12037_Imperial Campus_RevPIIR_20091006

Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
710 Atlantic Avenue
Greenville, North Carolina
October 6, 2009
Prepared For
Atlantic Ave Holding Co., LLC
Greenville, North Carolina
Prepared By
Duncklee & Dunham, P.C.
Cary, North Carolina
t> DUNCKLEE & DUNHAM, P.C.

DUNCKLEE
& DUNHAM
October 6, 2009
Mr. Tom Taft
Atlantic Ave Holding Co, LLC
2217 Stantonsburg Road
Greenville, North Carolina 27835
Reference: Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
710 Atlantic Avenue
Greenville, North Carolina
Dear Mr. Taft:
ENVIRONMENTAL CONSULTANTS
511 KEISLER DRIVE - SUITE 102
CARY, NORTH CAROLINA 27518
OFFICE: (919) 858 - 9898
FACSIMILE: (919) 858 - 9899
While reviewing documents to assist Atlantic Ave Holding Co. (AAH) with the brownfields agreement
process, errors were found in the June 23, 2008, Phase II Environmental Site Assessment Report. Most of
the errors were associated with the data tabulation in Table 1 and the reporting of this information in
Figure 3.
As a result, Duncklee & Dunham, PC (Duncklee & Dunham) is issuing this revised report to replace the
previous submittal. The outside cover letter, also dated June 23, 2008, and containing estimated costs to
address known environmental issues and enter the brownfields program, does not require revision. We
apologize for the inconvenience and appreciate the opportunity to make this correction.
The attached report summarizes the findings of phase II soil and groundwater assessment tasks performed
at the above referenced property. The report evaluates environmental concerns identified in the May 30,
2008, Phase I Environmental Site Assessment report, includes information on environmental liabilities
associated with the property, provides guidance on inclusion of this development in the North Carolina
Brownfields Program, and outlines the tasks necessary to obtain a North Carolina brownfields agreement
as a means of environmental risk management.
Because a copy of the previous report version was submitted to the North Carolina Brownfields Program
(NCBP) as part of the brownfields agreement application dated October 12, 2008, Ms. Sharon Eckert is
being copied on this revised report so the agency's case file can be properly updated. The NCBP issued a
satisfactory eligibility determination to AAH on December 31, 2008. We have been in communication
with Ms. Eckert regarding the status of the report revision.
MAILING ADDRESS - POST OFFICE BOX 33366 - RALEIGH, NORTH CAROLINA 27636

Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
Greenville, North Carolina
October 6, 2009
Page 2 of 2
Duncklee & Dunham appreciates the opportunity to be of service to you. If you have any questions or
require any additional information, please do not hesitate to contact us at [phone].
Sincerely,
DUNCKLEE & DUNHAM, P.C.
Daphne J. Olszewski
Senior Project Manager
David L. Duncklee, P.G.
Senior Hydrogeologist
Senior Peer Review:
Bryson D. Trexler, Jr., Ph.D., P.G.
Senior Hydrogeologist
Attachments
cc: Ms. Sharon Eckert — NCBP
P:\Atlantic Ave. Holding Co., LLC - 200817\Reports\Revised Phase R Report\Revised Phase H Report - 09173.doc
DUNCKLEE & DUNHAM, P.C.

Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
710 Atlantic Ave
Greenville, North Carolina
October 6, 2009
1 Objectives of the Phase II Environmental Site Assessment
The objective of this assessment is to evaluate the recognized environmental conditions (RECs) and
business environmental concerns identified in the May 30, 2008, Duncklee & Dunham Phase I
Environmental Site Assessment (ESA) prepared for the subject site (see Figure 1). The scope of work
was also designed to acquire data necessary to evaluate the placement of this site into the North Carolina
Brownfields Program (NCBP) as administered by the North Carolina Department of Environment and
Natural Resources (DENR).
1.1 Previous Work
A May 30, 2008, Phase I ESA of the subject site prepared by Duncklee & Dunham was used to identify
areas of potential environmental concern targeted for further investigation. The Phase I ESA identified
seven RECs that included:
F.
� . i. :�rrn �frrStresscd 1 egrtrti
} Steel Tank
pn�
Tanks
F
0'_:• �A
• The area along the western edge of the main
facility identified on Parcel 1 (see Figure 2)
in the Phase I ESA that consists of the boiler
fuel system. This system includes the two
25,000-gallon #6 fuel oil underground
storage tanks (USTs) beneath the floor of the
northern portion of the main building, the
sump adjacent to the boilers containing
apparent #6 fuel oil, the staining/spillage in
the access vault near the rail car fill pipes
under the loading dock, and any associated
underfloor or underground connecting
piping,
• A possible fuel oil aboveground storage tank
(AST) formerly located adjacent to the
smokestack in a small courtyard (which may
or may not be associated with the boiler fuel
system described in the preceding bullet),
also on Parcel 1,
• An area of stained soil and stressed
vegetation on the northern part of Parcel 2
(see Figure 2),
• An abandoned steel AST on the northern portion of Parcel 2,
• A gasoline containing UST system on the west side of the brick garage on Parcel 2,
DUNCKLEE & DUNHAM, P.C.

Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
Greenville, North Carolina
October 6, 2009
Page 2 of 8
The likely presence of a petroleum release from the upgradient adjoining property (Texas Oil
property) to the north of Parcel 1, which could potentially impact groundwater on Parcel 2, and
• Chemicals historically used at the site as fumigants for tobacco.
1.2 Scope of Work
To assess the above areas of concern, Duncklee & Dunham developed a scope of work that included the
installation of soil borings and groundwater monitoring wells to collect samples for analytical laboratory
testing. To facilitate this, Duncklee & Dunham originally proposed to advance ten soil borings.
However, a subsequent fire at the facility made access to the fuel oil AST adjacent to the smokestack
inaccessible (identified as Soil Boring #9 in the proposal).
Six soil borings were advanced at the site and
converted to temporary groundwater monitoring
wells. Each well, constructed of one -inch
diameter PVC well screen and pipe, was
developed and sampled upon completion.
Collected groundwater samples were shipped to
the laboratory for analysis.
The soil and groundwater data obtained have
been used to evaluate the RECs identified in the
Phase I ESA and to provide ample information to
allow the preparation of a suitable Brownfields
Agreement (BFA) application to the NCBP.
2 Methodology
This section presents the soil boring and
monitoring well installation methods used to
collect soil and groundwater samples. The
results from the independent analytical
laboratory were reviewed and used to prepare the
conclusions presented.
2.1 Soil Assessment
On May 27, 2008, a direct push technology (DPT) drill rig was mobilized to the site by Brown
Environmental to advance the soil borings and install temporary groundwater monitoring wells. Soil
borings were advanced in the vicinity of RECs identified in the Phase I ESA. Soil characteristics were
logged visually during the installation of the soil borings.
DUNCKLEE & DUNHAM, P.C.

Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
Greenville, North Carolina
October 6, 2009
Page 3 of 8
A summary of the soil borings and samples collected is included in the following table (see Appendix A
for soil boring log information). See Figure 3 for the location and analytical results obtained from these
soil borings.
Sample
Soil
Soil Sample Laboratory
Purpose of Boring
Depth
Boring ID
Analysis
(ft b s)
SB-1
Evaluate stained soil and stressed
SVOCs, VOCs, HSL Metals, Oil and
0-1
vegetation in Parcel 2
Grease, TPH DRO and TPH GRO
S13-2
Assess impact from disposed steel tank
TPH DRO and GRO
0-1
on Parcel 2
SB-3
Assess impact from former gas tank at
TPH DRO and GRO
3-4
NW property corner of Parcel 1
S13-4
Assess impact from fuel oil tanks
TPH DRO and GRO
14-15
SB-5
Assess impact from activities in metal
TPH DRO and GRO
0-1
shed on Parcel 2
SB-6
Assess impact from activities in metal
TPH DRO and GRO
0-1
shed and brick garage on Parcel 2
SB-7
Assess impact from activities in metal
TPH DRO and GRO
0-1
shed and brick garage on Parcel 2
Assess impact from the presumed
S13-8
former presence of pad -mounted
SVOCs, VOC, HSL Metals, and PCBs
1-2
electrical transformers
SB-10
Characterize soil near rail spur and
SVOCs, VOCs, and HSL Metals
0-1
loading dock area of Parcel 1
SB-11
Characterize soil in the south portion of
SVOCs, VOCs, and HSL Metals
0-1
Parcel 2
SB-16
Assess impact to soil from gas UST
TPH DRO and GRO
10-11
SB-17
Assess impact to soil from boiler room
SVOCs, VOCs, and HSL Metals
0-1
and offsite concerns
SVOCs — Semivolatile organic compounds according to EPA Method 8270
VOCs — Volatile organic compounds according to EPA Method 8260
HSL Metals — Hazardous substance list metals according to EPA Method 3010
Oil and Grease - According to EPA Method 9071
TPHDRO and GRO — Total petroleum hydrocarbons diesel range organics and gasoline range organics
according to EPA Method 8015
PCBs - Polychlorinated biphenyls according to EPA Method 8082
bgs - below ground surface
DUNCKLEE & DUNHAM, P.C.

Z2 Groundwater Assessment
On May 27 and 28, 2008, six
temporary monitoring wells (SB-
12 through SB-17) were installed
at the site by Brown
Environmental under the
supervision of a Duncklee &
Dunham geologist (see Figure 3,
Appendix A, and table to right).
The wells were constructed using
one -inch diameter PVC casing
and screen. The geologist was
present to supervise the drilling,
log the boreholes, and direct the
construction of the wells.
Upon completion, the wells were
developed by removing water
from the well using a peristaltic
pump with new polyethylene
tubing changed between wells.
Well development continued
until turbidity of the water was
such that sediment was no longer
visible.
Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
Greenville, North Carolina
October 6, 2009
Page 4 of 8
Well
Purpose of Well
Groundwater Sample
ID
Laboratory Analysis
Evaluate impact from plant
VOCs, SVOCs, HSL Metals,
SB-12
operations and potential
Chloropicrin and Methyl
impact from Texaco property
Bromide
to north of Parcel 1
Assess impact to
VOCs, SVOCs, HSL Metals,
SB-13
groundwater from plant
Chloropicrin and Methyl
operations
Bromide
Assess impact to
SB-14
groundwater from offsite
VOCs, SVOCs, and HSL Metals
concerns
Characterize groundwater on
SB-15
Parcel 2 and evaluate impact
VOCs, SVOCs, and HSL Metals
form Texaco property
VOCs with IPE and MTBE
SB-16
Assess impact of gasoline
according to EPA Method 6210,
UST
Lead (Method 200.7), and
MADEP VPH
Assess impact to
SB-17
groundwater from activities
VOCs, SVOCs, and HSL Metals
near boiler room and offsite
concerns
VOCs according to EPA Method 8260
SVOCs according to EPA Method 8270
HSL Metals according to EPA Method 6010
Chloropicrin and methyl bromide according to EPA Method 8260
To determine the direction of
ground water flow, each well was surveyed to determine the relative elevations of the measuring points
(ground surface). Elevations were referenced to an assumed elevation of 100.00 feet established at the
site.
The wells were then purged of at least three volumes to remove stagnant water so that a representative
groundwater sample could be collected. A low -flow peristaltic pump with new polyethylene tubing
changed between wells was used to purge and withdraw the sample from each well.
The water samples were collected in laboratory -provided containers, labeled, logged onto a chain -of -
custody form, and transported to the laboratory in an insulated cooler with ice. The groundwater samples
were submitted to Pace Analytical Laboratories in Huntersville, North Carolina, and analyzed for
constituents of concern using the analytical tests identified above (see Appendix B).
Prior to sampling, water levels were measured in each monitoring well using an electric water level probe
decontaminated between readings. The water level elevations were used to create a shallow groundwater
contour map for the site (see Figure 4).
DUNCKLEE & DUNHAM, P.C.

Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
Greenville, North Carolina
October 6, 2009
Page 5 of 8
3 Findings
3.1 Soil Assessment
With the exception of SB-1 and SB-16, observations of soil samples characterized from each of the soil
borings advanced did not indicate the obvious presence of petroleum or hazardous substances. No
staining or odors were observed in the soil. Soil sample SB-1, collected from the ground surface at the
stained soil and stressed vegetation location in Parcel 2, did contain odors indicative of petroleum
hydrocarbons. Slight petroleum odors were also detected in the soil sample collected from a depth of 10-
11 feet below bgs in soil boring SB-16.
The observed petroleum impact in SB-16 prompted a second boring immediately south of the gasoline
UST. The second boring was extended to a depth of 24 feet bgs with no evidence of petroleum impact.
Therefore, only the soil sample from boring SB-16 at a depth of 10-11 feet bgs was submitted for
laboratory analysis.
As summarized in Table 1, oil and grease was detected in soil sample SB-1 at a concentration of 555
mg/kg which exceeds the non -UST petroleum release action level of 40 mg/kg. TPH DRO concentrations
were detected above the non -UST petroleum release action level of 40 mg/kg in soil samples SB-1 (483
mg/kg) and SB-16 (377 mg/kg). Finally, the concentration of TPH GRO was detected above the non -
UST petroleum release action level of 10 mg/kg in soil sample SB-16 (914 mg/kg).
Non -petroleum related soil sample analytical testing results were compared to the Inactive Hazardous
Sites Branch Health -Based Soil Remediation Goals (IHSB RGs),(DENR, 2008, Hazardous Sites Branch
Health -Based Soil Renmediation Goals, Registered Environmental Consultant Program Implementation
Guidance: Division of Waste Management, Superfund Section, IHSB, August) (see Table 1). The
concentration of arsenic was detected at concentrations of 32.0, 59.8, and 8.8 mg/kg (commonly referred
to as parts per million in soil samples SB-5, SB-8 and SB-17, which exceeds the IHSB RG concentration
of 4.4 mg/kg. In SB-17, lead was detected at 680 mg/kg, above the IHSB RG of 400 mg/kg, but below
the EPA regional screening level of 800 mg/kg for industrial use.
The remaining soil samples did not have concentration of analytes either above the practical quantitation
limit or greater than their respective IHSB RG level (see Table 1). A copy of the laboratory analytical
report is included as Appendix B.
3.2 Groundwater Assessment
3.2.1 Groundwater Analytical Testing
The concentrations of analytes detected in the groundwater were compared to the North Carolina
groundwater standard (2L Standards, 15 NCAC 2L.0202). The data are summarized in Table 2 and
documented in Appendix B.
Arsenic was detected in groundwater sample SB-15 at a concentration of 90.4 µg/L; exceeding the 2L
Standard of 50 µg/L (analogous to parts per billion). Manganese, a common naturally occurring
inorganic compound, was detected in samples SB-13 (65.4 µg/L) and SB-15 (99.3 µg/L), at
DUNCKLEE & DUNHAM, P.C.

Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
Greenville, North Carolina
October 6, 2009
Page 6 of 8
concentrations that exceed the 2L Standard of 50 µg/L. The remaining samples collected either did not
have concentrations of analytes above the practical quantitation limit or that exceed 2L Standards.
3.2.2 Groundwater Flow Direction
Groundwater elevations included in the table below were used to construct the groundwater contour map
(see Figure 4). The contour lines indicate groundwater in the northern portion of the subject site flows
towards the southeast, while the groundwater in the southern portion of the site flows towards the
northeast. Using the groundwater contour lines in Figure 4 and the location of the Tar River relative to
the subject site, it appears the overall direction of regional groundwater flow would be towards the east,
northeast.
The data indicate wells SB-17 and
SB-14 were located in hydraulically
downgradient directions of off -site
concerns to the south and southwest
of the subject site. The placement of
wells SB-12 and SB-15 are present in
hydraulically downgradient directions
of the Texas Oil property. Wells SB-
13 and SB-16 appear hydraulically
downgradient of the main Imperial
Tobacco facility.
Well
ID
Ground
Elevation
Depth To
Groundwater
(ft.b s)
Groundwater
Elevation
Screen
Interval
(ft bgs)
SB-12
101.23
4.89
96.34
14-24
SB-13
101.59
16.75
84.84
14-24
SB-14
96.50
6.94
89.56
14-24
SB-15
105.78
15.96
89.82
14-24
SB-16
102.49
17.42
85.07
14-24
SB-17
102.07
15.00
87.07
9-19
4 Conclusions and Recommendations
Based on the Phase II assessment results, Duncklee & Dunham concludes the following:
The area of stained soil and stressed vegetation on Parcel 2 was evaluated through the installation
of a soil boring and the collection of soil sample SB-1. The analytical results indicate the
presence of low levels of TPH DRO and oil and grease. Therefore, it appears the soil staining
and stressed vegetation is a result of a surface spill of oil. Observations made of soil during the
installation of the boring did not indicate the presence of staining or petroleum odors below one
foot bgs. With a stained area of approximately 10 feet by 12 feet, it appears there is
approximately four cubic yards of impacted soil. This volume of soil should be removed and
disposed off -site at a licensed disposal facility.
During the installation of a soil boring and temporary monitoring well SB-16, adjacent to the
gasoline UST, petroleum odors were detected from 10 to 11 feet bgs. A soil sample collected
from this interval revealed the presence of TPH DRO and GRO above action levels, indicating a
release from this UST has occurred. Because the boring was extended to a depth of 24 feet bgs,
and petroleum odors or staining were not observed in the soil except for the 10 to 11 ft bgs layer,
the extent of the petroleum release appears limited.
There is an exclusion related to UST releases in the NCBP statute. UST contamination is
normally addressed in the BFA by referring the prospective developer (PD) to pursue closure of
DUNCKLEE & DUNHAM, P.C.

Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
Greenville, North Carolina
October 6, 2009
Page 7 of 8
USTs and contamination related to USTs under the oversight of the UST Section until a copy of a
no further action is received. The removal of the UST and a Limited Site Assessment under the
UST guidelines would be the next step towards closure of this area of concern under the UST
Section requirements. This work can be conducted by the PD prior to issuance of the BFA, or it
will become a requirement of the agreement.
Groundwater sample SB-16, collected from the temporary well installed in this boring, did not
indicate the presence of petroleum related constituents above the 2L Standard. This data
indicates that groundwater has not been impacted to a level that would constitute additional
groundwater assessment or remediation.
Based on the data available at this time, Duncklee & Dunham believes the petroleum impacted
soil around the gasoline UST can be readily removed during the removal of the tank. With the
low levels of dissolved gasoline compounds found in the well immediately adjacent to the tank,
we believe the UST can be closed according to the DENR guidelines without long term
monitoring or groundwater cleanup.
Arsenic was detected in soil samples SB-5, SB-8 and SB-17 at concentrations (8.8 to 59.8 mg/kg)
that exceed the IHSB RG of 4.4 mg/kg. Other samples analyzed for this metal revealed
concentrations between 1.2 and 2.3 mg/kg. Therefore, the concentration of arsenic detected in
SB-5, SB-8, and SB-17 appears to be elevated above what would be considered background or
naturally occurring concentrations. However, we believe the presence of arsenic in the soil can
be effectively managed without remediation through the use of a BFA.
Lead was detected in SB-17 at 680 mg/kg, exceeding the IHSB RG of 400 mg/kg at a depth of 0
to 1 feet bgs. The analytical result for lead in the groundwater from this location was not above
the detection limit of 5 µg/L, so it is not believed the soil lead impact is a source for groundwater
contamination.
As much of this property is planned for future use as an East Carolina University parking lot, we
believe low to moderate levels of surficial lead -contaminated soil can be managed by an asphalt
cap. It should be noted that the level of contamination is below EPA's level for industrial use of
800 mg/kg. Industrial use would allow direct exposure up to the 800 mg/kg level for a worker for
up to 40 hours a week, 50 weeks a year for 30 years. Capping of this area should be adequate
protection for any parking area users, and other institutional or engineering controls can be
written into the BFA if high -density residential units or landscaped areas were to be constructed
in this particular vicinity.
Analytical results of groundwater samples collected from temporary wells SB-13, SB-14, and SB-
15 revealed the presence of manganese at concentrations that exceed the North Carolina 2L
Standard. Groundwater samples SB-12, SB-14 and SB-17 also revealed the presence of
manganese but at concentrations that are below the 2L Standard.. With no known usage of
groundwater in the area and the lack of surface water bodies, we believe the risk of manganese in
the groundwater at concentrations that exceed the 2L Standard of 50 µg/L can be managed
without remediation through a BFA.
The presence of arsenic in soil and groundwater, lead in surficial soil, petroleum products
resulting from a surface spill, and manganese in the groundwater should provide adequate
conditions for this site to be accepted into the NCBP. Since the issuance of the original report, an
application to the NCBP was subsequently submitted by Atlantic Ave. Holding Co., LLC (AAH)
DUNCKLEE & DUNHAM, P.C.

Revised Phase II Environmental Site Assessment
Former Imperial Tobacco Facility
Greenville, North Carolina
October 6, 2009
Page 8 of 8
and this site was granted eligibility into the brownfields program, with the next goal being the
establishment of a BFA with the agency.
A significant benefit of receiving a BFA is to have specific work -to -be -performed requirements
outlined in the agreement that utilize risk -based cleanup goals that are dependent on the intended
end use. Furthermore, a covenant -not -to -sue from DENR will be effective if the prospective
developer and future owners of the property adhere to the agreement's requirements and land use
restrictions. Also, a property tax exclusion will be allowed for the first five years after
redevelopment is completed based on the incremental increase to the property tax value.
On the other hand, in the absence of pursuing a BFA under the NCBP, the concentration of
constituents in the groundwater that exceed the 2L Standards are reportable to the IHSB and can
be subject to further enforcement action, most likely under the Registered Environmental
Consultant (REC) Program.
Clearly, the NCBP is a more cost-effective way to achieve closure while ensuring the site suitable
for the intended re -use. On December 31, 2008, the NCBP issued a satisfactory eligibility
determination for the property to AAH. The next step in the process is for the NCBP to prepare a
draft BFA that will stipulate any further assessment or remedial efforts, which may include
institutional and engineering controls, required to make the site suitable for the intended
development while being protective to human health and the environment.
Closure of the gasoline UST under the UST Section is an expected work -to -be -performed
requirement of the BFA. Land use restrictions will then be recorded along with a plat map that
has additional information on it as requested by the NCBP. After negotiations, the final BFA has
public notification requirements that must be met, including providing a copy of the summary
Notice of Intent to all contiguous property owners (per House Bill 1288 passed in June 2009).
The required work to be performed can be completed either prior to or after the final BFA is
signed. Duncklee & Dunham can fully assist you in navigating through this BFA process.
Z DUNCKLEE & DUNHAM, P.C.

Figures

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`
°' =tea►,
r-
UAW
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i
-
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k
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Source Map: U.S. G.S. Greenville 7.5-Minute
DUNCKLEE & DUNHAM, P.C. Approximate Scale:
ENVIRONMENTAL CONSULTANTS I" = 2000'
511 KEISLER DRIVE - SUITE 102 Figure:
rowe) CARY, NORTH CAROLINA 27518
Title:
Project:
USGS Topographic Map
Former Imperial Tobacco Facility
Greenville, North Carolina

Figure 2: Site Map
Former Imperial Tobacco Facility
Greenville, North Carolina
.-_
Area pf�Stressed Vegetatign
F
Steel Tank r
- '`
�;
Fu 1 Oil Tanks �j
Wj
Gasoline UST 4
Transformer Pad
Boi 'r Room
Fuel Oil AST
0 75 150
REC
Parcel 1
Parcel 2
- Parcel 3
- Parcel 4
,.
300 450 600
Feet
DUNCKLEE & DUNHAM, P.C.
ENVIRONMENTAL CONSULTANTS
511 KEISLER DRIVE - SUITE 102
CARY NORTH CAROLINA 27518

Figure 3: Soil Boring and Monitoring Well Location Map
With Analytical Results
Former Imperial Tobacco Facility
("TrPPnvillP Nnrth Cnrnlinn
^•. t.J - -
SB-15 Mn: 99.3 ppb*
O & G: 555 ppm** - SB-1+r'
TPH/DRO: 479 ppm* --♦o ?�" 1 t i
SB-2
o
SB-12 -_ T
Mn: 65.4 ppb*
9$-401,
r gal SB-5 '
0
B-13 As: 32 ppb**
TPH/DRO: 377 ppm* oSB-7 -'
TPH/GRO: 776 ppm* oSB-6. "-
SB-10 SB-16
it 0
SB-8
� o As: 59.8 ppb**
Orpp ��$ � � r -
} SB-17
�r. SB-11
• Soil Boring Locations 0 75 150
O Temporary Monitoring Well Locations
O Soil Boring and Temporary Monitoring Well Locations
* = Ground Water Analytical Results Exceeding 2L Standard
** = Soil Analytical Results Exceeding IHSB RG t:>
300 450 600
Feet
DUNCKLEE & DUNHAM, P.C.
ENVIRONMENTAL CONSULTANTS
511 KEISLER DRIVE - SUITE 102
CARY, 14ORTH CAROLINA 27518

Figure 4: Ground Water Contour Map
Former Imperial Tobacco Facility
Greenville, North Carolina
96.34
95
r 94
- 93
92 ,
t
85.07 -
- - t 87
_ 87.07'71
i 88 Y
i
89.54 - �x
• ►.
0 75 150 300 450 600
Symbols on Map Feet
84.0 Temporary Monitoring Well Locations
and Ground Water Elevations
DUN CKLEE & DUNHAM, P.C.
Ground Water Elevation Contour ENVIRONMENTAL CONSULTANTS
511 KEISLER DRIVE - SUITE 102
Direction of Flow CARY, NORTH CAROLINA 27518
88 Relative Elevation to Top of Temporary Benchmark

Tables

Table: 1 Soil Analytical Results
Site: Former Imperial Tobacco Facility
Total Petroleum
EPA
Hydrocarbons EPA
Semivolatile Organic Compounds EPA
Volatile Organic Compounds
Method
Method 8015
Analytical Method
Metals 3030C/200.7
Method 8270
EPA Method 8260
9071
Modified
y
U
U
N
c03
Contaminant of Concern
O
Y
9i
-5
on
E
YY
Y
c
o
°
Q
a�
Sample LD
Date Collected
Depth (ft. bgs)
yl`
=1
UU
�U
z
�,
H
N
z
a
H
H
¢
O
Q
U
SB-1
5/27/2008
0-1
ND
1.5
ND
ND
2.8
4.6
79.9
24.5
0.19
0.92
0.8
ND
ND
45.2
ND
ND
ND
ND
ND
ND
ND
555
483
ND
SB-2
5/27/2008
0-1
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
ND
ND
SB-3
5/28/2008
3-4
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
ND
ND
SB-4
5/28/2008
14-15
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
33.1
ND
SB-5
5/28/2008
0-1
ND
32
ND
1.8
5.3
5.6
49.8
47.9
0.075
1.7
ND
ND
ND
445
ND
ND
ND
ND
ND
ND
ND
NA
NA
NA
SB-6
5/28/2008
0-1
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
110
ND
SB-7
5/27/2008
0-1
ND
1.2
ND
ND
3.4
4
62.4
37.7
0.063
2.9
ND
ND
ND
115
ND
ND
ND
ND
ND
ND
0.155
NA
NA
NA
SB-8
5/28/2008
1-2
ND
59.8
ND
ND
1.5
0.62
2.5
8.6
0.03
0.56
ND
ND
ND
10.8
ND
ND
ND
ND
ND
ND
ND
NA
NA
NA
SB-10
5/28/2008
0-1
ND
2.3
ND
0.11
2.1
6.1
28.1
23.8
0.053
1
ND
ND
ND
39.3
ND
ND
ND
ND
ND
ND
ND
NA
NA
NA
SB-11
5/27/2008
0-1
ND
2.1
ND
0.056
1.6
17.1
28.4
18.3
0.12
1.8
ND
ND
ND
64.4
ND
ND
ND
ND
ND
ND
0.197
NA
NA
NA
SB-16
5/27/2008
10-11
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
377
914
SB-17
5/28/2008
0-1
1.8
8.8
ND
1.5
12.4
58.9
680
95.5
0.21
7.7
ND
ND
ND
444
0.689
0.648
1.05
0.801
0.026
0.425
1 .226
NA
NA
NA
IHSB Remediation Goals
1
1 6.2
1 4.4
1 30
1 7.4
1 44
1 620
1 400
1 360
1 4.6
1 320
1 78
78
1.04
1 4600
1 22
1 62
11.2
1 NRG
1 0.053
0.48
1 2800
40
40
10
All Units in mg/kg
ND = Not detected at a concentration above the method detection limit
NA = Not Analyzed for this Compound
Bold indicated results greater than the IHSB Remediation Goals
NRG = No RG
Table: 2 Ground Water Analytical Results
Site: Former Imperial Tobacco Facility
Semivolatile Organic
Volatile Organic
Analytical Method
Compounds EPA
Compounds EPA
MADEP
Metals 3030C/200.7
Method 8270
Method 8260
VPH
Contaminant
of Concern
E
E
E
2
Screen Interval
o
a
q
,.U,
U
U
O
V
Sample I.D
Date Collected
(ft. bgs)
_
ca
U
U
>
U
N
SB-12
5/28/2008
14-24
ND
ND
ND
ND
8.8
ND
5.8
20.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
NA
SB-13
5/28/2008
14-24
ND
ND
ND
ND
ND
ND
ND
65.4
ND
9.9
11.5
ND
ND
ND
ND
1.8
NA
NA
SB-14
5/28/2008
14-24
ND
ND
ND
ND
ND
ND
ND
23.1
ND
ND
ND
ND
ND
ND
ND
ND
ND
NA
SB-15
5/28/2008
14-24
ND
90.4
ND
ND
5.5
ND
ND
99.3
ND
9.4
ND
ND
ND
22.1
ND
ND
ND
NA
SB-16
5/28/2008
14-24
NA
NA
NA
NA
NA
NA
5.8
NA
ND
ND
ND
ND
ND
ND
NA
1.4
0.95
ND
SB-17
5/28/2008
1 9-19
1 ND
ND
ND
ND
ND
ND
ND
6.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
NA
2L Standard
I
1 100*
50
1.0*
1.75
50
1000
15
50
1.05
100
50
17.5
10.0*
1050
70
350
All ground water results in ug/L, parts per billion * - 2L Standard Equal to the Method Detection Limit Bold indicated results greater than the North Carolina 2L Ground Water Standard
ND = Not detected at a concentration above the method detection limit NA = Not Analyzed for this Compound
P:\Atlantic Ave. Holding Co., LLC - 200817\Reports\Revised Phase 11 Report\REV 2009-9-25 Table 1 and 2 Soil and Ground Water Analytical Results
Page 1

Appendix A

Boring /Well Construction Log
Duncklee & Dunham, P.C.
I. D. Number
SB-3
Purpose
Gasoline Tank Area
Project Name
Imperial Tobacco
Contractor
Brown Environmental
Project No.
200817
Registration No.
3427
Geologist
Harold Thurston
Driller
Burt Brown
Start Date
512812008 Complete Date
512812008 Equipment
Geoprobe ® 54DT
Drilling Method Geoprobe®
Comments In vicinity of gas tank on Sanborn map
Sample collected at 3 - 4' bgs. Boring extended to 16' depth with no evidence of contamination.
FID / PID
(ppm)
@ Depth (ft.)
Well Construction
Information
Depth
From - To
Soil / Rock Description / Comments
Borehole Diameter
0 - 2'
Fill material, gravel and sand mix
Riser Type
Diameter
2 - 7'
Tan and gray fine-grained sand to silt
Screen Type
Diameter
7 - 9'
Tan clayey fine-grained sand
Riser Interval
Screen Interval
9 - 15.5'
Light gray stiff clay, moist
Slot Size
Grout Type
15.5 -16'
Dark gray clay.
Interval
No petroleum odors detected.
Bentonite Type
Bottom of boring 16'
Interval
Filter Pack
Interval
Total Depth
R.P. Elevation
Datum
Water Level Information
Date
W.L. Below R.P.
R.P. = Reference Point W.L. = Water Level TBM — Temporary Benchmark MSL = Mean Sea Level

Boring /Well Construction Log
Duncklee & Dunham, P.C.
I. D. Number
SB-4
Purpose
Fuel Oil Tanks Area
Project Name
Imperial Tobacco
Contractor
Brown Environmental
Project No.
200817
Registration No.
3427
Geologist
Harold Thurston
Driller
Burt Brown
Start Date
512812008 Complete Date
512812008 Equipment
Geoprobe® 54DT
Drilling Method Geoprobe®
Comments Soil boring near fuel oil tanks
Sample collected 14 -15' (just above water table). No evidence of petroleum contamination..
16' depth of boring sufficient depth to encounter bottom of a 25, 000-gallon UST.
FID / PID
(ppm)
@ Depth (ft.)
Well Construction
Information
Depth
From - To
Soil / Rock Description / Comments
Borehole Diameter
0 - 3'
Fill material - rocks, sand, asphalt pieces
Riser Type
Diameter
3 - 16'
Mottled tan and red brown clay, stiff, moist
Screen Type
Wet at 16'
Diameter
Riser Interval
Sample collected at 14-15' bgs
Screen Interval
Bottom of boring 16'
Slot Size
Grout Type
Interval
Bentonite Type
Interval
Filter Pack
Interval
Total Depth
R.P. Elevation
Datum
Water Level Information
Date
W.L. Below R.P.
R.P. = Reference Point W.L. = Water Level TBM — Temporary Benchmark MSL = Mean Sea Level

