 6.08.4 72 48-130
Acenaphthene mg/kg 1.41.7 81 60-130
Acenaphthylene mg/kg 1.41.7 86 60-130
Aniline mg/kg 1.21.7 73 43-130
Anthracene mg/kg 1.61.7 94 63-130
Benzo(a)anthracene mg/kg 1.51.7 88 59-130
Benzo(a)pyrene mg/kg 1.51.7 88 57-130
Benzo(b)fluoranthene mg/kg 1.51.7 88 54-130
Benzo(g,h,i)perylene mg/kg 1.51.7 92 59-130
Benzo(k)fluoranthene mg/kg 1.51.7 92 54-130
Benzoic Acid mg/kg 4.98.4 59 19-130
Benzyl alcohol mg/kg 2.63.3 78 50-130
bis(2-Chloroethoxy)methane mg/kg 1.31.7 76 54-130
bis(2-Chloroethyl) ether mg/kg 1.31.7 80 48-130
bis(2-Ethylhexyl)phthalate mg/kg 1.71.7 104 45-134
Butylbenzylphthalate mg/kg 1.71.7 103 46-138
Chrysene mg/kg 1.61.7 93 58-130
Di-n-butylphthalate mg/kg 1.61.7 93 60-130
Di-n-octylphthalate mg/kg 1.7 v11.7 103 53-130
Dibenz(a,h)anthracene mg/kg 1.51.7 91 59-130
Dibenzofuran mg/kg 1.31.7 77 60-130
Diethylphthalate mg/kg 1.31.7 80 60-130
Dimethylphthalate mg/kg 1.41.7 81 60-130
Fluoranthene mg/kg 1.51.7 89 65-130
Fluorene mg/kg 1.31.7 80 63-130
Hexachloro-1,3-butadiene mg/kg 0.921.7 55 46-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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Huntersville, NC 28078
[phone]
Page 81 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2650628LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene mg/kg 1.21.7 71 58-130
Hexachlorocyclopentadiene mg/kg 0.951.7 57 23-130
Hexachloroethane mg/kg 1.21.7 70 47-130
Indeno(1,2,3-cd)pyrene mg/kg 1.51.7 92 60-130
Isophorone mg/kg 1.21.7 70 49-130
N-Nitroso-di-n-propylamine mg/kg 1.41.7 85 47-130
N-Nitrosodimethylamine mg/kg 1.31.7 77 45-130
N-Nitrosodiphenylamine mg/kg 1.71.7 100 59-130
Naphthalene mg/kg 1.41.7 82 55-130
Nitrobenzene mg/kg 1.21.7 70 49-130
Pentachlorophenol mg/kg 2.33.3 69 10-132
Phenanthrene mg/kg 1.61.7 94 62-130
Phenol mg/kg 1.31.7 79 46-130
Pyrene mg/kg 1.61.7 98 53-130
2,4,6-Tribromophenol (S)%73 27-110
2-Fluorobiphenyl (S)%76 30-110
2-Fluorophenol (S)%82 13-110
Nitrobenzene-d5 (S)%75 23-110
Phenol-d6 (S)%82 22-110
Terphenyl-d14 (S)%86 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2650631MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92432117010
2650632
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene mg/kg 1.7 55 18-13058 5 301.7ND 0.92 0.96
1,2-Dichlorobenzene mg/kg 1.7 60 14-13065 8 301.7ND 1.0 1.1
1,3-Dichlorobenzene mg/kg 1.7 59 12-13065 9 301.7ND 0.98 1.1
1,4-Dichlorobenzene mg/kg 1.7 60 10-13064 5 301.7ND 1.0 1.1
1-Methylnaphthalene mg/kg 1.7 66 12-13069 4 301.7ND 1.1 1.2
2,2'-Oxybis(1-
chloropropane)mg/kg v11.7 98 10-130105 6 301.7ND 1.6 1.7
2,4,5-Trichlorophenol mg/kg 1.7 60 13-13059 2 301.7ND 1.0 0.99
2,4,6-Trichlorophenol mg/kg 1.7 63 17-13061 2 301.7ND 1.0 1.0
2,4-Dichlorophenol mg/kg 1.7 63 10-13063 2 301.7ND 1.1 1.0
2,4-Dimethylphenol mg/kg 1.7 63 10-13065 3 301.7ND 1.1 1.1
2,4-Dinitrophenol mg/kg 8.4 58 10-13059 1 308.3ND 4.9 4.9
2,4-Dinitrotoluene mg/kg 1.7 66 24-13063 4 301.7ND 1.1 1.1
2,6-Dinitrotoluene mg/kg 1.7 65 23-13064 1 301.7ND 1.1 1.1
2-Chloronaphthalene mg/kg 1.7 63 19-13064 2 301.7ND 1.0 1.1
2-Chlorophenol mg/kg 1.7 64 10-13071 10 301.7ND 1.1 1.2
2-Methylnaphthalene mg/kg 1.7 69 18-13071 2 301.7ND 1.2 1.2
2-Methylphenol(o-Cresol)mg/kg 1.7 62 10-13067 8 301.7ND 1.0 1.1
2-Nitroaniline mg/kg 3.3 80 17-13079 2 303.3ND 2.7 2.6
2-Nitrophenol mg/kg 1.7 60 10-13064 5 301.7ND 1.0 1.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2650631MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92432117010
2650632
