21059_609-615 West South Street_Brownfields_Stormwater Pipe Soil and GW Report_20180928

WithersRavenel
Our People. Your Success.
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington

September 28, 2018

State of North Carolina
Department of Environment Quality
Division of Waste Management - Brownfields Section
Mail Service Center 1646
Raleigh, NC 27699-1646

Attn: Mr. Brad Atkinson

Reference: Stormwater Pipe Corridor Investigation Report
609, 611, 615, and 617 West South Street
Raleigh, Wake County, North Carolina
WR Project Number: 02170761.00

Dear Mr. Atkinson:

WithersRavenel, Inc. (WR) has prepared this Stormwater Pipe Corridor Investigation Report to
document activities that took place on August 24, 2018.

Background

The property formerly identified as 609 West South Street is transected from north to south by a
sub-surface, 60-inch diameter stormwater pipe (Figure 1). The pipe is constructed of corrugated
aluminum and discharges stormwater, collected from properties to the north, to a tributary of
Rocky Branch along the southern property boundary of the subject site. The stormwater pipe is
in disrepair and is planned to be replaced in November 2018, prior to site redevelopment activities.

Unsuitable fill material surrounding the stormwater pipe was not removed during grading activities
that took place on the subject properties between December 2016 and September 2017. Soils
surrounding the stormwater pipe were deemed unsuitable for construction by a geotechnical
engineering firm due to the presence of fill and/or rubble material. Due to the presence of
unsuitable materials surrounding the stormwater pipe and the possibility of offsite disposal of said
material, WR wrote a Stormwater Pipe Replacement Investigation Work Plan, dated July 25, 2018,
outlining a soil and groundwater sampling plan along the stormwater pipe corridor. The
aforementioned work plan for this phase of site work was approved by the North Carolina
Brownfields Program in an email on July 31, 2018.

Soil Sampling Procedures

WR mobilized to the subject property on August 24, 2018 to advance eight soil borings along the
stormwater pipe using a direct-push Geoprobe drilling machine. Soil samples were collected with
60-inch long, new macrocore liners and decontaminated tooling.

Collected soil samples were immediately placed in laboratory supplied bottleware following the
opening of the macrocore liner by the onsite geologist. Collected soil samples were then placed
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Our People. Your Success.
609, 611, 613, & 615 West South Street WR Project # 02170761.00
Stormwater Pipe Corridor Investigation Report September 2018
Page 2 of 5

in a cooler containing ice and shipped under proper chain of custody procedures to ESC Lab
Sciences, in Mt. Juliet, TN (ESC) for analysis by the following methods:

• Volatile Organic Compounds (VOCS) by EPA Method 8260B, Semi-VOCs (SVOCs) by EPA
Method 8270D, and RCRA-8 Metals by 6010D / 7471B.

Soil samples were collected from the following depth intervals*:

• SWP-1**: 1 to 5 feet and 15 to 20 feet below ground surface;
• SWP-2**: 1 to 5 feet and 15 to 20 feet below ground surface;
• SWP-3: 1 to 5 feet and 10 to 15 feet below ground surface;
• SWP-4: 1 to 5 feet and 10 to 15 feet below ground surface;
• SWP-5: 1 to 5 feet and 12 to 15 feet below ground surface;
• SWP-6: 1 to 5 feet and 10 to 15 feet below ground surface;
• SWP-7: 2 to 5 feet and 12 to 14 feet below ground surface; and
• SWP-8: 1 to 5 feet and 10 to 15 feet below ground surface.
Notes:
* Soil collection intervals were increased with respect to the work plan due to low macrocore recovery. ** Borings SWP-1 and SWP-2 were advanced in the undisturbed / ungraded portion of the site located along the
southern property line.
Following sample collection, the remaining soils in the liner were classified and placed in zip-lock
baggies for field screening with a field calibrated MiniRAE 3000 photo-ionization detector (PID).
The field meter readings are shown on the boring logs which are included in the Appendix.

Sampling locations were recorded with a sub-meter GPS device. Sampling locations are illustrated
on Figure 1 and latitude / longitude coordinates are provided on Table 1.

Groundwater and Stormwater Sampling Procedures
Following the advancement of soil borings SWP-4 and SWP-7, 1-inch diameter well screen was
installed in each boring to facilitate the collection of a groundwater sample from each location.
The temporary wells were identified as TWSWP-4 and TWSWP-7. The following table summarize
temporary well information.

Temporary Well ID Total Depth
(ft)
Groundwater Depth Below
Ground Surface
(ft)
TWSWP-4 15 9.85
TWSWP-7 13 8.60

Each temporary well was purged with a peristaltic pump and dedicated polyethylene tubing for a
minimum of one hour to remove fine sediments from the water column. Prior to sample collection,
WithersRavenel
Our People. Your Success.
609, 611, 613, & 615 West South Street WR Project # 02170761.00
Stormwater Pipe Corridor Investigation Report September 2018
Page 3 of 5

turbidity readings were collected to verify that the turbidity was less than 10 NTUs in each
temporary well.

Groundwater samples were decanted from the tubing and placed in laboratory supplied
bottleware, immediately placed in a cooler containing ice, and shipped under proper chain of
custody procedures to ESC Lab Sciences, in Mt. Juliet, TN (ESC). Groundwater samples were
laboratory analyzed by the following methods:

• VOCS by EPA Method 8260B, SVOCs by EPA Method 8270D, and RCRA-8 Metals by
6010D / 7470A.

Following sample collection, each temporary well was properly abandoned by removing the well
screen and filling the boring void with bentonite.

WR also collected a sample of the stormwater exiting the pipe outfall near the southern property
line. At the time of the sample approximately four inches of water was flowing through the pipe.
The sample was collected by filling the laboratory supplied bottleware with the stormwater exiting
the pipe. Following sample collection, the sample was immediately placed in a cooler containing
ice and shipped under property chain of custody procedures to ESC Lab Sciences, in Mt. Juliet, TN
(ESC). The outfall sample was laboratory analyzed by the following method:

• VOCS by EPA Method 8260B.

Sampling locations are illustrated on Figure 1 and latitude / longitude coordinates are provided on
Table 1.

Soil Laboratory Analytical Results
The laboratory analytical results are summarized in Table 2 and the laboratory analytical report is
included in the Appendix. Boring locations are illustrated on Figure 1.

RCRA-8 Metals:

Arsenic, barium, chromium (total), cadmium, lead, and mercury were detected at concentrations
above the laboratory method detection limit (MDL) in one or more of the collected soil samples.

Arsenic and chromium were detected in one or more of the soil samples at concentrations that
exceeded the Residential and / or the Industrial / Commercial Health Preliminary Soil Remediation
Goals (PSRGs) from February 2018. Though these concentrations exceeded published PSRGs,
their concentrations are comparable to typical background concentrations according to the U.S.
Geological Survey Professional (USGS) Paper 1648. Arsenic and chromium concentration
distribution figures from USGS Paper 1648 are provided in the appendix.

WithersRavenel
Our People. Your Success.
609, 611, 613, & 615 West South Street WR Project # 02170761.00
Stormwater Pipe Corridor Investigation Report September 2018
Page 4 of 5

Volatile Organic Compounds:

A number of VOCs were detected at concentrations above their laboratory method detection limit
(MDL) in one or more of the collected soil samples. Naphthalene was detected in boring SWP-2
(15-20) at a concentration of 54.7 mg/kg; which exceeds the Industrial / Commercial PSRG of 18
mg/kg. No other VOCs were detected at concentrations that exceeded the Residential or
Industrial / Commercial PSRGs.

Semi-Volatile Organic Compounds:

A number of SVOCs were detected at concentrations above their laboratory method detection
limit (MDL) in one or more of the collected soil samples.

The following borings contained one or more SVOCs that exceeded their respective Residential
PSRGs:
• SWP-1 (1-4);
• SWP-1 (15-20);
• SWP-2 (1-5);
• SWP-2 (15-20);
• SWP-3 (1-5);
• SWP-4 (10-15);
• SWP-6 (1-5);
• SWP-6 (10-15);
• SWP-7 (2-5);
• SWP-8 (1-5); and
• SWP-8 (10-15).

The following borings contained one or more SVOCs that exceeded their respective Industrial /
Commercial PSRGs:
• SWP-1 (1-4);
• SWP-2 (15-20); and
• SWP-8 (10-15).

Groundwater & Stormwater Laboratory Analytical Results
The laboratory analytical results are summarized in Table 3 and the laboratory analytical report is
included in the Appendix. Temporary well locations are illustrated on Figure 1.

RCRA-8 Metals:

Arsenic, barium, and lead were detected at concentrations above the laboratory method detection
limit (MDL) in one or more of the collected groundwater samples; however, no RCRA-8 metals
concentrations exceeded their respective NC Groundwater Standard.

Volatile Organic Compounds:

FIGURES

TABLES

TABLE 1 - GPS LOCATIONS - STORMWATER PIPE CORRIDOR ASSESSMENT
609, 611, 615, & 617 West South Street, Raleigh, NC 27603
WR JOB NO. 02170761.00
Sample ID Latitude Longitude
SWP-1 35.7718909 -78.6489646
SWP-2 35.7719500 -78.6489411
SWP-3 35.7720030 -78.6489688
SWP-4 / TWSWP-4 35.7720619 -78.6489481
SWP-5 35.72112 -78.6489767
SWP-6 35.772172 -786489526
SWP-7 / TWSWP-7 35.7722232 -78.6489736
SWP-8 35.7722796 -78.6489481
Note:
1) GPS data collected with sub-meter GPS unit.
Page 1 of 1
TABLE 2 - STORMWATER PIPE CORRIDOR SOIL ANALYTICAL RESULTS (HITS AND QUALIFIERS ONLY)
609, 611, 615, and 617 West South Street, Raleigh, NC 27603
WR Job No. 02170761.00
Method Analyte CAS
NC IHSB
Residential
Health PSRG
February
2018
NC IHSBIndustrial / Commercial Health PSRG
February
2018
Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier Result Qualifier
6010D ARSENIC 7440-38-2 0.68 3 2.04 J 1.73 J 1.62 J 1.9 J 1.3 J <2.18 0.908 J 7.25 1.36 J <2.15 2.55 5.61 4.18 <2.32 2.03 J 4.616010DBARIUM7440-39-3 3100 47000 86.1 85.8 59.9 61.2 128 62.3 88.6 69.9 116 55.8 114 65.4 122 9.7 202 306010DCADMIUM7440-43-9 14 200 0.224 J 0.0961 J <0.614 0.201 J <0.624 <0.546 0.305 J 0.425 J <0.641 <0.538 0.143 J 0.154 J 0.469 J <0.581 1.19 0.0899 J6010DCHROMIUM7440-47-3 0.31 6.5 31.2 18.1 14.4 14.6 16.7 8.53 21.9 42.6 22.9 34.8 28.5 50.7 23.5 4.44 8.9 9.626010DLEAD7439-92-1 NL NL 61.3 42.8 22.6 55.7 12.1 2.89 128 J6 138 12.9 3.62 79.5 145 167 8.45 384 1416010DSELENIUM7782-49-2 78 1200 <2.53 <2.61 <2.46 <2.53 <2.50 <2.18 <2.53 <2.54 <2.56 <2.15 <2.48 <2.38 <2.42 <2.32 0.881 J <2.406010DSILVER7440-22-4 78 1200 <1.27 <1.30 <1.23 <1.26 <1.25 <1.09 <1.26 <1.27 <1.28 <1.08 <1.24 <1.19 <1.21 <1.16 <1.14 <1.207471BMERCURY7439-97-6 2.3 NL 0.0928 0.113 0.055 B 0.0465 B 0.0403 B 0.0079 B J 0.184 0.11 0.0702 0.00629 B J 0.111 0.11 0.165 0.00652 B J 0.177 0.13
8260B BENZENE 71-43-2 1.2 5.4 0.00867 <0.00130 <0.00123 0.0569 <0.00125 <0.00157 <0.00126 <0.00127 <0.00128 <0.00108 <0.00124 <0.00119 <0.00121 <0.00116 0.00525 0.01858260BBROMOBENZENE108-86-1 59 370 <0.0158 <0.0163 <0.0153 <0.0158 <0.0156 <0.0197 <0.0158 <0.0159 <0.0160 <0.0135 <0.0155 <0.0149 <0.0151 <0.0145 J4 <0.0143 J4 <0.0150 J48260BN-BUTYLBENZENE 104-51-8 780 1200 <0.0158 J4 <0.0163 J4 <0.0153 J4 <0.0158 J4 <0.0156 J4 0.00631 B J J4 <0.0158 J4 <0.0159 J4 <0.0160 J4 <0.0135 J4 <0.0155 J4 <0.0149 J4 <0.0151 J4 <0.0145 <0.0143 0.00519 J8260BSEC-BUTYLBENZENE 135-98-8 1600 23000 <0.0158 <0.0163 <0.0153 0.0312 B 0.00397 B J <0.0197 <0.0158 <0.0159 <0.0160 <0.0135 <0.0155 <0.0149 <0.0151 <0.0145 <0.0143 0.00581 J8260BTERT-BUTYLBENZENE 98-06-6 1600 23000 <0.00633 <0.00652 <0.00614 <0.00632 <0.00624 <0.00786 <0.00632 <0.00635 <0.00641 <0.00538 <0.00619 <0.00595 <0.00604 <0.00581 J4 <0.00571 J4 <0.00600 J48260BCHLOROBENZENE108-90-7 58 280 <0.00317 <0.00326 <0.00307 0.468 0.00614 <0.00393 <0.00316 0.00636 <0.00320 <0.00269 <0.00310 0.00877 0.00614 0.00113 J <0.00286 0.1668260BCHLOROFORM67-66-3 0.34 1.5 <0.00317 <0.00326 <0.00307 <0.00316 <0.00312 <0.00393 <0.00316 <0.00318 <0.00320 <0.00269 <0.00310 0.00125 J <0.00302 <0.00291 <0.00286 <0.003008260B4-CHLOROTOLUENE 106-43-4 310 4700 <0.00633 <0.00652 <0.00614 <0.00632 <0.00624 <0.00786 <0.00632 <0.00635 <0.00641 <0.00538 <0.00619 <0.00595 <0.00604 <0.00581 J4 <0.00571 J4 <0.00600 J48260B1,2-DICHLOROBENZENE 95-50-1 380 2000 <0.00633 <0.00652 <0.00614 <0.00632 <0.00624 <0.00786 <0.00632 <0.00635 <0.00641 <0.00538 <0.00619 <0.00595 <0.00604 <0.00581 <0.00571 0.007888260B1,3-DICHLOROBENZENE 541-73-1 NL NL <0.00633 <0.00652 <0.00614 0.182 0.0143 <0.00786 <0.00632 0.0137 <0.00641 <0.00538 <0.00619 0.0051 J 0.0119 <0.00581 <0.00571 0.1278260B1,4-DICHLOROBENZENE 106-46-7 2.8 12 <0.00633 <0.00652 <0.00614 0.237 0.0175 <0.00786 <0.00632 0.0868 0.00404 J <0.00538 <0.00619 0.00745 0.0328 <0.00581 <0.00571 0.4468260B1,1-DICHLOROETHANE 75-34-3 3.8 17 <0.00317 <0.00326 <0.00307 <0.00316 <0.00312 <0.00393 <0.00316 <0.00318 <0.00320 <0.00269 <0.00310 <0.00298 <0.00302 <0.00291 <0.00286 0.000986 J8260B1,2-DICHLOROETHANE 107-06-2 0.49 2.2 <0.00317 <0.00326 <0.00307 <0.00316 <0.00312 <0.00393 <0.00316 0.0215 <0.00320 <0.00269 <0.00310 0.022 <0.00302 <0.00291 <0.00286 0.08378260B1,1-DICHLOROETHENE 75-35-4 48 210 <0.00317 <0.00326 <0.00307 <0.00316 <0.00312 <0.00393 <0.00316 0.0237 <0.00320 <0.00269 <0.00310 0.00687 <0.00302 0.00248 J <0.00286 0.003448260BCIS-1,2-DICHLOROETHENE 156-59-2 31 470 <0.00317 <0.00326 <0.00307 <0.00316 <0.00312 <0.00393 <0.00316 0.258 0.00299 J <0.00269 <0.00310 0.0106 0.00291 J 0.00133 J <0.00286 0.118260BTRANS-1,2-DICHLOROETHENE 156-60-5 310 4700 <0.00633 <0.00652 <0.00614 <0.00632 <0.00624 <0.00786 <0.00632 0.0146 <0.00641 <0.00538 <0.00619 <0.00595 <0.00604 <0.00581 <0.00571 0.0288260BDI-ISOPROPYL ETHER 108-20-3 480 2000 <0.00127 0.0068 <0.00123 <0.00126 <0.00125 <0.00157 <0.00126 <0.00127 <0.00128 <0.00108 <0.00124 0.00158 <0.00121 <0.00116 <0.00114 0.005498260BETHYLBENZENE100-41-4 6.1 27 0.00208 J 0.002 J <0.00307 0.242 0.0053 0.00113 J <0.00316 0.00408 <0.00320 <0.00269 <0.00310 0.00102 J 0.00262 J <0.00291 0.0019 J 0.005368260BISOPROPYLBENZENE98-82-8 410 2100 <0.00317 <0.00326 <0.00307 0.697 0.0373 0.00763 0.00111 J 0.00136 J <0.00320 <0.00269 <0.00310 <0.00298 <0.00302 <0.00291 <0.00286 0.01058260BP-ISOPROPYLTOLUENE 99-87-6 NL NL <0.00633 <0.00652 <0.00614 0.416 0.0581 0.0244 0.00519 J 0.00326 J <0.00641 <0.00538 <0.00619 <0.00595 <0.00604 <0.00581 <0.00571 0.00322 J8260B2-BUTANONE (MEK)78-93-3 5500 40000 <0.0317 <0.0326 <0.0307 <0.0316 0.0265 J <0.0393 <0.0316 <0.0318 0.0229 J <0.0269 <0.0310 <0.0298 <0.0302 <0.0291 <0.0286 <0.03008260BMETHYLENE CHLORIDE 75-09-2 58 650 <0.0317 <0.0326 <0.0307 <0.0316 <0.0312 <0.0393 <0.0316 <0.0318 <0.0320 <0.0269 <0.0310 <0.0298 <0.0302 <0.0291 <0.0286 <0.03008260BNAPHTHALENE91-20-3 4.1 18 0.0307 0.0414 0.0122 J 54.7 0.0413 0.0096 J <0.0158 0.0614 <0.0160 <0.0135 0.00481 J 0.0271 0.0381 <0.0145 J3 0.0118 J J3 0.168 J38260BN-PROPYLBENZENE 103-65-1 780 5100 <0.00633 <0.00652 <0.00614 0.588 0.0375 0.01 B <0.00632 <0.00635 <0.00641 <0.00538 <0.00619 <0.00595 <0.00604 <0.00581 <0.00571 0.00469 J8260BTETRACHLOROETHENE127-18-4 17 82 0.00593 <0.00326 <0.00307 <0.126 <0.00312 <0.00393 0.00882 0.0478 <0.00320 <0.00269 <0.00310 0.108 0.00776 0.00695 2.51 0.01058260BTOLUENE108-88-3 990 9700 0.00934 0.0129 0.00168 J <0.253 0.00211 J <0.00786 <0.00632 0.00866 <0.00641 <0.00538 <0.00619 0.00574 J 0.00527 J <0.00581 0.0224 0.01538260B1,2,3-TRICHLOROBENZENE 87-61-6 13 190 <0.00317 <0.00326 <0.00307 <0.00316 <0.00312 <0.00393 <0.00316 <0.00318 <0.00320 <0.00269 <0.00310 <0.00298 <0.00302 <0.00291 J3 <0.00286 J3 0.0162 J38260B1,2,4-TRICHLOROBENZENE 120-82-1 12 55 <0.0158 <0.0163 <0.0153 <0.0158 <0.0156 <0.0197 <0.0158 <0.0159 <0.0160 <0.0135 <0.0155 <0.0149 <0.0151 <0.0145 J3 <0.0143 J3 0.193 J38260BTRICHLOROETHENE79-01-6 0.87 4 <0.00127 <0.00130 <0.00123 <0.00126 <0.00125 <0.00157 <0.00126 0.11 <0.00128 <0.00108 <0.00124 0.667 0.00748 0.0264 0.00412 1.148260B1,2,4-TRIMETHYLBENZENE 95-63-6 63 370 0.00463 B J 0.00503 B J 0.00247 B J 2.29 0.00378 J <0.00786 <0.00632 0.00251 J <0.00641 <0.00538 <0.00619 0.00243 B J 0.00483 B J <0.00581 0.00493 J 0.01478260B1,3,5-TRIMETHYLBENZENE 108-67-8 56 320 <0.00633 <0.00652 <0.00614 0.991 0.072 0.0197 B 0.00394 B J <0.00635 <0.00641 <0.00538 <0.00619 <0.00595 <0.00604 <0.00581 0.00155 J 0.00558 J8260BXYLENES, TOTAL 1330-20-7 120 530 0.0117 B 0.0111 B <0.00798 B 0.411 0.0115 B <0.0102 <0.00821 B 0.0108 B <0.00833 <0.00700 <0.00805 B 0.00691 B J 0.00911 B <0.00755 0.0243 0.0206
8270D ACENAPHTHENE 83-32-9 720 9000 0.331 0.1 <0.0405 50.6 0.236 0.0166 J <0.0834 0.943 <0.0423 <0.0355 <0.204 0.0667 J 0.195 J <0.0383 0.0748 J 0.238270DACENAPHTHYLENE208-96-8 NL NL 0.441 0.0225 J 0.0578 5.74 0.0896 <0.0360 <0.0834 0.381 J <0.0423 <0.0355 <0.204 0.186 J 0.225 J <0.0383 0.0855 J 0.5128270DANTHRACENE120-12-7 3600 45000 1.15 0.128 0.222 29.5 0.286 <0.0360 <0.0834 0.768 <0.0423 <0.0355 0.0572 J 0.255 0.458 <0.0383 0.229 J 1.118270DBENZIDINE92-87-5 0.00053 0.01 <2.12 J4 <0.434 J4 <0.409 J4 <4.21 J4 <0.416 J4 <0.364 J4 <0.842 J4 <4.23 J4 <0.427 J4 <0.358 J4 <2.07 J4 J6 <1.99 J4 <4.02 J4 <0.387 J4 <3.81 J4 <2.00 J48270DBENZO(A)ANTHRACENE 56-55-3 1.1 21 3.5 0.384 1.13 16.3 0.216 0.0052 B J 0.0316 B J 1.32 <0.0423 <0.0355 0.194 B J 0.968 1.13 <0.0383 0.739 2.638270DBENZO(B)FLUORANTHENE 205-99-2 1.1 21 4.04 0.474 1.26 10.6 0.152 <0.0360 0.0509 J 0.63 J <0.0423 <0.0355 0.258 1.38 1.53 <0.0383 0.993 2.918270DBENZO(K)FLUORANTHENE 207-08-9 1.1 210 1.49 0.185 0.471 4.41 0.0539 <0.0360 0.0216 J 1.02 J <0.0423 <0.0355 0.0825 J 0.417 0.521 <0.0383 0.479 1.088270DBENZO(G,H,I)PERYLENE 191-24-2 NL NL 1.1 0.287 0.724 2.44 0.0665 <0.0360 0.0252 J <2.10 <0.0423 <0.0355 0.0911 J 0.37 0.405 <0.0383 0.305 J 0.8568270DBENZO(A)PYRENE 50-32-8 0.11 2.1 2.91 0.371 1.03 11.8 0.173 <0.0360 0.0361 J 0.898 J <0.0423 <0.0355 0.182 J 1.05 1.09 <0.0383 0.735 2.488270DBIS(2-CHLOROISOPROPYL)ETHER 39638-32-9 NL NL <2.12 <0.434 <0.409 0.106 J <0.416 <0.364 <0.842 <4.23 <0.427 <0.358 <2.07 <1.99 <4.02 <0.387 <3.81 <2.008270DCHRYSENE218-01-9 110 2100.0 3.33 0.392 1.07 13.9 0.173 <0.0360 0.0325 J 1.3 <0.0423 <0.0355 0.182 J 0.927 1.09 <0.0383 0.737 2.318270DDIBENZ(A,H)ANTHRACENE 53-70-3 0.11 2.1 0.837 0.714 1.84 1.33 0.301 <0.0360 <0.0834 <0.165 <0.0423 <0.0355 <0.204 0.288 0.181 <0.0383 <0.0330 0.5298270D3,3-DICHLOROBENZIDINE 91-94-1 1.2 5.1 <2.12 <0.434 <0.409 <4.21 <0.416 <0.364 <0.842 <4.23 <0.427 <0.358 <2.07 J3 J6 <1.99 <4.02 <0.387 <3.81 <2.008270DFLUORANTHENE206-44-0 480 6000 7.39 0.774 2.52 36.8 0.424 0.0105 J 0.0416 J 1.66 <0.0423 <0.0355 0.326 1.35 2.45 <0.0383 1.5 5.048270DFLUORENE86-73-7 480 6000 0.338 0.0715 0.0201 J 15 0.121 0.00857 J <0.0834 0.393 J <0.0423 <0.0355 <0.204 0.0761 J 0.172 J <0.0383 <0.377 0.3858270DHEXACHLOROCYCLOPENTADIENE77-47-4 0.38 1.6 <2.12 <0.434 <0.409 <4.21 <0.416 <0.364 <0.842 <4.23 <0.427 <0.358 <2.07 J6 <1.99 <4.02 <0.387 <3.81 <2.008270DINDENO(1,2,3-CD)PYRENE 193-39-5 1.1 21 7.37 7.65 19.2 7.57 1.72 <0.0360 0.308 <0.165 <0.0423 <0.0355 0.572 J6 2.39 1.29 <0.0383 0.942 5.238270DISOPHORONE78-59-1 570 2400 <2.12 <0.434 <0.409 0.173 J <0.416 <0.364 <0.842 <4.23 <0.427 <0.358 <2.07 <1.99 <4.02 <0.387 <3.81 <2.008270DNAPHTHALENE91-20-3 4.1 18 0.365 0.151 0.0248 J 30.3 0.0171 J <0.0360 <0.0834 0.648 <0.0423 <0.0355 <0.204 0.12 J 0.159 J <0.0383 <0.377 0.4998270DN-NITROSODIMETHYLAMINE 62-75-9 0.002 0.035 <2.12 <0.434 <0.409 <4.21 <0.416 <0.364 <0.842 <4.23 <0.427 <0.358 <2.07 J6 <1.99 <4.02 <0.387 <3.81 <2.008270DPHENANTHRENE85-01-8 NL NL 4.5 0.54 0.67 85.7 0.805 0.0235 J <0.0834 1.2 <0.0423 <0.0355 0.144 J 0.451 1.23 <0.0383 0.842 2.588270DBENZYLBUTYL PHTHALATE 85-68-7 290 1200 <2.12 <0.434 0.0333 J <4.21 <0.416 <0.364 <0.842 <4.23 <0.427 <0.358 <2.07 <1.99 <4.02 <0.387 <3.81 <2.008270DBIS(2-ETHYLHEXYL)PHTHALATE 117-81-7 39 160 0.123 J <0.434 0.0157 J <4.21 <0.416 0.0284 J <0.842 <4.23 <0.427 <0.358 <2.07 <1.99 <4.02 <0.387 <3.81 <2.008270DPYRENE129-00-0 360 4500 6.38 0.637 2.26 48.7 0.54 <0.0360 0.0383 J 3.3 <0.0423 <0.0355 0.312 1.55 2.28 <0.0383 1.25 5.098270D1,2,4-TRICHLOROBENZENE 120-82-1 12 55 <2.12 <0.434 <0.409 <4.21 <0.416 <0.364 <0.842 0.166 J <0.427 <0.358 <2.07 0.154 J <4.02 <0.387 <3.81 0.115 J8270D4,6-DINITRO-2-METHYLPHENOL 534-52-1 1 13 <2.12 <0.434 <0.409 <4.21 <0.416 <0.364 <0.842 <4.23 <0.427 <0.358 <2.07 J6 <1.99 <4.02 <0.387 <3.81 <2.008270D2,4-DINITROPHENOL 51-28-5 25 330 <2.12 <0.434 <0.409 <4.21 <0.416 <0.364 <0.842 <4.23 <0.427 <0.358 <2.07 J6 <1.99 <4.02 <0.387 <3.81 <2.008270DPENTACHLOROPHENOL87-86-5 1 4 <2.12 <0.434 <0.409 <4.21 <0.416 <0.364 <0.842 <4.23 <0.427 <0.358 <2.07 J3 <1.99 <4.02 <0.387 <3.81 <2.00
Qualifiers:
B: The same analyte is found in the associated blank.
J: The identification of the analyte is acceptable; the reported value is an estimate.
J1: Surrogate recovery limits have been exceeded; values are outside upper control limits.
J2: Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3: The associated batch QC was outside the established quality control range for precision.
J4: The associated batch QC was outside the established quality control range for accuracy.
J7: Surrogate recovery cannot be used for control limit evaluation due to dilution.
Notes:1) All results provided in mg/kg or parts per million.NL = Not Listed.Result = Result Exceeds MDL.Result = Result Exceeds Residential Health Based PSRG.
Result = Result Exceeds Industrial / Commercial Use Health Based PSRG.
J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low.
STORMWATER PIPE CORRIDOR
08/24/2018 08/24/2018mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg08/24/2018 08/24/2018 08/24/2018 08/24/2018 08/24/2018 08/24/2018SWP-5 1-5 SWP-5 12-15 SWP-6 1-5 SWP-6 10-15 SWP-7 2-5 SWP-7 12-14 SWP-8 1-5 SWP-8 10-15
Semi-Volatile Organic Compounds (SVOCs)
mg/kg mg/kg mg/kg
RCRA-8 Metals
Volatile Organic Compounds (VOCs)
Units mg/kg mg/kg mg/kg mg/kg mg/kg
SWP-4 10-15 Date Collected 08/24/2018 08/24/2018 08/24/2018 08/24/2018 08/24/2018 08/24/2018 08/24/2018 08/24/2018SWP-2 15-20 SWP-3 1-5 SWP-3 10-15 SWP-4 1-5
Sample Locations
Client Sample ID SWP-1 1-4 SWP-1 15-20 SWP-2 1-5
Page 1 of1
TABLE 3 - STORMWATER PIPE CORRIDOR GROUNDWATER AND STORMWATER OUTFALL ANALYTICAL RESULTS (HITS AND QUALIFIERS ONLY)
609, 611, 615, and 617 West South Street, Raleigh, NC 27603
WR Job No. 02170761.00
Method Analyte CAS
2L
Groundwater
Standard
(µg/L)
GCL
Groundwater
Standard
(µg/L)
Result Qualifier Result Qualifier Result Qualifier
6010D ARSENIC 7440-38-2 10 NL 7.05 J <10.0 NR
6010D BARIUM 7440-39-3 700 2000000 72.9 84.8 NR6010DCADMIUM7440-43-9 2 NL <2.00 <2.00 NR
6010D CHROMIUM 7440-47-3 10 NL <10.0 <10.0 NR
6010D LEAD 7439-92-1 15 15000 4.66 B J <5.00 NR
6010D SELENIUM 7782-49-2 20 NL <10.0 <10.0 NR6010DSILVER7440-22-4 20 18000 <5.00 <5.00 NR
7470A MERCURY 7439-97-6 1 NL <0.200 <0.200 NR
8260B CHLOROBENZENE 108-90-7 50 50000 <1.00 0.533 J <1.00
8260B CHLOROFORM 67-66-3 70 70000 <5.00 0.418 J <5.008260B1,1-DICHLOROETHANE 75-34-3 6 70000 <1.00 0.408 J <1.00
8260B 1,2-DICHLOROETHANE 107-06-2 0.4 380 <1.00 2.98 0.407 J
8260B 1,1-DICHLOROETHENE 75-35-4 350 7000 <1.00 10.5 0.772 J
8260B CIS-1,2-DICHLOROETHENE 156-59-2 70 70000 1.16 1.59 0.476 J8260B1,2-DICHLOROPROPANE 78-87-5 0.6 510 <1.00 0.487 J <1.00
8260B DI-ISOPROPYL ETHER 108-20-3 70 70000 <1.00 2.33 0.434 J
8260B METHYL TERT-BUTYL ETHER 1634-04-4 20 200000 <1.00 1.16 <1.00
8260B TETRACHLOROETHENE 127-18-4 0.7 700 0.379 J 6.64 18260BTRICHLOROETHENE79-01-6 3 2800 3.17 39.8 5.4
8270D DIMETHYL PHTHALATE 131-11-3 NL NL <3.00 J4 <3.00 J4 NR
8270D 2-CHLOROPHENOL 95-57-8 0.4 NL <10.0 J3 J4 <10.0 J3 J4 NR8270D2,4-DICHLOROPHENOL 120-83-2 NL NL <10.0 J3 J4 <10.0 J3 J4 NR
8270D 4,6-DINITRO-2-METHYLPHENOL 534-52-1 NL NL <10.0 J3 <10.0 J3 NR
8270D 2-NITROPHENOL 88-75-5 NL NL <10.0 J3 <10.0 J3 NR
8270D PENTACHLOROPHENOL 87-86-5 0.3 290 <10.0 J3 <10.0 J3 NR
8270D PHENOL 108-95-2 30 300000 0.575 J 0.62 J NR
Qualifiers:
Notes:
1) All results provided in ug/L (micrograms per liter) or parts per billion.
NL = Not Listed.NR = Not Reported.
Result = Result Exceeds MDL.
Result = Result Exceeds Unrestricted Use Health Based PSRG.
B: The same analyte is found in the associated blank.
J: The identification of the analyte is acceptable; the reported value is an estimate.
J1: Surrogate recovery limits have been exceeded; values are outside upper control limits.
J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7: Surrogate recovery cannot be used for control limit evaluation due to dilution.
J3: The associated batch QC was outside the established quality control range for precision.
J4: The associated batch QC was outside the established quality control range for accuracy.
RCRA-8 Metals
Volatile Organic Compounds (VOCs)
Semi-Volatile Organic Compounds (SVOCs)
Date Collected 08/24/2018 08/24/2018 08/24/2018
Units ug/L ug/L ug/L
Sample Locations Stormwater Pipe Groundwater and Outfall Samples
Sample ID TWSWP-4 TWSWP-7 OUTFALL
Page 1 of 1