Boring /Well Construction Log
Duncklee & Dunham, P.C.
I. D. Number
GP-13
Purpose
Temporary Monitoring Well
Project Name
Imperial Tobacco
Contractor
Brown Environmental
Project No.
200817
Registration No.
3427
Geologist
Harold Thurston
Driller
Burt Brown
Start Date
512712009 Complete Date
512712009 Equipment
Geoprobe® 54DT
Drilling Method Geoprobe®
Comments Soil core, then push 3-1/4"pipe to install well inside rods with a ground water sand pack.
FID / PID
(ppm)
@ Depth (ft.)
Well Construction
Information
Depth
From - To
Soil / Rock Description / Comments
Borehole Diameter
0 - 0.5'
Grass/topsoil
Riser Type PVC
Diameter I "
0.5 - 6'
Gray fine sand
Screen Type PVC
moist
Diameter I"
Riser Interval 0 - 9 'bgs
6 -19.5'
Reddish brown fine- to medium -grained sand.
Screen Interval 9 - 19' bgs
Some clay, more moisture.
Slot Size 0.011,
Drillers indicate stiff at 7, wet at 13' bgs
Grout Type neat
Clay lens 2" thick at 15'
Interval
More water 16 - 20'
Bentonite Type chips
19.5 - 20'
Medium to coarse sand, saturated.
Interval
Bottom of boring at 20'
Filter Pack sand
Gray clay in sample in bottom 2" of boring
Interval
Total Depth 20'
R.P. Elevation N/A
Datum ground surface
Water Level Information
Date
W.L. Below R.P.
5/28/2008
16. 7' bgs
R.P. = Reference Point W.L. = Water Level TBM — Temporary Benchmark MSL = Mean Sea Level

Boring /Well Construction Log
Duncklee & Dunham, P.C.
I. D. Number GP-15 Purpose Temporary Monitoring Well
Project Name
Imperial Tobacco
Contractor
Brown Environmental
Project No.
200817
Registration No.
3427
Geologist
Harold Thurston
Driller
Burt Brown
Start Date
512712008 Complete Date
512712009 Equipment
Geoprobe® 54DT
Drilling Method Geoprobe®
Comments Could not push 3-114" rods. Installed well in bare hole because hole stayed open in the clay
FID / PID
(ppm)
@ Depth (ft.)
Well Construction
Information
Depth
From - To
Soil / Rock Description / Comments
Borehole Diameter
0 - 0.5'
Grass/topsoil
Riser Type PVC
Diameter I "
0.5 - 6'
Tan fine-grained sand
Screen Type PVC
Diameter I "
6 - 8'
Tan clayey fine-grained sand
Riser Interval 0 -14'
Screen Interval 14 - 24'
8 - 18'
Tan with reddish brown silt mottling with stiff clay
Slot Size 0.01 "
Moist
Grout Type Neat
18 - 24'
Dark gray to black stiff clay, saturated. Sticky clay.
Interval
Bentonite Type Chips
Bottom of boring at 24' bgs
Interval
Filter Pack Sand
Interval
Total Depth 24'
R.P. Elevation N/A
Datum ground surface
Water Level Information
Date
W.L. Below R.P.
512712008
17.8' bgs
R.P. = Reference Point W.L. = Water Level TBM= Temporary Benchmark MSL = Mean Sea Level

Boring /Well Construction Log
I. D. Number
Project Name
Project No.
Geologist
Start Date
GP-16
Imperial Tobacco
200817
Harold Thurston
512712008 Complete Date
Purpose
Contractor
Registration No.
Driller
512712008 Equipment
Duncklee & Dunham, P.C.
Monitoring Well
Brown Environmental
3427
Burt Brown
Geoprobe® 54DT
Drilling Method Geoprobe®
Comments Soil sample GP-16 collected from 10-11' bgs where odors detected. No petroleum odors from boring
placed on south side of UST - mostly sand to 20'bgs. Collected soil sample from boring placed in grass
on north side of UST. Well installed in north boring.
FID / PID
(ppm)
@ Depth (ft.)
Well Construction
Information
Depth
From - To
Soil / Rock Description / Comments
Borehole Diameter
0 - 0.5'
Grass/topsoil
Riser Type PVC
Diameter I "
0.5 - 3'
Gray fine-grained sand. Moist.
Screen Type PVC
Diameter I "
3 - 6'
Reddish brown clayey fine-grained sand, hard.
Riser Interval 0 -14' bgs
Screen Interval 14 -24' bgs
6 - 10'
gray//white fine- to medium -grained sand
Slot Size 0.01 "
Grout Type neat
10 - 11,
Gray clay, petroleum odors
Interval
Bentonite Type chips
11 - 15'
White fine- to med-grained sand. Moist.
Interval
Filter Pack sand
15 - 19'
Reddish -brown medium- to coarse -grained sand; wet
Interval
Total Depth 24'
19 - 24'
Gray fine- to coarse -grained sand. Saturated at 20'
R.P. Elevation N/A
Datum ground surface
Bottom of boring at 24' bgs
Water Level Information
Date
W.L. Below R.P.
512712008
17.35' bgs
R.P. = Reference Point W.L. = Water Level TBM= Temporary Benchmark MSL = Mean Sea Level

FIELD NOTES WITH DESCRIPTIONS OF SAMPLE LOCATIONS NOT DESCRIBED BORING LOGS
May 27, 2008
13:45 - Collected sample GP-1 from stained area with stressed vegetation. Collected from 0 - 1' depth in area of staining
approximately 10 x 12'
14:00 - Collected soil sample GP-2 adjacent to tank. Probed three areas. No odors. Collected sample from 0 - 1' bgs next to bung
hole of tank (empty tank sitting on ground surface). No holes in tank.
16:30 - Collected soil sample GP -I I from 0 - F bgs. Soil was sandy with no odors.
17:00 - Soil sample GP-7 collected from 0 - l' bgs. Fill debris - brick, concrete, glass bottles in soil.
May 28, 2008
09:30 - Soil sample SB-6 collected 0 - l' bgs. Soil boring went to 8 feet bgs.
09:45 - Brown re -installed SB-13 to a depth of 24' rather than previous 19' depth.
10:00 - Installed temporary monitoring well SB-14 to depth of 24' bgs. Screened 14 - 24' bgs with sand pack. Soil: clayey/sand.
Dark gray clay layer detected at about 12' bgs.
11:00 - SB-17 - Soil sample and well installation. Soil boring to 20' bgs. No evidence of contamination. SB-17 MW installed to
19' bgs. Screened 9 - 19' with sand back; riser 1-9'. Soil sample SB-17 collected at 11:30 0 - 11 bgs. Well developed. Water was
clear. Depth to water 15' bgs.
13:00 - SB-10 on west side of plant. Soil sample collected at 0 - l' bgs. Soil boring was advanced to 8' bgs. No evidence of
contamination.
15:00 - SB-8 collected adjacent to transformer pad at 1-2' bgs in sandy soil. No evidence of contamination.
15:45 - Hand auger north of metal shed to collect soil sample SB-5 from 1 -2' bgs. No evidence of contamination. Empty motor oil
containers near boring location. Highly overgrown with vegetation.

Appendix B

aceAnalytical
—pacelabs.com
June 18, 2008
Mr. Harold Thurston
Duncklee & Dunham
P.O. Box 33366
Raleigh, NC 27636
RE: Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Dear Mr. Thurston:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2008. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 97

acmnalytical
www.pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Charlotte Certification IDs
Florida/NELAP Certification Number: E87627
Kansas Certification Number: E-10364
Louisiana/LELAP Certification Number: 04034
North Carolina Drinking Water Certification Number: 37706
North Carolina Wastewater Certification Number: 12
Asheville Certification IDs
Florida/NELAP Certification Number: E87648
Louisiana/LELAP Certification Number: 03095
New Jersey Certification Number: NC011
North Carolina Drinking Water Certification Number: 37712
North Carolina Wastewater Certification Number: 40
North Carolina Bioassay Certification Number: 9
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
North Carolina Field Services Certification Number: 5342
South Carolina Certification Number: 990060001
South Carolina Bioassay Certification Number: 990060003
Tennessee Certification Number: 04010
Virginia Certification Number: 00213
Pennsylvania Certification Number: 68-03578
South Carolina Certification Number: 99030001
South Carolina Bioassay Certification Number: 99030002
Tennessee Certification Number: 2980
Virginia Certification Number: 00072
Eden Certification IDs
North Carolina Drinking Water Certification Number: 37738 North Carolina Wastewater Certification Number: 633
Virginia Drinking Water Certification Number: 00424
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
1 � 9p9
c
�®x
Page 2 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-1 Lab ID: 9220393001 Collected: 05/27/08 13:45 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components 483 mg/kg 20.2 4 06/02/08 00:00 06/05/08 17:39 68334-30-5
n-Pentacosane (S) 0 % 50-135 4 06/02/08 00:00 06/05/08 17:39 629-99-2 S4
9071 Oil and Grease Analytical Method: 9071 B ASE Preparation Method: 9071 B ASE
Oil and Grease 555 mg/kg 169 1 06/04/08 00:00 06/04/08 00:00
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 5.9 1 06/02/08 15:52 06/03/08 01:55 8006-61-9
4-Bromofluorobenzene (S) 89 % 50-135 1 06/02/08 15:52 06/03/08 01:55 460-00-4
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony
ND mg/kg
0.39
1
06/02/08 15:35
06/02/08 23:41
7440-36-0
Arsenic
1.5 mg/kg
0.39
1
06/02/08 15:35
06/02/08 23:41
7440-38-2
Beryllium
ND mg/kg
0.079
1
06/02/08 15:35
06/02/08 23:41
7440-41-7
Cadmium
ND mg/kg
0.079
1
06/02/08 15:35
06/02/08 23:41
7440-43-9
Chromium
2.8 mg/kg
0.39
1
06/02/08 15:35
06/02/08 23:41
7440-47-3
Copper
4.6 mg/kg
0.39
1
06/02/08 15:35
06/02/08 23:41
7440-50-8
Lead
79.9 mg/kg
0.39
1
06/02/08 15:35
06/02/08 23:41
7439-92-1
Manganese
24.5 mg/kg
0.39
1
06/02/08 15:35
06/02/08 23:41
7439-96-5
Nickel
0.92 mg/kg
0.39
1
06/02/08 15:35
06/02/08 23:41
7440-02-0
Selenium
0.80 mg/kg
0.79
1
06/02/08 15:35
06/02/08 23:41
7782-49-2
Silver
ND mg/kg
0.39
1
06/02/08 15:35
06/02/08 23:41
7440-22-4
Thallium
ND mg/kg
0.79
1
06/02/08 15:35
06/02/08 23:41
7440-28-0
Zinc
45.2 mg/kg
0.79
1
06/02/08 15:35
06/02/08 23:41
7440-66-6
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
0.19 mg/kg
0.0078
2
06/05/0811:30
06/05/08 18:16
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
83-32-9
Acenaphthylene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
208-96-8
Aniline
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
62-53-3
Anthracene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
120-12-7
Benzo(a)anthracene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
56-55-3
Benzo(a)pyrene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
50-32-8
Benzo(b)fluoranthene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
191-24-2
Benzo(k)fluoranthene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
207-08-9
Benzoic acid
ND ug/kg
1670
1
06/02/08 00:00
06/10/08 23:09
65-85-0
Benzyl alcohol
ND ug/kg
666
1
06/02/08 00:00
06/10/08 23:09
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
101-55-3
Butylbenzylphthalate
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
85-68-7
4-Chloro-3-methyl phenol
ND ug/kg
666
1
06/02/08 00:00
06/10/08 23:09
59-50-7
4-Chloroaniline
ND ug/kg
1670
1
06/02/08 00:00
06/10/08 23:09
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
111-91-1
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 3 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-1 Lab ID: 9220393001 Collected: 05/27/08 13:45 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
[phone]
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroethyl) ether
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
108-60-1
2-Chloronaphthalene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
91-58-7
2-Chlorophenol
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
7005-72-3
Chrysene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
53-70-3
Dibenzofuran
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
132-64-9
1,2-Dichlorobenzene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
95-50-1
1,3-Dichlorobenzene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
541-73-1
1,4-Dichlorobenzene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1670
1
06/02/08 00:00
06/10/08 23:09
91-94-1
2,4-Dichlorophenol
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
120-83-2
Diethylphthalate
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
84-66-2
2,4-Dimethylphenol
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
105-67-9
Dimethylphthalate
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
131-11-3
Di-n-butylphthalate
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
666
1
06/02/08 00:00
06/10/08 23:09
534-52-1
2,4-Dinitrophenol
ND ug/kg
1670
1
06/02/08 00:00
06/10/08 23:09
51-28-5
2,4-Dinitrotoluene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
121-14-2
2,6-Dinitrotoluene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
606-20-2
Di-n-octylphthalate
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
117-84-0
1,2-Diphenylhydrazine
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
117-81-7
Fluoranthene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
206-44-0
Fluorene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
87-68-3
Hexachlorobenzene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
77-47-4
Hexachloroethane
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
193-39-5
Isophorone
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
78-59-1
1-Methylnaphthalene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
90-12-0
2-Methylnaphthalene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
Naphthalene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
91-20-3
2-Nitroaniline
ND ug/kg
1670
1
06/02/08 00:00
06/10/08 23:09
88-74-4
3-Nitroaniline
ND ug/kg
1670
1
06/02/08 00:00
06/10/08 23:09
99-09-2
4-Nitroaniline
ND ug/kg
666
1
06/02/08 00:00
06/10/08 23:09
100-01-6
Nitrobenzene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
98-95-3
2-Nitrophenol
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
88-75-5
4-Nitrophenol
ND ug/kg
1670
1
06/02/08 00:00
06/10/08 23:09
100-02-7
N-Nitrosodimethylamine
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
86-30-6
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 4 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-1
Lab ID: 9220393001
Collected: 05/27/08
13:45
Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
Pentachlorophenol
ND ug/kg
1670
1
06/02/08 00:00
06/10/08 23:09
87-86-5
Phenanthrene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
85-01-8
Phenol
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
108-95-2
Pyrene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
333
1
06/02/08 00:00
06/10/08 23:09
88-06-2
Nitrobenzene-d5 (S)
59 %
30-150
1
06/02/08 00:00
06/10/08 23:09
4165-60-0
2-Fluorobiphenyl (S)
60 %
30-150
1
06/02/08 00:00
06/10/08 23:09
321-60-8
Terphenyl-d14 (S)
125 %
30-150
1
06/02/08 00:00
06/10/08 23:09
1718-51-0
Phenol-d6 (S)
48 %
30-150
1
06/02/08 00:00
06/10/08 23:09
13127-88-3
2-Fluorophenol (S)
49 %
30-150
1
06/02/08 00:00
06/10/08 23:09
367-12-4
2,4,6-Tribromophenol (S)
85 %
30-150
1
06/02/08 00:00
06/10/08 23:09
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
104
1
06/03/08 22:10
67-64-1
Benzene
ND ug/kg
5.2
1
06/03/08 22:10
71-43-2
Bromobenzene
ND ug/kg
5.2
1
06/03/08 22:10
108-86-1
Bromochloromethane
ND ug/kg
5.2
1
06/03/08 22:10
74-97-5
Bromodichloromethane
ND ug/kg
5.2
1
06/03/08 22:10
75-27-4
Bromoform
ND ug/kg
5.2
1
06/03/08 22:10
75-25-2
Bromomethane
ND ug/kg
10.4
1
06/03/08 22:10
74-83-9
2-Butanone (MEK)
ND ug/kg
104
1
06/03/08 22:10
78-93-3
n-Butylbenzene
ND ug/kg
5.2
1
06/03/08 22:10
104-51-8
sec-Butylbenzene
ND ug/kg
5.2
1
06/03/08 22:10
135-98-8
tert-Butyl benzene
ND ug/kg
5.2
1
06/03/08 22:10
98-06-6
Carbon tetrachloride
ND ug/kg
5.2
1
06/03/08 22:10
56-23-5
Chlorobenzene
ND ug/kg
5.2
1
06/03/08 22:10
108-90-7
Chloroethane
ND ug/kg
10.4
1
06/03/08 22:10
75-00-3
Chloroform
ND ug/kg
5.2
1
06/03/08 22:10
67-66-3
Chloromethane
ND ug/kg
10.4
1
06/03/08 22:10
74-87-3
2-Chlorotoluene
ND ug/kg
5.2
1
06/03/08 22:10
95-49-8
4-Chlorotoluene
ND ug/kg
5.2
1
06/03/08 22:10
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
5.2
1
06/03/08 22:10
96-12-8
Dibromochloromethane
ND ug/kg
5.2
1
06/03/08 22:10
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
5.2
1
06/03/08 22:10
106-93-4
Dibromomethane
ND ug/kg
5.2
1
06/03/08 22:10
74-95-3
1,2-Dichlorobenzene
ND ug/kg
5.2
1
06/03/08 22:10
95-50-1
1,3-Dichlorobenzene
ND ug/kg
5.2
1
06/03/08 22:10
541-73-1
1,4-Dichlorobenzene
ND ug/kg
5.2
1
06/03/08 22:10
106-46-7
Dichlorodifluoromethane
ND ug/kg
10.4
1
06/03/08 22:10
75-71-8
1,1-Dichloroethane
ND ug/kg
5.2
1
06/03/08 22:10
75-34-3
1,2-Dichloroethane
ND ug/kg
5.2
1
06/03/08 22:10
107-06-2
1,1-Dichloroethene
ND ug/kg
5.2
1
06/03/08 22:10
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
5.2
1
06/03/08 22:10
156-59-2
trans-1,2-Dichloroethene
ND ug/kg
5.2
1
06/03/08 22:10
156-60-5
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
Page 5 of 97
This report shall
not be reproduced, except in full,
without the written
consent of Pace Analytical
Services, Inc..

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-1 Lab ID: 9220393001 Collected: 05/27/08 13:45 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,2-Dichloropropane
ND ug/kg
5.2
1
06/03/08 22:10
78-87-5
1,3-Dichloropropane
ND ug/kg
5.2
1
06/03/08 22:10
142-28-9
2,2-Dichloropropane
ND ug/kg
5.2
1
06/03/08 22:10
594-20-7
1,1-Dichloropropene
ND ug/kg
5.2
1
06/03/08 22:10
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
5.2
1
06/03/08 22:10
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
5.2
1
06/03/08 22:10
10061-02-6
Diisopropyl ether
ND ug/kg
5.2
1
06/03/08 22:10
108-20-3
Ethylbenzene
ND ug/kg
5.2
1
06/03/08 22:10
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
5.2
1
06/03/08 22:10
87-68-3
2-Hexanone
ND ug/kg
52.0
1
06/03/08 22:10
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
5.2
1
06/03/08 22:10
98-82-8
p-Isopropyltoluene
ND ug/kg
5.2
1
06/03/08 22:10
99-87-6
Methylene Chloride
ND ug/kg
26.0
5
06/03/08 22:10
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
52.0
1
06/03/08 22:10
108-10-1
Methyl-tert-butyl ether
ND ug/kg
5.2
1
06/03/08 22:10
1634-04-4
Naphthalene
ND ug/kg
5.2
1
06/03/08 22:10
91-20-3
n-Propylbenzene
ND ug/kg
5.2
1
06/03/08 22:10
103-65-1
Styrene
ND ug/kg
5.2
1
06/03/08 22:10
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
5.2
1
06/03/08 22:10
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
5.2
1
06/03/08 22:10
79-34-5
Tetrachloroethene
ND ug/kg
5.2
1
06/03/08 22:10
127-18-4
Toluene
ND ug/kg
5.2
1
06/03/08 22:10
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
5.2
1
06/03/08 22:10
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
5.2
1
06/03/08 22:10
120-82-1
1,1,1-Trichloroethane
ND ug/kg
5.2
1
06/03/08 22:10
71-55-6
1,1,2-Trichloroethane
ND ug/kg
5.2
1
06/03/08 22:10
79-00-5
Trichloroethene
ND ug/kg
5.2
1
06/03/08 22:10
79-01-6
Trichlorofluoromethane
ND ug/kg
5.2
1
06/03/08 22:10
75-69-4
1,2,3-Trichloropropane
ND ug/kg
5.2
1
06/03/08 22:10
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
5.2
1
06/03/08 22:10
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
5.2
1
06/03/08 22:10
108-67-8
Vinyl acetate
ND ug/kg
52.0
1
06/03/08 22:10
108-05-4
Vinyl chloride
ND ug/kg
10.4
1
06/03/08 22:10
75-01-4
Xylene (Total)
ND ug/kg
15.6
1
06/03/08 22:10
1330-20-7
m&p-Xylene
ND ug/kg
10.4
1
06/03/08 22:10
1330-20-7
o-Xylene
ND ug/kg
5.2
1
06/03/08 22:10
95-47-6
Dibromofluoromethane (S)
116 %
79-116
1
06/03/08 22:10
1868-53-7
Toluene-d8 (S)
97 %
88-110
1
06/03/08 22:10
2037-26-5
4-Bromofluorobenzene (S)
93 %
74-115
1
06/03/08 22:10
460-00-4
1,2-Dichloroethane-d4 (S)
116 %
69-121
1
06/03/08 22:10
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
0.96 %
0.10
1
06/02/08 09:05
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 6 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-2 Lab ID: 9220393002 Collected: 05/27/08 14:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components
ND mg/kg 5.2 1 06/02/08 00:00
06/04/08 20:20
68334-30-5
n-Pentacosane (S)
74 % 50-135 1 06/02/08 00:00
06/04/08 20:20
629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics
ND mg/kg 13.5 1 06/02/08 15:52
06/03/08 02:22
8006-61-9
4-Bromofluorobenzene (S)
91 % 50-135 1 06/02/08 15:52
06/03/08 02:22
460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
4.3 % 0.10 1
06/02/08 09:06
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-3 Lab ID: 9220393003 Collected: 05/28/08 14:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components
ND mg/kg 5.7 1 06/02/08 00:00
06/05/08 17:39
68334-30-5
n-Pentacosane (S)
72 % 50-135 1 06/02/08 00:00
06/05/08 17:39
629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics
ND mg/kg 5.4 1 06/02/08 15:52
06/03/08 02:48
8006-61-9
4-Bromofluorobenzene (S)
89 % 50-135 1 06/02/08 15:52
06/03/08 02:48
460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
12.5 % 0.10 1
06/02/08 09:06
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-4 Lab ID: 9220393004 Collected: 05/28/08 14:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components
33.1 mg/kg 5.9 1 06/05/08 00:00
06/10/08 18:33
68334-30-5
n-Pentacosane (S)
76 % 50-135 1 06/05/08 00:00
06/10/08 18:33
629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics
ND mg/kg 10 1 06/02/08 15:52
06/03/08 03:15
8006-61-9
4-Bromofluorobenzene (S)
91 % 50-135 1 06/02/08 15:52
06/03/08 03:15
460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
14.9 % 0.10 1
06/02/08 09:06
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-6 Lab ID: 9220393005 Collected: 05/28/08 09:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Diesel Components
n-Pentacosane (S)
Gasoline Range Organics
Gasoline Range Organics
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 06/18/2008 12:11 PM
Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
110 mg/kg 5.4 1 06/02/08 00:00
06/05/08 18:05
68334-30-5
146 % 50-135 1 06/02/08 00:00
06/05/08 18:05
629-99-2 S5
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
ND mg/kg 6.1 1 06/02/08 15:52
06/03/08 03:41
8006-61-9
89 % 50-135 1 06/02/08 15:52
06/03/08 03:41
460-00-4
Analytical Method: ASTM D2974-87
6.6 % 0.10 1
06/02/08 09:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-16 Lab ID: 9220393006 Collected: 05/27/08 15:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Diesel Components
n-Pentacosane (S)
Gasoline Range Organics
Gasoline Range Organics
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 06/18/2008 12:11 PM
Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
377 mg/kg 5.9 1 06/02/08 00:00
06/04/08 23:19
68334-30-5
86 % 50-135 1 06/02/08 00:00
06/04/08 23:19
629-99-2
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
914 mg/kg 36.4 5 06/02/08 15:52
06/03/08 23:56
8006-61-9
275 % 50-135 5 06/02/08 15:52
06/03/08 23:56
460-00-4 S1
Analytical Method: ASTM D2974-87
15.1 % 0.10 1
06/02/08 09:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-5 Lab ID: 9220393007 Collected: 05/28/08 15:45 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony
ND mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:06
7440-36-0
Arsenic
32.0 mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:06
7440-38-2
Beryllium
ND mg/kg
0.10
1
06/02/08 15:35
06/03/08 00:06
7440-41-7
Cadmium
1.8 mg/kg
0.10
1
06/02/08 15:35
06/03/08 00:06
7440-43-9
Chromium
5.3 mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:06
7440-47-3
Copper
5.6 mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:06
7440-50-8
Lead
49.8 mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:06
7439-92-1
Manganese
47.9 mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:06
7439-96-5
Nickel
1.7 mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:06
7440-02-0
Selenium
ND mg/kg
1.0
1
06/02/08 15:35
06/03/08 00:06
7782-49-2
Silver
ND mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:06
7440-22-4
Thallium
ND mg/kg
1.0
1
06/02/08 15:35
06/03/08 00:06
7440-28-0
Zinc
445 mg/kg
1.0
1
06/02/08 15:35
06/03/08 00:06
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.075 mg/kg
0.0066
1
06/05/08 11:30
06/05/08 17:06
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
83-32-9
Acenaphthylene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
208-96-8
Aniline
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
62-53-3
Anthracene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
120-12-7
Benzo(a)anthracene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
56-55-3
Benzo(a)pyrene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
50-32-8
Benzo(b)fluoranthene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
191-24-2
Benzo(k)fluoranthene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
207-08-9
Benzoic acid
ND ug/kg
1870
1
06/02/08 00:00
06/09/08 21:17
65-85-0
Benzyl alcohol
ND ug/kg
750
1
06/02/08 00:00
06/09/08 21:17
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
101-55-3
Butylbenzylphthalate
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
85-68-7
4-Chloro-3-methyl phenol
ND ug/kg
750
1
06/02/08 00:00
06/09/08 21:17
59-50-7
4-Chloroaniline
ND ug/kg
1870
1
06/02/08 00:00
06/09/08 21:17
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
108-60-1
2-Chloronaphthalene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
91-58-7
2-Chlorophenol
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
7005-72-3
Chrysene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
53-70-3
Dibenzofuran
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
132-64-9
1,2-Dichlorobenzene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
95-50-1
1,3-Dichlorobenzene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
541-73-1
1,4-Dichlorobenzene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
106-46-7
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY
ANALYSIS
This report shall
not be reproduced, except
in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 97

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-5 Lab ID: 9220393007 Collected: 05/28/08 15:45 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
[phone]
3,3'-Dichlorobenzidine
ND ug/kg
1870
1
06/02/08 00:00
06/09/08 21:17
91-94-1
2,4-Dichlorophenol
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
120-83-2
Diethylphthalate
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
84-66-2
2,4-Dimethylphenol
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
105-67-9
Dimethylphthalate
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
131-11-3
Di-n-butylphthalate
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
750
1
06/02/08 00:00
06/09/08 21:17
534-52-1
2,4-Dinitrophenol
ND ug/kg
1870
1
06/02/08 00:00
06/09/08 21:17
51-28-5
2,4-Dinitrotoluene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
121-14-2
2,6-Dinitrotoluene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
606-20-2
Di-n-octylphthalate
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
117-84-0
1,2-Diphenylhydrazine
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
117-81-7
Fluoranthene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
206-44-0
Fluorene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
87-68-3
Hexachlorobenzene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
77-47-4
Hexachloroethane
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
193-39-5
Isophorone
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
78-59-1
1-Methylnaphthalene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
90-12-0
2-Methylnaphthalene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
Naphthalene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
91-20-3
2-Nitroaniline
ND ug/kg
1870
1
06/02/08 00:00
06/09/08 21:17
88-74-4
3-Nitroaniline
ND ug/kg
1870
1
06/02/08 00:00
06/09/08 21:17
99-09-2
4-Nitroaniline
ND ug/kg
750
1
06/02/08 00:00
06/09/08 21:17
100-01-6
Nitrobenzene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
98-95-3
2-Nitrophenol
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
88-75-5
4-Nitrophenol
ND ug/kg
1870
1
06/02/08 00:00
06/09/08 21:17
100-02-7
N-Nitrosodimethylamine
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
86-30-6
Pentachlorophenol
ND ug/kg
1870
1
06/02/08 00:00
06/09/08 21:17
87-86-5
Phenanthrene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
85-01-8
Phenol
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
108-95-2
Pyrene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
375
1
06/02/08 00:00
06/09/08 21:17
88-06-2
Nitrobenzene-d5 (S)
67 %
30-150
1
06/02/08 00:00
06/09/08 21:17
4165-60-0
2-Fluorobiphenyl (S)
59 %
30-150
1
06/02/08 00:00
06/09/08 21:17
321-60-8
Terphenyl-d14 (S)
43 %
30-150
1
06/02/08 00:00
06/09/08 21:17
1718-51-0
Phenol-d6 (S)
57 %
30-150
1
06/02/08 00:00
06/09/08 21:17
13127-88-3
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 13 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-5 Lab ID: 9220393007 Collected: 05/28/08 15:45 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Fluorophenol (S)
61 %
30-150
1
06/02/08 00:00 06/09/08 21:17
367-12-4
2,4,6-Tribromophenol (S)
83 %
30-150
1
06/02/08 00:00 06/09/08 21:17
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
99.1
1
06/03/08 23:05
67-64-1
Benzene
ND ug/kg
5.0
1
06/03/08 23:05
71-43-2
Bromobenzene
ND ug/kg
5.0
1
06/03/08 23:05
108-86-1
Bromochloromethane
ND ug/kg
5.0
1
06/03/08 23:05
74-97-5
Bromodichloromethane
ND ug/kg
5.0
1
06/03/08 23:05
75-27-4
Bromoform
ND ug/kg
5.0
1
06/03/08 23:05
75-25-2
Bromomethane
ND ug/kg
9.9
1
06/03/08 23:05
74-83-9
2-Butanone (MEK)
ND ug/kg
99.1
1
06/03/08 23:05
78-93-3
n-Butylbenzene
ND ug/kg
5.0
1
06/03/08 23:05
104-51-8
sec-Butylbenzene
ND ug/kg
5.0
1
06/03/08 23:05
135-98-8
tert-Butyl benzene
ND ug/kg
5.0
1
06/03/08 23:05
98-06-6
Carbon tetrachloride
ND ug/kg
5.0
1
06/03/08 23:05
56-23-5
Chlorobenzene
ND ug/kg
5.0
1
06/03/08 23:05
108-90-7
Chloroethane
ND ug/kg
9.9
1
06/03/08 23:05
75-00-3
Chloroform
ND ug/kg
5.0
1
06/03/08 23:05
67-66-3
Chloromethane
ND ug/kg
9.9
1
06/03/08 23:05
74-87-3
2-Chlorotoluene
ND ug/kg
5.0
1
06/03/08 23:05
95-49-8
4-Chlorotoluene
ND ug/kg
5.0
1
06/03/08 23:05
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
5.0
1
06/03/08 23:05
96-12-8
Dibromochloromethane
ND ug/kg
5.0
1
06/03/08 23:05
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
5.0
1
06/03/08 23:05
106-93-4
Dibromomethane
ND ug/kg
5.0
1
06/03/08 23:05
74-95-3
1,2-Dichlorobenzene
ND ug/kg
5.0
1
06/03/08 23:05
95-50-1
1,3-Dichlorobenzene
ND ug/kg
5.0
1
06/03/08 23:05
541-73-1
1,4-Dichlorobenzene
ND ug/kg
5.0
1
06/03/08 23:05
106-46-7
Dichlorodifluoromethane
ND ug/kg
9.9
1
06/03/08 23:05
75-71-8
1,1-Dichloroethane
ND ug/kg
5.0
1
06/03/08 23:05
75-34-3
1,2-Dichloroethane
ND ug/kg
5.0
1
06/03/08 23:05
107-06-2
1,1-Dichloroethene
ND ug/kg
5.0
1
06/03/08 23:05
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
5.0
1
06/03/08 23:05
156-59-2
trans-1,2-Dichloroethene
ND ug/kg
5.0
1
06/03/08 23:05
156-60-5
1,2-Dichloropropane
ND ug/kg
5.0
1
06/03/08 23:05
78-87-5
1,3-Dichloropropane
ND ug/kg
5.0
1
06/03/08 23:05
142-28-9
2,2-Dichloropropane
ND ug/kg
5.0
1
06/03/08 23:05
594-20-7
1,1-Dichloropropene
ND ug/kg
5.0
1
06/03/08 23:05
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
5.0
1
06/03/08 23:05
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
5.0
1
06/03/08 23:05
10061-02-6
Diisopropyl ether
ND ug/kg
5.0
1
06/03/08 23:05
108-20-3
Ethylbenzene
ND ug/kg
5.0
1
06/03/08 23:05
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
5.0
1
06/03/08 23:05
87-68-3
2-Hexanone
ND ug/kg
49.6
1
06/03/08 23:05
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
5.0
1
06/03/08 23:05
98-82-8
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 14 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-5 Lab ID: 9220393007 Collected: 05/28/08 15:45 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
p-Isopropyltoluene
ND ug/kg
5.0
1
06/03/08 23:05
99-87-6
Methylene Chloride
ND ug/kg
5.0
1
06/03/08 23:05
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
49.6
1
06/03/08 23:05
108-10-1
Methyl-tert-butyl ether
ND ug/kg
5.0
1
06/03/08 23:05
1634-04-4
Naphthalene
ND ug/kg
5.0
1
06/03/08 23:05
91-20-3
n-Propylbenzene
ND ug/kg
5.0
1
06/03/08 23:05
103-65-1
Styrene
ND ug/kg
5.0
1
06/03/08 23:05
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
5.0
1
06/03/08 23:05
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
5.0
1
06/03/08 23:05
79-34-5
Tetrachloroethene
ND ug/kg
5.0
1
06/03/08 23:05
127-18-4
Toluene
ND ug/kg
5.0
1
06/03/08 23:05
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
5.0
1
06/03/08 23:05
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
5.0
1
06/03/08 23:05
120-82-1
1,1,1-Trichloroethane
ND ug/kg
5.0
1
06/03/08 23:05
71-55-6
1,1,2-Trichloroethane
ND ug/kg
5.0
1
06/03/08 23:05
79-00-5
Trichloroethene
ND ug/kg
5.0
1
06/03/08 23:05
79-01-6
Trichlorofluoromethane
ND ug/kg
5.0
1
06/03/08 23:05
75-69-4
1,2,3-Trichloropropane
ND ug/kg
5.0
1
06/03/08 23:05
96-18-4
1,2,4-Trimethyl benzene
ND ug/kg
5.0
1
06/03/08 23:05
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
5.0
1
06/03/08 23:05
108-67-8
Vinyl acetate
ND ug/kg
49.6
1
06/03/08 23:05
108-05-4
Vinyl chloride
ND ug/kg
9.9
1
06/03/08 23:05
75-01-4
Xylene (Total)
ND ug/kg
14.9
1
06/03/08 23:05
1330-20-7
m&p-Xylene
ND ug/kg
9.9
1
06/03/08 23:05
1330-20-7
o-Xylene
ND ug/kg
5.0
1
06/03/08 23:05
95-47-6
Dibromofluoromethane (S)
105 %
79-116
1
06/03/08 23:05
1868-53-7
Toluene-d8 (S)
100 %
88-110
1
06/03/08 23:05
2037-26-5
4-Bromofluorobenzene (S)
104 %
74-115
1
06/03/08 23:05
460-00-4
1,2-Dichloroethane-d4 (S)
115 %
69-121
1
06/03/08 23:05
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
12.0 %
0.10
1
06/02/08 09:11
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-7 Lab ID: 9220393008 Collected: 05/27/08 18:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony
ND mg/kg
0.38
1
06/02/08 15:35
06/03/08 00:11
7440-36-0
Arsenic
1.2 mg/kg
0.38
1
06/02/08 15:35
06/03/08 00:11
7440-38-2
Beryllium
ND mg/kg
0.077
1
06/02/08 15:35
06/03/08 00:11
7440-41-7
Cadmium
ND mg/kg
0.077
1
06/02/08 15:35
06/03/08 00:11
7440-43-9
Chromium
3.4 mg/kg
0.38
1
06/02/08 15:35
06/03/08 00:11
7440-47-3
Copper
4.0 mg/kg
0.38
1
06/02/08 15:35
06/03/08 00:11
7440-50-8
Lead
62.4 mg/kg
0.38
1
06/02/08 15:35
06/03/08 00:11
7439-92-1
Manganese
37.7 mg/kg
0.38
1
06/02/08 15:35
06/03/08 00:11
7439-96-5
Nickel
2.9 mg/kg
0.38
1
06/02/08 15:35
06/03/08 00:11
7440-02-0
Selenium
ND mg/kg
0.77
1
06/02/08 15:35
06/03/08 00:11
7782-49-2
Silver
ND mg/kg
0.38
1
06/02/08 15:35
06/03/08 00:11
7440-22-4
Thallium
ND mg/kg
0.77
1
06/02/08 15:35
06/03/08 00:11
7440-28-0
Zinc
115 mg/kg
0.77
1
06/02/08 15:35
06/03/08 00:11
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.063 mg/kg
0.0051
1
06/05/0811:30
06/05/08 17:11
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
83-32-9
Acenaphthylene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
208-96-8
Aniline
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
62-53-3
Anthracene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
120-12-7
Benzo(a)anthracene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
56-55-3
Benzo(a)pyrene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
50-32-8
Benzo(b)fluoranthene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
191-24-2
Benzo(k)fluoranthene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
207-08-9
Benzoic acid
ND ug/kg
1690
1
06/02/08 00:00
06/09/08 21:43
65-85-0
Benzyl alcohol
ND ug/kg
677
1
06/02/08 00:00
06/09/08 21:43
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
101-55-3
Butylbenzylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
85-68-7
4-Chloro-3-methyl phenol
ND ug/kg
677
1
06/02/08 00:00
06/09/08 21:43
59-50-7
4-Chloroaniline
ND ug/kg
1690
1
06/02/08 00:00
06/09/08 21:43
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
108-60-1
2-Chloronaphthalene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
91-58-7
2-Chlorophenol
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
7005-72-3
Chrysene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
53-70-3
Dibenzofuran
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
132-64-9
1,2-Dichlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
95-50-1
1,3-Dichlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
541-73-1
1,4-Dichlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
106-46-7
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY
ANALYSIS
This report shall
not be reproduced, except
in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 97

