23058_Durable Wood_ EPA SESD FINAL Report 20130715

Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 1 of 11

United States Environmental Protection Agency
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720

Sampling Investigation Report

Durable Woods Preservers, Inc.
Charlotte, North Carolina
SESD Project Identification Number: 13-0231

Investigation conducted: April 23, 2013
Report issued: July 15, 2013

Requestor: John E. Johnston SESD Project Leader: Mike Neill Corrective Action Section Enforcement Section Restoration and Underground Storage Tank Branch Enforcement and Investigations Branch
RCRA Division Science and Ecosystem Support Division
USEPA-R4, Sam Nunn Atlanta Federal Center 980 College Station Rd. 61 Forsyth St., Atlanta, GA 30303 Athens, GA 30605
Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 3 of 11
SAMPLING INVESTIGATION REPORT
DURABLE WOODS PRESERVERS, INC.
CHARLOTTE, NORTH CAROLINA

I. INTRODUCTION

On April 23, 2013, Science and Ecosystem Support Division (SESD) personnel conducted a
sampling investigation at the Durable Woods Preservers, Inc. (DWP) facility in Charlotte, North
Carolina. This investigation was requested by the RCRA, Restoration and Underground Storage
Tank (RUST) Branch, Corrective Action Section (CAS).
.
Personnel that were present for all or some of the investigation included:
PERSONNEL AFFILIATION PHONE
Mike Neill USEPA, SESD, Project Leader
706-355-8614
Art Masters USEPA, SESD, Safety Officer/Sampler 706-355-8612
Mark Wilkins NC Department of Environment and Natural Resources 919-707-8207
Bevo Barksdale Durable Woods Preservers 704- 537-3113
Brian Barksdale Durable Woods Preservers 704- 537-3113

II. SUMMARY

During SESD’s investigation, eight composite surface soil samples (DW01 –DW08) were
collected from the facility’s treated wood storage areas (TWSAs). In addition, a grab control soil
sample was collected from a vegetated area in front of the office. Samples were analyzed for
semi-volatile organic compounds (SVOCs), metals and hexavalent chromium. Several
semivolatile organic analytes were detected in the surface soil samples. Pentachlorophenol,
which had been used as a preservative by DWP, was detected above its Regional Screening
Level (RSL) for Chemical Contaminants at Superfund Sites for residential soil of 890 ug/kg
(0.89 mg/kg) in five of the eight samples collected from the TWSAs. Three of the samples were
found to exceed the pentachlorophenol RSL for industrial soil of 2,700 ug/kg. Samples DW01,
DW07 and DW08 were found to contain concentrations of pentachlorophenol of 25,000 ug/kg,
12,000 ug/kg, and 220,000 ug/kg, respectively. Aliquots for samples DW01, DW07 and DW08
were sent to Maxxam Analytics for chlorinated dibenzo-P-dioxins (CDDs) and chlorinated
dibenzofurans (CDFs) analyses. CDDs/CDFs results will be reviewed and validated by SESD’s
Quality Assurance Section, and will be reported as an addendum to this report.

Five of the samples from the TWSAs as well as the control sample were found to contain
benzo(a)pyrene above the RSL for residential soil of 15 ug/kg. Sample DW08 was found to
contain 210 ug/kg of benzo(a)pyrene which equals the RSL for industrial soil, and sample DW08
exceeded the benzo(b)fluoranthene RSL for residential soil of 150 ug/kg.

Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 4 of 11

Laboratory analyses showed that all of the samples except the control station exceeded the
arsenic RSLs for both residential soil (0.39 mg/kg) and industrial soil (1.6 mg/kg). Arsenic
concentrations ranged from 2.7 mg/kg to 1,500 mg/kg. The control sample contained 0.3 mg/kg
of arsenic.

III. BACKGROUND

Since 1955, Durable Wood has produced treated lumber at this facility using wood preservatives
injected into the wood under pressure. After pressure treatment is complete, excess preservative
is drained from the cylinder back into a preservative product storage tank. The treated wood
remains in the cylinder for a period of time to allow excess preservative to drip from the lumber.
The treated wood is then removed and taken to a treated wood storage yard. The treated wood
remains on site for weeks or months depending on product demand. During this time, rain falling
on the treated wood causes excess/residual preservative on the exterior of the lumber to be
washed off and onto the underlying soil. Durable Wood has not segregated lumber into different
areas based on preservative type. Therefore it is possible that any type of wood preservative used
at the site may be found at any location within the TWSAs. Wood preservatives used at the site
include chromated copper arsenate (CCA), pentachlorophenol (PCP), and chromated zinc
chloride.

Although not identified as an area of concern (AOC) in the RCRA Facility Assessment (RFA)
performed at Durable Wood, TWSAs are considered an AOC by NCDENR, and CAS has
requested SESD to investigate to determine whether releases of hazardous constituents are above
EPA’s Regional Screening Levels (RSLs).

IV. DISCUSSION OF FIELD ACTIVITIES

An authoritative sampling investigation was conducted, and nine proposed samples in the
SESD’s Quality Assurance Project Plan dated April 15, 2013, were collected during the
investigation.

SESD personnel arrived at the site at about 12:20 PM on April 23, 2013, and met with Mr.
Wilkens (NCDENR) and Mr. Bevo Barksdale (DWP). Figure 2 shows the sample stations that
target the various TWSAs. Composite surface samples (0 - 6˝) were collected from each station.
The control sample was a grab sample, and the station was selected because it was not the
process or operational areas of the facility. The control station was in an area vegetated with
grass in front of the office and under a large tree. Sampling was completed at approximately
4:00 PM. Field sample data collected during the investigation are presented in Table 1, and
photographs are in Appendix A.

The objective of this sampling investigation was to assess the analytical data with EPA’s RSLs
for both industrial and residential soils (November 2012). Samples were analyzed for semi-
volatile organic compounds (SVOCs), metals, and hexavalent chromium. An extra aliquot was
collected from each station for potential CDD/CDFs analyses.

Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 5 of 11
V. RESULTS OF ANALYSES

Samples were analyzed for metals using EPA methods 200.8, 6010, and 7473. Standard method
3500 was used to analyze the samples for hexavalent chromium. Samples were analyzed for
SVOCs using EPA method 8270D. Table 2 summarizes the laboratory SVOCs analytical results
and Table 3 summarizes the metals analytical results. The tables present results only for detected
analytes. SESD’s complete analytical reports are included as Appendix B.

Several semivolatile organic analytes were detected in the surface soil samples. Pentachloro-
phenol, which had been used as a preservative by DWP, was detected above its RSL for
residential soil of 890 ug/kg in five of the samples (DW01, DW02, DW06, DW07 and DW08)
collected from TWSAs. Three of the samples were found to exceed the pentachlorophenol RSL
for industrial soil of 2,700 ug/kg. Samples DW01, DW07 and DW08 were found to contain
concentrations of pentachlorophenol of 25,000 ug/kg, 12,000 ug/kg, and 220,000 ug/kg,
respectively. The aliquots collected from the sample stations with the three highest
concentrations of pentachlorophenol, DW01, DW07 and DW08, were sent to a Maxxam
Analytics on June 5th for CDDs/CDFs analyses. CDDs/CDFs results will be reviewed and
validated by SESD’s Quality Assurance Section, and will be reported as an addendum to this
report.

Two polycyclic aromatic hydrocarbons (PAHs), benzo(a)pyrene and benzo(b)fluoranthene, were
detected above their residential soil RSLs. Five of the samples from TWSAs and the control
sample were found to contain benzo(a)pyrene above the RSL for residential soil of 15 ug/kg.
Benzo(a)pyrene ranged from 30 ug/kg to 210 ug/kg in samples DW01, DW02, DW05, DW06
and DW08, and it was detected in the control sample at 34 ug/kg. Sample DW08 was found to
contain highest concentration of benzo(a)pyrene at 210 ug/kg which equals the RSL for
industrial soil. Sample DW08 also exceeded the benzo(b)fluoranthene RSL for residential soil of
150 ug/kg.

Laboratory analyses showed that all of the samples except the control station exceeded the
arsenic RSLs for both residential soil (0.39 mg/kg) and industrial soil (1.6 mg/kg). Arsenic
concentrations ranged from 2.7mg/kg to 1,500 mg/kg. The control sample contained 0.3 mg/kg
of arsenic.

None of the samples were found to contain hexavalent chromium. Sample DW05 was
determined to be reducing in nature which is not supportive of the presence hexavalent
chromium. Using standard method 3500, the method reporting limits (MRLs) for the samples
were at or below the hexavalent chromium RSL for industrial soil of 5.6 mg/kg for all but two
samples, the control sample and sample DW04.

VII. RESULTS OF FIELD QUALITY CONTROL SAMPLES

Sample DW01 was designated as the SVOC laboratory the matrix spike/matrix spike duplicate
(MS/MSD) sample. For the metal analyses, sample DW05 was used as a quality control sample.
Results of quality control analyses are contained in the Laboratory Analytical Reports in
Appendix B, and are acceptable for the purposes of this investigation. The reported results are
accurate within the limits of the methods.
Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 6 of 11

VIII. METHODOLOGY

Field activities were conducted in accordance with the Region 4, SESD Field Branches Quality
System and Technical Procedures. Specific field procedures applicable to this investigation
included the following:

Soil Sampling, SESDPROC-300-R2
Global Positioning System, SESDPROC-110-R3
Field Equipment Cleaning and Decontamination, SESDPROC-205-R2
Management of Investigation Derived Waste, SESDPROC-202-R2

Samples were analyzed at the SESD laboratory in accordance with the SESD Analytical Support
Branch Laboratory Operations and Quality Assurance Manual, February 2013. The SESD
laboratory is accredited by the ANSI-ASQ National Accreditation Board/ACLASS for ISO/IEC
17025.

Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 7 of 11

TABLE 1. FIELD SAMPLE DATA

SAMPLE DATE LATITUDE LONGITUDE DEPTH EQUIPMENT DESCRIPTION
Control 04/23/13 33.93276044 -80.3608732 0-6" Auger
Grab, grass area SW of office;
Red, orange clay
DW01

04/23/13 35.22033921 -80.69893557 0-6" Spoon
Composite- 3 points, SE of retort
area; light tan silt
DW02

04/23/13 35.22010485 -80.69849937 0-6" Auger
Comp. – 4 points, S. TWSA;
Red clay
DW03

04/23/13 35.22018531 -80.69827474 0-6" Auger
Comp. – 3 points, TW storage
shed; brown soil, clay w/ gravel
DW04

04/23/13 35.22055185 -80.69804063 0-6" Auger
Comp. – 4 points, Central TWSA;
Red clay
DW05

04/23/13 35.2204335 -80.69747183 0-6" Auger
Comp. – 4 points, TWSA;
brown soil w/ gravel
DW06

04/23/13
35.22063358 -80.697946 0-6" Auger
Comp. – 4 points, TWSA;
brown soil, orange clay w/ small
chips of wood
DW07

04/23/13 35.22113666 -80.69864279 0-6" Auger
Comp. – 4 aliquots, S. TWSA;
Red clay
DW08

04/23/13 35.22174141 -80.69976906 0-6" Auger
Comp. – 4 aliquots, S. TWSA;
Light brown soil w/ gravel

Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 8 of 11
- Exceedances of Regional Screening Levels (RSLs) for Chemical Contaminants at Superfund Sites – residential soil are highlighted in red.
- Exceedances of Regional Screening Levels (RSLs) for Chemical Contaminants at Superfund Sites – industrial soil have a yellow background.

Table 2 - Semivolatile Organic Data Summary and
Regional Screening Levels for Soils (November 2012)
Analyte Units
Residential
Soil RSL
Industrial
Soil RSL Control DW01 DW02 DW03 DW04 DW05 DW06 DW07 DW08
1-Methylnaphthalene ug/kg dry 16,000 ug/kg 53,000 ug/kg 60 < 37 U 24 < 3.7 U < 4.2 U 4.1 < 3.9 U < 3.8 U < 73 U
2,3,4,6-Tetrachlorophenol ug/kg dry 1,800,000 ug/kg 18,000,000 ug/kg < 390 U 960 J,O 110 J,O < 360 U < 420 U < 370 U < 380 U 50 J,O 6400 J,O
2-Methylnaphthalene ug/kg dry 230,000 ug/kg 2,200,000 ug/kg 140 50 40 4.8 < 4.2 U 8.2 6.3 < 3.8 U 120
Acenaphthene ug/kg dry 3,400,000 ug/kg 33,000,000 ug/kg < 4.0 U < 37 U 4.3 < 3.7 U < 4.2 U < 3.7 U < 3.9 U < 3.8 U < 73 U
Acenaphthylene ug/kg dry 17 < 37 U 4.4 < 3.7 U < 4.2 U 4.2 < 3.9 U < 3.8 U < 73 U
Anthracene ug/kg dry 17,000,000 ug/kg 170,000,000ug/kg 8.1 < 37 U 8.8 < 3.7 U < 4.2 U 4.7 6.9 < 3.8 U 77
Benzaldehyde ug/kg dry 7,800,000 ug/kg 100,000,000ug/kg < 390 U < 3700 U < 380 U 87 J,O < 420 U 50 J,O 51 J,O < 380 U < 7300 U
Benzo(a)anthracene ug/kg dry 150 ug/kg 2,100 ug/kg 31 55 28 5.3 < 4.2 U 37 8.2 5.7 < 73 U
Benzo(a)pyrene ug/kg dry 15 ug/kg 210 ug/kg 34 130 30 7 < 4.2 U 42 37 11 210
Benzo(b)fluoranthene ug/kg dry 150 ug/kg 2,100 ug/kg 48 120 52 15 < 4.2 U 100 41 11 180
Benzo(g,h,i)perylene ug/kg dry 30 68 24 12 < 4.2 U 44 14 7.3 83
Benzo(k)fluoranthene ug/kg dry 1,500 ug/kg 21,000 ug/kg 34 65 41 9.9 < 4.2 U 72 21 8.1 140
Bis(2-ethylhexyl) phthalate ug/kg dry 35,000 ug/kg 120,000 ug/kg < 390 U < 3700 U < 380 U < 360 U < 420 U < 370 U < 380 U < 380 U 3800 J,O
Carbazole ug/kg dry 8.3 < 37 U 11 < 3.7 U < 4.2 U 6.3 < 3.9 U < 3.8 U 540
Chrysene ug/kg dry 15, 000 ug/kg 210,000 ug/kg 55 130 77 12 < 4.2 U 96 35 13 350
Di-n-octylphthalate ug/kg dry 730,000 ug/kg 7,400,000 ug/kg < 390 U < 3700 U < 380 U < 360 U < 420 U < 370 U < 380 U 2600 1200 J,O
Dibenz(a,h)anthracene ug/kg dry 15 ug/kg 210 ug/kg 11 < 37 U 7.8 3.9 < 4.2 U 11 4 < 3.8 U < 73 U
Fluoranthene ug/kg dry 2,300,000 ug/kg 22,000,000 ug/kg 110 96 170 12 < 4.2 U 120 24 13 330
Fluorene ug/kg dry 2,300,000 ug/kg 22,000,000 ug/kg 4.2 < 37 U < 3.8 U < 3.7 U < 4.2 U < 3.7 U < 3.9 U < 3.8 U < 73 U
Hexachlorobenzene (HCB) ug/kg dry 300 ug/kg 1,100 ug/kg < 4.0 U,J,O < 37 U,J,O 14 J,O < 3.7 U,J,O < 4.2 U,J,O < 3.7 U,J,O < 3.9 U,J,O < 3.8 U,J,O < 73 U,J,O
Indeno (1,2,3-cd) pyrene ug/kg dry 150 ug/kg 2,100 ug/kg 25 57 20 8.6 < 4.2 U 32 14 5.9 < 73 U
Naphthalene ug/kg dry 3,600 ug/kg 18,000 ug/kg 170 < 37 U 23 4.2 < 4.2 U 6.6 5.3 < 3.8 U < 73 U
Pentachlorophenol ug/kg dry 890 ug/kg 2,700 ug/kg 100 25000 2000 830 49 610 960 12000 220000
Phenanthrene ug/kg dry 140 86 100 11 < 4.2 U 21 12 6.2 290
Pyrene ug/kg dry 1,700,000 ug/kg 17,000,000 ug/kg 77 130 140 16 < 4.2 U 140 30 36 2400
Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 9 of 11

- Exceedances of Regional Screening Levels (RSLs) for Chemical Contaminants at Superfund Sites – residential soil are highlighted in red.
- Exceedances of Regional Screening Levels (RSLs) for Chemical Contaminants at Superfund Sites – industrial soil have a yellow background.

ANALYTICAL DATA QUALIFIERS
U The analyte was not detected at or above the reporting limit.
J The identification of the analyte is acceptable; the reported value is an estimate.
O Other data qualifier(s), see Analytical Reports for specific qualifier and definition.

Table 3 - Metals Data Summary and
Regional Screening Levels for Soils (November 2012)
Analyte Units
Residential Soil
RSL Industrial Soil RSL Control DW01 DW02 DW03 DW04 DW05 DW06 DW07 DW08
Aluminum mg/kg dry 77000 mg/kg 990000 mg/kg 6000 12000 7100 6500 7700 7200 7400 7100 4700
Arsenic mg/kg dry 0.39 mg/kg 1.6 mg/kg 0.3 1500 39 480 2.7 200 160 14 600
Barium mg/kg dry 15000 mg/kg 190000 mg/kg 34 120 52 65 14 72 39 26 36
Calcium mg/kg dry 180 4500 440 3600 400 5200 1800 1200 1700
Chromium mg/kg dry 13 1900 51 680 53 250 J,O 250 42 600
Cobalt mg/kg dry 23 mg/kg 300 mg/kg 1.6 12 5 7.7 < 0.99 U 9 4 2.8 4.1
Copper mg/kg dry 3100 mg/kg 41000 mg/kg 30 1200 28 350 28 180 J,O 160 27 270
Iron mg/kg dry 55000 mg/kg 720000 mg/kg 13000 21000 14000 13000 34000 18000 18000 16000 13000
Lead mg/kg dry 400 mg/kg 800 mg/kg 5.3 < 25 U 22 11 7 12 6.8 6.6 17
Magnesium mg/kg dry 210 7800 540 3700 220 4600 J,O 1800 870 2100
Manganese mg/kg dry 1800 mg/kg 23000 mg/kg 82 580 410 320 120 400 230 150 230
Nickel mg/kg dry 1500 mg/kg 20000 mg/kg 2.2 16 3.6 23 < 2.0 U 13 4.7 2.2 6
Potassium mg/kg dry 240 4000 200 1700 230 1700 850 580 1000
Strontium mg/kg dry 47000 mg/kg 610000 mg/kg 2.3 28 3.7 16 2.7 17 7.9 4.7 7.1
Titanium mg/kg dry 44 550 41 280 140 310 J,O 140 110 170
Vanadium mg/kg dry 390 mg/kg 5200 mg/kg 35 45 38 28 92 32 47 39 21
Yttrium mg/kg dry 3.8 5.5 3.8 3.1 2.4 4.7 3.2 2 4.1
Zinc mg/kg dry 23000 mg/kg 310000 mg/kg 26 550 110 500 10 56 50 29 140
Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 10 of 11
Figure 1. Durable Wood Preservers, Inc. - Facility Location

Location

Durable Woods Preservers, Inc.
SESD Project ID # 13-0231
Page 11 of 11

Figure 2. Durable Wood Preservers, Inc. - Sample Locations

Location

Durable Woods Preservers, Inc.
Sampling Investigation Report, Appendix A
Charlotte, North Carolina
SESD Project ID # 13-0231 Page 1 of 4
APPENDIX A

SESD SAMPLING INVESTIGATION PHOTOGRAPHS
Durable Woods Preservers, Inc.
Sampling Investigation Report, Appendix A
Charlotte, North Carolina
SESD Project ID # 13-0231 Page 2 of 4

Photo 02 taken by M. Neill – 04/23/13

Looking East – Station DW01

Photo 01 taken by M. Neill – 04/23/13

Looking East – Control station

Photo 03 taken by M. Neill – 04/23/13

Looking Southeast – Station DW02

Durable Woods Preservers, Inc.
Sampling Investigation Report, Appendix A
Charlotte, North Carolina
SESD Project ID # 13-0231 Page 3 of 4

Photo 04 taken by M. Neill – 04/23/13

Looking West – Station DW03

Photo 05 taken by M. Neill – 04/23/13

Looking East – Station DW04

Photo 06 taken by M. Neill – 04/23/13

Looking North – Station DW05

Durable Woods Preservers, Inc.
Sampling Investigation Report, Appendix A
Charlotte, North Carolina
SESD Project ID # 13-0231 Page 4 of 4