APPENDIX A

Laboratory Analytical Report

ANALYTICAL REPORT
September 11, 2018
Withers & Ravenel Eng. - Standard
Sample Delivery Group:L1020964
Samples Received:08/25/2018
Project Number:02170761
Description:601-617 South West St
Site:LAMBERT
Report To:Matt James
115 MacKenan Drive
Cary, NC 27511
Entire Report Reviewed By:
September 11, 2018
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Nationalis performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
September 11, 2018
Heather J Wagner
Project Manager
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 7
Sr: Sample Results 8
SWP-1 1-4 L1020964-01 8
SWP-1 15-20 L1020964-02 11
SWP-2 1-5 L1020964-03 14
SWP-2 15-20 L1020964-04 17
SWP-3 1-5 L1020964-05 20
SWP-3 10-15 L1020964-06 23
SWP-4 1-5 L1020964-07 26
SWP-4 10-15 L1020964-08 29
SWP-5 1-5 L1020964-09 32
SWP-5 12-15 L1020964-10 35
SWP-6 1-5 L1020964-11 38
SWP-6 10-15 L1020964-12 41
SWP-7 2-5 L1020964-13 44
SWP-7 12-14 L1020964-14 47
SWP-8 1-5 L1020964-15 50
SWP-8 10-15 L1020964-16 53
TWSWP-4 L1020964-17 56
TWSWP-7 L1020964-18 59
OUTFALL L1020964-19 62
Qc: Quality Control Summary 64
Total Solids by Method 2540 G-2011 64
Mercury by Method 7470A 69
Mercury by Method 7471B 70
Metals (ICP) by Method 6010D 71
Volatile Organic Compounds (GC/MS) by Method 8260B 73
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 91
Gl: Glossary of Terms 100
Al: Accreditations & Locations 101
Sc: Sample Chain of Custody 102
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 2 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 2 of 105
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SWP-1 1-4 L1020964-01 Solid M James 08/24/18 09:00 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159443 1 08/31/18 10:34 08/31/18 10:44 KS
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 11:42 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 14:56 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/30/18 21:48 ACG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 5 09/02/18 01:41 09/03/18 09:27 SNR
Collected by Collected date/time Received date/time
SWP-1 15-20 L1020964-02 Solid M James 08/24/18 09:15 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159443 1 08/31/18 10:34 08/31/18 10:44 KS
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 11:44 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 14:59 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/30/18 22:08 ACG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 1 09/02/18 01:41 09/03/18 06:20 SNR
Collected by Collected date/time Received date/time
SWP-2 1-5 L1020964-03 Solid M James 08/24/18 09:30 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 11:47 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:07 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/30/18 22:28 ACG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 1 09/02/18 01:41 09/03/18 06:43 JF
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 5 09/02/18 01:41 09/04/18 16:01 LEA
Collected by Collected date/time Received date/time
SWP-2 15-20 L1020964-04 Solid M James 08/24/18 09:40 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 11:49 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:10 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/30/18 22:48 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160083 40 08/29/18 00:22 08/31/18 21:21 JHH
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 10 09/02/18 01:41 09/03/18 11:25 SNR
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 100 09/02/18 01:41 09/04/18 16:48 LEA
Collected by Collected date/time Received date/time
SWP-3 1-5 L1020964-05 Solid M James 08/24/18 09:50 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 11:57 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:12 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/30/18 23:08 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG1161063 1 08/29/18 00:22 09/04/18 11:13 DWR
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 1 09/02/18 01:41 09/03/18 07:06 SNR
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 3 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 3 of 105
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SWP-3 10-15 L1020964-06 Solid M James 08/24/18 10:00 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:00 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:15 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1.44 08/29/18 00:22 08/30/18 23:28 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160083 1.44 08/29/18 00:22 08/31/18 21:58 JHH
Volatile Organic Compounds (GC/MS) by Method 8260B WG1161063 1.44 08/29/18 00:22 09/04/18 11:31 DWR
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 1 09/02/18 01:41 09/03/18 03:59 SNR
Collected by Collected date/time Received date/time
SWP-4 1-5 L1020964-07 Solid M James 08/24/18 10:10 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:02 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 14:43 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/30/18 23:48 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160083 1 08/29/18 00:22 08/31/18 22:16 JHH
Volatile Organic Compounds (GC/MS) by Method 8260B WG1161063 1 08/29/18 00:22 09/04/18 11:50 DWR
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 2 09/02/18 01:41 09/03/18 07:53 SNR
Collected by Collected date/time Received date/time
SWP-4 10-15 L1020964-08 Solid M James 08/24/18 10:15 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:05 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:18 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/31/18 00:08 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160083 1 08/29/18 00:22 08/31/18 22:35 JHH
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 10 09/02/18 01:41 09/03/18 11:48 SNR
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 50 09/02/18 01:41 09/04/18 16:25 LEA
Collected by Collected date/time Received date/time
SWP-5 1-5 L1020964-09 Solid M James 08/24/18 10:25 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:07 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:20 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/31/18 00:28 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160083 1 08/29/18 00:22 08/31/18 22:53 JHH
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 1 09/02/18 01:41 09/03/18 04:23 SNR
Collected by Collected date/time Received date/time
SWP-5 12-15 L1020964-10 Solid M James 08/24/18 10:35 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:10 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:23 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/31/18 00:49 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160083 1 08/29/18 00:22 08/31/18 23:12 JHH
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SWP-5 12-15 L1020964-10 Solid M James 08/24/18 10:35 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 1 09/02/18 01:41 09/03/18 04:46 SNR
Collected by Collected date/time Received date/time
SWP-6 1-5 L1020964-11 Solid M James 08/24/18 10:45 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:12 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:26 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/31/18 01:09 ACG
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160083 1 08/29/18 00:22 08/31/18 23:31 JHH
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 5 09/02/18 01:41 09/03/18 08:17 SNR
Collected by Collected date/time Received date/time
SWP-6 10-15 L1020964-12 Solid M James 08/24/18 10:55 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159446 1 08/30/18 13:18 08/30/18 13:29 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:15 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:28 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/31/18 01:29 ACG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 5 09/02/18 01:41 09/03/18 09:51 SNR
Collected by Collected date/time Received date/time
SWP-7 2-5 L1020964-13 Solid M James 08/24/18 11:05 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159535 1 08/30/18 12:31 08/30/18 12:50 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:18 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:31 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1159831 1 08/29/18 00:22 08/31/18 01:50 ACG
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 10 09/02/18 01:41 09/03/18 10:38 SNR
Collected by Collected date/time Received date/time
SWP-7 12-14 L1020964-14 Solid M James 08/24/18 11:15 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159714 1 08/31/18 10:46 08/31/18 10:56 KS
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 11:34 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:39 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160333 1 08/29/18 00:22 08/31/18 20:09 BMB
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 1 09/02/18 01:41 09/03/18 05:10 ADF
Collected by Collected date/time Received date/time
SWP-8 1-5 L1020964-15 Solid M James 08/24/18 11:25 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159714 1 08/31/18 10:46 08/31/18 10:56 KS
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:20 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:42 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160333 1 08/29/18 00:22 08/31/18 20:29 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SWP-8 1-5 L1020964-15 Solid M James 08/24/18 11:25 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160867 10 08/29/18 00:22 09/03/18 13:58 DWR
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 10 09/02/18 01:41 09/03/18 11:01 SNR
Collected by Collected date/time Received date/time
SWP-8 10-15 L1020964-16 Solid M James 08/24/18 11:35 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1159541 1 08/30/18 12:57 08/30/18 13:15 JD
Mercury by Method 7471B WG1159451 1 08/30/18 09:15 08/31/18 12:30 ABL
Metals (ICP) by Method 6010D WG1159261 1 08/30/18 07:05 08/31/18 15:45 TRB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160333 1 08/29/18 00:22 08/31/18 20:49 BMB
Volatile Organic Compounds (GC/MS) by Method 8260B WG1160867 1 08/29/18 00:22 09/03/18 09:14 DWR
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159283 5 09/02/18 01:41 09/03/18 10:14 SNR
Collected by Collected date/time Received date/time
TWSWP-4 L1020964-17 GW M James 08/24/18 12:00 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG1157576 1 08/27/18 08:06 08/27/18 12:33 TCT
Metals (ICP) by Method 6010D WG1158118 1 08/28/18 13:58 08/29/18 11:56 ST
Volatile Organic Compounds (GC/MS) by Method 8260B WG1158295 1 08/29/18 00:54 08/29/18 00:54 BMB
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159178 1 08/31/18 16:24 09/01/18 13:38 SNR
Collected by Collected date/time Received date/time
TWSWP-7 L1020964-18 GW M James 08/24/18 13:00 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Mercury by Method 7470A WG1157576 1 08/27/18 08:06 08/27/18 12:35 TCT
Metals (ICP) by Method 6010D WG1158118 1 08/28/18 13:58 08/29/18 11:59 ST
Volatile Organic Compounds (GC/MS) by Method 8260B WG1158295 1 08/29/18 01:14 08/29/18 01:14 BMB
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1159178 1 08/31/18 16:24 09/01/18 14:02 SNR
Collected by Collected date/time Received date/time
OUTFALL L1020964-19 GW M James 08/24/18 13:15 08/25/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 8260B WG1158295 1 08/29/18 01:34 08/29/18 01:34 BMB
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Heather J Wagner
Project Manager
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1020964
SWP-1 1-4
Collected date/time: 08/24/18 09:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.9 1 08/31/2018 10:44 WG1159443
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0928 0.00355 0.0253 1 08/31/2018 11:42 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.04 J 0.583 2.53 1 08/31/2018 14:56 WG1159261
Barium 86.1 0.215 0.633 1 08/31/2018 14:56 WG1159261
Cadmium 0.224 J 0.0887 0.633 1 08/31/2018 14:56 WG1159261
Chromium 31.2 0.177 1.27 1 08/31/2018 14:56 WG1159261
Lead 61.3 0.241 0.633 1 08/31/2018 14:56 WG1159261
Selenium U 0.785 2.53 1 08/31/2018 14:56 WG1159261
Silver U 0.152 1.27 1 08/31/2018 14:56 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0174 0.0317 1 08/30/2018 21:48 WG1159831
Acrylonitrile U 0.00241 0.0158 1 08/30/2018 21:48 WG1159831
Benzene 0.00867 0.000507 0.00127 1 08/30/2018 21:48 WG1159831
Bromobenzene U 0.00133 0.0158 1 08/30/2018 21:48 WG1159831
Bromodichloromethane U 0.000998 0.00317 1 08/30/2018 21:48 WG1159831
Bromoform U 0.00758 0.0317 1 08/30/2018 21:48 WG1159831
Bromomethane U 0.00469 0.0158 1 08/30/2018 21:48 WG1159831
n-Butylbenzene U J4 0.00486 0.0158 1 08/30/2018 21:48 WG1159831
sec-Butylbenzene U 0.00321 0.0158 1 08/30/2018 21:48 WG1159831
tert-Butylbenzene U 0.00196 0.00633 1 08/30/2018 21:48 WG1159831
Carbon tetrachloride U 0.00137 0.00633 1 08/30/2018 21:48 WG1159831
Chlorobenzene U 0.000726 0.00317 1 08/30/2018 21:48 WG1159831
Chlorodibromomethane U 0.000570 0.00317 1 08/30/2018 21:48 WG1159831
Chloroethane U 0.00137 0.00633 1 08/30/2018 21:48 WG1159831
Chloroform U 0.000526 0.00317 1 08/30/2018 21:48 WG1159831
Chloromethane U 0.00176 0.0158 1 08/30/2018 21:48 WG1159831
2-Chlorotoluene U 0.00117 0.00317 1 08/30/2018 21:48 WG1159831
4-Chlorotoluene U 0.00143 0.00633 1 08/30/2018 21:48 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00646 0.0317 1 08/30/2018 21:48 WG1159831
1,2-Dibromoethane U 0.000665 0.00317 1 08/30/2018 21:48 WG1159831
Dibromomethane U 0.00127 0.00633 1 08/30/2018 21:48 WG1159831
1,2-Dichlorobenzene U 0.00184 0.00633 1 08/30/2018 21:48 WG1159831
1,3-Dichlorobenzene U 0.00215 0.00633 1 08/30/2018 21:48 WG1159831
1,4-Dichlorobenzene U 0.00250 0.00633 1 08/30/2018 21:48 WG1159831
Dichlorodifluoromethane U 0.00104 0.00317 1 08/30/2018 21:48 WG1159831
1,1-Dichloroethane U 0.000728 0.00317 1 08/30/2018 21:48 WG1159831
1,2-Dichloroethane U 0.000602 0.00317 1 08/30/2018 21:48 WG1159831
1,1-Dichloroethene U 0.000633 0.00317 1 08/30/2018 21:48 WG1159831
cis-1,2-Dichloroethene U 0.000874 0.00317 1 08/30/2018 21:48 WG1159831
trans-1,2-Dichloroethene U 0.00181 0.00633 1 08/30/2018 21:48 WG1159831
1,2-Dichloropropane U 0.00161 0.00633 1 08/30/2018 21:48 WG1159831
1,1-Dichloropropene U 0.000887 0.00317 1 08/30/2018 21:48 WG1159831
1,3-Dichloropropane U 0.00222 0.00633 1 08/30/2018 21:48 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1020964
SWP-1 1-4
Collected date/time: 08/24/18 09:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000859 0.00317 1 08/30/2018 21:48 WG1159831
trans-1,3-Dichloropropene U 0.00194 0.00633 1 08/30/2018 21:48 WG1159831
2,2-Dichloropropane U 0.00100 0.00317 1 08/30/2018 21:48 WG1159831
Di-isopropyl ether U 0.000443 0.00127 1 08/30/2018 21:48 WG1159831
Ethylbenzene 0.00208 J 0.000671 0.00317 1 08/30/2018 21:48 WG1159831
Hexachloro-1,3-butadiene U 0.0161 0.0317 1 08/30/2018 21:48 WG1159831
Isopropylbenzene U 0.00109 0.00317 1 08/30/2018 21:48 WG1159831
p-Isopropyltoluene U 0.00295 0.00633 1 08/30/2018 21:48 WG1159831
2-Butanone (MEK)U 0.0158 0.0317 1 08/30/2018 21:48 WG1159831
Methylene Chloride U 0.00841 0.0317 1 08/30/2018 21:48 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0127 0.0317 1 08/30/2018 21:48 WG1159831
Methyl tert-butyl ether U 0.000374 0.00127 1 08/30/2018 21:48 WG1159831
Naphthalene 0.0307 0.00395 0.0158 1 08/30/2018 21:48 WG1159831
n-Propylbenzene U 0.00149 0.00633 1 08/30/2018 21:48 WG1159831
Styrene U 0.00346 0.0158 1 08/30/2018 21:48 WG1159831
1,1,1,2-Tetrachloroethane U 0.000633 0.00317 1 08/30/2018 21:48 WG1159831
1,1,2,2-Tetrachloroethane U 0.000494 0.00317 1 08/30/2018 21:48 WG1159831
Tetrachloroethene 0.00593 0.000887 0.00317 1 08/30/2018 21:48 WG1159831
Toluene 0.00934 0.00158 0.00633 1 08/30/2018 21:48 WG1159831
1,2,3-Trichlorobenzene U 0.000792 0.00317 1 08/30/2018 21:48 WG1159831
1,2,4-Trichlorobenzene U 0.00611 0.0158 1 08/30/2018 21:48 WG1159831
1,1,1-Trichloroethane U 0.000348 0.00317 1 08/30/2018 21:48 WG1159831
1,1,2-Trichloroethane U 0.00112 0.00317 1 08/30/2018 21:48 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000855 0.00317 1 08/30/2018 21:48 WG1159831
Trichloroethene U 0.000507 0.00127 1 08/30/2018 21:48 WG1159831
Trichlorofluoromethane U 0.000633 0.00317 1 08/30/2018 21:48 WG1159831
1,2,3-Trichloropropane U 0.00646 0.0158 1 08/30/2018 21:48 WG1159831
1,2,4-Trimethylbenzene 0.00463 B J 0.00147 0.00633 1 08/30/2018 21:48 WG1159831
1,3,5-Trimethylbenzene U 0.00137 0.00633 1 08/30/2018 21:48 WG1159831
Vinyl chloride U 0.000865 0.00317 1 08/30/2018 21:48 WG1159831
Xylenes, Total 0.0117 B 0.00606 0.00823 1 08/30/2018 21:48 WG1159831
(S) Toluene-d8 107 75.0-131 08/30/2018 21:48 WG1159831
(S) Dibromofluoromethane 101 65.0-129 08/30/2018 21:48 WG1159831
(S) 4-Bromofluorobenzene 105 67.0-138 08/30/2018 21:48 WG1159831
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.331 0.0407 0.209 5 09/03/2018 09:27 WG1159283
Acenaphthylene 0.441 0.0424 0.209 5 09/03/2018 09:27 WG1159283
Anthracene 1.15 0.0400 0.209 5 09/03/2018 09:27 WG1159283
Benzidine U J4 0.404 2.12 5 09/03/2018 09:27 WG1159283
Benzo(a)anthracene 3.50 0.0271 0.209 5 09/03/2018 09:27 WG1159283
Benzo(b)fluoranthene 4.04 0.0440 0.209 5 09/03/2018 09:27 WG1159283
Benzo(k)fluoranthene 1.49 0.0369 0.209 5 09/03/2018 09:27 WG1159283
Benzo(g,h,i)perylene 1.10 0.0457 0.209 5 09/03/2018 09:27 WG1159283
Benzo(a)pyrene 2.91 0.0347 0.209 5 09/03/2018 09:27 WG1159283
Bis(2-chlorethoxy)methane U 0.0488 2.12 5 09/03/2018 09:27 WG1159283
Bis(2-chloroethyl)ether U 0.0568 2.12 5 09/03/2018 09:27 WG1159283
Bis(2-chloroisopropyl)ether U 0.0481 2.12 5 09/03/2018 09:27 WG1159283
4-Bromophenyl-phenylether U 0.0722 2.12 5 09/03/2018 09:27 WG1159283
2-Chloronaphthalene U 0.0405 0.209 5 09/03/2018 09:27 WG1159283
4-Chlorophenyl-phenylether U 0.0398 2.12 5 09/03/2018 09:27 WG1159283
Chrysene 3.33 0.0352 0.209 5 09/03/2018 09:27 WG1159283
Dibenz(a,h)anthracene 0.837 0.0521 0.209 5 09/03/2018 09:27 WG1159283
3,3-Dichlorobenzidine U 0.503 2.12 5 09/03/2018 09:27 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1020964
SWP-1 1-4
Collected date/time: 08/24/18 09:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
2,4-Dinitrotoluene U 0.0385 2.12 5 09/03/2018 09:27 WG1159283
2,6-Dinitrotoluene U 0.0467 2.12 5 09/03/2018 09:27 WG1159283
Fluoranthene 7.39 0.0314 0.209 5 09/03/2018 09:27 WG1159283
Fluorene 0.338 0.0432 0.209 5 09/03/2018 09:27 WG1159283
Hexachlorobenzene U 0.0542 2.12 5 09/03/2018 09:27 WG1159283
Hexachloro-1,3-butadiene U 0.0633 2.12 5 09/03/2018 09:27 WG1159283
Hexachlorocyclopentadiene U 0.371 2.12 5 09/03/2018 09:27 WG1159283
Hexachloroethane U 0.0849 2.12 5 09/03/2018 09:27 WG1159283
Indeno(1,2,3-cd)pyrene 7.37 0.0489 0.209 5 09/03/2018 09:27 WG1159283
Isophorone U 0.0331 2.12 5 09/03/2018 09:27 WG1159283
Naphthalene 0.365 0.0564 0.209 5 09/03/2018 09:27 WG1159283
Nitrobenzene U 0.0440 2.12 5 09/03/2018 09:27 WG1159283
n-Nitrosodimethylamine U 0.409 2.12 5 09/03/2018 09:27 WG1159283
n-Nitrosodiphenylamine U 0.570 2.12 5 09/03/2018 09:27 WG1159283
n-Nitrosodi-n-propylamine U 0.0574 2.12 5 09/03/2018 09:27 WG1159283
Phenanthrene 4.50 0.0334 0.209 5 09/03/2018 09:27 WG1159283
Benzylbutyl phthalate U 0.0652 2.12 5 09/03/2018 09:27 WG1159283
Bis(2-ethylhexyl)phthalate 0.123 J 0.0760 2.12 5 09/03/2018 09:27 WG1159283
Di-n-butyl phthalate U 0.0690 2.12 5 09/03/2018 09:27 WG1159283
Diethyl phthalate U 0.0438 2.12 5 09/03/2018 09:27 WG1159283
Dimethyl phthalate U 0.0342 2.12 5 09/03/2018 09:27 WG1159283
Di-n-octyl phthalate U 0.0575 2.12 5 09/03/2018 09:27 WG1159283
Pyrene 6.38 0.0779 0.209 5 09/03/2018 09:27 WG1159283
1,2,4-Trichlorobenzene U 0.0555 2.12 5 09/03/2018 09:27 WG1159283
4-Chloro-3-methylphenol U 0.0303 2.12 5 09/03/2018 09:27 WG1159283
2-Chlorophenol U 0.0526 2.12 5 09/03/2018 09:27 WG1159283
2,4-Dichlorophenol U 0.0473 2.12 5 09/03/2018 09:27 WG1159283
2,4-Dimethylphenol U 0.299 2.12 5 09/03/2018 09:27 WG1159283
4,6-Dinitro-2-methylphenol U 0.785 2.12 5 09/03/2018 09:27 WG1159283
2,4-Dinitrophenol U 0.621 2.12 5 09/03/2018 09:27 WG1159283
2-Nitrophenol U 0.0823 2.12 5 09/03/2018 09:27 WG1159283
4-Nitrophenol U 0.333 2.12 5 09/03/2018 09:27 WG1159283
Pentachlorophenol U 0.304 2.12 5 09/03/2018 09:27 WG1159283
Phenol U 0.0440 2.12 5 09/03/2018 09:27 WG1159283
2,4,6-Trichlorophenol U 0.0493 2.12 5 09/03/2018 09:27 WG1159283
(S) 2-Fluorophenol 66.6 12.0-120 09/03/2018 09:27 WG1159283
(S) Phenol-d5 58.3 10.0-120 09/03/2018 09:27 WG1159283
(S) Nitrobenzene-d5 52.8 10.0-122 09/03/2018 09:27 WG1159283
(S) 2-Fluorobiphenyl 68.4 15.0-120 09/03/2018 09:27 WG1159283
(S) 2,4,6-Tribromophenol 76.8 10.0-127 09/03/2018 09:27 WG1159283
(S) p-Terphenyl-d14 63.5 10.0-120 09/03/2018 09:27 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 10 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 10 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1020964
SWP-1 15-20
Collected date/time: 08/24/18 09:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 76.7 1 08/31/2018 10:44 WG1159443
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.113 0.00365 0.0261 1 08/31/2018 11:44 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 1.73 J 0.599 2.61 1 08/31/2018 14:59 WG1159261
Barium 85.8 0.222 0.652 1 08/31/2018 14:59 WG1159261
Cadmium 0.0961 J 0.0912 0.652 1 08/31/2018 14:59 WG1159261
Chromium 18.1 0.182 1.30 1 08/31/2018 14:59 WG1159261
Lead 42.8 0.248 0.652 1 08/31/2018 14:59 WG1159261
Selenium U 0.808 2.61 1 08/31/2018 14:59 WG1159261
Silver U 0.156 1.30 1 08/31/2018 14:59 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0179 0.0326 1 08/30/2018 22:08 WG1159831
Acrylonitrile U 0.00248 0.0163 1 08/30/2018 22:08 WG1159831
Benzene U 0.000521 0.00130 1 08/30/2018 22:08 WG1159831
Bromobenzene U 0.00137 0.0163 1 08/30/2018 22:08 WG1159831
Bromodichloromethane U 0.00103 0.00326 1 08/30/2018 22:08 WG1159831
Bromoform U 0.00779 0.0326 1 08/30/2018 22:08 WG1159831
Bromomethane U 0.00482 0.0163 1 08/30/2018 22:08 WG1159831
n-Butylbenzene U J4 0.00500 0.0163 1 08/30/2018 22:08 WG1159831
sec-Butylbenzene U 0.00330 0.0163 1 08/30/2018 22:08 WG1159831
tert-Butylbenzene U 0.00202 0.00652 1 08/30/2018 22:08 WG1159831
Carbon tetrachloride U 0.00141 0.00652 1 08/30/2018 22:08 WG1159831
Chlorobenzene U 0.000747 0.00326 1 08/30/2018 22:08 WG1159831
Chlorodibromomethane U 0.000586 0.00326 1 08/30/2018 22:08 WG1159831
Chloroethane U 0.00141 0.00652 1 08/30/2018 22:08 WG1159831
Chloroform U 0.000541 0.00326 1 08/30/2018 22:08 WG1159831
Chloromethane U 0.00181 0.0163 1 08/30/2018 22:08 WG1159831
2-Chlorotoluene U 0.00120 0.00326 1 08/30/2018 22:08 WG1159831
4-Chlorotoluene U 0.00147 0.00652 1 08/30/2018 22:08 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00665 0.0326 1 08/30/2018 22:08 WG1159831
1,2-Dibromoethane U 0.000684 0.00326 1 08/30/2018 22:08 WG1159831
Dibromomethane U 0.00130 0.00652 1 08/30/2018 22:08 WG1159831
1,2-Dichlorobenzene U 0.00189 0.00652 1 08/30/2018 22:08 WG1159831
1,3-Dichlorobenzene U 0.00222 0.00652 1 08/30/2018 22:08 WG1159831
1,4-Dichlorobenzene U 0.00257 0.00652 1 08/30/2018 22:08 WG1159831
Dichlorodifluoromethane U 0.00107 0.00326 1 08/30/2018 22:08 WG1159831
1,1-Dichloroethane U 0.000749 0.00326 1 08/30/2018 22:08 WG1159831
1,2-Dichloroethane U 0.000619 0.00326 1 08/30/2018 22:08 WG1159831
1,1-Dichloroethene U 0.000652 0.00326 1 08/30/2018 22:08 WG1159831
cis-1,2-Dichloroethene U 0.000899 0.00326 1 08/30/2018 22:08 WG1159831
trans-1,2-Dichloroethene U 0.00186 0.00652 1 08/30/2018 22:08 WG1159831
1,2-Dichloropropane U 0.00166 0.00652 1 08/30/2018 22:08 WG1159831
1,1-Dichloropropene U 0.000912 0.00326 1 08/30/2018 22:08 WG1159831
1,3-Dichloropropane U 0.00228 0.00652 1 08/30/2018 22:08 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 11 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 11 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1020964
SWP-1 15-20
Collected date/time: 08/24/18 09:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000884 0.00326 1 08/30/2018 22:08 WG1159831
trans-1,3-Dichloropropene U 0.00199 0.00652 1 08/30/2018 22:08 WG1159831
2,2-Dichloropropane U 0.00103 0.00326 1 08/30/2018 22:08 WG1159831
Di-isopropyl ether 0.00680 0.000456 0.00130 1 08/30/2018 22:08 WG1159831
Ethylbenzene 0.00200 J 0.000691 0.00326 1 08/30/2018 22:08 WG1159831
Hexachloro-1,3-butadiene U 0.0166 0.0326 1 08/30/2018 22:08 WG1159831
Isopropylbenzene U 0.00112 0.00326 1 08/30/2018 22:08 WG1159831
p-Isopropyltoluene U 0.00304 0.00652 1 08/30/2018 22:08 WG1159831
2-Butanone (MEK)U 0.0163 0.0326 1 08/30/2018 22:08 WG1159831
Methylene Chloride U 0.00865 0.0326 1 08/30/2018 22:08 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0130 0.0326 1 08/30/2018 22:08 WG1159831
Methyl tert-butyl ether U 0.000384 0.00130 1 08/30/2018 22:08 WG1159831
Naphthalene 0.0414 0.00407 0.0163 1 08/30/2018 22:08 WG1159831
n-Propylbenzene U 0.00154 0.00652 1 08/30/2018 22:08 WG1159831
Styrene U 0.00356 0.0163 1 08/30/2018 22:08 WG1159831
1,1,1,2-Tetrachloroethane U 0.000652 0.00326 1 08/30/2018 22:08 WG1159831
1,1,2,2-Tetrachloroethane U 0.000508 0.00326 1 08/30/2018 22:08 WG1159831
Tetrachloroethene U 0.000912 0.00326 1 08/30/2018 22:08 WG1159831
Toluene 0.0129 0.00163 0.00652 1 08/30/2018 22:08 WG1159831
1,2,3-Trichlorobenzene U 0.000814 0.00326 1 08/30/2018 22:08 WG1159831
1,2,4-Trichlorobenzene U 0.00628 0.0163 1 08/30/2018 22:08 WG1159831
1,1,1-Trichloroethane U 0.000358 0.00326 1 08/30/2018 22:08 WG1159831
1,1,2-Trichloroethane U 0.00115 0.00326 1 08/30/2018 22:08 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000880 0.00326 1 08/30/2018 22:08 WG1159831
Trichloroethene U 0.000521 0.00130 1 08/30/2018 22:08 WG1159831
Trichlorofluoromethane U 0.000652 0.00326 1 08/30/2018 22:08 WG1159831
1,2,3-Trichloropropane U 0.00665 0.0163 1 08/30/2018 22:08 WG1159831
1,2,4-Trimethylbenzene 0.00503 B J 0.00151 0.00652 1 08/30/2018 22:08 WG1159831
1,3,5-Trimethylbenzene U 0.00141 0.00652 1 08/30/2018 22:08 WG1159831
Vinyl chloride U 0.000890 0.00326 1 08/30/2018 22:08 WG1159831
Xylenes, Total 0.0111 B 0.00623 0.00847 1 08/30/2018 22:08 WG1159831
(S) Toluene-d8 80.5 75.0-131 08/30/2018 22:08 WG1159831
(S) Dibromofluoromethane 100 65.0-129 08/30/2018 22:08 WG1159831
(S) 4-Bromofluorobenzene 105 67.0-138 08/30/2018 22:08 WG1159831
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.100 0.00837 0.0430 1 09/03/2018 06:20 WG1159283
Acenaphthylene 0.0225 J 0.00874 0.0430 1 09/03/2018 06:20 WG1159283
Anthracene 0.128 0.00824 0.0430 1 09/03/2018 06:20 WG1159283
Benzidine U J4 0.0830 0.434 1 09/03/2018 06:20 WG1159283
Benzo(a)anthracene 0.384 0.00558 0.0430 1 09/03/2018 06:20 WG1159283
Benzo(b)fluoranthene 0.474 0.00906 0.0430 1 09/03/2018 06:20 WG1159283
Benzo(k)fluoranthene 0.185 0.00758 0.0430 1 09/03/2018 06:20 WG1159283
Benzo(g,h,i)perylene 0.287 0.00940 0.0430 1 09/03/2018 06:20 WG1159283
Benzo(a)pyrene 0.371 0.00714 0.0430 1 09/03/2018 06:20 WG1159283
Bis(2-chlorethoxy)methane U 0.0100 0.434 1 09/03/2018 06:20 WG1159283
Bis(2-chloroethyl)ether U 0.0117 0.434 1 09/03/2018 06:20 WG1159283
Bis(2-chloroisopropyl)ether U 0.00990 0.434 1 09/03/2018 06:20 WG1159283
4-Bromophenyl-phenylether U 0.0149 0.434 1 09/03/2018 06:20 WG1159283
2-Chloronaphthalene U 0.00833 0.0430 1 09/03/2018 06:20 WG1159283
4-Chlorophenyl-phenylether U 0.00817 0.434 1 09/03/2018 06:20 WG1159283
Chrysene 0.392 0.00723 0.0430 1 09/03/2018 06:20 WG1159283
Dibenz(a,h)anthracene 0.714 0.0107 0.0430 1 09/03/2018 06:20 WG1159283
3,3-Dichlorobenzidine U 0.103 0.434 1 09/03/2018 06:20 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 12 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 12 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1020964
SWP-1 15-20
Collected date/time: 08/24/18 09:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
2,4-Dinitrotoluene U 0.00791 0.434 1 09/03/2018 06:20 WG1159283
2,6-Dinitrotoluene U 0.00960 0.434 1 09/03/2018 06:20 WG1159283
Fluoranthene 0.774 0.00646 0.0430 1 09/03/2018 06:20 WG1159283
Fluorene 0.0715 0.00889 0.0430 1 09/03/2018 06:20 WG1159283
Hexachlorobenzene U 0.0112 0.434 1 09/03/2018 06:20 WG1159283
Hexachloro-1,3-butadiene U 0.0130 0.434 1 09/03/2018 06:20 WG1159283
Hexachlorocyclopentadiene U 0.0765 0.434 1 09/03/2018 06:20 WG1159283
Hexachloroethane U 0.0175 0.434 1 09/03/2018 06:20 WG1159283
Indeno(1,2,3-cd)pyrene 7.65 0.0101 0.0430 1 09/03/2018 06:20 WG1159283
Isophorone U 0.00680 0.434 1 09/03/2018 06:20 WG1159283
Naphthalene 0.151 0.0116 0.0430 1 09/03/2018 06:20 WG1159283
Nitrobenzene U 0.00906 0.434 1 09/03/2018 06:20 WG1159283
n-Nitrosodimethylamine U 0.0843 0.434 1 09/03/2018 06:20 WG1159283
n-Nitrosodiphenylamine U 0.117 0.434 1 09/03/2018 06:20 WG1159283
n-Nitrosodi-n-propylamine U 0.0118 0.434 1 09/03/2018 06:20 WG1159283
Phenanthrene 0.540 0.00688 0.0430 1 09/03/2018 06:20 WG1159283
Benzylbutyl phthalate U 0.0134 0.434 1 09/03/2018 06:20 WG1159283
Bis(2-ethylhexyl)phthalate U 0.0156 0.434 1 09/03/2018 06:20 WG1159283
Di-n-butyl phthalate U 0.0142 0.434 1 09/03/2018 06:20 WG1159283
Diethyl phthalate U 0.00900 0.434 1 09/03/2018 06:20 WG1159283
Dimethyl phthalate U 0.00704 0.434 1 09/03/2018 06:20 WG1159283
Di-n-octyl phthalate U 0.0118 0.434 1 09/03/2018 06:20 WG1159283
Pyrene 0.637 0.0160 0.0430 1 09/03/2018 06:20 WG1159283
1,2,4-Trichlorobenzene U 0.0114 0.434 1 09/03/2018 06:20 WG1159283
4-Chloro-3-methylphenol U 0.00622 0.434 1 09/03/2018 06:20 WG1159283
2-Chlorophenol U 0.0108 0.434 1 09/03/2018 06:20 WG1159283
2,4-Dichlorophenol U 0.00972 0.434 1 09/03/2018 06:20 WG1159283
2,4-Dimethylphenol U 0.0614 0.434 1 09/03/2018 06:20 WG1159283
4,6-Dinitro-2-methylphenol U 0.162 0.434 1 09/03/2018 06:20 WG1159283
2,4-Dinitrophenol U 0.128 0.434 1 09/03/2018 06:20 WG1159283
2-Nitrophenol U 0.0169 0.434 1 09/03/2018 06:20 WG1159283
4-Nitrophenol U 0.0684 0.434 1 09/03/2018 06:20 WG1159283
Pentachlorophenol U 0.0626 0.434 1 09/03/2018 06:20 WG1159283
Phenol U 0.00906 0.434 1 09/03/2018 06:20 WG1159283
2,4,6-Trichlorophenol U 0.0102 0.434 1 09/03/2018 06:20 WG1159283
(S) 2-Fluorophenol 72.2 12.0-120 09/03/2018 06:20 WG1159283
(S) Phenol-d5 63.4 10.0-120 09/03/2018 06:20 WG1159283
(S) Nitrobenzene-d5 61.1 10.0-122 09/03/2018 06:20 WG1159283
(S) 2-Fluorobiphenyl 71.9 15.0-120 09/03/2018 06:20 WG1159283
(S) 2,4,6-Tribromophenol 87.7 10.0-127 09/03/2018 06:20 WG1159283
(S) p-Terphenyl-d14 66.4 10.0-120 09/03/2018 06:20 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 13 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 13 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1020964
SWP-2 1-5
Collected date/time: 08/24/18 09:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.5 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0550 B 0.00344 0.0246 1 08/31/2018 11:47 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 1.62 J 0.565 2.46 1 08/31/2018 15:07 WG1159261
Barium 59.9 0.209 0.614 1 08/31/2018 15:07 WG1159261
Cadmium U 0.0859 0.614 1 08/31/2018 15:07 WG1159261
Chromium 14.4 0.172 1.23 1 08/31/2018 15:07 WG1159261
Lead 22.6 0.233 0.614 1 08/31/2018 15:07 WG1159261
Selenium U 0.761 2.46 1 08/31/2018 15:07 WG1159261
Silver U 0.147 1.23 1 08/31/2018 15:07 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0168 0.0307 1 08/30/2018 22:28 WG1159831
Acrylonitrile U 0.00233 0.0153 1 08/30/2018 22:28 WG1159831
Benzene U 0.000491 0.00123 1 08/30/2018 22:28 WG1159831
Bromobenzene U 0.00129 0.0153 1 08/30/2018 22:28 WG1159831
Bromodichloromethane U 0.000967 0.00307 1 08/30/2018 22:28 WG1159831
Bromoform U 0.00734 0.0307 1 08/30/2018 22:28 WG1159831
Bromomethane U 0.00454 0.0153 1 08/30/2018 22:28 WG1159831
n-Butylbenzene U J4 0.00471 0.0153 1 08/30/2018 22:28 WG1159831
sec-Butylbenzene U 0.00311 0.0153 1 08/30/2018 22:28 WG1159831
tert-Butylbenzene U 0.00190 0.00614 1 08/30/2018 22:28 WG1159831
Carbon tetrachloride U 0.00133 0.00614 1 08/30/2018 22:28 WG1159831
Chlorobenzene U 0.000703 0.00307 1 08/30/2018 22:28 WG1159831
Chlorodibromomethane U 0.000552 0.00307 1 08/30/2018 22:28 WG1159831
Chloroethane U 0.00133 0.00614 1 08/30/2018 22:28 WG1159831
Chloroform U 0.000510 0.00307 1 08/30/2018 22:28 WG1159831
Chloromethane U 0.00171 0.0153 1 08/30/2018 22:28 WG1159831
2-Chlorotoluene U 0.00113 0.00307 1 08/30/2018 22:28 WG1159831
4-Chlorotoluene U 0.00139 0.00614 1 08/30/2018 22:28 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00626 0.0307 1 08/30/2018 22:28 WG1159831
1,2-Dibromoethane U 0.000645 0.00307 1 08/30/2018 22:28 WG1159831
Dibromomethane U 0.00123 0.00614 1 08/30/2018 22:28 WG1159831
1,2-Dichlorobenzene U 0.00178 0.00614 1 08/30/2018 22:28 WG1159831
1,3-Dichlorobenzene U 0.00209 0.00614 1 08/30/2018 22:28 WG1159831
1,4-Dichlorobenzene U 0.00242 0.00614 1 08/30/2018 22:28 WG1159831
Dichlorodifluoromethane U 0.00100 0.00307 1 08/30/2018 22:28 WG1159831
1,1-Dichloroethane U 0.000706 0.00307 1 08/30/2018 22:28 WG1159831
1,2-Dichloroethane U 0.000583 0.00307 1 08/30/2018 22:28 WG1159831
1,1-Dichloroethene U 0.000614 0.00307 1 08/30/2018 22:28 WG1159831
cis-1,2-Dichloroethene U 0.000847 0.00307 1 08/30/2018 22:28 WG1159831
trans-1,2-Dichloroethene U 0.00176 0.00614 1 08/30/2018 22:28 WG1159831
1,2-Dichloropropane U 0.00156 0.00614 1 08/30/2018 22:28 WG1159831
1,1-Dichloropropene U 0.000859 0.00307 1 08/30/2018 22:28 WG1159831
1,3-Dichloropropane U 0.00215 0.00614 1 08/30/2018 22:28 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 14 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1020964
SWP-2 1-5
Collected date/time: 08/24/18 09:30
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000832 0.00307 1 08/30/2018 22:28 WG1159831
trans-1,3-Dichloropropene U 0.00188 0.00614 1 08/30/2018 22:28 WG1159831
2,2-Dichloropropane U 0.000974 0.00307 1 08/30/2018 22:28 WG1159831
Di-isopropyl ether U 0.000430 0.00123 1 08/30/2018 22:28 WG1159831
Ethylbenzene U 0.000651 0.00307 1 08/30/2018 22:28 WG1159831
Hexachloro-1,3-butadiene U 0.0156 0.0307 1 08/30/2018 22:28 WG1159831
Isopropylbenzene U 0.00106 0.00307 1 08/30/2018 22:28 WG1159831
p-Isopropyltoluene U 0.00286 0.00614 1 08/30/2018 22:28 WG1159831
2-Butanone (MEK)U 0.0153 0.0307 1 08/30/2018 22:28 WG1159831
Methylene Chloride U 0.00815 0.0307 1 08/30/2018 22:28 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0123 0.0307 1 08/30/2018 22:28 WG1159831
Methyl tert-butyl ether U 0.000362 0.00123 1 08/30/2018 22:28 WG1159831
Naphthalene 0.0122 J 0.00383 0.0153 1 08/30/2018 22:28 WG1159831
n-Propylbenzene U 0.00145 0.00614 1 08/30/2018 22:28 WG1159831
Styrene U 0.00335 0.0153 1 08/30/2018 22:28 WG1159831
1,1,1,2-Tetrachloroethane U 0.000614 0.00307 1 08/30/2018 22:28 WG1159831
1,1,2,2-Tetrachloroethane U 0.000479 0.00307 1 08/30/2018 22:28 WG1159831
Tetrachloroethene U 0.000859 0.00307 1 08/30/2018 22:28 WG1159831
Toluene 0.00168 J 0.00153 0.00614 1 08/30/2018 22:28 WG1159831
1,2,3-Trichlorobenzene U 0.000767 0.00307 1 08/30/2018 22:28 WG1159831
1,2,4-Trichlorobenzene U 0.00592 0.0153 1 08/30/2018 22:28 WG1159831
1,1,1-Trichloroethane U 0.000338 0.00307 1 08/30/2018 22:28 WG1159831
1,1,2-Trichloroethane U 0.00108 0.00307 1 08/30/2018 22:28 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000829 0.00307 1 08/30/2018 22:28 WG1159831
Trichloroethene U 0.000491 0.00123 1 08/30/2018 22:28 WG1159831
Trichlorofluoromethane U 0.000614 0.00307 1 08/30/2018 22:28 WG1159831
1,2,3-Trichloropropane U 0.00626 0.0153 1 08/30/2018 22:28 WG1159831
1,2,4-Trimethylbenzene 0.00247 B J 0.00142 0.00614 1 08/30/2018 22:28 WG1159831
1,3,5-Trimethylbenzene U 0.00133 0.00614 1 08/30/2018 22:28 WG1159831
Vinyl chloride U 0.000839 0.00307 1 08/30/2018 22:28 WG1159831
Xylenes, Total U B 0.00587 0.00798 1 08/30/2018 22:28 WG1159831
(S) Toluene-d8 104 75.0-131 08/30/2018 22:28 WG1159831
(S) Dibromofluoromethane 102 65.0-129 08/30/2018 22:28 WG1159831
(S) 4-Bromofluorobenzene 106 67.0-138 08/30/2018 22:28 WG1159831
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00788 0.0405 1 09/03/2018 06:43 WG1159283
Acenaphthylene 0.0578 0.00824 0.0405 1 09/03/2018 06:43 WG1159283
Anthracene 0.222 0.00776 0.0405 1 09/03/2018 06:43 WG1159283
Benzidine U J4 0.0782 0.409 1 09/03/2018 06:43 WG1159283
Benzo(a)anthracene 1.13 0.00525 0.0405 1 09/03/2018 06:43 WG1159283
Benzo(b)fluoranthene 1.26 0.00853 0.0405 1 09/03/2018 06:43 WG1159283
Benzo(k)fluoranthene 0.471 0.00715 0.0405 1 09/03/2018 06:43 WG1159283
Benzo(g,h,i)perylene 0.724 0.00885 0.0405 1 09/03/2018 06:43 WG1159283
Benzo(a)pyrene 1.03 0.00673 0.0405 1 09/03/2018 06:43 WG1159283
Bis(2-chlorethoxy)methane U 0.00945 0.409 1 09/03/2018 06:43 WG1159283
Bis(2-chloroethyl)ether U 0.0110 0.409 1 09/03/2018 06:43 WG1159283
Bis(2-chloroisopropyl)ether U 0.00933 0.409 1 09/03/2018 06:43 WG1159283
4-Bromophenyl-phenylether U 0.0140 0.409 1 09/03/2018 06:43 WG1159283
2-Chloronaphthalene U 0.00785 0.0405 1 09/03/2018 06:43 WG1159283
4-Chlorophenyl-phenylether U 0.00770 0.409 1 09/03/2018 06:43 WG1159283
Chrysene 1.07 0.00681 0.0405 1 09/03/2018 06:43 WG1159283
Dibenz(a,h)anthracene 1.84 0.0101 0.0405 1 09/03/2018 06:43 WG1159283
3,3-Dichlorobenzidine U 0.0975 0.409 1 09/03/2018 06:43 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 15 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1020964
SWP-2 1-5
Collected date/time: 08/24/18 09:30
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
2,4-Dinitrotoluene U 0.00745 0.409 1 09/03/2018 06:43 WG1159283
2,6-Dinitrotoluene U 0.00905 0.409 1 09/03/2018 06:43 WG1159283
Fluoranthene 2.52 0.0304 0.203 5 09/04/2018 16:01 WG1159283
Fluorene 0.0201 J 0.00837 0.0405 1 09/03/2018 06:43 WG1159283
Hexachlorobenzene U 0.0105 0.409 1 09/03/2018 06:43 WG1159283
Hexachloro-1,3-butadiene U 0.0123 0.409 1 09/03/2018 06:43 WG1159283
Hexachlorocyclopentadiene U 0.0721 0.409 1 09/03/2018 06:43 WG1159283
Hexachloroethane U 0.0165 0.409 1 09/03/2018 06:43 WG1159283
Indeno(1,2,3-cd)pyrene 19.2 0.00948 0.0405 1 09/03/2018 06:43 WG1159283
Isophorone U 0.00641 0.409 1 09/03/2018 06:43 WG1159283
Naphthalene 0.0248 J 0.0109 0.0405 1 09/03/2018 06:43 WG1159283
Nitrobenzene U 0.00853 0.409 1 09/03/2018 06:43 WG1159283
n-Nitrosodimethylamine U 0.0794 0.409 1 09/03/2018 06:43 WG1159283
n-Nitrosodiphenylamine U 0.110 0.409 1 09/03/2018 06:43 WG1159283
n-Nitrosodi-n-propylamine U 0.0111 0.409 1 09/03/2018 06:43 WG1159283
Phenanthrene 0.670 0.00648 0.0405 1 09/03/2018 06:43 WG1159283
Benzylbutyl phthalate 0.0333 J 0.0126 0.409 1 09/03/2018 06:43 WG1159283
Bis(2-ethylhexyl)phthalate 0.0157 J 0.0147 0.409 1 09/03/2018 06:43 WG1159283
Di-n-butyl phthalate U 0.0134 0.409 1 09/03/2018 06:43 WG1159283
Diethyl phthalate U 0.00848 0.409 1 09/03/2018 06:43 WG1159283
Dimethyl phthalate U 0.00663 0.409 1 09/03/2018 06:43 WG1159283
Di-n-octyl phthalate U 0.0111 0.409 1 09/03/2018 06:43 WG1159283
Pyrene 2.26 0.0755 0.203 5 09/04/2018 16:01 WG1159283
1,2,4-Trichlorobenzene U 0.0108 0.409 1 09/03/2018 06:43 WG1159283
4-Chloro-3-methylphenol U 0.00586 0.409 1 09/03/2018 06:43 WG1159283
2-Chlorophenol U 0.0102 0.409 1 09/03/2018 06:43 WG1159283
2,4-Dichlorophenol U 0.00916 0.409 1 09/03/2018 06:43 WG1159283
2,4-Dimethylphenol U 0.0578 0.409 1 09/03/2018 06:43 WG1159283
4,6-Dinitro-2-methylphenol U 0.152 0.409 1 09/03/2018 06:43 WG1159283
2,4-Dinitrophenol U 0.120 0.409 1 09/03/2018 06:43 WG1159283
2-Nitrophenol U 0.0160 0.409 1 09/03/2018 06:43 WG1159283
4-Nitrophenol U 0.0645 0.409 1 09/03/2018 06:43 WG1159283
Pentachlorophenol U 0.0589 0.409 1 09/03/2018 06:43 WG1159283
Phenol U 0.00853 0.409 1 09/03/2018 06:43 WG1159283
2,4,6-Trichlorophenol U 0.00956 0.409 1 09/03/2018 06:43 WG1159283
(S) 2-Fluorophenol 70.3 12.0-120 09/04/2018 16:01 WG1159283
(S) 2-Fluorophenol 73.8 12.0-120 09/03/2018 06:43 WG1159283
(S) Phenol-d5 65.4 10.0-120 09/03/2018 06:43 WG1159283
(S) Phenol-d5 60.2 10.0-120 09/04/2018 16:01 WG1159283
(S) Nitrobenzene-d5 58.2 10.0-122 09/04/2018 16:01 WG1159283
(S) Nitrobenzene-d5 63.7 10.0-122 09/03/2018 06:43 WG1159283
(S) 2-Fluorobiphenyl 75.9 15.0-120 09/03/2018 06:43 WG1159283
(S) 2-Fluorobiphenyl 62.2 15.0-120 09/04/2018 16:01 WG1159283
(S) 2,4,6-Tribromophenol 93.1 10.0-127 09/03/2018 06:43 WG1159283
(S) 2,4,6-Tribromophenol 70.1 10.0-127 09/04/2018 16:01 WG1159283
(S) p-Terphenyl-d14 78.4 10.0-120 09/03/2018 06:43 WG1159283
(S) p-Terphenyl-d14 66.5 10.0-120 09/04/2018 16:01 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 16 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 16 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1020964
SWP-2 15-20
Collected date/time: 08/24/18 09:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.1 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0465 B 0.00354 0.0253 1 08/31/2018 11:49 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 1.90 J 0.581 2.53 1 08/31/2018 15:10 WG1159261
Barium 61.2 0.215 0.632 1 08/31/2018 15:10 WG1159261