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)mg/kg 1.7 64 10-13069 7 301.7ND 1.1 1.2
3,3'-Dichlorobenzidine mg/kg 3.3 65 10-13068 4 303.3ND 2.2 2.3
3-Nitroaniline mg/kg 3.3 70 24-13073 3 303.3ND 2.4 2.4
4,6-Dinitro-2-methylphenol mg/kg 3.3 71 10-15270 2 303.3ND 2.4 2.3
4-Bromophenylphenyl ether mg/kg 1.7 70 29-13070 1 301.7ND 1.2 1.2
4-Chloro-3-methylphenol mg/kg 3.3 67 17-13068 1 303.3ND 2.2 2.3
4-Chloroaniline mg/kg 3.3 64 14-13069 7 303.3ND 2.2 2.3
4-Chlorophenylphenyl ether mg/kg 1.7 63 25-13062 3 301.7ND 1.1 1.0
4-Nitroaniline mg/kg 3.3 74 22-13071 4 303.3ND 2.5 2.4
4-Nitrophenol mg/kg 8.4 62 10-13063 1 308.3ND 5.2 5.3
Acenaphthene mg/kg 1.7 72 20-13072 1 301.7ND 1.2 1.2
Acenaphthylene mg/kg 1.7 75 25-13077 2 301.7ND 1.3 1.3
Aniline mg/kg 1.7 45 10-13052 15 301.7ND 0.75 0.87
Anthracene mg/kg 1.7 82 29-13081 2 301.7ND 1.4 1.4
Benzo(a)anthracene mg/kg 1.7 76 19-13077 1 301.7ND 1.3 1.3
Benzo(a)pyrene mg/kg 1.7 77 12-13077 1 301.7ND 1.3 1.3
Benzo(b)fluoranthene mg/kg 1.7 78 14-13078 0 301.7ND 1.3 1.3
Benzo(g,h,i)perylene mg/kg 1.7 81 10-13079 2 301.7ND 1.3 1.3
Benzo(k)fluoranthene mg/kg 1.7 77 14-13077 1 301.7ND 1.3 1.3
Benzoic Acid mg/kg 8.4 25 10-13030 20 308.3ND 2.1 2.5
Benzyl alcohol mg/kg 3.3 63 13-13070 10 303.3ND 2.1 2.3
bis(2-
Chloroethoxy)methane mg/kg 1.7 64 16-13070 8 301.7ND 1.1 1.2
bis(2-Chloroethyl) ether mg/kg 1.7 68 11-13074 8 301.7ND 1.1 1.2
bis(2-Ethylhexyl)phthalate mg/kg 1.7 87 21-13089 1 301.7ND 1.5 1.5
Butylbenzylphthalate mg/kg 1.7 87 23-13089 2 301.7ND 1.5 1.5
Chrysene mg/kg 1.7 81 22-13082 2 301.7ND 1.4 1.4
Di-n-butylphthalate mg/kg 1.7 81 30-13081 0 301.7ND 1.4 1.4
Di-n-octylphthalate mg/kg v11.7 87 23-14287 0 301.7ND 1.5 1.4
Dibenz(a,h)anthracene mg/kg 1.7 79 10-13077 3 301.7ND 1.3 1.3
Dibenzofuran mg/kg 1.7 70 24-13068 3 301.7ND 1.2 1.1
Diethylphthalate mg/kg 1.7 71 26-13071 1 301.7ND 1.2 1.2
Dimethylphthalate mg/kg 1.7 73 22-13073 0 301.7ND 1.2 1.2
Fluoranthene mg/kg 1.7 79 33-13079 0 301.7ND 1.3 1.3
Fluorene mg/kg 1.7 72 22-13071 2 301.7ND 1.2 1.2
Hexachloro-1,3-butadiene mg/kg 1.7 48 13-13050 3 301.7ND 0.81 0.84
Hexachlorobenzene mg/kg 1.7 64 29-13064 1 301.7ND 1.1 1.1
Hexachlorocyclopentadiene mg/kg 1.7 48 10-13049 2 301.7ND 0.81 0.82
Hexachloroethane mg/kg 1.7 61 10-13067 8 301.7ND 1.0 1.1
Indeno(1,2,3-cd)pyrene mg/kg 1.7 79 10-13078 1 301.7ND 1.3 1.3
Isophorone mg/kg 1.7 61 13-13063 2 301.7ND 1.0 1.0
N-Nitroso-di-n-propylamine mg/kg 1.7 69 12-13075 8 301.7ND 1.2 1.2
N-Nitrosodimethylamine mg/kg 1.7 68 11-13073 7 301.7ND 1.1 1.2
N-Nitrosodiphenylamine mg/kg 1.7 88 15-13088 0 301.7ND 1.5 1.5
Naphthalene mg/kg 1.7 72 15-13074 2 301.7ND 1.2 1.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2650631MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92432117010
2650632
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrobenzene mg/kg 1.7 60 12-13063 5 301.7ND 1.0 1.1
Pentachlorophenol mg/kg 3.3 63 10-13063 1 303.3ND 2.1 2.1
Phenanthrene mg/kg 1.7 84 27-13083 1 301.7ND 1.4 1.4
Phenol mg/kg 1.7 62 10-13068 8 301.7ND 1.0 1.1
Pyrene mg/kg 1.7 86 19-13088 1 301.7ND 1.4 1.5
2,4,6-Tribromophenol (S)%67 27-11068
2-Fluorobiphenyl (S)%66 30-11068
2-Fluorophenol (S)%67 13-11072
Nitrobenzene-d5 (S)%63 23-11066
Phenol-d6 (S)%64 22-11070
Terphenyl-d14 (S)%74 28-11075
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
490897
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2647748
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg ND 10.0 N208/12/19 11:5610.0
Aliphatic (C19-C36)mg/kg ND 10.0 N208/12/19 11:5610.0
