23009_Phase II Environmental Site Assessment - Former Clorox Facility - 07.03.2019

Phase II Environmental Site Assessment

Former Clorox Facility
800 Gesco Street
Charlotte, North Carolina

July 3, 2019
H&H Job No. BCP-129

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Phase II Environmental Site Assessment Former Clorox Facility 800 Gesco Street Charlotte, North Carolina H&H Job No. BCP-129
Table of Contents

1.0 Introduction and Background ........................................................................................................ 1
2.0 Phase II ESA Activities ................................................................................................................... 5
3.0 Soil Assessment Activities .............................................................................................................. 6
3.1 Soil Sampling Methodology ................................................................................................... 6
3.2 Soil Analytical Results ............................................................................................................ 7
4.0 Groundwater Assessment Activities ............................................................................................. 9
4.1 Groundwater Sampling Methodology .................................................................................... 9
4.2 Groundwater Analytical Results .......................................................................................... 10
5.0 Vapor Intrusion Assessment Activities ...................................................................................... 12
5.1 Exterior Soil Gas Sampling Methodology ........................................................................... 12
5.2 Exterior Soil Gas Analytical Results .................................................................................... 13
6.0 Conclusions and Recommendations ........................................................................................... 14
List of Tables
Table 1 Summary of Soil Analytical Results
Table 2 Summary of Temporary Monitoring Well Construction and Water Level Data
Table 3 Summary of Groundwater Analytical Results
Table 4 Summary of Exterior Soil Gas Analytical Results
List of Figures
Figure 1 Site Location Map
Figure 2 Site and Sample Location Map
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List of Appendices

Appendix A Boring Logs
Appendix B Laboratory Analytical Reports
Appendix C Field Forms

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Phase II Environmental Site Assessment Former Clorox Facility 800 Gesco Street Charlotte, North Carolina H&H Job No. BCP-129 1.0 Introduction and Background

Hart & Hickman, PC (H&H) has prepared this Phase II Environmental Site Assessment (ESA)
report to document assessment activities conducted at the former Clorox facility located at 800
Gesco Street in Charlotte, Mecklenburg County, North Carolina (Site). A Site location map is
included as Figure 1.

The Site consists of three parcels of land (Parcel Identification Numbers 07108101, 07108102, and
07107805) that total approximately 4.63 acres. The western portion of the Site is developed with an
approximately 32,973-square foot (sq ft) industrial building that was constructed in 1952. The
building is utilized by Plyler Paper Stock Company to store, sort, bale, and distribute recyclable
(primarily paper) products. Historically, the existing Site building was utilized by Clorox as a
bleach manufacturing facility from the early 1950s until the late 1980s, when Plyler Paper Stock
Company began using the building for the current recycling operation. The eastern portion of the
Site consists of a truck/trailer parking lot and undeveloped land. A Site map is included as Figure 2.

During recent Phase I ESA activities conducted on the Site, H&H identified the following
Recognized Environmental Conditions (RECs):

• In March 1990, two soil borings were advanced adjacent to two petroleum aboveground
storage tanks (ASTs; specific contents not reported), a former 5,000-gallon heating oil
underground storage tank (UST), and a former 2,000-gallon UST (presumed to have
contained heating oil) located adjacent to the northeastern corner of the Site building.
Total Petroleum Hydrocarbons-Diesel Range Organics (TPH-DRO) were detected in a
boring identified as Boring 1 (11 ft) at a concentration of 1,600 mg/kg, which exceeds the

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current North Carolina Department of Environmental Quality (DEQ) UST Section Action
Level of 100 mg/kg.

A separate heating oil UST release incident was identified in this area in November 1990;
however, the soil data pertaining to the release did not indicate TPH-DRO in soil above
the DEQ Action Level. The UST release incident received regulatory closure in July
1996. The soil impacts identified in Boring 1 (noted above) do not appear to have been
included in DEQ’s evaluation of the UST release and No Further Action determination,
and may be associated with the two ASTs. H&H identified the presence of TPH-DRO in
soil adjacent to the northeastern portion of the Site building at a concentration above the
DEQ Action Level as a REC.

• H&H reviewed a Combined Preliminary Assessment/Site Inspection (September 2005)
and an Expanded Site Inspection (September 2006) prepared by the DEQ Superfund
Section for the former Clorox facility, which included the Site and off-Site properties
located north of the Site along State Street. According to the report, the former Clorox
facility operated in the northern portion of the Site building from the early 1950s until the
late 1980s.

No samples were collected on the subject Site during the Preliminary Assessment;
however, several soil samples were collected on the Site during the Expanded Site
Inspection. Soil analytical data indicated the presence of cadmium (3.7 mg/kg) and
mercury (48.09 mg/kg) in sample CLX-009-SS (west side of the building near former rail
spur) at concentrations above the Protection of Groundwater Preliminary Soil
Remediation Goal (PSRG) of 3.0 mg/kg for cadmium and the Residential PSRG of 14
mg/kg for mercury. The polynuclear aromatic hydrocarbon (PAH) benzo(a)anthracene
was detected near northeast exterior corner of the building in samples CLX-009-SS (0.83
mg/kg) and CLX-011-SS (1.1 mg/kg) at concentrations above the Protection of
Groundwater PSRG of 0.35 mg/kg in both samples and equal to the Residential PSRG of
1.1 mg/kg in one of the samples. The PAH benzo(a)pyrene was detected in samples
CLX-009-SS (0.57 mg/kg) and CLX-011-SS (0.73 mg/kg) at concentrations above the

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Residential PSRG of 0.11 mg/kg. H&H identified the presence of metals and PAHs at
concentrations above PSRGs in soil near the northeastern corner of the building as a
REC.

• Based on review of Sanborn Maps and interviews with Site contacts, Clorox operated a
mixing room that was used to manufacture bleach in the northwestern portion of the Site
building. The Site owner reported that the room contained multiple ASTs when she
purchased the Site in the late 1980s. During Site reconnaissance, H&H observed an
earthen floor and a sump in the former mixing room. Previous reports indicate that the
bleach manufacturing facility may have included the use of a mercury cell, which
produces chlorine-free sodium hydroxide. H&H identified potential environmental
impacts associated with bleach manufacturing at the Site from the early 1950s to the late
1980s as a REC.

• In 1990, two soil borings (Boring 1 and Boring 2) were advanced adjacent to a concrete
basin located adjacent to a rail spur along the western portion of the Site. Previous
reports indicate that sodium hydroxide and mercury releases may have occurred from the
concrete basin. Analytical data indicated the presence of mercury in a soil sample
collected from Boring 1 (0.5 ft) at a concentration of 2.8 mg/kg, which exceeds the
protection of groundwater PSRG of 1.0 mg/kg. The measured pH levels in samples
collected from Boring 1 and Boring 2 were 13 (2.5 ft) and 13.5 (0.5 ft), respectively,
which are elevated (i.e., alkaline) compared to typical soil pH levels in the area and may
indicate that a release of sodium hydroxide occurred from the concrete basin. H&H
identified the apparent soil impacts in the area of the former concrete basin as a REC.

• Worth Chemical Corp. (818 Tuckaseegee Road) operated a chemical distribution facility
located approximately 250 ft west and topographically upgradient of the subject Site.
H&H reviewed a Site Assessment Work Plan prepared by Arcadis dated December 13,
2010. According to the report, the facility utilized ASTs and USTs for the storage of
petroleum products, chlorinated solvents, and other hazardous materials. Results of

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historical soil and groundwater assessment activities conducted at the facility indicated
the presence of soil and groundwater impacts associated with releases from the petroleum
and chlorinated solvent storage tanks. Based on the documented solvent releases,
proximity of the facility to the Site, and area topography, H&H identified the former
Worth Chemical Corp. facility and associated releases as a REC for the Site.

H&H understands that plans for the Site include commercial redevelopment in accordance with a
potential Brownfields Agreement with DEQ. Therefore, H&H conducted Phase II ESA activities
at the Site in general accordance with DEQ Brownfields Program guidance to evaluate the potential
for the above-mentioned RECs to impact the proposed redevelopment project. The Phase II ESA
activities included collection of soil, groundwater, and exterior soil gas samples. The methods and
results of the assessment activities are detailed in the following sections.

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2.0 Phase II ESA Activities
Between February 7 and 13, 2019, H&H completed soil, groundwater, and vapor intrusion
assessment activities at the Site to evaluate potential impacts associated with historical Site and
nearby upgradient property uses. Prior to conducting assessment activities, H&H contacted North
Carolina 811, the public utility locator, to mark subsurface utilities on the Site. H&H also
contracted with Ground Penetrating Radar Systems (GPRS), a private utility locator, to screen
proposed sample locations for subgrade utilities and to confirm public utility locator markings.
Additionally, boring locations were hand cleared to approximately 5 ft below the ground surface
(bgs) to further screen the boring locations for the presence of subsurface utilities.

In accordance with Mecklenburg County regulations, H&H obtained a Subsurface Investigation
Permit (SIP No. 70002585) from the Mecklenburg County Land Use and Environmental Services
Agency (LUESA) prior to beginning groundwater assessment activities. After sampling was
completed, the SIP was closed out by submitting a well abandonment record to LUESA.

The assessment activities were conducted in general accordance with the DEQ Inactive Hazardous
Sites Branch (IHSB) Guidelines for Assessment and Cleanup dated October 2015, DEQ’s Division
of Waste Management (DWM) Vapor Intrusion Guidance dated March 2018, and the most recent
versions of the U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem
Support (SESD) Field Branches Quality System and Technical Procedures guidance.

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3.0 Soil Assessment Activities

3.1 Soil Sampling Methodology

On February 7 and 8, 2019, H&H contracted Innovative Environmental Technologies (IET), a
North Carolina-licensed drilling contractor, to advance nine soil borings (SB-2 through SB-6,
and SB-9 through SB-12) using a track-mounted direct push technology (DPT) drill rig and hand
auger. Soil boring locations are described below and are depicted on Figure 2.

• Soil borings SB-2 and SB-3 were advanced to approximately 5 ft bgs within the former
bleach mixing room in the northwestern portion of the building.
• Soil boring SB-4 was advanced to approximately 15 ft bgs adjacent to former heating oil
USTs/ASTs and previously identified petroleum-related soil impacts in the northern
portion of the Site.
• Soil boring SB-5 was advanced to approximately 18 ft bgs downgradient of the former
bleach manufacturing facility and within a proposed landscaped area located east of the
building.
• Soil boring SB-6 was advanced to approximately 5 ft bgs within a proposed sub-grade
patio on the west side of the building.
• Soil borings SB-9 through SB-12 were advanced to approximately 5 ft bgs within a
proposed parking lot along the eastern portion of the Site across Gesco Street to evaluate
background soil conditions.

Continuous soil samples were collected from each boring, logged for lithologic description, and
field screened for the presence of staining, odors, and volatile organic vapors using a calibrated
photoionization detector (PID). Based upon field screening results, H&H collected one soil
sample for laboratory analysis from the depth interval that exhibited the greatest evidence of
potential impact (i.e., elevated PID readings, staining, and/or odors). If no obvious indications of
soil impacts were observed during field screening, H&H collected a soil sample from
approximately 0 to 2 ft bgs to evaluate a potential surface release.

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Soil samples selected for laboratory analysis were placed directly into dedicated laboratory-
supplied sample containers; labeled with the sample identification, date, and requested analysis;
and placed in a laboratory-supplied sample cooler with ice. The samples were delivered to Pace
Analytical Services, LLC (Pace), a North Carolina certified laboratory, under standard chain of
custody protocols for analysis of volatile organic compounds (VOCs) by EPA Method 8260B,
semi-VOCs (SVOCs) by EPA Method 8270D, Resource Conservation and Recovery Act
(RCRA) metals by EPA Methods 6020B/7471B, and hexavalent chromium by EPA Method
7199.

3.2 Soil Analytical Results

The soil analytical results were compared to the DEQ IHSB Protection of Groundwater,
Residential, and Industrial/Commercial PSRGs dated May 2019. In addition to the PSRGs,
metals data were compared to the Site-specific background data, and the range and average
background metals concentrations reported in literature for North Carolina soil or southeastern
United States soil (if North Carolina data was not available). A tabular summary of soil
analytical results is presented in Table 1. The laboratory analytical report and chain of custody
record are provided in Appendix B.

Laboratory analytical results indicate detections of acetone (0.0121 to 0.167 mg/kg) in the nine
soil samples collected for laboratory analysis. The detected acetone concentrations are below the
most stringent (i.e., Protection of Groundwater) PSRG. Further, acetone is a common laboratory
contaminant; therefore, the detection of trace levels of acetone may not be representative of Site
soil conditions. Trace concentrations of the VOCs 2-butanone, toluene, m&p-xylene,
chloroform, 4-methyl-2-pentanone, and/or naphthalene were detected each soil sample at
concentrations below the Protection of Groundwater, Residential, and Industrial/Commercial
PSRGs.

Several SVOCs (specifically PAHs) were detected in samples collected in the former bleach
mixing room (SB-2 and SB-3) and adjacent to the former heating oil USTs/ASTs (SB-4). Several
PAHs were detected above the Protection of Groundwater and Residential PSRGs in sample SB-

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3 (0-2 ft). Of the PAHs, benzo(a)pyrene (6.81 mg/kg) was detected in SB-3 (0-2 ft) above the
Industrial/Commercial PSRG of 2.1 mg/kg. Benzo(a)pyrene was also detected in sample SB-4
(7-9 ft) at an estimated concentration of 0.144 J mg/kg, which exceeds the Protection of
Groundwater and Residential PSRGs of 0.12 mg/kg and 0.11 mg/kg, respectively. No SVOCs
were detected above the laboratory method detection limits (MDLs) in samples SB-5 (0-2 ft),
SB-6 (0-2 ft), or SB-9 (0-2 ft) through SB-12 (0-2 ft).

The metals arsenic, barium, chromium (hexavalent and trivalent), lead, mercury, and/or selenium
were detected in the nine soil samples analyzed by the laboratory. The arsenic concentrations,
which range from 1.42 mg/kg in sample SB-10 (0-2 ft) to 3.07 mg/kg in SB-6 (0-2 ft), exceed the
Residential PSRG of 0.68 mg/kg in all nine soil samples and slightly exceed the
Industrial/Commercial PSRG of 3.0 mg/kg in sample SB-6 (0-2 ft). The detected concentrations
of arsenic in the samples collected from the developed portion of the Site (SB-2 through SB-6)
are consistent with arsenic concentrations detected in background samples SB-9 through SB-12.
Further, the detected concentrations are below the average published background concentration
for North Carolina soils of 4.8 mg/kg. As such, the detected arsenic concentrations appear to be
naturally occurring.

Hexavalent chromium was detected at estimated concentrations in samples SB-2 (0-2 ft), SB-3
(0-2 ft), SB-6 (0-2 ft), SB-9 (0-2 ft), and SB-11 (0-2 ft) at concentrations ranging from 0.376
mg/kg in SB-11 (0-2 ft) to 0.913 mg/kg in SB-9 (0-2 ft). The detections exceed the Residential
PSRG of 0.31 mg/kg. The detected concentrations of hexavalent chromium in the samples
collected from the developed portion of the Site (SB-2 through SB-6) are consistent with
hexavalent chromium concentrations detected in background samples SB-9 through SB-12. As
such, the hexavalent chromium concentrations are likely representative of background
conditions. Published background concentrations for hexavalent chromium in North Carolina
soils are not available.

The remaining metals were detected at concentrations below the Protection of Groundwater,
Residential, and Industrial/Commercial PSRGs and generally consistent with published and Site-
specific background levels.

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4.0 Groundwater Assessment Activities
4.1 Groundwater Sampling Methodology

On February 7, 2019, IET installed one temporary monitoring well (TMW-2) using DPT drilling
methods. The temporary monitoring well (depicted on Figure 2) was installed within boring SB-5
which is located downgradient of the former bleach manufacturing facility.

The temporary monitoring well was constructed of 2-inch diameter PVC riser pipe with 10 ft of pre-
packed well screen set to bracket the water table. Additional filter sand was placed in the well
annulus from the base of the borehole to approximately two feet above the well screen. Hydrated
bentonite was installed from the top of the filter pack to approximately 0.5 ft bgs. A temporary
monitoring well boring log is provided in Appendix A, and temporary well construction details are
provided in Table 2.

The approximate depth to groundwater in the well (11.38 ft bgs) was measured using an electronic
water level indicator on February 11, 2019. Groundwater flow direction could not be determined
with the one temporary monitoring well. However, groundwater elevation data obtained during
assessment activities at the upgradient Worth Chemical Corp. facility indicate an easterly flow
direction near the Site toward Stewart Creek.

The temporary well was developed by removing approximately five volumes of water from the
well. The well was purged dry multiple times during development and field parameters did not
stabilize (stabilization criteria of pH ± 0.1 SU and conductivity varied no more than 5%). The well
development log is provided in Appendix C. After development efforts, the temporary monitoring
well was purged using low-flow/low-stress purging techniques using a peristaltic pump and
dedicated polyethylene tubing. The intake point of the pump tubing was placed in the approximate
mid-portion of the saturated portion of the screened interval of the well, and groundwater was
removed at a rate no greater than 200 milliliters per minute. H&H utilized a calibrated water quality
meter to collect measurements of pH, temperature, dissolved oxygen, oxidation-reduction potential,
turbidity, and specific conductivity during the purging process. Purging was considered complete
when the parameters had stabilized (pH ± 0.1 SU, conductivity varied no more than 5%, and

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turbidity was less than 10 Nephelometric Turbidity Units or NTUs). A groundwater sampling form
completed by H&H sampling personnel is provided in Appendix C.

Following well purging, a groundwater sample was collected for laboratory analyses. The
groundwater sample for VOC analysis was collected directly into laboratory supplied sample
containers using the “soda straw” method to minimize volatile loss through the peristaltic pump
head. The sample containers were labeled with the sample identification, date, and requested
analysis, and placed in an iced laboratory supplied cooler. The sample was delivered to Pace under
standard chain of custody protocols for analysis of VOCs by EPA Method 8260B, SVOCs by EPA
Method 8270D, and RCRA metals by EPA Method 6020B/7470A. For quality assurance/quality
control purposes, a trip blank sample was analyzed for VOCs by EPA Method 8260B.

Upon completion of soil and groundwater sampling activities, the soil borings and temporary
monitoring well boring were abandoned using hydrated bentonite. The ground surface was restored
at each boring location to approximately match pre-drilling conditions. Soil cuttings and well
development/purge water generated during Phase II ESA activities were spread on-Site, as obvious
evidence of significant impact (such as free product) was not observed.

4.2 Groundwater Analytical Results

Groundwater data were compared to the 2L Standards and the DEQ DWM Residential and Non-
Residential Groundwater Vapor Intrusion Groundwater Screening Levels (GWSLs) dated February
2018. A tabular summary of groundwater analytical results is presented in Table 3. The laboratory
analytical report and chain of custody record are provided in Appendix B.

Benzene (3.3 µg/l) and vinyl chloride (0.77 J µg/L) were detected in sample TMW-2 at
concentrations above the 2L Standards of 1.0 µg/L and 0.03 µg/L, respectively, but below the
Residential and Non-Residential GWSLs. Several other VOCs were detected in TMW-2 at
concentrations below the 2L Standards and below the Residential and Non-Residential GWSLs. No
VOCs were detected above the MDLs in the trip blank.

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No SVOCs were detected above the MDLs in sample TMW-2.

The metals arsenic (0.503 J µg/L), barium (238 µg/L), chromium (2.41 µg/L), and lead (0.254 J
µg/L) were detected in sample TMW-2 at concentrations below the respective 2L Standards of
10 µg/L, 700 µg/L, 10 µg/L, and 15 µg/L.

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5.0 Vapor Intrusion Assessment Activities
On February 13, 2019, H&H collected two exterior soil gas samples (SG-1 and SG-2) to evaluate
the potential for vapor intrusion into the Site building from potential groundwater impacts
associated with the upgradient former Worth Chemical facility. The temporary soil gas points were
installed between a former rail spur and the western exterior wall of the former Clorox facility, as
shown on Figure 2.

5.1 Exterior Soil Gas Sampling Methodology

Borings for exterior soil gas points SG-1 and SG-2 were advanced to depths of 6.5 and 7.5 ft bgs,
respectively, using a hand auger. The borings were terminated at depths interpreted to be within
one foot of the capillary fringe based on field observations. Continuous soil samples were
collected from each boring, logged for lithologic description, and screened for the presence of
staining, odors, and volatile organic vapors using a calibrated PID. Boring logs are provided in
Appendix A.

Each exterior soil gas point was constructed with a six-inch long stainless-steel screen point
installed at the base of the boring and fitted with ¼-inch diameter Teflon® tubing that extended to
the ground surface. Filter sand was then installed around the soil gas point from the base of the
boring to approximately six-inches above the top of the screen. The sampling points were
completed by placing hydrated bentonite from the top of the filter sand to approximately 0.5 ft bgs.

After installation, a leak check was conducted at each soil gas sample location by constructing a
shroud around the sampling point and flooding the shroud with helium gas. Helium concentrations
inside the shroud were measured using a helium gas detector. Using a peristaltic pump and three-
way valve, approximately three volumes of air within the Teflon tubing and soil gas point borehole
annular space were purged. Following purging, a sample was collected into a Tedlar bag from the
soil gas point and field screened using the helium gas detector to ensure that helium concentrations
in the soil gas point were less than 10% of the helium concentrations in the shroud. A soil gas
sampling QA/QC form that provides leak test results is included in Appendix D.

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Following a successful leak check, a laboratory-supplied 1-liter stainless steel Summa canister
connected to an in-line flow controller with a vacuum gauge was connected to the tubing at each
sampling point using a brass nut and ferrule assembly to form an air-tight seal. The flow regulator
was pre-set by the laboratory to regulate the vapor intake rate to approximately 100 milliliters per
minute. Once the sample train was assembled, the intake valve on the canister was fully opened to
begin collection of the soil gas sample. Vacuum in each of the canisters was measured using a
laboratory-supplied vacuum gauge prior to and after collection of the soil gas samples. These
measurements were recorded on the sample chain of custody. Per laboratory standard operating
procedures, a vacuum was maintained within the canisters at the conclusion of the sampling event.

After sample collection, the Summa canister’s valve was closed prior to the regulator being
disconnected from the canister. The Summa canisters were then placed in laboratory-supplied
shipping containers, properly labeled, and shipped under standard chain of custody protocols to
Con-Test Analytical Laboratory (Con-Test), a North Carolina certified laboratory, for analysis of
VOCs by EPA Method TO-15. Upon completion of sampling activities, each exterior soil gas
sampling point was abandoned, and the surface was repaired to approximately match pre-drilling
conditions.

5.2 Exterior Soil Gas Analytical Results

Soil gas analytical results were compared to the February 2018 DEQ DWM Residential and Non-
Residential Sub-Slab and Exterior Soil Gas Screening Levels (SGSLs). Results of soil gas analysis
are summarized in Table 4. The laboratory analytical report and chain of custody record are
provided in Appendix B.

Laboratory analytical results indicate the presence of several low concentrations of VOCs, including
chlorinated and petroleum-related compounds, in soil gas samples SG-1 and SG-2. The VOC
detections were generally higher in sample SG-1 compared to SG-2. None of the detected
compounds were reported at concentrations exceeding Residential or Non-Residential SGSLs.

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6.0 Conclusions and Recommendations
H&H has completed Phase II ESA activities at an industrial property located at 800 Gesco Street in
Charlotte, Mecklenburg County, North Carolina. The assessment activities were conducted in
general accordance with DEQ and EPA guidance and included soil, groundwater, and exterior
soil gas sampling to evaluate potential environmental risks that may affect Site redevelopment.
A summary of the assessment results is provided below.

Soil
H&H collected nine soil samples for laboratory analysis to evaluate the potential for soil impacts
at the Site. Samples were collected in areas of previously identified RECs and areas of potential
soil disturbance as part of Site redevelopment.

Laboratory analytical results do not indicate the presence of VOCs in soil samples at
concentrations above the DEQ PSRGs. PAHs were detected at concentrations exceeding
Protection of Groundwater, Residential, and/or Industrial/Commercial PSRGs in a shallow sample
(0-2 ft) collected in the former bleach mixing room. The PAH benzo(a)pyrene was also detected
above the Protection of Groundwater and Residential PSRG in one sample collected at 7-9 ft bgs
adjacent to former heating oil USTs/ASTs.

Arsenic was detected at concentrations above the Residential PSRG in the nine soil samples
collected for laboratory analysis and slightly above the Industrial/Commercial PSRG in one sample.
The detected concentrations of arsenic in the samples collected from the developed portion of the
Site are consistent with arsenic concentrations detected in the background samples. Further, the
detected concentrations are below the average published background concentration for North
Carolina soils. As such, the detected arsenic concentrations appear to be naturally occurring.

Hexavalent chromium was detected at estimated concentrations in samples SB-2 (0-2 ft), SB-3
(0-2 ft), SB-6 (0-2 ft), SB-9 (0-2 ft), and SB-11 (0-2 ft) above the Residential PSRG. The
detected concentrations of hexavalent chromium in the samples collected from the developed
portion of the Site are consistent with hexavalent chromium concentrations detected in

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background samples. As such, the hexavalent chromium concentrations are likely representative
of background conditions.

Groundwater
H&H installed and sampled one temporary groundwater monitoring well (TMW-2) located
downgradient of the Site building. Concentrations of benzene and vinyl chloride detected in
TMW-2 exceed the 2L Standards, but are below Residential and Non-Residential GWSLs. No
SVOCs were detected in sample TMW-2 above the MDLs, and no metals were detected in sample
TMW-2 at concentrations above the 2L Standards.

Exterior Soil Gas
H&H collected two soil gas samples (SG-1 and SG-2) near the western exterior wall of the former
Clorox facility. VOCs were detected in the exterior soil gas samples at concentrations below the
Residential and Non-Residential SGSLs.

Table 1
Summary of Soil Analytical Results
Former Clorox Facility
800 Gesco Street
Charlotte, North Carolina
H&H Job No. BCP-129
Sample ID SB-2 SB-3 SB-4 SB-5 SB-6 SB-9 SB-10 SB-11 SB-12Date2/7/2019 2/7/2019 2/8/2019 2/7/2019 2/7/2019 2/8/2019 2/8/2019 2/8/2019 2/8/2019
Area of Potential Concern
Former
Heating
Oil USTs/
ASTs
Downgradient of
Former Clorox
Facility/
Proposed
Landscaped Area
Proposed
Sub-Grade
Patio
Depth (ft bgs)0-2 0-2 7-9 0-2 0-2 0-2 0-2 0-2 0-2 Range Mean
VOCs (8260B)Acetone 0.0891 J 0.0175 J 0.0121 J 0.0380 J 0.0173 J 0.0588 J 0.0313 J 0.0406 J 0.167 12,000 140,000 25 ----
2-Butanone (MEK)0.0080 J <0.0035 <0.0027 <0.0028 <0.0028 <0.0031 0.0031 J <0.0029 0.0117 J 5,500 40,000 17 ----Chloroform <0.0016 <0.002 <0.0015 <0.0016 <0.0015 <0.0017 <0.0015 <0.0016 0.0023 J 0.34 1.5 0.39 ----
4-Methyl-2-pentanone (MIBK)<0.0037 <0.0045 <0.0034 <0.0036 <0.0036 <0.0039 <0.0034 <0.0037 0.0038 J 7,000 30,000 0.45 ----
Naphthalene <0.0012 <0.0015 <0.0011 <0.0012 <0.0012 <0.0013 <0.0011 <0.0012 0.0061 4.1 18 0.39 ----
Toluene 0.0019 J <0.0022 <0.0017 <0.0018 <0.0017 <0.0019 <0.0016 <0.0018 0.0029 J 990 9,700 8.3 ----m&p-Xylene 0.0056 J <0.0044 <0.0033 <0.0035 <0.0035 <0.0038 <0.0033 <0.0036 0.0037 J 240 1,020 19.6 ----
SVOCs (8270D)Acenaphthene <0.0778 0.699 <0.0977 <0.102 <0.469 <0.094 <0.0978 <0.0934 <0.0994 720 9,000 16 ----
Anthracene <0.0758 1.55 <0.0952 <0.0993 <0.457 <0.0915 <0.0952 <0.091 <0.0968 3,600 45,000 1,300 ----Benzo(a)anthracene <0.0625 9.45 0.127 J <0.0819 <0.376 <0.0755 <0.0785 <0.075 <0.0798 1.1 21 0.35 ----Benzo(a)pyrene <0.0645 6.81 0.144 J <0.0846 <0.389 <0.0779 <0.081 <0.0774 <0.0824 0.11 2.1 0.12 ----
Benzo(b)fluoranthene <0.0584 11.2 0.204 J <0.0765 <0.352 <0.0705 <0.0733 <0.0701 <0.0746 1.1 21 1.2 ----Benzo(g,h,i)perylene <0.086 5.08 <0.108 <0.113 <0.518 <0.104 <0.108 <0.103 <0.11 NS NS 15,600 ----Benzo(k)fluoranthene <0.0666 3.40 <0.0836 <0.0873 <0.401 <0.0804 <0.0836 <0.0799 <0.0851 11 210 12 ----
Chrysene 0.0468 J 8.32 0.135 J <0.0591 <0.272 <0.0544 <0.0566 <0.0541 <0.0576 110 2,100 36 ----Dibenz(a,h)anthracene <0.0717 1.3 <0.09 <0.094 <0.432 <0.0866 <0.0901 <0.086 <0.0916 0.11 2.1 0.38 ----Dibenzofuran <0.0553 0.280 J <0.0694 <0.0725 <0.333 <0.0668 <0.0695 <0.0664 <0.0707 15 210 10 ----
Fluoranthene 0.101 J 18.0 0.371 J <0.0644 <0.296 <0.0594 <0.0617 <0.059 <0.0628 480 6,000 670 ----Fluorene <0.0696 0.284 J <0.0874 <0.0913 <0.42 <0.0841 <0.0875 <0.0836 <0.0890 480 6,000 110 ----Indeno(1,2,3-cd)pyrene <0.0696 5.17 0.0919 J <0.0913 <0.42 <0.0841 <0.0875 <0.0836 <0.0890 1.1 21 3.9 ----
Naphthalene <0.083 0.0968 J <0.104 <0.109 <0.5 <0.1 <0.104 <0.0996 <0.106 4.1 18 0.39 ----
Phenanthrene 0.0635 J 8.97 0.165 J <0.0738 <0.339 <0.068 <0.0708 <0.0676 <0.0720 NS NS 134 ----Pyrene 0.0801 J 16.6 0.274 J <0.0752 <0.346 <0.0693 <0.072 <0.0688 <0.0733 360 4,500 440 ----
Metals (6020B/7471B/7199)Arsenic 2.64 2.76 2.33 2.75 3.07 1.92 1.42 2.10 2.28 0.68 3.0 5.8 1.0 - 18 4.8
Barium 56.5 75.3 86.0 58.7 87.9 86.4 105 127 118 3,100 47,000 580 50 - 1,000 356
Cadmium <0.0836 <0.0834 <0.0989 <0.107 <0.103 <0.101 <0.102 <0.0998 <0.103 14 200 3.0 1.0 - 10 (3)4.3 (3)
Chromium (total)77.1 91.4 38.3 37.5 46.5 77.3 51.7 56.0 169 NS NS NS 7.0 - 300 65
Hexavalent Chromium 0.726 J 0.686 J <0.315 <0.340 0.392 J 0.913 J <0.327 0.376 J <0.327 0.31 6.5 3.8 NS NS
Trivalent Chromium 76.4 90.7 38.0 37.2 46.1 76.4 51.4 55.6 169 23,000 350,000 360,000 NS NSLead22.6 22.9 10.1 10.6 32.9 10.0 6.95 10.7 12.8 400 800 250 ND - 50 16
Mercury 0.0929 0.0883 0.0528 0.290 0.0827 0.0616 0.0431 0.0495 <0.00359 2.3 9.7 1.0 0.03 - 0.52 0.12
Selenium 0.545 0.721 0.521 J 0.466 J 0.875 0.703 0.645 0.794 1.26 78 1,200 2.1 <0.1 - 0.8 0.42Silver<0.162 <0.162 <0.192 <0.207 <0.199 <0.195 <0.199 <0.193 <0.199 78 1,200 3.4 ND - 5.0 (3)NS
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (May 2019).
2) Range and mean values of background metals for North Carolina soils obtained from Elements in North American Soils by Dragun and Chekiri, 2005.
3) North Carolina background values were not specified; therefore, background values for the southeastern United States are shown.
With the exception of metals, only constituents detected in at least one sample are shown.
Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.
Bold indicates concentration exceeds DEQ IHSB Protection of Groundwater PSRG (and average published background concentrations for metals)
Underlined indicates concentration exceeds DEQ IHSB Residential PSRGs (and average published background concentrations for metals)
Gray shading indicates concentration exceeds DEQ IHSB Industrial/Commercial PSRGs (and average published background concentrations for metals)
Laboratory analytical methods are shown in parenthesesVOCs = volatile organic compounds; SVOCs = semi-volatile organic compoundsUST = underground storage tank; AST = aboveground storage tank; ft bgs = feet below ground surface; NS = not specified; -- = not applicable
J = estimated value between the laboratory method detection limit and the laboratory reporting limit
Industrial/
Commercial
PSRGs (1)
Former Bleach
Mixing Room
Undeveloped Parcels East of Gesco Street/
Proposed Parking Lot/Background
Published
Background
Metals
Concentrations for
North Carolina Soils
(2)
Protection of
Groundwater
PSRGs (1)
Residential
PSRGs (1)
S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-129 Gesco Street\Phase II ESA - Revised\Tables\Draft Data Tables
7/2/2019
Table 1
Hart & Hickman, PC
Table 2
Summary of Temporary Monitoring Well Construction and Water Level Data
Former Clorox Facility
800 Gesco Street
Charlotte, North Carolina
H&H Job No. BCP-129
Well Depth Depth to
Groundwater(ft bgs)(ft bgs)
TMW-2 2.0 18 8-18 11.38
Notes:
ft bgs = feet below ground surface
Depth to groundwater measurement collected on February 11, 2019.
Well ID
Screen Interval
(ft bgs)
Well Diameter
(inches)
S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-129 Gesco Street\Phase II ESA - Revised\Tables\Draft Data Tables
7/2/2019
Table 2
Hart & Hickman, PC
Table 3
Summary of Groundwater Analytical Results
Former Clorox Facility
800 Gesco Street
Charlotte, North Carolina
H&H Job No. BCP-129
Sample ID TMW-2
Date 2/12/2019
Location Description
Downgradient of Former
Clorox Facility/Plyler
Paper Stock
VOCs (8260B)Benzene 3.3 1 16 69
1,2-Dichlorobenzene 2.8 20 530 2,200
1,1-Dichloroethane 0.34 J 6 76 330cis-1,2-Dichloroethylene 8.6 70 NS NSDiisopropyl Ether (DIPE)2.2 70 1,400 5,900Vinyl Chloride 0.77 J 0.03 1.5 25Xylenes (Total)1.5 500 77 320
SVOCs (8270D)BDL ------
RCRA Metals (6020B, 7470A)
Arsenic 0.503 J 10 ----
Barium 238 700 ----
Cadmium <0.160 2 ----
Chromium 2.41 10 ----
Lead 0.254 J 15 ----
Mercury <0.0490 1 0.18 0.75
Selenium <0.380 20 ----Silver <0.310 20 ----
Notes:
3) NC DEQ DWM Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) (February 2018)With the exception of metals, only constituents detected in at least one sample are shown.Concentrations are reported in micrograms per liter (µg/L)
Compound concentrations are reported to the laboratory method detection limits
Bold indicates concentration exceeds DEQ 2L Standard
NA = not applicable; NS = not specified; -- = not applicable
J = estimated value between the laboratory method detection limit and the laboratory reporting limit
2) NC DEQ Division of Waste Management (DWM) Residential Vapor Intrusion Groundwater Screening Level (GWSLs)
(February 2018)
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds, RCRA = Resource Conservation and
Recovery Act; BDL = below method detection limits
Non-Residential
GWSLs(3)
NC 2L
Groundwater
Standards (1)
Residential
GWSLs(2)
1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L
Standards) (April 2013)
S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-129 Gesco Street\Phase II ESA - Revised\Tables\Draft Data Tables
7/2/2019
Table 3
Hart & Hickman, PC
Table 4
Summary of Exterior Soil Gas Analytical Results
Former Clorox Facility
800 Gesco Street
Charlotte, North Carolina
H&H Job No. BCP-129
Sample IDSample LocationScreen Depth (ft bgs)Sample DateAnalytical MethodAcetoneBenzene2-Butanone (MEK)Dichlorodifluoromethane (Freon 12)1,1-Dichloroethylenecis-1,2-DichloroethyleneEthanolEthyl AcetateEthylbenzene4-Ethyltoluene4-Methyl-2-pentanone (MIBK)TetrachloroethyleneTolueneTrichlorofluoromethane (Freon 11)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneVinyl Chloridem&p-Xyleneo-XyleneSG-1 6.5 2/13/2019 19 J <0.26 5.3 J 1.6 30 36 47 <0.54 2.4 5.5 12 71 6.0 2.0 J 6.7 3.5 1.4 12 3.2
SG-2 7.5 2/13/2019 12 J 0.79 2.7 J <0.43 <0.32 <0.32 27 3.8 <0.50 <0.60 <0.39 8.0 7.2 2.1 J <0.63 <0.62 <0.32 2.4 <0.54
220,000 120 35,000 700 1,400 NS NS 490 370 NS 21,000 280 35,000 NS 420 420 56 700 700
2,700,000 1,600 440,000 8,800 18,000 NS NS 6,100 4,900 NS 260,000 3,500 440,000 NS 5,300 5,300 2,800 8,800 8,800
Notes:
1) North Carolina Department of Environment Quality (DEQ) Division of Waste Management (DWM) Residential Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) (February 2018)2) DEQ DWM Non-Residential SGSLs (February 2018)
Only constituents detected in at least one sample are shown.Compound concentrations and SGSLs are reported in micrograms per cubic meter (µg/m3).
Compound concentrations are reported to the laboratory detection limits.Bold indicates concentration exceeds Residential SGSL
J = estimated value between the laboratory method detection limit and the laboratory reporting limit
ft bgs = feet below ground surface; NS = not specified
Non-Residential SGSL (2)
TO-15
Residential SGSL (1)
West/Upgradient of
Plyler Paper Stock
Warehouse
S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-129 Gesco Street\Phase II ESA - Revised\Tables\Draft Data Tables
7/2/2019
Table 4
Hart & Hickman, PC
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
SITE MAP: CHARLOTTE EAST, NC 1991
TITLE
PROJECT
SITE LOCATION MAP
FORMER CLOROX FACILITY
800 GESCO STREET
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
6-28-19 0
1BCP-129
SITE
SB-4
SB-9
SB-10
SB-11
SB-12
SG-1
SG-2
SB-6
SB-2
SB-3
POWERLINERIGHT-OF-WAY
HYDRAULICBALER
SORTING AREA
FORMER CLOROXMIXING ROOM
FORMER HEATINGOIL UST/AST
TRUCK & TRAILERPARKING
VACANT LAND(724 GESCO STREET)GESCO STREET
STATE STREET
VACANTLAND
SOUTHERN CONCRETE
MATERIALS(715 STATE STREET)
VACANT INDUSTRIALBUILDING(FORMER WORTH CHEMICAL)(818 TUCKASEEGEE ROAD)
TUCKASEEGEE ROAD
JAY STREETGELBACH DESIGNS INC.(808 TUCKASEEGEE ROAD)
ACTION GRAPHICS
(720 TUCKASEEGEE ROAD)
CUSTOM POLYMERS(700 TUCKASEEGEE ROAD)
PLYLER PAPER STOCK COMPANY(800 GESCO STREET)
SB-5/TMW-2
REVISION NO. 0
JOB NO. BCP-129
DATE: 2-21-19
FIGURE NO. 2
FORMER CLOROX FACILITY
800 GESCO STREETCHARLOTTE, NORTH CAROLINA
SITE AND SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
STEWART CREEK
FORMER RAIL SPURS
TEMPORARY MONITORING WELLAND SOIL BORING
SOIL BORING
SOIL GAS SAMPLE
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
CITY OF CHARLOTTE MAINTENANCE FACILITY
(701 TUCKASEEGEE ROAD)

Appendix A
Boring Logs
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/07/2019
02/07/2019
IET
Other
Hand Auger
Mark King
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Gravelly SILT (ML); some fine-coarse gravel, clay, dry, orange
(2') SILT (ML); clay, hard, dry, orange, some roots
(5') Boring terminated
4.6
4.5
4.1
4.7
4.3
SB-2(0-2)
0
5
10
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/07/2019
02/07/2019
IET
Other
Hand Auger
John Allen
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Poorly graded GRAVEL (GP); dry, gray
(0.25') Gravelly SILT (ML); clay, medium stiff, dry, light orange
(3') Fill: fine gravel-sized crushed concrete with some orange silty clay
(5') Boring terminated
3.7
4.8
5.8
6.3
6.2
SB-3(0-2)
0
5
10
NOTES: Hole precleared to 5.0' on 02/08/2019 by IET using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/08/2019
02/08/2019
IET
Direct Push
AMS PowerProbe 9500-VTR
Mark King
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
2.25
Direct Push, Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Poorly graded GRAVEL (GP); very dense, dark gray
(2') Silty SAND (SM); some medium-coarse grained sand, trace fine gravel, dense,
light brown with dark reddish brown and white mottling
(5.5') Lean CLAY with sand (CL); trace fine gravel, fine-medium sand, some
silt, medium plasticity, medium stiff, moist, dark reddish-brown
(11') Sandy SILT (ML); trace fine gravel, some medium-coarse sand, few
clay, stiff, moist, light reddish brown with tan sand grains
(15') Boring terminated
0.3
0.0
0.2
3.6
6.8
5.7
2.9
3.8
0.2
0.4
SB-4(7-9)
0
5
10
15
20
NOTES: Hole precleared to 5.0' on 02/07/2019 by IET using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
WELL LOG
Well No.
Page:
SB-5/TMW-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/07/2019
02/07/2019
IET
Direct Push
AMS PowerProbe 9500-VTR
Mark King
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
18.0
4.00
DP, GR
11.38
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
18.46
2.0
0.010
Sch 40 PVC
PVC Prepack
Bent. Chips
No. 2 Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Asphalt
(0.5') SILT (ML); some clay, stiff, dark red, slightly moist, some mica
(3.5') As Above: brownish red
(5') SILT (ML); trace clay, stiff, moist, light reddish brown with
yellowish brown mottling, some mica, organic matter
(7') As Above: dark red with light gray mottling, some roots
(9') As Above: some wood fragments
(10.5') Lean CLAY (CL); silt, medium plasticity, medium stiff, wet, grayish brown with
dark reddish-brown mottling
(11.5') Sandy SILT (ML); trace fine-coarse gravel, trace clay, soft, wet, light
reddish-gray
(15.5') As Above: dark gray
(17') Silty SAND (SM); medium dense, wet, light gray
(17.5') BEDROCK: light greenish gray, angular, coarse gravel-sized, partially
weathered rock
(18') Boring terminated
13.1
8.0
9.8
8.9
9.3
12.7
13.4
6.7
14.6
12.5
12.9
SB-5(0-2)
0
5
10
15
20
NOTES: Hole advanced to 5.0' on 2/7/19 by IET using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/7/19
2/7/19
IET
Other
Soil Auger
Mike Mark
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Lean CLAY (CL); trace fine-coarse gravel, some silt, medium plasticity,
medium stiff, moist, dark reddish-black
(1') As Above: some roots
(2') As Above: wet
(3') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, dark reddish-brown
(4') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, orange
(5') Boring terminated
14.6
16.7
13.6
14.2
5.5
SB-6(0-2)
0
5
10
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-9
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/08/2019
02/08/2019
IET
Other
Soil Auger
Mike Mark
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Well-graded GRAVEL (GW); dense, dark greenish-gray, slightly moist
(0.5') SILT (ML); some clay, stiff, reddish-brown, slightly moist, some mica
(1.5') As Above: with yellowish brown mottling
(4') As Above: dark red, moist
(5') Boring terminated
6.0
6.9
6.1
6.4
6.2
SB-9(0-2)
0
5
10
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-10
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/08/2019
02/08/2019
IET
Other
Hand Auger
Mike Mark
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') SILT (ML); trace fine gravel, fine-medium sand, trace clay, medium stiff,
dry, light yellowish-brown
(1') SILT (ML); few fine-medium sand, trace clay, medium stiff, light
reddish-brown, slightly moist, some roots
(2.5') As Above: some mica
(3.5') As Above: stiff
(5') Boring terminated
6.0
6.9
7.5
7.3
6.4
SB-10(0-2)
0
5
10
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-11
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/8/19
2/8/19
IET
Other
Hand Auger
Mike Mark
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') SILT (ML); some clay, stiff, dry, dark reddish-brown
(1') As Above: some roots, slightly moist
(2.5') SILT (ML); clay, stiff, moist, light orange
(4') As Above: moist, orange
(5') Boring terminated
4.5
5.3
5.3
5.7
6.0
SB-11(0-2)
0
5
10
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
BORING LOG
Boring No.
Page:
SB-12
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/8/2019
2/8/2019
IET
Other
Hand Auger
Mike Mark
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
2.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') SILT (ML); some clay, stiff, dark red, slightly moist
(2') SILT (ML); some clay, stiff, moist, light yellowish brown with dark red mottling
(3.5') As Above: dull orange
(5') Boring terminated
4.9
5.7
6.0
5.3
5.2
SB-12(0-2)
0
5
10
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
WELL LOG
Well No.
Page:
SG-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/13/2019
02/13/2019
H&H
Other
Hand Auger
DPG
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
6.5
3.25
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
6.5
0.5
Other
Other
Other
No. 2 Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') potential sand-sized ash
(1.25') SILT (ML); some clay, stiff, reddish-brown, slightly moist
(2') SILT (ML); very stiff, yellowish-brown, slightly moist
(3.5') As Above: hard, with trace gravel
(6') As Above: moist
(6.5') Boring terminated
2.3
4.1
3.1
4.6
5.1
5.9
6.7
0
5
10
Grab
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-129
800 Gesco Street, Charlotte, NC
WELL LOG
Well No.
Page:
SG-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/13/2019
02/13/2019
H&H
Other
Hand Auger
DPG
DPG
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
7.5
3.25
Grab
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
7.5
0.5
Other
Other
Other
No. 2 Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') potential sand-sized ash
(1') SILT (ML); some clay, medium stiff, moist, reddish brown with yellowish brown
mottling
(2.5') SILT (ML); some clay, medium stiff, reddish with yellowish brown mottling,
slightly moist
(5') SILT (ML); very stiff, reddish brown with white mottling, slightly mois
(7') As Above: moist
(7.5') Boring terminated
4.1
5.2
5.7
6.5
4.3
5.5
6.3
6.9
0
5
10