Photo 07 taken by M. Neill – 04/23/13

Looking Northeast – Station DW06

Photo 09 taken by M. Neill – 04/23/13

Looking Southwest – Station DW08

Photo 08 taken by M. Neill – 04/23/13

Looking Northeast – Station DW07

APPENDIX B

SESD LABORATORY ANALYTICAL REPORTS

SESD Project ID # 13-0231 Durable Woods 1 of 78
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SESD Project ID # 13-0231 Durable Woods 2 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
June 3, 2013
MEMORANDUM
SUBJECT:
FROM:
FINAL Analytical Report
Project: 13-0231, Durable Wood Preservers, Inc.
Resource Conservation and Recovery Act
4SESD-ASB
Diana Burdette
OCS Chemist
ASB Organic Chemistry Section
Sallie Hale, ChiefTHRU:
TO:Mike Neill
Attached are the final results for the analytical groups listed below. These analyses were performed in
accordance with the Analytical Support Branch's (ASB) Laboratory Operations and Quality Assurance Manual
(ASB LOQAM) found at www.epa.gov/region4/sesd/asbsop. Any unique project data quality objectives
specified in writing by the data requestor have also been incorporated into the data unless otherwise noted in the
Report Narrative. Chemistry data have been verified based on the ASB LOQAM specifications and have been
qualified by this laboratory if the applicable quality control criteria were not met. Verification is defined in
Section 5.2 of the ASB LOQAM. For a listing of specific data qualifiers and explanations, please refer to the
Data Qualifier Definitions included in this report. The reported results are accurate within the limits of the
method(s) and are representative only of the samples as received by the laboratory.
Analyses Included in this report:Method Used:Accreditations:
Semi Volatile Organics (SVOA)
Semivolatile organic compounds ISOEPA 8270 SIM (Soil)
Semivolatile organic compounds ISOEPA 8270D (Soil)
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 1 of 44 SESD Project ID # 13-0231 Durable Woods 3 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Sample Disposal Policy
Because of the laboratory's limited space for long term sample storage, our policy is to dispose of samples on a
periodic schedule. Please note that within 60 days of this memo, the original samples and all sample extracts
and/or sample digestates will be disposed of in accordance with applicable regulations. The 60-day sample
disposal policy does not apply to criminal samples which are held until the laboratory is notified by the criminal
investigators that case development and litigation are complete.
These samples may be held in the laboratory's custody for a longer period of time if you have a special project
need. If you wish for the laboratory to hold samples beyond the 60-day period, please contact our Sample Control
Coordinator by e-mail at [e-mail], and provide a reason for holding samples beyond 60 days
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 2 of 44 SESD Project ID # 13-0231 Durable Woods 4 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Date ReceivedDate CollectedMatrixLaboratory IDSample ID
SAMPLES INCLUDED IN THIS REPORT
Project: 13-0231, Durable Wood Preservers, Inc.
Control E131702-01 Surface Soil 4/23/13 13:15 4/24/13 11:25
DW01 E131702-02 Surface Soil 4/23/13 13:40 4/24/13 11:25
DW02 E131702-03 Surface Soil 4/23/13 14:00 4/24/13 11:25
DW03 E131702-04 Surface Soil 4/23/13 14:15 4/24/13 11:25
DW04 E131702-05 Surface Soil 4/23/13 14:45 4/24/13 11:25
DW05 E131702-06 Surface Soil 4/23/13 15:10 4/24/13 11:25
DW06 E131702-07 Surface Soil 4/23/13 15:20 4/24/13 11:25
DW07 E131702-08 Surface Soil 4/23/13 15:40 4/24/13 11:25
DW08 E131702-09 Surface Soil 4/23/13 16:00 4/24/13 11:25
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 3 of 44 SESD Project ID # 13-0231 Durable Woods 5 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
DATA QUALIFIER DEFINITIONS
U The analyte was not detected at or above the reporting limit.
J The identification of the analyte is acceptable; the reported value is an estimate.
N There is presumptive evidence that the analyte is present; the analyte is reported as a tentative identification.
NJ Presumptive evidence that analyte is present; reported as a tentative identification with an estimated value.
Q-2 Result greater than MDL but less than MRL.
QL-1 Laboratory Control Spike Recovery less than method control limits
QS-5 Surrogate recovery is higher than established control limits
ACRONYMS AND ABBREVIATIONS
CAS Chemical Abstracts Service
Note: Analytes with no known CAS identifiers have been assigned codes beginning with "E", the EPA ID as assigned by
the EPA Substance Registry System (www.epa.gov/srs), or beginning with "R4-", a unique identifier assigned by the EPA
Region 4 laboratory.
ISO The test, if analyzed after June 26, 2012, is accredited under the EPA Region 4 ASB's ISO/IEC 17025 accreditation
issued by ANSI-ASQ National Accreditation Board/ACLASS. Refer to certificate and scope of accreditation
AT-1691.
MDL Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and
reported with a 99% confidence that the analyte concentration is greater than zero.
MRL Minimum Reporting Limit - Analyte concentration that corresponds to the lowest demonstrated level of acceptable
quantitation. The MRL is sample-specific and accounts for preparation weights and volumes, dilutions, and
moisture content of soil/sediments.
TIC Tentatively Identified Compound - An analyte identified based on a match with the instrument software's mass
spectral library. A calibration standard has not been analyzed to confirm the compound's identification or the
estimated concentration reported.
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D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: Control E131702-01
Matrix:Surface Soil
Date Collected:4/23/13 13:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:CONTROL
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
(3-and/or 4-)Methylphenol ug/kg dry EPA 8270D390U1319-77-3 5/15/1317:154/29/1310:51390
1,1-Biphenyl ug/kg dry EPA 8270D39U92-52-4 5/15/1317:154/29/1310:5139
1-Methylnaphthalene ug/kg dry EPA 8270D6090-12-0 5/15/1317:154/29/1310:514.0
2,3,4,6-Tetrachlorophenol ug/kg dry EPA 8270D390U58-90-2 5/15/1317:154/29/1310:51390
2,4,5-Trichlorophenol ug/kg dry EPA 8270D390U95-95-4 5/15/1317:154/29/1310:51390
2,4,6-Trichlorophenol ug/kg dry EPA 8270D390U88-06-2 5/15/1317:154/29/1310:51390
2,4-Dichlorophenol ug/kg dry EPA 8270D390U120-83-2 5/15/1317:154/29/1310:51390
2,4-Dimethylphenol ug/kg dry EPA 8270D390U105-67-9 5/15/1317:154/29/1310:51390
2,4-Dinitrophenol ug/kg dry EPA 8270D390U51-28-5 5/15/1317:154/29/1310:51390
2,4-Dinitrotoluene ug/kg dry EPA 8270D390U121-14-2 5/15/1317:154/29/1310:51390
2,6-Dinitrotoluene ug/kg dry EPA 8270D390U606-20-2 5/15/1317:154/29/1310:51390
2-Chloronaphthalene ug/kg dry EPA 8270D390U91-58-7 5/15/1317:154/29/1310:51390
2-Chlorophenol ug/kg dry EPA 8270D390U95-57-8 5/15/1317:154/29/1310:51390
2-Methyl-4,6-dinitrophenol ug/kg dry EPA 8270D390U534-52-1 5/15/1317:154/29/1310:51390
2-Methylnaphthalene ug/kg dry EPA 8270D14091-57-6 5/15/1317:154/29/1310:514.0
2-Methylphenol ug/kg dry EPA 8270D390U95-48-7 5/15/1317:154/29/1310:51390
2-Nitroaniline ug/kg dry EPA 8270D390U88-74-4 5/15/1317:154/29/1310:51390
2-Nitrophenol ug/kg dry EPA 8270D390U88-75-5 5/15/1317:154/29/1310:51390
3,3'-Dichlorobenzidine ug/kg dry EPA 8270D390U91-94-1 5/15/1317:154/29/1310:51390
3-Nitroaniline ug/kg dry EPA 8270D390U99-09-2 5/15/1317:154/29/1310:51390
4-Bromophenyl phenyl ether ug/kg dry EPA 8270D390U101-55-3 5/15/1317:154/29/1310:51390
4-Chloro-3-methylphenol ug/kg dry EPA 8270D390U59-50-7 5/15/1317:154/29/1310:51390
4-Chloroaniline ug/kg dry EPA 8270D390U106-47-8 5/15/1317:154/29/1310:51390
4-Chlorophenyl phenyl ether ug/kg dry EPA 8270D390U7005-72-3 5/15/1317:154/29/1310:51390
4-Nitroaniline ug/kg dry EPA 8270D390U100-01-6 5/15/1317:154/29/1310:51390
4-Nitrophenol ug/kg dry EPA 8270D390U100-02-7 5/15/1317:154/29/1310:51390
Acenaphthene ug/kg dry EPA 8270D4.0 U83-32-9 5/15/1317:154/29/1310:514.0
Acenaphthylene ug/kg dry EPA 8270D17208-96-8 5/15/1317:154/29/1310:514.0
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 5 of 44 SESD Project ID # 13-0231 Durable Woods 7 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: Control E131702-01
Matrix:Surface Soil
Date Collected:4/23/13 13:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:CONTROL
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Acetophenone ug/kg dry EPA 8270D390U98-86-2 5/15/1317:154/29/1310:51390
Anthracene ug/kg dry EPA 8270D8.1120-12-7 5/15/1317:154/29/1310:514.0
Atrazine ug/kg dry EPA 8270D390U1912-24-9 5/15/1317:154/29/1310:51390
Benzaldehyde ug/kg dry EPA 8270D390U100-52-7 5/15/1317:154/29/1310:51390
Benzo(a)anthracene ug/kg dry EPA 8270D3156-55-3 5/15/1317:154/29/1310:514.0
Benzo(a)pyrene ug/kg dry EPA 8270D3450-32-8 5/15/1317:154/29/1310:514.0
Benzo(b)fluoranthene ug/kg dry EPA 8270D48205-99-2 5/15/1317:154/29/1310:514.0
Benzo(g,h,i)perylene ug/kg dry EPA 8270D30191-24-2 5/15/1317:154/29/1310:514.0
Benzo(k)fluoranthene ug/kg dry EPA 8270D34207-08-9 5/15/1317:154/29/1310:514.0
Benzyl butyl phthalate ug/kg dry EPA 8270D390U85-68-7 5/15/1317:154/29/1310:51390
Bis(2-chloroethoxy)methane ug/kg dry EPA 8270D390U111-91-1 5/15/1317:154/29/1310:51390
bis(2-Chloroethyl) Ether ug/kg dry EPA 8270D390U111-44-4 5/15/1317:154/29/1310:51390
Bis(2-chloroisopropyl) ether ug/kg dry EPA 8270D390U39638-32-9 5/15/1317:154/29/1310:51390
Bis(2-ethylhexyl) phthalate ug/kg dry EPA 8270D390U117-81-7 5/15/1317:154/29/1310:51390
Caprolactam ug/kg dry EPA 8270D390U105-60-2 5/15/1317:154/29/1310:51390
Carbazole ug/kg dry EPA 8270D8.386-74-8 5/15/1317:154/29/1310:514.0
Chrysene ug/kg dry EPA 8270D55218-01-9 5/15/1317:154/29/1310:514.0
Dibenz(a,h)anthracene ug/kg dry EPA 8270D1153-70-3 5/15/1317:154/29/1310:514.0
Dibenzofuran ug/kg dry EPA 8270D40U132-64-9 5/15/1317:154/29/1310:5140
Diethyl phthalate ug/kg dry EPA 8270D390U84-66-2 5/15/1317:154/29/1310:51390
Dimethyl phthalate ug/kg dry EPA 8270D390U131-11-3 5/15/1317:154/29/1310:51390
Di-n-butylphthalate ug/kg dry EPA 8270D390U84-74-2 5/15/1317:154/29/1310:51390
Di-n-octylphthalate ug/kg dry EPA 8270D390U117-84-0 5/15/1317:154/29/1310:51390
Fluoranthene ug/kg dry EPA 8270D110206-44-0 5/15/1317:154/29/1310:514.0
Fluorene ug/kg dry EPA 8270D4.286-73-7 5/15/1317:154/29/1310:514.0
Hexachlorobenzene (HCB)ug/kg dry EPA 8270D4.0 U, J, QL-1118-74-1 5/15/1317:154/29/1310:514.0
Hexachlorocyclopentadiene (HCCP)ug/kg dry EPA 8270D390U77-47-4 5/15/1317:154/29/1310:51390
Hexachloroethane ug/kg dry EPA 8270D390U67-72-1 5/15/1317:154/29/1310:51390
Indeno (1,2,3-cd) pyrene ug/kg dry EPA 8270D25193-39-5 5/15/1317:154/29/1310:514.0
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 6 of 44 SESD Project ID # 13-0231 Durable Woods 8 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: Control E131702-01
Matrix:Surface Soil
Date Collected:4/23/13 13:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:CONTROL
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Isophorone ug/kg dry EPA 8270D390U78-59-1 5/15/1317:154/29/1310:51390
Naphthalene ug/kg dry EPA 8270D17091-20-3 5/15/1317:154/29/1310:514.0
Nitrobenzene ug/kg dry EPA 8270D390U98-95-3 5/15/1317:154/29/1310:51390
n-Nitroso di-n-Propylamine ug/kg dry EPA 8270D390U621-64-7 5/15/1317:154/29/1310:51390
n-Nitrosodiphenylamine/Diphenylamine ug/kg dry EPA 8270D390U122-39-4 5/15/1317:154/29/1310:51390
Pentachlorophenol ug/kg dry EPA 8270D10087-86-5 5/15/1317:154/29/1310:517.9
Phenanthrene ug/kg dry EPA 8270D14085-01-8 5/15/1317:154/29/1310:514.0
Phenol ug/kg dry EPA 8270D390U108-95-2 5/15/1317:154/29/1310:51390
Pyrene ug/kg dry EPA 8270D77129-00-0 5/15/1317:154/29/1310:514.0
Tentatively Identified Compounds:
EPA 8270Dug/kg dry800Decahydrotrimethylmethylenemethanoazu
lene (TIC)
NJR4-6506 5/15/1317:154/29/1310:51
EPA 8270Dug/kg dry900Hexadecanoic acid (TIC)NJR4-6510 5/15/1317:154/29/1310:51
EPA 8270DPetroleum Product: NR4-6500 5/15/1317:1510:5110:51
EPA 8270Dug/kg dry2000Phenanthrenol (TIC)NJR4-8000496 5/15/1317:154/29/1310:51
EPA 8270Dug/kg dry800Sitosterol (TIC)NJR4-6521 5/15/1317:154/29/1310:51
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 7 of 44 SESD Project ID # 13-0231 Durable Woods 9 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW01 E131702-02
Matrix:Surface Soil
Date Collected:4/23/13 13:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW01
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
(3-and/or 4-)Methylphenol ug/kg dry EPA 8270D3700U1319-77-3 5/15/1321:084/29/1310:513700
1,1-Biphenyl ug/kg dry EPA 8270D370U92-52-4 5/15/1321:084/29/1310:51370
1-Methylnaphthalene ug/kg dry EPA 8270D37U90-12-0 5/15/1321:084/29/1310:5137
2,3,4,6-Tetrachlorophenol ug/kg dry EPA 8270D960J, Q-258-90-2 5/15/1321:084/29/1310:513700
2,4,5-Trichlorophenol ug/kg dry EPA 8270D3700U95-95-4 5/15/1321:084/29/1310:513700
2,4,6-Trichlorophenol ug/kg dry EPA 8270D3700U88-06-2 5/15/1321:084/29/1310:513700
2,4-Dichlorophenol ug/kg dry EPA 8270D3700U120-83-2 5/15/1321:084/29/1310:513700
2,4-Dimethylphenol ug/kg dry EPA 8270D3700U105-67-9 5/15/1321:084/29/1310:513700
2,4-Dinitrophenol ug/kg dry EPA 8270D3700U51-28-5 5/15/1321:084/29/1310:513700
2,4-Dinitrotoluene ug/kg dry EPA 8270D3700U121-14-2 5/15/1321:084/29/1310:513700
2,6-Dinitrotoluene ug/kg dry EPA 8270D3700U606-20-2 5/15/1321:084/29/1310:513700
2-Chloronaphthalene ug/kg dry EPA 8270D3700U91-58-7 5/15/1321:084/29/1310:513700
2-Chlorophenol ug/kg dry EPA 8270D3700U95-57-8 5/15/1321:084/29/1310:513700
2-Methyl-4,6-dinitrophenol ug/kg dry EPA 8270D3700U534-52-1 5/15/1321:084/29/1310:513700
2-Methylnaphthalene ug/kg dry EPA 8270D5091-57-6 5/15/1321:084/29/1310:5137
2-Methylphenol ug/kg dry EPA 8270D3700U95-48-7 5/15/1321:084/29/1310:513700
2-Nitroaniline ug/kg dry EPA 8270D3700U88-74-4 5/15/1321:084/29/1310:513700
2-Nitrophenol ug/kg dry EPA 8270D3700U88-75-5 5/15/1321:084/29/1310:513700
3,3'-Dichlorobenzidine ug/kg dry EPA 8270D3700U91-94-1 5/15/1321:084/29/1310:513700
3-Nitroaniline ug/kg dry EPA 8270D3700U99-09-2 5/15/1321:084/29/1310:513700
4-Bromophenyl phenyl ether ug/kg dry EPA 8270D3700U101-55-3 5/15/1321:084/29/1310:513700
4-Chloro-3-methylphenol ug/kg dry EPA 8270D3700U59-50-7 5/15/1321:084/29/1310:513700
4-Chloroaniline ug/kg dry EPA 8270D3700U106-47-8 5/15/1321:084/29/1310:513700
4-Chlorophenyl phenyl ether ug/kg dry EPA 8270D3700U7005-72-3 5/15/1321:084/29/1310:513700
4-Nitroaniline ug/kg dry EPA 8270D3700U100-01-6 5/15/1321:084/29/1310:513700
4-Nitrophenol ug/kg dry EPA 8270D3700U100-02-7 5/15/1321:084/29/1310:513700
Acenaphthene ug/kg dry EPA 8270D37U83-32-9 5/15/1321:084/29/1310:5137
Acenaphthylene ug/kg dry EPA 8270D37U208-96-8 5/15/1321:084/29/1310:5137
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 8 of 44 SESD Project ID # 13-0231 Durable Woods 10 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW01 E131702-02
Matrix:Surface Soil
Date Collected:4/23/13 13:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW01
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Acetophenone ug/kg dry EPA 8270D3700U98-86-2 5/15/1321:084/29/1310:513700
Anthracene ug/kg dry EPA 8270D37U120-12-7 5/15/1321:084/29/1310:5137
Atrazine ug/kg dry EPA 8270D3700U1912-24-9 5/15/1321:084/29/1310:513700
Benzaldehyde ug/kg dry EPA 8270D3700U100-52-7 5/15/1321:084/29/1310:513700
Benzo(a)anthracene ug/kg dry EPA 8270D5556-55-3 5/15/1321:084/29/1310:5137
Benzo(a)pyrene ug/kg dry EPA 8270D13050-32-8 5/15/1321:084/29/1310:5137
Benzo(b)fluoranthene ug/kg dry EPA 8270D120205-99-2 5/15/1321:084/29/1310:5137
Benzo(g,h,i)perylene ug/kg dry EPA 8270D68191-24-2 5/15/1321:084/29/1310:5137
Benzo(k)fluoranthene ug/kg dry EPA 8270D65207-08-9 5/15/1321:084/29/1310:5137
Benzyl butyl phthalate ug/kg dry EPA 8270D3700U85-68-7 5/15/1321:084/29/1310:513700
Bis(2-chloroethoxy)methane ug/kg dry EPA 8270D3700U111-91-1 5/15/1321:084/29/1310:513700
bis(2-Chloroethyl) Ether ug/kg dry EPA 8270D3700U111-44-4 5/15/1321:084/29/1310:513700
Bis(2-chloroisopropyl) ether ug/kg dry EPA 8270D3700U39638-32-9 5/15/1321:084/29/1310:513700
Bis(2-ethylhexyl) phthalate ug/kg dry EPA 8270D3700U117-81-7 5/15/1321:084/29/1310:513700
Caprolactam ug/kg dry EPA 8270D3700U105-60-2 5/15/1321:084/29/1310:513700
Carbazole ug/kg dry EPA 8270D37U86-74-8 5/15/1321:084/29/1310:5137
Chrysene ug/kg dry EPA 8270D130218-01-9 5/15/1321:084/29/1310:5137
Dibenz(a,h)anthracene ug/kg dry EPA 8270D37U53-70-3 5/15/1321:084/29/1310:5137
Dibenzofuran ug/kg dry EPA 8270D370U132-64-9 5/15/1321:084/29/1310:51370
Diethyl phthalate ug/kg dry EPA 8270D3700U84-66-2 5/15/1321:084/29/1310:513700
Dimethyl phthalate ug/kg dry EPA 8270D3700U131-11-3 5/15/1321:084/29/1310:513700
Di-n-butylphthalate ug/kg dry EPA 8270D3700U84-74-2 5/15/1321:084/29/1310:513700
Di-n-octylphthalate ug/kg dry EPA 8270D3700U117-84-0 5/15/1321:084/29/1310:513700
Fluoranthene ug/kg dry EPA 8270D96206-44-0 5/15/1321:084/29/1310:5137
Fluorene ug/kg dry EPA 8270D37U86-73-7 5/15/1321:084/29/1310:5137
Hexachlorobenzene (HCB)ug/kg dry EPA 8270D37U, J, QL-1118-74-1 5/15/1321:084/29/1310:5137
Hexachlorocyclopentadiene (HCCP)ug/kg dry EPA 8270D3700U77-47-4 5/15/1321:084/29/1310:513700
Hexachloroethane ug/kg dry EPA 8270D3700U67-72-1 5/15/1321:084/29/1310:513700
Indeno (1,2,3-cd) pyrene ug/kg dry EPA 8270D57193-39-5 5/15/1321:084/29/1310:5137
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 9 of 44 SESD Project ID # 13-0231 Durable Woods 11 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW01 E131702-02
Matrix:Surface Soil
Date Collected:4/23/13 13:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW01
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Isophorone ug/kg dry EPA 8270D3700U78-59-1 5/15/1321:084/29/1310:513700
Naphthalene ug/kg dry EPA 8270D37U91-20-3 5/15/1321:084/29/1310:5137
Nitrobenzene ug/kg dry EPA 8270D3700U98-95-3 5/15/1321:084/29/1310:513700
