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Home My WebLink About21059_601-617 West South Street_Fill Soil Sampling Report_2018.01.29 WithersRavenel Our People. Your Success. 115 MacKenan Drive | Cary, NC 27511 t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832 Cary | Greensboro | Pittsboro | Raleigh | Wilmington January 29, 2018 State of North Carolina Department of Environment Quality Division of Waste Management - Brownfields Section Mail Service Center 1646 Raleigh, NC 27699-1646 Attn: Mr. Brad Atkinson Reference: Fill Soil Sampling Report 601 – 617 West South Street Raleigh, Wake County, North Carolina WR Project Number: 02170761.00 Dear Mr. Atkinson: WithersRavenel, Inc. (WR) has prepared this Fill Soil Sampling Letter Report to document sampling activities that took place on January 11, 2018. Background Between December 2016 and September 2017, approximately 15,000 to 20,000 cubic yards of soil were removed from the parcels identified as 601 through 617 West South Street. Soils removed from the parcel identified at 601 West South Street were impacted with petroleum constitutes associated with a UST system removed in the 1980s. Soils removed from the remaining parcels were deemed unsuitable for construction by a geotechnical engineering firm due to the presence of fill and rubble material. Following removal of the petroleum impacted and unsuitable soils, the grading contractor replaced the removed soils with fill soil sourced from two offsite locations: • Approximately 1,000 cubic yards of soil was obtained from the North Carolina Department of Transportation (NCDOT) from road-bed soils removed during the reconstruction of I-40 in Wake County; and • The remainder of the fill soils was obtained from expansion activities at the Buffaloe Landfill where previously undisturbed areas were being excavated. Fill Soil Sampling Procedures WR mobilized to the subject property on January 11, 2018 to advance soil borings at various locations within the subject properties using a direct-push Geoprobe drilling machine. Soils were collected with 60-inch long, new macrocore liners and decontaminated tooling. Borings at the former gas station property (601 West South Street) were advanced a minimum of 10-feet below ground surface where native / undisturbed soils were encountered. The borings on the parcels WithersRavenel Our People. Your Success. 601 – 617 West South Street WR Project # 02170761.00 Fill Soil Sampling Report January 2018 Page 2 of 4 identified as 607 through 617 West South Street were advanced to a depth of 5-feet below ground surface. Soil samples from the former gas station area (601 West South Street) were collected from the following three intervals: • Surficial Buffaloe Landfill fill from the depths less than 3-feet foot below ground surface; • Intermediate depth sample from fill soil obtained from the DOT; and • Native soils collected from, saturated, undisturbed soils. Soil samples from 607 through 617 South West Street, which were all in Buffaloe Landfill material, were collected at depths ranging from 0.5 to 4-feet below ground surface. Collected soil samples were immediately placed in laboratory supplied bottleware following the opening of the macrocore liner by the onsite geologist. Collected soil samples were then placed in a cooler containing ice and shipped under property chain of custody procedures to ESC Lab Sciences, in Mt. Juliet, TN (ESC) for analysis by the following methods: • Volatile Organic Compounds (VOCS) by EPA Method 8260B, Semi-VOCs (SVOCs)by EPA Method 8270D, and RCRA-8 Metals by 6010D / 7471B. WR also collected three soil samples from sidewall cuts of relic fill remaining on the subject properties. The samples were collected by removing approximately 3 to 6-inchs of the surficial soils to expose soil for sample collection. Relic fill samples were submitted to ESC for analysis by the following methods: • VOCS by EPA Method 8260B, SVOCs by EPA Method 8270D, and RCRA-8 Metals by 6010D / 7471B. Following sample collection, the remaining soils in the liner were cataloged and placed in zip-lock baggies for field screening with a field calibrated Foxboro TVA-2020, with a flame-ionization and photo-ionization detector (FID/PID). These readings are shown on the boring logs contained in the Appendix. Sampling locations were recorded with a sub-meter GPS device. Sampling locations are illustrated on Figure 1 and latitude / longitude coordinates are provided on Table 1. WithersRavenel Our People. Your Success. 601 – 617 West South Street WR Project # 02170761.00 Fill Soil Sampling Report January 2018 Page 3 of 4 Laboratory Analytical Results 607 – 617 South West Street Buffaloe Landfill Fill Samples - BF1 through BF8: The laboratory analytical results are summarized in Tables 2, 3, and 4 and the laboratory analytical report is included in the Appendix. Detectable concentrations of VOCs or SVOCs were not identified in any of the soil samples submitted for analysis. Therefore, there are no exceedances of the October 2017 NCDEQ Inactive Hazardous Sites Branch (IHSB) Health Based Preliminary Soil Remediation Goals (PSRGs) for unrestricted site use. Barium, chromium (total), lead, and mercury were detected at concentrations above the laboratory method detection limit (MDL) but below the IHSB Health Based PSRG for unrestricted site use in 8 samples collected from the Buffaloe Landfill fill. Former Gas Station Area Fill – BF6, BF12, and BF13: The laboratory analytical results are summarized in Tables 2, 3, and 4 and the laboratory analytical report is included in the Appendix. Several petroleum-related VOCs and a trace concentration of a solvent related VOC were identified in the soil samples from the former gas station area fill. However, none of the reported concentrations exceeded the NCDEQ IHSB Health Based PSRG for unrestricted site use. The petroleum-related compound Naphthalene was not detected in any of the samples analyzed for VOCs by EPA Method 8260B. However, Naphthalene can also be identified in analyses for SVOCs by EPA Method 8270D and detectable concentrations of the compound were identified in three of the samples from the former gas station area. The reported concentrations of Naphthalene in two of the three samples were below the NCDEQ IHSB Health Based PSRG for unrestricted use. However, the reported concentration of Naphthalene in the 0.5 to 1.5 foot depth sample from boring B6 (4.49 mg/Kg) exceeded the PSRG of 3.8 mg/Kg. Boring B6 was located adjacent to monitoring well MW-1. No other SVOCs were identified in the soil samples form the former gas station area. Several RCRA-8 Metals were detected at concentrations above their respective MDLs. However, the reported concentrations were all below the IHSB Health Based PSRGs for unrestricted site use in the 9 samples collected from the former gas station area. Relic Fill - RF-1, RF-2, and RF-3: The laboratory analytical results are summarized in Tables 2, 3, and 4 and the laboratory analytical report is included in the Appendix. Trace concentrations of one petroleum-related VOC and one solvent-related VOC were identified in relic fill sample RF-3. However, neither of the detected concentrations exceeded the NCDEQ FIGURES SOUTH WEST STREETSOUTH SAUNDERS STREETBF12 BF16MW-1BF6BF13BF15BF14RF2BF4BF1BF2BF3BF5BF6BF7RF1RF3BF8APPROXIMATE LOCATIONOF 550-GALLON USTMJMJDRAWN BY:01/24/1802170761.001SCALE:FIGURE NO.:PROJECT NO.:DATE:APPROVED BY:601-617 SOUTH WEST STREET601-617 SOUTH WEST STREETRALEIGH, WAKE COUNTY, NCFILL SOIL SAMPLING MAPWithersRavenelEngineers | Planners | Surveyors115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: C-0832 | www.withersravenel.com1"=60 'GRAPHIC SCALE1 inch = 60 ft.06030120LEGENDFILL SOIL SAMPLE LOCATION RFRELIC FILL SAMPLES BFFILL SOIL SAMPLESINTERMITTENT STREAMNOTES: 1.) 2017 AERIAL OBTAINED FROM THE LOCAL COUNTY GIS DEPARTMENT. TABLES TABLE 1 - GPS LOCATIONS FILL SOIL SAMPLING DATA 601-617 WEST SOUTH STREET RALEIGH, NC 27603 WR JOB NO. 02170761.00 Sample ID Latitude Longitude BF1 35.77226898 -78.64935701 BF2 35.77226557 -78.64923902 BF3 35.7722621 -78.64909531 BF4 35.77225846 -78.64865535 BF5 35.77202566 -78.64937262 BF6 35.77202963 -78.64924408 BF7 35.77203578 -78.64909353 BF8 35.77205645 -78.64867295 BF12 35.77214817 -78.64838581 BF13 35.77214271 -78.64821952 BF14 35.77229938 -78.64834366 BF15 35.77225108 -78.64817238 BF16 35.77222298 -78.64836156 BF6 35.77224002 -78.6482756 RF1 35.77234815 -78.64843636 RF2 35.77236484 -78.64910853 RF3 35.77196203 -78.64906567 MW-1 35.77224411 -78.64825723 Note: 1) GPS data collected with sub-meter GPS unit. Page 1 of 1 TABLE 2 - RCRA 8 METALS601-617 WEST SOUTH STREETRALEIGH, NC 27603 WR JOB NO. 02170761.00 Method Analyte CAS NCDEQ IHSB Unrestricted Use Health Based PSRG (October 2017) Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier 6010D ARSENIC 7440-38-2 0.68 <0.867 <0.754 <0.764 <0.798 <0.945 <0.817 <0.812 <0.824 6010D BARIUM 7440-39-3 3000 75.5 97.6 99.4 72.2 41.7 46.6 39.6 164 6010D CADMIUM 7440-43-9 14.2 <0.0934 <0.0812 <0.0823 <0.0859 <0.102 <0.088 <0.0875 <0.0887 6010D CHROMIUM (TOTAL)7440-47-3 NL 143 14.5 28.3 22.9 210 96.4 34.6 17.1 6010D LEAD 7439-92-1 400 3.67 8.57 11.6 12 7.52 7.27 7.05 6.97 6010D SELENIUM 7782-49-2 78 <0.987 <0.859 <0.87 <0.908 <1.08 <0.93 <0.925 <0.938 6010D SILVER 7440-22-4 78 <0.373 <0.325 <0.329 <0.344 <0.407 <0.352 <0.35 <0.355 7471B MERCURY 7439-97-6 2.2 0.036 B 0.0398 B 0.0454 B 0.0353 B 0.106 0.0915 0.0631 0.0364 B Qualifiers: Notes: 1) All results provided in ug/L (micrograms per liter) or parts per billion. 2) IHSB - Inactive Hazardous Sites Branch.3) PSRG - Preliminary Soil Remediation Goals. NL = Not Listed Result = Result Exceeds MDL. Result = Result Exceeds Unrestricted Use Health Based PSRG. J7: Surrogate recovery cannot be used for control limit evaluation due to dilution RCRA 8 Metals J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low. B: The same analyte is found in the associated blank. J0: Calibration verification outside of acceptance limits. Result is estimated. J3: The associated batch QC was outside the established quality control range for precision. J4: The associated batch QC was outside the established quality control range for accuracy. mg/kg Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 01/11/2018 01/11/2018 Date Collected 01/11/2018 01/11/2018 01/11/2018 01/11/2018 01/11/2018 01/11/2018 BF6 1-3 BF7 2-4 BF8 2-4 Sample Locations Buffaloe Landfill Fill Samples Client Sample ID BF1 0.5-1.5 BF2 2-4 BF3 2-4 BF4 2-4 BF5 2-4 Page 1 of 3 TABLE 2 - RCRA 8 METALS601-617 WEST SOUTH STREETRALEIGH, NC 27603 WR JOB NO. 02170761.00 Method Analyte CAS NCDEQ IHSB Unrestricted Use Health Based PSRG (October 2017) 6010D ARSENIC 7440-38-2 0.68 6010D BARIUM 7440-39-3 3000 6010D CADMIUM 7440-43-9 14.2 6010D CHROMIUM (TOTAL)7440-47-3 NL 6010D LEAD 7439-92-1 400 6010D SELENIUM 7782-49-2 78 6010D SILVER 7440-22-4 78 7471B MERCURY 7439-97-6 2.2 Qualifiers: Notes: 1) All results provided in ug/L (micrograms per liter) or parts per billion. 2) IHSB - Inactive Hazardous Sites Branch.3) PSRG - Preliminary Soil Remediation Goals. NL = Not Listed Result = Result Exceeds MDL. Result = Result Exceeds Unrestricted Use Health Based PSRG. J7: Surrogate recovery cannot be used for control limit evaluation due to dilution RCRA 8 Metals J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low. B: The same analyte is found in the associated blank. J0: Calibration verification outside of acceptance limits. Result is estimated. J3: The associated batch QC was outside the established quality control range for precision. J4: The associated batch QC was outside the established quality control range for accuracy. Units Date Collected Sample Locations Client Sample ID Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier <0.754 <0.863 <0.746 <0.726 <0.715 <0.75 <0.823 <0.767 <1.03 103 44.1 26.7 27.7 36.6 32.1 107 68.8 182 <0.0812 <0.0929 <0.0803 <0.0782 <0.077 <0.0808 <0.0886 <0.0826 <0.111 25.1 25.1 1.57 15.9 17.7 3.51 27.3 36.2 22.2 5.15 6.81 1.49 2.65 5.51 11 4.21 5.85 2.83 <0.859 <0.982 <0.849 <0.827 <0.814 <0.854 <0.937 <0.874 <1.18 <0.325 <0.372 <0.321 <0.313 <0.308 <0.323 <0.354 <0.331 <0.445 <0.00325 <0.00372 <0.00321 0.101 <0.00308 <0.00323 <0.00354 <0.00331 <0.00445 mg/kg mg/kg mg/kg mg/kgmg/kg mg/kg mg/kg mg/kg mg/kg 01/11/2018 01/11/2018 01/11/2018 01/11/2018 01/11/201801/11/2018 01/11/2018 01/11/2018 01/11/2018 BF12 2-3 BF12 4-6 BF12 9-11 BF13 1-3 BF13 4-5 BF13 8-10BF6 0.5-1.5 (Adjacent to MW-1) BF6 4-5 (Adjacent to MW-1) BF6 14-15 (Adjacent to MW-1) 601 West South Street - Former Gas Station - Buffaloe Landfill and DOT Fill Area Samples Page 2 of 3 TABLE 2 - RCRA 8 METALS601-617 WEST SOUTH STREETRALEIGH, NC 27603 WR JOB NO. 02170761.00 Method Analyte CAS NCDEQ IHSB Unrestricted Use Health Based PSRG (October 2017) 6010D ARSENIC 7440-38-2 0.68 6010D BARIUM 7440-39-3 3000 6010D CADMIUM 7440-43-9 14.2 6010D CHROMIUM (TOTAL)7440-47-3 NL 6010D LEAD 7439-92-1 400 6010D SELENIUM 7782-49-2 78 6010D SILVER 7440-22-4 78 7471B MERCURY 7439-97-6 2.2 Qualifiers: Notes: 1) All results provided in ug/L (micrograms per liter) or parts per billion. 2) IHSB - Inactive Hazardous Sites Branch.3) PSRG - Preliminary Soil Remediation Goals. NL = Not Listed Result = Result Exceeds MDL. Result = Result Exceeds Unrestricted Use Health Based PSRG. J7: Surrogate recovery cannot be used for control limit evaluation due to dilution RCRA 8 Metals J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low. B: The same analyte is found in the associated blank. J0: Calibration verification outside of acceptance limits. Result is estimated. J3: The associated batch QC was outside the established quality control range for precision. J4: The associated batch QC was outside the established quality control range for accuracy. Units Date Collected Sample Locations Client Sample ID Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier <0.785 <0.778 3.41 91.3 51 104 <0.0846 <0.0838 <0.0805 13.6 18.8 36.1 228 8.64 91.5 <0.894 <0.886 <0.851 <0.338 <0.335 <0.322 0.417 0.07 0.138 mg/kgmg/kg mg/kg 01/11/2018 01/11/201801/11/2018 RF-1 RF-2 RF-3 Relic Fill Sidewall Samples Page 3 of 3 TABLE 3 - VOLATILE ORGANIC COMPOUNDS 601-617 WEST SOUTH STREET RALEIGH, NC 27603 WR JOB NO. 02170761.00 Method Analyte CAS NCDEQ IHSB Unrestricted Use Health Based PSRG (October 2017) Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier 8260B ACETONE 67-64-1 12200 <0.0133 <0.0116 <0.0118 <0.0123 <0.0145 <0.0126 <0.0125 <0.01278260BACRYLONITRILE107-13-1 0.25 <0.00239 <0.00208 <0.0021 <0.0022 <0.0026 <0.00225 <0.00224 <0.002278260BBENZENE71-43-2 1.2 <0.00036 <0.000313 <0.000317 <0.000331 <0.000393 <0.000339 <0.000337 <0.0003428260BBROMOBENZENE108-86-1 58 <0.000379 <0.00033 <0.000334 <0.000348 <0.000413 <0.000357 <0.000355 <0.00036 8260B BROMODICHLOROMETHANE 75-27-4 0.29 <0.000339 <0.000295 <0.000299 <0.000312 <0.000369 <0.000319 <0.000317 <0.000322 8260B BROMOFORM 75-25-2 19 <0.000566 <0.000492 <0.000499 <0.00052 <0.000617 <0.000533 <0.00053 <0.000537 8260B BROMOMETHANE 74-83-9 1.36 <0.00179 <0.00156 <0.00158 <0.00164 <0.00195 <0.00168 <0.00167 <0.0017 8260B N-BUTYLBENZENE 104-51-8 108 <0.000344 <0.000299 <0.000303 <0.000317 <0.000375 <0.000324 <0.000322 <0.000327 8260B SEC-BUTYLBENZENE 135-98-8 145 <0.000268 <0.000233 <0.000236 <0.000247 <0.000292 <0.000253 <0.000251 <0.000255 8260B TERT-BUTYLBENZENE 98-06-6 183 <0.000275 <0.000239 <0.000242 <0.000253 <0.0003 <0.000259 <0.000257 <0.000261 8260B CARBON TETRACHLORIDE 56-23-5 0.65 <0.000438 <0.000381 <0.000386 <0.000402 <0.000477 <0.000412 <0.00041 <0.000416 8260B CHLOROBENZENE 108-90-7 56 <0.000283 <0.000246 <0.000249 <0.00026 <0.000308 <0.000266 <0.000265 <0.000269 8260B CHLORODIBROMOMETHANE 124-48-1 8.3 <0.000498 <0.000433 <0.000439 <0.000458 <0.000542 <0.000469 <0.000466 <0.000473 8260B CHLOROETHANE 75-00-3 2120 <0.00126 <0.0011 <0.00111 <0.00116 <0.00138 <0.00119 <0.00118 <0.0012 8260B CHLOROFORM 67-66-3 0.32 <0.000305 <0.000266 <0.000269 <0.000281 <0.000333 <0.000288 <0.000286 <0.00029 8260B CHLOROMETHANE 74-87-3 22 <0.0005 <0.000435 <0.000441 <0.00046 <0.000545 <0.000471 <0.000469 <0.000475 8260B 2-CHLOROTOLUENE 95-49-8 320 <0.000402 <0.000349 <0.000354 <0.000369 <0.000438 <0.000378 <0.000376 <0.000381 8260B 4-CHLOROTOLUENE 106-43-4 253 <0.00032 <0.000279 <0.000282 <0.000294 <0.000349 <0.000302 <0.0003 <0.000304 8260B 1,2-DIBROMO-3-CHLOROPROPANE 96-12-8 0.0053 <0.0014 <0.00122 <0.00123 <0.00129 <0.00153 <0.00132 <0.00131 <0.00133 8260B 1,2-DIBROMOETHANE 106-93-4 0.036 <0.000458 <0.000398 <0.000403 <0.000421 <0.000499 <0.000431 <0.000429 <0.000435 8260B DIBROMOMETHANE 74-95-3 4.8 <0.00051 <0.000443 <0.000449 <0.000469 <0.000555 <0.00048 <0.000477 <0.000484 8260B 1,2-DICHLOROBENZENE 95-50-1 360 <0.000407 <0.000354 <0.000359 <0.000374 <0.000444 <0.000383 <0.000381 <0.000387 8260B 1,3-DICHLOROBENZENE 541-73-1 NL <0.000319 <0.000277 <0.000281 <0.000293 <0.000348 <0.0003 <0.000299 <0.0003038260B1,4-DICHLOROBENZENE 106-46-7 2.6 <0.000301 <0.000262 <0.000266 <0.000277 <0.000329 <0.000284 <0.000282 <0.0002868260BDICHLORODIFLUOROMETHANE75-71-8 17.4 <0.000951 <0.000827 <0.000838 <0.000875 <0.00104 <0.000896 <0.000891 <0.0009048260B1,1-DICHLOROETHANE 75-34-3 3.6 <0.000265 <0.000231 <0.000234 <0.000244 <0.000289 <0.00025 <0.000249 <0.0002528260B1,2-DICHLOROETHANE 107-06-2 0.46 <0.000353 <0.000308 <0.000312 <0.000325 <0.000385 <0.000333 <0.000331 <0.0003368260B1,1-DICHLOROETHENE 75-35-4 46 <0.000404 <0.000352 <0.000356 <0.000372 <0.000441 <0.000381 <0.000379 <0.0003848260BCIS-1,2-DICHLOROETHENE 156-59-2 32 <0.000313 <0.000273 <0.000276 <0.000288 <0.000342 <0.000295 <0.000294 <0.0002988260BTRANS-1,2-DICHLOROETHENE 156-60-5 320 <0.000352 <0.000306 <0.00031 <0.000324 <0.000384 <0.000332 <0.00033 <0.0003358260B1,2-DICHLOROPROPANE 78-87-5 1 <0.000478 <0.000415 <0.000421 <0.000439 <0.000521 <0.00045 <0.000447 <0.0004548260B1,1-DICHLOROPROPENE 563-58-6 NL <0.000423 <0.000368 <0.000373 <0.000389 <0.000461 <0.000398 <0.000396 <0.0004028260B1,3-DICHLOROPROPANE 142-28-9 320 <0.000276 <0.00024 <0.000243 <0.000254 <0.000301 <0.00026 <0.000259 <0.000262 8260B CIS-1,3-DICHLOROPROPENE 10061-01-5 NL <0.000349 <0.000304 <0.000308 <0.000321 <0.000381 <0.000329 <0.000327 <0.000332 8260B TRANS-1,3-DICHLOROPROPENE 10061-02-6 NL <0.000356 <0.00031 <0.000314 <0.000328 <0.000388 <0.000336 <0.000334 <0.000338 8260B 2,2-DICHLOROPROPANE 594-20-7 NL <0.000372 <0.000324 <0.000328 <0.000342 <0.000406 <0.000351 <0.000349 <0.000354 8260B DI-ISOPROPYL ETHER 108-20-3 440 <0.000331 <0.000288 <0.000292 <0.000304 <0.000361 <0.000312 <0.00031 <0.000314 8260B ETHYLBENZENE 100-41-4 5.8 <0.000396 <0.000345 <0.000349 <0.000364 <0.000432 <0.000373 <0.000371 <0.000376 8260B HEXACHLORO-1,3-BUTADIENE 87-68-3 1.2 <0.000456 <0.000397 <0.000402 <0.00042 <0.000497 <0.00043 <0.000427 <0.000433 8260B ISOPROPYLBENZENE 98-82-8 268 <0.000324 <0.000282 <0.000286 <0.000298 <0.000353 <0.000305 <0.000304 <0.000308 8260B P-ISOPROPYLTOLUENE 99-87-6 NL <0.000272 <0.000237 <0.00024 <0.00025 <0.000297 <0.000256 <0.000255 <0.000259 8260B 2-BUTANONE (MEK)78-93-3 5400 <0.00624 <0.00543 <0.0055 <0.00574 <0.00681 <0.00588 <0.00585 <0.00593 8260B METHYLENE CHLORIDE 75-09-2 57 <0.00133 <0.00116 <0.00118 <0.00123 <0.00145 <0.00126 <0.00125 <0.00127 8260B 4-METHYL-2-PENTANONE (MIBK)108-10-1 3360 <0.00251 <0.00218 <0.00221 <0.00231 <0.00273 <0.00236 <0.00235 <0.00238 8260B METHYL TERT-BUTYL ETHER 1634-04-4 47 <0.000283 <0.000246 <0.000249 <0.00026 <0.000308 <0.000266 <0.000265 <0.000269 8260B NAPHTHALENE 91-20-3 3.8 <0.00133 <0.00116 <0.00118 <0.00123 <0.00145 <0.00126 <0.00125 <0.00127 8260B N-PROPYLBENZENE 103-65-1 264 <0.000275 <0.000239 <0.000242 <0.000253 <0.0003 <0.000259 <0.000257 <0.000261 8260B STYRENE 100-42-5 867 <0.000312 <0.000272 <0.000275 <0.000287 <0.00034 <0.000294 <0.000292 <0.000297 8260B 1,1,1,2-TETRACHLOROETHANE 630-20-6 2 <0.000352 <0.000306 <0.00031 <0.000324 <0.000384 <0.000332 <0.00033 <0.000335 8260B 1,1,2,2-TETRACHLOROETHANE 79-34-5 0.6 <0.000487 <0.000424 <0.000429 <0.000448 <0.000531 <0.000459 <0.000456 <0.000463 8260B TETRACHLOROETHENE 127-18-4 16.2 <0.000368 <0.00032 <0.000325 <0.000339 <0.000401 <0.000347 <0.000345 <0.00035 8260B TOLUENE 108-88-3 818 <0.000579 <0.000504 <0.00051 <0.000533 <0.000631 <0.000546 <0.000542 <0.00055 8260B 1,2,3-TRICHLOROBENZENE 87-61-6 12.6 <0.000408 <0.000355 <0.00036 <0.000375 <0.000445 <0.000385 <0.000382 <0.0003888260B1,2,4-TRICHLOROBENZENE 120-82-1 11.6 <0.000518 <0.00045 <0.000456 <0.000476 <0.000564 <0.000488 <0.000485 <0.0004928260B1,1,1-TRICHLOROETHANE 71-55-6 640 <0.000382 <0.000332 <0.000336 <0.000351 <0.000416 <0.00036 <0.000357 <0.0003628260B1,1,2-TRICHLOROETHANE 79-00-5 0.3 <0.000369 <0.000321 <0.000326 <0.00034 <0.000403 <0.000348 <0.000346 <0.0003518260B1,1,2-TRICHLOROTRIFLUOROETHANE 76-13-1 910 <0.000487 <0.000424 <0.000429 <0.000448 <0.000531 <0.000459 <0.000456 <0.0004638260BTRICHLOROETHENE79-01-6 0.82 <0.000372 <0.000324 <0.000328 <0.000342 <0.000406 <0.000351 <0.000349 <0.0003548260BTRICHLOROFLUOROMETHANE75-69-4 1230 <0.00051 J3 J4 <0.000443 J3 J4 <0.000449 J3 J4 <0.000469 J3 J4 <0.000555 J3 J4 <0.00048 J3 J4 <0.000477 J3 J4 <0.0004848260B1,2,3-TRICHLOROPROPANE 96-18-4 0.0051 <0.000988 <0.00086 <0.000871 <0.000909 <0.00108 <0.000931 <0.000926 <0.0009398260B1,2,4-TRIMETHYLBENZENE 95-63-6 11.6 <0.000281 <0.000245 <0.000248 <0.000259 <0.000307 <0.000265 <0.000264 <0.0002678260B1,3,5-TRIMETHYLBENZENE 108-67-8 156 <0.000355 <0.000309 <0.000313 <0.000326 <0.000387 <0.000334 <0.000332 <0.0003378260BVINYL CHLORIDE 75-01-4 0.059 <0.000388 <0.000338 <0.000342 <0.000357 <0.000423 <0.000366 <0.000364 <0.000369 8260B XYLENES, TOTAL 1330-20-7 116 <0.000931 <0.00081 <0.000821 <0.000856 <0.00101 <0.000877 <0.000872 <0.000885 Qualifiers: Notes: 1) All results provided in ug/L (micrograms per liter) or parts per billion.2) IHSB - Inactive Hazardous Sites Branch.3) PSRG - Preliminary Soil Remediation Goals. NL = Not Listed Result = Result Exceeds MDL.Result = Result Exceeds Unrestricted Use Health Based PSRG. J3: The associated batch QC was outside the established quality control range for precision. J4: The associated batch QC was outside the established quality control range for accuracy. J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low.J7: Surrogate recovery cannot be used for control limit evaluation due to dilution Volatile Organic Compounds B: The same analyte is found in the associated blank.J0: Calibration verification outside of acceptance limits. Result is estimated. mg/kg Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 01/11/2018 01/11/2018 Date Collected 01/11/2018 01/11/2018 01/11/2018 01/11/2018 01/11/2018 01/11/2018BF6 1-3 BF7 2-4 BF8 2-4 Sample Locations Buffaloe Landfill Fill Samples Client Sample ID BF1 0.5-1.5 BF2 2-4 BF3 2-4 BF4 2-4 BF5 2-4 Page 1 of 3 TABLE 3 - VOLATILE ORGANIC COMPOUNDS 601-617 WEST SOUTH STREET RALEIGH, NC 27603 WR JOB NO. 02170761.00 Method Analyte CAS NCDEQ IHSB Unrestricted Use Health Based PSRG (October 2017) 8260B ACETONE 67-64-1 122008260BACRYLONITRILE107-13-1 0.258260BBENZENE71-43-2 1.28260BBROMOBENZENE108-86-1 58 8260B BROMODICHLOROMETHANE 75-27-4 0.29 8260B BROMOFORM 75-25-2 19 8260B BROMOMETHANE 74-83-9 1.36 8260B N-BUTYLBENZENE 104-51-8 108 8260B SEC-BUTYLBENZENE 135-98-8 145 8260B TERT-BUTYLBENZENE 98-06-6 183 8260B CARBON TETRACHLORIDE 56-23-5 0.65 8260B CHLOROBENZENE 108-90-7 56 8260B CHLORODIBROMOMETHANE 124-48-1 8.3 8260B CHLOROETHANE 75-00-3 2120 8260B CHLOROFORM 67-66-3 0.32 8260B CHLOROMETHANE 74-87-3 22 8260B 2-CHLOROTOLUENE 95-49-8 320 8260B 4-CHLOROTOLUENE 106-43-4 253 8260B 1,2-DIBROMO-3-CHLOROPROPANE 96-12-8 0.0053 8260B 1,2-DIBROMOETHANE 106-93-4 0.036 8260B DIBROMOMETHANE 74-95-3 4.8 8260B 1,2-DICHLOROBENZENE 95-50-1 360 8260B 1,3-DICHLOROBENZENE 541-73-1 NL8260B1,4-DICHLOROBENZENE 106-46-7 2.68260BDICHLORODIFLUOROMETHANE75-71-8 17.48260B1,1-DICHLOROETHANE 75-34-3 3.68260B1,2-DICHLOROETHANE 107-06-2 0.468260B1,1-DICHLOROETHENE 75-35-4 468260BCIS-1,2-DICHLOROETHENE 156-59-2 328260BTRANS-1,2-DICHLOROETHENE 156-60-5 3208260B1,2-DICHLOROPROPANE 78-87-5 18260B1,1-DICHLOROPROPENE 563-58-6 NL8260B1,3-DICHLOROPROPANE 142-28-9 320 8260B CIS-1,3-DICHLOROPROPENE 10061-01-5 NL 8260B TRANS-1,3-DICHLOROPROPENE 10061-02-6 NL 8260B 2,2-DICHLOROPROPANE 594-20-7 NL 8260B DI-ISOPROPYL ETHER 108-20-3 440 8260B ETHYLBENZENE 100-41-4 5.8 8260B HEXACHLORO-1,3-BUTADIENE 87-68-3 1.2 8260B ISOPROPYLBENZENE 98-82-8 268 8260B P-ISOPROPYLTOLUENE 99-87-6 NL 8260B 2-BUTANONE (MEK)78-93-3 5400 8260B METHYLENE CHLORIDE 75-09-2 57 8260B 4-METHYL-2-PENTANONE (MIBK)108-10-1 3360 8260B METHYL TERT-BUTYL ETHER 1634-04-4 47 8260B NAPHTHALENE 91-20-3 3.8 8260B N-PROPYLBENZENE 103-65-1 264 8260B STYRENE 100-42-5 867 8260B 1,1,1,2-TETRACHLOROETHANE 630-20-6 2 8260B 1,1,2,2-TETRACHLOROETHANE 79-34-5 0.6 8260B TETRACHLOROETHENE 127-18-4 16.2 8260B TOLUENE 108-88-3 818 8260B 1,2,3-TRICHLOROBENZENE 87-61-6 12.68260B1,2,4-TRICHLOROBENZENE 120-82-1 11.68260B1,1,1-TRICHLOROETHANE 71-55-6 6408260B1,1,2-TRICHLOROETHANE 79-00-5 0.38260B1,1,2-TRICHLOROTRIFLUOROETHANE 76-13-1 9108260BTRICHLOROETHENE79-01-6 0.828260BTRICHLOROFLUOROMETHANE75-69-4 12308260B1,2,3-TRICHLOROPROPANE 96-18-4 0.00518260B1,2,4-TRIMETHYLBENZENE 95-63-6 11.68260B1,3,5-TRIMETHYLBENZENE 108-67-8 1568260BVINYL CHLORIDE 75-01-4 0.059 8260B XYLENES, TOTAL 1330-20-7 116 Qualifiers: Notes: 1) All results provided in ug/L (micrograms per liter) or parts per billion.2) IHSB - Inactive Hazardous Sites Branch.3) PSRG - Preliminary Soil Remediation Goals. NL = Not Listed Result = Result Exceeds MDL.Result = Result Exceeds Unrestricted Use Health Based PSRG. J3: The associated batch QC was outside the established quality control range for precision. J4: The associated batch QC was outside the established quality control range for accuracy. J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low.J7: Surrogate recovery cannot be used for control limit evaluation due to dilution Volatile Organic Compounds B: The same analyte is found in the associated blank.J0: Calibration verification outside of acceptance limits. Result is estimated. Units Date Collected Sample Locations Client Sample ID Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier <0.0116 <2.65 <0.0115 <0.0112 <0.011 <0.0115 <0.0127 <1.18 <0.397<0.00208 <0.475 <0.00205 <0.002 <0.00197 <0.00207 <0.00227 <0.211 <0.0712<0.000313 <0.0717 0.0807 <0.000302 <0.000297 0.00695 <0.000342 <0.0319 0.339<0.00033 <0.0754 <0.000326 <0.000317 <0.000313 <0.000328 <0.00036 <0.0335 <0.0113 <0.000295 <0.0674 <0.000292 <0.000284 <0.00028 <0.000293 <0.000322 <0.03 <0.0101 <0.000492 <0.113 <0.000487 <0.000474 <0.000467 <0.000489 <0.000537 <0.0501 <0.0168 <0.00156 <0.356 <0.00154 <0.0015 <0.00147 <0.00155 <0.0017 <0.158 <0.0532 <0.000299 <0.0685 <0.000296 <0.000288 <0.000284 <0.000298 <0.000327 0.67 <0.0102 <0.000233 <0.0534 <0.000231 <0.000225 <0.000221 <0.000232 <0.000254 0.235 <0.00798 <0.000239 <0.0547 <0.000236 <0.00023 <0.000227 <0.000238 <0.000261 <0.0243 <0.00818 <0.000381 <0.0871 <0.000376 <0.000367 <0.000361 <0.000379 <0.000415 <0.0387 <0.013 <0.000246 <0.0563 <0.000243 <0.000237 <0.000233 <0.000245 <0.000268 <0.025 <0.00842 <0.000433 <0.099 <0.000428 <0.000417 <0.000411 <0.000431 <0.000472 <0.044 <0.0148 <0.0011 <0.251 <0.00109 <0.00106 <0.00104 <0.00109 <0.0012 <0.112 <0.0375 <0.000266 <0.0608 <0.000263 <0.000256 <0.000252 <0.000264 <0.00029 <0.027 <0.00909 <0.000435 <0.0995 <0.00043 <0.000419 <0.000413 <0.000433 <0.000475 <0.0443 <0.0149 <0.000349 <0.0799 <0.000345 <0.000336 <0.000331 <0.000347 <0.000381 <0.0355 <0.0119 <0.000279 <0.0637 <0.000275 <0.000268 <0.000264 <0.000277 <0.000304 <0.0283 <0.00953 <0.00122 <0.279 <0.00121 <0.00117 <0.00116 <0.00121 <0.00133 <0.124 <0.0416 <0.000398 <0.091 <0.000394 <0.000383 <0.000378 <0.000396 <0.000434 <0.0405 <0.0136 <0.000443 <0.101 <0.000438 <0.000427 <0.00042 <0.000441 <0.000484 <0.0451 <0.0152 <0.000354 <0.081 <0.00035 <0.000341 <0.000336 <0.000352 <0.000386 <0.036 <0.0121 <0.000277 <0.0634 <0.000274 <0.000267 <0.000263 <0.000276 <0.000303 <0.0282 <0.0095<0.000262 <0.06 <0.000259 <0.000253 <0.000249 <0.000261 <0.000286 <0.0267 <0.00898<0.000828 <0.19 <0.000818 <0.000797 <0.000785 <0.000823 <0.000903 <0.0842 <0.0283<0.000231 <0.0528 <0.000228 <0.000222 <0.000219 <0.00023 <0.000252 <0.0235 <0.00791<0.000308 <0.0703 <0.000304 <0.000296 <0.000292 <0.000306 <0.000335 <0.0313 <0.0105<0.000352 <0.0804 <0.000348 <0.000339 <0.000333 <0.00035 <0.000384 <0.0358 <0.012<0.000273 <0.0624 <0.00027 <0.000263 <0.000259 0.00396 <0.000297 <0.0277 <0.00934<0.000306 <0.0701 <0.000303 <0.000295 <0.000291 <0.000305 <0.000334 <0.0312 <0.0105<0.000416 <0.095 <0.000411 <0.0004 <0.000394 <0.000413 <0.000453 <0.0423 <0.0142<0.000368 <0.0841 <0.000364 <0.000354 <0.000349 <0.000366 <0.000401 <0.0374 <0.0126<0.00024 <0.0549 <0.000238 <0.000231 <0.000228 <0.000239 <0.000262 <0.0244 <0.00823 <0.000304 <0.0695 <0.000301 <0.000293 <0.000288 <0.000302 <0.000332 <0.0309 <0.0104 <0.00031 <0.0709 <0.000306 <0.000298 <0.000294 <0.000308 <0.000338 <0.0315 <0.0106 <0.000324 <0.0741 <0.00032 <0.000312 <0.000307 <0.000322 <0.000353 <0.0329 <0.0111 <0.000288 <0.0658 <0.000285 <0.000277 <0.000273 <0.000286 <0.000314 <0.0293 <0.00985 <0.000345 0.526 0.0676 <0.000332 <0.000327 0.00185 <0.000376 0.539 <0.0118 <0.000397 <0.0908 <0.000393 <0.000382 <0.000376 <0.000395 <0.000433 <0.0404 <0.0136 <0.000282 <0.0645 0.00294 <0.000272 <0.000267 <0.00028 <0.000308 0.261 <0.00966 <0.000237 <0.0541 <0.000234 <0.000228 <0.000225 <0.000235 <0.000258 <0.0241 <0.0081 <0.00543 <1.24 <0.00537 <0.00523 <0.00515 <0.0054 <0.00592 <0.552 <0.186 <0.00116 <0.265 <0.00115 <0.00112 <0.0011 <0.00115 <0.00127 <0.118 <0.0397 <0.00218 <0.499 <0.00216 <0.0021 <0.00207 <0.00217 <0.00238 <0.222 <0.0747 <0.000246 <0.0563 <0.000243 <0.000237 <0.000233 <0.000245 <0.000268 <0.025 <0.00842 <0.00116 <0.265 <0.00115 <0.00112 <0.0011 <0.00115 <0.00127 <0.118 <0.0397 <0.000239 0.528 0.00686 <0.00023 <0.000227 <0.000238 <0.000261 1.33 <0.00818 <0.000272 <0.0621 <0.000269 <0.000261 <0.000258 <0.00027 <0.000296 <0.0276 <0.0093 <0.000306 <0.0701 <0.000303 <0.000295 <0.000291 <0.000305 <0.000334 <0.0312 <0.0105 <0.000424 <0.0969 <0.000419 <0.000408 <0.000402 <0.000421 <0.000462 <0.0431 <0.0145 <0.00032 <0.0733 <0.000317 <0.000308 <0.000304 <0.000319 <0.000349 <0.0326 <0.011 <0.000504 <0.115 0.289 <0.000485 <0.000478 <0.000501 <0.000549 <0.0512 <0.0172 <0.000355 <0.0812 <0.000351 <0.000342 <0.000337 <0.000353 <0.000387 <0.0361 <0.0122<0.00045 <0.103 <0.000445 <0.000434 <0.000427 <0.000448 <0.000491 <0.0458 <0.0154<0.000332 <0.0759 <0.000328 <0.00032 <0.000315 <0.00033 <0.000362 <0.0338 <0.0114<0.000322 <0.0735 <0.000318 <0.00031 <0.000305 <0.00032 <0.000351 <0.0327 <0.011<0.000424 <0.0969 <0.000419 <0.000408 <0.000402 <0.000421 <0.000462 <0.0431 <0.0145<0.000324 <0.0741 <0.00032 <0.000312 <0.000307 <0.000322 <0.000353 <0.0329 <0.0111<0.000443 <0.101 <0.000438 <0.000427 <0.00042 <0.000441 <0.000484 <0.0451 <0.0152<0.00086 <0.196 <0.00085 <0.000828 <0.000816 <0.000855 <0.000938 <0.0875 <0.0294<0.000245 1.84 0.0317 <0.000236 <0.000232 <0.000244 <0.000267 2.85 <0.00839<0.000309 0.645 0.0107 <0.000297 <0.000293 <0.000307 <0.000337 1.1 <0.0106<0.000338 <0.0772 <0.000334 <0.000325 <0.00032 <0.000336 <0.000368 <0.0344 <0.0116 <0.00081 1.8 0.304 <0.00078 <0.000768 0.00395 <0.000884 0.391 <0.0277 mg/kg mg/kg mg/kg mg/kgmg/kg mg/kg mg/kg mg/kg mg/kg 01/11/2018 01/11/2018 01/11/2018 01/11/2018 01/11/201801/11/2018 01/11/2018 01/11/2018 01/11/2018BF12 2-3 BF12 4-6 BF12 9-11 BF13 1-3 BF13 4-5 BF13 8-10BF6 0.5-1.5 BF6 4-5 BF6 14-15 601 West South Street - Former Gas Station - Buffaloe Landfill and DOT Fill Area Samples Page 2 of 3 TABLE 3 - VOLATILE ORGANIC COMPOUNDS 601-617 WEST SOUTH STREET RALEIGH, NC 27603 WR JOB NO. 02170761.00 Method Analyte CAS NCDEQ IHSB Unrestricted Use Health Based PSRG (October 2017) 8260B ACETONE 67-64-1 122008260BACRYLONITRILE107-13-1 0.258260BBENZENE71-43-2 1.28260BBROMOBENZENE108-86-1 58 8260B BROMODICHLOROMETHANE 75-27-4 0.29 8260B BROMOFORM 75-25-2 19 8260B BROMOMETHANE 74-83-9 1.36 8260B N-BUTYLBENZENE 104-51-8 108 8260B SEC-BUTYLBENZENE 135-98-8 145 8260B TERT-BUTYLBENZENE 98-06-6 183 8260B CARBON TETRACHLORIDE 56-23-5 0.65 8260B CHLOROBENZENE 108-90-7 56 8260B CHLORODIBROMOMETHANE 124-48-1 8.3 8260B CHLOROETHANE 75-00-3 2120 8260B CHLOROFORM 67-66-3 0.32 8260B CHLOROMETHANE 74-87-3 22 8260B 2-CHLOROTOLUENE 95-49-8 320 8260B 4-CHLOROTOLUENE 106-43-4 253 8260B 1,2-DIBROMO-3-CHLOROPROPANE 96-12-8 0.0053 8260B 1,2-DIBROMOETHANE 106-93-4 0.036 8260B DIBROMOMETHANE 74-95-3 4.8 8260B 1,2-DICHLOROBENZENE 95-50-1 360 8260B 1,3-DICHLOROBENZENE 541-73-1 NL8260B1,4-DICHLOROBENZENE 106-46-7 2.68260BDICHLORODIFLUOROMETHANE75-71-8 17.48260B1,1-DICHLOROETHANE 75-34-3 3.68260B1,2-DICHLOROETHANE 107-06-2 0.468260B1,1-DICHLOROETHENE 75-35-4 468260BCIS-1,2-DICHLOROETHENE 156-59-2 328260BTRANS-1,2-DICHLOROETHENE 156-60-5 3208260B1,2-DICHLOROPROPANE 78-87-5 18260B1,1-DICHLOROPROPENE 563-58-6 NL8260B1,3-DICHLOROPROPANE 142-28-9 320 8260B CIS-1,3-DICHLOROPROPENE 10061-01-5 NL 8260B TRANS-1,3-DICHLOROPROPENE 10061-02-6 NL 8260B 2,2-DICHLOROPROPANE 594-20-7 NL 8260B DI-ISOPROPYL ETHER 108-20-3 440 8260B ETHYLBENZENE 100-41-4 5.8 8260B HEXACHLORO-1,3-BUTADIENE 87-68-3 1.2 8260B ISOPROPYLBENZENE 98-82-8 268 8260B P-ISOPROPYLTOLUENE 99-87-6 NL 8260B 2-BUTANONE (MEK)78-93-3 5400 8260B METHYLENE CHLORIDE 75-09-2 57 8260B 4-METHYL-2-PENTANONE (MIBK)108-10-1 3360 8260B METHYL TERT-BUTYL ETHER 1634-04-4 47 8260B NAPHTHALENE 91-20-3 3.8 8260B N-PROPYLBENZENE 103-65-1 264 8260B STYRENE 100-42-5 867 8260B 1,1,1,2-TETRACHLOROETHANE 630-20-6 2 8260B 1,1,2,2-TETRACHLOROETHANE 79-34-5 0.6 8260B TETRACHLOROETHENE 127-18-4 16.2 8260B TOLUENE 108-88-3 818 8260B 1,2,3-TRICHLOROBENZENE 87-61-6 12.68260B1,2,4-TRICHLOROBENZENE 120-82-1 11.68260B1,1,1-TRICHLOROETHANE 71-55-6 6408260B1,1,2-TRICHLOROETHANE 79-00-5 0.38260B1,1,2-TRICHLOROTRIFLUOROETHANE 76-13-1 9108260BTRICHLOROETHENE79-01-6 0.828260BTRICHLOROFLUOROMETHANE75-69-4 12308260B1,2,3-TRICHLOROPROPANE 96-18-4 0.00518260B1,2,4-TRIMETHYLBENZENE 95-63-6 11.68260B1,3,5-TRIMETHYLBENZENE 108-67-8 1568260BVINYL CHLORIDE 75-01-4 0.059 8260B XYLENES, TOTAL 1330-20-7 116 Qualifiers: Notes: 1) All results provided in ug/L (micrograms per liter) or parts per billion.2) IHSB - Inactive Hazardous Sites Branch.3) PSRG - Preliminary Soil Remediation Goals. NL = Not Listed Result = Result Exceeds MDL.Result = Result Exceeds Unrestricted Use Health Based PSRG. J3: The associated batch QC was outside the established quality control range for precision. J4: The associated batch QC was outside the established quality control range for accuracy. J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low.J7: Surrogate recovery cannot be used for control limit evaluation due to dilution Volatile Organic Compounds B: The same analyte is found in the associated blank.J0: Calibration verification outside of acceptance limits. Result is estimated. Units Date Collected Sample Locations Client Sample ID Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier <0.0121 <0.012 <0.0115<0.00216 <0.00214 <0.00206<0.000326 <0.000323 0.00181<0.000343 <0.00034 <0.000327 <0.000307 <0.000304 <0.000292 <0.000512 <0.000508 <0.000488 <0.00162 <0.0016 <0.00154 <0.000312 <0.000309 <0.000297 <0.000243 <0.000241 <0.000231 <0.000249 <0.000247 <0.000237 <0.000396 <0.000393 <0.000377 <0.000256 <0.000254 <0.000244 <0.000451 <0.000447 <0.000429 <0.00114 <0.00113 <0.00109 <0.000277 <0.000274 <0.000263 <0.000453 <0.000449 <0.000431 <0.000364 <0.00036 <0.000346 <0.00029 <0.000287 <0.000276 <0.00127 <0.00126 <0.00121 <0.000414 <0.000411 <0.000395 <0.000461 <0.000457 <0.000439 <0.000368 <0.000365 <0.000351 <0.000289 <0.000286 <0.000275<0.000273 <0.000271 <0.00026<0.000861 <0.000854 <0.00082<0.00024 <0.000238 <0.000229<0.00032 <0.000317 <0.000305<0.000366 <0.000363 <0.000349<0.000284 <0.000281 <0.00027<0.000319 <0.000316 <0.000304<0.000432 <0.000429 <0.000412<0.000383 <0.00038 <0.000365<0.00025 <0.000248 <0.000238 <0.000317 <0.000314 <0.000301 <0.000323 <0.00032 <0.000307 <0.000337 <0.000334 <0.000321 <0.0003 <0.000297 <0.000285 <0.000359 <0.000356 <0.000342 <0.000413 <0.000409 <0.000393 <0.000294 <0.000291 <0.00028 <0.000246 <0.000244 <0.000235 <0.00565 <0.0056 <0.00538 <0.00121 <0.0012 <0.00115 <0.00227 <0.00225 <0.00216 <0.000256 <0.000254 <0.000244 <0.00121 <0.0012 <0.00115 <0.000249 <0.000247 <0.000237 <0.000283 <0.00028 <0.000269 <0.000319 <0.000316 <0.000304 <0.000441 <0.000437 <0.00042 <0.000333 <0.00033 0.00164 <0.000524 <0.00052 <0.000499 <0.00037 <0.000366 <0.000352<0.000469 <0.000465 <0.000446<0.000345 <0.000342 <0.000329<0.000335 <0.000332 <0.000319<0.000441 <0.000437 <0.00042<0.000337 <0.000334 <0.000321<0.000461 <0.000457 <0.000439<0.000895 <0.000887 <0.000852<0.000255 <0.000253 <0.000243<0.000321 <0.000318 <0.000306<0.000352 <0.000348 <0.000335 <0.000843 <0.000836 <0.000803 mg/kgmg/kg mg/kg 01/11/2018 01/11/201801/11/2018RF-1 RF-2 RF-3 Relic Fill Sidewall Samples Page 3 of 3 TABLE 4 - SEMI-VOLATILE ORGANIC COMPOUNDS 601-617 WEST SOUTH STREETRALEIGH, NC 27603 WR JOB NO. 02170761.00 Method Analyte CAS NCDEQ IHSB Unrestricted Use Health Based PSRG (October 2017) Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier 8270D ACENAPHTHENE 83-32-9 720 <0.00856 <0.00745 <0.00755 <0.00788 <0.00934 <0.00807 <0.00802 <0.00814 8270D ACENAPHTHYLENE 208-96-8 NL <0.00895 <0.00779 <0.00789 <0.00823 <0.00976 <0.00843 <0.00839 <0.0085 8270D ANTHRACENE 120-12-7 3600 <0.00843 <0.00733 <0.00743 <0.00776 <0.00919 <0.00794 <0.0079 <0.008018270DBENZIDINE92-87-5 0.00053 <0.085 J4 <0.0739 J4 <0.0749 J4 <0.0782 J4 <0.0926 J4 <0.0801 J4 <0.0796 J4 <0.0807 J4 8270D BENZO(A)ANTHRACENE 56-55-3 0.16 <0.00571 <0.00497 <0.00503 <0.00525 <0.00622 <0.00538 <0.00535 <0.00542 8270D BENZO(B)FLUORANTHENE 205-99-2 0.16 <0.00927 <0.00807 <0.00817 <0.00853 <0.0101 <0.00874 <0.00869 <0.00881 8270D BENZO(K)FLUORANTHENE 207-08-9 1.6 <0.00776 <0.00675 <0.00684 <0.00714 <0.00846 <0.00732 <0.00727 <0.00738 8270D BENZO(G,H,I)PERYLENE 191-24-2 NL <0.00962 <0.00837 <0.00848 <0.00885 <0.0105 <0.00906 <0.00901 <0.00914 8270D BENZO(A)PYRENE 50-32-8 0.016 <0.00731 <0.00636 <0.00644 <0.00672 <0.00797 <0.00689 <0.00685 <0.00694 8270D BIS(2-CHLORETHOXY)METHANE 111-91-1 38 <0.0103 <0.00894 <0.00905 <0.00945 <0.0112 <0.00968 <0.00962 <0.00976 8270D BIS(2-CHLOROETHYL)ETHER 111-44-4 0.23 <0.012 <0.0104 <0.0105 <0.011 <0.013 <0.0113 <0.0112 <0.0114 8270D BIS(2-CHLOROISOPROPYL)ETHER 39638-32-9 NL <0.0101 <0.00882 <0.00894 <0.00933 <0.0111 <0.00955 <0.0095 <0.00963 8270D 4-BROMOPHENYL-PHENYLETHER 101-55-3 NL <0.0152 <0.0132 <0.0134 <0.014 <0.0166 <0.0143 <0.0142 <0.0144 8270D 2-CHLORONAPHTHALENE 91-58-7 960 <0.00852 <0.00742 <0.00751 <0.00784 <0.00929 <0.00803 <0.00799 <0.00818270D4-CHLOROPHENYL-PHENYLETHER 7005-72-3 NL <0.00836 <0.00728 <0.00737 <0.00769 <0.00912 <0.00788 <0.00784 <0.00795 8270D CHRYSENE 218-01-9 16 <0.0074 <0.00644 <0.00653 <0.00681 <0.00807 <0.00698 <0.00694 <0.00703 8270D DIBENZ(A,H)ANTHRACENE 53-70-3 0.016 <0.011 <0.00953 <0.00965 <0.0101 <0.0119 <0.0103 <0.0103 <0.01048270D3,3-DICHLOROBENZIDINE 91-94-1 1.2 <0.106 <0.0921 <0.0934 <0.0974 <0.115 <0.0998 <0.0992 <0.101 8270D 2,4-DINITROTOLUENE 121-14-2 1.7 <0.0081 <0.00704 <0.00714 <0.00745 <0.00883 <0.00763 <0.00759 <0.00769 8270D 2,6-DINITROTOLUENE 606-20-2 0.36 <0.00983 <0.00855 <0.00867 <0.00904 <0.0107 <0.00926 <0.00921 <0.009348270DFLUORANTHENE206-44-0 480 <0.00662 <0.00576 <0.00583 <0.00609 <0.00721 <0.00623 <0.0062 <0.00629 8270D FLUORENE 86-73-7 480 <0.0091 <0.00792 <0.00802 <0.00837 <0.00992 <0.00857 <0.00852 <0.00864 8270D HEXACHLOROBENZENE 118-74-1 0.21 <0.0114 <0.00993 <0.0101 <0.0105 <0.0124 <0.0108 <0.0107 <0.01088270DHEXACHLORO-1,3-BUTADIENE 87-68-3 1.2 <0.0133 <0.0116 <0.0118 <0.0123 <0.0145 <0.0126 <0.0125 <0.0127 8270D HEXACHLOROCYCLOPENTADIENE 77-47-4 0.36 <0.0783 J0 <0.0681 J0 <0.069 J0 <0.072 J0 <0.0854 J0 <0.0738 J0 <0.0734 J0 <0.0744 J0 8270D HEXACHLOROETHANE 67-72-1 1.8 <0.0179 <0.0156 <0.0158 <0.0164 <0.0195 <0.0168 <0.0167 <0.0178270DINDENO(1,2,3-CD)PYRENE 193-39-5 0.16 <0.0103 <0.00896 <0.00908 <0.00947 <0.0112 <0.0097 <0.00965 <0.00978 8270D ISOPHORONE 78-59-1 570 <0.00696 <0.00606 <0.00614 <0.00641 <0.00759 <0.00656 <0.00652 <0.00661 8270D NAPHTHALENE 91-20-3 3.8 <0.0119 <0.0103 <0.0105 <0.0109 <0.0129 <0.0112 <0.0111 <0.0113 8270D NITROBENZENE 98-95-3 5.1 <0.00927 <0.00807 <0.00817 <0.00853 <0.0101 <0.00874 <0.00869 <0.00881 8270D N-NITROSODIMETHYLAMINE 62-75-9 0.002 <0.0863 <0.0751 <0.0761 <0.0794 <0.0941 <0.0813 <0.0809 <0.082 8270D N-NITROSODIPHENYLAMINE 86-30-6 110 <0.00792 <0.00689 <0.00698 <0.00729 <0.00864 <0.00747 <0.00742 <0.00753 8270D N-NITROSODI-N-PROPYLAMINE 621-64-7 0.078 <0.0121 <0.0105 <0.0107 <0.0111 <0.0132 <0.0114 <0.0113 <0.0115 8270D PHENANTHRENE 85-01-8 NL <0.00704 <0.00613 <0.00621 <0.00648 <0.00768 <0.00664 <0.0066 <0.00669 8270D BENZYLBUTYL PHTHALATE 85-68-7 290 <0.0137 <0.012 <0.0121 <0.0126 <0.015 <0.0129 <0.0129 <0.0131 8270D BIS(2-ETHYLHEXYL)PHTHALATE 117-81-7 39 <0.016 <0.0139 <0.0141 <0.0147 <0.0174 <0.0151 <0.015 <0.0152 8270D DI-N-BUTYL PHTHALATE 84-74-2 1260 <0.0145 <0.0127 <0.0128 <0.0134 <0.0159 <0.0137 <0.0136 <0.01388270DDIETHYL PHTHALATE 84-66-2 10200 <0.00922 <0.00802 <0.00813 <0.00848 <0.01 <0.00869 <0.00864 <0.00876 8270D DIMETHYL PHTHALATE 131-11-3 NL <0.0072 <0.00627 <0.00635 <0.00663 <0.00785 <0.00679 <0.00675 <0.00684 8270D DI-N-OCTYL PHTHALATE 117-84-0 126 <0.0121 <0.0105 <0.0107 <0.0111 <0.0132 <0.0114 <0.0113 <0.01158270DPYRENE129-00-0 360 <0.0164 <0.0143 <0.0145 <0.0151 <0.0179 <0.0155 <0.0154 <0.0156 8270D 1,2,4-TRICHLOROBENZENE 120-82-1 11.6 <0.0117 <0.0102 <0.0103 <0.0107 <0.0127 <0.011 <0.0109 <0.0111 8270D 4-CHLORO-3-METHYLPHENOL 59-50-7 1260 <0.00636 <0.00554 <0.00561 <0.00585 <0.00694 <0.006 <0.00596 <0.006048270D2-CHLOROPHENOL 95-57-8 78 <0.0111 <0.00964 <0.00977 <0.0102 <0.0121 <0.0104 <0.0104 <0.0105 8270D 2,4-DICHLOROPHENOL 120-83-2 38 <0.00995 <0.00866 <0.00877 <0.00915 <0.0108 <0.00938 <0.00932 <0.00945 8270D 2,4-DIMETHYLPHENOL 105-67-9 260 <0.0628 <0.0547 <0.0554 <0.0578 <0.0685 <0.0592 <0.0589 <0.05978270D4,6-DINITRO-2-METHYLPHENOL 534-52-1 1.02 <0.165 <0.144 <0.146 <0.152 <0.18 <0.156 <0.155 <0.157 8270D 2,4-DINITROPHENOL 51-28-5 26 <0.131 <0.114 <0.115 <0.12 <0.143 <0.123 <0.122 <0.124 8270D 2-NITROPHENOL 88-75-5 NL <0.0173 <0.0151 <0.0153 <0.016 <0.0189 <0.0163 <0.0162 <0.01658270D4-NITROPHENOL 100-02-7 NL <0.07 J0 <0.0609 J0 <0.0617 J0 <0.0644 J0 <0.0763 J0 <0.066 J0 <0.0656 J0 <0.0665 J0 8270D PENTACHLOROPHENOL 87-86-5 1 <0.064 <0.0557 <0.0564 <0.0589 <0.0698 <0.0603 <0.06 <0.0608 8270D PHENOL 108-95-2 3800 <0.00927 <0.00807 <0.00817 <0.00853 <0.0101 <0.00874 <0.00869 <0.00881 8270D 2,4,6-TRICHLOROPHENOL 88-06-2 12.6 <0.0104 <0.00904 <0.00916 <0.00956 <0.0113 <0.00979 <0.00974 <0.00987 Qualifiers: Notes: 1) All results provided in ug/L (micrograms per liter) or parts per billion.2) IHSB - Inactive Hazardous Sites Branch. 