Appendix B Laboratory Analytical Reports
#=CL#
June 26, 2019
LIMS USE: FR - BO CAPPLEMAN
LIMS OBJECT ID: 92417206
92417206
Project:
Pace Project No.:
RE:
Bo Cappleman
Hart & Hickman
2923 South Tryon Street
Charlotte, NC 28203
BCP-129
Dear Bo Cappleman:
Enclosed are the analytical results for sample(s) received by the laboratory on February 11, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
Per client request, report revised 6/26/19 to relocate samples SB-1, SB-7, SB-8, and Soil Dup-1 to a
separate project.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 91
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92417206
BCP-129
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 91
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92417206
BCP-129
Lab ID Sample ID Matrix Date Collected Date Received
92417206002 SB-2 (0-2)Solid 02/07/19 17:00 02/11/19 09:10
92417206003 SB-3 (0-2)Solid 02/07/19 17:00 02/11/19 09:10
92417206004 SB-4 (7-9)Solid 02/08/19 13:00 02/11/19 09:10
92417206005 SB-5 (0-2)Solid 02/07/19 13:15 02/11/19 09:10
92417206006 SB-6 (0-2)Solid 02/07/19 15:00 02/11/19 09:10
92417206009 SB-9 (0-2)Solid 02/08/19 14:00 02/11/19 09:10
92417206010 SB-10 (0-2)Solid 02/08/19 14:30 02/11/19 09:10
92417206011 SB-11 (0-2)Solid 02/08/19 15:00 02/11/19 09:10
92417206012 SB-12 (0-2)Solid 02/08/19 15:30 02/11/19 09:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 91
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92417206
BCP-129
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92417206002 SB-2 (0-2)EPA 8270D 74 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92417206003 SB-3 (0-2)EPA 8270D 74 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92417206004 SB-4 (7-9)EPA 8270D 74 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92417206005 SB-5 (0-2)EPA 8270D 74 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92417206006 SB-6 (0-2)EPA 8270D 74 PASI-CBPJ
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92417206009 SB-9 (0-2)EPA 8270D 74 PASI-CBPJ
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92417206010 SB-10 (0-2)EPA 8270D 74 PASI-CBPJ
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92417206011 SB-11 (0-2)EPA 8270D 74 PASI-CBPJ
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92417206012 SB-12 (0-2)EPA 8270D 74 PASI-CBPJ
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-2 (0-2)Lab ID: 92417206002 Collected: 02/07/19 17:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 02/13/19 12:30 83-32-902/12/19 15:11338 77.8 1
Acenaphthylene ND ug/kg 02/13/19 12:30 208-96-802/12/19 15:11338 79.9 1
Aniline ND ug/kg 02/13/19 12:30 62-53-302/12/19 15:11338 91.2 1
Anthracene ND ug/kg 02/13/19 12:30 120-12-702/12/19 15:11338 75.8 1
Benzo(a)anthracene ND ug/kg 02/13/19 12:30 56-55-302/12/19 15:11338 62.5 1
Benzo(a)pyrene ND ug/kg 02/13/19 12:30 50-32-802/12/19 15:11338 64.5 1
Benzo(b)fluoranthene ND ug/kg 02/13/19 12:30 205-99-202/12/19 15:11338 58.4 1
Benzo(g,h,i)perylene ND ug/kg 02/13/19 12:30 191-24-202/12/19 15:11338 86.0 1
Benzo(k)fluoranthene ND ug/kg 02/13/19 12:30 207-08-902/12/19 15:11338 66.6 1
Benzoic Acid ND ug/kg 02/13/19 12:30 65-85-002/12/19 15:111690 61.5 1
Benzyl alcohol ND ug/kg 02/13/19 12:30 100-51-602/12/19 15:11676 67.6 1
4-Bromophenylphenyl ether ND ug/kg 02/13/19 12:30 101-55-302/12/19 15:11338 61.5 1
Butylbenzylphthalate ND ug/kg 02/13/19 12:30 85-68-702/12/19 15:11338 71.7 1
4-Chloro-3-methylphenol ND ug/kg 02/13/19 12:30 59-50-702/12/19 15:11676 69.6 1
4-Chloroaniline ND ug/kg 02/13/19 12:30 106-47-802/12/19 15:111690 94.2 1
bis(2-Chloroethoxy)methane ND ug/kg 02/13/19 12:30 111-91-102/12/19 15:11338 78.9 1
bis(2-Chloroethyl) ether ND ug/kg 02/13/19 12:30 111-44-402/12/19 15:11338 86.0 1
2-Chloronaphthalene ND ug/kg 02/13/19 12:30 91-58-702/12/19 15:11338 66.6 1
2-Chlorophenol ND ug/kg 02/13/19 12:30 95-57-802/12/19 15:11338 92.2 1
4-Chlorophenylphenyl ether ND ug/kg 02/13/19 12:30 7005-72-302/12/19 15:11338 69.6 1
Chrysene 46.8J ug/kg 02/13/19 12:30 218-01-902/12/19 15:11338 45.1 1
Dibenz(a,h)anthracene ND ug/kg 02/13/19 12:30 53-70-302/12/19 15:11338 71.7 1
Dibenzofuran ND ug/kg 02/13/19 12:30 132-64-902/12/19 15:11338 55.3 1
1,2-Dichlorobenzene ND ug/kg 02/13/19 12:30 95-50-102/12/19 15:11338 90.1 1
1,3-Dichlorobenzene ND ug/kg 02/13/19 12:30 541-73-102/12/19 15:11338 76.8 1
1,4-Dichlorobenzene ND ug/kg 02/13/19 12:30 106-46-702/12/19 15:11338 95.3 1
3,3'-Dichlorobenzidine ND ug/kg 02/13/19 12:30 91-94-102/12/19 15:111690 73.7 1
2,4-Dichlorophenol ND ug/kg 02/13/19 12:30 120-83-202/12/19 15:11338 73.7 1
Diethylphthalate ND ug/kg 02/13/19 12:30 84-66-202/12/19 15:11338 52.2 1
2,4-Dimethylphenol ND ug/kg 02/13/19 12:30 105-67-902/12/19 15:11338 133 1
Dimethylphthalate ND ug/kg 02/13/19 12:30 131-11-302/12/19 15:11338 68.6 1
Di-n-butylphthalate ND ug/kg 02/13/19 12:30 84-74-202/12/19 15:11338 55.3 1
4,6-Dinitro-2-methylphenol ND ug/kg 02/13/19 12:30 534-52-102/12/19 15:11676 67.6 1
2,4-Dinitrophenol ND ug/kg 02/13/19 12:30 51-28-502/12/19 15:111690 55.3 1
2,4-Dinitrotoluene ND ug/kg 02/13/19 12:30 121-14-202/12/19 15:11338 63.5 1
2,6-Dinitrotoluene ND ug/kg 02/13/19 12:30 606-20-202/12/19 15:11338 70.7 1
Di-n-octylphthalate ND ug/kg 02/13/19 12:30 117-84-002/12/19 15:11338 70.7 1
bis(2-Ethylhexyl)phthalate ND ug/kg 02/13/19 12:30 117-81-702/12/19 15:11338 92.2 1
Fluoranthene 101J ug/kg 02/13/19 12:30 206-44-002/12/19 15:11338 49.2 1
Fluorene ND ug/kg 02/13/19 12:30 86-73-702/12/19 15:11338 69.6 1
Hexachloro-1,3-butadiene ND ug/kg 02/13/19 12:30 87-68-302/12/19 15:11338 58.4 1
Hexachlorobenzene ND ug/kg 02/13/19 12:30 118-74-102/12/19 15:11338 43.0 1
Hexachlorocyclopentadiene ND ug/kg 02/13/19 12:30 77-47-402/12/19 15:11338 62.5 1
Hexachloroethane ND ug/kg 02/13/19 12:30 67-72-102/12/19 15:11338 89.1 1
Indeno(1,2,3-cd)pyrene ND ug/kg 02/13/19 12:30 193-39-502/12/19 15:11338 69.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-2 (0-2)Lab ID: 92417206002 Collected: 02/07/19 17:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 02/13/19 12:30 78-59-102/12/19 15:11338 75.8 1
1-Methylnaphthalene ND ug/kg 02/13/19 12:30 90-12-002/12/19 15:11338 88.1 1
2-Methylnaphthalene ND ug/kg 02/13/19 12:30 91-57-602/12/19 15:11338 72.7 1
2-Methylphenol(o-Cresol)ND ug/kg 02/13/19 12:30 95-48-702/12/19 15:11338 102 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/13/19 12:30 15831-10-402/12/19 15:11338 133 1
Naphthalene ND ug/kg 02/13/19 12:30 91-20-302/12/19 15:11338 83.0 1
2-Nitroaniline ND ug/kg 02/13/19 12:30 88-74-402/12/19 15:111690 104 1
3-Nitroaniline ND ug/kg 02/13/19 12:30 99-09-202/12/19 15:111690 92.2 1
4-Nitroaniline ND ug/kg 02/13/19 12:30 100-01-602/12/19 15:11676 95.3 1
Nitrobenzene ND ug/kg 02/13/19 12:30 98-95-302/12/19 15:11338 92.2 1
2-Nitrophenol ND ug/kg 02/13/19 12:30 88-75-502/12/19 15:11338 81.9 1
4-Nitrophenol ND ug/kg 02/13/19 12:30 100-02-702/12/19 15:111690 60.4 1
N-Nitrosodimethylamine ND ug/kg 02/13/19 12:30 62-75-902/12/19 15:11338 110 1
N-Nitroso-di-n-propylamine ND ug/kg 02/13/19 12:30 621-64-702/12/19 15:11338 64.5 1
N-Nitrosodiphenylamine ND ug/kg 02/13/19 12:30 86-30-602/12/19 15:11338 100 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/13/19 12:30 108-60-102/12/19 15:11338 90.1 1
Pentachlorophenol ND ug/kg 02/13/19 12:30 87-86-502/12/19 15:111690 61.5 1
Phenanthrene 63.5J ug/kg 02/13/19 12:30 85-01-802/12/19 15:11338 56.3 1
Phenol ND ug/kg 02/13/19 12:30 108-95-202/12/19 15:11338 101 1
Pyrene 80.1J ug/kg 02/13/19 12:30 129-00-002/12/19 15:11338 57.4 1
1,2,4-Trichlorobenzene ND ug/kg 02/13/19 12:30 120-82-102/12/19 15:11338 65.6 1
2,4,5-Trichlorophenol ND ug/kg 02/13/19 12:30 95-95-402/12/19 15:11338 104 1
2,4,6-Trichlorophenol ND ug/kg 02/13/19 12:30 88-06-202/12/19 15:11338 74.8 1
Surrogates
Nitrobenzene-d5 (S)54 %02/13/19 12:30 4165-60-002/12/19 15:1123-110 1
2-Fluorobiphenyl (S)55 %02/13/19 12:30 321-60-802/12/19 15:1130-110 1
Terphenyl-d14 (S)62 %02/13/19 12:30 1718-51-002/12/19 15:1128-110 1
Phenol-d6 (S)56 %02/13/19 12:30 13127-88-302/12/19 15:1122-110 1
2-Fluorophenol (S)49 %02/13/19 12:30 367-12-402/12/19 15:1113-110 1
2,4,6-Tribromophenol (S)58 %02/13/19 12:30 118-79-602/12/19 15:1127-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 89.1J ug/kg 02/11/19 16:58 67-64-102/11/19 13:3799.3 9.9 1
Benzene ND ug/kg 02/11/19 16:58 71-43-202/11/19 13:375.0 1.6 1
Bromobenzene ND ug/kg 02/11/19 16:58 108-86-102/11/19 13:375.0 2.0 1
Bromochloromethane ND ug/kg 02/11/19 16:58 74-97-502/11/19 13:375.0 1.7 1
Bromodichloromethane ND ug/kg 02/11/19 16:58 75-27-402/11/19 13:375.0 1.9 1
Bromoform ND ug/kg 02/11/19 16:58 75-25-202/11/19 13:375.0 2.3 1
Bromomethane ND ug/kg 02/11/19 16:58 74-83-902/11/19 13:379.9 2.5 1
2-Butanone (MEK)8.0J ug/kg 02/11/19 16:58 78-93-302/11/19 13:3799.3 2.9 1
n-Butylbenzene ND ug/kg 02/11/19 16:58 104-51-802/11/19 13:375.0 1.8 1
sec-Butylbenzene ND ug/kg 02/11/19 16:58 135-98-802/11/19 13:375.0 1.6 1
tert-Butylbenzene ND ug/kg 02/11/19 16:58 98-06-602/11/19 13:375.0 2.0 1
Carbon tetrachloride ND ug/kg 02/11/19 16:58 56-23-502/11/19 13:375.0 2.6 1
Chlorobenzene ND ug/kg 02/11/19 16:58 108-90-702/11/19 13:375.0 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-2 (0-2)Lab ID: 92417206002 Collected: 02/07/19 17:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 02/11/19 16:58 75-00-302/11/19 13:379.9 2.4 1
Chloroform ND ug/kg 02/11/19 16:58 67-66-302/11/19 13:375.0 1.6 1
Chloromethane ND ug/kg 02/11/19 16:58 74-87-302/11/19 13:379.9 2.4 1
2-Chlorotoluene ND ug/kg 02/11/19 16:58 95-49-802/11/19 13:375.0 1.7 1
4-Chlorotoluene ND ug/kg 02/11/19 16:58 106-43-402/11/19 13:375.0 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/11/19 16:58 96-12-802/11/19 13:375.0 3.6 1
Dibromochloromethane ND ug/kg 02/11/19 16:58 124-48-102/11/19 13:375.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 02/11/19 16:58 106-93-402/11/19 13:375.0 1.8 1
Dibromomethane ND ug/kg 02/11/19 16:58 74-95-302/11/19 13:375.0 2.5 1
1,2-Dichlorobenzene ND ug/kg 02/11/19 16:58 95-50-102/11/19 13:375.0 1.9 1
1,3-Dichlorobenzene ND ug/kg 02/11/19 16:58 541-73-102/11/19 13:375.0 2.0 1
1,4-Dichlorobenzene ND ug/kg 02/11/19 16:58 106-46-702/11/19 13:375.0 1.7 1
Dichlorodifluoromethane ND ug/kg 02/11/19 16:58 75-71-802/11/19 13:379.9 3.6 1
1,1-Dichloroethane ND ug/kg 02/11/19 16:58 75-34-302/11/19 13:375.0 1.5 1
1,2-Dichloroethane ND ug/kg 02/11/19 16:58 107-06-202/11/19 13:375.0 2.2 1
1,1-Dichloroethene ND ug/kg 02/11/19 16:58 75-35-402/11/19 13:375.0 1.8 1
cis-1,2-Dichloroethene ND ug/kg 02/11/19 16:58 156-59-202/11/19 13:375.0 1.4 1
trans-1,2-Dichloroethene ND ug/kg 02/11/19 16:58 156-60-502/11/19 13:375.0 1.9 1
1,2-Dichloropropane ND ug/kg 02/11/19 16:58 78-87-502/11/19 13:375.0 1.7 1
1,3-Dichloropropane ND ug/kg 02/11/19 16:58 142-28-902/11/19 13:375.0 1.9 1
2,2-Dichloropropane ND ug/kg 02/11/19 16:58 594-20-702/11/19 13:375.0 1.7 1
1,1-Dichloropropene ND ug/kg 02/11/19 16:58 563-58-602/11/19 13:375.0 1.5 1
cis-1,3-Dichloropropene ND ug/kg 02/11/19 16:58 10061-01-502/11/19 13:375.0 1.8 1
trans-1,3-Dichloropropene ND ug/kg 02/11/19 16:58 10061-02-602/11/19 13:375.0 1.5 1
Diisopropyl ether ND ug/kg 02/11/19 16:58 108-20-302/11/19 13:375.0 1.7 1
Ethylbenzene ND ug/kg 02/11/19 16:58 100-41-402/11/19 13:375.0 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 02/11/19 16:58 87-68-302/11/19 13:375.0 2.0 1
2-Hexanone ND ug/kg 02/11/19 16:58 591-78-602/11/19 13:3749.7 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 02/11/19 16:58 98-82-802/11/19 13:375.0 1.9 1
p-Isopropyltoluene ND ug/kg 02/11/19 16:58 99-87-602/11/19 13:375.0 1.7 1
Methylene Chloride ND ug/kg 02/11/19 16:58 75-09-202/11/19 13:3719.9 3.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/11/19 16:58 108-10-102/11/19 13:3749.7 3.7 1
Methyl-tert-butyl ether ND ug/kg 02/11/19 16:58 1634-04-402/11/19 13:375.0 1.5 1
Naphthalene ND ug/kg 02/11/19 16:58 91-20-302/11/19 13:375.0 1.2 1
n-Propylbenzene ND ug/kg 02/11/19 16:58 103-65-102/11/19 13:375.0 1.7 1
Styrene ND ug/kg 02/11/19 16:58 100-42-502/11/19 13:375.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/11/19 16:58 630-20-602/11/19 13:375.0 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/11/19 16:58 79-34-502/11/19 13:375.0 1.9 1
Tetrachloroethene ND ug/kg 02/11/19 16:58 127-18-402/11/19 13:375.0 1.7 1
Toluene 1.9J ug/kg 02/11/19 16:58 108-88-302/11/19 13:375.0 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 02/11/19 16:58 87-61-602/11/19 13:375.0 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 02/11/19 16:58 120-82-102/11/19 13:375.0 1.6 1
1,1,1-Trichloroethane ND ug/kg 02/11/19 16:58 71-55-602/11/19 13:375.0 1.8 1
1,1,2-Trichloroethane ND ug/kg 02/11/19 16:58 79-00-502/11/19 13:375.0 2.1 1
Trichloroethene ND ug/kg 02/11/19 16:58 79-01-602/11/19 13:375.0 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-2 (0-2)Lab ID: 92417206002 Collected: 02/07/19 17:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 02/11/19 16:58 75-69-402/11/19 13:375.0 2.2 1
1,2,3-Trichloropropane ND ug/kg 02/11/19 16:58 96-18-402/11/19 13:375.0 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 02/11/19 16:58 95-63-602/11/19 13:375.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/11/19 16:58 108-67-802/11/19 13:375.0 1.8 1
Vinyl acetate ND ug/kg 02/11/19 16:58 108-05-402/11/19 13:3749.7 8.7 1
Vinyl chloride ND ug/kg 02/11/19 16:58 75-01-402/11/19 13:379.9 1.8 1
Xylene (Total)ND ug/kg 02/11/19 16:58 1330-20-702/11/19 13:379.9 3.6 1
m&p-Xylene 5.6J ug/kg 02/11/19 16:58 179601-23-102/11/19 13:379.9 3.6 1
o-Xylene ND ug/kg 02/11/19 16:58 95-47-602/11/19 13:375.0 1.9 1
Surrogates
Toluene-d8 (S)100 %02/11/19 16:58 2037-26-502/11/19 13:3770-130 1
4-Bromofluorobenzene (S)99 %02/11/19 16:58 460-00-402/11/19 13:3770-130 1
1,2-Dichloroethane-d4 (S)104 %02/11/19 16:58 17060-07-002/11/19 13:3770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 3.0 %02/11/19 14:130.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-3 (0-2)Lab ID: 92417206003 Collected: 02/07/19 17:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene 699 ug/kg 02/13/19 13:31 83-32-902/12/19 15:11343 79.0 1
Acenaphthylene ND ug/kg 02/13/19 13:31 208-96-802/12/19 15:11343 81.1 1
Aniline ND ug/kg 02/13/19 13:31 62-53-302/12/19 15:11343 92.6 1
Anthracene 1550 ug/kg 02/13/19 13:31 120-12-702/12/19 15:11343 77.0 1
Benzo(a)anthracene 9450 ug/kg 02/13/19 19:07 56-55-302/12/19 15:113430 634 10
Benzo(a)pyrene 6810 ug/kg 02/13/19 19:07 50-32-802/12/19 15:113430 655 10
Benzo(b)fluoranthene 11200 ug/kg 02/13/19 19:07 205-99-202/12/19 15:113430 593 10
Benzo(g,h,i)perylene 5080 ug/kg 02/13/19 19:07 191-24-202/12/19 15:113430 874 10
Benzo(k)fluoranthene 3400 ug/kg 02/13/19 13:31 207-08-902/12/19 15:11343 67.6 1
Benzoic Acid ND ug/kg 02/13/19 13:31 65-85-002/12/19 15:111720 62.4 1
Benzyl alcohol ND ug/kg 02/13/19 13:31 100-51-602/12/19 15:11686 68.6 1
4-Bromophenylphenyl ether ND ug/kg 02/13/19 13:31 101-55-302/12/19 15:11343 62.4 1
Butylbenzylphthalate ND ug/kg 02/13/19 13:31 85-68-702/12/19 15:11343 72.8 1
4-Chloro-3-methylphenol ND ug/kg 02/13/19 13:31 59-50-702/12/19 15:11686 70.7 1
4-Chloroaniline ND ug/kg 02/13/19 13:31 106-47-802/12/19 15:111720 95.7 1
bis(2-Chloroethoxy)methane ND ug/kg 02/13/19 13:31 111-91-102/12/19 15:11343 80.1 1
bis(2-Chloroethyl) ether ND ug/kg 02/13/19 13:31 111-44-402/12/19 15:11343 87.4 1
2-Chloronaphthalene ND ug/kg 02/13/19 13:31 91-58-702/12/19 15:11343 67.6 1
2-Chlorophenol ND ug/kg 02/13/19 13:31 95-57-802/12/19 15:11343 93.6 1
4-Chlorophenylphenyl ether ND ug/kg 02/13/19 13:31 7005-72-302/12/19 15:11343 70.7 1
Chrysene 8320 ug/kg 02/13/19 19:07 218-01-902/12/19 15:113430 458 10
Dibenz(a,h)anthracene 1300 ug/kg 02/13/19 13:31 53-70-302/12/19 15:11343 72.8 1
Dibenzofuran 280J ug/kg 02/13/19 13:31 132-64-902/12/19 15:11343 56.2 1
1,2-Dichlorobenzene ND ug/kg 02/13/19 13:31 95-50-102/12/19 15:11343 91.5 1
1,3-Dichlorobenzene ND ug/kg 02/13/19 13:31 541-73-102/12/19 15:11343 78.0 1
1,4-Dichlorobenzene ND ug/kg 02/13/19 13:31 106-46-702/12/19 15:11343 96.7 1
3,3'-Dichlorobenzidine ND ug/kg 02/13/19 13:31 91-94-102/12/19 15:111720 74.9 1
2,4-Dichlorophenol ND ug/kg 02/13/19 13:31 120-83-202/12/19 15:11343 74.9 1
Diethylphthalate ND ug/kg 02/13/19 13:31 84-66-202/12/19 15:11343 53.0 1
2,4-Dimethylphenol ND ug/kg 02/13/19 13:31 105-67-902/12/19 15:11343 135 1
Dimethylphthalate ND ug/kg 02/13/19 13:31 131-11-302/12/19 15:11343 69.7 1
Di-n-butylphthalate ND ug/kg 02/13/19 13:31 84-74-202/12/19 15:11343 56.2 1
4,6-Dinitro-2-methylphenol ND ug/kg 02/13/19 13:31 534-52-102/12/19 15:11686 68.6 1
2,4-Dinitrophenol ND ug/kg 02/13/19 13:31 51-28-502/12/19 15:111720 56.2 1
2,4-Dinitrotoluene ND ug/kg 02/13/19 13:31 121-14-202/12/19 15:11343 64.5 1
2,6-Dinitrotoluene ND ug/kg 02/13/19 13:31 606-20-202/12/19 15:11343 71.8 1
Di-n-octylphthalate ND ug/kg 02/13/19 13:31 117-84-002/12/19 15:11343 71.8 1
bis(2-Ethylhexyl)phthalate ND ug/kg 02/13/19 13:31 117-81-702/12/19 15:11343 93.6 1
Fluoranthene 18000 ug/kg 02/13/19 19:07 206-44-002/12/19 15:113430 499 10
Fluorene 284J ug/kg 02/13/19 13:31 86-73-702/12/19 15:11343 70.7 1
Hexachloro-1,3-butadiene ND ug/kg 02/13/19 13:31 87-68-302/12/19 15:11343 59.3 1
Hexachlorobenzene ND ug/kg 02/13/19 13:31 118-74-102/12/19 15:11343 43.7 1
Hexachlorocyclopentadiene ND ug/kg 02/13/19 13:31 77-47-402/12/19 15:11343 63.4 1
Hexachloroethane ND ug/kg 02/13/19 13:31 67-72-102/12/19 15:11343 90.5 1
Indeno(1,2,3-cd)pyrene 5170 ug/kg 02/13/19 19:07 193-39-502/12/19 15:113430 707 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-3 (0-2)Lab ID: 92417206003 Collected: 02/07/19 17:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 02/13/19 13:31 78-59-102/12/19 15:11343 77.0 1
1-Methylnaphthalene ND ug/kg 02/13/19 13:31 90-12-002/12/19 15:11343 89.4 1
2-Methylnaphthalene ND ug/kg 02/13/19 13:31 91-57-602/12/19 15:11343 73.8 1
2-Methylphenol(o-Cresol)ND ug/kg 02/13/19 13:31 95-48-702/12/19 15:11343 104 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/13/19 13:31 15831-10-402/12/19 15:11343 135 1
Naphthalene 96.8J ug/kg 02/13/19 13:31 91-20-302/12/19 15:11343 84.2 1
2-Nitroaniline ND ug/kg 02/13/19 13:31 88-74-402/12/19 15:111720 106 1
3-Nitroaniline ND ug/kg 02/13/19 13:31 99-09-202/12/19 15:111720 93.6 1
4-Nitroaniline ND ug/kg 02/13/19 13:31 100-01-602/12/19 15:11686 96.7 1
Nitrobenzene ND ug/kg 02/13/19 13:31 98-95-302/12/19 15:11343 93.6 1
2-Nitrophenol ND ug/kg 02/13/19 13:31 88-75-502/12/19 15:11343 83.2 1
4-Nitrophenol ND ug/kg 02/13/19 13:31 100-02-702/12/19 15:111720 61.4 1
N-Nitrosodimethylamine ND ug/kg 02/13/19 13:31 62-75-902/12/19 15:11343 111 1
N-Nitroso-di-n-propylamine ND ug/kg 02/13/19 13:31 621-64-702/12/19 15:11343 65.5 1
N-Nitrosodiphenylamine ND ug/kg 02/13/19 13:31 86-30-602/12/19 15:11343 102 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/13/19 13:31 108-60-102/12/19 15:11343 91.5 1
Pentachlorophenol ND ug/kg 02/13/19 13:31 87-86-502/12/19 15:111720 62.4 1
Phenanthrene 8970 ug/kg 02/13/19 19:07 85-01-802/12/19 15:113430 572 10
Phenol ND ug/kg 02/13/19 13:31 108-95-202/12/19 15:11343 103 1
Pyrene 16600 ug/kg 02/13/19 19:07 129-00-002/12/19 15:113430 582 10
1,2,4-Trichlorobenzene ND ug/kg 02/13/19 13:31 120-82-102/12/19 15:11343 66.6 1
2,4,5-Trichlorophenol ND ug/kg 02/13/19 13:31 95-95-402/12/19 15:11343 106 1
2,4,6-Trichlorophenol ND ug/kg 02/13/19 13:31 88-06-202/12/19 15:11343 75.9 1
Surrogates
Nitrobenzene-d5 (S)48 %02/13/19 13:31 4165-60-002/12/19 15:1123-110 1
2-Fluorobiphenyl (S)57 %02/13/19 13:31 321-60-802/12/19 15:1130-110 1
Terphenyl-d14 (S)64 %02/13/19 13:31 1718-51-002/12/19 15:1128-110 1
Phenol-d6 (S)56 %02/13/19 13:31 13127-88-302/12/19 15:1122-110 1
2-Fluorophenol (S)44 %02/13/19 13:31 367-12-402/12/19 15:1113-110 1
2,4,6-Tribromophenol (S)73 %02/13/19 13:31 118-79-602/12/19 15:1127-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 17.5J ug/kg 02/11/19 17:17 67-64-102/11/19 13:37122 12.2 1
Benzene ND ug/kg 02/11/19 17:17 71-43-202/11/19 13:376.1 2.0 1
Bromobenzene ND ug/kg 02/11/19 17:17 108-86-102/11/19 13:376.1 2.4 1
Bromochloromethane ND ug/kg 02/11/19 17:17 74-97-502/11/19 13:376.1 2.1 1
Bromodichloromethane ND ug/kg 02/11/19 17:17 75-27-402/11/19 13:376.1 2.3 1
Bromoform ND ug/kg 02/11/19 17:17 75-25-202/11/19 13:376.1 2.8 1
Bromomethane ND ug/kg 02/11/19 17:17 74-83-902/11/19 13:3712.2 3.1 1
2-Butanone (MEK)ND ug/kg 02/11/19 17:17 78-93-302/11/19 13:37122 3.5 1
n-Butylbenzene ND ug/kg 02/11/19 17:17 104-51-802/11/19 13:376.1 2.2 1
sec-Butylbenzene ND ug/kg 02/11/19 17:17 135-98-802/11/19 13:376.1 2.0 1
tert-Butylbenzene ND ug/kg 02/11/19 17:17 98-06-602/11/19 13:376.1 2.4 1
Carbon tetrachloride ND ug/kg 02/11/19 17:17 56-23-502/11/19 13:376.1 3.2 1
Chlorobenzene ND ug/kg 02/11/19 17:17 108-90-702/11/19 13:376.1 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-3 (0-2)Lab ID: 92417206003 Collected: 02/07/19 17:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 02/11/19 17:17 75-00-302/11/19 13:3712.2 2.9 1
Chloroform ND ug/kg 02/11/19 17:17 67-66-302/11/19 13:376.1 2.0 1
Chloromethane ND ug/kg 02/11/19 17:17 74-87-302/11/19 13:3712.2 2.9 1
2-Chlorotoluene ND ug/kg 02/11/19 17:17 95-49-802/11/19 13:376.1 2.1 1
4-Chlorotoluene ND ug/kg 02/11/19 17:17 106-43-402/11/19 13:376.1 2.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/11/19 17:17 96-12-802/11/19 13:376.1 4.4 1
Dibromochloromethane ND ug/kg 02/11/19 17:17 124-48-102/11/19 13:376.1 2.2 1
1,2-Dibromoethane (EDB)ND ug/kg 02/11/19 17:17 106-93-402/11/19 13:376.1 2.2 1
Dibromomethane ND ug/kg 02/11/19 17:17 74-95-302/11/19 13:376.1 3.1 1
1,2-Dichlorobenzene ND ug/kg 02/11/19 17:17 95-50-102/11/19 13:376.1 2.3 1
1,3-Dichlorobenzene ND ug/kg 02/11/19 17:17 541-73-102/11/19 13:376.1 2.4 1
1,4-Dichlorobenzene ND ug/kg 02/11/19 17:17 106-46-702/11/19 13:376.1 2.1 1
Dichlorodifluoromethane ND ug/kg 02/11/19 17:17 75-71-802/11/19 13:3712.2 4.4 1
1,1-Dichloroethane ND ug/kg 02/11/19 17:17 75-34-302/11/19 13:376.1 1.8 1
1,2-Dichloroethane ND ug/kg 02/11/19 17:17 107-06-202/11/19 13:376.1 2.7 1
1,1-Dichloroethene ND ug/kg 02/11/19 17:17 75-35-402/11/19 13:376.1 2.2 1
cis-1,2-Dichloroethene ND ug/kg 02/11/19 17:17 156-59-202/11/19 13:376.1 1.7 1
trans-1,2-Dichloroethene ND ug/kg 02/11/19 17:17 156-60-502/11/19 13:376.1 2.3 1
1,2-Dichloropropane ND ug/kg 02/11/19 17:17 78-87-502/11/19 13:376.1 2.1 1
1,3-Dichloropropane ND ug/kg 02/11/19 17:17 142-28-902/11/19 13:376.1 2.3 1
2,2-Dichloropropane ND ug/kg 02/11/19 17:17 594-20-702/11/19 13:376.1 2.1 1
1,1-Dichloropropene ND ug/kg 02/11/19 17:17 563-58-602/11/19 13:376.1 1.8 1
cis-1,3-Dichloropropene ND ug/kg 02/11/19 17:17 10061-01-502/11/19 13:376.1 2.2 1
trans-1,3-Dichloropropene ND ug/kg 02/11/19 17:17 10061-02-602/11/19 13:376.1 1.8 1
Diisopropyl ether ND ug/kg 02/11/19 17:17 108-20-302/11/19 13:376.1 2.1 1
Ethylbenzene ND ug/kg 02/11/19 17:17 100-41-402/11/19 13:376.1 2.2 1
Hexachloro-1,3-butadiene ND ug/kg 02/11/19 17:17 87-68-302/11/19 13:376.1 2.4 1
2-Hexanone ND ug/kg 02/11/19 17:17 591-78-602/11/19 13:3761.1 4.8 1
Isopropylbenzene (Cumene)ND ug/kg 02/11/19 17:17 98-82-802/11/19 13:376.1 2.3 1
p-Isopropyltoluene ND ug/kg 02/11/19 17:17 99-87-602/11/19 13:376.1 2.1 1
Methylene Chloride ND ug/kg 02/11/19 17:17 75-09-202/11/19 13:3724.4 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/11/19 17:17 108-10-102/11/19 13:3761.1 4.5 1
Methyl-tert-butyl ether ND ug/kg 02/11/19 17:17 1634-04-402/11/19 13:376.1 1.8 1
Naphthalene ND ug/kg 02/11/19 17:17 91-20-302/11/19 13:376.1 1.5 1
n-Propylbenzene ND ug/kg 02/11/19 17:17 103-65-102/11/19 13:376.1 2.1 1
Styrene ND ug/kg 02/11/19 17:17 100-42-502/11/19 13:376.1 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/11/19 17:17 630-20-602/11/19 13:376.1 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/11/19 17:17 79-34-502/11/19 13:376.1 2.3 1
Tetrachloroethene ND ug/kg 02/11/19 17:17 127-18-402/11/19 13:376.1 2.1 1
Toluene ND ug/kg 02/11/19 17:17 108-88-302/11/19 13:376.1 2.2 1
1,2,3-Trichlorobenzene ND ug/kg 02/11/19 17:17 87-61-602/11/19 13:376.1 2.7 1
1,2,4-Trichlorobenzene ND ug/kg 02/11/19 17:17 120-82-102/11/19 13:376.1 2.0 1
1,1,1-Trichloroethane ND ug/kg 02/11/19 17:17 71-55-602/11/19 13:376.1 2.2 1
1,1,2-Trichloroethane ND ug/kg 02/11/19 17:17 79-00-502/11/19 13:376.1 2.6 1
Trichloroethene ND ug/kg 02/11/19 17:17 79-01-602/11/19 13:376.1 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-3 (0-2)Lab ID: 92417206003 Collected: 02/07/19 17:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 02/11/19 17:17 75-69-402/11/19 13:376.1 2.7 1
1,2,3-Trichloropropane ND ug/kg 02/11/19 17:17 96-18-402/11/19 13:376.1 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 02/11/19 17:17 95-63-602/11/19 13:376.1 2.4 1
1,3,5-Trimethylbenzene ND ug/kg 02/11/19 17:17 108-67-802/11/19 13:376.1 2.2 1
Vinyl acetate ND ug/kg 02/11/19 17:17 108-05-402/11/19 13:3761.1 10.8 1
Vinyl chloride ND ug/kg 02/11/19 17:17 75-01-402/11/19 13:3712.2 2.2 1
Xylene (Total)ND ug/kg 02/11/19 17:17 1330-20-702/11/19 13:3712.2 4.4 1
m&p-Xylene ND ug/kg 02/11/19 17:17 179601-23-102/11/19 13:3712.2 4.4 1
o-Xylene ND ug/kg 02/11/19 17:17 95-47-602/11/19 13:376.1 2.3 1
Surrogates
Toluene-d8 (S)100 %02/11/19 17:17 2037-26-502/11/19 13:3770-130 1
4-Bromofluorobenzene (S)97 %02/11/19 17:17 460-00-402/11/19 13:3770-130 1
1,2-Dichloroethane-d4 (S)100 %02/11/19 17:17 17060-07-002/11/19 13:3770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 3.5 %02/11/19 14:130.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-4 (7-9)Lab ID: 92417206004 Collected: 02/08/19 13:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 02/13/19 14:01 83-32-902/12/19 15:11424 97.7 1
Acenaphthylene ND ug/kg 02/13/19 14:01 208-96-802/12/19 15:11424 100 1
Aniline ND ug/kg 02/13/19 14:01 62-53-302/12/19 15:11424 114 1
Anthracene ND ug/kg 02/13/19 14:01 120-12-702/12/19 15:11424 95.2 1
Benzo(a)anthracene 127J ug/kg 02/13/19 14:01 56-55-302/12/19 15:11424 78.4 1
Benzo(a)pyrene 144J ug/kg 02/13/19 14:01 50-32-802/12/19 15:11424 81.0 1
Benzo(b)fluoranthene 204J ug/kg 02/13/19 14:01 205-99-202/12/19 15:11424 73.3 1
Benzo(g,h,i)perylene ND ug/kg 02/13/19 14:01 191-24-202/12/19 15:11424 108 1
Benzo(k)fluoranthene ND ug/kg 02/13/19 14:01 207-08-902/12/19 15:11424 83.6 1
Benzoic Acid ND ug/kg 02/13/19 14:01 65-85-002/12/19 15:112120 77.2 1
Benzyl alcohol ND ug/kg 02/13/19 14:01 100-51-602/12/19 15:11849 84.9 1
4-Bromophenylphenyl ether ND ug/kg 02/13/19 14:01 101-55-302/12/19 15:11424 77.2 1
Butylbenzylphthalate ND ug/kg 02/13/19 14:01 85-68-702/12/19 15:11424 90.0 1
4-Chloro-3-methylphenol ND ug/kg 02/13/19 14:01 59-50-702/12/19 15:11849 87.4 1
4-Chloroaniline ND ug/kg 02/13/19 14:01 106-47-802/12/19 15:112120 118 1
bis(2-Chloroethoxy)methane ND ug/kg 02/13/19 14:01 111-91-102/12/19 15:11424 99.0 1
bis(2-Chloroethyl) ether ND ug/kg 02/13/19 14:01 111-44-402/12/19 15:11424 108 1
2-Chloronaphthalene ND ug/kg 02/13/19 14:01 91-58-702/12/19 15:11424 83.6 1
2-Chlorophenol ND ug/kg 02/13/19 14:01 95-57-802/12/19 15:11424 116 1
4-Chlorophenylphenyl ether ND ug/kg 02/13/19 14:01 7005-72-302/12/19 15:11424 87.4 1
Chrysene 135J ug/kg 02/13/19 14:01 218-01-902/12/19 15:11424 56.6 1
Dibenz(a,h)anthracene ND ug/kg 02/13/19 14:01 53-70-302/12/19 15:11424 90.0 1
Dibenzofuran ND ug/kg 02/13/19 14:01 132-64-902/12/19 15:11424 69.4 1
1,2-Dichlorobenzene ND ug/kg 02/13/19 14:01 95-50-102/12/19 15:11424 113 1
1,3-Dichlorobenzene ND ug/kg 02/13/19 14:01 541-73-102/12/19 15:11424 96.4 1
1,4-Dichlorobenzene ND ug/kg 02/13/19 14:01 106-46-702/12/19 15:11424 120 1
3,3'-Dichlorobenzidine ND ug/kg 02/13/19 14:01 91-94-102/12/19 15:112120 92.6 1
2,4-Dichlorophenol ND ug/kg 02/13/19 14:01 120-83-202/12/19 15:11424 92.6 1
Diethylphthalate ND ug/kg 02/13/19 14:01 84-66-202/12/19 15:11424 65.6 1
2,4-Dimethylphenol ND ug/kg 02/13/19 14:01 105-67-902/12/19 15:11424 167 1
Dimethylphthalate ND ug/kg 02/13/19 14:01 131-11-302/12/19 15:11424 86.2 1
Di-n-butylphthalate ND ug/kg 02/13/19 14:01 84-74-202/12/19 15:11424 69.4 1
4,6-Dinitro-2-methylphenol ND ug/kg 02/13/19 14:01 534-52-102/12/19 15:11849 84.9 1
2,4-Dinitrophenol ND ug/kg 02/13/19 14:01 51-28-502/12/19 15:112120 69.4 1
2,4-Dinitrotoluene ND ug/kg 02/13/19 14:01 121-14-202/12/19 15:11424 79.7 1
2,6-Dinitrotoluene ND ug/kg 02/13/19 14:01 606-20-202/12/19 15:11424 88.7 1
Di-n-octylphthalate ND ug/kg 02/13/19 14:01 117-84-002/12/19 15:11424 88.7 1
bis(2-Ethylhexyl)phthalate ND ug/kg 02/13/19 14:01 117-81-702/12/19 15:11424 116 1
Fluoranthene 371J ug/kg 02/13/19 14:01 206-44-002/12/19 15:11424 61.7 1
Fluorene ND ug/kg 02/13/19 14:01 86-73-702/12/19 15:11424 87.4 1
Hexachloro-1,3-butadiene ND ug/kg 02/13/19 14:01 87-68-302/12/19 15:11424 73.3 1
Hexachlorobenzene ND ug/kg 02/13/19 14:01 118-74-102/12/19 15:11424 54.0 1
Hexachlorocyclopentadiene ND ug/kg 02/13/19 14:01 77-47-402/12/19 15:11424 78.4 1
Hexachloroethane ND ug/kg 02/13/19 14:01 67-72-102/12/19 15:11424 112 1
Indeno(1,2,3-cd)pyrene 91.9J ug/kg 02/13/19 14:01 193-39-502/12/19 15:11424 87.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-4 (7-9)Lab ID: 92417206004 Collected: 02/08/19 13:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 02/13/19 14:01 78-59-102/12/19 15:11424 95.2 1
1-Methylnaphthalene ND ug/kg 02/13/19 14:01 90-12-002/12/19 15:11424 111 1
2-Methylnaphthalene ND ug/kg 02/13/19 14:01 91-57-602/12/19 15:11424 91.3 1
2-Methylphenol(o-Cresol)ND ug/kg 02/13/19 14:01 95-48-702/12/19 15:11424 129 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/13/19 14:01 15831-10-402/12/19 15:11424 167 1
Naphthalene ND ug/kg 02/13/19 14:01 91-20-302/12/19 15:11424 104 1
2-Nitroaniline ND ug/kg 02/13/19 14:01 88-74-402/12/19 15:112120 131 1
3-Nitroaniline ND ug/kg 02/13/19 14:01 99-09-202/12/19 15:112120 116 1
4-Nitroaniline ND ug/kg 02/13/19 14:01 100-01-602/12/19 15:11849 120 1
Nitrobenzene ND ug/kg 02/13/19 14:01 98-95-302/12/19 15:11424 116 1
2-Nitrophenol ND ug/kg 02/13/19 14:01 88-75-502/12/19 15:11424 103 1
4-Nitrophenol ND ug/kg 02/13/19 14:01 100-02-702/12/19 15:112120 75.9 1
N-Nitrosodimethylamine ND ug/kg 02/13/19 14:01 62-75-902/12/19 15:11424 138 1
N-Nitroso-di-n-propylamine ND ug/kg 02/13/19 14:01 621-64-702/12/19 15:11424 81.0 1
N-Nitrosodiphenylamine ND ug/kg 02/13/19 14:01 86-30-602/12/19 15:11424 126 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/13/19 14:01 108-60-102/12/19 15:11424 113 1
Pentachlorophenol ND ug/kg 02/13/19 14:01 87-86-502/12/19 15:112120 77.2 1
Phenanthrene 165J ug/kg 02/13/19 14:01 85-01-802/12/19 15:11424 70.7 1
Phenol ND ug/kg 02/13/19 14:01 108-95-202/12/19 15:11424 127 1
Pyrene 274J ug/kg 02/13/19 14:01 129-00-002/12/19 15:11424 72.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/13/19 14:01 120-82-102/12/19 15:11424 82.3 1
2,4,5-Trichlorophenol ND ug/kg 02/13/19 14:01 95-95-402/12/19 15:11424 131 1
2,4,6-Trichlorophenol ND ug/kg 02/13/19 14:01 88-06-202/12/19 15:11424 93.9 1
Surrogates
Nitrobenzene-d5 (S)86 %02/13/19 14:01 4165-60-002/12/19 15:1123-110 1
2-Fluorobiphenyl (S)72 %02/13/19 14:01 321-60-802/12/19 15:1130-110 1
Terphenyl-d14 (S)66 %02/13/19 14:01 1718-51-002/12/19 15:1128-110 1
Phenol-d6 (S)89 %02/13/19 14:01 13127-88-302/12/19 15:1122-110 1
2-Fluorophenol (S)71 %02/13/19 14:01 367-12-402/12/19 15:1113-110 1
2,4,6-Tribromophenol (S)96 %02/13/19 14:01 118-79-602/12/19 15:1127-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 12.1J ug/kg 02/11/19 17:36 67-64-102/11/19 13:3791.9 9.2 1
Benzene ND ug/kg 02/11/19 17:36 71-43-202/11/19 13:374.6 1.5 1
Bromobenzene ND ug/kg 02/11/19 17:36 108-86-102/11/19 13:374.6 1.8 1
Bromochloromethane ND ug/kg 02/11/19 17:36 74-97-502/11/19 13:374.6 1.6 1
Bromodichloromethane ND ug/kg 02/11/19 17:36 75-27-402/11/19 13:374.6 1.7 1
Bromoform ND ug/kg 02/11/19 17:36 75-25-202/11/19 13:374.6 2.1 1
Bromomethane ND ug/kg 02/11/19 17:36 74-83-902/11/19 13:379.2 2.3 1
2-Butanone (MEK)ND ug/kg 02/11/19 17:36 78-93-302/11/19 13:3791.9 2.7 1
n-Butylbenzene ND ug/kg 02/11/19 17:36 104-51-802/11/19 13:374.6 1.7 1
sec-Butylbenzene ND ug/kg 02/11/19 17:36 135-98-802/11/19 13:374.6 1.5 1
tert-Butylbenzene ND ug/kg 02/11/19 17:36 98-06-602/11/19 13:374.6 1.8 1
Carbon tetrachloride ND ug/kg 02/11/19 17:36 56-23-502/11/19 13:374.6 2.4 1
Chlorobenzene ND ug/kg 02/11/19 17:36 108-90-702/11/19 13:374.6 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-4 (7-9)Lab ID: 92417206004 Collected: 02/08/19 13:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 02/11/19 17:36 75-00-302/11/19 13:379.2 2.2 1
Chloroform ND ug/kg 02/11/19 17:36 67-66-302/11/19 13:374.6 1.5 1
Chloromethane ND ug/kg 02/11/19 17:36 74-87-302/11/19 13:379.2 2.2 1
2-Chlorotoluene ND ug/kg 02/11/19 17:36 95-49-802/11/19 13:374.6 1.6 1
4-Chlorotoluene ND ug/kg 02/11/19 17:36 106-43-402/11/19 13:374.6 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/11/19 17:36 96-12-802/11/19 13:374.6 3.3 1
Dibromochloromethane ND ug/kg 02/11/19 17:36 124-48-102/11/19 13:374.6 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 02/11/19 17:36 106-93-402/11/19 13:374.6 1.7 1
Dibromomethane ND ug/kg 02/11/19 17:36 74-95-302/11/19 13:374.6 2.3 1
1,2-Dichlorobenzene ND ug/kg 02/11/19 17:36 95-50-102/11/19 13:374.6 1.7 1
1,3-Dichlorobenzene ND ug/kg 02/11/19 17:36 541-73-102/11/19 13:374.6 1.8 1
1,4-Dichlorobenzene ND ug/kg 02/11/19 17:36 106-46-702/11/19 13:374.6 1.6 1
Dichlorodifluoromethane ND ug/kg 02/11/19 17:36 75-71-802/11/19 13:379.2 3.3 1
1,1-Dichloroethane ND ug/kg 02/11/19 17:36 75-34-302/11/19 13:374.6 1.4 1