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-7 Lab ID: 9220393008 Collected: 05/27/08 18:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
[phone]
3,3'-Dichlorobenzidine
ND ug/kg
1690
1
06/02/08 00:00
06/09/08 21:43
91-94-1
2,4-Dichlorophenol
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
120-83-2
Diethylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
84-66-2
2,4-Dimethylphenol
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
105-67-9
Dimethylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
131-11-3
Di-n-butylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
677
1
06/02/08 00:00
06/09/08 21:43
534-52-1
2,4-Dinitrophenol
ND ug/kg
1690
1
06/02/08 00:00
06/09/08 21:43
51-28-5
2,4-Dinitrotoluene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
121-14-2
2,6-Dinitrotoluene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
606-20-2
Di-n-octylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
117-84-0
1,2-Diphenylhydrazine
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
117-81-7
Fluoranthene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
206-44-0
Fluorene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
87-68-3
Hexachlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
77-47-4
Hexachloroethane
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
193-39-5
Isophorone
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
78-59-1
1-Methylnaphthalene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
90-12-0
2-Methylnaphthalene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
Naphthalene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
91-20-3
2-Nitroaniline
ND ug/kg
1690
1
06/02/08 00:00
06/09/08 21:43
88-74-4
3-Nitroaniline
ND ug/kg
1690
1
06/02/08 00:00
06/09/08 21:43
99-09-2
4-Nitroaniline
ND ug/kg
677
1
06/02/08 00:00
06/09/08 21:43
100-01-6
Nitrobenzene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
98-95-3
2-Nitrophenol
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
88-75-5
4-Nitrophenol
ND ug/kg
1690
1
06/02/08 00:00
06/09/08 21:43
100-02-7
N-Nitrosodimethylamine
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
86-30-6
Pentachlorophenol
ND ug/kg
1690
1
06/02/08 00:00
06/09/08 21:43
87-86-5
Phenanthrene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
85-01-8
Phenol
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
108-95-2
Pyrene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
339
1
06/02/08 00:00
06/09/08 21:43
88-06-2
Nitrobenzene-d5 (S)
46 %
30-150
1
06/02/08 00:00
06/09/08 21:43
4165-60-0
2-Fluorobiphenyl (S)
50 %
30-150
1
06/02/08 00:00
06/09/08 21:43
321-60-8
Terphenyl-d14 (S)
66 %
30-150
1
06/02/08 00:00
06/09/08 21:43
1718-51-0
Phenol-d6 (S)
44 %
30-150
1
06/02/08 00:00
06/09/08 21:43
13127-88-3
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 17 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-7 Lab ID: 9220393008 Collected: 05/27/08 18:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Fluorophenol (S)
42 %
30-150
1
06/02/08 00:00 06/09/08 21:43
367-12-4
2,4,6-Tribromophenol (S)
67 %
30-150
1
06/02/08 00:00 06/09/08 21:43
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
159 ug/kg
134
1
06/03/08 22:29
67-64-1
Benzene
ND ug/kg
6.7
1
06/03/08 22:29
71-43-2
Bromobenzene
ND ug/kg
6.7
1
06/03/08 22:29
108-86-1
Bromochloromethane
ND ug/kg
6.7
1
06/03/08 22:29
74-97-5
Bromodichloromethane
ND ug/kg
6.7
1
06/03/08 22:29
75-27-4
Bromoform
ND ug/kg
6.7
1
06/03/08 22:29
75-25-2
Bromomethane
ND ug/kg
13.4
1
06/03/08 22:29
74-83-9
2-Butanone (MEK)
ND ug/kg
134
1
06/03/08 22:29
78-93-3
n-Butylbenzene
ND ug/kg
6.7
1
06/03/08 22:29
104-51-8
sec-Butylbenzene
ND ug/kg
6.7
1
06/03/08 22:29
135-98-8
tert-Butyl benzene
ND ug/kg
6.7
1
06/03/08 22:29
98-06-6
Carbon tetrachloride
ND ug/kg
6.7
1
06/03/08 22:29
56-23-5
Chlorobenzene
ND ug/kg
6.7
1
06/03/08 22:29
108-90-7
Chloroethane
ND ug/kg
13.4
1
06/03/08 22:29
75-00-3
Chloroform
ND ug/kg
6.7
1
06/03/08 22:29
67-66-3
Chloromethane
ND ug/kg
13.4
1
06/03/08 22:29
74-87-3
2-Chlorotoluene
ND ug/kg
6.7
1
06/03/08 22:29
95-49-8
4-Chlorotoluene
ND ug/kg
6.7
1
06/03/08 22:29
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
6.7
1
06/03/08 22:29
96-12-8
Dibromochloromethane
ND ug/kg
6.7
1
06/03/08 22:29
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
6.7
1
06/03/08 22:29
106-93-4
Dibromomethane
ND ug/kg
6.7
1
06/03/08 22:29
74-95-3
1,2-Dichlorobenzene
ND ug/kg
6.7
1
06/03/08 22:29
95-50-1
1,3-Dichlorobenzene
ND ug/kg
6.7
1
06/03/08 22:29
541-73-1
1,4-Dichlorobenzene
ND ug/kg
6.7
1
06/03/08 22:29
106-46-7
Dichlorodifluoromethane
ND ug/kg
13.4
1
06/03/08 22:29
75-71-8
1,1-Dichloroethane
ND ug/kg
6.7
1
06/03/08 22:29
75-34-3
1,2-Dichloroethane
ND ug/kg
6.7
1
06/03/08 22:29
107-06-2
1,1-Dichloroethene
ND ug/kg
6.7
1
06/03/08 22:29
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
6.7
1
06/03/08 22:29
156-59-2
trans-1,2-Dichloroethene
ND ug/kg
6.7
1
06/03/08 22:29
156-60-5
1,2-Dichloropropane
ND ug/kg
6.7
1
06/03/08 22:29
78-87-5
1,3-Dichloropropane
ND ug/kg
6.7
1
06/03/08 22:29
142-28-9
2,2-Dichloropropane
ND ug/kg
6.7
1
06/03/08 22:29
594-20-7
1,1-Dichloropropene
ND ug/kg
6.7
1
06/03/08 22:29
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
6.7
1
06/03/08 22:29
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
6.7
1
06/03/08 22:29
10061-02-6
Diisopropyl ether
ND ug/kg
6.7
1
06/03/08 22:29
108-20-3
Ethylbenzene
ND ug/kg
6.7
1
06/03/08 22:29
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
6.7
1
06/03/08 22:29
87-68-3
2-Hexanone
ND ug/kg
67.0
1
06/03/08 22:29
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
6.7
1
06/03/08 22:29
98-82-8
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 18 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-7 Lab ID: 9220393008 Collected: 05/27/08 18:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
p-Isopropyltoluene
ND ug/kg
6.7
1
06/03/08 22:29
99-87-6
Methylene Chloride
ND ug/kg
6.7
1
06/03/08 22:29
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
67.0
1
06/03/08 22:29
108-10-1
Methyl-tert-butyl ether
ND ug/kg
6.7
1
06/03/08 22:29
1634-04-4
Naphthalene
ND ug/kg
6.7
1
06/03/08 22:29
91-20-3
n-Propylbenzene
ND ug/kg
6.7
1
06/03/08 22:29
103-65-1
Styrene
ND ug/kg
6.7
1
06/03/08 22:29
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
6.7
1
06/03/08 22:29
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
6.7
1
06/03/08 22:29
79-34-5
Tetrachloroethene
ND ug/kg
6.7
1
06/03/08 22:29
127-18-4
Toluene
ND ug/kg
6.7
1
06/03/08 22:29
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
6.7
1
06/03/08 22:29
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
6.7
1
06/03/08 22:29
120-82-1
1,1,1-Trichloroethane
ND ug/kg
6.7
1
06/03/08 22:29
71-55-6
1,1,2-Trichloroethane
ND ug/kg
6.7
1
06/03/08 22:29
79-00-5
Trichloroethene
ND ug/kg
6.7
1
06/03/08 22:29
79-01-6
Trichlorofluoromethane
ND ug/kg
6.7
1
06/03/08 22:29
75-69-4
1,2,3-Trichloropropane
ND ug/kg
6.7
1
06/03/08 22:29
96-18-4
1,2,4-Trimethyl benzene
ND ug/kg
6.7
1
06/03/08 22:29
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
6.7
1
06/03/08 22:29
108-67-8
Vinyl acetate
ND ug/kg
67.0
1
06/03/08 22:29
108-05-4
Vinyl chloride
ND ug/kg
13.4
1
06/03/08 22:29
75-01-4
Xylene (Total)
ND ug/kg
20.1
1
06/03/08 22:29
1330-20-7
m&p-Xylene
ND ug/kg
13.4
1
06/03/08 22:29
1330-20-7
o-Xylene
ND ug/kg
6.7
1
06/03/08 22:29
95-47-6
Dibromofluoromethane (S)
113 %
79-116
1
06/03/08 22:29
1868-53-7
Toluene-d8 (S)
94 %
88-110
1
06/03/08 22:29
2037-26-5
4-Bromofluorobenzene (S)
82 %
74-115
1
06/03/08 22:29
460-00-4
1,2-Dichloroethane-d4 (S)
121 %
69-121
1
06/03/08 22:29
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
2.5 %
0.10
1
06/02/08 09:12
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-10 Lab ID: 9220393009 Collected: 05/28/08 13:10 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony
ND mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:16
7440-36-0
Arsenic
2.3 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:16
7440-38-2
Beryllium
ND mg/kg
0.068
1
06/02/08 15:35
06/03/08 00:16
7440-41-7
Cadmium
0.11 mg/kg
0.068
1
06/02/08 15:35
06/03/08 00:16
7440-43-9
Chromium
2.1 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:16
7440-47-3
Copper
6.1 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:16
7440-50-8
Lead
28.1 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:16
7439-92-1
Manganese
23.8 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:16
7439-96-5
Nickel
1.0 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:16
7440-02-0
Selenium
ND mg/kg
0.68
1
06/02/08 15:35
06/03/08 00:16
7782-49-2
Silver
ND mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:16
7440-22-4
Thallium
ND mg/kg
0.68
1
06/02/08 15:35
06/03/08 00:16
7440-28-0
Zinc
39.3 mg/kg
0.68
1
06/02/08 15:35
06/03/08 00:16
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.053 mg/kg
0.0041
1
06/05/0811:30
06/05/08 17:14
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
83-32-9
Acenaphthylene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
208-96-8
Aniline
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
62-53-3
Anthracene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
120-12-7
Benzo(a)anthracene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
56-55-3
Benzo(a)pyrene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
50-32-8
Benzo(b)fluoranthene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
191-24-2
Benzo(k)fluoranthene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
207-08-9
Benzoic acid
ND ug/kg
1960
1
06/02/08 00:00
06/09/08 22:10
65-85-0
Benzyl alcohol
ND ug/kg
785
1
06/02/08 00:00
06/09/08 22:10
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
101-55-3
Butylbenzylphthalate
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
85-68-7
4-Chloro-3-methyl phenol
ND ug/kg
785
1
06/02/08 00:00
06/09/08 22:10
59-50-7
4-Chloroaniline
ND ug/kg
1960
1
06/02/08 00:00
06/09/08 22:10
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
108-60-1
2-Chloronaphthalene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
91-58-7
2-Chlorophenol
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
7005-72-3
Chrysene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
53-70-3
Dibenzofuran
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
132-64-9
1,2-Dichlorobenzene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
95-50-1
1,3-Dichlorobenzene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
541-73-1
1,4-Dichlorobenzene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
106-46-7
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY
ANALYSIS
This report shall
not be reproduced, except
in full,
without the written consent of Pace Analytical Services, Inc..
Page 20 of 97

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-10 Lab ID: 9220393009 Collected: 05/28/08 13:10 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
[phone]
3,3'-Dichlorobenzidine
ND ug/kg
1960
1
06/02/08 00:00
06/09/08 22:10
91-94-1
2,4-Dichlorophenol
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
120-83-2
Diethylphthalate
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
84-66-2
2,4-Dimethylphenol
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
105-67-9
Dimethylphthalate
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
131-11-3
Di-n-butylphthalate
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
785
1
06/02/08 00:00
06/09/08 22:10
534-52-1
2,4-Dinitrophenol
ND ug/kg
1960
1
06/02/08 00:00
06/09/08 22:10
51-28-5
2,4-Dinitrotoluene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
121-14-2
2,6-Dinitrotoluene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
606-20-2
Di-n-octylphthalate
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
117-84-0
1,2-Diphenylhydrazine
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
117-81-7
Fluoranthene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
206-44-0
Fluorene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
87-68-3
Hexachlorobenzene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
77-47-4
Hexachloroethane
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
193-39-5
Isophorone
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
78-59-1
1-Methylnaphthalene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
90-12-0
2-Methylnaphthalene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
Naphthalene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
91-20-3
2-Nitroaniline
ND ug/kg
1960
1
06/02/08 00:00
06/09/08 22:10
88-74-4
3-Nitroaniline
ND ug/kg
1960
1
06/02/08 00:00
06/09/08 22:10
99-09-2
4-Nitroaniline
ND ug/kg
785
1
06/02/08 00:00
06/09/08 22:10
100-01-6
Nitrobenzene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
98-95-3
2-Nitrophenol
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
88-75-5
4-Nitrophenol
ND ug/kg
1960
1
06/02/08 00:00
06/09/08 22:10
100-02-7
N-Nitrosodimethylamine
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
86-30-6
Pentachlorophenol
ND ug/kg
1960
1
06/02/08 00:00
06/09/08 22:10
87-86-5
Phenanthrene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
85-01-8
Phenol
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
108-95-2
Pyrene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
392
1
06/02/08 00:00
06/09/08 22:10
88-06-2
Nitrobenzene-d5 (S)
80 %
30-150
1
06/02/08 00:00
06/09/08 22:10
4165-60-0
2-Fluorobiphenyl (S)
76 %
30-150
1
06/02/08 00:00
06/09/08 22:10
321-60-8
Terphenyl-d14 (S)
79 %
30-150
1
06/02/08 00:00
06/09/08 22:10
1718-51-0
Phenol-d6 (S)
68 %
30-150
1
06/02/08 00:00
06/09/08 22:10
13127-88-3
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 21 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-10 Lab ID: 9220393009 Collected: 05/28/08 13:10 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Fluorophenol (S)
77 %
30-150
1
06/02/08 00:00 06/09/08 22:10
367-12-4
2,4,6-Tribromophenol (S)
88 %
30-150
1
06/02/08 00:00 06/09/08 22:10
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
97.9
1
06/03/08 23:24
67-64-1
Benzene
ND ug/kg
4.9
1
06/03/08 23:24
71-43-2
Bromobenzene
ND ug/kg
4.9
1
06/03/08 23:24
108-86-1
Bromochloromethane
ND ug/kg
4.9
1
06/03/08 23:24
74-97-5
Bromodichloromethane
ND ug/kg
4.9
1
06/03/08 23:24
75-27-4
Bromoform
ND ug/kg
4.9
1
06/03/08 23:24
75-25-2
Bromomethane
ND ug/kg
9.8
1
06/03/08 23:24
74-83-9
2-Butanone (MEK)
ND ug/kg
97.9
1
06/03/08 23:24
78-93-3
n-Butylbenzene
ND ug/kg
4.9
1
06/03/08 23:24
104-51-8
sec-Butylbenzene
ND ug/kg
4.9
1
06/03/08 23:24
135-98-8
tert-Butyl benzene
ND ug/kg
4.9
1
06/03/08 23:24
98-06-6
Carbon tetrachloride
ND ug/kg
4.9
1
06/03/08 23:24
56-23-5
Chlorobenzene
ND ug/kg
4.9
1
06/03/08 23:24
108-90-7
Chloroethane
ND ug/kg
9.8
1
06/03/08 23:24
75-00-3
Chloroform
ND ug/kg
4.9
1
06/03/08 23:24
67-66-3
Chloromethane
ND ug/kg
9.8
1
06/03/08 23:24
74-87-3
2-Chlorotoluene
ND ug/kg
4.9
1
06/03/08 23:24
95-49-8
4-Chlorotoluene
ND ug/kg
4.9
1
06/03/08 23:24
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
4.9
1
06/03/08 23:24
96-12-8
Dibromochloromethane
ND ug/kg
4.9
1
06/03/08 23:24
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
4.9
1
06/03/08 23:24
106-93-4
Dibromomethane
ND ug/kg
4.9
1
06/03/08 23:24
74-95-3
1,2-Dichlorobenzene
ND ug/kg
4.9
1
06/03/08 23:24
95-50-1
1,3-Dichlorobenzene
ND ug/kg
4.9
1
06/03/08 23:24
541-73-1
1,4-Dichlorobenzene
ND ug/kg
4.9
1
06/03/08 23:24
106-46-7
Dichlorodifluoromethane
ND ug/kg
9.8
1
06/03/08 23:24
75-71-8
1,1-Dichloroethane
ND ug/kg
4.9
1
06/03/08 23:24
75-34-3
1,2-Dichloroethane
ND ug/kg
4.9
1
06/03/08 23:24
107-06-2
1,1-Dichloroethene
ND ug/kg
4.9
1
06/03/08 23:24
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
4.9
1
06/03/08 23:24
156-59-2
trans-1,2-Dichloroethene
ND ug/kg
4.9
1
06/03/08 23:24
156-60-5
1,2-Dichloropropane
ND ug/kg
4.9
1
06/03/08 23:24
78-87-5
1,3-Dichloropropane
ND ug/kg
4.9
1
06/03/08 23:24
142-28-9
2,2-Dichloropropane
ND ug/kg
4.9
1
06/03/08 23:24
594-20-7
1,1-Dichloropropene
ND ug/kg
4.9
1
06/03/08 23:24
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
4.9
1
06/03/08 23:24
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
4.9
1
06/03/08 23:24
10061-02-6
Diisopropyl ether
ND ug/kg
4.9
1
06/03/08 23:24
108-20-3
Ethylbenzene
ND ug/kg
4.9
1
06/03/08 23:24
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
4.9
1
06/03/08 23:24
87-68-3
2-Hexanone
ND ug/kg
49.0
1
06/03/08 23:24
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
4.9
1
06/03/08 23:24
98-82-8
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 22 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-10 Lab ID: 9220393009 Collected: 05/28/08 13:10 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
p-Isopropyltoluene
ND ug/kg
4.9
1
06/03/08 23:24
99-87-6
Methylene Chloride
ND ug/kg
4.9
1
06/03/08 23:24
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
49.0
1
06/03/08 23:24
108-10-1
Methyl-tert-butyl ether
ND ug/kg
4.9
1
06/03/08 23:24
1634-04-4
Naphthalene
ND ug/kg
4.9
1
06/03/08 23:24
91-20-3
n-Propylbenzene
ND ug/kg
4.9
1
06/03/08 23:24
103-65-1
Styrene
ND ug/kg
4.9
1
06/03/08 23:24
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
4.9
1
06/03/08 23:24
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
4.9
1
06/03/08 23:24
79-34-5
Tetrachloroethene
ND ug/kg
4.9
1
06/03/08 23:24
127-18-4
Toluene
ND ug/kg
4.9
1
06/03/08 23:24
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
4.9
1
06/03/08 23:24
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
4.9
1
06/03/08 23:24
120-82-1
1,1,1-Trichloroethane
ND ug/kg
4.9
1
06/03/08 23:24
71-55-6
1,1,2-Trichloroethane
ND ug/kg
4.9
1
06/03/08 23:24
79-00-5
Trichloroethene
ND ug/kg
4.9
1
06/03/08 23:24
79-01-6
Trichlorofluoromethane
ND ug/kg
4.9
1
06/03/08 23:24
75-69-4
1,2,3-Trichloropropane
ND ug/kg
4.9
1
06/03/08 23:24
96-18-4
1,2,4-Trimethyl benzene
ND ug/kg
4.9
1
06/03/08 23:24
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
4.9
1
06/03/08 23:24
108-67-8
Vinyl acetate
ND ug/kg
49.0
1
06/03/08 23:24
108-05-4
Vinyl chloride
ND ug/kg
9.8
1
06/03/08 23:24
75-01-4
Xylene (Total)
ND ug/kg
14.7
1
06/03/08 23:24
1330-20-7
m&p-Xylene
ND ug/kg
9.8
1
06/03/08 23:24
1330-20-7
o-Xylene
ND ug/kg
4.9
1
06/03/08 23:24
95-47-6
Dibromofluoromethane (S)
110 %
79-116
1
06/03/08 23:24
1868-53-7
Toluene-d8 (S)
103 %
88-110
1
06/03/08 23:24
2037-26-5
4-Bromofluorobenzene (S)
91 %
74-115
1
06/03/08 23:24
460-00-4
1,2-Dichloroethane-d4 (S)
108 %
69-121
1
06/03/08 23:24
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
15.9 %
0.10
1
06/02/08 09:12
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 23 of 97

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-11 Lab ID: 9220393010 Collected: 05/27/08 16:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
[phone]
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony
ND mg/kg
0.26
1
06/02/08 15:35
06/03/08 00:20
7440-36-0
Arsenic
2.1 mg/kg
0.26
1
06/02/08 15:35
06/03/08 00:20
7440-38-2
Beryllium
ND mg/kg
0.052
1
06/02/08 15:35
06/03/08 00:20
7440-41-7
Cadmium
0.056 mg/kg
0.052
1
06/02/08 15:35
06/03/08 00:20
7440-43-9
Chromium
1.6 mg/kg
0.26
1
06/02/08 15:35
06/03/08 00:20
7440-47-3
Copper
17.1 mg/kg
0.26
1
06/02/08 15:35
06/03/08 00:20
7440-50-8
Lead
28.4 mg/kg
0.26
1
06/02/08 15:35
06/03/08 00:20
7439-92-1
Manganese
18.3 mg/kg
0.26
1
06/02/08 15:35
06/03/08 00:20
7439-96-5
Nickel
1.8 mg/kg
0.26
1
06/02/08 15:35
06/03/08 00:20
7440-02-0
Selenium
ND mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:20
7782-49-2
Silver
ND mg/kg
0.26
1
06/02/08 15:35
06/03/08 00:20
7440-22-4
Thallium
ND mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:20
7440-28-0
Zinc
64.4 mg/kg
0.52
1
06/02/08 15:35
06/03/08 00:20
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.12 mg/kg
0.0053
1
06/05/0811:30
06/05/08 17:17
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
83-32-9
Acenaphthylene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
208-96-8
Aniline
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
62-53-3
Anthracene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
120-12-7
Benzo(a)anthracene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
56-55-3
Benzo(a)pyrene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
50-32-8
Benzo(b)fluoranthene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
191-24-2
Benzo(k)fluoranthene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
207-08-9
Benzoic acid
ND ug/kg
1700
1
06/02/08 00:00
06/10/08 23:37
65-85-0
Benzyl alcohol
ND ug/kg
679
1
06/02/08 00:00
06/10/08 23:37
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
101-55-3
Butylbenzylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
85-68-7
4-Chloro-3-methyl phenol
ND ug/kg
679
1
06/02/08 00:00
06/10/08 23:37
59-50-7
4-Chloroaniline
ND ug/kg
1700
1
06/02/08 00:00
06/10/08 23:37
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
108-60-1
2-Chloronaphthalene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
91-58-7
2-Chlorophenol
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
7005-72-3
Chrysene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
53-70-3
Dibenzofuran
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
132-64-9
1,2-Dichlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
95-50-1
1,3-Dichlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
541-73-1
1,4-Dichlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
106-46-7
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 24 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-11 Lab ID: 9220393010 Collected: 05/27/08 16:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
[phone]
3,3'-Dichlorobenzidine
ND ug/kg
1700
1
06/02/08 00:00
06/10/08 23:37
91-94-1
2,4-Dichlorophenol
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
120-83-2
Diethylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
84-66-2
2,4-Dimethylphenol
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
105-67-9
Dimethylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
131-11-3
Di-n-butylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
679
1
06/02/08 00:00
06/10/08 23:37
534-52-1
2,4-Dinitrophenol
ND ug/kg
1700
1
06/02/08 00:00
06/10/08 23:37
51-28-5
2,4-Dinitrotoluene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
121-14-2
2,6-Dinitrotoluene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
606-20-2
Di-n-octylphthalate
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
117-84-0
1,2-Diphenylhydrazine
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
117-81-7
Fluoranthene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
206-44-0
Fluorene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
87-68-3
Hexachlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
77-47-4
Hexachloroethane
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
193-39-5
Isophorone
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
78-59-1
1-Methylnaphthalene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
90-12-0
2-Methylnaphthalene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
Naphthalene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
91-20-3
2-Nitroaniline
ND ug/kg
1700
1
06/02/08 00:00
06/10/08 23:37
88-74-4
3-Nitroaniline
ND ug/kg
1700
1
06/02/08 00:00
06/10/08 23:37
99-09-2
4-Nitroaniline
ND ug/kg
679
1
06/02/08 00:00
06/10/08 23:37
100-01-6
Nitrobenzene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
98-95-3
2-Nitrophenol
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
88-75-5
4-Nitrophenol
ND ug/kg
1700
1
06/02/08 00:00
06/10/08 23:37
100-02-7
N-Nitrosodimethylamine
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
86-30-6
Pentachlorophenol
ND ug/kg
1700
1
06/02/08 00:00
06/10/08 23:37
87-86-5
Phenanthrene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
85-01-8
Phenol
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
108-95-2
Pyrene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
339
1
06/02/08 00:00
06/10/08 23:37
88-06-2
Nitrobenzene-d5 (S)
39 %
30-150
1
06/02/08 00:00
06/10/08 23:37
4165-60-0
2-Fluorobiphenyl (S)
37 %
30-150
1
06/02/08 00:00
06/10/08 23:37
321-60-8
Terphenyl-d14 (S)
72 %
30-150
1
06/02/08 00:00
06/10/08 23:37
1718-51-0
Phenol-d6 (S)
34 %
30-150
1
06/02/08 00:00
06/10/08 23:37
13127-88-3
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 25 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-11
Lab ID: 9220393010
Collected: 05/27/08
16:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units
Report Limit
DF Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Fluorophenol (S)
38 %
30-150
1 06/02/08 00:00
06/10/08 23:37
367-12-4
2,4,6-Tribromophenol (S)
40 %
30-150
1 06/02/08 00:00
06/10/08 23:37
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
197 ug/kg
127
1
06/04/08 20:40
67-64-1 C9
Benzene
ND ug/kg
6.3
1
06/04/08 20:40
71-43-2
Bromobenzene
ND ug/kg
6.3
1
06/04/08 20:40
108-86-1
Bromochloromethane
ND ug/kg
6.3
1
06/04/08 20:40
74-97-5
Bromodichloromethane
ND ug/kg
6.3
1
06/04/08 20:40
75-27-4
Bromoform
ND ug/kg
6.3
1
06/04/08 20:40
75-25-2
Bromomethane
ND ug/kg
12.7
1
06/04/08 20:40
74-83-9
2-Butanone (MEK)
ND ug/kg
127
1
06/04/08 20:40
78-93-3
n-Butylbenzene
ND ug/kg
6.3
1
06/04/08 20:40
104-51-8
sec-Butylbenzene
ND ug/kg
6.3
1
06/04/08 20:40
135-98-8
tert-Butyl benzene
ND ug/kg
6.3
1
06/04/08 20:40
98-06-6
Carbon tetrachloride
ND ug/kg
6.3
1
06/04/08 20:40
56-23-5
Chlorobenzene
ND ug/kg
6.3
1
06/04/08 20:40
108-90-7
Chloroethane
ND ug/kg
12.7
1
06/04/08 20:40
75-00-3
Chloroform
ND ug/kg
6.3
1
06/04/08 20:40
67-66-3
Chloromethane
ND ug/kg
12.7
1
06/04/08 20:40
74-87-3
2-Chlorotoluene
ND ug/kg
6.3
1
06/04/08 20:40
95-49-8
4-Chlorotoluene
ND ug/kg
6.3
1
06/04/08 20:40
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
6.3
1
06/04/08 20:40
96-12-8
Dibromochloromethane
ND ug/kg
6.3
1
06/04/08 20:40
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
6.3
1
06/04/08 20:40
106-93-4
Dibromomethane
ND ug/kg
6.3
1
06/04/08 20:40
74-95-3
1,2-Dichlorobenzene
ND ug/kg
6.3
1
06/04/08 20:40
95-50-1
1,3-Dichlorobenzene
ND ug/kg
6.3
1
06/04/08 20:40
541-73-1
1,4-Dichlorobenzene
ND ug/kg
6.3
1
06/04/08 20:40
106-46-7
Dichlorodifluoromethane
ND ug/kg
12.7
1
06/04/08 20:40
75-71-8
1,1-Dichloroethane
ND ug/kg
6.3
1
06/04/08 20:40
75-34-3
1,2-Dichloroethane
ND ug/kg
6.3
1
06/04/08 20:40
107-06-2
1,1-Dichloroethene
ND ug/kg
6.3
1
06/04/08 20:40
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
6.3
1
06/04/08 20:40
156-59-2
trans-1,2-Dichloroethene
ND ug/kg
6.3
1
06/04/08 20:40
156-60-5
1,2-Dichloropropane
ND ug/kg
6.3
1
06/04/08 20:40
78-87-5
1,3-Dichloropropane
ND ug/kg
6.3
1
06/04/08 20:40
142-28-9
2,2-Dichloropropane
ND ug/kg
6.3
1
06/04/08 20:40
594-20-7
1,1-Dichloropropene
ND ug/kg
6.3
1
06/04/08 20:40
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
6.3
1
06/04/08 20:40
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
6.3
1
06/04/08 20:40
10061-02-6
Diisopropyl ether
ND ug/kg
6.3
1
06/04/08 20:40
108-20-3
Ethylbenzene
ND ug/kg
6.3
1
06/04/08 20:40
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
6.3
1
06/04/08 20:40
87-68-3
2-Hexanone
ND ug/kg
63.5
1
06/04/08 20:40
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
6.3
1
06/04/08 20:40
98-82-8
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
Page 26 of 97
This report shall
not be reproduced, except in full,
without the written
consent of Pace Analytical
Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-11 Lab ID: 9220393010 Collected: 05/27/08 16:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
p-Isopropyltoluene
ND ug/kg
6.3
1
06/04/08 20:40
99-87-6
Methylene Chloride
ND ug/kg
6.3
1
06/04/08 20:40
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
63.5
1
06/04/08 20:40
108-10-1
Methyl-tert-butyl ether
ND ug/kg
6.3
1
06/04/08 20:40
1634-04-4
Naphthalene
ND ug/kg
6.3
1
06/04/08 20:40
91-20-3
n-Propylbenzene
ND ug/kg
6.3
1
06/04/08 20:40
103-65-1
Styrene
ND ug/kg
6.3
1
06/04/08 20:40
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
6.3
1
06/04/08 20:40
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
6.3
1
06/04/08 20:40
79-34-5
Tetrachloroethene
ND ug/kg
6.3
1
06/04/08 20:40
127-18-4
Toluene
ND ug/kg
6.3
1
06/04/08 20:40
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
6.3
1
06/04/08 20:40
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
6.3
1
06/04/08 20:40
120-82-1
1,1,1-Trichloroethane
ND ug/kg
6.3
1
06/04/08 20:40
71-55-6
1,1,2-Trichloroethane
ND ug/kg
6.3
1
06/04/08 20:40
79-00-5
Trichloroethene
ND ug/kg
6.3
1
06/04/08 20:40
79-01-6
Trichlorofluoromethane
ND ug/kg
6.3
1
06/04/08 20:40
75-69-4
1,2,3-Trichloropropane
ND ug/kg
6.3
1
06/04/08 20:40
96-18-4
1,2,4-Trimethyl benzene
ND ug/kg
6.3
1
06/04/08 20:40
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
6.3
1
06/04/08 20:40
108-67-8
Vinyl acetate
ND ug/kg
63.5
1
06/04/08 20:40
108-05-4
Vinyl chloride
ND ug/kg
12.7
1
06/04/08 20:40
75-01-4
Xylene (Total)
ND ug/kg
19.0
1
06/04/08 20:40
1330-20-7
m&p-Xylene
ND ug/kg
12.7
1
06/04/08 20:40
1330-20-7
o-Xylene
ND ug/kg
6.3
1
06/04/08 20:40
95-47-6
Dibromofluoromethane (S)
113 %
79-116
1
06/04/08 20:40
1868-53-7
Toluene-d8 (S)
99 %
88-110
1
06/04/08 20:40
2037-26-5
4-Bromofluorobenzene (S)
83 %
74-115
1
06/04/08 20:40
460-00-4
1,2-Dichloroethane-d4 (S)
119 %
69-121
1
06/04/08 20:40
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
2.8 %
0.10
1
06/02/08 09:12
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 27 of 97