Aromatic (C11-C22)mg/kg ND 10.0 N208/12/19 11:5610.0
2-Bromonaphthalene (S)%103 40-140 08/12/19 11:56
2-Fluorobiphenyl (S)%103 40-140 08/12/19 11:56
Nonatriacontane (S)%62 40-140 08/12/19 11:56
o-Terphenyl (S)%84 40-140 08/12/19 11:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2647749LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2647750
Aliphatic (C09-C18)mg/kg ND N29.9 63 40-14067ND 50
Aliphatic (C19-C36)mg/kg ND N213.2 71 40-14072ND 50
Aromatic (C11-C22)mg/kg 21.4 N2287640-1408724.9 15 50
2-Bromonaphthalene (S)%99 40-140103
2-Fluorobiphenyl (S)%100 40-140104
Nonatriacontane (S)%66 40-14068
o-Terphenyl (S)%84 40-14092
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
489070
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92438947001, 92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007,
92438947008, 92438947009, 92438947010
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438769001
2639624SAMPLE DUPLICATE:
Percent Moisture %18.2 18 2515.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438895003
2639625SAMPLE DUPLICATE:
Percent Moisture %8.4 8 257.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1322462
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92438947002, 92438947003, 92438947004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3437500-1
Associated Lab Samples:92438947002, 92438947003, 92438947004
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 08/03/19 16:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3437500-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 99.9 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438947003
R3437500-3SAMPLE DUPLICATE:
Total Solids %83.9 0.978 1083.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1322464
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92438947005, 92438947006, 92438947007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3437491-1
Associated Lab Samples:92438947005, 92438947006, 92438947007
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 08/03/19 16:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3437491-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1124305-01
R3437491-3SAMPLE DUPLICATE:
Total Solids %85.4 1.12 1084.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1326357
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3439783-1
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 08/12/19 14:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3439783-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1126235-01
R3439783-3SAMPLE DUPLICATE:
Total Solids %76.8 0.504 1076.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1323060
3060A
EPA 7199
Wet Chemistry 7199
Associated Lab Samples:92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3437577-1
Associated Lab Samples:92438947002, 92438947003, 92438947004, 92438947005, 92438947006, 92438947007
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 08/05/19 13:530.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3437577-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.010.0 100 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3437577-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92438947004
R3437577-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 28.2 98.4 75.0-12596.2 2.27 2028.2ND 27.8 27.1
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3437577-6MATRIX SPIKE SAMPLE:
MSSpike
Result
92438947004
Chromium, Hexavalent mg/kg 12901320 97.3 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92438947002