1,2-Dichloroethane ND ug/kg 02/11/19 17:36 107-06-202/11/19 13:374.6 2.0 1
1,1-Dichloroethene ND ug/kg 02/11/19 17:36 75-35-402/11/19 13:374.6 1.7 1
cis-1,2-Dichloroethene ND ug/kg 02/11/19 17:36 156-59-202/11/19 13:374.6 1.3 1
trans-1,2-Dichloroethene ND ug/kg 02/11/19 17:36 156-60-502/11/19 13:374.6 1.7 1
1,2-Dichloropropane ND ug/kg 02/11/19 17:36 78-87-502/11/19 13:374.6 1.6 1
1,3-Dichloropropane ND ug/kg 02/11/19 17:36 142-28-902/11/19 13:374.6 1.7 1
2,2-Dichloropropane ND ug/kg 02/11/19 17:36 594-20-702/11/19 13:374.6 1.6 1
1,1-Dichloropropene ND ug/kg 02/11/19 17:36 563-58-602/11/19 13:374.6 1.4 1
cis-1,3-Dichloropropene ND ug/kg 02/11/19 17:36 10061-01-502/11/19 13:374.6 1.7 1
trans-1,3-Dichloropropene ND ug/kg 02/11/19 17:36 10061-02-602/11/19 13:374.6 1.4 1
Diisopropyl ether ND ug/kg 02/11/19 17:36 108-20-302/11/19 13:374.6 1.6 1
Ethylbenzene ND ug/kg 02/11/19 17:36 100-41-402/11/19 13:374.6 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 02/11/19 17:36 87-68-302/11/19 13:374.6 1.8 1
2-Hexanone ND ug/kg 02/11/19 17:36 591-78-602/11/19 13:3745.9 3.6 1
Isopropylbenzene (Cumene)ND ug/kg 02/11/19 17:36 98-82-802/11/19 13:374.6 1.7 1
p-Isopropyltoluene ND ug/kg 02/11/19 17:36 99-87-602/11/19 13:374.6 1.6 1
Methylene Chloride ND ug/kg 02/11/19 17:36 75-09-202/11/19 13:3718.4 2.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/11/19 17:36 108-10-102/11/19 13:3745.9 3.4 1
Methyl-tert-butyl ether ND ug/kg 02/11/19 17:36 1634-04-402/11/19 13:374.6 1.4 1
Naphthalene ND ug/kg 02/11/19 17:36 91-20-302/11/19 13:374.6 1.1 1
n-Propylbenzene ND ug/kg 02/11/19 17:36 103-65-102/11/19 13:374.6 1.6 1
Styrene ND ug/kg 02/11/19 17:36 100-42-502/11/19 13:374.6 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/11/19 17:36 630-20-602/11/19 13:374.6 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/11/19 17:36 79-34-502/11/19 13:374.6 1.7 1
Tetrachloroethene ND ug/kg 02/11/19 17:36 127-18-402/11/19 13:374.6 1.6 1
Toluene ND ug/kg 02/11/19 17:36 108-88-302/11/19 13:374.6 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 02/11/19 17:36 87-61-602/11/19 13:374.6 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/11/19 17:36 120-82-102/11/19 13:374.6 1.5 1
1,1,1-Trichloroethane ND ug/kg 02/11/19 17:36 71-55-602/11/19 13:374.6 1.7 1
1,1,2-Trichloroethane ND ug/kg 02/11/19 17:36 79-00-502/11/19 13:374.6 1.9 1
Trichloroethene ND ug/kg 02/11/19 17:36 79-01-602/11/19 13:374.6 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-4 (7-9)Lab ID: 92417206004 Collected: 02/08/19 13:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 02/11/19 17:36 75-69-402/11/19 13:374.6 2.0 1
1,2,3-Trichloropropane ND ug/kg 02/11/19 17:36 96-18-402/11/19 13:374.6 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 02/11/19 17:36 95-63-602/11/19 13:374.6 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 02/11/19 17:36 108-67-802/11/19 13:374.6 1.7 1
Vinyl acetate ND ug/kg 02/11/19 17:36 108-05-402/11/19 13:3745.9 8.1 1
Vinyl chloride ND ug/kg 02/11/19 17:36 75-01-402/11/19 13:379.2 1.7 1
Xylene (Total)ND ug/kg 02/11/19 17:36 1330-20-702/11/19 13:379.2 3.3 1
m&p-Xylene ND ug/kg 02/11/19 17:36 179601-23-102/11/19 13:379.2 3.3 1
o-Xylene ND ug/kg 02/11/19 17:36 95-47-602/11/19 13:374.6 1.7 1
Surrogates
Toluene-d8 (S)99 %02/11/19 17:36 2037-26-502/11/19 13:3770-130 1
4-Bromofluorobenzene (S)99 %02/11/19 17:36 460-00-402/11/19 13:3770-130 1
1,2-Dichloroethane-d4 (S)97 %02/11/19 17:36 17060-07-002/11/19 13:3770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.7 %02/11/19 14:130.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-5 (0-2)Lab ID: 92417206005 Collected: 02/07/19 13:15 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 02/13/19 14:32 83-32-902/12/19 15:11443 102 1
Acenaphthylene ND ug/kg 02/13/19 14:32 208-96-802/12/19 15:11443 105 1
Aniline ND ug/kg 02/13/19 14:32 62-53-302/12/19 15:11443 119 1
Anthracene ND ug/kg 02/13/19 14:32 120-12-702/12/19 15:11443 99.3 1
Benzo(a)anthracene ND ug/kg 02/13/19 14:32 56-55-302/12/19 15:11443 81.9 1
Benzo(a)pyrene ND ug/kg 02/13/19 14:32 50-32-802/12/19 15:11443 84.6 1
Benzo(b)fluoranthene ND ug/kg 02/13/19 14:32 205-99-202/12/19 15:11443 76.5 1
Benzo(g,h,i)perylene ND ug/kg 02/13/19 14:32 191-24-202/12/19 15:11443 113 1
Benzo(k)fluoranthene ND ug/kg 02/13/19 14:32 207-08-902/12/19 15:11443 87.3 1
Benzoic Acid ND ug/kg 02/13/19 14:32 65-85-002/12/19 15:112210 80.5 1
Benzyl alcohol ND ug/kg 02/13/19 14:32 100-51-602/12/19 15:11886 88.6 1
4-Bromophenylphenyl ether ND ug/kg 02/13/19 14:32 101-55-302/12/19 15:11443 80.5 1
Butylbenzylphthalate ND ug/kg 02/13/19 14:32 85-68-702/12/19 15:11443 94.0 1
4-Chloro-3-methylphenol ND ug/kg 02/13/19 14:32 59-50-702/12/19 15:11886 91.3 1
4-Chloroaniline ND ug/kg 02/13/19 14:32 106-47-802/12/19 15:112210 124 1
bis(2-Chloroethoxy)methane ND ug/kg 02/13/19 14:32 111-91-102/12/19 15:11443 103 1
bis(2-Chloroethyl) ether ND ug/kg 02/13/19 14:32 111-44-402/12/19 15:11443 113 1
2-Chloronaphthalene ND ug/kg 02/13/19 14:32 91-58-702/12/19 15:11443 87.3 1
2-Chlorophenol ND ug/kg 02/13/19 14:32 95-57-802/12/19 15:11443 121 1
4-Chlorophenylphenyl ether ND ug/kg 02/13/19 14:32 7005-72-302/12/19 15:11443 91.3 1
Chrysene ND ug/kg 02/13/19 14:32 218-01-902/12/19 15:11443 59.1 1
Dibenz(a,h)anthracene ND ug/kg 02/13/19 14:32 53-70-302/12/19 15:11443 94.0 1
Dibenzofuran ND ug/kg 02/13/19 14:32 132-64-902/12/19 15:11443 72.5 1
1,2-Dichlorobenzene ND ug/kg 02/13/19 14:32 95-50-102/12/19 15:11443 118 1
1,3-Dichlorobenzene ND ug/kg 02/13/19 14:32 541-73-102/12/19 15:11443 101 1
1,4-Dichlorobenzene ND ug/kg 02/13/19 14:32 106-46-702/12/19 15:11443 125 1
3,3'-Dichlorobenzidine ND ug/kg 02/13/19 14:32 91-94-102/12/19 15:112210 96.7 1
2,4-Dichlorophenol ND ug/kg 02/13/19 14:32 120-83-202/12/19 15:11443 96.7 1
Diethylphthalate ND ug/kg 02/13/19 14:32 84-66-202/12/19 15:11443 68.5 1
2,4-Dimethylphenol ND ug/kg 02/13/19 14:32 105-67-902/12/19 15:11443 175 1
Dimethylphthalate ND ug/kg 02/13/19 14:32 131-11-302/12/19 15:11443 89.9 1
Di-n-butylphthalate ND ug/kg 02/13/19 14:32 84-74-202/12/19 15:11443 72.5 1
4,6-Dinitro-2-methylphenol ND ug/kg 02/13/19 14:32 534-52-102/12/19 15:11886 88.6 1
2,4-Dinitrophenol ND ug/kg 02/13/19 14:32 51-28-502/12/19 15:112210 72.5 1
2,4-Dinitrotoluene ND ug/kg 02/13/19 14:32 121-14-202/12/19 15:11443 83.2 1
2,6-Dinitrotoluene ND ug/kg 02/13/19 14:32 606-20-202/12/19 15:11443 92.6 1
Di-n-octylphthalate ND ug/kg 02/13/19 14:32 117-84-002/12/19 15:11443 92.6 1
bis(2-Ethylhexyl)phthalate ND ug/kg 02/13/19 14:32 117-81-702/12/19 15:11443 121 1
Fluoranthene ND ug/kg 02/13/19 14:32 206-44-002/12/19 15:11443 64.4 1
Fluorene ND ug/kg 02/13/19 14:32 86-73-702/12/19 15:11443 91.3 1
Hexachloro-1,3-butadiene ND ug/kg 02/13/19 14:32 87-68-302/12/19 15:11443 76.5 1
Hexachlorobenzene ND ug/kg 02/13/19 14:32 118-74-102/12/19 15:11443 56.4 1
Hexachlorocyclopentadiene ND ug/kg 02/13/19 14:32 77-47-402/12/19 15:11443 81.9 1
Hexachloroethane ND ug/kg 02/13/19 14:32 67-72-102/12/19 15:11443 117 1
Indeno(1,2,3-cd)pyrene ND ug/kg 02/13/19 14:32 193-39-502/12/19 15:11443 91.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-5 (0-2)Lab ID: 92417206005 Collected: 02/07/19 13:15 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 02/13/19 14:32 78-59-102/12/19 15:11443 99.3 1
1-Methylnaphthalene ND ug/kg 02/13/19 14:32 90-12-002/12/19 15:11443 115 1
2-Methylnaphthalene ND ug/kg 02/13/19 14:32 91-57-602/12/19 15:11443 95.3 1
2-Methylphenol(o-Cresol)ND ug/kg 02/13/19 14:32 95-48-702/12/19 15:11443 134 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/13/19 14:32 15831-10-402/12/19 15:11443 175 1
Naphthalene ND ug/kg 02/13/19 14:32 91-20-302/12/19 15:11443 109 1
2-Nitroaniline ND ug/kg 02/13/19 14:32 88-74-402/12/19 15:112210 137 1
3-Nitroaniline ND ug/kg 02/13/19 14:32 99-09-202/12/19 15:112210 121 1
4-Nitroaniline ND ug/kg 02/13/19 14:32 100-01-602/12/19 15:11886 125 1
Nitrobenzene ND ug/kg 02/13/19 14:32 98-95-302/12/19 15:11443 121 1
2-Nitrophenol ND ug/kg 02/13/19 14:32 88-75-502/12/19 15:11443 107 1
4-Nitrophenol ND ug/kg 02/13/19 14:32 100-02-702/12/19 15:112210 79.2 1
N-Nitrosodimethylamine ND ug/kg 02/13/19 14:32 62-75-902/12/19 15:11443 144 1
N-Nitroso-di-n-propylamine ND ug/kg 02/13/19 14:32 621-64-702/12/19 15:11443 84.6 1
N-Nitrosodiphenylamine ND ug/kg 02/13/19 14:32 86-30-602/12/19 15:11443 132 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/13/19 14:32 108-60-102/12/19 15:11443 118 1
Pentachlorophenol ND ug/kg 02/13/19 14:32 87-86-502/12/19 15:112210 80.5 1
Phenanthrene ND ug/kg 02/13/19 14:32 85-01-802/12/19 15:11443 73.8 1
Phenol ND ug/kg 02/13/19 14:32 108-95-202/12/19 15:11443 133 1
Pyrene ND ug/kg 02/13/19 14:32 129-00-002/12/19 15:11443 75.2 1
1,2,4-Trichlorobenzene ND ug/kg 02/13/19 14:32 120-82-102/12/19 15:11443 85.9 1
2,4,5-Trichlorophenol ND ug/kg 02/13/19 14:32 95-95-402/12/19 15:11443 137 1
2,4,6-Trichlorophenol ND ug/kg 02/13/19 14:32 88-06-202/12/19 15:11443 98.0 1
Surrogates
Nitrobenzene-d5 (S)59 %02/13/19 14:32 4165-60-002/12/19 15:1123-110 1
2-Fluorobiphenyl (S)52 %02/13/19 14:32 321-60-802/12/19 15:1130-110 1
Terphenyl-d14 (S)98 %02/13/19 14:32 1718-51-002/12/19 15:1128-110 1
Phenol-d6 (S)67 %02/13/19 14:32 13127-88-302/12/19 15:1122-110 1
2-Fluorophenol (S)56 %02/13/19 14:32 367-12-402/12/19 15:1113-110 1
2,4,6-Tribromophenol (S)66 %02/13/19 14:32 118-79-602/12/19 15:1127-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 38.0J ug/kg 02/11/19 17:54 67-64-102/11/19 13:3797.7 9.8 1
Benzene ND ug/kg 02/11/19 17:54 71-43-202/11/19 13:374.9 1.6 1
Bromobenzene ND ug/kg 02/11/19 17:54 108-86-102/11/19 13:374.9 2.0 1
Bromochloromethane ND ug/kg 02/11/19 17:54 74-97-502/11/19 13:374.9 1.7 1
Bromodichloromethane ND ug/kg 02/11/19 17:54 75-27-402/11/19 13:374.9 1.9 1
Bromoform ND ug/kg 02/11/19 17:54 75-25-202/11/19 13:374.9 2.2 1
Bromomethane ND ug/kg 02/11/19 17:54 74-83-902/11/19 13:379.8 2.4 1
2-Butanone (MEK)ND ug/kg 02/11/19 17:54 78-93-302/11/19 13:3797.7 2.8 1
n-Butylbenzene ND ug/kg 02/11/19 17:54 104-51-802/11/19 13:374.9 1.8 1
sec-Butylbenzene ND ug/kg 02/11/19 17:54 135-98-802/11/19 13:374.9 1.6 1
tert-Butylbenzene ND ug/kg 02/11/19 17:54 98-06-602/11/19 13:374.9 2.0 1
Carbon tetrachloride ND ug/kg 02/11/19 17:54 56-23-502/11/19 13:374.9 2.5 1
Chlorobenzene ND ug/kg 02/11/19 17:54 108-90-702/11/19 13:374.9 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-5 (0-2)Lab ID: 92417206005 Collected: 02/07/19 13:15 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 02/11/19 17:54 75-00-302/11/19 13:379.8 2.3 1
Chloroform ND ug/kg 02/11/19 17:54 67-66-302/11/19 13:374.9 1.6 1
Chloromethane ND ug/kg 02/11/19 17:54 74-87-302/11/19 13:379.8 2.3 1
2-Chlorotoluene ND ug/kg 02/11/19 17:54 95-49-802/11/19 13:374.9 1.7 1
4-Chlorotoluene ND ug/kg 02/11/19 17:54 106-43-402/11/19 13:374.9 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/11/19 17:54 96-12-802/11/19 13:374.9 3.5 1
Dibromochloromethane ND ug/kg 02/11/19 17:54 124-48-102/11/19 13:374.9 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 02/11/19 17:54 106-93-402/11/19 13:374.9 1.8 1
Dibromomethane ND ug/kg 02/11/19 17:54 74-95-302/11/19 13:374.9 2.4 1
1,2-Dichlorobenzene ND ug/kg 02/11/19 17:54 95-50-102/11/19 13:374.9 1.9 1
1,3-Dichlorobenzene ND ug/kg 02/11/19 17:54 541-73-102/11/19 13:374.9 2.0 1
1,4-Dichlorobenzene ND ug/kg 02/11/19 17:54 106-46-702/11/19 13:374.9 1.7 1
Dichlorodifluoromethane ND ug/kg 02/11/19 17:54 75-71-802/11/19 13:379.8 3.5 1
1,1-Dichloroethane ND ug/kg 02/11/19 17:54 75-34-302/11/19 13:374.9 1.5 1
1,2-Dichloroethane ND ug/kg 02/11/19 17:54 107-06-202/11/19 13:374.9 2.1 1
1,1-Dichloroethene ND ug/kg 02/11/19 17:54 75-35-402/11/19 13:374.9 1.8 1
cis-1,2-Dichloroethene ND ug/kg 02/11/19 17:54 156-59-202/11/19 13:374.9 1.4 1
trans-1,2-Dichloroethene ND ug/kg 02/11/19 17:54 156-60-502/11/19 13:374.9 1.9 1
1,2-Dichloropropane ND ug/kg 02/11/19 17:54 78-87-502/11/19 13:374.9 1.7 1
1,3-Dichloropropane ND ug/kg 02/11/19 17:54 142-28-902/11/19 13:374.9 1.9 1
2,2-Dichloropropane ND ug/kg 02/11/19 17:54 594-20-702/11/19 13:374.9 1.7 1
1,1-Dichloropropene ND ug/kg 02/11/19 17:54 563-58-602/11/19 13:374.9 1.5 1
cis-1,3-Dichloropropene ND ug/kg 02/11/19 17:54 10061-01-502/11/19 13:374.9 1.8 1
trans-1,3-Dichloropropene ND ug/kg 02/11/19 17:54 10061-02-602/11/19 13:374.9 1.5 1
Diisopropyl ether ND ug/kg 02/11/19 17:54 108-20-302/11/19 13:374.9 1.7 1
Ethylbenzene ND ug/kg 02/11/19 17:54 100-41-402/11/19 13:374.9 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 02/11/19 17:54 87-68-302/11/19 13:374.9 2.0 1
2-Hexanone ND ug/kg 02/11/19 17:54 591-78-602/11/19 13:3748.9 3.8 1
Isopropylbenzene (Cumene)ND ug/kg 02/11/19 17:54 98-82-802/11/19 13:374.9 1.9 1
p-Isopropyltoluene ND ug/kg 02/11/19 17:54 99-87-602/11/19 13:374.9 1.7 1
Methylene Chloride ND ug/kg 02/11/19 17:54 75-09-202/11/19 13:3719.5 2.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/11/19 17:54 108-10-102/11/19 13:3748.9 3.6 1
Methyl-tert-butyl ether ND ug/kg 02/11/19 17:54 1634-04-402/11/19 13:374.9 1.5 1
Naphthalene ND ug/kg 02/11/19 17:54 91-20-302/11/19 13:374.9 1.2 1
n-Propylbenzene ND ug/kg 02/11/19 17:54 103-65-102/11/19 13:374.9 1.7 1
Styrene ND ug/kg 02/11/19 17:54 100-42-502/11/19 13:374.9 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/11/19 17:54 630-20-602/11/19 13:374.9 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/11/19 17:54 79-34-502/11/19 13:374.9 1.9 1
Tetrachloroethene ND ug/kg 02/11/19 17:54 127-18-402/11/19 13:374.9 1.7 1
Toluene ND ug/kg 02/11/19 17:54 108-88-302/11/19 13:374.9 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 02/11/19 17:54 87-61-602/11/19 13:374.9 2.1 1
1,2,4-Trichlorobenzene ND ug/kg 02/11/19 17:54 120-82-102/11/19 13:374.9 1.6 1
1,1,1-Trichloroethane ND ug/kg 02/11/19 17:54 71-55-602/11/19 13:374.9 1.8 1
1,1,2-Trichloroethane ND ug/kg 02/11/19 17:54 79-00-502/11/19 13:374.9 2.1 1
Trichloroethene ND ug/kg 02/11/19 17:54 79-01-602/11/19 13:374.9 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-5 (0-2)Lab ID: 92417206005 Collected: 02/07/19 13:15 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 02/11/19 17:54 75-69-402/11/19 13:374.9 2.1 1
1,2,3-Trichloropropane ND ug/kg 02/11/19 17:54 96-18-402/11/19 13:374.9 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 02/11/19 17:54 95-63-602/11/19 13:374.9 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/11/19 17:54 108-67-802/11/19 13:374.9 1.8 1
Vinyl acetate ND ug/kg 02/11/19 17:54 108-05-402/11/19 13:3748.9 8.6 1
Vinyl chloride ND ug/kg 02/11/19 17:54 75-01-402/11/19 13:379.8 1.8 1
Xylene (Total)ND ug/kg 02/11/19 17:54 1330-20-702/11/19 13:379.8 3.5 1
m&p-Xylene ND ug/kg 02/11/19 17:54 179601-23-102/11/19 13:379.8 3.5 1
o-Xylene ND ug/kg 02/11/19 17:54 95-47-602/11/19 13:374.9 1.9 1
Surrogates
Toluene-d8 (S)101 %02/11/19 17:54 2037-26-502/11/19 13:3770-130 1
4-Bromofluorobenzene (S)98 %02/11/19 17:54 460-00-402/11/19 13:3770-130 1
1,2-Dichloroethane-d4 (S)98 %02/11/19 17:54 17060-07-002/11/19 13:3770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.8 %02/11/19 14:130.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-6 (0-2)Lab ID: 92417206006 Collected: 02/07/19 15:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 02/15/19 18:14 83-32-902/15/19 10:132040 469 5
Acenaphthylene ND ug/kg 02/15/19 18:14 208-96-802/15/19 10:132040 481 5
Aniline ND ug/kg 02/15/19 18:14 62-53-302/15/19 10:132040 549 5
Anthracene ND ug/kg 02/15/19 18:14 120-12-702/15/19 10:132040 457 5
Benzo(a)anthracene ND ug/kg 02/15/19 18:14 56-55-302/15/19 10:132040 376 5
Benzo(a)pyrene ND ug/kg 02/15/19 18:14 50-32-802/15/19 10:132040 389 5
Benzo(b)fluoranthene ND ug/kg 02/15/19 18:14 205-99-202/15/19 10:132040 352 5
Benzo(g,h,i)perylene ND ug/kg 02/15/19 18:14 191-24-202/15/19 10:132040 518 5
Benzo(k)fluoranthene ND ug/kg 02/15/19 18:14 207-08-902/15/19 10:132040 401 5
Benzoic Acid ND ug/kg 02/15/19 18:14 65-85-002/15/19 10:1310200 370 5
Benzyl alcohol ND ug/kg 02/15/19 18:14 100-51-602/15/19 10:134070 407 5
4-Bromophenylphenyl ether ND ug/kg 02/15/19 18:14 101-55-302/15/19 10:132040 370 5
Butylbenzylphthalate ND ug/kg 02/15/19 18:14 85-68-702/15/19 10:132040 432 5
4-Chloro-3-methylphenol ND ug/kg 02/15/19 18:14 59-50-702/15/19 10:134070 420 5
4-Chloroaniline ND ug/kg 02/15/19 18:14 106-47-802/15/19 10:1310200 568 5
bis(2-Chloroethoxy)methane ND ug/kg 02/15/19 18:14 111-91-102/15/19 10:132040 475 5
bis(2-Chloroethyl) ether ND ug/kg 02/15/19 18:14 111-44-402/15/19 10:132040 518 5
2-Chloronaphthalene ND ug/kg 02/15/19 18:14 91-58-702/15/19 10:132040 401 5
2-Chlorophenol ND ug/kg 02/15/19 18:14 95-57-802/15/19 10:132040 555 5
4-Chlorophenylphenyl ether ND ug/kg 02/15/19 18:14 7005-72-302/15/19 10:132040 420 5
Chrysene ND ug/kg 02/15/19 18:14 218-01-902/15/19 10:132040 272 5
Dibenz(a,h)anthracene ND ug/kg 02/15/19 18:14 53-70-302/15/19 10:132040 432 5
Dibenzofuran ND ug/kg 02/15/19 18:14 132-64-902/15/19 10:132040 333 5
1,2-Dichlorobenzene ND ug/kg 02/15/19 18:14 95-50-102/15/19 10:132040 543 5
1,3-Dichlorobenzene ND ug/kg 02/15/19 18:14 541-73-102/15/19 10:132040 463 5
1,4-Dichlorobenzene ND ug/kg 02/15/19 18:14 106-46-702/15/19 10:132040 574 5
3,3'-Dichlorobenzidine ND ug/kg 02/15/19 18:14 91-94-102/15/19 10:1310200 444 5
2,4-Dichlorophenol ND ug/kg 02/15/19 18:14 120-83-202/15/19 10:132040 444 5
Diethylphthalate ND ug/kg 02/15/19 18:14 84-66-202/15/19 10:132040 315 5
2,4-Dimethylphenol ND ug/kg 02/15/19 18:14 105-67-902/15/19 10:132040 802 5
Dimethylphthalate ND ug/kg 02/15/19 18:14 131-11-302/15/19 10:132040 413 5
Di-n-butylphthalate ND ug/kg 02/15/19 18:14 84-74-202/15/19 10:132040 333 5
4,6-Dinitro-2-methylphenol ND ug/kg 02/15/19 18:14 534-52-102/15/19 10:134070 407 5
2,4-Dinitrophenol ND ug/kg 02/15/19 18:14 51-28-502/15/19 10:1310200 333 5
2,4-Dinitrotoluene ND ug/kg 02/15/19 18:14 121-14-202/15/19 10:132040 383 5
2,6-Dinitrotoluene ND ug/kg 02/15/19 18:14 606-20-202/15/19 10:132040 426 5
Di-n-octylphthalate ND ug/kg 02/15/19 18:14 117-84-002/15/19 10:132040 426 5
bis(2-Ethylhexyl)phthalate ND ug/kg 02/15/19 18:14 117-81-702/15/19 10:132040 555 5
Fluoranthene ND ug/kg 02/15/19 18:14 206-44-002/15/19 10:132040 296 5
Fluorene ND ug/kg 02/15/19 18:14 86-73-702/15/19 10:132040 420 5
Hexachloro-1,3-butadiene ND ug/kg 02/15/19 18:14 87-68-302/15/19 10:132040 352 5
Hexachlorobenzene ND ug/kg 02/15/19 18:14 118-74-102/15/19 10:132040 259 5
Hexachlorocyclopentadiene ND ug/kg 02/15/19 18:14 77-47-402/15/19 10:132040 376 5
Hexachloroethane ND ug/kg 02/15/19 18:14 67-72-102/15/19 10:132040 537 5
Indeno(1,2,3-cd)pyrene ND ug/kg 02/15/19 18:14 193-39-502/15/19 10:132040 420 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-6 (0-2)Lab ID: 92417206006 Collected: 02/07/19 15:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 02/15/19 18:14 78-59-102/15/19 10:132040 457 5
1-Methylnaphthalene ND ug/kg 02/15/19 18:14 90-12-002/15/19 10:132040 531 5
2-Methylnaphthalene ND ug/kg 02/15/19 18:14 91-57-602/15/19 10:132040 438 5
2-Methylphenol(o-Cresol)ND ug/kg 02/15/19 18:14 95-48-702/15/19 10:132040 617 5
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/15/19 18:14 15831-10-402/15/19 10:132040 802 5
Naphthalene ND ug/kg 02/15/19 18:14 91-20-302/15/19 10:132040 500 5
2-Nitroaniline ND ug/kg 02/15/19 18:14 88-74-402/15/19 10:1310200 629 5
3-Nitroaniline ND ug/kg 02/15/19 18:14 99-09-202/15/19 10:1310200 555 5
4-Nitroaniline ND ug/kg 02/15/19 18:14 100-01-602/15/19 10:134070 574 5
Nitrobenzene ND ug/kg 02/15/19 18:14 98-95-302/15/19 10:132040 555 5
2-Nitrophenol ND ug/kg 02/15/19 18:14 88-75-502/15/19 10:132040 494 5
4-Nitrophenol ND ug/kg 02/15/19 18:14 100-02-702/15/19 10:1310200 364 5
N-Nitrosodimethylamine ND ug/kg 02/15/19 18:14 62-75-902/15/19 10:132040 660 5
N-Nitroso-di-n-propylamine ND ug/kg 02/15/19 18:14 621-64-702/15/19 10:132040 389 5
N-Nitrosodiphenylamine ND ug/kg 02/15/19 18:14 86-30-602/15/19 10:132040 605 5
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/15/19 18:14 108-60-102/15/19 10:132040 543 5
Pentachlorophenol ND ug/kg 02/15/19 18:14 87-86-502/15/19 10:1310200 370 5
Phenanthrene ND ug/kg 02/15/19 18:14 85-01-802/15/19 10:132040 339 5
Phenol ND ug/kg 02/15/19 18:14 108-95-202/15/19 10:132040 611 5
Pyrene ND ug/kg 02/15/19 18:14 129-00-002/15/19 10:132040 346 5
1,2,4-Trichlorobenzene ND ug/kg 02/15/19 18:14 120-82-102/15/19 10:132040 395 5
2,4,5-Trichlorophenol ND ug/kg 02/15/19 18:14 95-95-402/15/19 10:132040 629 5
2,4,6-Trichlorophenol ND ug/kg 02/15/19 18:14 88-06-202/15/19 10:132040 450 5
Surrogates
Nitrobenzene-d5 (S)41 %02/15/19 18:14 4165-60-0 D302/15/19 10:1323-110 5
2-Fluorobiphenyl (S)37 %02/15/19 18:14 321-60-802/15/19 10:1330-110 5
Terphenyl-d14 (S)45 %02/15/19 18:14 1718-51-002/15/19 10:1328-110 5
Phenol-d6 (S)38 %02/15/19 18:14 13127-88-302/15/19 10:1322-110 5
2-Fluorophenol (S)30 %02/15/19 18:14 367-12-402/15/19 10:1313-110 5
2,4,6-Tribromophenol (S)37 %02/15/19 18:14 118-79-602/15/19 10:1327-110 5
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 17.3J ug/kg 02/11/19 18:13 67-64-102/11/19 13:3796.0 9.6 1
Benzene ND ug/kg 02/11/19 18:13 71-43-202/11/19 13:374.8 1.5 1
Bromobenzene ND ug/kg 02/11/19 18:13 108-86-102/11/19 13:374.8 1.9 1
Bromochloromethane ND ug/kg 02/11/19 18:13 74-97-502/11/19 13:374.8 1.6 1
Bromodichloromethane ND ug/kg 02/11/19 18:13 75-27-402/11/19 13:374.8 1.8 1
Bromoform ND ug/kg 02/11/19 18:13 75-25-202/11/19 13:374.8 2.2 1
Bromomethane ND ug/kg 02/11/19 18:13 74-83-902/11/19 13:379.6 2.4 1
2-Butanone (MEK)ND ug/kg 02/11/19 18:13 78-93-302/11/19 13:3796.0 2.8 1
n-Butylbenzene ND ug/kg 02/11/19 18:13 104-51-802/11/19 13:374.8 1.7 1
sec-Butylbenzene ND ug/kg 02/11/19 18:13 135-98-802/11/19 13:374.8 1.5 1
tert-Butylbenzene ND ug/kg 02/11/19 18:13 98-06-602/11/19 13:374.8 1.9 1
Carbon tetrachloride ND ug/kg 02/11/19 18:13 56-23-502/11/19 13:374.8 2.5 1
Chlorobenzene ND ug/kg 02/11/19 18:13 108-90-702/11/19 13:374.8 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-6 (0-2)Lab ID: 92417206006 Collected: 02/07/19 15:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 02/11/19 18:13 75-00-302/11/19 13:379.6 2.3 1
Chloroform ND ug/kg 02/11/19 18:13 67-66-302/11/19 13:374.8 1.5 1
Chloromethane ND ug/kg 02/11/19 18:13 74-87-302/11/19 13:379.6 2.3 1
2-Chlorotoluene ND ug/kg 02/11/19 18:13 95-49-802/11/19 13:374.8 1.6 1
4-Chlorotoluene ND ug/kg 02/11/19 18:13 106-43-402/11/19 13:374.8 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/11/19 18:13 96-12-802/11/19 13:374.8 3.5 1
Dibromochloromethane ND ug/kg 02/11/19 18:13 124-48-102/11/19 13:374.8 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 02/11/19 18:13 106-93-402/11/19 13:374.8 1.7 1
Dibromomethane ND ug/kg 02/11/19 18:13 74-95-302/11/19 13:374.8 2.4 1
1,2-Dichlorobenzene ND ug/kg 02/11/19 18:13 95-50-102/11/19 13:374.8 1.8 1
1,3-Dichlorobenzene ND ug/kg 02/11/19 18:13 541-73-102/11/19 13:374.8 1.9 1
1,4-Dichlorobenzene ND ug/kg 02/11/19 18:13 106-46-702/11/19 13:374.8 1.6 1
Dichlorodifluoromethane ND ug/kg 02/11/19 18:13 75-71-802/11/19 13:379.6 3.5 1
1,1-Dichloroethane ND ug/kg 02/11/19 18:13 75-34-302/11/19 13:374.8 1.4 1
1,2-Dichloroethane ND ug/kg 02/11/19 18:13 107-06-202/11/19 13:374.8 2.1 1
1,1-Dichloroethene ND ug/kg 02/11/19 18:13 75-35-402/11/19 13:374.8 1.7 1
cis-1,2-Dichloroethene ND ug/kg 02/11/19 18:13 156-59-202/11/19 13:374.8 1.3 1
trans-1,2-Dichloroethene ND ug/kg 02/11/19 18:13 156-60-502/11/19 13:374.8 1.8 1
1,2-Dichloropropane ND ug/kg 02/11/19 18:13 78-87-502/11/19 13:374.8 1.6 1
1,3-Dichloropropane ND ug/kg 02/11/19 18:13 142-28-902/11/19 13:374.8 1.8 1
2,2-Dichloropropane ND ug/kg 02/11/19 18:13 594-20-702/11/19 13:374.8 1.6 1
1,1-Dichloropropene ND ug/kg 02/11/19 18:13 563-58-602/11/19 13:374.8 1.4 1
cis-1,3-Dichloropropene ND ug/kg 02/11/19 18:13 10061-01-502/11/19 13:374.8 1.7 1
trans-1,3-Dichloropropene ND ug/kg 02/11/19 18:13 10061-02-602/11/19 13:374.8 1.4 1
Diisopropyl ether ND ug/kg 02/11/19 18:13 108-20-302/11/19 13:374.8 1.6 1
Ethylbenzene ND ug/kg 02/11/19 18:13 100-41-402/11/19 13:374.8 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 02/11/19 18:13 87-68-302/11/19 13:374.8 1.9 1
2-Hexanone ND ug/kg 02/11/19 18:13 591-78-602/11/19 13:3748.0 3.7 1
Isopropylbenzene (Cumene)ND ug/kg 02/11/19 18:13 98-82-802/11/19 13:374.8 1.8 1
p-Isopropyltoluene ND ug/kg 02/11/19 18:13 99-87-602/11/19 13:374.8 1.6 1
Methylene Chloride ND ug/kg 02/11/19 18:13 75-09-202/11/19 13:3719.2 2.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/11/19 18:13 108-10-102/11/19 13:3748.0 3.6 1
Methyl-tert-butyl ether ND ug/kg 02/11/19 18:13 1634-04-402/11/19 13:374.8 1.4 1
Naphthalene ND ug/kg 02/11/19 18:13 91-20-302/11/19 13:374.8 1.2 1
n-Propylbenzene ND ug/kg 02/11/19 18:13 103-65-102/11/19 13:374.8 1.6 1
Styrene ND ug/kg 02/11/19 18:13 100-42-502/11/19 13:374.8 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/11/19 18:13 630-20-602/11/19 13:374.8 2.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/11/19 18:13 79-34-502/11/19 13:374.8 1.8 1
Tetrachloroethene ND ug/kg 02/11/19 18:13 127-18-402/11/19 13:374.8 1.6 1
Toluene ND ug/kg 02/11/19 18:13 108-88-302/11/19 13:374.8 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 02/11/19 18:13 87-61-602/11/19 13:374.8 2.1 1
1,2,4-Trichlorobenzene ND ug/kg 02/11/19 18:13 120-82-102/11/19 13:374.8 1.5 1
1,1,1-Trichloroethane ND ug/kg 02/11/19 18:13 71-55-602/11/19 13:374.8 1.7 1
1,1,2-Trichloroethane ND ug/kg 02/11/19 18:13 79-00-502/11/19 13:374.8 2.0 1
Trichloroethene ND ug/kg 02/11/19 18:13 79-01-602/11/19 13:374.8 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-6 (0-2)Lab ID: 92417206006 Collected: 02/07/19 15:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 02/11/19 18:13 75-69-402/11/19 13:374.8 2.1 1
1,2,3-Trichloropropane ND ug/kg 02/11/19 18:13 96-18-402/11/19 13:374.8 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 02/11/19 18:13 95-63-602/11/19 13:374.8 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 02/11/19 18:13 108-67-802/11/19 13:374.8 1.7 1
Vinyl acetate ND ug/kg 02/11/19 18:13 108-05-402/11/19 13:3748.0 8.4 1
Vinyl chloride ND ug/kg 02/11/19 18:13 75-01-402/11/19 13:379.6 1.7 1
Xylene (Total)ND ug/kg 02/11/19 18:13 1330-20-702/11/19 13:379.6 3.5 1
m&p-Xylene ND ug/kg 02/11/19 18:13 179601-23-102/11/19 13:379.6 3.5 1
o-Xylene ND ug/kg 02/11/19 18:13 95-47-602/11/19 13:374.8 1.8 1
Surrogates
Toluene-d8 (S)100 %02/11/19 18:13 2037-26-502/11/19 13:3770-130 1
4-Bromofluorobenzene (S)99 %02/11/19 18:13 460-00-402/11/19 13:3770-130 1
1,2-Dichloroethane-d4 (S)93 %02/11/19 18:13 17060-07-002/11/19 13:3770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.2 %02/11/19 14:130.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-9 (0-2)Lab ID: 92417206009 Collected: 02/08/19 14:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 02/15/19 19:58 83-32-902/15/19 10:13408 94.0 1
Acenaphthylene ND ug/kg 02/15/19 19:58 208-96-802/15/19 10:13408 96.5 1
Aniline ND ug/kg 02/15/19 19:58 62-53-302/15/19 10:13408 110 1
Anthracene ND ug/kg 02/15/19 19:58 120-12-702/15/19 10:13408 91.5 1
Benzo(a)anthracene ND ug/kg 02/15/19 19:58 56-55-302/15/19 10:13408 75.5 1
Benzo(a)pyrene ND ug/kg 02/15/19 19:58 50-32-802/15/19 10:13408 77.9 1
Benzo(b)fluoranthene ND ug/kg 02/15/19 19:58 205-99-202/15/19 10:13408 70.5 1
Benzo(g,h,i)perylene ND ug/kg 02/15/19 19:58 191-24-202/15/19 10:13408 104 1
Benzo(k)fluoranthene ND ug/kg 02/15/19 19:58 207-08-902/15/19 10:13408 80.4 1
Benzoic Acid ND ug/kg 02/15/19 19:58 65-85-002/15/19 10:132040 74.2 1
Benzyl alcohol ND ug/kg 02/15/19 19:58 100-51-602/15/19 10:13817 81.7 1
4-Bromophenylphenyl ether ND ug/kg 02/15/19 19:58 101-55-302/15/19 10:13408 74.2 1
Butylbenzylphthalate ND ug/kg 02/15/19 19:58 85-68-702/15/19 10:13408 86.6 1
4-Chloro-3-methylphenol ND ug/kg 02/15/19 19:58 59-50-702/15/19 10:13817 84.1 1
4-Chloroaniline ND ug/kg 02/15/19 19:58 106-47-802/15/19 10:132040 114 1
bis(2-Chloroethoxy)methane ND ug/kg 02/15/19 19:58 111-91-102/15/19 10:13408 95.3 1
bis(2-Chloroethyl) ether ND ug/kg 02/15/19 19:58 111-44-402/15/19 10:13408 104 1
2-Chloronaphthalene ND ug/kg 02/15/19 19:58 91-58-702/15/19 10:13408 80.4 1
2-Chlorophenol ND ug/kg 02/15/19 19:58 95-57-802/15/19 10:13408 111 1
4-Chlorophenylphenyl ether ND ug/kg 02/15/19 19:58 7005-72-302/15/19 10:13408 84.1 1
Chrysene ND ug/kg 02/15/19 19:58 218-01-902/15/19 10:13408 54.4 1
Dibenz(a,h)anthracene ND ug/kg 02/15/19 19:58 53-70-302/15/19 10:13408 86.6 1
Dibenzofuran ND ug/kg 02/15/19 19:58 132-64-902/15/19 10:13408 66.8 1
1,2-Dichlorobenzene ND ug/kg 02/15/19 19:58 95-50-102/15/19 10:13408 109 1
1,3-Dichlorobenzene ND ug/kg 02/15/19 19:58 541-73-102/15/19 10:13408 92.8 1
1,4-Dichlorobenzene ND ug/kg 02/15/19 19:58 106-46-702/15/19 10:13408 115 1
3,3'-Dichlorobenzidine ND ug/kg 02/15/19 19:58 91-94-102/15/19 10:132040 89.1 1
2,4-Dichlorophenol ND ug/kg 02/15/19 19:58 120-83-202/15/19 10:13408 89.1 1
Diethylphthalate ND ug/kg 02/15/19 19:58 84-66-202/15/19 10:13408 63.1 1
2,4-Dimethylphenol ND ug/kg 02/15/19 19:58 105-67-902/15/19 10:13408 161 1
Dimethylphthalate ND ug/kg 02/15/19 19:58 131-11-302/15/19 10:13408 82.9 1
Di-n-butylphthalate ND ug/kg 02/15/19 19:58 84-74-202/15/19 10:13408 66.8 1
4,6-Dinitro-2-methylphenol ND ug/kg 02/15/19 19:58 534-52-102/15/19 10:13817 81.7 1
2,4-Dinitrophenol ND ug/kg 02/15/19 19:58 51-28-502/15/19 10:132040 66.8 1
2,4-Dinitrotoluene ND ug/kg 02/15/19 19:58 121-14-202/15/19 10:13408 76.7 1
2,6-Dinitrotoluene ND ug/kg 02/15/19 19:58 606-20-202/15/19 10:13408 85.4 1
Di-n-octylphthalate ND ug/kg 02/15/19 19:58 117-84-002/15/19 10:13408 85.4 1
bis(2-Ethylhexyl)phthalate ND ug/kg 02/15/19 19:58 117-81-702/15/19 10:13408 111 1
Fluoranthene ND ug/kg 02/15/19 19:58 206-44-002/15/19 10:13408 59.4 1
Fluorene ND ug/kg 02/15/19 19:58 86-73-702/15/19 10:13408 84.1 1
Hexachloro-1,3-butadiene ND ug/kg 02/15/19 19:58 87-68-302/15/19 10:13408 70.5 1
Hexachlorobenzene ND ug/kg 02/15/19 19:58 118-74-102/15/19 10:13408 52.0 1
Hexachlorocyclopentadiene ND ug/kg 02/15/19 19:58 77-47-402/15/19 10:13408 75.5 1
Hexachloroethane ND ug/kg 02/15/19 19:58 67-72-102/15/19 10:13408 108 1
Indeno(1,2,3-cd)pyrene ND ug/kg 02/15/19 19:58 193-39-502/15/19 10:13408 84.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-9 (0-2)Lab ID: 92417206009 Collected: 02/08/19 14:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 02/15/19 19:58 78-59-102/15/19 10:13408 91.5 1
1-Methylnaphthalene ND ug/kg 02/15/19 19:58 90-12-002/15/19 10:13408 106 1
2-Methylnaphthalene ND ug/kg 02/15/19 19:58 91-57-602/15/19 10:13408 87.8 1
2-Methylphenol(o-Cresol)ND ug/kg 02/15/19 19:58 95-48-702/15/19 10:13408 124 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/15/19 19:58 15831-10-402/15/19 10:13408 161 1
Naphthalene ND ug/kg 02/15/19 19:58 91-20-302/15/19 10:13408 100 1
2-Nitroaniline ND ug/kg 02/15/19 19:58 88-74-402/15/19 10:132040 126 1
3-Nitroaniline ND ug/kg 02/15/19 19:58 99-09-202/15/19 10:132040 111 1
4-Nitroaniline ND ug/kg 02/15/19 19:58 100-01-602/15/19 10:13817 115 1
Nitrobenzene ND ug/kg 02/15/19 19:58 98-95-302/15/19 10:13408 111 1
2-Nitrophenol ND ug/kg 02/15/19 19:58 88-75-502/15/19 10:13408 99.0 1
4-Nitrophenol ND ug/kg 02/15/19 19:58 100-02-702/15/19 10:132040 73.0 1
N-Nitrosodimethylamine ND ug/kg 02/15/19 19:58 62-75-902/15/19 10:13408 132 1
N-Nitroso-di-n-propylamine ND ug/kg 02/15/19 19:58 621-64-702/15/19 10:13408 77.9 1
N-Nitrosodiphenylamine ND ug/kg 02/15/19 19:58 86-30-602/15/19 10:13408 121 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/15/19 19:58 108-60-102/15/19 10:13408 109 1
Pentachlorophenol ND ug/kg 02/15/19 19:58 87-86-502/15/19 10:132040 74.2 1
Phenanthrene ND ug/kg 02/15/19 19:58 85-01-802/15/19 10:13408 68.0 1
Phenol ND ug/kg 02/15/19 19:58 108-95-202/15/19 10:13408 122 1
Pyrene ND ug/kg 02/15/19 19:58 129-00-002/15/19 10:13408 69.3 1
1,2,4-Trichlorobenzene ND ug/kg 02/15/19 19:58 120-82-102/15/19 10:13408 79.2 1
2,4,5-Trichlorophenol ND ug/kg 02/15/19 19:58 95-95-402/15/19 10:13408 126 1
2,4,6-Trichlorophenol ND ug/kg 02/15/19 19:58 88-06-202/15/19 10:13408 90.3 1
Surrogates
Nitrobenzene-d5 (S)50 %02/15/19 19:58 4165-60-002/15/19 10:1323-110 1
2-Fluorobiphenyl (S)51 %02/15/19 19:58 321-60-802/15/19 10:1330-110 1
Terphenyl-d14 (S)58 %02/15/19 19:58 1718-51-002/15/19 10:1328-110 1
Phenol-d6 (S)47 %02/15/19 19:58 13127-88-302/15/19 10:1322-110 1
2-Fluorophenol (S)42 %02/15/19 19:58 367-12-402/15/19 10:1313-110 1
2,4,6-Tribromophenol (S)52 %02/15/19 19:58 118-79-602/15/19 10:1327-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 58.8J ug/kg 02/11/19 19:09 67-64-102/11/19 13:37107 10.7 1
Benzene ND ug/kg 02/11/19 19:09 71-43-202/11/19 13:375.3 1.7 1
Bromobenzene ND ug/kg 02/11/19 19:09 108-86-102/11/19 13:375.3 2.1 1
Bromochloromethane ND ug/kg 02/11/19 19:09 74-97-502/11/19 13:375.3 1.8 1
Bromodichloromethane ND ug/kg 02/11/19 19:09 75-27-402/11/19 13:375.3 2.0 1
Bromoform ND ug/kg 02/11/19 19:09 75-25-202/11/19 13:375.3 2.5 1
Bromomethane ND ug/kg 02/11/19 19:09 74-83-902/11/19 13:3710.7 2.7 1
2-Butanone (MEK)ND ug/kg 02/11/19 19:09 78-93-302/11/19 13:37107 3.1 1
n-Butylbenzene ND ug/kg 02/11/19 19:09 104-51-802/11/19 13:375.3 1.9 1
sec-Butylbenzene ND ug/kg 02/11/19 19:09 135-98-802/11/19 13:375.3 1.7 1
tert-Butylbenzene ND ug/kg 02/11/19 19:09 98-06-602/11/19 13:375.3 2.1 1
Carbon tetrachloride ND ug/kg 02/11/19 19:09 56-23-502/11/19 13:375.3 2.8 1