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-17 Lab ID: 9220393011 Collected: 05/28/08 11:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
[phone]
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony
1.8 mg/kg
0.27
1
06/02/08 15:35
06/03/08 00:32
7440-36-0
Arsenic
8.8 mg/kg
0.27
1
06/02/08 15:35
06/03/08 00:32
7440-38-2
Beryllium
ND mg/kg
0.054
1
06/02/08 15:35
06/03/08 00:32
7440-41-7
Cadmium
1.5 mg/kg
0.054
1
06/02/08 15:35
06/03/08 00:32
7440-43-9
Chromium
12.4 mg/kg
0.27
1
06/02/08 15:35
06/03/08 00:32
7440-47-3
Copper
58.9 mg/kg
0.27
1
06/02/08 15:35
06/03/08 00:32
7440-50-8
Lead
680 mg/kg
1.4
5
06/02/08 15:35
06/04/08 05:25
7439-92-1
Manganese
95.5 mg/kg
0.27
1
06/02/08 15:35
06/03/08 00:32
7439-96-5
Nickel
7.7 mg/kg
0.27
1
06/02/08 15:35
06/03/08 00:32
7440-02-0
Selenium
ND mg/kg
0.54
1
06/02/08 15:35
06/03/08 00:32
7782-49-2
Silver
ND mg/kg
0.27
1
06/02/08 15:35
06/03/08 00:32
7440-22-4
Thallium
ND mg/kg
0.54
1
06/02/08 15:35
06/03/08 00:32
7440-28-0
Zinc
444 mg/kg
0.54
1
06/02/08 15:35
06/03/08 00:32
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.21 mg/kg
0.040
10
06/05/0811:30
06/05/0818:10
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
83-32-9
Acenaphthylene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
208-96-8
Aniline
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
62-53-3
Anthracene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
120-12-7
Benzo(a)anthracene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
56-55-3
Benzo(a)pyrene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
50-32-8
Benzo(b)fluoranthene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
191-24-2
Benzo(k)fluoranthene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
207-08-9
Benzoic acid
ND ug/kg
2000
1
06/02/08 00:00
06/11/08 00:05
65-85-0
Benzyl alcohol
ND ug/kg
799
1
06/02/08 00:00
06/11/08 00:05
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
101-55-3
Butylbenzylphthalate
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
85-68-7
4-Chloro-3-methyl phenol
ND ug/kg
799
1
06/02/08 00:00
06/11/08 00:05
59-50-7
4-Chloroaniline
ND ug/kg
2000
1
06/02/08 00:00
06/11/08 00:05
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
108-60-1
2-Chloronaphthalene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
91-58-7
2-Chlorophenol
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
7005-72-3
Chrysene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
53-70-3
Dibenzofuran
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
132-64-9
1,2-Dichlorobenzene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
95-50-1
1,3-Dichlorobenzene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
541-73-1
1,4-Dichlorobenzene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
106-46-7
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 28 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-17 Lab ID: 9220393011 Collected: 05/28/08 11:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine
ND ug/kg
2000
1
06/02/08 00:00
06/11/08 00:05
2,4-Dichlorophenol
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Diethylphthalate
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
2,4-Dimethylphenol
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Dimethylphthalate
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Di-n-butylphthalate
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
4,6-Dinitro-2-methyl phenol
ND ug/kg
799
1
06/02/08 00:00
06/11/08 00:05
2,4-Dinitrophenol
ND ug/kg
2000
1
06/02/08 00:00
06/11/08 00:05
2,4-Dinitrotoluene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
2,6-Dinitrotoluene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Di-n-octylphthalate
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
1,2-Diphenylhydrazine
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
bis(2- Ethyl hexyl)phthalate
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Fluoranthene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Fluorene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Hexachloro-1,3-butadiene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Hexachlorobenzene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Hexachlorocyclopentadiene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Hexachloroethane
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Indeno(1,2,3-cd)pyrene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Isophorone
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
1-Methylnaphthalene
689 ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
2-Methylnaphthalene
648 ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
2-Methylphenol(o-Cresol)
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
3&4-Methyl phenol (m&p Cresol)
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Naphthalene
1050 ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
2-Nitroaniline
ND ug/kg
2000
1
06/02/08 00:00
06/11/08 00:05
3-Nitroaniline
ND ug/kg
2000
1
06/02/08 00:00
06/11/08 00:05
4-Nitroaniline
ND ug/kg
799
1
06/02/08 00:00
06/11/08 00:05
Nitrobenzene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
2-Nitrophenol
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
4-Nitrophenol
ND ug/kg
2000
1
06/02/08 00:00
06/11/08 00:05
N-Nitrosodimethylamine
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
N-Nitroso-di-n-propylamine
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
N-Nitrosodiphenylamine
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Pentachlorophenol
ND ug/kg
2000
1
06/02/08 00:00
06/11/08 00:05
Phenanthrene
801 ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Phenol
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Pyrene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
1,2,4-Trichlorobenzene
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
2,4,5-Trichlorophenol
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
2,4,6-Trichlorophenol
ND ug/kg
399
1
06/02/08 00:00
06/11/08 00:05
Nitrobenzene-d5 (S)
47 %
30-150
1
06/02/08 00:00
06/11/08 00:05
2-Fluorobiphenyl (S)
64 %
30-150
1
06/02/08 00:00
06/11/08 00:05
Terphenyl-d14 (S)
138 %
30-150
1
06/02/08 00:00
06/11/08 00:05
Phenol-d6 (S)
33 %
30-150
1
06/02/08 00:00
06/11/08 00:05
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
without the written
consent of Pace Analytical Services, Inc..
[phone]
CAS No. Qual
91-94-1
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
122-66-7
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
90-12-0
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
62-75-9
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
120-82-1
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
Page 29 of 97

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-17
Lab ID: 9220393011
Collected: 05/28/08
11:30 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units
Report Limit
DF Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2-Fluorophenol (S)
39 %
30-150
1 06/02/08 00:00
06/11/08 00:05
367-12-4
2,4,6-Tribromophenol (S)
54 %
30-150
1 06/02/08 00:00
06/11/08 00:05
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
226 ug/kg
130
1
06/04/08 20:58
67-64-1 C9
Benzene
ND ug/kg
6.5
1
06/04/08 20:58
71-43-2
Bromobenzene
ND ug/kg
6.5
1
06/04/08 20:58
108-86-1
Bromochloromethane
ND ug/kg
6.5
1
06/04/08 20:58
74-97-5
Bromodichloromethane
ND ug/kg
6.5
1
06/04/08 20:58
75-27-4
Bromoform
ND ug/kg
6.5
1
06/04/08 20:58
75-25-2
Bromomethane
ND ug/kg
13.0
1
06/04/08 20:58
74-83-9
2-Butanone (MEK)
ND ug/kg
130
1
06/04/08 20:58
78-93-3
n-Butylbenzene
ND ug/kg
6.5
1
06/04/08 20:58
104-51-8
sec-Butylbenzene
ND ug/kg
6.5
1
06/04/08 20:58
135-98-8
tert-Butyl benzene
ND ug/kg
6.5
1
06/04/08 20:58
98-06-6
Carbon tetrachloride
ND ug/kg
6.5
1
06/04/08 20:58
56-23-5
Chlorobenzene
ND ug/kg
6.5
1
06/04/08 20:58
108-90-7
Chloroethane
ND ug/kg
13.0
1
06/04/08 20:58
75-00-3
Chloroform
ND ug/kg
6.5
1
06/04/08 20:58
67-66-3
Chloromethane
ND ug/kg
13.0
1
06/04/08 20:58
74-87-3
2-Chlorotoluene
ND ug/kg
6.5
1
06/04/08 20:58
95-49-8
4-Chlorotoluene
ND ug/kg
6.5
1
06/04/08 20:58
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
6.5
1
06/04/08 20:58
96-12-8
Dibromochloromethane
ND ug/kg
6.5
1
06/04/08 20:58
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
6.5
1
06/04/08 20:58
106-93-4
Dibromomethane
ND ug/kg
6.5
1
06/04/08 20:58
74-95-3
1,2-Dichlorobenzene
ND ug/kg
6.5
1
06/04/08 20:58
95-50-1
1,3-Dichlorobenzene
ND ug/kg
6.5
1
06/04/08 20:58
541-73-1
1,4-Dichlorobenzene
ND ug/kg
6.5
1
06/04/08 20:58
106-46-7
Dichlorodifluoromethane
ND ug/kg
13.0
1
06/04/08 20:58
75-71-8
1,1-Dichloroethane
ND ug/kg
6.5
1
06/04/08 20:58
75-34-3
1,2-Dichloroethane
ND ug/kg
6.5
1
06/04/08 20:58
107-06-2
1,1-Dichloroethene
ND ug/kg
6.5
1
06/04/08 20:58
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
6.5
1
06/04/08 20:58
156-59-2
trans-1,2-Dichloroethene
ND ug/kg
6.5
1
06/04/08 20:58
156-60-5
1,2-Dichloropropane
ND ug/kg
6.5
1
06/04/08 20:58
78-87-5
1,3-Dichloropropane
ND ug/kg
6.5
1
06/04/08 20:58
142-28-9
2,2-Dichloropropane
ND ug/kg
6.5
1
06/04/08 20:58
594-20-7
1,1-Dichloropropene
ND ug/kg
6.5
1
06/04/08 20:58
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
6.5
1
06/04/08 20:58
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
6.5
1
06/04/08 20:58
10061-02-6
Diisopropyl ether
ND ug/kg
6.5
1
06/04/08 20:58
108-20-3
Ethylbenzene
ND ug/kg
6.5
1
06/04/08 20:58
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
6.5
1
06/04/08 20:58
87-68-3
2-Hexanone
ND ug/kg
65.2
1
06/04/08 20:58
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
6.5
1
06/04/08 20:58
98-82-8
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
Page 30 of 97
This report shall
not be reproduced, except in full,
without the written
consent of Pace Analytical
Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-17
Lab ID: 9220393011 Collected:
05/28/08 11:30
Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260/5035A Volatile Organics
Analytical Method: EPA 8260
p-Isopropyltoluene
ND ug/kg
6.5
1
06/04/08 20:58
99-87-6
Methylene Chloride
ND ug/kg
6.5
1
06/04/08 20:58
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
65.2
1
06/04/08 20:58
108-10-1
Methyl-tert-butyl ether
ND ug/kg
6.5
1
06/04/08 20:58
1634-04-4
Naphthalene
ND ug/kg
6.5
1
06/04/08 20:58
91-20-3
n-Propylbenzene
ND ug/kg
6.5
1
06/04/08 20:58
103-65-1
Styrene
ND ug/kg
6.5
1
06/04/08 20:58
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
6.5
1
06/04/08 20:58
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
6.5
1
06/04/08 20:58
79-34-5
Tetrachloroethene
425 ug/kg
6.5
1
06/04/08 20:58
127-18-4 E
Toluene
ND ug/kg
6.5
1
06/04/08 20:58
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
6.5
1
06/04/08 20:58
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
6.5
1
06/04/08 20:58
120-82-1
1,1,1-Trichloroethane
ND ug/kg
6.5
1
06/04/08 20:58
71-55-6
1,1,2-Trichloroethane
ND ug/kg
6.5
1
06/04/08 20:58
79-00-5
Trichloroethene
31.1 ug/kg
6.5
1
06/04/08 20:58
79-01-6
Trichlorofluoromethane
ND ug/kg
6.5
1
06/04/08 20:58
75-69-4
1,2,3-Trichloropropane
ND ug/kg
6.5
1
06/04/08 20:58
96-18-4
1,2,4-Trimethyl benzene
ND ug/kg
6.5
1
06/04/08 20:58
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
6.5
1
06/04/08 20:58
108-67-8
Vinyl acetate
ND ug/kg
65.2
1
06/04/08 20:58
108-05-4
Vinyl chloride
ND ug/kg
13.0
1
06/04/08 20:58
75-01-4
Xylene (Total)
ND ug/kg
19.6
1
06/04/08 20:58
1330-20-7
m&p-Xylene
ND ug/kg
13.0
1
06/04/08 20:58
1330-20-7
o-Xylene
ND ug/kg
6.5
1
06/04/08 20:58
95-47-6
Dibromofluoromethane (S)
121 %
79-116
1
06/04/08 20:58
1868-53-7 S2
Toluene-d8(S)
89 %
88-110
1
06/04/08 20:58
2037-26-5
4-Bromofluorobenzene (S)
79 %
74-115
1
06/04/08 20:58
460-00-4
1,2-Dichloroethane-d4 (S)
140 %
69-121
1
06/04/08 20:58
17060-07-0 S2
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
17.4 %
0.10
1
06/02/08 09:12
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 31 of 97

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-8 Lab ID: 9220393012 Collected: 05/28/08 15:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3545
[phone]
PCB-1016 (Aroclor 1016)
ND ug/kg
38.5
1
06/03/08 00:00
06/05/08 21:22
12674-11-2
PCB-1221 (Aroclor 1221)
ND ug/kg
38.5
1
06/03/08 00:00
06/05/08 21:22
11104-28-2
PCB-1232 (Aroclor 1232)
ND ug/kg
38.5
1
06/03/08 00:00
06/05/08 21:22
11141-16-5
PCB-1242 (Aroclor 1242)
ND ug/kg
38.5
1
06/03/08 00:00
06/05/08 21:22
53469-21-9
PCB-1248 (Aroclor 1248)
ND ug/kg
38.5
1
06/03/08 00:00
06/05/08 21:22
12672-29-6
PCB-1254 (Aroclor 1254)
ND ug/kg
38.5
1
06/03/08 00:00
06/05/08 21:22
11097-69-1
PCB-1260 (Aroclor 1260)
ND ug/kg
38.5
1
06/03/08 00:00
06/05/08 21:22
11096-82-5
Decachlorobiphenyl (S)
85 %
10-128
1
06/03/08 00:00
06/05/08 21:22
2051-24-3
6010 MET ICP
Analytical Method: EPA 6010
Preparation Method:
EPA 3050
Antimony
ND mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:37
7440-36-0
Arsenic
59.8 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:37
7440-38-2
Beryllium
ND mg/kg
0.069
1
06/02/08 15:35
06/03/08 00:37
7440-41-7
Cadmium
ND mg/kg
0.069
1
06/02/08 15:35
06/03/08 00:37
7440-43-9
Chromium
1.5 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:37
7440-47-3
Copper
0.62 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:37
7440-50-8
Lead
2.5 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:37
7439-92-1
Manganese
8.6 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:37
7439-96-5
Nickel
0.56 mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:37
7440-02-0
Selenium
ND mg/kg
0.69
1
06/02/08 15:35
06/03/08 00:37
7782-49-2
Silver
ND mg/kg
0.34
1
06/02/08 15:35
06/03/08 00:37
7440-22-4
Thallium
ND mg/kg
0.69
1
06/02/08 15:35
06/03/08 00:37
7440-28-0
Zinc
10.8 mg/kg
0.69
1
06/02/08 15:35
06/03/08 00:37
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.030 mg/kg
0.0037
1
06/05/0811:30
06/05/08 17:31
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
83-32-9
Acenaphthylene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
208-96-8
Aniline
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
62-53-3
Anthracene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
120-12-7
Benzo(a)anthracene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
56-55-3
Benzo(a)pyrene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
50-32-8
Benzo(b)fluoranthene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
205-99-2
Benzo(g,h,i)perylene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
191-24-2
Benzo(k)fluoranthene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
207-08-9
Benzoic acid
ND ug/kg
1920
1
06/04/08 00:00
06/06/08 09:27
65-85-0
Benzyl alcohol
ND ug/kg
769
1
06/04/08 00:00
06/06/08 09:27
100-51-6
4-Bromophenylphenyl ether
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
101-55-3
Butylbenzylphthalate
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
85-68-7
4-Chloro-3-methyl phenol
ND ug/kg
769
1
06/04/08 00:00
06/06/08 09:27
59-50-7
4-Chloroaniline
ND ug/kg
1920
1
06/04/08 00:00
06/06/08 09:27
106-47-8
bis(2-Chloroethoxy)methane
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
111-91-1
bis(2-Chloroethyl) ether
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
111-44-4
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 32 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-8 Lab ID: 9220393012 Collected: 05/28/08 15:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
[phone]
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
bis(2-Chloroisopropyl) ether
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
108-60-1
2-Chloronaphthalene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
91-58-7
2-Chlorophenol
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
95-57-8
4-Chlorophenylphenyl ether
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
7005-72-3
Chrysene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
218-01-9
Dibenz(a,h)anthracene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
53-70-3
Dibenzofuran
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
132-64-9
1,2-Dichlorobenzene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
95-50-1
1,3-Dichlorobenzene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
541-73-1
1,4-Dichlorobenzene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
106-46-7
3,3'-Dichlorobenzidine
ND ug/kg
1920
1
06/04/08 00:00
06/06/08 09:27
91-94-1
2,4-Dichlorophenol
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
120-83-2
Diethylphthalate
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
84-66-2
2,4-Dimethylphenol
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
105-67-9
Dimethylphthalate
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
131-11-3
Di-n-butylphthalate
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/kg
769
1
06/04/08 00:00
06/06/08 09:27
534-52-1
2,4-Dinitrophenol
ND ug/kg
1920
1
06/04/08 00:00
06/06/08 09:27
51-28-5
2,4-Dinitrotoluene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
121-14-2
2,6-Dinitrotoluene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
606-20-2
Di-n-octylphthalate
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
117-84-0
1,2-Diphenylhydrazine
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
117-81-7
Fluoranthene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
206-44-0
Fluorene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
87-68-3
Hexachlorobenzene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
118-74-1
Hexachlorocyclopentadiene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
77-47-4
Hexachloroethane
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
193-39-5
Isophorone
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
78-59-1
1-Methylnaphthalene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
90-12-0
2-Methylnaphthalene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
91-57-6
2-Methylphenol(o-Cresol)
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
Naphthalene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
91-20-3
2-Nitroaniline
ND ug/kg
1920
1
06/04/08 00:00
06/06/08 09:27
88-74-4
3-Nitroaniline
ND ug/kg
1920
1
06/04/08 00:00
06/06/08 09:27
99-09-2
4-Nitroaniline
ND ug/kg
769
1
06/04/08 00:00
06/06/08 09:27
100-01-6
Nitrobenzene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
98-95-3
2-Nitrophenol
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
88-75-5
4-Nitrophenol
ND ug/kg
1920
1
06/04/08 00:00
06/06/08 09:27
100-02-7
N-Nitrosodimethylamine
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
62-75-9
N-Nitroso-di-n-propylamine
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
621-64-7
N-Nitrosodiphenylamine
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
86-30-6
Pentachlorophenol
ND ug/kg
1920
1
06/04/08 00:00
06/06/08 09:27
87-86-5
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 33 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-8 Lab ID: 9220393012 Collected: 05/28/08 15:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Phenanthrene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
85-01-8
Phenol
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
108-95-2
Pyrene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
129-00-0
1,2,4-Trichlorobenzene
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
120-82-1
2,4,5-Trichlorophenol
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
95-95-4
2,4,6-Trichlorophenol
ND ug/kg
385
1
06/04/08 00:00
06/06/08 09:27
88-06-2
Nitrobenzene-d5 (S)
73 %
30-150
1
06/04/08 00:00
06/06/08 09:27
4165-60-0
2-Fluorobiphenyl (S)
70 %
30-150
1
06/04/08 00:00
06/06/08 09:27
321-60-8
Terphenyl-d14 (S)
59 %
30-150
1
06/04/08 00:00
06/06/08 09:27
1718-51-0
Phenol-d6 (S)
66 %
30-150
1
06/04/08 00:00
06/06/08 09:27
13127-88-3
2-Fluorophenol (S)
76 %
30-150
1
06/04/08 00:00
06/06/08 09:27
367-12-4
2,4,6-Tribromophenol (S)
78 %
30-150
1
06/04/08 00:00
06/06/08 09:27
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND ug/kg
98.6
1
06/04/08 00:01
67-64-1
Benzene
ND ug/kg
4.9
1
06/04/08 00:01
71-43-2
Bromobenzene
ND ug/kg
4.9
1
06/04/08 00:01
108-86-1
Bromochloromethane
ND ug/kg
4.9
1
06/04/08 00:01
74-97-5
Bromodichloromethane
ND ug/kg
4.9
1
06/04/08 00:01
75-27-4
Bromoform
ND ug/kg
4.9
1
06/04/08 00:01
75-25-2
Bromomethane
ND ug/kg
9.9
1
06/04/08 00:01
74-83-9
2-Butanone (MEK)
ND ug/kg
98.6
1
06/04/08 00:01
78-93-3
n-Butylbenzene
ND ug/kg
4.9
1
06/04/08 00:01
104-51-8
sec-Butylbenzene
ND ug/kg
4.9
1
06/04/08 00:01
135-98-8
tert-Butyl benzene
ND ug/kg
4.9
1
06/04/08 00:01
98-06-6
Carbon tetrachloride
ND ug/kg
4.9
1
06/04/08 00:01
56-23-5
Chlorobenzene
ND ug/kg
4.9
1
06/04/08 00:01
108-90-7
Chloroethane
ND ug/kg
9.9
1
06/04/08 00:01
75-00-3
Chloroform
ND ug/kg
4.9
1
06/04/08 00:01
67-66-3
Chloromethane
ND ug/kg
9.9
1
06/04/08 00:01
74-87-3
2-Chlorotoluene
ND ug/kg
4.9
1
06/04/08 00:01
95-49-8
4-Chlorotoluene
ND ug/kg
4.9
1
06/04/08 00:01
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/kg
4.9
1
06/04/08 00:01
96-12-8
Dibromochloromethane
ND ug/kg
4.9
1
06/04/08 00:01
124-48-1
1,2-Dibromoethane (EDB)
ND ug/kg
4.9
1
06/04/08 00:01
106-93-4
Dibromomethane
ND ug/kg
4.9
1
06/04/08 00:01
74-95-3
1,2-Dichlorobenzene
ND ug/kg
4.9
1
06/04/08 00:01
95-50-1
1,3-Dichlorobenzene
ND ug/kg
4.9
1
06/04/08 00:01
541-73-1
1,4-Dichlorobenzene
ND ug/kg
4.9
1
06/04/08 00:01
106-46-7
Dichlorodifluoromethane
ND ug/kg
9.9
1
06/04/08 00:01
75-71-8
1,1-Dichloroethane
ND ug/kg
4.9
1
06/04/08 00:01
75-34-3
1,2-Dichloroethane
ND ug/kg
4.9
1
06/04/08 00:01
107-06-2
1,1-Dichloroethene
ND ug/kg
4.9
1
06/04/08 00:01
75-35-4
cis-1,2-Dichloroethene
ND ug/kg
4.9
1
06/04/08 00:01
156-59-2
trans-1,2-Dichloroethene
ND ug/kg
4.9
1
06/04/08 00:01
156-60-5
1,2-Dichloropropane
ND ug/kg
4.9
1
06/04/08 00:01
78-87-5
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY
ANALYSIS
Page 34 of 97
This report shall
not be reproduced, except
in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-8 Lab ID: 9220393012 Collected: 05/28/08 15:00 Received: 05/29/08 13:00 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,3-Dichloropropane
ND ug/kg
4.9
1
06/04/08 00:01
142-28-9
2,2-Dichloropropane
ND ug/kg
4.9
1
06/04/08 00:01
594-20-7
1,1-Dichloropropene
ND ug/kg
4.9
1
06/04/08 00:01
563-58-6
cis-1,3-Dichloropropene
ND ug/kg
4.9
1
06/04/08 00:01
10061-01-5
trans- 1,3-Dichloropropene
ND ug/kg
4.9
1
06/04/08 00:01
10061-02-6
Diisopropyl ether
ND ug/kg
4.9
1
06/04/08 00:01
108-20-3
Ethylbenzene
ND ug/kg
4.9
1
06/04/08 00:01
100-41-4
Hexachloro-1,3-butadiene
ND ug/kg
4.9
1
06/04/08 00:01
87-68-3
2-Hexanone
ND ug/kg
49.3
1
06/04/08 00:01
591-78-6
Isopropylbenzene (Cumene)
ND ug/kg
4.9
1
06/04/08 00:01
98-82-8
p-Isopropyltoluene
ND ug/kg
4.9
1
06/04/08 00:01
99-87-6
Methylene Chloride
ND ug/kg
4.9
1
06/04/08 00:01
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/kg
49.3
1
06/04/08 00:01
108-10-1
Methyl-tert-butyl ether
ND ug/kg
4.9
1
06/04/08 00:01
1634-04-4
Naphthalene
ND ug/kg
4.9
1
06/04/08 00:01
91-20-3
n-Propylbenzene
ND ug/kg
4.9
1
06/04/08 00:01
103-65-1
Styrene
ND ug/kg
4.9
1
06/04/08 00:01
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/kg
4.9
1
06/04/08 00:01
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/kg
4.9
1
06/04/08 00:01
79-34-5
Tetrachloroethene
ND ug/kg
4.9
1
06/04/08 00:01
127-18-4
Toluene
ND ug/kg
4.9
1
06/04/08 00:01
108-88-3
1,2,3-Trichlorobenzene
ND ug/kg
4.9
1
06/04/08 00:01
87-61-6
1,2,4-Trichlorobenzene
ND ug/kg
4.9
1
06/04/08 00:01
120-82-1
1,1,1-Trichloroethane
ND ug/kg
4.9
1
06/04/08 00:01
71-55-6
1,1,2-Trichloroethane
ND ug/kg
4.9
1
06/04/08 00:01
79-00-5
Trichloroethene
ND ug/kg
4.9
1
06/04/08 00:01
79-01-6
Trichlorofluoromethane
ND ug/kg
4.9
1
06/04/08 00:01
75-69-4
1,2,3-Trichloropropane
ND ug/kg
4.9
1
06/04/08 00:01
96-18-4
1,2,4-Trimethylbenzene
ND ug/kg
4.9
1
06/04/08 00:01
95-63-6
1,3,5-Trimethylbenzene
ND ug/kg
4.9
1
06/04/08 00:01
108-67-8
Vinyl acetate
ND ug/kg
49.3
1
06/04/08 00:01
108-05-4
Vinyl chloride
ND ug/kg
9.9
1
06/04/08 00:01
75-01-4
Xylene (Total)
ND ug/kg
14.8
1
06/04/08 00:01
1330-20-7
m&p-Xylene
ND ug/kg
9.9
1
06/04/08 00:01
1330-20-7
o-Xylene
ND ug/kg
4.9
1
06/04/08 00:01
95-47-6
Dibromofluoromethane (S)
109 %
79-116
1
06/04/08 00:01
1868-53-7
Toluene-d8 (S)
104 %
88-110
1
06/04/08 00:01
2037-26-5
4-Bromofluorobenzene (S)
95 %
74-115
1
06/04/08 00:01
460-00-4
1,2-Dichloroethane-d4 (S)
109 %
69-121
1
06/04/08 00:01
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
14.2 %
0.10
1
06/02/08 09:12
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 35 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-12 Lab ID: 9220393013 Collected: 05/28/08 14:20 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:33
7440-36-0
Arsenic
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:33
7440-38-2
Beryllium
ND ug/L
1.0
1
06/02/08 10:25
06/02/08 18:33
7440-41-7
Cadmium
ND ug/L
1.0
1
06/02/08 10:25
06/02/08 18:33
7440-43-9
Chromium
8.8 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:33
7440-47-3
Copper
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:33
7440-50-8
Lead
5.8 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:33
7439-92-1
Manganese
20.2 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:33
7439-96-5
Nickel
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:33
7440-02-0
Selenium
ND ug/L
10.0
1
06/02/08 10:25
06/02/08 18:33
7782-49-2
Silver
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:33
7440-22-4
Thallium
ND ug/L
10.0
1
06/02/08 10:25
06/02/08 18:33
7440-28-0
Zinc
ND ug/L
10.0
1
06/02/08 10:25
06/02/08 18:33
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
06/05/0810:00
06/05/08 15:57
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
83-32-9
Acenaphthylene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
208-96-8
Aniline
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
62-53-3
Anthracene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
120-12-7
Benzo(a)anthracene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
56-55-3
Benzo(a)pyrene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
50-32-8
Benzo(b)fluoranthene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
205-99-2
Benzo(g,h,i)perylene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
191-24-2
Benzo(k)fluoranthene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
207-08-9
Benzoic acid
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 19:16
65-85-0
Benzyl alcohol
ND ug/L
25.3
1
05/31/08 00:00
06/07/08 19:16
100-51-6
4-Bromophenylphenyl ether
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
101-55-3
Butylbenzylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
85-68-7
4-ChIoro-3-methyl phenol
ND ug/L
25.3
1
05/31/08 00:00
06/07/08 19:16
59-50-7
4-Chloroaniline
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 19:16
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
108-60-1
2-Chloronaphthalene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
91-58-7
2-Chlorophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
7005-72-3
Chrysene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
218-01-9
Dibenz(a,h)anthracene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
53-70-3
Dibenzofuran
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
132-64-9
1,2-Dichlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
95-50-1
1,3-Dichlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
541-73-1
1,4-Dichlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 19:16
91-94-1
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 36 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-12 Lab ID: 9220393013 Collected: 05/28/08 14:20 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
[phone]
2,4-Dichlorophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
120-83-2
Diethylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
84-66-2
2,4-Dimethylphenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
105-67-9
Dimethylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
131-11-3
Di-n-butylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
25.3
1
05/31/08 00:00
06/07/08 19:16
534-52-1
2,4-Dinitrophenol
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 19:16
51-28-5
2,4-Dinitrotoluene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
121-14-2
2,6-Dinitrotoluene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
606-20-2
Di-n-octylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
117-84-0
1,2-Diphenylhydrazine
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
117-81-7
Fluoranthene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
206-44-0
Fluorene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
87-68-3
Hexachlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
118-74-1
Hexachlorocyclopentadiene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
77-47-4
Hexachloroethane
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
193-39-5
Isophorone
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
78-59-1
1-Methylnaphthalene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
90-12-0
2-Methylnaphthalene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
Naphthalene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
91-20-3
2-Nitroaniline
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 19:16
88-74-4
3-Nitroaniline
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 19:16
99-09-2
4-Nitroaniline
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 19:16
100-01-6
Nitrobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
98-95-3
2-Nitrophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
88-75-5
4-Nitrophenol
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 19:16
100-02-7
N-Nitrosodimethylamine
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
621-64-7
N-Nitrosodiphenylamine
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
86-30-6
Pentachlorophenol
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 19:16
87-86-5
Phenanthrene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
85-01-8
Phenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
108-95-2
Pyrene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
120-82-1
2,4,5-Trichlorophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
95-95-4
2,4,6-Trichlorophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 19:16
88-06-2
Nitrobenzene-d5 (S)
72 %
30-150
1
05/31/08 00:00
06/07/08 19:16
4165-60-0
2-Fluorobiphenyl (S)
86 %
30-150
1
05/31/08 00:00
06/07/08 19:16
321-60-8
Terphenyl-d14 (S)
91 %
30-150
1
05/31/08 00:00
06/07/08 19:16
1718-51-0
Phenol-d6 (S)
30 %
25-150
1
05/31/08 00:00
06/07/08 19:16
13127-88-3
2-Fluorophenol (S)
41 %
25-150
1
05/31/08 00:00
06/07/08 19:16
367-12-4
2,4,6-Tribromophenol (S)
83 %
25-150
1
05/31/08 00:00
06/07/08 19:16
118-79-6
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 37 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-12 Lab ID: 9220393013 Collected: 05/28/08 14:20 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/31/08 18:52
67-64-1
Benzene
ND ug/L
1.0
1
05/31/08 18:52
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/31/08 18:52
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/31/08 18:52
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/31/08 18:52
75-27-4
Bromoform
ND ug/L
1.0
1
05/31/08 18:52
75-25-2
Bromomethane
ND ug/L
5.0
1
05/31/08 18:52
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/31/08 18:52
78-93-3
n-Butylbenzene
ND ug/L
1.0
1
05/31/08 18:52
104-51-8
sec-Butylbenzene
ND ug/L
1.0
1
05/31/08 18:52
135-98-8
tert-Butyl benzene
ND ug/L
1.0
1
05/31/08 18:52
98-06-6
Carbon tetrachloride
ND ug/L
1.0
1
05/31/08 18:52
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/31/08 18:52
108-90-7
Chloroethane
ND ug/L
1.0
1
05/31/08 18:52
75-00-3
Chloroform
ND ug/L
1.0
1
05/31/08 18:52
67-66-3
Chloromethane
ND ug/L
1.0
1
05/31/08 18:52
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/31/08 18:52
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/31/08 18:52
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
3.0
1
05/31/08 18:52
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/31/08 18:52
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/31/08 18:52
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/31/08 18:52
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 18:52
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 18:52
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 18:52
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/31/08 18:52
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/31/08 18:52
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/31/08 18:52
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/31/08 18:52
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 18:52
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 18:52
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 18:52
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/31/08 18:52
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 18:52
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/31/08 18:52
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 18:52
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 18:52
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/31/08 18:52
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/31/08 18:52
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/31/08 18:52
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/31/08 18:52
591-78-6
Isopropylbenzene (Cumene)
ND ug/L
1.0
1
05/31/08 18:52
98-82-8
p-Isopropyltoluene
ND ug/L
1.0
1
05/31/08 18:52
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/31/08 18:52
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/31/08 18:52
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/31/08 18:52
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/31/08 18:52
91-20-3
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 38 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-12 Lab ID: 9220393013 Collected: 05/28/08 14:20 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
n-Propylbenzene
ND ug/L
1.0
1
05/31/08 18:52
103-65-1
Styrene
ND ug/L
1.0
1
05/31/08 18:52
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 18:52
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 18:52
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/31/08 18:52
127-18-4
Toluene
ND ug/L
1.0
1
05/31/08 18:52
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 18:52
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 18:52
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/31/08 18:52
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/31/08 18:52
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/31/08 18:52
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/31/08 18:52
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/31/08 18:52
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 18:52
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 18:52
108-67-8
Vinyl acetate
ND ug/L
2.0
1
05/31/08 18:52
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/31/08 18:52
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/31/08 18:52
1330-20-7
o-Xylene
ND ug/L
1.0
1
05/31/08 18:52
95-47-6
4-Bromofluorobenzene (S)
101 %
87-109
1
05/31/08 18:52
460-00-4
Dibromofluoromethane (S)
105 %
85-115
1
05/31/08 18:52
1868-53-7
1,2-Dichloroethane-d4 (S)
102 %
79-120
1
05/31/08 18:52
17060-07-0
Toluene-d8(S)
100 %
70-120
1
05/31/08 18:52
2037-26-5
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 39 of 97