R3437577-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.391J J4.85 200.372
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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Huntersville, NC 28078
[phone]
Page 90 of 99
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92438947
LEH-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1325763
3060A
EPA 7199
Wet Chemistry 7199
Associated Lab Samples:92438947001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3439409-1
Associated Lab Samples:92438947001
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 08/09/19 16:280.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3439409-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.8110.0 98.1 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3439409-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1125683-04
R3439409-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 24.2 77.2 75.0-12583.9 8.22 2024.2ND 18.7 20.3
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3439409-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1125683-04
Chromium, Hexavalent mg/kg 11601410 82.3 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1124635-11
R3439409-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 99
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92438947
LEH-005
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.1g
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The internal standard response was outside the laboratory acceptance limits confirmed by reanalysis. The results
reported are from the most QC compliant analysis.IO
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The analyte failed the method required serial dilution test and/or subsequent post-spike criteria. These failures indicate
matrix interference.PH
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 99
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92438947
LEH-005
ANALYTE QUALIFIERS
Surrogate recovery outside laboratory control limits (confirmed by re-analysis).S1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 99
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92438947
LEH-005
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92438947001 489792 489987SB-1 (8-10)EPA 3546 EPA 8015C Modified
92438947008 489516 489706SB-8 (7-10)EPA 3546 EPA 8015C Modified
92438947009 489259 489458SB-9 (7-10)EPA 3546 EPA 8015C Modified
92438947010 489259 489458SP-10 (7-10)EPA 3546 EPA 8015C Modified
92438947008 489260 489459SB-8 (7-10)EPA 3546 EPA 8015C Modified
92438947009 489260 489459SB-9 (7-10)EPA 3546 EPA 8015C Modified
92438947010 489260 489459SP-10 (7-10)EPA 3546 EPA 8015C Modified
92438947008 507284 507417SB-8 (7-10)EPA 3546 EPA 8082A
92438947001 490897 491663SB-1 (8-10)MADEP EPH MADEP EPH
92438947001 489013 489024SB-1 (8-10)EPA 5030B EPA 8015C Modified
92438947001 490884 490907SB-1 (8-10)MADEP VPH MADEP VPH
92438947001 1324994 1324994SB-1 (8-10)3051 EPA 6020B
92438947002 1321597 1321597SB-2 (3-4)3050B EPA 6020B
92438947003 1321597 1321597SB-3 (0-2)3050B EPA 6020B
92438947004 1321597 1321597SB-4 (0-2)3050B EPA 6020B
92438947005 1321597 1321597SB-5 (0-2)3050B EPA 6020B
92438947006 1321597 1321597SB-6 (2-3)3050B EPA 6020B
92438947007 1321597 1321597SB-7 (0-2)3050B EPA 6020B
92438947001 1324990 1324990SB-1 (8-10)7471A EPA 7471B
92438947002 1321702 1321702SB-2 (3-4)7471A EPA 7471B
92438947003 1321702 1321702SB-3 (0-2)7471A EPA 7471B