n-Nitroso di-n-Propylamine ug/kg dry EPA 8270D3700U621-64-7 5/15/1321:084/29/1310:513700
n-Nitrosodiphenylamine/Diphenylamine ug/kg dry EPA 8270D3700U122-39-4 5/15/1321:084/29/1310:513700
Pentachlorophenol ug/kg dry EPA 8270D2500087-86-5 5/15/1321:084/29/1310:5175
Phenanthrene ug/kg dry EPA 8270D8685-01-8 5/15/1321:084/29/1310:5137
Phenol ug/kg dry EPA 8270D3700U108-95-2 5/15/1321:084/29/1310:513700
Pyrene ug/kg dry EPA 8270D130129-00-0 5/15/1321:084/29/1310:5137
Tentatively Identified Compounds:
EPA 8270Dug/kg dry4000Tentatively Identified Compounds UR4-0000 4000 5/15/1321:084/29/1310:51
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 10 of 44 SESD Project ID # 13-0231 Durable Woods 12 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW02 E131702-03
Matrix:Surface Soil
Date Collected:4/23/13 14:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW02
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
(3-and/or 4-)Methylphenol ug/kg dry EPA 8270D380U1319-77-3 5/15/1317:444/29/1310:51380
1,1-Biphenyl ug/kg dry EPA 8270D38U92-52-4 5/15/1317:444/29/1310:5138
1-Methylnaphthalene ug/kg dry EPA 8270D2490-12-0 5/15/1317:444/29/1310:513.8
2,3,4,6-Tetrachlorophenol ug/kg dry EPA 8270D110J, Q-258-90-2 5/15/1317:444/29/1310:51380
2,4,5-Trichlorophenol ug/kg dry EPA 8270D380U95-95-4 5/15/1317:444/29/1310:51380
2,4,6-Trichlorophenol ug/kg dry EPA 8270D380U88-06-2 5/15/1317:444/29/1310:51380
2,4-Dichlorophenol ug/kg dry EPA 8270D380U120-83-2 5/15/1317:444/29/1310:51380
2,4-Dimethylphenol ug/kg dry EPA 8270D380U105-67-9 5/15/1317:444/29/1310:51380
2,4-Dinitrophenol ug/kg dry EPA 8270D380U51-28-5 5/15/1317:444/29/1310:51380
2,4-Dinitrotoluene ug/kg dry EPA 8270D380U121-14-2 5/15/1317:444/29/1310:51380
2,6-Dinitrotoluene ug/kg dry EPA 8270D380U606-20-2 5/15/1317:444/29/1310:51380
2-Chloronaphthalene ug/kg dry EPA 8270D380U91-58-7 5/15/1317:444/29/1310:51380
2-Chlorophenol ug/kg dry EPA 8270D380U95-57-8 5/15/1317:444/29/1310:51380
2-Methyl-4,6-dinitrophenol ug/kg dry EPA 8270D380U534-52-1 5/15/1317:444/29/1310:51380
2-Methylnaphthalene ug/kg dry EPA 8270D4091-57-6 5/15/1317:444/29/1310:513.8
2-Methylphenol ug/kg dry EPA 8270D380U95-48-7 5/15/1317:444/29/1310:51380
2-Nitroaniline ug/kg dry EPA 8270D380U88-74-4 5/15/1317:444/29/1310:51380
2-Nitrophenol ug/kg dry EPA 8270D380U88-75-5 5/15/1317:444/29/1310:51380
3,3'-Dichlorobenzidine ug/kg dry EPA 8270D380U91-94-1 5/15/1317:444/29/1310:51380
3-Nitroaniline ug/kg dry EPA 8270D380U99-09-2 5/15/1317:444/29/1310:51380
4-Bromophenyl phenyl ether ug/kg dry EPA 8270D380U101-55-3 5/15/1317:444/29/1310:51380
4-Chloro-3-methylphenol ug/kg dry EPA 8270D380U59-50-7 5/15/1317:444/29/1310:51380
4-Chloroaniline ug/kg dry EPA 8270D380U106-47-8 5/15/1317:444/29/1310:51380
4-Chlorophenyl phenyl ether ug/kg dry EPA 8270D380U7005-72-3 5/15/1317:444/29/1310:51380
4-Nitroaniline ug/kg dry EPA 8270D380U100-01-6 5/15/1317:444/29/1310:51380
4-Nitrophenol ug/kg dry EPA 8270D380U100-02-7 5/15/1317:444/29/1310:51380
Acenaphthene ug/kg dry EPA 8270D4.383-32-9 5/15/1317:444/29/1310:513.8
Acenaphthylene ug/kg dry EPA 8270D4.4208-96-8 5/15/1317:444/29/1310:513.8
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 11 of 44 SESD Project ID # 13-0231 Durable Woods 13 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW02 E131702-03
Matrix:Surface Soil
Date Collected:4/23/13 14:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW02
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Acetophenone ug/kg dry EPA 8270D380U98-86-2 5/15/1317:444/29/1310:51380
Anthracene ug/kg dry EPA 8270D8.8120-12-7 5/15/1317:444/29/1310:513.8
Atrazine ug/kg dry EPA 8270D380U1912-24-9 5/15/1317:444/29/1310:51380
Benzaldehyde ug/kg dry EPA 8270D380U100-52-7 5/15/1317:444/29/1310:51380
Benzo(a)anthracene ug/kg dry EPA 8270D2856-55-3 5/15/1317:444/29/1310:513.8
Benzo(a)pyrene ug/kg dry EPA 8270D3050-32-8 5/15/1317:444/29/1310:513.8
Benzo(b)fluoranthene ug/kg dry EPA 8270D52205-99-2 5/15/1317:444/29/1310:513.8
Benzo(g,h,i)perylene ug/kg dry EPA 8270D24191-24-2 5/15/1317:444/29/1310:513.8
Benzo(k)fluoranthene ug/kg dry EPA 8270D41207-08-9 5/15/1317:444/29/1310:513.8
Benzyl butyl phthalate ug/kg dry EPA 8270D380U85-68-7 5/15/1317:444/29/1310:51380
Bis(2-chloroethoxy)methane ug/kg dry EPA 8270D380U111-91-1 5/15/1317:444/29/1310:51380
bis(2-Chloroethyl) Ether ug/kg dry EPA 8270D380U111-44-4 5/15/1317:444/29/1310:51380
Bis(2-chloroisopropyl) ether ug/kg dry EPA 8270D380U39638-32-9 5/15/1317:444/29/1310:51380
Bis(2-ethylhexyl) phthalate ug/kg dry EPA 8270D380U117-81-7 5/15/1317:444/29/1310:51380
Caprolactam ug/kg dry EPA 8270D380U105-60-2 5/15/1317:444/29/1310:51380
Carbazole ug/kg dry EPA 8270D1186-74-8 5/15/1317:444/29/1310:513.8
Chrysene ug/kg dry EPA 8270D77218-01-9 5/15/1317:444/29/1310:513.8
Dibenz(a,h)anthracene ug/kg dry EPA 8270D7.853-70-3 5/15/1317:444/29/1310:513.8
Dibenzofuran ug/kg dry EPA 8270D38U132-64-9 5/15/1317:444/29/1310:5138
Diethyl phthalate ug/kg dry EPA 8270D380U84-66-2 5/15/1317:444/29/1310:51380
Dimethyl phthalate ug/kg dry EPA 8270D380U131-11-3 5/15/1317:444/29/1310:51380
Di-n-butylphthalate ug/kg dry EPA 8270D380U84-74-2 5/15/1317:444/29/1310:51380
Di-n-octylphthalate ug/kg dry EPA 8270D380U117-84-0 5/15/1317:444/29/1310:51380
Fluoranthene ug/kg dry EPA 8270D170206-44-0 5/15/1317:444/29/1310:513.8
Fluorene ug/kg dry EPA 8270D3.8 U86-73-7 5/15/1317:444/29/1310:513.8
Hexachlorobenzene (HCB)ug/kg dry EPA 8270D14J, QL-1118-74-1 5/15/1317:444/29/1310:513.8
Hexachlorocyclopentadiene (HCCP)ug/kg dry EPA 8270D380U77-47-4 5/15/1317:444/29/1310:51380
Hexachloroethane ug/kg dry EPA 8270D380U67-72-1 5/15/1317:444/29/1310:51380
Indeno (1,2,3-cd) pyrene ug/kg dry EPA 8270D20193-39-5 5/15/1317:444/29/1310:513.8
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 12 of 44 SESD Project ID # 13-0231 Durable Woods 14 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW02 E131702-03
Matrix:Surface Soil
Date Collected:4/23/13 14:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW02
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Isophorone ug/kg dry EPA 8270D380U78-59-1 5/15/1317:444/29/1310:51380
Naphthalene ug/kg dry EPA 8270D2391-20-3 5/15/1317:444/29/1310:513.8
Nitrobenzene ug/kg dry EPA 8270D380U98-95-3 5/15/1317:444/29/1310:51380
n-Nitroso di-n-Propylamine ug/kg dry EPA 8270D380U621-64-7 5/15/1317:444/29/1310:51380
n-Nitrosodiphenylamine/Diphenylamine ug/kg dry EPA 8270D380U122-39-4 5/15/1317:444/29/1310:51380
Pentachlorophenol ug/kg dry EPA 8270D200087-86-5 5/15/1317:444/29/1310:517.6
Phenanthrene ug/kg dry EPA 8270D10085-01-8 5/15/1317:444/29/1310:513.8
Phenol ug/kg dry EPA 8270D380U108-95-2 5/15/1317:444/29/1310:51380
Pyrene ug/kg dry EPA 8270D140129-00-0 5/15/1317:444/29/1310:513.8
Tentatively Identified Compounds:
EPA 8270Dug/kg dry2000Chlordane (TIC)NJR4-8000798 5/15/1317:444/29/1310:51
EPA 8270Dug/kg dry900Dieldrin (TIC)NJR4-6578 5/15/1317:444/29/1310:51
EPA 8270Dug/kg dry1000Nonachloromethanoindene (TIC)NJR4-8001170 5/15/1317:444/29/1310:51
EPA 8270Dug/kg dry900Phenanthrenol (TIC)NJR4-8000496 5/15/1317:444/29/1310:51
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 13 of 44 SESD Project ID # 13-0231 Durable Woods 15 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW03 E131702-04
Matrix:Surface Soil
Date Collected:4/23/13 14:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW03
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
(3-and/or 4-)Methylphenol ug/kg dry EPA 8270D360U1319-77-3 5/15/1318:144/29/1310:51360
1,1-Biphenyl ug/kg dry EPA 8270D36U92-52-4 5/15/1318:144/29/1310:5136
1-Methylnaphthalene ug/kg dry EPA 8270D3.7 U90-12-0 5/15/1318:144/29/1310:513.7
2,3,4,6-Tetrachlorophenol ug/kg dry EPA 8270D360U58-90-2 5/15/1318:144/29/1310:51360
2,4,5-Trichlorophenol ug/kg dry EPA 8270D360U95-95-4 5/15/1318:144/29/1310:51360
2,4,6-Trichlorophenol ug/kg dry EPA 8270D360U88-06-2 5/15/1318:144/29/1310:51360
2,4-Dichlorophenol ug/kg dry EPA 8270D360U120-83-2 5/15/1318:144/29/1310:51360
2,4-Dimethylphenol ug/kg dry EPA 8270D360U105-67-9 5/15/1318:144/29/1310:51360
2,4-Dinitrophenol ug/kg dry EPA 8270D360U51-28-5 5/15/1318:144/29/1310:51360
2,4-Dinitrotoluene ug/kg dry EPA 8270D360U121-14-2 5/15/1318:144/29/1310:51360
2,6-Dinitrotoluene ug/kg dry EPA 8270D360U606-20-2 5/15/1318:144/29/1310:51360
2-Chloronaphthalene ug/kg dry EPA 8270D360U91-58-7 5/15/1318:144/29/1310:51360
2-Chlorophenol ug/kg dry EPA 8270D360U95-57-8 5/15/1318:144/29/1310:51360
2-Methyl-4,6-dinitrophenol ug/kg dry EPA 8270D360U534-52-1 5/15/1318:144/29/1310:51360
2-Methylnaphthalene ug/kg dry EPA 8270D4.891-57-6 5/15/1318:144/29/1310:513.7
2-Methylphenol ug/kg dry EPA 8270D360U95-48-7 5/15/1318:144/29/1310:51360
2-Nitroaniline ug/kg dry EPA 8270D360U88-74-4 5/15/1318:144/29/1310:51360
2-Nitrophenol ug/kg dry EPA 8270D360U88-75-5 5/15/1318:144/29/1310:51360
3,3'-Dichlorobenzidine ug/kg dry EPA 8270D360U91-94-1 5/15/1318:144/29/1310:51360
3-Nitroaniline ug/kg dry EPA 8270D360U99-09-2 5/15/1318:144/29/1310:51360
4-Bromophenyl phenyl ether ug/kg dry EPA 8270D360U101-55-3 5/15/1318:144/29/1310:51360
4-Chloro-3-methylphenol ug/kg dry EPA 8270D360U59-50-7 5/15/1318:144/29/1310:51360
4-Chloroaniline ug/kg dry EPA 8270D360U106-47-8 5/15/1318:144/29/1310:51360
4-Chlorophenyl phenyl ether ug/kg dry EPA 8270D360U7005-72-3 5/15/1318:144/29/1310:51360
4-Nitroaniline ug/kg dry EPA 8270D360U100-01-6 5/15/1318:144/29/1310:51360
4-Nitrophenol ug/kg dry EPA 8270D360U100-02-7 5/15/1318:144/29/1310:51360
Acenaphthene ug/kg dry EPA 8270D3.7 U83-32-9 5/15/1318:144/29/1310:513.7
Acenaphthylene ug/kg dry EPA 8270D3.7 U208-96-8 5/15/1318:144/29/1310:513.7
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 14 of 44 SESD Project ID # 13-0231 Durable Woods 16 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW03 E131702-04
Matrix:Surface Soil
Date Collected:4/23/13 14:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW03
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Acetophenone ug/kg dry EPA 8270D360U98-86-2 5/15/1318:144/29/1310:51360
Anthracene ug/kg dry EPA 8270D3.7 U120-12-7 5/15/1318:144/29/1310:513.7
Atrazine ug/kg dry EPA 8270D360U1912-24-9 5/15/1318:144/29/1310:51360
Benzaldehyde ug/kg dry EPA 8270D87J, Q-2100-52-7 5/15/1318:144/29/1310:51360
Benzo(a)anthracene ug/kg dry EPA 8270D5.356-55-3 5/15/1318:144/29/1310:513.7
Benzo(a)pyrene ug/kg dry EPA 8270D7.050-32-8 5/15/1318:144/29/1310:513.7
Benzo(b)fluoranthene ug/kg dry EPA 8270D15205-99-2 5/15/1318:144/29/1310:513.7
Benzo(g,h,i)perylene ug/kg dry EPA 8270D12191-24-2 5/15/1318:144/29/1310:513.7
Benzo(k)fluoranthene ug/kg dry EPA 8270D9.9207-08-9 5/15/1318:144/29/1310:513.7
Benzyl butyl phthalate ug/kg dry EPA 8270D360U85-68-7 5/15/1318:144/29/1310:51360
Bis(2-chloroethoxy)methane ug/kg dry EPA 8270D360U111-91-1 5/15/1318:144/29/1310:51360
bis(2-Chloroethyl) Ether ug/kg dry EPA 8270D360U111-44-4 5/15/1318:144/29/1310:51360
Bis(2-chloroisopropyl) ether ug/kg dry EPA 8270D360U39638-32-9 5/15/1318:144/29/1310:51360
Bis(2-ethylhexyl) phthalate ug/kg dry EPA 8270D360U117-81-7 5/15/1318:144/29/1310:51360
Caprolactam ug/kg dry EPA 8270D360U105-60-2 5/15/1318:144/29/1310:51360
Carbazole ug/kg dry EPA 8270D3.7 U86-74-8 5/15/1318:144/29/1310:513.7
Chrysene ug/kg dry EPA 8270D12218-01-9 5/15/1318:144/29/1310:513.7
Dibenz(a,h)anthracene ug/kg dry EPA 8270D3.953-70-3 5/15/1318:144/29/1310:513.7
Dibenzofuran ug/kg dry EPA 8270D37U132-64-9 5/15/1318:144/29/1310:5137
Diethyl phthalate ug/kg dry EPA 8270D360U84-66-2 5/15/1318:144/29/1310:51360
Dimethyl phthalate ug/kg dry EPA 8270D360U131-11-3 5/15/1318:144/29/1310:51360
Di-n-butylphthalate ug/kg dry EPA 8270D360U84-74-2 5/15/1318:144/29/1310:51360
Di-n-octylphthalate ug/kg dry EPA 8270D360U117-84-0 5/15/1318:144/29/1310:51360
Fluoranthene ug/kg dry EPA 8270D12206-44-0 5/15/1318:144/29/1310:513.7
Fluorene ug/kg dry EPA 8270D3.7 U86-73-7 5/15/1318:144/29/1310:513.7
Hexachlorobenzene (HCB)ug/kg dry EPA 8270D3.7 U, J, QL-1118-74-1 5/15/1318:144/29/1310:513.7
Hexachlorocyclopentadiene (HCCP)ug/kg dry EPA 8270D360U77-47-4 5/15/1318:144/29/1310:51360
Hexachloroethane ug/kg dry EPA 8270D360U67-72-1 5/15/1318:144/29/1310:51360
Indeno (1,2,3-cd) pyrene ug/kg dry EPA 8270D8.6193-39-5 5/15/1318:144/29/1310:513.7
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 15 of 44 SESD Project ID # 13-0231 Durable Woods 17 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW03 E131702-04
Matrix:Surface Soil
Date Collected:4/23/13 14:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW03
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Isophorone ug/kg dry EPA 8270D360U78-59-1 5/15/1318:144/29/1310:51360
Naphthalene ug/kg dry EPA 8270D4.291-20-3 5/15/1318:144/29/1310:513.7
Nitrobenzene ug/kg dry EPA 8270D360U98-95-3 5/15/1318:144/29/1310:51360
n-Nitroso di-n-Propylamine ug/kg dry EPA 8270D360U621-64-7 5/15/1318:144/29/1310:51360
n-Nitrosodiphenylamine/Diphenylamine ug/kg dry EPA 8270D360U122-39-4 5/15/1318:144/29/1310:51360
Pentachlorophenol ug/kg dry EPA 8270D83087-86-5 5/15/1318:144/29/1310:517.4
Phenanthrene ug/kg dry EPA 8270D1185-01-8 5/15/1318:144/29/1310:513.7
Phenol ug/kg dry EPA 8270D360U108-95-2 5/15/1318:144/29/1310:51360
Pyrene ug/kg dry EPA 8270D16129-00-0 5/15/1318:144/29/1310:513.7
Tentatively Identified Compounds:
EPA 8270Dug/kg dry400Unidentified Compounds JR4-6501 5/15/1318:144/29/1310:51
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 16 of 44 SESD Project ID # 13-0231 Durable Woods 18 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW04 E131702-05
Matrix:Surface Soil
Date Collected:4/23/13 14:45
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW04
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
(3-and/or 4-)Methylphenol ug/kg dry EPA 8270D420U1319-77-3 5/15/1316:174/29/1310:51420
1,1-Biphenyl ug/kg dry EPA 8270D42U92-52-4 5/15/1316:174/29/1310:5142
1-Methylnaphthalene ug/kg dry EPA 8270D4.2 U90-12-0 5/15/1316:174/29/1310:514.2
2,3,4,6-Tetrachlorophenol ug/kg dry EPA 8270D420U58-90-2 5/15/1316:174/29/1310:51420
2,4,5-Trichlorophenol ug/kg dry EPA 8270D420U95-95-4 5/15/1316:174/29/1310:51420
2,4,6-Trichlorophenol ug/kg dry EPA 8270D420U88-06-2 5/15/1316:174/29/1310:51420
2,4-Dichlorophenol ug/kg dry EPA 8270D420U120-83-2 5/15/1316:174/29/1310:51420
2,4-Dimethylphenol ug/kg dry EPA 8270D420U105-67-9 5/15/1316:174/29/1310:51420
2,4-Dinitrophenol ug/kg dry EPA 8270D420U51-28-5 5/15/1316:174/29/1310:51420
2,4-Dinitrotoluene ug/kg dry EPA 8270D420U121-14-2 5/15/1316:174/29/1310:51420
2,6-Dinitrotoluene ug/kg dry EPA 8270D420U606-20-2 5/15/1316:174/29/1310:51420
2-Chloronaphthalene ug/kg dry EPA 8270D420U91-58-7 5/15/1316:174/29/1310:51420
2-Chlorophenol ug/kg dry EPA 8270D420U95-57-8 5/15/1316:174/29/1310:51420
2-Methyl-4,6-dinitrophenol ug/kg dry EPA 8270D420U534-52-1 5/15/1316:174/29/1310:51420
2-Methylnaphthalene ug/kg dry EPA 8270D4.2 U91-57-6 5/15/1316:174/29/1310:514.2
2-Methylphenol ug/kg dry EPA 8270D420U95-48-7 5/15/1316:174/29/1310:51420
2-Nitroaniline ug/kg dry EPA 8270D420U88-74-4 5/15/1316:174/29/1310:51420
2-Nitrophenol ug/kg dry EPA 8270D420U88-75-5 5/15/1316:174/29/1310:51420
3,3'-Dichlorobenzidine ug/kg dry EPA 8270D420U91-94-1 5/15/1316:174/29/1310:51420
3-Nitroaniline ug/kg dry EPA 8270D420U99-09-2 5/15/1316:174/29/1310:51420
4-Bromophenyl phenyl ether ug/kg dry EPA 8270D420U101-55-3 5/15/1316:174/29/1310:51420
4-Chloro-3-methylphenol ug/kg dry EPA 8270D420U59-50-7 5/15/1316:174/29/1310:51420
4-Chloroaniline ug/kg dry EPA 8270D420U106-47-8 5/15/1316:174/29/1310:51420
4-Chlorophenyl phenyl ether ug/kg dry EPA 8270D420U7005-72-3 5/15/1316:174/29/1310:51420
4-Nitroaniline ug/kg dry EPA 8270D420U100-01-6 5/15/1316:174/29/1310:51420
4-Nitrophenol ug/kg dry EPA 8270D420U100-02-7 5/15/1316:174/29/1310:51420
Acenaphthene ug/kg dry EPA 8270D4.2 U83-32-9 5/15/1316:174/29/1310:514.2
Acenaphthylene ug/kg dry EPA 8270D4.2 U208-96-8 5/15/1316:174/29/1310:514.2
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 17 of 44 SESD Project ID # 13-0231 Durable Woods 19 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW04 E131702-05
Matrix:Surface Soil
Date Collected:4/23/13 14:45
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW04
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Acetophenone ug/kg dry EPA 8270D420U98-86-2 5/15/1316:174/29/1310:51420
Anthracene ug/kg dry EPA 8270D4.2 U120-12-7 5/15/1316:174/29/1310:514.2
Atrazine ug/kg dry EPA 8270D420U1912-24-9 5/15/1316:174/29/1310:51420
Benzaldehyde ug/kg dry EPA 8270D420U100-52-7 5/15/1316:174/29/1310:51420
Benzo(a)anthracene ug/kg dry EPA 8270D4.2 U56-55-3 5/15/1316:174/29/1310:514.2
Benzo(a)pyrene ug/kg dry EPA 8270D4.2 U50-32-8 5/15/1316:174/29/1310:514.2
Benzo(b)fluoranthene ug/kg dry EPA 8270D4.2 U205-99-2 5/15/1316:174/29/1310:514.2
Benzo(g,h,i)perylene ug/kg dry EPA 8270D4.2 U191-24-2 5/15/1316:174/29/1310:514.2
Benzo(k)fluoranthene ug/kg dry EPA 8270D4.2 U207-08-9 5/15/1316:174/29/1310:514.2
Benzyl butyl phthalate ug/kg dry EPA 8270D420U85-68-7 5/15/1316:174/29/1310:51420
Bis(2-chloroethoxy)methane ug/kg dry EPA 8270D420U111-91-1 5/15/1316:174/29/1310:51420
bis(2-Chloroethyl) Ether ug/kg dry EPA 8270D420U111-44-4 5/15/1316:174/29/1310:51420
Bis(2-chloroisopropyl) ether ug/kg dry EPA 8270D420U39638-32-9 5/15/1316:174/29/1310:51420
Bis(2-ethylhexyl) phthalate ug/kg dry EPA 8270D420U117-81-7 5/15/1316:174/29/1310:51420
Caprolactam ug/kg dry EPA 8270D420U105-60-2 5/15/1316:174/29/1310:51420
Carbazole ug/kg dry EPA 8270D4.2 U86-74-8 5/15/1316:174/29/1310:514.2
Chrysene ug/kg dry EPA 8270D4.2 U218-01-9 5/15/1316:174/29/1310:514.2
Dibenz(a,h)anthracene ug/kg dry EPA 8270D4.2 U53-70-3 5/15/1316:174/29/1310:514.2
Dibenzofuran ug/kg dry EPA 8270D42U132-64-9 5/15/1316:174/29/1310:5142
Diethyl phthalate ug/kg dry EPA 8270D420U84-66-2 5/15/1316:174/29/1310:51420
Dimethyl phthalate ug/kg dry EPA 8270D420U131-11-3 5/15/1316:174/29/1310:51420
Di-n-butylphthalate ug/kg dry EPA 8270D420U84-74-2 5/15/1316:174/29/1310:51420