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-13 Lab ID: 9220393014 Collected: 05/28/08 14:00 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:44
7440-36-0
Arsenic
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:44
7440-38-2
Beryllium
ND ug/L
1.0
1
06/02/08 10:25
06/02/08 18:44
7440-41-7
Cadmium
ND ug/L
1.0
1
06/02/08 10:25
06/02/08 18:44
7440-43-9
Chromium
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:44
7440-47-3
Copper
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:44
7440-50-8
Lead
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:44
7439-92-1
Manganese
65.4 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:44
7439-96-5
Nickel
9.9 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:44
7440-02-0
Selenium
11.5 ug/L
10.0
1
06/02/08 10:25
06/02/08 18:44
7782-49-2
Silver
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:44
7440-22-4
Thallium
ND ug/L
10.0
1
06/02/08 10:25
06/02/08 18:44
7440-28-0
Zinc
ND ug/L
10.0
1
06/02/08 10:25
06/02/08 18:44
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
06/05/0810:00
06/05/08 16:05
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
83-32-9
Acenaphthylene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
208-96-8
Aniline
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
62-53-3
Anthracene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
120-12-7
Benzo(a)anthracene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
56-55-3
Benzo(a)pyrene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
50-32-8
Benzo(b)fluoranthene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
205-99-2
Benzo(g,h,i)perylene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
191-24-2
Benzo(k)fluoranthene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
207-08-9
Benzoic acid
ND ug/L
73.5
1
05/31/08 00:00
06/07/08 19:38
65-85-0
Benzyl alcohol
ND ug/L
29.4
1
05/31/08 00:00
06/07/08 19:38
100-51-6
4-Bromophenylphenyl ether
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
101-55-3
Butylbenzylphthalate
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
85-68-7
4-ChIoro-3-methyl phenol
ND ug/L
29.4
1
05/31/08 00:00
06/07/08 19:38
59-50-7
4-Chloroaniline
ND ug/L
73.5
1
05/31/08 00:00
06/07/08 19:38
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
108-60-1
2-Chloronaphthalene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
91-58-7
2-Chlorophenol
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
7005-72-3
Chrysene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
218-01-9
Dibenz(a,h)anthracene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
53-70-3
Dibenzofuran
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
132-64-9
1,2-Dichlorobenzene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
95-50-1
1,3-Dichlorobenzene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
541-73-1
1,4-Dichlorobenzene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
73.5
1
05/31/08 00:00
06/07/08 19:38
91-94-1
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 40 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-13 Lab ID: 9220393014 Collected: 05/28/08 14:00 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
[phone]
2,4-Dichlorophenol
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
120-83-2
Diethylphthalate
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
84-66-2
2,4-Dimethylphenol
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
105-67-9
Dimethylphthalate
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
131-11-3
Di-n-butylphthalate
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
29.4
1
05/31/08 00:00
06/07/08 19:38
534-52-1
2,4-Dinitrophenol
ND ug/L
73.5
1
05/31/08 00:00
06/07/08 19:38
51-28-5
2,4-Dinitrotoluene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
121-14-2
2,6-Dinitrotoluene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
606-20-2
Di-n-octylphthalate
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
117-84-0
1,2-Diphenylhydrazine
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
117-81-7
Fluoranthene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
206-44-0
Fluorene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
87-68-3
Hexachlorobenzene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
118-74-1
Hexachlorocyclopentadiene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
77-47-4
Hexachloroethane
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
193-39-5
Isophorone
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
78-59-1
1-Methylnaphthalene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
90-12-0
2-Methylnaphthalene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
Naphthalene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
91-20-3
2-Nitroaniline
ND ug/L
73.5
1
05/31/08 00:00
06/07/08 19:38
88-74-4
3-Nitroaniline
ND ug/L
73.5
1
05/31/08 00:00
06/07/08 19:38
99-09-2
4-Nitroaniline
ND ug/L
73.5
1
05/31/08 00:00
06/07/08 19:38
100-01-6
Nitrobenzene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
98-95-3
2-Nitrophenol
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
88-75-5
4-Nitrophenol
ND ug/L
73.5
1
05/31/08 00:00
06/07/08 19:38
100-02-7
N-Nitrosodimethylamine
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
621-64-7
N-Nitrosodiphenylamine
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
86-30-6
Pentachlorophenol
ND ug/L
73.5
1
05/31/08 00:00
06/07/08 19:38
87-86-5
Phenanthrene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
85-01-8
Phenol
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
108-95-2
Pyrene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
120-82-1
2,4,5-Trichlorophenol
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
95-95-4
2,4,6-Trichlorophenol
ND ug/L
14.7
1
05/31/08 00:00
06/07/08 19:38
88-06-2
Nitrobenzene-d5 (S)
66 %
30-150
1
05/31/08 00:00
06/07/08 19:38
4165-60-0
2-Fluorobiphenyl (S)
71 %
30-150
1
05/31/08 00:00
06/07/08 19:38
321-60-8
Terphenyl-d14 (S)
77 %
30-150
1
05/31/08 00:00
06/07/08 19:38
1718-51-0
Phenol-d6 (S)
29 %
25-150
1
05/31/08 00:00
06/07/08 19:38
13127-88-3
2-Fluorophenol (S)
41 %
25-150
1
05/31/08 00:00
06/07/08 19:38
367-12-4
2,4,6-Tribromophenol (S)
71 %
25-150
1
05/31/08 00:00
06/07/08 19:38
118-79-6
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 41 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-13 Lab ID: 9220393014 Collected: 05/28/08 14:00 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/31/08 19:16
67-64-1
Benzene
ND ug/L
1.0
1
05/31/08 19:16
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/31/08 19:16
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/31/08 19:16
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/31/08 19:16
75-27-4
Bromoform
ND ug/L
1.0
1
05/31/08 19:16
75-25-2
Bromomethane
ND ug/L
5.0
1
05/31/08 19:16
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/31/08 19:16
78-93-3
n-Butylbenzene
ND ug/L
1.0
1
05/31/08 19:16
104-51-8
sec-Butylbenzene
ND ug/L
1.0
1
05/31/08 19:16
135-98-8
tert-Butyl benzene
ND ug/L
1.0
1
05/31/08 19:16
98-06-6
Carbon tetrachloride
ND ug/L
1.0
1
05/31/08 19:16
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/31/08 19:16
108-90-7
Chloroethane
ND ug/L
1.0
1
05/31/08 19:16
75-00-3
Chloroform
1.8 ug/L
1.0
1
05/31/08 19:16
67-66-3
Chloromethane
ND ug/L
1.0
1
05/31/08 19:16
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/31/08 19:16
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/31/08 19:16
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
3.0
1
05/31/08 19:16
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/31/08 19:16
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/31/08 19:16
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/31/08 19:16
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 19:16
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 19:16
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 19:16
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/31/08 19:16
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/31/08 19:16
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/31/08 19:16
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/31/08 19:16
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 19:16
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 19:16
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 19:16
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/31/08 19:16
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 19:16
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/31/08 19:16
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 19:16
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 19:16
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/31/08 19:16
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/31/08 19:16
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/31/08 19:16
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/31/08 19:16
591-78-6
Isopropylbenzene (Cumene)
ND ug/L
1.0
1
05/31/08 19:16
98-82-8
p-Isopropyltoluene
ND ug/L
1.0
1
05/31/08 19:16
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/31/08 19:16
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/31/08 19:16
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/31/08 19:16
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/31/08 19:16
91-20-3
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 42 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-13 Lab ID: 9220393014 Collected: 05/28/08 14:00 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
n-Propylbenzene
ND ug/L
1.0
1
05/31/08 19:16
103-65-1
Styrene
ND ug/L
1.0
1
05/31/08 19:16
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 19:16
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 19:16
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/31/08 19:16
127-18-4
Toluene
ND ug/L
1.0
1
05/31/08 19:16
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 19:16
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 19:16
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/31/08 19:16
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/31/08 19:16
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/31/08 19:16
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/31/08 19:16
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/31/08 19:16
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 19:16
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 19:16
108-67-8
Vinyl acetate
ND ug/L
2.0
1
05/31/08 19:16
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/31/08 19:16
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/31/08 19:16
1330-20-7
o-Xylene
ND ug/L
1.0
1
05/31/08 19:16
95-47-6
4-Bromofluorobenzene (S)
102 %
87-109
1
05/31/08 19:16
460-00-4
Dibromofluoromethane (S)
104 %
85-115
1
05/31/08 19:16
1868-53-7
1,2-Dichloroethane-d4 (S)
102 %
79-120
1
05/31/08 19:16
17060-07-0
Toluene-d8 (S)
99 %
70-120
1
05/31/08 19:16
2037-26-5
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 43 of 97

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-14 Lab ID: 9220393015 Collected: 05/28/08 15:00 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:48
7440-36-0
Arsenic
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:48
7440-38-2
Beryllium
ND ug/L
1.0
1
06/02/0810:25
06/02/08 18:48
7440-41-7
Cadmium
ND ug/L
1.0
1
06/02/0810:25
06/02/08 18:48
7440-43-9
Chromium
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:48
7440-47-3
Copper
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:48
7440-50-8
Lead
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:48
7439-92-1
Manganese
23.1 ug/L
5.0
1
06/02/0810:25
06/02/08 18:48
7439-96-5
Nickel
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:48
7440-02-0
Selenium
ND ug/L
10.0
1
06/02/0810:25
06/02/08 18:48
7782-49-2
Silver
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:48
7440-22-4
Thallium
ND ug/L
10.0
1
06/02/0810:25
06/02/08 18:48
7440-28-0
Zinc
ND ug/L
10.0
1
06/02/0810:25
06/02/08 18:48
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
06/05/0810:00
06/05/08 16:07
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
83-32-9
Acenaphthylene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
208-96-8
Aniline
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
62-53-3
Anthracene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
120-12-7
Benzo(a)anthracene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
56-55-3
Benzo(a)pyrene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
50-32-8
Benzo(b)fluoranthene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
205-99-2
Benzo(g,h,i)perylene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
191-24-2
Benzo(k)fluoranthene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
207-08-9
Benzoic acid
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 20:00
65-85-0
Benzyl alcohol
ND ug/L
25.3
1
05/31/08 00:00
06/07/08 20:00
100-51-6
4-Bromophenylphenyl ether
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
101-55-3
Butylbenzylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
85-68-7
4-ChIoro-3-methyl phenol
ND ug/L
25.3
1
05/31/08 00:00
06/07/08 20:00
59-50-7
4-Chloroaniline
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 20:00
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
108-60-1
2-Chloronaphthalene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
91-58-7
2-Chlorophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
7005-72-3
Chrysene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
218-01-9
Dibenz(a,h)anthracene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
53-70-3
Dibenzofuran
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
132-64-9
1,2-Dichlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
95-50-1
1,3-Dichlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
541-73-1
1,4-Dichlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 20:00
91-94-1
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 44 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-14 Lab ID: 9220393015 Collected: 05/28/08 15:00 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
[phone]
2,4-Dichlorophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
120-83-2
Diethylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
84-66-2
2,4-Dimethylphenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
105-67-9
Dimethylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
131-11-3
Di-n-butylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
25.3
1
05/31/08 00:00
06/07/08 20:00
534-52-1
2,4-Dinitrophenol
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 20:00
51-28-5
2,4-Dinitrotoluene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
121-14-2
2,6-Dinitrotoluene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
606-20-2
Di-n-octylphthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
117-84-0
1,2-Diphenylhydrazine
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
117-81-7
Fluoranthene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
206-44-0
Fluorene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
87-68-3
Hexachlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
118-74-1
Hexachlorocyclopentadiene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
77-47-4
Hexachloroethane
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
193-39-5
Isophorone
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
78-59-1
1-Methylnaphthalene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
90-12-0
2-Methylnaphthalene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
Naphthalene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
91-20-3
2-Nitroaniline
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 20:00
88-74-4
3-Nitroaniline
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 20:00
99-09-2
4-Nitroaniline
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 20:00
100-01-6
Nitrobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
98-95-3
2-Nitrophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
88-75-5
4-Nitrophenol
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 20:00
100-02-7
N-Nitrosodimethylamine
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
621-64-7
N-Nitrosodiphenylamine
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
86-30-6
Pentachlorophenol
ND ug/L
63.3
1
05/31/08 00:00
06/07/08 20:00
87-86-5
Phenanthrene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
85-01-8
Phenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
108-95-2
Pyrene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
120-82-1
2,4,5-Trichlorophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
95-95-4
2,4,6-Trichlorophenol
ND ug/L
12.7
1
05/31/08 00:00
06/07/08 20:00
88-06-2
Nitrobenzene-d5 (S)
61 %
30-150
1
05/31/08 00:00
06/07/08 20:00
4165-60-0
2-Fluorobiphenyl (S)
68 %
30-150
1
05/31/08 00:00
06/07/08 20:00
321-60-8
Terphenyl-d14 (S)
83 %
30-150
1
05/31/08 00:00
06/07/08 20:00
1718-51-0
Phenol-d6 (S)
24 %
25-150
1
05/31/08 00:00
06/07/08 20:00
13127-88-3 1g
2-Fluorophenol (S)
36 %
25-150
1
05/31/08 00:00
06/07/08 20:00
367-12-4
2,4,6-Tribromophenol (S)
69 %
25-150
1
05/31/08 00:00
06/07/08 20:00
118-79-6
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 45 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-14 Lab ID: 9220393015 Collected: 05/28/08 15:00 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/31/08 19:40
67-64-1
Benzene
ND ug/L
1.0
1
05/31/08 19:40
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/31/08 19:40
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/31/08 19:40
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/31/08 19:40
75-27-4
Bromoform
ND ug/L
1.0
1
05/31/08 19:40
75-25-2
Bromomethane
ND ug/L
5.0
1
05/31/08 19:40
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/31/08 19:40
78-93-3
n-Butylbenzene
ND ug/L
1.0
1
05/31/08 19:40
104-51-8
sec-Butylbenzene
ND ug/L
1.0
1
05/31/08 19:40
135-98-8
tert-Butyl benzene
ND ug/L
1.0
1
05/31/08 19:40
98-06-6
Carbon tetrachloride
ND ug/L
1.0
1
05/31/08 19:40
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/31/08 19:40
108-90-7
Chloroethane
ND ug/L
1.0
1
05/31/08 19:40
75-00-3
Chloroform
ND ug/L
1.0
1
05/31/08 19:40
67-66-3
Chloromethane
ND ug/L
1.0
1
05/31/08 19:40
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/31/08 19:40
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/31/08 19:40
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
3.0
1
05/31/08 19:40
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/31/08 19:40
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/31/08 19:40
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/31/08 19:40
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 19:40
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 19:40
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 19:40
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/31/08 19:40
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/31/08 19:40
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/31/08 19:40
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/31/08 19:40
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 19:40
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 19:40
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 19:40
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/31/08 19:40
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 19:40
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/31/08 19:40
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 19:40
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 19:40
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/31/08 19:40
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/31/08 19:40
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/31/08 19:40
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/31/08 19:40
591-78-6
Isopropylbenzene (Cumene)
ND ug/L
1.0
1
05/31/08 19:40
98-82-8
p-Isopropyltoluene
ND ug/L
1.0
1
05/31/08 19:40
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/31/08 19:40
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/31/08 19:40
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/31/08 19:40
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/31/08 19:40
91-20-3
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 46 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-14 Lab ID: 9220393015 Collected: 05/28/08 15:00 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
n-Propylbenzene
ND ug/L
1.0
1
05/31/08 19:40
103-65-1
Styrene
ND ug/L
1.0
1
05/31/08 19:40
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 19:40
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 19:40
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/31/08 19:40
127-18-4
Toluene
ND ug/L
1.0
1
05/31/08 19:40
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 19:40
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 19:40
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/31/08 19:40
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/31/08 19:40
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/31/08 19:40
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/31/08 19:40
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/31/08 19:40
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 19:40
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 19:40
108-67-8
Vinyl acetate
ND ug/L
2.0
1
05/31/08 19:40
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/31/08 19:40
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/31/08 19:40
1330-20-7
o-Xylene
ND ug/L
1.0
1
05/31/08 19:40
95-47-6
4-Bromofluorobenzene (S)
101 %
87-109
1
05/31/08 19:40
460-00-4
Dibromofluoromethane (S)
101 %
85-115
1
05/31/08 19:40
1868-53-7
1,2-Dichloroethane-d4 (S)
94 %
79-120
1
05/31/08 19:40
17060-07-0
Toluene-d8 (S)
98 %
70-120
1
05/31/08 19:40
2037-26-5
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 47 of 97

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-15 Lab ID: 9220393016 Collected: 05/28/08 13:40 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:52
7440-36-0
Arsenic
90.4 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:52
7440-38-2
Beryllium
ND ug/L
1.0
1
06/02/08 10:25
06/02/08 18:52
7440-41-7
Cadmium
ND ug/L
1.0
1
06/02/08 10:25
06/02/08 18:52
7440-43-9
Chromium
5.5 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:52
7440-47-3
Copper
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:52
7440-50-8
Lead
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:52
7439-92-1
Manganese
99.3 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:52
7439-96-5
Nickel
9.4 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:52
7440-02-0
Selenium
ND ug/L
10.0
1
06/02/08 10:25
06/02/08 18:52
7782-49-2
Silver
ND ug/L
5.0
1
06/02/08 10:25
06/02/08 18:52
7440-22-4
Thallium
ND ug/L
10.0
1
06/02/08 10:25
06/02/08 18:52
7440-28-0
Zinc
22.1 ug/L
10.0
1
06/02/08 10:25
06/02/08 18:52
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
06/05/0810:00
06/05/08 16:10
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
83-32-9
Acenaphthylene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
208-96-8
Aniline
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
62-53-3
Anthracene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
120-12-7
Benzo(a)anthracene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
56-55-3
Benzo(a)pyrene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
50-32-8
Benzo(b)fluoranthene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
205-99-2
Benzo(g,h,i)perylene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
191-24-2
Benzo(k)fluoranthene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
207-08-9
Benzoic acid
ND ug/L
79.4
1
05/31/08 00:00
06/07/08 20:22
65-85-0
Benzyl alcohol
ND ug/L
31.7
1
05/31/08 00:00
06/07/08 20:22
100-51-6
4-Bromophenylphenyl ether
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
101-55-3
Butylbenzylphthalate
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
85-68-7
4-ChIoro-3-methyl phenol
ND ug/L
31.7
1
05/31/08 00:00
06/07/08 20:22
59-50-7
4-Chloroaniline
ND ug/L
79.4
1
05/31/08 00:00
06/07/08 20:22
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
108-60-1
2-Chloronaphthalene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
91-58-7
2-Chlorophenol
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
7005-72-3
Chrysene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
218-01-9
Dibenz(a,h)anthracene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
53-70-3
Dibenzofuran
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
132-64-9
1,2-Dichlorobenzene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
95-50-1
1,3-Dichlorobenzene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
541-73-1
1,4-Dichlorobenzene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
79.4
1
05/31/08 00:00
06/07/08 20:22
91-94-1
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 48 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-15 Lab ID: 9220393016 Collected: 05/28/08 13:40 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
[phone]
2,4-Dichlorophenol
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
120-83-2
Diethylphthalate
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
84-66-2
2,4-Dimethylphenol
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
105-67-9
Dimethylphthalate
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
131-11-3
Di-n-butylphthalate
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
31.7
1
05/31/08 00:00
06/07/08 20:22
534-52-1
2,4-Dinitrophenol
ND ug/L
79.4
1
05/31/08 00:00
06/07/08 20:22
51-28-5
2,4-Dinitrotoluene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
121-14-2
2,6-Dinitrotoluene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
606-20-2
Di-n-octylphthalate
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
117-84-0
1,2-Diphenylhydrazine
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
117-81-7
Fluoranthene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
206-44-0
Fluorene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
87-68-3
Hexachlorobenzene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
118-74-1
Hexachlorocyclopentadiene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
77-47-4
Hexachloroethane
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
193-39-5
Isophorone
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
78-59-1
1-Methylnaphthalene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
90-12-0
2-Methylnaphthalene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
Naphthalene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
91-20-3
2-Nitroaniline
ND ug/L
79.4
1
05/31/08 00:00
06/07/08 20:22
88-74-4
3-Nitroaniline
ND ug/L
79.4
1
05/31/08 00:00
06/07/08 20:22
99-09-2
4-Nitroaniline
ND ug/L
79.4
1
05/31/08 00:00
06/07/08 20:22
100-01-6
Nitrobenzene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
98-95-3
2-Nitrophenol
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
88-75-5
4-Nitrophenol
ND ug/L
79.4
1
05/31/08 00:00
06/07/08 20:22
100-02-7
N-Nitrosodimethylamine
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
621-64-7
N-Nitrosodiphenylamine
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
86-30-6
Pentachlorophenol
ND ug/L
79.4
1
05/31/08 00:00
06/07/08 20:22
87-86-5
Phenanthrene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
85-01-8
Phenol
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
108-95-2
Pyrene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
120-82-1
2,4,5-Trichlorophenol
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
95-95-4
2,4,6-Trichlorophenol
ND ug/L
15.9
1
05/31/08 00:00
06/07/08 20:22
88-06-2
Nitrobenzene-d5 (S)
55 %
30-150
1
05/31/08 00:00
06/07/08 20:22
4165-60-0
2-Fluorobiphenyl (S)
58 %
30-150
1
05/31/08 00:00
06/07/08 20:22
321-60-8
Terphenyl-d14 (S)
65 %
30-150
1
05/31/08 00:00
06/07/08 20:22
1718-51-0
Phenol-d6 (S)
25 %
25-150
1
05/31/08 00:00
06/07/08 20:22
13127-88-3
2-Fluorophenol (S)
35 %
25-150
1
05/31/08 00:00
06/07/08 20:22
367-12-4
2,4,6-Tribromophenol (S)
55 %
25-150
1
05/31/08 00:00
06/07/08 20:22
118-79-6
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 49 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-15 Lab ID: 9220393016 Collected: 05/28/08 13:40 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/31/08 20:03
67-64-1
Benzene
ND ug/L
1.0
1
05/31/08 20:03
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/31/08 20:03
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/31/08 20:03
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/31/08 20:03
75-27-4
Bromoform
ND ug/L
1.0
1
05/31/08 20:03
75-25-2
Bromomethane
ND ug/L
5.0
1
05/31/08 20:03
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/31/08 20:03
78-93-3
n-Butylbenzene
ND ug/L
1.0
1
05/31/08 20:03
104-51-8
sec-Butylbenzene
ND ug/L
1.0
1
05/31/08 20:03
135-98-8
tert-Butyl benzene
ND ug/L
1.0
1
05/31/08 20:03
98-06-6
Carbon tetrachloride
ND ug/L
1.0
1
05/31/08 20:03
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/31/08 20:03
108-90-7
Chloroethane
ND ug/L
1.0
1
05/31/08 20:03
75-00-3
Chloroform
ND ug/L
1.0
1
05/31/08 20:03
67-66-3
Chloromethane
ND ug/L
1.0
1
05/31/08 20:03
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/31/08 20:03
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/31/08 20:03
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
3.0
1
05/31/08 20:03
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/31/08 20:03
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/31/08 20:03
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/31/08 20:03
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 20:03
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 20:03
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 20:03
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/31/08 20:03
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/31/08 20:03
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/31/08 20:03
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/31/08 20:03
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 20:03
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 20:03
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 20:03
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/31/08 20:03
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 20:03
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/31/08 20:03
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 20:03
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 20:03
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/31/08 20:03
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/31/08 20:03
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/31/08 20:03
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/31/08 20:03
591-78-6
Isopropylbenzene (Cumene)
ND ug/L
1.0
1
05/31/08 20:03
98-82-8
p-Isopropyltoluene
ND ug/L
1.0
1
05/31/08 20:03
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/31/08 20:03
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/31/08 20:03
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/31/08 20:03
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/31/08 20:03
91-20-3
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 50 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-15 Lab ID: 9220393016 Collected: 05/28/08 13:40 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
n-Propylbenzene
ND ug/L
1.0
1
05/31/08 20:03
103-65-1
Styrene
ND ug/L
1.0
1
05/31/08 20:03
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 20:03
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 20:03
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/31/08 20:03
127-18-4
Toluene
ND ug/L
1.0
1
05/31/08 20:03
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 20:03
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 20:03
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/31/08 20:03
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/31/08 20:03
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/31/08 20:03
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/31/08 20:03
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/31/08 20:03
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 20:03
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 20:03
108-67-8
Vinyl acetate
ND ug/L
2.0
1
05/31/08 20:03
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/31/08 20:03
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/31/08 20:03
1330-20-7
o-Xylene
ND ug/L
1.0
1
05/31/08 20:03
95-47-6
4-Bromofluorobenzene (S)
101 %
87-109
1
05/31/08 20:03
460-00-4
Dibromofluoromethane (S)
105 %
85-115
1
05/31/08 20:03
1868-53-7
1,2-Dichloroethane-d4 (S)
102 %
79-120
1
05/31/08 20:03
17060-07-0
Toluene-d8 (S)
99 %
70-120
1
05/31/08 20:03
2037-26-5
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 51 of 97