Cadmium 0.201 J 0.0885 0.632 1 08/31/2018 15:10 WG1159261
Chromium 14.6 0.177 1.26 1 08/31/2018 15:10 WG1159261
Lead 55.7 0.240 0.632 1 08/31/2018 15:10 WG1159261
Selenium U 0.784 2.53 1 08/31/2018 15:10 WG1159261
Silver U 0.152 1.26 1 08/31/2018 15:10 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0173 0.0316 1 08/30/2018 22:48 WG1159831
Acrylonitrile U 0.00240 0.0158 1 08/30/2018 22:48 WG1159831
Benzene 0.0569 0.000506 0.00126 1 08/30/2018 22:48 WG1159831
Bromobenzene U 0.00133 0.0158 1 08/30/2018 22:48 WG1159831
Bromodichloromethane U 0.000996 0.00316 1 08/30/2018 22:48 WG1159831
Bromoform U 0.00756 0.0316 1 08/30/2018 22:48 WG1159831
Bromomethane U 0.00468 0.0158 1 08/30/2018 22:48 WG1159831
n-Butylbenzene U J4 0.00485 0.0158 1 08/30/2018 22:48 WG1159831
sec-Butylbenzene 0.0312 B 0.00320 0.0158 1 08/30/2018 22:48 WG1159831
tert-Butylbenzene U 0.00196 0.00632 1 08/30/2018 22:48 WG1159831
Carbon tetrachloride U 0.00137 0.00632 1 08/30/2018 22:48 WG1159831
Chlorobenzene 0.468 0.0289 0.126 40 08/31/2018 21:21 WG1160083
Chlorodibromomethane U 0.0228 0.126 40 08/31/2018 21:21 WG1160083
Chloroethane U 0.00137 0.00632 1 08/30/2018 22:48 WG1159831
Chloroform U 0.000525 0.00316 1 08/30/2018 22:48 WG1159831
Chloromethane U 0.00176 0.0158 1 08/30/2018 22:48 WG1159831
2-Chlorotoluene U 0.00116 0.00316 1 08/30/2018 22:48 WG1159831
4-Chlorotoluene U 0.00143 0.00632 1 08/30/2018 22:48 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00645 0.0316 1 08/30/2018 22:48 WG1159831
1,2-Dibromoethane U 0.0265 0.126 40 08/31/2018 21:21 WG1160083
Dibromomethane U 0.00126 0.00632 1 08/30/2018 22:48 WG1159831
1,2-Dichlorobenzene U 0.00183 0.00632 1 08/30/2018 22:48 WG1159831
1,3-Dichlorobenzene 0.182 0.00215 0.00632 1 08/30/2018 22:48 WG1159831
1,4-Dichlorobenzene 0.237 0.00249 0.00632 1 08/30/2018 22:48 WG1159831
Dichlorodifluoromethane U 0.00103 0.00316 1 08/30/2018 22:48 WG1159831
1,1-Dichloroethane U 0.000727 0.00316 1 08/30/2018 22:48 WG1159831
1,2-Dichloroethane U 0.000600 0.00316 1 08/30/2018 22:48 WG1159831
1,1-Dichloroethene U 0.000632 0.00316 1 08/30/2018 22:48 WG1159831
cis-1,2-Dichloroethene U 0.000872 0.00316 1 08/30/2018 22:48 WG1159831
trans-1,2-Dichloroethene U 0.00181 0.00632 1 08/30/2018 22:48 WG1159831
1,2-Dichloropropane U 0.00161 0.00632 1 08/30/2018 22:48 WG1159831
1,1-Dichloropropene U 0.000885 0.00316 1 08/30/2018 22:48 WG1159831
1,3-Dichloropropane U 0.0885 0.253 40 08/31/2018 21:21 WG1160083
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 17 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 17 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1020964
SWP-2 15-20
Collected date/time: 08/24/18 09:40
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.0343 0.126 40 08/31/2018 21:21 WG1160083
trans-1,3-Dichloropropene U 0.0774 0.253 40 08/31/2018 21:21 WG1160083
2,2-Dichloropropane U 0.00100 0.00316 1 08/30/2018 22:48 WG1159831
Di-isopropyl ether U 0.000442 0.00126 1 08/30/2018 22:48 WG1159831
Ethylbenzene 0.242 0.0268 0.126 40 08/31/2018 21:21 WG1160083
Hexachloro-1,3-butadiene U 0.0161 0.0316 1 08/30/2018 22:48 WG1159831
Isopropylbenzene 0.697 0.00109 0.00316 1 08/30/2018 22:48 WG1159831
p-Isopropyltoluene 0.416 0.00295 0.00632 1 08/30/2018 22:48 WG1159831
2-Butanone (MEK)U 0.0158 0.0316 1 08/30/2018 22:48 WG1159831
Methylene Chloride U 0.00839 0.0316 1 08/30/2018 22:48 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.506 1.26 40 08/31/2018 21:21 WG1160083
Methyl tert-butyl ether U 0.000373 0.00126 1 08/30/2018 22:48 WG1159831
Naphthalene 54.7 0.158 0.632 40 08/31/2018 21:21 WG1160083
n-Propylbenzene 0.588 0.00149 0.00632 1 08/30/2018 22:48 WG1159831
Styrene U 0.00345 0.0158 1 08/30/2018 22:48 WG1159831
1,1,1,2-Tetrachloroethane U 0.0253 0.126 40 08/31/2018 21:21 WG1160083
1,1,2,2-Tetrachloroethane U 0.000493 0.00316 1 08/30/2018 22:48 WG1159831
Tetrachloroethene U 0.0354 0.126 40 08/31/2018 21:21 WG1160083
Toluene U 0.0632 0.253 40 08/31/2018 21:21 WG1160083
1,2,3-Trichlorobenzene U 0.000790 0.00316 1 08/30/2018 22:48 WG1159831
1,2,4-Trichlorobenzene U 0.00609 0.0158 1 08/30/2018 22:48 WG1159831
1,1,1-Trichloroethane U 0.000348 0.00316 1 08/30/2018 22:48 WG1159831
1,1,2-Trichloroethane U 0.0446 0.126 40 08/31/2018 21:21 WG1160083
1,1,2-Trichlorotrifluoroethane U 0.000853 0.00316 1 08/30/2018 22:48 WG1159831
Trichloroethene U 0.000506 0.00126 1 08/30/2018 22:48 WG1159831
Trichlorofluoromethane U 0.000632 0.00316 1 08/30/2018 22:48 WG1159831
1,2,3-Trichloropropane U 0.00645 0.0158 1 08/30/2018 22:48 WG1159831
1,2,4-Trimethylbenzene 2.29 0.0587 0.253 40 08/31/2018 21:21 WG1160083
1,3,5-Trimethylbenzene 0.991 0.00137 0.00632 1 08/30/2018 22:48 WG1159831
Vinyl chloride U 0.000863 0.00316 1 08/30/2018 22:48 WG1159831
Xylenes, Total 0.411 0.241 0.329 40 08/31/2018 21:21 WG1160083
(S) Toluene-d8 27.4 J2 75.0-131 08/30/2018 22:48 WG1159831
(S) Toluene-d8 88.5 75.0-131 08/31/2018 21:21 WG1160083
(S) Dibromofluoromethane 105 65.0-129 08/30/2018 22:48 WG1159831
(S) Dibromofluoromethane 110 65.0-129 08/31/2018 21:21 WG1160083
(S) 4-Bromofluorobenzene 115 67.0-138 08/30/2018 22:48 WG1159831
(S) 4-Bromofluorobenzene 99.1 67.0-138 08/31/2018 21:21 WG1160083
Sample Narrative:
L1020964-04 WG1160083: IS/SURR failed on lower dilution.
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 50.6 0.812 4.17 100 09/04/2018 16:48 WG1159283
Acenaphthylene 5.74 0.0848 0.417 10 09/03/2018 11:25 WG1159283
Anthracene 29.5 0.799 4.17 100 09/04/2018 16:48 WG1159283
Benzidine U J4 0.805 4.21 10 09/03/2018 11:25 WG1159283
Benzo(a)anthracene 16.3 0.0541 0.417 10 09/03/2018 11:25 WG1159283
Benzo(b)fluoranthene 10.6 0.0879 0.417 10 09/03/2018 11:25 WG1159283
Benzo(k)fluoranthene 4.41 0.0736 0.417 10 09/03/2018 11:25 WG1159283
Benzo(g,h,i)perylene 2.44 0.0911 0.417 10 09/03/2018 11:25 WG1159283
Benzo(a)pyrene 11.8 0.0693 0.417 10 09/03/2018 11:25 WG1159283
Bis(2-chlorethoxy)methane U 0.0973 4.21 10 09/03/2018 11:25 WG1159283
Bis(2-chloroethyl)ether U 0.113 4.21 10 09/03/2018 11:25 WG1159283
Bis(2-chloroisopropyl)ether 0.106 J 0.0961 4.21 10 09/03/2018 11:25 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 18 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 18 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1020964
SWP-2 15-20
Collected date/time: 08/24/18 09:40
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Bromophenyl-phenylether U 0.144 4.21 10 09/03/2018 11:25 WG1159283
2-Chloronaphthalene U 0.0808 0.417 10 09/03/2018 11:25 WG1159283
4-Chlorophenyl-phenylether U 0.0793 4.21 10 09/03/2018 11:25 WG1159283
Chrysene 13.9 0.0702 0.417 10 09/03/2018 11:25 WG1159283
Dibenz(a,h)anthracene 1.33 0.0104 0.0330 10 09/03/2018 11:25 WG1159283
3,3-Dichlorobenzidine U 1.00 4.21 10 09/03/2018 11:25 WG1159283
2,4-Dinitrotoluene U 0.0767 4.21 10 09/03/2018 11:25 WG1159283
2,6-Dinitrotoluene U 0.0932 4.21 10 09/03/2018 11:25 WG1159283
Fluoranthene 36.8 0.627 4.17 100 09/04/2018 16:48 WG1159283
Fluorene 15.0 0.0862 0.417 10 09/03/2018 11:25 WG1159283
Hexachlorobenzene U 0.108 4.21 10 09/03/2018 11:25 WG1159283
Hexachloro-1,3-butadiene U 0.126 4.21 10 09/03/2018 11:25 WG1159283
Hexachlorocyclopentadiene U 0.742 4.21 10 09/03/2018 11:25 WG1159283
Hexachloroethane U 0.169 4.21 10 09/03/2018 11:25 WG1159283
Indeno(1,2,3-cd)pyrene 7.57 0.00976 0.0330 10 09/03/2018 11:25 WG1159283
Isophorone 0.173 J 0.0660 4.21 10 09/03/2018 11:25 WG1159283
Naphthalene 30.3 1.12 4.17 100 09/04/2018 16:48 WG1159283
Nitrobenzene U 0.0879 4.21 10 09/03/2018 11:25 WG1159283
n-Nitrosodimethylamine U 0.818 4.21 10 09/03/2018 11:25 WG1159283
n-Nitrosodiphenylamine U 1.14 4.21 10 09/03/2018 11:25 WG1159283
n-Nitrosodi-n-propylamine U 0.115 4.21 10 09/03/2018 11:25 WG1159283
Phenanthrene 85.7 0.667 4.17 100 09/04/2018 16:48 WG1159283
Benzylbutyl phthalate U 0.130 4.21 10 09/03/2018 11:25 WG1159283
Bis(2-ethylhexyl)phthalate U 0.152 4.21 10 09/03/2018 11:25 WG1159283
Di-n-butyl phthalate U 0.138 4.21 10 09/03/2018 11:25 WG1159283
Diethyl phthalate U 0.0874 4.21 10 09/03/2018 11:25 WG1159283
Dimethyl phthalate U 0.0683 4.21 10 09/03/2018 11:25 WG1159283
Di-n-octyl phthalate U 0.115 4.21 10 09/03/2018 11:25 WG1159283
Pyrene 48.7 1.55 4.17 100 09/04/2018 16:48 WG1159283
1,2,4-Trichlorobenzene U 0.111 4.21 10 09/03/2018 11:25 WG1159283
4-Chloro-3-methylphenol U 0.0603 4.21 10 09/03/2018 11:25 WG1159283
2-Chlorophenol U 0.105 4.21 10 09/03/2018 11:25 WG1159283
2,4-Dichlorophenol U 0.0943 4.21 10 09/03/2018 11:25 WG1159283
2,4-Dimethylphenol U 0.595 4.21 10 09/03/2018 11:25 WG1159283
4,6-Dinitro-2-methylphenol U 1.57 4.21 10 09/03/2018 11:25 WG1159283
2,4-Dinitrophenol U 1.24 4.21 10 09/03/2018 11:25 WG1159283
2-Nitrophenol U 0.164 4.21 10 09/03/2018 11:25 WG1159283
4-Nitrophenol U 0.664 4.21 10 09/03/2018 11:25 WG1159283
Pentachlorophenol U 0.607 4.21 10 09/03/2018 11:25 WG1159283
Phenol U 0.0879 4.21 10 09/03/2018 11:25 WG1159283
2,4,6-Trichlorophenol U 0.0985 4.21 10 09/03/2018 11:25 WG1159283
(S) 2-Fluorophenol 81.4 J7 12.0-120 09/04/2018 16:48 WG1159283
(S) 2-Fluorophenol 72.7 12.0-120 09/03/2018 11:25 WG1159283
(S) Phenol-d5 66.6 J7 10.0-120 09/04/2018 16:48 WG1159283
(S) Phenol-d5 65.4 10.0-120 09/03/2018 11:25 WG1159283
(S) Nitrobenzene-d5 78.2 10.0-122 09/03/2018 11:25 WG1159283
(S) Nitrobenzene-d5 90.3 J7 10.0-122 09/04/2018 16:48 WG1159283
(S) 2-Fluorobiphenyl 82.8 15.0-120 09/03/2018 11:25 WG1159283
(S) 2-Fluorobiphenyl 113 J7 15.0-120 09/04/2018 16:48 WG1159283
(S) 2,4,6-Tribromophenol 70.4 J7 10.0-127 09/04/2018 16:48 WG1159283
(S) 2,4,6-Tribromophenol 75.5 10.0-127 09/03/2018 11:25 WG1159283
(S) p-Terphenyl-d14 111 J7 10.0-120 09/04/2018 16:48 WG1159283
(S) p-Terphenyl-d14 88.5 10.0-120 09/03/2018 11:25 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 19 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1020964
SWP-3 1-5
Collected date/time: 08/24/18 09:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.1 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0403 B 0.00349 0.0250 1 08/31/2018 11:57 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 1.30 J 0.574 2.50 1 08/31/2018 15:12 WG1159261
Barium 128 0.212 0.624 1 08/31/2018 15:12 WG1159261
Cadmium U 0.0874 0.624 1 08/31/2018 15:12 WG1159261
Chromium 16.7 0.175 1.25 1 08/31/2018 15:12 WG1159261
Lead 12.1 0.237 0.624 1 08/31/2018 15:12 WG1159261
Selenium U 0.774 2.50 1 08/31/2018 15:12 WG1159261
Silver U 0.150 1.25 1 08/31/2018 15:12 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0183 J 0.0171 0.0312 1 08/30/2018 23:08 WG1159831
Acrylonitrile U 0.00237 0.0156 1 08/30/2018 23:08 WG1159831
Benzene U 0.000499 0.00125 1 08/30/2018 23:08 WG1159831
Bromobenzene U 0.00131 0.0156 1 08/30/2018 23:08 WG1159831
Bromodichloromethane U 0.000983 0.00312 1 08/30/2018 23:08 WG1159831
Bromoform U 0.00746 0.0312 1 08/30/2018 23:08 WG1159831
Bromomethane U 0.00462 0.0156 1 08/30/2018 23:08 WG1159831
n-Butylbenzene U J4 0.00479 0.0156 1 08/30/2018 23:08 WG1159831
sec-Butylbenzene 0.00397 B J 0.00316 0.0156 1 08/30/2018 23:08 WG1159831
tert-Butylbenzene U 0.00193 0.00624 1 08/30/2018 23:08 WG1159831
Carbon tetrachloride U 0.00135 0.00624 1 08/30/2018 23:08 WG1159831
Chlorobenzene 0.00614 0.000715 0.00312 1 08/30/2018 23:08 WG1159831
Chlorodibromomethane U 0.000562 0.00312 1 08/30/2018 23:08 WG1159831
Chloroethane U 0.00135 0.00624 1 08/30/2018 23:08 WG1159831
Chloroform U 0.000518 0.00312 1 08/30/2018 23:08 WG1159831
Chloromethane U 0.00173 0.0156 1 08/30/2018 23:08 WG1159831
2-Chlorotoluene U 0.00115 0.00312 1 08/30/2018 23:08 WG1159831
4-Chlorotoluene U 0.00141 0.00624 1 08/30/2018 23:08 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00636 0.0312 1 08/30/2018 23:08 WG1159831
1,2-Dibromoethane U 0.000655 0.00312 1 08/30/2018 23:08 WG1159831
Dibromomethane U 0.00125 0.00624 1 08/30/2018 23:08 WG1159831
1,2-Dichlorobenzene U 0.00181 0.00624 1 08/30/2018 23:08 WG1159831
1,3-Dichlorobenzene 0.0143 0.00212 0.00624 1 08/30/2018 23:08 WG1159831
1,4-Dichlorobenzene 0.0175 0.00246 0.00624 1 08/30/2018 23:08 WG1159831
Dichlorodifluoromethane U 0.00102 0.00312 1 08/30/2018 23:08 WG1159831
1,1-Dichloroethane U 0.000718 0.00312 1 08/30/2018 23:08 WG1159831
1,2-Dichloroethane U 0.000593 0.00312 1 08/30/2018 23:08 WG1159831
1,1-Dichloroethene U 0.000624 0.00312 1 08/30/2018 23:08 WG1159831
cis-1,2-Dichloroethene U 0.000861 0.00312 1 08/30/2018 23:08 WG1159831
trans-1,2-Dichloroethene U 0.00178 0.00624 1 08/30/2018 23:08 WG1159831
1,2-Dichloropropane U 0.00158 0.00624 1 08/30/2018 23:08 WG1159831
1,1-Dichloropropene U 0.000874 0.00312 1 08/30/2018 23:08 WG1159831
1,3-Dichloropropane U 0.00218 0.00624 1 08/30/2018 23:08 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 20 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 20 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1020964
SWP-3 1-5
Collected date/time: 08/24/18 09:50
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000846 0.00312 1 08/30/2018 23:08 WG1159831
trans-1,3-Dichloropropene U 0.00191 0.00624 1 08/30/2018 23:08 WG1159831
2,2-Dichloropropane U 0.000990 0.00312 1 08/30/2018 23:08 WG1159831
Di-isopropyl ether U 0.000437 0.00125 1 08/30/2018 23:08 WG1159831
Ethylbenzene 0.00530 0.000661 0.00312 1 08/30/2018 23:08 WG1159831
Hexachloro-1,3-butadiene U 0.0158 0.0312 1 08/30/2018 23:08 WG1159831
Isopropylbenzene 0.0373 0.00108 0.00312 1 08/30/2018 23:08 WG1159831
p-Isopropyltoluene 0.0581 0.00291 0.00624 1 08/30/2018 23:08 WG1159831
2-Butanone (MEK)0.0265 J 0.0156 0.0312 1 08/30/2018 23:08 WG1159831
Methylene Chloride U 0.00829 0.0312 1 08/30/2018 23:08 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0125 0.0312 1 08/30/2018 23:08 WG1159831
Methyl tert-butyl ether U 0.000368 0.00125 1 08/30/2018 23:08 WG1159831
Naphthalene 0.0413 0.00389 0.0156 1 09/04/2018 11:13 WG1161063
n-Propylbenzene 0.0375 0.00147 0.00624 1 08/30/2018 23:08 WG1159831
Styrene U 0.00341 0.0156 1 08/30/2018 23:08 WG1159831
1,1,1,2-Tetrachloroethane U 0.000624 0.00312 1 08/30/2018 23:08 WG1159831
1,1,2,2-Tetrachloroethane U 0.000487 0.00312 1 08/30/2018 23:08 WG1159831
Tetrachloroethene U 0.000874 0.00312 1 08/30/2018 23:08 WG1159831
Toluene 0.00211 J 0.00156 0.00624 1 08/30/2018 23:08 WG1159831
1,2,3-Trichlorobenzene U 0.000780 0.00312 1 08/30/2018 23:08 WG1159831
1,2,4-Trichlorobenzene U 0.00601 0.0156 1 08/30/2018 23:08 WG1159831
1,1,1-Trichloroethane U 0.000343 0.00312 1 08/30/2018 23:08 WG1159831
1,1,2-Trichloroethane U 0.00110 0.00312 1 08/30/2018 23:08 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000842 0.00312 1 08/30/2018 23:08 WG1159831
Trichloroethene U 0.000499 0.00125 1 08/30/2018 23:08 WG1159831
Trichlorofluoromethane U 0.000624 0.00312 1 08/30/2018 23:08 WG1159831
1,2,3-Trichloropropane U 0.00636 0.0156 1 08/30/2018 23:08 WG1159831
1,2,4-Trimethylbenzene 0.00378 J 0.00145 0.00624 1 09/04/2018 11:13 WG1161063
1,3,5-Trimethylbenzene 0.0720 0.00135 0.00624 1 08/30/2018 23:08 WG1159831
Vinyl chloride U 0.000852 0.00312 1 08/30/2018 23:08 WG1159831
Xylenes, Total 0.0115 B 0.00596 0.00811 1 08/30/2018 23:08 WG1159831
(S) Toluene-d8 85.8 75.0-131 08/30/2018 23:08 WG1159831
(S) Toluene-d8 101 75.0-131 09/04/2018 11:13 WG1161063
(S) Dibromofluoromethane 101 65.0-129 08/30/2018 23:08 WG1159831
(S) Dibromofluoromethane 84.5 65.0-129 09/04/2018 11:13 WG1161063
(S) 4-Bromofluorobenzene 104 67.0-138 08/30/2018 23:08 WG1159831
(S) 4-Bromofluorobenzene 100 67.0-138 09/04/2018 11:13 WG1161063
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.236 0.00801 0.0412 1 09/03/2018 07:06 WG1159283
Acenaphthylene 0.0896 0.00837 0.0412 1 09/03/2018 07:06 WG1159283
Anthracene 0.286 0.00789 0.0412 1 09/03/2018 07:06 WG1159283
Benzidine U J4 0.0795 0.416 1 09/03/2018 07:06 WG1159283
Benzo(a)anthracene 0.216 0.00534 0.0412 1 09/03/2018 07:06 WG1159283
Benzo(b)fluoranthene 0.152 0.00867 0.0412 1 09/03/2018 07:06 WG1159283
Benzo(k)fluoranthene 0.0539 0.00726 0.0412 1 09/03/2018 07:06 WG1159283
Benzo(g,h,i)perylene 0.0665 0.00900 0.0412 1 09/03/2018 07:06 WG1159283
Benzo(a)pyrene 0.173 0.00684 0.0412 1 09/03/2018 07:06 WG1159283
Bis(2-chlorethoxy)methane U 0.00961 0.416 1 09/03/2018 07:06 WG1159283
Bis(2-chloroethyl)ether U 0.0112 0.416 1 09/03/2018 07:06 WG1159283
Bis(2-chloroisopropyl)ether U 0.00948 0.416 1 09/03/2018 07:06 WG1159283
4-Bromophenyl-phenylether U 0.0142 0.416 1 09/03/2018 07:06 WG1159283
2-Chloronaphthalene U 0.00797 0.0412 1 09/03/2018 07:06 WG1159283
4-Chlorophenyl-phenylether U 0.00782 0.416 1 09/03/2018 07:06 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 21 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 21 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1020964
SWP-3 1-5
Collected date/time: 08/24/18 09:50
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Chrysene 0.173 0.00693 0.0412 1 09/03/2018 07:06 WG1159283
Dibenz(a,h)anthracene 0.301 0.0102 0.0412 1 09/03/2018 07:06 WG1159283
3,3-Dichlorobenzidine U 0.0991 0.416 1 09/03/2018 07:06 WG1159283
2,4-Dinitrotoluene U 0.00757 0.416 1 09/03/2018 07:06 WG1159283
2,6-Dinitrotoluene U 0.00920 0.416 1 09/03/2018 07:06 WG1159283
Fluoranthene 0.424 0.00619 0.0412 1 09/03/2018 07:06 WG1159283
Fluorene 0.121 0.00851 0.0412 1 09/03/2018 07:06 WG1159283
Hexachlorobenzene U 0.0107 0.416 1 09/03/2018 07:06 WG1159283
Hexachloro-1,3-butadiene U 0.0125 0.416 1 09/03/2018 07:06 WG1159283
Hexachlorocyclopentadiene U 0.0733 0.416 1 09/03/2018 07:06 WG1159283
Hexachloroethane U 0.0167 0.416 1 09/03/2018 07:06 WG1159283
Indeno(1,2,3-cd)pyrene 1.72 0.00963 0.0412 1 09/03/2018 07:06 WG1159283
Isophorone U 0.00651 0.416 1 09/03/2018 07:06 WG1159283
Naphthalene 0.0171 J 0.0111 0.0412 1 09/03/2018 07:06 WG1159283
Nitrobenzene U 0.00867 0.416 1 09/03/2018 07:06 WG1159283
n-Nitrosodimethylamine U 0.0807 0.416 1 09/03/2018 07:06 WG1159283
n-Nitrosodiphenylamine U 0.112 0.416 1 09/03/2018 07:06 WG1159283
n-Nitrosodi-n-propylamine U 0.0113 0.416 1 09/03/2018 07:06 WG1159283
Phenanthrene 0.805 0.00659 0.0412 1 09/03/2018 07:06 WG1159283
Benzylbutyl phthalate U 0.0129 0.416 1 09/03/2018 07:06 WG1159283
Bis(2-ethylhexyl)phthalate U 0.0150 0.416 1 09/03/2018 07:06 WG1159283
Di-n-butyl phthalate U 0.0136 0.416 1 09/03/2018 07:06 WG1159283
Diethyl phthalate U 0.00862 0.416 1 09/03/2018 07:06 WG1159283
Dimethyl phthalate U 0.00674 0.416 1 09/03/2018 07:06 WG1159283
Di-n-octyl phthalate U 0.0113 0.416 1 09/03/2018 07:06 WG1159283
Pyrene 0.540 0.0153 0.0412 1 09/03/2018 07:06 WG1159283
1,2,4-Trichlorobenzene U 0.0109 0.416 1 09/03/2018 07:06 WG1159283
4-Chloro-3-methylphenol U 0.00595 0.416 1 09/03/2018 07:06 WG1159283
2-Chlorophenol U 0.0104 0.416 1 09/03/2018 07:06 WG1159283
2,4-Dichlorophenol U 0.00931 0.416 1 09/03/2018 07:06 WG1159283
2,4-Dimethylphenol U 0.0588 0.416 1 09/03/2018 07:06 WG1159283
4,6-Dinitro-2-methylphenol U 0.155 0.416 1 09/03/2018 07:06 WG1159283
2,4-Dinitrophenol U 0.122 0.416 1 09/03/2018 07:06 WG1159283
2-Nitrophenol U 0.0162 0.416 1 09/03/2018 07:06 WG1159283
4-Nitrophenol U 0.0655 0.416 1 09/03/2018 07:06 WG1159283
Pentachlorophenol U 0.0599 0.416 1 09/03/2018 07:06 WG1159283
Phenol U 0.00867 0.416 1 09/03/2018 07:06 WG1159283
2,4,6-Trichlorophenol U 0.00972 0.416 1 09/03/2018 07:06 WG1159283
(S) 2-Fluorophenol 74.2 12.0-120 09/03/2018 07:06 WG1159283
(S) Phenol-d5 65.0 10.0-120 09/03/2018 07:06 WG1159283
(S) Nitrobenzene-d5 64.0 10.0-122 09/03/2018 07:06 WG1159283
(S) 2-Fluorobiphenyl 76.6 15.0-120 09/03/2018 07:06 WG1159283
(S) 2,4,6-Tribromophenol 92.6 10.0-127 09/03/2018 07:06 WG1159283
(S) p-Terphenyl-d14 65.2 10.0-120 09/03/2018 07:06 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 22 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 22 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L1020964
SWP-3 10-15
Collected date/time: 08/24/18 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 91.6 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.00790 B J 0.00306 0.0218 1 08/31/2018 12:00 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic U 0.502 2.18 1 08/31/2018 15:15 WG1159261
Barium 62.3 0.186 0.546 1 08/31/2018 15:15 WG1159261
Cadmium U 0.0764 0.546 1 08/31/2018 15:15 WG1159261
Chromium 8.53 0.153 1.09 1 08/31/2018 15:15 WG1159261
Lead 2.89 0.208 0.546 1 08/31/2018 15:15 WG1159261
Selenium U 0.677 2.18 1 08/31/2018 15:15 WG1159261
Silver U 0.131 1.09 1 08/31/2018 15:15 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0215 0.0393 1.44 08/30/2018 23:28 WG1159831
Acrylonitrile U 0.00299 0.0197 1.44 08/30/2018 23:28 WG1159831
Benzene U 0.000629 0.00157 1.44 08/30/2018 23:28 WG1159831
Bromobenzene U 0.00165 0.0197 1.44 08/30/2018 23:28 WG1159831
Bromodichloromethane U 0.00123 0.00393 1.44 08/30/2018 23:28 WG1159831
Bromoform U 0.00940 0.0393 1.44 08/30/2018 23:28 WG1159831
Bromomethane U 0.00582 0.0197 1.44 08/30/2018 23:28 WG1159831
n-Butylbenzene 0.00631 B J J4 0.00604 0.0197 1.44 08/30/2018 23:28 WG1159831
sec-Butylbenzene U 0.00398 0.0197 1.44 08/30/2018 23:28 WG1159831
tert-Butylbenzene U 0.00244 0.00786 1.44 08/30/2018 23:28 WG1159831
Carbon tetrachloride U 0.00170 0.00786 1.44 08/30/2018 23:28 WG1159831
Chlorobenzene U 0.000901 0.00393 1.44 08/30/2018 23:28 WG1159831
Chlorodibromomethane U 0.000708 0.00393 1.44 08/30/2018 23:28 WG1159831
Chloroethane U 0.00170 0.00786 1.44 08/30/2018 23:28 WG1159831
Chloroform U 0.000653 0.00393 1.44 08/30/2018 23:28 WG1159831
Chloromethane U 0.00218 0.0197 1.44 08/30/2018 23:28 WG1159831
2-Chlorotoluene U 0.00144 0.00393 1.44 08/30/2018 23:28 WG1159831
4-Chlorotoluene U 0.00178 0.00786 1.44 08/30/2018 23:28 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00802 0.0393 1.44 08/30/2018 23:28 WG1159831
1,2-Dibromoethane U 0.000826 0.00393 1.44 08/30/2018 23:28 WG1159831
Dibromomethane U 0.00157 0.00786 1.44 08/30/2018 23:28 WG1159831
1,2-Dichlorobenzene U 0.00228 0.00786 1.44 08/30/2018 23:28 WG1159831
1,3-Dichlorobenzene U 0.00268 0.00786 1.44 08/30/2018 23:28 WG1159831
1,4-Dichlorobenzene U 0.00310 0.00786 1.44 08/30/2018 23:28 WG1159831
Dichlorodifluoromethane U 0.00129 0.00393 1.44 08/30/2018 23:28 WG1159831
1,1-Dichloroethane U 0.000904 0.00393 1.44 08/30/2018 23:28 WG1159831
1,2-Dichloroethane U 0.000747 0.00393 1.44 08/30/2018 23:28 WG1159831
1,1-Dichloroethene U 0.000786 0.00393 1.44 08/30/2018 23:28 WG1159831
cis-1,2-Dichloroethene U 0.00109 0.00393 1.44 08/30/2018 23:28 WG1159831
trans-1,2-Dichloroethene U 0.00225 0.00786 1.44 08/30/2018 23:28 WG1159831
1,2-Dichloropropane U 0.00200 0.00786 1.44 08/30/2018 23:28 WG1159831
1,1-Dichloropropene U 0.00110 0.00393 1.44 08/30/2018 23:28 WG1159831
1,3-Dichloropropane U 0.00275 0.00786 1.44 08/30/2018 23:28 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 23 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L1020964
SWP-3 10-15
Collected date/time: 08/24/18 10:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.00107 0.00393 1.44 08/30/2018 23:28 WG1159831
trans-1,3-Dichloropropene U 0.00240 0.00786 1.44 08/30/2018 23:28 WG1159831
2,2-Dichloropropane U 0.00125 0.00393 1.44 08/30/2018 23:28 WG1159831
Di-isopropyl ether U 0.000550 0.00157 1.44 08/30/2018 23:28 WG1159831
Ethylbenzene 0.00113 J 0.000833 0.00393 1.44 08/30/2018 23:28 WG1159831
Hexachloro-1,3-butadiene U 0.0200 0.0393 1.44 08/30/2018 23:28 WG1159831
Isopropylbenzene 0.00763 0.00135 0.00393 1.44 08/30/2018 23:28 WG1159831
p-Isopropyltoluene 0.0244 0.00367 0.00786 1.44 08/30/2018 23:28 WG1159831
2-Butanone (MEK)U 0.0197 0.0393 1.44 08/30/2018 23:28 WG1159831
Methylene Chloride U 0.0104 0.0393 1.44 08/30/2018 23:28 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0157 0.0393 1.44 08/30/2018 23:28 WG1159831
Methyl tert-butyl ether U 0.000464 0.00157 1.44 08/30/2018 23:28 WG1159831
Naphthalene 0.00960 J 0.00490 0.0197 1.44 09/04/2018 11:31 WG1161063
n-Propylbenzene 0.0100 B 0.00186 0.00786 1.44 08/30/2018 23:28 WG1159831
Styrene U 0.00429 0.0197 1.44 08/30/2018 23:28 WG1159831
1,1,1,2-Tetrachloroethane U 0.000786 0.00393 1.44 08/30/2018 23:28 WG1159831
1,1,2,2-Tetrachloroethane U 0.000614 0.00393 1.44 08/30/2018 23:28 WG1159831
Tetrachloroethene U 0.00110 0.00393 1.44 08/30/2018 23:28 WG1159831
Toluene U 0.00197 0.00786 1.44 08/30/2018 23:28 WG1159831
1,2,3-Trichlorobenzene U 0.000983 0.00393 1.44 08/30/2018 23:28 WG1159831
1,2,4-Trichlorobenzene U 0.00758 0.0197 1.44 08/30/2018 23:28 WG1159831
1,1,1-Trichloroethane U 0.000432 0.00393 1.44 08/30/2018 23:28 WG1159831
1,1,2-Trichloroethane U 0.00139 0.00393 1.44 08/30/2018 23:28 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.00106 0.00393 1.44 08/30/2018 23:28 WG1159831
Trichloroethene U 0.000629 0.00157 1.44 08/30/2018 23:28 WG1159831
Trichlorofluoromethane U 0.000786 0.00393 1.44 08/30/2018 23:28 WG1159831
1,2,3-Trichloropropane U 0.00802 0.0197 1.44 08/30/2018 23:28 WG1159831
1,2,4-Trimethylbenzene U 0.00182 0.00786 1.44 08/31/2018 21:58 WG1160083
1,3,5-Trimethylbenzene 0.0197 B 0.00170 0.00786 1.44 08/30/2018 23:28 WG1159831
Vinyl chloride U 0.00107 0.00393 1.44 08/30/2018 23:28 WG1159831
Xylenes, Total U 0.00751 0.0102 1.44 08/30/2018 23:28 WG1159831
(S) Toluene-d8 103 75.0-131 08/30/2018 23:28 WG1159831
(S) Toluene-d8 103 75.0-131 08/31/2018 21:58 WG1160083
(S) Toluene-d8 105 75.0-131 09/04/2018 11:31 WG1161063
(S) Dibromofluoromethane 102 65.0-129 08/30/2018 23:28 WG1159831
(S) Dibromofluoromethane 89.2 65.0-129 08/31/2018 21:58 WG1160083
(S) Dibromofluoromethane 94.5 65.0-129 09/04/2018 11:31 WG1161063
(S) 4-Bromofluorobenzene 104 67.0-138 08/30/2018 23:28 WG1159831
(S) 4-Bromofluorobenzene 109 67.0-138 08/31/2018 21:58 WG1160083
(S) 4-Bromofluorobenzene 104 67.0-138 09/04/2018 11:31 WG1161063
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0166 J 0.00701 0.0360 1 09/03/2018 03:59 WG1159283
Acenaphthylene U 0.00733 0.0360 1 09/03/2018 03:59 WG1159283
Anthracene U 0.00690 0.0360 1 09/03/2018 03:59 WG1159283
Benzidine U J4 0.0696 0.364 1 09/03/2018 03:59 WG1159283
Benzo(a)anthracene 0.00520 B J 0.00467 0.0360 1 09/03/2018 03:59 WG1159283
Benzo(b)fluoranthene U 0.00759 0.0360 1 09/03/2018 03:59 WG1159283
Benzo(k)fluoranthene U 0.00636 0.0360 1 09/03/2018 03:59 WG1159283
Benzo(g,h,i)perylene U 0.00787 0.0360 1 09/03/2018 03:59 WG1159283
Benzo(a)pyrene U 0.00598 0.0360 1 09/03/2018 03:59 WG1159283
Bis(2-chlorethoxy)methane U 0.00841 0.364 1 09/03/2018 03:59 WG1159283
Bis(2-chloroethyl)ether U 0.00979 0.364 1 09/03/2018 03:59 WG1159283
Bis(2-chloroisopropyl)ether U 0.00830 0.364 1 09/03/2018 03:59 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 24 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L1020964
SWP-3 10-15
Collected date/time: 08/24/18 10:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Bromophenyl-phenylether U 0.0125 0.364 1 09/03/2018 03:59 WG1159283
2-Chloronaphthalene U 0.00698 0.0360 1 09/03/2018 03:59 WG1159283
4-Chlorophenyl-phenylether U 0.00685 0.364 1 09/03/2018 03:59 WG1159283
Chrysene U 0.00606 0.0360 1 09/03/2018 03:59 WG1159283
Dibenz(a,h)anthracene U 0.00897 0.0360 1 09/03/2018 03:59 WG1159283
3,3-Dichlorobenzidine U 0.0867 0.364 1 09/03/2018 03:59 WG1159283
2,4-Dinitrotoluene U 0.00663 0.364 1 09/03/2018 03:59 WG1159283
2,6-Dinitrotoluene U 0.00805 0.364 1 09/03/2018 03:59 WG1159283
Fluoranthene 0.0105 J 0.00542 0.0360 1 09/03/2018 03:59 WG1159283
Fluorene 0.00857 J 0.00745 0.0360 1 09/03/2018 03:59 WG1159283
Hexachlorobenzene U 0.00935 0.364 1 09/03/2018 03:59 WG1159283
Hexachloro-1,3-butadiene U 0.0109 0.364 1 09/03/2018 03:59 WG1159283
Hexachlorocyclopentadiene U 0.0641 0.364 1 09/03/2018 03:59 WG1159283
Hexachloroethane U 0.0146 0.364 1 09/03/2018 03:59 WG1159283
Indeno(1,2,3-cd)pyrene U 0.00843 0.0360 1 09/03/2018 03:59 WG1159283
Isophorone U 0.00570 0.364 1 09/03/2018 03:59 WG1159283
Naphthalene U 0.00971 0.0360 1 09/03/2018 03:59 WG1159283
Nitrobenzene U 0.00759 0.364 1 09/03/2018 03:59 WG1159283
n-Nitrosodimethylamine U 0.0707 0.364 1 09/03/2018 03:59 WG1159283
n-Nitrosodiphenylamine U 0.0983 0.364 1 09/03/2018 03:59 WG1159283
n-Nitrosodi-n-propylamine U 0.00989 0.364 1 09/03/2018 03:59 WG1159283
Phenanthrene 0.0235 J 0.00577 0.0360 1 09/03/2018 03:59 WG1159283
Benzylbutyl phthalate U 0.0112 0.364 1 09/03/2018 03:59 WG1159283
Bis(2-ethylhexyl)phthalate 0.0284 J 0.0131 0.364 1 09/03/2018 03:59 WG1159283
Di-n-butyl phthalate U 0.0119 0.364 1 09/03/2018 03:59 WG1159283
Diethyl phthalate U 0.00755 0.364 1 09/03/2018 03:59 WG1159283
Dimethyl phthalate U 0.00590 0.364 1 09/03/2018 03:59 WG1159283
Di-n-octyl phthalate U 0.00991 0.364 1 09/03/2018 03:59 WG1159283
Pyrene U 0.0134 0.0360 1 09/03/2018 03:59 WG1159283
1,2,4-Trichlorobenzene U 0.00957 0.364 1 09/03/2018 03:59 WG1159283
4-Chloro-3-methylphenol U 0.00521 0.364 1 09/03/2018 03:59 WG1159283
2-Chlorophenol U 0.00908 0.364 1 09/03/2018 03:59 WG1159283
2,4-Dichlorophenol U 0.00815 0.364 1 09/03/2018 03:59 WG1159283
2,4-Dimethylphenol U 0.0514 0.364 1 09/03/2018 03:59 WG1159283
4,6-Dinitro-2-methylphenol U 0.135 0.364 1 09/03/2018 03:59 WG1159283
2,4-Dinitrophenol U 0.107 0.364 1 09/03/2018 03:59 WG1159283
2-Nitrophenol U 0.0142 0.364 1 09/03/2018 03:59 WG1159283
4-Nitrophenol U 0.0573 0.364 1 09/03/2018 03:59 WG1159283
Pentachlorophenol U 0.0524 0.364 1 09/03/2018 03:59 WG1159283
Phenol U 0.00759 0.364 1 09/03/2018 03:59 WG1159283
2,4,6-Trichlorophenol U 0.00851 0.364 1 09/03/2018 03:59 WG1159283
(S) 2-Fluorophenol 83.3 12.0-120 09/03/2018 03:59 WG1159283
(S) Phenol-d5 70.5 10.0-120 09/03/2018 03:59 WG1159283
(S) Nitrobenzene-d5 70.4 10.0-122 09/03/2018 03:59 WG1159283
(S) 2-Fluorobiphenyl 78.0 15.0-120 09/03/2018 03:59 WG1159283
(S) 2,4,6-Tribromophenol 98.7 10.0-127 09/03/2018 03:59 WG1159283
(S) p-Terphenyl-d14 61.8 10.0-120 09/03/2018 03:59 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 25 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 25 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L1020964
SWP-4 1-5
Collected date/time: 08/24/18 10:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.1 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.184 0.00354 0.0253 1 08/31/2018 12:02 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 0.908 J 0.581 2.53 1 08/31/2018 14:43 WG1159261
Barium 88.6 0.215 0.632 1 08/31/2018 14:43 WG1159261
Cadmium 0.305 J 0.0885 0.632 1 08/31/2018 14:43 WG1159261
Chromium 21.9 0.177 1.26 1 08/31/2018 14:43 WG1159261
Lead 128 J6 0.240 0.632 1 08/31/2018 14:43 WG1159261
Selenium U 0.784 2.53 1 08/31/2018 14:43 WG1159261
Silver U 0.152 1.26 1 08/31/2018 14:43 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0173 0.0316 1 08/30/2018 23:48 WG1159831
Acrylonitrile U 0.00240 0.0158 1 08/30/2018 23:48 WG1159831
Benzene U 0.000506 0.00126 1 08/30/2018 23:48 WG1159831
Bromobenzene U 0.00133 0.0158 1 08/30/2018 23:48 WG1159831
Bromodichloromethane U 0.000996 0.00316 1 08/30/2018 23:48 WG1159831
Bromoform U 0.00756 0.0316 1 08/30/2018 23:48 WG1159831
Bromomethane U 0.00468 0.0158 1 08/30/2018 23:48 WG1159831
n-Butylbenzene U J4 0.00485 0.0158 1 08/30/2018 23:48 WG1159831
sec-Butylbenzene U 0.00320 0.0158 1 08/30/2018 23:48 WG1159831
tert-Butylbenzene U 0.00196 0.00632 1 08/30/2018 23:48 WG1159831
Carbon tetrachloride U 0.00136 0.00632 1 08/30/2018 23:48 WG1159831
Chlorobenzene U 0.000724 0.00316 1 08/30/2018 23:48 WG1159831
Chlorodibromomethane U 0.000569 0.00316 1 08/30/2018 23:48 WG1159831
Chloroethane U 0.00136 0.00632 1 08/30/2018 23:48 WG1159831
Chloroform U 0.000524 0.00316 1 08/30/2018 23:48 WG1159831
Chloromethane U 0.00176 0.0158 1 08/30/2018 23:48 WG1159831
2-Chlorotoluene U 0.00116 0.00316 1 08/30/2018 23:48 WG1159831
4-Chlorotoluene U 0.00143 0.00632 1 08/30/2018 23:48 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00645 0.0316 1 08/30/2018 23:48 WG1159831
1,2-Dibromoethane U 0.000664 0.00316 1 08/30/2018 23:48 WG1159831
Dibromomethane U 0.00126 0.00632 1 08/30/2018 23:48 WG1159831
1,2-Dichlorobenzene U 0.00183 0.00632 1 08/30/2018 23:48 WG1159831
1,3-Dichlorobenzene U 0.00215 0.00632 1 08/30/2018 23:48 WG1159831
1,4-Dichlorobenzene U 0.00249 0.00632 1 08/30/2018 23:48 WG1159831
Dichlorodifluoromethane U 0.00103 0.00316 1 08/30/2018 23:48 WG1159831
1,1-Dichloroethane U 0.000727 0.00316 1 08/30/2018 23:48 WG1159831
1,2-Dichloroethane U 0.000600 0.00316 1 08/30/2018 23:48 WG1159831
1,1-Dichloroethene U 0.000632 0.00316 1 08/30/2018 23:48 WG1159831
cis-1,2-Dichloroethene U 0.000872 0.00316 1 08/30/2018 23:48 WG1159831
trans-1,2-Dichloroethene U 0.00181 0.00632 1 08/30/2018 23:48 WG1159831
1,2-Dichloropropane U 0.00161 0.00632 1 08/30/2018 23:48 WG1159831
1,1-Dichloropropene U 0.000885 0.00316 1 08/30/2018 23:48 WG1159831
1,3-Dichloropropane U 0.00221 0.00632 1 08/30/2018 23:48 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 26 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L1020964
SWP-4 1-5
Collected date/time: 08/24/18 10:10
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000857 0.00316 1 08/30/2018 23:48 WG1159831
trans-1,3-Dichloropropene U 0.00193 0.00632 1 08/30/2018 23:48 WG1159831
2,2-Dichloropropane U 0.00100 0.00316 1 08/30/2018 23:48 WG1159831
Di-isopropyl ether U 0.000442 0.00126 1 08/30/2018 23:48 WG1159831
Ethylbenzene U 0.000670 0.00316 1 08/30/2018 23:48 WG1159831
Hexachloro-1,3-butadiene U 0.0161 0.0316 1 08/30/2018 23:48 WG1159831
Isopropylbenzene 0.00111 J 0.00109 0.00316 1 08/30/2018 23:48 WG1159831
p-Isopropyltoluene 0.00519 J 0.00294 0.00632 1 08/30/2018 23:48 WG1159831
2-Butanone (MEK)U 0.0158 0.0316 1 08/30/2018 23:48 WG1159831
Methylene Chloride U 0.00839 0.0316 1 08/30/2018 23:48 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0126 0.0316 1 08/30/2018 23:48 WG1159831
Methyl tert-butyl ether U 0.000373 0.00126 1 08/30/2018 23:48 WG1159831
Naphthalene U 0.00394 0.0158 1 09/04/2018 11:50 WG1161063
n-Propylbenzene U 0.00149 0.00632 1 08/30/2018 23:48 WG1159831
Styrene U 0.00345 0.0158 1 08/30/2018 23:48 WG1159831
1,1,1,2-Tetrachloroethane U 0.000632 0.00316 1 08/30/2018 23:48 WG1159831
1,1,2,2-Tetrachloroethane U 0.000493 0.00316 1 08/30/2018 23:48 WG1159831
Tetrachloroethene 0.00882 0.000885 0.00316 1 08/30/2018 23:48 WG1159831
Toluene U 0.00158 0.00632 1 08/30/2018 23:48 WG1159831
1,2,3-Trichlorobenzene U 0.000790 0.00316 1 08/30/2018 23:48 WG1159831
1,2,4-Trichlorobenzene U 0.00609 0.0158 1 08/30/2018 23:48 WG1159831
1,1,1-Trichloroethane U 0.000348 0.00316 1 08/30/2018 23:48 WG1159831
1,1,2-Trichloroethane U 0.00112 0.00316 1 08/30/2018 23:48 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000853 0.00316 1 08/30/2018 23:48 WG1159831
Trichloroethene U 0.000506 0.00126 1 08/30/2018 23:48 WG1159831
Trichlorofluoromethane U 0.000632 0.00316 1 08/30/2018 23:48 WG1159831
1,2,3-Trichloropropane U 0.00645 0.0158 1 08/30/2018 23:48 WG1159831
1,2,4-Trimethylbenzene U 0.00147 0.00632 1 08/31/2018 22:16 WG1160083
1,3,5-Trimethylbenzene 0.00394 B J 0.00136 0.00632 1 08/30/2018 23:48 WG1159831
Vinyl chloride U 0.000863 0.00316 1 08/30/2018 23:48 WG1159831
Xylenes, Total U B 0.00604 0.00821 1 08/30/2018 23:48 WG1159831
(S) Toluene-d8 106 75.0-131 08/30/2018 23:48 WG1159831
(S) Toluene-d8 101 75.0-131 08/31/2018 22:16 WG1160083
(S) Toluene-d8 104 75.0-131 09/04/2018 11:50 WG1161063
(S) Dibromofluoromethane 102 65.0-129 08/30/2018 23:48 WG1159831
(S) Dibromofluoromethane 98.3 65.0-129 08/31/2018 22:16 WG1160083
(S) Dibromofluoromethane 99.5 65.0-129 09/04/2018 11:50 WG1161063
(S) 4-Bromofluorobenzene 107 67.0-138 08/30/2018 23:48 WG1159831
(S) 4-Bromofluorobenzene 105 67.0-138 08/31/2018 22:16 WG1160083
(S) 4-Bromofluorobenzene 107 67.0-138 09/04/2018 11:50 WG1161063
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.0162 0.0834 2 09/03/2018 07:53 WG1159283
Acenaphthylene U 0.0169 0.0834 2 09/03/2018 07:53 WG1159283
Anthracene U 0.0159 0.0834 2 09/03/2018 07:53 WG1159283
Benzidine U J4 0.161 0.842 2 09/03/2018 07:53 WG1159283
Benzo(a)anthracene 0.0316 B J 0.0108 0.0834 2 09/03/2018 07:53 WG1159283
Benzo(b)fluoranthene 0.0509 J 0.0176 0.0834 2 09/03/2018 07:53 WG1159283
Benzo(k)fluoranthene 0.0216 J 0.0147 0.0834 2 09/03/2018 07:53 WG1159283
Benzo(g,h,i)perylene 0.0252 J 0.0182 0.0834 2 09/03/2018 07:53 WG1159283
Benzo(a)pyrene 0.0361 J 0.0139 0.0834 2 09/03/2018 07:53 WG1159283
Bis(2-chlorethoxy)methane U 0.0195 0.842 2 09/03/2018 07:53 WG1159283
Bis(2-chloroethyl)ether U 0.0226 0.842 2 09/03/2018 07:53 WG1159283
Bis(2-chloroisopropyl)ether U 0.0192 0.842 2 09/03/2018 07:53 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 27 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 27 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L1020964
SWP-4 1-5
Collected date/time: 08/24/18 10:10
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
4-Bromophenyl-phenylether U 0.0288 0.842 2 09/03/2018 07:53 WG1159283
2-Chloronaphthalene U 0.0162 0.0834 2 09/03/2018 07:53 WG1159283
4-Chlorophenyl-phenylether U 0.0158 0.842 2 09/03/2018 07:53 WG1159283
Chrysene 0.0325 J 0.0140 0.0834 2 09/03/2018 07:53 WG1159283
Dibenz(a,h)anthracene U 0.0207 0.0834 2 09/03/2018 07:53 WG1159283
3,3-Dichlorobenzidine U 0.201 0.842 2 09/03/2018 07:53 WG1159283
2,4-Dinitrotoluene U 0.0153 0.842 2 09/03/2018 07:53 WG1159283
2,6-Dinitrotoluene U 0.0186 0.842 2 09/03/2018 07:53 WG1159283
Fluoranthene 0.0416 J 0.0125 0.0834 2 09/03/2018 07:53 WG1159283
Fluorene U 0.0172 0.0834 2 09/03/2018 07:53 WG1159283
Hexachlorobenzene U 0.0216 0.842 2 09/03/2018 07:53 WG1159283
Hexachloro-1,3-butadiene U 0.0253 0.842 2 09/03/2018 07:53 WG1159283
Hexachlorocyclopentadiene U 0.148 0.842 2 09/03/2018 07:53 WG1159283
Hexachloroethane U 0.0339 0.842 2 09/03/2018 07:53 WG1159283
Indeno(1,2,3-cd)pyrene 0.308 0.0195 0.0834 2 09/03/2018 07:53 WG1159283
Isophorone U 0.0131 0.842 2 09/03/2018 07:53 WG1159283
Naphthalene U 0.0225 0.0834 2 09/03/2018 07:53 WG1159283
Nitrobenzene U 0.0176 0.842 2 09/03/2018 07:53 WG1159283
n-Nitrosodimethylamine U 0.163 0.842 2 09/03/2018 07:53 WG1159283
n-Nitrosodiphenylamine U 0.227 0.842 2 09/03/2018 07:53 WG1159283
n-Nitrosodi-n-propylamine U 0.0229 0.842 2 09/03/2018 07:53 WG1159283
Phenanthrene U 0.0134 0.0834 2 09/03/2018 07:53 WG1159283
Benzylbutyl phthalate U 0.0260 0.842 2 09/03/2018 07:53 WG1159283
Bis(2-ethylhexyl)phthalate U 0.0303 0.842 2 09/03/2018 07:53 WG1159283
Di-n-butyl phthalate U 0.0276 0.842 2 09/03/2018 07:53 WG1159283
Diethyl phthalate U 0.0174 0.842 2 09/03/2018 07:53 WG1159283
Dimethyl phthalate U 0.0136 0.842 2 09/03/2018 07:53 WG1159283
Di-n-octyl phthalate U 0.0229 0.842 2 09/03/2018 07:53 WG1159283
Pyrene 0.0383 J 0.0311 0.0834 2 09/03/2018 07:53 WG1159283
1,2,4-Trichlorobenzene U 0.0221 0.842 2 09/03/2018 07:53 WG1159283
4-Chloro-3-methylphenol U 0.0121 0.842 2 09/03/2018 07:53 WG1159283
2-Chlorophenol U 0.0210 0.842 2 09/03/2018 07:53 WG1159283
2,4-Dichlorophenol U 0.0188 0.842 2 09/03/2018 07:53 WG1159283
2,4-Dimethylphenol U 0.119 0.842 2 09/03/2018 07:53 WG1159283
4,6-Dinitro-2-methylphenol U 0.313 0.842 2 09/03/2018 07:53 WG1159283
2,4-Dinitrophenol U 0.248 0.842 2 09/03/2018 07:53 WG1159283
2-Nitrophenol U 0.0329 0.842 2 09/03/2018 07:53 WG1159283
4-Nitrophenol U 0.133 0.842 2 09/03/2018 07:53 WG1159283
Pentachlorophenol U 0.121 0.842 2 09/03/2018 07:53 WG1159283
Phenol U 0.0176 0.842 2 09/03/2018 07:53 WG1159283
2,4,6-Trichlorophenol U 0.0197 0.842 2 09/03/2018 07:53 WG1159283
(S) 2-Fluorophenol 74.2 12.0-120 09/03/2018 07:53 WG1159283
(S) Phenol-d5 66.6 10.0-120 09/03/2018 07:53 WG1159283
(S) Nitrobenzene-d5 60.8 10.0-122 09/03/2018 07:53 WG1159283
(S) 2-Fluorobiphenyl 78.1 15.0-120 09/03/2018 07:53 WG1159283
(S) 2,4,6-Tribromophenol 95.1 10.0-127 09/03/2018 07:53 WG1159283
(S) p-Terphenyl-d14 69.0 10.0-120 09/03/2018 07:53 WG1159283
Sample Narrative:
L1020964-07 WG1159283: Dilution due to matrix
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 28 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 28 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L1020964
SWP-4 10-15
Collected date/time: 08/24/18 10:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.7 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.110 0.00356 0.0254 1 08/31/2018 12:05 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 7.25 0.585 2.54 1 08/31/2018 15:18 WG1159261
Barium 69.9 0.216 0.635 1 08/31/2018 15:18 WG1159261
Cadmium 0.425 J 0.0890 0.635 1 08/31/2018 15:18 WG1159261
Chromium 42.6 0.178 1.27 1 08/31/2018 15:18 WG1159261
Lead 138 0.241 0.635 1 08/31/2018 15:18 WG1159261
Selenium U 0.788 2.54 1 08/31/2018 15:18 WG1159261
Silver U 0.152 1.27 1 08/31/2018 15:18 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0174 0.0318 1 08/31/2018 00:08 WG1159831
Acrylonitrile U 0.00241 0.0159 1 08/31/2018 00:08 WG1159831
Benzene U 0.000508 0.00127 1 08/31/2018 00:08 WG1159831
Bromobenzene U 0.00133 0.0159 1 08/31/2018 00:08 WG1159831
Bromodichloromethane U 0.00100 0.00318 1 08/31/2018 00:08 WG1159831
Bromoform U 0.00760 0.0318 1 08/31/2018 00:08 WG1159831