Di-n-octylphthalate ug/kg dry EPA 8270D420U117-84-0 5/15/1316:174/29/1310:51420
Fluoranthene ug/kg dry EPA 8270D4.2 U206-44-0 5/15/1316:174/29/1310:514.2
Fluorene ug/kg dry EPA 8270D4.2 U86-73-7 5/15/1316:174/29/1310:514.2
Hexachlorobenzene (HCB)ug/kg dry EPA 8270D4.2 U, J, QL-1118-74-1 5/15/1316:174/29/1310:514.2
Hexachlorocyclopentadiene (HCCP)ug/kg dry EPA 8270D420U77-47-4 5/15/1316:174/29/1310:51420
Hexachloroethane ug/kg dry EPA 8270D420U67-72-1 5/15/1316:174/29/1310:51420
Indeno (1,2,3-cd) pyrene ug/kg dry EPA 8270D4.2 U193-39-5 5/15/1316:174/29/1310:514.2
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 18 of 44 SESD Project ID # 13-0231 Durable Woods 20 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW04 E131702-05
Matrix:Surface Soil
Date Collected:4/23/13 14:45
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW04
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Isophorone ug/kg dry EPA 8270D420U78-59-1 5/15/1316:174/29/1310:51420
Naphthalene ug/kg dry EPA 8270D4.2 U91-20-3 5/15/1316:174/29/1310:514.2
Nitrobenzene ug/kg dry EPA 8270D420U98-95-3 5/15/1316:174/29/1310:51420
n-Nitroso di-n-Propylamine ug/kg dry EPA 8270D420U621-64-7 5/15/1316:174/29/1310:51420
n-Nitrosodiphenylamine/Diphenylamine ug/kg dry EPA 8270D420U122-39-4 5/15/1316:174/29/1310:51420
Pentachlorophenol ug/kg dry EPA 8270D4987-86-5 5/15/1316:174/29/1310:518.4
Phenanthrene ug/kg dry EPA 8270D4.2 U85-01-8 5/15/1316:174/29/1310:514.2
Phenol ug/kg dry EPA 8270D420U108-95-2 5/15/1316:174/29/1310:51420
Pyrene ug/kg dry EPA 8270D4.2 U129-00-0 5/15/1316:174/29/1310:514.2
Tentatively Identified Compounds:
EPA 8270Dug/kg dry400Tentatively Identified Compounds UR4-0000 400 5/15/1316:174/29/1310:51
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 19 of 44 SESD Project ID # 13-0231 Durable Woods 21 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW05 E131702-06
Matrix:Surface Soil
Date Collected:4/23/13 15:10
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW05
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
(3-and/or 4-)Methylphenol ug/kg dry EPA 8270D370U1319-77-3 5/15/1318:434/29/1310:51370
1,1-Biphenyl ug/kg dry EPA 8270D37U92-52-4 5/15/1318:434/29/1310:5137
1-Methylnaphthalene ug/kg dry EPA 8270D4.190-12-0 5/15/1318:434/29/1310:513.7
2,3,4,6-Tetrachlorophenol ug/kg dry EPA 8270D370U58-90-2 5/15/1318:434/29/1310:51370
2,4,5-Trichlorophenol ug/kg dry EPA 8270D370U95-95-4 5/15/1318:434/29/1310:51370
2,4,6-Trichlorophenol ug/kg dry EPA 8270D370U88-06-2 5/15/1318:434/29/1310:51370
2,4-Dichlorophenol ug/kg dry EPA 8270D370U120-83-2 5/15/1318:434/29/1310:51370
2,4-Dimethylphenol ug/kg dry EPA 8270D370U105-67-9 5/15/1318:434/29/1310:51370
2,4-Dinitrophenol ug/kg dry EPA 8270D370U51-28-5 5/15/1318:434/29/1310:51370
2,4-Dinitrotoluene ug/kg dry EPA 8270D370U121-14-2 5/15/1318:434/29/1310:51370
2,6-Dinitrotoluene ug/kg dry EPA 8270D370U606-20-2 5/15/1318:434/29/1310:51370
2-Chloronaphthalene ug/kg dry EPA 8270D370U91-58-7 5/15/1318:434/29/1310:51370
2-Chlorophenol ug/kg dry EPA 8270D370U95-57-8 5/15/1318:434/29/1310:51370
2-Methyl-4,6-dinitrophenol ug/kg dry EPA 8270D370U534-52-1 5/15/1318:434/29/1310:51370
2-Methylnaphthalene ug/kg dry EPA 8270D8.291-57-6 5/15/1318:434/29/1310:513.7
2-Methylphenol ug/kg dry EPA 8270D370U95-48-7 5/15/1318:434/29/1310:51370
2-Nitroaniline ug/kg dry EPA 8270D370U88-74-4 5/15/1318:434/29/1310:51370
2-Nitrophenol ug/kg dry EPA 8270D370U88-75-5 5/15/1318:434/29/1310:51370
3,3'-Dichlorobenzidine ug/kg dry EPA 8270D370U91-94-1 5/15/1318:434/29/1310:51370
3-Nitroaniline ug/kg dry EPA 8270D370U99-09-2 5/15/1318:434/29/1310:51370
4-Bromophenyl phenyl ether ug/kg dry EPA 8270D370U101-55-3 5/15/1318:434/29/1310:51370
4-Chloro-3-methylphenol ug/kg dry EPA 8270D370U59-50-7 5/15/1318:434/29/1310:51370
4-Chloroaniline ug/kg dry EPA 8270D370U106-47-8 5/15/1318:434/29/1310:51370
4-Chlorophenyl phenyl ether ug/kg dry EPA 8270D370U7005-72-3 5/15/1318:434/29/1310:51370
4-Nitroaniline ug/kg dry EPA 8270D370U100-01-6 5/15/1318:434/29/1310:51370
4-Nitrophenol ug/kg dry EPA 8270D370U100-02-7 5/15/1318:434/29/1310:51370
Acenaphthene ug/kg dry EPA 8270D3.7 U83-32-9 5/15/1318:434/29/1310:513.7
Acenaphthylene ug/kg dry EPA 8270D4.2208-96-8 5/15/1318:434/29/1310:513.7
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 20 of 44 SESD Project ID # 13-0231 Durable Woods 22 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW05 E131702-06
Matrix:Surface Soil
Date Collected:4/23/13 15:10
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW05
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Acetophenone ug/kg dry EPA 8270D370U98-86-2 5/15/1318:434/29/1310:51370
Anthracene ug/kg dry EPA 8270D4.7120-12-7 5/15/1318:434/29/1310:513.7
Atrazine ug/kg dry EPA 8270D370U1912-24-9 5/15/1318:434/29/1310:51370
Benzaldehyde ug/kg dry EPA 8270D50J, Q-2100-52-7 5/15/1318:434/29/1310:51370
Benzo(a)anthracene ug/kg dry EPA 8270D3756-55-3 5/15/1318:434/29/1310:513.7
Benzo(a)pyrene ug/kg dry EPA 8270D4250-32-8 5/15/1318:434/29/1310:513.7
Benzo(b)fluoranthene ug/kg dry EPA 8270D100205-99-2 5/15/1318:434/29/1310:513.7
Benzo(g,h,i)perylene ug/kg dry EPA 8270D44191-24-2 5/15/1318:434/29/1310:513.7
Benzo(k)fluoranthene ug/kg dry EPA 8270D72207-08-9 5/15/1318:434/29/1310:513.7
Benzyl butyl phthalate ug/kg dry EPA 8270D370U85-68-7 5/15/1318:434/29/1310:51370
Bis(2-chloroethoxy)methane ug/kg dry EPA 8270D370U111-91-1 5/15/1318:434/29/1310:51370
bis(2-Chloroethyl) Ether ug/kg dry EPA 8270D370U111-44-4 5/15/1318:434/29/1310:51370
Bis(2-chloroisopropyl) ether ug/kg dry EPA 8270D370U39638-32-9 5/15/1318:434/29/1310:51370
Bis(2-ethylhexyl) phthalate ug/kg dry EPA 8270D370U117-81-7 5/15/1318:434/29/1310:51370
Caprolactam ug/kg dry EPA 8270D370U105-60-2 5/15/1318:434/29/1310:51370
Carbazole ug/kg dry EPA 8270D6.386-74-8 5/15/1318:434/29/1310:513.7
Chrysene ug/kg dry EPA 8270D96218-01-9 5/15/1318:434/29/1310:513.7
Dibenz(a,h)anthracene ug/kg dry EPA 8270D1153-70-3 5/15/1318:434/29/1310:513.7
Dibenzofuran ug/kg dry EPA 8270D37U132-64-9 5/15/1318:434/29/1310:5137
Diethyl phthalate ug/kg dry EPA 8270D370U84-66-2 5/15/1318:434/29/1310:51370
Dimethyl phthalate ug/kg dry EPA 8270D370U131-11-3 5/15/1318:434/29/1310:51370
Di-n-butylphthalate ug/kg dry EPA 8270D370U84-74-2 5/15/1318:434/29/1310:51370
Di-n-octylphthalate ug/kg dry EPA 8270D370U117-84-0 5/15/1318:434/29/1310:51370
Fluoranthene ug/kg dry EPA 8270D120206-44-0 5/15/1318:434/29/1310:513.7
Fluorene ug/kg dry EPA 8270D3.7 U86-73-7 5/15/1318:434/29/1310:513.7
Hexachlorobenzene (HCB)ug/kg dry EPA 8270D3.7 U, J, QL-1118-74-1 5/15/1318:434/29/1310:513.7
Hexachlorocyclopentadiene (HCCP)ug/kg dry EPA 8270D370U77-47-4 5/15/1318:434/29/1310:51370
Hexachloroethane ug/kg dry EPA 8270D370U67-72-1 5/15/1318:434/29/1310:51370
Indeno (1,2,3-cd) pyrene ug/kg dry EPA 8270D32193-39-5 5/15/1318:434/29/1310:513.7
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 21 of 44 SESD Project ID # 13-0231 Durable Woods 23 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW05 E131702-06
Matrix:Surface Soil
Date Collected:4/23/13 15:10
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW05
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Isophorone ug/kg dry EPA 8270D370U78-59-1 5/15/1318:434/29/1310:51370
Naphthalene ug/kg dry EPA 8270D6.691-20-3 5/15/1318:434/29/1310:513.7
Nitrobenzene ug/kg dry EPA 8270D370U98-95-3 5/15/1318:434/29/1310:51370
n-Nitroso di-n-Propylamine ug/kg dry EPA 8270D370U621-64-7 5/15/1318:434/29/1310:51370
n-Nitrosodiphenylamine/Diphenylamine ug/kg dry EPA 8270D370U122-39-4 5/15/1318:434/29/1310:51370
Pentachlorophenol ug/kg dry EPA 8270D61087-86-5 5/15/1318:434/29/1310:517.4
Phenanthrene ug/kg dry EPA 8270D2185-01-8 5/15/1318:434/29/1310:513.7
Phenol ug/kg dry EPA 8270D370U108-95-2 5/15/1318:434/29/1310:51370
Pyrene ug/kg dry EPA 8270D140129-00-0 5/15/1318:434/29/1310:513.7
Tentatively Identified Compounds:
EPA 8270Dug/kg dry400Tentatively Identified Compounds UR4-0000 400 5/15/1318:434/29/1310:51
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 22 of 44 SESD Project ID # 13-0231 Durable Woods 24 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW06 E131702-07
Matrix:Surface Soil
Date Collected:4/23/13 15:20
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW06
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
(3-and/or 4-)Methylphenol ug/kg dry EPA 8270D380U1319-77-3 5/15/1319:124/29/1310:51380
1,1-Biphenyl ug/kg dry EPA 8270D38U92-52-4 5/15/1319:124/29/1310:5138
1-Methylnaphthalene ug/kg dry EPA 8270D3.9 U90-12-0 5/15/1319:124/29/1310:513.9
2,3,4,6-Tetrachlorophenol ug/kg dry EPA 8270D380U58-90-2 5/15/1319:124/29/1310:51380
2,4,5-Trichlorophenol ug/kg dry EPA 8270D380U95-95-4 5/15/1319:124/29/1310:51380
2,4,6-Trichlorophenol ug/kg dry EPA 8270D380U88-06-2 5/15/1319:124/29/1310:51380
2,4-Dichlorophenol ug/kg dry EPA 8270D380U120-83-2 5/15/1319:124/29/1310:51380
2,4-Dimethylphenol ug/kg dry EPA 8270D380U105-67-9 5/15/1319:124/29/1310:51380
2,4-Dinitrophenol ug/kg dry EPA 8270D380U51-28-5 5/15/1319:124/29/1310:51380
2,4-Dinitrotoluene ug/kg dry EPA 8270D380U121-14-2 5/15/1319:124/29/1310:51380
2,6-Dinitrotoluene ug/kg dry EPA 8270D380U606-20-2 5/15/1319:124/29/1310:51380
2-Chloronaphthalene ug/kg dry EPA 8270D380U91-58-7 5/15/1319:124/29/1310:51380
2-Chlorophenol ug/kg dry EPA 8270D380U95-57-8 5/15/1319:124/29/1310:51380
2-Methyl-4,6-dinitrophenol ug/kg dry EPA 8270D380U534-52-1 5/15/1319:124/29/1310:51380
2-Methylnaphthalene ug/kg dry EPA 8270D6.391-57-6 5/15/1319:124/29/1310:513.9
2-Methylphenol ug/kg dry EPA 8270D380U95-48-7 5/15/1319:124/29/1310:51380
2-Nitroaniline ug/kg dry EPA 8270D380U88-74-4 5/15/1319:124/29/1310:51380
2-Nitrophenol ug/kg dry EPA 8270D380U88-75-5 5/15/1319:124/29/1310:51380
3,3'-Dichlorobenzidine ug/kg dry EPA 8270D380U91-94-1 5/15/1319:124/29/1310:51380
3-Nitroaniline ug/kg dry EPA 8270D380U99-09-2 5/15/1319:124/29/1310:51380
4-Bromophenyl phenyl ether ug/kg dry EPA 8270D380U101-55-3 5/15/1319:124/29/1310:51380
4-Chloro-3-methylphenol ug/kg dry EPA 8270D380U59-50-7 5/15/1319:124/29/1310:51380
4-Chloroaniline ug/kg dry EPA 8270D380U106-47-8 5/15/1319:124/29/1310:51380
4-Chlorophenyl phenyl ether ug/kg dry EPA 8270D380U7005-72-3 5/15/1319:124/29/1310:51380
4-Nitroaniline ug/kg dry EPA 8270D380U100-01-6 5/15/1319:124/29/1310:51380
4-Nitrophenol ug/kg dry EPA 8270D380U100-02-7 5/15/1319:124/29/1310:51380
Acenaphthene ug/kg dry EPA 8270D3.9 U83-32-9 5/15/1319:124/29/1310:513.9
Acenaphthylene ug/kg dry EPA 8270D3.9 U208-96-8 5/15/1319:124/29/1310:513.9
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 23 of 44 SESD Project ID # 13-0231 Durable Woods 25 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW06 E131702-07
Matrix:Surface Soil
Date Collected:4/23/13 15:20
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW06
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Acetophenone ug/kg dry EPA 8270D380U98-86-2 5/15/1319:124/29/1310:51380
Anthracene ug/kg dry EPA 8270D6.9120-12-7 5/15/1319:124/29/1310:513.9
Atrazine ug/kg dry EPA 8270D380U1912-24-9 5/15/1319:124/29/1310:51380
Benzaldehyde ug/kg dry EPA 8270D51J, Q-2100-52-7 5/15/1319:124/29/1310:51380
Benzo(a)anthracene ug/kg dry EPA 8270D8.256-55-3 5/15/1319:124/29/1310:513.9
Benzo(a)pyrene ug/kg dry EPA 8270D3750-32-8 5/15/1319:124/29/1310:513.9
Benzo(b)fluoranthene ug/kg dry EPA 8270D41205-99-2 5/15/1319:124/29/1310:513.9
Benzo(g,h,i)perylene ug/kg dry EPA 8270D14191-24-2 5/15/1319:124/29/1310:513.9
Benzo(k)fluoranthene ug/kg dry EPA 8270D21207-08-9 5/15/1319:124/29/1310:513.9
Benzyl butyl phthalate ug/kg dry EPA 8270D380U85-68-7 5/15/1319:124/29/1310:51380
Bis(2-chloroethoxy)methane ug/kg dry EPA 8270D380U111-91-1 5/15/1319:124/29/1310:51380
bis(2-Chloroethyl) Ether ug/kg dry EPA 8270D380U111-44-4 5/15/1319:124/29/1310:51380
Bis(2-chloroisopropyl) ether ug/kg dry EPA 8270D380U39638-32-9 5/15/1319:124/29/1310:51380
Bis(2-ethylhexyl) phthalate ug/kg dry EPA 8270D380U117-81-7 5/15/1319:124/29/1310:51380
Caprolactam ug/kg dry EPA 8270D380U105-60-2 5/15/1319:124/29/1310:51380
Carbazole ug/kg dry EPA 8270D3.9 U86-74-8 5/15/1319:124/29/1310:513.9
Chrysene ug/kg dry EPA 8270D35218-01-9 5/15/1319:124/29/1310:513.9
Dibenz(a,h)anthracene ug/kg dry EPA 8270D4.053-70-3 5/15/1319:124/29/1310:513.9
Dibenzofuran ug/kg dry EPA 8270D39U132-64-9 5/15/1319:124/29/1310:5139
Diethyl phthalate ug/kg dry EPA 8270D380U84-66-2 5/15/1319:124/29/1310:51380
Dimethyl phthalate ug/kg dry EPA 8270D380U131-11-3 5/15/1319:124/29/1310:51380
Di-n-butylphthalate ug/kg dry EPA 8270D380U84-74-2 5/15/1319:124/29/1310:51380
Di-n-octylphthalate ug/kg dry EPA 8270D380U117-84-0 5/15/1319:124/29/1310:51380
Fluoranthene ug/kg dry EPA 8270D24206-44-0 5/15/1319:124/29/1310:513.9
Fluorene ug/kg dry EPA 8270D3.9 U86-73-7 5/15/1319:124/29/1310:513.9
Hexachlorobenzene (HCB)ug/kg dry EPA 8270D3.9 U, J, QL-1118-74-1 5/15/1319:124/29/1310:513.9
Hexachlorocyclopentadiene (HCCP)ug/kg dry EPA 8270D380U77-47-4 5/15/1319:124/29/1310:51380
Hexachloroethane ug/kg dry EPA 8270D380U67-72-1 5/15/1319:124/29/1310:51380
Indeno (1,2,3-cd) pyrene ug/kg dry EPA 8270D14193-39-5 5/15/1319:124/29/1310:513.9
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 24 of 44 SESD Project ID # 13-0231 Durable Woods 26 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW06 E131702-07
Matrix:Surface Soil
Date Collected:4/23/13 15:20
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW06
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Isophorone ug/kg dry EPA 8270D380U78-59-1 5/15/1319:124/29/1310:51380
Naphthalene ug/kg dry EPA 8270D5.391-20-3 5/15/1319:124/29/1310:513.9
Nitrobenzene ug/kg dry EPA 8270D380U98-95-3 5/15/1319:124/29/1310:51380
n-Nitroso di-n-Propylamine ug/kg dry EPA 8270D380U621-64-7 5/15/1319:124/29/1310:51380
n-Nitrosodiphenylamine/Diphenylamine ug/kg dry EPA 8270D380U122-39-4 5/15/1319:124/29/1310:51380
Pentachlorophenol ug/kg dry EPA 8270D96087-86-5 5/15/1319:124/29/1310:517.7
Phenanthrene ug/kg dry EPA 8270D1285-01-8 5/15/1319:124/29/1310:513.9
Phenol ug/kg dry EPA 8270D380U108-95-2 5/15/1319:124/29/1310:51380
Pyrene ug/kg dry EPA 8270D30129-00-0 5/15/1319:124/29/1310:513.9
Tentatively Identified Compounds:
EPA 8270Dug/kg dry800Cinnamylcinnamate (TIC)NJR4-6505 5/15/1319:124/29/1310:51
EPA 8270Dug/kg dry500Decahydrotrimethylmethylenemethanoazu
lene (TIC)
NJR4-6506 5/15/1319:124/29/1310:51
EPA 8270Dug/kg dry400Hexadecenoic acid, methyl ester (TIC)NJR4-8000349 5/15/1319:124/29/1310:51
EPA 8270Dug/kg dry700Phenanthrenol (TIC)NJR4-8000496 5/15/1319:124/29/1310:51
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 25 of 44 SESD Project ID # 13-0231 Durable Woods 27 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW07 E131702-08
Matrix:Surface Soil
Date Collected:4/23/13 15:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW07
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
(3-and/or 4-)Methylphenol ug/kg dry EPA 8270D380U1319-77-3 5/15/1320:104/29/1310:51380
1,1-Biphenyl ug/kg dry EPA 8270D38U92-52-4 5/15/1320:104/29/1310:5138
1-Methylnaphthalene ug/kg dry EPA 8270D3.8 U90-12-0 5/15/1320:104/29/1310:513.8
2,3,4,6-Tetrachlorophenol ug/kg dry EPA 8270D50J, Q-258-90-2 5/15/1320:104/29/1310:51380
2,4,5-Trichlorophenol ug/kg dry EPA 8270D380U95-95-4 5/15/1320:104/29/1310:51380
2,4,6-Trichlorophenol ug/kg dry EPA 8270D380U88-06-2 5/15/1320:104/29/1310:51380
2,4-Dichlorophenol ug/kg dry EPA 8270D380U120-83-2 5/15/1320:104/29/1310:51380
2,4-Dimethylphenol ug/kg dry EPA 8270D380U105-67-9 5/15/1320:104/29/1310:51380
2,4-Dinitrophenol ug/kg dry EPA 8270D380U51-28-5 5/15/1320:104/29/1310:51380
2,4-Dinitrotoluene ug/kg dry EPA 8270D380U121-14-2 5/15/1320:104/29/1310:51380
2,6-Dinitrotoluene ug/kg dry EPA 8270D380U606-20-2 5/15/1320:104/29/1310:51380
2-Chloronaphthalene ug/kg dry EPA 8270D380U91-58-7 5/15/1320:104/29/1310:51380
2-Chlorophenol ug/kg dry EPA 8270D380U95-57-8 5/15/1320:104/29/1310:51380
2-Methyl-4,6-dinitrophenol ug/kg dry EPA 8270D380U534-52-1 5/15/1320:104/29/1310:51380
2-Methylnaphthalene ug/kg dry EPA 8270D3.8 U91-57-6 5/15/1320:104/29/1310:513.8
2-Methylphenol ug/kg dry EPA 8270D380U95-48-7 5/15/1320:104/29/1310:51380
2-Nitroaniline ug/kg dry EPA 8270D380U88-74-4 5/15/1320:104/29/1310:51380
2-Nitrophenol ug/kg dry EPA 8270D380U88-75-5 5/15/1320:104/29/1310:51380
3,3'-Dichlorobenzidine ug/kg dry EPA 8270D380U91-94-1 5/15/1320:104/29/1310:51380
3-Nitroaniline ug/kg dry EPA 8270D380U99-09-2 5/15/1320:104/29/1310:51380
4-Bromophenyl phenyl ether ug/kg dry EPA 8270D380U101-55-3 5/15/1320:104/29/1310:51380
4-Chloro-3-methylphenol ug/kg dry EPA 8270D380U59-50-7 5/15/1320:104/29/1310:51380
4-Chloroaniline ug/kg dry EPA 8270D380U106-47-8 5/15/1320:104/29/1310:51380
4-Chlorophenyl phenyl ether ug/kg dry EPA 8270D380U7005-72-3 5/15/1320:104/29/1310:51380
4-Nitroaniline ug/kg dry EPA 8270D380U100-01-6 5/15/1320:104/29/1310:51380
4-Nitrophenol ug/kg dry EPA 8270D380U100-02-7 5/15/1320:104/29/1310:51380
Acenaphthene ug/kg dry EPA 8270D3.8 U83-32-9 5/15/1320:104/29/1310:513.8
Acenaphthylene ug/kg dry EPA 8270D3.8 U208-96-8 5/15/1320:104/29/1310:513.8
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 26 of 44 SESD Project ID # 13-0231 Durable Woods 28 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW07 E131702-08
Matrix:Surface Soil
Date Collected:4/23/13 15:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW07
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Acetophenone ug/kg dry EPA 8270D380U98-86-2 5/15/1320:104/29/1310:51380
Anthracene ug/kg dry EPA 8270D3.8 U120-12-7 5/15/1320:104/29/1310:513.8
Atrazine ug/kg dry EPA 8270D380U1912-24-9 5/15/1320:104/29/1310:51380
Benzaldehyde ug/kg dry EPA 8270D380U100-52-7 5/15/1320:104/29/1310:51380
Benzo(a)anthracene ug/kg dry EPA 8270D5.756-55-3 5/15/1320:104/29/1310:513.8
Benzo(a)pyrene ug/kg dry EPA 8270D1150-32-8 5/15/1320:104/29/1310:513.8
Benzo(b)fluoranthene ug/kg dry EPA 8270D11205-99-2 5/15/1320:104/29/1310:513.8
Benzo(g,h,i)perylene ug/kg dry EPA 8270D7.3191-24-2 5/15/1320:104/29/1310:513.8