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-17 Lab ID: 9220393017 Collected: 05/28/08 12:45 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:56
7440-36-0
Arsenic
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:56
7440-38-2
Beryllium
ND ug/L
1.0
1
06/02/0810:25
06/02/08 18:56
7440-41-7
Cadmium
ND ug/L
1.0
1
06/02/0810:25
06/02/08 18:56
7440-43-9
Chromium
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:56
7440-47-3
Copper
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:56
7440-50-8
Lead
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:56
7439-92-1
Manganese
6.8 ug/L
5.0
1
06/02/08 10:25
06/02/08 18:56
7439-96-5
Nickel
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:56
7440-02-0
Selenium
ND ug/L
10.0
1
06/02/0810:25
06/02/08 18:56
7782-49-2
Silver
ND ug/L
5.0
1
06/02/0810:25
06/02/08 18:56
7440-22-4
Thallium
ND ug/L
10.0
1
06/02/0810:25
06/02/08 18:56
7440-28-0
Zinc
ND ug/L
10.0
1
06/02/0810:25
06/02/08 18:56
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
06/05/0810:00
06/05/08 16:12
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Acenaphthene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
83-32-9
Acenaphthylene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
208-96-8
Aniline
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
62-53-3
Anthracene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
120-12-7
Benzo(a)anthracene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
56-55-3
Benzo(a)pyrene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
50-32-8
Benzo(b)fluoranthene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
205-99-2
Benzo(g,h,i)perylene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
191-24-2
Benzo(k)fluoranthene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
207-08-9
Benzoic acid
ND ug/L
58.1
1
05/31/08 00:00
06/07/08 20:43
65-85-0
Benzyl alcohol
ND ug/L
23.3
1
05/31/08 00:00
06/07/08 20:43
100-51-6
4-Bromophenylphenyl ether
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
101-55-3
Butylbenzylphthalate
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
85-68-7
4-ChIoro-3-methyl phenol
ND ug/L
23.3
1
05/31/08 00:00
06/07/08 20:43
59-50-7
4-Chloroaniline
ND ug/L
58.1
1
05/31/08 00:00
06/07/08 20:43
106-47-8
bis(2-Chloroethoxy)methane
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
108-60-1
2-Chloronaphthalene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
91-58-7
2-Chlorophenol
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
7005-72-3
Chrysene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
218-01-9
Dibenz(a,h)anthracene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
53-70-3
Dibenzofuran
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
132-64-9
1,2-Dichlorobenzene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
95-50-1
1,3-Dichlorobenzene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
541-73-1
1,4-Dichlorobenzene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
106-46-7
3,3'-Dichlorobenzidine
ND ug/L
58.1
1
05/31/08 00:00
06/07/08 20:43
91-94-1
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 52 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
ANALYTICAL RESULTS
[phone]
Sample: SB-17 Lab ID: 9220393017 Collected: 05/28/08 12:45 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
[phone]
2,4-Dichlorophenol
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
120-83-2
Diethylphthalate
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
84-66-2
2,4-Dimethylphenol
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
105-67-9
Dimethylphthalate
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
131-11-3
Di-n-butylphthalate
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
84-74-2
4,6-Dinitro-2-methyl phenol
ND ug/L
23.3
1
05/31/08 00:00
06/07/08 20:43
534-52-1
2,4-Dinitrophenol
ND ug/L
58.1
1
05/31/08 00:00
06/07/08 20:43
51-28-5
2,4-Dinitrotoluene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
121-14-2
2,6-Dinitrotoluene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
606-20-2
Di-n-octylphthalate
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
117-84-0
1,2-Diphenylhydrazine
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
122-66-7
bis(2- Ethyl hexyl)phthalate
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
117-81-7
Fluoranthene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
206-44-0
Fluorene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
86-73-7
Hexachloro-1,3-butadiene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
87-68-3
Hexachlorobenzene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
118-74-1
Hexachlorocyclopentadiene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
77-47-4
Hexachloroethane
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
193-39-5
Isophorone
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
78-59-1
1-Methylnaphthalene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
90-12-0
2-Methylnaphthalene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
91-57-6
2-Methylphenol(o-Cresol)
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
Naphthalene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
91-20-3
2-Nitroaniline
ND ug/L
58.1
1
05/31/08 00:00
06/07/08 20:43
88-74-4
3-Nitroaniline
ND ug/L
58.1
1
05/31/08 00:00
06/07/08 20:43
99-09-2
4-Nitroaniline
ND ug/L
58.1
1
05/31/08 00:00
06/07/08 20:43
100-01-6
Nitrobenzene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
98-95-3
2-Nitrophenol
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
88-75-5
4-Nitrophenol
ND ug/L
58.1
1
05/31/08 00:00
06/07/08 20:43
100-02-7
N-Nitrosodimethylamine
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
621-64-7
N-Nitrosodiphenylamine
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
86-30-6
Pentachlorophenol
ND ug/L
58.1
1
05/31/08 00:00
06/07/08 20:43
87-86-5
Phenanthrene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
85-01-8
Phenol
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
108-95-2
Pyrene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
120-82-1
2,4,5-Trichlorophenol
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
95-95-4
2,4,6-Trichlorophenol
ND ug/L
11.6
1
05/31/08 00:00
06/07/08 20:43
88-06-2
Nitrobenzene-d5 (S)
70 %
30-150
1
05/31/08 00:00
06/07/08 20:43
4165-60-0
2-Fluorobiphenyl (S)
78 %
30-150
1
05/31/08 00:00
06/07/08 20:43
321-60-8
Terphenyl-d14 (S)
88 %
30-150
1
05/31/08 00:00
06/07/08 20:43
1718-51-0
Phenol-d6 (S)
28 %
25-150
1
05/31/08 00:00
06/07/08 20:43
13127-88-3
2-Fluorophenol (S)
39 %
25-150
1
05/31/08 00:00
06/07/08 20:43
367-12-4
2,4,6-Tribromophenol (S)
74 %
25-150
1
05/31/08 00:00
06/07/08 20:43
118-79-6
Qual
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 53 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-17 Lab ID: 9220393017 Collected: 05/28/08 12:45 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
1
05/31/08 20:27
67-64-1
Benzene
ND ug/L
1.0
1
05/31/08 20:27
71-43-2
Bromobenzene
ND ug/L
1.0
1
05/31/08 20:27
108-86-1
Bromochloromethane
ND ug/L
1.0
1
05/31/08 20:27
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
05/31/08 20:27
75-27-4
Bromoform
ND ug/L
1.0
1
05/31/08 20:27
75-25-2
Bromomethane
ND ug/L
5.0
1
05/31/08 20:27
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
05/31/08 20:27
78-93-3
n-Butylbenzene
ND ug/L
1.0
1
05/31/08 20:27
104-51-8
sec-Butylbenzene
ND ug/L
1.0
1
05/31/08 20:27
135-98-8
tert-Butyl benzene
ND ug/L
1.0
1
05/31/08 20:27
98-06-6
Carbon tetrachloride
ND ug/L
1.0
1
05/31/08 20:27
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/31/08 20:27
108-90-7
Chloroethane
ND ug/L
1.0
1
05/31/08 20:27
75-00-3
Chloroform
ND ug/L
1.0
1
05/31/08 20:27
67-66-3
Chloromethane
ND ug/L
1.0
1
05/31/08 20:27
74-87-3
2-Chlorotoluene
ND ug/L
1.0
1
05/31/08 20:27
95-49-8
4-Chlorotoluene
ND ug/L
1.0
1
05/31/08 20:27
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
3.0
1
05/31/08 20:27
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
05/31/08 20:27
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/31/08 20:27
106-93-4
Dibromomethane
ND ug/L
1.0
1
05/31/08 20:27
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 20:27
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 20:27
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/31/08 20:27
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
05/31/08 20:27
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
05/31/08 20:27
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
05/31/08 20:27
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
05/31/08 20:27
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 20:27
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/31/08 20:27
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 20:27
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
1
05/31/08 20:27
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
1
05/31/08 20:27
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
1
05/31/08 20:27
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 20:27
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
05/31/08 20:27
10061-02-6
Diisopropyl ether
ND ug/L
1.0
1
05/31/08 20:27
108-20-3
Ethylbenzene
ND ug/L
1.0
1
05/31/08 20:27
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
1
05/31/08 20:27
87-68-3
2-Hexanone
ND ug/L
5.0
1
05/31/08 20:27
591-78-6
Isopropylbenzene (Cumene)
ND ug/L
1.0
1
05/31/08 20:27
98-82-8
p-Isopropyltoluene
ND ug/L
1.0
1
05/31/08 20:27
99-87-6
Methylene Chloride
ND ug/L
2.0
1
05/31/08 20:27
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
05/31/08 20:27
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
05/31/08 20:27
1634-04-4
Naphthalene
ND ug/L
1.0
1
05/31/08 20:27
91-20-3
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 54 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-17 Lab ID: 9220393017 Collected: 05/28/08 12:45 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
n-Propylbenzene
ND ug/L
1.0
1
05/31/08 20:27
103-65-1
Styrene
ND ug/L
1.0
1
05/31/08 20:27
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 20:27
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/31/08 20:27
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
05/31/08 20:27
127-18-4
Toluene
ND ug/L
1.0
1
05/31/08 20:27
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 20:27
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
05/31/08 20:27
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/31/08 20:27
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/31/08 20:27
79-00-5
Trichloroethene
ND ug/L
1.0
1
05/31/08 20:27
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/31/08 20:27
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
05/31/08 20:27
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 20:27
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
1.0
1
05/31/08 20:27
108-67-8
Vinyl acetate
ND ug/L
2.0
1
05/31/08 20:27
108-05-4
Vinyl chloride
ND ug/L
1.0
1
05/31/08 20:27
75-01-4
m&p-Xylene
ND ug/L
2.0
1
05/31/08 20:27
1330-20-7
o-Xylene
ND ug/L
1.0
1
05/31/08 20:27
95-47-6
4-Bromofluorobenzene (S)
101 %
87-109
1
05/31/08 20:27
460-00-4
Dibromofluoromethane (S)
100 %
85-115
1
05/31/08 20:27
1868-53-7
1,2-Dichloroethane-d4 (S)
101 %
79-120
1
05/31/08 20:27
17060-07-0
Toluene-d8 (S)
99 %
70-120
1
05/31/08 20:27
2037-26-5
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 55 of 97

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Sample: SB-16 Lab ID: 9220393018 Collected: 05/28/08 14:40 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-CO8)
ND ug/L
100
1
05/30/08 17:41
Aliphatic (C09-C12)
ND ug/L
100
1
05/30/08 17:41
Aromatic (C09-C10)
ND ug/L
100
1
05/30/08 17:41
2,5-Dibromotoluene (PID)(S)
120 %
70-130
1
05/30/08 17:41
2,5-Dibromotoluene (FID)(S)
123 %
70-130
1
05/30/08 17:41
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead
5.8 ug/L
5.0
1
05/30/08 10:43 05/31/08 04:59
7439-92-1
6210 MSV
Analytical Method: SM 6210
Benzene
ND ug/L
0.50
1
06/06/08 16:54
71-43-2
Bromobenzene
ND ug/L
0.50
1
06/06/08 16:54
108-86-1
Bromochloromethane
ND ug/L
0.50
1
06/06/08 16:54
74-97-5
Bromodichloromethane
ND ug/L
0.50
1
06/06/08 16:54
75-27-4
Bromoform
ND ug/L
0.50
1
06/06/08 16:54
75-25-2
Bromomethane
ND ug/L
1.0
1
06/06/08 16:54
74-83-9
n-Butylbenzene
ND ug/L
0.50
1
06/06/08 16:54
104-51-8
sec-Butylbenzene
ND ug/L
0.50
1
06/06/08 16:54
135-98-8
tert-Butyl benzene
ND ug/L
0.50
1
06/06/08 16:54
98-06-6
Carbon tetrachloride
ND ug/L
0.50
1
06/06/08 16:54
56-23-5
Chlorobenzene
ND ug/L
0.50
1
06/06/08 16:54
108-90-7
Chloroethane
ND ug/L
1.0
1
06/06/08 16:54
75-00-3
Chloroform
1.4 ug/L
0.50
1
06/06/08 16:54
67-66-3
Chloromethane
ND ug/L
1.0
1
06/06/08 16:54
74-87-3
2-Chlorotoluene
ND ug/L
0.50
1
06/06/08 16:54
95-49-8
4-Chlorotoluene
ND ug/L
0.50
1
06/06/08 16:54
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1
06/06/08 16:54
96-12-8
Dibromochloromethane
ND ug/L
0.50
1
06/06/08 16:54
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
0.50
1
06/06/08 16:54
106-93-4
Dibromomethane
ND ug/L
0.50
1
06/06/08 16:54
74-95-3
1,2-Dichlorobenzene
ND ug/L
0.50
1
06/06/08 16:54
95-50-1
1,3-Dichlorobenzene
ND ug/L
0.50
1
06/06/08 16:54
541-73-1
1,4-Dichlorobenzene
ND ug/L
0.50
1
06/06/08 16:54
106-46-7
Dichlorodifluoromethane
ND ug/L
0.50
1
06/06/08 16:54
75-71-8
1,1-Dichloroethane
ND ug/L
0.50
1
06/06/08 16:54
75-34-3
1,2-Dichloroethane
ND ug/L
0.50
1
06/06/08 16:54
107-06-2
1,1-Dichloroethene
ND ug/L
0.50
1
06/06/08 16:54
75-35-4
cis-1,2-Dichloroethene
ND ug/L
0.50
1
06/06/08 16:54
156-59-2
trans-1,2-Dichloroethene
ND ug/L
0.50
1
06/06/08 16:54
156-60-5
1,2-Dichloropropane
ND ug/L
0.50
1
06/06/08 16:54
78-87-5
1,3-Dichloropropane
ND ug/L
0.50
1
06/06/08 16:54
142-28-9
2,2-Dichloropropane
ND ug/L
0.50
1
06/06/08 16:54
594-20-7
1,1-Dichloropropene
ND ug/L
0.50
1
06/06/08 16:54
563-58-6
cis-1,3-Dichloropropene
ND ug/L
0.50
1
06/06/08 16:54
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
0.50
1
06/06/08 16:54
10061-02-6
Diisopropyl ether
ND ug/L
0.50
1
06/06/08 16:54
108-20-3
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 56 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-16 Lab ID: 9220393018 Collected: 05/28/08 14:40 Received: 05/29/08 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6210 MSV Analytical Method: SM 6210
Ethylbenzene
ND ug/L
0.50
1
06/06/08 16:54
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
2.0
1
06/06/08 16:54
87-68-3
Isopropylbenzene (Cumene)
ND ug/L
0.50
1
06/06/08 16:54
98-82-8
p-Isopropyltoluene
ND ug/L
0.50
1
06/06/08 16:54
99-87-6
Methylene Chloride
ND ug/L
2.0
1
06/06/08 16:54
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
1
06/06/08 16:54
1634-04-4
Naphthalene
ND ug/L
2.0
1
06/06/08 16:54
91-20-3
n-Propylbenzene
ND ug/L
0.50
1
06/06/08 16:54
103-65-1
Styrene
ND ug/L
0.50
1
06/06/08 16:54
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
0.50
1
06/06/08 16:54
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
0.50
1
06/06/08 16:54
79-34-5
Tetrachloroethene
ND ug/L
0.50
1
06/06/08 16:54
127-18-4
Toluene
ND ug/L
0.50
1
06/06/08 16:54
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
2.0
1
06/06/08 16:54
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
2.0
1
06/06/08 16:54
120-82-1
1,1,1-Trichloroethane
ND ug/L
0.50
1
06/06/08 16:54
71-55-6
1,1,2-Trichloroethane
ND ug/L
0.50
1
06/06/08 16:54
79-00-5
Trichloroethene
ND ug/L
0.50
1
06/06/08 16:54
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
06/06/08 16:54
75-69-4
1,2,3-Trichloropropane
ND ug/L
0.50
1
06/06/08 16:54
96-18-4
1,2,4-Trimethylbenzene
0.95 ug/L
0.50
1
06/06/08 16:54
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
0.50
1
06/06/08 16:54
108-67-8
Vinyl chloride
ND ug/L
1.0
1
06/06/08 16:54
75-01-4
m&p-Xylene
ND ug/L
1.0
1
06/06/08 16:54
1330-20-7
o-Xylene
ND ug/L
0.50
1
06/06/08 16:54
95-47-6
1,2-Dichloroethane-d4 (S)
94 %
60-140
1
06/06/08 16:54
17060-07-0
Dibromofluoromethane (S)
104 %
60-140
1
06/06/08 16:54
1868-53-7
4-Bromofluorobenzene (S)
102 %
60-140
1
06/06/08 16:54
460-00-4
Toluene-d8 (S)
100 %
60-140
1
06/06/08 16:54
2037-26-5
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 57 of 97

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
QC Batch: MPRP/2439
Analysis Method:
EPA200.7
QC Batch Method: SM 3030C
Analysis Description:
200.7 MET 3030C
Associated Lab Samples: 9220393018
METHOD BLANK: 121641
Associated Lab Samples: 9220393018
Blank Reporting
Parameter
Units
Result Limit
Qualifiers
Lead
ug/L
ND 5.0
LABORATORY CONTROL SAMPLE:
121642
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Lead
ug/L
500 548
110
85-115
MATRIX SPIKE SAMPLE:
121643
9220259001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Lead
ug/L
ND 500
504
101
70-130
SAMPLE DUPLICATE: 121644
9220393018 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Lead
ug/L
5.8 5.3
10
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 58 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/2444 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET
Associated Lab Samples: 9220393013, 9220393014, 9220393015, 9220393016, 9220393017
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
121769
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
521
104
80-120
Arsenic
ug/L
500
492
98
80-120
Beryllium
ug/L
500
478
96
80-120
Cadmium
ug/L
500
488
98
80-120
Chromium
ug/L
500
503
101
80-120
Copper
ug/L
500
480
96
80-120
Lead
ug/L
500
489
98
80-120
Manganese
ug/L
500
492
98
80-120
Nickel
ug/L
500
491
98
80-120
Selenium
ug/L
500
481
96
80-120
Silver
ug/L
250
253
101
80-120
Thallium
ug/L
500
465
93
80-120
Zinc
ug/L
500
494
99
80-120
MATRIX SPIKE SAMPLE:
Parameter
121770
9220395006 Spike MS
Units Result Conc. Result
MS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
ND 500
402
80
75-125
Arsenic
ug/L
13.0 500
517
101
75-125
Beryllium
ug/L
ND 500
457
91
75-125
Cadmium
ug/L
2.0 500
457
91
75-125
Chromium
ug/L
275 500
756
96
75-125
Copper
ug/L
162 500
655
99
75-125
Lead
ug/L
127 500
546
84
75-125
Manganese
ug/L
23.5 500
481
92
75-125
Nickel
ug/L
27.2 500
472
89
75-125
Selenium
ug/L
15.5 500
507
98
75-125
Silver
ug/L
ND 250
249
100
75-125
Thallium
ug/L
ND 500
408
80
75-125
Zinc
ug/L
35.0 500
546
102
75-125
SAMPLE DUPLICATE: 121771
9220395007 Dup
Parameter
Units Result Result RPD
Qualifiers
Antimony
ug/L
ND ND
200
Arsenic
ug/L
ND ND
32
Beryllium
ug/L
ND ND
0
Cadmium
ug/L
ND ND
16
Chromium
ug/L
40.0 40.5
1
Copper
ug/L
17.2 17.1
.6
Lead
ug/L
20.7 21.2
2
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
Page 59 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 121771
9220395007
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Manganese
ug/L
9.2
9.0
2
Nickel
ug/L
12.6
12.5
.8
Selenium
ug/L
ND
ND
17
Silver
ug/L
ND
ND
0
Thallium
ug/L
ND
ND
200
Zinc
ug/L
10.7
12.9
19
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: PMST/1699 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 9220393001, 9220393002, 9220393003, 9220393004, 9220393005, 9220393006, 9220393007, 9220393008,
9220393009,9220393010,9220393011,9220393012
SAMPLE DUPLICATE: 121779
Parameter
Percent Moisture
Date: 06/18/2008 12:11 PM
9220059001 Dup
Units Result Result
% 57.6 58.1
RPD Qualifiers
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 61 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: GCV/2106 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 9220393018
METHOD BLANK: 121875
Associated Lab Samples:
9220393018
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
Aliphatic (C05-008)
ug/L
ND
100
Aliphatic (C09-C12)
ug/L
ND
100
Aromatic (C09-C10)
ug/L
ND
100
2,5-Dibromotoluene (FID)(S)
%
110
70-130
2,5-Dibromotoluene (PID)(S)
%
105
70-130
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 121876
121877
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
274
287
91
96
70-130 4 25
Aliphatic (C09-C12)
ug/L
300
263
296
88
99
30-130 12 25
Aromatic (C09-C10)
ug/L
100
109
117
109
117
70-130 7 25
2,5-Dibromotoluene (FID)(S)
%
102
113
70-130
2,5-Dibromotoluene (PID)(S)
%
101
114
70-130
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 62 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/3578 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 9220393013, 9220393014, 9220393015, 9220393016, 9220393017
METHOD BLANK: 122306
Associated Lab Samples: 9220393013, 9220393014, 9220393015, 9220393016, 9220393017
Blank Reporting
Parameter Units Result Limit Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
1,1,1-Trichloroethane
ug/L
ND
1.0
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
1,1,2-Trichloroethane
ug/L
ND
1.0
1,1-Dichloroethane
ug/L
ND
1.0
1,1-Dichloroethene
ug/L
ND
1.0
1,1-Dichloropropene
ug/L
ND
1.0
1,2,3-Trichlorobenzene
ug/L
ND
1.0
1,2,3-Trichloropropane
ug/L
ND
1.0
1,2,4-Trichlorobenzene
ug/L
ND
1.0
1,2,4-Trimethylbenzene
ug/L
ND
1.0
1,2-Dibromo-3-chloropropane
ug/L
ND
3.0
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
1,2-Dichlorobenzene
ug/L
ND
1.0
1,2-Dichloroethane
ug/L
ND
1.0
1,2-Dichloropropane
ug/L
ND
1.0
1,3,5-Trimethylbenzene
ug/L
ND
1.0
1,3-Dichlorobenzene
ug/L
ND
1.0
1,3-Dichloropropane
ug/L
ND
1.0
1,4-Dichlorobenzene
ug/L
ND
1.0
2,2-Dichloropropane
ug/L
ND
1.0
2-Butanone (MEK)
ug/L
ND
5.0
2-Chlorotoluene
ug/L
ND
1.0
2-Hexanone
ug/L
ND
5.0
4-Chlorotoluene
ug/L
ND
1.0
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
Acetone
ug/L
ND
25.0
Benzene
ug/L
ND
1.0
Bromobenzene
ug/L
ND
1.0
Bromochloromethane
ug/L
ND
1.0
Bromodichloromethane
ug/L
ND
1.0
Bromoform
ug/L
ND
1.0
Bromomethane
ug/L
ND
5.0
Carbon tetrachloride
ug/L
ND
1.0
Chlorobenzene
ug/L
ND
1.0
Chloroethane
ug/L
ND
1.0
Chloroform
ug/L
ND
1.0
Chloromethane
ug/L
ND
1.0
cis-1,2-Dichloroethene
ug/L
ND
1.0
cis-1,3-Dichloropropene
ug/L
ND
1.0
Dibromochloromethane
ug/L
ND
1.0
Dibromomethane
ug/L
ND
1.0
Dichlorodifluoromethane
ug/L
ND
1.0
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 97

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
METHOD BLANK: 122306
QUALITY CONTROL DATA
[phone]
Associated Lab Samples: 9220393013, 9220393014, 9220393015, 9220393016, 9220393017
Blank Reporting
Parameter Units Result Limit Qualifiers
Diisopropyl ether
ug/L
ND
1.0
Ethylbenzene
ug/L
ND
1.0
Hexachloro-1,3-butadiene
ug/L
ND
1.0
Isopropylbenzene (Cumene)
ug/L
ND
1.0
m&p-Xylene
ug/L
ND
2.0
Methyl-tert-butyl ether
ug/L
ND
1.0
Methylene Chloride
ug/L
3.6
2.0 B-,C9
n-Butylbenzene
ug/L
ND
1.0
n-Propylbenzene
ug/L
ND
1.0
Naphthalene
ug/L
ND
1.0
o-Xylene
ug/L
ND
1.0
p-Isopropyltoluene
ug/L
ND
1.0
sec-Butylbenzene
ug/L
ND
1.0
Styrene
ug/L
ND
1.0
tert-Butyl benzene
ug/L
ND
1.0
Tetrachloroethene
ug/L
ND
1.0
Toluene
ug/L
ND
1.0
trans-1,2-Dichloroethene
ug/L
ND
1.0
trans- 1,3-Dichloropropene
ug/L
ND
1.0
Trichloroethene
ug/L
ND
1.0
Trichlorofluoromethane
ug/L
ND
1.0
Vinyl acetate
ug/L
ND
2.0
Vinyl chloride
ug/L
ND
1.0
1,2-Dichloroethane-d4 (S)
%
100
79-120
4-Bromofluorobenzene (S)
%
104
87-109
Dibromofluoromethane (S)
%
103
85-115
Toluene-d8 (S)
%
98
70-120
LABORATORY CONTROL SAMPLE:
Parameter
122307
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
64.2
128
83-125 L3
1,1,1-Trichloroethane
ug/L
50
51.5
103
80-129
1,1,2,2-Tetrachloroethane
ug/L
50
57.0
114
73-127
1,1,2-Trichloroethane
ug/L
50
57.2
114
77-123
1,1-Dichloroethane
ug/L
50
57.8
116
76-129
1,1-Dichloroethene
ug/L
50
52.7
105
78-146
1,1-Dichloropropene
ug/L
50
57.7
115
79-134
1,2,3-Trichlorobenzene
ug/L
50
57.2
114
70-150
1,2,3-Trichloropropane
ug/L
50
59.7
119
72-125
1,2,4-Trichlorobenzene
ug/L
50
56.3
113
68-127
1,2,4-Trimethylbenzene
ug/L
50
55.8
112
78-138
1,2-Dibromo-3-chloropropane
ug/L
50
59.8
120
65-128
1,2-Dibromoethane (EDB)
ug/L
50
62.5
125
81-125
1,2-Dichlorobenzene
ug/L
50
58.4
117
82-126
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 64 of 97

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
122307
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2-Dichloroethane
ug/L
50
58.7
117
72-126
1,2-Dichloropropane
ug/L
50
57.9
116
80-127
1,3,5-Trimethylbenzene
ug/L
50
56.8
114
73-118
1,3-Dichlorobenzene
ug/L
50
56.9
114
82-124
1,3-Dichloropropane
ug/L
50
57.7
115
79-124
1,4-Dichlorobenzene
ug/L
50
58.2
116
79-125
2,2-Dichloropropane
ug/L
50
51.3
103
58-140
2-Butanone (MEK)
ug/L
100
95.7
96
50-134
2-Chlorotoluene
ug/L
50
56.0
112
81-126
2-Hexanone
ug/L
100
127
127
58-138
4-Chlorotoluene
ug/L
50
55.3
111
82-126
4-Methyl-2-pentanone (MIBK)
ug/L
100
118
118
70-131
Acetone
ug/L
100
135
135
50-146
Benzene
ug/L
50
55.2
110
78-128
Bromobenzene
ug/L
50
51.8
104
81-127
Bromochloromethane
ug/L
50
59.6
119
73-124
Bromodichloromethane
ug/L
50
61.9
124
81-125
Bromoform
ug/L
50
57.0
114
71-125
Bromomethane
ug/L
50
95.1
190
50-150 L3
Carbon tetrachloride
ug/L
50
52.3
105
81-137
Chlorobenzene
ug/L
50
59.0
118
82-126
Chloroethane
ug/L
50
56.3
113
69-140
Chloroform
ug/L
50
59.0
118
77-129
Chloromethane
ug/L
50
56.9
114
54-139
cis-1,2-Dichloroethene
ug/L
50
55.0
110
76-133
cis-1,3-Dichloropropene
ug/L
50
60.0
120
76-127
Dibromochloromethane
ug/L
50
57.4
115
77-125
Dibromomethane
ug/L
50
58.6
117
77-125
Dichlorodifluoromethane
ug/L
50
57.6
115
50-150
Diisopropyl ether
ug/L
50
61.7
123
74-131
Ethylbenzene
ug/L
50
59.7
119
80-127
Hexachloro-1,3-butadiene
ug/L
50
58.0
116
78-145
Isopropylbenzene(Cumene)
ug/L
50
59.6
119
84-135
m&p-Xylene
ug/L
100
118
118
82-127
Methyl-tert-butyl ether
ug/L
50
58.6
117
71-130
Methylene Chloride
ug/L
50
62.0
124
67-133
n-Butylbenzene
ug/L
50
59.8
120
73-122
n-Propylbenzene
ug/L
50
56.5
113
82-129
Naphthalene
ug/L
50
63.0
126
52-136
o-Xylene
ug/L
50
56.6
113
83-124
p-Isopropyltoluene
ug/L
50
59.9
120
73-122
sec-Butylbenzene
ug/L
50
58.5
117
82-131
Styrene
ug/L
50
59.2
118
80-130
tert-Butyl benzene
ug/L
50
59.2
118
80-130
Tetrachloroethene
ug/L
50
58.1
116
78-128
Toluene
ug/L
50
56.4
113
76-126
trans-1,2-Dichloroethene
ug/L
50
53.6
107
78-134
trans- 1,3-Dichloropropene
ug/L
50
59.6
119
75-125
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 65 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
122307
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Trichloroethene
ug/L
50
57.8
116
79-127
Trichlorofluoromethane
ug/L
50
62.4
125
76-148
Vinyl acetate
ug/L
100
126
126
50-150
Vinyl chloride
ug/L
50
64.9
130
67-143
1,2-Dichloroethane-d4 (S)
%
112
79-120
4-Bromofluorobenzene (S)
%
99
87-109
Dibromofluoromethane (S)
%
102
85-115
Toluene-d8 (S)
%
99
70-120
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
122308
122309
MS
MSD
9220377007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1-Dichloroethene
ug/L
ND
50
50
59.5
55.9
119
112
60-150
6
Benzene
ug/L
ND
50
50
59.8
58.5
120
117
74-136
2
Chlorobenzene
ug/L
ND
50
50
64.2
62.2
128
124
79-135
3
Toluene
ug/L
ND
50
50
61.3
58.8
123
118
73-131
4
Trichloroethene
ug/L
ND
50
50
62.2
60.6
124
121
73-131
3
1,2-Dichloroethane-d4 (S)
%
101
97
79-120
4-Bromofluorobenzene (S)
%
101
99
87-109
Dibromofluoromethane (S)
%
95
100
85-115
Toluene-d8(S)
%
100
99
70-120
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 66 of 97

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/3376 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV
Associated Lab Samples: 9220393013, 9220393014, 9220393015, 9220393016, 9220393017
METHOD BLANK: 122390
Associated Lab Samples: 9220393013, 9220393014, 9220393015, 9220393016, 9220393017
Blank Reporting
Parameter Units Result Limit Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
10.0
1,2-Dichlorobenzene
ug/L
ND
10.0
1,2-Diphenylhydrazine
ug/L
ND
10.0
1,3-Dichlorobenzene
ug/L
ND
10.0
1,4-Dichlorobenzene
ug/L
ND
10.0
1-Methylnaphthalene
ug/L
ND
10.0
2,4,5-Trichlorophenol
ug/L
ND
10.0
2,4,6-Trichlorophenol
ug/L
ND
10.0
2,4-Dichlorophenol
ug/L
ND
10.0
2,4-Dimethylphenol
ug/L
ND
10.0
2,4-Dinitrophenol
ug/L
ND
50.0
2,4-Dinitrotoluene
ug/L
ND
10.0
2,6-Dinitrotoluene
ug/L
ND
10.0
2-Chloronaphthalene
ug/L
ND
10.0
2-Chlorophenol
ug/L
ND
10.0
2-Methylnaphthalene
ug/L
ND
10.0
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
2-Nitroaniline
ug/L
ND
50.0
2-Nitrophenol
ug/L
ND
10.0
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
10.0
3,3'-Dichlorobenzidine
ug/L
ND
50.0
3-Nitroaniline
ug/L
ND
50.0
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
4-Bromophenylphenyl ether
ug/L
ND
10.0
4-ChIoro-3-methyl phenol
ug/L
ND
20.0
4-Chloroaniline
ug/L
ND
50.0
4-Chlorophenylphenyl ether
ug/L
ND
10.0
4-Nitroaniline
ug/L
ND
50.0
4-Nitrophenol
ug/L
ND
50.0
Acenaphthene
ug/L
ND
10.0
Acenaphthylene
ug/L
ND
10.0
Aniline
ug/L
ND
10.0
Anthracene
ug/L
ND
10.0
Benzo(a)anthracene
ug/L
ND
10.0
Benzo(a)pyrene
ug/L
ND
10.0
Benzo(b)fluoranthene
ug/L
ND
10.0
Benzo(g,h,i)perylene
ug/L
ND
10.0
Benzo(k)fluoranthene
ug/L
ND
10.0
Benzoic acid
ug/L
ND
50.0
Benzyl alcohol
ug/L
ND
20.0
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
bis(2-Chloroethyl) ether
ug/L
ND
10.0
bis(2-Chloroisopropyl) ether
ug/L
ND
10.0
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 97

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
METHOD BLANK: 122390
QUALITY CONTROL DATA
[phone]
Associated Lab Samples: 9220393013, 9220393014, 9220393015, 9220393016, 9220393017
Blank Reporting
Parameter Units Result Limit Qualifiers
bis(2-Ethylhexyl)phthalate
ug/L
ND
10.0
Butylbenzylphthalate
ug/L
ND
10.0
Chrysene
ug/L
ND
10.0
Di-n-butylphthalate
ug/L
ND
10.0
Di-n-octylphthalate
ug/L
ND
10.0
Dibenz(a,h)anthracene
ug/L
ND
10.0
Dibenzofuran
ug/L
ND
10.0
Diethylphthalate
ug/L
ND
10.0
Dimethylphthalate
ug/L
ND
10.0
Fluoranthene
ug/L
ND
10.0
Fluorene
ug/L
ND
10.0
Hexachloro-1,3-butadiene
ug/L
ND
10.0
Hexachlorobenzene
ug/L
ND
10.0
Hexachlorocyclopentadiene
ug/L
ND
10.0
Hexachloroethane
ug/L
ND
10.0
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
Isophorone
ug/L
ND
10.0
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
N-Nitrosodimethylamine
ug/L
ND
10.0
N-Nitrosodiphenylamine
ug/L
ND
10.0
Naphthalene
ug/L
ND
10.0
Nitrobenzene
ug/L
ND
10.0
Pentachlorophenol
ug/L
ND
50.0
Phenanthrene
ug/L
ND
10.0
Phenol
ug/L
ND
10.0
Pyrene
ug/L
ND
10.0
2,4,6-Tribromophenol (S)
%
79
25-150
2-Fluorobiphenyl (S)
%
82
30-150
2-Fluorophenol (S)
%
36
25-150
Nitrobenzene-d5 (S)
%
71
30-150
Phenol-d6 (S)
%
24
25-150 1g
Terphenyl-d14 (S)
%
87
30-150
LABORATORY CONTROL SAMPLE:
Parameter
122391
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
28.0
56
19-120
1,2-Dichlorobenzene
ug/L
50
33.8
68
19-120
1,2-Diphenylhydrazine
ug/L
50
39.4
79
50-150
1,3-Dichlorobenzene
ug/L
50
31.0
62
15-120
1,4-Dichlorobenzene
ug/L
50
32.8
66
15-120
1-Methylnaphthalene
ug/L
50
49.1
98
21-120
2,4,5-Trichlorophenol
ug/L
50
33.9
68
23-113
2,4,6-Trichlorophenol
ug/L
50
32.8
66
21-113
2,4-Dichlorophenol
ug/L
50
33.5
67
12-127
[phone]
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 68 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
122391
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4-Dimethylphenol
ug/L
50
31.2
62
24-120
2,4-Dinitrophenol
ug/L
50
27.1J
54
10-127
2,4-Dinitrotoluene
ug/L
50
36.2
72
36-115
2,6-Dinitrotoluene
ug/L
50
31.5
63
37-114
2-Chloronaphthalene
ug/L
50
34.6
69
36-101
2-Chlorophenol
ug/L
50
37.1
74
24-120
2-Methylnaphthalene
ug/L
50
46.3
93
19-120
2-Methylphenol(o-Cresol)
ug/L
50
27.0
54
25-120
2-Nitroaniline
ug/L
50
43.5J
87
30-109
2-Nitrophenol
ug/L
50
38.8
78
24-120
3&4-Methyl phenol (m&p Cresol)
ug/L
50
27.5
55
24-120
3,3'-Dichlorobenzidine
ug/L
50
43.9J
88
14-120
3-Nitroaniline
ug/L
50
48.2J
96
23-133
4,6-Dinitro-2-methyl phenol
ug/L
50
36.6
73
10-128
4-Bromophenylphenyl ether
ug/L
50
37.8
76
35-113
4-Chloro-3-methylphenol
ug/L
50
34.7
69
32-107
4-Chloroaniline
ug/L
50
48.3J
97
12-150
4-Chlorophenylphenyl ether
ug/L
50
34.6
69
36-110
4-Nitroaniline
ug/L
50
46.8J
94
12-150
4-Nitrophenol
ug/L
50
111
22
10-120
Acenaphthene
ug/L
50
45.8
92
27-102
Acenaphthylene
ug/L
50
41.1
82
25-105
Aniline
ug/L
50
52.2
104
10-150
Anthracene
ug/L
50
50.2
100
30-113
Benzo(a)anthracene
ug/L
50
40.2
80
27-113
Benzo(a)pyrene
ug/L
50
40.3
81
27-119
Benzo(b)fluoranthene
ug/L
50
45.5
91
22-114
Benzo(g,h,i)perylene
ug/L
50
27.0
54
10-129
Benzo(k)fluoranthene
ug/L
50
45.6
91
24-111
Benzoic acid
ug/L
50
ND
6
24-120 L2
Benzyl alcohol
ug/L
50
32.8
66
24-120
bis(2-Chloroethoxy)methane
ug/L
50
37.1
74
32-120
bis(2-Chloroethyl) ether
ug/L
50
38.9
78
29-120
bis(2-Chloroisopropyl) ether
ug/L
50
51.2
102
22-120
bis(2-Ethylhexyl)phthalate
ug/L
50
51.2
102
29-125
Butylbenzylphthalate
ug/L
50
49.0
98
33-120
Chrysene
ug/L
50
38.8
78
23-112
Di-n-butylphthalate
ug/L
50
52.1
104
38-116
Di-n-octylphthalate
ug/L
50
48.2
96
32-122
Dibenz(a,h)anthracene
ug/L
50
31.4
63
10-129
Dibenzofuran
ug/L
50
37.1
74
37-107
Diethylphthalate
ug/L
50
43.2
86
40-111
Dimethylphthalate
ug/L
50
39.6
79
39-108
Fluoranthene
ug/L
50
39.3
79
27-112
Fluorene
ug/L
50
46.3
93
29-107
Hexachloro-1,3-butadiene
ug/L
50
28.0
56
10-113
Hexachlorobenzene
ug/L
50
35.7
71
29-119
Hexachlorocyclopentadiene
ug/L
50
20.0
40
10-113
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 69 of 97