Bromomethane U 0.00470 0.0159 1 08/31/2018 00:08 WG1159831
n-Butylbenzene U J4 0.00488 0.0159 1 08/31/2018 00:08 WG1159831
sec-Butylbenzene U 0.00322 0.0159 1 08/31/2018 00:08 WG1159831
tert-Butylbenzene U 0.00197 0.00635 1 08/31/2018 00:08 WG1159831
Carbon tetrachloride U 0.00137 0.00635 1 08/31/2018 00:08 WG1159831
Chlorobenzene 0.00636 0.000728 0.00318 1 08/31/2018 00:08 WG1159831
Chlorodibromomethane U 0.000572 0.00318 1 08/31/2018 00:08 WG1159831
Chloroethane U 0.00137 0.00635 1 08/31/2018 00:08 WG1159831
Chloroform U 0.000527 0.00318 1 08/31/2018 00:08 WG1159831
Chloromethane U 0.00177 0.0159 1 08/31/2018 00:08 WG1159831
2-Chlorotoluene U 0.00117 0.00318 1 08/31/2018 00:08 WG1159831
4-Chlorotoluene U 0.00144 0.00635 1 08/31/2018 00:08 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00648 0.0318 1 08/31/2018 00:08 WG1159831
1,2-Dibromoethane U 0.000667 0.00318 1 08/31/2018 00:08 WG1159831
Dibromomethane U 0.00127 0.00635 1 08/31/2018 00:08 WG1159831
1,2-Dichlorobenzene U 0.00184 0.00635 1 08/31/2018 00:08 WG1159831
1,3-Dichlorobenzene 0.0137 0.00216 0.00635 1 08/31/2018 00:08 WG1159831
1,4-Dichlorobenzene 0.0868 0.00250 0.00635 1 08/31/2018 00:08 WG1159831
Dichlorodifluoromethane U 0.00104 0.00318 1 08/31/2018 00:08 WG1159831
1,1-Dichloroethane U 0.000731 0.00318 1 08/31/2018 00:08 WG1159831
1,2-Dichloroethane 0.0215 0.000604 0.00318 1 08/31/2018 00:08 WG1159831
1,1-Dichloroethene 0.0237 0.000635 0.00318 1 08/31/2018 00:08 WG1159831
cis-1,2-Dichloroethene 0.258 0.000877 0.00318 1 08/31/2018 00:08 WG1159831
trans-1,2-Dichloroethene 0.0146 0.00182 0.00635 1 08/31/2018 00:08 WG1159831
1,2-Dichloropropane U 0.00161 0.00635 1 08/31/2018 00:08 WG1159831
1,1-Dichloropropene U 0.000890 0.00318 1 08/31/2018 00:08 WG1159831
1,3-Dichloropropane U 0.00222 0.00635 1 08/31/2018 00:08 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 29 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 29 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L1020964
SWP-4 10-15
Collected date/time: 08/24/18 10:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000862 0.00318 1 08/31/2018 00:08 WG1159831
trans-1,3-Dichloropropene U 0.00194 0.00635 1 08/31/2018 00:08 WG1159831
2,2-Dichloropropane U 0.00101 0.00318 1 08/31/2018 00:08 WG1159831
Di-isopropyl ether U 0.000445 0.00127 1 08/31/2018 00:08 WG1159831
Ethylbenzene 0.00408 0.000674 0.00318 1 08/31/2018 00:08 WG1159831
Hexachloro-1,3-butadiene U 0.0161 0.0318 1 08/31/2018 00:08 WG1159831
Isopropylbenzene 0.00136 J 0.00110 0.00318 1 08/31/2018 00:08 WG1159831
p-Isopropyltoluene 0.00326 J 0.00296 0.00635 1 08/31/2018 00:08 WG1159831
2-Butanone (MEK)U 0.0159 0.0318 1 08/31/2018 00:08 WG1159831
Methylene Chloride U 0.00844 0.0318 1 08/31/2018 00:08 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0127 0.0318 1 08/31/2018 00:08 WG1159831
Methyl tert-butyl ether U 0.000375 0.00127 1 08/31/2018 00:08 WG1159831
Naphthalene 0.0614 0.00396 0.0159 1 08/31/2018 22:35 WG1160083
n-Propylbenzene U 0.00150 0.00635 1 08/31/2018 00:08 WG1159831
Styrene U 0.00347 0.0159 1 08/31/2018 00:08 WG1159831
1,1,1,2-Tetrachloroethane U 0.000635 0.00318 1 08/31/2018 00:08 WG1159831
1,1,2,2-Tetrachloroethane U 0.000496 0.00318 1 08/31/2018 00:08 WG1159831
Tetrachloroethene 0.0478 0.000890 0.00318 1 08/31/2018 00:08 WG1159831
Toluene 0.00866 0.00159 0.00635 1 08/31/2018 00:08 WG1159831
1,2,3-Trichlorobenzene U 0.000794 0.00318 1 08/31/2018 00:08 WG1159831
1,2,4-Trichlorobenzene U 0.00613 0.0159 1 08/31/2018 00:08 WG1159831
1,1,1-Trichloroethane U 0.000349 0.00318 1 08/31/2018 00:08 WG1159831
1,1,2-Trichloroethane U 0.00112 0.00318 1 08/31/2018 00:08 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000858 0.00318 1 08/31/2018 00:08 WG1159831
Trichloroethene 0.110 0.000508 0.00127 1 08/31/2018 00:08 WG1159831
Trichlorofluoromethane U 0.000635 0.00318 1 08/31/2018 00:08 WG1159831
1,2,3-Trichloropropane U 0.00648 0.0159 1 08/31/2018 00:08 WG1159831
1,2,4-Trimethylbenzene 0.00251 J 0.00147 0.00635 1 08/31/2018 22:35 WG1160083
1,3,5-Trimethylbenzene U 0.00137 0.00635 1 08/31/2018 00:08 WG1159831
Vinyl chloride U 0.000868 0.00318 1 08/31/2018 00:08 WG1159831
Xylenes, Total 0.0108 B 0.00607 0.00826 1 08/31/2018 00:08 WG1159831
(S) Toluene-d8 84.9 75.0-131 08/31/2018 00:08 WG1159831
(S) Toluene-d8 101 75.0-131 08/31/2018 22:35 WG1160083
(S) Dibromofluoromethane 102 65.0-129 08/31/2018 00:08 WG1159831
(S) Dibromofluoromethane 100 65.0-129 08/31/2018 22:35 WG1160083
(S) 4-Bromofluorobenzene 103 67.0-138 08/31/2018 00:08 WG1159831
(S) 4-Bromofluorobenzene 109 67.0-138 08/31/2018 22:35 WG1160083
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.943 0.0816 0.419 10 09/03/2018 11:48 WG1159283
Acenaphthylene 0.381 J 0.0853 0.419 10 09/03/2018 11:48 WG1159283
Anthracene 0.768 0.0803 0.419 10 09/03/2018 11:48 WG1159283
Benzidine U J4 0.810 4.23 10 09/03/2018 11:48 WG1159283
Benzo(a)anthracene 1.32 0.0544 0.419 10 09/03/2018 11:48 WG1159283
Benzo(b)fluoranthene 0.630 J 0.441 2.10 50 09/04/2018 16:25 WG1159283
Benzo(k)fluoranthene 1.02 J 0.370 2.10 50 09/04/2018 16:25 WG1159283
Benzo(g,h,i)perylene U 0.459 2.10 50 09/04/2018 16:25 WG1159283
Benzo(a)pyrene 0.898 J 0.348 2.10 50 09/04/2018 16:25 WG1159283
Bis(2-chlorethoxy)methane U 0.0979 4.23 10 09/03/2018 11:48 WG1159283
Bis(2-chloroethyl)ether U 0.114 4.23 10 09/03/2018 11:48 WG1159283
Bis(2-chloroisopropyl)ether U 0.0966 4.23 10 09/03/2018 11:48 WG1159283
4-Bromophenyl-phenylether U 0.145 4.23 10 09/03/2018 11:48 WG1159283
2-Chloronaphthalene U 0.0812 0.419 10 09/03/2018 11:48 WG1159283
4-Chlorophenyl-phenylether U 0.0797 4.23 10 09/03/2018 11:48 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 30 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 30 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L1020964
SWP-4 10-15
Collected date/time: 08/24/18 10:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Chrysene 1.30 0.0705 0.419 10 09/03/2018 11:48 WG1159283
Dibenz(a,h)anthracene U 0.0522 0.165 50 09/04/2018 16:25 WG1159283
3,3-Dichlorobenzidine U 1.01 4.23 10 09/03/2018 11:48 WG1159283
2,4-Dinitrotoluene U 0.0771 4.23 10 09/03/2018 11:48 WG1159283
2,6-Dinitrotoluene U 0.0937 4.23 10 09/03/2018 11:48 WG1159283
Fluoranthene 1.66 0.0630 0.419 10 09/03/2018 11:48 WG1159283
Fluorene 0.393 J 0.0867 0.419 10 09/03/2018 11:48 WG1159283
Hexachlorobenzene U 0.109 4.23 10 09/03/2018 11:48 WG1159283
Hexachloro-1,3-butadiene U 0.127 4.23 10 09/03/2018 11:48 WG1159283
Hexachlorocyclopentadiene U 0.746 4.23 10 09/03/2018 11:48 WG1159283
Hexachloroethane U 0.170 4.23 10 09/03/2018 11:48 WG1159283
Indeno(1,2,3-cd)pyrene U 0.0491 0.165 50 09/04/2018 16:25 WG1159283
Isophorone U 0.0663 4.23 10 09/03/2018 11:48 WG1159283
Naphthalene 0.648 0.113 0.419 10 09/03/2018 11:48 WG1159283
Nitrobenzene U 0.0883 4.23 10 09/03/2018 11:48 WG1159283
n-Nitrosodimethylamine U 0.822 4.23 10 09/03/2018 11:48 WG1159283
n-Nitrosodiphenylamine U 1.14 4.23 10 09/03/2018 11:48 WG1159283
n-Nitrosodi-n-propylamine U 0.115 4.23 10 09/03/2018 11:48 WG1159283
Phenanthrene 1.20 0.0671 0.419 10 09/03/2018 11:48 WG1159283
Benzylbutyl phthalate U 0.131 4.23 10 09/03/2018 11:48 WG1159283
Bis(2-ethylhexyl)phthalate U 0.152 4.23 10 09/03/2018 11:48 WG1159283
Di-n-butyl phthalate U 0.139 4.23 10 09/03/2018 11:48 WG1159283
Diethyl phthalate U 0.0878 4.23 10 09/03/2018 11:48 WG1159283
Dimethyl phthalate U 0.0686 4.23 10 09/03/2018 11:48 WG1159283
Di-n-octyl phthalate U 0.115 4.23 10 09/03/2018 11:48 WG1159283
Pyrene 3.30 0.156 0.419 10 09/03/2018 11:48 WG1159283
1,2,4-Trichlorobenzene 0.166 J 0.111 4.23 10 09/03/2018 11:48 WG1159283
4-Chloro-3-methylphenol U 0.0606 4.23 10 09/03/2018 11:48 WG1159283
2-Chlorophenol U 0.106 4.23 10 09/03/2018 11:48 WG1159283
2,4-Dichlorophenol U 0.0948 4.23 10 09/03/2018 11:48 WG1159283
2,4-Dimethylphenol U 0.599 4.23 10 09/03/2018 11:48 WG1159283
4,6-Dinitro-2-methylphenol U 1.58 4.23 10 09/03/2018 11:48 WG1159283
2,4-Dinitrophenol U 1.25 4.23 10 09/03/2018 11:48 WG1159283
2-Nitrophenol U 0.165 4.23 10 09/03/2018 11:48 WG1159283
4-Nitrophenol U 0.667 4.23 10 09/03/2018 11:48 WG1159283
Pentachlorophenol U 0.610 4.23 10 09/03/2018 11:48 WG1159283
Phenol U 0.0883 4.23 10 09/03/2018 11:48 WG1159283
2,4,6-Trichlorophenol U 0.0990 4.23 10 09/03/2018 11:48 WG1159283
(S) 2-Fluorophenol 87.5 12.0-120 09/03/2018 11:48 WG1159283
(S) 2-Fluorophenol 71.0 J7 12.0-120 09/04/2018 16:25 WG1159283
(S) Phenol-d5 76.2 J7 10.0-120 09/04/2018 16:25 WG1159283
(S) Phenol-d5 79.4 10.0-120 09/03/2018 11:48 WG1159283
(S) Nitrobenzene-d5 78.7 J7 10.0-122 09/04/2018 16:25 WG1159283
(S) Nitrobenzene-d5 75.2 10.0-122 09/03/2018 11:48 WG1159283
(S) 2-Fluorobiphenyl 83.2 J7 15.0-120 09/04/2018 16:25 WG1159283
(S) 2-Fluorobiphenyl 90.8 15.0-120 09/03/2018 11:48 WG1159283
(S) 2,4,6-Tribromophenol 98.9 10.0-127 09/03/2018 11:48 WG1159283
(S) 2,4,6-Tribromophenol 86.3 J7 10.0-127 09/04/2018 16:25 WG1159283
(S) p-Terphenyl-d14 83.8 10.0-120 09/03/2018 11:48 WG1159283
(S) p-Terphenyl-d14 87.0 J7 10.0-120 09/04/2018 16:25 WG1159283
Sample Narrative:
L1020964-08 WG1159283: Dilution due to matrix impact during extract concentration procedure
L1020964-08 WG1159283: IS/SURR failed on lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 31 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 31 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L1020964
SWP-5 1-5
Collected date/time: 08/24/18 10:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 78.0 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0702 0.00359 0.0256 1 08/31/2018 12:07 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 1.36 J 0.590 2.56 1 08/31/2018 15:20 WG1159261
Barium 116 0.218 0.641 1 08/31/2018 15:20 WG1159261
Cadmium U 0.0897 0.641 1 08/31/2018 15:20 WG1159261
Chromium 22.9 0.179 1.28 1 08/31/2018 15:20 WG1159261
Lead 12.9 0.244 0.641 1 08/31/2018 15:20 WG1159261
Selenium U 0.795 2.56 1 08/31/2018 15:20 WG1159261
Silver U 0.154 1.28 1 08/31/2018 15:20 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0176 0.0320 1 08/31/2018 00:28 WG1159831
Acrylonitrile U 0.00244 0.0160 1 08/31/2018 00:28 WG1159831
Benzene U 0.000513 0.00128 1 08/31/2018 00:28 WG1159831
Bromobenzene U 0.00135 0.0160 1 08/31/2018 00:28 WG1159831
Bromodichloromethane U 0.00101 0.00320 1 08/31/2018 00:28 WG1159831
Bromoform U 0.00766 0.0320 1 08/31/2018 00:28 WG1159831
Bromomethane U 0.00474 0.0160 1 08/31/2018 00:28 WG1159831
n-Butylbenzene U J4 0.00492 0.0160 1 08/31/2018 00:28 WG1159831
sec-Butylbenzene U 0.00324 0.0160 1 08/31/2018 00:28 WG1159831
tert-Butylbenzene U 0.00199 0.00641 1 08/31/2018 00:28 WG1159831
Carbon tetrachloride U 0.00138 0.00641 1 08/31/2018 00:28 WG1159831
Chlorobenzene U 0.000734 0.00320 1 08/31/2018 00:28 WG1159831
Chlorodibromomethane U 0.000577 0.00320 1 08/31/2018 00:28 WG1159831
Chloroethane U 0.00138 0.00641 1 08/31/2018 00:28 WG1159831
Chloroform U 0.000532 0.00320 1 08/31/2018 00:28 WG1159831
Chloromethane U 0.00178 0.0160 1 08/31/2018 00:28 WG1159831
2-Chlorotoluene U 0.00118 0.00320 1 08/31/2018 00:28 WG1159831
4-Chlorotoluene U 0.00145 0.00641 1 08/31/2018 00:28 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00654 0.0320 1 08/31/2018 00:28 WG1159831
1,2-Dibromoethane U 0.000673 0.00320 1 08/31/2018 00:28 WG1159831
Dibromomethane U 0.00128 0.00641 1 08/31/2018 00:28 WG1159831
1,2-Dichlorobenzene U 0.00186 0.00641 1 08/31/2018 00:28 WG1159831
1,3-Dichlorobenzene U 0.00218 0.00641 1 08/31/2018 00:28 WG1159831
1,4-Dichlorobenzene 0.00404 J 0.00252 0.00641 1 08/31/2018 00:28 WG1159831
Dichlorodifluoromethane U 0.00105 0.00320 1 08/31/2018 00:28 WG1159831
1,1-Dichloroethane U 0.000737 0.00320 1 08/31/2018 00:28 WG1159831
1,2-Dichloroethane U 0.000609 0.00320 1 08/31/2018 00:28 WG1159831
1,1-Dichloroethene U 0.000641 0.00320 1 08/31/2018 00:28 WG1159831
cis-1,2-Dichloroethene 0.00299 J 0.000884 0.00320 1 08/31/2018 00:28 WG1159831
trans-1,2-Dichloroethene U 0.00183 0.00641 1 08/31/2018 00:28 WG1159831
1,2-Dichloropropane U 0.00163 0.00641 1 08/31/2018 00:28 WG1159831
1,1-Dichloropropene U 0.000897 0.00320 1 08/31/2018 00:28 WG1159831
1,3-Dichloropropane U 0.00224 0.00641 1 08/31/2018 00:28 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 32 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 32 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L1020964
SWP-5 1-5
Collected date/time: 08/24/18 10:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000869 0.00320 1 08/31/2018 00:28 WG1159831
trans-1,3-Dichloropropene U 0.00196 0.00641 1 08/31/2018 00:28 WG1159831
2,2-Dichloropropane U 0.00102 0.00320 1 08/31/2018 00:28 WG1159831
Di-isopropyl ether U 0.000449 0.00128 1 08/31/2018 00:28 WG1159831
Ethylbenzene U 0.000679 0.00320 1 08/31/2018 00:28 WG1159831
Hexachloro-1,3-butadiene U 0.0163 0.0320 1 08/31/2018 00:28 WG1159831
Isopropylbenzene U 0.00111 0.00320 1 08/31/2018 00:28 WG1159831
p-Isopropyltoluene U 0.00299 0.00641 1 08/31/2018 00:28 WG1159831
2-Butanone (MEK)0.0229 J 0.0160 0.0320 1 08/31/2018 00:28 WG1159831
Methylene Chloride U 0.00851 0.0320 1 08/31/2018 00:28 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0128 0.0320 1 08/31/2018 00:28 WG1159831
Methyl tert-butyl ether U 0.000378 0.00128 1 08/31/2018 00:28 WG1159831
Naphthalene U 0.00400 0.0160 1 08/31/2018 22:53 WG1160083
n-Propylbenzene U 0.00151 0.00641 1 08/31/2018 00:28 WG1159831
Styrene U 0.00350 0.0160 1 08/31/2018 00:28 WG1159831
1,1,1,2-Tetrachloroethane U 0.000641 0.00320 1 08/31/2018 00:28 WG1159831
1,1,2,2-Tetrachloroethane U 0.000500 0.00320 1 08/31/2018 00:28 WG1159831
Tetrachloroethene U 0.000897 0.00320 1 08/31/2018 00:28 WG1159831
Toluene U 0.00160 0.00641 1 08/31/2018 00:28 WG1159831
1,2,3-Trichlorobenzene U 0.000801 0.00320 1 08/31/2018 00:28 WG1159831
1,2,4-Trichlorobenzene U 0.00618 0.0160 1 08/31/2018 00:28 WG1159831
1,1,1-Trichloroethane U 0.000352 0.00320 1 08/31/2018 00:28 WG1159831
1,1,2-Trichloroethane U 0.00113 0.00320 1 08/31/2018 00:28 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000865 0.00320 1 08/31/2018 00:28 WG1159831
Trichloroethene U 0.000513 0.00128 1 08/31/2018 00:28 WG1159831
Trichlorofluoromethane U 0.000641 0.00320 1 08/31/2018 00:28 WG1159831
1,2,3-Trichloropropane U 0.00654 0.0160 1 08/31/2018 00:28 WG1159831
1,2,4-Trimethylbenzene U 0.00149 0.00641 1 08/31/2018 22:53 WG1160083
1,3,5-Trimethylbenzene U 0.00138 0.00641 1 08/31/2018 00:28 WG1159831
Vinyl chloride U 0.000875 0.00320 1 08/31/2018 00:28 WG1159831
Xylenes, Total U 0.00613 0.00833 1 08/31/2018 00:28 WG1159831
(S) Toluene-d8 106 75.0-131 08/31/2018 00:28 WG1159831
(S) Toluene-d8 106 75.0-131 08/31/2018 22:53 WG1160083
(S) Dibromofluoromethane 101 65.0-129 08/31/2018 00:28 WG1159831
(S) Dibromofluoromethane 92.1 65.0-129 08/31/2018 22:53 WG1160083
(S) 4-Bromofluorobenzene 101 67.0-138 08/31/2018 00:28 WG1159831
(S) 4-Bromofluorobenzene 105 67.0-138 08/31/2018 22:53 WG1160083
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00823 0.0423 1 09/03/2018 04:23 WG1159283
Acenaphthylene U 0.00860 0.0423 1 09/03/2018 04:23 WG1159283
Anthracene U 0.00810 0.0423 1 09/03/2018 04:23 WG1159283
Benzidine U J4 0.0816 0.427 1 09/03/2018 04:23 WG1159283
Benzo(a)anthracene U 0.00549 0.0423 1 09/03/2018 04:23 WG1159283
Benzo(b)fluoranthene U 0.00891 0.0423 1 09/03/2018 04:23 WG1159283
Benzo(k)fluoranthene U 0.00746 0.0423 1 09/03/2018 04:23 WG1159283
Benzo(g,h,i)perylene U 0.00924 0.0423 1 09/03/2018 04:23 WG1159283
Benzo(a)pyrene U 0.00702 0.0423 1 09/03/2018 04:23 WG1159283
Bis(2-chlorethoxy)methane U 0.00987 0.427 1 09/03/2018 04:23 WG1159283
Bis(2-chloroethyl)ether U 0.0115 0.427 1 09/03/2018 04:23 WG1159283
Bis(2-chloroisopropyl)ether U 0.00974 0.427 1 09/03/2018 04:23 WG1159283
4-Bromophenyl-phenylether U 0.0146 0.427 1 09/03/2018 04:23 WG1159283
2-Chloronaphthalene U 0.00819 0.0423 1 09/03/2018 04:23 WG1159283
4-Chlorophenyl-phenylether U 0.00804 0.427 1 09/03/2018 04:23 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 33 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 33 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L1020964
SWP-5 1-5
Collected date/time: 08/24/18 10:25
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Chrysene U 0.00711 0.0423 1 09/03/2018 04:23 WG1159283
Dibenz(a,h)anthracene U 0.0105 0.0423 1 09/03/2018 04:23 WG1159283
3,3-Dichlorobenzidine U 0.102 0.427 1 09/03/2018 04:23 WG1159283
2,4-Dinitrotoluene U 0.00778 0.427 1 09/03/2018 04:23 WG1159283
2,6-Dinitrotoluene U 0.00945 0.427 1 09/03/2018 04:23 WG1159283
Fluoranthene U 0.00636 0.0423 1 09/03/2018 04:23 WG1159283
Fluorene U 0.00874 0.0423 1 09/03/2018 04:23 WG1159283
Hexachlorobenzene U 0.0110 0.427 1 09/03/2018 04:23 WG1159283
Hexachloro-1,3-butadiene U 0.0128 0.427 1 09/03/2018 04:23 WG1159283
Hexachlorocyclopentadiene U 0.0752 0.427 1 09/03/2018 04:23 WG1159283
Hexachloroethane U 0.0172 0.427 1 09/03/2018 04:23 WG1159283
Indeno(1,2,3-cd)pyrene U 0.00989 0.0423 1 09/03/2018 04:23 WG1159283
Isophorone U 0.00669 0.427 1 09/03/2018 04:23 WG1159283
Naphthalene U 0.0114 0.0423 1 09/03/2018 04:23 WG1159283
Nitrobenzene U 0.00891 0.427 1 09/03/2018 04:23 WG1159283
n-Nitrosodimethylamine U 0.0829 0.427 1 09/03/2018 04:23 WG1159283
n-Nitrosodiphenylamine U 0.115 0.427 1 09/03/2018 04:23 WG1159283
n-Nitrosodi-n-propylamine U 0.0116 0.427 1 09/03/2018 04:23 WG1159283
Phenanthrene U 0.00677 0.0423 1 09/03/2018 04:23 WG1159283
Benzylbutyl phthalate U 0.0132 0.427 1 09/03/2018 04:23 WG1159283
Bis(2-ethylhexyl)phthalate U 0.0154 0.427 1 09/03/2018 04:23 WG1159283
Di-n-butyl phthalate U 0.0140 0.427 1 09/03/2018 04:23 WG1159283
Diethyl phthalate U 0.00886 0.427 1 09/03/2018 04:23 WG1159283
Dimethyl phthalate U 0.00692 0.427 1 09/03/2018 04:23 WG1159283
Di-n-octyl phthalate U 0.0116 0.427 1 09/03/2018 04:23 WG1159283
Pyrene U 0.0158 0.0423 1 09/03/2018 04:23 WG1159283
1,2,4-Trichlorobenzene U 0.0112 0.427 1 09/03/2018 04:23 WG1159283
4-Chloro-3-methylphenol U 0.00611 0.427 1 09/03/2018 04:23 WG1159283
2-Chlorophenol U 0.0107 0.427 1 09/03/2018 04:23 WG1159283
2,4-Dichlorophenol U 0.00956 0.427 1 09/03/2018 04:23 WG1159283
2,4-Dimethylphenol U 0.0604 0.427 1 09/03/2018 04:23 WG1159283
4,6-Dinitro-2-methylphenol U 0.159 0.427 1 09/03/2018 04:23 WG1159283
2,4-Dinitrophenol U 0.126 0.427 1 09/03/2018 04:23 WG1159283
2-Nitrophenol U 0.0167 0.427 1 09/03/2018 04:23 WG1159283
4-Nitrophenol U 0.0673 0.427 1 09/03/2018 04:23 WG1159283
Pentachlorophenol U 0.0615 0.427 1 09/03/2018 04:23 WG1159283
Phenol U 0.00891 0.427 1 09/03/2018 04:23 WG1159283
2,4,6-Trichlorophenol U 0.00998 0.427 1 09/03/2018 04:23 WG1159283
(S) 2-Fluorophenol 81.5 12.0-120 09/03/2018 04:23 WG1159283
(S) Phenol-d5 70.5 10.0-120 09/03/2018 04:23 WG1159283
(S) Nitrobenzene-d5 65.0 10.0-122 09/03/2018 04:23 WG1159283
(S) 2-Fluorobiphenyl 76.9 15.0-120 09/03/2018 04:23 WG1159283
(S) 2,4,6-Tribromophenol 91.8 10.0-127 09/03/2018 04:23 WG1159283
(S) p-Terphenyl-d14 80.5 10.0-120 09/03/2018 04:23 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 34 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 34 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L1020964
SWP-5 12-15
Collected date/time: 08/24/18 10:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 92.9 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.00629 B J 0.00301 0.0215 1 08/31/2018 12:10 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic U 0.495 2.15 1 08/31/2018 15:23 WG1159261
Barium 55.8 0.183 0.538 1 08/31/2018 15:23 WG1159261
Cadmium U 0.0753 0.538 1 08/31/2018 15:23 WG1159261
Chromium 34.8 0.151 1.08 1 08/31/2018 15:23 WG1159261
Lead 3.62 0.204 0.538 1 08/31/2018 15:23 WG1159261
Selenium U 0.667 2.15 1 08/31/2018 15:23 WG1159261
Silver U 0.129 1.08 1 08/31/2018 15:23 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0147 0.0269 1 08/31/2018 00:49 WG1159831
Acrylonitrile U 0.00204 0.0135 1 08/31/2018 00:49 WG1159831
Benzene U 0.000431 0.00108 1 08/31/2018 00:49 WG1159831
Bromobenzene U 0.00113 0.0135 1 08/31/2018 00:49 WG1159831
Bromodichloromethane U 0.000848 0.00269 1 08/31/2018 00:49 WG1159831
Bromoform U 0.00644 0.0269 1 08/31/2018 00:49 WG1159831
Bromomethane U 0.00398 0.0135 1 08/31/2018 00:49 WG1159831
n-Butylbenzene U J4 0.00413 0.0135 1 08/31/2018 00:49 WG1159831
sec-Butylbenzene U 0.00272 0.0135 1 08/31/2018 00:49 WG1159831
tert-Butylbenzene U 0.00167 0.00538 1 08/31/2018 00:49 WG1159831
Carbon tetrachloride U 0.00116 0.00538 1 08/31/2018 00:49 WG1159831
Chlorobenzene U 0.000617 0.00269 1 08/31/2018 00:49 WG1159831
Chlorodibromomethane U 0.000484 0.00269 1 08/31/2018 00:49 WG1159831
Chloroethane U 0.00116 0.00538 1 08/31/2018 00:49 WG1159831
Chloroform U 0.000447 0.00269 1 08/31/2018 00:49 WG1159831
Chloromethane U 0.00150 0.0135 1 08/31/2018 00:49 WG1159831
2-Chlorotoluene U 0.000990 0.00269 1 08/31/2018 00:49 WG1159831
4-Chlorotoluene U 0.00122 0.00538 1 08/31/2018 00:49 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00549 0.0269 1 08/31/2018 00:49 WG1159831
1,2-Dibromoethane U 0.000565 0.00269 1 08/31/2018 00:49 WG1159831
Dibromomethane U 0.00108 0.00538 1 08/31/2018 00:49 WG1159831
1,2-Dichlorobenzene U 0.00156 0.00538 1 08/31/2018 00:49 WG1159831
1,3-Dichlorobenzene U 0.00183 0.00538 1 08/31/2018 00:49 WG1159831
1,4-Dichlorobenzene U 0.00212 0.00538 1 08/31/2018 00:49 WG1159831
Dichlorodifluoromethane U 0.000880 0.00269 1 08/31/2018 00:49 WG1159831
1,1-Dichloroethane U 0.000619 0.00269 1 08/31/2018 00:49 WG1159831
1,2-Dichloroethane U 0.000511 0.00269 1 08/31/2018 00:49 WG1159831
1,1-Dichloroethene U 0.000538 0.00269 1 08/31/2018 00:49 WG1159831
cis-1,2-Dichloroethene U 0.000743 0.00269 1 08/31/2018 00:49 WG1159831
trans-1,2-Dichloroethene U 0.00154 0.00538 1 08/31/2018 00:49 WG1159831
1,2-Dichloropropane U 0.00137 0.00538 1 08/31/2018 00:49 WG1159831
1,1-Dichloropropene U 0.000753 0.00269 1 08/31/2018 00:49 WG1159831
1,3-Dichloropropane U 0.00188 0.00538 1 08/31/2018 00:49 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 35 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 35 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L1020964
SWP-5 12-15
Collected date/time: 08/24/18 10:35
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000730 0.00269 1 08/31/2018 00:49 WG1159831
trans-1,3-Dichloropropene U 0.00165 0.00538 1 08/31/2018 00:49 WG1159831
2,2-Dichloropropane U 0.000854 0.00269 1 08/31/2018 00:49 WG1159831
Di-isopropyl ether U 0.000377 0.00108 1 08/31/2018 00:49 WG1159831
Ethylbenzene U 0.000570 0.00269 1 08/31/2018 00:49 WG1159831
Hexachloro-1,3-butadiene U 0.0137 0.0269 1 08/31/2018 00:49 WG1159831
Isopropylbenzene U 0.000929 0.00269 1 08/31/2018 00:49 WG1159831
p-Isopropyltoluene U 0.00251 0.00538 1 08/31/2018 00:49 WG1159831
2-Butanone (MEK)U 0.0135 0.0269 1 08/31/2018 00:49 WG1159831
Methylene Chloride U 0.00715 0.0269 1 08/31/2018 00:49 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0108 0.0269 1 08/31/2018 00:49 WG1159831
Methyl tert-butyl ether U 0.000318 0.00108 1 08/31/2018 00:49 WG1159831
Naphthalene U 0.00336 0.0135 1 08/31/2018 23:12 WG1160083
n-Propylbenzene U 0.00127 0.00538 1 08/31/2018 00:49 WG1159831
Styrene U 0.00294 0.0135 1 08/31/2018 00:49 WG1159831
1,1,1,2-Tetrachloroethane U 0.000538 0.00269 1 08/31/2018 00:49 WG1159831
1,1,2,2-Tetrachloroethane U 0.000420 0.00269 1 08/31/2018 00:49 WG1159831
Tetrachloroethene U 0.000753 0.00269 1 08/31/2018 00:49 WG1159831
Toluene U 0.00135 0.00538 1 08/31/2018 00:49 WG1159831
1,2,3-Trichlorobenzene U 0.000673 0.00269 1 08/31/2018 00:49 WG1159831
1,2,4-Trichlorobenzene U 0.00519 0.0135 1 08/31/2018 00:49 WG1159831
1,1,1-Trichloroethane U 0.000296 0.00269 1 08/31/2018 00:49 WG1159831
1,1,2-Trichloroethane U 0.000950 0.00269 1 08/31/2018 00:49 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000727 0.00269 1 08/31/2018 00:49 WG1159831
Trichloroethene U 0.000431 0.00108 1 08/31/2018 00:49 WG1159831
Trichlorofluoromethane U 0.000538 0.00269 1 08/31/2018 00:49 WG1159831
1,2,3-Trichloropropane U 0.00549 0.0135 1 08/31/2018 00:49 WG1159831
1,2,4-Trimethylbenzene U 0.00125 0.00538 1 08/31/2018 23:12 WG1160083
1,3,5-Trimethylbenzene U 0.00116 0.00538 1 08/31/2018 00:49 WG1159831
Vinyl chloride U 0.000735 0.00269 1 08/31/2018 00:49 WG1159831
Xylenes, Total U 0.00514 0.00700 1 08/31/2018 00:49 WG1159831
(S) Toluene-d8 106 75.0-131 08/31/2018 00:49 WG1159831
(S) Toluene-d8 101 75.0-131 08/31/2018 23:12 WG1160083
(S) Dibromofluoromethane 99.3 65.0-129 08/31/2018 00:49 WG1159831
(S) Dibromofluoromethane 93.1 65.0-129 08/31/2018 23:12 WG1160083
(S) 4-Bromofluorobenzene 101 67.0-138 08/31/2018 00:49 WG1159831
(S) 4-Bromofluorobenzene 104 67.0-138 08/31/2018 23:12 WG1160083
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00691 0.0355 1 09/03/2018 04:46 WG1159283
Acenaphthylene U 0.00722 0.0355 1 09/03/2018 04:46 WG1159283
Anthracene U 0.00680 0.0355 1 09/03/2018 04:46 WG1159283
Benzidine U J4 0.0686 0.358 1 09/03/2018 04:46 WG1159283
Benzo(a)anthracene U 0.00461 0.0355 1 09/03/2018 04:46 WG1159283
Benzo(b)fluoranthene U 0.00748 0.0355 1 09/03/2018 04:46 WG1159283
Benzo(k)fluoranthene U 0.00626 0.0355 1 09/03/2018 04:46 WG1159283
Benzo(g,h,i)perylene U 0.00776 0.0355 1 09/03/2018 04:46 WG1159283
Benzo(a)pyrene U 0.00590 0.0355 1 09/03/2018 04:46 WG1159283
Bis(2-chlorethoxy)methane U 0.00829 0.358 1 09/03/2018 04:46 WG1159283
Bis(2-chloroethyl)ether U 0.00964 0.358 1 09/03/2018 04:46 WG1159283
Bis(2-chloroisopropyl)ether U 0.00818 0.358 1 09/03/2018 04:46 WG1159283
4-Bromophenyl-phenylether U 0.0123 0.358 1 09/03/2018 04:46 WG1159283
2-Chloronaphthalene U 0.00688 0.0355 1 09/03/2018 04:46 WG1159283
4-Chlorophenyl-phenylether U 0.00675 0.358 1 09/03/2018 04:46 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 36 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 36 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L1020964
SWP-5 12-15
Collected date/time: 08/24/18 10:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Chrysene U 0.00597 0.0355 1 09/03/2018 04:46 WG1159283
Dibenz(a,h)anthracene U 0.00884 0.0355 1 09/03/2018 04:46 WG1159283
3,3-Dichlorobenzidine U 0.0855 0.358 1 09/03/2018 04:46 WG1159283
2,4-Dinitrotoluene U 0.00653 0.358 1 09/03/2018 04:46 WG1159283
2,6-Dinitrotoluene U 0.00793 0.358 1 09/03/2018 04:46 WG1159283
Fluoranthene U 0.00534 0.0355 1 09/03/2018 04:46 WG1159283
Fluorene U 0.00734 0.0355 1 09/03/2018 04:46 WG1159283
Hexachlorobenzene U 0.00921 0.358 1 09/03/2018 04:46 WG1159283
Hexachloro-1,3-butadiene U 0.0108 0.358 1 09/03/2018 04:46 WG1159283
Hexachlorocyclopentadiene U 0.0632 0.358 1 09/03/2018 04:46 WG1159283
Hexachloroethane U 0.0144 0.358 1 09/03/2018 04:46 WG1159283
Indeno(1,2,3-cd)pyrene U 0.00831 0.0355 1 09/03/2018 04:46 WG1159283
Isophorone U 0.00562 0.358 1 09/03/2018 04:46 WG1159283
Naphthalene U 0.00957 0.0355 1 09/03/2018 04:46 WG1159283
Nitrobenzene U 0.00748 0.358 1 09/03/2018 04:46 WG1159283
n-Nitrosodimethylamine U 0.0696 0.358 1 09/03/2018 04:46 WG1159283
n-Nitrosodiphenylamine U 0.0969 0.358 1 09/03/2018 04:46 WG1159283
n-Nitrosodi-n-propylamine U 0.00975 0.358 1 09/03/2018 04:46 WG1159283
Phenanthrene U 0.00568 0.0355 1 09/03/2018 04:46 WG1159283
Benzylbutyl phthalate U 0.0111 0.358 1 09/03/2018 04:46 WG1159283
Bis(2-ethylhexyl)phthalate U 0.0129 0.358 1 09/03/2018 04:46 WG1159283
Di-n-butyl phthalate U 0.0117 0.358 1 09/03/2018 04:46 WG1159283
Diethyl phthalate U 0.00744 0.358 1 09/03/2018 04:46 WG1159283
Dimethyl phthalate U 0.00581 0.358 1 09/03/2018 04:46 WG1159283
Di-n-octyl phthalate U 0.00976 0.358 1 09/03/2018 04:46 WG1159283
Pyrene U 0.0132 0.0355 1 09/03/2018 04:46 WG1159283
1,2,4-Trichlorobenzene U 0.00943 0.358 1 09/03/2018 04:46 WG1159283
4-Chloro-3-methylphenol U 0.00513 0.358 1 09/03/2018 04:46 WG1159283
2-Chlorophenol U 0.00894 0.358 1 09/03/2018 04:46 WG1159283
2,4-Dichlorophenol U 0.00803 0.358 1 09/03/2018 04:46 WG1159283
2,4-Dimethylphenol U 0.0507 0.358 1 09/03/2018 04:46 WG1159283
4,6-Dinitro-2-methylphenol U 0.133 0.358 1 09/03/2018 04:46 WG1159283
2,4-Dinitrophenol U 0.105 0.358 1 09/03/2018 04:46 WG1159283
2-Nitrophenol U 0.0140 0.358 1 09/03/2018 04:46 WG1159283
4-Nitrophenol U 0.0565 0.358 1 09/03/2018 04:46 WG1159283
Pentachlorophenol U 0.0517 0.358 1 09/03/2018 04:46 WG1159283
Phenol U 0.00748 0.358 1 09/03/2018 04:46 WG1159283
2,4,6-Trichlorophenol U 0.00838 0.358 1 09/03/2018 04:46 WG1159283
(S) 2-Fluorophenol 81.2 12.0-120 09/03/2018 04:46 WG1159283
(S) Phenol-d5 71.4 10.0-120 09/03/2018 04:46 WG1159283
(S) Nitrobenzene-d5 66.9 10.0-122 09/03/2018 04:46 WG1159283
(S) 2-Fluorobiphenyl 80.1 15.0-120 09/03/2018 04:46 WG1159283
(S) 2,4,6-Tribromophenol 95.8 10.0-127 09/03/2018 04:46 WG1159283
(S) p-Terphenyl-d14 70.8 10.0-120 09/03/2018 04:46 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 37 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L1020964
SWP-6 1-5
Collected date/time: 08/24/18 10:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.7 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.111 0.00347 0.0248 1 08/31/2018 12:12 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.55 0.570 2.48 1 08/31/2018 15:26 WG1159261
Barium 114 0.211 0.619 1 08/31/2018 15:26 WG1159261
Cadmium 0.143 J 0.0867 0.619 1 08/31/2018 15:26 WG1159261
Chromium 28.5 0.173 1.24 1 08/31/2018 15:26 WG1159261
Lead 79.5 0.235 0.619 1 08/31/2018 15:26 WG1159261
Selenium U 0.768 2.48 1 08/31/2018 15:26 WG1159261
Silver U 0.149 1.24 1 08/31/2018 15:26 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0170 0.0310 1 08/31/2018 01:09 WG1159831
Acrylonitrile U 0.00235 0.0155 1 08/31/2018 01:09 WG1159831
Benzene U 0.000495 0.00124 1 08/31/2018 01:09 WG1159831
Bromobenzene U 0.00130 0.0155 1 08/31/2018 01:09 WG1159831
Bromodichloromethane U 0.000976 0.00310 1 08/31/2018 01:09 WG1159831
Bromoform U 0.00741 0.0310 1 08/31/2018 01:09 WG1159831
Bromomethane U 0.00458 0.0155 1 08/31/2018 01:09 WG1159831
n-Butylbenzene U J4 0.00476 0.0155 1 08/31/2018 01:09 WG1159831
sec-Butylbenzene U 0.00313 0.0155 1 08/31/2018 01:09 WG1159831
tert-Butylbenzene U 0.00192 0.00619 1 08/31/2018 01:09 WG1159831
Carbon tetrachloride U 0.00134 0.00619 1 08/31/2018 01:09 WG1159831
Chlorobenzene U 0.000710 0.00310 1 08/31/2018 01:09 WG1159831
Chlorodibromomethane U 0.000557 0.00310 1 08/31/2018 01:09 WG1159831
Chloroethane U 0.00134 0.00619 1 08/31/2018 01:09 WG1159831
Chloroform U 0.000514 0.00310 1 08/31/2018 01:09 WG1159831
Chloromethane U 0.00172 0.0155 1 08/31/2018 01:09 WG1159831
2-Chlorotoluene U 0.00114 0.00310 1 08/31/2018 01:09 WG1159831
4-Chlorotoluene U 0.00140 0.00619 1 08/31/2018 01:09 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00632 0.0310 1 08/31/2018 01:09 WG1159831
1,2-Dibromoethane U 0.000650 0.00310 1 08/31/2018 01:09 WG1159831
Dibromomethane U 0.00124 0.00619 1 08/31/2018 01:09 WG1159831
1,2-Dichlorobenzene U 0.00180 0.00619 1 08/31/2018 01:09 WG1159831
1,3-Dichlorobenzene U 0.00211 0.00619 1 08/31/2018 01:09 WG1159831
1,4-Dichlorobenzene U 0.00244 0.00619 1 08/31/2018 01:09 WG1159831
Dichlorodifluoromethane U 0.00101 0.00310 1 08/31/2018 01:09 WG1159831
1,1-Dichloroethane U 0.000712 0.00310 1 08/31/2018 01:09 WG1159831
1,2-Dichloroethane U 0.000588 0.00310 1 08/31/2018 01:09 WG1159831
1,1-Dichloroethene U 0.000619 0.00310 1 08/31/2018 01:09 WG1159831
cis-1,2-Dichloroethene U 0.000855 0.00310 1 08/31/2018 01:09 WG1159831
trans-1,2-Dichloroethene U 0.00177 0.00619 1 08/31/2018 01:09 WG1159831
1,2-Dichloropropane U 0.00157 0.00619 1 08/31/2018 01:09 WG1159831
1,1-Dichloropropene U 0.000867 0.00310 1 08/31/2018 01:09 WG1159831
1,3-Dichloropropane U 0.00217 0.00619 1 08/31/2018 01:09 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 38 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 38 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L1020964
SWP-6 1-5
Collected date/time: 08/24/18 10:45
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000840 0.00310 1 08/31/2018 01:09 WG1159831
trans-1,3-Dichloropropene U 0.00189 0.00619 1 08/31/2018 01:09 WG1159831
2,2-Dichloropropane U 0.000982 0.00310 1 08/31/2018 01:09 WG1159831
Di-isopropyl ether U 0.000433 0.00124 1 08/31/2018 01:09 WG1159831
Ethylbenzene U 0.000656 0.00310 1 08/31/2018 01:09 WG1159831
Hexachloro-1,3-butadiene U 0.0157 0.0310 1 08/31/2018 01:09 WG1159831
Isopropylbenzene U 0.00107 0.00310 1 08/31/2018 01:09 WG1159831
p-Isopropyltoluene U 0.00289 0.00619 1 08/31/2018 01:09 WG1159831
2-Butanone (MEK)U 0.0155 0.0310 1 08/31/2018 01:09 WG1159831
Methylene Chloride U 0.00822 0.0310 1 08/31/2018 01:09 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0124 0.0310 1 08/31/2018 01:09 WG1159831
Methyl tert-butyl ether U 0.000365 0.00124 1 08/31/2018 01:09 WG1159831
Naphthalene 0.00481 J 0.00386 0.0155 1 08/31/2018 23:31 WG1160083
n-Propylbenzene U 0.00146 0.00619 1 08/31/2018 01:09 WG1159831
Styrene U 0.00338 0.0155 1 08/31/2018 01:09 WG1159831
1,1,1,2-Tetrachloroethane U 0.000619 0.00310 1 08/31/2018 01:09 WG1159831
1,1,2,2-Tetrachloroethane U 0.000483 0.00310 1 08/31/2018 01:09 WG1159831
Tetrachloroethene U 0.000867 0.00310 1 08/31/2018 01:09 WG1159831
Toluene U 0.00155 0.00619 1 08/31/2018 01:09 WG1159831
1,2,3-Trichlorobenzene U 0.000774 0.00310 1 08/31/2018 01:09 WG1159831
1,2,4-Trichlorobenzene U 0.00597 0.0155 1 08/31/2018 01:09 WG1159831
1,1,1-Trichloroethane U 0.000341 0.00310 1 08/31/2018 01:09 WG1159831
1,1,2-Trichloroethane U 0.00109 0.00310 1 08/31/2018 01:09 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000836 0.00310 1 08/31/2018 01:09 WG1159831
Trichloroethene U 0.000495 0.00124 1 08/31/2018 01:09 WG1159831
Trichlorofluoromethane U 0.000619 0.00310 1 08/31/2018 01:09 WG1159831
1,2,3-Trichloropropane U 0.00632 0.0155 1 08/31/2018 01:09 WG1159831
1,2,4-Trimethylbenzene U 0.00144 0.00619 1 08/31/2018 23:31 WG1160083
1,3,5-Trimethylbenzene U 0.00134 0.00619 1 08/31/2018 01:09 WG1159831
Vinyl chloride U 0.000846 0.00310 1 08/31/2018 01:09 WG1159831
Xylenes, Total U B 0.00592 0.00805 1 08/31/2018 01:09 WG1159831
(S) Toluene-d8 111 75.0-131 08/31/2018 01:09 WG1159831
(S) Toluene-d8 103 75.0-131 08/31/2018 23:31 WG1160083
(S) Dibromofluoromethane 102 65.0-129 08/31/2018 01:09 WG1159831
(S) Dibromofluoromethane 94.6 65.0-129 08/31/2018 23:31 WG1160083
(S) 4-Bromofluorobenzene 102 67.0-138 08/31/2018 01:09 WG1159831
(S) 4-Bromofluorobenzene 108 67.0-138 08/31/2018 23:31 WG1160083
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.0398 0.204 5 09/03/2018 08:17 WG1159283
Acenaphthylene U 0.0415 0.204 5 09/03/2018 08:17 WG1159283
Anthracene 0.0572 J 0.0391 0.204 5 09/03/2018 08:17 WG1159283
Benzidine U J4 J6 0.395 2.07 5 09/03/2018 08:17 WG1159283
Benzo(a)anthracene 0.194 B J 0.0265 0.204 5 09/03/2018 08:17 WG1159283
Benzo(b)fluoranthene 0.258 0.0430 0.204 5 09/03/2018 08:17 WG1159283
Benzo(k)fluoranthene 0.0825 J 0.0360 0.204 5 09/03/2018 08:17 WG1159283
Benzo(g,h,i)perylene 0.0911 J 0.0447 0.204 5 09/03/2018 08:17 WG1159283
Benzo(a)pyrene 0.182 J 0.0339 0.204 5 09/03/2018 08:17 WG1159283
Bis(2-chlorethoxy)methane U 0.0477 2.07 5 09/03/2018 08:17 WG1159283
Bis(2-chloroethyl)ether U 0.0555 2.07 5 09/03/2018 08:17 WG1159283
Bis(2-chloroisopropyl)ether U 0.0471 2.07 5 09/03/2018 08:17 WG1159283
4-Bromophenyl-phenylether U 0.0706 2.07 5 09/03/2018 08:17 WG1159283
2-Chloronaphthalene U 0.0396 0.204 5 09/03/2018 08:17 WG1159283
4-Chlorophenyl-phenylether U 0.0389 2.07 5 09/03/2018 08:17 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 39 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 39 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L1020964
SWP-6 1-5
Collected date/time: 08/24/18 10:45
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Chrysene 0.182 J 0.0344 0.204 5 09/03/2018 08:17 WG1159283
Dibenz(a,h)anthracene U 0.0509 0.204 5 09/03/2018 08:17 WG1159283
3,3-Dichlorobenzidine U J3 J6 0.492 2.07 5 09/03/2018 08:17 WG1159283
2,4-Dinitrotoluene U 0.0376 2.07 5 09/03/2018 08:17 WG1159283
2,6-Dinitrotoluene U 0.0457 2.07 5 09/03/2018 08:17 WG1159283
Fluoranthene 0.326 0.0307 0.204 5 09/03/2018 08:17 WG1159283
Fluorene U 0.0422 0.204 5 09/03/2018 08:17 WG1159283
Hexachlorobenzene U 0.0530 2.07 5 09/03/2018 08:17 WG1159283
Hexachloro-1,3-butadiene U 0.0619 2.07 5 09/03/2018 08:17 WG1159283
Hexachlorocyclopentadiene U J6 0.363 2.07 5 09/03/2018 08:17 WG1159283
Hexachloroethane U 0.0830 2.07 5 09/03/2018 08:17 WG1159283
Indeno(1,2,3-cd)pyrene 0.572 J6 0.0478 0.204 5 09/03/2018 08:17 WG1159283
Isophorone U 0.0323 2.07 5 09/03/2018 08:17 WG1159283
Naphthalene U 0.0551 0.204 5 09/03/2018 08:17 WG1159283
Nitrobenzene U 0.0430 2.07 5 09/03/2018 08:17 WG1159283
n-Nitrosodimethylamine U J6 0.400 2.07 5 09/03/2018 08:17 WG1159283
n-Nitrosodiphenylamine U 0.557 2.07 5 09/03/2018 08:17 WG1159283
n-Nitrosodi-n-propylamine U 0.0561 2.07 5 09/03/2018 08:17 WG1159283
Phenanthrene 0.144 J 0.0327 0.204 5 09/03/2018 08:17 WG1159283
Benzylbutyl phthalate U 0.0638 2.07 5 09/03/2018 08:17 WG1159283
Bis(2-ethylhexyl)phthalate U 0.0743 2.07 5 09/03/2018 08:17 WG1159283
Di-n-butyl phthalate U 0.0675 2.07 5 09/03/2018 08:17 WG1159283
Diethyl phthalate U 0.0428 2.07 5 09/03/2018 08:17 WG1159283
Dimethyl phthalate U 0.0334 2.07 5 09/03/2018 08:17 WG1159283
Di-n-octyl phthalate U 0.0562 2.07 5 09/03/2018 08:17 WG1159283
Pyrene 0.312 0.0762 0.204 5 09/03/2018 08:17 WG1159283
1,2,4-Trichlorobenzene U 0.0542 2.07 5 09/03/2018 08:17 WG1159283
4-Chloro-3-methylphenol U 0.0296 2.07 5 09/03/2018 08:17 WG1159283
2-Chlorophenol U 0.0514 2.07 5 09/03/2018 08:17 WG1159283
2,4-Dichlorophenol U 0.0462 2.07 5 09/03/2018 08:17 WG1159283
2,4-Dimethylphenol U 0.292 2.07 5 09/03/2018 08:17 WG1159283
4,6-Dinitro-2-methylphenol U J6 0.768 2.07 5 09/03/2018 08:17 WG1159283
2,4-Dinitrophenol U J6 0.607 2.07 5 09/03/2018 08:17 WG1159283
2-Nitrophenol U 0.0805 2.07 5 09/03/2018 08:17 WG1159283
4-Nitrophenol U 0.326 2.07 5 09/03/2018 08:17 WG1159283
Pentachlorophenol U J3 0.297 2.07 5 09/03/2018 08:17 WG1159283
Phenol U 0.0430 2.07 5 09/03/2018 08:17 WG1159283
2,4,6-Trichlorophenol U 0.0482 2.07 5 09/03/2018 08:17 WG1159283
(S) 2-Fluorophenol 73.3 12.0-120 09/03/2018 08:17 WG1159283
(S) Phenol-d5 65.2 10.0-120 09/03/2018 08:17 WG1159283
(S) Nitrobenzene-d5 60.2 10.0-122 09/03/2018 08:17 WG1159283
(S) 2-Fluorobiphenyl 74.7 15.0-120 09/03/2018 08:17 WG1159283
(S) 2,4,6-Tribromophenol 82.4 10.0-127 09/03/2018 08:17 WG1159283
(S) p-Terphenyl-d14 66.3 10.0-120 09/03/2018 08:17 WG1159283
Sample Narrative:
L1020964-11 WG1159283: Dilution due to matrix
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 40 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 40 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L1020964
SWP-6 10-15
Collected date/time: 08/24/18 10:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 84.0 1 08/30/2018 13:29 WG1159446
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.110 0.00333 0.0238 1 08/31/2018 12:15 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 5.61 0.548 2.38 1 08/31/2018 15:28 WG1159261
Barium 65.4 0.202 0.595 1 08/31/2018 15:28 WG1159261
Cadmium 0.154 J 0.0833 0.595 1 08/31/2018 15:28 WG1159261
Chromium 50.7 0.167 1.19 1 08/31/2018 15:28 WG1159261
Lead 145 0.226 0.595 1 08/31/2018 15:28 WG1159261
Selenium U 0.738 2.38 1 08/31/2018 15:28 WG1159261
Silver U 0.143 1.19 1 08/31/2018 15:28 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0163 0.0298 1 08/31/2018 01:29 WG1159831
Acrylonitrile U 0.00226 0.0149 1 08/31/2018 01:29 WG1159831
Benzene U 0.000476 0.00119 1 08/31/2018 01:29 WG1159831
Bromobenzene U 0.00125 0.0149 1 08/31/2018 01:29 WG1159831
Bromodichloromethane U 0.000938 0.00298 1 08/31/2018 01:29 WG1159831
Bromoform U 0.00712 0.0298 1 08/31/2018 01:29 WG1159831
Bromomethane U 0.00441 0.0149 1 08/31/2018 01:29 WG1159831
n-Butylbenzene U J4 0.00457 0.0149 1 08/31/2018 01:29 WG1159831
sec-Butylbenzene U 0.00301 0.0149 1 08/31/2018 01:29 WG1159831
tert-Butylbenzene U 0.00185 0.00595 1 08/31/2018 01:29 WG1159831
Carbon tetrachloride U 0.00129 0.00595 1 08/31/2018 01:29 WG1159831
Chlorobenzene 0.00877 0.000682 0.00298 1 08/31/2018 01:29 WG1159831
Chlorodibromomethane U 0.000536 0.00298 1 08/31/2018 01:29 WG1159831
Chloroethane U 0.00129 0.00595 1 08/31/2018 01:29 WG1159831
Chloroform 0.00125 J 0.000494 0.00298 1 08/31/2018 01:29 WG1159831
Chloromethane U 0.00165 0.0149 1 08/31/2018 01:29 WG1159831
2-Chlorotoluene U 0.00110 0.00298 1 08/31/2018 01:29 WG1159831
4-Chlorotoluene U 0.00135 0.00595 1 08/31/2018 01:29 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00607 0.0298 1 08/31/2018 01:29 WG1159831
1,2-Dibromoethane U 0.000625 0.00298 1 08/31/2018 01:29 WG1159831
Dibromomethane U 0.00119 0.00595 1 08/31/2018 01:29 WG1159831
1,2-Dichlorobenzene U 0.00173 0.00595 1 08/31/2018 01:29 WG1159831
1,3-Dichlorobenzene 0.00510 J 0.00202 0.00595 1 08/31/2018 01:29 WG1159831