3) PSRG - Preliminary Soil Remediation Goals. NL = Not Listed Result = Result Exceeds MDL.Result = Result Exceeds Unrestricted Use Health Based PSRG. J0: Calibration verification outside of acceptance limits. Result is estimated. J3: The associated batch QC was outside the established quality control range for precision. J4: The associated batch QC was outside the established quality control range for accuracy. J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low.J7: Surrogate recovery cannot be used for control limit evaluation due to dilution Semi-Volatile Organic Compounds B: The same analyte is found in the associated blank. mg/kg Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg 01/11/2018 01/11/2018 Date Collected 01/11/2018 01/11/2018 01/11/2018 01/11/2018 01/11/2018 01/11/2018 BF6 1-3 BF7 2-4 BF8 2-4 Sample Locations Buffaloe Landfill Fill Samples Client Sample ID BF1 0.5-1.5 BF2 2-4 BF3 2-4 BF4 2-4 BF5 2-4 Page 1 of 3 TABLE 4 - SEMI-VOLATILE ORGANIC COMPOUNDS 601-617 WEST SOUTH STREETRALEIGH, NC 27603 WR JOB NO. 02170761.00 Method Analyte CAS NCDEQ IHSB Unrestricted Use Health Based PSRG (October 2017) 8270D ACENAPHTHENE 83-32-9 720 8270D ACENAPHTHYLENE 208-96-8 NL 8270D ANTHRACENE 120-12-7 36008270DBENZIDINE92-87-5 0.00053 8270D BENZO(A)ANTHRACENE 56-55-3 0.16 8270D BENZO(B)FLUORANTHENE 205-99-2 0.16 8270D BENZO(K)FLUORANTHENE 207-08-9 1.6 8270D BENZO(G,H,I)PERYLENE 191-24-2 NL 8270D BENZO(A)PYRENE 50-32-8 0.016 8270D BIS(2-CHLORETHOXY)METHANE 111-91-1 38 8270D BIS(2-CHLOROETHYL)ETHER 111-44-4 0.23 8270D BIS(2-CHLOROISOPROPYL)ETHER 39638-32-9 NL 8270D 4-BROMOPHENYL-PHENYLETHER 101-55-3 NL 8270D 2-CHLORONAPHTHALENE 91-58-7 9608270D4-CHLOROPHENYL-PHENYLETHER 7005-72-3 NL 8270D CHRYSENE 218-01-9 16 8270D DIBENZ(A,H)ANTHRACENE 53-70-3 0.0168270D3,3-DICHLOROBENZIDINE 91-94-1 1.2 8270D 2,4-DINITROTOLUENE 121-14-2 1.7 8270D 2,6-DINITROTOLUENE 606-20-2 0.368270DFLUORANTHENE206-44-0 480 8270D FLUORENE 86-73-7 480 8270D HEXACHLOROBENZENE 118-74-1 0.218270DHEXACHLORO-1,3-BUTADIENE 87-68-3 1.2 8270D HEXACHLOROCYCLOPENTADIENE 77-47-4 0.36 8270D HEXACHLOROETHANE 67-72-1 1.88270DINDENO(1,2,3-CD)PYRENE 193-39-5 0.16 8270D ISOPHORONE 78-59-1 570 8270D NAPHTHALENE 91-20-3 3.8 8270D NITROBENZENE 98-95-3 5.1 8270D N-NITROSODIMETHYLAMINE 62-75-9 0.002 8270D N-NITROSODIPHENYLAMINE 86-30-6 110 8270D N-NITROSODI-N-PROPYLAMINE 621-64-7 0.078 8270D PHENANTHRENE 85-01-8 NL 8270D BENZYLBUTYL PHTHALATE 85-68-7 290 8270D BIS(2-ETHYLHEXYL)PHTHALATE 117-81-7 39 8270D DI-N-BUTYL PHTHALATE 84-74-2 12608270DDIETHYL PHTHALATE 84-66-2 10200 8270D DIMETHYL PHTHALATE 131-11-3 NL 8270D DI-N-OCTYL PHTHALATE 117-84-0 1268270DPYRENE129-00-0 360 8270D 1,2,4-TRICHLOROBENZENE 120-82-1 11.6 8270D 4-CHLORO-3-METHYLPHENOL 59-50-7 12608270D2-CHLOROPHENOL 95-57-8 78 8270D 2,4-DICHLOROPHENOL 120-83-2 38 8270D 2,4-DIMETHYLPHENOL 105-67-9 2608270D4,6-DINITRO-2-METHYLPHENOL 534-52-1 1.02 8270D 2,4-DINITROPHENOL 51-28-5 26 8270D 2-NITROPHENOL 88-75-5 NL8270D4-NITROPHENOL 100-02-7 NL 8270D PENTACHLOROPHENOL 87-86-5 1 8270D PHENOL 108-95-2 3800 8270D 2,4,6-TRICHLOROPHENOL 88-06-2 12.6 Qualifiers: Notes: 1) All results provided in ug/L (micrograms per liter) or parts per billion.2) IHSB - Inactive Hazardous Sites Branch. 3) PSRG - Preliminary Soil Remediation Goals. NL = Not Listed Result = Result Exceeds MDL.Result = Result Exceeds Unrestricted Use Health Based PSRG. J0: Calibration verification outside of acceptance limits. Result is estimated. J3: The associated batch QC was outside the established quality control range for precision. J4: The associated batch QC was outside the established quality control range for accuracy. J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low.J7: Surrogate recovery cannot be used for control limit evaluation due to dilution Semi-Volatile Organic Compounds B: The same analyte is found in the associated blank. Units Date Collected Sample Locations Client Sample ID Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier <0.149 <0.00852 <0.00737 <0.00717 <0.00707 <0.00741 <0.162 <0.00758 <0.0102 <0.156 <0.00891 <0.0077 <0.0075 <0.00739 <0.00774 <0.17 <0.00792 <0.0107 <0.146 <0.00839 <0.00725 <0.00706 <0.00696 <0.00729 <0.16 <0.00746 <0.01<1.47 J4 <0.0845 J4 <0.0731 J3 J4 <0.0712 J4 J6 <0.0701 J4 <0.0735 J4 <1.61 J4 <0.0752 J4 <0.101 J4 <0.0994 <0.00568 <0.00491 <0.00478 <0.00471 <0.00494 <0.108 <0.00505 <0.0068 <0.161 <0.00922 <0.00798 <0.00777 <0.00765 <0.00802 <0.176 <0.0082 <0.011 <0.135 <0.00772 <0.00668 <0.0065 <0.00641 <0.00672 <0.147 <0.00687 <0.00925 <0.167 <0.00957 <0.00828 <0.00806 <0.00794 <0.00832 <0.182 <0.00851 <0.0115 <0.128 <0.00727 <0.00629 <0.00612 <0.00603 <0.00633 <0.139 <0.00647 <0.00871 <0.179 <0.0102 <0.00884 <0.0086 <0.00848 <0.00889 <0.195 <0.00909 <0.0122 <0.208 <0.0119 <0.0103 <0.01 <0.00986 <0.0103 <0.227 <0.0106 <0.0142 <0.176 <0.0101 <0.00872 <0.00849 <0.00837 <0.00877 <0.192 <0.00897 <0.0121 <0.265 <0.0151 <0.0131 <0.0127 <0.0125 <0.0132 <0.289 <0.0135 <0.0181 <0.149 <0.00848 <0.00733 <0.00714 <0.00703 <0.00738 <0.162 <0.00754 <0.0102<0.145 <0.00832 <0.0072 <0.00701 <0.0069 <0.00724 <0.158 <0.0074 <0.00996 <0.129 <0.00737 <0.00637 <0.0062 <0.00611 <0.00641 <0.141 <0.00655 <0.00882 <0.19 <0.0109 <0.00942 <0.00917 <0.00904 <0.00948 <0.208 <0.00969 <0.013<1.85 <0.105 <0.0911 <0.0887 <0.0874 <0.0916 <2.01 <0.0937 <0.126 <0.14 <0.00806 <0.00697 <0.00678 <0.00668 <0.00701 <0.153 <0.00717 <0.00965 <0.171 <0.00978 <0.00846 <0.00824 <0.00811 <0.00851 <0.186 <0.0087 <0.0117<0.115 <0.00658 <0.00569 <0.00554 <0.00546 <0.00573 <0.126 <0.00586 <0.00788 1.14 <0.00905 <0.00783 <0.00762 <0.00751 <0.00787 <0.172 <0.00805 <0.0108 <0.198 <0.0114 <0.00982 <0.00957 <0.00942 <0.00988 <0.216 <0.0101 <0.0136<0.232 <0.0133 <0.0115 <0.0112 <0.011 <0.0115 <0.253 <0.0118 <0.0159 <1.36 J0 <0.0779 J0 <0.0674 <0.0656 J0 <0.0646 J0 <0.0678 J0 <1.48 J0 <0.0693 J0 <0.0933 J0 <0.311 <0.0178 <0.0154 <0.015 <0.0147 <0.0155 <0.339 <0.0158 <0.0213<0.179 <0.0102 <0.00886 <0.00863 <0.0085 <0.00891 <0.195 <0.00911 <0.0123 <0.121 <0.00693 <0.00599 <0.00583 <0.00575 <0.00603 <0.132 <0.00616 <0.0083 4.49 1.91 <0.0102 <0.00993 <0.00978 <0.0103 <0.225 0.193 <0.0141 <0.161 <0.00922 <0.00798 <0.00777 <0.00765 <0.00802 <0.176 <0.0082 <0.011 <1.5 <0.0859 <0.0743 <0.0723 <0.0712 <0.0747 <1.63 <0.0764 <0.103 <0.138 <0.00788 <0.00682 <0.00664 <0.00654 <0.00686 <0.151 <0.00701 <0.00944 <0.21 <0.012 <0.0104 <0.0101 <0.00997 <0.0105 <0.229 <0.0107 <0.0144 <0.123 <0.00701 <0.00606 <0.0059 <0.00581 <0.00609 <0.134 <0.00623 <0.00839 <0.239 <0.0137 <0.0118 <0.0115 <0.0113 <0.0119 <0.261 <0.0122 <0.0164 <0.279 <0.0159 <0.0138 <0.0134 <0.0132 <0.0139 <0.304 <0.0142 <0.0191 <0.253 <0.0145 <0.0125 <0.0122 <0.012 <0.0126 <0.276 <0.0129 <0.0173<0.16 <0.00917 <0.00793 <0.00772 <0.00761 <0.00798 <0.175 <0.00816 <0.011 <0.125 <0.00717 <0.0062 <0.00603 <0.00594 <0.00623 <0.137 <0.00637 <0.00858 <0.21 <0.012 <0.0104 <0.0101 <0.00998 <0.0105 <0.229 <0.0107 <0.0144<0.286 <0.0163 <0.0141 <0.0137 <0.0135 <0.0142 <0.311 <0.0145 <0.0195 <0.203 <0.0116 <0.0101 <0.00979 <0.00964 <0.0101 <0.222 <0.0103 <0.0139 <0.111 <0.00633 <0.00547 <0.00533 <0.00525 <0.00551 <0.121 <0.00563 <0.00758<0.193 <0.011 <0.00954 <0.00929 <0.00915 <0.00959 <0.21 <0.00981 <0.0132 <0.173 <0.0099 <0.00856 <0.00834 <0.00821 <0.00861 <0.189 <0.00881 <0.0119 <1.09 <0.0625 <0.0541 <0.0526 <0.0518 <0.0544 <1.19 <0.0556 <0.0748<2.88 <0.165 <0.142 <0.139 <0.136 <0.143 <3.14 <0.146 <0.197 <2.27 <0.13 <0.112 <0.11 <0.108 <0.113 <2.48 <0.116 <0.156 <0.302 <0.0173 <0.0149 <0.0145 <0.0143 <0.015 <0.329 <0.0153 <0.0207<1.22 J0 <0.0697 J0 <0.0603 <0.0587 J0 J3 J6 <0.0578 J0 <0.0606 J0 <1.33 J0 <0.062 J0 <0.0834 J0 <1.11 <0.0637 <0.0551 <0.0536 <0.0528 <0.0554 <1.22 <0.0567 <0.0763 <0.161 <0.00922 <0.00798 <0.00777 <0.00765 <0.00802 <0.176 <0.0082 <0.011 <0.181 <0.0103 <0.00894 <0.00871 <0.00857 <0.00899 <0.197 <0.0092 <0.0124 mg/kg mg/kg mg/kg mg/kgmg/kg mg/kg mg/kg mg/kg mg/kg 01/11/2018 01/11/2018 01/11/2018 01/11/2018 01/11/201801/11/2018 01/11/2018 01/11/2018 01/11/2018 BF12 2-3 BF12 4-6 BF12 9-11 BF13 1-3 BF13 4-5 BF13 8-10BF6 0.5-1.5 BF6 4-5 BF6 14-15 601 West South Street - Former Gas Station - Buffaloe Landfill and DOT Fill Area Samples Page 2 of 3 TABLE 4 - SEMI-VOLATILE ORGANIC COMPOUNDS 601-617 WEST SOUTH STREETRALEIGH, NC 27603 WR JOB NO. 02170761.00 Method Analyte CAS NCDEQ IHSB Unrestricted Use Health Based PSRG (October 2017) 8270D ACENAPHTHENE 83-32-9 720 8270D ACENAPHTHYLENE 208-96-8 NL 8270D ANTHRACENE 120-12-7 36008270DBENZIDINE92-87-5 0.00053 8270D BENZO(A)ANTHRACENE 56-55-3 0.16 8270D BENZO(B)FLUORANTHENE 205-99-2 0.16 8270D BENZO(K)FLUORANTHENE 207-08-9 1.6 8270D BENZO(G,H,I)PERYLENE 191-24-2 NL 8270D BENZO(A)PYRENE 50-32-8 0.016 8270D BIS(2-CHLORETHOXY)METHANE 111-91-1 38 8270D BIS(2-CHLOROETHYL)ETHER 111-44-4 0.23 8270D BIS(2-CHLOROISOPROPYL)ETHER 39638-32-9 NL 8270D 4-BROMOPHENYL-PHENYLETHER 101-55-3 NL 8270D 2-CHLORONAPHTHALENE 91-58-7 9608270D4-CHLOROPHENYL-PHENYLETHER 7005-72-3 NL 8270D CHRYSENE 218-01-9 16 8270D DIBENZ(A,H)ANTHRACENE 53-70-3 0.0168270D3,3-DICHLOROBENZIDINE 91-94-1 1.2 8270D 2,4-DINITROTOLUENE 121-14-2 1.7 8270D 2,6-DINITROTOLUENE 606-20-2 0.368270DFLUORANTHENE206-44-0 480 8270D FLUORENE 86-73-7 480 8270D HEXACHLOROBENZENE 118-74-1 0.218270DHEXACHLORO-1,3-BUTADIENE 87-68-3 1.2 8270D HEXACHLOROCYCLOPENTADIENE 77-47-4 0.36 8270D HEXACHLOROETHANE 67-72-1 1.88270DINDENO(1,2,3-CD)PYRENE 193-39-5 0.16 8270D ISOPHORONE 78-59-1 570 8270D NAPHTHALENE 91-20-3 3.8 8270D NITROBENZENE 98-95-3 5.1 8270D N-NITROSODIMETHYLAMINE 62-75-9 0.002 8270D N-NITROSODIPHENYLAMINE 86-30-6 110 8270D N-NITROSODI-N-PROPYLAMINE 621-64-7 0.078 8270D PHENANTHRENE 85-01-8 NL 8270D BENZYLBUTYL PHTHALATE 85-68-7 290 8270D BIS(2-ETHYLHEXYL)PHTHALATE 117-81-7 39 8270D DI-N-BUTYL PHTHALATE 84-74-2 12608270DDIETHYL PHTHALATE 84-66-2 10200 8270D DIMETHYL PHTHALATE 131-11-3 NL 8270D DI-N-OCTYL PHTHALATE 117-84-0 1268270DPYRENE129-00-0 360 8270D 1,2,4-TRICHLOROBENZENE 120-82-1 11.6 8270D 4-CHLORO-3-METHYLPHENOL 59-50-7 12608270D2-CHLOROPHENOL 95-57-8 78 8270D 2,4-DICHLOROPHENOL 120-83-2 38 8270D 2,4-DIMETHYLPHENOL 105-67-9 2608270D4,6-DINITRO-2-METHYLPHENOL 534-52-1 1.02 8270D 2,4-DINITROPHENOL 51-28-5 26 8270D 2-NITROPHENOL 88-75-5 NL8270D4-NITROPHENOL 100-02-7 NL 8270D PENTACHLOROPHENOL 87-86-5 1 8270D PHENOL 108-95-2 3800 8270D 2,4,6-TRICHLOROPHENOL 88-06-2 12.6 Qualifiers: Notes: 1) All results provided in ug/L (micrograms per liter) or parts per billion.2) IHSB - Inactive Hazardous Sites Branch. 3) PSRG - Preliminary Soil Remediation Goals. NL = Not Listed Result = Result Exceeds MDL.Result = Result Exceeds Unrestricted Use Health Based PSRG. J0: Calibration verification outside of acceptance limits. Result is estimated. J3: The associated batch QC was outside the established quality control range for precision. J4: The associated batch QC was outside the established quality control range for accuracy. J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low.J7: Surrogate recovery cannot be used for control limit evaluation due to dilution Semi-Volatile Organic Compounds B: The same analyte is found in the associated blank. Units Date Collected Sample Locations Client Sample ID Result (MDL)Qualifier Result (MDL)Qualifier Result (MDL)Qualifier <0.00776 <0.00769 <0.00738 <0.00811 <0.00803 <0.00772 <0.00763 <0.00757 <0.00727<0.077 J4 <0.0763 J4 <0.0733 J4 <0.00517 <0.00512 <0.00492 <0.0084 <0.00832 <0.00799 <0.00703 <0.00697 <0.00669 <0.00871 <0.00863 <0.00829 <0.00662 <0.00656 <0.0063 <0.0093 <0.00922 <0.00886 <0.0108 <0.0107 <0.0103 <0.00918 <0.0091 <0.00874 <0.0138 <0.0136 <0.0131 <0.00772 <0.00765 <0.00735<0.00757 <0.00751 <0.00721 <0.0067 <0.00664 <0.00638 <0.00992 <0.00983 <0.00944<0.0959 <0.0951 <0.0913 <0.00733 <0.00727 <0.00698 <0.0089 <0.00882 <0.00848<0.00599 <0.00594 0.112 <0.00824 <0.00817 <0.00784 <0.0103 <0.0102 <0.00985<0.0121 <0.012 <0.0115 <0.0709 J0 <0.0703 J0 <0.0675 J0 <0.0162 <0.016 <0.0154<0.00933 <0.00924 <0.00888 <0.00631 <0.00625 <0.006 <0.0107 <0.0106 <0.0102 <0.0084 <0.00832 <0.00799 <0.0782 <0.0775 <0.0744 <0.00718 <0.00711 <0.00683 <0.0109 <0.0108 <0.0104 <0.00638 <0.00632 <0.00607 <0.0124 <0.0123 <0.0118 <0.0145 <0.0144 <0.0138 <0.0132 <0.013 <0.0125<0.00835 <0.00827 <0.00795 <0.00652 <0.00647 <0.00621 <0.011 <0.0109 <0.0104<0.0149 <0.0147 <0.0141 <0.0106 <0.0105 <0.0101 <0.00576 <0.00571 <0.00549<0.01 <0.00995 <0.00956 <0.00901 <0.00893 <0.00858 <0.0569 <0.0564 <0.0542<0.15 <0.148 <0.143 <0.118 <0.117 <0.113 <0.0157 <0.0156 <0.015<0.0634 J0 <0.0629 J0 <0.0604 J0 <0.058 <0.0575 <0.0552 <0.0084 <0.00832 <0.00799 <0.00941 <0.00933 <0.00896 mg/kgmg/kg mg/kg 01/11/2018 01/11/201801/11/2018 RF-1 RF-2 RF-3Relic Fill Sidewall Samples Page 3 of 3 APPENDIX A Laboratory Analytical Report ANALYTICAL REPORT January 25, 2018 Withers & Ravenel Eng. - Standard Sample Delivery Group:L963090 Samples Received:01/12/2018 Project Number:02170761 Description:601-617 South West St Report To:Matt James 115 MacKenan Drive Cary, NC 27511 Entire Report Reviewed By: January 25, 2018 [Preliminary Report] Heather J Wagner Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. 12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com January 25, 2018 Heather J Wagner Technical Service Representative ONE LAB. NATIONWIDE.TABLE OF CONTENTS Cp: Cover Page 1 Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 7 Sr: Sample Results 8 BF1 0.3-1.5 L963090-01 8 BF2 2-4 L963090-02 11 BF3 2-4 L963090-03 14 BF4 2-4 L963090-04 17 BF5 2-4 L963090-05 20 BF6 1-3 L963090-06 23 BF7 2-4 L963090-07 26 BF8 2-4 L963090-08 29 RF-1 L963090-09 32 RF-2 L963090-10 35 RF-3 L963090-11 38 BF12 2-3 L963090-12 41 BF12 4-6 L963090-13 44 BF12 9-11 L963090-14 47 BF13 1-3 L963090-15 50 BF13 4-5 L963090-16 53 BF13 8-10 L963090-17 56 BF6 0.5-1.5 L963090-18 59 BF6 4-5 L963090-19 62 BF6 14-15 L963090-20 65 Qc: Quality Control Summary 68 Total Solids by Method 2540 G-2011 68 Mercury by Method 7471B 71 Metals (ICP) by Method 6010D 72 Volatile Organic Compounds (GC/MS) by Method 8260B 73 Semi Volatile Organic Compounds (GC/MS) by Method 8270D 83 Gl: Glossary of Terms 93 Al: Accreditations & Locations 94 Sc: Sample Chain of Custody 95 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 2 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 2 of 98 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time BF1 0.3-1.5 L963090-01 Solid M. James 01/11/18 08:30 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063379 1 01/17/18 09:36 01/17/18 09:47 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 20:43 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 02:12 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062584 1 01/11/18 08:30 01/14/18 00:53 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/18/18 20:53 SR Collected by Collected date/time Received date/time BF2 2-4 L963090-02 Solid M. James 01/11/18 11:50 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063379 1 01/17/18 09:36 01/17/18 09:47 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 20:58 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 02:28 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062584 1 01/11/18 11:50 01/14/18 01:12 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/18/18 21:16 SR Collected by Collected date/time Received date/time BF3 2-4 L963090-03 Solid M. James 01/11/18 12:00 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063379 1 01/17/18 09:36 01/17/18 09:47 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:00 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 02:31 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062584 1 01/11/18 12:00 01/14/18 08:33 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/18/18 21:40 SR Collected by Collected date/time Received date/time BF4 2-4 L963090-04 Solid M. James 01/11/18 12:10 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063379 1 01/17/18 09:36 01/17/18 09:47 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:03 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 02:41 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062584 1 01/11/18 12:10 01/14/18 08:53 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/18/18 22:03 SR Collected by Collected date/time Received date/time BF5 2-4 L963090-05 Solid M. James 01/11/18 12:20 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063379 1 01/17/18 09:36 01/17/18 09:47 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:06 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 02:44 RDS Volatile Organic Compounds (GC/MS) by Method 8260B WG1062584 1 01/11/18 12:20 01/14/18 09:13 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/18/18 22:26 SR 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 3 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 3 of 98 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time BF6 1-3 L963090-06 Solid M. James 01/11/18 12:30 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063379 1 01/17/18 09:36 01/17/18 09:47 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:08 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 02:47 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062584 1 01/11/18 12:30 01/14/18 09:33 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/18/18 22:50 SR Collected by Collected date/time Received date/time BF7 2-4 L963090-07 Solid M. James 01/11/18 12:40 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:11 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 02:51 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062584 1 01/11/18 12:40 01/14/18 09:52 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/18/18 23:13 SR Collected by Collected date/time Received date/time BF8 2-4 L963090-08 Solid M. James 01/11/18 13:00 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:13 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 02:54 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 13:00 01/14/18 15:09 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/18/18 23:36 SR Collected by Collected date/time Received date/time RF-1 L963090-09 Solid M. James 01/11/18 14:30 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:16 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 02:57 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 14:30 01/14/18 15:29 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/19/18 00:00 SR Collected by Collected date/time Received date/time RF-2 L963090-10 Solid M. James 01/11/18 14:40 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:18 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:00 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 14:40 01/14/18 15:48 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/19/18 00:23 SR 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 4 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 4 of 98 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time RF-3 L963090-11 Solid M. James 01/11/18 14:50 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:26 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:04 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 14:50 01/14/18 16:08 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/19/18 00:46 SR Collected by Collected date/time Received date/time BF12 2-3 L963090-12 Solid M. James 01/11/18 09:00 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:28 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:07 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 09:00 01/14/18 16:56 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/19/18 01:09 SR Collected by Collected date/time Received date/time BF12 4-6 L963090-13 Solid M. James 01/11/18 09:10 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:31 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:10 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 09:10 01/14/18 17:16 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/19/18 02:19 SR Collected by Collected date/time Received date/time BF12 9-11 