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
LABORATORY CONTROL SAMPLE:
122391
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Hexachloroethane
ug/L
50
33.9
68
10-120
Indeno(1,2,3-cd)pyrene
ug/L
50
29.7
59
14-123
Isophorone
ug/L
50
47.3
95
23-150
N-Nitroso-di-n-propylamine
ug/L
50
38.9
78
31-104
N-Nitrosodimethylamine
ug/L
50
23.5
47
10-120
N-Nitrosodiphenylamine
ug/L
50
42.1
84
27-139
Naphthalene
ug/L
50
41.2
82
17-120
Nitrobenzene
ug/L
50
39.8
80
27-120
Pentachlorophenol
ug/L
50
26.3J
53
10-135
Phenanthrene
ug/L
50
40.2
80
28-111
Phenol
ug/L
50
14.6
29
10-120
Pyrene
ug/L
50
39.8
80
27-113
2,4,6-Tribromophenol (S)
%
73
25-150
2-Fluorobiphenyl (S)
%
73
30-150
2-Fluorophenol (S)
%
39
25-150
Nitrobenzene-d5 (S)
%
77
30-150
Phenol-d6 (S)
%
29
25-150
Terphenyl-d14 (S)
%
77
30-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
122392
122393
MS
MSD
9220393013
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/L
ND
100
100
49.9
51.3
50
51
13-120
3
1,4-Dichlorobenzene
ug/L
ND
100
100
58.9
62.9
59
63
19-120
7
2,4-Dinitrotoluene
ug/L
ND
100
100
61.8
65.0
62
65
41-109
5
2-Chlorophenol
ug/L
ND
100
100
64.9
69.6
65
70
33-120
7
4-Chloro-3-methyl phenol
ug/L
ND
100
100
62.1
66.0
62
66
30-108
6
4-Nitrophenol
ug/L
ND
100
100
24J
25AJ
24
25
10-120
Acenaphthene
ug/L
ND
100
100
78.6
85.1
79
85
27-101
8
N-Nitroso-di-n-propylamine
ug/L
ND
100
100
75.3
80.5
75
81
34-120
7
Pentachlorophenol
ug/L
ND
100
100
48.1J
50.5J
48
51
10-138
Phenol
ug/L
ND
100
100
24.6
26.1
25
26
10-120
6
Pyrene
ug/L
ND
100
100
76.5
85.4
77
85
31-110
11
2,4,6-Tribromophenol (S)
%
65
72
25-150
2-Fluorobiphenyl (S)
%
64
72
30-150
2-Fluorophenol(S)
%
36
38
25-150
Nitrobenzene-d5 (S)
%
69
74
30-150
Phenol-d6 (S)
%
27
30
25-150
Terphenyl-d14 (S)
%
77
84
30-150
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 70 of 97

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
QC Batch: MPRP/2449
Analysis Method: EPA6010
QC Batch Method: EPA 3050
Analysis Description: 6010 MET
Associated Lab Samples: 9220393001, 9220393007, 9220393008, 9220393009, 9220393010, 9220393011,
9220393012
LABORATORY CONTROL SAMPLE:
122561
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Antimony
mg/kg
50 52.4
105
80-120
Arsenic
mg/kg
50 50.0
100
80-120
Beryllium
mg/kg
50 49.8
100
80-120
Cadmium
mg/kg
50 50.7
101
80-120
Chromium
mg/kg
50 52.8
106
80-120
Copper
mg/kg
50 47.6
95
80-120
Lead
mg/kg
50 50.4
101
80-120
Manganese
mg/kg
50 51.3
103
80-120
Nickel
mg/kg
50 50.6
101
80-120
Selenium
mg/kg
50 48.3
97
80-120
Silver
mg/kg
25 26.5
106
80-120
Thallium
mg/kg
50 48.4
97
80-120
Zinc
mg/kg
50 51.9
104
80-120
MATRIX SPIKE SAMPLE:
122562
9220332001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Antimony
mg/kg
ND 33.3
33.7
101
75-125
Arsenic
mg/kg
ND 33.3
37.2
112
75-125
Beryllium
mg/kg
ND 33.3
34.1
102
75-125
Cadmium
mg/kg
ND 33.3
31.9
96
75-125
Chromium
mg/kg
ND 33.3
34.7
104
75-125
Copper
mg/kg
ND 33.3
31.6
95
75-125
Lead
mg/kg
ND 33.3
29.8
89
75-125
Manganese
mg/kg
10.6 ug/g 33.3
43.4
98
75-125
Nickel
mg/kg
ND 33.3
32.0
96
75-125
Selenium
mg/kg
1.39 ug/g 33.3
44.8
130
75-125 MO
Silver
mg/kg
ND 16.7
16.5
99
75-125
Thallium
mg/kg
ND 33.3
27.1
81
75-125
Zinc
mg/kg
ND 33.3
31.8
95
75-125
SAMPLE DUPLICATE: 122563
9220336003 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Antimony
mg/kg
ND ND
200
Arsenic
mg/kg
ND ND
51
Beryllium
mg/kg
ND ND
200
Cadmium
mg/kg
0.32 0.25
22
R1
Chromium
mg/kg
6.3 7.8
21
R1
Copper
mg/kg
44.9 15.4
98
R1
Lead
mg/kg
30.5 34.0
11
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
Page 71 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 122563
9220336003
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Manganese
mg/kg
231
237
3
Nickel
mg/kg
5.0
2.2
78 R1
Selenium
mg/kg
ND
.64J
200
Silver
mg/kg
0.49
.053J
161
Thallium
mg/kg
ND
ND
0
Zinc
mg/kg
151
170
12
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/3385 Analysis Method: EPA 8015 Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 9220393001, 9220393002, 9220393003, 9220393005, 9220393006
METHOD BLANK: 122663
Associated Lab Samples: 9220393001, 9220393002, 9220393003, 9220393005, 9220393006
Blank Reporting
Parameter Units Result Limit Qualifiers
Diesel Components mg/kg ND 5.0
n-Pentacosane(S) % 77 50-135
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 122664
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Diesel Components mg/kg 167 158 95 50-114
n-Pentacosane(S) % 86 50-135
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 122665 122666
MS MSD
9220393002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Diesel Components mg/kg ND 174 174 129 115 73 66 50-107 11
n-Pentacosane(S) % 70 62 50-135
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 73 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: GCV/2115 Analysis Method: EPA 8015 Modified
QC Batch Method: EPA 5035A/5030B Analysis Description: Gasoline Range Organics
Associated Lab Samples: 9220393001, 9220393002, 9220393003, 9220393004, 9220393005, 9220393006
METHOD BLANK: 122719
Associated Lab Samples: 9220393001, 9220393002, 9220393003, 9220393004, 9220393005, 9220393006
Blank Reporting
Parameter Units Result Limit Qualifiers
Gasoline Range Organics mg/kg ND 6.0
4-Bromofluorobenzene (S) % 90 50-135
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
122720
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Gasoline Range Organics
mg/kg
25 30.3
121
70-150
4-Bromofluorobenzene (S)
%
108
50-135
MATRIX SPIKE SAMPLE:
122721
9220089001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Gasoline Range Organics
mg/kg
ND 27.4
25.0
91
70-148
4-Bromofluorobenzene (S)
%
90
50-135
SAMPLE DUPLICATE: 122722
9220255001 Dup
Parameter Units Result Result RPD Qualifiers
Gasoline Range Organics mg/kg 15.9 16.5 3
4-Bromofluorobenzene (S) % 106 3
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 74 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/3390 Analysis Method: EPA 8270
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 9220393001, 9220393007, 9220393008, 9220393009, 9220393010, 9220393011
METHOD BLANK: 122815
Associated Lab Samples: 9220393001, 9220393007, 9220393008, 9220393009, 9220393010, 9220393011
Blank Reporting
Parameter Units Result Limit Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
330
1,2-Dichlorobenzene
ug/kg
ND
330
1,2-Diphenylhydrazine
ug/kg
ND
330
1,3-Dichlorobenzene
ug/kg
ND
330
1,4-Dichlorobenzene
ug/kg
ND
330
1-Methylnaphthalene
ug/kg
ND
330
2,4,5-Trichlorophenol
ug/kg
ND
330
2,4,6-Trichlorophenol
ug/kg
ND
330
2,4-Dichlorophenol
ug/kg
ND
330
2,4-Dimethylphenol
ug/kg
ND
330
2,4-Dinitrophenol
ug/kg
ND
1650
2,4-Dinitrotoluene
ug/kg
ND
330
2,6-Dinitrotoluene
ug/kg
ND
330
2-Chloronaphthalene
ug/kg
ND
330
2-Chlorophenol
ug/kg
ND
330
2-Methylnaphthalene
ug/kg
ND
330
2-Methylphenol(o-Cresol)
ug/kg
ND
330
2-Nitroaniline
ug/kg
ND
1650
2-Nitrophenol
ug/kg
ND
330
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
330
3,3'-Dichlorobenzidine
ug/kg
ND
1650
3-Nitroaniline
ug/kg
ND
1650
4,6-Dinitro-2-methyl phenol
ug/kg
ND
660
4-Bromophenylphenyl ether
ug/kg
ND
330
4-ChIoro-3-methyl phenol
ug/kg
ND
660
4-Chloroaniline
ug/kg
ND
1650
4-Chlorophenylphenyl ether
ug/kg
ND
330
4-Nitroaniline
ug/kg
ND
660
4-Nitrophenol
ug/kg
ND
1650
Acenaphthene
ug/kg
ND
330
Acenaphthylene
ug/kg
ND
330
Aniline
ug/kg
ND
330
Anthracene
ug/kg
ND
330
Benzo(a)anthracene
ug/kg
ND
330
Benzo(a)pyrene
ug/kg
ND
330
Benzo(b)fluoranthene
ug/kg
ND
330
Benzo(g,h,i)perylene
ug/kg
ND
330
Benzo(k)fluoranthene
ug/kg
ND
330
Benzoic acid
ug/kg
ND
1650
Benzyl alcohol
ug/kg
ND
660
bis(2-Chloroethoxy)methane
ug/kg
ND
330
bis(2-Chloroethyl) ether
ug/kg
ND
330
bis(2-Chloroisopropyl) ether
ug/kg
ND
330
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 97

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
METHOD BLANK: 122815
QUALITY CONTROL DATA
[phone]
Associated Lab Samples: 9220393001, 9220393007, 9220393008, 9220393009, 9220393010, 9220393011
Blank Reporting
Parameter Units Result Limit Qualifiers
bis(2-Ethylhexyl)phthalate
ug/kg
ND
330
Butylbenzylphthalate
ug/kg
ND
330
Chrysene
ug/kg
ND
330
Di-n-butylphthalate
ug/kg
ND
330
Di-n-octylphthalate
ug/kg
ND
330
Dibenz(a,h)anthracene
ug/kg
ND
330
Dibenzofuran
ug/kg
ND
330
Diethylphthalate
ug/kg
ND
330
Dimethylphthalate
ug/kg
ND
330
Fluoranthene
ug/kg
ND
330
Fluorene
ug/kg
ND
330
Hexachloro-1,3-butadiene
ug/kg
ND
330
Hexachlorobenzene
ug/kg
ND
330
Hexachlorocyclopentadiene
ug/kg
ND
330
Hexachloroethane
ug/kg
ND
330
Indeno(1,2,3-cd)pyrene
ug/kg
ND
330
Isophorone
ug/kg
ND
330
N-Nitroso-di-n-propylamine
ug/kg
ND
330
N-Nitrosodimethylamine
ug/kg
ND
330
N-Nitrosodiphenylamine
ug/kg
ND
330
Naphthalene
ug/kg
ND
330
Nitrobenzene
ug/kg
ND
330
Pentachlorophenol
ug/kg
ND
1650
Phenanthrene
ug/kg
ND
330
Phenol
ug/kg
ND
330
Pyrene
ug/kg
ND
330
2,4,6-Tribromophenol (S)
%
76
30-150
2-Fluorobiphenyl (S)
%
66
30-150
2-Fluorophenol(S)
%
71
30-150
Nitrobenzene-d5 (S)
%
62
30-150
Phenol-d6 (S)
%
63
30-150
Terphenyl-d14 (S)
%
79
30-150
LABORATORY CONTROL SAMPLE:
Parameter
122816
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1670
1080
65
50-150
1,2-Dichlorobenzene
ug/kg
1670
996
60
50-150
1,2-Diphenylhydrazine
ug/kg
1670
1100
66
50-150
1,3-Dichlorobenzene
ug/kg
1670
982
59
50-150
1,4-Dichlorobenzene
ug/kg
1670
1010
60
50-150
1-Methylnaphthalene
ug/kg
1670
1830
110
50-150
2,4,5-Trichlorophenol
ug/kg
1670
1260
75
50-150
2,4,6-Trichlorophenol
ug/kg
1670
1160
70
50-150
2,4-Dichlorophenol
ug/kg
1670
1220
73
50-150
[phone]
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 76 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
QUALITY CONTROL DATA
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
122816
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4-Dimethylphenol
ug/kg
1670
1110
67
50-150
2,4-Dinitrophenol
ug/kg
1670
871J
52
50-150
2,4-Dinitrotoluene
ug/kg
1670
1200
72
50-150
2,6-Dinitrotoluene
ug/kg
1670
1130
68
50-150
2-Chloronaphthalene
ug/kg
1670
1140
69
50-150
2-Chlorophenol
ug/kg
1670
1120
67
50-150
2-Methylnaphthalene
ug/kg
1670
1230
74
50-150
2-Methylphenol(o-Cresol)
ug/kg
1670
999
60
50-150
2-Nitroaniline
ug/kg
1670
1370J
82
50-150
2-Nitrophenol
ug/kg
1670
1170
70
50-150
3&4-Methyl phenol (m&p Cresol)
ug/kg
1670
1180
71
50-150
3,3'-Dichlorobenzidine
ug/kg
1670
1500J
90
50-150
3-Nitroaniline
ug/kg
1670
1780
107
50-150
4,6-Dinitro-2-methyl phenol
ug/kg
1670
1100
66
50-150
4-Bromophenylphenyl ether
ug/kg
1670
1320
79
50-150
4-Chloro-3-methylphenol
ug/kg
1670
1380
83
50-150
4-Chloroaniline
ug/kg
1670
2080
125
50-150
4-Chlorophenylphenyl ether
ug/kg
1670
1310
79
50-150
4-Nitroaniline
ug/kg
1670
1440
87
50-150
4-Nitrophenol
ug/kg
1670
691J
41
50-150 LO
Acenaphthene
ug/kg
1670
1260
75
50-150
Acenaphthylene
ug/kg
1670
1320
79
50-150
Aniline
ug/kg
1670
1520
91
50-150
Anthracene
ug/kg
1670
1240
74
50-150
Benzo(a)anthracene
ug/kg
1670
1280
77
50-150
Benzo(a)pyrene
ug/kg
1670
1380
83
50-150
Benzo(b)fluoranthene
ug/kg
1670
995
60
50-150
Benzo(g,h,i)perylene
ug/kg
1670
1340
80
50-150
Benzo(k)fluoranthene
ug/kg
1670
1620
97
50-150
Benzoic acid
ug/kg
1670
634J
38
50-150 LO
Benzyl alcohol
ug/kg
1670
1050
63
50-150
bis(2-Chloroethoxy)methane
ug/kg
1670
1170
70
50-150
bis(2-Chloroethyl) ether
ug/kg
1670
969
58
50-150
bis(2-Chloroisopropyl) ether
ug/kg
1670
1170
70
50-150
bis(2-Ethylhexyl)phthalate
ug/kg
1670
1310
79
50-150
Butylbenzylphthalate
ug/kg
1670
1340
81
50-150
Chrysene
ug/kg
1670
1360
82
50-150
Di-n-butylphthalate
ug/kg
1670
1360
81
50-150
Di-n-octylphthalate
ug/kg
1670
1310
79
50-150
Dibenz(a,h)anthracene
ug/kg
1670
1330
80
50-150
Dibenzofuran
ug/kg
1670
1140
68
50-150
Diethylphthalate
ug/kg
1670
1320
79
50-150
Dimethylphthalate
ug/kg
1670
1360
82
50-150
Fluoranthene
ug/kg
1670
1300
78
50-150
Fluorene
ug/kg
1670
1280
77
50-150
Hexachloro-1,3-butadiene
ug/kg
1670
1120
67
50-150
Hexachlorobenzene
ug/kg
1670
1210
73
50-150
Hexachlorocyclopentadiene
ug/kg
1670
601
36
50-150 LO
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 77 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
LABORATORY CONTROL SAMPLE: 122816
Parameter
Hexachloroethane
ug/kg
Indeno(1,2,3-cd)pyrene
ug/kg
Isophorone
ug/kg
N-Nitroso-di-n-propylamine
ug/kg
N-Nitrosodimethylamine
ug/kg
N-Nitrosodiphenylamine
ug/kg
Naphthalene
ug/kg
Nitrobenzene
ug/kg
Pentachlorophenol
ug/kg
Phenanthrene
ug/kg
Phenol
ug/kg
Pyrene
ug/kg
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol(S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike
Units Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1670
1040
62
50-150
1670
1310
79
50-150
1670
2110
126
50-150
1670
1160
70
50-150
1670
1140
68
50-150
1670
1350
81
50-150
1670
1170
70
50-150
1670
1110
67
50-150
1670
11101
66
50-150
1670
1280
77
50-150
1670
1270
76
50-150
1670
1260
76
50-150
97
30-150
74
30-150
73
30-150
79
30-150
72
30-150
83
30-150
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 122817
9219978010
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
122818
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/kg
ND
2150
2150
1330
1380
62
65
50-150
4
1,4-Dichlorobenzene
ug/kg
ND
2150
2150
1310
1440
61
67
50-150
10
2,4-Dinitrotoluene
ug/kg
ND
2150
2150
1360
1420
64
66
50-150
4
2-Chlorophenol
ug/kg
ND
2150
2150
1380
1440
65
67
50-150
4
4-Chloro-3-methyl phenol
ug/kg
ND
2150
2150
1370
1440
64
67
50-150
5
4-Nitrophenol
ug/kg
ND
2150
2150
617J
583J
29
27
50-150
MO
Acenaphthene
ug/kg
ND
2150
2150
1630
1680
76
78
50-150
3
N-Nitroso-di-n-propylamine
ug/kg
ND
2150
2150
1280
1600
60
75
50-150
22
Pentachlorophenol
ug/kg
ND
2150
2150
1020J
1260J
47
59
50-150
MO
Phenol
ug/kg
ND
2150
2150
1290
1370
60
64
50-150
6
Pyrene
ug/kg
ND
2150
2150
2190
2440
102
114
50-150
10
2,4,6-Tribromophenol (S)
%
87
81
30-150
2-Fluorobiphenyl (S)
%
77
74
30-150
2-Fluorophenol(S)
%
55
61
30-150
Nitrobenzene-d5(S)
%
76
75
30-150
Phenol-d6 (S)
%
61
65
30-150
Terphenyl-d14(S)
%
109
119
30-150
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 78 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/3395 Analysis Method: EPA 8082
QC Batch Method: EPA 3545 Analysis Description: 8082 GCS PCB
Associated Lab Samples: 9220393012
METHOD BLANK: 122897
Associated Lab Samples:
9220393012
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
ND
33.0
PCB-1221 (Aroclor 1221)
ug/kg
ND
33.0
PCB-1232 (Aroclor 1232)
ug/kg
ND
33.0
PCB-1242 (Aroclor 1242)
ug/kg
ND
33.0
PCB-1248 (Aroclor 1248)
ug/kg
ND
33.0
PCB-1254 (Aroclor 1254)
ug/kg
ND
33.0
PCB-1260 (Aroclor 1260)
ug/kg
ND
33.0
Decachlorobiphenyl (S)
%
96
10-128
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
122898
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
167
163 98 42-137
PCB-1260 (Aroclor 1260)
ug/kg
167
177 106 46-140
Decachlorobiphenyl (S)
%
82 10-128
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
122899
122900
MS
MSD
9220054005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
PCB-1016 (Aroclor 1016) ug/kg
ND
170
170
138
111
82
65
30-128 22
PCB-1260 (Aroclor 1260) ug/kg
ND
170
170
150
102
89
60
29-128 38 2g
Decachlorobiphenyl (S) %
69
47
10-128
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 79 of 97

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
QC Batch: MERP/1514
Analysis Method: EPA 7470
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury
Associated Lab Samples: 9220393013, 9220393014,
9220393015, 9220393016, 9220393017
METHOD BLANK: 123205
Associated Lab Samples: 9220393013, 9220393014,
9220393015, 9220393016, 9220393017
Blank Reporting
Parameter
Units
Result Limit Qualifiers
Mercury
ug/L
ND 0.20
LABORATORY CONTROL SAMPLE:
123206
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
Qualifiers
Mercury
ug/L
2.5 2.2 90
80-120
MATRIX SPIKE SAMPLE:
123207
9220395006 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Mercury
ug/L
4.2 2.5 2.1
-81
75-125 M1
SAMPLE DUPLICATE: 123208
9220395007 Dup
Parameter
Units
Result Result RPD
Qualifiers
Mercury
ug/L
0.48 0.46
5
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 80 of 97

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
QC Batch: MERP/1515
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 9220393001, 9220393007,
9220393008, 9220393009, 9220393010, 9220393011,
9220393012
METHOD BLANK: 123217
Associated Lab Samples: 9220393001, 9220393007,
9220393008, 9220393009, 9220393010, 9220393011,
9220393012
Blank Reporting
Parameter
Units
Result Limit Qualifiers
Mercury
mg/kg
ND 0.0050
LABORATORY CONTROL SAMPLE:
123218
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Mercury
mg/kg
.065 0.055 85
80-120
MATRIX SPIKE SAMPLE:
123219
9220393001 Spike MS
MS % Rec
Parameter
Units
Result Conc. Result
% Rec Limits Qualifiers
Mercury
mg/kg
0.19 .055 0.089
-187 75-125 M1
SAMPLE DUPLICATE: 123220
9220393007 Dup
Parameter
Units
Result Result RPD
Qualifiers
Mercury
mg/kg
0.075 0.059 25
R1
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 81 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/3623 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 9220393001, 9220393007, 9220393008, 9220393009, 9220393010, 9220393011, 9220393012
METHOD BLANK: 123229
Associated Lab Samples: 9220393001, 9220393007, 9220393008, 9220393009, 9220393010, 9220393011, 9220393012
Blank Reporting
Parameter Units Result Limit Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1,1,1-Trichloroethane
ug/kg
ND
5.0
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1,1,2-Trichloroethane
ug/kg
ND
5.0
1,1-Dichloroethane
ug/kg
ND
5.0
1,1-Dichloroethene
ug/kg
ND
5.0
1,1-Dichloropropene
ug/kg
ND
5.0
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
1,2,3-Trichloropropane
ug/kg
ND
5.0
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
1,2-Dichlorobenzene
ug/kg
ND
5.0
1,2-Dichloroethane
ug/kg
ND
5.0
1,2-Dichloropropane
ug/kg
ND
5.0
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1,3-Dichlorobenzene
ug/kg
ND
5.0
1,3-Dichloropropane
ug/kg
ND
5.0
1,4-Dichlorobenzene
ug/kg
ND
5.0
2,2-Dichloropropane
ug/kg
ND
5.0
2-Butanone (MEK)
ug/kg
ND
100
2-Chlorotoluene
ug/kg
ND
5.0
2-Hexanone
ug/kg
ND
50.0
4-Chlorotoluene
ug/kg
ND
5.0
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
Acetone
ug/kg
ND
100
Benzene
ug/kg
ND
5.0
Bromobenzene
ug/kg
ND
5.0
Bromochloromethane
ug/kg
ND
5.0
Bromodichloromethane
ug/kg
ND
5.0
Bromoform
ug/kg
ND
5.0
Bromomethane
ug/kg
ND
10.0
Carbon tetrachloride
ug/kg
ND
5.0
Chlorobenzene
ug/kg
ND
5.0
Chloroethane
ug/kg
ND
10.0
Chloroform
ug/kg
ND
5.0
Chloromethane
ug/kg
ND
10.0
cis-1,2-Dichloroethene
ug/kg
ND
5.0
cis-1,3-Dichloropropene
ug/kg
ND
5.0
Dibromochloromethane
ug/kg
ND
5.0
Dibromomethane
ug/kg
ND
5.0
Dichlorodifluoromethane
ug/kg
ND
10.0
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 97

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
METHOD BLANK: 123229
QUALITY CONTROL DATA
[phone]
Associated Lab Samples: 9220393001, 9220393007, 9220393008, 9220393009, 9220393010, 9220393011, 9220393012
Blank Reporting
Parameter Units Result Limit Qualifiers
Diisopropyl ether
ug/kg
ND
5.0
Ethylbenzene
ug/kg
ND
5.0
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
m&p-Xylene
ug/kg
ND
10.0
Methyl-tert-butyl ether
ug/kg
ND
5.0
Methylene Chloride
ug/kg
ND
5.0
n-Butylbenzene
ug/kg
ND
5.0
n-Propylbenzene
ug/kg
ND
5.0
Naphthalene
ug/kg
ND
5.0
o-Xylene
ug/kg
ND
5.0
p-Isopropyltoluene
ug/kg
ND
5.0
sec-Butylbenzene
ug/kg
ND
5.0
Styrene
ug/kg
ND
5.0
tert-Butyl benzene
ug/kg
ND
5.0
Tetrachloroethene
ug/kg
ND
5.0
Toluene
ug/kg
ND
5.0
trans-1,2-Dichloroethene
ug/kg
ND
5.0
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
Trichloroethene
ug/kg
ND
5.0
Trichlorofluoromethane
ug/kg
ND
5.0
Vinyl acetate
ug/kg
ND
50.0
Vinyl chloride
ug/kg
ND
10.0
Xylene (Total)
ug/kg
ND
15.0
1,2-Dichloroethane-d4 (S)
%
96
69-121
4-Bromofluorobenzene (S)
%
99
74-115
Dibromofluoromethane (S)
%
96
79-116
Toluene-d8 (S)
%
103
88-110
LABORATORY CONTROL SAMPLE:
Parameter
123230
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
59.7
119
75-137
1,1,1-Trichloroethane
ug/kg
50
60.9
122
70-140
1,1,2,2-Tetrachloroethane
ug/kg
50
52.4
105
74-133
1,1,2-Trichloroethane
ug/kg
50
61.3
123
79-129
1,1-Dichloroethane
ug/kg
50
59.8
120
72-139
1,1-Dichloroethene
ug/kg
50
54.8
110
69-154
1,1-Dichloropropene
ug/kg
50
62.7
125
74-138
1,2,3-Trichlorobenzene
ug/kg
50
58.6
117
71-150
1,2,3-Trichloropropane
ug/kg
50
50.9
102
74-135
1,2,4-Trichlorobenzene
ug/kg
50
58.2
116
68-150
1,2,4-Trimethylbenzene
ug/kg
50
60.5
121
70-130
1,2-Dibromo-3-chloropropane
ug/kg
50
48.4
97
65-146
1,2-Dibromoethane (EDB)
ug/kg
50
54.5
109
77-136
[phone]
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 83 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
-pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
Parameter
123230
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dichlorobenzene
ug/kg
50
58.0
116
75-141
1,2-Dichloroethane
ug/kg
50
55.2
110
74-134
1,2-Dichloropropane
ug/kg
50
59.9
120
77-138
1,3,5-Trimethylbenzene
ug/kg
50
60.5
121
65-128
1,3-Dichlorobenzene
ug/kg
50
56.2
112
76-133
1,3-Dichloropropane
ug/kg
50
54.5
109
79-132
1,4-Dichlorobenzene
ug/kg
50
56.9
114
75-137
2,2-Dichloropropane
ug/kg
50
59.5
119
73-137
2-Butanone (MEK)
ug/kg
100
102
102
61-138
2-Chlorotoluene
ug/kg
50
58.4
117
73-138
2-Hexanone
ug/kg
100
104
104
58-159
4-Chlorotoluene
ug/kg
50
58.5
117
75-136
4-Methyl-2-pentanone (MIBK)
ug/kg
100
109
109
74-139
Acetone
ug/kg
100
111
111
58-150
Benzene
ug/kg
50
61.2
122
71-140
Bromobenzene
ug/kg
50
53.5
107
72-144
Bromochloromethane
ug/kg
50
56.8
114
78-133
Bromodichloromethane
ug/kg
50
59.7
119
78-133
Bromoform
ug/kg
50
56.3
113
74-132
Bromomethane
ug/kg
50
70.4
141
63-184
Carbon tetrachloride
ug/kg
50
62.6
125
73-143
Chlorobenzene
ug/kg
50
59.1
118
77-137
Chloroethane
ug/kg
50
65.9
132
68-146
Chloroform
ug/kg
50
62.8
126
75-137
Chloromethane
ug/kg
50
62.1
124
54-143
cis-1,2-Dichloroethene
ug/kg
50
57.6
115
71-143
cis-1,3-Dichloropropene
ug/kg
50
60.2
120
76-133
Dibromochloromethane
ug/kg
50
56.2
112
77-131
Dibromomethane
ug/kg
50
58.4
117
63-184
Dichlorodifluoromethane
ug/kg
50
57.6
115
36-173
Diisopropyl ether
ug/kg
50
65.2
130
68-144
Ethylbenzene
ug/kg
50
62.0
124
69-141
Hexachloro-1,3-butadiene
ug/kg
50
59.8
120
70-152
Isopropylbenzene(Cumene)
ug/kg
50
62.3
125
77-143
m&p-Xylene
ug/kg
100
122
122
72-138
Methyl-tert-butyl ether
ug/kg
50
60.6
121
2-138
Methylene Chloride
ug/kg
50
57.5
115
69-136
n-Butylbenzene
ug/kg
50
59.1
118
65-128
n-Propylbenzene
ug/kg
50
59.3
119
72-139
Naphthalene
ug/kg
50
59.1
118
61-138
o-Xylene
ug/kg
50
60.0
120
74-137
p-Isopropyltoluene
ug/kg
50
60.8
122
66-128
sec-Butylbenzene
ug/kg
50
60.2
120
72-140
Styrene
ug/kg
50
60.9
122
76-137
tert-Butyl benzene
ug/kg
50
61.0
122
68-141
Tetrachloroethene
ug/kg
50
59.9
120
72-136
Toluene
ug/kg
50
61.6
123
69-139
trans-1,2-Dichloroethene
ug/kg
50
54.8
110
72-144
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 84 of 97