1,4-Dichlorobenzene 0.00745 0.00235 0.00595 1 08/31/2018 01:29 WG1159831
Dichlorodifluoromethane U 0.000974 0.00298 1 08/31/2018 01:29 WG1159831
1,1-Dichloroethane U 0.000685 0.00298 1 08/31/2018 01:29 WG1159831
1,2-Dichloroethane 0.0220 0.000566 0.00298 1 08/31/2018 01:29 WG1159831
1,1-Dichloroethene 0.00687 0.000595 0.00298 1 08/31/2018 01:29 WG1159831
cis-1,2-Dichloroethene 0.0106 0.000822 0.00298 1 08/31/2018 01:29 WG1159831
trans-1,2-Dichloroethene U 0.00170 0.00595 1 08/31/2018 01:29 WG1159831
1,2-Dichloropropane U 0.00151 0.00595 1 08/31/2018 01:29 WG1159831
1,1-Dichloropropene U 0.000833 0.00298 1 08/31/2018 01:29 WG1159831
1,3-Dichloropropane U 0.00208 0.00595 1 08/31/2018 01:29 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 41 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 41 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L1020964
SWP-6 10-15
Collected date/time: 08/24/18 10:55
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000807 0.00298 1 08/31/2018 01:29 WG1159831
trans-1,3-Dichloropropene U 0.00182 0.00595 1 08/31/2018 01:29 WG1159831
2,2-Dichloropropane U 0.000944 0.00298 1 08/31/2018 01:29 WG1159831
Di-isopropyl ether 0.00158 0.000417 0.00119 1 08/31/2018 01:29 WG1159831
Ethylbenzene 0.00102 J 0.000631 0.00298 1 08/31/2018 01:29 WG1159831
Hexachloro-1,3-butadiene U 0.0151 0.0298 1 08/31/2018 01:29 WG1159831
Isopropylbenzene U 0.00103 0.00298 1 08/31/2018 01:29 WG1159831
p-Isopropyltoluene U 0.00277 0.00595 1 08/31/2018 01:29 WG1159831
2-Butanone (MEK)U 0.0149 0.0298 1 08/31/2018 01:29 WG1159831
Methylene Chloride U 0.00791 0.0298 1 08/31/2018 01:29 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0119 0.0298 1 08/31/2018 01:29 WG1159831
Methyl tert-butyl ether U 0.000351 0.00119 1 08/31/2018 01:29 WG1159831
Naphthalene 0.0271 0.00371 0.0149 1 08/31/2018 01:29 WG1159831
n-Propylbenzene U 0.00140 0.00595 1 08/31/2018 01:29 WG1159831
Styrene U 0.00325 0.0149 1 08/31/2018 01:29 WG1159831
1,1,1,2-Tetrachloroethane U 0.000595 0.00298 1 08/31/2018 01:29 WG1159831
1,1,2,2-Tetrachloroethane U 0.000464 0.00298 1 08/31/2018 01:29 WG1159831
Tetrachloroethene 0.108 0.000833 0.00298 1 08/31/2018 01:29 WG1159831
Toluene 0.00574 J 0.00149 0.00595 1 08/31/2018 01:29 WG1159831
1,2,3-Trichlorobenzene U 0.000744 0.00298 1 08/31/2018 01:29 WG1159831
1,2,4-Trichlorobenzene U 0.00574 0.0149 1 08/31/2018 01:29 WG1159831
1,1,1-Trichloroethane U 0.000327 0.00298 1 08/31/2018 01:29 WG1159831
1,1,2-Trichloroethane U 0.00105 0.00298 1 08/31/2018 01:29 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000804 0.00298 1 08/31/2018 01:29 WG1159831
Trichloroethene 0.667 0.000476 0.00119 1 08/31/2018 01:29 WG1159831
Trichlorofluoromethane U 0.000595 0.00298 1 08/31/2018 01:29 WG1159831
1,2,3-Trichloropropane U 0.00607 0.0149 1 08/31/2018 01:29 WG1159831
1,2,4-Trimethylbenzene 0.00243 B J 0.00138 0.00595 1 08/31/2018 01:29 WG1159831
1,3,5-Trimethylbenzene U 0.00129 0.00595 1 08/31/2018 01:29 WG1159831
Vinyl chloride U 0.000813 0.00298 1 08/31/2018 01:29 WG1159831
Xylenes, Total 0.00691 B J 0.00569 0.00774 1 08/31/2018 01:29 WG1159831
(S) Toluene-d8 100 75.0-131 08/31/2018 01:29 WG1159831
(S) Dibromofluoromethane 99.3 65.0-129 08/31/2018 01:29 WG1159831
(S) 4-Bromofluorobenzene 103 67.0-138 08/31/2018 01:29 WG1159831
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0667 J 0.0382 0.196 5 09/03/2018 09:51 WG1159283
Acenaphthylene 0.186 J 0.0399 0.196 5 09/03/2018 09:51 WG1159283
Anthracene 0.255 0.0376 0.196 5 09/03/2018 09:51 WG1159283
Benzidine U J4 0.380 1.99 5 09/03/2018 09:51 WG1159283
Benzo(a)anthracene 0.968 0.0255 0.196 5 09/03/2018 09:51 WG1159283
Benzo(b)fluoranthene 1.38 0.0413 0.196 5 09/03/2018 09:51 WG1159283
Benzo(k)fluoranthene 0.417 0.0346 0.196 5 09/03/2018 09:51 WG1159283
Benzo(g,h,i)perylene 0.370 0.0430 0.196 5 09/03/2018 09:51 WG1159283
Benzo(a)pyrene 1.05 0.0326 0.196 5 09/03/2018 09:51 WG1159283
Bis(2-chlorethoxy)methane U 0.0458 1.99 5 09/03/2018 09:51 WG1159283
Bis(2-chloroethyl)ether U 0.0533 1.99 5 09/03/2018 09:51 WG1159283
Bis(2-chloroisopropyl)ether U 0.0452 1.99 5 09/03/2018 09:51 WG1159283
4-Bromophenyl-phenylether U 0.0679 1.99 5 09/03/2018 09:51 WG1159283
2-Chloronaphthalene U 0.0381 0.196 5 09/03/2018 09:51 WG1159283
4-Chlorophenyl-phenylether U 0.0374 1.99 5 09/03/2018 09:51 WG1159283
Chrysene 0.927 0.0331 0.196 5 09/03/2018 09:51 WG1159283
Dibenz(a,h)anthracene 0.288 0.0489 0.196 5 09/03/2018 09:51 WG1159283
3,3-Dichlorobenzidine U 0.473 1.99 5 09/03/2018 09:51 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 42 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 42 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L1020964
SWP-6 10-15
Collected date/time: 08/24/18 10:55
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
2,4-Dinitrotoluene U 0.0362 1.99 5 09/03/2018 09:51 WG1159283
2,6-Dinitrotoluene U 0.0439 1.99 5 09/03/2018 09:51 WG1159283
Fluoranthene 1.35 0.0295 0.196 5 09/03/2018 09:51 WG1159283
Fluorene 0.0761 J 0.0406 0.196 5 09/03/2018 09:51 WG1159283
Hexachlorobenzene U 0.0510 1.99 5 09/03/2018 09:51 WG1159283
Hexachloro-1,3-butadiene U 0.0595 1.99 5 09/03/2018 09:51 WG1159283
Hexachlorocyclopentadiene U 0.349 1.99 5 09/03/2018 09:51 WG1159283
Hexachloroethane U 0.0798 1.99 5 09/03/2018 09:51 WG1159283
Indeno(1,2,3-cd)pyrene 2.39 0.0460 0.196 5 09/03/2018 09:51 WG1159283
Isophorone U 0.0311 1.99 5 09/03/2018 09:51 WG1159283
Naphthalene 0.120 J 0.0530 0.196 5 09/03/2018 09:51 WG1159283
Nitrobenzene U 0.0413 1.99 5 09/03/2018 09:51 WG1159283
n-Nitrosodimethylamine U 0.385 1.99 5 09/03/2018 09:51 WG1159283
n-Nitrosodiphenylamine U 0.536 1.99 5 09/03/2018 09:51 WG1159283
n-Nitrosodi-n-propylamine U 0.0539 1.99 5 09/03/2018 09:51 WG1159283
Phenanthrene 0.451 0.0314 0.196 5 09/03/2018 09:51 WG1159283
Benzylbutyl phthalate U 0.0613 1.99 5 09/03/2018 09:51 WG1159283
Bis(2-ethylhexyl)phthalate U 0.0714 1.99 5 09/03/2018 09:51 WG1159283
Di-n-butyl phthalate U 0.0649 1.99 5 09/03/2018 09:51 WG1159283
Diethyl phthalate U 0.0412 1.99 5 09/03/2018 09:51 WG1159283
Dimethyl phthalate U 0.0321 1.99 5 09/03/2018 09:51 WG1159283
Di-n-octyl phthalate U 0.0541 1.99 5 09/03/2018 09:51 WG1159283
Pyrene 1.55 0.0732 0.196 5 09/03/2018 09:51 WG1159283
1,2,4-Trichlorobenzene 0.154 J 0.0521 1.99 5 09/03/2018 09:51 WG1159283
4-Chloro-3-methylphenol U 0.0285 1.99 5 09/03/2018 09:51 WG1159283
2-Chlorophenol U 0.0494 1.99 5 09/03/2018 09:51 WG1159283
2,4-Dichlorophenol U 0.0444 1.99 5 09/03/2018 09:51 WG1159283
2,4-Dimethylphenol U 0.281 1.99 5 09/03/2018 09:51 WG1159283
4,6-Dinitro-2-methylphenol U 0.738 1.99 5 09/03/2018 09:51 WG1159283
2,4-Dinitrophenol U 0.583 1.99 5 09/03/2018 09:51 WG1159283
2-Nitrophenol U 0.0774 1.99 5 09/03/2018 09:51 WG1159283
4-Nitrophenol U 0.313 1.99 5 09/03/2018 09:51 WG1159283
Pentachlorophenol U 0.286 1.99 5 09/03/2018 09:51 WG1159283
Phenol U 0.0413 1.99 5 09/03/2018 09:51 WG1159283
2,4,6-Trichlorophenol U 0.0463 1.99 5 09/03/2018 09:51 WG1159283
(S) 2-Fluorophenol 70.3 12.0-120 09/03/2018 09:51 WG1159283
(S) Phenol-d5 64.1 10.0-120 09/03/2018 09:51 WG1159283
(S) Nitrobenzene-d5 57.6 10.0-122 09/03/2018 09:51 WG1159283
(S) 2-Fluorobiphenyl 74.2 15.0-120 09/03/2018 09:51 WG1159283
(S) 2,4,6-Tribromophenol 87.9 10.0-127 09/03/2018 09:51 WG1159283
(S) p-Terphenyl-d14 77.0 10.0-120 09/03/2018 09:51 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 43 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 43 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L1020964
SWP-7 2-5
Collected date/time: 08/24/18 11:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.8 1 08/30/2018 12:50 WG1159535
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.165 0.00338 0.0242 1 08/31/2018 12:18 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 4.18 0.556 2.42 1 08/31/2018 15:31 WG1159261
Barium 122 0.205 0.604 1 08/31/2018 15:31 WG1159261
Cadmium 0.469 J 0.0846 0.604 1 08/31/2018 15:31 WG1159261
Chromium 23.5 0.169 1.21 1 08/31/2018 15:31 WG1159261
Lead 167 0.230 0.604 1 08/31/2018 15:31 WG1159261
Selenium U 0.749 2.42 1 08/31/2018 15:31 WG1159261
Silver U 0.145 1.21 1 08/31/2018 15:31 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0166 0.0302 1 08/31/2018 01:50 WG1159831
Acrylonitrile U 0.00230 0.0151 1 08/31/2018 01:50 WG1159831
Benzene U 0.000483 0.00121 1 08/31/2018 01:50 WG1159831
Bromobenzene U 0.00127 0.0151 1 08/31/2018 01:50 WG1159831
Bromodichloromethane U 0.000952 0.00302 1 08/31/2018 01:50 WG1159831
Bromoform U 0.00723 0.0302 1 08/31/2018 01:50 WG1159831
Bromomethane U 0.00447 0.0151 1 08/31/2018 01:50 WG1159831
n-Butylbenzene U J4 0.00464 0.0151 1 08/31/2018 01:50 WG1159831
sec-Butylbenzene U 0.00306 0.0151 1 08/31/2018 01:50 WG1159831
tert-Butylbenzene U 0.00187 0.00604 1 08/31/2018 01:50 WG1159831
Carbon tetrachloride U 0.00130 0.00604 1 08/31/2018 01:50 WG1159831
Chlorobenzene 0.00614 0.000692 0.00302 1 08/31/2018 01:50 WG1159831
Chlorodibromomethane U 0.000544 0.00302 1 08/31/2018 01:50 WG1159831
Chloroethane U 0.00130 0.00604 1 08/31/2018 01:50 WG1159831
Chloroform U 0.000501 0.00302 1 08/31/2018 01:50 WG1159831
Chloromethane U 0.00168 0.0151 1 08/31/2018 01:50 WG1159831
2-Chlorotoluene U 0.00111 0.00302 1 08/31/2018 01:50 WG1159831
4-Chlorotoluene U 0.00137 0.00604 1 08/31/2018 01:50 WG1159831
1,2-Dibromo-3-Chloropropane U 0.00616 0.0302 1 08/31/2018 01:50 WG1159831
1,2-Dibromoethane U 0.000634 0.00302 1 08/31/2018 01:50 WG1159831
Dibromomethane U 0.00121 0.00604 1 08/31/2018 01:50 WG1159831
1,2-Dichlorobenzene U 0.00175 0.00604 1 08/31/2018 01:50 WG1159831
1,3-Dichlorobenzene 0.0119 0.00205 0.00604 1 08/31/2018 01:50 WG1159831
1,4-Dichlorobenzene 0.0328 0.00238 0.00604 1 08/31/2018 01:50 WG1159831
Dichlorodifluoromethane U 0.000988 0.00302 1 08/31/2018 01:50 WG1159831
1,1-Dichloroethane U 0.000695 0.00302 1 08/31/2018 01:50 WG1159831
1,2-Dichloroethane U 0.000574 0.00302 1 08/31/2018 01:50 WG1159831
1,1-Dichloroethene U 0.000604 0.00302 1 08/31/2018 01:50 WG1159831
cis-1,2-Dichloroethene 0.00291 J 0.000834 0.00302 1 08/31/2018 01:50 WG1159831
trans-1,2-Dichloroethene U 0.00173 0.00604 1 08/31/2018 01:50 WG1159831
1,2-Dichloropropane U 0.00153 0.00604 1 08/31/2018 01:50 WG1159831
1,1-Dichloropropene U 0.000846 0.00302 1 08/31/2018 01:50 WG1159831
1,3-Dichloropropane U 0.00211 0.00604 1 08/31/2018 01:50 WG1159831
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 44 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 44 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L1020964
SWP-7 2-5
Collected date/time: 08/24/18 11:05
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000819 0.00302 1 08/31/2018 01:50 WG1159831
trans-1,3-Dichloropropene U 0.00185 0.00604 1 08/31/2018 01:50 WG1159831
2,2-Dichloropropane U 0.000958 0.00302 1 08/31/2018 01:50 WG1159831
Di-isopropyl ether U 0.000423 0.00121 1 08/31/2018 01:50 WG1159831
Ethylbenzene 0.00262 J 0.000640 0.00302 1 08/31/2018 01:50 WG1159831
Hexachloro-1,3-butadiene U 0.0153 0.0302 1 08/31/2018 01:50 WG1159831
Isopropylbenzene U 0.00104 0.00302 1 08/31/2018 01:50 WG1159831
p-Isopropyltoluene U 0.00282 0.00604 1 08/31/2018 01:50 WG1159831
2-Butanone (MEK)U 0.0151 0.0302 1 08/31/2018 01:50 WG1159831
Methylene Chloride U 0.00802 0.0302 1 08/31/2018 01:50 WG1159831
4-Methyl-2-pentanone (MIBK) U 0.0121 0.0302 1 08/31/2018 01:50 WG1159831
Methyl tert-butyl ether U 0.000356 0.00121 1 08/31/2018 01:50 WG1159831
Naphthalene 0.0381 0.00377 0.0151 1 08/31/2018 01:50 WG1159831
n-Propylbenzene U 0.00143 0.00604 1 08/31/2018 01:50 WG1159831
Styrene U 0.00330 0.0151 1 08/31/2018 01:50 WG1159831
1,1,1,2-Tetrachloroethane U 0.000604 0.00302 1 08/31/2018 01:50 WG1159831
1,1,2,2-Tetrachloroethane U 0.000471 0.00302 1 08/31/2018 01:50 WG1159831
Tetrachloroethene 0.00776 0.000846 0.00302 1 08/31/2018 01:50 WG1159831
Toluene 0.00527 J 0.00151 0.00604 1 08/31/2018 01:50 WG1159831
1,2,3-Trichlorobenzene U 0.000755 0.00302 1 08/31/2018 01:50 WG1159831
1,2,4-Trichlorobenzene U 0.00582 0.0151 1 08/31/2018 01:50 WG1159831
1,1,1-Trichloroethane U 0.000332 0.00302 1 08/31/2018 01:50 WG1159831
1,1,2-Trichloroethane U 0.00107 0.00302 1 08/31/2018 01:50 WG1159831
1,1,2-Trichlorotrifluoroethane U 0.000816 0.00302 1 08/31/2018 01:50 WG1159831
Trichloroethene 0.00748 0.000483 0.00121 1 08/31/2018 01:50 WG1159831
Trichlorofluoromethane U 0.000604 0.00302 1 08/31/2018 01:50 WG1159831
1,2,3-Trichloropropane U 0.00616 0.0151 1 08/31/2018 01:50 WG1159831
1,2,4-Trimethylbenzene 0.00483 B J 0.00140 0.00604 1 08/31/2018 01:50 WG1159831
1,3,5-Trimethylbenzene U 0.00130 0.00604 1 08/31/2018 01:50 WG1159831
Vinyl chloride U 0.000825 0.00302 1 08/31/2018 01:50 WG1159831
Xylenes, Total 0.00911 B 0.00578 0.00785 1 08/31/2018 01:50 WG1159831
(S) Toluene-d8 97.3 75.0-131 08/31/2018 01:50 WG1159831
(S) Dibromofluoromethane 101 65.0-129 08/31/2018 01:50 WG1159831
(S) 4-Bromofluorobenzene 103 67.0-138 08/31/2018 01:50 WG1159831
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.195 J 0.0776 0.399 10 09/03/2018 10:38 WG1159283
Acenaphthylene 0.225 J 0.0811 0.399 10 09/03/2018 10:38 WG1159283
Anthracene 0.458 0.0764 0.399 10 09/03/2018 10:38 WG1159283
Benzidine U J4 0.770 4.02 10 09/03/2018 10:38 WG1159283
Benzo(a)anthracene 1.13 0.0517 0.399 10 09/03/2018 10:38 WG1159283
Benzo(b)fluoranthene 1.53 0.0840 0.399 10 09/03/2018 10:38 WG1159283
Benzo(k)fluoranthene 0.521 0.0703 0.399 10 09/03/2018 10:38 WG1159283
Benzo(g,h,i)perylene 0.405 0.0871 0.399 10 09/03/2018 10:38 WG1159283
Benzo(a)pyrene 1.09 0.0662 0.399 10 09/03/2018 10:38 WG1159283
Bis(2-chlorethoxy)methane U 0.0930 4.02 10 09/03/2018 10:38 WG1159283
Bis(2-chloroethyl)ether U 0.108 4.02 10 09/03/2018 10:38 WG1159283
Bis(2-chloroisopropyl)ether U 0.0918 4.02 10 09/03/2018 10:38 WG1159283
4-Bromophenyl-phenylether U 0.138 4.02 10 09/03/2018 10:38 WG1159283
2-Chloronaphthalene U 0.0772 0.399 10 09/03/2018 10:38 WG1159283
4-Chlorophenyl-phenylether U 0.0758 4.02 10 09/03/2018 10:38 WG1159283
Chrysene 1.09 0.0671 0.399 10 09/03/2018 10:38 WG1159283
Dibenz(a,h)anthracene 0.181 0.00992 0.0330 10 09/03/2018 10:38 WG1159283
3,3-Dichlorobenzidine U 0.959 4.02 10 09/03/2018 10:38 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 45 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 45 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L1020964
SWP-7 2-5
Collected date/time: 08/24/18 11:05
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
2,4-Dinitrotoluene U 0.0733 4.02 10 09/03/2018 10:38 WG1159283
2,6-Dinitrotoluene U 0.0890 4.02 10 09/03/2018 10:38 WG1159283
Fluoranthene 2.45 0.0599 0.399 10 09/03/2018 10:38 WG1159283
Fluorene 0.172 J 0.0824 0.399 10 09/03/2018 10:38 WG1159283
Hexachlorobenzene U 0.103 4.02 10 09/03/2018 10:38 WG1159283
Hexachloro-1,3-butadiene U 0.121 4.02 10 09/03/2018 10:38 WG1159283
Hexachlorocyclopentadiene U 0.709 4.02 10 09/03/2018 10:38 WG1159283
Hexachloroethane U 0.162 4.02 10 09/03/2018 10:38 WG1159283
Indeno(1,2,3-cd)pyrene 1.29 0.00933 0.0330 10 09/03/2018 10:38 WG1159283
Isophorone U 0.0631 4.02 10 09/03/2018 10:38 WG1159283
Naphthalene 0.159 J 0.107 0.399 10 09/03/2018 10:38 WG1159283
Nitrobenzene U 0.0840 4.02 10 09/03/2018 10:38 WG1159283
n-Nitrosodimethylamine U 0.782 4.02 10 09/03/2018 10:38 WG1159283
n-Nitrosodiphenylamine U 1.09 4.02 10 09/03/2018 10:38 WG1159283
n-Nitrosodi-n-propylamine U 0.109 4.02 10 09/03/2018 10:38 WG1159283
Phenanthrene 1.23 0.0638 0.399 10 09/03/2018 10:38 WG1159283
Benzylbutyl phthalate U 0.124 4.02 10 09/03/2018 10:38 WG1159283
Bis(2-ethylhexyl)phthalate U 0.145 4.02 10 09/03/2018 10:38 WG1159283
Di-n-butyl phthalate U 0.132 4.02 10 09/03/2018 10:38 WG1159283
Diethyl phthalate U 0.0835 4.02 10 09/03/2018 10:38 WG1159283
Dimethyl phthalate U 0.0652 4.02 10 09/03/2018 10:38 WG1159283
Di-n-octyl phthalate U 0.110 4.02 10 09/03/2018 10:38 WG1159283
Pyrene 2.28 0.149 0.399 10 09/03/2018 10:38 WG1159283
1,2,4-Trichlorobenzene U 0.106 4.02 10 09/03/2018 10:38 WG1159283
4-Chloro-3-methylphenol U 0.0576 4.02 10 09/03/2018 10:38 WG1159283
2-Chlorophenol U 0.100 4.02 10 09/03/2018 10:38 WG1159283
2,4-Dichlorophenol U 0.0901 4.02 10 09/03/2018 10:38 WG1159283
2,4-Dimethylphenol U 0.569 4.02 10 09/03/2018 10:38 WG1159283
4,6-Dinitro-2-methylphenol U 1.50 4.02 10 09/03/2018 10:38 WG1159283
2,4-Dinitrophenol U 1.18 4.02 10 09/03/2018 10:38 WG1159283
2-Nitrophenol U 0.157 4.02 10 09/03/2018 10:38 WG1159283
4-Nitrophenol U 0.634 4.02 10 09/03/2018 10:38 WG1159283
Pentachlorophenol U 0.580 4.02 10 09/03/2018 10:38 WG1159283
Phenol U 0.0840 4.02 10 09/03/2018 10:38 WG1159283
2,4,6-Trichlorophenol U 0.0941 4.02 10 09/03/2018 10:38 WG1159283
(S) 2-Fluorophenol 80.6 12.0-120 09/03/2018 10:38 WG1159283
(S) Phenol-d5 69.4 10.0-120 09/03/2018 10:38 WG1159283
(S) Nitrobenzene-d5 63.7 10.0-122 09/03/2018 10:38 WG1159283
(S) 2-Fluorobiphenyl 80.5 15.0-120 09/03/2018 10:38 WG1159283
(S) 2,4,6-Tribromophenol 90.8 10.0-127 09/03/2018 10:38 WG1159283
(S) p-Terphenyl-d14 75.7 10.0-120 09/03/2018 10:38 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 46 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L1020964
SWP-7 12-14
Collected date/time: 08/24/18 11:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 86.1 1 08/31/2018 10:56 WG1159714
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.00652 B J 0.00325 0.0232 1 08/31/2018 11:34 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic U 0.535 2.32 1 08/31/2018 15:39 WG1159261
Barium 9.70 0.198 0.581 1 08/31/2018 15:39 WG1159261
Cadmium U 0.0813 0.581 1 08/31/2018 15:39 WG1159261
Chromium 4.44 0.163 1.16 1 08/31/2018 15:39 WG1159261
Lead 8.45 0.221 0.581 1 08/31/2018 15:39 WG1159261
Selenium U 0.720 2.32 1 08/31/2018 15:39 WG1159261
Silver U 0.139 1.16 1 08/31/2018 15:39 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0159 0.0291 1 08/31/2018 20:09 WG1160333
Acrylonitrile U 0.00221 0.0145 1 08/31/2018 20:09 WG1160333
Benzene U 0.000465 0.00116 1 08/31/2018 20:09 WG1160333
Bromobenzene U J4 0.00122 0.0145 1 08/31/2018 20:09 WG1160333
Bromodichloromethane U 0.000916 0.00291 1 08/31/2018 20:09 WG1160333
Bromoform U 0.00695 0.0291 1 08/31/2018 20:09 WG1160333
Bromomethane U 0.00430 0.0145 1 08/31/2018 20:09 WG1160333
n-Butylbenzene U 0.00446 0.0145 1 08/31/2018 20:09 WG1160333
sec-Butylbenzene U 0.00294 0.0145 1 08/31/2018 20:09 WG1160333
tert-Butylbenzene U J4 0.00180 0.00581 1 08/31/2018 20:09 WG1160333
Carbon tetrachloride U 0.00126 0.00581 1 08/31/2018 20:09 WG1160333
Chlorobenzene 0.00113 J 0.000666 0.00291 1 08/31/2018 20:09 WG1160333
Chlorodibromomethane U 0.000523 0.00291 1 08/31/2018 20:09 WG1160333
Chloroethane U 0.00126 0.00581 1 08/31/2018 20:09 WG1160333
Chloroform U 0.000482 0.00291 1 08/31/2018 20:09 WG1160333
Chloromethane U 0.00162 0.0145 1 08/31/2018 20:09 WG1160333
2-Chlorotoluene U 0.00107 0.00291 1 08/31/2018 20:09 WG1160333
4-Chlorotoluene U J4 0.00131 0.00581 1 08/31/2018 20:09 WG1160333
1,2-Dibromo-3-Chloropropane U 0.00593 0.0291 1 08/31/2018 20:09 WG1160333
1,2-Dibromoethane U 0.000610 0.00291 1 08/31/2018 20:09 WG1160333
Dibromomethane U 0.00116 0.00581 1 08/31/2018 20:09 WG1160333
1,2-Dichlorobenzene U 0.00168 0.00581 1 08/31/2018 20:09 WG1160333
1,3-Dichlorobenzene U 0.00198 0.00581 1 08/31/2018 20:09 WG1160333
1,4-Dichlorobenzene U 0.00229 0.00581 1 08/31/2018 20:09 WG1160333
Dichlorodifluoromethane U 0.000951 0.00291 1 08/31/2018 20:09 WG1160333
1,1-Dichloroethane U 0.000668 0.00291 1 08/31/2018 20:09 WG1160333
1,2-Dichloroethane U 0.000552 0.00291 1 08/31/2018 20:09 WG1160333
1,1-Dichloroethene 0.00248 J 0.000581 0.00291 1 08/31/2018 20:09 WG1160333
cis-1,2-Dichloroethene 0.00133 J 0.000802 0.00291 1 08/31/2018 20:09 WG1160333
trans-1,2-Dichloroethene U 0.00166 0.00581 1 08/31/2018 20:09 WG1160333
1,2-Dichloropropane U 0.00148 0.00581 1 08/31/2018 20:09 WG1160333
1,1-Dichloropropene U 0.000813 0.00291 1 08/31/2018 20:09 WG1160333
1,3-Dichloropropane U 0.00203 0.00581 1 08/31/2018 20:09 WG1160333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 47 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L1020964
SWP-7 12-14
Collected date/time: 08/24/18 11:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000788 0.00291 1 08/31/2018 20:09 WG1160333
trans-1,3-Dichloropropene U 0.00178 0.00581 1 08/31/2018 20:09 WG1160333
2,2-Dichloropropane U 0.000921 0.00291 1 08/31/2018 20:09 WG1160333
Di-isopropyl ether U 0.000407 0.00116 1 08/31/2018 20:09 WG1160333
Ethylbenzene U 0.000616 0.00291 1 08/31/2018 20:09 WG1160333
Hexachloro-1,3-butadiene U 0.0148 0.0291 1 08/31/2018 20:09 WG1160333
Isopropylbenzene U 0.00100 0.00291 1 08/31/2018 20:09 WG1160333
p-Isopropyltoluene U 0.00271 0.00581 1 08/31/2018 20:09 WG1160333
2-Butanone (MEK)U 0.0145 0.0291 1 08/31/2018 20:09 WG1160333
Methylene Chloride U 0.00772 0.0291 1 08/31/2018 20:09 WG1160333
4-Methyl-2-pentanone (MIBK) U 0.0116 0.0291 1 08/31/2018 20:09 WG1160333
Methyl tert-butyl ether U 0.000343 0.00116 1 08/31/2018 20:09 WG1160333
Naphthalene U J3 0.00363 0.0145 1 08/31/2018 20:09 WG1160333
n-Propylbenzene U 0.00137 0.00581 1 08/31/2018 20:09 WG1160333
Styrene U 0.00317 0.0145 1 08/31/2018 20:09 WG1160333
1,1,1,2-Tetrachloroethane U 0.000581 0.00291 1 08/31/2018 20:09 WG1160333
1,1,2,2-Tetrachloroethane U 0.000453 0.00291 1 08/31/2018 20:09 WG1160333
Tetrachloroethene 0.00695 0.000813 0.00291 1 08/31/2018 20:09 WG1160333
Toluene U 0.00145 0.00581 1 08/31/2018 20:09 WG1160333
1,2,3-Trichlorobenzene U J3 0.000726 0.00291 1 08/31/2018 20:09 WG1160333
1,2,4-Trichlorobenzene U J3 0.00560 0.0145 1 08/31/2018 20:09 WG1160333
1,1,1-Trichloroethane U 0.000320 0.00291 1 08/31/2018 20:09 WG1160333
1,1,2-Trichloroethane U 0.00103 0.00291 1 08/31/2018 20:09 WG1160333
1,1,2-Trichlorotrifluoroethane U 0.000784 0.00291 1 08/31/2018 20:09 WG1160333
Trichloroethene 0.0264 0.000465 0.00116 1 08/31/2018 20:09 WG1160333
Trichlorofluoromethane U 0.000581 0.00291 1 08/31/2018 20:09 WG1160333
1,2,3-Trichloropropane U 0.00593 0.0145 1 08/31/2018 20:09 WG1160333
1,2,4-Trimethylbenzene U 0.00135 0.00581 1 08/31/2018 20:09 WG1160333
1,3,5-Trimethylbenzene U 0.00126 0.00581 1 08/31/2018 20:09 WG1160333
Vinyl chloride U 0.000794 0.00291 1 08/31/2018 20:09 WG1160333
Xylenes, Total U 0.00555 0.00755 1 08/31/2018 20:09 WG1160333
(S) Toluene-d8 104 75.0-131 08/31/2018 20:09 WG1160333
(S) Dibromofluoromethane 102 65.0-129 08/31/2018 20:09 WG1160333
(S) 4-Bromofluorobenzene 105 67.0-138 08/31/2018 20:09 WG1160333
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00746 0.0383 1 09/03/2018 05:10 WG1159283
Acenaphthylene U 0.00780 0.0383 1 09/03/2018 05:10 WG1159283
Anthracene U 0.00734 0.0383 1 09/03/2018 05:10 WG1159283
Benzidine U J4 0.0740 0.387 1 09/03/2018 05:10 WG1159283
Benzo(a)anthracene U 0.00497 0.0383 1 09/03/2018 05:10 WG1159283
Benzo(b)fluoranthene U 0.00808 0.0383 1 09/03/2018 05:10 WG1159283
Benzo(k)fluoranthene U 0.00676 0.0383 1 09/03/2018 05:10 WG1159283
Benzo(g,h,i)perylene U 0.00838 0.0383 1 09/03/2018 05:10 WG1159283
Benzo(a)pyrene U 0.00637 0.0383 1 09/03/2018 05:10 WG1159283
Bis(2-chlorethoxy)methane U 0.00895 0.387 1 09/03/2018 05:10 WG1159283
Bis(2-chloroethyl)ether U 0.0104 0.387 1 09/03/2018 05:10 WG1159283
Bis(2-chloroisopropyl)ether U 0.00883 0.387 1 09/03/2018 05:10 WG1159283
4-Bromophenyl-phenylether U 0.0132 0.387 1 09/03/2018 05:10 WG1159283
2-Chloronaphthalene U 0.00743 0.0383 1 09/03/2018 05:10 WG1159283
4-Chlorophenyl-phenylether U 0.00729 0.387 1 09/03/2018 05:10 WG1159283
Chrysene U 0.00645 0.0383 1 09/03/2018 05:10 WG1159283
Dibenz(a,h)anthracene U 0.00954 0.0383 1 09/03/2018 05:10 WG1159283
3,3-Dichlorobenzidine U 0.0923 0.387 1 09/03/2018 05:10 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 48 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L1020964
SWP-7 12-14
Collected date/time: 08/24/18 11:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
2,4-Dinitrotoluene U 0.00705 0.387 1 09/03/2018 05:10 WG1159283
2,6-Dinitrotoluene U 0.00856 0.387 1 09/03/2018 05:10 WG1159283
Fluoranthene U 0.00576 0.0383 1 09/03/2018 05:10 WG1159283
Fluorene U 0.00793 0.0383 1 09/03/2018 05:10 WG1159283
Hexachlorobenzene U 0.00995 0.387 1 09/03/2018 05:10 WG1159283
Hexachloro-1,3-butadiene U 0.0116 0.387 1 09/03/2018 05:10 WG1159283
Hexachlorocyclopentadiene U 0.0682 0.387 1 09/03/2018 05:10 WG1159283
Hexachloroethane U 0.0156 0.387 1 09/03/2018 05:10 WG1159283
Indeno(1,2,3-cd)pyrene U 0.00897 0.0383 1 09/03/2018 05:10 WG1159283
Isophorone U 0.00607 0.387 1 09/03/2018 05:10 WG1159283
Naphthalene U 0.0103 0.0383 1 09/03/2018 05:10 WG1159283
Nitrobenzene U 0.00808 0.387 1 09/03/2018 05:10 WG1159283
n-Nitrosodimethylamine U 0.0752 0.387 1 09/03/2018 05:10 WG1159283
n-Nitrosodiphenylamine U 0.105 0.387 1 09/03/2018 05:10 WG1159283
n-Nitrosodi-n-propylamine U 0.0105 0.387 1 09/03/2018 05:10 WG1159283
Phenanthrene U 0.00614 0.0383 1 09/03/2018 05:10 WG1159283
Benzylbutyl phthalate U 0.0120 0.387 1 09/03/2018 05:10 WG1159283
Bis(2-ethylhexyl)phthalate U 0.0139 0.387 1 09/03/2018 05:10 WG1159283
Di-n-butyl phthalate U 0.0127 0.387 1 09/03/2018 05:10 WG1159283
Diethyl phthalate U 0.00803 0.387 1 09/03/2018 05:10 WG1159283
Dimethyl phthalate U 0.00628 0.387 1 09/03/2018 05:10 WG1159283
Di-n-octyl phthalate U 0.0105 0.387 1 09/03/2018 05:10 WG1159283
Pyrene U 0.0143 0.0383 1 09/03/2018 05:10 WG1159283
1,2,4-Trichlorobenzene U 0.0102 0.387 1 09/03/2018 05:10 WG1159283
4-Chloro-3-methylphenol U 0.00554 0.387 1 09/03/2018 05:10 WG1159283
2-Chlorophenol U 0.00966 0.387 1 09/03/2018 05:10 WG1159283
2,4-Dichlorophenol U 0.00867 0.387 1 09/03/2018 05:10 WG1159283
2,4-Dimethylphenol U 0.0547 0.387 1 09/03/2018 05:10 WG1159283
4,6-Dinitro-2-methylphenol U 0.144 0.387 1 09/03/2018 05:10 WG1159283
2,4-Dinitrophenol U 0.114 0.387 1 09/03/2018 05:10 WG1159283
2-Nitrophenol U 0.0151 0.387 1 09/03/2018 05:10 WG1159283
4-Nitrophenol U 0.0610 0.387 1 09/03/2018 05:10 WG1159283
Pentachlorophenol U 0.0558 0.387 1 09/03/2018 05:10 WG1159283
Phenol U 0.00808 0.387 1 09/03/2018 05:10 WG1159283
2,4,6-Trichlorophenol U 0.00905 0.387 1 09/03/2018 05:10 WG1159283
(S) 2-Fluorophenol 151 J1 12.0-120 09/03/2018 05:10 WG1159283
(S) Phenol-d5 131 J1 10.0-120 09/03/2018 05:10 WG1159283
(S) Nitrobenzene-d5 125 J1 10.0-122 09/03/2018 05:10 WG1159283
(S) 2-Fluorobiphenyl 141 J1 15.0-120 09/03/2018 05:10 WG1159283
(S) 2,4,6-Tribromophenol 186 J1 10.0-127 09/03/2018 05:10 WG1159283
(S) p-Terphenyl-d14 134 J1 10.0-120 09/03/2018 05:10 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L1020964
SWP-8 1-5
Collected date/time: 08/24/18 11:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 87.5 1 08/31/2018 10:56 WG1159714
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.177 0.00320 0.0229 1 08/31/2018 12:20 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.03 J 0.526 2.29 1 08/31/2018 15:42 WG1159261
Barium 202 0.194 0.571 1 08/31/2018 15:42 WG1159261
Cadmium 1.19 0.0800 0.571 1 08/31/2018 15:42 WG1159261
Chromium 8.90 0.160 1.14 1 08/31/2018 15:42 WG1159261
Lead 384 0.217 0.571 1 08/31/2018 15:42 WG1159261
Selenium 0.881 J 0.708 2.29 1 08/31/2018 15:42 WG1159261
Silver U 0.137 1.14 1 08/31/2018 15:42 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0157 0.0286 1 08/31/2018 20:29 WG1160333
Acrylonitrile U 0.00217 0.0143 1 08/31/2018 20:29 WG1160333
Benzene 0.00525 0.000457 0.00114 1 08/31/2018 20:29 WG1160333
Bromobenzene U J4 0.00120 0.0143 1 08/31/2018 20:29 WG1160333
Bromodichloromethane U 0.000900 0.00286 1 08/31/2018 20:29 WG1160333
Bromoform U 0.00683 0.0286 1 08/31/2018 20:29 WG1160333
Bromomethane U 0.00423 0.0143 1 08/31/2018 20:29 WG1160333
n-Butylbenzene U 0.00439 0.0143 1 08/31/2018 20:29 WG1160333
sec-Butylbenzene U 0.00289 0.0143 1 08/31/2018 20:29 WG1160333
tert-Butylbenzene U J4 0.00177 0.00571 1 08/31/2018 20:29 WG1160333
Carbon tetrachloride U 0.00123 0.00571 1 08/31/2018 20:29 WG1160333
Chlorobenzene U 0.000655 0.00286 1 08/31/2018 20:29 WG1160333
Chlorodibromomethane U 0.000514 0.00286 1 08/31/2018 20:29 WG1160333
Chloroethane U 0.00123 0.00571 1 08/31/2018 20:29 WG1160333
Chloroform U 0.000474 0.00286 1 08/31/2018 20:29 WG1160333
Chloromethane U 0.00159 0.0143 1 08/31/2018 20:29 WG1160333
2-Chlorotoluene U 0.00105 0.00286 1 08/31/2018 20:29 WG1160333
4-Chlorotoluene U J4 0.00129 0.00571 1 08/31/2018 20:29 WG1160333
1,2-Dibromo-3-Chloropropane U 0.00583 0.0286 1 08/31/2018 20:29 WG1160333
1,2-Dibromoethane U 0.000600 0.00286 1 08/31/2018 20:29 WG1160333
Dibromomethane U 0.00114 0.00571 1 08/31/2018 20:29 WG1160333
1,2-Dichlorobenzene U 0.00166 0.00571 1 08/31/2018 20:29 WG1160333
1,3-Dichlorobenzene U 0.00194 0.00571 1 08/31/2018 20:29 WG1160333
1,4-Dichlorobenzene U 0.00225 0.00571 1 08/31/2018 20:29 WG1160333
Dichlorodifluoromethane U 0.000935 0.00286 1 08/31/2018 20:29 WG1160333
1,1-Dichloroethane U 0.000657 0.00286 1 08/31/2018 20:29 WG1160333
1,2-Dichloroethane U 0.000543 0.00286 1 08/31/2018 20:29 WG1160333
1,1-Dichloroethene U 0.000571 0.00286 1 08/31/2018 20:29 WG1160333
cis-1,2-Dichloroethene U 0.000788 0.00286 1 08/31/2018 20:29 WG1160333
trans-1,2-Dichloroethene U 0.00163 0.00571 1 08/31/2018 20:29 WG1160333
1,2-Dichloropropane U 0.00145 0.00571 1 08/31/2018 20:29 WG1160333
1,1-Dichloropropene U 0.000800 0.00286 1 08/31/2018 20:29 WG1160333
1,3-Dichloropropane U 0.00200 0.00571 1 08/31/2018 20:29 WG1160333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L1020964
SWP-8 1-5
Collected date/time: 08/24/18 11:25
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000775 0.00286 1 08/31/2018 20:29 WG1160333
trans-1,3-Dichloropropene U 0.00175 0.00571 1 08/31/2018 20:29 WG1160333
2,2-Dichloropropane U 0.000906 0.00286 1 08/31/2018 20:29 WG1160333
Di-isopropyl ether U 0.000400 0.00114 1 08/31/2018 20:29 WG1160333
Ethylbenzene 0.00190 J 0.000606 0.00286 1 08/31/2018 20:29 WG1160333
Hexachloro-1,3-butadiene U 0.0145 0.0286 1 08/31/2018 20:29 WG1160333
Isopropylbenzene U 0.000986 0.00286 1 08/31/2018 20:29 WG1160333
p-Isopropyltoluene U 0.00266 0.00571 1 08/31/2018 20:29 WG1160333
2-Butanone (MEK)U 0.0143 0.0286 1 08/31/2018 20:29 WG1160333
Methylene Chloride U 0.00759 0.0286 1 08/31/2018 20:29 WG1160333
4-Methyl-2-pentanone (MIBK) U 0.0114 0.0286 1 08/31/2018 20:29 WG1160333
Methyl tert-butyl ether U 0.000337 0.00114 1 08/31/2018 20:29 WG1160333
Naphthalene 0.0118 J J3 0.00357 0.0143 1 08/31/2018 20:29 WG1160333
n-Propylbenzene U 0.00135 0.00571 1 08/31/2018 20:29 WG1160333
Styrene U 0.00312 0.0143 1 08/31/2018 20:29 WG1160333
1,1,1,2-Tetrachloroethane U 0.000571 0.00286 1 08/31/2018 20:29 WG1160333
1,1,2,2-Tetrachloroethane U 0.000446 0.00286 1 08/31/2018 20:29 WG1160333
Tetrachloroethene 2.51 0.00800 0.0286 10 09/03/2018 13:58 WG1160867
Toluene 0.0224 0.00143 0.00571 1 08/31/2018 20:29 WG1160333
1,2,3-Trichlorobenzene U J3 0.000714 0.00286 1 08/31/2018 20:29 WG1160333
1,2,4-Trichlorobenzene U J3 0.00551 0.0143 1 08/31/2018 20:29 WG1160333
1,1,1-Trichloroethane U 0.000314 0.00286 1 08/31/2018 20:29 WG1160333
1,1,2-Trichloroethane U 0.00101 0.00286 1 08/31/2018 20:29 WG1160333
1,1,2-Trichlorotrifluoroethane U 0.000771 0.00286 1 08/31/2018 20:29 WG1160333
Trichloroethene 0.00412 0.000457 0.00114 1 08/31/2018 20:29 WG1160333
Trichlorofluoromethane U 0.000571 0.00286 1 08/31/2018 20:29 WG1160333
1,2,3-Trichloropropane U 0.00583 0.0143 1 08/31/2018 20:29 WG1160333
1,2,4-Trimethylbenzene 0.00493 J 0.00133 0.00571 1 08/31/2018 20:29 WG1160333
1,3,5-Trimethylbenzene 0.00155 J 0.00123 0.00571 1 08/31/2018 20:29 WG1160333
Vinyl chloride U 0.000780 0.00286 1 08/31/2018 20:29 WG1160333
Xylenes, Total 0.0243 0.00546 0.00743 1 08/31/2018 20:29 WG1160333
(S) Toluene-d8 106 75.0-131 08/31/2018 20:29 WG1160333
(S) Toluene-d8 102 75.0-131 09/03/2018 13:58 WG1160867
(S) Dibromofluoromethane 101 65.0-129 08/31/2018 20:29 WG1160333
(S) Dibromofluoromethane 103 65.0-129 09/03/2018 13:58 WG1160867
(S) 4-Bromofluorobenzene 101 67.0-138 08/31/2018 20:29 WG1160333
(S) 4-Bromofluorobenzene 104 67.0-138 09/03/2018 13:58 WG1160867
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.0748 J 0.0734 0.377 10 09/03/2018 11:01 WG1159283
Acenaphthylene 0.0855 J 0.0767 0.377 10 09/03/2018 11:01 WG1159283
Anthracene 0.229 J 0.0722 0.377 10 09/03/2018 11:01 WG1159283
Benzidine U J4 0.728 3.81 10 09/03/2018 11:01 WG1159283
Benzo(a)anthracene 0.739 0.0489 0.377 10 09/03/2018 11:01 WG1159283
Benzo(b)fluoranthene 0.993 0.0794 0.377 10 09/03/2018 11:01 WG1159283
Benzo(k)fluoranthene 0.479 0.0665 0.377 10 09/03/2018 11:01 WG1159283
Benzo(g,h,i)perylene 0.305 J 0.0824 0.377 10 09/03/2018 11:01 WG1159283
Benzo(a)pyrene 0.735 0.0626 0.377 10 09/03/2018 11:01 WG1159283
Bis(2-chlorethoxy)methane U 0.0880 3.81 10 09/03/2018 11:01 WG1159283
Bis(2-chloroethyl)ether U 0.102 3.81 10 09/03/2018 11:01 WG1159283
Bis(2-chloroisopropyl)ether U 0.0868 3.81 10 09/03/2018 11:01 WG1159283
4-Bromophenyl-phenylether U 0.130 3.81 10 09/03/2018 11:01 WG1159283
2-Chloronaphthalene U 0.0730 0.377 10 09/03/2018 11:01 WG1159283
4-Chlorophenyl-phenylether U 0.0716 3.81 10 09/03/2018 11:01 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L1020964
SWP-8 1-5
Collected date/time: 08/24/18 11:25
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Chrysene 0.737 0.0634 0.377 10 09/03/2018 11:01 WG1159283
Dibenz(a,h)anthracene U 0.00938 0.0330 10 09/03/2018 11:01 WG1159283
3,3-Dichlorobenzidine U 0.907 3.81 10 09/03/2018 11:01 WG1159283
2,4-Dinitrotoluene U 0.0694 3.81 10 09/03/2018 11:01 WG1159283
2,6-Dinitrotoluene U 0.0842 3.81 10 09/03/2018 11:01 WG1159283
Fluoranthene 1.50 0.0567 0.377 10 09/03/2018 11:01 WG1159283
Fluorene U 0.0779 0.377 10 09/03/2018 11:01 WG1159283
Hexachlorobenzene U 0.0978 3.81 10 09/03/2018 11:01 WG1159283
Hexachloro-1,3-butadiene U 0.114 3.81 10 09/03/2018 11:01 WG1159283
Hexachlorocyclopentadiene U 0.671 3.81 10 09/03/2018 11:01 WG1159283
Hexachloroethane U 0.153 3.81 10 09/03/2018 11:01 WG1159283
Indeno(1,2,3-cd)pyrene 0.942 0.00882 0.0330 10 09/03/2018 11:01 WG1159283
Isophorone U 0.0596 3.81 10 09/03/2018 11:01 WG1159283
Naphthalene U 0.102 0.377 10 09/03/2018 11:01 WG1159283
Nitrobenzene U 0.0794 3.81 10 09/03/2018 11:01 WG1159283
n-Nitrosodimethylamine U 0.739 3.81 10 09/03/2018 11:01 WG1159283
n-Nitrosodiphenylamine U 1.03 3.81 10 09/03/2018 11:01 WG1159283
n-Nitrosodi-n-propylamine U 0.104 3.81 10 09/03/2018 11:01 WG1159283
Phenanthrene 0.842 0.0603 0.377 10 09/03/2018 11:01 WG1159283
Benzylbutyl phthalate U 0.118 3.81 10 09/03/2018 11:01 WG1159283
Bis(2-ethylhexyl)phthalate U 0.137 3.81 10 09/03/2018 11:01 WG1159283
Di-n-butyl phthalate U 0.125 3.81 10 09/03/2018 11:01 WG1159283
Diethyl phthalate U 0.0790 3.81 10 09/03/2018 11:01 WG1159283
Dimethyl phthalate U 0.0617 3.81 10 09/03/2018 11:01 WG1159283
Di-n-octyl phthalate U 0.104 3.81 10 09/03/2018 11:01 WG1159283
Pyrene 1.25 0.141 0.377 10 09/03/2018 11:01 WG1159283
1,2,4-Trichlorobenzene U 0.100 3.81 10 09/03/2018 11:01 WG1159283
4-Chloro-3-methylphenol U 0.0545 3.81 10 09/03/2018 11:01 WG1159283
2-Chlorophenol U 0.0950 3.81 10 09/03/2018 11:01 WG1159283
2,4-Dichlorophenol U 0.0852 3.81 10 09/03/2018 11:01 WG1159283
2,4-Dimethylphenol U 0.538 3.81 10 09/03/2018 11:01 WG1159283
4,6-Dinitro-2-methylphenol U 1.42 3.81 10 09/03/2018 11:01 WG1159283
2,4-Dinitrophenol U 1.12 3.81 10 09/03/2018 11:01 WG1159283
2-Nitrophenol U 0.149 3.81 10 09/03/2018 11:01 WG1159283
4-Nitrophenol U 0.600 3.81 10 09/03/2018 11:01 WG1159283
Pentachlorophenol U 0.548 3.81 10 09/03/2018 11:01 WG1159283
Phenol U 0.0794 3.81 10 09/03/2018 11:01 WG1159283
2,4,6-Trichlorophenol U 0.0890 3.81 10 09/03/2018 11:01 WG1159283
(S) 2-Fluorophenol 73.6 12.0-120 09/03/2018 11:01 WG1159283
(S) Phenol-d5 70.5 10.0-120 09/03/2018 11:01 WG1159283
(S) Nitrobenzene-d5 67.6 10.0-122 09/03/2018 11:01 WG1159283
(S) 2-Fluorobiphenyl 87.6 15.0-120 09/03/2018 11:01 WG1159283
(S) 2,4,6-Tribromophenol 84.8 10.0-127 09/03/2018 11:01 WG1159283
(S) p-Terphenyl-d14 80.0 10.0-120 09/03/2018 11:01 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L1020964
SWP-8 10-15
Collected date/time: 08/24/18 11:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 83.4 1 08/30/2018 13:15 WG1159541
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.130 0.00336 0.0240 1 08/31/2018 12:30 WG1159451
Metals (ICP) by Method 6010D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 4.61 0.552 2.40 1 08/31/2018 15:45 WG1159261
Barium 30.0 0.204 0.600 1 08/31/2018 15:45 WG1159261
Cadmium 0.0899 J 0.0840 0.600 1 08/31/2018 15:45 WG1159261
Chromium 9.62 0.168 1.20 1 08/31/2018 15:45 WG1159261
Lead 141 0.228 0.600 1 08/31/2018 15:45 WG1159261
Selenium U 0.744 2.40 1 08/31/2018 15:45 WG1159261
Silver U 0.144 1.20 1 08/31/2018 15:45 WG1159261
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone U 0.0164 0.0300 1 08/31/2018 20:49 WG1160333
Acrylonitrile U 0.00228 0.0150 1 08/31/2018 20:49 WG1160333
Benzene 0.0185 0.000480 0.00120 1 08/31/2018 20:49 WG1160333
Bromobenzene U J4 0.00126 0.0150 1 08/31/2018 20:49 WG1160333
Bromodichloromethane U 0.000945 0.00300 1 08/31/2018 20:49 WG1160333
Bromoform U 0.00717 0.0300 1 08/31/2018 20:49 WG1160333
Bromomethane U 0.00444 0.0150 1 08/31/2018 20:49 WG1160333
n-Butylbenzene 0.00519 J 0.00461 0.0150 1 08/31/2018 20:49 WG1160333
sec-Butylbenzene 0.00581 J 0.00303 0.0150 1 08/31/2018 20:49 WG1160333
tert-Butylbenzene U J4 0.00186 0.00600 1 08/31/2018 20:49 WG1160333
Carbon tetrachloride U 0.00130 0.00600 1 08/31/2018 20:49 WG1160333
Chlorobenzene 0.166 0.000687 0.00300 1 08/31/2018 20:49 WG1160333
Chlorodibromomethane U 0.000540 0.00300 1 08/31/2018 20:49 WG1160333
Chloroethane U 0.00130 0.00600 1 08/31/2018 20:49 WG1160333
Chloroform U 0.000498 0.00300 1 08/31/2018 20:49 WG1160333
Chloromethane U 0.00167 0.0150 1 08/31/2018 20:49 WG1160333
2-Chlorotoluene U 0.00110 0.00300 1 08/31/2018 20:49 WG1160333
4-Chlorotoluene U J4 0.00136 0.00600 1 08/31/2018 20:49 WG1160333
1,2-Dibromo-3-Chloropropane U 0.00612 0.0300 1 08/31/2018 20:49 WG1160333
1,2-Dibromoethane U 0.000630 0.00300 1 08/31/2018 20:49 WG1160333
Dibromomethane U 0.00120 0.00600 1 08/31/2018 20:49 WG1160333
1,2-Dichlorobenzene 0.00788 0.00174 0.00600 1 08/31/2018 20:49 WG1160333
1,3-Dichlorobenzene 0.127 0.00204 0.00600 1 08/31/2018 20:49 WG1160333
1,4-Dichlorobenzene 0.446 0.00236 0.00600 1 08/31/2018 20:49 WG1160333
Dichlorodifluoromethane U 0.000981 0.00300 1 08/31/2018 20:49 WG1160333
1,1-Dichloroethane 0.000986 J 0.000690 0.00300 1 08/31/2018 20:49 WG1160333
1,2-Dichloroethane 0.0837 0.000570 0.00300 1 08/31/2018 20:49 WG1160333
1,1-Dichloroethene 0.00344 0.000600 0.00300 1 08/31/2018 20:49 WG1160333
cis-1,2-Dichloroethene 0.110 0.000828 0.00300 1 08/31/2018 20:49 WG1160333
trans-1,2-Dichloroethene 0.0280 0.00172 0.00600 1 08/31/2018 20:49 WG1160333
1,2-Dichloropropane U 0.00152 0.00600 1 08/31/2018 20:49 WG1160333
1,1-Dichloropropene U 0.000840 0.00300 1 08/31/2018 20:49 WG1160333
1,3-Dichloropropane U 0.00210 0.00600 1 08/31/2018 20:49 WG1160333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 53 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L1020964
SWP-8 10-15
Collected date/time: 08/24/18 11:35
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
cis-1,3-Dichloropropene U 0.000813 0.00300 1 08/31/2018 20:49 WG1160333
trans-1,3-Dichloropropene U 0.00184 0.00600 1 08/31/2018 20:49 WG1160333
2,2-Dichloropropane U 0.000951 0.00300 1 08/31/2018 20:49 WG1160333
Di-isopropyl ether 0.00549 0.000420 0.00120 1 08/31/2018 20:49 WG1160333
Ethylbenzene 0.00536 0.000636 0.00300 1 08/31/2018 20:49 WG1160333
Hexachloro-1,3-butadiene U 0.0152 0.0300 1 08/31/2018 20:49 WG1160333
Isopropylbenzene 0.0105 0.00104 0.00300 1 08/31/2018 20:49 WG1160333
p-Isopropyltoluene 0.00322 J 0.00279 0.00600 1 08/31/2018 20:49 WG1160333
2-Butanone (MEK)U 0.0150 0.0300 1 08/31/2018 20:49 WG1160333
Methylene Chloride U 0.00796 0.0300 1 08/31/2018 20:49 WG1160333
4-Methyl-2-pentanone (MIBK) U 0.0120 0.0300 1 08/31/2018 20:49 WG1160333
Methyl tert-butyl ether 0.00263 0.000354 0.00120 1 08/31/2018 20:49 WG1160333
Naphthalene 0.168 J3 0.00374 0.0150 1 08/31/2018 20:49 WG1160333
n-Propylbenzene 0.00469 J 0.00142 0.00600 1 08/31/2018 20:49 WG1160333
Styrene U 0.00327 0.0150 1 08/31/2018 20:49 WG1160333
1,1,1,2-Tetrachloroethane U 0.000600 0.00300 1 08/31/2018 20:49 WG1160333
1,1,2,2-Tetrachloroethane U 0.000468 0.00300 1 08/31/2018 20:49 WG1160333
Tetrachloroethene 0.0105 0.000840 0.00300 1 09/03/2018 09:14 WG1160867
Toluene 0.0153 0.00150 0.00600 1 08/31/2018 20:49 WG1160333
1,2,3-Trichlorobenzene 0.0162 J3 0.000750 0.00300 1 08/31/2018 20:49 WG1160333
1,2,4-Trichlorobenzene 0.193 J3 0.00578 0.0150 1 08/31/2018 20:49 WG1160333
1,1,1-Trichloroethane U 0.000330 0.00300 1 08/31/2018 20:49 WG1160333
1,1,2-Trichloroethane U 0.00106 0.00300 1 08/31/2018 20:49 WG1160333
1,1,2-Trichlorotrifluoroethane U 0.000810 0.00300 1 08/31/2018 20:49 WG1160333