Benzo(k)fluoranthene ug/kg dry EPA 8270D8.1207-08-9 5/15/1320:104/29/1310:513.8
Benzyl butyl phthalate ug/kg dry EPA 8270D380U85-68-7 5/15/1320:104/29/1310:51380
Bis(2-chloroethoxy)methane ug/kg dry EPA 8270D380U111-91-1 5/15/1320:104/29/1310:51380
bis(2-Chloroethyl) Ether ug/kg dry EPA 8270D380U111-44-4 5/15/1320:104/29/1310:51380
Bis(2-chloroisopropyl) ether ug/kg dry EPA 8270D380U39638-32-9 5/15/1320:104/29/1310:51380
Bis(2-ethylhexyl) phthalate ug/kg dry EPA 8270D380U117-81-7 5/15/1320:104/29/1310:51380
Caprolactam ug/kg dry EPA 8270D380U105-60-2 5/15/1320:104/29/1310:51380
Carbazole ug/kg dry EPA 8270D3.8 U86-74-8 5/15/1320:104/29/1310:513.8
Chrysene ug/kg dry EPA 8270D13218-01-9 5/15/1320:104/29/1310:513.8
Dibenz(a,h)anthracene ug/kg dry EPA 8270D3.8 U53-70-3 5/15/1320:104/29/1310:513.8
Dibenzofuran ug/kg dry EPA 8270D38U132-64-9 5/15/1320:104/29/1310:5138
Diethyl phthalate ug/kg dry EPA 8270D380U84-66-2 5/15/1320:104/29/1310:51380
Dimethyl phthalate ug/kg dry EPA 8270D380U131-11-3 5/15/1320:104/29/1310:51380
Di-n-butylphthalate ug/kg dry EPA 8270D380U84-74-2 5/15/1320:104/29/1310:51380
Di-n-octylphthalate ug/kg dry EPA 8270D2600117-84-0 5/15/1320:104/29/1310:51380
Fluoranthene ug/kg dry EPA 8270D13206-44-0 5/15/1320:104/29/1310:513.8
Fluorene ug/kg dry EPA 8270D3.8 U86-73-7 5/15/1320:104/29/1310:513.8
Hexachlorobenzene (HCB)ug/kg dry EPA 8270D3.8 U, J, QL-1118-74-1 5/15/1320:104/29/1310:513.8
Hexachlorocyclopentadiene (HCCP)ug/kg dry EPA 8270D380U77-47-4 5/15/1320:104/29/1310:51380
Hexachloroethane ug/kg dry EPA 8270D380U67-72-1 5/15/1320:104/29/1310:51380
Indeno (1,2,3-cd) pyrene ug/kg dry EPA 8270D5.9193-39-5 5/15/1320:104/29/1310:513.8
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 27 of 44 SESD Project ID # 13-0231 Durable Woods 29 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW07 E131702-08
Matrix:Surface Soil
Date Collected:4/23/13 15:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW07
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Isophorone ug/kg dry EPA 8270D380U78-59-1 5/15/1320:104/29/1310:51380
Naphthalene ug/kg dry EPA 8270D3.8 U91-20-3 5/15/1320:104/29/1310:513.8
Nitrobenzene ug/kg dry EPA 8270D380U98-95-3 5/15/1320:104/29/1310:51380
n-Nitroso di-n-Propylamine ug/kg dry EPA 8270D380U621-64-7 5/15/1320:104/29/1310:51380
n-Nitrosodiphenylamine/Diphenylamine ug/kg dry EPA 8270D380U122-39-4 5/15/1320:104/29/1310:51380
Pentachlorophenol ug/kg dry EPA 8270D1200087-86-5 5/15/1319:414/29/1310:5177
Phenanthrene ug/kg dry EPA 8270D6.285-01-8 5/15/1320:104/29/1310:513.8
Phenol ug/kg dry EPA 8270D380U108-95-2 5/15/1320:104/29/1310:51380
Pyrene ug/kg dry EPA 8270D36129-00-0 5/15/1320:104/29/1310:513.8
Tentatively Identified Compounds:
EPA 8270Dug/kg dry5000Benzenedicarboxylic acid butylethylhexyl
ester (TI
NJ 5/15/1320:104/29/1310:51
EPA 8270Dug/kg dry600Benzenedicarboxylic acid diheptyl ester
(TIC)
NJR4-8001171 5/15/1320:104/29/1310:51
EPA 8270Dug/kg dry5000Benzenedicarboxylic acid isodecyloctyl
ester (TIC)
NJR4-8001172 5/15/1320:104/29/1310:51
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 28 of 44 SESD Project ID # 13-0231 Durable Woods 30 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW08 E131702-09
Matrix:Surface Soil
Date Collected:4/23/13 16:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW08
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
(3-and/or 4-)Methylphenol ug/kg dry EPA 8270D7300U1319-77-3 5/15/1322:074/29/1310:517300
1,1-Biphenyl ug/kg dry EPA 8270D730U92-52-4 5/15/1322:074/29/1310:51730
1-Methylnaphthalene ug/kg dry EPA 8270D73U90-12-0 5/15/1322:074/29/1310:5173
2,3,4,6-Tetrachlorophenol ug/kg dry EPA 8270D6400J, Q-258-90-2 5/15/1322:074/29/1310:517300
2,4,5-Trichlorophenol ug/kg dry EPA 8270D7300U95-95-4 5/15/1322:074/29/1310:517300
2,4,6-Trichlorophenol ug/kg dry EPA 8270D7300U88-06-2 5/15/1322:074/29/1310:517300
2,4-Dichlorophenol ug/kg dry EPA 8270D7300U120-83-2 5/15/1322:074/29/1310:517300
2,4-Dimethylphenol ug/kg dry EPA 8270D7300U105-67-9 5/15/1322:074/29/1310:517300
2,4-Dinitrophenol ug/kg dry EPA 8270D7300U51-28-5 5/15/1322:074/29/1310:517300
2,4-Dinitrotoluene ug/kg dry EPA 8270D7300U121-14-2 5/15/1322:074/29/1310:517300
2,6-Dinitrotoluene ug/kg dry EPA 8270D7300U606-20-2 5/15/1322:074/29/1310:517300
2-Chloronaphthalene ug/kg dry EPA 8270D7300U91-58-7 5/15/1322:074/29/1310:517300
2-Chlorophenol ug/kg dry EPA 8270D7300U95-57-8 5/15/1322:074/29/1310:517300
2-Methyl-4,6-dinitrophenol ug/kg dry EPA 8270D7300U534-52-1 5/15/1322:074/29/1310:517300
2-Methylnaphthalene ug/kg dry EPA 8270D12091-57-6 5/15/1322:074/29/1310:5173
2-Methylphenol ug/kg dry EPA 8270D7300U95-48-7 5/15/1322:074/29/1310:517300
2-Nitroaniline ug/kg dry EPA 8270D7300U88-74-4 5/15/1322:074/29/1310:517300
2-Nitrophenol ug/kg dry EPA 8270D7300U88-75-5 5/15/1322:074/29/1310:517300
3,3'-Dichlorobenzidine ug/kg dry EPA 8270D7300U91-94-1 5/15/1322:074/29/1310:517300
3-Nitroaniline ug/kg dry EPA 8270D7300U99-09-2 5/15/1322:074/29/1310:517300
4-Bromophenyl phenyl ether ug/kg dry EPA 8270D7300U101-55-3 5/15/1322:074/29/1310:517300
4-Chloro-3-methylphenol ug/kg dry EPA 8270D7300U59-50-7 5/15/1322:074/29/1310:517300
4-Chloroaniline ug/kg dry EPA 8270D7300U106-47-8 5/15/1322:074/29/1310:517300
4-Chlorophenyl phenyl ether ug/kg dry EPA 8270D7300U7005-72-3 5/15/1322:074/29/1310:517300
4-Nitroaniline ug/kg dry EPA 8270D7300U100-01-6 5/15/1322:074/29/1310:517300
4-Nitrophenol ug/kg dry EPA 8270D7300U100-02-7 5/15/1322:074/29/1310:517300
Acenaphthene ug/kg dry EPA 8270D73U83-32-9 5/15/1322:074/29/1310:5173
Acenaphthylene ug/kg dry EPA 8270D73U208-96-8 5/15/1322:074/29/1310:5173
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 29 of 44 SESD Project ID # 13-0231 Durable Woods 31 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW08 E131702-09
Matrix:Surface Soil
Date Collected:4/23/13 16:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW08
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Acetophenone ug/kg dry EPA 8270D7300U98-86-2 5/15/1322:074/29/1310:517300
Anthracene ug/kg dry EPA 8270D77120-12-7 5/15/1322:074/29/1310:5173
Atrazine ug/kg dry EPA 8270D7300U1912-24-9 5/15/1322:074/29/1310:517300
Benzaldehyde ug/kg dry EPA 8270D7300U100-52-7 5/15/1322:074/29/1310:517300
Benzo(a)anthracene ug/kg dry EPA 8270D73U56-55-3 5/15/1322:074/29/1310:5173
Benzo(a)pyrene ug/kg dry EPA 8270D21050-32-8 5/15/1322:074/29/1310:5173
Benzo(b)fluoranthene ug/kg dry EPA 8270D180205-99-2 5/15/1322:074/29/1310:5173
Benzo(g,h,i)perylene ug/kg dry EPA 8270D83191-24-2 5/15/1322:074/29/1310:5173
Benzo(k)fluoranthene ug/kg dry EPA 8270D140207-08-9 5/15/1322:074/29/1310:5173
Benzyl butyl phthalate ug/kg dry EPA 8270D7300U85-68-7 5/15/1322:074/29/1310:517300
Bis(2-chloroethoxy)methane ug/kg dry EPA 8270D7300U111-91-1 5/15/1322:074/29/1310:517300
bis(2-Chloroethyl) Ether ug/kg dry EPA 8270D7300U111-44-4 5/15/1322:074/29/1310:517300
Bis(2-chloroisopropyl) ether ug/kg dry EPA 8270D7300U39638-32-9 5/15/1322:074/29/1310:517300
Bis(2-ethylhexyl) phthalate ug/kg dry EPA 8270D3800J, Q-2117-81-7 5/15/1322:074/29/1310:517300
Caprolactam ug/kg dry EPA 8270D7300U105-60-2 5/15/1322:074/29/1310:517300
Carbazole ug/kg dry EPA 8270D54086-74-8 5/15/1322:074/29/1310:5173
Chrysene ug/kg dry EPA 8270D350218-01-9 5/15/1322:074/29/1310:5173
Dibenz(a,h)anthracene ug/kg dry EPA 8270D73U53-70-3 5/15/1322:074/29/1310:5173
Dibenzofuran ug/kg dry EPA 8270D730U132-64-9 5/15/1322:074/29/1310:51730
Diethyl phthalate ug/kg dry EPA 8270D7300U84-66-2 5/15/1322:074/29/1310:517300
Dimethyl phthalate ug/kg dry EPA 8270D7300U131-11-3 5/15/1322:074/29/1310:517300
Di-n-butylphthalate ug/kg dry EPA 8270D7300U84-74-2 5/15/1322:074/29/1310:517300
Di-n-octylphthalate ug/kg dry EPA 8270D1200J, Q-2117-84-0 5/15/1322:074/29/1310:517300
Fluoranthene ug/kg dry EPA 8270D330206-44-0 5/15/1322:074/29/1310:5173
Fluorene ug/kg dry EPA 8270D73U86-73-7 5/15/1322:074/29/1310:5173
Hexachlorobenzene (HCB)ug/kg dry EPA 8270D73U, J, QL-1118-74-1 5/15/1322:074/29/1310:5173
Hexachlorocyclopentadiene (HCCP)ug/kg dry EPA 8270D7300U77-47-4 5/15/1322:074/29/1310:517300
Hexachloroethane ug/kg dry EPA 8270D7300U67-72-1 5/15/1322:074/29/1310:517300
Indeno (1,2,3-cd) pyrene ug/kg dry EPA 8270D73U193-39-5 5/15/1322:074/29/1310:5173
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 30 of 44 SESD Project ID # 13-0231 Durable Woods 32 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Semi Volatile Organics
Sample ID:Lab ID: DW08 E131702-09
Matrix:Surface Soil
Date Collected:4/23/13 16:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW08
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Isophorone ug/kg dry EPA 8270D7300U78-59-1 5/15/1322:074/29/1310:517300
Naphthalene ug/kg dry EPA 8270D73U91-20-3 5/15/1322:074/29/1310:5173
Nitrobenzene ug/kg dry EPA 8270D7300U98-95-3 5/15/1322:074/29/1310:517300
n-Nitroso di-n-Propylamine ug/kg dry EPA 8270D7300U621-64-7 5/15/1322:074/29/1310:517300
n-Nitrosodiphenylamine/Diphenylamine ug/kg dry EPA 8270D7300U122-39-4 5/15/1322:074/29/1310:517300
Pentachlorophenol ug/kg dry EPA 8270D22000087-86-5 5/15/1316:464/29/1310:517300
Phenanthrene ug/kg dry EPA 8270D29085-01-8 5/15/1322:074/29/1310:5173
Phenol ug/kg dry EPA 8270D7300U108-95-2 5/15/1322:074/29/1310:517300
Pyrene ug/kg dry EPA 8270D2400129-00-0 5/15/1322:074/29/1310:5173
Tentatively Identified Compounds:
EPA 8270DPetroleum Product: NR4-6500 5/15/1322:0710:5110:51
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 31 of 44 SESD Project ID # 13-0231 Durable Woods 33 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304113 - E 3545A Modified
Blank (1304113-BLK1)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270D
bis(2-Chloroethyl) Ether ug/kg dryU330 U
Benzaldehyde "U 330 U
Hexachloroethane "U 330 U
Bis(2-chloroisopropyl) ether "U 330 U
n-Nitroso di-n-Propylamine "U 330 U
Acetophenone "U 330 U
Nitrobenzene "U 330 U
Caprolactam "U 330 U
1-Methylnaphthalene "U 3.3 U
2-Methylnaphthalene "U 3.3 U
Naphthalene "U 3.3 U
4-Chloroaniline "U 330 U
Bis(2-chloroethoxy)methane "U 330 U
Isophorone "U 330 U
Hexachlorocyclopentadiene (HCCP)"U 330 U
1,1-Biphenyl "U 33 U
2-Chloronaphthalene "U 330 U
2-Nitroaniline "U 330 U
Acenaphthylene "U 3.3 U
Acenaphthene "U 3.3 U
Dimethyl phthalate "U 330 U
Dibenzofuran "U 33 U
2,4-Dinitrotoluene "U 330 U
2,6-Dinitrotoluene "U 330 U
3-Nitroaniline "U 330 U
4-Chlorophenyl phenyl ether "U 330 U
4-Nitroaniline "U 330 U
Fluorene "U 3.3 U
Diethyl phthalate "U 330 U
n-Nitrosodiphenylamine/Diphenylamine "U 330 U
Hexachlorobenzene (HCB)"U 3.3 U
Atrazine "U 330 U
4-Bromophenyl phenyl ether "U 330 U
Phenanthrene "U 3.3 U
Anthracene "U 3.3 U
Carbazole "U 3.3 U
Di-n-butylphthalate "U 330 U
Fluoranthene "U 3.3 U
Pyrene "U 3.3 U
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 32 of 44 SESD Project ID # 13-0231 Durable Woods 34 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304113 - E 3545A Modified
Blank (1304113-BLK1)Prepared: 04/29/13 Analyzed: 05/14/13
Benzyl butyl phthalate ug/kg dryU330 U
Bis(2-ethylhexyl) phthalate "U 330 U
Benzo(a)anthracene "U 3.3 U
Chrysene "U 3.3 U
3,3'-Dichlorobenzidine "U 330 U
Di-n-octylphthalate "U 330 U
Benzo(b)fluoranthene "U 3.3 U
Benzo(k)fluoranthene "U 3.3 U
Benzo(a)pyrene "U 3.3 U
Indeno (1,2,3-cd) pyrene "U 3.3 U
Dibenz(a,h)anthracene "U 3.3 U
Benzo(g,h,i)perylene "U 3.3 U
2-Chlorophenol "U 330 U
2-Methylphenol "U 330 U
(3-and/or 4-)Methylphenol "U 330 U
2-Nitrophenol "U 330 U
Phenol "U 330 U
2,4-Dimethylphenol "U 330 U
2,4-Dichlorophenol "U 330 U
2,4,6-Trichlorophenol "U 330 U
2,4,5-Trichlorophenol "U 330 U
4-Chloro-3-methylphenol "U 330 U
2,4-Dinitrophenol "U 330 U
2-Methyl-4,6-dinitrophenol "U 330 U
Pentachlorophenol "U 6.6 U
4-Nitrophenol "U 330 U
2,3,4,6-Tetrachlorophenol "U 330 U
Tentatively Identified Compounds "U 300
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 33 of 44 SESD Project ID # 13-0231 Durable Woods 35 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304113 - E 3545A Modified
LCS (1304113-BS1)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270D
bis(2-Chloroethyl) Ether ug/kg dry1494.9 330 1996.7 51.5-99.274.9
Benzaldehyde "1624.2 330 1996.7 44.4-10181.3
Hexachloroethane "1374.8 330 1996.7 51.6-9468.9
Bis(2-chloroisopropyl) ether "1593.3 330 1996.7 44.2-10479.8
n-Nitroso di-n-Propylamine "1584.4 330 1996.7 52.8-93.279.4
Acetophenone "1482.4 330 1996.7 51.3-9874.2
Nitrobenzene "1550.6 330 1996.7 56.7-91.377.7
Caprolactam "1551.0 330 1996.7 64.8-10877.7
1-Methylnaphthalene "1344.2 3.3 1996.7 59.5-96.867.3
2-Methylnaphthalene "1477.5 3.3 1996.7 59.5-96.874.0
Naphthalene "1404.5 3.3 1996.7 57.7-99.770.3
4-Chloroaniline "1102.0 330 1996.7 22.4-76.555.2
Bis(2-chloroethoxy)methane "1575.9 330 1996.7 57.1-98.578.9
Isophorone "1616.0 330 1996.7 57.3-95.480.9
Hexachlorocyclopentadiene (HCCP)"1470.2 330 1996.7 37.9-76.473.6
1,1-Biphenyl "1410.1 33 1996.7 64.9-94.870.6
2-Chloronaphthalene "1460.8 330 1996.7 66.4-95.573.2
2-Nitroaniline "1756.4 330 1996.7 60.9-10688.0
Acenaphthylene "1618.2 3.3 1996.7 66.8-98.681.0
Acenaphthene "1557.6 3.3 1996.7 63-97.978.0
Dimethyl phthalate "1488.1 330 1996.7 69.2-96.474.5
Dibenzofuran "1518.0 33 1996.7 61.4-9576.0
2,4-Dinitrotoluene "1775.4 330 1996.7 63-10688.9
2,6-Dinitrotoluene "1774.2 330 1996.7 63.1-10688.9
3-Nitroaniline "1647.6 330 1996.7 42.2-90.882.5
4-Chlorophenyl phenyl ether "1601.2 330 1996.7 66-10280.2
4-Nitroaniline "2050.9 330 1996.7 57.5-118103
Fluorene "1693.2 3.3 1996.7 65.6-10384.8
Diethyl phthalate "1500.8 330 1996.7 60.5-10675.2
n-Nitrosodiphenylamine/Diphenylamine "1640.9 330 1996.7 55.6-11082.2
Hexachlorobenzene (HCB)"1050.8 3.3 1996.7 QL-153.5-12352.6
Atrazine "1630.2 330 1996.7 35.6-15681.6
4-Bromophenyl phenyl ether "1697.5 330 1996.7 52.8-12685.0
Phenanthrene "1609.8 3.3 1996.7 56.5-11980.6
Anthracene "1685.3 3.3 1996.7 57.4-11684.4
Carbazole "1788.0 3.3 1996.7 69-11889.5
Di-n-butylphthalate "1591.5 330 1996.7 60.6-12279.7
Fluoranthene "1671.4 3.3 1996.7 59.4-11983.7
Pyrene "1688.1 3.3 1996.7 59.6-11384.5
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 34 of 44 SESD Project ID # 13-0231 Durable Woods 36 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304113 - E 3545A Modified
LCS (1304113-BS1)Prepared: 04/29/13 Analyzed: 05/14/13
Benzyl butyl phthalate ug/kg dry1641.5 330 1996.7 71.3-10982.2
Bis(2-ethylhexyl) phthalate "1673.2 330 1996.7 64.9-11283.8
Benzo(a)anthracene "1594.9 3.3 1996.7 63.9-11179.9
Chrysene "1566.9 3.3 1996.7 62.1-10978.5
3,3'-Dichlorobenzidine "1700.0 330 1996.7 28.8-87.185.1
Di-n-octylphthalate "1650.7 330 1996.7 47.6-12182.7
Benzo(b)fluoranthene "1706.7 3.3 1996.7 51.3-11085.5
Benzo(k)fluoranthene "1754.8 3.3 1996.7 57.5-10487.9
Benzo(a)pyrene "1851.7 3.3 1996.7 50-10292.7
Indeno (1,2,3-cd) pyrene "1697.3 3.3 1996.7 37.5-11885.0
Dibenz(a,h)anthracene "1664.7 3.3 1996.7 20-15383.4
Benzo(g,h,i)perylene "1598.7 3.3 1996.7 10-11180.1
2-Chlorophenol "1311.3 330 1996.7 55.1-95.865.7
2-Methylphenol "1286.6 330 1996.7 44.3-96.364.4
(3-and/or 4-)Methylphenol "1354.9 330 1996.7 45.2-10267.9
2-Nitrophenol "1346.2 330 1996.7 60.7-94.667.4
Phenol "1272.1 330 1996.7 54.3-98.563.7
2,4-Dimethylphenol "916.37 330 1996.7 24.5-75.845.9
2,4-Dichlorophenol "1338.7 330 1996.7 64-96.567.0
2,4,6-Trichlorophenol "1401.4 330 1996.7 66-10370.2
2,4,5-Trichlorophenol "1511.6 330 1996.7 59.3-11075.7
4-Chloro-3-methylphenol "1392.9 330 1996.7 66.8-10069.8
2,4-Dinitrophenol "1413.8 330 2995.0 12.4-63.847.2
2-Methyl-4,6-dinitrophenol "1447.1 330 1996.7 44-11472.5
Pentachlorophenol "1524.1 6.6 1996.7 57-11576.3
4-Nitrophenol "1633.1 330 1996.7 56.3-11881.8
2,3,4,6-Tetrachlorophenol "2144.2 330 1996.7 68.4-109107
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 35 of 44 SESD Project ID # 13-0231 Durable Woods 37 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304113 - E 3545A Modified
MRL Verification (1304113-PS1)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270D
bis(2-Chloroethyl) Ether ug/kg dry242.46 330 332.23 MRL-3,
Q-2, J
31.5-11973.0
Benzaldehyde "284.09 330 332.23 MRL-3,
Q-2, J
24.4-12185.5
Hexachloroethane "224.35 330 332.23 MRL-3,
Q-2, J
31.6-11467.5
Bis(2-chloroisopropyl) ether "259.63 330 332.23 MRL-3,
Q-2, J
24.2-12478.2
n-Nitroso di-n-Propylamine "244.88 330 332.23 MRL-3,
Q-2, J
32.8-11373.7
Acetophenone "239.97 330 332.23 MRL-3,
Q-2, J
31.3-11872.2
Nitrobenzene "262.16 330 332.23 MRL-3,
Q-2, J
36.7-11178.9
Caprolactam "251.00 330 332.23 MRL-3,
Q-2, J
44.8-12875.6
1-Methylnaphthalene "22.458 3.3 33.223 MRL-339.5-11767.6
2-Methylnaphthalene "25.116 3.3 33.223 MRL-339.5-11775.6
Naphthalene "25.282 3.3 33.223 MRL-337.7-12076.1
4-Chloroaniline "82.525 330 332.23 MRL-3,
Q-2, J
10-96.524.8
Bis(2-chloroethoxy)methane "267.64 330 332.23 MRL-3,
Q-2, J
37.1-11880.6
Isophorone "266.28 330 332.23 MRL-3,
Q-2, J
37.3-11580.2
Hexachlorocyclopentadiene (HCCP)"227.94 330 332.23 MRL-3,
Q-2, J
17.9-96.468.6
1,1-Biphenyl "25.748 33 33.223 MRL-3,
Q-2, J
44.9-11577.5
2-Chloronaphthalene "253.09 330 332.23 MRL-3,
Q-2, J
46.4-11676.2
2-Nitroaniline "288.17 330 332.23 MRL-3,
Q-2, J
40.9-12686.7
Acenaphthylene "27.176 3.3 33.223 MRL-346.8-11981.8
Acenaphthene "26.578 3.3 33.223 MRL-343-11880.0
Dimethyl phthalate "244.92 330 332.23 MRL-3,
Q-2, J
49.2-11673.7
Dibenzofuran "26.379 33 33.223 MRL-3,
Q-2, J
41.4-11579.4
2,4-Dinitrotoluene "277.91 330 332.23 MRL-3,
Q-2, J
43-12683.7
2,6-Dinitrotoluene "283.65 330 332.23 MRL-3,
Q-2, J
43.1-12685.4
3-Nitroaniline "235.32 330 332.23 MRL-3,
Q-2, J
22.2-11170.8
4-Chlorophenyl phenyl ether "282.19 330 332.23 MRL-3,
Q-2, J
46-12284.9
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 36 of 44 SESD Project ID # 13-0231 Durable Woods 38 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304113 - E 3545A Modified
MRL Verification (1304113-PS1)Prepared: 04/29/13 Analyzed: 05/14/13
4-Nitroaniline ug/kg dry282.92 330 332.23 MRL-3,
Q-2, J
37.5-13885.2
Fluorene "28.339 3.3 33.223 MRL-345.6-12385.3