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
LABORATORY CONTROL SAMPLE:
123230
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
trans- 1,3-Dichloropropene
ug/kg
50
55.9
112
73-135
Trichloroethene
ug/kg
50
63.0
126
75-136
Trichlorofluoromethane
ug/kg
50
65.4
131
69-144
Vinyl acetate
ug/kg
100
107
107
50-150
Vinyl chloride
ug/kg
50
70.1
140
61-145
Xylene (Total)
ug/kg
150
182
121
73-138
1,2-Dichloroethane-d4 (S)
%
90
69-121
4-Bromofluorobenzene (S)
%
97
74-115
Dibromofluoromethane (S)
%
93
79-116
Toluene-d8 (S)
%
100
88-110
MATRIX SPIKE SAMPLE:
123456
9220088003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1-Dichloroethene
ug/kg
ND
47.8
70.8
148
33-158
Benzene
ug/kg
ND
47.8
67.2
140
46-143
Chlorobenzene
ug/kg
ND
47.8
64.5
135
29-159
Toluene
ug/kg
ND
47.8
65.0
133
38-145
Trichloroethene
ug/kg
ND
47.8
65.5
137
70-130 M1
1,2-Dichloroethane-d4 (S)
%
110
69-121
4-Bromofluorobenzene (S)
%
99
74-115
Dibromofluoromethane (S)
%
106
79-116
Toluene-d8(S)
%
103
88-110
SAMPLE DUPLICATE: 123457
9220505003
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
0
1,1,1-Trichloroethane
ug/kg
ND
ND
0
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
0
1,1,2-Trichloroethane
ug/kg
ND
ND
0
1,1-Dichloroethane
ug/kg
ND
ND
0
1,1-Dichloroethene
ug/kg
ND
ND
0
1,1-Dichloropropene
ug/kg
ND
ND
0
1,2,3-Trichlorobenzene
ug/kg
ND
ND
0
1,2,3-Trichloropropane
ug/kg
ND
ND
0
1,2,4-Trichlorobenzene
ug/kg
ND
ND
0
1,2,4-Trimethylbenzene
ug/kg
ND
ND
0
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
0
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
0
1,2-Dichlorobenzene
ug/kg
ND
ND
0
1,2-Dichloroethane
ug/kg
ND
ND
0
1,2-Dichloropropane
ug/kg
ND
ND
0
1,3,5-Trimethylbenzene
ug/kg
ND
ND
0
1,3-Dichlorobenzene
ug/kg
ND
ND
0
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 85 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 123457
Parameter
Units
9220505003
Result
Dup
Result
RPD
1,3-Dichloropropane
ug/kg
ND
ND
0
1,4-Dichlorobenzene
ug/kg
ND
ND
0
2,2-Dichloropropane
ug/kg
ND
ND
0
2-Butanone (MEK)
ug/kg
ND
ND
0
2-Chlorotoluene
ug/kg
ND
ND
0
2-Hexanone
ug/kg
ND
ND
0
4-Chlorotoluene
ug/kg
ND
ND
0
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
0
Acetone
ug/kg
ND
43.8J
31
Benzene
ug/kg
ND
ND
0
Bromobenzene
ug/kg
ND
ND
0
Bromochloromethane
ug/kg
ND
ND
0
Bromodichloromethane
ug/kg
ND
ND
0
Bromoform
ug/kg
ND
ND
0
Bromomethane
ug/kg
ND
ND
0
Carbon tetrachloride
ug/kg
ND
ND
0
Chlorobenzene
ug/kg
ND
ND
0
Chloroethane
ug/kg
ND
ND
0
Chloroform
ug/kg
ND
ND
0
Chloromethane
ug/kg
ND
ND
0
cis-1,2-Dichloroethene
ug/kg
ND
ND
0
cis-1,3-Dichloropropene
ug/kg
ND
ND
0
Dibromochloromethane
ug/kg
ND
ND
0
Dibromomethane
ug/kg
ND
ND
0
Dichlorodifluoromethane
ug/kg
ND
ND
0
Diisopropyl ether
ug/kg
ND
ND
0
Ethylbenzene
ug/kg
ND
ND
0
Hexachloro-1,3-butadiene
ug/kg
ND
ND
0
Isopropylbenzene (Cumene)
ug/kg
ND
ND
0
m&p-Xylene
ug/kg
ND
ND
0
Methyl-tert-butyl ether
ug/kg
ND
ND
0
Methylene Chloride
ug/kg
ND
ND
0
n-Butylbenzene
ug/kg
ND
ND
0
n-Propylbenzene
ug/kg
ND
ND
0
Naphthalene
ug/kg
ND
3J
200
o-Xylene
ug/kg
ND
ND
0
p-Isopropyltoluene
ug/kg
ND
ND
0
sec-Butylbenzene
ug/kg
ND
ND
0
Styrene
ug/kg
ND
ND
0
tert-Butyl benzene
ug/kg
ND
ND
0
Tetrachloroethene
ug/kg
ND
ND
0
Toluene
ug/kg
ND
ND
0
trans-1,2-Dichloroethene
ug/kg
ND
ND
0
trans- 1,3-Dichloropropene
ug/kg
ND
ND
0
Trichloroethene
ug/kg
ND
ND
0
Trichlorofluoromethane
ug/kg
ND
ND
0
Vinyl acetate
ug/kg
ND
ND
0
Vinyl chloride
ug/kg
ND
ND
0
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
SAMPLE DUPLICATE: 123457
9220505003
Dup
Parameter
Units
Result
Result
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
100
115
4-Bromofluorobenzene (S)
%
100
98
Dibromofluoromethane (S)
%
107
106
Toluene-d8 (S)
%
103
103
Date: 06/18/2008 12:11 PM
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
9
22
6
8
8
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 97

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cal 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
QC Batch: GCSV/2948
Analysis Method:
9071 B ASE
QC Batch Method: 9071 B ASE
Analysis Description:
9071 ASE, Oil and Grease
Associated Lab Samples: 9220393001
METHOD BLANK: 123316
Associated Lab Samples: 9220393001
Blank
Reporting
Parameter Units
Result
Limit
Qualifiers
Oil and Grease mg/kg
ND 167
LABORATORY CONTROL SAMPLE: 123317
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Oil and Grease mg/kg
1330
1220
92 78-114
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 123318
123319
MS
MSD
9220312001
Spike
Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Oil and Grease mg/kg ND
1450
1450 1280
1250 88 85 78-114 3
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 88 of 97

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/3427 Analysis Method: EPA 8270
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 9220393012
METHOD BLANK: 124102
Associated Lab Samples: 9220393012
Parameter Units
Blank
Result
Reporting
Limit
1,2,4-Trichlorobenzene
ug/kg
ND
330
1,2-Dichlorobenzene
ug/kg
ND
330
1,2-Diphenylhydrazine
ug/kg
ND
330
1,3-Dichlorobenzene
ug/kg
ND
330
1,4-Dichlorobenzene
ug/kg
ND
330
1-Methylnaphthalene
ug/kg
ND
330
2,4,5-Trichlorophenol
ug/kg
ND
330
2,4,6-Trichlorophenol
ug/kg
ND
330
2,4-Dichlorophenol
ug/kg
ND
330
2,4-Dimethylphenol
ug/kg
ND
330
2,4-Dinitrophenol
ug/kg
ND
1650
2,4-Dinitrotoluene
ug/kg
ND
330
2,6-Dinitrotoluene
ug/kg
ND
330
2-Chloronaphthalene
ug/kg
ND
330
2-Chlorophenol
ug/kg
ND
330
2-Methylnaphthalene
ug/kg
ND
330
2-Methylphenol(o-Cresol)
ug/kg
ND
330
2-Nitroaniline
ug/kg
ND
1650
2-Nitrophenol
ug/kg
ND
330
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
330
3,3'-Dichlorobenzidine
ug/kg
ND
1650
3-Nitroaniline
ug/kg
ND
1650
4,6-Dinitro-2-methyl phenol
ug/kg
ND
660
4-Bromophenylphenyl ether
ug/kg
ND
330
4-ChIoro-3-methyl phenol
ug/kg
ND
660
4-Chloroaniline
ug/kg
ND
1650
4-Chlorophenylphenyl ether
ug/kg
ND
330
4-Nitroaniline
ug/kg
ND
660
4-Nitrophenol
ug/kg
ND
1650
Acenaphthene
ug/kg
ND
330
Acenaphthylene
ug/kg
ND
330
Aniline
ug/kg
ND
330
Anthracene
ug/kg
ND
330
Benzo(a)anthracene
ug/kg
ND
330
Benzo(a)pyrene
ug/kg
ND
330
Benzo(b)fluoranthene
ug/kg
ND
330
Benzo(g,h,i)perylene
ug/kg
ND
330
Benzo(k)fluoranthene
ug/kg
ND
330
Benzoic acid
ug/kg
ND
1650
Benzyl alcohol
ug/kg
ND
660
bis(2-Chloroethoxy)methane
ug/kg
ND
330
bis(2-Chloroethyl) ether
ug/kg
ND
330
bis(2-Chloroisopropyl) ether
ug/kg
ND
330
Qualifiers
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 89 of 97
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
—pacelabs.com
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
METHOD BLANK: 124102
Associated Lab Samples:
Parameter
9220393012
Units
Blank
Result
Reporting
Limit
bis(2-Ethylhexyl)phthalate
ug/kg
ND
330
Butylbenzylphthalate
ug/kg
ND
330
Chrysene
ug/kg
ND
330
Di-n-butylphthalate
ug/kg
ND
330
Di-n-octylphthalate
ug/kg
ND
330
Dibenz(a,h)anthracene
ug/kg
ND
330
Dibenzofuran
ug/kg
ND
330
Diethylphthalate
ug/kg
ND
330
Dimethylphthalate
ug/kg
ND
330
Fluoranthene
ug/kg
ND
330
Fluorene
ug/kg
ND
330
Hexachloro-1,3-butadiene
ug/kg
ND
330
Hexachlorobenzene
ug/kg
ND
330
Hexachlorocyclopentadiene
ug/kg
ND
330
Hexachloroethane
ug/kg
ND
330
Indeno(1,2,3-cd)pyrene
ug/kg
ND
330
Isophorone
ug/kg
ND
330
N-Nitroso-di-n-propylamine
ug/kg
ND
330
N-Nitrosodimethylamine
ug/kg
ND
330
N-Nitrosodiphenylamine
ug/kg
ND
330
Naphthalene
ug/kg
ND
330
Nitrobenzene
ug/kg
ND
330
Pentachlorophenol
ug/kg
ND
1650
Phenanthrene
ug/kg
ND
330
Phenol
ug/kg
ND
330
Pyrene
ug/kg
ND
330
2,4,6-Tribromophenol (S)
%
65
30-150
2-Fluorobiphenyl (S)
%
59
30-150
2-Fluorophenol (S)
%
63
30-150
Nitrobenzene-d5 (S)
%
60
30-150
Phenol-d6 (S)
%
58
30-150
Terphenyl-d14 (S)
%
66
30-150
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
124103
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/kg
1670
1120
67
50-150
1,2-Dichlorobenzene
ug/kg
1670
1100
66
50-150
1,2-Diphenylhydrazine
ug/kg
1670
975
59
50-150
1,3-Dichlorobenzene
ug/kg
1670
1100
66
50-150
1,4-Dichlorobenzene
ug/kg
1670
1140
68
50-150
1-Methylnaphthalene
ug/kg
1670
1620
97
50-150
2,4,5-Trichlorophenol
ug/kg
1670
1340
80
50-150
2,4,6-Trichlorophenol
ug/kg
1670
1230
74
50-150
2,4-Dichlorophenol
ug/kg
1670
1260
76
50-150
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 90 of 97

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
QUALITY CONTROL DATA
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
124103
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4-Dimethylphenol
ug/kg
1670
1350
81
50-150
2,4-Dinitrophenol
ug/kg
1670
886J
53
50-150
2,4-Dinitrotoluene
ug/kg
1670
1220
73
50-150
2,6-Dinitrotoluene
ug/kg
1670
1210
73
50-150
2-Chloronaphthalene
ug/kg
1670
1190
72
50-150
2-Chlorophenol
ug/kg
1670
1270
76
50-150
2-Methylnaphthalene
ug/kg
1670
1280
77
50-150
2-Methylphenol(o-Cresol)
ug/kg
1670
1200
72
50-150
2-Nitroaniline
ug/kg
1670
1460J
88
50-150
2-Nitrophenol
ug/kg
1670
1300
78
50-150
3&4-Methyl phenol (m&p Cresol)
ug/kg
1670
1290
78
50-150
3,3'-Dichlorobenzidine
ug/kg
1670
1660
100
50-150
3-Nitroaniline
ug/kg
1670
1860
112
50-150
4,6-Dinitro-2-methyl phenol
ug/kg
1670
1100
66
50-150
4-Bromophenylphenyl ether
ug/kg
1670
1320
79
50-150
4-Chloro-3-methylphenol
ug/kg
1670
1270
76
50-150
4-Chloroaniline
ug/kg
1670
1860
111
50-150
4-Chlorophenylphenyl ether
ug/kg
1670
1220
73
50-150
4-Nitroaniline
ug/kg
1670
1430
86
50-150
4-Nitrophenol
ug/kg
1670
988J
59
50-150
Acenaphthene
ug/kg
1670
1320
79
50-150
Acenaphthylene
ug/kg
1670
1420
85
50-150
Aniline
ug/kg
1670
1660
99
50-150
Anthracene
ug/kg
1670
1280
77
50-150
Benzo(a)anthracene
ug/kg
1670
1320
79
50-150
Benzo(a)pyrene
ug/kg
1670
1330
80
50-150
Benzo(b)fluoranthene
ug/kg
1670
1140
69
50-150
Benzo(g,h,i)perylene
ug/kg
1670
1360
82
50-150
Benzo(k)fluoranthene
ug/kg
1670
1220
73
50-150
Benzoic acid
ug/kg
1670
604J
36
50-150 LO
Benzyl alcohol
ug/kg
1670
981
59
50-150
bis(2-Chloroethoxy)methane
ug/kg
1670
1280
77
50-150
bis(2-Chloroethyl) ether
ug/kg
1670
1070
64
50-150
bis(2-Chloroisopropyl) ether
ug/kg
1670
1330
80
50-150
bis(2-Ethylhexyl)phthalate
ug/kg
1670
1440
86
50-150
Butylbenzylphthalate
ug/kg
1670
1350
81
50-150
Chrysene
ug/kg
1670
1290
77
50-150
Di-n-butylphthalate
ug/kg
1670
1300
78
50-150
Di-n-octylphthalate
ug/kg
1670
1320
79
50-150
Dibenz(a,h)anthracene
ug/kg
1670
1390
83
50-150
Dibenzofuran
ug/kg
1670
1200
72
50-150
Diethylphthalate
ug/kg
1670
1280
77
50-150
Dimethylphthalate
ug/kg
1670
1330
80
50-150
Fluoranthene
ug/kg
1670
1300
78
50-150
Fluorene
ug/kg
1670
1310
79
50-150
Hexachloro-1,3-butadiene
ug/kg
1670
1110
67
50-150
Hexachlorobenzene
ug/kg
1670
1180
71
50-150
Hexachlorocyclopentadiene
ug/kg
1670
1020
61
50-150
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
[phone]
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Pace Project No.: 9220393
LABORATORY CONTROL SAMPLE: 124103
Parameter
Hexachloroethane
ug/kg
Indeno(1,2,3-cd)pyrene
ug/kg
Isophorone
ug/kg
N-Nitroso-di-n-propylamine
ug/kg
N-Nitrosodimethylamine
ug/kg
N-Nitrosodiphenylamine
ug/kg
Naphthalene
ug/kg
Nitrobenzene
ug/kg
Pentachlorophenol
ug/kg
Phenanthrene
ug/kg
Phenol
ug/kg
Pyrene
ug/kg
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol(S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike
Units Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1670
1130
68
50-150
1670
1350
81
50-150
1670
2140
129
50-150
1670
1070
64
50-150
1670
1440
86
50-150
1670
1350
81
50-150
1670
1190
71
50-150
1670
1100
66
50-150
1670
11901
71
50-150
1670
1300
78
50-150
1670
1290
77
50-150
1670
1210
73
50-150
87
30-150
79
30-150
84
30-150
79
30-150
84
30-150
78
30-150
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 124104
9220463004
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
124105
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/kg
ND
1980
1980
1310
1240
66
63
50-150
6
1,4-Dichlorobenzene
ug/kg
ND
1980
1980
1270
1220
64
62
50-150
4
2,4-Dinitrotoluene
ug/kg
ND
1980
1980
1430
1330
72
67
50-150
8
2-Chlorophenol
ug/kg
ND
1980
1980
1170
1150
59
58
50-150
1
4-Chloro-3-methyl phenol
ug/kg
ND
1980
1980
1160
1190
59
60
50-150
3
4-Nitrophenol
ug/kg
ND
1980
1980
802J
790J
41
40
50-150
MO
Acenaphthene
ug/kg
ND
1980
1980
1450
1360
73
69
50-150
6
N-Nitroso-di-n-propylamine
ug/kg
ND
1980
1980
1490
1420
75
72
50-150
5
Pentachlorophenol
ug/kg
ND
1980
1980
1250J
1180J
63
60
50-150
Phenol
ug/kg
ND
1980
1980
1210
1250
61
63
50-150
3
Pyrene
ug/kg
ND
1980
1980
1320
1190
67
60
50-150
11
2,4,6-Tribromophenol (S)
%
59
60
30-150
2-Fluorobiphenyl (S)
%
71
68
30-150
2-Fluorophenol(S)
%
56
57
30-150
Nitrobenzene-d5(S)
%
78
77
30-150
Phenol-d6 (S)
%
60
62
30-150
Terphenyl-d14(S)
%
70
64
30-150
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/3431 Analysis Method: EPA 8015 Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 9220393004
METHOD BLANK: 124189
Associated Lab Samples: 9220393004
Blank Reporting
Parameter Units Result Limit Qualifiers
Diesel Components mg/kg ND 5.0
n-Pentacosane(S) % 88 50-135
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 124190
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
% Rec
Limits Qualifiers
Diesel Components mg/kg
167
138
83
50-114
n-Pentacosane(S) %
74
50-135
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 124191
124192
MS
MSD
9220615001
Spike
Spike MS
MSD
MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result
% Rec % Rec
Limits RPD Qual
Diesel Components mg/kg ND
202
202 190
138
93 67
50-107 32 R1
n-Pentacosane(S) %
116 81
50-135
Date: 06/18/2008 12:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 93 of 97

aceAnalytical
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Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/3653 Analysis Method: SM 6210
QC Batch Method: SM 6210 Analysis Description: 6210 MSV
Associated Lab Samples: 9220393018
METHOD BLANK: 124847
Associated Lab Samples: 9220393018
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 06/18/2008 12:11 PM
Units
Blank
Result
Reporting
Limit
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
2.0
ug/L
ND
0.50
ug/L
ND
2.0
ug/L
ND
0.50
ug/L
ND
1.0
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
1.0
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
1.0
ug/L
ND
0.50
ug/L
ND
1.0
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
2.0
ug/L
ND
0.50
Qualifiers
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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aceAnalytical
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Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
METHOD BLANK: 124847
Associated Lab Samples:
Parameter
9220393018
Units
Blank
Result
Reporting
Limit Qualifiers
m&p-Xylene
ug/L
ND
1.0
Methyl-tert-butyl ether
ug/L
ND
0.50
Methylene Chloride
ug/L
ND
2.0
n-Butylbenzene
ug/L
ND
0.50
n-Propylbenzene
ug/L
ND
0.50
Naphthalene
ug/L
ND
2.0
o-Xylene
ug/L
ND
0.50
p-Isopropyltoluene
ug/L
ND
0.50
sec-Butylbenzene
ug/L
ND
0.50
Styrene
ug/L
ND
0.50
tert-Butyl benzene
ug/L
ND
0.50
Tetrachloroethene
ug/L
ND
0.50
Toluene
ug/L
ND
0.50
trans-1,2-Dichloroethene
ug/L
ND
0.50
trans- 1,3-Dichloropropene
ug/L
ND
0.50
Trichloroethene
ug/L
ND
0.50
Trichlorofluoromethane
ug/L
ND
1.0
Vinyl chloride
ug/L
ND
1.0
1,2-Dichloroethane-d4 (S)
%
93
60-140
4-Bromofluorobenzene (S)
%
102
60-140
Dibromofluoromethane (S)
%
104
60-140
Toluene-d8 (S)
%
100
60-140
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
124848
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
10
12.2
122
60-140
1,1,1-Trichloroethane
ug/L
10
13.2
132
60-140
1,1,2,2-Tetrachloroethane
ug/L
10
10.0
100
60-140
1,1,2-Trichloroethane
ug/L
10
11.2
112
60-140
1,1-Dichloroethane
ug/L
10
12.5
125
60-140
1,1-Dichloroethene
ug/L
10
11.3
113
60-140
1,1-Dichloropropene
ug/L
10
11.6
116
60-140
1,2,3-Trichlorobenzene
ug/L
10
9.7
97
60-140
1,2,3-Trichloropropane
ug/L
10
10.6
106
60-140
1,2,4-Trichlorobenzene
ug/L
10
10.6
106
60-140
1,2,4-Trimethylbenzene
ug/L
10
12.2
122
60-140
1,2-Dibromo-3-chloropropane
ug/L
10
9.5
95
60-140
1,2-Dibromoethane (EDB)
ug/L
10
11.2
112
60-140
1,2-Dichlorobenzene
ug/L
10
11.6
116
60-140
1,2-Dichloroethane
ug/L
10
12.0
120
60-140
1,2-Dichloropropane
ug/L
10
12.2
122
60-140
1,3,5-Trimethylbenzene
ug/L
10
12.0
120
60-140
1,3-Dichlorobenzene
ug/L
10
11.4
114
60-140
1,3-Dichloropropane
ug/L
10
11.2
112
60-140
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 95 of 97
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aceAnalytical
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Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
124848
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
10
11.3
113
60-140
2,2-Dichloropropane
ug/L
10
13.5
135
60-140
2-Chlorotoluene
ug/L
10
11.7
117
60-140
4-Chlorotoluene
ug/L
10
11.8
118
60-140
Benzene
ug/L
10
11.7
117
60-140
Bromobenzene
ug/L
10
10.6
106
60-140
Bromochloromethane
ug/L
10
12.3
123
60-140
Bromodichloromethane
ug/L
10
13.0
130
60-140
Bromoform
ug/L
10
10.6
106
60-140
Bromomethane
ug/L
10
15.4
154
60-140 L3
Carbon tetrachloride
ug/L
10
12.3
123
60-140
Chlorobenzene
ug/L
10
11.9
119
60-140
Chloroethane
ug/L
10
13.3
133
60-140
Chloroform
ug/L
10
13.1
131
60-140
Chloromethane
ug/L
10
13.0
130
60-140
cis-1,2-Dichloroethene
ug/L
10
13.0
130
60-140
cis-1,3-Dichloropropene
ug/L
10
12.2
122
60-140
Dibromochloromethane
ug/L
10
11.8
118
60-140
Dibromomethane
ug/L
10
11.9
119
60-140
Dichlorodifluoromethane
ug/L
10
15.3
153
60-140 L3
Diisopropyl ether
ug/L
10
12.5
125
60-140
Ethylbenzene
ug/L
10
12.2
122
60-140
Hexachloro-1,3-butadiene
ug/L
10
12.0
120
60-140
Isopropylbenzene (Cumene)
ug/L
10
12.2
122
60-140
m&p-Xylene
ug/L
20
24.2
121
60-140
Methyl-tert-butyl ether
ug/L
10
11.3
113
60-140
Methylene Chloride
ug/L
10
11.9
119
60-140
n-Butylbenzene
ug/L
10
11.8
118
60-140
n-Propylbenzene
ug/L
10
11.8
118
60-140
Naphthalene
ug/L
10
9.6
96
60-140
o-Xylene
ug/L
10
12.1
121
60-140
p-Isopropyltoluene
ug/L
10
12.1
121
60-140
sec-Butylbenzene
ug/L
10
12.0
120
60-140
Styrene
ug/L
10
11.9
119
60-140
tert-Butyl benzene
ug/L
10
12.2
122
60-140
Tetrachloroethene
ug/L
10
11.7
117
60-140
Toluene
ug/L
10
11.6
116
60-140
trans-1,2-Dichloroethene
ug/L
10
11.2
112
60-140
trans- 1,3-Dichloropropene
ug/L
10
11.8
118
60-140
Trichloroethene
ug/L
10
11.7
117
60-140
Trichlorofluoromethane
ug/L
10
13.6
136
60-140
Vinyl chloride
ug/L
10
14.1
141
60-140 L3
1,2-Dichloroethane-d4 (S)
%
96
60-140
4-Bromofluorobenzene (S)
%
102
60-140
Dibromofluoromethane (S)
%
108
60-140
Toluene-d8 (S)
%
100
60-140
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 96 of 97
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® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
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www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALIFIERS
Project: IMPERIAL TOBACCO 200817
Pace Project No.: 9220393
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
ANALYTE QUALIFIERS
1g Acid surrogate recovery outside of control limits. The data was accepted based on valid recovery of the 2 remaining acid
surrogates.
2g RPD value was outside of control limits, however % recoveries were acceptable. Samples for QC batch accepted based
on % recoveries and completeness of QC data.
B- Analyte detected in method blank but was not detected in the associated samples.
C9 Common Laboratory Contaminant.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
MO Matrix spike recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
S1 Surrogate recovery outside laboratory control limits (confirmed by re -analysis).
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
Date: 06/18/2008 12:11 PM REPORT OF LABORATORY ANALYSIS Page 97 of 97
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i
a
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Section A Section B
Required Client Information: Required Project Information:
Companaj
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Address- Copy To:
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Phone: `� ax: Project Name MAk
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Requested Due Date/TAT: Project Number:
260 0 / :?---
CHAIN-OF-CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
0
Section C
Invoice Information:
Attention:
Company Name:
Address:
Pace Quote
Reference:
Pace Project
Manager:
Pace Profile #: r
Woo, 2
K 1A
Section D
Matrix Codes
-
Required Client Information
MATRIX / CODE
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COLLECTED
Preservatives
Drinking Water DW
0
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0U
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Water WT
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COMPOSITE
COMPOSITE
Waste Water WW
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START
END/GRAB
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Product P
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Soil/Solid SL
a
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SAMPLE ID
Oil
wP
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(A-Z, 0-9 / ,-)
wipe
Air AR
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Sample IDS MUST BE UNIQUE
Tissue TS
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Other OT
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ADDITIONAL COMME T$
Site Locat`tor
O R I NL PRINT Name of SAMPLER: IZ�J,"
i SIGNATURE of SAMPLER• DATE Signed �y9 6 fi
(MM/DD/YY):
*Important Note: By signing this rm you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days.
Pace Pro"
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SAMPLE CONDITIONS
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F-ALL-Q-020rev.07, 15-May-2007

............
OR I� =� I N A L PRINT Name of SAMPLER:
SIGNATURE of SAMPLER:
"Important Note: By signing this 111,
rm you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days.
SAMPLE CONDITIONS
C � CU
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DATE Signed aEi v CU E
(MM/DD/YY):
F-ALL-Q-020rev.07, 15-May-2007

£ i � �r•:.t- c"��. � .r.}�> ./ rv.. tT.. "�>'-te• •�'. r. �� �'b"^ ' �wf� r�+�:��r�-1
aceAnalytical r •
Client Name:�1aae393
Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client EJ Commercial Pace Other
O Ilona( .....'
p
Custody Seal on Cooler/Box Present: EJ es
Y
�no
Se als Intact. ❑ yes
\Z no Prod Die Date N/A
Packing Material: Bubble W ra u�_L�g _ t\Lone [30the r
Pro
Thermometer Used T060
Type of ice:
Blue None
Samples on ice, coolingprocess has begun
un 9
Cooler Temperature
Biological
Tissue is Frozen: Yes No
N/A Date and Initi Is of erson ping
Temp should be above freezing to 6°C
Comments:
ixam
contents:
Chain of Custody Present:
Yes ONo
ON/A 1.
Chain of Custody Filled Out:
bdYes ONo
ON/A 2.
Chain of Custody Relinquished: -
bdYes ONo
ON/A 3.
Sampler Name & Signature on COC:
`CJYes ONo
ON/A 4
Samples Arrived within Hold Time:
-QYes ONo
ON/A 5.
Short Hold Time Analysis (<72hr):
OYes Nl o
ON/A 6.
Rush Turn Around Time Requested:
OYes o
ON/A 7.
17
Sufficient Volume:
OYes Nco
ON/A 8.
L) CA
Correct Containers Used:
des ONo
ON/A
g. =i5e-
-
-Pace Containers Used:
Xes ONo
El N/A
Containers Intact:
fires ONo
ON/A
10.
Filtered volume received for Dissolved tests
OYes O No
a1A
11.
Sample Labels match COC:
C;4es ONo
ON/A
12.
-Includes date/time/ID/Analysis Matrix: Sil
All containers needing preservation have been check d
vd Y e s O No O N/A j 00 1 V icAk
All containers needing preservation are found to be in
es LJ No O N/A Q
compliance with EPA recommendation. �\1 sk
exceptions. VOA, coliform, TOC, O&G, WI-DRO water OYes ONo
Initial when completed
Samples checked for dechlorination:- %of!]Yes ONo ON/A 14. _.
Headspace in VOA Vials ( >6mm): ❑Yes Rio ON/A 15.
Trip Blank Present: \L;es ONo . ON/A 16.
Trip Blank Custody Seals Present es ONo ON/A
Pace Trip Blank Lot # (if purchased): N/A kL
Client Notification/ Resolution:
Person Contacted, -
Comments/ Resolution:
Date/Time,
Field Data Required? Y / N / N/A
7
Project Manager Review:
Date: -1500/30/0,
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)

June 13, 2008
Pace Analytical Services Inc.
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
Attn: Kevin Herring
RE: 9220393
NORTH COAST
LABORATORIES LTD.
Order No.: 0806089
Invoice No.: 75172
PO No.: CHSO4200
ELAP No. 1247-Expires July 2008
SAMPLE IDENTIFICATION
Fraction Client Sample Description
ND =Not Detected at the Reporting Limit
01A 9220393013/SB-12 Limit=Reporting Limit
02A 9220393014/SB-13
All solid results are expressed on a wet -
weight basis unless otherwise noted.
REPORT CERTIFIED BY
Laboratory Supervisor(s) QA Llfiit Jesse G. Chaney, Jr.
Laboratory Director
5680 West End Road d Arcata California 95521-9202 - 707-822-4649 • FAX [phone]
------------------------------—fhinletlnrrAecVded PePer_--_---__ _.-__—___—_.--_ _---- ___--_____—_—.____ _ - ___---_—__—

Date: 13-Jun-2008
WorkOrder: 0806089
Client Sample ID: 9220393013/SB-12
Lab ID: 0806089-OIA
ANALYTICAL DEPORT
Received:06/03/08 Collected: 05/28/08 14:20
Test Name: Chloropicrin Reference: EPA 8021 B Modified
Parameter Result Limit Units DF Extracted Analyzed
Chloropicrin ND 10 pg/L 1.0 06/11/08
Surrogate: 2-Bromo-1-chloropropane 80.2 70-130 % Rec 1.0 06/11/08
Client Sample ID: 9220393014/SB-13 Received: 06/03/08 Collected: 05/28/08 14:00
Lab ID: 0806089-02A
Test Name: Chloropicrin Reference: EPA 8021 B Modified
Parameter Result Limit Units DF Extracted Analyzed
Chloropicrin ND 10 pg/L 1.0 06/11/08
Surrogate: 2-Bromo-1-chloropropane 81.5 70-130 % Rec 1.0 06/11/08
Page 1 of 1
NORTH COAST LABORATORIES
5680 West End Road • Arcata, California 95521-9202 = 707-822-4649 FAX 707=822-6831

North Coast Laboratories, Ltd. Date: 13-Jun-2009
CLIENT: Pace Analytical Services Inc. QC SUMMARY REPORT
Work Order: 0806089
Project: 9220393 Method Blank
Sample ID: MS 061108 Batch ID: R52777 Test Code: CHLORW Units: pg/L Analysis Date 06111/08 19:34:08 Prep Date:
Client ID: Run ID: ORGC1_080611A SegNo: 769342
Analyte Result Limit SPK value SPK Ref Val % Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual
Chloropicrin ND 10
2-Bromo-l-chloropropane 0.843 0.10 1.00 0 84.8% 70 130 0
Qualifiers: ND - Not Detected at the Reporting Limit S - Spike Recovery outside accepted recovery limits B - Analyte detected in the associated Method Blank
J - Analyte detected below quantitation limits R - RPD outside accepted recovery limits

- ---- _ -1- -EILM
North Coast Laboratories, Ltd. Date: 13-Jun-2008
CLIENT: Pace Analytical Services Inc.
QC SUMMARY REPORT
Work Order: 0806089
Laboratory Control Spike
Project: 9220393
Sample ID: LCS-08331
Batch ID: R52777
Test Code: CHLORW
Units: pg/L
Analysis Date 06111108 17:35:411
Prep Date:
Client ID:
Run ID: ,
ORGC1_080611A
SegNo:
7F 9340
Analyte
Result
Limit
SPK value
SPK Ref Val
% Rec
LowLimit
Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Chloropicrin
52.22
10
50.0
0
1040/6
70
130 0
2-Bromo-1-chloropropane
1.02
0.10
1.00
0
102%
70
130 0
Sample ID: LCSD-08331
Batch ID: R52777
Test Code: CHLORW
Units: Ng/L
Analysis Date 06/11/08 18:32:25
Prep Date:
Client ID:
Run ID:
ORGC1_080611A
SegNo:
769341
Analyte
Result
Limit
SPK value
SPK Ref Val
% Rec
Lowl-imit
HighUrnit RPD Ref Val
%RPD RPDLimit Qual
Chloropicrin
50.46
10
50.0
0
101%
70
130 52.2
3.43% 20
2-Bromo-1-chloropropane
1.02
0.10
1.00
0
102%
70
130 1.02
0.561% 20
Qualifiers: ND - Not Detected at the Reporting Limit S - Spike Recovery outside accepted ;recovery limits B - Analyte detected in the associated Method Blank
J - Analyte detected below quantitation limits R - RPD outside accepted recovery limits

accAna/ytica/
i
SUBCONTRACTOR CHAIN -OF -CUSTODY RECORD
Sub Lab: NORTH COAST LABS
Contact: �O�C�L}i�l�E C9©11IC4
Address: 5-tydy Pees - e-r4'r> 91> .
,4f?-c�-171-, C g597P
Phone:
REQUESTED DUE DATE Pace Project Number:
6/5/08 Pace Project Manager:
P.O.#
Price Per Analysis:
Total Price:
Pace Analytical Services Inc.
9800 Kincey Avenue, Suite 1b0
Hun'tersville, NC 28078
Phone: [phone]
Fax: [phone]
9220393
Kevin Herring
CHSO4200
$ 100.00
$ 200.00
=Z'ace=Sam `le No /_.Clxeni I D
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9220393013/SB-12
WT
5/28/0814:20
3
NA
CHLOROPICRIN
9220393014/SB-13
WT
5/28/0814:00
3
NA
CHLOROPICRIN
f
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10,
Please fax or email allresults bytequested due date to: [phone] or [e-mail].f