Trichloroethene 1.14 0.000480 0.00120 1 08/31/2018 20:49 WG1160333
Trichlorofluoromethane U 0.000600 0.00300 1 08/31/2018 20:49 WG1160333
1,2,3-Trichloropropane U 0.00612 0.0150 1 08/31/2018 20:49 WG1160333
1,2,4-Trimethylbenzene 0.0147 0.00139 0.00600 1 08/31/2018 20:49 WG1160333
1,3,5-Trimethylbenzene 0.00558 J 0.00130 0.00600 1 08/31/2018 20:49 WG1160333
Vinyl chloride U 0.000819 0.00300 1 08/31/2018 20:49 WG1160333
Xylenes, Total 0.0206 0.00573 0.00780 1 08/31/2018 20:49 WG1160333
(S) Toluene-d8 64.5 J2 75.0-131 08/31/2018 20:49 WG1160333
(S) Toluene-d8 67.2 J2 75.0-131 09/03/2018 09:14 WG1160867
(S) Dibromofluoromethane 101 65.0-129 08/31/2018 20:49 WG1160333
(S) Dibromofluoromethane 101 65.0-129 09/03/2018 09:14 WG1160867
(S) 4-Bromofluorobenzene 105 67.0-138 08/31/2018 20:49 WG1160333
(S) 4-Bromofluorobenzene 96.0 67.0-138 09/03/2018 09:14 WG1160867
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.230 0.0385 0.198 5 09/03/2018 10:14 WG1159283
Acenaphthylene 0.512 0.0402 0.198 5 09/03/2018 10:14 WG1159283
Anthracene 1.11 0.0379 0.198 5 09/03/2018 10:14 WG1159283
Benzidine U J4 0.383 2.00 5 09/03/2018 10:14 WG1159283
Benzo(a)anthracene 2.63 0.0257 0.198 5 09/03/2018 10:14 WG1159283
Benzo(b)fluoranthene 2.91 0.0416 0.198 5 09/03/2018 10:14 WG1159283
Benzo(k)fluoranthene 1.08 0.0349 0.198 5 09/03/2018 10:14 WG1159283
Benzo(g,h,i)perylene 0.856 0.0433 0.198 5 09/03/2018 10:14 WG1159283
Benzo(a)pyrene 2.48 0.0329 0.198 5 09/03/2018 10:14 WG1159283
Bis(2-chlorethoxy)methane U 0.0462 2.00 5 09/03/2018 10:14 WG1159283
Bis(2-chloroethyl)ether U 0.0537 2.00 5 09/03/2018 10:14 WG1159283
Bis(2-chloroisopropyl)ether U 0.0456 2.00 5 09/03/2018 10:14 WG1159283
4-Bromophenyl-phenylether U 0.0684 2.00 5 09/03/2018 10:14 WG1159283
2-Chloronaphthalene U 0.0384 0.198 5 09/03/2018 10:14 WG1159283
4-Chlorophenyl-phenylether U 0.0377 2.00 5 09/03/2018 10:14 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 54 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L1020964
SWP-8 10-15
Collected date/time: 08/24/18 11:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Chrysene 2.31 0.0333 0.198 5 09/03/2018 10:14 WG1159283
Dibenz(a,h)anthracene 0.529 0.0493 0.198 5 09/03/2018 10:14 WG1159283
3,3-Dichlorobenzidine U 0.476 2.00 5 09/03/2018 10:14 WG1159283
2,4-Dinitrotoluene U 0.0365 2.00 5 09/03/2018 10:14 WG1159283
2,6-Dinitrotoluene U 0.0443 2.00 5 09/03/2018 10:14 WG1159283
Fluoranthene 5.04 0.0297 0.198 5 09/03/2018 10:14 WG1159283
Fluorene 0.385 0.0409 0.198 5 09/03/2018 10:14 WG1159283
Hexachlorobenzene U 0.0513 2.00 5 09/03/2018 10:14 WG1159283
Hexachloro-1,3-butadiene U 0.0600 2.00 5 09/03/2018 10:14 WG1159283
Hexachlorocyclopentadiene U 0.351 2.00 5 09/03/2018 10:14 WG1159283
Hexachloroethane U 0.0804 2.00 5 09/03/2018 10:14 WG1159283
Indeno(1,2,3-cd)pyrene 5.23 0.0463 0.198 5 09/03/2018 10:14 WG1159283
Isophorone U 0.0313 2.00 5 09/03/2018 10:14 WG1159283
Naphthalene 0.499 0.0534 0.198 5 09/03/2018 10:14 WG1159283
Nitrobenzene U 0.0416 2.00 5 09/03/2018 10:14 WG1159283
n-Nitrosodimethylamine U 0.387 2.00 5 09/03/2018 10:14 WG1159283
n-Nitrosodiphenylamine U 0.540 2.00 5 09/03/2018 10:14 WG1159283
n-Nitrosodi-n-propylamine U 0.0543 2.00 5 09/03/2018 10:14 WG1159283
Phenanthrene 2.58 0.0317 0.198 5 09/03/2018 10:14 WG1159283
Benzylbutyl phthalate U 0.0618 2.00 5 09/03/2018 10:14 WG1159283
Bis(2-ethylhexyl)phthalate U 0.0720 2.00 5 09/03/2018 10:14 WG1159283
Di-n-butyl phthalate U 0.0654 2.00 5 09/03/2018 10:14 WG1159283
Diethyl phthalate U 0.0415 2.00 5 09/03/2018 10:14 WG1159283
Dimethyl phthalate U 0.0324 2.00 5 09/03/2018 10:14 WG1159283
Di-n-octyl phthalate U 0.0545 2.00 5 09/03/2018 10:14 WG1159283
Pyrene 5.09 0.0738 0.198 5 09/03/2018 10:14 WG1159283
1,2,4-Trichlorobenzene 0.115 J 0.0525 2.00 5 09/03/2018 10:14 WG1159283
4-Chloro-3-methylphenol U 0.0287 2.00 5 09/03/2018 10:14 WG1159283
2-Chlorophenol U 0.0498 2.00 5 09/03/2018 10:14 WG1159283
2,4-Dichlorophenol U 0.0447 2.00 5 09/03/2018 10:14 WG1159283
2,4-Dimethylphenol U 0.283 2.00 5 09/03/2018 10:14 WG1159283
4,6-Dinitro-2-methylphenol U 0.744 2.00 5 09/03/2018 10:14 WG1159283
2,4-Dinitrophenol U 0.588 2.00 5 09/03/2018 10:14 WG1159283
2-Nitrophenol U 0.0780 2.00 5 09/03/2018 10:14 WG1159283
4-Nitrophenol U 0.315 2.00 5 09/03/2018 10:14 WG1159283
Pentachlorophenol U 0.288 2.00 5 09/03/2018 10:14 WG1159283
Phenol U 0.0416 2.00 5 09/03/2018 10:14 WG1159283
2,4,6-Trichlorophenol U 0.0467 2.00 5 09/03/2018 10:14 WG1159283
(S) 2-Fluorophenol 58.7 12.0-120 09/03/2018 10:14 WG1159283
(S) Phenol-d5 54.9 10.0-120 09/03/2018 10:14 WG1159283
(S) Nitrobenzene-d5 50.0 10.0-122 09/03/2018 10:14 WG1159283
(S) 2-Fluorobiphenyl 61.6 15.0-120 09/03/2018 10:14 WG1159283
(S) 2,4,6-Tribromophenol 73.0 10.0-127 09/03/2018 10:14 WG1159283
(S) p-Terphenyl-d14 58.2 10.0-120 09/03/2018 10:14 WG1159283
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 55 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L1020964
TWSWP-4
Collected date/time: 08/24/18 12:00
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 08/27/2018 12:33 WG1157576
Metals (ICP) by Method 6010D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Arsenic 7.05 J 6.50 10.0 1 08/29/2018 11:56 WG1158118
Barium 72.9 1.70 5.00 1 08/29/2018 11:56 WG1158118
Cadmium U 0.700 2.00 1 08/29/2018 11:56 WG1158118
Chromium U 1.40 10.0 1 08/29/2018 11:56 WG1158118
Lead 4.66 B J 1.90 5.00 1 08/29/2018 11:56 WG1158118
Selenium U 7.40 10.0 1 08/29/2018 11:56 WG1158118
Silver U 2.80 5.00 1 08/29/2018 11:56 WG1158118
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 08/29/2018 00:54 WG1158295
Acrolein U 8.87 50.0 1 08/29/2018 00:54 WG1158295
Acrylonitrile U 1.87 10.0 1 08/29/2018 00:54 WG1158295
Benzene U 0.331 1.00 1 08/29/2018 00:54 WG1158295
Bromobenzene U 0.352 1.00 1 08/29/2018 00:54 WG1158295
Bromodichloromethane U 0.380 1.00 1 08/29/2018 00:54 WG1158295
Bromoform U 0.469 1.00 1 08/29/2018 00:54 WG1158295
Bromomethane U 0.866 5.00 1 08/29/2018 00:54 WG1158295
n-Butylbenzene U 0.361 1.00 1 08/29/2018 00:54 WG1158295
sec-Butylbenzene U 0.365 1.00 1 08/29/2018 00:54 WG1158295
tert-Butylbenzene U 0.399 1.00 1 08/29/2018 00:54 WG1158295
Carbon tetrachloride U 0.379 1.00 1 08/29/2018 00:54 WG1158295
Chlorobenzene U 0.348 1.00 1 08/29/2018 00:54 WG1158295
Chlorodibromomethane U 0.327 1.00 1 08/29/2018 00:54 WG1158295
Chloroethane U 0.453 5.00 1 08/29/2018 00:54 WG1158295
Chloroform U 0.324 5.00 1 08/29/2018 00:54 WG1158295
Chloromethane U 0.276 2.50 1 08/29/2018 00:54 WG1158295
2-Chlorotoluene U 0.375 1.00 1 08/29/2018 00:54 WG1158295
4-Chlorotoluene U 0.351 1.00 1 08/29/2018 00:54 WG1158295
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 08/29/2018 00:54 WG1158295
1,2-Dibromoethane U 0.381 1.00 1 08/29/2018 00:54 WG1158295
Dibromomethane U 0.346 1.00 1 08/29/2018 00:54 WG1158295
1,2-Dichlorobenzene U 0.349 1.00 1 08/29/2018 00:54 WG1158295
1,3-Dichlorobenzene U 0.220 1.00 1 08/29/2018 00:54 WG1158295
1,4-Dichlorobenzene U 0.274 1.00 1 08/29/2018 00:54 WG1158295
Dichlorodifluoromethane U 0.551 5.00 1 08/29/2018 00:54 WG1158295
1,1-Dichloroethane U 0.259 1.00 1 08/29/2018 00:54 WG1158295
1,2-Dichloroethane U 0.361 1.00 1 08/29/2018 00:54 WG1158295
1,1-Dichloroethene U 0.398 1.00 1 08/29/2018 00:54 WG1158295
cis-1,2-Dichloroethene 1.16 0.260 1.00 1 08/29/2018 00:54 WG1158295
trans-1,2-Dichloroethene U 0.396 1.00 1 08/29/2018 00:54 WG1158295
1,2-Dichloropropane U 0.306 1.00 1 08/29/2018 00:54 WG1158295
1,1-Dichloropropene U 0.352 1.00 1 08/29/2018 00:54 WG1158295
1,3-Dichloropropane U 0.366 1.00 1 08/29/2018 00:54 WG1158295
cis-1,3-Dichloropropene U 0.418 1.00 1 08/29/2018 00:54 WG1158295
trans-1,3-Dichloropropene U 0.419 1.00 1 08/29/2018 00:54 WG1158295
2,2-Dichloropropane U 0.321 1.00 1 08/29/2018 00:54 WG1158295
Di-isopropyl ether U 0.320 1.00 1 08/29/2018 00:54 WG1158295
Ethylbenzene U 0.384 1.00 1 08/29/2018 00:54 WG1158295
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 56 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 56 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L1020964
TWSWP-4
Collected date/time: 08/24/18 12:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachloro-1,3-butadiene U 0.256 1.00 1 08/29/2018 00:54 WG1158295
Isopropylbenzene U 0.326 1.00 1 08/29/2018 00:54 WG1158295
p-Isopropyltoluene U 0.350 1.00 1 08/29/2018 00:54 WG1158295
2-Butanone (MEK)U 3.93 10.0 1 08/29/2018 00:54 WG1158295
Methylene Chloride U 1.00 5.00 1 08/29/2018 00:54 WG1158295
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 08/29/2018 00:54 WG1158295
Methyl tert-butyl ether U 0.367 1.00 1 08/29/2018 00:54 WG1158295
Naphthalene U 1.00 5.00 1 08/29/2018 00:54 WG1158295
n-Propylbenzene U 0.349 1.00 1 08/29/2018 00:54 WG1158295
Styrene U 0.307 1.00 1 08/29/2018 00:54 WG1158295
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 08/29/2018 00:54 WG1158295
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 08/29/2018 00:54 WG1158295
1,1,2-Trichlorotrifluoroethane U 0.303 1.00 1 08/29/2018 00:54 WG1158295
Tetrachloroethene 0.379 J 0.372 1.00 1 08/29/2018 00:54 WG1158295
Toluene U 0.412 1.00 1 08/29/2018 00:54 WG1158295
1,2,3-Trichlorobenzene U 0.230 1.00 1 08/29/2018 00:54 WG1158295
1,2,4-Trichlorobenzene U 0.355 1.00 1 08/29/2018 00:54 WG1158295
1,1,1-Trichloroethane U 0.319 1.00 1 08/29/2018 00:54 WG1158295
1,1,2-Trichloroethane U 0.383 1.00 1 08/29/2018 00:54 WG1158295
Trichloroethene 3.17 0.398 1.00 1 08/29/2018 00:54 WG1158295
Trichlorofluoromethane U 1.20 5.00 1 08/29/2018 00:54 WG1158295
1,2,3-Trichloropropane U 0.807 2.50 1 08/29/2018 00:54 WG1158295
1,2,4-Trimethylbenzene U 0.373 1.00 1 08/29/2018 00:54 WG1158295
1,2,3-Trimethylbenzene U 0.321 1.00 1 08/29/2018 00:54 WG1158295
1,3,5-Trimethylbenzene U 0.387 1.00 1 08/29/2018 00:54 WG1158295
Vinyl chloride U 0.259 1.00 1 08/29/2018 00:54 WG1158295
Xylenes, Total U 1.06 3.00 1 08/29/2018 00:54 WG1158295
(S) Toluene-d8 102 80.0-120 08/29/2018 00:54 WG1158295
(S) Dibromofluoromethane 102 75.0-120 08/29/2018 00:54 WG1158295
(S) 4-Bromofluorobenzene 96.6 77.0-126 08/29/2018 00:54 WG1158295
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 09/01/2018 13:38 WG1159178
Acenaphthylene U 0.309 1.00 1 09/01/2018 13:38 WG1159178
Anthracene U 0.291 1.00 1 09/01/2018 13:38 WG1159178
Benzidine U 4.32 10.0 1 09/01/2018 13:38 WG1159178
Benzo(a)anthracene U 0.0975 1.00 1 09/01/2018 13:38 WG1159178
Benzo(b)fluoranthene U 0.0896 1.00 1 09/01/2018 13:38 WG1159178
Benzo(k)fluoranthene U 0.355 1.00 1 09/01/2018 13:38 WG1159178
Benzo(g,h,i)perylene U 0.161 1.00 1 09/01/2018 13:38 WG1159178
Benzo(a)pyrene U 0.340 1.00 1 09/01/2018 13:38 WG1159178
Bis(2-chlorethoxy)methane U 0.329 10.0 1 09/01/2018 13:38 WG1159178
Bis(2-chloroethyl)ether U 1.62 10.0 1 09/01/2018 13:38 WG1159178
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 09/01/2018 13:38 WG1159178
4-Bromophenyl-phenylether U 0.335 10.0 1 09/01/2018 13:38 WG1159178
2-Chloronaphthalene U 0.330 1.00 1 09/01/2018 13:38 WG1159178
4-Chlorophenyl-phenylether U 0.303 10.0 1 09/01/2018 13:38 WG1159178
Chrysene U 0.332 1.00 1 09/01/2018 13:38 WG1159178
Dibenz(a,h)anthracene U 0.279 1.00 1 09/01/2018 13:38 WG1159178
3,3-Dichlorobenzidine U 2.02 10.0 1 09/01/2018 13:38 WG1159178
2,4-Dinitrotoluene U 1.65 10.0 1 09/01/2018 13:38 WG1159178
2,6-Dinitrotoluene U 0.279 10.0 1 09/01/2018 13:38 WG1159178
Fluoranthene U 0.310 1.00 1 09/01/2018 13:38 WG1159178
Fluorene U 0.323 1.00 1 09/01/2018 13:38 WG1159178
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 57 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 57 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L1020964
TWSWP-4
Collected date/time: 08/24/18 12:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorobenzene U 0.341 1.00 1 09/01/2018 13:38 WG1159178
Hexachloro-1,3-butadiene U 0.329 10.0 1 09/01/2018 13:38 WG1159178
Hexachlorocyclopentadiene U 2.33 10.0 1 09/01/2018 13:38 WG1159178
Hexachloroethane U 0.365 10.0 1 09/01/2018 13:38 WG1159178
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/01/2018 13:38 WG1159178
Isophorone U 0.272 10.0 1 09/01/2018 13:38 WG1159178
Naphthalene U 0.372 1.00 1 09/01/2018 13:38 WG1159178
Nitrobenzene U 0.367 10.0 1 09/01/2018 13:38 WG1159178
n-Nitrosodimethylamine U 1.26 10.0 1 09/01/2018 13:38 WG1159178
n-Nitrosodiphenylamine U 1.19 10.0 1 09/01/2018 13:38 WG1159178
n-Nitrosodi-n-propylamine U 0.403 10.0 1 09/01/2018 13:38 WG1159178
Phenanthrene U 0.366 1.00 1 09/01/2018 13:38 WG1159178
Benzylbutyl phthalate U 0.275 3.00 1 09/01/2018 13:38 WG1159178
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 09/01/2018 13:38 WG1159178
Di-n-butyl phthalate U 0.266 3.00 1 09/01/2018 13:38 WG1159178
Diethyl phthalate U 0.282 3.00 1 09/01/2018 13:38 WG1159178
Dimethyl phthalate U J4 0.283 3.00 1 09/01/2018 13:38 WG1159178
Di-n-octyl phthalate U 0.278 3.00 1 09/01/2018 13:38 WG1159178
Pyrene U 0.330 1.00 1 09/01/2018 13:38 WG1159178
1,2,4-Trichlorobenzene U 0.355 10.0 1 09/01/2018 13:38 WG1159178
4-Chloro-3-methylphenol U 0.263 10.0 1 09/01/2018 13:38 WG1159178
2-Chlorophenol U J3 J4 0.283 10.0 1 09/01/2018 13:38 WG1159178
2,4-Dichlorophenol U J3 J4 0.284 10.0 1 09/01/2018 13:38 WG1159178
2,4-Dimethylphenol U 0.264 10.0 1 09/01/2018 13:38 WG1159178
4,6-Dinitro-2-methylphenol U J3 2.62 10.0 1 09/01/2018 13:38 WG1159178
2,4-Dinitrophenol U 3.25 10.0 1 09/01/2018 13:38 WG1159178
2-Nitrophenol U J3 0.320 10.0 1 09/01/2018 13:38 WG1159178
4-Nitrophenol U 2.01 10.0 1 09/01/2018 13:38 WG1159178
Pentachlorophenol U J3 0.313 10.0 1 09/01/2018 13:38 WG1159178
Phenol 0.575 J 0.334 10.0 1 09/01/2018 13:38 WG1159178
2,4,6-Trichlorophenol U 0.297 10.0 1 09/01/2018 13:38 WG1159178
(S) 2-Fluorophenol 20.0 10.0-120 09/01/2018 13:38 WG1159178
(S) Phenol-d5 14.1 10.0-120 09/01/2018 13:38 WG1159178
(S) Nitrobenzene-d5 42.0 10.0-127 09/01/2018 13:38 WG1159178
(S) 2-Fluorobiphenyl 50.4 10.0-130 09/01/2018 13:38 WG1159178
(S) 2,4,6-Tribromophenol 39.0 10.0-155 09/01/2018 13:38 WG1159178
(S) p-Terphenyl-d14 64.3 10.0-128 09/01/2018 13:38 WG1159178
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 58 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 58 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L1020964
TWSWP-7
Collected date/time: 08/24/18 13:00
Mercury by Method 7470A
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Mercury U 0.0490 0.200 1 08/27/2018 12:35 WG1157576
Metals (ICP) by Method 6010D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Arsenic U 6.50 10.0 1 08/29/2018 11:59 WG1158118
Barium 84.8 1.70 5.00 1 08/29/2018 11:59 WG1158118
Cadmium U 0.700 2.00 1 08/29/2018 11:59 WG1158118
Chromium U 1.40 10.0 1 08/29/2018 11:59 WG1158118
Lead U 1.90 5.00 1 08/29/2018 11:59 WG1158118
Selenium U 7.40 10.0 1 08/29/2018 11:59 WG1158118
Silver U 2.80 5.00 1 08/29/2018 11:59 WG1158118
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 08/29/2018 01:14 WG1158295
Acrolein U 8.87 50.0 1 08/29/2018 01:14 WG1158295
Acrylonitrile U 1.87 10.0 1 08/29/2018 01:14 WG1158295
Benzene U 0.331 1.00 1 08/29/2018 01:14 WG1158295
Bromobenzene U 0.352 1.00 1 08/29/2018 01:14 WG1158295
Bromodichloromethane U 0.380 1.00 1 08/29/2018 01:14 WG1158295
Bromoform U 0.469 1.00 1 08/29/2018 01:14 WG1158295
Bromomethane U 0.866 5.00 1 08/29/2018 01:14 WG1158295
n-Butylbenzene U 0.361 1.00 1 08/29/2018 01:14 WG1158295
sec-Butylbenzene U 0.365 1.00 1 08/29/2018 01:14 WG1158295
tert-Butylbenzene U 0.399 1.00 1 08/29/2018 01:14 WG1158295
Carbon tetrachloride U 0.379 1.00 1 08/29/2018 01:14 WG1158295
Chlorobenzene 0.533 J 0.348 1.00 1 08/29/2018 01:14 WG1158295
Chlorodibromomethane U 0.327 1.00 1 08/29/2018 01:14 WG1158295
Chloroethane U 0.453 5.00 1 08/29/2018 01:14 WG1158295
Chloroform 0.418 J 0.324 5.00 1 08/29/2018 01:14 WG1158295
Chloromethane U 0.276 2.50 1 08/29/2018 01:14 WG1158295
2-Chlorotoluene U 0.375 1.00 1 08/29/2018 01:14 WG1158295
4-Chlorotoluene U 0.351 1.00 1 08/29/2018 01:14 WG1158295
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 08/29/2018 01:14 WG1158295
1,2-Dibromoethane U 0.381 1.00 1 08/29/2018 01:14 WG1158295
Dibromomethane U 0.346 1.00 1 08/29/2018 01:14 WG1158295
1,2-Dichlorobenzene U 0.349 1.00 1 08/29/2018 01:14 WG1158295
1,3-Dichlorobenzene U 0.220 1.00 1 08/29/2018 01:14 WG1158295
1,4-Dichlorobenzene U 0.274 1.00 1 08/29/2018 01:14 WG1158295
Dichlorodifluoromethane U 0.551 5.00 1 08/29/2018 01:14 WG1158295
1,1-Dichloroethane 0.408 J 0.259 1.00 1 08/29/2018 01:14 WG1158295
1,2-Dichloroethane 2.98 0.361 1.00 1 08/29/2018 01:14 WG1158295
1,1-Dichloroethene 10.5 0.398 1.00 1 08/29/2018 01:14 WG1158295
cis-1,2-Dichloroethene 1.59 0.260 1.00 1 08/29/2018 01:14 WG1158295
trans-1,2-Dichloroethene U 0.396 1.00 1 08/29/2018 01:14 WG1158295
1,2-Dichloropropane 0.487 J 0.306 1.00 1 08/29/2018 01:14 WG1158295
1,1-Dichloropropene U 0.352 1.00 1 08/29/2018 01:14 WG1158295
1,3-Dichloropropane U 0.366 1.00 1 08/29/2018 01:14 WG1158295
cis-1,3-Dichloropropene U 0.418 1.00 1 08/29/2018 01:14 WG1158295
trans-1,3-Dichloropropene U 0.419 1.00 1 08/29/2018 01:14 WG1158295
2,2-Dichloropropane U 0.321 1.00 1 08/29/2018 01:14 WG1158295
Di-isopropyl ether 2.33 0.320 1.00 1 08/29/2018 01:14 WG1158295
Ethylbenzene U 0.384 1.00 1 08/29/2018 01:14 WG1158295
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 59 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 59 of 105
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L1020964
TWSWP-7
Collected date/time: 08/24/18 13:00
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachloro-1,3-butadiene U 0.256 1.00 1 08/29/2018 01:14 WG1158295
Isopropylbenzene U 0.326 1.00 1 08/29/2018 01:14 WG1158295
p-Isopropyltoluene U 0.350 1.00 1 08/29/2018 01:14 WG1158295
2-Butanone (MEK)U 3.93 10.0 1 08/29/2018 01:14 WG1158295
Methylene Chloride U 1.00 5.00 1 08/29/2018 01:14 WG1158295
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 08/29/2018 01:14 WG1158295
Methyl tert-butyl ether 1.16 0.367 1.00 1 08/29/2018 01:14 WG1158295
Naphthalene U 1.00 5.00 1 08/29/2018 01:14 WG1158295
n-Propylbenzene U 0.349 1.00 1 08/29/2018 01:14 WG1158295
Styrene U 0.307 1.00 1 08/29/2018 01:14 WG1158295
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 08/29/2018 01:14 WG1158295
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 08/29/2018 01:14 WG1158295
1,1,2-Trichlorotrifluoroethane U 0.303 1.00 1 08/29/2018 01:14 WG1158295
Tetrachloroethene 6.64 0.372 1.00 1 08/29/2018 01:14 WG1158295
Toluene U 0.412 1.00 1 08/29/2018 01:14 WG1158295
1,2,3-Trichlorobenzene U 0.230 1.00 1 08/29/2018 01:14 WG1158295
1,2,4-Trichlorobenzene U 0.355 1.00 1 08/29/2018 01:14 WG1158295
1,1,1-Trichloroethane U 0.319 1.00 1 08/29/2018 01:14 WG1158295
1,1,2-Trichloroethane U 0.383 1.00 1 08/29/2018 01:14 WG1158295
Trichloroethene 39.8 0.398 1.00 1 08/29/2018 01:14 WG1158295
Trichlorofluoromethane U 1.20 5.00 1 08/29/2018 01:14 WG1158295
1,2,3-Trichloropropane U 0.807 2.50 1 08/29/2018 01:14 WG1158295
1,2,4-Trimethylbenzene U 0.373 1.00 1 08/29/2018 01:14 WG1158295
1,2,3-Trimethylbenzene U 0.321 1.00 1 08/29/2018 01:14 WG1158295
1,3,5-Trimethylbenzene U 0.387 1.00 1 08/29/2018 01:14 WG1158295
Vinyl chloride U 0.259 1.00 1 08/29/2018 01:14 WG1158295
Xylenes, Total U 1.06 3.00 1 08/29/2018 01:14 WG1158295
(S) Toluene-d8 99.0 80.0-120 08/29/2018 01:14 WG1158295
(S) Dibromofluoromethane 101 75.0-120 08/29/2018 01:14 WG1158295
(S) 4-Bromofluorobenzene 98.4 77.0-126 08/29/2018 01:14 WG1158295
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 09/01/2018 14:02 WG1159178
Acenaphthylene U 0.309 1.00 1 09/01/2018 14:02 WG1159178
Anthracene U 0.291 1.00 1 09/01/2018 14:02 WG1159178
Benzidine U 4.32 10.0 1 09/01/2018 14:02 WG1159178
Benzo(a)anthracene U 0.0975 1.00 1 09/01/2018 14:02 WG1159178
Benzo(b)fluoranthene U 0.0896 1.00 1 09/01/2018 14:02 WG1159178
Benzo(k)fluoranthene U 0.355 1.00 1 09/01/2018 14:02 WG1159178
Benzo(g,h,i)perylene U 0.161 1.00 1 09/01/2018 14:02 WG1159178
Benzo(a)pyrene U 0.340 1.00 1 09/01/2018 14:02 WG1159178
Bis(2-chlorethoxy)methane U 0.329 10.0 1 09/01/2018 14:02 WG1159178
Bis(2-chloroethyl)ether U 1.62 10.0 1 09/01/2018 14:02 WG1159178
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 09/01/2018 14:02 WG1159178
4-Bromophenyl-phenylether U 0.335 10.0 1 09/01/2018 14:02 WG1159178
2-Chloronaphthalene U 0.330 1.00 1 09/01/2018 14:02 WG1159178
4-Chlorophenyl-phenylether U 0.303 10.0 1 09/01/2018 14:02 WG1159178
Chrysene U 0.332 1.00 1 09/01/2018 14:02 WG1159178
Dibenz(a,h)anthracene U 0.279 1.00 1 09/01/2018 14:02 WG1159178
3,3-Dichlorobenzidine U 2.02 10.0 1 09/01/2018 14:02 WG1159178
2,4-Dinitrotoluene U 1.65 10.0 1 09/01/2018 14:02 WG1159178
2,6-Dinitrotoluene U 0.279 10.0 1 09/01/2018 14:02 WG1159178
Fluoranthene U 0.310 1.00 1 09/01/2018 14:02 WG1159178
Fluorene U 0.323 1.00 1 09/01/2018 14:02 WG1159178
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L1020964
TWSWP-7
Collected date/time: 08/24/18 13:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachlorobenzene U 0.341 1.00 1 09/01/2018 14:02 WG1159178
Hexachloro-1,3-butadiene U 0.329 10.0 1 09/01/2018 14:02 WG1159178
Hexachlorocyclopentadiene U 2.33 10.0 1 09/01/2018 14:02 WG1159178
Hexachloroethane U 0.365 10.0 1 09/01/2018 14:02 WG1159178
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 09/01/2018 14:02 WG1159178
Isophorone U 0.272 10.0 1 09/01/2018 14:02 WG1159178
Naphthalene U 0.372 1.00 1 09/01/2018 14:02 WG1159178
Nitrobenzene U 0.367 10.0 1 09/01/2018 14:02 WG1159178
n-Nitrosodimethylamine U 1.26 10.0 1 09/01/2018 14:02 WG1159178
n-Nitrosodiphenylamine U 1.19 10.0 1 09/01/2018 14:02 WG1159178
n-Nitrosodi-n-propylamine U 0.403 10.0 1 09/01/2018 14:02 WG1159178
Phenanthrene U 0.366 1.00 1 09/01/2018 14:02 WG1159178
Benzylbutyl phthalate U 0.275 3.00 1 09/01/2018 14:02 WG1159178
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 09/01/2018 14:02 WG1159178
Di-n-butyl phthalate U 0.266 3.00 1 09/01/2018 14:02 WG1159178
Diethyl phthalate U 0.282 3.00 1 09/01/2018 14:02 WG1159178
Dimethyl phthalate U J4 0.283 3.00 1 09/01/2018 14:02 WG1159178
Di-n-octyl phthalate U 0.278 3.00 1 09/01/2018 14:02 WG1159178
Pyrene U 0.330 1.00 1 09/01/2018 14:02 WG1159178
1,2,4-Trichlorobenzene U 0.355 10.0 1 09/01/2018 14:02 WG1159178
4-Chloro-3-methylphenol U 0.263 10.0 1 09/01/2018 14:02 WG1159178
2-Chlorophenol U J3 J4 0.283 10.0 1 09/01/2018 14:02 WG1159178
2,4-Dichlorophenol U J3 J4 0.284 10.0 1 09/01/2018 14:02 WG1159178
2,4-Dimethylphenol U 0.264 10.0 1 09/01/2018 14:02 WG1159178
4,6-Dinitro-2-methylphenol U J3 2.62 10.0 1 09/01/2018 14:02 WG1159178
2,4-Dinitrophenol U 3.25 10.0 1 09/01/2018 14:02 WG1159178
2-Nitrophenol U J3 0.320 10.0 1 09/01/2018 14:02 WG1159178
4-Nitrophenol U 2.01 10.0 1 09/01/2018 14:02 WG1159178
Pentachlorophenol U J3 0.313 10.0 1 09/01/2018 14:02 WG1159178
Phenol 0.620 J 0.334 10.0 1 09/01/2018 14:02 WG1159178
2,4,6-Trichlorophenol U 0.297 10.0 1 09/01/2018 14:02 WG1159178
(S) 2-Fluorophenol 14.3 10.0-120 09/01/2018 14:02 WG1159178
(S) Phenol-d5 9.07 J2 10.0-120 09/01/2018 14:02 WG1159178
(S) Nitrobenzene-d5 50.7 10.0-127 09/01/2018 14:02 WG1159178
(S) 2-Fluorobiphenyl 56.2 10.0-130 09/01/2018 14:02 WG1159178
(S) 2,4,6-Tribromophenol 28.1 10.0-155 09/01/2018 14:02 WG1159178
(S) p-Terphenyl-d14 61.3 10.0-128 09/01/2018 14:02 WG1159178
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L1020964
OUTFALL
Collected date/time: 08/24/18 13:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 08/29/2018 01:34 WG1158295
Acrolein U 8.87 50.0 1 08/29/2018 01:34 WG1158295
Acrylonitrile U 1.87 10.0 1 08/29/2018 01:34 WG1158295
Benzene U 0.331 1.00 1 08/29/2018 01:34 WG1158295
Bromobenzene U 0.352 1.00 1 08/29/2018 01:34 WG1158295
Bromodichloromethane U 0.380 1.00 1 08/29/2018 01:34 WG1158295
Bromoform U 0.469 1.00 1 08/29/2018 01:34 WG1158295
Bromomethane U 0.866 5.00 1 08/29/2018 01:34 WG1158295
n-Butylbenzene U 0.361 1.00 1 08/29/2018 01:34 WG1158295
sec-Butylbenzene U 0.365 1.00 1 08/29/2018 01:34 WG1158295
tert-Butylbenzene U 0.399 1.00 1 08/29/2018 01:34 WG1158295
Carbon tetrachloride U 0.379 1.00 1 08/29/2018 01:34 WG1158295
Chlorobenzene U 0.348 1.00 1 08/29/2018 01:34 WG1158295
Chlorodibromomethane U 0.327 1.00 1 08/29/2018 01:34 WG1158295
Chloroethane U 0.453 5.00 1 08/29/2018 01:34 WG1158295
Chloroform U 0.324 5.00 1 08/29/2018 01:34 WG1158295
Chloromethane U 0.276 2.50 1 08/29/2018 01:34 WG1158295
2-Chlorotoluene U 0.375 1.00 1 08/29/2018 01:34 WG1158295
4-Chlorotoluene U 0.351 1.00 1 08/29/2018 01:34 WG1158295
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 08/29/2018 01:34 WG1158295
1,2-Dibromoethane U 0.381 1.00 1 08/29/2018 01:34 WG1158295
Dibromomethane U 0.346 1.00 1 08/29/2018 01:34 WG1158295
1,2-Dichlorobenzene U 0.349 1.00 1 08/29/2018 01:34 WG1158295
1,3-Dichlorobenzene U 0.220 1.00 1 08/29/2018 01:34 WG1158295
1,4-Dichlorobenzene U 0.274 1.00 1 08/29/2018 01:34 WG1158295
Dichlorodifluoromethane U 0.551 5.00 1 08/29/2018 01:34 WG1158295
1,1-Dichloroethane U 0.259 1.00 1 08/29/2018 01:34 WG1158295
1,2-Dichloroethane 0.407 J 0.361 1.00 1 08/29/2018 01:34 WG1158295
1,1-Dichloroethene 0.772 J 0.398 1.00 1 08/29/2018 01:34 WG1158295
cis-1,2-Dichloroethene 0.476 J 0.260 1.00 1 08/29/2018 01:34 WG1158295
trans-1,2-Dichloroethene U 0.396 1.00 1 08/29/2018 01:34 WG1158295
1,2-Dichloropropane U 0.306 1.00 1 08/29/2018 01:34 WG1158295
1,1-Dichloropropene U 0.352 1.00 1 08/29/2018 01:34 WG1158295
1,3-Dichloropropane U 0.366 1.00 1 08/29/2018 01:34 WG1158295
cis-1,3-Dichloropropene U 0.418 1.00 1 08/29/2018 01:34 WG1158295
trans-1,3-Dichloropropene U 0.419 1.00 1 08/29/2018 01:34 WG1158295
2,2-Dichloropropane U 0.321 1.00 1 08/29/2018 01:34 WG1158295
Di-isopropyl ether 0.434 J 0.320 1.00 1 08/29/2018 01:34 WG1158295
Ethylbenzene U 0.384 1.00 1 08/29/2018 01:34 WG1158295
Hexachloro-1,3-butadiene U 0.256 1.00 1 08/29/2018 01:34 WG1158295
Isopropylbenzene U 0.326 1.00 1 08/29/2018 01:34 WG1158295
p-Isopropyltoluene U 0.350 1.00 1 08/29/2018 01:34 WG1158295
2-Butanone (MEK)U 3.93 10.0 1 08/29/2018 01:34 WG1158295
Methylene Chloride U 1.00 5.00 1 08/29/2018 01:34 WG1158295
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 08/29/2018 01:34 WG1158295
Methyl tert-butyl ether U 0.367 1.00 1 08/29/2018 01:34 WG1158295
Naphthalene U 1.00 5.00 1 08/29/2018 01:34 WG1158295
n-Propylbenzene U 0.349 1.00 1 08/29/2018 01:34 WG1158295
Styrene U 0.307 1.00 1 08/29/2018 01:34 WG1158295
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 08/29/2018 01:34 WG1158295
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 08/29/2018 01:34 WG1158295
1,1,2-Trichlorotrifluoroethane U 0.303 1.00 1 08/29/2018 01:34 WG1158295
Tetrachloroethene 1.00 0.372 1.00 1 08/29/2018 01:34 WG1158295
Toluene U 0.412 1.00 1 08/29/2018 01:34 WG1158295
1,2,3-Trichlorobenzene U 0.230 1.00 1 08/29/2018 01:34 WG1158295
1,2,4-Trichlorobenzene U 0.355 1.00 1 08/29/2018 01:34 WG1158295
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L1020964
OUTFALL
Collected date/time: 08/24/18 13:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
1,1,1-Trichloroethane U 0.319 1.00 1 08/29/2018 01:34 WG1158295
1,1,2-Trichloroethane U 0.383 1.00 1 08/29/2018 01:34 WG1158295
Trichloroethene 5.40 0.398 1.00 1 08/29/2018 01:34 WG1158295
Trichlorofluoromethane U 1.20 5.00 1 08/29/2018 01:34 WG1158295
1,2,3-Trichloropropane U 0.807 2.50 1 08/29/2018 01:34 WG1158295
1,2,4-Trimethylbenzene U 0.373 1.00 1 08/29/2018 01:34 WG1158295
1,2,3-Trimethylbenzene U 0.321 1.00 1 08/29/2018 01:34 WG1158295
1,3,5-Trimethylbenzene U 0.387 1.00 1 08/29/2018 01:34 WG1158295
Vinyl chloride U 0.259 1.00 1 08/29/2018 01:34 WG1158295
Xylenes, Total U 1.06 3.00 1 08/29/2018 01:34 WG1158295
(S) Toluene-d8 98.1 80.0-120 08/29/2018 01:34 WG1158295
(S) Dibromofluoromethane 105 75.0-120 08/29/2018 01:34 WG1158295
(S) 4-Bromofluorobenzene 97.6 77.0-126 08/29/2018 01:34 WG1158295
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 63 of 105
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159443
Total Solids by Method 2540 G-2011 L1020964-01,02
Method Blank (MB)
(MB) R3338797-1 08/31/18 10:44
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1020937-14 Original Sample (OS) • Duplicate (DUP)
(OS) L1020937-14 08/31/18 10:44 • (DUP) R3338797-3 08/31/18 10:44
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 81.3 85.9 1 5.46 10
Laboratory Control Sample (LCS)
(LCS) R3338797-2 08/31/18 10:44
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 64 of 105
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159446
Total Solids by Method 2540 G-2011 L1020964-03,04,05,06,07,08,09,10,11,12
Method Blank (MB)
(MB) R3338239-1 08/30/18 13:29
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1020964-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1020964-04 08/30/18 13:29 • (DUP) R3338239-3 08/30/18 13:29
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 79.1 81.3 1 2.70 10
Laboratory Control Sample (LCS)
(LCS) R3338239-2 08/30/18 13:29
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 65 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 65 of 105
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159535
Total Solids by Method 2540 G-2011 L1020964-13
Method Blank (MB)
(MB) R3338236-1 08/30/18 12:50
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1021483-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1021483-01 08/30/18 12:50 • (DUP) R3338236-3 08/30/18 12:50
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 83.6 80.7 1 3.45 10
Laboratory Control Sample (LCS)
(LCS) R3338236-2 08/30/18 12:50
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 66 of 105
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159541
Total Solids by Method 2540 G-2011 L1020964-16
Method Blank (MB)
(MB) R3338237-1 08/30/18 13:15
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1021301-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1021301-04 08/30/18 13:15 • (DUP) R3338237-3 08/30/18 13:15
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 85.3 84.3 1 1.14 10
Laboratory Control Sample (LCS)
(LCS) R3338237-2 08/30/18 13:15
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 67 of 105
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159714
Total Solids by Method 2540 G-2011 L1020964-14,15
Method Blank (MB)
(MB) R3338800-1 08/31/18 10:56
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1021681-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1021681-01 08/31/18 10:56 • (DUP) R3338800-3 08/31/18 10:56
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 84.8 85.2 1 0.502 10
Laboratory Control Sample (LCS)
(LCS) R3338800-2 08/31/18 10:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 68 of 105
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1157576
Mercury by Method 7470A L1020964-17,18
Method Blank (MB)
(MB) R3336930-1 08/27/18 11:30
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Mercury U 0.0490 0.200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3336930-2 08/27/18 11:32 • (LCSD) R3336930-3 08/27/18 11:34
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Mercury 3.00 3.16 3.11 105 104 80.0-120 1.55 20
L1020499-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1020499-01 08/27/18 11:37 • (MS) R3336930-4 08/27/18 11:39 • (MSD) R3336930-5 08/27/18 11:41
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Mercury 3.00 U 3.24 3.26 108 109 1 75.0-125 0.689 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 69 of 105
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159451
Mercury by Method 7471B L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16
Method Blank (MB)
(MB) R3338410-1 08/31/18 11:26
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury 0.00460 J 0.00280 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338410-2 08/31/18 11:29 • (LCSD) R3338410-3 08/31/18 11:31
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.253 0.255 84.2 84.9 80.0-120 0.897 20
L1020964-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1020964-14 08/31/18 11:34 • (MS) R3338410-4 08/31/18 11:36 • (MSD) R3338410-5 08/31/18 11:39
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.349 0.00652 0.300 0.325 84.2 91.5 1 75.0-125 8.07 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1158118
Metals (ICP) by Method 6010D L1020964-17,18
Method Blank (MB)
(MB) R3337782-1 08/29/18 11:12
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Arsenic U 6.50 10.0
Barium U 1.70 5.00
Cadmium U 0.700 2.00
Chromium U 1.40 10.0
Lead 3.09 J 1.90 5.00
Selenium U 7.40 10.0
Silver U 2.80 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3337782-2 08/29/18 11:14 • (LCSD) R3337782-3 08/29/18 11:17
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Arsenic 1000 1000 1030 100 103 80.0-120 2.98 20
Barium 1000 1040 1070 104 107 80.0-120 2.82 20
Cadmium 1000 1030 1060 103 106 80.0-120 2.89 20
Chromium 1000 995 1030 99.5 103 80.0-120 3.04 20
Lead 1000 979 1010 97.9 101 80.0-120 3.55 20
Selenium 1000 1010 1040 101 104 80.0-120 2.16 20
Silver 200 201 207 100 103 80.0-120 3.01 20
L1020695-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1020695-04 08/29/18 11:19 • (MS) R3337782-5 08/29/18 11:24 • (MSD) R3337782-6 08/29/18 11:27
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Arsenic 1000 U 1020 1030 102 103 1 75.0-125 0.619 20
Barium 1000 41.6 1100 1110 105 106 1 75.0-125 1.02 20
Cadmium 1000 U 1040 1050 104 105 1 75.0-125 1.17 20
Chromium 1000 2.01 997 1010 99.5 101 1 75.0-125 1.70 20
Lead 1000 3.82 988 996 98.4 99.2 1 75.0-125 0.846 20
Selenium 1000 U 1020 1030 102 103 1 75.0-125 0.976 20
Silver 200 U 202 205 101 102 1 75.0-125 1.07 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159261
Metals (ICP) by Method 6010D L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16
Method Blank (MB)
(MB) R3338494-1 08/31/18 14:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.460 2.00
Barium U 0.170 0.500
Cadmium U 0.0700 0.500
Chromium U 0.140 1.00
Lead U 0.190 0.500
Selenium U 0.620 2.00
Silver U 0.120 1.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338494-2 08/31/18 14:38 • (LCSD) R3338494-3 08/31/18 14:40
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Arsenic 100 93.8 95.6 93.8 95.6 80.0-120 1.89 20
Barium 100 99.7 101 99.7 101 80.0-120 1.46 20
Cadmium 100 94.6 96.0 94.6 96.0 80.0-120 1.52 20
Chromium 100 98.2 98.6 98.2 98.6 80.0-120 0.401 20
Lead 100 96.1 97.7 96.1 97.7 80.0-120 1.61 20
Selenium 100 93.3 95.4 93.3 95.4 80.0-120 2.18 20
Silver 20.0 18.4 18.6 91.8 93.0 80.0-120 1.21 20
L1020964-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1020964-07 08/31/18 14:43 • (MS) R3338494-6 08/31/18 14:51 • (MSD) R3338494-7 08/31/18 14:53
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 126 0.908 118 120 93.0 94.2 1 75.0-125 1.26 20
Barium 126 88.6 203 192 90.5 81.7 1 75.0-125 5.63 20
Cadmium 126 0.305 124 125 97.9 98.4 1 75.0-125 0.426 20
Chromium 126 21.9 147 143 99.3 95.6 1 75.0-125 3.22 20
Lead 126 128 197 192 55.2 50.6 1 75.0-125 J6 J6 2.96 20
Selenium 126 U 118 120 93.2 94.6 1 75.0-125 1.49 20
Silver 25.3 U 24.0 24.2 95.0 95.9 1 75.0-125 0.990 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1158295
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-17,18,19
Method Blank (MB)
(MB) R3337351-3 08/28/18 10:18
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 10.0 50.0
Acrolein U 8.87 50.0
Acrylonitrile U 1.87 10.0
Benzene U 0.331 1.00
Bromobenzene U 0.352 1.00
Bromodichloromethane U 0.380 1.00
Bromoform U 0.469 1.00
Bromomethane U 0.866 5.00
n-Butylbenzene U 0.361 1.00
sec-Butylbenzene U 0.365 1.00
tert-Butylbenzene U 0.399 1.00
Carbon tetrachloride U 0.379 1.00
Chlorobenzene U 0.348 1.00
Chlorodibromomethane U 0.327 1.00
Chloroethane U 0.453 5.00
Chloroform U 0.324 5.00
Chloromethane U 0.276 2.50
2-Chlorotoluene U 0.375 1.00
4-Chlorotoluene U 0.351 1.00
1,2-Dibromo-3-Chloropropane U 1.33 5.00
1,2-Dibromoethane U 0.381 1.00
Dibromomethane U 0.346 1.00
1,2-Dichlorobenzene U 0.349 1.00
1,3-Dichlorobenzene U 0.220 1.00
1,4-Dichlorobenzene U 0.274 1.00
Dichlorodifluoromethane U 0.551 5.00
1,1-Dichloroethane U 0.259 1.00
1,2-Dichloroethane U 0.361 1.00
1,1-Dichloroethene U 0.398 1.00
cis-1,2-Dichloroethene U 0.260 1.00
trans-1,2-Dichloroethene U 0.396 1.00
1,2-Dichloropropane U 0.306 1.00
1,1-Dichloropropene U 0.352 1.00
1,3-Dichloropropane U 0.366 1.00
cis-1,3-Dichloropropene U 0.418 1.00
trans-1,3-Dichloropropene U 0.419 1.00
2,2-Dichloropropane U 0.321 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
Hexachloro-1,3-butadiene U 0.256 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1158295
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-17,18,19
Method Blank (MB)
(MB) R3337351-3 08/28/18 10:18
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Isopropylbenzene U 0.326 1.00
p-Isopropyltoluene U 0.350 1.00
2-Butanone (MEK)U 3.93 10.0
Methylene Chloride U 1.00 5.00
4-Methyl-2-pentanone (MIBK) U 2.14 10.0
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.349 1.00
Styrene U 0.307 1.00
1,1,1,2-Tetrachloroethane U 0.385 1.00
1,1,2,2-Tetrachloroethane U 0.130 1.00
Tetrachloroethene U 0.372 1.00
Toluene U 0.412 1.00
1,1,2-Trichlorotrifluoroethane U 0.303 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.355 1.00
1,1,1-Trichloroethane U 0.319 1.00
1,1,2-Trichloroethane U 0.383 1.00
Trichloroethene U 0.398 1.00
Trichlorofluoromethane U 1.20 5.00
1,2,3-Trichloropropane U 0.807 2.50
1,2,3-Trimethylbenzene U 0.321 1.00
1,2,4-Trimethylbenzene U 0.373 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
Vinyl chloride U 0.259 1.00
Xylenes, Total U 1.06 3.00
(S) Toluene-d8 102 80.0-120
(S) Dibromofluoromethane 105 75.0-120
(S) 4-Bromofluorobenzene 96.3 77.0-126
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3337351-1 08/28/18 09:19 • (LCSD) R3337351-2 08/28/18 09:38
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 125 197 169 158 135 19.0-160 15.6 27
Acrolein 125 16.0 17.2 12.8 13.7 10.0-160 6.71 26
Acrylonitrile 125 146 139 117 111 55.0-149 5.04 20
Benzene 25.0 28.6 28.2 115 113 70.0-123 1.65 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1158295
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-17,18,19
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3337351-1 08/28/18 09:19 • (LCSD) R3337351-2 08/28/18 09:38
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromobenzene 25.0 25.3 27.0 101 108 73.0-121 6.76 20
Bromodichloromethane 25.0 24.6 24.5 98.6 98.0 75.0-120 0.599 20
Bromoform 25.0 24.4 25.3 97.5 101 68.0-132 3.49 20
Bromomethane 25.0 27.5 28.1 110 112 10.0-160 2.11 25
n-Butylbenzene 25.0 26.2 27.7 105 111 73.0-125 5.68 20
sec-Butylbenzene 25.0 27.4 28.5 109 114 75.0-125 4.15 20
tert-Butylbenzene 25.0 27.3 28.0 109 112 76.0-124 2.66 20
Carbon tetrachloride 25.0 27.0 26.2 108 105 68.0-126 3.08 20
Chlorobenzene 25.0 25.7 26.3 103 105 80.0-121 1.99 20
Chlorodibromomethane 25.0 24.8 25.2 99.3 101 77.0-125 1.59 20
Chloroethane 25.0 30.4 28.7 122 115 47.0-150 5.89 20
Chloroform 25.0 27.7 27.6 111 110 73.0-120 0.551 20
Chloromethane 25.0 27.1 27.1 108 108 41.0-142 0.0614 20
2-Chlorotoluene 25.0 27.5 28.6 110 114 76.0-123 3.87 20
4-Chlorotoluene 25.0 26.7 27.2 107 109 75.0-122 2.12 20
1,2-Dibromo-3-Chloropropane 25.0 26.9 26.1 108 105 58.0-134 2.87 20
1,2-Dibromoethane 25.0 26.4 27.4 105 110 80.0-122 4.07 20
Dibromomethane 25.0 27.4 26.9 110 108 80.0-120 1.84 20
1,2-Dichlorobenzene 25.0 26.6 26.5 107 106 79.0-121 0.415 20
1,3-Dichlorobenzene 25.0 27.1 27.6 108 110 79.0-120 1.91 20
1,4-Dichlorobenzene 25.0 26.1 26.8 105 107 79.0-120 2.30 20
Dichlorodifluoromethane 25.0 27.5 27.6 110 110 51.0-149 0.164 20
1,1-Dichloroethane 25.0 28.7 28.8 115 115 70.0-126 0.237 20
1,2-Dichloroethane 25.0 27.9 27.0 112 108 70.0-128 3.48 20
1,1-Dichloroethene 25.0 28.9 29.0 116 116 71.0-124 0.266 20
cis-1,2-Dichloroethene 25.0 27.9 27.7 112 111 73.0-120 0.748 20
trans-1,2-Dichloroethene 25.0 28.0 27.4 112 109 73.0-120 2.30 20
1,2-Dichloropropane 25.0 26.5 26.7 106 107 77.0-125 0.816 20
1,1-Dichloropropene 25.0 29.6 30.2 118 121 74.0-126 2.05 20
1,3-Dichloropropane 25.0 26.1 26.6 104 106 80.0-120 1.86 20
cis-1,3-Dichloropropene 25.0 25.8 25.8 103 103 80.0-123 0.142 20
trans-1,3-Dichloropropene 25.0 25.4 26.4 101 106 78.0-124 4.21 20
2,2-Dichloropropane 25.0 30.4 29.9 122 120 58.0-130 1.46 20
Di-isopropyl ether 25.0 26.7 26.2 107 105 58.0-138 1.70 20
Ethylbenzene 25.0 26.4 26.4 106 106 79.0-123 0.0858 20
Hexachloro-1,3-butadiene 25.0 23.9 25.0 95.5 99.9 54.0-138 4.46 20
Isopropylbenzene 25.0 25.4 26.2 102 105 76.0-127 3.12 20
p-Isopropyltoluene 25.0 26.4 27.7 106 111 76.0-125 4.80 20
2-Butanone (MEK)125 194 182 155 146 44.0-160 6.05 20
Methylene Chloride 25.0 25.3 24.5 101 98.1 67.0-120 3.00 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1158295
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-17,18,19