L963090-14 Solid M. James 01/11/18 09:20 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:33 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:20 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 09:20 01/14/18 17:35 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/19/18 02:42 SR Collected by Collected date/time Received date/time BF13 1-3 L963090-15 Solid M. James 01/11/18 09:40 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:36 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:23 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 09:40 01/14/18 17:55 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 20 01/17/18 06:53 01/19/18 05:02 SR 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 5 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 5 of 98 ONE LAB. NATIONWIDE.SAMPLE SUMMARY Collected by Collected date/time Received date/time BF13 4-5 L963090-16 Solid M. James 01/11/18 09:50 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063380 1 01/17/18 10:01 01/17/18 10:09 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:39 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:27 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 100 01/11/18 09:50 01/14/18 19:33 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/19/18 03:05 SR Collected by Collected date/time Received date/time BF13 8-10 L963090-17 Solid M. James 01/11/18 10:00 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063382 1 01/17/18 10:24 01/17/18 10:33 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:41 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:30 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 25 01/11/18 10:00 01/14/18 19:52 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/19/18 03:29 SR Collected by Collected date/time Received date/time BF6 0.5-1.5 L963090-18 Solid M. James 01/11/18 08:50 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063382 1 01/17/18 10:24 01/17/18 10:33 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:44 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:33 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 08:50 01/14/18 18:15 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 20 01/17/18 06:53 01/19/18 04:38 SR Collected by Collected date/time Received date/time BF6 4-5 L963090-19 Solid M. James 01/11/18 08:55 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063382 1 01/17/18 10:24 01/17/18 10:33 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:46 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:37 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 200 01/11/18 08:55 01/14/18 20:12 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 1 01/17/18 06:53 01/19/18 03:52 SR Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062710 10 01/17/18 06:53 01/19/18 16:19 CJR Collected by Collected date/time Received date/time BF6 14-15 L963090-20 Solid M. James 01/11/18 08:45 01/12/18 13:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Total Solids by Method 2540 G-2011 WG1063382 1 01/17/18 10:24 01/17/18 10:33 JD Mercury by Method 7471B WG1062912 1 01/16/18 19:57 01/17/18 21:49 EL Metals (ICP) by Method 6010D WG1062607 1 01/14/18 16:37 01/16/18 03:40 BRJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 1 01/11/18 08:45 01/14/18 18:34 LRL Volatile Organic Compounds (GC/MS) by Method 8260B WG1062672 25 01/11/18 08:45 01/17/18 17:52 LRL Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1062000 1 01/15/18 06:20 01/15/18 19:44 CJR 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 6 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 6 of 98 ONE LAB. NATIONWIDE.CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All radiochemical sample results for solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet weight was requested by the client. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. [Preliminary Report] Heather J Wagner Technical Service Representative 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 7 of 98 Heather J Wagner Technical Service Representative ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 7 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L963090 BF1 0.3-1.5 Collected date/time: 01/11/18 08:30 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 75.0 1 01/17/2018 09:47 WG1063379 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0360 B 0.00373 0.0267 1 01/17/2018 20:43 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic U 0.867 2.67 1 01/16/2018 02:12 WG1062607 Barium 75.5 0.227 0.667 1 01/16/2018 02:12 WG1062607 Cadmium U 0.0934 0.667 1 01/16/2018 02:12 WG1062607 Chromium 143 0.187 1.33 1 01/16/2018 02:12 WG1062607 Lead 3.67 0.253 0.667 1 01/16/2018 02:12 WG1062607 Selenium U 0.987 2.67 1 01/16/2018 02:12 WG1062607 Silver U 0.373 1.33 1 01/16/2018 02:12 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0133 0.0667 1 01/14/2018 00:53 WG1062584 Acrylonitrile U 0.00239 0.0133 1 01/14/2018 00:53 WG1062584 Benzene U 0.000360 0.00133 1 01/14/2018 00:53 WG1062584 Bromobenzene U 0.000379 0.00133 1 01/14/2018 00:53 WG1062584 Bromodichloromethane U 0.000339 0.00133 1 01/14/2018 00:53 WG1062584 Bromoform U 0.000566 0.00133 1 01/14/2018 00:53 WG1062584 Bromomethane U 0.00179 0.00667 1 01/14/2018 00:53 WG1062584 n-Butylbenzene U 0.000344 0.00133 1 01/14/2018 00:53 WG1062584 sec-Butylbenzene U 0.000268 0.00133 1 01/14/2018 00:53 WG1062584 tert-Butylbenzene U 0.000275 0.00133 1 01/14/2018 00:53 WG1062584 Carbon tetrachloride U 0.000438 0.00133 1 01/14/2018 00:53 WG1062584 Chlorobenzene U 0.000283 0.00133 1 01/14/2018 00:53 WG1062584 Chlorodibromomethane U 0.000498 0.00133 1 01/14/2018 00:53 WG1062584 Chloroethane U 0.00126 0.00667 1 01/14/2018 00:53 WG1062584 Chloroform U 0.000305 0.00667 1 01/14/2018 00:53 WG1062584 Chloromethane U 0.000500 0.00333 1 01/14/2018 00:53 WG1062584 2-Chlorotoluene U 0.000402 0.00133 1 01/14/2018 00:53 WG1062584 4-Chlorotoluene U 0.000320 0.00133 1 01/14/2018 00:53 WG1062584 1,2-Dibromo-3-Chloropropane U 0.00140 0.00667 1 01/14/2018 00:53 WG1062584 1,2-Dibromoethane U 0.000458 0.00133 1 01/14/2018 00:53 WG1062584 Dibromomethane U 0.000510 0.00133 1 01/14/2018 00:53 WG1062584 1,2-Dichlorobenzene U 0.000407 0.00133 1 01/14/2018 00:53 WG1062584 1,3-Dichlorobenzene U 0.000319 0.00133 1 01/14/2018 00:53 WG1062584 1,4-Dichlorobenzene U 0.000301 0.00133 1 01/14/2018 00:53 WG1062584 Dichlorodifluoromethane U 0.000951 0.00667 1 01/14/2018 00:53 WG1062584 1,1-Dichloroethane U 0.000265 0.00133 1 01/14/2018 00:53 WG1062584 1,2-Dichloroethane U 0.000353 0.00133 1 01/14/2018 00:53 WG1062584 1,1-Dichloroethene U 0.000404 0.00133 1 01/14/2018 00:53 WG1062584 cis-1,2-Dichloroethene U 0.000313 0.00133 1 01/14/2018 00:53 WG1062584 trans-1,2-Dichloroethene U 0.000352 0.00133 1 01/14/2018 00:53 WG1062584 1,2-Dichloropropane U 0.000478 0.00133 1 01/14/2018 00:53 WG1062584 1,1-Dichloropropene U 0.000423 0.00133 1 01/14/2018 00:53 WG1062584 1,3-Dichloropropane U 0.000276 0.00133 1 01/14/2018 00:53 WG1062584 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 8 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 8 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L963090 BF1 0.3-1.5 Collected date/time: 01/11/18 08:30 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000349 0.00133 1 01/14/2018 00:53 WG1062584 trans-1,3-Dichloropropene U 0.000356 0.00133 1 01/14/2018 00:53 WG1062584 2,2-Dichloropropane U 0.000372 0.00133 1 01/14/2018 00:53 WG1062584 Di-isopropyl ether U 0.000331 0.00133 1 01/14/2018 00:53 WG1062584 Ethylbenzene U 0.000396 0.00133 1 01/14/2018 00:53 WG1062584 Hexachloro-1,3-butadiene U 0.000456 0.00133 1 01/14/2018 00:53 WG1062584 Isopropylbenzene U 0.000324 0.00133 1 01/14/2018 00:53 WG1062584 p-Isopropyltoluene U 0.000272 0.00133 1 01/14/2018 00:53 WG1062584 2-Butanone (MEK)U 0.00624 0.0133 1 01/14/2018 00:53 WG1062584 Methylene Chloride U 0.00133 0.00667 1 01/14/2018 00:53 WG1062584 4-Methyl-2-pentanone (MIBK)U 0.00251 0.0133 1 01/14/2018 00:53 WG1062584 Methyl tert-butyl ether U 0.000283 0.00133 1 01/14/2018 00:53 WG1062584 Naphthalene U 0.00133 0.00667 1 01/14/2018 00:53 WG1062584 n-Propylbenzene U 0.000275 0.00133 1 01/14/2018 00:53 WG1062584 Styrene U 0.000312 0.00133 1 01/14/2018 00:53 WG1062584 1,1,1,2-Tetrachloroethane U 0.000352 0.00133 1 01/14/2018 00:53 WG1062584 1,1,2,2-Tetrachloroethane U 0.000487 0.00133 1 01/14/2018 00:53 WG1062584 Tetrachloroethene U 0.000368 0.00133 1 01/14/2018 00:53 WG1062584 Toluene U 0.000579 0.00667 1 01/14/2018 00:53 WG1062584 1,2,3-Trichlorobenzene U 0.000408 0.00133 1 01/14/2018 00:53 WG1062584 1,2,4-Trichlorobenzene U 0.000518 0.00133 1 01/14/2018 00:53 WG1062584 1,1,1-Trichloroethane U 0.000382 0.00133 1 01/14/2018 00:53 WG1062584 1,1,2-Trichloroethane U 0.000369 0.00133 1 01/14/2018 00:53 WG1062584 1,1,2-Trichlorotrifluoroethane U 0.000487 0.00133 1 01/14/2018 00:53 WG1062584 Trichloroethene U 0.000372 0.00133 1 01/14/2018 00:53 WG1062584 Trichlorofluoromethane U J3 J4 0.000510 0.00667 1 01/14/2018 00:53 WG1062584 1,2,3-Trichloropropane U 0.000988 0.00333 1 01/14/2018 00:53 WG1062584 1,2,4-Trimethylbenzene U 0.000281 0.00133 1 01/14/2018 00:53 WG1062584 1,3,5-Trimethylbenzene U 0.000355 0.00133 1 01/14/2018 00:53 WG1062584 Vinyl chloride U 0.000388 0.00133 1 01/14/2018 00:53 WG1062584 Xylenes, Total U 0.000931 0.00400 1 01/14/2018 00:53 WG1062584 (S) Toluene-d8 99.8 80.0-120 01/14/2018 00:53 WG1062584 (S) Dibromofluoromethane 99.6 74.0-131 01/14/2018 00:53 WG1062584 (S) 4-Bromofluorobenzene 98.7 64.0-132 01/14/2018 00:53 WG1062584 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00856 0.0440 1 01/18/2018 20:53 WG1062710 Acenaphthylene U 0.00895 0.0440 1 01/18/2018 20:53 WG1062710 Anthracene U 0.00843 0.0440 1 01/18/2018 20:53 WG1062710 Benzidine U J4 0.0850 0.444 1 01/18/2018 20:53 WG1062710 Benzo(a)anthracene U 0.00571 0.0440 1 01/18/2018 20:53 WG1062710 Benzo(b)fluoranthene U 0.00927 0.0440 1 01/18/2018 20:53 WG1062710 Benzo(k)fluoranthene U 0.00776 0.0440 1 01/18/2018 20:53 WG1062710 Benzo(g,h,i)perylene U 0.00962 0.0440 1 01/18/2018 20:53 WG1062710 Benzo(a)pyrene U 0.00731 0.0440 1 01/18/2018 20:53 WG1062710 Bis(2-chlorethoxy)methane U 0.0103 0.444 1 01/18/2018 20:53 WG1062710 Bis(2-chloroethyl)ether U 0.0120 0.444 1 01/18/2018 20:53 WG1062710 Bis(2-chloroisopropyl)ether U 0.0101 0.444 1 01/18/2018 20:53 WG1062710 4-Bromophenyl-phenylether U 0.0152 0.444 1 01/18/2018 20:53 WG1062710 2-Chloronaphthalene U 0.00852 0.0440 1 01/18/2018 20:53 WG1062710 4-Chlorophenyl-phenylether U 0.00836 0.444 1 01/18/2018 20:53 WG1062710 Chrysene U 0.00740 0.0440 1 01/18/2018 20:53 WG1062710 Dibenz(a,h)anthracene U 0.0110 0.0440 1 01/18/2018 20:53 WG1062710 3,3-Dichlorobenzidine U 0.106 0.444 1 01/18/2018 20:53 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 9 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 9 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01 L963090 BF1 0.3-1.5 Collected date/time: 01/11/18 08:30 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00810 0.444 1 01/18/2018 20:53 WG1062710 2,6-Dinitrotoluene U 0.00983 0.444 1 01/18/2018 20:53 WG1062710 Fluoranthene U 0.00662 0.0440 1 01/18/2018 20:53 WG1062710 Fluorene U 0.00910 0.0440 1 01/18/2018 20:53 WG1062710 Hexachlorobenzene U 0.0114 0.444 1 01/18/2018 20:53 WG1062710 Hexachloro-1,3-butadiene U 0.0133 0.444 1 01/18/2018 20:53 WG1062710 Hexachlorocyclopentadiene U J0 0.0783 0.444 1 01/18/2018 20:53 WG1062710 Hexachloroethane U 0.0179 0.444 1 01/18/2018 20:53 WG1062710 Indeno(1,2,3-cd)pyrene U 0.0103 0.0440 1 01/18/2018 20:53 WG1062710 Isophorone U 0.00696 0.444 1 01/18/2018 20:53 WG1062710 Naphthalene U 0.0119 0.0440 1 01/18/2018 20:53 WG1062710 Nitrobenzene U 0.00927 0.444 1 01/18/2018 20:53 WG1062710 n-Nitrosodimethylamine U 0.0863 0.444 1 01/18/2018 20:53 WG1062710 n-Nitrosodiphenylamine U 0.00792 0.444 1 01/18/2018 20:53 WG1062710 n-Nitrosodi-n-propylamine U 0.0121 0.444 1 01/18/2018 20:53 WG1062710 Phenanthrene U 0.00704 0.0440 1 01/18/2018 20:53 WG1062710 Benzylbutyl phthalate U 0.0137 0.444 1 01/18/2018 20:53 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0160 0.444 1 01/18/2018 20:53 WG1062710 Di-n-butyl phthalate U 0.0145 0.444 1 01/18/2018 20:53 WG1062710 Diethyl phthalate U 0.00922 0.444 1 01/18/2018 20:53 WG1062710 Dimethyl phthalate U 0.00720 0.444 1 01/18/2018 20:53 WG1062710 Di-n-octyl phthalate U 0.0121 0.444 1 01/18/2018 20:53 WG1062710 Pyrene U 0.0164 0.0440 1 01/18/2018 20:53 WG1062710 1,2,4-Trichlorobenzene U 0.0117 0.444 1 01/18/2018 20:53 WG1062710 4-Chloro-3-methylphenol U 0.00636 0.444 1 01/18/2018 20:53 WG1062710 2-Chlorophenol U 0.0111 0.444 1 01/18/2018 20:53 WG1062710 2,4-Dichlorophenol U 0.00995 0.444 1 01/18/2018 20:53 WG1062710 2,4-Dimethylphenol U 0.0628 0.444 1 01/18/2018 20:53 WG1062710 4,6-Dinitro-2-methylphenol U 0.165 0.444 1 01/18/2018 20:53 WG1062710 2,4-Dinitrophenol U 0.131 0.444 1 01/18/2018 20:53 WG1062710 2-Nitrophenol U 0.0173 0.444 1 01/18/2018 20:53 WG1062710 4-Nitrophenol U J0 0.0700 0.444 1 01/18/2018 20:53 WG1062710 Pentachlorophenol U 0.0640 0.444 1 01/18/2018 20:53 WG1062710 Phenol U 0.00927 0.444 1 01/18/2018 20:53 WG1062710 2,4,6-Trichlorophenol U 0.0104 0.444 1 01/18/2018 20:53 WG1062710 (S) 2-Fluorophenol 53.4 20.0-120 01/18/2018 20:53 WG1062710 (S) Phenol-d5 50.4 20.0-120 01/18/2018 20:53 WG1062710 (S) Nitrobenzene-d5 44.8 18.0-125 01/18/2018 20:53 WG1062710 (S) 2-Fluorobiphenyl 51.0 28.0-120 01/18/2018 20:53 WG1062710 (S) 2,4,6-Tribromophenol 81.2 17.0-137 01/18/2018 20:53 WG1062710 (S) p-Terphenyl-d14 54.4 13.0-131 01/18/2018 20:53 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 10 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 10 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L963090 BF2 2-4 Collected date/time: 01/11/18 11:50 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 86.2 1 01/17/2018 09:47 WG1063379 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0398 B 0.00325 0.0232 1 01/17/2018 20:58 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 2.00 J 0.754 2.32 1 01/16/2018 02:28 WG1062607 Barium 97.6 0.197 0.580 1 01/16/2018 02:28 WG1062607 Cadmium U 0.0812 0.580 1 01/16/2018 02:28 WG1062607 Chromium 14.5 0.162 1.16 1 01/16/2018 02:28 WG1062607 Lead 8.57 0.221 0.580 1 01/16/2018 02:28 WG1062607 Selenium U 0.859 2.32 1 01/16/2018 02:28 WG1062607 Silver U 0.325 1.16 1 01/16/2018 02:28 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0116 0.0580 1 01/14/2018 01:12 WG1062584 Acrylonitrile U 0.00208 0.0116 1 01/14/2018 01:12 WG1062584 Benzene U 0.000313 0.00116 1 01/14/2018 01:12 WG1062584 Bromobenzene U 0.000330 0.00116 1 01/14/2018 01:12 WG1062584 Bromodichloromethane U 0.000295 0.00116 1 01/14/2018 01:12 WG1062584 Bromoform U 0.000492 0.00116 1 01/14/2018 01:12 WG1062584 Bromomethane U 0.00156 0.00580 1 01/14/2018 01:12 WG1062584 n-Butylbenzene U 0.000299 0.00116 1 01/14/2018 01:12 WG1062584 sec-Butylbenzene U 0.000233 0.00116 1 01/14/2018 01:12 WG1062584 tert-Butylbenzene U 0.000239 0.00116 1 01/14/2018 01:12 WG1062584 Carbon tetrachloride U 0.000381 0.00116 1 01/14/2018 01:12 WG1062584 Chlorobenzene U 0.000246 0.00116 1 01/14/2018 01:12 WG1062584 Chlorodibromomethane U 0.000433 0.00116 1 01/14/2018 01:12 WG1062584 Chloroethane U 0.00110 0.00580 1 01/14/2018 01:12 WG1062584 Chloroform U 0.000266 0.00580 1 01/14/2018 01:12 WG1062584 Chloromethane U 0.000435 0.00290 1 01/14/2018 01:12 WG1062584 2-Chlorotoluene U 0.000349 0.00116 1 01/14/2018 01:12 WG1062584 4-Chlorotoluene U 0.000279 0.00116 1 01/14/2018 01:12 WG1062584 1,2-Dibromo-3-Chloropropane U 0.00122 0.00580 1 01/14/2018 01:12 WG1062584 1,2-Dibromoethane U 0.000398 0.00116 1 01/14/2018 01:12 WG1062584 Dibromomethane U 0.000443 0.00116 1 01/14/2018 01:12 WG1062584 1,2-Dichlorobenzene U 0.000354 0.00116 1 01/14/2018 01:12 WG1062584 1,3-Dichlorobenzene U 0.000277 0.00116 1 01/14/2018 01:12 WG1062584 1,4-Dichlorobenzene U 0.000262 0.00116 1 01/14/2018 01:12 WG1062584 Dichlorodifluoromethane U 0.000827 0.00580 1 01/14/2018 01:12 WG1062584 1,1-Dichloroethane U 0.000231 0.00116 1 01/14/2018 01:12 WG1062584 1,2-Dichloroethane U 0.000308 0.00116 1 01/14/2018 01:12 WG1062584 1,1-Dichloroethene U 0.000352 0.00116 1 01/14/2018 01:12 WG1062584 cis-1,2-Dichloroethene U 0.000273 0.00116 1 01/14/2018 01:12 WG1062584 trans-1,2-Dichloroethene U 0.000306 0.00116 1 01/14/2018 01:12 WG1062584 1,2-Dichloropropane U 0.000415 0.00116 1 01/14/2018 01:12 WG1062584 1,1-Dichloropropene U 0.000368 0.00116 1 01/14/2018 01:12 WG1062584 1,3-Dichloropropane U 0.000240 0.00116 1 01/14/2018 01:12 WG1062584 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 11 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 11 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L963090 BF2 2-4 Collected date/time: 01/11/18 11:50 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000304 0.00116 1 01/14/2018 01:12 WG1062584 trans-1,3-Dichloropropene U 0.000310 0.00116 1 01/14/2018 01:12 WG1062584 2,2-Dichloropropane U 0.000324 0.00116 1 01/14/2018 01:12 WG1062584 Di-isopropyl ether U 0.000288 0.00116 1 01/14/2018 01:12 WG1062584 Ethylbenzene U 0.000345 0.00116 1 01/14/2018 01:12 WG1062584 Hexachloro-1,3-butadiene U 0.000397 0.00116 1 01/14/2018 01:12 WG1062584 Isopropylbenzene U 0.000282 0.00116 1 01/14/2018 01:12 WG1062584 p-Isopropyltoluene U 0.000237 0.00116 1 01/14/2018 01:12 WG1062584 2-Butanone (MEK)U 0.00543 0.0116 1 01/14/2018 01:12 WG1062584 Methylene Chloride U 0.00116 0.00580 1 01/14/2018 01:12 WG1062584 4-Methyl-2-pentanone (MIBK)U 0.00218 0.0116 1 01/14/2018 01:12 WG1062584 Methyl tert-butyl ether U 0.000246 0.00116 1 01/14/2018 01:12 WG1062584 Naphthalene U 0.00116 0.00580 1 01/14/2018 01:12 WG1062584 n-Propylbenzene U 0.000239 0.00116 1 01/14/2018 01:12 WG1062584 Styrene U 0.000272 0.00116 1 01/14/2018 01:12 WG1062584 1,1,1,2-Tetrachloroethane U 0.000306 0.00116 1 01/14/2018 01:12 WG1062584 1,1,2,2-Tetrachloroethane U 0.000424 0.00116 1 01/14/2018 01:12 WG1062584 Tetrachloroethene U 0.000320 0.00116 1 01/14/2018 01:12 WG1062584 Toluene U 0.000504 0.00580 1 01/14/2018 01:12 WG1062584 1,2,3-Trichlorobenzene U 0.000355 0.00116 1 01/14/2018 01:12 WG1062584 1,2,4-Trichlorobenzene U 0.000450 0.00116 1 01/14/2018 01:12 WG1062584 1,1,1-Trichloroethane U 0.000332 0.00116 1 01/14/2018 01:12 WG1062584 1,1,2-Trichloroethane U 0.000321 0.00116 1 01/14/2018 01:12 WG1062584 1,1,2-Trichlorotrifluoroethane U 0.000424 0.00116 1 01/14/2018 01:12 WG1062584 Trichloroethene U 0.000324 0.00116 1 01/14/2018 01:12 WG1062584 Trichlorofluoromethane U J3 J4 0.000443 0.00580 1 01/14/2018 01:12 WG1062584 1,2,3-Trichloropropane U 0.000860 0.00290 1 01/14/2018 01:12 WG1062584 1,2,4-Trimethylbenzene U 0.000245 0.00116 1 01/14/2018 01:12 WG1062584 1,3,5-Trimethylbenzene U 0.000309 0.00116 1 01/14/2018 01:12 WG1062584 Vinyl chloride U 0.000338 0.00116 1 01/14/2018 01:12 WG1062584 Xylenes, Total U 0.000810 0.00348 1 01/14/2018 01:12 WG1062584 (S) Toluene-d8 98.3 80.0-120 01/14/2018 01:12 WG1062584 (S) Dibromofluoromethane 98.9 74.0-131 01/14/2018 01:12 WG1062584 (S) 4-Bromofluorobenzene 100 64.0-132 01/14/2018 01:12 WG1062584 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00745 0.0383 1 01/18/2018 21:16 WG1062710 Acenaphthylene U 0.00779 0.0383 1 01/18/2018 21:16 WG1062710 Anthracene U 0.00733 0.0383 1 01/18/2018 21:16 WG1062710 Benzidine U J4 0.0739 0.386 1 01/18/2018 21:16 WG1062710 Benzo(a)anthracene U 0.00497 0.0383 1 01/18/2018 21:16 WG1062710 Benzo(b)fluoranthene U 0.00807 0.0383 1 01/18/2018 21:16 WG1062710 Benzo(k)fluoranthene U 0.00675 0.0383 1 01/18/2018 21:16 WG1062710 Benzo(g,h,i)perylene U 0.00837 0.0383 1 01/18/2018 21:16 WG1062710 Benzo(a)pyrene U 0.00636 0.0383 1 01/18/2018 21:16 WG1062710 Bis(2-chlorethoxy)methane U 0.00894 0.386 1 01/18/2018 21:16 WG1062710 Bis(2-chloroethyl)ether U 0.0104 0.386 1 01/18/2018 21:16 WG1062710 Bis(2-chloroisopropyl)ether U 0.00882 0.386 1 01/18/2018 21:16 WG1062710 4-Bromophenyl-phenylether U 0.0132 0.386 1 01/18/2018 21:16 WG1062710 2-Chloronaphthalene U 0.00742 0.0383 1 01/18/2018 21:16 WG1062710 4-Chlorophenyl-phenylether U 0.00728 0.386 1 01/18/2018 21:16 WG1062710 Chrysene U 0.00644 0.0383 1 01/18/2018 21:16 WG1062710 Dibenz(a,h)anthracene U 0.00953 0.0383 1 01/18/2018 21:16 WG1062710 3,3-Dichlorobenzidine U 0.0921 0.386 1 01/18/2018 21:16 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 12 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 12 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02 L963090 BF2 2-4 Collected date/time: 01/11/18 11:50 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00704 0.386 1 01/18/2018 21:16 WG1062710 2,6-Dinitrotoluene U 0.00855 0.386 1 01/18/2018 21:16 WG1062710 Fluoranthene U 0.00576 0.0383 1 01/18/2018 21:16 WG1062710 Fluorene U 0.00792 0.0383 1 01/18/2018 21:16 WG1062710 Hexachlorobenzene U 0.00993 0.386 1 01/18/2018 21:16 WG1062710 Hexachloro-1,3-butadiene U 0.0116 0.386 1 01/18/2018 21:16 WG1062710 Hexachlorocyclopentadiene U J0 0.0681 0.386 1 01/18/2018 21:16 WG1062710 Hexachloroethane U 0.0156 0.386 1 01/18/2018 21:16 