Chlorobenzene ND ug/kg 02/11/19 19:09 108-90-702/11/19 13:375.3 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-9 (0-2)Lab ID: 92417206009 Collected: 02/08/19 14:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 02/11/19 19:09 75-00-302/11/19 13:3710.7 2.6 1
Chloroform ND ug/kg 02/11/19 19:09 67-66-302/11/19 13:375.3 1.7 1
Chloromethane ND ug/kg 02/11/19 19:09 74-87-302/11/19 13:3710.7 2.6 1
2-Chlorotoluene ND ug/kg 02/11/19 19:09 95-49-802/11/19 13:375.3 1.8 1
4-Chlorotoluene ND ug/kg 02/11/19 19:09 106-43-402/11/19 13:375.3 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/11/19 19:09 96-12-802/11/19 13:375.3 3.8 1
Dibromochloromethane ND ug/kg 02/11/19 19:09 124-48-102/11/19 13:375.3 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 02/11/19 19:09 106-93-402/11/19 13:375.3 1.9 1
Dibromomethane ND ug/kg 02/11/19 19:09 74-95-302/11/19 13:375.3 2.7 1
1,2-Dichlorobenzene ND ug/kg 02/11/19 19:09 95-50-102/11/19 13:375.3 2.0 1
1,3-Dichlorobenzene ND ug/kg 02/11/19 19:09 541-73-102/11/19 13:375.3 2.1 1
1,4-Dichlorobenzene ND ug/kg 02/11/19 19:09 106-46-702/11/19 13:375.3 1.8 1
Dichlorodifluoromethane ND ug/kg 02/11/19 19:09 75-71-802/11/19 13:3710.7 3.8 1
1,1-Dichloroethane ND ug/kg 02/11/19 19:09 75-34-302/11/19 13:375.3 1.6 1
1,2-Dichloroethane ND ug/kg 02/11/19 19:09 107-06-202/11/19 13:375.3 2.3 1
1,1-Dichloroethene ND ug/kg 02/11/19 19:09 75-35-402/11/19 13:375.3 1.9 1
cis-1,2-Dichloroethene ND ug/kg 02/11/19 19:09 156-59-202/11/19 13:375.3 1.5 1
trans-1,2-Dichloroethene ND ug/kg 02/11/19 19:09 156-60-502/11/19 13:375.3 2.0 1
1,2-Dichloropropane ND ug/kg 02/11/19 19:09 78-87-502/11/19 13:375.3 1.8 1
1,3-Dichloropropane ND ug/kg 02/11/19 19:09 142-28-902/11/19 13:375.3 2.0 1
2,2-Dichloropropane ND ug/kg 02/11/19 19:09 594-20-702/11/19 13:375.3 1.8 1
1,1-Dichloropropene ND ug/kg 02/11/19 19:09 563-58-602/11/19 13:375.3 1.6 1
cis-1,3-Dichloropropene ND ug/kg 02/11/19 19:09 10061-01-502/11/19 13:375.3 1.9 1
trans-1,3-Dichloropropene ND ug/kg 02/11/19 19:09 10061-02-602/11/19 13:375.3 1.6 1
Diisopropyl ether ND ug/kg 02/11/19 19:09 108-20-302/11/19 13:375.3 1.8 1
Ethylbenzene ND ug/kg 02/11/19 19:09 100-41-402/11/19 13:375.3 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 02/11/19 19:09 87-68-302/11/19 13:375.3 2.1 1
2-Hexanone ND ug/kg 02/11/19 19:09 591-78-602/11/19 13:3753.3 4.2 1
Isopropylbenzene (Cumene)ND ug/kg 02/11/19 19:09 98-82-802/11/19 13:375.3 2.0 1
p-Isopropyltoluene ND ug/kg 02/11/19 19:09 99-87-602/11/19 13:375.3 1.8 1
Methylene Chloride ND ug/kg 02/11/19 19:09 75-09-202/11/19 13:3721.3 3.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/11/19 19:09 108-10-102/11/19 13:3753.3 3.9 1
Methyl-tert-butyl ether ND ug/kg 02/11/19 19:09 1634-04-402/11/19 13:375.3 1.6 1
Naphthalene ND ug/kg 02/11/19 19:09 91-20-302/11/19 13:375.3 1.3 1
n-Propylbenzene ND ug/kg 02/11/19 19:09 103-65-102/11/19 13:375.3 1.8 1
Styrene ND ug/kg 02/11/19 19:09 100-42-502/11/19 13:375.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/11/19 19:09 630-20-602/11/19 13:375.3 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/11/19 19:09 79-34-502/11/19 13:375.3 2.0 1
Tetrachloroethene ND ug/kg 02/11/19 19:09 127-18-402/11/19 13:375.3 1.8 1
Toluene ND ug/kg 02/11/19 19:09 108-88-302/11/19 13:375.3 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 02/11/19 19:09 87-61-602/11/19 13:375.3 2.3 1
1,2,4-Trichlorobenzene ND ug/kg 02/11/19 19:09 120-82-102/11/19 13:375.3 1.7 1
1,1,1-Trichloroethane ND ug/kg 02/11/19 19:09 71-55-602/11/19 13:375.3 1.9 1
1,1,2-Trichloroethane ND ug/kg 02/11/19 19:09 79-00-502/11/19 13:375.3 2.2 1
Trichloroethene ND ug/kg 02/11/19 19:09 79-01-602/11/19 13:375.3 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-9 (0-2)Lab ID: 92417206009 Collected: 02/08/19 14:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 02/11/19 19:09 75-69-402/11/19 13:375.3 2.3 1
1,2,3-Trichloropropane ND ug/kg 02/11/19 19:09 96-18-402/11/19 13:375.3 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 02/11/19 19:09 95-63-602/11/19 13:375.3 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 02/11/19 19:09 108-67-802/11/19 13:375.3 1.9 1
Vinyl acetate ND ug/kg 02/11/19 19:09 108-05-402/11/19 13:3753.3 9.4 1
Vinyl chloride ND ug/kg 02/11/19 19:09 75-01-402/11/19 13:3710.7 1.9 1
Xylene (Total)ND ug/kg 02/11/19 19:09 1330-20-702/11/19 13:3710.7 3.8 1
m&p-Xylene ND ug/kg 02/11/19 19:09 179601-23-102/11/19 13:3710.7 3.8 1
o-Xylene ND ug/kg 02/11/19 19:09 95-47-602/11/19 13:375.3 2.0 1
Surrogates
Toluene-d8 (S)100 %02/11/19 19:09 2037-26-502/11/19 13:3770-130 1
4-Bromofluorobenzene (S)101 %02/11/19 19:09 460-00-402/11/19 13:3770-130 1
1,2-Dichloroethane-d4 (S)95 %02/11/19 19:09 17060-07-002/11/19 13:3770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.2 %02/11/19 17:160.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-10 (0-2)Lab ID: 92417206010 Collected: 02/08/19 14:30 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 02/15/19 20:31 83-32-902/15/19 10:13425 97.8 1
Acenaphthylene ND ug/kg 02/15/19 20:31 208-96-802/15/19 10:13425 100 1
Aniline ND ug/kg 02/15/19 20:31 62-53-302/15/19 10:13425 114 1
Anthracene ND ug/kg 02/15/19 20:31 120-12-702/15/19 10:13425 95.2 1
Benzo(a)anthracene ND ug/kg 02/15/19 20:31 56-55-302/15/19 10:13425 78.5 1
Benzo(a)pyrene ND ug/kg 02/15/19 20:31 50-32-802/15/19 10:13425 81.0 1
Benzo(b)fluoranthene ND ug/kg 02/15/19 20:31 205-99-202/15/19 10:13425 73.3 1
Benzo(g,h,i)perylene ND ug/kg 02/15/19 20:31 191-24-202/15/19 10:13425 108 1
Benzo(k)fluoranthene ND ug/kg 02/15/19 20:31 207-08-902/15/19 10:13425 83.6 1
Benzoic Acid ND ug/kg 02/15/19 20:31 65-85-002/15/19 10:132120 77.2 1
Benzyl alcohol ND ug/kg 02/15/19 20:31 100-51-602/15/19 10:13849 84.9 1
4-Bromophenylphenyl ether ND ug/kg 02/15/19 20:31 101-55-302/15/19 10:13425 77.2 1
Butylbenzylphthalate ND ug/kg 02/15/19 20:31 85-68-702/15/19 10:13425 90.1 1
4-Chloro-3-methylphenol ND ug/kg 02/15/19 20:31 59-50-702/15/19 10:13849 87.5 1
4-Chloroaniline ND ug/kg 02/15/19 20:31 106-47-802/15/19 10:132120 118 1
bis(2-Chloroethoxy)methane ND ug/kg 02/15/19 20:31 111-91-102/15/19 10:13425 99.1 1
bis(2-Chloroethyl) ether ND ug/kg 02/15/19 20:31 111-44-402/15/19 10:13425 108 1
2-Chloronaphthalene ND ug/kg 02/15/19 20:31 91-58-702/15/19 10:13425 83.6 1
2-Chlorophenol ND ug/kg 02/15/19 20:31 95-57-802/15/19 10:13425 116 1
4-Chlorophenylphenyl ether ND ug/kg 02/15/19 20:31 7005-72-302/15/19 10:13425 87.5 1
Chrysene ND ug/kg 02/15/19 20:31 218-01-902/15/19 10:13425 56.6 1
Dibenz(a,h)anthracene ND ug/kg 02/15/19 20:31 53-70-302/15/19 10:13425 90.1 1
Dibenzofuran ND ug/kg 02/15/19 20:31 132-64-902/15/19 10:13425 69.5 1
1,2-Dichlorobenzene ND ug/kg 02/15/19 20:31 95-50-102/15/19 10:13425 113 1
1,3-Dichlorobenzene ND ug/kg 02/15/19 20:31 541-73-102/15/19 10:13425 96.5 1
1,4-Dichlorobenzene ND ug/kg 02/15/19 20:31 106-46-702/15/19 10:13425 120 1
3,3'-Dichlorobenzidine ND ug/kg 02/15/19 20:31 91-94-102/15/19 10:132120 92.6 1
2,4-Dichlorophenol ND ug/kg 02/15/19 20:31 120-83-202/15/19 10:13425 92.6 1
Diethylphthalate ND ug/kg 02/15/19 20:31 84-66-202/15/19 10:13425 65.6 1
2,4-Dimethylphenol ND ug/kg 02/15/19 20:31 105-67-902/15/19 10:13425 167 1
Dimethylphthalate ND ug/kg 02/15/19 20:31 131-11-302/15/19 10:13425 86.2 1
Di-n-butylphthalate ND ug/kg 02/15/19 20:31 84-74-202/15/19 10:13425 69.5 1
4,6-Dinitro-2-methylphenol ND ug/kg 02/15/19 20:31 534-52-102/15/19 10:13849 84.9 1
2,4-Dinitrophenol ND ug/kg 02/15/19 20:31 51-28-502/15/19 10:132120 69.5 1
2,4-Dinitrotoluene ND ug/kg 02/15/19 20:31 121-14-202/15/19 10:13425 79.8 1
2,6-Dinitrotoluene ND ug/kg 02/15/19 20:31 606-20-202/15/19 10:13425 88.8 1
Di-n-octylphthalate ND ug/kg 02/15/19 20:31 117-84-002/15/19 10:13425 88.8 1
bis(2-Ethylhexyl)phthalate ND ug/kg 02/15/19 20:31 117-81-702/15/19 10:13425 116 1
Fluoranthene ND ug/kg 02/15/19 20:31 206-44-002/15/19 10:13425 61.7 1
Fluorene ND ug/kg 02/15/19 20:31 86-73-702/15/19 10:13425 87.5 1
Hexachloro-1,3-butadiene ND ug/kg 02/15/19 20:31 87-68-302/15/19 10:13425 73.3 1
Hexachlorobenzene ND ug/kg 02/15/19 20:31 118-74-102/15/19 10:13425 54.0 1
Hexachlorocyclopentadiene ND ug/kg 02/15/19 20:31 77-47-402/15/19 10:13425 78.5 1
Hexachloroethane ND ug/kg 02/15/19 20:31 67-72-102/15/19 10:13425 112 1
Indeno(1,2,3-cd)pyrene ND ug/kg 02/15/19 20:31 193-39-502/15/19 10:13425 87.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-10 (0-2)Lab ID: 92417206010 Collected: 02/08/19 14:30 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 02/15/19 20:31 78-59-102/15/19 10:13425 95.2 1
1-Methylnaphthalene ND ug/kg 02/15/19 20:31 90-12-002/15/19 10:13425 111 1
2-Methylnaphthalene ND ug/kg 02/15/19 20:31 91-57-602/15/19 10:13425 91.3 1
2-Methylphenol(o-Cresol)ND ug/kg 02/15/19 20:31 95-48-702/15/19 10:13425 129 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/15/19 20:31 15831-10-402/15/19 10:13425 167 1
Naphthalene ND ug/kg 02/15/19 20:31 91-20-302/15/19 10:13425 104 1
2-Nitroaniline ND ug/kg 02/15/19 20:31 88-74-402/15/19 10:132120 131 1
3-Nitroaniline ND ug/kg 02/15/19 20:31 99-09-202/15/19 10:132120 116 1
4-Nitroaniline ND ug/kg 02/15/19 20:31 100-01-602/15/19 10:13849 120 1
Nitrobenzene ND ug/kg 02/15/19 20:31 98-95-302/15/19 10:13425 116 1
2-Nitrophenol ND ug/kg 02/15/19 20:31 88-75-502/15/19 10:13425 103 1
4-Nitrophenol ND ug/kg 02/15/19 20:31 100-02-702/15/19 10:132120 75.9 1
N-Nitrosodimethylamine ND ug/kg 02/15/19 20:31 62-75-902/15/19 10:13425 138 1
N-Nitroso-di-n-propylamine ND ug/kg 02/15/19 20:31 621-64-702/15/19 10:13425 81.0 1
N-Nitrosodiphenylamine ND ug/kg 02/15/19 20:31 86-30-602/15/19 10:13425 126 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/15/19 20:31 108-60-102/15/19 10:13425 113 1
Pentachlorophenol ND ug/kg 02/15/19 20:31 87-86-502/15/19 10:132120 77.2 1
Phenanthrene ND ug/kg 02/15/19 20:31 85-01-802/15/19 10:13425 70.8 1
Phenol ND ug/kg 02/15/19 20:31 108-95-202/15/19 10:13425 127 1
Pyrene ND ug/kg 02/15/19 20:31 129-00-002/15/19 10:13425 72.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/15/19 20:31 120-82-102/15/19 10:13425 82.3 1
2,4,5-Trichlorophenol ND ug/kg 02/15/19 20:31 95-95-402/15/19 10:13425 131 1
2,4,6-Trichlorophenol ND ug/kg 02/15/19 20:31 88-06-202/15/19 10:13425 93.9 1
Surrogates
Nitrobenzene-d5 (S)55 %02/15/19 20:31 4165-60-002/15/19 10:1323-110 1
2-Fluorobiphenyl (S)58 %02/15/19 20:31 321-60-802/15/19 10:1330-110 1
Terphenyl-d14 (S)64 %02/15/19 20:31 1718-51-002/15/19 10:1328-110 1
Phenol-d6 (S)50 %02/15/19 20:31 13127-88-302/15/19 10:1322-110 1
2-Fluorophenol (S)45 %02/15/19 20:31 367-12-402/15/19 10:1313-110 1
2,4,6-Tribromophenol (S)60 %02/15/19 20:31 118-79-602/15/19 10:1327-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 31.3J ug/kg 02/11/19 19:28 67-64-102/11/19 13:3791.6 9.2 1
Benzene ND ug/kg 02/11/19 19:28 71-43-202/11/19 13:374.6 1.5 1
Bromobenzene ND ug/kg 02/11/19 19:28 108-86-102/11/19 13:374.6 1.8 1
Bromochloromethane ND ug/kg 02/11/19 19:28 74-97-502/11/19 13:374.6 1.6 1
Bromodichloromethane ND ug/kg 02/11/19 19:28 75-27-402/11/19 13:374.6 1.7 1
Bromoform ND ug/kg 02/11/19 19:28 75-25-202/11/19 13:374.6 2.1 1
Bromomethane ND ug/kg 02/11/19 19:28 74-83-902/11/19 13:379.2 2.3 1
2-Butanone (MEK)3.1J ug/kg 02/11/19 19:28 78-93-302/11/19 13:3791.6 2.7 1
n-Butylbenzene ND ug/kg 02/11/19 19:28 104-51-802/11/19 13:374.6 1.6 1
sec-Butylbenzene ND ug/kg 02/11/19 19:28 135-98-802/11/19 13:374.6 1.5 1
tert-Butylbenzene ND ug/kg 02/11/19 19:28 98-06-602/11/19 13:374.6 1.8 1
Carbon tetrachloride ND ug/kg 02/11/19 19:28 56-23-502/11/19 13:374.6 2.4 1
Chlorobenzene ND ug/kg 02/11/19 19:28 108-90-702/11/19 13:374.6 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-10 (0-2)Lab ID: 92417206010 Collected: 02/08/19 14:30 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 02/11/19 19:28 75-00-302/11/19 13:379.2 2.2 1
Chloroform ND ug/kg 02/11/19 19:28 67-66-302/11/19 13:374.6 1.5 1
Chloromethane ND ug/kg 02/11/19 19:28 74-87-302/11/19 13:379.2 2.2 1
2-Chlorotoluene ND ug/kg 02/11/19 19:28 95-49-802/11/19 13:374.6 1.6 1
4-Chlorotoluene ND ug/kg 02/11/19 19:28 106-43-402/11/19 13:374.6 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/11/19 19:28 96-12-802/11/19 13:374.6 3.3 1
Dibromochloromethane ND ug/kg 02/11/19 19:28 124-48-102/11/19 13:374.6 1.6 1
1,2-Dibromoethane (EDB)ND ug/kg 02/11/19 19:28 106-93-402/11/19 13:374.6 1.6 1
Dibromomethane ND ug/kg 02/11/19 19:28 74-95-302/11/19 13:374.6 2.3 1
1,2-Dichlorobenzene ND ug/kg 02/11/19 19:28 95-50-102/11/19 13:374.6 1.7 1
1,3-Dichlorobenzene ND ug/kg 02/11/19 19:28 541-73-102/11/19 13:374.6 1.8 1
1,4-Dichlorobenzene ND ug/kg 02/11/19 19:28 106-46-702/11/19 13:374.6 1.6 1
Dichlorodifluoromethane ND ug/kg 02/11/19 19:28 75-71-802/11/19 13:379.2 3.3 1
1,1-Dichloroethane ND ug/kg 02/11/19 19:28 75-34-302/11/19 13:374.6 1.4 1
1,2-Dichloroethane ND ug/kg 02/11/19 19:28 107-06-202/11/19 13:374.6 2.0 1
1,1-Dichloroethene ND ug/kg 02/11/19 19:28 75-35-402/11/19 13:374.6 1.6 1
cis-1,2-Dichloroethene ND ug/kg 02/11/19 19:28 156-59-202/11/19 13:374.6 1.3 1
trans-1,2-Dichloroethene ND ug/kg 02/11/19 19:28 156-60-502/11/19 13:374.6 1.7 1
1,2-Dichloropropane ND ug/kg 02/11/19 19:28 78-87-502/11/19 13:374.6 1.6 1
1,3-Dichloropropane ND ug/kg 02/11/19 19:28 142-28-902/11/19 13:374.6 1.7 1
2,2-Dichloropropane ND ug/kg 02/11/19 19:28 594-20-702/11/19 13:374.6 1.6 1
1,1-Dichloropropene ND ug/kg 02/11/19 19:28 563-58-602/11/19 13:374.6 1.4 1
cis-1,3-Dichloropropene ND ug/kg 02/11/19 19:28 10061-01-502/11/19 13:374.6 1.6 1
trans-1,3-Dichloropropene ND ug/kg 02/11/19 19:28 10061-02-602/11/19 13:374.6 1.4 1
Diisopropyl ether ND ug/kg 02/11/19 19:28 108-20-302/11/19 13:374.6 1.6 1
Ethylbenzene ND ug/kg 02/11/19 19:28 100-41-402/11/19 13:374.6 1.6 1
Hexachloro-1,3-butadiene ND ug/kg 02/11/19 19:28 87-68-302/11/19 13:374.6 1.8 1
2-Hexanone ND ug/kg 02/11/19 19:28 591-78-602/11/19 13:3745.8 3.6 1
Isopropylbenzene (Cumene)ND ug/kg 02/11/19 19:28 98-82-802/11/19 13:374.6 1.7 1
p-Isopropyltoluene ND ug/kg 02/11/19 19:28 99-87-602/11/19 13:374.6 1.6 1
Methylene Chloride ND ug/kg 02/11/19 19:28 75-09-202/11/19 13:3718.3 2.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/11/19 19:28 108-10-102/11/19 13:3745.8 3.4 1
Methyl-tert-butyl ether ND ug/kg 02/11/19 19:28 1634-04-402/11/19 13:374.6 1.4 1
Naphthalene ND ug/kg 02/11/19 19:28 91-20-302/11/19 13:374.6 1.1 1
n-Propylbenzene ND ug/kg 02/11/19 19:28 103-65-102/11/19 13:374.6 1.6 1
Styrene ND ug/kg 02/11/19 19:28 100-42-502/11/19 13:374.6 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/11/19 19:28 630-20-602/11/19 13:374.6 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/11/19 19:28 79-34-502/11/19 13:374.6 1.7 1
Tetrachloroethene ND ug/kg 02/11/19 19:28 127-18-402/11/19 13:374.6 1.6 1
Toluene ND ug/kg 02/11/19 19:28 108-88-302/11/19 13:374.6 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 02/11/19 19:28 87-61-602/11/19 13:374.6 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 02/11/19 19:28 120-82-102/11/19 13:374.6 1.5 1
1,1,1-Trichloroethane ND ug/kg 02/11/19 19:28 71-55-602/11/19 13:374.6 1.6 1
1,1,2-Trichloroethane ND ug/kg 02/11/19 19:28 79-00-502/11/19 13:374.6 1.9 1
Trichloroethene ND ug/kg 02/11/19 19:28 79-01-602/11/19 13:374.6 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-10 (0-2)Lab ID: 92417206010 Collected: 02/08/19 14:30 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 02/11/19 19:28 75-69-402/11/19 13:374.6 2.0 1
1,2,3-Trichloropropane ND ug/kg 02/11/19 19:28 96-18-402/11/19 13:374.6 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 02/11/19 19:28 95-63-602/11/19 13:374.6 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 02/11/19 19:28 108-67-802/11/19 13:374.6 1.6 1
Vinyl acetate ND ug/kg 02/11/19 19:28 108-05-402/11/19 13:3745.8 8.1 1
Vinyl chloride ND ug/kg 02/11/19 19:28 75-01-402/11/19 13:379.2 1.6 1
Xylene (Total)ND ug/kg 02/11/19 19:28 1330-20-702/11/19 13:379.2 3.3 1
m&p-Xylene ND ug/kg 02/11/19 19:28 179601-23-102/11/19 13:379.2 3.3 1
o-Xylene ND ug/kg 02/11/19 19:28 95-47-602/11/19 13:374.6 1.7 1
Surrogates
Toluene-d8 (S)99 %02/11/19 19:28 2037-26-502/11/19 13:3770-130 1
4-Bromofluorobenzene (S)99 %02/11/19 19:28 460-00-402/11/19 13:3770-130 1
1,2-Dichloroethane-d4 (S)92 %02/11/19 19:28 17060-07-002/11/19 13:3770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.5 %02/11/19 17:160.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-11 (0-2)Lab ID: 92417206011 Collected: 02/08/19 15:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 02/15/19 21:06 83-32-902/15/19 10:13406 93.4 1
Acenaphthylene ND ug/kg 02/15/19 21:06 208-96-802/15/19 10:13406 95.9 1
Aniline ND ug/kg 02/15/19 21:06 62-53-302/15/19 10:13406 109 1
Anthracene ND ug/kg 02/15/19 21:06 120-12-702/15/19 10:13406 91.0 1
Benzo(a)anthracene ND ug/kg 02/15/19 21:06 56-55-302/15/19 10:13406 75.0 1
Benzo(a)pyrene ND ug/kg 02/15/19 21:06 50-32-802/15/19 10:13406 77.4 1
Benzo(b)fluoranthene ND ug/kg 02/15/19 21:06 205-99-202/15/19 10:13406 70.1 1
Benzo(g,h,i)perylene ND ug/kg 02/15/19 21:06 191-24-202/15/19 10:13406 103 1
Benzo(k)fluoranthene ND ug/kg 02/15/19 21:06 207-08-902/15/19 10:13406 79.9 1
Benzoic Acid ND ug/kg 02/15/19 21:06 65-85-002/15/19 10:132030 73.8 1
Benzyl alcohol ND ug/kg 02/15/19 21:06 100-51-602/15/19 10:13811 81.1 1
4-Bromophenylphenyl ether ND ug/kg 02/15/19 21:06 101-55-302/15/19 10:13406 73.8 1
Butylbenzylphthalate ND ug/kg 02/15/19 21:06 85-68-702/15/19 10:13406 86.0 1
4-Chloro-3-methylphenol ND ug/kg 02/15/19 21:06 59-50-702/15/19 10:13811 83.6 1
4-Chloroaniline ND ug/kg 02/15/19 21:06 106-47-802/15/19 10:132030 113 1
bis(2-Chloroethoxy)methane ND ug/kg 02/15/19 21:06 111-91-102/15/19 10:13406 94.7 1
bis(2-Chloroethyl) ether ND ug/kg 02/15/19 21:06 111-44-402/15/19 10:13406 103 1
2-Chloronaphthalene ND ug/kg 02/15/19 21:06 91-58-702/15/19 10:13406 79.9 1
2-Chlorophenol ND ug/kg 02/15/19 21:06 95-57-802/15/19 10:13406 111 1
4-Chlorophenylphenyl ether ND ug/kg 02/15/19 21:06 7005-72-302/15/19 10:13406 83.6 1
Chrysene ND ug/kg 02/15/19 21:06 218-01-902/15/19 10:13406 54.1 1
Dibenz(a,h)anthracene ND ug/kg 02/15/19 21:06 53-70-302/15/19 10:13406 86.0 1
Dibenzofuran ND ug/kg 02/15/19 21:06 132-64-902/15/19 10:13406 66.4 1
1,2-Dichlorobenzene ND ug/kg 02/15/19 21:06 95-50-102/15/19 10:13406 108 1
1,3-Dichlorobenzene ND ug/kg 02/15/19 21:06 541-73-102/15/19 10:13406 92.2 1
1,4-Dichlorobenzene ND ug/kg 02/15/19 21:06 106-46-702/15/19 10:13406 114 1
3,3'-Dichlorobenzidine ND ug/kg 02/15/19 21:06 91-94-102/15/19 10:132030 88.5 1
2,4-Dichlorophenol ND ug/kg 02/15/19 21:06 120-83-202/15/19 10:13406 88.5 1
Diethylphthalate ND ug/kg 02/15/19 21:06 84-66-202/15/19 10:13406 62.7 1
2,4-Dimethylphenol ND ug/kg 02/15/19 21:06 105-67-902/15/19 10:13406 160 1
Dimethylphthalate ND ug/kg 02/15/19 21:06 131-11-302/15/19 10:13406 82.4 1
Di-n-butylphthalate ND ug/kg 02/15/19 21:06 84-74-202/15/19 10:13406 66.4 1
4,6-Dinitro-2-methylphenol ND ug/kg 02/15/19 21:06 534-52-102/15/19 10:13811 81.1 1
2,4-Dinitrophenol ND ug/kg 02/15/19 21:06 51-28-502/15/19 10:132030 66.4 1
2,4-Dinitrotoluene ND ug/kg 02/15/19 21:06 121-14-202/15/19 10:13406 76.2 1
2,6-Dinitrotoluene ND ug/kg 02/15/19 21:06 606-20-202/15/19 10:13406 84.8 1
Di-n-octylphthalate ND ug/kg 02/15/19 21:06 117-84-002/15/19 10:13406 84.8 1
bis(2-Ethylhexyl)phthalate ND ug/kg 02/15/19 21:06 117-81-702/15/19 10:13406 111 1
Fluoranthene ND ug/kg 02/15/19 21:06 206-44-002/15/19 10:13406 59.0 1
Fluorene ND ug/kg 02/15/19 21:06 86-73-702/15/19 10:13406 83.6 1
Hexachloro-1,3-butadiene ND ug/kg 02/15/19 21:06 87-68-302/15/19 10:13406 70.1 1
Hexachlorobenzene ND ug/kg 02/15/19 21:06 118-74-102/15/19 10:13406 51.6 1
Hexachlorocyclopentadiene ND ug/kg 02/15/19 21:06 77-47-402/15/19 10:13406 75.0 1
Hexachloroethane ND ug/kg 02/15/19 21:06 67-72-102/15/19 10:13406 107 1
Indeno(1,2,3-cd)pyrene ND ug/kg 02/15/19 21:06 193-39-502/15/19 10:13406 83.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-11 (0-2)Lab ID: 92417206011 Collected: 02/08/19 15:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 02/15/19 21:06 78-59-102/15/19 10:13406 91.0 1
1-Methylnaphthalene ND ug/kg 02/15/19 21:06 90-12-002/15/19 10:13406 106 1
2-Methylnaphthalene ND ug/kg 02/15/19 21:06 91-57-602/15/19 10:13406 87.3 1
2-Methylphenol(o-Cresol)ND ug/kg 02/15/19 21:06 95-48-702/15/19 10:13406 123 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/15/19 21:06 15831-10-402/15/19 10:13406 160 1
Naphthalene ND ug/kg 02/15/19 21:06 91-20-302/15/19 10:13406 99.6 1
2-Nitroaniline ND ug/kg 02/15/19 21:06 88-74-402/15/19 10:132030 125 1
3-Nitroaniline ND ug/kg 02/15/19 21:06 99-09-202/15/19 10:132030 111 1
4-Nitroaniline ND ug/kg 02/15/19 21:06 100-01-602/15/19 10:13811 114 1
Nitrobenzene ND ug/kg 02/15/19 21:06 98-95-302/15/19 10:13406 111 1
2-Nitrophenol ND ug/kg 02/15/19 21:06 88-75-502/15/19 10:13406 98.3 1
4-Nitrophenol ND ug/kg 02/15/19 21:06 100-02-702/15/19 10:132030 72.5 1
N-Nitrosodimethylamine ND ug/kg 02/15/19 21:06 62-75-902/15/19 10:13406 132 1
N-Nitroso-di-n-propylamine ND ug/kg 02/15/19 21:06 621-64-702/15/19 10:13406 77.4 1
N-Nitrosodiphenylamine ND ug/kg 02/15/19 21:06 86-30-602/15/19 10:13406 120 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/15/19 21:06 108-60-102/15/19 10:13406 108 1
Pentachlorophenol ND ug/kg 02/15/19 21:06 87-86-502/15/19 10:132030 73.8 1
Phenanthrene ND ug/kg 02/15/19 21:06 85-01-802/15/19 10:13406 67.6 1
Phenol ND ug/kg 02/15/19 21:06 108-95-202/15/19 10:13406 122 1
Pyrene ND ug/kg 02/15/19 21:06 129-00-002/15/19 10:13406 68.8 1
1,2,4-Trichlorobenzene ND ug/kg 02/15/19 21:06 120-82-102/15/19 10:13406 78.7 1
2,4,5-Trichlorophenol ND ug/kg 02/15/19 21:06 95-95-402/15/19 10:13406 125 1
2,4,6-Trichlorophenol ND ug/kg 02/15/19 21:06 88-06-202/15/19 10:13406 89.7 1
Surrogates
Nitrobenzene-d5 (S)53 %02/15/19 21:06 4165-60-002/15/19 10:1323-110 1
2-Fluorobiphenyl (S)54 %02/15/19 21:06 321-60-802/15/19 10:1330-110 1
Terphenyl-d14 (S)74 %02/15/19 21:06 1718-51-002/15/19 10:1328-110 1
Phenol-d6 (S)46 %02/15/19 21:06 13127-88-302/15/19 10:1322-110 1
2-Fluorophenol (S)41 %02/15/19 21:06 367-12-402/15/19 10:1313-110 1
2,4,6-Tribromophenol (S)56 %02/15/19 21:06 118-79-602/15/19 10:1327-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 40.6J ug/kg 02/11/19 19:47 67-64-102/11/19 13:37100 10.0 1
Benzene ND ug/kg 02/11/19 19:47 71-43-202/11/19 13:375.0 1.6 1
Bromobenzene ND ug/kg 02/11/19 19:47 108-86-102/11/19 13:375.0 2.0 1
Bromochloromethane ND ug/kg 02/11/19 19:47 74-97-502/11/19 13:375.0 1.7 1
Bromodichloromethane ND ug/kg 02/11/19 19:47 75-27-402/11/19 13:375.0 1.9 1
Bromoform ND ug/kg 02/11/19 19:47 75-25-202/11/19 13:375.0 2.3 1
Bromomethane ND ug/kg 02/11/19 19:47 74-83-902/11/19 13:3710.0 2.5 1
2-Butanone (MEK)ND ug/kg 02/11/19 19:47 78-93-302/11/19 13:37100 2.9 1
n-Butylbenzene ND ug/kg 02/11/19 19:47 104-51-802/11/19 13:375.0 1.8 1
sec-Butylbenzene ND ug/kg 02/11/19 19:47 135-98-802/11/19 13:375.0 1.6 1
tert-Butylbenzene ND ug/kg 02/11/19 19:47 98-06-602/11/19 13:375.0 2.0 1
Carbon tetrachloride ND ug/kg 02/11/19 19:47 56-23-502/11/19 13:375.0 2.6 1
Chlorobenzene ND ug/kg 02/11/19 19:47 108-90-702/11/19 13:375.0 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-11 (0-2)Lab ID: 92417206011 Collected: 02/08/19 15:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 02/11/19 19:47 75-00-302/11/19 13:3710.0 2.4 1
Chloroform ND ug/kg 02/11/19 19:47 67-66-302/11/19 13:375.0 1.6 1
Chloromethane ND ug/kg 02/11/19 19:47 74-87-302/11/19 13:3710.0 2.4 1
2-Chlorotoluene ND ug/kg 02/11/19 19:47 95-49-802/11/19 13:375.0 1.7 1
4-Chlorotoluene ND ug/kg 02/11/19 19:47 106-43-402/11/19 13:375.0 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/11/19 19:47 96-12-802/11/19 13:375.0 3.6 1
Dibromochloromethane ND ug/kg 02/11/19 19:47 124-48-102/11/19 13:375.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 02/11/19 19:47 106-93-402/11/19 13:375.0 1.8 1
Dibromomethane ND ug/kg 02/11/19 19:47 74-95-302/11/19 13:375.0 2.5 1
1,2-Dichlorobenzene ND ug/kg 02/11/19 19:47 95-50-102/11/19 13:375.0 1.9 1
1,3-Dichlorobenzene ND ug/kg 02/11/19 19:47 541-73-102/11/19 13:375.0 2.0 1
1,4-Dichlorobenzene ND ug/kg 02/11/19 19:47 106-46-702/11/19 13:375.0 1.7 1
Dichlorodifluoromethane ND ug/kg 02/11/19 19:47 75-71-802/11/19 13:3710.0 3.6 1
1,1-Dichloroethane ND ug/kg 02/11/19 19:47 75-34-302/11/19 13:375.0 1.5 1
1,2-Dichloroethane ND ug/kg 02/11/19 19:47 107-06-202/11/19 13:375.0 2.2 1
1,1-Dichloroethene ND ug/kg 02/11/19 19:47 75-35-402/11/19 13:375.0 1.8 1
cis-1,2-Dichloroethene ND ug/kg 02/11/19 19:47 156-59-202/11/19 13:375.0 1.4 1
trans-1,2-Dichloroethene ND ug/kg 02/11/19 19:47 156-60-502/11/19 13:375.0 1.9 1
1,2-Dichloropropane ND ug/kg 02/11/19 19:47 78-87-502/11/19 13:375.0 1.7 1
1,3-Dichloropropane ND ug/kg 02/11/19 19:47 142-28-902/11/19 13:375.0 1.9 1
2,2-Dichloropropane ND ug/kg 02/11/19 19:47 594-20-702/11/19 13:375.0 1.7 1
1,1-Dichloropropene ND ug/kg 02/11/19 19:47 563-58-602/11/19 13:375.0 1.5 1
cis-1,3-Dichloropropene ND ug/kg 02/11/19 19:47 10061-01-502/11/19 13:375.0 1.8 1
trans-1,3-Dichloropropene ND ug/kg 02/11/19 19:47 10061-02-602/11/19 13:375.0 1.5 1
Diisopropyl ether ND ug/kg 02/11/19 19:47 108-20-302/11/19 13:375.0 1.7 1
Ethylbenzene ND ug/kg 02/11/19 19:47 100-41-402/11/19 13:375.0 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 02/11/19 19:47 87-68-302/11/19 13:375.0 2.0 1
2-Hexanone ND ug/kg 02/11/19 19:47 591-78-602/11/19 13:3750.0 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 02/11/19 19:47 98-82-802/11/19 13:375.0 1.9 1
p-Isopropyltoluene ND ug/kg 02/11/19 19:47 99-87-602/11/19 13:375.0 1.7 1
Methylene Chloride ND ug/kg 02/11/19 19:47 75-09-202/11/19 13:3720.0 3.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/11/19 19:47 108-10-102/11/19 13:3750.0 3.7 1
Methyl-tert-butyl ether ND ug/kg 02/11/19 19:47 1634-04-402/11/19 13:375.0 1.5 1
Naphthalene ND ug/kg 02/11/19 19:47 91-20-302/11/19 13:375.0 1.2 1
n-Propylbenzene ND ug/kg 02/11/19 19:47 103-65-102/11/19 13:375.0 1.7 1
Styrene ND ug/kg 02/11/19 19:47 100-42-502/11/19 13:375.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/11/19 19:47 630-20-602/11/19 13:375.0 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/11/19 19:47 79-34-502/11/19 13:375.0 1.9 1
Tetrachloroethene ND ug/kg 02/11/19 19:47 127-18-402/11/19 13:375.0 1.7 1
Toluene ND ug/kg 02/11/19 19:47 108-88-302/11/19 13:375.0 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 02/11/19 19:47 87-61-602/11/19 13:375.0 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 02/11/19 19:47 120-82-102/11/19 13:375.0 1.6 1
1,1,1-Trichloroethane ND ug/kg 02/11/19 19:47 71-55-602/11/19 13:375.0 1.8 1
1,1,2-Trichloroethane ND ug/kg 02/11/19 19:47 79-00-502/11/19 13:375.0 2.1 1
Trichloroethene ND ug/kg 02/11/19 19:47 79-01-602/11/19 13:375.0 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-11 (0-2)Lab ID: 92417206011 Collected: 02/08/19 15:00 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 02/11/19 19:47 75-69-402/11/19 13:375.0 2.2 1
1,2,3-Trichloropropane ND ug/kg 02/11/19 19:47 96-18-402/11/19 13:375.0 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 02/11/19 19:47 95-63-602/11/19 13:375.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/11/19 19:47 108-67-802/11/19 13:375.0 1.8 1
Vinyl acetate ND ug/kg 02/11/19 19:47 108-05-402/11/19 13:3750.0 8.8 1
Vinyl chloride ND ug/kg 02/11/19 19:47 75-01-402/11/19 13:3710.0 1.8 1
Xylene (Total)ND ug/kg 02/11/19 19:47 1330-20-702/11/19 13:3710.0 3.6 1
m&p-Xylene ND ug/kg 02/11/19 19:47 179601-23-102/11/19 13:3710.0 3.6 1
o-Xylene ND ug/kg 02/11/19 19:47 95-47-602/11/19 13:375.0 1.9 1
Surrogates
Toluene-d8 (S)98 %02/11/19 19:47 2037-26-502/11/19 13:3770-130 1
4-Bromofluorobenzene (S)99 %02/11/19 19:47 460-00-402/11/19 13:3770-130 1
1,2-Dichloroethane-d4 (S)99 %02/11/19 19:47 17060-07-002/11/19 13:3770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.4 %02/11/19 17:160.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-12 (0-2)Lab ID: 92417206012 Collected: 02/08/19 15:30 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 02/15/19 21:41 83-32-902/15/19 10:13432 99.4 1
Acenaphthylene ND ug/kg 02/15/19 21:41 208-96-802/15/19 10:13432 102 1
Aniline ND ug/kg 02/15/19 21:41 62-53-302/15/19 10:13432 116 1
Anthracene ND ug/kg 02/15/19 21:41 120-12-702/15/19 10:13432 96.8 1
Benzo(a)anthracene ND ug/kg 02/15/19 21:41 56-55-302/15/19 10:13432 79.8 1
Benzo(a)pyrene ND ug/kg 02/15/19 21:41 50-32-802/15/19 10:13432 82.4 1
Benzo(b)fluoranthene ND ug/kg 02/15/19 21:41 205-99-202/15/19 10:13432 74.6 1
Benzo(g,h,i)perylene ND ug/kg 02/15/19 21:41 191-24-202/15/19 10:13432 110 1
Benzo(k)fluoranthene ND ug/kg 02/15/19 21:41 207-08-902/15/19 10:13432 85.1 1
Benzoic Acid ND ug/kg 02/15/19 21:41 65-85-002/15/19 10:132160 78.5 1
Benzyl alcohol ND ug/kg 02/15/19 21:41 100-51-602/15/19 10:13864 86.4 1
4-Bromophenylphenyl ether ND ug/kg 02/15/19 21:41 101-55-302/15/19 10:13432 78.5 1
Butylbenzylphthalate ND ug/kg 02/15/19 21:41 85-68-702/15/19 10:13432 91.6 1
4-Chloro-3-methylphenol ND ug/kg 02/15/19 21:41 59-50-702/15/19 10:13864 89.0 1
4-Chloroaniline ND ug/kg 02/15/19 21:41 106-47-802/15/19 10:132160 120 1
bis(2-Chloroethoxy)methane ND ug/kg 02/15/19 21:41 111-91-102/15/19 10:13432 101 1
bis(2-Chloroethyl) ether ND ug/kg 02/15/19 21:41 111-44-402/15/19 10:13432 110 1
2-Chloronaphthalene ND ug/kg 02/15/19 21:41 91-58-702/15/19 10:13432 85.1 1
2-Chlorophenol ND ug/kg 02/15/19 21:41 95-57-802/15/19 10:13432 118 1
4-Chlorophenylphenyl ether ND ug/kg 02/15/19 21:41 7005-72-302/15/19 10:13432 89.0 1
Chrysene ND ug/kg 02/15/19 21:41 218-01-902/15/19 10:13432 57.6 1
Dibenz(a,h)anthracene ND ug/kg 02/15/19 21:41 53-70-302/15/19 10:13432 91.6 1
Dibenzofuran ND ug/kg 02/15/19 21:41 132-64-902/15/19 10:13432 70.7 1
1,2-Dichlorobenzene ND ug/kg 02/15/19 21:41 95-50-102/15/19 10:13432 115 1
1,3-Dichlorobenzene ND ug/kg 02/15/19 21:41 541-73-102/15/19 10:13432 98.1 1
1,4-Dichlorobenzene ND ug/kg 02/15/19 21:41 106-46-702/15/19 10:13432 122 1
3,3'-Dichlorobenzidine ND ug/kg 02/15/19 21:41 91-94-102/15/19 10:132160 94.2 1
2,4-Dichlorophenol ND ug/kg 02/15/19 21:41 120-83-202/15/19 10:13432 94.2 1
Diethylphthalate ND ug/kg 02/15/19 21:41 84-66-202/15/19 10:13432 66.7 1
2,4-Dimethylphenol ND ug/kg 02/15/19 21:41 105-67-902/15/19 10:13432 170 1
Dimethylphthalate ND ug/kg 02/15/19 21:41 131-11-302/15/19 10:13432 87.7 1
Di-n-butylphthalate ND ug/kg 02/15/19 21:41 84-74-202/15/19 10:13432 70.7 1
4,6-Dinitro-2-methylphenol ND ug/kg 02/15/19 21:41 534-52-102/15/19 10:13864 86.4 1
2,4-Dinitrophenol ND ug/kg 02/15/19 21:41 51-28-502/15/19 10:132160 70.7 1
2,4-Dinitrotoluene ND ug/kg 02/15/19 21:41 121-14-202/15/19 10:13432 81.1 1
2,6-Dinitrotoluene ND ug/kg 02/15/19 21:41 606-20-202/15/19 10:13432 90.3 1
Di-n-octylphthalate ND ug/kg 02/15/19 21:41 117-84-002/15/19 10:13432 90.3 1
bis(2-Ethylhexyl)phthalate ND ug/kg 02/15/19 21:41 117-81-702/15/19 10:13432 118 1
Fluoranthene ND ug/kg 02/15/19 21:41 206-44-002/15/19 10:13432 62.8 1
Fluorene ND ug/kg 02/15/19 21:41 86-73-702/15/19 10:13432 89.0 1
Hexachloro-1,3-butadiene ND ug/kg 02/15/19 21:41 87-68-302/15/19 10:13432 74.6 1
Hexachlorobenzene ND ug/kg 02/15/19 21:41 118-74-102/15/19 10:13432 55.0 1
Hexachlorocyclopentadiene ND ug/kg 02/15/19 21:41 77-47-402/15/19 10:13432 79.8 1
Hexachloroethane ND ug/kg 02/15/19 21:41 67-72-102/15/19 10:13432 114 1
Indeno(1,2,3-cd)pyrene ND ug/kg 02/15/19 21:41 193-39-502/15/19 10:13432 89.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
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Page 37 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-12 (0-2)Lab ID: 92417206012 Collected: 02/08/19 15:30 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 02/15/19 21:41 78-59-102/15/19 10:13432 96.8 1
1-Methylnaphthalene ND ug/kg 02/15/19 21:41 90-12-002/15/19 10:13432 113 1
2-Methylnaphthalene ND ug/kg 02/15/19 21:41 91-57-602/15/19 10:13432 92.9 1
2-Methylphenol(o-Cresol)ND ug/kg 02/15/19 21:41 95-48-702/15/19 10:13432 131 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/15/19 21:41 15831-10-402/15/19 10:13432 170 1
Naphthalene ND ug/kg 02/15/19 21:41 91-20-302/15/19 10:13432 106 1
2-Nitroaniline ND ug/kg 02/15/19 21:41 88-74-402/15/19 10:132160 133 1
3-Nitroaniline ND ug/kg 02/15/19 21:41 99-09-202/15/19 10:132160 118 1
4-Nitroaniline ND ug/kg 02/15/19 21:41 100-01-602/15/19 10:13864 122 1
Nitrobenzene ND ug/kg 02/15/19 21:41 98-95-302/15/19 10:13432 118 1
2-Nitrophenol ND ug/kg 02/15/19 21:41 88-75-502/15/19 10:13432 105 1
4-Nitrophenol ND ug/kg 02/15/19 21:41 100-02-702/15/19 10:132160 77.2 1
N-Nitrosodimethylamine ND ug/kg 02/15/19 21:41 62-75-902/15/19 10:13432 140 1
N-Nitroso-di-n-propylamine ND ug/kg 02/15/19 21:41 621-64-702/15/19 10:13432 82.4 1
N-Nitrosodiphenylamine ND ug/kg 02/15/19 21:41 86-30-602/15/19 10:13432 128 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/15/19 21:41 108-60-102/15/19 10:13432 115 1
Pentachlorophenol ND ug/kg 02/15/19 21:41 87-86-502/15/19 10:132160 78.5 1
Phenanthrene ND ug/kg 02/15/19 21:41 85-01-802/15/19 10:13432 72.0 1
Phenol ND ug/kg 02/15/19 21:41 108-95-202/15/19 10:13432 130 1
Pyrene ND ug/kg 02/15/19 21:41 129-00-002/15/19 10:13432 73.3 1
1,2,4-Trichlorobenzene ND ug/kg 02/15/19 21:41 120-82-102/15/19 10:13432 83.7 1
2,4,5-Trichlorophenol ND ug/kg 02/15/19 21:41 95-95-402/15/19 10:13432 133 1
2,4,6-Trichlorophenol ND ug/kg 02/15/19 21:41 88-06-202/15/19 10:13432 95.5 1
Surrogates
Nitrobenzene-d5 (S)56 %02/15/19 21:41 4165-60-002/15/19 10:1323-110 1