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3337351-1 08/28/18 09:19 • (LCSD) R3337351-2 08/28/18 09:38
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
4-Methyl-2-pentanone (MIBK) 125 132 130 106 104 68.0-142 1.69 20
Methyl tert-butyl ether 25.0 26.5 26.2 106 105 68.0-125 1.18 20
Naphthalene 25.0 25.3 27.2 101 109 54.0-135 7.35 20
n-Propylbenzene 25.0 27.3 28.6 109 115 77.0-124 4.94 20
Styrene 25.0 25.4 26.5 102 106 73.0-130 4.36 20
1,1,1,2-Tetrachloroethane 25.0 24.5 23.9 98.1 95.8 75.0-125 2.44 20
1,1,2,2-Tetrachloroethane 25.0 26.1 26.8 105 107 65.0-130 2.44 20
Tetrachloroethene 25.0 25.9 26.0 103 104 72.0-132 0.394 20
Toluene 25.0 24.8 24.9 99.0 99.7 79.0-120 0.657 20
1,1,2-Trichlorotrifluoroethane 25.0 28.3 28.8 113 115 69.0-132 1.52 20
1,2,3-Trichlorobenzene 25.0 25.3 26.7 101 107 50.0-138 5.66 20
1,2,4-Trichlorobenzene 25.0 25.2 26.7 101 107 57.0-137 5.97 20
1,1,1-Trichloroethane 25.0 28.8 28.4 115 114 73.0-124 1.08 20
1,1,2-Trichloroethane 25.0 24.4 25.0 97.5 100 80.0-120 2.69 20
Trichloroethene 25.0 26.2 27.0 105 108 78.0-124 3.11 20
Trichlorofluoromethane 25.0 28.6 28.1 114 112 59.0-147 1.64 20
1,2,3-Trichloropropane 25.0 26.3 25.6 105 103 73.0-130 2.48 20
1,2,3-Trimethylbenzene 25.0 26.5 27.6 106 111 77.0-120 4.37 20
1,2,4-Trimethylbenzene 25.0 27.1 26.9 108 107 76.0-121 0.752 20
1,3,5-Trimethylbenzene 25.0 26.2 27.7 105 111 76.0-122 5.51 20
Vinyl chloride 25.0 29.9 29.8 120 119 67.0-131 0.377 20
Xylenes, Total 75.0 76.9 78.1 103 104 79.0-123 1.55 20
(S) Toluene-d8 99.4 100 80.0-120
(S) Dibromofluoromethane 106 103 75.0-120
(S) 4-Bromofluorobenzene 98.7 103 77.0-126
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159831
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3338241-2 08/30/18 21:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0137 0.0250
Acrylonitrile U 0.00190 0.0125
Benzene U 0.000400 0.00100
Bromobenzene U 0.00105 0.0125
Bromodichloromethane U 0.000788 0.00250
Bromoform U 0.00598 0.0250
Bromomethane U 0.00370 0.0125
n-Butylbenzene 0.00737 J 0.00384 0.0125
sec-Butylbenzene 0.00621 J 0.00253 0.0125
tert-Butylbenzene 0.00157 J 0.00155 0.00500
Carbon tetrachloride U 0.00108 0.00500
Chlorobenzene U 0.000573 0.00250
Chlorodibromomethane U 0.000450 0.00250
Chloroethane U 0.00108 0.00500
Chloroform U 0.000415 0.00250
Chloromethane U 0.00139 0.0125
2-Chlorotoluene U 0.000920 0.00250
4-Chlorotoluene U 0.00113 0.00500
1,2-Dibromo-3-Chloropropane U 0.00510 0.0250
1,2-Dibromoethane U 0.000525 0.00250
Dibromomethane U 0.00100 0.00500
1,2-Dichlorobenzene U 0.00145 0.00500
1,3-Dichlorobenzene U 0.00170 0.00500
1,4-Dichlorobenzene U 0.00197 0.00500
Dichlorodifluoromethane U 0.000818 0.00250
1,1-Dichloroethane U 0.000575 0.00250
1,2-Dichloroethane U 0.000475 0.00250
1,1-Dichloroethene U 0.000500 0.00250
cis-1,2-Dichloroethene U 0.000690 0.00250
trans-1,2-Dichloroethene U 0.00143 0.00500
1,2-Dichloropropane U 0.00127 0.00500
1,1-Dichloropropene U 0.000700 0.00250
1,3-Dichloropropane U 0.00175 0.00500
cis-1,3-Dichloropropene U 0.000678 0.00250
trans-1,3-Dichloropropene U 0.00153 0.00500
2,2-Dichloropropane U 0.000793 0.00250
Di-isopropyl ether U 0.000350 0.00100
Ethylbenzene U 0.000530 0.00250
Hexachloro-1,3-butadiene 0.0138 J 0.0127 0.0250
Isopropylbenzene U 0.000863 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159831
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3338241-2 08/30/18 21:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00233 0.00500
2-Butanone (MEK)U 0.0125 0.0250
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.0100 0.0250
Methyl tert-butyl ether U 0.000295 0.00100
Naphthalene U 0.00312 0.0125
n-Propylbenzene 0.00119 J 0.00118 0.00500
Styrene U 0.00273 0.0125
1,1,1,2-Tetrachloroethane U 0.000500 0.00250
1,1,2,2-Tetrachloroethane U 0.000390 0.00250
Tetrachloroethene U 0.000700 0.00250
Toluene U 0.00125 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000675 0.00250
1,2,3-Trichlorobenzene U 0.000625 0.00250
1,2,4-Trichlorobenzene U 0.00482 0.0125
1,1,1-Trichloroethane U 0.000275 0.00250
1,1,2-Trichloroethane U 0.000883 0.00250
Trichloroethene U 0.000400 0.00100
Trichlorofluoromethane U 0.000500 0.00250
1,2,3-Trichloropropane U 0.00510 0.0125
1,2,4-Trimethylbenzene 0.00475 J 0.00116 0.00500
1,3,5-Trimethylbenzene 0.00127 J 0.00108 0.00500
Vinyl chloride U 0.000683 0.00250
Xylenes, Total U 0.00478 0.00650
(S) Toluene-d8 108 75.0-131
(S) Dibromofluoromethane 100 65.0-129
(S) 4-Bromofluorobenzene 106 67.0-138
Laboratory Control Sample (LCS)
(LCS) R3338241-1 08/30/18 19:48
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.685 110 10.0-160
Acrylonitrile 0.625 0.633 101 45.0-153
Benzene 0.125 0.124 98.9 70.0-123
Bromobenzene 0.125 0.123 98.5 73.0-121
Bromodichloromethane 0.125 0.124 99.5 73.0-121
Bromoform 0.125 0.125 100 64.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159831
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13
Laboratory Control Sample (LCS)
(LCS) R3338241-1 08/30/18 19:48
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bromomethane 0.125 0.133 106 56.0-147
n-Butylbenzene 0.125 0.178 142 68.0-135 J4
sec-Butylbenzene 0.125 0.127 102 74.0-130
tert-Butylbenzene 0.125 0.109 87.4 75.0-127
Carbon tetrachloride 0.125 0.126 101 66.0-128
Chlorobenzene 0.125 0.123 98.3 76.0-128
Chlorodibromomethane 0.125 0.117 93.6 74.0-127
Chloroethane 0.125 0.133 107 61.0-134
Chloroform 0.125 0.126 101 72.0-123
Chloromethane 0.125 0.142 113 51.0-138
2-Chlorotoluene 0.125 0.127 102 75.0-124
4-Chlorotoluene 0.125 0.118 94.6 75.0-124
1,2-Dibromo-3-Chloropropane 0.125 0.139 111 59.0-130
1,2-Dibromoethane 0.125 0.128 103 74.0-128
Dibromomethane 0.125 0.123 98.5 75.0-122
1,2-Dichlorobenzene 0.125 0.114 91.4 76.0-124
1,3-Dichlorobenzene 0.125 0.110 87.9 76.0-125
1,4-Dichlorobenzene 0.125 0.114 91.5 77.0-121
Dichlorodifluoromethane 0.125 0.144 115 43.0-156
1,1-Dichloroethane 0.125 0.130 104 70.0-127
1,2-Dichloroethane 0.125 0.126 101 65.0-131
1,1-Dichloroethene 0.125 0.133 106 65.0-131
cis-1,2-Dichloroethene 0.125 0.102 81.9 73.0-125
trans-1,2-Dichloroethene 0.125 0.131 105 71.0-125
1,2-Dichloropropane 0.125 0.129 103 74.0-125
1,1-Dichloropropene 0.125 0.144 115 73.0-125
1,3-Dichloropropane 0.125 0.134 107 80.0-125
cis-1,3-Dichloropropene 0.125 0.120 95.7 76.0-127
trans-1,3-Dichloropropene 0.125 0.130 104 73.0-127
2,2-Dichloropropane 0.125 0.112 89.8 59.0-135
Di-isopropyl ether 0.125 0.116 92.9 60.0-136
Ethylbenzene 0.125 0.127 101 74.0-126
Hexachloro-1,3-butadiene 0.125 0.119 95.2 57.0-150
Isopropylbenzene 0.125 0.106 84.7 72.0-127
p-Isopropyltoluene 0.125 0.136 109 72.0-133
2-Butanone (MEK)0.625 0.668 107 30.0-160
Methylene Chloride 0.125 0.129 103 68.0-123
4-Methyl-2-pentanone (MIBK) 0.625 0.627 100 56.0-143
Methyl tert-butyl ether 0.125 0.150 120 66.0-132
Naphthalene 0.125 0.141 113 59.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159831
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13
Laboratory Control Sample (LCS)
(LCS) R3338241-1 08/30/18 19:48
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
n-Propylbenzene 0.125 0.109 87.5 74.0-126
Styrene 0.125 0.130 104 72.0-127
1,1,1,2-Tetrachloroethane 0.125 0.111 89.0 74.0-129
1,1,2,2-Tetrachloroethane 0.125 0.102 81.6 68.0-128
Tetrachloroethene 0.125 0.118 94.1 70.0-136
Toluene 0.125 0.129 103 75.0-121
1,1,2-Trichlorotrifluoroethane 0.125 0.141 112 61.0-139
1,2,3-Trichlorobenzene 0.125 0.147 118 59.0-139
1,2,4-Trichlorobenzene 0.125 0.122 97.7 62.0-137
1,1,1-Trichloroethane 0.125 0.132 105 69.0-126
1,1,2-Trichloroethane 0.125 0.123 98.1 78.0-123
Trichloroethene 0.125 0.150 120 76.0-126
Trichlorofluoromethane 0.125 0.138 111 61.0-142
1,2,3-Trichloropropane 0.125 0.138 111 67.0-129
1,2,4-Trimethylbenzene 0.125 0.141 113 70.0-126
1,3,5-Trimethylbenzene 0.125 0.114 91.1 73.0-127
Vinyl chloride 0.125 0.129 103 63.0-134
Xylenes, Total 0.375 0.347 92.5 72.0-127
(S) Toluene-d8 107 75.0-131
(S) Dibromofluoromethane 105 65.0-129
(S) 4-Bromofluorobenzene 105 67.0-138
L1021179-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1021179-06 08/31/18 03:51 • (MS) R3338241-3 08/31/18 04:12 • (MSD) R3338241-4 08/31/18 04:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.677 ND 0.296 0.278 43.7 41.0 1 10.0-160 6.33 40
Acrylonitrile 0.677 ND 0.544 0.539 80.3 79.6 1 10.0-160 0.935 40
Benzene 0.135 ND 0.138 0.142 102 105 1 10.0-149 2.87 37
Bromobenzene 0.135 ND 0.141 0.141 104 104 1 10.0-156 0.320 38
Bromodichloromethane 0.135 ND 0.146 0.150 108 111 1 10.0-143 2.84 37
Bromoform 0.135 ND 0.132 0.140 97.7 104 1 10.0-146 5.76 36
Bromomethane 0.135 ND 0.110 0.128 81.4 94.5 1 10.0-149 14.8 38
n-Butylbenzene 0.135 ND 0.140 0.167 104 124 1 10.0-160 17.6 40
sec-Butylbenzene 0.135 ND 0.125 0.145 92.5 107 1 10.0-159 14.5 39
tert-Butylbenzene 0.135 ND 0.123 0.140 91.1 103 1 10.0-156 12.3 39
Carbon tetrachloride 0.135 ND 0.139 0.156 103 115 1 10.0-145 11.1 37
Chlorobenzene 0.135 ND 0.143 0.147 106 108 1 10.0-152 2.34 39
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159831
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13
L1021179-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1021179-06 08/31/18 03:51 • (MS) R3338241-3 08/31/18 04:12 • (MSD) R3338241-4 08/31/18 04:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Chlorodibromomethane 0.135 ND 0.132 0.135 97.2 99.8 1 10.0-146 2.72 37
Chloroethane 0.135 ND 0.116 0.126 85.8 93.0 1 10.0-146 7.98 40
Chloroform 0.135 ND 0.141 0.145 104 107 1 10.0-146 2.57 37
Chloromethane 0.135 ND 0.206 0.174 152 129 1 10.0-159 16.6 37
2-Chlorotoluene 0.135 ND 0.141 0.154 104 113 1 10.0-159 8.38 38
4-Chlorotoluene 0.135 ND 0.115 0.139 84.8 103 1 10.0-155 19.1 39
1,2-Dibromo-3-Chloropropane 0.135 ND 0.0910 0.111 67.2 81.6 1 10.0-151 19.4 39
1,2-Dibromoethane 0.135 ND 0.139 0.141 103 104 1 10.0-148 0.985 34
Dibromomethane 0.135 ND 0.143 0.149 106 110 1 10.0-147 3.70 35
1,2-Dichlorobenzene 0.135 ND 0.128 0.135 94.4 99.3 1 10.0-155 5.09 37
1,3-Dichlorobenzene 0.135 ND 0.126 0.139 93.3 102 1 10.0-153 9.33 38
1,4-Dichlorobenzene 0.135 ND 0.124 0.132 91.3 97.6 1 10.0-151 6.59 38
Dichlorodifluoromethane 0.135 ND 0.200 0.213 148 157 1 10.0-160 6.18 35
1,1-Dichloroethane 0.135 ND 0.142 0.152 105 112 1 10.0-147 6.68 37
1,2-Dichloroethane 0.135 ND 0.139 0.142 103 105 1 10.0-148 2.27 35
1,1-Dichloroethene 0.135 ND 0.153 0.166 113 123 1 10.0-155 8.42 37
cis-1,2-Dichloroethene 0.135 ND 0.108 0.117 80.0 86.5 1 10.0-149 7.75 37
trans-1,2-Dichloroethene 0.135 ND 0.142 0.148 105 109 1 10.0-150 4.25 37
1,2-Dichloropropane 0.135 ND 0.169 0.172 125 127 1 10.0-148 1.70 37
1,1-Dichloropropene 0.135 ND 0.157 0.164 116 121 1 10.0-153 4.75 35
1,3-Dichloropropane 0.135 ND 0.151 0.154 112 114 1 10.0-154 2.13 35
cis-1,3-Dichloropropene 0.135 ND 0.126 0.125 92.9 92.5 1 10.0-151 0.481 37
trans-1,3-Dichloropropene 0.135 ND 0.139 0.141 103 104 1 10.0-148 1.33 37
2,2-Dichloropropane 0.135 ND 0.0829 0.0970 61.2 71.6 1 10.0-138 15.6 36
Di-isopropyl ether 0.135 ND 0.128 0.132 94.2 97.7 1 10.0-147 3.65 36
Ethylbenzene 0.135 ND 0.147 0.149 108 110 1 10.0-160 1.87 38
Hexachloro-1,3-butadiene 0.135 ND 0.129 0.154 95.2 113 1 10.0-160 17.5 40
Isopropylbenzene 0.135 ND 0.125 0.133 92.1 98.1 1 10.0-155 6.37 38
p-Isopropyltoluene 0.135 ND 0.123 0.143 90.9 106 1 10.0-160 15.0 40
2-Butanone (MEK)0.677 ND 0.611 0.684 90.2 101 1 10.0-160 11.3 40
Methylene Chloride 0.135 ND 0.151 0.159 111 117 1 10.0-141 5.41 37
4-Methyl-2-pentanone (MIBK) 0.677 ND 0.544 0.570 80.4 84.2 1 10.0-160 4.69 35
Methyl tert-butyl ether 0.135 ND 0.153 0.148 113 109 1 11.0-147 3.14 35
Naphthalene 0.135 ND 0.100 0.148 71.1 106 1 10.0-160 J3 38.2 36
n-Propylbenzene 0.135 ND 0.124 0.136 91.3 100 1 10.0-158 9.27 38
Styrene 0.135 ND 0.156 0.163 115 120 1 10.0-160 4.52 40
1,1,1,2-Tetrachloroethane 0.135 ND 0.123 0.126 90.6 93.2 1 10.0-149 2.89 39
1,1,2,2-Tetrachloroethane 0.135 ND 0.104 0.106 76.8 78.5 1 10.0-160 2.22 35
Tetrachloroethene 0.135 ND 0.139 0.152 103 112 1 10.0-156 8.60 39
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159831
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13
L1021179-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1021179-06 08/31/18 03:51 • (MS) R3338241-3 08/31/18 04:12 • (MSD) R3338241-4 08/31/18 04:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Toluene 0.135 ND 0.145 0.155 107 114 1 10.0-156 6.43 38
1,1,2-Trichlorotrifluoroethane 0.135 ND 0.152 0.168 112 124 1 10.0-160 10.2 36
1,2,3-Trichlorobenzene 0.135 ND 0.0987 0.160 72.9 118 1 10.0-160 J3 47.4 40
1,2,4-Trichlorobenzene 0.135 ND 0.108 0.147 79.5 109 1 10.0-160 31.1 40
1,1,1-Trichloroethane 0.135 ND 0.137 0.156 101 115 1 10.0-144 13.0 35
1,1,2-Trichloroethane 0.135 ND 0.131 0.138 96.9 102 1 10.0-160 4.72 35
Trichloroethene 0.135 ND 0.171 0.169 126 125 1 10.0-156 0.836 38
Trichlorofluoromethane 0.135 ND 0.103 0.134 76.4 98.8 1 10.0-160 25.5 40
1,2,3-Trichloropropane 0.135 ND 0.140 0.149 103 110 1 10.0-156 6.34 35
1,2,4-Trimethylbenzene 0.135 ND 0.126 0.140 92.8 104 1 10.0-160 10.9 36
1,3,5-Trimethylbenzene 0.135 ND 0.121 0.134 89.2 98.8 1 10.0-160 10.2 38
Vinyl chloride 0.135 ND 0.229 0.249 169 184 1 10.0-160 J5 J5 8.47 37
Xylenes, Total 0.406 ND 0.389 0.413 95.7 102 1 10.0-160 5.95 38
(S) Toluene-d8 104 106 75.0-131
(S) Dibromofluoromethane 98.7 100 65.0-129
(S) 4-Bromofluorobenzene 106 106 67.0-138
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1160083
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-04,06,07,08,09,10,11
Method Blank (MB)
(MB) R3338755-2 08/31/18 20:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Chlorobenzene U 0.000573 0.00250
Chlorodibromomethane U 0.000450 0.00250
1,2-Dibromoethane U 0.000525 0.00250
1,3-Dichloropropane U 0.00175 0.00500
cis-1,3-Dichloropropene U 0.000678 0.00250
trans-1,3-Dichloropropene U 0.00153 0.00500
Ethylbenzene U 0.000530 0.00250
4-Methyl-2-pentanone (MIBK) U 0.0100 0.0250
Naphthalene U 0.00312 0.0125
1,1,1,2-Tetrachloroethane U 0.000500 0.00250
Tetrachloroethene U 0.000700 0.00250
Toluene U 0.00125 0.00500
1,1,2-Trichloroethane U 0.000883 0.00250
1,2,4-Trimethylbenzene U 0.00116 0.00500
Xylenes, Total U 0.00478 0.00650
(S) Toluene-d8 105 75.0-131
(S) Dibromofluoromethane 92.8 65.0-129
(S) 4-Bromofluorobenzene 109 67.0-138
Laboratory Control Sample (LCS)
(LCS) R3338755-1 08/31/18 19:23
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Chlorobenzene 0.125 0.126 101 76.0-128
Chlorodibromomethane 0.125 0.132 106 74.0-127
1,2-Dibromoethane 0.125 0.126 101 74.0-128
1,3-Dichloropropane 0.125 0.135 108 80.0-125
cis-1,3-Dichloropropene 0.125 0.133 106 76.0-127
trans-1,3-Dichloropropene 0.125 0.137 109 73.0-127
Ethylbenzene 0.125 0.127 102 74.0-126
4-Methyl-2-pentanone (MIBK) 0.625 0.706 113 56.0-143
Naphthalene 0.125 0.121 97.1 59.0-130
1,1,1,2-Tetrachloroethane 0.125 0.122 97.8 74.0-129
Tetrachloroethene 0.125 0.126 101 70.0-136
Toluene 0.125 0.123 98.2 75.0-121
1,1,2-Trichloroethane 0.125 0.123 98.8 78.0-123
1,2,4-Trimethylbenzene 0.125 0.125 100 70.0-126
Xylenes, Total 0.375 0.371 98.9 72.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1160083
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-04,06,07,08,09,10,11
Laboratory Control Sample (LCS)
(LCS) R3338755-1 08/31/18 19:23
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) Toluene-d8 106 75.0-131
(S) Dibromofluoromethane 91.5 65.0-129
(S) 4-Bromofluorobenzene 107 67.0-138
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1160333
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-14,15,16
Method Blank (MB)
(MB) R3338648-3 08/31/18 19:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0137 0.0250
Acrylonitrile U 0.00190 0.0125
Benzene U 0.000400 0.00100
Bromobenzene U 0.00105 0.0125
Bromodichloromethane U 0.000788 0.00250
Bromoform U 0.00598 0.0250
Bromomethane U 0.00370 0.0125
n-Butylbenzene U 0.00384 0.0125
sec-Butylbenzene U 0.00253 0.0125
tert-Butylbenzene U 0.00155 0.00500
Carbon tetrachloride U 0.00108 0.00500
Chlorobenzene U 0.000573 0.00250
Chlorodibromomethane U 0.000450 0.00250
Chloroethane U 0.00108 0.00500
Chloroform U 0.000415 0.00250
Chloromethane U 0.00139 0.0125
2-Chlorotoluene U 0.000920 0.00250
4-Chlorotoluene U 0.00113 0.00500
1,2-Dibromo-3-Chloropropane U 0.00510 0.0250
1,2-Dibromoethane U 0.000525 0.00250
Dibromomethane U 0.00100 0.00500
1,2-Dichlorobenzene U 0.00145 0.00500
1,3-Dichlorobenzene U 0.00170 0.00500
1,4-Dichlorobenzene U 0.00197 0.00500
Dichlorodifluoromethane U 0.000818 0.00250
1,1-Dichloroethane U 0.000575 0.00250
1,2-Dichloroethane U 0.000475 0.00250
1,1-Dichloroethene U 0.000500 0.00250
cis-1,2-Dichloroethene U 0.000690 0.00250
trans-1,2-Dichloroethene U 0.00143 0.00500
1,2-Dichloropropane U 0.00127 0.00500
1,1-Dichloropropene U 0.000700 0.00250
1,3-Dichloropropane U 0.00175 0.00500
cis-1,3-Dichloropropene U 0.000678 0.00250
trans-1,3-Dichloropropene U 0.00153 0.00500
2,2-Dichloropropane U 0.000793 0.00250
Di-isopropyl ether U 0.000350 0.00100
Ethylbenzene U 0.000530 0.00250
Hexachloro-1,3-butadiene U 0.0127 0.0250
Isopropylbenzene U 0.000863 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1160333
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-14,15,16
Method Blank (MB)
(MB) R3338648-3 08/31/18 19:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00233 0.00500
2-Butanone (MEK)U 0.0125 0.0250
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK) U 0.0100 0.0250
Methyl tert-butyl ether U 0.000295 0.00100
Naphthalene U 0.00312 0.0125
n-Propylbenzene U 0.00118 0.00500
Styrene U 0.00273 0.0125
1,1,1,2-Tetrachloroethane U 0.000500 0.00250
1,1,2,2-Tetrachloroethane U 0.000390 0.00250
Tetrachloroethene U 0.000700 0.00250
Toluene U 0.00125 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000675 0.00250
1,2,3-Trichlorobenzene U 0.000625 0.00250
1,2,4-Trichlorobenzene U 0.00482 0.0125
1,1,1-Trichloroethane U 0.000275 0.00250
1,1,2-Trichloroethane U 0.000883 0.00250
Trichloroethene U 0.000400 0.00100
Trichlorofluoromethane U 0.000500 0.00250
1,2,3-Trichloropropane U 0.00510 0.0125
1,2,4-Trimethylbenzene U 0.00116 0.00500
1,3,5-Trimethylbenzene U 0.00108 0.00500
Vinyl chloride U 0.000683 0.00250
Xylenes, Total U 0.00478 0.00650
(S) Toluene-d8 105 75.0-131
(S) Dibromofluoromethane 101 65.0-129
(S) 4-Bromofluorobenzene 99.4 67.0-138
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338648-1 08/31/18 18:05 • (LCSD) R3338648-2 08/31/18 18:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.684 0.872 109 139 10.0-160 24.1 31
Acrylonitrile 0.625 0.610 0.659 97.6 105 45.0-153 7.73 22
Benzene 0.125 0.112 0.113 89.6 90.0 70.0-123 0.470 20
Bromobenzene 0.125 0.144 0.160 115 128 73.0-121 J4 10.5 20
Bromodichloromethane 0.125 0.125 0.115 100 92.1 73.0-121 8.19 20
Bromoform 0.125 0.123 0.115 98.2 91.7 64.0-132 6.85 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1160333
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-14,15,16
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338648-1 08/31/18 18:05 • (LCSD) R3338648-2 08/31/18 18:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromomethane 0.125 0.106 0.102 85.1 81.9 56.0-147 3.79 20
n-Butylbenzene 0.125 0.112 0.120 89.5 96.3 68.0-135 7.30 20
sec-Butylbenzene 0.125 0.0972 0.102 77.7 81.4 74.0-130 4.55 20
tert-Butylbenzene 0.125 0.0927 0.103 74.1 82.5 75.0-127 J4 10.6 20
Carbon tetrachloride 0.125 0.117 0.118 93.8 94.5 66.0-128 0.744 20
Chlorobenzene 0.125 0.121 0.115 97.0 91.9 76.0-128 5.42 20
Chlorodibromomethane 0.125 0.112 0.113 90.0 90.2 74.0-127 0.268 20
Chloroethane 0.125 0.110 0.109 87.8 86.9 61.0-134 1.01 20
Chloroform 0.125 0.116 0.120 92.8 95.8 72.0-123 3.10 20
Chloromethane 0.125 0.118 0.110 94.1 87.6 51.0-138 7.11 20
2-Chlorotoluene 0.125 0.137 0.120 109 96.2 75.0-124 12.9 20
4-Chlorotoluene 0.125 0.109 0.0921 87.2 73.7 75.0-124 J4 16.8 20
1,2-Dibromo-3-Chloropropane 0.125 0.114 0.133 91.4 107 59.0-130 15.5 20
1,2-Dibromoethane 0.125 0.124 0.118 98.9 94.0 74.0-128 5.05 20
Dibromomethane 0.125 0.120 0.123 95.7 98.2 75.0-122 2.56 20
1,2-Dichlorobenzene 0.125 0.106 0.110 84.8 88.3 76.0-124 4.05 20
1,3-Dichlorobenzene 0.125 0.101 0.104 80.5 82.9 76.0-125 2.89 20
1,4-Dichlorobenzene 0.125 0.0997 0.102 79.7 81.5 77.0-121 2.12 20
Dichlorodifluoromethane 0.125 0.0986 0.0891 78.9 71.3 43.0-156 10.1 20
1,1-Dichloroethane 0.125 0.122 0.119 97.3 95.3 70.0-127 2.10 20
1,2-Dichloroethane 0.125 0.124 0.121 98.9 96.5 65.0-131 2.43 20
1,1-Dichloroethene 0.125 0.116 0.118 92.9 94.0 65.0-131 1.22 20
cis-1,2-Dichloroethene 0.125 0.0933 0.0967 74.6 77.3 73.0-125 3.58 20
trans-1,2-Dichloroethene 0.125 0.114 0.109 91.5 87.4 71.0-125 4.59 20
1,2-Dichloropropane 0.125 0.124 0.123 99.1 98.5 74.0-125 0.575 20
1,1-Dichloropropene 0.125 0.133 0.127 106 102 73.0-125 4.12 20
1,3-Dichloropropane 0.125 0.129 0.127 103 102 80.0-125 1.48 20
cis-1,3-Dichloropropene 0.125 0.113 0.109 90.2 87.2 76.0-127 3.34 20
trans-1,3-Dichloropropene 0.125 0.125 0.123 100 98.2 73.0-127 2.08 20
2,2-Dichloropropane 0.125 0.121 0.104 96.7 83.4 59.0-135 14.7 20
Di-isopropyl ether 0.125 0.108 0.108 86.0 86.4 60.0-136 0.456 20
Ethylbenzene 0.125 0.123 0.117 98.2 93.2 74.0-126 5.22 20
Hexachloro-1,3-butadiene 0.125 0.0948 0.108 75.9 86.3 57.0-150 12.9 20
Isopropylbenzene 0.125 0.0954 0.0918 76.3 73.5 72.0-127 3.79 20
p-Isopropyltoluene 0.125 0.101 0.106 80.6 84.5 72.0-133 4.69 20
2-Butanone (MEK)0.625 0.635 0.698 102 112 30.0-160 9.41 24
Methylene Chloride 0.125 0.121 0.117 96.6 93.5 68.0-123 3.35 20
4-Methyl-2-pentanone (MIBK) 0.625 0.621 0.629 99.4 101 56.0-143 1.27 20
Methyl tert-butyl ether 0.125 0.140 0.143 112 114 66.0-132 1.79 20
Naphthalene 0.125 0.114 0.143 90.9 114 59.0-130 J3 22.9 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1160333
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-14,15,16
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338648-1 08/31/18 18:05 • (LCSD) R3338648-2 08/31/18 18:25
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
n-Propylbenzene 0.125 0.0954 0.0952 76.3 76.2 74.0-126 0.249 20
Styrene 0.125 0.124 0.120 99.1 95.7 72.0-127 3.50 20
1,1,1,2-Tetrachloroethane 0.125 0.113 0.106 90.3 85.2 74.0-129 5.89 20
1,1,2,2-Tetrachloroethane 0.125 0.106 0.102 84.4 81.4 68.0-128 3.68 20
Tetrachloroethene 0.125 0.111 0.109 89.1 87.6 70.0-136 1.75 20
Toluene 0.125 0.120 0.116 96.3 92.5 75.0-121 4.12 20
1,1,2-Trichlorotrifluoroethane 0.125 0.129 0.124 103 99.5 61.0-139 3.71 20
1,2,3-Trichlorobenzene 0.125 0.102 0.142 81.4 114 59.0-139 J3 33.3 20
1,2,4-Trichlorobenzene 0.125 0.0864 0.118 69.1 94.8 62.0-137 J3 31.3 20
1,1,1-Trichloroethane 0.125 0.122 0.119 97.3 95.1 69.0-126 2.34 20
1,1,2-Trichloroethane 0.125 0.109 0.107 86.8 85.5 78.0-123 1.50 20
Trichloroethene 0.125 0.134 0.134 107 107 76.0-126 0.0836 20
Trichlorofluoromethane 0.125 0.126 0.121 101 96.7 61.0-142 4.51 20
1,2,3-Trichloropropane 0.125 0.132 0.135 106 108 67.0-129 1.73 20
1,2,4-Trimethylbenzene 0.125 0.100 0.100 80.2 80.3 70.0-126 0.146 20
1,3,5-Trimethylbenzene 0.125 0.0949 0.101 75.9 80.6 73.0-127 6.04 20
Vinyl chloride 0.125 0.116 0.112 93.1 89.7 63.0-134 3.73 20
Xylenes, Total 0.375 0.328 0.330 87.5 88.0 72.0-127 0.608 20
(S) Toluene-d8 105 104 75.0-131
(S) Dibromofluoromethane 101 104 65.0-129
(S) 4-Bromofluorobenzene 100 99.1 67.0-138
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1160867
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-15,16
Method Blank (MB)
(MB) R3338826-3 09/03/18 08:42
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Tetrachloroethene U 0.000700 0.00250
(S) Toluene-d8 110 75.0-131
(S) Dibromofluoromethane 98.4 65.0-129
(S) 4-Bromofluorobenzene 103 67.0-138
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338826-1 09/03/18 06:30 • (LCSD) R3338826-2 09/03/18 06:49
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Tetrachloroethene 0.125 0.116 0.110 93.0 87.7 70.0-136 5.88 20
(S) Toluene-d8 105 102 75.0-131
(S) Dibromofluoromethane 102 106 65.0-129
(S) 4-Bromofluorobenzene 104 103 67.0-138
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1161063
Volatile Organic Compounds (GC/MS) by Method 8260B L1020964-05,06,07
Method Blank (MB)
(MB) R3338933-3 09/04/18 04:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Naphthalene U 0.00312 0.0125
1,2,4-Trimethylbenzene U 0.00116 0.00500
(S) Toluene-d8 104 75.0-131
(S) Dibromofluoromethane 93.1 65.0-129
(S) 4-Bromofluorobenzene 102 67.0-138
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338933-1 09/04/18 03:07 • (LCSD) R3338933-2 09/04/18 03:26
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.135 0.136 108 109 59.0-130 0.650 20
1,2,4-Trimethylbenzene 0.125 0.131 0.115 105 92.0 70.0-126 12.9 20
(S) Toluene-d8 107 102 75.0-131
(S) Dibromofluoromethane 88.9 96.0 65.0-129
(S) 4-Bromofluorobenzene 101 100 67.0-138
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159178
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1020964-17,18
Method Blank (MB)
(MB) R3338534-3 09/01/18 09:34
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroethyl)ether U 1.62 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
Benzo(g,h,i)perylene U 0.161 1.00
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 1.19 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
Diethyl phthalate U 0.282 3.00
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate U 0.278 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159178
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1020964-17,18
Method Blank (MB)
(MB) R3338534-3 09/01/18 09:34
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
4-Chloro-3-methylphenol U 0.263 10.0
2-Chlorophenol U 0.283 10.0
2,4-Dichlorophenol U 0.284 10.0
2,4-Dimethylphenol U 0.264 10.0
4,6-Dinitro-2-methylphenol U 2.62 10.0
2,4-Dinitrophenol U 3.25 10.0
2-Nitrophenol U 0.320 10.0
4-Nitrophenol U 2.01 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 0.334 10.0
2,4,6-Trichlorophenol U 0.297 10.0
(S) 2-Fluorophenol 33.0 10.0-120
(S) Phenol-d5 20.3 10.0-120
(S) Nitrobenzene-d5 55.9 10.0-127
(S) 2-Fluorobiphenyl 63.5 10.0-130
(S) 2,4,6-Tribromophenol 49.6 10.0-155
(S) p-Terphenyl-d14 69.1 10.0-128
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338534-1 09/01/18 08:45 • (LCSD) R3338534-2 09/01/18 09:10
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Anthracene 50.0 30.4 32.0 60.8 64.0 45.0-120 5.13 20
Benzidine 50.0 10.1 9.89 20.2 19.8 1.00-120 2.10 36
Benzo(a)anthracene 50.0 34.7 35.4 69.4 70.8 47.0-120 2.00 20
Benzo(b)fluoranthene 50.0 33.0 33.1 66.0 66.2 46.0-120 0.303 20
Benzo(k)fluoranthene 50.0 34.1 35.0 68.2 70.0 46.0-120 2.60 21
Benzo(a)pyrene 50.0 32.8 32.9 65.6 65.8 47.0-120 0.304 20
Bis(2-chlorethoxy)methane 50.0 26.8 25.7 53.6 51.4 33.0-120 4.19 24
Bis(2-chloroethyl)ether 50.0 26.9 24.2 53.8 48.4 23.0-120 10.6 33
Bis(2-chloroisopropyl)ether 50.0 29.0 27.2 58.0 54.4 28.0-120 6.41 31
4-Bromophenyl-phenylether 50.0 34.7 36.9 69.4 73.8 45.0-120 6.15 20
2-Chloronaphthalene 50.0 32.1 31.5 64.2 63.0 37.0-120 1.89 25
4-Chlorophenyl-phenylether 50.0 33.9 35.1 67.8 70.2 44.0-120 3.48 20
Chrysene 50.0 33.7 34.7 67.4 69.4 48.0-120 2.92 20
Dibenz(a,h)anthracene 50.0 32.7 33.5 65.4 67.0 47.0-120 2.42 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159178
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1020964-17,18
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338534-1 09/01/18 08:45 • (LCSD) R3338534-2 09/01/18 09:10
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 32.9 33.6 65.8 67.2 41.0-120 2.11 22
3,3-Dichlorobenzidine 50.0 34.9 36.3 69.8 72.6 44.0-120 3.93 20
Acenaphthylene 50.0 32.3 32.0 64.6 64.0 43.0-120 0.933 22
2,4-Dinitrotoluene 50.0 36.3 36.5 72.6 73.0 49.0-124 0.549 20
2,6-Dinitrotoluene 50.0 32.3 33.3 64.6 66.6 46.0-120 3.05 21
Fluoranthene 50.0 35.3 36.5 70.6 73.0 51.0-120 3.34 20
Fluorene 50.0 33.3 34.7 66.6 69.4 47.0-120 4.12 20
Hexachlorobenzene 50.0 37.5 39.3 75.0 78.6 44.0-120 4.69 20
Hexachloro-1,3-butadiene 50.0 31.2 29.4 62.4 58.8 19.0-120 5.94 32
Hexachlorocyclopentadiene 50.0 29.7 27.9 59.4 55.8 15.0-120 6.25 31
Hexachloroethane 50.0 27.1 24.8 54.2 49.6 15.0-120 8.86 37
Indeno(1,2,3-cd)pyrene 50.0 34.7 35.3 69.4 70.6 49.0-122 1.71 20
Isophorone 50.0 28.5 28.2 57.0 56.4 36.0-120 1.06 23
Benzo(g,h,i)perylene 50.0 34.7 34.9 69.4 69.8 48.0-121 0.575 20
Naphthalene 50.0 29.3 27.3 58.6 54.6 27.0-120 7.07 27
Nitrobenzene 50.0 28.0 26.0 56.0 52.0 27.0-120 7.41 29
n-Nitrosodimethylamine 50.0 16.2 12.5 32.4 25.0 10.0-120 25.8 40
n-Nitrosodiphenylamine 50.0 33.2 34.6 66.4 69.2 47.0-120 4.13 20
n-Nitrosodi-n-propylamine 50.0 27.7 26.4 55.4 52.8 31.0-120 4.81 28
Phenanthrene 50.0 31.6 33.4 63.2 66.8 46.0-120 5.54 20
Benzylbutyl phthalate 50.0 27.5 25.7 55.0 51.4 43.0-121 6.77 20
Bis(2-ethylhexyl)phthalate 50.0 31.0 32.2 62.0 64.4 43.0-122 3.80 20
Di-n-butyl phthalate 50.0 32.2 32.6 64.4 65.2 49.0-121 1.23 20
Diethyl phthalate 50.0 28.8 29.6 57.6 59.2 48.0-122 2.74 20
Dimethyl phthalate 50.0 22.4 21.3 44.8 42.6 48.0-120 J4 J4 5.03 20
Di-n-octyl phthalate 50.0 33.0 33.5 66.0 67.0 42.0-125 1.50 20
Pyrene 50.0 34.4 35.9 68.8 71.8 47.0-120 4.27 20
1,2,4-Trichlorobenzene 50.0 29.8 27.6 59.6 55.2 24.0-120 7.67 29
4-Chloro-3-methylphenol 50.0 27.4 24.1 54.8 48.2 40.0-120 12.8 21
2-Chlorophenol 50.0 21.0 12.0 42.0 24.0 25.0-120 J3 J4 54.5 35
2,4-Dichlorophenol 50.0 25.6 17.9 51.2 35.8 36.0-120 J3 J4 35.4 26
2,4-Dimethylphenol 50.0 24.1 19.3 48.2 38.6 33.0-120 22.1 26
4,6-Dinitro-2-methylphenol 50.0 32.0 24.2 64.0 48.4 38.0-138 J3 27.8 25
2,4-Dinitrophenol 50.0 21.9 16.6 43.8 33.2 10.0-120 27.5 39
2-Nitrophenol 50.0 26.0 18.5 52.0 37.0 31.0-120 J3 33.7 29
4-Nitrophenol 50.0 15.0 14.4 30.0 28.8 10.0-120 4.08 33
Pentachlorophenol 50.0 35.0 25.3 70.0 50.6 23.0-120 J3 32.2 25
Phenol 50.0 11.3 9.04 22.6 18.1 10.0-120 22.2 36
2,4,6-Trichlorophenol 50.0 30.4 25.2 60.8 50.4 42.0-120 18.7 23
(S) 2-Fluorophenol 31.4 21.8 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159178
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1020964-17,18
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338534-1 09/01/18 08:45 • (LCSD) R3338534-2 09/01/18 09:10
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
(S) Phenol-d5 20.8 16.3 10.0-120
(S) Nitrobenzene-d5 53.4 47.4 10.0-127
(S) 2-Fluorobiphenyl 61.0 60.9 10.0-130
(S) 2,4,6-Tribromophenol 66.0 58.0 10.0-155
(S) p-Terphenyl-d14 66.1 68.0 10.0-128
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159283
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16
Method Blank (MB)
(MB) R3338839-3 09/03/18 03:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0330
Acenaphthylene U 0.00671 0.0330
Anthracene U 0.00632 0.0330
Benzidine U 0.0637 0.333
Benzo(a)anthracene 0.00476 J 0.00428 0.0330
Benzo(b)fluoranthene U 0.00695 0.0330
Benzo(k)fluoranthene U 0.00582 0.0330
Benzo(g,h,i)perylene U 0.00721 0.0330
Benzo(a)pyrene U 0.00548 0.0330
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0330
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0330
Dibenz(a,h)anthracene U 0.00821 0.0330
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0330
Fluorene U 0.00682 0.0330
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0330
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0330
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.0900 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0330
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159283
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16
Method Blank (MB)
(MB) R3338839-3 09/03/18 03:25
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.0123 0.0330
1,2,4-Trichlorobenzene U 0.00876 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 60.7 10.0-122
(S) 2-Fluorobiphenyl 70.0 15.0-120
(S) p-Terphenyl-d14 66.7 10.0-120
(S) Phenol-d5 64.9 10.0-120
(S) 2-Fluorophenol 72.8 12.0-120
(S) 2,4,6-Tribromophenol 82.3 10.0-127
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338839-1 09/03/18 02:38 • (LCSD) R3338839-2 09/03/18 03:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.666 0.475 0.519 71.3 77.9 38.0-120 8.85 22
Acenaphthylene 0.666 0.460 0.511 69.1 76.7 40.0-120 10.5 22
Anthracene 0.666 0.443 0.494 66.5 74.2 42.0-120 10.9 20
Benzidine 0.666 ND ND 0.000 0.000 1.00-120 J4 J4 0.000 40
Benzo(a)anthracene 0.666 0.494 0.531 74.2 79.7 44.0-120 7.22 20
Benzo(b)fluoranthene 0.666 0.486 0.542 73.0 81.4 43.0-120 10.9 22
Benzo(k)fluoranthene 0.666 0.524 0.556 78.7 83.5 44.0-120 5.93 21
Benzo(g,h,i)perylene 0.666 0.536 0.578 80.5 86.8 43.0-120 7.54 22
Benzo(a)pyrene 0.666 0.506 0.549 76.0 82.4 45.0-120 8.15 20
Bis(2-chlorethoxy)methane 0.666 0.320 0.339 48.0 50.9 20.0-120 5.77 23
Bis(2-chloroethyl)ether 0.666 0.416 0.429 62.5 64.4 16.0-120 3.08 31
Bis(2-chloroisopropyl)ether 0.666 0.390 0.422 58.6 63.4 23.0-120 7.88 30
4-Bromophenyl-phenylether 0.666 0.507 0.559 76.1 83.9 40.0-120 9.76 21
2-Chloronaphthalene 0.666 0.465 0.508 69.8 76.3 35.0-120 8.84 24
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159283
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338839-1 09/03/18 02:38 • (LCSD) R3338839-2 09/03/18 03:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
4-Chlorophenyl-phenylether 0.666 0.503 0.549 75.5 82.4 40.0-120 8.75 22
Chrysene 0.666 0.503 0.544 75.5 81.7 43.0-120 7.83 20
Dibenz(a,h)anthracene 0.666 0.515 0.548 77.3 82.3 44.0-120 6.21 22
3,3-Dichlorobenzidine 0.666 0.423 0.488 63.5 73.3 28.0-120 14.3 23
2,4-Dinitrotoluene 0.666 0.525 0.568 78.8 85.3 45.0-120 7.87 21
2,6-Dinitrotoluene 0.666 0.483 0.532 72.5 79.9 42.0-120 9.66 21
Fluoranthene 0.666 0.511 0.570 76.7 85.6 44.0-120 10.9 21
Fluorene 0.666 0.491 0.531 73.7 79.7 41.0-120 7.83 22
Hexachlorobenzene 0.666 0.530 0.575 79.6 86.3 39.0-120 8.14 21
Hexachloro-1,3-butadiene 0.666 0.418 0.441 62.8 66.2 15.0-120 5.36 28
Hexachlorocyclopentadiene 0.666 0.421 0.448 63.2 67.3 15.0-120 6.21 31
Hexachloroethane 0.666 0.374 0.403 56.2 60.5 17.0-120 7.46 31
Indeno(1,2,3-cd)pyrene 0.666 0.523 0.570 78.5 85.6 45.0-120 8.60 21
Isophorone 0.666 0.344 0.357 51.7 53.6 23.0-120 3.71 23
Naphthalene 0.666 0.381 0.401 57.2 60.2 18.0-120 5.12 24
Nitrobenzene 0.666 0.356 0.368 53.5 55.3 17.0-120 3.31 26
n-Nitrosodimethylamine 0.666 0.373 0.380 56.0 57.1 10.0-125 1.86 33
n-Nitrosodiphenylamine 0.666 0.466 0.511 70.0 76.7 40.0-120 9.21 21
n-Nitrosodi-n-propylamine 0.666 0.379 0.404 56.9 60.7 26.0-120 6.39 27
Phenanthrene 0.666 0.470 0.519 70.6 77.9 42.0-120 9.91 20
Benzylbutyl phthalate 0.666 0.466 0.510 70.0 76.6 40.0-120 9.02 21
Bis(2-ethylhexyl)phthalate 0.666 0.462 0.512 69.4 76.9 41.0-120 10.3 21
Di-n-butyl phthalate 0.666 0.471 0.520 70.7 78.1 43.0-120 9.89 20
Diethyl phthalate 0.666 0.473 0.504 71.0 75.7 43.0-120 6.35 21
Dimethyl phthalate 0.666 0.475 0.527 71.3 79.1 43.0-120 10.4 22
Di-n-octyl phthalate 0.666 0.495 0.546 74.3 82.0 40.0-120 9.80 21
Pyrene 0.666 0.486 0.531 73.0 79.7 41.0-120 8.85 21
1,2,4-Trichlorobenzene 0.666 0.413 0.433 62.0 65.0 17.0-120 4.73 26
4-Chloro-3-methylphenol 0.666 0.389 0.419 58.4 62.9 28.0-120 7.43 20
2-Chlorophenol 0.666 0.459 0.494 68.9 74.2 28.0-120 7.35 28
2,4-Dichlorophenol 0.666 0.459 0.477 68.9 71.6 25.0-120 3.85 21
2,4-Dimethylphenol 0.666 0.370 0.393 55.6 59.0 15.0-120 6.03 26
4,6-Dinitro-2-methylphenol 0.666 0.485 0.512 72.8 76.9 16.0-120 5.42 33
2,4-Dinitrophenol 0.666 0.352 0.371 52.9 55.7 10.0-120 5.26 40
2-Nitrophenol 0.666 0.444 0.479 66.7 71.9 20.0-120 7.58 25
4-Nitrophenol 0.666 0.526 0.560 79.0 84.1 27.0-120 6.26 24
Pentachlorophenol 0.666 0.616 0.687 92.5 103 29.0-120 10.9 25
Phenol 0.666 0.430 0.466 64.6 70.0 28.0-120 8.04 27
2,4,6-Trichlorophenol 0.666 0.525 0.568 78.8 85.3 37.0-120 7.87 24
(S) Nitrobenzene-d5 54.4 56.5 10.0-122
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159283
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3338839-1 09/03/18 02:38 • (LCSD) R3338839-2 09/03/18 03:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
(S) 2-Fluorobiphenyl 73.9 77.2 15.0-120
(S) p-Terphenyl-d14 62.2 80.8 10.0-120
(S) Phenol-d5 66.5 71.3 10.0-120
(S) 2-Fluorophenol 78.2 79.4 12.0-120
(S) 2,4,6-Tribromophenol 90.8 95.0 10.0-127
L1020964-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1020964-11 09/03/18 08:17 • (MS) R3338839-4 09/03/18 08:40 • (MSD) R3338839-5 09/03/18 09:04
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.825 U 0.677 0.640 82.1 77.6 5 18.0-120 5.64 32
Acenaphthylene 0.825 U 0.656 0.628 79.6 76.1 5 25.0-120 4.44 32
Anthracene 0.825 0.0572 0.672 0.644 74.6 71.1 5 22.0-120 4.33 29
Benzidine 0.825 U ND ND 0.000 0.000 5 1.00-120 J6 J6 0.000 40
Benzo(a)anthracene 0.825 0.194 0.936 0.986 89.9 95.9 5 25.0-120 5.15 29
Benzo(b)fluoranthene 0.825 0.258 1.05 1.15 95.8 108 5 19.0-122 9.35 31
Benzo(k)fluoranthene 0.825 0.0825 0.855 0.915 93.6 101 5 23.0-120 6.86 30
Benzo(g,h,i)perylene 0.825 0.0911 0.559 0.464 56.7 45.3 5 10.0-120 18.4 33
Benzo(a)pyrene 0.825 0.182 0.936 1.01 91.4 100 5 24.0-120 7.39 30
Bis(2-chlorethoxy)methane 0.825 U 0.467 0.425 56.6 51.5 5 10.0-120 9.44 34
Bis(2-chloroethyl)ether 0.825 U 0.479 0.482 58.1 58.4 5 10.0-120 0.515 40
Bis(2-chloroisopropyl)ether 0.825 U 0.481 0.482 58.3 58.4 5 10.0-120 0.257 40
4-Bromophenyl-phenylether 0.825 U 0.698 0.637 84.7 77.2 5 27.0-120 9.28 30
2-Chloronaphthalene 0.825 U 0.637 0.585 77.2 70.9 5 20.0-120 8.52 32
4-Chlorophenyl-phenylether 0.825 U 0.703 0.654 85.3 79.3 5 24.0-120 7.30 29
Chrysene 0.825 0.182 0.941 0.991 92.0 98.0 5 21.0-120 5.13 29
Dibenz(a,h)anthracene 0.825 U 0.557 0.463 67.6 56.2 5 10.0-120 18.4 32
3,3-Dichlorobenzidine 0.825 U ND 0.521 0.000 63.2 5 10.0-120 J6 J3 200 34
2,4-Dinitrotoluene 0.825 U 0.625 0.562 75.8 68.2 5 30.0-120 10.6 31
2,6-Dinitrotoluene 0.825 U 0.597 0.545 72.4 66.1 5 25.0-120 9.11 31
Fluoranthene 0.825 0.326 1.20 1.33 106 121 5 18.0-126 9.60 32
Fluorene 0.825 U 0.718 0.695 87.1 84.2 5 25.0-120 3.33 30
Hexachlorobenzene 0.825 U 0.753 0.666 91.3 80.8 5 27.0-120 12.2 28
Hexachloro-1,3-butadiene 0.825 U 0.654 0.593 79.3 71.9 5 10.0-120 9.73 38
Hexachlorocyclopentadiene 0.825 U ND ND 0.000 0.000 5 10.0-120 J6 J6 0.000 40
Hexachloroethane 0.825 U 0.425 0.406 51.5 49.2 5 10.0-120 4.47 40
Indeno(1,2,3-cd)pyrene 0.825 0.572 0.613 0.554 4.95 0.000 5 10.0-120 J6 J6 10.2 32
Isophorone 0.825 U 0.495 0.447 60.1 54.2 5 13.0-120 10.2 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1159283
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L1020964-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16
L1020964-11 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1020964-11 09/03/18 08:17 • (MS) R3338839-4 09/03/18 08:40 • (MSD) R3338839-5 09/03/18 09:04
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.825 U 0.619 0.585 75.1 70.9 5 10.0-120 5.76 35
Nitrobenzene 0.825 U 0.497 0.462 60.2 56.0 5 10.0-120 7.24 36
n-Nitrosodimethylamine 0.825 U ND ND 0.000 0.000 5 10.0-127 J6 J6 0.000 40
n-Nitrosodiphenylamine 0.825 U 0.659 0.603 79.9 73.1 5 17.0-120 8.83 29
n-Nitrosodi-n-propylamine 0.825 U 0.477 0.457 57.8 55.4 5 10.0-120 4.24 37
Phenanthrene 0.825 0.144 0.842 0.867 84.7 87.7 5 17.0-120 2.90 31
Benzylbutyl phthalate 0.825 U 0.622 0.577 75.4 70.0 5 23.0-120 7.44 30
Bis(2-ethylhexyl)phthalate 0.825 U 0.645 0.588 78.2 71.3 5 17.0-126 9.24 30
Di-n-butyl phthalate 0.825 U 0.643 0.591 77.9 71.6 5 30.0-120 8.43 29
Diethyl phthalate 0.825 U 0.633 0.587 76.7 71.2 5 26.0-120 7.51 28
Dimethyl phthalate 0.825 U 0.628 0.575 76.1 69.7 5 25.0-120 8.86 29
Di-n-octyl phthalate 0.825 U 0.650 0.592 78.8 71.8 5 21.0-123 9.37 29
Pyrene 0.825 0.312 1.11 1.30 97.1 120 5 16.0-121 15.5 32
1,2,4-Trichlorobenzene 0.825 U 0.639 0.581 77.5 70.4 5 12.0-120 9.54 37
4-Chloro-3-methylphenol 0.825 U 0.596 0.559 72.2 67.7 5 15.0-120 6.44 30
2-Chlorophenol 0.825 U 0.589 0.571 71.5 69.2 5 15.0-120 3.20 37
2,4-Dichlorophenol 0.825 U 0.708 0.603 85.9 73.1 5 20.0-120 16.1 31
2,4-Dimethylphenol 0.825 U 0.555 0.474 67.3 57.5 5 10.0-120 15.6 33
4,6-Dinitro-2-methylphenol 0.825 U ND ND 0.000 0.000 5 10.0-120 J6 J6 0.000 39
2,4-Dinitrophenol 0.825 U ND ND 0.000 0.000 5 10.0-121 J6 J6 0.000 40
2-Nitrophenol 0.825 U 0.624 0.536 75.7 65.0 5 12.0-120 15.2 39
4-Nitrophenol 0.825 U 0.619 0.534 75.1 64.7 5 10.0-137 14.8 32
Pentachlorophenol 0.825 U 0.627 0.440 76.0 53.3 5 10.0-160 J3 35.1 31
Phenol 0.825 U 0.536 0.525 65.0 63.7 5 12.0-120 2.10 38
2,4,6-Trichlorophenol 0.825 U 0.720 0.617 87.2 74.8 5 19.0-120 15.4 32
(S) Nitrobenzene-d5 58.6 55.6 10.0-122
(S) 2-Fluorobiphenyl 79.6 73.0 15.0-120
(S) p-Terphenyl-d14 69.7 73.3 10.0-120
(S) Phenol-d5 67.0 64.6 10.0-120
(S) 2-Fluorophenol 76.6 71.8 12.0-120
(S) 2,4,6-Tribromophenol 89.0 74.2 10.0-127
Sample Narrative:
OS: Dilution due to matrix
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 100 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 100 of 105
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T 104704245-17-14
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 17:24 101 of 105
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02170761 L1020964 09/11/18 22:29 101 of 105