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00896 0.0383 1 01/18/2018 21:16 WG1062710 Isophorone U 0.00606 0.386 1 01/18/2018 21:16 WG1062710 Naphthalene U 0.0103 0.0383 1 01/18/2018 21:16 WG1062710 Nitrobenzene U 0.00807 0.386 1 01/18/2018 21:16 WG1062710 n-Nitrosodimethylamine U 0.0751 0.386 1 01/18/2018 21:16 WG1062710 n-Nitrosodiphenylamine U 0.00689 0.386 1 01/18/2018 21:16 WG1062710 n-Nitrosodi-n-propylamine U 0.0105 0.386 1 01/18/2018 21:16 WG1062710 Phenanthrene U 0.00613 0.0383 1 01/18/2018 21:16 WG1062710 Benzylbutyl phthalate U 0.0120 0.386 1 01/18/2018 21:16 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0139 0.386 1 01/18/2018 21:16 WG1062710 Di-n-butyl phthalate U 0.0127 0.386 1 01/18/2018 21:16 WG1062710 Diethyl phthalate U 0.00802 0.386 1 01/18/2018 21:16 WG1062710 Dimethyl phthalate U 0.00627 0.386 1 01/18/2018 21:16 WG1062710 Di-n-octyl phthalate U 0.0105 0.386 1 01/18/2018 21:16 WG1062710 Pyrene U 0.0143 0.0383 1 01/18/2018 21:16 WG1062710 1,2,4-Trichlorobenzene U 0.0102 0.386 1 01/18/2018 21:16 WG1062710 4-Chloro-3-methylphenol U 0.00554 0.386 1 01/18/2018 21:16 WG1062710 2-Chlorophenol U 0.00964 0.386 1 01/18/2018 21:16 WG1062710 2,4-Dichlorophenol U 0.00866 0.386 1 01/18/2018 21:16 WG1062710 2,4-Dimethylphenol U 0.0547 0.386 1 01/18/2018 21:16 WG1062710 4,6-Dinitro-2-methylphenol U 0.144 0.386 1 01/18/2018 21:16 WG1062710 2,4-Dinitrophenol U 0.114 0.386 1 01/18/2018 21:16 WG1062710 2-Nitrophenol U 0.0151 0.386 1 01/18/2018 21:16 WG1062710 4-Nitrophenol U J0 0.0609 0.386 1 01/18/2018 21:16 WG1062710 Pentachlorophenol U 0.0557 0.386 1 01/18/2018 21:16 WG1062710 Phenol U 0.00807 0.386 1 01/18/2018 21:16 WG1062710 2,4,6-Trichlorophenol U 0.00904 0.386 1 01/18/2018 21:16 WG1062710 (S) 2-Fluorophenol 48.2 20.0-120 01/18/2018 21:16 WG1062710 (S) Phenol-d5 45.4 20.0-120 01/18/2018 21:16 WG1062710 (S) Nitrobenzene-d5 38.8 18.0-125 01/18/2018 21:16 WG1062710 (S) 2-Fluorobiphenyl 47.0 28.0-120 01/18/2018 21:16 WG1062710 (S) 2,4,6-Tribromophenol 79.0 17.0-137 01/18/2018 21:16 WG1062710 (S) p-Terphenyl-d14 51.6 13.0-131 01/18/2018 21:16 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 13 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 13 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03 L963090 BF3 2-4 Collected date/time: 01/11/18 12:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 85.0 1 01/17/2018 09:47 WG1063379 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0454 B 0.00329 0.0235 1 01/17/2018 21:00 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.72 J 0.764 2.35 1 01/16/2018 02:31 WG1062607 Barium 99.4 0.200 0.588 1 01/16/2018 02:31 WG1062607 Cadmium U 0.0823 0.588 1 01/16/2018 02:31 WG1062607 Chromium 28.3 0.165 1.18 1 01/16/2018 02:31 WG1062607 Lead 11.6 0.223 0.588 1 01/16/2018 02:31 WG1062607 Selenium U 0.870 2.35 1 01/16/2018 02:31 WG1062607 Silver U 0.329 1.18 1 01/16/2018 02:31 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0118 0.0588 1 01/14/2018 08:33 WG1062584 Acrylonitrile U 0.00210 0.0118 1 01/14/2018 08:33 WG1062584 Benzene U 0.000317 0.00118 1 01/14/2018 08:33 WG1062584 Bromobenzene U 0.000334 0.00118 1 01/14/2018 08:33 WG1062584 Bromodichloromethane U 0.000299 0.00118 1 01/14/2018 08:33 WG1062584 Bromoform U 0.000499 0.00118 1 01/14/2018 08:33 WG1062584 Bromomethane U 0.00158 0.00588 1 01/14/2018 08:33 WG1062584 n-Butylbenzene U 0.000303 0.00118 1 01/14/2018 08:33 WG1062584 sec-Butylbenzene U 0.000236 0.00118 1 01/14/2018 08:33 WG1062584 tert-Butylbenzene U 0.000242 0.00118 1 01/14/2018 08:33 WG1062584 Carbon tetrachloride U 0.000386 0.00118 1 01/14/2018 08:33 WG1062584 Chlorobenzene U 0.000249 0.00118 1 01/14/2018 08:33 WG1062584 Chlorodibromomethane U 0.000439 0.00118 1 01/14/2018 08:33 WG1062584 Chloroethane U 0.00111 0.00588 1 01/14/2018 08:33 WG1062584 Chloroform U 0.000269 0.00588 1 01/14/2018 08:33 WG1062584 Chloromethane U 0.000441 0.00294 1 01/14/2018 08:33 WG1062584 2-Chlorotoluene U 0.000354 0.00118 1 01/14/2018 08:33 WG1062584 4-Chlorotoluene U 0.000282 0.00118 1 01/14/2018 08:33 WG1062584 1,2-Dibromo-3-Chloropropane U 0.00123 0.00588 1 01/14/2018 08:33 WG1062584 1,2-Dibromoethane U 0.000403 0.00118 1 01/14/2018 08:33 WG1062584 Dibromomethane U 0.000449 0.00118 1 01/14/2018 08:33 WG1062584 1,2-Dichlorobenzene U 0.000359 0.00118 1 01/14/2018 08:33 WG1062584 1,3-Dichlorobenzene U 0.000281 0.00118 1 01/14/2018 08:33 WG1062584 1,4-Dichlorobenzene U 0.000266 0.00118 1 01/14/2018 08:33 WG1062584 Dichlorodifluoromethane U 0.000838 0.00588 1 01/14/2018 08:33 WG1062584 1,1-Dichloroethane U 0.000234 0.00118 1 01/14/2018 08:33 WG1062584 1,2-Dichloroethane U 0.000312 0.00118 1 01/14/2018 08:33 WG1062584 1,1-Dichloroethene U 0.000356 0.00118 1 01/14/2018 08:33 WG1062584 cis-1,2-Dichloroethene U 0.000276 0.00118 1 01/14/2018 08:33 WG1062584 trans-1,2-Dichloroethene U 0.000310 0.00118 1 01/14/2018 08:33 WG1062584 1,2-Dichloropropane U 0.000421 0.00118 1 01/14/2018 08:33 WG1062584 1,1-Dichloropropene U 0.000373 0.00118 1 01/14/2018 08:33 WG1062584 1,3-Dichloropropane U 0.000243 0.00118 1 01/14/2018 08:33 WG1062584 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 14 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 14 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03 L963090 BF3 2-4 Collected date/time: 01/11/18 12:00 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000308 0.00118 1 01/14/2018 08:33 WG1062584 trans-1,3-Dichloropropene U 0.000314 0.00118 1 01/14/2018 08:33 WG1062584 2,2-Dichloropropane U 0.000328 0.00118 1 01/14/2018 08:33 WG1062584 Di-isopropyl ether U 0.000292 0.00118 1 01/14/2018 08:33 WG1062584 Ethylbenzene U 0.000349 0.00118 1 01/14/2018 08:33 WG1062584 Hexachloro-1,3-butadiene U 0.000402 0.00118 1 01/14/2018 08:33 WG1062584 Isopropylbenzene U 0.000286 0.00118 1 01/14/2018 08:33 WG1062584 p-Isopropyltoluene U 0.000240 0.00118 1 01/14/2018 08:33 WG1062584 2-Butanone (MEK)U 0.00550 0.0118 1 01/14/2018 08:33 WG1062584 Methylene Chloride U 0.00118 0.00588 1 01/14/2018 08:33 WG1062584 4-Methyl-2-pentanone (MIBK)U 0.00221 0.0118 1 01/14/2018 08:33 WG1062584 Methyl tert-butyl ether U 0.000249 0.00118 1 01/14/2018 08:33 WG1062584 Naphthalene U 0.00118 0.00588 1 01/14/2018 08:33 WG1062584 n-Propylbenzene U 0.000242 0.00118 1 01/14/2018 08:33 WG1062584 Styrene U 0.000275 0.00118 1 01/14/2018 08:33 WG1062584 1,1,1,2-Tetrachloroethane U 0.000310 0.00118 1 01/14/2018 08:33 WG1062584 1,1,2,2-Tetrachloroethane U 0.000429 0.00118 1 01/14/2018 08:33 WG1062584 Tetrachloroethene U 0.000325 0.00118 1 01/14/2018 08:33 WG1062584 Toluene U 0.000510 0.00588 1 01/14/2018 08:33 WG1062584 1,2,3-Trichlorobenzene U 0.000360 0.00118 1 01/14/2018 08:33 WG1062584 1,2,4-Trichlorobenzene U 0.000456 0.00118 1 01/14/2018 08:33 WG1062584 1,1,1-Trichloroethane U 0.000336 0.00118 1 01/14/2018 08:33 WG1062584 1,1,2-Trichloroethane U 0.000326 0.00118 1 01/14/2018 08:33 WG1062584 1,1,2-Trichlorotrifluoroethane U 0.000429 0.00118 1 01/14/2018 08:33 WG1062584 Trichloroethene U 0.000328 0.00118 1 01/14/2018 08:33 WG1062584 Trichlorofluoromethane U J3 J4 0.000449 0.00588 1 01/14/2018 08:33 WG1062584 1,2,3-Trichloropropane U 0.000871 0.00294 1 01/14/2018 08:33 WG1062584 1,2,4-Trimethylbenzene U 0.000248 0.00118 1 01/14/2018 08:33 WG1062584 1,3,5-Trimethylbenzene U 0.000313 0.00118 1 01/14/2018 08:33 WG1062584 Vinyl chloride U 0.000342 0.00118 1 01/14/2018 08:33 WG1062584 Xylenes, Total U 0.000821 0.00353 1 01/14/2018 08:33 WG1062584 (S) Toluene-d8 96.2 80.0-120 01/14/2018 08:33 WG1062584 (S) Dibromofluoromethane 105 74.0-131 01/14/2018 08:33 WG1062584 (S) 4-Bromofluorobenzene 97.7 64.0-132 01/14/2018 08:33 WG1062584 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00755 0.0388 1 01/18/2018 21:40 WG1062710 Acenaphthylene U 0.00789 0.0388 1 01/18/2018 21:40 WG1062710 Anthracene U 0.00743 0.0388 1 01/18/2018 21:40 WG1062710 Benzidine U J4 0.0749 0.392 1 01/18/2018 21:40 WG1062710 Benzo(a)anthracene U 0.00503 0.0388 1 01/18/2018 21:40 WG1062710 Benzo(b)fluoranthene U 0.00817 0.0388 1 01/18/2018 21:40 WG1062710 Benzo(k)fluoranthene U 0.00684 0.0388 1 01/18/2018 21:40 WG1062710 Benzo(g,h,i)perylene U 0.00848 0.0388 1 01/18/2018 21:40 WG1062710 Benzo(a)pyrene U 0.00644 0.0388 1 01/18/2018 21:40 WG1062710 Bis(2-chlorethoxy)methane U 0.00905 0.392 1 01/18/2018 21:40 WG1062710 Bis(2-chloroethyl)ether U 0.0105 0.392 1 01/18/2018 21:40 WG1062710 Bis(2-chloroisopropyl)ether U 0.00894 0.392 1 01/18/2018 21:40 WG1062710 4-Bromophenyl-phenylether U 0.0134 0.392 1 01/18/2018 21:40 WG1062710 2-Chloronaphthalene U 0.00751 0.0388 1 01/18/2018 21:40 WG1062710 4-Chlorophenyl-phenylether U 0.00737 0.392 1 01/18/2018 21:40 WG1062710 Chrysene U 0.00653 0.0388 1 01/18/2018 21:40 WG1062710 Dibenz(a,h)anthracene U 0.00965 0.0388 1 01/18/2018 21:40 WG1062710 3,3-Dichlorobenzidine U 0.0934 0.392 1 01/18/2018 21:40 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 15 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 15 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03 L963090 BF3 2-4 Collected date/time: 01/11/18 12:00 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00714 0.392 1 01/18/2018 21:40 WG1062710 2,6-Dinitrotoluene U 0.00867 0.392 1 01/18/2018 21:40 WG1062710 Fluoranthene U 0.00583 0.0388 1 01/18/2018 21:40 WG1062710 Fluorene U 0.00802 0.0388 1 01/18/2018 21:40 WG1062710 Hexachlorobenzene U 0.0101 0.392 1 01/18/2018 21:40 WG1062710 Hexachloro-1,3-butadiene U 0.0118 0.392 1 01/18/2018 21:40 WG1062710 Hexachlorocyclopentadiene U J0 0.0690 0.392 1 01/18/2018 21:40 WG1062710 Hexachloroethane U 0.0158 0.392 1 01/18/2018 21:40 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00908 0.0388 1 01/18/2018 21:40 WG1062710 Isophorone U 0.00614 0.392 1 01/18/2018 21:40 WG1062710 Naphthalene U 0.0105 0.0388 1 01/18/2018 21:40 WG1062710 Nitrobenzene U 0.00817 0.392 1 01/18/2018 21:40 WG1062710 n-Nitrosodimethylamine U 0.0761 0.392 1 01/18/2018 21:40 WG1062710 n-Nitrosodiphenylamine U 0.00698 0.392 1 01/18/2018 21:40 WG1062710 n-Nitrosodi-n-propylamine U 0.0107 0.392 1 01/18/2018 21:40 WG1062710 Phenanthrene U 0.00621 0.0388 1 01/18/2018 21:40 WG1062710 Benzylbutyl phthalate U 0.0121 0.392 1 01/18/2018 21:40 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0141 0.392 1 01/18/2018 21:40 WG1062710 Di-n-butyl phthalate U 0.0128 0.392 1 01/18/2018 21:40 WG1062710 Diethyl phthalate U 0.00813 0.392 1 01/18/2018 21:40 WG1062710 Dimethyl phthalate U 0.00635 0.392 1 01/18/2018 21:40 WG1062710 Di-n-octyl phthalate U 0.0107 0.392 1 01/18/2018 21:40 WG1062710 Pyrene U 0.0145 0.0388 1 01/18/2018 21:40 WG1062710 1,2,4-Trichlorobenzene U 0.0103 0.392 1 01/18/2018 21:40 WG1062710 4-Chloro-3-methylphenol U 0.00561 0.392 1 01/18/2018 21:40 WG1062710 2-Chlorophenol U 0.00977 0.392 1 01/18/2018 21:40 WG1062710 2,4-Dichlorophenol U 0.00877 0.392 1 01/18/2018 21:40 WG1062710 2,4-Dimethylphenol U 0.0554 0.392 1 01/18/2018 21:40 WG1062710 4,6-Dinitro-2-methylphenol U 0.146 0.392 1 01/18/2018 21:40 WG1062710 2,4-Dinitrophenol U 0.115 0.392 1 01/18/2018 21:40 WG1062710 2-Nitrophenol U 0.0153 0.392 1 01/18/2018 21:40 WG1062710 4-Nitrophenol U J0 0.0617 0.392 1 01/18/2018 21:40 WG1062710 Pentachlorophenol U 0.0564 0.392 1 01/18/2018 21:40 WG1062710 Phenol U 0.00817 0.392 1 01/18/2018 21:40 WG1062710 2,4,6-Trichlorophenol U 0.00916 0.392 1 01/18/2018 21:40 WG1062710 (S) 2-Fluorophenol 71.2 20.0-120 01/18/2018 21:40 WG1062710 (S) Phenol-d5 63.2 20.0-120 01/18/2018 21:40 WG1062710 (S) Nitrobenzene-d5 55.4 18.0-125 01/18/2018 21:40 WG1062710 (S) 2-Fluorobiphenyl 62.2 28.0-120 01/18/2018 21:40 WG1062710 (S) 2,4,6-Tribromophenol 90.2 17.0-137 01/18/2018 21:40 WG1062710 (S) p-Terphenyl-d14 57.4 13.0-131 01/18/2018 21:40 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 16 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 16 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04 L963090 BF4 2-4 Collected date/time: 01/11/18 12:10 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 81.5 1 01/17/2018 09:47 WG1063379 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0353 B 0.00344 0.0245 1 01/17/2018 21:03 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.09 J 0.798 2.45 1 01/16/2018 02:41 WG1062607 Barium 72.2 0.209 0.614 1 01/16/2018 02:41 WG1062607 Cadmium U 0.0859 0.614 1 01/16/2018 02:41 WG1062607 Chromium 22.9 0.172 1.23 1 01/16/2018 02:41 WG1062607 Lead 12.0 0.233 0.614 1 01/16/2018 02:41 WG1062607 Selenium U 0.908 2.45 1 01/16/2018 02:41 WG1062607 Silver U 0.344 1.23 1 01/16/2018 02:41 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.0225 J 0.0123 0.0614 1 01/14/2018 08:53 WG1062584 Acrylonitrile U 0.00220 0.0123 1 01/14/2018 08:53 WG1062584 Benzene U 0.000331 0.00123 1 01/14/2018 08:53 WG1062584 Bromobenzene U 0.000348 0.00123 1 01/14/2018 08:53 WG1062584 Bromodichloromethane U 0.000312 0.00123 1 01/14/2018 08:53 WG1062584 Bromoform U 0.000520 0.00123 1 01/14/2018 08:53 WG1062584 Bromomethane U 0.00164 0.00614 1 01/14/2018 08:53 WG1062584 n-Butylbenzene U 0.000317 0.00123 1 01/14/2018 08:53 WG1062584 sec-Butylbenzene U 0.000247 0.00123 1 01/14/2018 08:53 WG1062584 tert-Butylbenzene U 0.000253 0.00123 1 01/14/2018 08:53 WG1062584 Carbon tetrachloride U 0.000402 0.00123 1 01/14/2018 08:53 WG1062584 Chlorobenzene U 0.000260 0.00123 1 01/14/2018 08:53 WG1062584 Chlorodibromomethane U 0.000458 0.00123 1 01/14/2018 08:53 WG1062584 Chloroethane U 0.00116 0.00614 1 01/14/2018 08:53 WG1062584 Chloroform U 0.000281 0.00614 1 01/14/2018 08:53 WG1062584 Chloromethane U 0.000460 0.00307 1 01/14/2018 08:53 WG1062584 2-Chlorotoluene U 0.000369 0.00123 1 01/14/2018 08:53 WG1062584 4-Chlorotoluene U 0.000294 0.00123 1 01/14/2018 08:53 WG1062584 1,2-Dibromo-3-Chloropropane U 0.00129 0.00614 1 01/14/2018 08:53 WG1062584 1,2-Dibromoethane U 0.000421 0.00123 1 01/14/2018 08:53 WG1062584 Dibromomethane U 0.000469 0.00123 1 01/14/2018 08:53 WG1062584 1,2-Dichlorobenzene U 0.000374 0.00123 1 01/14/2018 08:53 WG1062584 1,3-Dichlorobenzene U 0.000293 0.00123 1 01/14/2018 08:53 WG1062584 1,4-Dichlorobenzene U 0.000277 0.00123 1 01/14/2018 08:53 WG1062584 Dichlorodifluoromethane U 0.000875 0.00614 1 01/14/2018 08:53 WG1062584 1,1-Dichloroethane U 0.000244 0.00123 1 01/14/2018 08:53 WG1062584 1,2-Dichloroethane U 0.000325 0.00123 1 01/14/2018 08:53 WG1062584 1,1-Dichloroethene U 0.000372 0.00123 1 01/14/2018 08:53 WG1062584 cis-1,2-Dichloroethene U 0.000288 0.00123 1 01/14/2018 08:53 WG1062584 trans-1,2-Dichloroethene U 0.000324 0.00123 1 01/14/2018 08:53 WG1062584 1,2-Dichloropropane U 0.000439 0.00123 1 01/14/2018 08:53 WG1062584 1,1-Dichloropropene U 0.000389 0.00123 1 01/14/2018 08:53 WG1062584 1,3-Dichloropropane U 0.000254 0.00123 1 01/14/2018 08:53 WG1062584 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 17 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 17 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04 L963090 BF4 2-4 Collected date/time: 01/11/18 12:10 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000321 0.00123 1 01/14/2018 08:53 WG1062584 trans-1,3-Dichloropropene U 0.000328 0.00123 1 01/14/2018 08:53 WG1062584 2,2-Dichloropropane U 0.000342 0.00123 1 01/14/2018 08:53 WG1062584 Di-isopropyl ether U 0.000304 0.00123 1 01/14/2018 08:53 WG1062584 Ethylbenzene U 0.000364 0.00123 1 01/14/2018 08:53 WG1062584 Hexachloro-1,3-butadiene U 0.000420 0.00123 1 01/14/2018 08:53 WG1062584 Isopropylbenzene U 0.000298 0.00123 1 01/14/2018 08:53 WG1062584 p-Isopropyltoluene U 0.000250 0.00123 1 01/14/2018 08:53 WG1062584 2-Butanone (MEK)U 0.00574 0.0123 1 01/14/2018 08:53 WG1062584 Methylene Chloride U 0.00123 0.00614 1 01/14/2018 08:53 WG1062584 4-Methyl-2-pentanone (MIBK)U 0.00231 0.0123 1 01/14/2018 08:53 WG1062584 Methyl tert-butyl ether U 0.000260 0.00123 1 01/14/2018 08:53 WG1062584 Naphthalene U 0.00123 0.00614 1 01/14/2018 08:53 WG1062584 n-Propylbenzene U 0.000253 0.00123 1 01/14/2018 08:53 WG1062584 Styrene U 0.000287 0.00123 1 01/14/2018 08:53 WG1062584 1,1,1,2-Tetrachloroethane U 0.000324 0.00123 1 01/14/2018 08:53 WG1062584 1,1,2,2-Tetrachloroethane U 0.000448 0.00123 1 01/14/2018 08:53 WG1062584 Tetrachloroethene U 0.000339 0.00123 1 01/14/2018 08:53 WG1062584 Toluene U 0.000533 0.00614 1 01/14/2018 08:53 WG1062584 1,2,3-Trichlorobenzene U 0.000375 0.00123 1 01/14/2018 08:53 WG1062584 1,2,4-Trichlorobenzene U 0.000476 0.00123 1 01/14/2018 08:53 WG1062584 1,1,1-Trichloroethane U 0.000351 0.00123 1 01/14/2018 08:53 WG1062584 1,1,2-Trichloroethane U 0.000340 0.00123 1 01/14/2018 08:53 WG1062584 1,1,2-Trichlorotrifluoroethane U 0.000448 0.00123 1 01/14/2018 08:53 WG1062584 Trichloroethene U 0.000342 0.00123 1 01/14/2018 08:53 WG1062584 Trichlorofluoromethane U J3 J4 0.000469 0.00614 1 01/14/2018 08:53 WG1062584 1,2,3-Trichloropropane U 0.000909 0.00307 1 01/14/2018 08:53 WG1062584 1,2,4-Trimethylbenzene U 0.000259 0.00123 1 01/14/2018 08:53 WG1062584 1,3,5-Trimethylbenzene U 0.000326 0.00123 1 01/14/2018 08:53 WG1062584 Vinyl chloride U 0.000357 0.00123 1 01/14/2018 08:53 WG1062584 Xylenes, Total U 0.000856 0.00368 1 01/14/2018 08:53 WG1062584 (S) Toluene-d8 98.6 80.0-120 01/14/2018 08:53 WG1062584 (S) Dibromofluoromethane 101 74.0-131 01/14/2018 08:53 WG1062584 (S) 4-Bromofluorobenzene 97.9 64.0-132 01/14/2018 08:53 WG1062584 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00788 0.0405 1 01/18/2018 22:03 WG1062710 Acenaphthylene U 0.00823 0.0405 1 01/18/2018 22:03 WG1062710 Anthracene U 0.00776 0.0405 1 01/18/2018 22:03 WG1062710 Benzidine U J4 0.0782 0.409 1 01/18/2018 22:03 WG1062710 Benzo(a)anthracene U 0.00525 0.0405 1 01/18/2018 22:03 WG1062710 Benzo(b)fluoranthene U 0.00853 0.0405 1 01/18/2018 22:03 WG1062710 Benzo(k)fluoranthene U 0.00714 0.0405 1 01/18/2018 22:03 WG1062710 Benzo(g,h,i)perylene U 0.00885 0.0405 1 01/18/2018 22:03 WG1062710 Benzo(a)pyrene U 0.00672 0.0405 1 01/18/2018 22:03 WG1062710 Bis(2-chlorethoxy)methane U 0.00945 0.409 1 01/18/2018 22:03 WG1062710 Bis(2-chloroethyl)ether U 0.0110 0.409 1 01/18/2018 22:03 WG1062710 Bis(2-chloroisopropyl)ether U 0.00933 0.409 1 01/18/2018 22:03 WG1062710 4-Bromophenyl-phenylether U 0.0140 0.409 1 01/18/2018 22:03 WG1062710 2-Chloronaphthalene U 0.00784 0.0405 1 01/18/2018 22:03 WG1062710 4-Chlorophenyl-phenylether U 0.00769 0.409 1 01/18/2018 22:03 WG1062710 Chrysene U 0.00681 0.0405 1 01/18/2018 22:03 WG1062710 Dibenz(a,h)anthracene U 0.0101 0.0405 1 01/18/2018 22:03 WG1062710 3,3-Dichlorobenzidine U 0.0974 0.409 1 01/18/2018 22:03 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 18 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 18 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04 L963090 BF4 2-4 Collected date/time: 01/11/18 12:10 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00745 0.409 1 01/18/2018 22:03 WG1062710 2,6-Dinitrotoluene U 0.00904 0.409 1 01/18/2018 22:03 WG1062710 Fluoranthene U 0.00609 0.0405 1 01/18/2018 22:03 WG1062710 Fluorene U 0.00837 0.0405 1 01/18/2018 22:03 WG1062710 Hexachlorobenzene U 0.0105 0.409 1 01/18/2018 22:03 WG1062710 Hexachloro-1,3-butadiene U 0.0123 0.409 1 01/18/2018 22:03 WG1062710 Hexachlorocyclopentadiene U J0 0.0720 0.409 1 01/18/2018 22:03 WG1062710 Hexachloroethane U 0.0164 0.409 1 01/18/2018 22:03 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00947 0.0405 1 01/18/2018 22:03 WG1062710 Isophorone U 0.00641 0.409 1 01/18/2018 22:03 WG1062710 Naphthalene U 0.0109 0.0405 1 01/18/2018 22:03 WG1062710 Nitrobenzene U 0.00853 0.409 1 01/18/2018 22:03 WG1062710 n-Nitrosodimethylamine U 0.0794 0.409 1 01/18/2018 22:03 WG1062710 n-Nitrosodiphenylamine U 0.00729 0.409 1 01/18/2018 22:03 WG1062710 n-Nitrosodi-n-propylamine U 0.0111 0.409 1 01/18/2018 22:03 WG1062710 Phenanthrene U 0.00648 0.0405 1 01/18/2018 22:03 WG1062710 Benzylbutyl phthalate U 0.0126 0.409 1 01/18/2018 22:03 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0147 0.409 1 01/18/2018 22:03 WG1062710 Di-n-butyl phthalate U 0.0134 0.409 1 01/18/2018 22:03 WG1062710 Diethyl phthalate U 0.00848 0.409 1 01/18/2018 22:03 WG1062710 Dimethyl phthalate U 0.00663 0.409 1 01/18/2018 22:03 WG1062710 Di-n-octyl phthalate U 0.0111 0.409 1 01/18/2018 22:03 WG1062710 Pyrene U 0.0151 0.0405 1 01/18/2018 22:03 WG1062710 1,2,4-Trichlorobenzene U 0.0107 0.409 1 01/18/2018 22:03 WG1062710 4-Chloro-3-methylphenol U 0.00585 0.409 1 01/18/2018 22:03 WG1062710 2-Chlorophenol U 0.0102 0.409 1 01/18/2018 22:03 WG1062710 2,4-Dichlorophenol U 0.00915 0.409 1 01/18/2018 22:03 WG1062710 2,4-Dimethylphenol U 0.0578 0.409 1 01/18/2018 22:03 WG1062710 4,6-Dinitro-2-methylphenol U 0.152 0.409 1 01/18/2018 22:03 WG1062710 2,4-Dinitrophenol U 0.120 0.409 1 01/18/2018 22:03 WG1062710 2-Nitrophenol U 0.0160 0.409 1 01/18/2018 22:03 WG1062710 4-Nitrophenol U J0 0.0644 0.409 1 01/18/2018 22:03 WG1062710 Pentachlorophenol U 0.0589 0.409 1 01/18/2018 22:03 WG1062710 Phenol U 0.00853 0.409 1 01/18/2018 22:03 WG1062710 2,4,6-Trichlorophenol U 0.00956 0.409 1 01/18/2018 22:03 WG1062710 (S) 2-Fluorophenol 69.2 20.0-120 01/18/2018 22:03 WG1062710 (S) Phenol-d5 61.4 20.0-120 01/18/2018 22:03 WG1062710 (S) Nitrobenzene-d5 