Diethyl phthalate "250.07 330 332.23 MRL-3,
Q-2, J
40.5-12675.3
n-Nitrosodiphenylamine/Diphenylamine "256.84 330 332.23 MRL-3,
Q-2, J
35.6-13077.3
Hexachlorobenzene (HCB)"181.93 3.3 332.23 MRL-333.5-14354.8
Atrazine "270.47 330 332.23 MRL-3,
Q-2, J
15.6-17681.4
4-Bromophenyl phenyl ether "289.60 330 332.23 MRL-3,
Q-2, J
32.8-14687.2
Phenanthrene "28.837 3.3 33.223 MRL-336.5-13986.8
Anthracene "28.173 3.3 33.223 MRL-337.4-13684.8
Carbazole "28.837 3.3 33.223 MRL-349-13886.8
Di-n-butylphthalate "274.88 330 332.23 MRL-3,
Q-2, J
40.6-14282.7
Fluoranthene "28.007 3.3 33.223 MRL-339.4-13984.3
Pyrene "29.834 3.3 33.223 MRL-339.6-13389.8
Benzyl butyl phthalate "285.95 330 332.23 MRL-3,
Q-2, J
51.3-12986.1
Bis(2-ethylhexyl) phthalate "272.36 330 332.23 MRL-3,
Q-2, J
44.9-13282.0
Benzo(a)anthracene "28.638 3.3 33.223 MRL-343.9-13186.2
Chrysene "27.608 3.3 33.223 MRL-342.1-12983.1
3,3'-Dichlorobenzidine "212.09 330 332.23 MRL-3,
Q-2, J
10-10763.8
Di-n-octylphthalate "259.14 330 332.23 MRL-3,
Q-2, J
27.6-14178.0
Benzo(b)fluoranthene "27.110 3.3 33.223 MRL-331.3-13081.6
Benzo(k)fluoranthene "30.698 3.3 33.223 MRL-337.5-12492.4
Benzo(a)pyrene "27.674 3.3 33.223 MRL-330-12283.3
Indeno (1,2,3-cd) pyrene "25.083 3.3 33.223 MRL-317.5-13875.5
Dibenz(a,h)anthracene "25.947 3.3 33.223 MRL-310-17378.1
Benzo(g,h,i)perylene "23.920 3.3 33.223 MRL-310-13172.0
2-Chlorophenol "199.47 330 332.23 MRL-3,
Q-2, J
35.1-11660.0
2-Methylphenol "173.99 330 332.23 MRL-3,
Q-2, J
24.3-11652.4
(3-and/or 4-)Methylphenol "184.55 330 332.23 MRL-3,
Q-2, J
25.2-12255.6
2-Nitrophenol "202.29 330 332.23 MRL-3,
Q-2, J
40.7-11560.9
Phenol "199.80 330 332.23 MRL-3,
Q-2, J
34.3-11860.1
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 37 of 44 SESD Project ID # 13-0231 Durable Woods 39 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304113 - E 3545A Modified
MRL Verification (1304113-PS1)Prepared: 04/29/13 Analyzed: 05/14/13
2,4-Dimethylphenol ug/kg dry43.256 330 332.23 MRL-3,
Q-2, J
10-9613.0
2,4-Dichlorophenol "204.45 330 332.23 MRL-3,
Q-2, J
44-11661.5
2,4,6-Trichlorophenol "201.00 330 332.23 MRL-3,
Q-2, J
46-12360.5
2,4,5-Trichlorophenol "223.06 330 332.23 MRL-3,
Q-2, J
39.3-13067.1
4-Chloro-3-methylphenol "201.20 330 332.23 MRL-3,
Q-2, J
46.8-12060.6
2,4-Dinitrophenol "153.52 330 664.45 MRL-3,
Q-2, J
10-83.823.1
2-Methyl-4,6-dinitrophenol "144.88 330 332.23 MRL-3,
Q-2, J
24-13443.6
Pentachlorophenol "190.73 6.6 332.23 MRL-337-13557.4
4-Nitrophenol "214.52 330 332.23 MRL-3,
Q-2, J
36.3-13864.6
2,3,4,6-Tetrachlorophenol "270.47 330 332.23 MRL-3,
Q-2, J
48.4-12981.4
Batch 1304114 - E 3545A Modified
Blank (1304114-BLK1)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270 SIM
ug/kg dry 33.234 24-132Surrogate: 2-Methylnaphthalene-d10 65.021.6
" 33.234 27-130Surrogate: Fluoranthene-d10 75.024.9
1-Methylnaphthalene "U 3.3 U
2-Methylnaphthalene "U 3.3 U
Naphthalene "U 3.3 U
Acenaphthylene "U 3.3 U
Acenaphthene "U 3.3 U
Fluorene "U 3.3 U
Phenanthrene "U 3.3 U
Anthracene "U 3.3 U
Carbazole "U 3.3 U
Fluoranthene "U 3.3 U
Pyrene "U 3.3 U
Benzo(a)anthracene "U 3.3 U
Chrysene "U 3.3 U
Benzo(b)fluoranthene "U 3.3 U
Benzo(k)fluoranthene "U 3.3 U
Benzo(a)pyrene "U 3.3 U
Indeno (1,2,3-cd) pyrene "U 3.3 U
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 38 of 44 SESD Project ID # 13-0231 Durable Woods 40 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304114 - E 3545A Modified
Blank (1304114-BLK1)Prepared: 04/29/13 Analyzed: 05/14/13
Dibenz(a,h)anthracene ug/kg dryU3.3 U
Benzo(g,h,i)perylene "U 3.3 U
Pentachlorophenol "U 6.7 U
LCS (1304114-BS1)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270 SIM
ug/kg dry 33.289 24-132Surrogate: 2-Methylnaphthalene-d10 75.025.0
" 33.289 27-130Surrogate: Fluoranthene-d10 85.028.3
1-Methylnaphthalene "22.537 3.3 33.289 50-15067.7
2-Methylnaphthalene "23.302 3.3 33.289 23-12670.0
Naphthalene "27.330 3.3 33.289 10-15082.1
Acenaphthylene "25.932 3.3 33.289 15-14277.9
Acenaphthene "26.798 3.3 33.289 25-12680.5
Fluorene "28.961 3.3 33.289 28-13887.0
Phenanthrene "30.093 3.3 33.289 22-13690.4
Anthracene "25.067 3.3 33.289 10-13675.3
Carbazole "26.099 3.3 33.289 20-16278.4
Fluoranthene "30.326 3.3 33.289 43-13391.1
Pyrene "32.557 3.3 33.289 40-11797.8
Benzo(a)anthracene "29.927 3.3 33.289 48-14389.9
Chrysene "29.095 3.3 33.289 46-11187.4
Benzo(b)fluoranthene "29.161 3.3 33.289 40-14287.6
Benzo(k)fluoranthene "31.158 3.3 33.289 42-13593.6
Benzo(a)pyrene "19.574 3.3 33.289 10-15358.8
Indeno (1,2,3-cd) pyrene "26.664 3.3 33.289 42-13580.1
Dibenz(a,h)anthracene "26.931 3.3 33.289 41-13880.9
Benzo(g,h,i)perylene "24.800 3.3 33.289 10-13074.5
Pentachlorophenol "39.481 6.7 66.578 10-15559.3
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 39 of 44 SESD Project ID # 13-0231 Durable Woods 41 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304114 - E 3545A Modified
LCS (1304114-BS2)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270 SIM
ug/kg dry 33.300 24-132Surrogate: 2-Methylnaphthalene-d10 77.025.6
" 33.300 27-130Surrogate: Fluoranthene-d10 85.028.3
1-Methylnaphthalene "23.144 3.3 33.300 50-15069.5
2-Methylnaphthalene "23.776 3.3 33.300 23-12671.4
Naphthalene "28.005 3.3 33.300 10-15084.1
Acenaphthylene "25.574 3.3 33.300 15-14276.8
Acenaphthene "27.106 3.3 33.300 25-12681.4
Fluorene "28.139 3.3 33.300 28-13884.5
Phenanthrene "28.938 3.3 33.300 22-13686.9
Anthracene "24.242 3.3 33.300 10-13672.8
Carbazole "25.241 3.3 33.300 20-16275.8
Fluoranthene "29.404 3.3 33.300 43-13388.3
Pyrene "31.635 3.3 33.300 40-11795.0
Benzo(a)anthracene "28.205 3.3 33.300 48-14384.7
Chrysene "26.374 3.3 33.300 46-11179.2
Benzo(b)fluoranthene "28.638 3.3 33.300 40-14286.0
Benzo(k)fluoranthene "31.469 3.3 33.300 42-13594.5
Benzo(a)pyrene "19.980 3.3 33.300 10-15360.0
Indeno (1,2,3-cd) pyrene "25.641 3.3 33.300 42-13577.0
Dibenz(a,h)anthracene "25.508 3.3 33.300 41-13876.6
Benzo(g,h,i)perylene "24.242 3.3 33.300 10-13072.8
Pentachlorophenol "30.003 6.7 66.600 10-15545.0
LCS (1304114-BS3)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270 SIM
ug/kg dry 33.278 24-132Surrogate: 2-Methylnaphthalene-d10 80.026.6
" 33.278 27-130Surrogate: Fluoranthene-d10 85.028.3
1-Methylnaphthalene "24.326 3.3 33.278 50-15073.1
2-Methylnaphthalene "24.958 3.3 33.278 23-12675.0
Naphthalene "29.917 3.3 33.278 10-15089.9
Acenaphthylene "27.022 3.3 33.278 15-14281.2
Acenaphthene "28.020 3.3 33.278 25-12684.2
Fluorene "30.116 3.3 33.278 28-13890.5
Phenanthrene "30.050 3.3 33.278 22-13690.3
Anthracene "25.324 3.3 33.278 10-13676.1
Carbazole "25.824 3.3 33.278 20-16277.6
Fluoranthene "30.316 3.3 33.278 43-13391.1
Pyrene "32.679 3.3 33.278 40-11798.2
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 40 of 44 SESD Project ID # 13-0231 Durable Woods 42 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304114 - E 3545A Modified
LCS (1304114-BS3)Prepared: 04/29/13 Analyzed: 05/14/13
Benzo(a)anthracene ug/kg dry30.250 3.3 33.278 48-14390.9
Chrysene "29.052 3.3 33.278 46-11187.3
Benzo(b)fluoranthene "27.687 3.3 33.278 40-14283.2
Benzo(k)fluoranthene "32.113 3.3 33.278 42-13596.5
Benzo(a)pyrene "20.865 3.3 33.278 10-15362.7
Indeno (1,2,3-cd) pyrene "27.887 3.3 33.278 42-13583.8
Dibenz(a,h)anthracene "27.920 3.3 33.278 41-13883.9
Benzo(g,h,i)perylene "26.090 3.3 33.278 10-13078.4
Pentachlorophenol "32.280 6.7 66.556 10-15548.5
LCS (1304114-BS4)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270 SIM
ug/kg dry 33.256 24-132Surrogate: 2-Methylnaphthalene-d10 77.025.6
" 33.256 27-130Surrogate: Fluoranthene-d10 85.028.3
1-Methylnaphthalene "23.545 3.3 33.256 50-15070.8
2-Methylnaphthalene "24.909 3.3 33.256 23-12674.9
Naphthalene "29.066 3.3 33.256 10-15087.4
Acenaphthylene "26.970 3.3 33.256 15-14281.1
Acenaphthene "27.004 3.3 33.256 25-12681.2
Fluorene "29.332 3.3 33.256 28-13888.2
Phenanthrene "29.864 3.3 33.256 22-13689.8
Anthracene "23.811 3.3 33.256 10-13671.6
Carbazole "25.840 3.3 33.256 20-16277.7
Fluoranthene "29.332 3.3 33.256 43-13388.2
Pyrene "33.987 3.3 33.256 40-117102
Benzo(a)anthracene "29.697 3.3 33.256 48-14389.3
Chrysene "28.533 3.3 33.256 46-11185.8
Benzo(b)fluoranthene "28.234 3.3 33.256 40-14284.9
Benzo(k)fluoranthene "30.928 3.3 33.256 42-13593.0
Benzo(a)pyrene "22.148 3.3 33.256 10-15366.6
Indeno (1,2,3-cd) pyrene "26.472 3.3 33.256 42-13579.6
Dibenz(a,h)anthracene "27.536 3.3 33.256 41-13882.8
Benzo(g,h,i)perylene "25.341 3.3 33.256 10-13076.2
Pentachlorophenol "30.695 6.7 66.511 10-15546.2
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 41 of 44 SESD Project ID # 13-0231 Durable Woods 43 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304114 - E 3545A Modified
LCS (1304114-BS5)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270 SIM
ug/kg dry 33.267 24-132Surrogate: 2-Methylnaphthalene-d10 82.027.3
" 33.267 27-130Surrogate: Fluoranthene-d10 87.028.9
1-Methylnaphthalene "24.518 3.3 33.267 50-15073.7
2-Methylnaphthalene "25.083 3.3 33.267 23-12675.4
Naphthalene "29.741 3.3 33.267 10-15089.4
Acenaphthylene "26.680 3.3 33.267 15-14280.2
Acenaphthene "28.576 3.3 33.267 25-12685.9
Fluorene "30.073 3.3 33.267 28-13890.4
Phenanthrene "30.073 3.3 33.267 22-13690.4
Anthracene "24.884 3.3 33.267 10-13674.8
Carbazole "26.314 3.3 33.267 20-16279.1
Fluoranthene "30.539 3.3 33.267 43-13391.8
Pyrene "32.868 3.3 33.267 40-11798.8
Benzo(a)anthracene "29.308 3.3 33.267 48-14388.1
Chrysene "28.443 3.3 33.267 46-11185.5
Benzo(b)fluoranthene "29.341 3.3 33.267 40-14288.2
Benzo(k)fluoranthene "33.134 3.3 33.267 42-13599.6
Benzo(a)pyrene "17.898 3.3 33.267 10-15353.8
Indeno (1,2,3-cd) pyrene "27.312 3.3 33.267 42-13582.1
Dibenz(a,h)anthracene "27.911 3.3 33.267 41-13883.9
Benzo(g,h,i)perylene "26.647 3.3 33.267 10-13080.1
Pentachlorophenol "31.670 6.7 66.534 10-15547.6
MRL Verification (1304114-PS1)Prepared: 04/29/13 Analyzed: 05/14/13
EPA 8270 SIM
ug/kg dry 33.278 24-132Surrogate: 2-Methylnaphthalene-d10 77.025.6
" 33.278 27-130Surrogate: Fluoranthene-d10 83.027.6
1-Methylnaphthalene "2.0965 3.3 3.3278 MRL-3,
Q-2, J
30-17063.0
2-Methylnaphthalene "2.1298 3.3 3.3278 MRL-3,
Q-2, J
10-14664.0
Naphthalene "2.7621 3.3 3.3278 MRL-3,
Q-2, J
10-17083.0
Acenaphthylene "2.0965 3.3 3.3278 MRL-3,
Q-2, J
10-16263.0
Acenaphthene "2.3295 3.3 3.3278 MRL-3,
Q-2, J
10-14670.0
Fluorene "2.5957 3.3 3.3278 MRL-3,
Q-2, J
10-15878.0
Phenanthrene "2.8286 3.3 3.3278 MRL-3,
Q-2, J
10-15685.0
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 42 of 44 SESD Project ID # 13-0231 Durable Woods 44 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semi Volatile Organics (SVOA) - Quality Control
US-EPA, Region 4, SESD
Batch 1304114 - E 3545A Modified
MRL Verification (1304114-PS1)Prepared: 04/29/13 Analyzed: 05/14/13
Anthracene ug/kg dry1.8303 3.3 3.3278 MRL-3,
Q-2, J
10-15655.0
Carbazole "2.2296 3.3 3.3278 MRL-3,
Q-2, J
10-18267.0
Fluoranthene "2.6290 3.3 3.3278 MRL-3,
Q-2, J
23-15379.0
Pyrene "2.7621 3.3 3.3278 MRL-3,
Q-2, J
20-13783.0
Benzo(a)anthracene "3.8602 3.3 3.3278 MRL-328-163116
Chrysene "2.5957 3.3 3.3278 MRL-3,
Q-2, J
26-13178.0
Benzo(b)fluoranthene "2.7953 3.3 3.3278 MRL-3,
Q-2, J
20-16284.0
Benzo(k)fluoranthene "2.8286 3.3 3.3278 MRL-3,
Q-2, J
22-15585.0
Benzo(a)pyrene "1.7637 3.3 3.3278 MRL-3,
Q-2, J
10-17353.0
Indeno (1,2,3-cd) pyrene "2.4958 3.3 3.3278 MRL-3,
Q-2, J
22-15575.0
Dibenz(a,h)anthracene "2.5291 3.3 3.3278 MRL-3,
Q-2, J
21-15876.0
Benzo(g,h,i)perylene "2.4293 3.3 3.3278 MRL-3,
Q-2, J
10-15073.0
Pentachlorophenol "7.9534 6.7 6.6556 MRL-310-175120
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 43 of 44 SESD Project ID # 13-0231 Durable Woods 45 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Diana Burdette
Notes and Definitions for QC Samples
U The analyte was not detected at or above the reporting limit.
J The identification of the analyte is acceptable; the reported value is an estimate.
MRL-3 MRL verification for Soil matrix
Q-2 Result greater than MDL but less than MRL.
QL-1 Laboratory Control Spike Recovery less than method control limits
6/3/13 9:30E131702 SVOA FINAL 06 03 13 0930Page 44 of 44 SESD Project ID # 13-0231 Durable Woods 46 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
June 5, 2013
MEMORANDUM
SUBJECT:
FROM:
FINAL Analytical Report
Project: 13-0231, Durable Wood Preservers, Inc.
Resource Conservation and Recovery Act
4SESD-ASB
Roberta Howes
ICS Chemist
ASB Inorganic Chemistry Section
Mike Wasko, ChiefTHRU:
TO:Mike Neill
Attached are the final results for the analytical groups listed below. These analyses were performed in
accordance with the Analytical Support Branch's (ASB) Laboratory Operations and Quality Assurance Manual
(ASB LOQAM) found at www.epa.gov/region4/sesd/asbsop. Any unique project data quality objectives
specified in writing by the data requestor have also been incorporated into the data unless otherwise noted in the
Report Narrative. Chemistry data have been verified based on the ASB LOQAM specifications and have been
qualified by this laboratory if the applicable quality control criteria were not met. Verification is defined in
Section 5.2 of the ASB LOQAM. For a listing of specific data qualifiers and explanations, please refer to the
Data Qualifier Definitions included in this report. The reported results are accurate within the limits of the
method(s) and are representative only of the samples as received by the laboratory.
Analyses Included in this report:Method Used:Accreditations:
Physical Properties (PHYSP)
Physical Properties NoneEPA 200.2 (Soil)
Total Metals (TMTL)
Speciated Metals ISOSM 3500 Cr (Soil)
Total Metals ISOEPA 200.8 (Soil)
Total Metals ISOEPA 6010 (Soil)
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 1 of 32 SESD Project ID # 13-0231 Durable Woods 47 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Sample Disposal Policy
Because of the laboratory's limited space for long term sample storage, our policy is to dispose of samples on a
periodic schedule. Please note that within 60 days of this memo, the original samples and all sample extracts
and/or sample digestates will be disposed of in accordance with applicable regulations. The 60-day sample
disposal policy does not apply to criminal samples which are held until the laboratory is notified by the criminal
investigators that case development and litigation are complete.
These samples may be held in the laboratory's custody for a longer period of time if you have a special project
need. If you wish for the laboratory to hold samples beyond the 60-day period, please contact our Sample Control
Coordinator by e-mail at [e-mail], and provide a reason for holding samples beyond 60 days
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 2 of 32 SESD Project ID # 13-0231 Durable Woods 48 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Date ReceivedDate CollectedMatrixLaboratory IDSample ID
SAMPLES INCLUDED IN THIS REPORT
Project: 13-0231, Durable Wood Preservers, Inc.
Control E131702-01 Surface Soil 4/23/13 13:15 4/24/13 11:25
DW01 E131702-02 Surface Soil 4/23/13 13:40 4/24/13 11:25
DW02 E131702-03 Surface Soil 4/23/13 14:00 4/24/13 11:25
DW03 E131702-04 Surface Soil 4/23/13 14:15 4/24/13 11:25
DW04 E131702-05 Surface Soil 4/23/13 14:45 4/24/13 11:25
DW05 E131702-06 Surface Soil 4/23/13 15:10 4/24/13 11:25
DW06 E131702-07 Surface Soil 4/23/13 15:20 4/24/13 11:25
DW07 E131702-08 Surface Soil 4/23/13 15:40 4/24/13 11:25
DW08 E131702-09 Surface Soil 4/23/13 16:00 4/24/13 11:25
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 3 of 32 SESD Project ID # 13-0231 Durable Woods 49 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
DATA QUALIFIER DEFINITIONS
U The analyte was not detected at or above the reporting limit.
J The identification of the analyte is acceptable; the reported value is an estimate.
QM-1 Matrix Spike Recovery less than method control limits
QM-2 Matrix Spike Recovery greater than method control limits
QM-3 Matrix Spike Precision outside method control limits
X-CH6 Sample is reducing in nature. Should not support hexavalent chromium
ACRONYMS AND ABBREVIATIONS
CAS Chemical Abstracts Service
Note: Analytes with no known CAS identifiers have been assigned codes beginning with "E", the EPA ID as assigned by
the EPA Substance Registry System (www.epa.gov/srs), or beginning with "R4-", a unique identifier assigned by the EPA
Region 4 laboratory.
ISO The test, if analyzed after June 26, 2012, is accredited under the EPA Region 4 ASB's ISO/IEC 17025 accreditation
issued by ANSI-ASQ National Accreditation Board/ACLASS. Refer to certificate and scope of accreditation
AT-1691.
MDL Method Detection Limit - The minimum concentration of a substance (an analyte) that can be measured and
reported with a 99% confidence that the analyte concentration is greater than zero.
MRL Minimum Reporting Limit - Analyte concentration that corresponds to the lowest demonstrated level of acceptable
quantitation. The MRL is sample-specific and accounts for preparation weights and volumes, dilutions, and
moisture content of soil/sediments.
TIC Tentatively Identified Compound - An analyte identified based on a match with the instrument software's mass
spectral library. A calibration standard has not been analyzed to confirm the compound's identification or the
estimated concentration reported.
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 4 of 32 SESD Project ID # 13-0231 Durable Woods 50 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: Control E131702-01
Matrix:Surface Soil
Date Collected:4/23/13 13:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:CONTROL
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Chromium, Hexavalent mg/kg dry SM 3500 Cr5.7 U18540-29-9 5/22/1321:465/20/1318:075.7
Aluminum mg/kg dry EPA 601060007429-90-5 5/06/1318:065/03/1312:589.8
Antimony mg/kg dry EPA 200.80.25 U7440-36-0 5/20/1318:455/03/1313:010.25
Arsenic mg/kg dry EPA 200.80.307440-38-2 5/20/1318:455/03/1313:010.25
Barium mg/kg dry EPA 6010347440-39-3 5/06/1318:065/03/1312:580.49