APPENDIX B

Boring Logs

Boring #Job Name
Date Site Loc.
WR Rep Driller
NC NAD83 Easting:
From To
0.0 16.0
16.0 20.0
Sample
Depth PID
0-5 0.6 Sample
5-10 0.3
10-15 0.3
15-20 0 Sample
Note:
TOC - Top of Casing
BLS - Below land surface
SWP-1
M. James Quantex
NC NAD83 Northing:See Table 1
Stormwater Pipe Corridor Investigation
SOIL BORING LOG
August 24, 2018 Raleigh, NC
02170761.00Job #
Soil Description
(Field USCS Classification)
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington
Page 1 of 1
See Table 1
Depth in Feet
Clayey Silt (ML); Brown/Red, Moist, some coarse Sand, Low Elasticity, No Odor, Resembles Fill
Silty Clay (CH); Black, Wet, Organics; No Odor
Boring #Job Name
Date Site Loc.
WR Rep Driller
NC NAD83 Easting:
From To
0.0 16.0
16.0 20.0
Sample
Depth PID Sample
0-5 0.7
5-10 0.5
10-15 2.2
15-20 259 Sample
Note:
TOC - Top of Casing
BLS - Below land surface
Clayey Silt (ML); Brown/Red, Moist, some coarse Sand, Low Elasticity, No Odor, Resembles Fill
Sand (SW); Medium, Black, Wet, Organics; Petroleum Odor
Page 1 of 1
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington
See Table 1 NC NAD83 Northing:See Table 1
Depth in Feet Soil Description
(Field USCS Classification)
August 24, 2018 Raleigh, NC
M. James Quantex
SOIL BORING LOG
SWP-2 Stormwater Pipe Corridor Investigation Job #02170761.00
Boring #Job Name
Date Site Loc.
WR Rep Driller
NC NAD83 Easting:
From To
0.0 11.0
11.0 15.0
Sample
Depth PID
0-5 2.1 Sample
5-10 1.3
10-15 2.1 Sample
Note:
TOC - Top of Casing
BLS - Below land surface
Clayey Silt (ML); Brown/Red, Moist, some coarse Sand, Low Elasticity, No Odor, Resembles Fill
Clayey Sand (SC), Tan, Grades to SW with depth, Dry, Native Material, Boring Refusal @15'
Page 1 of 1
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington
See Table 1 NC NAD83 Northing:See Table 1
Depth in Feet Soil Description
(Field USCS Classification)
August 24, 2018 Raleigh, NC
M. James Quantex
SOIL BORING LOG
SWP-3 Stormwater Pipe Corridor Investigation Job #02170761.00
Boring #Job Name
Date Site Loc.
WR Rep Driller
NC NAD83 Easting:
From To
0.0 10.0
10.0 15.0
Sample
Depth PID
0-5 2.7 Sample
5-10 3.4
10-15 40.6 Sample
Note:
TOC - Top of Casing
BLS - Below land surface
Clayey Silt (ML); Brown/Red, Moist, some coarse Sand, Low Elasticity, No Odor, Resembles Fill, Wood
and Brick Debris Observed in Recovered Material
Coarse Sand (SW), Black, Wet, No Odor, Brick Debris
Page 1 of 1
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington
1" Temporary Well Installed to a total depth of 15 ft. Groundwater encountered 9.85 feet below ground
surface
See Table 1 NC NAD83 Northing:See Table 1
Depth in Feet Soil Description
(Field USCS Classification)
August 24, 2018 Raleigh, NC
M. James Quantex
SOIL BORING LOG
SWP-4 / TWSWP-4 Stormwater Pipe Corridor Investigation Job #02170761.00
Boring #Job Name
Date Site Loc.
WR Rep Driller
NC NAD83 Easting:
From To
0.0 12.0
12.0 15.0
Sample
Depth PID
0-5 3.2 Sample
5-10 2.7
12-15 3.6 Sample
Note:
TOC - Top of Casing
BLS - Below land surface
Clayey Silt (ML); Brown/Red, Moist, some coarse Sand, Low Elasticity, No Odor, Resembles Fill, Wood,
Asphalt, Brick Debris Observed in Recovered Material
Coarse Sand (SW), Tan, Dry, No Odor, Native Material
Page 1 of 1
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington
See Table 1 NC NAD83 Northing:See Table 1
Depth in Feet Soil Description
(Field USCS Classification)
August 24, 2018 Raleigh, NC
M. James Quantex
SOIL BORING LOG
SWP-5 Stormwater Pipe Corridor Investigation Job #02170761.00
Boring #Job Name
Date Site Loc.
WR Rep Driller
NC NAD83 Easting:
From To
0.0 10.0
10.0 15.0
Sample
Depth PID
0-5 1.1 Sample
5-10 No Recovery
12-15 11.5 Sample
Note:
TOC - Top of Casing
BLS - Below land surface
Clayey Silt (ML); Brown/Red, Moist, some coarse Sand, Low Elasticity, No Odor, Resembles Fill, Wood,
Asphalt, Brick Debris Observed in Recovered Material
Coarse Sand (SW), Tan, Dry, No Odor, Native Material
Page 1 of 1
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington
See Table 1 NC NAD83 Northing:See Table 1
Depth in Feet Soil Description
(Field USCS Classification)
August 24, 2018 Raleigh, NC
M. James Quantex
SOIL BORING LOG
SWP-6 Stormwater Pipe Corridor Investigation Job #02170761.00
Boring #Job Name
Date Site Loc.
WR Rep Driller
NC NAD83 Easting:
From To
0.0 14.0
14.0 15.0
Sample
Depth PID
0-5 2.4 Sample
5-10 20.7
14-Dec 1.2 Sample
Note:
TOC - Top of Casing
BLS - Below land surface
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington
Clayey Silt (ML); Brown/Red, Moist, some coarse Sand, Low Elasticity, No Odor, Resembles Fill, Wood
and Brick Debris Observed in Recovered Material
Coarse Sand (SW), Tan, Wet, No Odor, Native Material
1" Temporary Well Installed to a total depth of 15 ft. Groundwater encountered 8.60 feet below ground
surface
Page 1 of 1
See Table 1 NC NAD83 Northing:See Table 1
Depth in Feet Soil Description
(Field USCS Classification)
August 24, 2018 Raleigh, NC
M. James Quantex
SOIL BORING LOG
SWP-7 / TWSWP-7 Stormwater Pipe Corridor Investigation Job #02170761.00
Boring #Job Name
Date Site Loc.
WR Rep Driller
NC NAD83 Easting:
From To
0.0 12.0
12.0 15.0
Sample
Depth PID
0-5 0.5 Sample
5-10 1.2
12-15 26 Sample
Note:
TOC - Top of Casing
BLS - Below land surface
Clayey Silt (ML); Brown/Red, Moist, some coarse Sand, Low Elasticity, No Odor, Resembles Fill, Wood,
Asphalt, Brick Debris Observed in Recovered Material
Coarse Sand (SW), Black, Wet, No Odor, Native Material
Page 1 of 1
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington
See Table 1 NC NAD83 Northing:See Table 1
Depth in Feet Soil Description
(Field USCS Classification)
August 24, 2018 Raleigh, NC
M. James Quantex
SOIL BORING LOG
SWP-8 Stormwater Pipe Corridor Investigation Job #02170761.00

APPENDIX C

USGS Paper 1648
Arsenic and Chromium Background Concentrations

Geochemical Landscapes of the
Conterminous United States—
New Map Presentations for 22 Elements
U.S. Department of the Interior
U.S. Geological Survey
U.S. Geological Survey Professional Paper 1648
2.78
2.54
2.32
2.12
1.94
1.77
1.62
1.48
1.35
1.23
1.13
1.03
0.94
0.86
0.79
0.72
0.66
0.60
0.55
Percent
0 1,000 KILOMETERS
POTASSIUM
12 PPMCHROMIUM0 1,000 KILOMETERS Geochemical Landscapes of the Conterminous United States—New Map Presentations for 22 Elements Figure 7. Colored surface map of Cr distribution in soils and other surficial materials of the conterminous United States.
ARSENICPPM0 1,000 KILOMETERS Results and Interpretation Figure 4. Colored surface map of As distribution in soils and other surficial materials of the conterminous United States. 9