54.8 18.0-125 01/18/2018 22:03 WG1062710 (S) 2-Fluorobiphenyl 61.0 28.0-120 01/18/2018 22:03 WG1062710 (S) 2,4,6-Tribromophenol 85.4 17.0-137 01/18/2018 22:03 WG1062710 (S) p-Terphenyl-d14 52.4 13.0-131 01/18/2018 22:03 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 19 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 19 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05 L963090 BF5 2-4 Collected date/time: 01/11/18 12:20 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 68.8 1 01/17/2018 09:47 WG1063379 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.106 0.00407 0.0291 1 01/17/2018 21:06 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic U 0.945 2.91 1 01/16/2018 02:44 WG1062607 Barium 41.7 0.247 0.727 1 01/16/2018 02:44 WG1062607 Cadmium 0.142 J 0.102 0.727 1 01/16/2018 02:44 WG1062607 Chromium 210 0.204 1.45 1 01/16/2018 02:44 WG1062607 Lead 7.52 0.276 0.727 1 01/16/2018 02:44 WG1062607 Selenium U 1.08 2.91 1 01/16/2018 02:44 WG1062607 Silver U 0.407 1.45 1 01/16/2018 02:44 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.0252 J 0.0145 0.0727 1 01/14/2018 09:13 WG1062584 Acrylonitrile U 0.00260 0.0145 1 01/14/2018 09:13 WG1062584 Benzene U 0.000393 0.00145 1 01/14/2018 09:13 WG1062584 Bromobenzene U 0.000413 0.00145 1 01/14/2018 09:13 WG1062584 Bromodichloromethane U 0.000369 0.00145 1 01/14/2018 09:13 WG1062584 Bromoform U 0.000617 0.00145 1 01/14/2018 09:13 WG1062584 Bromomethane U 0.00195 0.00727 1 01/14/2018 09:13 WG1062584 n-Butylbenzene U 0.000375 0.00145 1 01/14/2018 09:13 WG1062584 sec-Butylbenzene U 0.000292 0.00145 1 01/14/2018 09:13 WG1062584 tert-Butylbenzene U 0.000300 0.00145 1 01/14/2018 09:13 WG1062584 Carbon tetrachloride U 0.000477 0.00145 1 01/14/2018 09:13 WG1062584 Chlorobenzene U 0.000308 0.00145 1 01/14/2018 09:13 WG1062584 Chlorodibromomethane U 0.000542 0.00145 1 01/14/2018 09:13 WG1062584 Chloroethane U 0.00138 0.00727 1 01/14/2018 09:13 WG1062584 Chloroform U 0.000333 0.00727 1 01/14/2018 09:13 WG1062584 Chloromethane U 0.000545 0.00364 1 01/14/2018 09:13 WG1062584 2-Chlorotoluene U 0.000438 0.00145 1 01/14/2018 09:13 WG1062584 4-Chlorotoluene U 0.000349 0.00145 1 01/14/2018 09:13 WG1062584 1,2-Dibromo-3-Chloropropane U 0.00153 0.00727 1 01/14/2018 09:13 WG1062584 1,2-Dibromoethane U 0.000499 0.00145 1 01/14/2018 09:13 WG1062584 Dibromomethane U 0.000555 0.00145 1 01/14/2018 09:13 WG1062584 1,2-Dichlorobenzene U 0.000444 0.00145 1 01/14/2018 09:13 WG1062584 1,3-Dichlorobenzene U 0.000348 0.00145 1 01/14/2018 09:13 WG1062584 1,4-Dichlorobenzene U 0.000329 0.00145 1 01/14/2018 09:13 WG1062584 Dichlorodifluoromethane U 0.00104 0.00727 1 01/14/2018 09:13 WG1062584 1,1-Dichloroethane U 0.000289 0.00145 1 01/14/2018 09:13 WG1062584 1,2-Dichloroethane U 0.000385 0.00145 1 01/14/2018 09:13 WG1062584 1,1-Dichloroethene U 0.000441 0.00145 1 01/14/2018 09:13 WG1062584 cis-1,2-Dichloroethene U 0.000342 0.00145 1 01/14/2018 09:13 WG1062584 trans-1,2-Dichloroethene U 0.000384 0.00145 1 01/14/2018 09:13 WG1062584 1,2-Dichloropropane U 0.000521 0.00145 1 01/14/2018 09:13 WG1062584 1,1-Dichloropropene U 0.000461 0.00145 1 01/14/2018 09:13 WG1062584 1,3-Dichloropropane U 0.000301 0.00145 1 01/14/2018 09:13 WG1062584 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 20 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 20 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05 L963090 BF5 2-4 Collected date/time: 01/11/18 12:20 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000381 0.00145 1 01/14/2018 09:13 WG1062584 trans-1,3-Dichloropropene U 0.000388 0.00145 1 01/14/2018 09:13 WG1062584 2,2-Dichloropropane U 0.000406 0.00145 1 01/14/2018 09:13 WG1062584 Di-isopropyl ether U 0.000361 0.00145 1 01/14/2018 09:13 WG1062584 Ethylbenzene U 0.000432 0.00145 1 01/14/2018 09:13 WG1062584 Hexachloro-1,3-butadiene U 0.000497 0.00145 1 01/14/2018 09:13 WG1062584 Isopropylbenzene U 0.000353 0.00145 1 01/14/2018 09:13 WG1062584 p-Isopropyltoluene U 0.000297 0.00145 1 01/14/2018 09:13 WG1062584 2-Butanone (MEK)U 0.00681 0.0145 1 01/14/2018 09:13 WG1062584 Methylene Chloride U 0.00145 0.00727 1 01/14/2018 09:13 WG1062584 4-Methyl-2-pentanone (MIBK)U 0.00273 0.0145 1 01/14/2018 09:13 WG1062584 Methyl tert-butyl ether U 0.000308 0.00145 1 01/14/2018 09:13 WG1062584 Naphthalene U 0.00145 0.00727 1 01/14/2018 09:13 WG1062584 n-Propylbenzene U 0.000300 0.00145 1 01/14/2018 09:13 WG1062584 Styrene U 0.000340 0.00145 1 01/14/2018 09:13 WG1062584 1,1,1,2-Tetrachloroethane U 0.000384 0.00145 1 01/14/2018 09:13 WG1062584 1,1,2,2-Tetrachloroethane U 0.000531 0.00145 1 01/14/2018 09:13 WG1062584 Tetrachloroethene U 0.000401 0.00145 1 01/14/2018 09:13 WG1062584 Toluene U 0.000631 0.00727 1 01/14/2018 09:13 WG1062584 1,2,3-Trichlorobenzene U 0.000445 0.00145 1 01/14/2018 09:13 WG1062584 1,2,4-Trichlorobenzene U 0.000564 0.00145 1 01/14/2018 09:13 WG1062584 1,1,1-Trichloroethane U 0.000416 0.00145 1 01/14/2018 09:13 WG1062584 1,1,2-Trichloroethane U 0.000403 0.00145 1 01/14/2018 09:13 WG1062584 1,1,2-Trichlorotrifluoroethane U 0.000531 0.00145 1 01/14/2018 09:13 WG1062584 Trichloroethene U 0.000406 0.00145 1 01/14/2018 09:13 WG1062584 Trichlorofluoromethane U J3 J4 0.000555 0.00727 1 01/14/2018 09:13 WG1062584 1,2,3-Trichloropropane U 0.00108 0.00364 1 01/14/2018 09:13 WG1062584 1,2,4-Trimethylbenzene U 0.000307 0.00145 1 01/14/2018 09:13 WG1062584 1,3,5-Trimethylbenzene U 0.000387 0.00145 1 01/14/2018 09:13 WG1062584 Vinyl chloride U 0.000423 0.00145 1 01/14/2018 09:13 WG1062584 Xylenes, Total U 0.00101 0.00436 1 01/14/2018 09:13 WG1062584 (S) Toluene-d8 96.2 80.0-120 01/14/2018 09:13 WG1062584 (S) Dibromofluoromethane 102 74.0-131 01/14/2018 09:13 WG1062584 (S) 4-Bromofluorobenzene 98.2 64.0-132 01/14/2018 09:13 WG1062584 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00934 0.0480 1 01/18/2018 22:26 WG1062710 Acenaphthylene U 0.00976 0.0480 1 01/18/2018 22:26 WG1062710 Anthracene U 0.00919 0.0480 1 01/18/2018 22:26 WG1062710 Benzidine U J4 0.0926 0.484 1 01/18/2018 22:26 WG1062710 Benzo(a)anthracene U 0.00622 0.0480 1 01/18/2018 22:26 WG1062710 Benzo(b)fluoranthene U 0.0101 0.0480 1 01/18/2018 22:26 WG1062710 Benzo(k)fluoranthene U 0.00846 0.0480 1 01/18/2018 22:26 WG1062710 Benzo(g,h,i)perylene U 0.0105 0.0480 1 01/18/2018 22:26 WG1062710 Benzo(a)pyrene U 0.00797 0.0480 1 01/18/2018 22:26 WG1062710 Bis(2-chlorethoxy)methane U 0.0112 0.484 1 01/18/2018 22:26 WG1062710 Bis(2-chloroethyl)ether U 0.0130 0.484 1 01/18/2018 22:26 WG1062710 Bis(2-chloroisopropyl)ether U 0.0111 0.484 1 01/18/2018 22:26 WG1062710 4-Bromophenyl-phenylether U 0.0166 0.484 1 01/18/2018 22:26 WG1062710 2-Chloronaphthalene U 0.00929 0.0480 1 01/18/2018 22:26 WG1062710 4-Chlorophenyl-phenylether U 0.00912 0.484 1 01/18/2018 22:26 WG1062710 Chrysene U 0.00807 0.0480 1 01/18/2018 22:26 WG1062710 Dibenz(a,h)anthracene U 0.0119 0.0480 1 01/18/2018 22:26 WG1062710 3,3-Dichlorobenzidine U 0.115 0.484 1 01/18/2018 22:26 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 21 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 21 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05 L963090 BF5 2-4 Collected date/time: 01/11/18 12:20 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00883 0.484 1 01/18/2018 22:26 WG1062710 2,6-Dinitrotoluene U 0.0107 0.484 1 01/18/2018 22:26 WG1062710 Fluoranthene U 0.00721 0.0480 1 01/18/2018 22:26 WG1062710 Fluorene U 0.00992 0.0480 1 01/18/2018 22:26 WG1062710 Hexachlorobenzene U 0.0124 0.484 1 01/18/2018 22:26 WG1062710 Hexachloro-1,3-butadiene U 0.0145 0.484 1 01/18/2018 22:26 WG1062710 Hexachlorocyclopentadiene U J0 0.0854 0.484 1 01/18/2018 22:26 WG1062710 Hexachloroethane U 0.0195 0.484 1 01/18/2018 22:26 WG1062710 Indeno(1,2,3-cd)pyrene U 0.0112 0.0480 1 01/18/2018 22:26 WG1062710 Isophorone U 0.00759 0.484 1 01/18/2018 22:26 WG1062710 Naphthalene U 0.0129 0.0480 1 01/18/2018 22:26 WG1062710 Nitrobenzene U 0.0101 0.484 1 01/18/2018 22:26 WG1062710 n-Nitrosodimethylamine U 0.0941 0.484 1 01/18/2018 22:26 WG1062710 n-Nitrosodiphenylamine U 0.00864 0.484 1 01/18/2018 22:26 WG1062710 n-Nitrosodi-n-propylamine U 0.0132 0.484 1 01/18/2018 22:26 WG1062710 Phenanthrene U 0.00768 0.0480 1 01/18/2018 22:26 WG1062710 Benzylbutyl phthalate U 0.0150 0.484 1 01/18/2018 22:26 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0174 0.484 1 01/18/2018 22:26 WG1062710 Di-n-butyl phthalate U 0.0159 0.484 1 01/18/2018 22:26 WG1062710 Diethyl phthalate U 0.0100 0.484 1 01/18/2018 22:26 WG1062710 Dimethyl phthalate U 0.00785 0.484 1 01/18/2018 22:26 WG1062710 Di-n-octyl phthalate U 0.0132 0.484 1 01/18/2018 22:26 WG1062710 Pyrene U 0.0179 0.0480 1 01/18/2018 22:26 WG1062710 1,2,4-Trichlorobenzene U 0.0127 0.484 1 01/18/2018 22:26 WG1062710 4-Chloro-3-methylphenol U 0.00694 0.484 1 01/18/2018 22:26 WG1062710 2-Chlorophenol U 0.0121 0.484 1 01/18/2018 22:26 WG1062710 2,4-Dichlorophenol U 0.0108 0.484 1 01/18/2018 22:26 WG1062710 2,4-Dimethylphenol U 0.0685 0.484 1 01/18/2018 22:26 WG1062710 4,6-Dinitro-2-methylphenol U 0.180 0.484 1 01/18/2018 22:26 WG1062710 2,4-Dinitrophenol U 0.143 0.484 1 01/18/2018 22:26 WG1062710 2-Nitrophenol U 0.0189 0.484 1 01/18/2018 22:26 WG1062710 4-Nitrophenol U J0 0.0763 0.484 1 01/18/2018 22:26 WG1062710 Pentachlorophenol U 0.0698 0.484 1 01/18/2018 22:26 WG1062710 Phenol U 0.0101 0.484 1 01/18/2018 22:26 WG1062710 2,4,6-Trichlorophenol U 0.0113 0.484 1 01/18/2018 22:26 WG1062710 (S) 2-Fluorophenol 72.2 20.0-120 01/18/2018 22:26 WG1062710 (S) Phenol-d5 63.6 20.0-120 01/18/2018 22:26 WG1062710 (S) Nitrobenzene-d5 55.4 18.0-125 01/18/2018 22:26 WG1062710 (S) 2-Fluorobiphenyl 64.8 28.0-120 01/18/2018 22:26 WG1062710 (S) 2,4,6-Tribromophenol 96.6 17.0-137 01/18/2018 22:26 WG1062710 (S) p-Terphenyl-d14 56.8 13.0-131 01/18/2018 22:26 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 22 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 22 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06 L963090 BF6 1-3 Collected date/time: 01/11/18 12:30 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 79.6 1 01/17/2018 09:47 WG1063379 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0915 0.00352 0.0251 1 01/17/2018 21:08 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.97 J 0.817 2.51 1 01/16/2018 02:47 WG1062607 Barium 46.6 0.214 0.629 1 01/16/2018 02:47 WG1062607 Cadmium U 0.0880 0.629 1 01/16/2018 02:47 WG1062607 Chromium 96.4 0.176 1.26 1 01/16/2018 02:47 WG1062607 Lead 7.27 0.239 0.629 1 01/16/2018 02:47 WG1062607 Selenium U 0.930 2.51 1 01/16/2018 02:47 WG1062607 Silver U 0.352 1.26 1 01/16/2018 02:47 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.0333 J 0.0126 0.0629 1 01/14/2018 09:33 WG1062584 Acrylonitrile U 0.00225 0.0126 1 01/14/2018 09:33 WG1062584 Benzene U 0.000339 0.00126 1 01/14/2018 09:33 WG1062584 Bromobenzene U 0.000357 0.00126 1 01/14/2018 09:33 WG1062584 Bromodichloromethane U 0.000319 0.00126 1 01/14/2018 09:33 WG1062584 Bromoform U 0.000533 0.00126 1 01/14/2018 09:33 WG1062584 Bromomethane U 0.00168 0.00629 1 01/14/2018 09:33 WG1062584 n-Butylbenzene U 0.000324 0.00126 1 01/14/2018 09:33 WG1062584 sec-Butylbenzene U 0.000253 0.00126 1 01/14/2018 09:33 WG1062584 tert-Butylbenzene U 0.000259 0.00126 1 01/14/2018 09:33 WG1062584 Carbon tetrachloride U 0.000412 0.00126 1 01/14/2018 09:33 WG1062584 Chlorobenzene U 0.000266 0.00126 1 01/14/2018 09:33 WG1062584 Chlorodibromomethane U 0.000469 0.00126 1 01/14/2018 09:33 WG1062584 Chloroethane U 0.00119 0.00629 1 01/14/2018 09:33 WG1062584 Chloroform U 0.000288 0.00629 1 01/14/2018 09:33 WG1062584 Chloromethane U 0.000471 0.00314 1 01/14/2018 09:33 WG1062584 2-Chlorotoluene U 0.000378 0.00126 1 01/14/2018 09:33 WG1062584 4-Chlorotoluene U 0.000302 0.00126 1 01/14/2018 09:33 WG1062584 1,2-Dibromo-3-Chloropropane U 0.00132 0.00629 1 01/14/2018 09:33 WG1062584 1,2-Dibromoethane U 0.000431 0.00126 1 01/14/2018 09:33 WG1062584 Dibromomethane U 0.000480 0.00126 1 01/14/2018 09:33 WG1062584 1,2-Dichlorobenzene U 0.000383 0.00126 1 01/14/2018 09:33 WG1062584 1,3-Dichlorobenzene U 0.000300 0.00126 1 01/14/2018 09:33 WG1062584 1,4-Dichlorobenzene U 0.000284 0.00126 1 01/14/2018 09:33 WG1062584 Dichlorodifluoromethane U 0.000896 0.00629 1 01/14/2018 09:33 WG1062584 1,1-Dichloroethane U 0.000250 0.00126 1 01/14/2018 09:33 WG1062584 1,2-Dichloroethane U 0.000333 0.00126 1 01/14/2018 09:33 WG1062584 1,1-Dichloroethene U 0.000381 0.00126 1 01/14/2018 09:33 WG1062584 cis-1,2-Dichloroethene U 0.000295 0.00126 1 01/14/2018 09:33 WG1062584 trans-1,2-Dichloroethene U 0.000332 0.00126 1 01/14/2018 09:33 WG1062584 1,2-Dichloropropane U 0.000450 0.00126 1 01/14/2018 09:33 WG1062584 1,1-Dichloropropene U 0.000398 0.00126 1 01/14/2018 09:33 WG1062584 1,3-Dichloropropane U 0.000260 0.00126 1 01/14/2018 09:33 WG1062584 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 23 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 23 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06 L963090 BF6 1-3 Collected date/time: 01/11/18 12:30 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000329 0.00126 1 01/14/2018 09:33 WG1062584 trans-1,3-Dichloropropene U 0.000336 0.00126 1 01/14/2018 09:33 WG1062584 2,2-Dichloropropane U 0.000351 0.00126 1 01/14/2018 09:33 WG1062584 Di-isopropyl ether U 0.000312 0.00126 1 01/14/2018 09:33 WG1062584 Ethylbenzene U 0.000373 0.00126 1 01/14/2018 09:33 WG1062584 Hexachloro-1,3-butadiene U 0.000430 0.00126 1 01/14/2018 09:33 WG1062584 Isopropylbenzene U 0.000305 0.00126 1 01/14/2018 09:33 WG1062584 p-Isopropyltoluene U 0.000256 0.00126 1 01/14/2018 09:33 WG1062584 2-Butanone (MEK)U 0.00588 0.0126 1 01/14/2018 09:33 WG1062584 Methylene Chloride U 0.00126 0.00629 1 01/14/2018 09:33 WG1062584 4-Methyl-2-pentanone (MIBK)U 0.00236 0.0126 1 01/14/2018 09:33 WG1062584 Methyl tert-butyl ether U 0.000266 0.00126 1 01/14/2018 09:33 WG1062584 Naphthalene U 0.00126 0.00629 1 01/14/2018 09:33 WG1062584 n-Propylbenzene U 0.000259 0.00126 1 01/14/2018 09:33 WG1062584 Styrene U 0.000294 0.00126 1 01/14/2018 09:33 WG1062584 1,1,1,2-Tetrachloroethane U 0.000332 0.00126 1 01/14/2018 09:33 WG1062584 1,1,2,2-Tetrachloroethane U 0.000459 0.00126 1 01/14/2018 09:33 WG1062584 Tetrachloroethene U 0.000347 0.00126 1 01/14/2018 09:33 WG1062584 Toluene U 0.000546 0.00629 1 01/14/2018 09:33 WG1062584 1,2,3-Trichlorobenzene U 0.000385 0.00126 1 01/14/2018 09:33 WG1062584 1,2,4-Trichlorobenzene U 0.000488 0.00126 1 01/14/2018 09:33 WG1062584 1,1,1-Trichloroethane U 0.000360 0.00126 1 01/14/2018 09:33 WG1062584 1,1,2-Trichloroethane U 0.000348 0.00126 1 01/14/2018 09:33 WG1062584 1,1,2-Trichlorotrifluoroethane U 0.000459 0.00126 1 01/14/2018 09:33 WG1062584 Trichloroethene U 0.000351 0.00126 1 01/14/2018 09:33 WG1062584 Trichlorofluoromethane U J3 J4 0.000480 0.00629 1 01/14/2018 09:33 WG1062584 1,2,3-Trichloropropane U 0.000931 0.00314 1 01/14/2018 09:33 WG1062584 1,2,4-Trimethylbenzene U 0.000265 0.00126 1 01/14/2018 09:33 WG1062584 1,3,5-Trimethylbenzene U 0.000334 0.00126 1 01/14/2018 09:33 WG1062584 Vinyl chloride U 0.000366 0.00126 1 01/14/2018 09:33 WG1062584 Xylenes, Total U 0.000877 0.00377 1 01/14/2018 09:33 WG1062584 (S) Toluene-d8 96.5 80.0-120 01/14/2018 09:33 WG1062584 (S) Dibromofluoromethane 103 74.0-131 01/14/2018 09:33 WG1062584 (S) 4-Bromofluorobenzene 99.1 64.0-132 01/14/2018 09:33 WG1062584 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00807 0.0415 1 01/18/2018 22:50 WG1062710 Acenaphthylene U 0.00843 0.0415 1 01/18/2018 22:50 WG1062710 Anthracene U 0.00794 0.0415 1 01/18/2018 22:50 WG1062710 Benzidine U J4 0.0801 0.419 1 01/18/2018 22:50 WG1062710 Benzo(a)anthracene U 0.00538 0.0415 1 01/18/2018 22:50 WG1062710 Benzo(b)fluoranthene U 0.00874 0.0415 1 01/18/2018 22:50 WG1062710 Benzo(k)fluoranthene U 0.00732 0.0415 1 01/18/2018 22:50 WG1062710 Benzo(g,h,i)perylene U 0.00906 0.0415 1 01/18/2018 22:50 WG1062710 Benzo(a)pyrene U 0.00689 0.0415 1 01/18/2018 22:50 WG1062710 Bis(2-chlorethoxy)methane U 0.00968 0.419 1 01/18/2018 22:50 WG1062710 Bis(2-chloroethyl)ether U 0.0113 0.419 1 01/18/2018 22:50 WG1062710 Bis(2-chloroisopropyl)ether U 0.00955 0.419 1 01/18/2018 22:50 WG1062710 4-Bromophenyl-phenylether U 0.0143 0.419 1 01/18/2018 22:50 WG1062710 2-Chloronaphthalene U 0.00803 0.0415 1 01/18/2018 22:50 WG1062710 4-Chlorophenyl-phenylether U 0.00788 0.419 1 01/18/2018 22:50 WG1062710 Chrysene U 0.00698 0.0415 1 01/18/2018 22:50 WG1062710 Dibenz(a,h)anthracene U 0.0103 0.0415 1 01/18/2018 22:50 WG1062710 3,3-Dichlorobenzidine U 0.0998 0.419 1 01/18/2018 22:50 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 24 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 24 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06 L963090 BF6 1-3 Collected date/time: 01/11/18 12:30 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00763 0.419 1 01/18/2018 22:50 WG1062710 2,6-Dinitrotoluene U 0.00926 0.419 1 01/18/2018 22:50 WG1062710 Fluoranthene U 0.00623 0.0415 1 01/18/2018 22:50 WG1062710 Fluorene U 0.00857 0.0415 1 01/18/2018 22:50 WG1062710 Hexachlorobenzene U 0.0108 0.419 1 01/18/2018 22:50 WG1062710 Hexachloro-1,3-butadiene U 0.0126 0.419 1 01/18/2018 22:50 WG1062710 Hexachlorocyclopentadiene U J0 0.0738 0.419 1 01/18/2018 22:50 WG1062710 Hexachloroethane U 0.0168 0.419 1 01/18/2018 22:50 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00970 0.0415 1 01/18/2018 22:50 WG1062710 Isophorone U 0.00656 0.419 1 01/18/2018 22:50 WG1062710 Naphthalene U 0.0112 0.0415 1 01/18/2018 22:50 WG1062710 Nitrobenzene U 0.00874 0.419 1 01/18/2018 22:50 WG1062710 n-Nitrosodimethylamine U 0.0813 0.419 1 01/18/2018 22:50 WG1062710 n-Nitrosodiphenylamine U 0.00747 0.419 1 01/18/2018 22:50 WG1062710 n-Nitrosodi-n-propylamine U 0.0114 0.419 1 01/18/2018 22:50 WG1062710 Phenanthrene U 0.00664 0.0415 1 01/18/2018 22:50 WG1062710 Benzylbutyl phthalate U 0.0129 0.419 1 01/18/2018 22:50 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0151 0.419 1 01/18/2018 22:50 WG1062710 Di-n-butyl phthalate U 0.0137 0.419 1 01/18/2018 22:50 WG1062710 Diethyl phthalate U 0.00869 0.419 1 01/18/2018 22:50 WG1062710 Dimethyl phthalate U 0.00679 0.419 1 01/18/2018 22:50 WG1062710 Di-n-octyl phthalate U 0.0114 0.419 1 01/18/2018 22:50 WG1062710 Pyrene U 0.0155 0.0415 1 01/18/2018 22:50 WG1062710 1,2,4-Trichlorobenzene U 0.0110 0.419 1 01/18/2018 22:50 WG1062710 4-Chloro-3-methylphenol U 0.00600 0.419 1 01/18/2018 22:50 WG1062710 2-Chlorophenol U 0.0104 0.419 1 01/18/2018 22:50 WG1062710 2,4-Dichlorophenol U 0.00938 0.419 1 01/18/2018 22:50 WG1062710 2,4-Dimethylphenol U 0.0592 0.419 1 01/18/2018 22:50 WG1062710 4,6-Dinitro-2-methylphenol U 0.156 0.419 1 01/18/2018 22:50 WG1062710 2,4-Dinitrophenol U 0.123 0.419 1 01/18/2018 22:50 WG1062710 2-Nitrophenol U 0.0163 0.419 1 01/18/2018 22:50 WG1062710 4-Nitrophenol U J0 0.0660 0.419 1 01/18/2018 22:50 WG1062710 Pentachlorophenol U 0.0603 0.419 1 01/18/2018 22:50 WG1062710 Phenol U 0.00874 0.419 1 01/18/2018 22:50 WG1062710 2,4,6-Trichlorophenol U 0.00979 0.419 1 01/18/2018 22:50 WG1062710 (S) 2-Fluorophenol 80.6 20.0-120 01/18/2018 22:50 WG1062710 (S) Phenol-d5 70.2 20.0-120 01/18/2018 22:50 WG1062710 (S) Nitrobenzene-d5 60.6 18.0-125 01/18/2018 22:50 WG1062710 (S) 2-Fluorobiphenyl 68.8 28.0-120 01/18/2018 22:50 WG1062710 (S) 2,4,6-Tribromophenol 102 17.0-137 01/18/2018 22:50 WG1062710 (S) p-Terphenyl-d14 61.6 13.0-131 01/18/2018 22:50 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 25 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 25 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07 L963090 BF7 2-4 Collected date/time: 01/11/18 12:40 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 80.0 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0631 0.00350 0.0250 1 01/17/2018 21:11 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic U 0.812 2.50 1 01/16/2018 02:51 WG1062607 Barium 39.6 0.212 0.625 1 01/16/2018 02:51 WG1062607 Cadmium U 0.0875 0.625 1 01/16/2018 02:51 WG1062607 Chromium 34.6 0.175 1.25 1 01/16/2018 02:51 WG1062607 Lead 7.05 0.237 0.625 1 01/16/2018 02:51 WG1062607 Selenium U 0.925 2.50 1 01/16/2018 02:51 WG1062607 Silver U 0.350 1.25 1 01/16/2018 02:51 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0125 0.0625 1 01/14/2018 09:52 WG1062584 Acrylonitrile U 0.00224 0.0125 1 01/14/2018 09:52 WG1062584 Benzene U 0.000337 0.00125 1 01/14/2018 09:52 WG1062584 Bromobenzene U 0.000355 0.00125 1 01/14/2018 09:52 WG1062584 Bromodichloromethane U 0.000317 0.00125 1 01/14/2018 09:52 WG1062584 Bromoform U 0.000530 0.00125 1 01/14/2018 09:52 WG1062584 Bromomethane U 0.00167 0.00625 1 01/14/2018 09:52 WG1062584 n-Butylbenzene U 0.000322 0.00125 1 01/14/2018 09:52 WG1062584 sec-Butylbenzene U 0.000251 0.00125 1 01/14/2018 09:52 WG1062584 tert-Butylbenzene U 0.000257 0.00125 1 01/14/2018 09:52 WG1062584 Carbon tetrachloride U 0.000410 0.00125 1 01/14/2018 09:52 WG1062584 Chlorobenzene U 0.000265 0.00125 1 01/14/2018 09:52 WG1062584 Chlorodibromomethane U 0.000466 0.00125 1 01/14/2018 09:52 WG1062584 Chloroethane U 0.00118 0.00625 1 01/14/2018 09:52 