92438947004 1321702 1321702SB-4 (0-2)7471A EPA 7471B
92438947005 1321702 1321702SB-5 (0-2)7471A EPA 7471B
92438947006 1321702 1321702SB-6 (2-3)7471A EPA 7471B
92438947007 1321702 1321702SB-7 (0-2)7471A EPA 7471B
92438947001 491465 491670SB-1 (8-10)EPA 3546 EPA 8270E
92438947002 489492 489564SB-2 (3-4)EPA 3546 EPA 8270E
92438947003 489492 489564SB-3 (0-2)EPA 3546 EPA 8270E
92438947004 489492 489564SB-4 (0-2)EPA 3546 EPA 8270E
92438947005 489492 489564SB-5 (0-2)EPA 3546 EPA 8270E
92438947006 489492 489564SB-6 (2-3)EPA 3546 EPA 8270E
92438947007 489492 489564SB-7 (0-2)EPA 3546 EPA 8270E
92438947001 490929 490936SB-1 (8-10)EPA 5035A EPA 8260D
92438947002 489263 489274SB-2 (3-4)EPA 5035A EPA 8260D
92438947003 489527 489532SB-3 (0-2)EPA 5035A EPA 8260D
92438947004 489263 489274SB-4 (0-2)EPA 5035A EPA 8260D
92438947005 489511 489518SB-5 (0-2)EPA 5035A EPA 8260D
92438947006 489527 489532SB-6 (2-3)EPA 5035A EPA 8260D
92438947007 489263 489274SB-7 (0-2)EPA 5035A EPA 8260D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 99
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92438947
LEH-005
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92438947001 489070SB-1 (8-10)ASTM D2974-87
92438947002 489070SB-2 (3-4)ASTM D2974-87
92438947003 489070SB-3 (0-2)ASTM D2974-87
92438947004 489070SB-4 (0-2)ASTM D2974-87
92438947005 489070SB-5 (0-2)ASTM D2974-87
92438947006 489070SB-6 (2-3)ASTM D2974-87
92438947007 489070SB-7 (0-2)ASTM D2974-87
92438947008 489070SB-8 (7-10)ASTM D2974-87
92438947009 489070SB-9 (7-10)ASTM D2974-87
92438947010 489070SP-10 (7-10)ASTM D2974-87
92438947001 1326357 1326357SB-1 (8-10)SM 2540 G SM 2540G
92438947002 1322462 1322462SB-2 (3-4)SM 2540 G SM 2540G
92438947003 1322462 1322462SB-3 (0-2)SM 2540 G SM 2540G
92438947004 1322462 1322462SB-4 (0-2)SM 2540 G SM 2540G
92438947005 1322464 1322464SB-5 (0-2)SM 2540 G SM 2540G
92438947006 1322464 1322464SB-6 (2-3)SM 2540 G SM 2540G
92438947007 1322464 1322464SB-7 (0-2)SM 2540 G SM 2540G
92438947001 1325763 1325763SB-1 (8-10)3060A EPA 7199
92438947002 1323060 1323060SB-2 (3-4)3060A EPA 7199
92438947003 1323060 1323060SB-3 (0-2)3060A EPA 7199
92438947004 1323060 1323060SB-4 (0-2)3060A EPA 7199
92438947005 1323060 1323060SB-5 (0-2)3060A EPA 7199
92438947006 1323060 1323060SB-6 (2-3)3060A EPA 7199
92438947007 1323060 1323060SB-7 (0-2)3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 12:21 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 95 of 99
Page 96 of 99
Page 97 of 99
Page 98 of 99
Page 99 of 99

Appendix C
Groundwater Sampling Forms
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/LEH-004QualityProducts Co.404 Westwood Avenue11/9/1920.0017.08AEM19Sunny, 40s13:4513:5014:2514:3514:4017.0818.6117.2018.1018.3005004,0005,0005,500100 4.594.395.005.265.2812.813.712.911.411.6312.5306.1308.1308.9309.06.665.945.565.635.64-4.113.828.629.830.183.7074.4027.4012.305.00HACH 2100Q, YSI Pro PlusVOCs by8260, SVOCs by8270, RCRA metals by6020/7471PeristalticPVC1-inch14:45Pace AnalyticalTMW-51020Polyethylene bgs
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/LEH-004QualityProducts Co.1537 S. Mint Street11/9/1924.0017.58AEM21Sunny, 40s14:5014:5515:0015:0515:1517.5817.4717.4217.4017.4005001,0001,5002,000100 8.979.188.518.338.2412.512.413.013.113.4178.9176.2175.0175.8175.95.565.575.575.565.5624.223.123.324.725.155.6039.1036.5018.209.41HACH 2100Q, YSI Pro PlusVOCs by8260, SVOCs by8270, RCRA metals by6020/7471PeristalticPVC1-inch15:20Pace AnalyticalTMW-61424Polyethylene bgs