2-Fluorobiphenyl (S)51 %02/15/19 21:41 321-60-802/15/19 10:1330-110 1
Terphenyl-d14 (S)58 %02/15/19 21:41 1718-51-002/15/19 10:1328-110 1
Phenol-d6 (S)48 %02/15/19 21:41 13127-88-302/15/19 10:1322-110 1
2-Fluorophenol (S)43 %02/15/19 21:41 367-12-402/15/19 10:1313-110 1
2,4,6-Tribromophenol (S)46 %02/15/19 21:41 118-79-602/15/19 10:1327-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 167 ug/kg 02/11/19 20:06 67-64-102/11/19 13:37100 10.0 1
Benzene ND ug/kg 02/11/19 20:06 71-43-202/11/19 13:375.0 1.6 1
Bromobenzene ND ug/kg 02/11/19 20:06 108-86-102/11/19 13:375.0 2.0 1
Bromochloromethane ND ug/kg 02/11/19 20:06 74-97-502/11/19 13:375.0 1.7 1
Bromodichloromethane ND ug/kg 02/11/19 20:06 75-27-402/11/19 13:375.0 1.9 1
Bromoform ND ug/kg 02/11/19 20:06 75-25-202/11/19 13:375.0 2.3 1
Bromomethane ND ug/kg 02/11/19 20:06 74-83-902/11/19 13:3710.0 2.5 1
2-Butanone (MEK)11.7J ug/kg 02/11/19 20:06 78-93-302/11/19 13:37100 2.9 1
n-Butylbenzene ND ug/kg 02/11/19 20:06 104-51-802/11/19 13:375.0 1.8 1
sec-Butylbenzene ND ug/kg 02/11/19 20:06 135-98-802/11/19 13:375.0 1.6 1
tert-Butylbenzene ND ug/kg 02/11/19 20:06 98-06-602/11/19 13:375.0 2.0 1
Carbon tetrachloride ND ug/kg 02/11/19 20:06 56-23-502/11/19 13:375.0 2.6 1
Chlorobenzene ND ug/kg 02/11/19 20:06 108-90-702/11/19 13:375.0 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-12 (0-2)Lab ID: 92417206012 Collected: 02/08/19 15:30 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 02/11/19 20:06 75-00-302/11/19 13:3710.0 2.4 1
Chloroform 2.3J ug/kg 02/11/19 20:06 67-66-302/11/19 13:375.0 1.6 1
Chloromethane ND ug/kg 02/11/19 20:06 74-87-302/11/19 13:3710.0 2.4 1
2-Chlorotoluene ND ug/kg 02/11/19 20:06 95-49-802/11/19 13:375.0 1.7 1
4-Chlorotoluene ND ug/kg 02/11/19 20:06 106-43-402/11/19 13:375.0 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 02/11/19 20:06 96-12-802/11/19 13:375.0 3.6 1
Dibromochloromethane ND ug/kg 02/11/19 20:06 124-48-102/11/19 13:375.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 02/11/19 20:06 106-93-402/11/19 13:375.0 1.8 1
Dibromomethane ND ug/kg 02/11/19 20:06 74-95-302/11/19 13:375.0 2.5 1
1,2-Dichlorobenzene ND ug/kg 02/11/19 20:06 95-50-102/11/19 13:375.0 1.9 1
1,3-Dichlorobenzene ND ug/kg 02/11/19 20:06 541-73-102/11/19 13:375.0 2.0 1
1,4-Dichlorobenzene ND ug/kg 02/11/19 20:06 106-46-702/11/19 13:375.0 1.7 1
Dichlorodifluoromethane ND ug/kg 02/11/19 20:06 75-71-802/11/19 13:3710.0 3.6 1
1,1-Dichloroethane ND ug/kg 02/11/19 20:06 75-34-302/11/19 13:375.0 1.5 1
1,2-Dichloroethane ND ug/kg 02/11/19 20:06 107-06-202/11/19 13:375.0 2.2 1
1,1-Dichloroethene ND ug/kg 02/11/19 20:06 75-35-402/11/19 13:375.0 1.8 1
cis-1,2-Dichloroethene ND ug/kg 02/11/19 20:06 156-59-202/11/19 13:375.0 1.4 1
trans-1,2-Dichloroethene ND ug/kg 02/11/19 20:06 156-60-502/11/19 13:375.0 1.9 1
1,2-Dichloropropane ND ug/kg 02/11/19 20:06 78-87-502/11/19 13:375.0 1.7 1
1,3-Dichloropropane ND ug/kg 02/11/19 20:06 142-28-902/11/19 13:375.0 1.9 1
2,2-Dichloropropane ND ug/kg 02/11/19 20:06 594-20-702/11/19 13:375.0 1.7 1
1,1-Dichloropropene ND ug/kg 02/11/19 20:06 563-58-602/11/19 13:375.0 1.5 1
cis-1,3-Dichloropropene ND ug/kg 02/11/19 20:06 10061-01-502/11/19 13:375.0 1.8 1
trans-1,3-Dichloropropene ND ug/kg 02/11/19 20:06 10061-02-602/11/19 13:375.0 1.5 1
Diisopropyl ether ND ug/kg 02/11/19 20:06 108-20-302/11/19 13:375.0 1.7 1
Ethylbenzene ND ug/kg 02/11/19 20:06 100-41-402/11/19 13:375.0 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 02/11/19 20:06 87-68-302/11/19 13:375.0 2.0 1
2-Hexanone ND ug/kg 02/11/19 20:06 591-78-602/11/19 13:3750.0 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 02/11/19 20:06 98-82-802/11/19 13:375.0 1.9 1
p-Isopropyltoluene ND ug/kg 02/11/19 20:06 99-87-602/11/19 13:375.0 1.7 1
Methylene Chloride ND ug/kg 02/11/19 20:06 75-09-202/11/19 13:3720.0 3.0 1
4-Methyl-2-pentanone (MIBK)3.8J ug/kg 02/11/19 20:06 108-10-102/11/19 13:3750.0 3.7 1
Methyl-tert-butyl ether ND ug/kg 02/11/19 20:06 1634-04-402/11/19 13:375.0 1.5 1
Naphthalene 6.1 ug/kg 02/11/19 20:06 91-20-302/11/19 13:375.0 1.2 1
n-Propylbenzene ND ug/kg 02/11/19 20:06 103-65-102/11/19 13:375.0 1.7 1
Styrene ND ug/kg 02/11/19 20:06 100-42-502/11/19 13:375.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 02/11/19 20:06 630-20-602/11/19 13:375.0 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 02/11/19 20:06 79-34-502/11/19 13:375.0 1.9 1
Tetrachloroethene ND ug/kg 02/11/19 20:06 127-18-402/11/19 13:375.0 1.7 1
Toluene 2.9J ug/kg 02/11/19 20:06 108-88-302/11/19 13:375.0 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 02/11/19 20:06 87-61-602/11/19 13:375.0 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 02/11/19 20:06 120-82-102/11/19 13:375.0 1.6 1
1,1,1-Trichloroethane ND ug/kg 02/11/19 20:06 71-55-602/11/19 13:375.0 1.8 1
1,1,2-Trichloroethane ND ug/kg 02/11/19 20:06 79-00-502/11/19 13:375.0 2.1 1
Trichloroethene ND ug/kg 02/11/19 20:06 79-01-602/11/19 13:375.0 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 91
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417206
BCP-129
Sample: SB-12 (0-2)Lab ID: 92417206012 Collected: 02/08/19 15:30 Received: 02/11/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 02/11/19 20:06 75-69-402/11/19 13:375.0 2.2 1
1,2,3-Trichloropropane ND ug/kg 02/11/19 20:06 96-18-402/11/19 13:375.0 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 02/11/19 20:06 95-63-602/11/19 13:375.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 02/11/19 20:06 108-67-802/11/19 13:375.0 1.8 1
Vinyl acetate ND ug/kg 02/11/19 20:06 108-05-402/11/19 13:3750.0 8.8 1
Vinyl chloride ND ug/kg 02/11/19 20:06 75-01-402/11/19 13:3710.0 1.8 1
Xylene (Total)ND ug/kg 02/11/19 20:06 1330-20-702/11/19 13:3710.0 3.6 1
m&p-Xylene 3.7J ug/kg 02/11/19 20:06 179601-23-102/11/19 13:3710.0 3.6 1
o-Xylene ND ug/kg 02/11/19 20:06 95-47-602/11/19 13:375.0 1.9 1
Surrogates
Toluene-d8 (S)101 %02/11/19 20:06 2037-26-502/11/19 13:3770-130 1
4-Bromofluorobenzene (S)97 %02/11/19 20:06 460-00-402/11/19 13:3770-130 1
1,2-Dichloroethane-d4 (S)96 %02/11/19 20:06 17060-07-002/11/19 13:3770-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.6 %02/11/19 17:160.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
457453
EPA 5035A
EPA 8260B
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92417206002, 92417206003, 92417206004, 92417206005, 92417206006, 92417206009, 92417206010,
92417206011, 92417206012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2495077
Associated Lab Samples: 92417206002, 92417206003, 92417206004, 92417206005, 92417206006, 92417206009, 92417206010,
92417206011, 92417206012
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.3 02/11/19 15:052.2
1,1,1-Trichloroethane ug/kg ND 5.3 02/11/19 15:051.9
1,1,2,2-Tetrachloroethane ug/kg ND 5.3 02/11/19 15:052.0
1,1,2-Trichloroethane ug/kg ND 5.3 02/11/19 15:052.2
1,1-Dichloroethane ug/kg ND 5.3 02/11/19 15:051.6
1,1-Dichloroethene ug/kg ND 5.3 02/11/19 15:051.9
1,1-Dichloropropene ug/kg ND 5.3 02/11/19 15:051.6
1,2,3-Trichlorobenzene ug/kg ND 5.3 02/11/19 15:052.3
1,2,3-Trichloropropane ug/kg ND 5.3 02/11/19 15:051.7
1,2,4-Trichlorobenzene ug/kg ND 5.3 02/11/19 15:051.7
1,2,4-Trimethylbenzene ug/kg ND 5.3 02/11/19 15:052.1
1,2-Dibromo-3-chloropropane ug/kg ND 5.3 02/11/19 15:053.8
1,2-Dibromoethane (EDB)ug/kg ND 5.3 02/11/19 15:051.9
1,2-Dichlorobenzene ug/kg ND 5.3 02/11/19 15:052.0
1,2-Dichloroethane ug/kg ND 5.3 02/11/19 15:052.3
1,2-Dichloropropane ug/kg ND 5.3 02/11/19 15:051.8
1,3,5-Trimethylbenzene ug/kg ND 5.3 02/11/19 15:051.9
1,3-Dichlorobenzene ug/kg ND 5.3 02/11/19 15:052.1
1,3-Dichloropropane ug/kg ND 5.3 02/11/19 15:052.0
1,4-Dichlorobenzene ug/kg ND 5.3 02/11/19 15:051.8
2,2-Dichloropropane ug/kg ND 5.3 02/11/19 15:051.8
2-Butanone (MEK)ug/kg ND 106 02/11/19 15:053.1
2-Chlorotoluene ug/kg ND 5.3 02/11/19 15:051.8
2-Hexanone ug/kg ND 53.0 02/11/19 15:054.1
4-Chlorotoluene ug/kg ND 5.3 02/11/19 15:051.9
4-Methyl-2-pentanone (MIBK)ug/kg ND 53.0 02/11/19 15:053.9
Acetone ug/kg ND 106 02/11/19 15:0510.6
Benzene ug/kg ND 5.3 02/11/19 15:051.7
Bromobenzene ug/kg ND 5.3 02/11/19 15:052.1
Bromochloromethane ug/kg ND 5.3 02/11/19 15:051.8
Bromodichloromethane ug/kg ND 5.3 02/11/19 15:052.0
Bromoform ug/kg ND 5.3 02/11/19 15:052.4
Bromomethane ug/kg ND 10.6 02/11/19 15:052.6
Carbon tetrachloride ug/kg ND 5.3 02/11/19 15:052.8
Chlorobenzene ug/kg ND 5.3 02/11/19 15:052.0
Chloroethane ug/kg ND 10.6 02/11/19 15:052.5
Chloroform ug/kg ND 5.3 02/11/19 15:051.7
Chloromethane ug/kg ND 10.6 02/11/19 15:052.5
cis-1,2-Dichloroethene ug/kg ND 5.3 02/11/19 15:051.5
cis-1,3-Dichloropropene ug/kg ND 5.3 02/11/19 15:051.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2495077
Associated Lab Samples: 92417206002, 92417206003, 92417206004, 92417206005, 92417206006, 92417206009, 92417206010,
92417206011, 92417206012
Matrix: Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.3 02/11/19 15:051.9
Dibromomethane ug/kg ND 5.3 02/11/19 15:052.6
Dichlorodifluoromethane ug/kg ND 10.6 02/11/19 15:053.8
Diisopropyl ether ug/kg ND 5.3 02/11/19 15:051.8
Ethylbenzene ug/kg ND 5.3 02/11/19 15:051.9
Hexachloro-1,3-butadiene ug/kg ND 5.3 02/11/19 15:052.1
Isopropylbenzene (Cumene)ug/kg ND 5.3 02/11/19 15:052.0
m&p-Xylene ug/kg ND 10.6 02/11/19 15:053.8
Methyl-tert-butyl ether ug/kg ND 5.3 02/11/19 15:051.6
Methylene Chloride ug/kg ND 21.2 02/11/19 15:053.2
n-Butylbenzene ug/kg ND 5.3 02/11/19 15:051.9
n-Propylbenzene ug/kg ND 5.3 02/11/19 15:051.8
Naphthalene ug/kg ND 5.3 02/11/19 15:051.3
o-Xylene ug/kg ND 5.3 02/11/19 15:052.0
p-Isopropyltoluene ug/kg ND 5.3 02/11/19 15:051.8
sec-Butylbenzene ug/kg ND 5.3 02/11/19 15:051.7
Styrene ug/kg ND 5.3 02/11/19 15:051.9
tert-Butylbenzene ug/kg ND 5.3 02/11/19 15:052.1
Tetrachloroethene ug/kg ND 5.3 02/11/19 15:051.8
Toluene ug/kg ND 5.3 02/11/19 15:051.9
trans-1,2-Dichloroethene ug/kg ND 5.3 02/11/19 15:052.0
trans-1,3-Dichloropropene ug/kg ND 5.3 02/11/19 15:051.6
Trichloroethene ug/kg ND 5.3 02/11/19 15:052.2
Trichlorofluoromethane ug/kg ND 5.3 02/11/19 15:052.3
Vinyl acetate ug/kg ND 53.0 02/11/19 15:059.3
Vinyl chloride ug/kg ND 10.6 02/11/19 15:051.9
Xylene (Total)ug/kg ND 10.6 02/11/19 15:053.8
1,2-Dichloroethane-d4 (S)%100 70-132 02/11/19 15:05
4-Bromofluorobenzene (S)%98 70-130 02/11/19 15:05
Toluene-d8 (S)%100 70-130 02/11/19 15:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2495078LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2495079
1,1,1,2-Tetrachloroethane ug/kg 52.251.8 101 70-13010053.1 2 30
1,1,1-Trichloroethane ug/kg 51.751.8 100 70-13010052.8 2 30
1,1,2,2-Tetrachloroethane ug/kg 50.051.8 97 55-1309952.5 5 30
1,1,2-Trichloroethane ug/kg 53.251.8 103 70-13010354.5 2 30
1,1-Dichloroethane ug/kg 50.551.8 98 68-1309952.4 4 30
1,1-Dichloroethene ug/kg 51.751.8 100 70-13010656.4 9 30
1,1-Dichloropropene ug/kg 48.651.8 94 70-1309047.6 2 30
1,2,3-Trichlorobenzene ug/kg 52.051.8 100 70-13010052.9 2 30
1,2,3-Trichloropropane ug/kg 51.251.8 99 70-1309650.7 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
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[phone]
Page 42 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2495078LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2495079
1,2,4-Trichlorobenzene ug/kg 51.751.8 100 70-1309952.3 1 30
1,2,4-Trimethylbenzene ug/kg 49.451.8 95 69-1309248.5 2 30
1,2-Dibromo-3-chloropropane ug/kg 53.451.8 103 57-14110354.6 2 30
1,2-Dibromoethane (EDB)ug/kg 52.551.8 101 70-13010254.1 3 30
1,2-Dichlorobenzene ug/kg 51.051.8 99 70-1309449.9 2 30
1,2-Dichloroethane ug/kg 47.551.8 92 70-1309449.8 5 30
1,2-Dichloropropane ug/kg 50.251.8 97 70-1309651.1 2 30
1,3,5-Trimethylbenzene ug/kg 50.251.8 97 70-1309449.9 1 30
1,3-Dichlorobenzene ug/kg 50.951.8 98 70-1309449.6 3 30
1,3-Dichloropropane ug/kg 49.551.8 96 70-1309550.1 1 30
1,4-Dichlorobenzene ug/kg 49.051.8 95 70-1309248.6 1 30
2,2-Dichloropropane ug/kg 51.051.8 99 70-1309751.5 1 30
2-Butanone (MEK)ug/kg 104104 100 60-13097103J 30
2-Chlorotoluene ug/kg 49.551.8 96 70-1309349.4 0 30
2-Hexanone ug/kg 101104 98 70-132101107 6 30
4-Chlorotoluene ug/kg 50.451.8 97 70-1309349.3 2 30
4-Methyl-2-pentanone (MIBK)ug/kg 106104 102 69-130101107 1 30
Acetone ug/kg 102J104 99 49-148103109 30
Benzene ug/kg 51.751.8 100 70-1309852.1 1 30
Bromobenzene ug/kg 50.951.8 98 70-1309751.6 1 30
Bromochloromethane ug/kg 53.751.8 104 70-13010253.8 0 30
Bromodichloromethane ug/kg 53.451.8 103 70-13010153.5 0 30
Bromoform ug/kg 51.751.8 100 68-1369952.6 2 30
Bromomethane ug/kg 44.451.8 86 60-1409751.5 15 30
Carbon tetrachloride ug/kg 53.551.8 103 70-13010354.4 2 30
Chlorobenzene ug/kg 50.451.8 97 70-1309650.7 1 30
Chloroethane ug/kg 58.551.8 113 51-14710454.9 7 30
Chloroform ug/kg 45.351.8 87 70-1309047.9 6 30
Chloromethane ug/kg 48.751.8 94 48-1309349.3 1 30
cis-1,2-Dichloroethene ug/kg 50.951.8 98 70-1309650.9 0 30
cis-1,3-Dichloropropene ug/kg 53.651.8 104 70-13010052.9 1 30
Dibromochloromethane ug/kg 53.951.8 104 70-13010555.5 3 30
Dibromomethane ug/kg 52.451.8 101 70-13010555.6 6 30
Dichlorodifluoromethane ug/kg 48.051.8 93 49-1309349.5 3 30
Diisopropyl ether ug/kg 51.051.8 99 66-13010052.7 3 30
Ethylbenzene ug/kg 50.351.8 97 70-1309450.0 1 30
Hexachloro-1,3-butadiene ug/kg 50.951.8 98 70-1309751.4 1 30
Isopropylbenzene (Cumene)ug/kg 51.851.8 100 70-1309952.4 1 30
m&p-Xylene ug/kg 101104 97 70-13096102 1 30
Methyl-tert-butyl ether ug/kg 48.551.8 94 70-13010153.7 10 30
Methylene Chloride ug/kg 48.851.8 94 50-1379349.5 1 30
n-Butylbenzene ug/kg 50.451.8 97 70-1309248.5 4 30
n-Propylbenzene ug/kg 51.351.8 99 70-1309450.0 3 30
Naphthalene ug/kg 50.151.8 97 70-1319751.4 2 30
o-Xylene ug/kg 52.051.8 100 70-1309751.5 1 30
p-Isopropyltoluene ug/kg 49.551.8 96 70-1309349.1 1 30
sec-Butylbenzene ug/kg 52.151.8 101 70-1309751.3 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 43 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2495078LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2495079
Styrene ug/kg 52.151.8 101 70-1309852.0 0 30
tert-Butylbenzene ug/kg 46.451.8 90 69-1308545.2 2 30
Tetrachloroethene ug/kg 49.451.8 95 56-1309550.2 2 30
Toluene ug/kg 50.751.8 98 70-1309651.0 1 30
trans-1,2-Dichloroethene ug/kg 50.551.8 98 70-1309751.2 1 30
trans-1,3-Dichloropropene ug/kg 51.951.8 100 70-13010052.9 2 30
Trichloroethene ug/kg 53.151.8 103 70-1419751.6 3 30
Trichlorofluoromethane ug/kg 52.951.8 102 67-13010153.6 1 30
Vinyl acetate ug/kg 116104 112 10-136110116 0 30
Vinyl chloride ug/kg 52.151.8 101 67-13010052.7 1 30
Xylene (Total)ug/kg 153155 98 70-13097153 0 30
1,2-Dichloroethane-d4 (S)%92 70-13296
4-Bromofluorobenzene (S)%98 70-13099
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
457705
EPA 3546
EPA 8270D
8270 Solid MSSV Microwave
Associated Lab Samples: 92417206002, 92417206003, 92417206004, 92417206005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2496042
Associated Lab Samples:92417206002, 92417206003, 92417206004, 92417206005
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 325 02/13/19 09:5963.0
1,2-Dichlorobenzene ug/kg ND 325 02/13/19 09:5986.6
1,3-Dichlorobenzene ug/kg ND 325 02/13/19 09:5973.8
1,4-Dichlorobenzene ug/kg ND 325 02/13/19 09:5991.5
1-Methylnaphthalene ug/kg ND 325 02/13/19 09:5984.6
2,2'-Oxybis(1-chloropropane)ug/kg ND 325 02/13/19 09:5986.6
2,4,5-Trichlorophenol ug/kg ND 325 02/13/19 09:59100
2,4,6-Trichlorophenol ug/kg ND 325 02/13/19 09:5971.8
2,4-Dichlorophenol ug/kg ND 325 02/13/19 09:5970.8
2,4-Dimethylphenol ug/kg ND 325 02/13/19 09:59128
2,4-Dinitrophenol ug/kg ND 1620 02/13/19 09:5953.1
2,4-Dinitrotoluene ug/kg ND 325 02/13/19 09:5961.0
2,6-Dinitrotoluene ug/kg ND 325 02/13/19 09:5967.9
2-Chloronaphthalene ug/kg ND 325 02/13/19 09:5963.9
2-Chlorophenol ug/kg ND 325 02/13/19 09:5988.5
2-Methylnaphthalene ug/kg ND 325 02/13/19 09:5969.8
2-Methylphenol(o-Cresol)ug/kg ND 325 02/13/19 09:5998.4
2-Nitroaniline ug/kg ND 1620 02/13/19 09:59100
2-Nitrophenol ug/kg ND 325 02/13/19 09:5978.7
3&4-Methylphenol(m&p Cresol)ug/kg ND 325 02/13/19 09:59128
3,3'-Dichlorobenzidine ug/kg ND 1620 02/13/19 09:5970.8
3-Nitroaniline ug/kg ND 1620 02/13/19 09:5988.5
4,6-Dinitro-2-methylphenol ug/kg ND 649 02/13/19 09:5964.9
4-Bromophenylphenyl ether ug/kg ND 325 02/13/19 09:5959.0
4-Chloro-3-methylphenol ug/kg ND 649 02/13/19 09:5966.9
4-Chloroaniline ug/kg ND 1620 02/13/19 09:5990.5
4-Chlorophenylphenyl ether ug/kg ND 325 02/13/19 09:5966.9
4-Nitroaniline ug/kg ND 649 02/13/19 09:5991.5
4-Nitrophenol ug/kg ND 1620 02/13/19 09:5958.0
Acenaphthene ug/kg ND 325 02/13/19 09:5974.8
Acenaphthylene ug/kg ND 325 02/13/19 09:5976.7
Aniline ug/kg ND 325 02/13/19 09:5987.5
Anthracene ug/kg ND 325 02/13/19 09:5972.8
Benzo(a)anthracene ug/kg ND 325 02/13/19 09:5960.0
Benzo(a)pyrene ug/kg ND 325 02/13/19 09:5962.0
Benzo(b)fluoranthene ug/kg ND 325 02/13/19 09:5956.1
Benzo(g,h,i)perylene ug/kg ND 325 02/13/19 09:5982.6
Benzo(k)fluoranthene ug/kg ND 325 02/13/19 09:5963.9
Benzoic Acid ug/kg ND 1620 02/13/19 09:5959.0
Benzyl alcohol ug/kg ND 649 02/13/19 09:5964.9
bis(2-Chloroethoxy)methane ug/kg ND 325 02/13/19 09:5975.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2496042
Associated Lab Samples:92417206002, 92417206003, 92417206004, 92417206005
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 325 02/13/19 09:5982.6
bis(2-Ethylhexyl)phthalate ug/kg ND 325 02/13/19 09:5988.5
Butylbenzylphthalate ug/kg ND 325 02/13/19 09:5968.9
Chrysene ug/kg ND 325 02/13/19 09:5943.3
Di-n-butylphthalate ug/kg ND 325 02/13/19 09:5953.1
Di-n-octylphthalate ug/kg ND 325 02/13/19 09:5967.9
Dibenz(a,h)anthracene ug/kg ND 325 02/13/19 09:5968.9
Dibenzofuran ug/kg ND 325 02/13/19 09:5953.1
Diethylphthalate ug/kg ND 325 02/13/19 09:5950.2
Dimethylphthalate ug/kg ND 325 02/13/19 09:5965.9
Fluoranthene ug/kg ND 325 02/13/19 09:5947.2
Fluorene ug/kg ND 325 02/13/19 09:5966.9
Hexachloro-1,3-butadiene ug/kg ND 325 02/13/19 09:5956.1
Hexachlorobenzene ug/kg ND 325 02/13/19 09:5941.3
Hexachlorocyclopentadiene ug/kg ND 325 02/13/19 09:5960.0
Hexachloroethane ug/kg ND 325 02/13/19 09:5985.6
Indeno(1,2,3-cd)pyrene ug/kg ND 325 02/13/19 09:5966.9
Isophorone ug/kg ND 325 02/13/19 09:5972.8
N-Nitroso-di-n-propylamine ug/kg ND 325 02/13/19 09:5962.0
N-Nitrosodimethylamine ug/kg ND 325 02/13/19 09:59105
N-Nitrosodiphenylamine ug/kg ND 325 02/13/19 09:5996.4
Naphthalene ug/kg ND 325 02/13/19 09:5979.7
Nitrobenzene ug/kg ND 325 02/13/19 09:5988.5
Pentachlorophenol ug/kg ND 1620 02/13/19 09:5959.0
Phenanthrene ug/kg ND 325 02/13/19 09:5954.1
Phenol ug/kg ND 325 02/13/19 09:5997.4
Pyrene ug/kg ND 325 02/13/19 09:5955.1
2,4,6-Tribromophenol (S)%83 27-110 02/13/19 09:59
2-Fluorobiphenyl (S)%78 30-110 02/13/19 09:59
2-Fluorophenol (S)%75 13-110 02/13/19 09:59
Nitrobenzene-d5 (S)%84 23-110 02/13/19 09:59
Phenol-d6 (S)%82 22-110 02/13/19 09:59
Terphenyl-d14 (S)%92 28-110 02/13/19 09:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2496044LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11601640 71 52-130
1,2-Dichlorobenzene ug/kg 12501640 76 51-130
1,3-Dichlorobenzene ug/kg 11801640 72 50-130
1,4-Dichlorobenzene ug/kg 12501640 76 49-130
1-Methylnaphthalene ug/kg 14001640 85 55-130
2,2'-Oxybis(1-chloropropane)ug/kg 17001640 103 30-130
2,4,5-Trichlorophenol ug/kg 12601640 77 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2496044LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 13401640 81 57-130
2,4-Dichlorophenol ug/kg 12801640 78 56-130
2,4-Dimethylphenol ug/kg 13901640 84 51-130
2,4-Dinitrophenol ug/kg 79508220 97 27-133
2,4-Dinitrotoluene ug/kg 14201640 86 61-130
2,6-Dinitrotoluene ug/kg 14501640 88 60-130
2-Chloronaphthalene ug/kg 12601640 77 52-130
2-Chlorophenol ug/kg 13301640 81 54-130
2-Methylnaphthalene ug/kg 13901640 85 54-130
2-Methylphenol(o-Cresol)ug/kg 14001640 85 51-130
2-Nitroaniline ug/kg 30903290 94 51-130
2-Nitrophenol ug/kg 13101640 80 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 14101640 86 11-163
3,3'-Dichlorobenzidine ug/kg 23703290 72 10-132
3-Nitroaniline ug/kg 25203290 77 55-130
4,6-Dinitro-2-methylphenol ug/kg 35003290 106 47-142
4-Bromophenylphenyl ether ug/kg 13901640 84 59-130
4-Chloro-3-methylphenol ug/kg 29203290 89 55-130
4-Chloroaniline ug/kg 25403290 77 54-130
4-Chlorophenylphenyl ether ug/kg 14001640 85 58-130
4-Nitroaniline ug/kg 28003290 85 54-130
4-Nitrophenol ug/kg 75408220 92 48-130
Acenaphthene ug/kg 14301640 87 60-130
Acenaphthylene ug/kg 15101640 92 60-130
Aniline ug/kg 11901640 73 43-130
Anthracene ug/kg 15101640 92 63-130
Benzo(a)anthracene ug/kg 15301640 93 59-130
Benzo(a)pyrene ug/kg 15501640 94 57-130
Benzo(b)fluoranthene ug/kg 14401640 87 54-130
Benzo(g,h,i)perylene ug/kg 16901640 102 59-130
Benzo(k)fluoranthene ug/kg 14301640 87 54-130
Benzoic Acid ug/kg 68408220 83 19-130
Benzyl alcohol ug/kg 29603290 90 50-130
bis(2-Chloroethoxy)methane ug/kg 13801640 84 54-130
bis(2-Chloroethyl) ether ug/kg 13601640 83 48-130
bis(2-Ethylhexyl)phthalate ug/kg 15301640 93 45-134
Butylbenzylphthalate ug/kg 15001640 91 46-138
Chrysene ug/kg 14601640 89 58-130
Di-n-butylphthalate ug/kg 14401640 87 60-130
Di-n-octylphthalate ug/kg 16501640 100 53-130
Dibenz(a,h)anthracene ug/kg 15901640 97 59-130
Dibenzofuran ug/kg 13201640 80 60-130
Diethylphthalate ug/kg 14501640 88 60-130
Dimethylphthalate ug/kg 14301640 87 60-130
Fluoranthene ug/kg 14801640 90 65-130
Fluorene ug/kg 14601640 89 63-130
Hexachloro-1,3-butadiene ug/kg 11501640 70 46-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2496044LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 13301640 81 58-130
Hexachlorocyclopentadiene ug/kg 11201640 68 23-130
Hexachloroethane ug/kg 12801640 78 47-130
Indeno(1,2,3-cd)pyrene ug/kg 15601640 95 60-130
Isophorone ug/kg 14201640 86 49-130
N-Nitroso-di-n-propylamine ug/kg 15401640 94 47-130
N-Nitrosodimethylamine ug/kg 13001640 79 45-130
N-Nitrosodiphenylamine ug/kg 14901640 91 59-130
Naphthalene ug/kg 13401640 81 55-130
Nitrobenzene ug/kg 12701640 77 49-130
Pentachlorophenol ug/kg 26103290 79 10-132
Phenanthrene ug/kg 15001640 91 62-130
Phenol ug/kg 13001640 79 46-130
Pyrene ug/kg 14501640 88 53-130
2,4,6-Tribromophenol (S)%93 27-110
2-Fluorobiphenyl (S)%80 30-110
2-Fluorophenol (S)%79 13-110
Nitrobenzene-d5 (S)%85 23-110
Phenol-d6 (S)%93 22-110
Terphenyl-d14 (S)%83 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2496045MATRIX SPIKE SAMPLE:
MSSpike
Result
92417206001
1,2,4-Trichlorobenzene ug/kg 16002180 73 18-130ND
1,2-Dichlorobenzene ug/kg 17002180 78 14-130ND
1,3-Dichlorobenzene ug/kg 16102180 74 12-130ND
1,4-Dichlorobenzene ug/kg 16802180 77 10-130ND
1-Methylnaphthalene ug/kg 19502180 89 12-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 23402180 107 10-130ND
2,4,5-Trichlorophenol ug/kg 17602180 81 13-130ND
2,4,6-Trichlorophenol ug/kg 18102180 83 17-130ND
2,4-Dichlorophenol ug/kg 17102180 78 10-130ND
2,4-Dimethylphenol ug/kg 17802180 82 10-130ND
2,4-Dinitrophenol ug/kg 1100010900 101 10-130ND
2,4-Dinitrotoluene ug/kg 19502180 90 24-130ND
2,6-Dinitrotoluene ug/kg 19702180 90 23-130ND
2-Chloronaphthalene ug/kg 17702180 81 19-130ND
2-Chlorophenol ug/kg 18302180 84 10-130ND
2-Methylnaphthalene ug/kg 19302180 88 18-130ND
2-Methylphenol(o-Cresol)ug/kg 18702180 86 10-130ND
2-Nitroaniline ug/kg 41504350 95 17-130ND
2-Nitrophenol ug/kg 16502180 76 10-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 19202180 88 10-130ND
3,3'-Dichlorobenzidine ug/kg 31404350 72 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2496045MATRIX SPIKE SAMPLE:
MSSpike
Result
92417206001
3-Nitroaniline ug/kg 33904350 78 24-130ND
4,6-Dinitro-2-methylphenol ug/kg 48804350 112 10-152ND
4-Bromophenylphenyl ether ug/kg 18702180 86 29-130ND
4-Chloro-3-methylphenol ug/kg 38804350 89 17-130ND
4-Chloroaniline ug/kg 34004350 78 14-130ND
4-Chlorophenylphenyl ether ug/kg 18502180 85 25-130ND
4-Nitroaniline ug/kg 36804350 84 22-130ND
4-Nitrophenol ug/kg 1050010900 96 10-130ND
Acenaphthene ug/kg 19602180 90 20-130ND
Acenaphthylene ug/kg 20302180 93 25-130ND
Aniline ug/kg 15602180 72 10-130ND
Anthracene ug/kg 21002180 96 29-130ND
Benzo(a)anthracene ug/kg 20802180 95 19-130ND
Benzo(a)pyrene ug/kg 20202180 93 12-130ND
Benzo(b)fluoranthene ug/kg 22402180 103 14-130ND
Benzo(g,h,i)perylene ug/kg 21502180 99 10-130ND
Benzo(k)fluoranthene ug/kg 21402180 98 14-130ND
Benzoic Acid ug/kg 927010900 85 10-130ND
Benzyl alcohol ug/kg 39704350 91 13-130ND
bis(2-Chloroethoxy)methane ug/kg 17602180 81 16-130ND
bis(2-Chloroethyl) ether ug/kg 18802180 86 11-130ND
bis(2-Ethylhexyl)phthalate ug/kg 21102180 97 21-130ND
Butylbenzylphthalate ug/kg 20702180 95 23-130ND
Chrysene ug/kg 20702180 95 22-130ND
Di-n-butylphthalate ug/kg 21202180 98 30-130ND
Di-n-octylphthalate ug/kg 22102180 102 23-142ND
Dibenz(a,h)anthracene ug/kg 22102180 102 10-130ND
Dibenzofuran ug/kg 18202180 84 24-130ND
Diethylphthalate ug/kg 19702180 90 26-130ND
Dimethylphthalate ug/kg 19702180 90 22-130ND
Fluoranthene ug/kg 22702180 104 33-130ND
Fluorene ug/kg 19602180 90 22-130ND
Hexachloro-1,3-butadiene ug/kg 15602180 72 13-130ND
Hexachlorobenzene ug/kg 18702180 86 29-130ND
Hexachlorocyclopentadiene ug/kg 15502180 71 10-130ND
Hexachloroethane ug/kg 17302180 79 10-130ND
Indeno(1,2,3-cd)pyrene ug/kg 20702180 95 10-130ND
Isophorone ug/kg 18002180 83 13-130ND
N-Nitroso-di-n-propylamine ug/kg 20502180 94 12-130ND
N-Nitrosodimethylamine ug/kg 18002180 82 11-130ND
N-Nitrosodiphenylamine ug/kg 20202180 93 15-130ND
Naphthalene ug/kg 18402180 84 15-130ND
Nitrobenzene ug/kg 16102180 74 12-130ND
Pentachlorophenol ug/kg 36404350 83 10-130ND
Phenanthrene ug/kg 21002180 96 27-130ND
Phenol ug/kg 17802180 81 10-130ND
Pyrene ug/kg 21102180 97 19-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
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Huntersville, NC 28078
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Page 49 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2496045MATRIX SPIKE SAMPLE:
MSSpike
Result
92417206001
2,4,6-Tribromophenol (S)%94 27-110
2-Fluorobiphenyl (S)%83 30-110
2-Fluorophenol (S)%77 13-110
Nitrobenzene-d5 (S)%83 23-110
Phenol-d6 (S)%93 22-110
Terphenyl-d14 (S)%88 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92417206002
2496046SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 50 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92417206002
2496046SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 3046.8J
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg 61.1J 30101J
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 3063.5J
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 3080.1J
2,4,6-Tribromophenol (S)%5358
2-Fluorobiphenyl (S)%4755
2-Fluorophenol (S)%4049
Nitrobenzene-d5 (S)%4754
Phenol-d6 (S)%4856
Terphenyl-d14 (S)%5662
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458360
EPA 3546
EPA 8270D
8270 Solid MSSV Microwave
Associated Lab Samples: 92417206006, 92417206009, 92417206010, 92417206011, 92417206012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2498909
Associated Lab Samples:92417206006, 92417206009, 92417206010, 92417206011, 92417206012
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 334 02/15/19 14:2164.9
1,2-Dichlorobenzene ug/kg ND 334 02/15/19 14:2189.2
1,3-Dichlorobenzene ug/kg ND 334 02/15/19 14:2176.0
1,4-Dichlorobenzene ug/kg ND 334 02/15/19 14:2194.3
1-Methylnaphthalene ug/kg ND 334 02/15/19 14:2187.2
2,2'-Oxybis(1-chloropropane)ug/kg ND 334 02/15/19 14:2189.2
2,4,5-Trichlorophenol ug/kg ND 334 02/15/19 14:21103
2,4,6-Trichlorophenol ug/kg ND 334 02/15/19 14:2174.0
2,4-Dichlorophenol ug/kg ND 334 02/15/19 14:2173.0
2,4-Dimethylphenol ug/kg ND 334 02/15/19 14:21132
2,4-Dinitrophenol ug/kg ND 1670 02/15/19 14:2154.7
2,4-Dinitrotoluene ug/kg ND 334 02/15/19 14:2162.8
2,6-Dinitrotoluene ug/kg ND 334 02/15/19 14:2169.9
2-Chloronaphthalene ug/kg ND 334 02/15/19 14:2165.9
2-Chlorophenol ug/kg ND 334 02/15/19 14:2191.2
2-Methylnaphthalene ug/kg ND 334 02/15/19 14:2172.0
2-Methylphenol(o-Cresol)ug/kg ND 334 02/15/19 14:21101
2-Nitroaniline ug/kg ND 1670 02/15/19 14:21103
2-Nitrophenol ug/kg ND 334 02/15/19 14:2181.1
3&4-Methylphenol(m&p Cresol)ug/kg ND 334 02/15/19 14:21132
3,3'-Dichlorobenzidine ug/kg ND 1670 02/15/19 14:2173.0
3-Nitroaniline ug/kg ND 1670 02/15/19 14:2191.2
4,6-Dinitro-2-methylphenol ug/kg ND 669 02/15/19 14:2166.9
4-Bromophenylphenyl ether ug/kg ND 334 02/15/19 14:2160.8
4-Chloro-3-methylphenol ug/kg ND 669 02/15/19 14:2168.9
4-Chloroaniline ug/kg ND 1670 02/15/19 14:2193.2
4-Chlorophenylphenyl ether ug/kg ND 334 02/15/19 14:2168.9
4-Nitroaniline ug/kg ND 669 02/15/19 14:2194.3
4-Nitrophenol ug/kg ND 1670 02/15/19 14:2159.8
Acenaphthene ug/kg ND 334 02/15/19 14:2177.0
Acenaphthylene ug/kg ND 334 02/15/19 14:2179.1
Aniline ug/kg ND 334 02/15/19 14:2190.2
Anthracene ug/kg ND 334 02/15/19 14:2175.0
Benzo(a)anthracene ug/kg ND 334 02/15/19 14:2161.8
Benzo(a)pyrene ug/kg ND 334 02/15/19 14:2163.9
Benzo(b)fluoranthene ug/kg ND 334 02/15/19 14:2157.8
Benzo(g,h,i)perylene ug/kg ND 334 02/15/19 14:2185.1
Benzo(k)fluoranthene ug/kg ND 334 02/15/19 14:2165.9
Benzoic Acid ug/kg ND 1670 02/15/19 14:2160.8
Benzyl alcohol ug/kg ND 669 02/15/19 14:2166.9
bis(2-Chloroethoxy)methane ug/kg ND 334 02/15/19 14:2178.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2498909
Associated Lab Samples:92417206006, 92417206009, 92417206010, 92417206011, 92417206012
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 334 02/15/19 14:2185.1
bis(2-Ethylhexyl)phthalate ug/kg ND 334 02/15/19 14:2191.2
Butylbenzylphthalate ug/kg ND 334 02/15/19 14:2170.9
Chrysene ug/kg ND 334 02/15/19 14:2144.6
Di-n-butylphthalate ug/kg ND 334 02/15/19 14:2154.7
Di-n-octylphthalate ug/kg ND 334 02/15/19 14:2169.9
Dibenz(a,h)anthracene ug/kg ND 334 02/15/19 14:2170.9
Dibenzofuran ug/kg ND 334 02/15/19 14:2154.7
Diethylphthalate ug/kg ND 334 02/15/19 14:2151.7
Dimethylphthalate ug/kg ND 334 02/15/19 14:2167.9
Fluoranthene ug/kg ND 334 02/15/19 14:2148.6
Fluorene ug/kg ND 334 02/15/19 14:2168.9
Hexachloro-1,3-butadiene ug/kg ND 334 02/15/19 14:2157.8
Hexachlorobenzene ug/kg ND 334 02/15/19 14:2142.6
Hexachlorocyclopentadiene ug/kg ND 334 02/15/19 14:2161.8
Hexachloroethane ug/kg ND 334 02/15/19 14:2188.2
Indeno(1,2,3-cd)pyrene ug/kg ND 334 02/15/19 14:2168.9
Isophorone ug/kg ND 334 02/15/19 14:2175.0
N-Nitroso-di-n-propylamine ug/kg ND 334 02/15/19 14:2163.9
N-Nitrosodimethylamine ug/kg ND 334 02/15/19 14:21108
N-Nitrosodiphenylamine ug/kg ND 334 02/15/19 14:2199.3
Naphthalene ug/kg ND 334 02/15/19 14:2182.1
Nitrobenzene ug/kg ND 334 02/15/19 14:2191.2
Pentachlorophenol ug/kg ND 1670 02/15/19 14:2160.8
Phenanthrene ug/kg ND 334 02/15/19 14:2155.7
Phenol ug/kg ND 334 02/15/19 14:21100
Pyrene ug/kg ND 334 02/15/19 14:2156.8
2,4,6-Tribromophenol (S)%69 27-110 02/15/19 14:21
2-Fluorobiphenyl (S)%68 30-110 02/15/19 14:21
2-Fluorophenol (S)%58 13-110 02/15/19 14:21
Nitrobenzene-d5 (S)%62 23-110 02/15/19 14:21
Phenol-d6 (S)%60 22-110 02/15/19 14:21
Terphenyl-d14 (S)%76 28-110 02/15/19 14:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2498910LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12701690 75 52-130
1,2-Dichlorobenzene ug/kg 11401690 67 51-130
1,3-Dichlorobenzene ug/kg 11901690 70 50-130
1,4-Dichlorobenzene ug/kg 11901690 70 49-130
1-Methylnaphthalene ug/kg 13401690 79 55-130
2,2'-Oxybis(1-chloropropane)ug/kg 10801690 64 30-130
2,4,5-Trichlorophenol ug/kg 12101690 72 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2498910LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 12901690 76 57-130
2,4-Dichlorophenol ug/kg 12501690 74 56-130
2,4-Dimethylphenol ug/kg 12401690 73 51-130
2,4-Dinitrophenol ug/kg 56908470 67 27-133
2,4-Dinitrotoluene ug/kg 14101690 83 61-130
2,6-Dinitrotoluene ug/kg 14001690 83 60-130
2-Chloronaphthalene ug/kg 12301690 72 52-130
2-Chlorophenol ug/kg 12601690 74 54-130
2-Methylnaphthalene ug/kg 13301690 78 54-130
2-Methylphenol(o-Cresol)ug/kg 12101690 72 51-130
2-Nitroaniline ug/kg 23103390 68 51-130
2-Nitrophenol ug/kg 12801690 76 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 12401690 73 11-163
3,3'-Dichlorobenzidine ug/kg 21703390 64 10-132
3-Nitroaniline ug/kg 20703390 61 55-130
4,6-Dinitro-2-methylphenol ug/kg 27403390 81 47-142
4-Bromophenylphenyl ether ug/kg 13001690 77 59-130
4-Chloro-3-methylphenol ug/kg 27203390 80 55-130
4-Chloroaniline ug/kg 22103390 65 54-130
4-Chlorophenylphenyl ether ug/kg 13501690 80 58-130
4-Nitroaniline ug/kg 23003390 68 54-130
4-Nitrophenol ug/kg 57708470 68 48-130
Acenaphthene ug/kg 14201690 84 60-130
Acenaphthylene ug/kg 14601690 86 60-130
Aniline ug/kg 9231690 54 43-130
Anthracene ug/kg 13501690 79 63-130
Benzo(a)anthracene ug/kg 14901690 88 59-130
Benzo(a)pyrene ug/kg 13701690 81 57-130
Benzo(b)fluoranthene ug/kg 13701690 81 54-130
Benzo(g,h,i)perylene ug/kg 14501690 86 59-130
Benzo(k)fluoranthene ug/kg 13301690 79 54-130
Benzoic Acid ug/kg 47808470 56 19-130
Benzyl alcohol ug/kg 19903390 59 50-130
bis(2-Chloroethoxy)methane ug/kg 12601690 74 54-130
bis(2-Chloroethyl) ether ug/kg 12501690 74 48-130
bis(2-Ethylhexyl)phthalate ug/kg 14701690 86 45-134
Butylbenzylphthalate ug/kg 14901690 88 46-138
Chrysene ug/kg 14601690 86 58-130
Di-n-butylphthalate ug/kg 13701690 81 60-130
Di-n-octylphthalate ug/kg 13901690 82 53-130
Dibenz(a,h)anthracene ug/kg 15101690 89 59-130
Dibenzofuran ug/kg 13101690 77 60-130
Diethylphthalate ug/kg 14601690 86 60-130
Dimethylphthalate ug/kg 13501690 79 60-130
Fluoranthene ug/kg 13601690 80 65-130