WG1062584 Chloroform U 0.000286 0.00625 1 01/14/2018 09:52 WG1062584 Chloromethane U 0.000469 0.00312 1 01/14/2018 09:52 WG1062584 2-Chlorotoluene U 0.000376 0.00125 1 01/14/2018 09:52 WG1062584 4-Chlorotoluene U 0.000300 0.00125 1 01/14/2018 09:52 WG1062584 1,2-Dibromo-3-Chloropropane U 0.00131 0.00625 1 01/14/2018 09:52 WG1062584 1,2-Dibromoethane U 0.000429 0.00125 1 01/14/2018 09:52 WG1062584 Dibromomethane U 0.000477 0.00125 1 01/14/2018 09:52 WG1062584 1,2-Dichlorobenzene U 0.000381 0.00125 1 01/14/2018 09:52 WG1062584 1,3-Dichlorobenzene U 0.000299 0.00125 1 01/14/2018 09:52 WG1062584 1,4-Dichlorobenzene U 0.000282 0.00125 1 01/14/2018 09:52 WG1062584 Dichlorodifluoromethane U 0.000891 0.00625 1 01/14/2018 09:52 WG1062584 1,1-Dichloroethane U 0.000249 0.00125 1 01/14/2018 09:52 WG1062584 1,2-Dichloroethane U 0.000331 0.00125 1 01/14/2018 09:52 WG1062584 1,1-Dichloroethene U 0.000379 0.00125 1 01/14/2018 09:52 WG1062584 cis-1,2-Dichloroethene U 0.000294 0.00125 1 01/14/2018 09:52 WG1062584 trans-1,2-Dichloroethene U 0.000330 0.00125 1 01/14/2018 09:52 WG1062584 1,2-Dichloropropane U 0.000447 0.00125 1 01/14/2018 09:52 WG1062584 1,1-Dichloropropene U 0.000396 0.00125 1 01/14/2018 09:52 WG1062584 1,3-Dichloropropane U 0.000259 0.00125 1 01/14/2018 09:52 WG1062584 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 26 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 26 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07 L963090 BF7 2-4 Collected date/time: 01/11/18 12:40 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000327 0.00125 1 01/14/2018 09:52 WG1062584 trans-1,3-Dichloropropene U 0.000334 0.00125 1 01/14/2018 09:52 WG1062584 2,2-Dichloropropane U 0.000349 0.00125 1 01/14/2018 09:52 WG1062584 Di-isopropyl ether U 0.000310 0.00125 1 01/14/2018 09:52 WG1062584 Ethylbenzene U 0.000371 0.00125 1 01/14/2018 09:52 WG1062584 Hexachloro-1,3-butadiene U 0.000427 0.00125 1 01/14/2018 09:52 WG1062584 Isopropylbenzene U 0.000304 0.00125 1 01/14/2018 09:52 WG1062584 p-Isopropyltoluene U 0.000255 0.00125 1 01/14/2018 09:52 WG1062584 2-Butanone (MEK)U 0.00585 0.0125 1 01/14/2018 09:52 WG1062584 Methylene Chloride U 0.00125 0.00625 1 01/14/2018 09:52 WG1062584 4-Methyl-2-pentanone (MIBK)U 0.00235 0.0125 1 01/14/2018 09:52 WG1062584 Methyl tert-butyl ether U 0.000265 0.00125 1 01/14/2018 09:52 WG1062584 Naphthalene U 0.00125 0.00625 1 01/14/2018 09:52 WG1062584 n-Propylbenzene U 0.000257 0.00125 1 01/14/2018 09:52 WG1062584 Styrene U 0.000292 0.00125 1 01/14/2018 09:52 WG1062584 1,1,1,2-Tetrachloroethane U 0.000330 0.00125 1 01/14/2018 09:52 WG1062584 1,1,2,2-Tetrachloroethane U 0.000456 0.00125 1 01/14/2018 09:52 WG1062584 Tetrachloroethene U 0.000345 0.00125 1 01/14/2018 09:52 WG1062584 Toluene U 0.000542 0.00625 1 01/14/2018 09:52 WG1062584 1,2,3-Trichlorobenzene U 0.000382 0.00125 1 01/14/2018 09:52 WG1062584 1,2,4-Trichlorobenzene U 0.000485 0.00125 1 01/14/2018 09:52 WG1062584 1,1,1-Trichloroethane U 0.000357 0.00125 1 01/14/2018 09:52 WG1062584 1,1,2-Trichloroethane U 0.000346 0.00125 1 01/14/2018 09:52 WG1062584 1,1,2-Trichlorotrifluoroethane U 0.000456 0.00125 1 01/14/2018 09:52 WG1062584 Trichloroethene U 0.000349 0.00125 1 01/14/2018 09:52 WG1062584 Trichlorofluoromethane U J3 J4 0.000477 0.00625 1 01/14/2018 09:52 WG1062584 1,2,3-Trichloropropane U 0.000926 0.00312 1 01/14/2018 09:52 WG1062584 1,2,4-Trimethylbenzene U 0.000264 0.00125 1 01/14/2018 09:52 WG1062584 1,3,5-Trimethylbenzene U 0.000332 0.00125 1 01/14/2018 09:52 WG1062584 Vinyl chloride U 0.000364 0.00125 1 01/14/2018 09:52 WG1062584 Xylenes, Total U 0.000872 0.00375 1 01/14/2018 09:52 WG1062584 (S) Toluene-d8 97.6 80.0-120 01/14/2018 09:52 WG1062584 (S) Dibromofluoromethane 104 74.0-131 01/14/2018 09:52 WG1062584 (S) 4-Bromofluorobenzene 97.6 64.0-132 01/14/2018 09:52 WG1062584 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00802 0.0412 1 01/18/2018 23:13 WG1062710 Acenaphthylene U 0.00839 0.0412 1 01/18/2018 23:13 WG1062710 Anthracene U 0.00790 0.0412 1 01/18/2018 23:13 WG1062710 Benzidine U J4 0.0796 0.416 1 01/18/2018 23:13 WG1062710 Benzo(a)anthracene U 0.00535 0.0412 1 01/18/2018 23:13 WG1062710 Benzo(b)fluoranthene U 0.00869 0.0412 1 01/18/2018 23:13 WG1062710 Benzo(k)fluoranthene U 0.00727 0.0412 1 01/18/2018 23:13 WG1062710 Benzo(g,h,i)perylene U 0.00901 0.0412 1 01/18/2018 23:13 WG1062710 Benzo(a)pyrene U 0.00685 0.0412 1 01/18/2018 23:13 WG1062710 Bis(2-chlorethoxy)methane U 0.00962 0.416 1 01/18/2018 23:13 WG1062710 Bis(2-chloroethyl)ether U 0.0112 0.416 1 01/18/2018 23:13 WG1062710 Bis(2-chloroisopropyl)ether U 0.00950 0.416 1 01/18/2018 23:13 WG1062710 4-Bromophenyl-phenylether U 0.0142 0.416 1 01/18/2018 23:13 WG1062710 2-Chloronaphthalene U 0.00799 0.0412 1 01/18/2018 23:13 WG1062710 4-Chlorophenyl-phenylether U 0.00784 0.416 1 01/18/2018 23:13 WG1062710 Chrysene U 0.00694 0.0412 1 01/18/2018 23:13 WG1062710 Dibenz(a,h)anthracene U 0.0103 0.0412 1 01/18/2018 23:13 WG1062710 3,3-Dichlorobenzidine U 0.0992 0.416 1 01/18/2018 23:13 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 27 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 27 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07 L963090 BF7 2-4 Collected date/time: 01/11/18 12:40 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00759 0.416 1 01/18/2018 23:13 WG1062710 2,6-Dinitrotoluene U 0.00921 0.416 1 01/18/2018 23:13 WG1062710 Fluoranthene U 0.00620 0.0412 1 01/18/2018 23:13 WG1062710 Fluorene U 0.00852 0.0412 1 01/18/2018 23:13 WG1062710 Hexachlorobenzene U 0.0107 0.416 1 01/18/2018 23:13 WG1062710 Hexachloro-1,3-butadiene U 0.0125 0.416 1 01/18/2018 23:13 WG1062710 Hexachlorocyclopentadiene U J0 0.0734 0.416 1 01/18/2018 23:13 WG1062710 Hexachloroethane U 0.0167 0.416 1 01/18/2018 23:13 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00965 0.0412 1 01/18/2018 23:13 WG1062710 Isophorone U 0.00652 0.416 1 01/18/2018 23:13 WG1062710 Naphthalene U 0.0111 0.0412 1 01/18/2018 23:13 WG1062710 Nitrobenzene U 0.00869 0.416 1 01/18/2018 23:13 WG1062710 n-Nitrosodimethylamine U 0.0809 0.416 1 01/18/2018 23:13 WG1062710 n-Nitrosodiphenylamine U 0.00742 0.416 1 01/18/2018 23:13 WG1062710 n-Nitrosodi-n-propylamine U 0.0113 0.416 1 01/18/2018 23:13 WG1062710 Phenanthrene U 0.00660 0.0412 1 01/18/2018 23:13 WG1062710 Benzylbutyl phthalate U 0.0129 0.416 1 01/18/2018 23:13 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0150 0.416 1 01/18/2018 23:13 WG1062710 Di-n-butyl phthalate U 0.0136 0.416 1 01/18/2018 23:13 WG1062710 Diethyl phthalate U 0.00864 0.416 1 01/18/2018 23:13 WG1062710 Dimethyl phthalate U 0.00675 0.416 1 01/18/2018 23:13 WG1062710 Di-n-octyl phthalate U 0.0113 0.416 1 01/18/2018 23:13 WG1062710 Pyrene U 0.0154 0.0412 1 01/18/2018 23:13 WG1062710 1,2,4-Trichlorobenzene U 0.0109 0.416 1 01/18/2018 23:13 WG1062710 4-Chloro-3-methylphenol U 0.00596 0.416 1 01/18/2018 23:13 WG1062710 2-Chlorophenol U 0.0104 0.416 1 01/18/2018 23:13 WG1062710 2,4-Dichlorophenol U 0.00932 0.416 1 01/18/2018 23:13 WG1062710 2,4-Dimethylphenol U 0.0589 0.416 1 01/18/2018 23:13 WG1062710 4,6-Dinitro-2-methylphenol U 0.155 0.416 1 01/18/2018 23:13 WG1062710 2,4-Dinitrophenol U 0.122 0.416 1 01/18/2018 23:13 WG1062710 2-Nitrophenol U 0.0162 0.416 1 01/18/2018 23:13 WG1062710 4-Nitrophenol U J0 0.0656 0.416 1 01/18/2018 23:13 WG1062710 Pentachlorophenol U 0.0600 0.416 1 01/18/2018 23:13 WG1062710 Phenol U 0.00869 0.416 1 01/18/2018 23:13 WG1062710 2,4,6-Trichlorophenol U 0.00974 0.416 1 01/18/2018 23:13 WG1062710 (S) 2-Fluorophenol 71.2 20.0-120 01/18/2018 23:13 WG1062710 (S) Phenol-d5 62.6 20.0-120 01/18/2018 23:13 WG1062710 (S) Nitrobenzene-d5 57.0 18.0-125 01/18/2018 23:13 WG1062710 (S) 2-Fluorobiphenyl 64.8 28.0-120 01/18/2018 23:13 WG1062710 (S) 2,4,6-Tribromophenol 92.8 17.0-137 01/18/2018 23:13 WG1062710 (S) p-Terphenyl-d14 58.4 13.0-131 01/18/2018 23:13 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 28 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 28 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08 L963090 BF8 2-4 Collected date/time: 01/11/18 13:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 78.9 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0364 B 0.00355 0.0253 1 01/17/2018 21:13 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.33 J 0.824 2.53 1 01/16/2018 02:54 WG1062607 Barium 164 0.215 0.634 1 01/16/2018 02:54 WG1062607 Cadmium U 0.0887 0.634 1 01/16/2018 02:54 WG1062607 Chromium 17.1 0.177 1.27 1 01/16/2018 02:54 WG1062607 Lead 6.97 0.241 0.634 1 01/16/2018 02:54 WG1062607 Selenium U 0.938 2.53 1 01/16/2018 02:54 WG1062607 Silver U 0.355 1.27 1 01/16/2018 02:54 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.0201 J 0.0127 0.0634 1 01/14/2018 15:09 WG1062672 Acrylonitrile U 0.00227 0.0127 1 01/14/2018 15:09 WG1062672 Benzene U 0.000342 0.00127 1 01/14/2018 15:09 WG1062672 Bromobenzene U 0.000360 0.00127 1 01/14/2018 15:09 WG1062672 Bromodichloromethane U 0.000322 0.00127 1 01/14/2018 15:09 WG1062672 Bromoform U 0.000537 0.00127 1 01/14/2018 15:09 WG1062672 Bromomethane U 0.00170 0.00634 1 01/14/2018 15:09 WG1062672 n-Butylbenzene U 0.000327 0.00127 1 01/14/2018 15:09 WG1062672 sec-Butylbenzene U 0.000255 0.00127 1 01/14/2018 15:09 WG1062672 tert-Butylbenzene U 0.000261 0.00127 1 01/14/2018 15:09 WG1062672 Carbon tetrachloride U 0.000416 0.00127 1 01/14/2018 15:09 WG1062672 Chlorobenzene U 0.000269 0.00127 1 01/14/2018 15:09 WG1062672 Chlorodibromomethane U 0.000473 0.00127 1 01/14/2018 15:09 WG1062672 Chloroethane U 0.00120 0.00634 1 01/14/2018 15:09 WG1062672 Chloroform U 0.000290 0.00634 1 01/14/2018 15:09 WG1062672 Chloromethane U 0.000475 0.00317 1 01/14/2018 15:09 WG1062672 2-Chlorotoluene U 0.000381 0.00127 1 01/14/2018 15:09 WG1062672 4-Chlorotoluene U 0.000304 0.00127 1 01/14/2018 15:09 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00133 0.00634 1 01/14/2018 15:09 WG1062672 1,2-Dibromoethane U 0.000435 0.00127 1 01/14/2018 15:09 WG1062672 Dibromomethane U 0.000484 0.00127 1 01/14/2018 15:09 WG1062672 1,2-Dichlorobenzene U 0.000387 0.00127 1 01/14/2018 15:09 WG1062672 1,3-Dichlorobenzene U 0.000303 0.00127 1 01/14/2018 15:09 WG1062672 1,4-Dichlorobenzene U 0.000286 0.00127 1 01/14/2018 15:09 WG1062672 Dichlorodifluoromethane U 0.000904 0.00634 1 01/14/2018 15:09 WG1062672 1,1-Dichloroethane U 0.000252 0.00127 1 01/14/2018 15:09 WG1062672 1,2-Dichloroethane U 0.000336 0.00127 1 01/14/2018 15:09 WG1062672 1,1-Dichloroethene U 0.000384 0.00127 1 01/14/2018 15:09 WG1062672 cis-1,2-Dichloroethene U 0.000298 0.00127 1 01/14/2018 15:09 WG1062672 trans-1,2-Dichloroethene U 0.000335 0.00127 1 01/14/2018 15:09 WG1062672 1,2-Dichloropropane U 0.000454 0.00127 1 01/14/2018 15:09 WG1062672 1,1-Dichloropropene U 0.000402 0.00127 1 01/14/2018 15:09 WG1062672 1,3-Dichloropropane U 0.000262 0.00127 1 01/14/2018 15:09 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 29 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 29 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08 L963090 BF8 2-4 Collected date/time: 01/11/18 13:00 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000332 0.00127 1 01/14/2018 15:09 WG1062672 trans-1,3-Dichloropropene U 0.000338 0.00127 1 01/14/2018 15:09 WG1062672 2,2-Dichloropropane U 0.000354 0.00127 1 01/14/2018 15:09 WG1062672 Di-isopropyl ether U 0.000314 0.00127 1 01/14/2018 15:09 WG1062672 Ethylbenzene U 0.000376 0.00127 1 01/14/2018 15:09 WG1062672 Hexachloro-1,3-butadiene U 0.000433 0.00127 1 01/14/2018 15:09 WG1062672 Isopropylbenzene U 0.000308 0.00127 1 01/14/2018 15:09 WG1062672 p-Isopropyltoluene U 0.000259 0.00127 1 01/14/2018 15:09 WG1062672 2-Butanone (MEK)U 0.00593 0.0127 1 01/14/2018 15:09 WG1062672 Methylene Chloride U 0.00127 0.00634 1 01/14/2018 15:09 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00238 0.0127 1 01/14/2018 15:09 WG1062672 Methyl tert-butyl ether U 0.000269 0.00127 1 01/14/2018 15:09 WG1062672 Naphthalene U 0.00127 0.00634 1 01/14/2018 15:09 WG1062672 n-Propylbenzene U 0.000261 0.00127 1 01/14/2018 15:09 WG1062672 Styrene U 0.000297 0.00127 1 01/14/2018 15:09 WG1062672 1,1,1,2-Tetrachloroethane U 0.000335 0.00127 1 01/14/2018 15:09 WG1062672 1,1,2,2-Tetrachloroethane U 0.000463 0.00127 1 01/14/2018 15:09 WG1062672 Tetrachloroethene U 0.000350 0.00127 1 01/14/2018 15:09 WG1062672 Toluene U 0.000550 0.00634 1 01/14/2018 15:09 WG1062672 1,2,3-Trichlorobenzene U 0.000388 0.00127 1 01/14/2018 15:09 WG1062672 1,2,4-Trichlorobenzene U 0.000492 0.00127 1 01/14/2018 15:09 WG1062672 1,1,1-Trichloroethane U 0.000362 0.00127 1 01/14/2018 15:09 WG1062672 1,1,2-Trichloroethane U 0.000351 0.00127 1 01/14/2018 15:09 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000463 0.00127 1 01/14/2018 15:09 WG1062672 Trichloroethene U 0.000354 0.00127 1 01/14/2018 15:09 WG1062672 Trichlorofluoromethane U 0.000484 0.00634 1 01/14/2018 15:09 WG1062672 1,2,3-Trichloropropane U 0.000939 0.00317 1 01/14/2018 15:09 WG1062672 1,2,4-Trimethylbenzene U 0.000267 0.00127 1 01/14/2018 15:09 WG1062672 1,3,5-Trimethylbenzene U 0.000337 0.00127 1 01/14/2018 15:09 WG1062672 Vinyl chloride U 0.000369 0.00127 1 01/14/2018 15:09 WG1062672 Xylenes, Total U 0.000885 0.00380 1 01/14/2018 15:09 WG1062672 (S) Toluene-d8 92.2 80.0-120 01/14/2018 15:09 WG1062672 (S) Dibromofluoromethane 103 74.0-131 01/14/2018 15:09 WG1062672 (S) 4-Bromofluorobenzene 101 64.0-132 01/14/2018 15:09 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00814 0.0418 1 01/18/2018 23:36 WG1062710 Acenaphthylene U 0.00850 0.0418 1 01/18/2018 23:36 WG1062710 Anthracene U 0.00801 0.0418 1 01/18/2018 23:36 WG1062710 Benzidine U J4 0.0807 0.422 1 01/18/2018 23:36 WG1062710 Benzo(a)anthracene U 0.00542 0.0418 1 01/18/2018 23:36 WG1062710 Benzo(b)fluoranthene U 0.00881 0.0418 1 01/18/2018 23:36 WG1062710 Benzo(k)fluoranthene U 0.00738 0.0418 1 01/18/2018 23:36 WG1062710 Benzo(g,h,i)perylene U 0.00914 0.0418 1 01/18/2018 23:36 WG1062710 Benzo(a)pyrene U 0.00694 0.0418 1 01/18/2018 23:36 WG1062710 Bis(2-chlorethoxy)methane U 0.00976 0.422 1 01/18/2018 23:36 WG1062710 Bis(2-chloroethyl)ether U 0.0114 0.422 1 01/18/2018 23:36 WG1062710 Bis(2-chloroisopropyl)ether U 0.00963 0.422 1 01/18/2018 23:36 WG1062710 4-Bromophenyl-phenylether U 0.0144 0.422 1 01/18/2018 23:36 WG1062710 2-Chloronaphthalene U 0.00810 0.0418 1 01/18/2018 23:36 WG1062710 4-Chlorophenyl-phenylether U 0.00795 0.422 1 01/18/2018 23:36 WG1062710 Chrysene U 0.00703 0.0418 1 01/18/2018 23:36 WG1062710 Dibenz(a,h)anthracene U 0.0104 0.0418 1 01/18/2018 23:36 WG1062710 3,3-Dichlorobenzidine U 0.101 0.422 1 01/18/2018 23:36 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 30 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 30 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08 L963090 BF8 2-4 Collected date/time: 01/11/18 13:00 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00769 0.422 1 01/18/2018 23:36 WG1062710 2,6-Dinitrotoluene U 0.00934 0.422 1 01/18/2018 23:36 WG1062710 Fluoranthene U 0.00629 0.0418 1 01/18/2018 23:36 WG1062710 Fluorene U 0.00864 0.0418 1 01/18/2018 23:36 WG1062710 Hexachlorobenzene U 0.0108 0.422 1 01/18/2018 23:36 WG1062710 Hexachloro-1,3-butadiene U 0.0127 0.422 1 01/18/2018 23:36 WG1062710 Hexachlorocyclopentadiene U J0 0.0744 0.422 1 01/18/2018 23:36 WG1062710 Hexachloroethane U 0.0170 0.422 1 01/18/2018 23:36 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00978 0.0418 1 01/18/2018 23:36 WG1062710 Isophorone U 0.00661 0.422 1 01/18/2018 23:36 WG1062710 Naphthalene U 0.0113 0.0418 1 01/18/2018 23:36 WG1062710 Nitrobenzene U 0.00881 0.422 1 01/18/2018 23:36 WG1062710 n-Nitrosodimethylamine U 0.0820 0.422 1 01/18/2018 23:36 WG1062710 n-Nitrosodiphenylamine U 0.00753 0.422 1 01/18/2018 23:36 WG1062710 n-Nitrosodi-n-propylamine U 0.0115 0.422 1 01/18/2018 23:36 WG1062710 Phenanthrene U 0.00669 0.0418 1 01/18/2018 23:36 WG1062710 Benzylbutyl phthalate U 0.0131 0.422 1 01/18/2018 23:36 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0152 0.422 1 01/18/2018 23:36 WG1062710 Di-n-butyl phthalate U 0.0138 0.422 1 01/18/2018 23:36 WG1062710 Diethyl phthalate U 0.00876 0.422 1 01/18/2018 23:36 WG1062710 Dimethyl phthalate U 0.00684 0.422 1 01/18/2018 23:36 WG1062710 Di-n-octyl phthalate U 0.0115 0.422 1 01/18/2018 23:36 WG1062710 Pyrene U 0.0156 0.0418 1 01/18/2018 23:36 WG1062710 1,2,4-Trichlorobenzene U 0.0111 0.422 1 01/18/2018 23:36 WG1062710 4-Chloro-3-methylphenol U 0.00604 0.422 1 01/18/2018 23:36 WG1062710 2-Chlorophenol U 0.0105 0.422 1 01/18/2018 23:36 WG1062710 2,4-Dichlorophenol U 0.00945 0.422 1 01/18/2018 23:36 WG1062710 2,4-Dimethylphenol U 0.0597 0.422 1 01/18/2018 23:36 WG1062710 4,6-Dinitro-2-methylphenol U 0.157 0.422 1 01/18/2018 23:36 WG1062710 2,4-Dinitrophenol U 0.124 0.422 1 01/18/2018 23:36 WG1062710 2-Nitrophenol U 0.0165 0.422 1 01/18/2018 23:36 WG1062710 4-Nitrophenol U J0 0.0665 0.422 1 01/18/2018 23:36 WG1062710 Pentachlorophenol U 0.0608 0.422 1 01/18/2018 23:36 WG1062710 Phenol U 0.00881 0.422 1 01/18/2018 23:36 WG1062710 2,4,6-Trichlorophenol U 0.00987 0.422 1 01/18/2018 23:36 WG1062710 (S) 2-Fluorophenol 57.2 20.0-120 01/18/2018 23:36 WG1062710 (S) Phenol-d5 52.6 20.0-120 01/18/2018 23:36 WG1062710 (S) Nitrobenzene-d5 43.6 18.0-125 01/18/2018 23:36 WG1062710 (S) 2-Fluorobiphenyl 56.8 28.0-120 01/18/2018 23:36 WG1062710 (S) 2,4,6-Tribromophenol 84.0 17.0-137 01/18/2018 23:36 WG1062710 (S) p-Terphenyl-d14 51.2 13.0-131 01/18/2018 23:36 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 31 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 31 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09 L963090 RF-1 Collected date/time: 01/11/18 14:30 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 82.8 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.417 0.00338 0.0242 1 01/17/2018 21:16 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 2.33 J 0.785 2.42 1 01/16/2018 02:57 WG1062607 Barium 91.3 0.205 0.604 1 01/16/2018 02:57 WG1062607 Cadmium 0.131 J 0.0846 0.604 1 01/16/2018 02:57 WG1062607 Chromium 13.6 0.169 1.21 1 01/16/2018 02:57 WG1062607 Lead 228 0.230 0.604 1 01/16/2018 02:57 WG1062607 Selenium U 0.894 2.42 1 01/16/2018 02:57 WG1062607 Silver U 0.338 1.21 1 01/16/2018 02:57 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.0293 J 0.0121 0.0604 1 01/14/2018 15:29 WG1062672 Acrylonitrile U 0.00216 0.0121 1 01/14/2018 15:29 WG1062672 Benzene U 0.000326 0.00121 1 01/14/2018 15:29 WG1062672 Bromobenzene U 0.000343 0.00121 1 01/14/2018 15:29 WG1062672 Bromodichloromethane U 0.000307 0.00121 1 01/14/2018 15:29 WG1062672 Bromoform U 0.000512 0.00121 1 01/14/2018 15:29 WG1062672 Bromomethane U 0.00162 0.00604 1 01/14/2018 15:29 WG1062672 n-Butylbenzene U 0.000312 0.00121 1 01/14/2018 15:29 WG1062672 sec-Butylbenzene U 0.000243 0.00121 1 01/14/2018 15:29 WG1062672 tert-Butylbenzene U 0.000249 0.00121 1 01/14/2018 15:29 WG1062672 Carbon tetrachloride U 0.000396 0.00121 1 01/14/2018 15:29 WG1062672 Chlorobenzene U 0.000256 0.00121 1 01/14/2018 15:29 WG1062672 Chlorodibromomethane U 0.000451 0.00121 1 01/14/2018 15:29 WG1062672 Chloroethane U 0.00114 0.00604 1 01/14/2018 15:29 WG1062672 Chloroform U 0.000277 0.00604 1 01/14/2018 15:29 WG1062672 Chloromethane U 0.000453 0.00302 1 01/14/2018 15:29 WG1062672 2-Chlorotoluene U 0.000364 0.00121 1 01/14/2018 15:29 WG1062672 4-Chlorotoluene U 0.000290 0.00121 1 01/14/2018 15:29 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00127 0.00604 1 01/14/2018 15:29 WG1062672 1,2-Dibromoethane U 0.000414 0.00121 1 01/14/2018 15:29 WG1062672 Dibromomethane U 0.000461 0.00121 1 01/14/2018 15:29 WG1062672 1,2-Dichlorobenzene U 0.000368 0.00121 1 01/14/2018 15:29 WG1062672 1,3-Dichlorobenzene U 0.000289 0.00121 1 01/14/2018 15:29 WG1062672 1,4-Dichlorobenzene U 0.000273 0.00121 1 01/14/2018 15:29 WG1062672 Dichlorodifluoromethane U 0.000861 0.00604 1 01/14/2018 15:29 WG1062672 1,1-Dichloroethane U 0.000240 0.00121 1 01/14/2018 15:29 WG1062672 1,2-Dichloroethane U 0.000320 0.00121 1 01/14/2018 15:29 WG1062672 1,1-Dichloroethene U 0.000366 0.00121 1 01/14/2018 15:29 WG1062672 cis-1,2-Dichloroethene U 0.000284 0.00121 1 01/14/2018 15:29 WG1062672 trans-1,2-Dichloroethene U 0.000319 0.00121 1 01/14/2018 15:29 WG1062672 1,2-Dichloropropane U 0.000432 0.00121 1 01/14/2018 15:29 WG1062672 1,1-Dichloropropene U 0.000383 0.00121 1 01/14/2018 15:29 WG1062672 1,3-Dichloropropane U 0.000250 0.00121 1 01/14/2018 15:29 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 32 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 32 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09 L963090 RF-1 Collected date/time: 01/11/18 14:30 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000317 0.00121 1 01/14/2018 15:29 WG1062672 trans-1,3-Dichloropropene U 0.000323 0.00121 1 01/14/2018 15:29 WG1062672 2,2-Dichloropropane U 0.000337 0.00121 1 01/14/2018 15:29 WG1062672 Di-isopropyl ether U 0.000300 0.00121 1 01/14/2018 15:29 WG1062672 Ethylbenzene U 0.000359 0.00121 1 01/14/2018 15:29 WG1062672 Hexachloro-1,3-butadiene U 0.000413 0.00121 