Beryllium mg/kg dry EPA 60100.30 U7440-41-7 5/06/1318:065/03/1312:580.30
Cadmium mg/kg dry EPA 200.80.12 U7440-43-9 5/20/1318:455/03/1313:010.12
Calcium mg/kg dry EPA 60101807440-70-2 5/06/1318:065/03/1312:5825
Chromium mg/kg dry EPA 6010137440-47-3 5/06/1318:065/03/1312:580.49
Cobalt mg/kg dry EPA 60101.67440-48-4 5/06/1318:065/03/1312:580.49
Copper mg/kg dry EPA 6010307440-50-8 5/06/1318:065/03/1312:580.98
Iron mg/kg dry EPA 6010130007439-89-6 5/06/1318:065/03/1312:589.8
Lead mg/kg dry EPA 200.85.37439-92-1 5/20/1318:455/03/1313:010.25
Magnesium mg/kg dry EPA 60102107439-95-4 5/06/1318:065/03/1312:5825
Manganese mg/kg dry EPA 6010827439-96-5 5/06/1318:065/03/1312:580.49
Molybdenum mg/kg dry EPA 60100.98 U7439-98-7 5/06/1318:065/03/1312:580.98
Nickel mg/kg dry EPA 60102.27440-02-0 5/06/1318:065/03/1312:580.98
Potassium mg/kg dry EPA 60102407440-09-7 5/06/1318:065/03/1312:5898
Selenium mg/kg dry EPA 200.80.49 U7782-49-2 5/20/1318:455/03/1313:010.49
Silver mg/kg dry EPA 60100.49 U7440-22-4 5/06/1318:065/03/1312:580.49
Sodium mg/kg dry EPA 601098U7440-23-5 5/06/1318:065/03/1312:5898
Strontium mg/kg dry EPA 60102.37440-24-6 5/06/1318:065/03/1312:580.49
Thallium mg/kg dry EPA 200.80.25 U7440-28-0 5/20/1318:455/03/1313:010.25
Tin mg/kg dry EPA 60101.5 U7440-31-5 5/06/1318:065/03/1312:581.5
Titanium mg/kg dry EPA 6010447440-32-6 5/06/1318:065/03/1312:580.49
Vanadium mg/kg dry EPA 6010357440-62-2 5/06/1318:065/03/1312:580.49
Yttrium mg/kg dry EPA 60103.87440-65-5 5/06/1318:065/03/1312:580.30
Zinc mg/kg dry EPA 6010267440-66-6 5/06/1318:065/03/1312:580.98
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 5 of 32 SESD Project ID # 13-0231 Durable Woods 51 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Physical Properties
Sample ID:Lab ID: Control E131702-01
Matrix:Surface Soil
Date Collected:4/23/13 13:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:CONTROL
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
% Solids %EPA 200.286E16429415/02/1313:305/01/1315:570.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 6 of 32 SESD Project ID # 13-0231 Durable Woods 52 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: DW01 E131702-02
Matrix:Surface Soil
Date Collected:4/23/13 13:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW01
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Chromium, Hexavalent mg/kg dry SM 3500 Cr5.4 U18540-29-9 5/22/1321:465/20/1318:075.4
Aluminum mg/kg dry EPA 6010120007429-90-5 5/06/1318:145/03/1312:5840
Antimony mg/kg dry EPA 200.825U7440-36-0 5/20/1318:495/03/1313:0125
Arsenic mg/kg dry EPA 200.815007440-38-2 5/20/1318:495/03/1313:0125
Barium mg/kg dry EPA 60101207440-39-3 5/06/1318:145/03/1312:582.0
Beryllium mg/kg dry EPA 60101.2 U7440-41-7 5/06/1318:145/03/1312:581.2
Cadmium mg/kg dry EPA 200.812U7440-43-9 5/20/1318:495/03/1313:0112
Calcium mg/kg dry EPA 601045007440-70-2 5/06/1318:145/03/1312:5899
Chromium mg/kg dry EPA 601019007440-47-3 5/06/1318:145/03/1312:582.0
Cobalt mg/kg dry EPA 6010127440-48-4 5/06/1318:145/03/1312:582.0
Copper mg/kg dry EPA 601012007440-50-8 5/06/1318:145/03/1312:584.0
Iron mg/kg dry EPA 6010210007439-89-6 5/06/1318:145/03/1312:5840
Lead mg/kg dry EPA 200.825U7439-92-1 5/20/1318:495/03/1313:0125
Magnesium mg/kg dry EPA 601078007439-95-4 5/06/1318:145/03/1312:5899
Manganese mg/kg dry EPA 60105807439-96-5 5/06/1318:145/03/1312:582.0
Molybdenum mg/kg dry EPA 60104.0 U7439-98-7 5/06/1318:145/03/1312:584.0
Nickel mg/kg dry EPA 6010167440-02-0 5/06/1318:145/03/1312:584.0
Potassium mg/kg dry EPA 601040007440-09-7 5/06/1318:145/03/1312:58400
Selenium mg/kg dry EPA 200.850U7782-49-2 5/20/1318:495/03/1313:0150
Silver mg/kg dry EPA 60102.0 U7440-22-4 5/06/1318:145/03/1312:582.0
Sodium mg/kg dry EPA 6010400U7440-23-5 5/06/1318:145/03/1312:58400
Strontium mg/kg dry EPA 6010287440-24-6 5/06/1318:145/03/1312:582.0
Thallium mg/kg dry EPA 200.825U7440-28-0 5/20/1318:495/03/1313:0125
Tin mg/kg dry EPA 60105.9 U7440-31-5 5/06/1318:145/03/1312:585.9
Titanium mg/kg dry EPA 60105507440-32-6 5/06/1318:145/03/1312:582.0
Vanadium mg/kg dry EPA 6010457440-62-2 5/06/1318:145/03/1312:582.0
Yttrium mg/kg dry EPA 60105.57440-65-5 5/06/1318:145/03/1312:581.2
Zinc mg/kg dry EPA 60105507440-66-6 5/06/1318:145/03/1312:584.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 7 of 32 SESD Project ID # 13-0231 Durable Woods 53 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Physical Properties
Sample ID:Lab ID: DW01 E131702-02
Matrix:Surface Soil
Date Collected:4/23/13 13:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW01
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
% Solids %EPA 200.290E16429415/02/1313:305/01/1315:570.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 8 of 32 SESD Project ID # 13-0231 Durable Woods 54 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: DW02 E131702-03
Matrix:Surface Soil
Date Collected:4/23/13 14:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW02
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Chromium, Hexavalent mg/kg dry SM 3500 Cr5.5 U18540-29-9 5/22/1321:465/20/1318:075.5
Aluminum mg/kg dry EPA 601071007429-90-5 5/06/1318:295/03/1312:589.9
Antimony mg/kg dry EPA 200.80.50 U7440-36-0 5/20/1318:535/03/1313:010.50
Arsenic mg/kg dry EPA 200.8397440-38-2 5/20/1318:535/03/1313:010.50
Barium mg/kg dry EPA 6010527440-39-3 5/06/1318:295/03/1312:580.50
Beryllium mg/kg dry EPA 60100.30 U7440-41-7 5/06/1318:295/03/1312:580.30
Cadmium mg/kg dry EPA 200.80.25 U7440-43-9 5/20/1318:535/03/1313:010.25
Calcium mg/kg dry EPA 60104407440-70-2 5/06/1318:295/03/1312:5825
Chromium mg/kg dry EPA 6010517440-47-3 5/06/1318:295/03/1312:580.50
Cobalt mg/kg dry EPA 60105.07440-48-4 5/06/1318:295/03/1312:580.50
Copper mg/kg dry EPA 6010287440-50-8 5/06/1318:295/03/1312:580.99
Iron mg/kg dry EPA 6010140007439-89-6 5/06/1318:295/03/1312:589.9
Lead mg/kg dry EPA 200.8227439-92-1 5/20/1318:535/03/1313:010.50
Magnesium mg/kg dry EPA 60105407439-95-4 5/06/1318:295/03/1312:5825
Manganese mg/kg dry EPA 60104107439-96-5 5/06/1318:295/03/1312:580.50
Molybdenum mg/kg dry EPA 60100.99 U7439-98-7 5/06/1318:295/03/1312:580.99
Nickel mg/kg dry EPA 60103.67440-02-0 5/06/1318:295/03/1312:580.99
Potassium mg/kg dry EPA 60102007440-09-7 5/06/1318:295/03/1312:5899
Selenium mg/kg dry EPA 200.80.99 U7782-49-2 5/20/1318:535/03/1313:010.99
Silver mg/kg dry EPA 60100.50 U7440-22-4 5/06/1318:295/03/1312:580.50
Sodium mg/kg dry EPA 601099U7440-23-5 5/06/1318:295/03/1312:5899
Strontium mg/kg dry EPA 60103.77440-24-6 5/06/1318:295/03/1312:580.50
Thallium mg/kg dry EPA 200.80.50 U7440-28-0 5/20/1318:535/03/1313:010.50
Tin mg/kg dry EPA 60101.5 U7440-31-5 5/06/1318:295/03/1312:581.5
Titanium mg/kg dry EPA 6010417440-32-6 5/06/1318:295/03/1312:580.50
Vanadium mg/kg dry EPA 6010387440-62-2 5/06/1318:295/03/1312:580.50
Yttrium mg/kg dry EPA 60103.87440-65-5 5/06/1318:295/03/1312:580.30
Zinc mg/kg dry EPA 60101107440-66-6 5/06/1318:295/03/1312:580.99
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 9 of 32 SESD Project ID # 13-0231 Durable Woods 55 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Physical Properties
Sample ID:Lab ID: DW02 E131702-03
Matrix:Surface Soil
Date Collected:4/23/13 14:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW02
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
% Solids %EPA 200.288E16429415/02/1313:305/01/1315:570.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 10 of 32 SESD Project ID # 13-0231 Durable Woods 56 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: DW03 E131702-04
Matrix:Surface Soil
Date Collected:4/23/13 14:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW03
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Chromium, Hexavalent mg/kg dry SM 3500 Cr5.2 U18540-29-9 5/22/1321:465/20/1318:075.2
Aluminum mg/kg dry EPA 601065007429-90-5 5/06/1318:365/03/1312:5830
Antimony mg/kg dry EPA 200.84.9 U7440-36-0 5/20/1319:055/03/1313:014.9
Arsenic mg/kg dry EPA 200.84807440-38-2 5/20/1319:055/03/1313:014.9
Barium mg/kg dry EPA 6010657440-39-3 5/06/1318:365/03/1312:581.5
Beryllium mg/kg dry EPA 60100.89 U7440-41-7 5/06/1318:365/03/1312:580.89
Cadmium mg/kg dry EPA 200.82.5 U7440-43-9 5/20/1319:055/03/1313:012.5
Calcium mg/kg dry EPA 601036007440-70-2 5/06/1318:365/03/1312:5874
Chromium mg/kg dry EPA 60106807440-47-3 5/06/1318:365/03/1312:581.5
Cobalt mg/kg dry EPA 60107.77440-48-4 5/06/1318:365/03/1312:581.5
Copper mg/kg dry EPA 60103507440-50-8 5/06/1318:365/03/1312:583.0
Iron mg/kg dry EPA 6010130007439-89-6 5/06/1318:365/03/1312:5830
Lead mg/kg dry EPA 200.8117439-92-1 5/20/1319:055/03/1313:014.9
Magnesium mg/kg dry EPA 601037007439-95-4 5/06/1318:365/03/1312:5874
Manganese mg/kg dry EPA 60103207439-96-5 5/06/1318:365/03/1312:581.5
Molybdenum mg/kg dry EPA 60103.0 U7439-98-7 5/06/1318:365/03/1312:583.0
Nickel mg/kg dry EPA 6010237440-02-0 5/06/1318:365/03/1312:583.0
Potassium mg/kg dry EPA 601017007440-09-7 5/06/1318:365/03/1312:58300
Selenium mg/kg dry EPA 200.89.8 U7782-49-2 5/20/1319:055/03/1313:019.8
Silver mg/kg dry EPA 60101.5 U7440-22-4 5/06/1318:365/03/1312:581.5
Sodium mg/kg dry EPA 6010300U7440-23-5 5/06/1318:365/03/1312:58300
Strontium mg/kg dry EPA 6010167440-24-6 5/06/1318:365/03/1312:581.5
Thallium mg/kg dry EPA 200.84.9 U7440-28-0 5/20/1319:055/03/1313:014.9
Tin mg/kg dry EPA 60104.4 U7440-31-5 5/06/1318:365/03/1312:584.4
Titanium mg/kg dry EPA 60102807440-32-6 5/06/1318:365/03/1312:581.5
Vanadium mg/kg dry EPA 6010287440-62-2 5/06/1318:365/03/1312:581.5
Yttrium mg/kg dry EPA 60103.17440-65-5 5/06/1318:365/03/1312:580.89
Zinc mg/kg dry EPA 60105007440-66-6 5/06/1318:365/03/1312:583.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 11 of 32 SESD Project ID # 13-0231 Durable Woods 57 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Physical Properties
Sample ID:Lab ID: DW03 E131702-04
Matrix:Surface Soil
Date Collected:4/23/13 14:15
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW03
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
% Solids %EPA 200.291E16429415/02/1313:305/01/1315:570.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 12 of 32 SESD Project ID # 13-0231 Durable Woods 58 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: DW04 E131702-05
Matrix:Surface Soil
Date Collected:4/23/13 14:45
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW04
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Chromium, Hexavalent mg/kg dry SM 3500 Cr6.0 U18540-29-9 5/22/1321:465/20/1318:076.0
Aluminum mg/kg dry EPA 601077007429-90-5 5/06/1318:435/03/1312:5820
Antimony mg/kg dry EPA 200.80.25 U7440-36-0 5/20/1319:105/03/1313:010.25
Arsenic mg/kg dry EPA 200.82.77440-38-2 5/20/1319:105/03/1313:010.25
Barium mg/kg dry EPA 6010147440-39-3 5/06/1318:435/03/1312:580.99
Beryllium mg/kg dry EPA 60100.59 U7440-41-7 5/06/1318:435/03/1312:580.59
Cadmium mg/kg dry EPA 200.80.12 U7440-43-9 5/20/1319:105/03/1313:010.12
Calcium mg/kg dry EPA 60104007440-70-2 5/06/1318:435/03/1312:5849
Chromium mg/kg dry EPA 6010537440-47-3 5/06/1318:435/03/1312:580.99
Cobalt mg/kg dry EPA 60100.99 U7440-48-4 5/06/1318:435/03/1312:580.99
Copper mg/kg dry EPA 6010287440-50-8 5/06/1318:435/03/1312:582.0
Iron mg/kg dry EPA 6010340007439-89-6 5/06/1318:435/03/1312:5820
Lead mg/kg dry EPA 200.87.07439-92-1 5/20/1319:105/03/1313:010.25
Magnesium mg/kg dry EPA 60102207439-95-4 5/06/1318:435/03/1312:5849
Manganese mg/kg dry EPA 60101207439-96-5 5/06/1318:435/03/1312:580.99
Molybdenum mg/kg dry EPA 60102.0 U7439-98-7 5/06/1318:435/03/1312:582.0
Nickel mg/kg dry EPA 60102.0 U7440-02-0 5/06/1318:435/03/1312:582.0
Potassium mg/kg dry EPA 60102307440-09-7 5/06/1318:435/03/1312:58200
Selenium mg/kg dry EPA 200.80.49 U7782-49-2 5/20/1319:105/03/1313:010.49
Silver mg/kg dry EPA 60100.99 U7440-22-4 5/06/1318:435/03/1312:580.99
Sodium mg/kg dry EPA 6010200U7440-23-5 5/06/1318:435/03/1312:58200
Strontium mg/kg dry EPA 60102.77440-24-6 5/06/1318:435/03/1312:580.99
Thallium mg/kg dry EPA 200.80.25 U7440-28-0 5/20/1319:105/03/1313:010.25
Tin mg/kg dry EPA 60103.0 U7440-31-5 5/06/1318:435/03/1312:583.0
Titanium mg/kg dry EPA 60101407440-32-6 5/06/1318:435/03/1312:580.99
Vanadium mg/kg dry EPA 6010927440-62-2 5/06/1318:435/03/1312:580.99
Yttrium mg/kg dry EPA 60102.47440-65-5 5/06/1318:435/03/1312:580.59
Zinc mg/kg dry EPA 6010107440-66-6 5/06/1318:435/03/1312:582.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 13 of 32 SESD Project ID # 13-0231 Durable Woods 59 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Physical Properties
Sample ID:Lab ID: DW04 E131702-05
Matrix:Surface Soil
Date Collected:4/23/13 14:45
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW04
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
% Solids %EPA 200.281E16429415/02/1313:305/01/1315:570.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 14 of 32 SESD Project ID # 13-0231 Durable Woods 60 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: DW05 E131702-06
Matrix:Surface Soil
Date Collected:4/23/13 15:10
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW05
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Chromium, Hexavalent mg/kg dry SM 3500 Cr5.2 U, X-CH618540-29-9 5/22/1321:465/20/1318:075.2
Aluminum mg/kg dry EPA 601072007429-90-5 5/06/1318:515/03/1312:5820
Antimony mg/kg dry EPA 200.82.5 U, J, QM-17440-36-0 5/20/1319:155/03/1313:012.5
Arsenic mg/kg dry EPA 200.82007440-38-2 5/20/1319:155/03/1313:012.5
Barium mg/kg dry EPA 6010727440-39-3 5/06/1318:515/03/1312:581.0
Beryllium mg/kg dry EPA 60100.60 U7440-41-7 5/06/1318:515/03/1312:580.60
Cadmium mg/kg dry EPA 200.81.2 U7440-43-9 5/20/1319:155/03/1313:011.2
Calcium mg/kg dry EPA 601052007440-70-2 5/06/1318:515/03/1312:5850
Chromium mg/kg dry EPA 6010250J, QM-1,
QM-2, QM-3
7440-47-3 5/06/1318:515/03/1312:581.0
Cobalt mg/kg dry EPA 60109.07440-48-4 5/06/1318:515/03/1312:581.0
Copper mg/kg dry EPA 6010180J, QM-27440-50-8 5/06/1318:515/03/1312:582.0
Iron mg/kg dry EPA 6010180007439-89-6 5/06/1318:515/03/1312:5820
Lead mg/kg dry EPA 200.8127439-92-1 5/20/1319:155/03/1313:012.5
Magnesium mg/kg dry EPA 60104600J, QM-27439-95-4 5/06/1318:515/03/1312:5850
Manganese mg/kg dry EPA 60104007439-96-5 5/06/1318:515/03/1312:581.0
Molybdenum mg/kg dry EPA 60102.0 U7439-98-7 5/06/1318:515/03/1312:582.0
Nickel mg/kg dry EPA 6010137440-02-0 5/06/1318:515/03/1312:582.0
Potassium mg/kg dry EPA 601017007440-09-7 5/06/1318:515/03/1312:58200
Selenium mg/kg dry EPA 200.85.0 U7782-49-2 5/20/1319:155/03/1313:015.0
Silver mg/kg dry EPA 60101.0 U7440-22-4 5/06/1318:515/03/1312:581.0
Sodium mg/kg dry EPA 6010200U7440-23-5 5/06/1318:515/03/1312:58200
Strontium mg/kg dry EPA 6010177440-24-6 5/06/1318:515/03/1312:581.0
Thallium mg/kg dry EPA 200.82.5 U7440-28-0 5/20/1319:155/03/1313:012.5
Tin mg/kg dry EPA 60103.0 U7440-31-5 5/06/1318:515/03/1312:583.0
Titanium mg/kg dry EPA 6010310J, QM-27440-32-6 5/06/1318:515/03/1312:581.0
Vanadium mg/kg dry EPA 6010327440-62-2 5/06/1318:515/03/1312:581.0
Yttrium mg/kg dry EPA 60104.77440-65-5 5/06/1318:515/03/1312:580.60
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 15 of 32 SESD Project ID # 13-0231 Durable Woods 61 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: DW05 E131702-06
Matrix:Surface Soil
Date Collected:4/23/13 15:10
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW05
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Zinc mg/kg dry EPA 6010567440-66-6 5/06/1318:515/03/1312:582.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 16 of 32 SESD Project ID # 13-0231 Durable Woods 62 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Physical Properties
Sample ID:Lab ID: DW05 E131702-06
Matrix:Surface Soil
Date Collected:4/23/13 15:10
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW05
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
% Solids %EPA 200.292E16429415/02/1313:305/01/1315:570.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 17 of 32 SESD Project ID # 13-0231 Durable Woods 63 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: DW06 E131702-07
Matrix:Surface Soil
Date Collected:4/23/13 15:20
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW06
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Chromium, Hexavalent mg/kg dry SM 3500 Cr5.6 U18540-29-9 5/22/1321:465/20/1318:075.6
Aluminum mg/kg dry EPA 601074007429-90-5 5/06/1319:135/03/1312:5810
Antimony mg/kg dry EPA 200.82.5 U7440-36-0 5/20/1319:295/03/1313:012.5
Arsenic mg/kg dry EPA 200.81607440-38-2 5/20/1319:295/03/1313:012.5
Barium mg/kg dry EPA 6010397440-39-3 5/06/1319:135/03/1312:580.50
Beryllium mg/kg dry EPA 60100.30 U7440-41-7 5/06/1319:135/03/1312:580.30
Cadmium mg/kg dry EPA 200.81.2 U7440-43-9 5/20/1319:295/03/1313:011.2
Calcium mg/kg dry EPA 601018007440-70-2 5/06/1319:135/03/1312:5825
Chromium mg/kg dry EPA 60102507440-47-3 5/06/1319:135/03/1312:580.50
Cobalt mg/kg dry EPA 60104.07440-48-4 5/06/1319:135/03/1312:580.50
Copper mg/kg dry EPA 60101607440-50-8 5/06/1319:135/03/1312:581.0
Iron mg/kg dry EPA 6010180007439-89-6 5/06/1319:135/03/1312:5810
Lead mg/kg dry EPA 200.86.87439-92-1 5/20/1319:295/03/1313:012.5
Magnesium mg/kg dry EPA 601018007439-95-4 5/06/1319:135/03/1312:5825
Manganese mg/kg dry EPA 60102307439-96-5 5/06/1319:135/03/1312:580.50
Molybdenum mg/kg dry EPA 60101.0 U7439-98-7 5/06/1319:135/03/1312:581.0
Nickel mg/kg dry EPA 60104.77440-02-0 5/06/1319:135/03/1312:581.0
Potassium mg/kg dry EPA 60108507440-09-7 5/06/1319:135/03/1312:58100
Selenium mg/kg dry EPA 200.85.0 U7782-49-2 5/20/1319:295/03/1313:015.0
Silver mg/kg dry EPA 60100.50 U7440-22-4 5/06/1319:135/03/1312:580.50
Sodium mg/kg dry EPA 6010100U7440-23-5 5/06/1319:135/03/1312:58100
Strontium mg/kg dry EPA 60107.97440-24-6 5/06/1319:135/03/1312:580.50
Thallium mg/kg dry EPA 200.82.5 U7440-28-0 5/20/1319:295/03/1313:012.5
Tin mg/kg dry EPA 60101.5 U7440-31-5 5/06/1319:135/03/1312:581.5
Titanium mg/kg dry EPA 60101407440-32-6 5/06/1319:135/03/1312:580.50