Fluorene ug/kg 14001690 82 63-130
Hexachloro-1,3-butadiene ug/kg 13101690 77 46-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2498910LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 13101690 77 58-130
Hexachlorocyclopentadiene ug/kg 11601690 68 23-130
Hexachloroethane ug/kg 11901690 70 47-130
Indeno(1,2,3-cd)pyrene ug/kg 14701690 87 60-130
Isophorone ug/kg 10701690 63 49-130
N-Nitroso-di-n-propylamine ug/kg 12801690 76 47-130
N-Nitrosodimethylamine ug/kg 10201690 60 45-130
N-Nitrosodiphenylamine ug/kg 12601690 74 59-130
Naphthalene ug/kg 13301690 78 55-130
Nitrobenzene ug/kg 11801690 69 49-130
Pentachlorophenol ug/kg 1670J3390 49 10-132
Phenanthrene ug/kg 13301690 79 62-130
Phenol ug/kg 12501690 73 46-130
Pyrene ug/kg 14301690 84 53-130
2,4,6-Tribromophenol (S)%80 27-110
2-Fluorobiphenyl (S)%71 30-110
2-Fluorophenol (S)%67 13-110
Nitrobenzene-d5 (S)%70 23-110
Phenol-d6 (S)%72 22-110
Terphenyl-d14 (S)%81 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2498911MATRIX SPIKE SAMPLE:
MSSpike
Result
92417820001
1,2,4-Trichlorobenzene ug/kg 11802090 57 18-130ND
1,2-Dichlorobenzene ug/kg 10102090 49 14-130ND
1,3-Dichlorobenzene ug/kg 10702090 52 12-130ND
1,4-Dichlorobenzene ug/kg 10702090 51 10-130ND
1-Methylnaphthalene ug/kg 13502090 65 12-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 10402090 50 10-130ND
2,4,5-Trichlorophenol ug/kg 12902090 62 13-130ND
2,4,6-Trichlorophenol ug/kg 14002090 67 17-130ND
2,4-Dichlorophenol ug/kg 12502090 60 10-130ND
2,4-Dimethylphenol ug/kg 13002090 62 10-130ND
2,4-Dinitrophenol ug/kg 699010400 67 10-130ND
2,4-Dinitrotoluene ug/kg 16602090 80 24-130ND
2,6-Dinitrotoluene ug/kg 16302090 78 23-130ND
2-Chloronaphthalene ug/kg 12502090 60 19-130ND
2-Chlorophenol ug/kg 11602090 56 10-130ND
2-Methylnaphthalene ug/kg 13102090 63 18-130ND
2-Methylphenol(o-Cresol)ug/kg 12802090 61 10-130ND
2-Nitroaniline ug/kg 25304160 61 17-130ND
2-Nitrophenol ug/kg 12402090 60 10-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 11702090 56 10-130ND
3,3'-Dichlorobenzidine ug/kg 26404160 63 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2498911MATRIX SPIKE SAMPLE:
MSSpike
Result
92417820001
3-Nitroaniline ug/kg 25904160 62 24-130ND
4,6-Dinitro-2-methylphenol ug/kg 31904160 77 10-152ND
4-Bromophenylphenyl ether ug/kg 13902090 67 29-130ND
4-Chloro-3-methylphenol ug/kg 28704160 69 17-130ND
4-Chloroaniline ug/kg 22604160 54 14-130ND
4-Chlorophenylphenyl ether ug/kg 13302090 64 25-130ND
4-Nitroaniline ug/kg 27304160 65 22-130ND
4-Nitrophenol ug/kg 699010400 67 10-130ND
Acenaphthene ug/kg 14302090 69 20-130ND
Acenaphthylene ug/kg 15002090 72 25-130ND
Aniline ug/kg 7742090 37 10-130ND
Anthracene ug/kg 15002090 72 29-130ND
Benzo(a)anthracene ug/kg 16402090 79 19-130ND
Benzo(a)pyrene ug/kg 15302090 73 12-130ND
Benzo(b)fluoranthene ug/kg 14802090 71 14-130ND
Benzo(g,h,i)perylene ug/kg 16202090 78 10-130ND
Benzo(k)fluoranthene ug/kg 14702090 71 14-130ND
Benzoic Acid ug/kg 520010400 50 10-130ND
Benzyl alcohol ug/kg 20004160 48 13-130ND
bis(2-Chloroethoxy)methane ug/kg 12602090 60 16-130ND
bis(2-Chloroethyl) ether ug/kg 11602090 56 11-130ND
bis(2-Ethylhexyl)phthalate ug/kg 18002090 86 21-130ND
Butylbenzylphthalate ug/kg 15102090 73 23-130ND
Chrysene ug/kg 17002090 82 22-130ND
Di-n-butylphthalate ug/kg 14902090 72 30-130ND
Di-n-octylphthalate ug/kg 17602090 85 23-142ND
Dibenz(a,h)anthracene ug/kg 17002090 82 10-130ND
Dibenzofuran ug/kg 13902090 67 24-130ND
Diethylphthalate ug/kg 15602090 75 26-130ND
Dimethylphthalate ug/kg 15902090 76 22-130ND
Fluoranthene ug/kg 14702090 71 33-130ND
Fluorene ug/kg 14002090 67 22-130ND
Hexachloro-1,3-butadiene ug/kg 11102090 54 13-130ND
Hexachlorobenzene ug/kg 14102090 68 29-130ND
Hexachlorocyclopentadiene ug/kg 9792090 47 10-130ND
Hexachloroethane ug/kg 10302090 49 10-130ND
Indeno(1,2,3-cd)pyrene ug/kg 16402090 79 10-130ND
Isophorone ug/kg 10702090 52 13-130ND
N-Nitroso-di-n-propylamine ug/kg 12802090 62 12-130ND
N-Nitrosodimethylamine ug/kg 9042090 43 11-130ND
N-Nitrosodiphenylamine ug/kg 14002090 67 15-130ND
Naphthalene ug/kg 12902090 62 15-130ND
Nitrobenzene ug/kg 11202090 54 12-130ND
Pentachlorophenol ug/kg 2020J4160 48 10-130ND
Phenanthrene ug/kg 14602090 70 27-130ND
Phenol ug/kg 11302090 55 10-130ND
Pyrene ug/kg 15502090 74 19-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 56 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2498911MATRIX SPIKE SAMPLE:
MSSpike
Result
92417820001
2,4,6-Tribromophenol (S)%75 27-110
2-Fluorobiphenyl (S)%55 30-110
2-Fluorophenol (S)%47 13-110
Nitrobenzene-d5 (S)%55 23-110
Phenol-d6 (S)%54 22-110
Terphenyl-d14 (S)%65 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92417820003
2498912SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92417820003
2498912SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%51119
2-Fluorobiphenyl (S)%47107
2-Fluorophenol (S)%4699
Nitrobenzene-d5 (S)%50107
Phenol-d6 (S)%4496
Terphenyl-d14 (S)%43109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
457452
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92417206002, 92417206003, 92417206004, 92417206005, 92417206006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92417140001
2495074SAMPLE DUPLICATE:
Percent Moisture %11.4 7 2512.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92417206007
2495075SAMPLE DUPLICATE:
Percent Moisture %23.8 0 2523.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 91
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417206
BCP-129
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
457521
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92417206009, 92417206010, 92417206011, 92417206012
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92416556005
2495323SAMPLE DUPLICATE:
Percent Moisture %97.6 0 2597.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92417129002
2495378SAMPLE DUPLICATE:
Percent Moisture %21.2 2 2520.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 91
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92417206
BCP-129
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 91
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92417206
BCP-129
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92417206002 457705 457833SB-2 (0-2)EPA 3546 EPA 8270D
92417206003 457705 457833SB-3 (0-2)EPA 3546 EPA 8270D
92417206004 457705 457833SB-4 (7-9)EPA 3546 EPA 8270D
92417206005 457705 457833SB-5 (0-2)EPA 3546 EPA 8270D
92417206006 458360 458649SB-6 (0-2)EPA 3546 EPA 8270D
92417206009 458360 458649SB-9 (0-2)EPA 3546 EPA 8270D
92417206010 458360 458649SB-10 (0-2)EPA 3546 EPA 8270D
92417206011 458360 458649SB-11 (0-2)EPA 3546 EPA 8270D
92417206012 458360 458649SB-12 (0-2)EPA 3546 EPA 8270D
92417206002 457453 457458SB-2 (0-2)EPA 5035A EPA 8260B
92417206003 457453 457458SB-3 (0-2)EPA 5035A EPA 8260B
92417206004 457453 457458SB-4 (7-9)EPA 5035A EPA 8260B
92417206005 457453 457458SB-5 (0-2)EPA 5035A EPA 8260B
92417206006 457453 457458SB-6 (0-2)EPA 5035A EPA 8260B
92417206009 457453 457458SB-9 (0-2)EPA 5035A EPA 8260B
92417206010 457453 457458SB-10 (0-2)EPA 5035A EPA 8260B
92417206011 457453 457458SB-11 (0-2)EPA 5035A EPA 8260B
92417206012 457453 457458SB-12 (0-2)EPA 5035A EPA 8260B
92417206002 457452SB-2 (0-2)ASTM D2974-87
92417206003 457452SB-3 (0-2)ASTM D2974-87
92417206004 457452SB-4 (7-9)ASTM D2974-87
92417206005 457452SB-5 (0-2)ASTM D2974-87
92417206006 457452SB-6 (0-2)ASTM D2974-87
92417206009 457521SB-9 (0-2)ASTM D2974-87
92417206010 457521SB-10 (0-2)ASTM D2974-87
92417206011 457521SB-11 (0-2)ASTM D2974-87
92417206012 457521SB-12 (0-2)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2019 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 91
Page 63 of 91
Page 64 of 91
Page 65 of 91
ANALYTICAL REPORT
June 25, 2019
Pace Analytical - Huntersville, NC
Sample Delivery Group:L1069045
Samples Received:02/12/2019
Project Number:92417206
Description:BCP-129
Site:001
Report To:Kevin Godwin
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By:
June 25, 2019
[Preliminary Report]
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Nationalis performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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June 25, 2019
Nancy McLain
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Huntersville, NC 92417206 L1069045 06/25/19 13:59 1 of 26
Page 66 of 91
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 5
Sr: Sample Results 6
SB-2 (0-2) L1069045-02 6
SB-3 (0-2) L1069045-03 7
SB-4 (7-9) L1069045-04 8
SB-5 (0-2) L1069045-05 9
SB-6 (0-2) L1069045-06 10
SB-9 (0-2) L1069045-09 11
SB-10 (0-2) L1069045-10 12
SB-11 (0-2) L1069045-11 13
SB-12 (0-2) L1069045-12 14
Qc: Quality Control Summary 15
Total Solids by Method 2540 G-2011 15
Wet Chemistry by Method 7199 18
Mercury by Method 7471B 19
Metals (ICPMS) by Method 6020B 21
Gl: Glossary of Terms 22
Al: Accreditations & Locations 23
Sc: Sample Chain of Custody 24
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 67 of 91
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-2 (0-2) L1069045-02 Solid 02/07/19 17:00 02/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1236468 1 02/13/19 15:26 02/13/19 15:59 JD Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1237805 1 02/18/19 13:32 02/19/19 13:04 MCG Mt. Juliet, TN
Mercury by Method 7471B WG1236131 1 02/12/19 20:21 02/13/19 10:40 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 5 02/13/19 15:34 02/16/19 14:20 JPD Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-3 (0-2) L1069045-03 Solid 02/07/19 17:00 02/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1236468 1 02/13/19 15:26 02/13/19 15:59 JD Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1237805 1 02/18/19 13:32 02/19/19 13:09 MCG Mt. Juliet, TN
Mercury by Method 7471B WG1236131 1 02/12/19 20:21 02/13/19 10:43 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 5 02/13/19 15:34 02/16/19 14:25 JPD Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-4 (7-9) L1069045-04 Solid 02/08/19 13:00 02/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1236468 1 02/13/19 15:26 02/13/19 15:59 JD Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1237805 1 02/18/19 13:32 02/19/19 13:14 MCG Mt. Juliet, TN
Mercury by Method 7471B WG1236131 1 02/12/19 20:21 02/13/19 10:45 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 5 02/13/19 15:34 02/16/19 14:29 JPD Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-5 (0-2) L1069045-05 Solid 02/07/19 13:15 02/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1236468 1 02/13/19 15:26 02/13/19 15:59 JD Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1237805 1 02/18/19 13:32 02/19/19 13:19 MCG Mt. Juliet, TN
Mercury by Method 7471B WG1236131 1 02/12/19 20:21 02/13/19 10:48 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 5 02/13/19 15:34 02/16/19 14:34 JPD Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-6 (0-2) L1069045-06 Solid 02/07/19 15:00 02/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1236468 1 02/13/19 15:26 02/13/19 15:59 JD Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1237805 1 02/18/19 13:32 02/19/19 13:24 MCG Mt. Juliet, TN
Mercury by Method 7471B WG1236131 1 02/12/19 20:21 02/13/19 10:55 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 5 02/13/19 15:34 02/16/19 14:38 JPD Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-9 (0-2) L1069045-09 Solid 02/08/19 14:00 02/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1236547 1 02/13/19 13:30 02/13/19 13:39 JD Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1237805 1 02/18/19 13:32 02/19/19 13:50 MCG Mt. Juliet, TN
Mercury by Method 7471B WG1236332 1 02/13/19 08:55 02/13/19 17:21 TCT Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 5 02/13/19 15:34 02/16/19 15:19 JPD Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 68 of 91
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SB-10 (0-2) L1069045-10 Solid 02/08/19 14:30 02/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1236547 1 02/13/19 13:30 02/13/19 13:39 JD Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1237805 1 02/18/19 13:32 02/19/19 13:56 MCG Mt. Juliet, TN
Mercury by Method 7471B WG1236332 1 02/13/19 08:55 02/13/19 17:23 TCT Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 5 02/13/19 15:34 02/16/19 15:23 JPD Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-11 (0-2) L1069045-11 Solid 02/08/19 15:00 02/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1236548 1 02/13/19 13:58 02/13/19 14:08 JD Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1237805 1 02/18/19 13:32 02/19/19 14:01 MCG Mt. Juliet, TN
Mercury by Method 7471B WG1236332 1 02/13/19 08:55 02/13/19 17:26 TCT Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 10 02/13/19 15:34 02/16/19 15:37 JPD Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 5 02/13/19 15:34 02/16/19 15:28 JPD Mt. Juliet, TN
Collected by Collected date/time Received date/time
SB-12 (0-2) L1069045-12 Solid 02/08/19 15:30 02/12/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1236548 1 02/13/19 13:58 02/13/19 14:08 JD Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1237805 1 02/18/19 13:32 02/19/19 14:06 MCG Mt. Juliet, TN
Mercury by Method 7471B WG1236332 1 02/13/19 08:55 02/13/19 17:28 TCT Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 10 02/13/19 15:34 02/16/19 15:42 JPD Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1236117 5 02/13/19 15:34 02/16/19 15:32 JPD Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 69 of 91
ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Nancy McLain
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Huntersville, NC 92417206 L1069045 06/25/19 13:42 5 of 26
Nancy McLain
Project Manager
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1069045
SB-2 (0-2)
Collected date/time: 02/07/19 17:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 95.7 1 02/13/2019 15:59 WG1236468
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium 0.726 J 0.266 1.04 1 02/19/2019 13:04 WG1237805
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0929 0.00292 0.0209 1 02/13/2019 10:40 WG1236131
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.64 0.131 0.522 5 02/16/2019 14:20 WG1236117
Barium 56.5 0.167 1.04 5 02/16/2019 14:20 WG1236117
Cadmium U 0.0836 0.522 5 02/16/2019 14:20 WG1236117
Chromium 77.1 0.282 1.04 5 02/16/2019 14:20 WG1236117
Lead 22.6 0.125 0.522 5 02/16/2019 14:20 WG1236117
Selenium 0.545 0.198 0.522 5 02/16/2019 14:20 WG1236117
Silver U 0.162 0.522 5 02/16/2019 14:20 WG1236117
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1069045
SB-3 (0-2)
Collected date/time: 02/07/19 17:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 95.9 1 02/13/2019 15:59 WG1236468
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium 0.686 J 0.266 1.04 1 02/19/2019 13:09 WG1237805
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0883 0.00292 0.0209 1 02/13/2019 10:43 WG1236131
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.76 0.130 0.521 5 02/16/2019 14:25 WG1236117
Barium 75.3 0.167 1.04 5 02/16/2019 14:25 WG1236117
Cadmium U 0.0834 0.521 5 02/16/2019 14:25 WG1236117
Chromium 91.4 0.282 1.04 5 02/16/2019 14:25 WG1236117
Lead 22.9 0.125 0.521 5 02/16/2019 14:25 WG1236117
Selenium 0.721 0.198 0.521 5 02/16/2019 14:25 WG1236117
Silver U 0.162 0.521 5 02/16/2019 14:25 WG1236117
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1069045
SB-4 (7-9)
Collected date/time: 02/08/19 13:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.9 1 02/13/2019 15:59 WG1236468
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium U 0.315 1.24 1 02/19/2019 13:14 WG1237805
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0528 0.00346 0.0247 1 02/13/2019 10:45 WG1236131
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.33 0.155 0.618 5 02/16/2019 14:29 WG1236117
Barium 86.0 0.198 1.24 5 02/16/2019 14:29 WG1236117
Cadmium U 0.0989 0.618 5 02/16/2019 14:29 WG1236117
Chromium 38.3 0.334 1.24 5 02/16/2019 14:29 WG1236117
Lead 10.1 0.148 0.618 5 02/16/2019 14:29 WG1236117
Selenium 0.521 J 0.235 0.618 5 02/16/2019 14:29 WG1236117
Silver U 0.192 0.618 5 02/16/2019 14:29 WG1236117
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1069045
SB-5 (0-2)
Collected date/time: 02/07/19 13:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 75.0 1 02/13/2019 15:59 WG1236468
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium U 0.340 1.33 1 02/19/2019 13:19 WG1237805
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.290 0.00374 0.0267 1 02/13/2019 10:48 WG1236131
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.75 0.167 0.667 5 02/16/2019 14:34 WG1236117
Barium 58.7 0.213 1.33 5 02/16/2019 14:34 WG1236117
Cadmium U 0.107 0.667 5 02/16/2019 14:34 WG1236117
Chromium 37.5 0.360 1.33 5 02/16/2019 14:34 WG1236117
Lead 10.6 0.160 0.667 5 02/16/2019 14:34 WG1236117
Selenium 0.466 J 0.253 0.667 5 02/16/2019 14:34 WG1236117
Silver U 0.207 0.667 5 02/16/2019 14:34 WG1236117
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L1069045
SB-6 (0-2)
Collected date/time: 02/07/19 15:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 77.8 1 02/13/2019 15:59 WG1236468
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium 0.392 J 0.328 1.28 1 02/19/2019 13:24 WG1237805
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0827 0.00360 0.0257 1 02/13/2019 10:55 WG1236131
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 3.07 0.161 0.642 5 02/16/2019 14:38 WG1236117
Barium 87.9 0.206 1.28 5 02/16/2019 14:38 WG1236117
Cadmium U 0.103 0.642 5 02/16/2019 14:38 WG1236117
Chromium 46.5 0.347 1.28 5 02/16/2019 14:38 WG1236117
Lead 32.9 0.154 0.642 5 02/16/2019 14:38 WG1236117
Selenium 0.875 0.244 0.642 5 02/16/2019 14:38 WG1236117
Silver U 0.199 0.642 5 02/16/2019 14:38 WG1236117
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L1069045
SB-9 (0-2)
Collected date/time: 02/08/19 14:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.3 1 02/13/2019 13:39 WG1236547
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium 0.913 J 0.321 1.26 1 02/19/2019 13:50 WG1237805
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0616 0.00353 0.0252 1 02/13/2019 17:21 WG1236332
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 1.92 0.158 0.630 5 02/16/2019 15:19 WG1236117
Barium 86.4 0.202 1.26 5 02/16/2019 15:19 WG1236117
Cadmium U 0.101 0.630 5 02/16/2019 15:19 WG1236117
Chromium 77.3 0.340 1.26 5 02/16/2019 15:19 WG1236117
Lead 10.0 0.151 0.630 5 02/16/2019 15:19 WG1236117
Selenium 0.703 0.240 0.630 5 02/16/2019 15:19 WG1236117
Silver U 0.195 0.630 5 02/16/2019 15:19 WG1236117
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L1069045
SB-10 (0-2)
Collected date/time: 02/08/19 14:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.1 1 02/13/2019 13:39 WG1236547
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium U 0.327 1.28 1 02/19/2019 13:56 WG1237805
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0431 0.00359 0.0256 1 02/13/2019 17:23 WG1236332
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 1.42 0.160 0.641 5 02/16/2019 15:23 WG1236117
Barium 105 0.205 1.28 5 02/16/2019 15:23 WG1236117
Cadmium U 0.102 0.641 5 02/16/2019 15:23 WG1236117
Chromium 51.7 0.346 1.28 5 02/16/2019 15:23 WG1236117
Lead 6.95 0.154 0.641 5 02/16/2019 15:23 WG1236117
Selenium 0.645 0.243 0.641 5 02/16/2019 15:23 WG1236117
Silver U 0.199 0.641 5 02/16/2019 15:23 WG1236117
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L1069045
SB-11 (0-2)
Collected date/time: 02/08/19 15:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.1 1 02/13/2019 14:08 WG1236548
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium 0.376 J 0.318 1.25 1 02/19/2019 14:01 WG1237805
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0495 0.00349 0.0250 1 02/13/2019 17:26 WG1236332
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.10 0.156 0.624 5 02/16/2019 15:28 WG1236117
Barium 127 0.399 2.50 10 02/16/2019 15:37 WG1236117
Cadmium U 0.0998 0.624 5 02/16/2019 15:28 WG1236117
Chromium 56.0 0.337 1.25 5 02/16/2019 15:28 WG1236117
Lead 10.7 0.150 0.624 5 02/16/2019 15:28 WG1236117
Selenium 0.794 0.237 0.624 5 02/16/2019 15:28 WG1236117
Silver U 0.193 0.624 5 02/16/2019 15:28 WG1236117
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L1069045
SB-12 (0-2)
Collected date/time: 02/08/19 15:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.0 1 02/13/2019 14:08 WG1236548
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium U 0.327 1.28 1 02/19/2019 14:06 WG1237805
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury U 0.00359 0.0256 1 02/13/2019 17:28 WG1236332
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.28 0.160 0.641 5 02/16/2019 15:32 WG1236117
Barium 118 0.410 2.56 10 02/16/2019 15:42 WG1236117
Cadmium U 0.103 0.641 5 02/16/2019 15:32 WG1236117
Chromium 169 0.692 2.56 10 02/16/2019 15:42 WG1236117
Lead 12.8 0.154 0.641 5 02/16/2019 15:32 WG1236117
Selenium 1.26 0.244 0.641 5 02/16/2019 15:32 WG1236117
Silver U 0.199 0.641 5 02/16/2019 15:32 WG1236117
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1236468
Total Solids by Method 2540 G-2011 L1069045-02,03,04,05,06
Method Blank (MB)
(MB) R3383694-1 02/13/19 15:59
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1069045-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1069045-04 02/13/19 15:59 • (DUP) R3383694-3 02/13/19 15:59
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 80.9 78.7 1 2.66 10
Laboratory Control Sample (LCS)
(LCS) R3383694-2 02/13/19 15:59
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1236547
Total Solids by Method 2540 G-2011 L1069045-09,10
Method Blank (MB)
(MB) R3383736-1 02/13/19 13:39
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1069394-11 Original Sample (OS) • Duplicate (DUP)
(OS) L1069394-11 02/13/19 13:39 • (DUP) R3383736-3 02/13/19 13:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 92.8 92.7 1 0.0617 10
Laboratory Control Sample (LCS)
(LCS) R3383736-2 02/13/19 13:39
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1236548
Total Solids by Method 2540 G-2011 L1069045-11,12
Method Blank (MB)
(MB) R3383739-1 02/13/19 14:08
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00200
L1069071-08 Original Sample (OS) • Duplicate (DUP)
(OS) L1069071-08 02/13/19 14:08 • (DUP) R3383739-3 02/13/19 14:08
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 88.4 89.2 1 0.824 10
Laboratory Control Sample (LCS)
(LCS) R3383739-2 02/13/19 14:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1237805
Wet Chemistry by Method 7199 L1069045-02,03,04,05,06,09,10,11,12
Method Blank (MB)
(MB) R3385040-1 02/19/19 12:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1069040-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1069040-01 02/19/19 12:48 • (DUP) R3385040-3 02/19/19 12:53
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium U 0.000 1 0.000 20
L1070497-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1070497-01 02/19/19 14:47 • (DUP) R3385040-7 02/19/19 14:53
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND 0.000 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3385040-2 02/19/19 12:43
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 9.65 96.5 80.0-120
L1070111-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1070111-01 02/19/19 14:11 • (MS) R3385040-4 02/19/19 14:16 • (MSD) R3385040-5 02/19/19 14:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 20.0 ND 16.9 18.1 84.4 90.7 1 75.0-125 7.21 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1236131
Mercury by Method 7471B L1069045-02,03,04,05,06
Method Blank (MB)
(MB) R3383381-5 02/13/19 12:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.00280 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3383381-1 02/13/19 09:59 • (LCSD) R3383381-2 02/13/19 10:02
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.500 0.509 0.510 102 102 80.0-120 0.0889 20
L1069197-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1069197-03 02/13/19 10:04 • (MS) R3383381-3 02/13/19 10:07 • (MSD) R3383381-4 02/13/19 10:09
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.500 0.00284 0.529 0.506 105 101 1 75.0-125 4.57 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1236332
Mercury by Method 7471B L1069045-09,10,11,12
Method Blank (MB)
(MB) R3383568-1 02/13/19 16:55
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.00280 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3383568-2 02/13/19 16:58 • (LCSD) R3383568-3 02/13/19 17:00
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.500 0.511 0.494 102 98.8 80.0-120 3.44 20
L1069106-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1069106-03 02/13/19 17:03 • (MS) R3383568-4 02/13/19 17:06 • (MSD) R3383568-5 02/13/19 17:16
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.550 0.0102 0.511 0.583 91.0 104 1 75.0-125 13.1 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1236117
Metals (ICPMS) by Method 6020B L1069045-02,03,04,05,06,09,10,11,12
Method Blank (MB)
(MB) R3384352-1 02/16/19 13:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.125 0.500
Barium U 0.160 1.00
Cadmium U 0.0800 0.500
Chromium U 0.270 1.00
Lead U 0.120 0.500
Selenium U 0.190 0.500
Silver U 0.155 0.500
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3384352-2 02/16/19 13:11 • (LCSD) R3384352-3 02/16/19 13:16
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Arsenic 100 96.3 92.0 96.3 92.0 80.0-120 4.58 20
Barium 100 101 95.2 101 95.2 80.0-120 5.93 20
Cadmium 100 97.8 94.4 97.8 94.4 80.0-120 3.49 20
Chromium 100 97.4 93.6 97.4 93.6 80.0-120 3.96 20
Lead 100 97.2 94.0 97.2 94.0 80.0-120 3.35 20
Selenium 100 105 98.7 105 98.7 80.0-120 6.52 20
Silver 100 101 97.2 101 97.2 80.0-120 3.71 20
L1069024-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1069024-01 02/16/19 13:20 • (MS) R3384352-6 02/16/19 13:34 • (MSD) R3384352-7 02/16/19 13:38
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 28.0 3.15 136 132 95.1 92.2 5 75.0-125 3.08 20
Barium 28.0 28.5 201 188 123 114 5 75.0-125 6.74 20
Cadmium 28.0 U 147 143 105 102 5 75.0-125 2.67 20
Chromium 28.0 26.8 179 219 109 137 5 75.0-125 J3 J5 20.3 20
Lead 28.0 7.28 152 148 104 100 5 75.0-125 3.08 20
Selenium 28.0 1.06 147 144 104 102 5 75.0-125 2.30 20
Silver 28.0 U 150 146 107 104 5 75.0-125 2.70 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 87 of 91
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 91 of 91
#=CL#
June 27, 2019
LIMS USE: FR - BO CAPPLEMAN
LIMS OBJECT ID: 92417688
92417688
Project:
Pace Project No.:
RE:
Bo Cappleman
Hart & Hickman
2923 South Tryon Street
Charlotte, NC 28203
BCP-129 Gresco Street Facility
Dear Bo Cappleman:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
Per client request, report revised 6/27/19 to relocate samples TMW-1, TMW-3, TMW-4, TMW-3-
F,and GW Dup-1 to a separate project.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 43
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 43
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Lab ID Sample ID Matrix Date Collected Date Received
92417688002 TMW-2 Water 02/12/19 19:45 02/13/19 13:55
92417688006 Trip Blank Water 02/12/19 00:00 02/13/19 13:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 43
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92417688002 TMW-2 EPA 8270D 74 PASI-CPKS
EPA 8260B 63 PASI-CSAS
92417688006 Trip Blank EPA 8260B 63 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Sample: TMW-2 Lab ID: 92417688002 Collected: 02/12/19 19:45 Received: 02/13/19 13:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 3510C8270 RVE
Acenaphthene ND ug/L 02/19/19 14:49 83-32-902/18/19 21:3710.0 3.4 1
Acenaphthylene ND ug/L 02/19/19 14:49 208-96-802/18/19 21:3710.0 3.0 1
Aniline ND ug/L 02/19/19 14:49 62-53-302/18/19 21:3710.0 3.1 1
Anthracene ND ug/L 02/19/19 14:49 120-12-702/18/19 21:3710.0 2.0 1
Benzo(a)anthracene ND ug/L 02/19/19 14:49 56-55-302/18/19 21:3710.0 1.3 1
Benzo(a)pyrene ND ug/L 02/19/19 14:49 50-32-802/18/19 21:3710.0 1.3 1
Benzo(b)fluoranthene ND ug/L 02/19/19 14:49 205-99-202/18/19 21:3710.0 1.5 1
Benzo(g,h,i)perylene ND ug/L 02/19/19 14:49 191-24-202/18/19 21:3710.0 1.8 1
Benzo(k)fluoranthene ND ug/L 02/19/19 14:49 207-08-902/18/19 21:3710.0 1.8 1
Benzoic Acid ND ug/L 02/19/19 14:49 65-85-002/18/19 21:3750.0 17.3 1
Benzyl alcohol ND ug/L 02/19/19 14:49 100-51-602/18/19 21:3720.0 7.0 1
4-Bromophenylphenyl ether ND ug/L 02/19/19 14:49 101-55-302/18/19 21:3710.0 2.7 1
Butylbenzylphthalate ND ug/L 02/19/19 14:49 85-68-702/18/19 21:3710.0 1.3 1
4-Chloro-3-methylphenol ND ug/L 02/19/19 14:49 59-50-702/18/19 21:3720.0 4.6 1
4-Chloroaniline ND ug/L 02/19/19 14:49 106-47-802/18/19 21:3720.0 6.8 1
bis(2-Chloroethoxy)methane ND ug/L 02/19/19 14:49 111-91-102/18/19 21:3710.0 3.0 1
bis(2-Chloroethyl) ether ND ug/L 02/19/19 14:49 111-44-402/18/19 21:3710.0 3.1 1
2-Chloronaphthalene ND ug/L 02/19/19 14:49 91-58-702/18/19 21:3710.0 2.9 1
2-Chlorophenol ND ug/L 02/19/19 14:49 95-57-802/18/19 21:3710.0 2.9 1
4-Chlorophenylphenyl ether ND ug/L 02/19/19 14:49 7005-72-302/18/19 21:3710.0 2.9 1
Chrysene ND ug/L 02/19/19 14:49 218-01-902/18/19 21:3710.0 1.2 1
Dibenz(a,h)anthracene ND ug/L 02/19/19 14:49 53-70-302/18/19 21:3710.0 1.9 1
Dibenzofuran ND ug/L 02/19/19 14:49 132-64-902/18/19 21:3710.0 3.4 1
1,2-Dichlorobenzene ND ug/L 02/19/19 14:49 95-50-102/18/19 21:3710.0 3.2 1
1,3-Dichlorobenzene ND ug/L 02/19/19 14:49 541-73-102/18/19 21:3710.0 3.2 1
1,4-Dichlorobenzene ND ug/L 02/19/19 14:49 106-46-702/18/19 21:3710.0 2.6 1
3,3'-Dichlorobenzidine ND ug/L 02/19/19 14:49 91-94-102/18/19 21:3720.0 2.8 1
2,4-Dichlorophenol ND ug/L 02/19/19 14:49 120-83-202/18/19 21:3710.0 2.7 1
Diethylphthalate ND ug/L 02/19/19 14:49 84-66-202/18/19 21:3710.0 2.0 1
2,4-Dimethylphenol ND ug/L 02/19/19 14:49 105-67-902/18/19 21:3710.0 1.9 1
Dimethylphthalate ND ug/L 02/19/19 14:49 131-11-302/18/19 21:3710.0 2.3 1
Di-n-butylphthalate ND ug/L 02/19/19 14:49 84-74-202/18/19 21:3710.0 1.2 1
4,6-Dinitro-2-methylphenol ND ug/L 02/19/19 14:49 534-52-102/18/19 21:3720.0 4.4 1
2,4-Dinitrophenol ND ug/L 02/19/19 14:49 51-28-502/18/19 21:3750.0 10.1 1
2,4-Dinitrotoluene ND ug/L 02/19/19 14:49 121-14-202/18/19 21:3710.0 2.4 1
2,6-Dinitrotoluene ND ug/L 02/19/19 14:49 606-20-202/18/19 21:3710.0 2.9 1
Di-n-octylphthalate ND ug/L 02/19/19 14:49 117-84-002/18/19 21:3710.0 1.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 02/19/19 14:49 117-81-702/18/19 21:376.0 1.4 1
Fluoranthene ND ug/L 02/19/19 14:49 206-44-002/18/19 21:3710.0 1.7 1
Fluorene ND ug/L 02/19/19 14:49 86-73-702/18/19 21:3710.0 3.0 1
Hexachloro-1,3-butadiene ND ug/L 02/19/19 14:49 87-68-302/18/19 21:3710.0 3.1 1
Hexachlorobenzene ND ug/L 02/19/19 14:49 118-74-102/18/19 21:3710.0 2.5 1
Hexachlorocyclopentadiene ND ug/L 02/19/19 14:49 77-47-402/18/19 21:3710.0 3.4 1
Hexachloroethane ND ug/L 02/19/19 14:49 67-72-102/18/19 21:3710.0 4.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 02/19/19 14:49 193-39-502/18/19 21:3710.0 1.7 1
Isophorone ND ug/L 02/19/19 14:49 78-59-102/18/19 21:3710.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Sample: TMW-2 Lab ID: 92417688002 Collected: 02/12/19 19:45 Received: 02/13/19 13:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 3510C8270 RVE
1-Methylnaphthalene ND ug/L 02/19/19 14:49 90-12-002/18/19 21:3710.0 2.8 1
2-Methylnaphthalene ND ug/L 02/19/19 14:49 91-57-602/18/19 21:3710.0 2.8 1
2-Methylphenol(o-Cresol)ND ug/L 02/19/19 14:49 95-48-702/18/19 21:3710.0 3.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 02/19/19 14:49 15831-10-402/18/19 21:3710.0 2.4 1
Naphthalene ND ug/L 02/19/19 14:49 91-20-302/18/19 21:3710.0 3.2 1
2-Nitroaniline ND ug/L 02/19/19 14:49 88-74-402/18/19 21:3750.0 5.5 1
3-Nitroaniline ND ug/L 02/19/19 14:49 99-09-202/18/19 21:3750.0 5.0 1
4-Nitroaniline ND ug/L 02/19/19 14:49 100-01-602/18/19 21:3720.0 3.6 1
Nitrobenzene ND ug/L 02/19/19 14:49 98-95-302/18/19 21:3710.0 3.4 1
2-Nitrophenol ND ug/L 02/19/19 14:49 88-75-502/18/19 21:3710.0 2.6 1
4-Nitrophenol ND ug/L 02/19/19 14:49 100-02-702/18/19 21:3750.0 7.8 1
N-Nitrosodimethylamine ND ug/L 02/19/19 14:49 62-75-902/18/19 21:3710.0 2.8 1
N-Nitroso-di-n-propylamine ND ug/L 02/19/19 14:49 621-64-702/18/19 21:3710.0 2.6 1
N-Nitrosodiphenylamine ND ug/L 02/19/19 14:49 86-30-602/18/19 21:3710.0 2.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 02/19/19 14:49 108-60-102/18/19 21:3710.0 2.5 1
Pentachlorophenol ND ug/L 02/19/19 14:49 87-86-502/18/19 21:3725.0 3.1 1
Phenanthrene ND ug/L 02/19/19 14:49 85-01-802/18/19 21:3710.0 2.4 1
Phenol ND ug/L 02/19/19 14:49 108-95-202/18/19 21:3710.0 2.7 1
Pyrene ND ug/L 02/19/19 14:49 129-00-002/18/19 21:3710.0 1.2 1
1,2,4-Trichlorobenzene ND ug/L 02/19/19 14:49 120-82-102/18/19 21:3710.0 2.6 1
2,4,5-Trichlorophenol ND ug/L 02/19/19 14:49 95-95-402/18/19 21:3710.0 2.3 1
2,4,6-Trichlorophenol ND ug/L 02/19/19 14:49 88-06-202/18/19 21:3710.0 2.8 1
Surrogates
Nitrobenzene-d5 (S)50 %02/19/19 14:49 4165-60-002/18/19 21:3713-130 1
2-Fluorobiphenyl (S)45 %02/19/19 14:49 321-60-802/18/19 21:3713-130 1
Terphenyl-d14 (S)63 %02/19/19 14:49 1718-51-002/18/19 21:3725-130 1
Phenol-d6 (S)13 %02/19/19 14:49 13127-88-302/18/19 21:3710-130 1
2-Fluorophenol (S)20 %02/19/19 14:49 367-12-402/18/19 21:3710-130 1
2,4,6-Tribromophenol (S)15 %02/19/19 14:49 118-79-602/18/19 21:3710-137 1
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 02/14/19 14:11 67-64-125.0 6.2 1