Vanadium mg/kg dry EPA 6010477440-62-2 5/06/1319:135/03/1312:580.50
Yttrium mg/kg dry EPA 60103.27440-65-5 5/06/1319:135/03/1312:580.30
Zinc mg/kg dry EPA 6010507440-66-6 5/06/1319:135/03/1312:581.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 18 of 32 SESD Project ID # 13-0231 Durable Woods 64 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Physical Properties
Sample ID:Lab ID: DW06 E131702-07
Matrix:Surface Soil
Date Collected:4/23/13 15:20
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW06
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
% Solids %EPA 200.287E16429415/02/1313:305/01/1315:570.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 19 of 32 SESD Project ID # 13-0231 Durable Woods 65 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: DW07 E131702-08
Matrix:Surface Soil
Date Collected:4/23/13 15:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW07
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Chromium, Hexavalent mg/kg dry SM 3500 Cr5.4 U18540-29-9 5/22/1321:465/20/1318:075.4
Aluminum mg/kg dry EPA 601071007429-90-5 5/06/1319:215/03/1312:5810
Antimony mg/kg dry EPA 200.80.25 U7440-36-0 5/20/1319:345/03/1313:010.25
Arsenic mg/kg dry EPA 200.8147440-38-2 5/20/1319:345/03/1313:010.25
Barium mg/kg dry EPA 6010267440-39-3 5/06/1319:215/03/1312:580.50
Beryllium mg/kg dry EPA 60100.30 U7440-41-7 5/06/1319:215/03/1312:580.30
Cadmium mg/kg dry EPA 200.80.12 U7440-43-9 5/20/1319:345/03/1313:010.12
Calcium mg/kg dry EPA 601012007440-70-2 5/06/1319:215/03/1312:5825
Chromium mg/kg dry EPA 6010427440-47-3 5/06/1319:215/03/1312:580.50
Cobalt mg/kg dry EPA 60102.87440-48-4 5/06/1319:215/03/1312:580.50
Copper mg/kg dry EPA 6010277440-50-8 5/06/1319:215/03/1312:581.0
Iron mg/kg dry EPA 6010160007439-89-6 5/06/1319:215/03/1312:5810
Lead mg/kg dry EPA 200.86.67439-92-1 5/20/1319:345/03/1313:010.25
Magnesium mg/kg dry EPA 60108707439-95-4 5/06/1319:215/03/1312:5825
Manganese mg/kg dry EPA 60101507439-96-5 5/06/1319:215/03/1312:580.50
Molybdenum mg/kg dry EPA 60101.0 U7439-98-7 5/06/1319:215/03/1312:581.0
Nickel mg/kg dry EPA 60102.27440-02-0 5/06/1319:215/03/1312:581.0
Potassium mg/kg dry EPA 60105807440-09-7 5/06/1319:215/03/1312:58100
Selenium mg/kg dry EPA 200.80.50 U7782-49-2 5/20/1319:345/03/1313:010.50
Silver mg/kg dry EPA 60100.50 U7440-22-4 5/06/1319:215/03/1312:580.50
Sodium mg/kg dry EPA 6010100U7440-23-5 5/06/1319:215/03/1312:58100
Strontium mg/kg dry EPA 60104.77440-24-6 5/06/1319:215/03/1312:580.50
Thallium mg/kg dry EPA 200.80.25 U7440-28-0 5/20/1319:345/03/1313:010.25
Tin mg/kg dry EPA 60101.5 U7440-31-5 5/06/1319:215/03/1312:581.5
Titanium mg/kg dry EPA 60101107440-32-6 5/06/1319:215/03/1312:580.50
Vanadium mg/kg dry EPA 6010397440-62-2 5/06/1319:215/03/1312:580.50
Yttrium mg/kg dry EPA 60102.07440-65-5 5/06/1319:215/03/1312:580.30
Zinc mg/kg dry EPA 6010297440-66-6 5/06/1319:215/03/1312:581.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 20 of 32 SESD Project ID # 13-0231 Durable Woods 66 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Physical Properties
Sample ID:Lab ID: DW07 E131702-08
Matrix:Surface Soil
Date Collected:4/23/13 15:40
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW07
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
% Solids %EPA 200.289E16429415/02/1313:305/01/1315:570.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 21 of 32 SESD Project ID # 13-0231 Durable Woods 67 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Total Metals
Sample ID:Lab ID: DW08 E131702-09
Matrix:Surface Soil
Date Collected:4/23/13 16:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW08
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
Chromium, Hexavalent mg/kg dry SM 3500 Cr5.3 U18540-29-9 5/22/1321:465/20/1318:075.3
Aluminum mg/kg dry EPA 601047007429-90-5 5/06/1319:285/03/1312:5820
Antimony mg/kg dry EPA 200.85.0 U7440-36-0 5/20/1319:385/03/1313:015.0
Arsenic mg/kg dry EPA 200.86007440-38-2 5/20/1319:385/03/1313:015.0
Barium mg/kg dry EPA 6010367440-39-3 5/06/1319:285/03/1312:580.99
Beryllium mg/kg dry EPA 60100.60 U7440-41-7 5/06/1319:285/03/1312:580.60
Cadmium mg/kg dry EPA 200.82.5 U7440-43-9 5/20/1319:385/03/1313:012.5
Calcium mg/kg dry EPA 601017007440-70-2 5/06/1319:285/03/1312:5850
Chromium mg/kg dry EPA 60106007440-47-3 5/06/1319:285/03/1312:580.99
Cobalt mg/kg dry EPA 60104.17440-48-4 5/06/1319:285/03/1312:580.99
Copper mg/kg dry EPA 60102707440-50-8 5/06/1319:285/03/1312:582.0
Iron mg/kg dry EPA 6010130007439-89-6 5/06/1319:285/03/1312:5820
Lead mg/kg dry EPA 200.8177439-92-1 5/20/1319:385/03/1313:015.0
Magnesium mg/kg dry EPA 601021007439-95-4 5/06/1319:285/03/1312:5850
Manganese mg/kg dry EPA 60102307439-96-5 5/06/1319:285/03/1312:580.99
Molybdenum mg/kg dry EPA 60102.0 U7439-98-7 5/06/1319:285/03/1312:582.0
Nickel mg/kg dry EPA 60106.07440-02-0 5/06/1319:285/03/1312:582.0
Potassium mg/kg dry EPA 601010007440-09-7 5/06/1319:285/03/1312:58200
Selenium mg/kg dry EPA 200.89.9 U7782-49-2 5/20/1319:385/03/1313:019.9
Silver mg/kg dry EPA 60100.99 U7440-22-4 5/06/1319:285/03/1312:580.99
Sodium mg/kg dry EPA 6010200U7440-23-5 5/06/1319:285/03/1312:58200
Strontium mg/kg dry EPA 60107.17440-24-6 5/06/1319:285/03/1312:580.99
Thallium mg/kg dry EPA 200.85.0 U7440-28-0 5/20/1319:385/03/1313:015.0
Tin mg/kg dry EPA 60103.0 U7440-31-5 5/06/1319:285/03/1312:583.0
Titanium mg/kg dry EPA 60101707440-32-6 5/06/1319:285/03/1312:580.99
Vanadium mg/kg dry EPA 6010217440-62-2 5/06/1319:285/03/1312:580.99
Yttrium mg/kg dry EPA 60104.17440-65-5 5/06/1319:285/03/1312:580.60
Zinc mg/kg dry EPA 60101407440-66-6 5/06/1319:285/03/1312:582.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 22 of 32 SESD Project ID # 13-0231 Durable Woods 68 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Physical Properties
Sample ID:Lab ID: DW08 E131702-09
Matrix:Surface Soil
Date Collected:4/23/13 16:00
Project: 13-0231, Durable Wood Preservers, Inc.
Station ID:DW08
CAS
Number Analyte Results Qualifiers Units MRL Prepared Analyzed Method
% Solids %EPA 200.292E16429415/02/1313:305/01/1315:570.0
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 23 of 32 SESD Project ID # 13-0231 Durable Woods 69 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals (TMTL) - Quality Control
US-EPA, Region 4, SESD
Batch 1305025 - M 200.2 Metals Soil
Blank (1305025-BLK1)Prepared: 05/03/13 Analyzed: 05/06/13
EPA 6010
Silver mg/kg dryU0.50 U
Barium "U 0.50 U
Beryllium "U 0.30 U
Cobalt "U 0.50 U
Chromium "U 0.50 U
Copper "U 1.0 U
Molybdenum "U 1.0 U
Nickel "U 1.0 U
Tin "U 1.5 U
Strontium "U 0.50 U
Titanium "U 0.50 U
Vanadium "U 0.50 U
Yttrium "U 0.30 U
Zinc "U 1.0 U
Aluminum "U 10 U
Manganese "U 0.50 U
Calcium "U 25 U
Magnesium "U 25 U
Iron "U 10 U
Sodium "U 100 U
Potassium "U 100 U
Blank (1305025-BLK2)Prepared: 05/03/13 Analyzed: 05/06/13
EPA 6010
Silver mg/kg dryU0.50 U
Barium "U 0.50 U
Beryllium "U 0.30 U
Cobalt "U 0.50 U
Chromium "U 0.50 U
Copper "U 1.0 U
Molybdenum "U 1.0 U
Nickel "U 1.0 U
Tin "U 1.5 U
Strontium "U 0.50 U
Titanium "U 0.50 U
Vanadium "U 0.50 U
Yttrium "U 0.30 U
Zinc "U 1.0 U
Aluminum "U 10 U
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 24 of 32 SESD Project ID # 13-0231 Durable Woods 70 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals (TMTL) - Quality Control
US-EPA, Region 4, SESD
Batch 1305025 - M 200.2 Metals Soil
Blank (1305025-BLK2)Prepared: 05/03/13 Analyzed: 05/06/13
Manganese mg/kg dryU0.50 U
Calcium "U 25 U
Magnesium "U 25 U
Iron "U 10 U
Sodium "U 100 U
Potassium "U 100 U
LCS (1305025-BS1)Prepared: 05/03/13 Analyzed: 05/06/13
EPA 6010
Silver mg/kg dry9.9436 0.50 10.000 85-11599.4
Barium "47.767 0.50 50.000 85-11595.5
Beryllium "20.359 0.30 20.000 85-115102
Cobalt "50.639 0.50 50.000 85-115101
Chromium "49.765 0.50 50.000 85-11599.5
Copper "30.205 1.0 30.000 85-115101
Molybdenum "30.720 1.0 30.000 85-115102
Nickel "80.966 1.0 80.000 85-115101
Tin "101.65 1.5 100.00 85-115102
Strontium "39.181 0.50 40.000 85-11598.0
Titanium "51.219 0.50 50.000 85-115102
Vanadium "40.864 0.50 40.000 85-115102
Yttrium "30.111 0.30 30.000 85-115100
Zinc "100.45 1.0 100.00 85-115100
Aluminum "501.22 10 500.00 85-115100
Manganese "512.93 0.50 500.00 85-115103
Calcium "518.55 25 500.00 85-115104
Magnesium "521.90 25 500.00 85-115104
Iron "525.01 10 500.00 85-115105
Sodium "983.79 100 1000.0 85-11598.4
Potassium "1014.3 100 1000.0 85-115101
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 25 of 32 SESD Project ID # 13-0231 Durable Woods 71 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals (TMTL) - Quality Control
US-EPA, Region 4, SESD
Batch 1305025 - M 200.2 Metals Soil
Matrix Spike (1305025-MS1)Prepared: 05/03/13 Analyzed: 05/06/13 Source: E131702-06
EPA 6010
Silver mg/kg dry9.4478 0.99 9.8580 U 75-12595.8
Barium "122.75 0.99 49.290 72.199 75-125103
Beryllium "20.040 0.59 19.716 0.087069 75-125101
Cobalt "57.510 0.99 49.290 9.0053 75-12598.4
Chromium "255.20 0.99 49.290 249.68 QM-175-12511.2
Copper "210.54 2.0 29.574 176.39 75-125115
Molybdenum "24.110 2.0 29.574 U 75-12581.5
Nickel "87.682 2.0 78.864 12.518 75-12595.3
Tin "95.239 3.0 98.580 2.0657 75-12594.5
Strontium "56.174 0.99 39.432 16.950 75-12599.5
Titanium "351.12 0.99 49.290 312.39 75-12578.6
Vanadium "66.299 0.99 39.432 31.505 75-12588.2
Yttrium "33.938 0.59 29.574 4.7475 75-12598.7
Zinc "153.25 2.0 98.580 55.849 75-12598.8
Aluminum "7378.3 20 492.90 7176.9 XM-175-12540.9
Manganese "882.51 0.99 492.90 396.26 75-12598.7
Calcium "5969.9 49 492.90 5157.1 XM-175-125165
Magnesium "5002.4 49 492.90 4602.8 75-12581.1
Iron "15053 20 492.90 17698 XM-175-125NR
Sodium "1107.2 200 985.80 121.91 75-12599.9
Potassium "2677.0 200 985.80 1722.5 75-12596.8
Matrix Spike Dup (1305025-MSD1)Prepared: 05/03/13 Analyzed: 05/06/13 Source: E131702-06
EPA 6010
Silver mg/kg dry9.7980 0.99 9.9108 U 2075-12598.9 3.64
Barium "124.28 0.99 49.554 72.199 2075-125105 1.24
Beryllium "20.026 0.59 19.822 0.087069 2075-125101 0.0667
Cobalt "58.635 0.99 49.554 9.0053 2075-125100 1.94
Chromium "318.49 0.99 49.554 249.68 20 QM-2,
QM-3
75-125139 22.1
Copper "232.30 2.0 29.732 176.39 20 QM-275-125188 9.83
Molybdenum "24.423 2.0 29.732 U 2075-12582.1 1.29
Nickel "91.122 2.0 79.286 12.518 2075-12599.1 3.85
Tin "95.356 3.0 99.108 2.0657 2075-12594.1 0.123
Strontium "55.708 0.99 39.643 16.950 2075-12597.8 0.832
Titanium "377.32 0.99 49.554 312.39 20 QM-275-125131 7.19
Vanadium "70.825 0.99 39.643 31.505 2075-12599.2 6.60
Yttrium "35.126 0.59 29.732 4.7475 2075-125102 3.44
Zinc "163.14 2.0 99.108 55.849 2075-125108 6.25
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 26 of 32 SESD Project ID # 13-0231 Durable Woods 72 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals (TMTL) - Quality Control
US-EPA, Region 4, SESD
Batch 1305025 - M 200.2 Metals Soil
Matrix Spike Dup (1305025-MSD1)Prepared: 05/03/13 Analyzed: 05/06/13 Source: E131702-06
Aluminum mg/kg dry7753.3 20 495.54 7176.9 20 XM-175-125116 4.96
Manganese "896.56 0.99 495.54 396.26 2075-125101 1.58
Calcium "5301.7 50 495.54 5157.1 20 XM-175-12529.2 11.9
Magnesium "5260.0 50 495.54 4602.8 20 QM-275-125133 5.02
Iron "16458 20 495.54 17698 20 XM-175-125NR 8.91
Sodium "1117.8 200 991.08 121.91 2075-125100 0.950
Potassium "2695.7 200 991.08 1722.5 2075-12598.2 0.696
MRL Verification (1305025-PS1)Prepared: 05/03/13 Analyzed: 05/06/13
EPA 6010
Silver mg/kg dry0.45554 0.50 0.50000 MRL-3,
U
70-13091.1
Barium "0.46129 0.50 0.50000 MRL-3,
U
70-13092.3
Beryllium "0.29574 0.30 0.30000 MRL-3,
U
70-13098.6
Cobalt "0.47918 0.50 0.50000 MRL-3,
U
70-13095.8
Chromium "0.50076 0.50 0.50000 MRL-370-130100
Copper "0.98089 1.0 1.0000 MRL-3,
U
70-13098.1
Molybdenum "1.0532 1.0 1.0000 MRL-370-130105
Nickel "1.0491 1.0 1.0000 MRL-370-130105
Tin "1.4076 1.5 1.5000 MRL-3,
U
70-13093.8
Strontium "0.46138 0.50 0.50000 MRL-3,
U
70-13092.3
Titanium "0.53280 0.50 0.50000 MRL-370-130107
Vanadium "0.63036 0.50 0.50000 MRL-370-130126
Yttrium "0.28684 0.30 0.30000 MRL-3,
U
70-13095.6
Zinc "1.0248 1.0 1.0000 MRL-370-130102
Aluminum "11.890 10 10.000 MRL-370-130119
Manganese "0.48022 0.50 0.50000 MRL-3,
U
70-13096.0
Calcium "27.472 25 25.000 MRL-370-130110
Magnesium "26.244 25 25.000 MRL-370-130105
Iron "10.273 10 10.000 MRL-370-130103
Sodium "96.165 100 100.00 MRL-3,
U
70-13096.2
Potassium "94.780 100 100.00 MRL-3,
U
70-13094.8
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 27 of 32 SESD Project ID # 13-0231 Durable Woods 73 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals (TMTL) - Quality Control
US-EPA, Region 4, SESD
Batch 1305026 - M 200.2 Metals Soil
Blank (1305026-BLK1)Prepared: 05/03/13 Analyzed: 05/20/13
EPA 200.8
Beryllium mg/kg dryU0.050 U
Arsenic "U 0.10 U
Selenium "U 0.20 B-3, U
Cadmium "U 0.050 U
Antimony "U 0.10 U
Thallium "U 0.10 U
Lead "U 0.10 U
Blank (1305026-BLK2)Prepared: 05/03/13 Analyzed: 05/20/13
EPA 200.8
Beryllium mg/kg dryU0.050 U
Arsenic "U 0.10 U
Selenium "U 0.20 U
Cadmium "U 0.050 U
Antimony "U 0.10 U
Thallium "U 0.10 U
Lead "U 0.10 U
LCS (1305026-BS1)Prepared: 05/03/13 Analyzed: 05/20/13
EPA 200.8
Beryllium mg/kg dry20.791 1.2 20.000 85-115104
Arsenic "50.627 2.5 50.000 85-115101
Selenium "101.37 5.0 100.00 85-115101
Cadmium "21.521 1.2 20.000 85-115108
Antimony "102.84 2.5 100.00 85-115103
Thallium "23.370 2.5 20.000 QC-285-115117
Lead "114.95 2.5 100.00 85-115115
Matrix Spike (1305026-MS1)Prepared: 05/03/13 Analyzed: 05/20/13 Source: E131702-06
EPA 200.8
Beryllium mg/kg dry20.314 1.2 19.716 U 70-130103
Arsenic "207.88 2.5 49.290 199.09 XM-170-13017.8
Selenium "78.905 4.9 98.580 U 70-13080.0
Cadmium "21.336 1.2 19.716 0.16197 70-130107
Antimony "36.844 2.5 98.580 0.58860 QM-170-13036.8
Thallium "21.742 2.5 19.716 U 70-130110
Lead "124.34 2.5 98.580 12.401 70-130114
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 28 of 32 SESD Project ID # 13-0231 Durable Woods 74 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals (TMTL) - Quality Control
US-EPA, Region 4, SESD
Batch 1305026 - M 200.2 Metals Soil
Matrix Spike Dup (1305026-MSD1)Prepared: 05/03/13 Analyzed: 05/20/13 Source: E131702-06
EPA 200.8
Beryllium mg/kg dry21.255 1.2 19.822 U 2070-130107 4.53
Arsenic "249.67 2.5 49.554 199.09 20 XM-170-130102 18.3
Selenium "83.221 5.0 99.108 U 2070-13084.0 5.32
Cadmium "21.705 1.2 19.822 0.16197 2070-130109 1.71
Antimony "36.980 2.5 99.108 0.58860 20 QM-170-13036.7 0.367
Thallium "22.058 2.5 19.822 U 2070-130111 1.44
Lead "126.01 2.5 99.108 12.401 2070-130115 1.33
MRL Verification (1305026-PS1)Prepared: 05/03/13 Analyzed: 05/20/13
EPA 200.8
Beryllium mg/kg dry0.057235 0.050 0.050000 MRL-365-135114
Arsenic "0.098880 0.10 0.10000 MRL-3,
U
65-13598.9
Selenium "0.29187 0.20 0.20000 MRL-3,
QR-2
65-135146
Cadmium "0.051539 0.050 0.050000 MRL-365-135103
Antimony "0.051526 0.10 0.050000 MRL-3,
U
65-135103
Thallium "0.055699 0.10 0.050000 MRL-3,
U
65-135111
Lead "0.11352 0.10 0.10000 MRL-365-135114
Batch 1305106 - M Hex Chrome in Solids 3060
Blank (1305106-BLK1)Prepared: 05/20/13 Analyzed: 05/22/13
SM 3500 Cr
Chromium, Hexavalent mg/kg wetU5.0 U
Blank (1305106-BLK2)Prepared: 05/20/13 Analyzed: 05/22/13
SM 3500 Cr
Chromium, Hexavalent mg/kg wetU4.8 U
LCS (1305106-BS1)Prepared: 05/20/13 Analyzed: 05/22/13
SM 3500 Cr
Chromium, Hexavalent mg/kg wet49.130 5.0 50.000 80-12098.3
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 29 of 32 SESD Project ID # 13-0231 Durable Woods 75 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals (TMTL) - Quality Control
US-EPA, Region 4, SESD
Batch 1305106 - M Hex Chrome in Solids 3060
LCS (1305106-BS2)Prepared: 05/20/13 Analyzed: 05/22/13
SM 3500 Cr
Chromium, Hexavalent mg/kg wet14482027000 160900 80-12090.0
LCS Dup (1305106-BSD1)Prepared: 05/20/13 Analyzed: 05/22/13
SM 3500 Cr
Chromium, Hexavalent mg/kg wet49.901 5.0 50.000 2080-12099.8 1.56
Duplicate (1305106-DUP1)Prepared: 05/20/13 Analyzed: 05/22/13 Source: E131702-06
SM 3500 Cr
Chromium, Hexavalent mg/kg dry0.80046 5.2 U 20 XD-1, U
Matrix Spike (1305106-MS1)Prepared: 05/20/13 Analyzed: 05/22/13 Source: E131702-06
SM 3500 Cr
Chromium, Hexavalent mg/kg dry19.737 5.3 105.15 U QM-175-12518.8
Matrix Spike (1305106-MS2)Prepared: 05/20/13 Analyzed: 05/22/13 Source: E131702-06
SM 3500 Cr
Chromium, Hexavalent mg/kg dry1107.3 110 2028.4 U QM-175-12554.6
Matrix Spike (1305106-MS3)Prepared: 05/20/13 Analyzed: 05/22/13 Source: E131702-06
SM 3500 Cr
Chromium, Hexavalent mg/kg dry72.942 5.2 104.42 U QM-185-11569.9
MRL Verification (1305106-PS1)Prepared: 05/20/13 Analyzed: 05/22/13
SM 3500 Cr
Chromium, Hexavalent mg/kg wet4.7550 5.0 5.0000 MRL-3,
U
60-14095.1
6/5/13 15:52E131702 PHYSP TMTL FINAL 06 05 13 1552Page 30 of 32 SESD Project ID # 13-0231 Durable Woods 76 of 78
D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Physical Properties (PHYSP) - Quality Control
US-EPA, Region 4, SESD
Batch 1305009 - M % Solids
Duplicate (1305009-DUP1)Prepared: 05/01/13 Analyzed: 05/02/13 Source: E131702-09
EPA 200.2
% Solids %91.652 0.0 92.106 100.494
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D.A.R.T. Id: 13-0231
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4 Science and Ecosystem Support Division
980 College Station Road, Athens, Georgia 30605-2700
Project: 13-0231, Durable Wood Preservers, Inc. - Reported by Roberta Howes
Notes and Definitions for QC Samples
U The analyte was not detected at or above the reporting limit.
B-3 Level in blank does not impact data quality
MRL-3 MRL verification for Soil matrix
QC-2 Analyte concentration high in continuing calibration verification standard
QC-6 Calibration check standard greater than method control limits.
QM-1 Matrix Spike Recovery less than method control limits
QM-2 Matrix Spike Recovery greater than method control limits
QM-3 Matrix Spike Precision outside method control limits
QR-2 MRL verification recovery greater than upper control limits.
XD-1 Duplicate results less than MRL
XM-1 Sample background/spike ratio higher than method evaluation criteria
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