Benzene 3.3 ug/L 02/14/19 14:11 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/14/19 14:11 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/14/19 14:11 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/14/19 14:11 75-27-41.0 0.26 1
Bromoform ND ug/L 02/14/19 14:11 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/14/19 14:11 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/14/19 14:11 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/14/19 14:11 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/14/19 14:11 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/14/19 14:11 75-00-31.0 0.49 1
Chloroform ND ug/L 02/14/19 14:11 67-66-35.0 2.3 1
Chloromethane ND ug/L 02/14/19 14:11 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 02/14/19 14:11 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/14/19 14:11 106-43-41.0 0.20 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
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Page 6 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Sample: TMW-2 Lab ID: 92417688002 Collected: 02/12/19 19:45 Received: 02/13/19 13:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 02/14/19 14:11 96-12-82.0 0.26 1
Dibromochloromethane ND ug/L 02/14/19 14:11 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/14/19 14:11 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/14/19 14:11 74-95-31.0 0.46 1
1,2-Dichlorobenzene 2.8 ug/L 02/14/19 14:11 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/14/19 14:11 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/14/19 14:11 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/14/19 14:11 75-71-81.0 0.23 1
1,1-Dichloroethane 0.34J ug/L 02/14/19 14:11 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/14/19 14:11 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/14/19 14:11 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 8.6 ug/L 02/14/19 14:11 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/14/19 14:11 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/14/19 14:11 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/14/19 14:11 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/14/19 14:11 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/14/19 14:11 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/14/19 14:11 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/14/19 14:11 10061-02-61.0 0.31 1
Diisopropyl ether 2.2 ug/L 02/14/19 14:11 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/14/19 14:11 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/14/19 14:11 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/14/19 14:11 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/14/19 14:11 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/14/19 14:11 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/14/19 14:11 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/14/19 14:11 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/14/19 14:11 91-20-31.0 0.35 1
Styrene ND ug/L 02/14/19 14:11 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/14/19 14:11 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/14/19 14:11 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 02/14/19 14:11 127-18-41.0 0.16 1
Toluene ND ug/L 02/14/19 14:11 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/14/19 14:11 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/14/19 14:11 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/14/19 14:11 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/14/19 14:11 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/14/19 14:11 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/14/19 14:11 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/14/19 14:11 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/14/19 14:11 108-05-42.0 1.4 1
Vinyl chloride 0.77J ug/L 02/14/19 14:11 75-01-41.0 0.24 1
Xylene (Total)1.5 ug/L 02/14/19 14:11 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/14/19 14:11 179601-23-12.0 0.41 1
o-Xylene 1.5 ug/L 02/14/19 14:11 95-47-61.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
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[phone]
Page 7 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Sample: TMW-2 Lab ID: 92417688002 Collected: 02/12/19 19:45 Received: 02/13/19 13:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)98 %02/14/19 14:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %02/14/19 14:11 17060-07-070-130 1
Toluene-d8 (S)101 %02/14/19 14:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Sample: Trip Blank Lab ID: 92417688006 Collected: 02/12/19 00:00 Received: 02/13/19 13:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 02/14/19 08:34 67-64-125.0 6.2 1
Benzene ND ug/L 02/14/19 08:34 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/14/19 08:34 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/14/19 08:34 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/14/19 08:34 75-27-41.0 0.26 1
Bromoform ND ug/L 02/14/19 08:34 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/14/19 08:34 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/14/19 08:34 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/14/19 08:34 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/14/19 08:34 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/14/19 08:34 75-00-31.0 0.49 1
Chloroform ND ug/L 02/14/19 08:34 67-66-35.0 2.3 1
Chloromethane ND ug/L 02/14/19 08:34 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 02/14/19 08:34 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/14/19 08:34 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/14/19 08:34 96-12-82.0 0.26 1
Dibromochloromethane ND ug/L 02/14/19 08:34 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/14/19 08:34 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/14/19 08:34 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/14/19 08:34 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/14/19 08:34 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/14/19 08:34 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/14/19 08:34 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/14/19 08:34 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/14/19 08:34 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/14/19 08:34 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/14/19 08:34 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/14/19 08:34 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/14/19 08:34 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/14/19 08:34 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/14/19 08:34 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/14/19 08:34 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/14/19 08:34 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/14/19 08:34 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/14/19 08:34 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/14/19 08:34 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/14/19 08:34 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/14/19 08:34 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/14/19 08:34 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/14/19 08:34 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/14/19 08:34 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/14/19 08:34 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/14/19 08:34 91-20-31.0 0.35 1
Styrene ND ug/L 02/14/19 08:34 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/14/19 08:34 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/14/19 08:34 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Sample: Trip Blank Lab ID: 92417688006 Collected: 02/12/19 00:00 Received: 02/13/19 13:55 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV Low Level
Tetrachloroethene ND ug/L 02/14/19 08:34 127-18-41.0 0.16 1
Toluene ND ug/L 02/14/19 08:34 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/14/19 08:34 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/14/19 08:34 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/14/19 08:34 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/14/19 08:34 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/14/19 08:34 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/14/19 08:34 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/14/19 08:34 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/14/19 08:34 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/14/19 08:34 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 02/14/19 08:34 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/14/19 08:34 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/14/19 08:34 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)101 %02/14/19 08:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %02/14/19 08:34 17060-07-070-130 1
Toluene-d8 (S)117 %02/14/19 08:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458039
EPA 8260B
EPA 8260B
8260 MSV Low Level
Associated Lab Samples: 92417688006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2497594
Associated Lab Samples:92417688006
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/14/19 01:250.34
1,1,1-Trichloroethane ug/L ND 1.0 02/14/19 01:250.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/14/19 01:250.22
1,1,2-Trichloroethane ug/L ND 1.0 02/14/19 01:250.24
1,1-Dichloroethane ug/L ND 1.0 02/14/19 01:250.27
1,1-Dichloroethene ug/L ND 1.0 02/14/19 01:250.24
1,1-Dichloropropene ug/L ND 1.0 02/14/19 01:250.21
1,2,3-Trichlorobenzene ug/L ND 1.0 02/14/19 01:250.34
1,2,3-Trichloropropane ug/L ND 1.0 02/14/19 01:250.35
1,2,4-Trichlorobenzene ug/L ND 1.0 02/14/19 01:250.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 02/14/19 01:250.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/14/19 01:250.26
1,2-Dichlorobenzene ug/L ND 1.0 02/14/19 01:250.29
1,2-Dichloroethane ug/L ND 1.0 02/14/19 01:250.34
1,2-Dichloropropane ug/L ND 1.0 02/14/19 01:250.19
1,3-Dichlorobenzene ug/L ND 1.0 02/14/19 01:250.22
1,3-Dichloropropane ug/L ND 1.0 02/14/19 01:250.16
1,4-Dichlorobenzene ug/L ND 1.0 02/14/19 01:250.26
2,2-Dichloropropane ug/L ND 1.0 02/14/19 01:250.27
2-Butanone (MEK)ug/L ND 5.0 02/14/19 01:253.3
2-Chlorotoluene ug/L ND 1.0 02/14/19 01:250.20
2-Hexanone ug/L ND 5.0 02/14/19 01:250.57
4-Chlorotoluene ug/L ND 1.0 02/14/19 01:250.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/14/19 01:254.5
Acetone ug/L ND 25.0 02/14/19 01:256.2
Benzene ug/L ND 1.0 02/14/19 01:250.15
Bromobenzene ug/L ND 1.0 02/14/19 01:250.22
Bromochloromethane ug/L ND 1.0 02/14/19 01:250.34
Bromodichloromethane ug/L ND 1.0 02/14/19 01:250.26
Bromoform ug/L ND 1.0 02/14/19 01:250.62
Bromomethane ug/L ND 2.0 02/14/19 01:250.62
Carbon tetrachloride ug/L ND 1.0 02/14/19 01:250.22
Chlorobenzene ug/L ND 1.0 02/14/19 01:250.23
Chloroethane ug/L ND 1.0 02/14/19 01:250.49
Chloroform ug/L ND 5.0 02/14/19 01:252.3
Chloromethane ug/L ND 1.0 02/14/19 01:250.39
cis-1,2-Dichloroethene ug/L ND 1.0 02/14/19 01:250.29
cis-1,3-Dichloropropene ug/L ND 1.0 02/14/19 01:250.30
Dibromochloromethane ug/L ND 1.0 02/14/19 01:250.41
Dibromomethane ug/L ND 1.0 02/14/19 01:250.46
Dichlorodifluoromethane ug/L ND 1.0 02/14/19 01:250.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2497594
Associated Lab Samples:92417688006
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 02/14/19 01:250.22
Ethylbenzene ug/L ND 1.0 02/14/19 01:250.26
Hexachloro-1,3-butadiene ug/L ND 1.0 02/14/19 01:250.44
m&p-Xylene ug/L ND 2.0 02/14/19 01:250.41
Methyl-tert-butyl ether ug/L ND 1.0 02/14/19 01:250.28
Methylene Chloride ug/L ND 5.0 02/14/19 01:253.7
Naphthalene ug/L ND 1.0 02/14/19 01:250.35
o-Xylene ug/L ND 1.0 02/14/19 01:250.22
p-Isopropyltoluene ug/L ND 1.0 02/14/19 01:250.21
Styrene ug/L ND 1.0 02/14/19 01:250.27
Tetrachloroethene ug/L ND 1.0 02/14/19 01:250.16
Toluene ug/L ND 1.0 02/14/19 01:250.24
trans-1,2-Dichloroethene ug/L ND 1.0 02/14/19 01:250.25
trans-1,3-Dichloropropene ug/L ND 1.0 02/14/19 01:250.31
Trichloroethene ug/L ND 1.0 02/14/19 01:250.22
Trichlorofluoromethane ug/L ND 1.0 02/14/19 01:250.31
Vinyl acetate ug/L ND 2.0 02/14/19 01:251.4
Vinyl chloride ug/L ND 1.0 02/14/19 01:250.24
Xylene (Total)ug/L ND 1.0 02/14/19 01:250.63
1,2-Dichloroethane-d4 (S)%103 70-130 02/14/19 01:25
4-Bromofluorobenzene (S)%103 70-130 02/14/19 01:25
Toluene-d8 (S)%116 70-130 02/14/19 01:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2497595LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 43.650 87 70-130
1,1,1-Trichloroethane ug/L 54.650 109 70-130
1,1,2,2-Tetrachloroethane ug/L 47.450 95 70-130
1,1,2-Trichloroethane ug/L 54.750 109 70-130
1,1-Dichloroethane ug/L 56.750 113 70-130
1,1-Dichloroethene ug/L 58.050 116 70-130
1,1-Dichloropropene ug/L 57.150 114 70-130
1,2,3-Trichlorobenzene ug/L 53.150 106 70-130
1,2,3-Trichloropropane ug/L 47.750 95 70-130
1,2,4-Trichlorobenzene ug/L 50.650 101 70-130
1,2-Dibromo-3-chloropropane ug/L 47.350 95 70-130
1,2-Dibromoethane (EDB)ug/L 54.650 109 70-130
1,2-Dichlorobenzene ug/L 48.750 97 70-130
1,2-Dichloroethane ug/L 51.950 104 70-130
1,2-Dichloropropane ug/L 56.350 113 70-130
1,3-Dichlorobenzene ug/L 49.250 98 70-130
1,3-Dichloropropane ug/L 55.450 111 70-131
1,4-Dichlorobenzene ug/L 48.950 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2497595LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 51.250 102 69-130
2-Butanone (MEK)ug/L 122100 122 64-135
2-Chlorotoluene ug/L 46.650 93 70-130
2-Hexanone ug/L 95.3100 95 66-135
4-Chlorotoluene ug/L 47.150 94 70-130
4-Methyl-2-pentanone (MIBK)ug/L 91.1100 91 70-130
Acetone ug/L 121100 121 61-157
Benzene ug/L 54.250 108 70-130
Bromobenzene ug/L 47.850 96 70-130
Bromochloromethane ug/L 59.150 118 70-130
Bromodichloromethane ug/L 50.050 100 70-130
Bromoform ug/L 38.050 76 70-130
Bromomethane ug/L 32.650 65 38-130
Carbon tetrachloride ug/L 48.350 97 70-130
Chlorobenzene ug/L 49.150 98 70-130
Chloroethane ug/L 44.050 88 37-142
Chloroform ug/L 53.250 106 70-130
Chloromethane ug/L 54.450 109 48-130
cis-1,2-Dichloroethene ug/L 55.450 111 70-130
cis-1,3-Dichloropropene ug/L 54.450 109 70-130
Dibromochloromethane ug/L 47.250 94 70-130
Dibromomethane ug/L 51.150 102 70-130
Dichlorodifluoromethane ug/L 60.550 121 53-134
Diisopropyl ether ug/L 57.450 115 70-135
Ethylbenzene ug/L 48.150 96 70-130
Hexachloro-1,3-butadiene ug/L 49.550 99 68-132
m&p-Xylene ug/L 95.4100 95 70-130
Methyl-tert-butyl ether ug/L 58.350 117 70-130
Methylene Chloride ug/L 53.450 107 67-132
Naphthalene ug/L 49.650 99 70-130
o-Xylene ug/L 48.850 98 70-130
p-Isopropyltoluene ug/L 48.150 96 70-130
Styrene ug/L 49.750 99 70-130
Tetrachloroethene ug/L 50.250 100 69-130
Toluene ug/L 47.350 95 70-130
trans-1,2-Dichloroethene ug/L 56.050 112 70-130
trans-1,3-Dichloropropene ug/L 51.850 104 70-130
Trichloroethene ug/L 57.650 115 70-130
Trichlorofluoromethane ug/L 58.650 117 63-130
Vinyl acetate ug/L 113100 113 55-143
Vinyl chloride ug/L 60.950 122 70-131
Xylene (Total)ug/L 144150 96 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2497596MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417431001
2497597
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 78 73-13479 1 3020ND15.6 15.8
1,1,1-Trichloroethane ug/L 20 126 82-143123 2 3020ND25.2 24.6
1,1,2,2-Tetrachloroethane ug/L 20 92 70-13689 3 3020ND18.5 17.8
1,1,2-Trichloroethane ug/L 20 117 70-135109 7 3020ND23.3 21.7
1,1-Dichloroethane ug/L 20 129 70-139125 3 30201.5 27.3 26.5
1,1-Dichloroethene ug/L 20 140 70-154134 4 3020ND28.0 26.9
1,1-Dichloropropene ug/L 20 113 70-149108 5 3020ND22.7 21.7
1,2,3-Trichlorobenzene ug/L 20 103 70-13598 4 3020ND20.6 19.7
1,2,3-Trichloropropane ug/L 20 92 71-13791 1 3020ND18.4 18.1
1,2,4-Trichlorobenzene ug/L 20 101 73-14097 4 3020ND20.3 19.4
1,2-Dibromo-3-
chloropropane ug/L 20 88 65-13482 6 3020ND17.5 16.5
1,2-Dibromoethane (EDB) ug/L 20 99 70-13796 3 3020ND19.8 19.2
1,2-Dichlorobenzene ug/L 20 101 70-13396 5 3020ND20.1 19.2
1,2-Dichloroethane ug/L 20 116 70-137113 3 3020ND23.2 22.5
1,2-Dichloropropane ug/L 20 128 70-140122 5 3020ND25.5 24.4
1,3-Dichlorobenzene ug/L 20 103 70-13599 4 3020ND20.7 19.8
1,3-Dichloropropane ug/L 20 103 70-14399 3 3020ND20.6 19.9
1,4-Dichlorobenzene ug/L 20 98 70-13396 3 3020ND19.7 19.1
2,2-Dichloropropane ug/L 20 109 61-148108 1 3020ND21.8 21.6
2-Butanone (MEK)ug/L 40 119 60-139113 5 3040ND47.7 45.3
2-Chlorotoluene ug/L 20 97 70-14492 5 3020ND19.5 18.5
2-Hexanone ug/L 40 95 65-13891 5 3040ND38.2 36.5
4-Chlorotoluene ug/L 20 96 70-13794 2 3020ND19.2 18.9
4-Methyl-2-pentanone
(MIBK)ug/L 40 99 65-13590 10 3040ND39.6 35.9
Acetone ug/L 40 134 60-148120 11 3040ND53.5 48.1
Benzene ug/L 20 122 70-151116 5 3020ND24.4 23.2
Bromobenzene ug/L 20 97 70-13692 5 3020ND19.4 18.5
Bromochloromethane ug/L 20 134 70-141132 2 3020ND26.9 26.5
Bromodichloromethane ug/L 20 117 70-138115 2 3020ND23.4 23.1
Bromoform ug/L 20 69 63-13068 1 3020ND13.8 13.6
Bromomethane ug/L 20 50 15-15255 9 3020ND10 10.9
Carbon tetrachloride ug/L 20 122 70-143118 4 3020ND24.5 23.5
Chlorobenzene ug/L 20 102 70-138100 2 3020ND20.4 20.1
Chloroethane ug/L 20 150 52-163146 3 3020ND30.1 29.3
Chloroform ug/L 20 121 70-139111 8 3020ND24.1 22.3
Chloromethane ug/L 20 117 41-139109 7 3020ND23.5 21.8
cis-1,2-Dichloroethene ug/L 20 126 70-141124 1 302016.4 41.6 41.2
cis-1,3-Dichloropropene ug/L 20 108 70-137106 3 3020ND21.7 21.1
Dibromochloromethane ug/L 20 84 70-13485 0 3020ND16.9 16.9
Dibromomethane ug/L 20 128 70-138123 4 3020ND25.7 24.6
Dichlorodifluoromethane ug/L 20 111 47-155107 4 3020ND22.2 21.4
Diisopropyl ether ug/L 20 104 63-14498 6 3020ND20.8 19.6
Ethylbenzene ug/L 20 104 66-153103 1 3020ND20.7 20.5
Hexachloro-1,3-butadiene ug/L 20 105 65-14998 7 3020ND21.1 19.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2497596MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92417431001
2497597
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 105 69-152105 0 3040ND42.1 42.1
Methyl-tert-butyl ether ug/L 20 110 54-156112 2 3020ND22.4 22.9
Methylene Chloride ug/L 20 126 42-159121 4 3020ND25.2 24.2
Naphthalene ug/L 20 94 61-14890 4 3020ND18.8 18.1
o-Xylene ug/L 20 103 70-148105 2 3020ND20.6 21.0
p-Isopropyltoluene ug/L 20 101 70-14695 6 3020ND20.2 19.1
Styrene ug/L 20 106 70-135104 2 3020ND21.3 20.8
Tetrachloroethene ug/L 20 104 59-143102 1 3020ND21.5 21.2
Toluene ug/L 20 114 59-148109 5 3020ND22.8 21.8
trans-1,2-Dichloroethene ug/L 20 129 70-146125 4 3020ND25.9 24.9
trans-1,3-Dichloropropene ug/L 20 97 70-13595 2 3020ND19.4 19.0
Trichloroethene ug/L 20 135 70-147129 4 30201.6 28.6 27.4
Trichlorofluoromethane ug/L 20 136 70-148132 3 3020ND27.1 26.3
Vinyl acetate ug/L 40 99 49-15197 2 3040ND39.7 38.8
Vinyl chloride ug/L 20 136 70-156128 6 3020ND27.1 25.5
Xylene (Total)ug/L 60 105 63-158105 1 3060ND62.7 63.1
1,2-Dichloroethane-d4 (S) %104 70-130106
4-Bromofluorobenzene (S) %101 70-130102
Toluene-d8 (S)%104 70-130104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458146
EPA 8260B
EPA 8260B
8260 MSV Low Level
Associated Lab Samples: 92417688002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2497910
Associated Lab Samples:92417688002
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/14/19 11:550.34
1,1,1-Trichloroethane ug/L ND 1.0 02/14/19 11:550.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/14/19 11:550.22
1,1,2-Trichloroethane ug/L ND 1.0 02/14/19 11:550.24
1,1-Dichloroethane ug/L ND 1.0 02/14/19 11:550.27
1,1-Dichloroethene ug/L ND 1.0 02/14/19 11:550.24
1,1-Dichloropropene ug/L ND 1.0 02/14/19 11:550.21
1,2,3-Trichlorobenzene ug/L ND 1.0 02/14/19 11:550.34
1,2,3-Trichloropropane ug/L ND 1.0 02/14/19 11:550.35
1,2,4-Trichlorobenzene ug/L ND 1.0 02/14/19 11:550.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 02/14/19 11:550.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/14/19 11:550.26
1,2-Dichlorobenzene ug/L ND 1.0 02/14/19 11:550.29
1,2-Dichloroethane ug/L ND 1.0 02/14/19 11:550.34
1,2-Dichloropropane ug/L ND 1.0 02/14/19 11:550.19
1,3-Dichlorobenzene ug/L ND 1.0 02/14/19 11:550.22
1,3-Dichloropropane ug/L ND 1.0 02/14/19 11:550.16
1,4-Dichlorobenzene ug/L ND 1.0 02/14/19 11:550.26
2,2-Dichloropropane ug/L ND 1.0 02/14/19 11:550.27
2-Butanone (MEK)ug/L ND 5.0 02/14/19 11:553.3
2-Chlorotoluene ug/L ND 1.0 02/14/19 11:550.20
2-Hexanone ug/L ND 5.0 02/14/19 11:550.57
4-Chlorotoluene ug/L ND 1.0 02/14/19 11:550.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/14/19 11:554.5
Acetone ug/L ND 25.0 02/14/19 11:556.2
Benzene ug/L ND 1.0 02/14/19 11:550.15
Bromobenzene ug/L ND 1.0 02/14/19 11:550.22
Bromochloromethane ug/L ND 1.0 02/14/19 11:550.34
Bromodichloromethane ug/L ND 1.0 02/14/19 11:550.26
Bromoform ug/L ND 1.0 02/14/19 11:550.62
Bromomethane ug/L ND 2.0 02/14/19 11:550.62
Carbon tetrachloride ug/L ND 1.0 02/14/19 11:550.22
Chlorobenzene ug/L ND 1.0 02/14/19 11:550.23
Chloroethane ug/L ND 1.0 02/14/19 11:550.49
Chloroform ug/L ND 5.0 02/14/19 11:552.3
Chloromethane ug/L ND 1.0 02/14/19 11:550.39
cis-1,2-Dichloroethene ug/L ND 1.0 02/14/19 11:550.29
cis-1,3-Dichloropropene ug/L ND 1.0 02/14/19 11:550.30
Dibromochloromethane ug/L ND 1.0 02/14/19 11:550.41
Dibromomethane ug/L ND 1.0 02/14/19 11:550.46
Dichlorodifluoromethane ug/L ND 1.0 02/14/19 11:550.23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2497910
Associated Lab Samples:92417688002
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 02/14/19 11:550.22
Ethylbenzene ug/L ND 1.0 02/14/19 11:550.26
Hexachloro-1,3-butadiene ug/L ND 1.0 02/14/19 11:550.44
m&p-Xylene ug/L ND 2.0 02/14/19 11:550.41
Methyl-tert-butyl ether ug/L ND 1.0 02/14/19 11:550.28
Methylene Chloride ug/L ND 5.0 02/14/19 11:553.7
Naphthalene ug/L ND 1.0 02/14/19 11:550.35
o-Xylene ug/L ND 1.0 02/14/19 11:550.22
p-Isopropyltoluene ug/L ND 1.0 02/14/19 11:550.21
Styrene ug/L ND 1.0 02/14/19 11:550.27
Tetrachloroethene ug/L ND 1.0 02/14/19 11:550.16
Toluene ug/L ND 1.0 02/14/19 11:550.24
trans-1,2-Dichloroethene ug/L ND 1.0 02/14/19 11:550.25
trans-1,3-Dichloropropene ug/L ND 1.0 02/14/19 11:550.31
Trichloroethene ug/L ND 1.0 02/14/19 11:550.22
Trichlorofluoromethane ug/L ND 1.0 02/14/19 11:550.31
Vinyl acetate ug/L ND 2.0 02/14/19 11:551.4
Vinyl chloride ug/L ND 1.0 02/14/19 11:550.24
Xylene (Total)ug/L ND 1.0 02/14/19 11:550.63
1,2-Dichloroethane-d4 (S)%88 70-130 02/14/19 11:55
4-Bromofluorobenzene (S)%101 70-130 02/14/19 11:55
Toluene-d8 (S)%101 70-130 02/14/19 11:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2497911LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.150 110 70-130
1,1,1-Trichloroethane ug/L 51.950 104 70-130
1,1,2,2-Tetrachloroethane ug/L 54.450 109 70-130
1,1,2-Trichloroethane ug/L 56.950 114 70-130
1,1-Dichloroethane ug/L 51.050 102 70-130
1,1-Dichloroethene ug/L 53.050 106 70-130
1,1-Dichloropropene ug/L 49.750 99 70-130
1,2,3-Trichlorobenzene ug/L 55.850 112 70-130
1,2,3-Trichloropropane ug/L 51.250 102 70-130
1,2,4-Trichlorobenzene ug/L 56.750 113 70-130
1,2-Dibromo-3-chloropropane ug/L 50.050 100 70-130
1,2-Dibromoethane (EDB)ug/L 58.050 116 70-130
1,2-Dichlorobenzene ug/L 52.750 105 70-130
1,2-Dichloroethane ug/L 45.650 91 70-130
1,2-Dichloropropane ug/L 51.950 104 70-130
1,3-Dichlorobenzene ug/L 52.150 104 70-130
1,3-Dichloropropane ug/L 55.650 111 70-131
1,4-Dichlorobenzene ug/L 51.150 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2497911LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 52.250 104 69-130
2-Butanone (MEK)ug/L 107100 107 64-135
2-Chlorotoluene ug/L 49.050 98 70-130
2-Hexanone ug/L 102100 102 66-135
4-Chlorotoluene ug/L 49.150 98 70-130
4-Methyl-2-pentanone (MIBK)ug/L 100100 100 70-130
Acetone ug/L 93.3100 93 61-157
Benzene ug/L 52.650 105 70-130
Bromobenzene ug/L 52.850 106 70-130
Bromochloromethane ug/L 57.050 114 70-130
Bromodichloromethane ug/L 51.750 103 70-130
Bromoform ug/L 54.050 108 70-130
Bromomethane ug/L 37.550 75 38-130
Carbon tetrachloride ug/L 49.950 100 70-130
Chlorobenzene ug/L 51.250 102 70-130
Chloroethane ug/L 42.750 85 37-142
Chloroform ug/L 48.350 97 70-130
Chloromethane ug/L 46.550 93 48-130
cis-1,2-Dichloroethene ug/L 49.850 100 70-130
cis-1,3-Dichloropropene ug/L 55.050 110 70-130
Dibromochloromethane ug/L 50.750 101 70-130
Dibromomethane ug/L 56.550 113 70-130
Dichlorodifluoromethane ug/L 51.850 104 53-134
Diisopropyl ether ug/L 50.750 101 70-135
Ethylbenzene ug/L 49.450 99 70-130
Hexachloro-1,3-butadiene ug/L 54.050 108 68-132
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 53.550 107 70-130
Methylene Chloride ug/L 47.350 95 67-132
Naphthalene ug/L 52.750 105 70-130
o-Xylene ug/L 52.250 104 70-130
p-Isopropyltoluene ug/L 50.350 101 70-130
Styrene ug/L 54.050 108 70-130
Tetrachloroethene ug/L 54.750 109 69-130
Toluene ug/L 47.950 96 70-130
trans-1,2-Dichloroethene ug/L 50.750 101 70-130
trans-1,3-Dichloropropene ug/L 54.450 109 70-130
Trichloroethene ug/L 54.650 109 70-130
Trichlorofluoromethane ug/L 48.750 97 63-130
Vinyl acetate ug/L 108100 108 55-143
Vinyl chloride ug/L 51.250 102 70-131
Xylene (Total)ug/L 153150 102 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2497912MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35447076005
2497913
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 800 101 73-134102 1 3080013.6U 806 814
1,1,1-Trichloroethane ug/L 800 100 82-143102 2 308007.0U 796 815
1,1,2,2-Tetrachloroethane ug/L 800 102 70-136102 0 308008.9U 818 818
1,1,2-Trichloroethane ug/L 800 102 70-135104 2 308009.4U 814 834
1,1-Dichloroethane ug/L 800 97 70-13999 2 3080010.7U 779 795
1,1-Dichloroethene ug/L 800 100 70-154101 1 308009.8U 798 805
1,1-Dichloropropene ug/L 800 96 70-14996 0 308008.5U 766 765
1,2,3-Trichlorobenzene ug/L 800 101 70-135107 6 3080013.8U 804 854
1,2,3-Trichloropropane ug/L 800 114 71-137101 12 3080013.9U 914 807
1,2,4-Trichlorobenzene ug/L 800 97 73-140106 9 308008.7U 775 851
1,2-Dibromo-3-
chloropropane ug/L 800 95 65-13498 3 3080010.3U 759 782
1,2-Dibromoethane (EDB) ug/L 800 104 70-137105 1 3080010.3U 829 840
1,2-Dichlorobenzene ug/L 800 99 70-133100 1 3080011.6U 792 801
1,2-Dichloroethane ug/L 800 90 70-13791 1 3080013.4U 722 731
1,2-Dichloropropane ug/L 800 97 70-14096 1 308007.5U 775 770
1,3-Dichlorobenzene ug/L 800 99 70-13598 1 308008.7U 794 785
1,3-Dichloropropane ug/L 800 102 70-143102 0 308006.3U 814 817
1,4-Dichlorobenzene ug/L 800 96 70-13398 3 3080010.3U 765 785
2,2-Dichloropropane ug/L 800 88 61-14889 1 3080010.8U 703 713
2-Butanone (MEK)ug/L 1600 95 60-13995 1 301600133U1520 1530
2-Chlorotoluene ug/L 800 99 70-144101 1 308008.1U 795 804
2-Hexanone ug/L 1600 95 65-13896 1 30160022.7U 1530 1540
4-Chlorotoluene ug/L 800 94 70-13795 1 308008.2U 753 761
4-Methyl-2-pentanone
(MIBK)ug/L 1600 93 65-13594 1 301600181U1490 1510
Acetone ug/L 1600 80 60-14882 3 301600247U1280 1310
Benzene ug/L 800 100 70-15199 1 308006.0U 804 796
Bromobenzene ug/L 800 101 70-136102 1 308008.8U 808 815
Bromochloromethane ug/L 800 105 70-141107 3 3080013.7U 837 860
Bromodichloromethane ug/L 800 90 70-13895 5 3080010.2U 724 761
Bromoform ug/L 800 89 63-13090 1 3080024.7U 712 717
Bromomethane ug/L 800 43 15-15258 28 3080024.8U 345 460
Carbon tetrachloride ug/L 800 96 70-14395 1 308009.0U 766 761
Chlorobenzene ug/L 800 100 70-138100 0 308009.3U 798 800
Chloroethane ug/L 800 92 52-16396 4 3080019.6U 735 767
Chloroform ug/L 800 90 70-13991 1 3080093.6U 744 755
Chloromethane ug/L 800 81 41-13985 5 3080015.6U 651 683
cis-1,2-Dichloroethene ug/L 800 95 70-14196 1 3080011.6U 760 769
cis-1,3-Dichloropropene ug/L 800 93 70-13794 1 3080011.8U 745 753
Dibromochloromethane ug/L 800 91 70-13493 3 3080016.5U 727 747
Dibromomethane ug/L 800 103 70-138103 0 3080018.4U 823 824
Dichlorodifluoromethane ug/L 800 74 47-15576 2 308009.0U 594 608
Diisopropyl ether ug/L 800 93 63-14492 1 308008.7U 740 734
Ethylbenzene ug/L 800 101 66-15389 3 3080024803280 3180
Hexachloro-1,3-butadiene ug/L 800 104 65-149100 4 3080017.5U 831 802
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2497912MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35447076005
2497913
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 1600 92 69-15276 2 3016001100012500 12200
Methyl-tert-butyl ether ug/L 800 92 54-15696 4 3080011.0U 739 766
Methylene Chloride ug/L 800 99 42-15998 2 30800148U796 783
Naphthalene ug/L 800 106 61-148112 4 308004001250 1290
o-Xylene ug/L 800 90 70-14876 2 3080051805900 5790
p-Isopropyltoluene ug/L 800 95 70-14697 2 308008.5U 758 776
Styrene ug/L 800 100 70-135102 2 3080010.7U 797 813
Tetrachloroethene ug/L 800 106 59-143105 0 308006.5U 845 841
Toluene ug/L M18006159-14851 2 3080047505230 5150
trans-1,2-Dichloroethene ug/L 800 98 70-146102 3 3080010.2U 787 815
trans-1,3-Dichloropropene ug/L 800 92 70-13593 2 3080012.4U 735 747
Trichloroethene ug/L 800 104 70-147105 1 308008.8U 831 843
Trichlorofluoromethane ug/L 800 100 70-14897 4 3080012.4U 800 772
Vinyl acetate ug/L 1600 91 49-15195 4 30160058.0U 1460 1520
Vinyl chloride ug/L 800 92 70-15695 3 308009.7U 738 758
Xylene (Total)ug/L 2400 91 63-15876 2 3024001620018400 18000
1,2-Dichloroethane-d4 (S) %90 70-13091
4-Bromofluorobenzene (S) %97 70-13096
Toluene-d8 (S)%95 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
458810
EPA 3510C
EPA 8270D
8270 Water MSSV RVE
Associated Lab Samples: 92417688002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2500900
Associated Lab Samples:92417688002
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 02/19/19 11:112.6
1,2-Dichlorobenzene ug/L ND 10.0 02/19/19 11:113.2
1,3-Dichlorobenzene ug/L ND 10.0 02/19/19 11:113.2
1,4-Dichlorobenzene ug/L ND 10.0 02/19/19 11:112.6
1-Methylnaphthalene ug/L ND 10.0 02/19/19 11:112.8
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 02/19/19 11:112.5
2,4,5-Trichlorophenol ug/L ND 10.0 02/19/19 11:112.3
2,4,6-Trichlorophenol ug/L ND 10.0 02/19/19 11:112.8
2,4-Dichlorophenol ug/L ND 10.0 02/19/19 11:112.7
2,4-Dimethylphenol ug/L ND 10.0 02/19/19 11:111.9
2,4-Dinitrophenol ug/L ND 50.0 02/19/19 11:1110.1
2,4-Dinitrotoluene ug/L ND 10.0 02/19/19 11:112.4
2,6-Dinitrotoluene ug/L ND 10.0 02/19/19 11:112.9
2-Chloronaphthalene ug/L ND 10.0 02/19/19 11:112.9
2-Chlorophenol ug/L ND 10.0 02/19/19 11:112.9
2-Methylnaphthalene ug/L ND 10.0 02/19/19 11:112.8
2-Methylphenol(o-Cresol)ug/L ND 10.0 02/19/19 11:113.6
2-Nitroaniline ug/L ND 50.0 02/19/19 11:115.5
2-Nitrophenol ug/L ND 10.0 02/19/19 11:112.6
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 02/19/19 11:112.4
3,3'-Dichlorobenzidine ug/L ND 20.0 02/19/19 11:112.8
3-Nitroaniline ug/L ND 50.0 02/19/19 11:115.0
4,6-Dinitro-2-methylphenol ug/L ND 20.0 02/19/19 11:114.4
4-Bromophenylphenyl ether ug/L ND 10.0 02/19/19 11:112.7
4-Chloro-3-methylphenol ug/L ND 20.0 02/19/19 11:114.6
4-Chloroaniline ug/L ND 20.0 02/19/19 11:116.8
4-Chlorophenylphenyl ether ug/L ND 10.0 02/19/19 11:112.9
4-Nitroaniline ug/L ND 20.0 02/19/19 11:113.6
4-Nitrophenol ug/L ND 50.0 02/19/19 11:117.8
Acenaphthene ug/L ND 10.0 02/19/19 11:113.4
Acenaphthylene ug/L ND 10.0 02/19/19 11:113.0
Aniline ug/L ND 10.0 02/19/19 11:113.1
Anthracene ug/L ND 10.0 02/19/19 11:112.0
Benzo(a)anthracene ug/L ND 10.0 02/19/19 11:111.3
Benzo(a)pyrene ug/L ND 10.0 02/19/19 11:111.3
Benzo(b)fluoranthene ug/L ND 10.0 02/19/19 11:111.5
Benzo(g,h,i)perylene ug/L ND 10.0 02/19/19 11:111.8
Benzo(k)fluoranthene ug/L ND 10.0 02/19/19 11:111.8
Benzoic Acid ug/L ND 50.0 02/19/19 11:1117.3
Benzyl alcohol ug/L ND 20.0 02/19/19 11:117.0
bis(2-Chloroethoxy)methane ug/L ND 10.0 02/19/19 11:113.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2500900
Associated Lab Samples:92417688002
Matrix: Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 02/19/19 11:113.1
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 02/19/19 11:111.4
Butylbenzylphthalate ug/L ND 10.0 02/19/19 11:111.3
Chrysene ug/L ND 10.0 02/19/19 11:111.2
Di-n-butylphthalate ug/L ND 10.0 02/19/19 11:111.2
Di-n-octylphthalate ug/L ND 10.0 02/19/19 11:111.2
Dibenz(a,h)anthracene ug/L ND 10.0 02/19/19 11:111.9
Dibenzofuran ug/L ND 10.0 02/19/19 11:113.4
Diethylphthalate ug/L ND 10.0 02/19/19 11:112.0
Dimethylphthalate ug/L ND 10.0 02/19/19 11:112.3
Fluoranthene ug/L ND 10.0 02/19/19 11:111.7
Fluorene ug/L ND 10.0 02/19/19 11:113.0
Hexachloro-1,3-butadiene ug/L ND 10.0 02/19/19 11:113.1
Hexachlorobenzene ug/L ND 10.0 02/19/19 11:112.5
Hexachlorocyclopentadiene ug/L ND 10.0 02/19/19 11:113.4
Hexachloroethane ug/L ND 10.0 02/19/19 11:114.0
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 02/19/19 11:111.7
Isophorone ug/L ND 10.0 02/19/19 11:112.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 02/19/19 11:112.6
N-Nitrosodimethylamine ug/L ND 10.0 02/19/19 11:112.8
N-Nitrosodiphenylamine ug/L ND 10.0 02/19/19 11:112.0
Naphthalene ug/L ND 10.0 02/19/19 11:113.2
Nitrobenzene ug/L ND 10.0 02/19/19 11:113.4
Pentachlorophenol ug/L ND 25.0 02/19/19 11:113.1
Phenanthrene ug/L ND 10.0 02/19/19 11:112.4
Phenol ug/L ND 10.0 02/19/19 11:112.7
Pyrene ug/L ND 10.0 02/19/19 11:111.2
2,4,6-Tribromophenol (S)%66 10-137 02/19/19 11:11
2-Fluorobiphenyl (S)%66 13-130 02/19/19 11:11
2-Fluorophenol (S)%43 10-130 02/19/19 11:11
Nitrobenzene-d5 (S)%76 13-130 02/19/19 11:11
Phenol-d6 (S)%27 10-130 02/19/19 11:11
Terphenyl-d14 (S)%95 25-130 02/19/19 11:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2500901LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 24.250 48 30-130
1,2-Dichlorobenzene ug/L 23.950 48 30-130
1,3-Dichlorobenzene ug/L 23.350 47 20-130
1,4-Dichlorobenzene ug/L 24.750 49 30-130
1-Methylnaphthalene ug/L 30.450 61 30-130
2,2'-Oxybis(1-chloropropane)ug/L 30.550 61 20-130
2,4,5-Trichlorophenol ug/L 33.050 66 40-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2500901LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 34.150 68 40-130
2,4-Dichlorophenol ug/L 31.550 63 31-130
2,4-Dimethylphenol ug/L 31.150 62 30-130
2,4-Dinitrophenol ug/L 193250 77 30-130
2,4-Dinitrotoluene ug/L 39.950 80 49-130
2,6-Dinitrotoluene ug/L 36.850 74 50-130
2-Chloronaphthalene ug/L 26.750 53 30-130
2-Chlorophenol ug/L 30.350 61 30-130
2-Methylnaphthalene ug/L 29.650 59 30-130
2-Methylphenol(o-Cresol)ug/L 25.150 50 30-130
2-Nitroaniline ug/L 69.0100 69 40-130
2-Nitrophenol ug/L 33.250 66 20-130
3&4-Methylphenol(m&p Cresol)ug/L 22.950 46 20-130
3,3'-Dichlorobenzidine ug/L 93.9100 94 10-150
3-Nitroaniline ug/L 77.7100 78 40-130
4,6-Dinitro-2-methylphenol ug/L 83.9100 84 40-130
4-Bromophenylphenyl ether ug/L 35.650 71 30-130
4-Chloro-3-methylphenol ug/L 66.2100 66 30-130
4-Chloroaniline ug/L 62.4100 62 20-130
4-Chlorophenylphenyl ether ug/L 29.750 59 20-130
4-Nitroaniline ug/L 87.4100 87 40-130
4-Nitrophenol ug/L 87.8250 35 10-130
Acenaphthene ug/L 31.850 64 30-130
Acenaphthylene ug/L 35.550 71 30-130
Aniline ug/L 24.350 49 20-130
Anthracene ug/L 43.250 86 50-130
Benzo(a)anthracene ug/L 49.450 99 50-130
Benzo(a)pyrene ug/L 49.750 99 50-130
Benzo(b)fluoranthene ug/L 46.450 93 50-130
Benzo(g,h,i)perylene ug/L 54.050 108 50-130
Benzo(k)fluoranthene ug/L 46.150 92 50-130
Benzoic Acid ug/L 64.3250 26 10-130
Benzyl alcohol ug/L 55.4100 55 20-130
bis(2-Chloroethoxy)methane ug/L 33.850 68 30-130
bis(2-Chloroethyl) ether ug/L 32.050 64 30-130
bis(2-Ethylhexyl)phthalate ug/L 50.850 102 50-130
Butylbenzylphthalate ug/L 48.450 97 50-150
Chrysene ug/L 47.650 95 50-130
Di-n-butylphthalate ug/L 46.150 92 50-130
Di-n-octylphthalate ug/L 53.050 106 50-130
Dibenz(a,h)anthracene ug/L 54.050 108 40-130
Dibenzofuran ug/L 30.250 60 40-130
Diethylphthalate ug/L 38.850 78 40-130
Dimethylphthalate ug/L 34.550 69 40-130
Fluoranthene ug/L 49.550 99 30-130
Fluorene ug/L 33.750 67 20-130
Hexachloro-1,3-butadiene ug/L 22.450 45 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2500901LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 34.850 70 30-130
Hexachlorocyclopentadiene ug/L 23.550 47 10-150
Hexachloroethane ug/L 22.150 44 10-130
Indeno(1,2,3-cd)pyrene ug/L 54.650 109 40-130
Isophorone ug/L 31.950 64 30-130
N-Nitroso-di-n-propylamine ug/L 29.650 59 30-130
N-Nitrosodimethylamine ug/L 22.550 45 10-130
N-Nitrosodiphenylamine ug/L 36.250 72 30-130
Naphthalene ug/L 30.450 61 20-130
Nitrobenzene ug/L 31.350 63 20-130
Pentachlorophenol ug/L 81.3100 81 10-140
Phenanthrene ug/L 41.950 84 50-130
Phenol ug/L 12.550 25 10-130
Pyrene ug/L 44.350 89 50-130
2,4,6-Tribromophenol (S)%87 10-137
2-Fluorobiphenyl (S)%59 13-130
2-Fluorophenol (S)%39 10-130
Nitrobenzene-d5 (S)%68 13-130
Phenol-d6 (S)%26 10-130
Terphenyl-d14 (S)%82 25-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2500902MATRIX SPIKE SAMPLE:
MSSpike
Result
92418056017
1,2,4-Trichlorobenzene ug/L 24.350 49 30-130ND
1,2-Dichlorobenzene ug/L 23.450 47 30-130ND
1,3-Dichlorobenzene ug/L 22.750 45 20-130ND
1,4-Dichlorobenzene ug/L 23.850 48 30-130ND
1-Methylnaphthalene ug/L 31.650 63 30-130ND
2,2'-Oxybis(1-chloropropane)ug/L 32.450 65 20-130ND
2,4,5-Trichlorophenol ug/L 20.050 40 40-130ND
2,4,6-Trichlorophenol ug/L 12.0 M15024 40-130ND
2,4-Dichlorophenol ug/L 28.750 57 31-130ND
2,4-Dimethylphenol ug/L 31.850 64 30-130ND
2,4-Dinitrophenol ug/L 23.7J M12509 30-130ND
2,4-Dinitrotoluene ug/L 45.950 92 49-130ND
2,6-Dinitrotoluene ug/L 43.050 86 50-130ND
2-Chloronaphthalene ug/L 27.150 54 30-130ND
2-Chlorophenol ug/L 28.250 56 30-130ND
2-Methylnaphthalene ug/L 31.250 62 30-130ND
2-Methylphenol(o-Cresol)ug/L 26.650 53 30-130ND
2-Nitroaniline ug/L 77.2100 77 40-130ND
2-Nitrophenol ug/L 32.950 66 20-130ND
3&4-Methylphenol(m&p Cresol)ug/L 22.850 46 20-130ND
3,3'-Dichlorobenzidine ug/L 70.1100 70 10-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2500902MATRIX SPIKE SAMPLE:
MSSpike
Result
92418056017
3-Nitroaniline ug/L 80.9100 81 40-130ND
4,6-Dinitro-2-methylphenol ug/L 16.2J M110016 40-130ND
4-Bromophenylphenyl ether ug/L 40.250 80 30-130ND
4-Chloro-3-methylphenol ug/L 73.8100 74 30-130ND
4-Chloroaniline ug/L 42.4100 42 20-130ND
4-Chlorophenylphenyl ether ug/L 33.350 67 20-130ND
4-Nitroaniline ug/L 98.3100 98 40-130ND
4-Nitrophenol ug/L 12.3J M12505 10-130ND
Acenaphthene ug/L 32.250 64 30-130ND
Acenaphthylene ug/L 37.550 75 30-130ND
Aniline ug/L 18.150 36 20-130ND
Anthracene ug/L 45.650 91 50-130ND
Benzo(a)anthracene ug/L 54.350 109 50-130ND
Benzo(a)pyrene ug/L 51.250 102 50-130ND
Benzo(b)fluoranthene ug/L 50.150 100 50-130ND
Benzo(g,h,i)perylene ug/L 57.550 115 50-130ND
Benzo(k)fluoranthene ug/L 49.850 100 50-130ND
Benzoic Acid ug/L ND M12504 10-130ND
Benzyl alcohol ug/L 61.6100 62 20-130ND
bis(2-Chloroethoxy)methane ug/L 38.250 76 30-130ND
bis(2-Chloroethyl) ether ug/L 37.050 74 30-130ND
bis(2-Ethylhexyl)phthalate ug/L 50.850 102 50-130ND
Butylbenzylphthalate ug/L 57.350 115 50-150ND
Chrysene ug/L 52.450 105 50-130ND
Di-n-butylphthalate ug/L 54.450 109 50-130ND
Di-n-octylphthalate ug/L 52.750 105 50-130ND
Dibenz(a,h)anthracene ug/L 59.650 119 40-130ND
Dibenzofuran ug/L 32.450 65 40-130ND
Diethylphthalate ug/L 43.850 88 40-130ND
Dimethylphthalate ug/L 39.250 78 40-130ND
Fluoranthene ug/L 56.150 112 30-130ND
Fluorene ug/L 37.350 75 20-130ND
Hexachloro-1,3-butadiene ug/L 21.750 43 10-130ND
Hexachlorobenzene ug/L 39.050 78 30-130ND
Hexachlorocyclopentadiene ug/L 22.950 46 10-150ND
Hexachloroethane ug/L 20.050 40 10-130ND
Indeno(1,2,3-cd)pyrene ug/L 58.850 118 40-130ND
Isophorone ug/L 38.150 76 30-130ND
N-Nitroso-di-n-propylamine ug/L 33.550 67 30-130ND
N-Nitrosodimethylamine ug/L 25.150 50 10-130ND
N-Nitrosodiphenylamine ug/L 30.750 61 30-130ND
Naphthalene ug/L 32.250 64 20-130ND
Nitrobenzene ug/L 35.750 71 20-130ND
Pentachlorophenol ug/L 4.2J M11004 10-140ND
Phenanthrene ug/L 46.950 94 50-130ND
Phenol ug/L 15.350 31 10-130ND
Pyrene ug/L 52.850 106 50-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2500902MATRIX SPIKE SAMPLE:
MSSpike
Result
92418056017
2,4,6-Tribromophenol (S)%37 10-137
2-Fluorobiphenyl (S)%64 13-130
2-Fluorophenol (S)%27 10-130
Nitrobenzene-d5 (S)%78 13-130
Phenol-d6 (S)%28 10-130
Terphenyl-d14 (S)%77 25-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92418056018
2500903SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
1-Methylnaphthalene ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 302.1J
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Aniline ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92418056018
2500903SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzoic Acid ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isophorone ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
Naphthalene ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Pyrene ug/L ND 30ND
2,4,6-Tribromophenol (S)%1375
2-Fluorobiphenyl (S)%6050
2-Fluorophenol (S)%1335
Nitrobenzene-d5 (S)%7361
Phenol-d6 (S)%2826
Terphenyl-d14 (S)%7764
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 43
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 43
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92417688
BCP-129 Gresco Street Facility
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92417688002 458810 458922TMW-2 EPA 3510C EPA 8270D
92417688002 458146TMW-2 EPA 8260B
92417688006 458039Trip Blank EPA 8260B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/27/2019 02:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 43
Page 30 of 43
Page 31 of 43
Page 32 of 43
ANALYTICAL REPORT
June 26, 2019
Pace Analytical - Huntersville, NC
Sample Delivery Group:L1070848
Samples Received:02/15/2019
Project Number:92417688
Description:BCP-129 Gresco Street Facility
Report To:Kevin Godwin
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By:
June 26, 2019
[Preliminary Report]
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Nationalis performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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June 26, 2019
Nancy McLain
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
TMW-2 L1070848-02 5
Qc: Quality Control Summary 6
Mercury by Method 7470A 6
Metals (ICPMS) by Method 6020B 7
Gl: Glossary of Terms 8
Al: Accreditations & Locations 9
Sc: Sample Chain of Custody 10
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TMW-2 L1070848-02 GW 02/12/19 14:45 02/15/19 08:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Mercury by Method 7470A WG1238325 1 02/17/19 16:35 02/18/19 11:27 ABL Mt. Juliet, TN
Metals (ICPMS) by Method 6020B WG1239118 1 02/19/19 14:32 02/20/19 20:41 LD Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Nancy McLain
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Nancy McLain
Project Manager
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1070848
TMW-2
Collected date/time: 02/12/19 14:45
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 02/18/2019 11:27 WG1238325
Metals (ICPMS) by Method 6020B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Arsenic 0.503 J 0.250 2.00 1 02/20/2019 20:41 WG1239118
Barium 238 0.360 5.00 1 02/20/2019 20:41 WG1239118
Cadmium U 0.160 1.00 1 02/20/2019 20:41 WG1239118
Chromium 2.41 B 0.540 2.00 1 02/20/2019 20:41 WG1239118
Lead 0.254 J 0.240 2.00 1 02/20/2019 20:41 WG1239118
Selenium U 0.380 2.00 1 02/20/2019 20:41 WG1239118
Silver U 0.310 2.00 1 02/20/2019 20:41 WG1239118
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1238325
Mercury by Method 7470A L1070848-02
Method Blank (MB)
(MB) R3384601-1 02/18/19 10:22
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Mercury U 0.0490 0.200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3384601-2 02/18/19 10:24 • (LCSD) R3384601-3 02/18/19 10:39
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Mercury 3.00 2.89 3.37 96.5 112 80.0-120 15.3 20
L1070593-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1070593-01 02/18/19 10:41 • (MS) R3384601-4 02/18/19 10:43 • (MSD) R3384601-5 02/18/19 10:46
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 U 2.43 2.37 81.2 79.1 1 75.0-125 2.58 20
1 Cp
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3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1239118
Metals (ICPMS) by Method 6020B L1070848-02
Method Blank (MB)
(MB) R3385591-1 02/20/19 19:31
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Arsenic U 0.250 2.00
Barium U 0.360 5.00
Cadmium U 0.160 1.00
Chromium 0.639 J 0.540 2.00
Lead U 0.240 2.00
Selenium U 0.380 2.00
Silver U 0.310 2.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3385591-2 02/20/19 19:35 • (LCSD) R3385591-3 02/20/19 19:40
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Arsenic 50.0 51.7 51.3 103 103 80.0-120 0.767 20
Barium 50.0 47.1 45.1 94.1 90.2 80.0-120 4.27 20
Cadmium 50.0 49.1 48.3 98.1 96.5 80.0-120 1.61 20
Chromium 50.0 50.6 50.8 101 102 80.0-120 0.250 20
Lead 50.0 51.0 50.5 102 101 80.0-120 0.954 20
Selenium 50.0 48.2 49.6 96.3 99.2 80.0-120 2.93 20
Silver 50.0 49.5 49.4 99.0 98.7 80.0-120 0.238 20
L1071253-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1071253-08 02/20/19 19:44 • (MS) R3385591-5 02/20/19 19:53 • (MSD) R3385591-6 02/20/19 19:57
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 50.0 2.11 50.7 51.3 97.1 98.4 1 75.0-125 1.27 20
Barium 50.0 136 181 189 90.0 105 1 75.0-125 4.12 20
Cadmium 50.0 ND 48.8 50.2 97.6 100 1 75.0-125 2.80 20
Chromium 50.0 ND 47.1 48.2 94.2 96.4 1 75.0-125 2.22 20
Lead 50.0 ND 48.3 50.3 95.3 99.3 1 75.0-125 4.10 20
Selenium 50.0 ND 49.3 51.0 98.6 102 1 75.0-125 3.45 20
Silver 50.0 ND 48.1 50.4 96.3 101 1 75.0-125 4.49 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
1 Cp
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Page 40 of 43
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
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Page 42 of 43
Page 43 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
June 21, 2019
Bo Cappleman
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
Project Location: Charlotte, NC
Client Job Number:
Project Number: BCP-129
Laboratory Work Order Number: 19B0726
Enclosed are results of analyses for samples received by the laboratory on February 14, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
6/21/2019Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
ATTN: Bo Cappleman
BCP-129
19B0726
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
BCP-129
SG-1 19B0726-03 Soil Gas EPA TO-15
SG-2 19B0726-04 Soil Gas EPA TO-15
Page 2 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
1,2,4-Trichlorobenzene, 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114), Hexachlorobutadiene
19B0726-03[SG-1], 19B0726-04[SG-2], S032743-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
Ethanol
19B0726-03[SG-1], 19B0726-04[SG-2], S032743-CCV1
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in
house limits of 50-150%.
Analyte & Samples(s) Qualified:
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114), Ethanol
19B0726-03[SG-1], 19B0726-04[SG-2]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 3 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/14/2019
Work Order: 19B0726Sample Description/Location:
Field Sample #: SG-1
Sample ID: 19B0726-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): 28.0
Final Vacuum(in Hg): 4.5
Receipt Vacuum(in Hg): -4.8
Sampled: 2/12/2019 17:40
Canister ID: 2343
Flow Controller ID: 4235
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 7.9 8.0 2/21/19 21:28 BRFJ194192.8 6.6
Benzene ND 0.20 2/21/19 21:28 BRFND40.640.082 0.26
Benzyl chloride ND 0.20 2/21/19 21:28 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 2/21/19 21:28 BRFND41.30.074 0.49
Bromoform ND 0.20 2/21/19 21:28 BRFND42.10.090 0.93
Bromomethane ND 0.20 2/21/19 21:28 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 2/21/19 21:28 BRFND40.440.13 0.28
2-Butanone (MEK)1.8 8.0 2/21/19 21:28 BRFJ5.3 4240.31 0.92
Carbon Disulfide ND 2.0 2/21/19 21:28 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 2/21/19 21:28 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 2/21/19 21:28 BRFND40.920.098 0.45
Chloroethane ND 0.40 2/21/19 21:28 BRFND41.10.12 0.32
Chloroform ND 0.20 2/21/19 21:28 BRFND40.980.074 0.36
Chloromethane ND 0.40 2/21/19 21:28 BRFND40.830.14 0.28
Cyclohexane ND 0.20 2/21/19 21:28 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 2/21/19 21:28 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 2/21/19 21:28 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 2/21/19 21:28 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 2/21/19 21:28 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 2/21/19 21:28 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.32 0.20 2/21/19 21:28 BRF1.6 40.990.087 0.43
1,1-Dichloroethane ND 0.20 2/21/19 21:28 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 2/21/19 21:28 BRFND40.810.076 0.31
1,1-Dichloroethylene 7.7 0.20 2/21/19 21:28 BRF3040.790.081 0.32
cis-1,2-Dichloroethylene 9.0 0.20 2/21/19 21:28 BRF3640.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 2/21/19 21:28 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 2/21/19 21:28 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 2/21/19 21:28 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 2/21/19 21:28 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 2/21/19 21:28 BRFV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 2/21/19 21:28 BRFND47.21.3 4.6
Ethanol 25 8.0 2/21/19 21:28 BRFV-06, Z-01 47 4153.6 6.7
Ethyl Acetate ND 0.40 2/21/19 21:28 BRFND41.40.15 0.54
Ethylbenzene 0.56 0.20 2/21/19 21:28 BRF2.4 40.870.12 0.50
4-Ethyltoluene 1.1 0.20 2/21/19 21:28 BRF5.5 40.980.12 0.60
Heptane ND 0.20 2/21/19 21:28 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.40 2/21/19 21:28 BRFV-05 ND 44.30.092 0.98
Hexane ND 8.0 2/21/19 21:28 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 2/21/19 21:28 BRFND40.820.12 0.48
Isopropanol ND 8.0 2/21/19 21:28 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 2/21/19 21:28 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 2/21/19 21:28 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)3.0 0.20 2/21/19 21:28 BRF1240.820.096 0.39
Naphthalene ND 0.20 2/21/19 21:28 BRFND41.00.15 0.80
Propene ND 8.0 2/21/19 21:28 BRFND4140.20 0.34
Styrene ND 0.20 2/21/19 21:28 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 2/21/19 21:28 BRFND41.40.089 0.61
Page 4 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/14/2019
Work Order: 19B0726Sample Description/Location:
Field Sample #: SG-1
Sample ID: 19B0726-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): 28.0
Final Vacuum(in Hg): 4.5
Receipt Vacuum(in Hg): -4.8
Sampled: 2/12/2019 17:40
Canister ID: 2343
Flow Controller ID: 4235
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 10 0.20 2/21/19 21:28 BRF7141.40.11 0.75
Tetrahydrofuran ND 0.20 2/21/19 21:28 BRFND40.590.13 0.39
Toluene 1.6 0.20 2/21/19 21:28 BRF6.0 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 2/21/19 21:28 BRFV-05 ND 43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 2/21/19 21:28 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 2/21/19 21:28 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 2/21/19 21:28 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.35 0.80 2/21/19 21:28 BRFJ2.0 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 2/21/19 21:28 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 1.4 0.20 2/21/19 21:28 BRF6.7 40.980.13 0.63
1,3,5-Trimethylbenzene 0.72 0.20 2/21/19 21:28 BRF3.5 40.980.13 0.62
Vinyl Acetate ND 4.0 2/21/19 21:28 BRFND4140.095 0.34
Vinyl Chloride 0.54 0.20 2/21/19 21:28 BRF1.4 40.510.13 0.32
m&p-Xylene 2.7 0.40 2/21/19 21:28 BRF1241.70.23 1.00
o-Xylene 0.73 0.20 2/21/19 21:28 BRF3.2 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)87.5 2/21/19 21:2870-130
Page 5 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/14/2019
Work Order: 19B0726Sample Description/Location:
Field Sample #: SG-2
Sample ID: 19B0726-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): 28.5
Final Vacuum(in Hg): 5.0
Receipt Vacuum(in Hg): -4.9
Sampled: 2/12/2019 17:04
Canister ID: 2342
Flow Controller ID: 4246
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 5.2 8.0 2/21/19 22:24 BRFJ124192.8 6.6
Benzene 0.25 0.20 2/21/19 22:24 BRF0.79 40.640.082 0.26
Benzyl chloride ND 0.20 2/21/19 22:24 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 2/21/19 22:24 BRFND41.30.074 0.49
Bromoform ND 0.20 2/21/19 22:24 BRFND42.10.090 0.93
Bromomethane ND 0.20 2/21/19 22:24 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 2/21/19 22:24 BRFND40.440.13 0.28
2-Butanone (MEK)0.90 8.0 2/21/19 22:24 BRFJ2.7 4240.31 0.92
Carbon Disulfide ND 2.0 2/21/19 22:24 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 2/21/19 22:24 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 2/21/19 22:24 BRFND40.920.098 0.45
Chloroethane ND 0.40 2/21/19 22:24 BRFND41.10.12 0.32
Chloroform ND 0.20 2/21/19 22:24 BRFND40.980.074 0.36
Chloromethane ND 0.40 2/21/19 22:24 BRFND40.830.14 0.28
Cyclohexane ND 0.20 2/21/19 22:24 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 2/21/19 22:24 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 2/21/19 22:24 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 2/21/19 22:24 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 2/21/19 22:24 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 2/21/19 22:24 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 2/21/19 22:24 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 2/21/19 22:24 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 2/21/19 22:24 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 2/21/19 22:24 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 2/21/19 22:24 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 2/21/19 22:24 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 2/21/19 22:24 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 2/21/19 22:24 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 2/21/19 22:24 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 2/21/19 22:24 BRFV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 2/21/19 22:24 BRFND47.21.3 4.6
Ethanol 14 8.0 2/21/19 22:24 BRFV-06, Z-01 27 4153.6 6.7
Ethyl Acetate 1.0 0.40 2/21/19 22:24 BRF3.8 41.40.15 0.54
Ethylbenzene ND 0.20 2/21/19 22:24 BRFND40.870.12 0.50
4-Ethyltoluene ND 0.20 2/21/19 22:24 BRFND40.980.12 0.60
Heptane ND 0.20 2/21/19 22:24 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.40 2/21/19 22:24 BRFV-05 ND 44.30.092 0.98
Hexane ND 8.0 2/21/19 22:24 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 2/21/19 22:24 BRFND40.820.12 0.48
Isopropanol ND 8.0 2/21/19 22:24 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 2/21/19 22:24 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 2/21/19 22:24 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 2/21/19 22:24 BRFND40.820.096 0.39
Naphthalene ND 0.20 2/21/19 22:24 BRFND41.00.15 0.80
Propene ND 8.0 2/21/19 22:24 BRFND4140.20 0.34
Styrene ND 0.20 2/21/19 22:24 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 2/21/19 22:24 BRFND41.40.089 0.61
Page 6 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/14/2019
Work Order: 19B0726Sample Description/Location:
Field Sample #: SG-2
Sample ID: 19B0726-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): 28.5
Final Vacuum(in Hg): 5.0
Receipt Vacuum(in Hg): -4.9
Sampled: 2/12/2019 17:04
Canister ID: 2342
Flow Controller ID: 4246
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 1.2 0.20 2/21/19 22:24 BRF8.0 41.40.11 0.75
Tetrahydrofuran ND 0.20 2/21/19 22:24 BRFND40.590.13 0.39
Toluene 1.9 0.20 2/21/19 22:24 BRF7.2 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 2/21/19 22:24 BRFV-05 ND 43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 2/21/19 22:24 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 2/21/19 22:24 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 2/21/19 22:24 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.38 0.80 2/21/19 22:24 BRFJ2.1 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 2/21/19 22:24 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 2/21/19 22:24 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 2/21/19 22:24 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 2/21/19 22:24 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 2/21/19 22:24 BRFND40.510.13 0.32
m&p-Xylene 0.56 0.40 2/21/19 22:24 BRF2.4 41.70.23 1.00
o-Xylene ND 0.20 2/21/19 22:24 BRFND40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)87.8 2/21/19 22:2470-130
Page 7 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
19B0726-03 [SG-1]B224186 1.5 1 N/A 1000 400 150 02/21/19
19B0726-04 [SG-2]B224186 1.5 1 N/A 1000 400 150 02/21/19
Page 8 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B224186 - TO-15 Prep
Blank (B224186-BLK1)Prepared & Analyzed: 02/21/19
0.035NDNaphthalene
0.035ND1,1,2,2-Tetrachloroethane
0.035NDTetrachloroethylene
0.035ND1,2,4-Trichlorobenzene
0.035ND1,1,2-Trichloroethane
0.035NDTrichloroethylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)87.06.96
LCS (B224186-BS1)Prepared & Analyzed: 02/21/19
5.00 70-13097.94.90Naphthalene
5.00 70-13082.04.101,1,2,2-Tetrachloroethane
5.00 70-13081.34.07Tetrachloroethylene
5.00 70-13090.44.521,2,4-Trichlorobenzene
5.00 70-13085.84.291,1,2-Trichloroethane
5.00 70-13085.44.27Trichloroethylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)91.37.30
Page 9 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for
this compound.
V-06
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult
compound and passes the in house limits of 50-150%.
Z-01
ANALYST
Raisa A. PetraitisRAP
Kerry K. McGeeKKM
Brittany R. FiskBRF
Page 10 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S032661-ICV1 )Lab File ID: B021945.D Analyzed: 02/20/19 09:26
Bromochloromethane (1)92871 5.068 89821 5.064 60 - 140103 0.0040 +/-0.50
1,4-Difluorobenzene (1)178650 6.282 169716 6.283 60 - 140105 -0.0010 +/-0.50
Chlorobenzene-d5 (1)166175 9.881 158958 9.883 60 - 140105 -0.0020 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S032743-CCV1 )Lab File ID: B022104.D Analyzed: 02/21/19 12:11
Bromochloromethane (1)89698 5.065 89821 5.064 60 - 140100 0.0010 +/-0.50
1,4-Difluorobenzene (1)125182 6.285 169716 6.283 60 - 14074 0.0020 +/-0.50
Chlorobenzene-d5 (1)134914 9.878 158958 9.883 60 - 14085 -0.0050 +/-0.50
LCS (B224186-BS1 )Lab File ID: B022105.D Analyzed: 02/21/19 12:38
Bromochloromethane (1)89429 5.07 89698 5.065 60 - 140100 0.0050 +/-0.50
1,4-Difluorobenzene (1)142552 6.284 125182 6.285 60 - 140114 -0.0010 +/-0.50
Chlorobenzene-d5 (1)130723 9.877 134914 9.878 60 - 14097 -0.0010 +/-0.50
Blank (B224186-BLK1 )Lab File ID: B022109.D Analyzed: 02/21/19 14:38
Bromochloromethane (1)79008 5.064 89698 5.065 60 - 14088 -0.0010 +/-0.50
1,4-Difluorobenzene (1)120502 6.284 125182 6.285 60 - 14096 -0.0010 +/-0.50
Chlorobenzene-d5 (1)107111 9.877 134914 9.878 60 - 14079 -0.0010 +/-0.50
SG-1 (19B0726-03 )Lab File ID: B022123.D Analyzed: 02/21/19 21:28
Bromochloromethane (1)71589 5.066 89698 5.065 60 - 14080 0.0010 +/-0.50
1,4-Difluorobenzene (1)106607 6.286 125182 6.285 60 - 14085 0.0010 +/-0.50
Chlorobenzene-d5 (1)96362 9.879 134914 9.878 60 - 14071 0.0010 +/-0.50
SG-2 (19B0726-04 )Lab File ID: B022125.D Analyzed: 02/21/19 22:24
Bromochloromethane (1)70413 5.071 89698 5.065 60 - 14079 0.0060 +/-0.50
1,4-Difluorobenzene (1)105327 6.29 125182 6.285 60 - 14084 0.0050 +/-0.50
Chlorobenzene-d5 (1)95413 9.878 134914 9.878 60 - 14071 0.0000 +/-0.50
Page 11 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S032743-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.8529243A -25.0 303.75 1.1374465.00Acetone
1.016683A -6.3 304.68 1.0853035.00Benzene
0.9941859A -17.1 304.14 1.1992935.00Benzyl chloride
0.7357991A 0.9 305.04 0.7292025.00Bromodichloromethane
0.5471574A -13.6 304.32 0.63321235.00Bromoform
0.7430444A 3.4 305.17 0.71876075.00Bromomethane
0.539196A 10.3 305.51 0.48900045.001,3-Butadiene
1.319824A -23.3 303.84 1.7201115.002-Butanone (MEK)
1.270914A -4.8 304.76 1.3352775.00Carbon Disulfide
0.5055679A 5.0 305.25 0.48129035.00Carbon Tetrachloride
0.6969536A -25.5 303.72 0.9359395.00Chlorobenzene
0.4150996A 26.4 306.32 0.32831495.00Chloroethane
0.9502285A -25.9 303.70 1.2826685.00Chloroform
0.6490401A -18.0 304.10 0.7919085.00Chloromethane
0.4379543A 2.8 305.14 0.42595235.00Cyclohexane
0.5496005A -17.7 304.12 0.66760865.00Dibromochloromethane
0.4802467A -19.8 304.01 0.59868755.001,2-Dibromoethane (EDB)
0.5663104A -18.3 304.09 0.69290245.001,2-Dichlorobenzene
0.6111745A -20.3 303.98 0.76721865.001,3-Dichlorobenzene
0.6170331A -19.6 304.02 0.76770885.001,4-Dichlorobenzene
1.314527A -25.8 303.71 1.7704925.00Dichlorodifluoromethane (Freon 12)
0.881072A -28.0 303.60 1.2243725.001,1-Dichloroethane
0.6642913A -17.6 304.12 0.80666525.001,2-Dichloroethane
0.9685121A 11.0 305.55 0.87236655.001,1-Dichloroethylene
0.6679837A -24.1 303.80 0.88007475.00cis-1,2-Dichloroethylene
0.6232469A -24.8 303.76 0.8292585.00trans-1,2-Dichloroethylene
0.3905865A -2.2 304.89 0.39937115.001,2-Dichloropropane
0.6142353A -0.7 304.97 0.61838285.00cis-1,3-Dichloropropene
0.5895161A 6.6 305.33 0.55306265.00trans-1,3-Dichloropropene
1.406158A -34.3 *303.28 2.1418545.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.2198783A 13.0 305.65 0.19449895.001,4-Dioxane
0.203795A 41.4 *307.07 0.14416395.00Ethanol
0.2155856A -13.7 304.32 0.24967725.00Ethyl Acetate
1.261473A -15.7 304.21 1.4968515.00Ethylbenzene
1.202402A -14.2 304.29 1.4009135.004-Ethyltoluene
0.3446502A 7.1 305.35 0.3219415.00Heptane
0.2947774A -30.2 *303.49 0.34715465.00Hexachlorobutadiene
0.37616A -16.0 304.20 0.44774075.00Hexane
Page 12 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S032743-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
1.031638A -5.4 304.73 1.0907445.002-Hexanone (MBK)
1.097603A -18.6 304.07 1.3481195.00Isopropanol
1.288876A -25.5 303.73 1.7293545.00Methyl tert-Butyl Ether (MTBE)
0.6625254A -22.8 303.86 0.85830445.00Methylene Chloride
1.216341A 18.2 305.91 1.0293155.004-Methyl-2-pentanone (MIBK)
0.984307A -11.5 304.42 1.1122215.00Naphthalene
0.5341479A -9.2 304.54 0.5880635.00Propene
0.7308834A -5.7 304.72 0.77480215.00Styrene
0.8526795A -20.9 303.96 1.0775175.001,1,2,2-Tetrachloroethane
0.3664438A -20.3 303.99 0.45956315.00Tetrachloroethylene
0.8539945A -17.5 304.12 1.0351895.00Tetrahydrofuran
0.9192463A -19.1 304.05 1.1359545.00Toluene
0.3681634A -30.6 *303.47 0.42344465.001,2,4-Trichlorobenzene
0.534505A 1.0 305.05 0.52925725.001,1,1-Trichloroethane
0.3170612A -16.3 304.19 0.37867675.001,1,2-Trichloroethane
0.3133358A -8.0 304.60 0.34045245.00Trichloroethylene
1.261174A -4.8 304.76 1.3250715.00Trichlorofluoromethane (Freon 11)
0.9373854A -15.7 304.21 1.1122045.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.9280697A -10.8 304.46 1.039945.001,2,4-Trimethylbenzene
0.9617623A -8.8 304.56 1.0544335.001,3,5-Trimethylbenzene
1.799264A -18.2 304.09 2.1983085.00Vinyl Acetate
0.6881402A -14.7 304.27 0.80659545.00Vinyl Chloride
0.9945595A -9.2 309.08 1.09574410.0m&p-Xylene
0.9205272A -14.7 304.27 1.0789915.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 13 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 14 of 18
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2019
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2019
Page 15 of 18
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Appendix C Field Forms
Job No.:Well No.:Date:
Site Name:Location:
Equipment ( ) Dedicated ( ) Decontaminated ( ) Bailer ( ) Pump
Material ( ) PVC ( ) Stainless Steel ( ) Teflon ( ) Other___________
Decontamination Method:
Coordinates:________________________________ Top of Casing (TOC) Elevation________ ft msl
Material ( ) PVC ( ) Carbon Steel ( ) Stainless Steel ( ) Other:______________
Measurements from (TOC) Riser_______ ft Water Level_______ ft Bottom_______ ft
Method ( ) Bailing ( ) Pumping ( ) Other
Weather Conditions:
Final Water Condition: ( ) Clear ( ) Cloudy ( ) Other:______________ Odor:________________
Comments:
Performed by:______________________________________ Date:________ Time:________
WELL INFORMATION
pH
(SU)
Temp.
(oC)
S. Cond.
(umhos/cm)
Volume
DEVELOPMENT INFORMATION
Redox (NTU)
TurbidityRate
Hart & Hickman, PC
GENERAL INFORMATION
Well Development Form
(gallons)
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record
Date:11/5/2018
Job No:
Well ID:
Water Volume Pumping DO Temp.S. Cond.pH ORP Turbidity
Time Level Pumped Rate (mg/l)(oC)(µS/cm)(SU)(mV)(NTU)
Stabilization Criteria
Primary: Secondary:
pH +/- 0.1 unit DO +/- 0.2 mg/l
S.Cond. +/- 5%ORP +/- 20 mV
Turb. +/- 10% (<10 NTUs for metals)LOW-FLOW GROUNDWATER
Other Sample Parameters:___________________________________________________________________________________________________
Sampled at:____________________________ Parameters taken with:
Sample Delivered to:________________________________ by ______________________________________ at ____________________________.
Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________
Sample Parameter Containers (Types, Number of Containers, Preservatives):
SAMPLING RECORD Well Location:
Facility Name: Date:
Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:
Total Well Depth (ft):_____________________ Depth to Water (ft):_________________________________ Well Diameter:
Sampling Personnel:___________________________, __________________________ Screen Interval (ft bgs): _____________-______________
Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.
Weather Conditions:_______________________________________________________ NOTES:
GROUNDWATER SAMPLING PARAMETERS
Stabilization criteria guidelines from the EPA SESD Operating Procedure for Groundwater Sampling, dated April 26, 2017.
Sub-Slab / Soil Gas Vapor QA/QC Field Form Project No.:____________________
Depth of
Screen Date & Time Ambient
Temp.Purge Method Purge Vol Helium Conc.
Shroud
Helium Conc.
Purge
Leak Test
Passed
Yes / No SS, SG perm.,
temp.
concrete, wood,
asphalt, grass, soil,
gravel etc.
thickness
inches
(if appl.)
ft bgs mm/dd/yy
24-hour clock oF syringe, peristaltic,
etc.Liters %% or ppm
(indicate units
below)
Yes / No
(see note)
S:
C:
R:
S:
C:
R:
S:
C:
R:
S:
C:
R:
S= sample; C/R = canister/regulator; SS = sub-slab; SG = soil gas; perm = permanent; temp = temporary
Sampler(s):___________________________________________________________
Weather:___________________________________________________________
Notes:___________________________________________________________
___________________________________________________________
___________________________________________________________
___________________________________________________________
Helium Leak TestCanister /
Regulator
Shut-in Test
Passed Ground SurfaceID Numbers
Sample /
Canister /
Regulator
Type
Vapor Monitoring Point Construction
General Field Sketch of Sample Locations

Note: Leak Test Requirements
Per NC DEQ DWM Vapor Intrusion
Guidance, leak test passes if helium
concentration in purge air is less than
10% of helium concentration in shroud.
S:\BBB Master Templates\Forms - Soil Gas\Sub-slab & Soil Gas QA_QC Field Form
Sub-Slab / Soil Gas Sampling Vapor QA/QC Field Form
Hart & Hickman, PCN0 to 50 feetCustom
Polymers
Plyer Paper