1 01/14/2018 15:29 WG1062672 Isopropylbenzene U 0.000294 0.00121 1 01/14/2018 15:29 WG1062672 p-Isopropyltoluene U 0.000246 0.00121 1 01/14/2018 15:29 WG1062672 2-Butanone (MEK)U 0.00565 0.0121 1 01/14/2018 15:29 WG1062672 Methylene Chloride U 0.00121 0.00604 1 01/14/2018 15:29 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00227 0.0121 1 01/14/2018 15:29 WG1062672 Methyl tert-butyl ether U 0.000256 0.00121 1 01/14/2018 15:29 WG1062672 Naphthalene U 0.00121 0.00604 1 01/14/2018 15:29 WG1062672 n-Propylbenzene U 0.000249 0.00121 1 01/14/2018 15:29 WG1062672 Styrene U 0.000283 0.00121 1 01/14/2018 15:29 WG1062672 1,1,1,2-Tetrachloroethane U 0.000319 0.00121 1 01/14/2018 15:29 WG1062672 1,1,2,2-Tetrachloroethane U 0.000441 0.00121 1 01/14/2018 15:29 WG1062672 Tetrachloroethene U 0.000333 0.00121 1 01/14/2018 15:29 WG1062672 Toluene U 0.000524 0.00604 1 01/14/2018 15:29 WG1062672 1,2,3-Trichlorobenzene U 0.000370 0.00121 1 01/14/2018 15:29 WG1062672 1,2,4-Trichlorobenzene U 0.000469 0.00121 1 01/14/2018 15:29 WG1062672 1,1,1-Trichloroethane U 0.000345 0.00121 1 01/14/2018 15:29 WG1062672 1,1,2-Trichloroethane U 0.000335 0.00121 1 01/14/2018 15:29 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000441 0.00121 1 01/14/2018 15:29 WG1062672 Trichloroethene U 0.000337 0.00121 1 01/14/2018 15:29 WG1062672 Trichlorofluoromethane U 0.000461 0.00604 1 01/14/2018 15:29 WG1062672 1,2,3-Trichloropropane U 0.000895 0.00302 1 01/14/2018 15:29 WG1062672 1,2,4-Trimethylbenzene U 0.000255 0.00121 1 01/14/2018 15:29 WG1062672 1,3,5-Trimethylbenzene U 0.000321 0.00121 1 01/14/2018 15:29 WG1062672 Vinyl chloride U 0.000352 0.00121 1 01/14/2018 15:29 WG1062672 Xylenes, Total U 0.000843 0.00362 1 01/14/2018 15:29 WG1062672 (S) Toluene-d8 95.2 80.0-120 01/14/2018 15:29 WG1062672 (S) Dibromofluoromethane 107 74.0-131 01/14/2018 15:29 WG1062672 (S) 4-Bromofluorobenzene 97.2 64.0-132 01/14/2018 15:29 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00776 0.0399 1 01/19/2018 00:00 WG1062710 Acenaphthylene U 0.00811 0.0399 1 01/19/2018 00:00 WG1062710 Anthracene U 0.00763 0.0399 1 01/19/2018 00:00 WG1062710 Benzidine U J4 0.0770 0.402 1 01/19/2018 00:00 WG1062710 Benzo(a)anthracene U 0.00517 0.0399 1 01/19/2018 00:00 WG1062710 Benzo(b)fluoranthene U 0.00840 0.0399 1 01/19/2018 00:00 WG1062710 Benzo(k)fluoranthene U 0.00703 0.0399 1 01/19/2018 00:00 WG1062710 Benzo(g,h,i)perylene U 0.00871 0.0399 1 01/19/2018 00:00 WG1062710 Benzo(a)pyrene U 0.00662 0.0399 1 01/19/2018 00:00 WG1062710 Bis(2-chlorethoxy)methane U 0.00930 0.402 1 01/19/2018 00:00 WG1062710 Bis(2-chloroethyl)ether U 0.0108 0.402 1 01/19/2018 00:00 WG1062710 Bis(2-chloroisopropyl)ether U 0.00918 0.402 1 01/19/2018 00:00 WG1062710 4-Bromophenyl-phenylether U 0.0138 0.402 1 01/19/2018 00:00 WG1062710 2-Chloronaphthalene U 0.00772 0.0399 1 01/19/2018 00:00 WG1062710 4-Chlorophenyl-phenylether U 0.00757 0.402 1 01/19/2018 00:00 WG1062710 Chrysene U 0.00670 0.0399 1 01/19/2018 00:00 WG1062710 Dibenz(a,h)anthracene U 0.00992 0.0399 1 01/19/2018 00:00 WG1062710 3,3-Dichlorobenzidine U 0.0959 0.402 1 01/19/2018 00:00 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 33 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 33 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09 L963090 RF-1 Collected date/time: 01/11/18 14:30 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00733 0.402 1 01/19/2018 00:00 WG1062710 2,6-Dinitrotoluene U 0.00890 0.402 1 01/19/2018 00:00 WG1062710 Fluoranthene U 0.00599 0.0399 1 01/19/2018 00:00 WG1062710 Fluorene U 0.00824 0.0399 1 01/19/2018 00:00 WG1062710 Hexachlorobenzene U 0.0103 0.402 1 01/19/2018 00:00 WG1062710 Hexachloro-1,3-butadiene U 0.0121 0.402 1 01/19/2018 00:00 WG1062710 Hexachlorocyclopentadiene U J0 0.0709 0.402 1 01/19/2018 00:00 WG1062710 Hexachloroethane U 0.0162 0.402 1 01/19/2018 00:00 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00933 0.0399 1 01/19/2018 00:00 WG1062710 Isophorone U 0.00631 0.402 1 01/19/2018 00:00 WG1062710 Naphthalene U 0.0107 0.0399 1 01/19/2018 00:00 WG1062710 Nitrobenzene U 0.00840 0.402 1 01/19/2018 00:00 WG1062710 n-Nitrosodimethylamine U 0.0782 0.402 1 01/19/2018 00:00 WG1062710 n-Nitrosodiphenylamine U 0.00718 0.402 1 01/19/2018 00:00 WG1062710 n-Nitrosodi-n-propylamine U 0.0109 0.402 1 01/19/2018 00:00 WG1062710 Phenanthrene U 0.00638 0.0399 1 01/19/2018 00:00 WG1062710 Benzylbutyl phthalate U 0.0124 0.402 1 01/19/2018 00:00 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0145 0.402 1 01/19/2018 00:00 WG1062710 Di-n-butyl phthalate U 0.0132 0.402 1 01/19/2018 00:00 WG1062710 Diethyl phthalate U 0.00835 0.402 1 01/19/2018 00:00 WG1062710 Dimethyl phthalate U 0.00652 0.402 1 01/19/2018 00:00 WG1062710 Di-n-octyl phthalate U 0.0110 0.402 1 01/19/2018 00:00 WG1062710 Pyrene U 0.0149 0.0399 1 01/19/2018 00:00 WG1062710 1,2,4-Trichlorobenzene U 0.0106 0.402 1 01/19/2018 00:00 WG1062710 4-Chloro-3-methylphenol U 0.00576 0.402 1 01/19/2018 00:00 WG1062710 2-Chlorophenol U 0.0100 0.402 1 01/19/2018 00:00 WG1062710 2,4-Dichlorophenol U 0.00901 0.402 1 01/19/2018 00:00 WG1062710 2,4-Dimethylphenol U 0.0569 0.402 1 01/19/2018 00:00 WG1062710 4,6-Dinitro-2-methylphenol U 0.150 0.402 1 01/19/2018 00:00 WG1062710 2,4-Dinitrophenol U 0.118 0.402 1 01/19/2018 00:00 WG1062710 2-Nitrophenol U 0.0157 0.402 1 01/19/2018 00:00 WG1062710 4-Nitrophenol U J0 0.0634 0.402 1 01/19/2018 00:00 WG1062710 Pentachlorophenol U 0.0580 0.402 1 01/19/2018 00:00 WG1062710 Phenol U 0.00840 0.402 1 01/19/2018 00:00 WG1062710 2,4,6-Trichlorophenol U 0.00941 0.402 1 01/19/2018 00:00 WG1062710 (S) 2-Fluorophenol 65.8 20.0-120 01/19/2018 00:00 WG1062710 (S) Phenol-d5 58.0 20.0-120 01/19/2018 00:00 WG1062710 (S) Nitrobenzene-d5 49.2 18.0-125 01/19/2018 00:00 WG1062710 (S) 2-Fluorobiphenyl 55.2 28.0-120 01/19/2018 00:00 WG1062710 (S) 2,4,6-Tribromophenol 79.6 17.0-137 01/19/2018 00:00 WG1062710 (S) p-Terphenyl-d14 45.8 13.0-131 01/19/2018 00:00 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 34 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 34 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10 L963090 RF-2 Collected date/time: 01/11/18 14:40 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 83.5 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0700 0.00335 0.0239 1 01/17/2018 21:18 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.03 J 0.778 2.39 1 01/16/2018 03:00 WG1062607 Barium 51.0 0.204 0.599 1 01/16/2018 03:00 WG1062607 Cadmium U 0.0838 0.599 1 01/16/2018 03:00 WG1062607 Chromium 18.8 0.168 1.20 1 01/16/2018 03:00 WG1062607 Lead 8.64 0.227 0.599 1 01/16/2018 03:00 WG1062607 Selenium U 0.886 2.39 1 01/16/2018 03:00 WG1062607 Silver U 0.335 1.20 1 01/16/2018 03:00 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.0256 J 0.0120 0.0599 1 01/14/2018 15:48 WG1062672 Acrylonitrile U 0.00214 0.0120 1 01/14/2018 15:48 WG1062672 Benzene U 0.000323 0.00120 1 01/14/2018 15:48 WG1062672 Bromobenzene U 0.000340 0.00120 1 01/14/2018 15:48 WG1062672 Bromodichloromethane U 0.000304 0.00120 1 01/14/2018 15:48 WG1062672 Bromoform U 0.000508 0.00120 1 01/14/2018 15:48 WG1062672 Bromomethane U 0.00160 0.00599 1 01/14/2018 15:48 WG1062672 n-Butylbenzene U 0.000309 0.00120 1 01/14/2018 15:48 WG1062672 sec-Butylbenzene U 0.000241 0.00120 1 01/14/2018 15:48 WG1062672 tert-Butylbenzene U 0.000247 0.00120 1 01/14/2018 15:48 WG1062672 Carbon tetrachloride U 0.000393 0.00120 1 01/14/2018 15:48 WG1062672 Chlorobenzene U 0.000254 0.00120 1 01/14/2018 15:48 WG1062672 Chlorodibromomethane U 0.000447 0.00120 1 01/14/2018 15:48 WG1062672 Chloroethane U 0.00113 0.00599 1 01/14/2018 15:48 WG1062672 Chloroform U 0.000274 0.00599 1 01/14/2018 15:48 WG1062672 Chloromethane U 0.000449 0.00299 1 01/14/2018 15:48 WG1062672 2-Chlorotoluene U 0.000360 0.00120 1 01/14/2018 15:48 WG1062672 4-Chlorotoluene U 0.000287 0.00120 1 01/14/2018 15:48 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00126 0.00599 1 01/14/2018 15:48 WG1062672 1,2-Dibromoethane U 0.000411 0.00120 1 01/14/2018 15:48 WG1062672 Dibromomethane U 0.000457 0.00120 1 01/14/2018 15:48 WG1062672 1,2-Dichlorobenzene U 0.000365 0.00120 1 01/14/2018 15:48 WG1062672 1,3-Dichlorobenzene U 0.000286 0.00120 1 01/14/2018 15:48 WG1062672 1,4-Dichlorobenzene U 0.000271 0.00120 1 01/14/2018 15:48 WG1062672 Dichlorodifluoromethane U 0.000854 0.00599 1 01/14/2018 15:48 WG1062672 1,1-Dichloroethane U 0.000238 0.00120 1 01/14/2018 15:48 WG1062672 1,2-Dichloroethane U 0.000317 0.00120 1 01/14/2018 15:48 WG1062672 1,1-Dichloroethene U 0.000363 0.00120 1 01/14/2018 15:48 WG1062672 cis-1,2-Dichloroethene U 0.000281 0.00120 1 01/14/2018 15:48 WG1062672 trans-1,2-Dichloroethene U 0.000316 0.00120 1 01/14/2018 15:48 WG1062672 1,2-Dichloropropane U 0.000429 0.00120 1 01/14/2018 15:48 WG1062672 1,1-Dichloropropene U 0.000380 0.00120 1 01/14/2018 15:48 WG1062672 1,3-Dichloropropane U 0.000248 0.00120 1 01/14/2018 15:48 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 35 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 35 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10 L963090 RF-2 Collected date/time: 01/11/18 14:40 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000314 0.00120 1 01/14/2018 15:48 WG1062672 trans-1,3-Dichloropropene U 0.000320 0.00120 1 01/14/2018 15:48 WG1062672 2,2-Dichloropropane U 0.000334 0.00120 1 01/14/2018 15:48 WG1062672 Di-isopropyl ether U 0.000297 0.00120 1 01/14/2018 15:48 WG1062672 Ethylbenzene U 0.000356 0.00120 1 01/14/2018 15:48 WG1062672 Hexachloro-1,3-butadiene U 0.000409 0.00120 1 01/14/2018 15:48 WG1062672 Isopropylbenzene U 0.000291 0.00120 1 01/14/2018 15:48 WG1062672 p-Isopropyltoluene U 0.000244 0.00120 1 01/14/2018 15:48 WG1062672 2-Butanone (MEK)0.00583 J 0.00560 0.0120 1 01/14/2018 15:48 WG1062672 Methylene Chloride U 0.00120 0.00599 1 01/14/2018 15:48 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00225 0.0120 1 01/14/2018 15:48 WG1062672 Methyl tert-butyl ether U 0.000254 0.00120 1 01/14/2018 15:48 WG1062672 Naphthalene U 0.00120 0.00599 1 01/14/2018 15:48 WG1062672 n-Propylbenzene U 0.000247 0.00120 1 01/14/2018 15:48 WG1062672 Styrene U 0.000280 0.00120 1 01/14/2018 15:48 WG1062672 1,1,1,2-Tetrachloroethane U 0.000316 0.00120 1 01/14/2018 15:48 WG1062672 1,1,2,2-Tetrachloroethane U 0.000437 0.00120 1 01/14/2018 15:48 WG1062672 Tetrachloroethene U 0.000330 0.00120 1 01/14/2018 15:48 WG1062672 Toluene U 0.000520 0.00599 1 01/14/2018 15:48 WG1062672 1,2,3-Trichlorobenzene U 0.000366 0.00120 1 01/14/2018 15:48 WG1062672 1,2,4-Trichlorobenzene U 0.000465 0.00120 1 01/14/2018 15:48 WG1062672 1,1,1-Trichloroethane U 0.000342 0.00120 1 01/14/2018 15:48 WG1062672 1,1,2-Trichloroethane U 0.000332 0.00120 1 01/14/2018 15:48 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000437 0.00120 1 01/14/2018 15:48 WG1062672 Trichloroethene U 0.000334 0.00120 1 01/14/2018 15:48 WG1062672 Trichlorofluoromethane U 0.000457 0.00599 1 01/14/2018 15:48 WG1062672 1,2,3-Trichloropropane U 0.000887 0.00299 1 01/14/2018 15:48 WG1062672 1,2,4-Trimethylbenzene U 0.000253 0.00120 1 01/14/2018 15:48 WG1062672 1,3,5-Trimethylbenzene U 0.000318 0.00120 1 01/14/2018 15:48 WG1062672 Vinyl chloride U 0.000348 0.00120 1 01/14/2018 15:48 WG1062672 Xylenes, Total U 0.000836 0.00359 1 01/14/2018 15:48 WG1062672 (S) Toluene-d8 93.5 80.0-120 01/14/2018 15:48 WG1062672 (S) Dibromofluoromethane 104 74.0-131 01/14/2018 15:48 WG1062672 (S) 4-Bromofluorobenzene 98.6 64.0-132 01/14/2018 15:48 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00769 0.0395 1 01/19/2018 00:23 WG1062710 Acenaphthylene U 0.00803 0.0395 1 01/19/2018 00:23 WG1062710 Anthracene U 0.00757 0.0395 1 01/19/2018 00:23 WG1062710 Benzidine U J4 0.0763 0.399 1 01/19/2018 00:23 WG1062710 Benzo(a)anthracene U 0.00512 0.0395 1 01/19/2018 00:23 WG1062710 Benzo(b)fluoranthene U 0.00832 0.0395 1 01/19/2018 00:23 WG1062710 Benzo(k)fluoranthene U 0.00697 0.0395 1 01/19/2018 00:23 WG1062710 Benzo(g,h,i)perylene U 0.00863 0.0395 1 01/19/2018 00:23 WG1062710 Benzo(a)pyrene U 0.00656 0.0395 1 01/19/2018 00:23 WG1062710 Bis(2-chlorethoxy)methane U 0.00922 0.399 1 01/19/2018 00:23 WG1062710 Bis(2-chloroethyl)ether U 0.0107 0.399 1 01/19/2018 00:23 WG1062710 Bis(2-chloroisopropyl)ether U 0.00910 0.399 1 01/19/2018 00:23 WG1062710 4-Bromophenyl-phenylether U 0.0136 0.399 1 01/19/2018 00:23 WG1062710 2-Chloronaphthalene U 0.00765 0.0395 1 01/19/2018 00:23 WG1062710 4-Chlorophenyl-phenylether U 0.00751 0.399 1 01/19/2018 00:23 WG1062710 Chrysene U 0.00664 0.0395 1 01/19/2018 00:23 WG1062710 Dibenz(a,h)anthracene U 0.00983 0.0395 1 01/19/2018 00:23 WG1062710 3,3-Dichlorobenzidine U 0.0951 0.399 1 01/19/2018 00:23 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 36 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 36 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10 L963090 RF-2 Collected date/time: 01/11/18 14:40 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00727 0.399 1 01/19/2018 00:23 WG1062710 2,6-Dinitrotoluene U 0.00882 0.399 1 01/19/2018 00:23 WG1062710 Fluoranthene U 0.00594 0.0395 1 01/19/2018 00:23 WG1062710 Fluorene U 0.00817 0.0395 1 01/19/2018 00:23 WG1062710 Hexachlorobenzene U 0.0102 0.399 1 01/19/2018 00:23 WG1062710 Hexachloro-1,3-butadiene U 0.0120 0.399 1 01/19/2018 00:23 WG1062710 Hexachlorocyclopentadiene U J0 0.0703 0.399 1 01/19/2018 00:23 WG1062710 Hexachloroethane U 0.0160 0.399 1 01/19/2018 00:23 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00924 0.0395 1 01/19/2018 00:23 WG1062710 Isophorone U 0.00625 0.399 1 01/19/2018 00:23 WG1062710 Naphthalene U 0.0106 0.0395 1 01/19/2018 00:23 WG1062710 Nitrobenzene U 0.00832 0.399 1 01/19/2018 00:23 WG1062710 n-Nitrosodimethylamine U 0.0775 0.399 1 01/19/2018 00:23 WG1062710 n-Nitrosodiphenylamine U 0.00711 0.399 1 01/19/2018 00:23 WG1062710 n-Nitrosodi-n-propylamine U 0.0108 0.399 1 01/19/2018 00:23 WG1062710 Phenanthrene U 0.00632 0.0395 1 01/19/2018 00:23 WG1062710 Benzylbutyl phthalate U 0.0123 0.399 1 01/19/2018 00:23 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0144 0.399 1 01/19/2018 00:23 WG1062710 Di-n-butyl phthalate U 0.0130 0.399 1 01/19/2018 00:23 WG1062710 Diethyl phthalate U 0.00827 0.399 1 01/19/2018 00:23 WG1062710 Dimethyl phthalate U 0.00647 0.399 1 01/19/2018 00:23 WG1062710 Di-n-octyl phthalate U 0.0109 0.399 1 01/19/2018 00:23 WG1062710 Pyrene U 0.0147 0.0395 1 01/19/2018 00:23 WG1062710 1,2,4-Trichlorobenzene U 0.0105 0.399 1 01/19/2018 00:23 WG1062710 4-Chloro-3-methylphenol U 0.00571 0.399 1 01/19/2018 00:23 WG1062710 2-Chlorophenol U 0.00995 0.399 1 01/19/2018 00:23 WG1062710 2,4-Dichlorophenol U 0.00893 0.399 1 01/19/2018 00:23 WG1062710 2,4-Dimethylphenol U 0.0564 0.399 1 01/19/2018 00:23 WG1062710 4,6-Dinitro-2-methylphenol U 0.148 0.399 1 01/19/2018 00:23 WG1062710 2,4-Dinitrophenol U 0.117 0.399 1 01/19/2018 00:23 WG1062710 2-Nitrophenol U 0.0156 0.399 1 01/19/2018 00:23 WG1062710 4-Nitrophenol U J0 0.0629 0.399 1 01/19/2018 00:23 WG1062710 Pentachlorophenol U 0.0575 0.399 1 01/19/2018 00:23 WG1062710 Phenol U 0.00832 0.399 1 01/19/2018 00:23 WG1062710 2,4,6-Trichlorophenol U 0.00933 0.399 1 01/19/2018 00:23 WG1062710 (S) 2-Fluorophenol 58.8 20.0-120 01/19/2018 00:23 WG1062710 (S) Phenol-d5 53.0 20.0-120 01/19/2018 00:23 WG1062710 (S) Nitrobenzene-d5 48.0 18.0-125 01/19/2018 00:23 WG1062710 (S) 2-Fluorobiphenyl 53.8 28.0-120 01/19/2018 00:23 WG1062710 (S) 2,4,6-Tribromophenol 73.8 17.0-137 01/19/2018 00:23 WG1062710 (S) p-Terphenyl-d14 53.0 13.0-131 01/19/2018 00:23 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 37 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 37 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11 L963090 RF-3 Collected date/time: 01/11/18 14:50 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 86.9 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.138 0.00322 0.0230 1 01/17/2018 21:26 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 3.41 0.748 2.30 1 01/16/2018 03:04 WG1062607 Barium 104 0.196 0.575 1 01/16/2018 03:04 WG1062607 Cadmium 0.449 J 0.0805 0.575 1 01/16/2018 03:04 WG1062607 Chromium 36.1 0.161 1.15 1 01/16/2018 03:04 WG1062607 Lead 91.5 0.219 0.575 1 01/16/2018 03:04 WG1062607 Selenium U 0.851 2.30 1 01/16/2018 03:04 WG1062607 Silver U 0.322 1.15 1 01/16/2018 03:04 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.0511 J 0.0115 0.0575 1 01/14/2018 16:08 WG1062672 Acrylonitrile U 0.00206 0.0115 1 01/14/2018 16:08 WG1062672 Benzene 0.00181 0.000311 0.00115 1 01/14/2018 16:08 WG1062672 Bromobenzene U 0.000327 0.00115 1 01/14/2018 16:08 WG1062672 Bromodichloromethane U 0.000292 0.00115 1 01/14/2018 16:08 WG1062672 Bromoform U 0.000488 0.00115 1 01/14/2018 16:08 WG1062672 Bromomethane U 0.00154 0.00575 1 01/14/2018 16:08 WG1062672 n-Butylbenzene U 0.000297 0.00115 1 01/14/2018 16:08 WG1062672 sec-Butylbenzene U 0.000231 0.00115 1 01/14/2018 16:08 WG1062672 tert-Butylbenzene U 0.000237 0.00115 1 01/14/2018 16:08 WG1062672 Carbon tetrachloride U 0.000377 0.00115 1 01/14/2018 16:08 WG1062672 Chlorobenzene U 0.000244 0.00115 1 01/14/2018 16:08 WG1062672 Chlorodibromomethane U 0.000429 0.00115 1 01/14/2018 16:08 WG1062672 Chloroethane U 0.00109 0.00575 1 01/14/2018 16:08 WG1062672 Chloroform U 0.000263 0.00575 1 01/14/2018 16:08 WG1062672 Chloromethane U 0.000431 0.00288 1 01/14/2018 16:08 WG1062672 2-Chlorotoluene U 0.000346 0.00115 1 01/14/2018 16:08 WG1062672 4-Chlorotoluene U 0.000276 0.00115 1 01/14/2018 16:08 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00121 0.00575 1 01/14/2018 16:08 WG1062672 1,2-Dibromoethane U 0.000395 0.00115 1 01/14/2018 16:08 WG1062672 Dibromomethane U 0.000439 0.00115 1 01/14/2018 16:08 WG1062672 1,2-Dichlorobenzene U 0.000351 0.00115 1 01/14/2018 16:08 WG1062672 1,3-Dichlorobenzene U 0.000275 0.00115 1 01/14/2018 16:08 WG1062672 1,4-Dichlorobenzene U 0.000260 0.00115 1 01/14/2018 16:08 WG1062672 Dichlorodifluoromethane U 0.000820 0.00575 1 01/14/2018 16:08 WG1062672 1,1-Dichloroethane U 0.000229 0.00115 1 01/14/2018 16:08 WG1062672 1,2-Dichloroethane U 0.000305 0.00115 1 01/14/2018 16:08 WG1062672 1,1-Dichloroethene U 0.000349 0.00115 1 01/14/2018 16:08 WG1062672 cis-1,2-Dichloroethene U 0.000270 0.00115 1 01/14/2018 16:08 WG1062672 trans-1,2-Dichloroethene U 0.000304 0.00115 1 01/14/2018 16:08 WG1062672 1,2-Dichloropropane U 0.000412 0.00115 1 01/14/2018 16:08 WG1062672 1,1-Dichloropropene U 0.000365 0.00115 1 01/14/2018 16:08 WG1062672 1,3-Dichloropropane U 0.000238 0.00115 1 01/14/2018 16:08 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 38 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 38 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11 L963090 RF-3 Collected date/time: 01/11/18 14:50 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000301 0.00115 1 01/14/2018 16:08 WG1062672 trans-1,3-Dichloropropene U 0.000307 0.00115 1 01/14/2018 16:08 WG1062672 2,2-Dichloropropane U 0.000321 0.00115 1 01/14/2018 16:08 WG1062672 Di-isopropyl ether U 0.000285 0.00115 1 01/14/2018 16:08 WG1062672 Ethylbenzene U 0.000342 0.00115 1 01/14/2018 16:08 WG1062672 Hexachloro-1,3-butadiene U 0.000393 0.00115 1 01/14/2018 16:08 WG1062672 Isopropylbenzene U 0.000280 0.00115 1 01/14/2018 16:08 WG1062672 p-Isopropyltoluene U 0.000235 0.00115 1 01/14/2018 16:08 WG1062672 2-Butanone (MEK)0.00648 J 0.00538 0.0115 1 01/14/2018 16:08 WG1062672 Methylene Chloride U 0.00115 0.00575 1 01/14/2018 16:08 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00216 0.0115 1 01/14/2018 16:08 WG1062672 Methyl tert-butyl ether U 0.000244 0.00115 1 01/14/2018 16:08 WG1062672 Naphthalene U 0.00115 0.00575 1 01/14/2018 16:08 WG1062672 n-Propylbenzene U 0.000237 0.00115 1 01/14/2018 16:08 WG1062672 Styrene U 0.000269 0.00115 1 01/14/2018 16:08 WG1062672 1,1,1,2-Tetrachloroethane U 0.000304 0.00115 1 01/14/2018 16:08 WG1062672 1,1,2,2-Tetrachloroethane U 0.000420 0.00115 1 01/14/2018 16:08 WG1062672 Tetrachloroethene 0.00164 0.000317 0.00115 1 01/14/2018 16:08 WG1062672 Toluene 0.000648 J 0.000499 0.00575 1 01/14/2018 16:08 WG1062672 1,2,3-Trichlorobenzene U 0.000352 0.00115 1 01/14/2018 16:08 WG1062672 1,2,4-Trichlorobenzene U 0.000446 0.00115 1 01/14/2018 16:08 WG1062672 1,1,1-Trichloroethane U 0.000329 0.00115 1 01/14/2018 16:08 WG1062672 1,1,2-Trichloroethane U 0.000319 0.00115 1 01/14/2018 16:08 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000420 0.00115 1 01/14/2018 16:08 WG1062672 Trichloroethene U 0.000321 0.00115 1 01/14/2018 16:08 WG1062672 Trichlorofluoromethane U 0.000439 0.00575 1 01/14/2018 16:08 WG1062672 1,2,3-Trichloropropane U 0.000852 0.00288 1 01/14/2018 16:08 WG1062672 1,2,4-Trimethylbenzene U 0.000243 0.00115 1 01/14/2018 16:08 WG1062672 1,3,5-Trimethylbenzene U 0.000306 0.00115 1 01/14/2018 16:08 WG1062672 Vinyl chloride U 0.000335 0.00115 1 01/14/2018 16:08 WG1062672 Xylenes, Total U 0.000803 0.00345 1 01/14/2018 16:08 WG1062672 (S) Toluene-d8 95.4 80.0-120 01/14/2018 16:08 WG1062672 (S) Dibromofluoromethane 104 74.0-131 01/14/2018 16:08 WG1062672 (S) 4-Bromofluorobenzene 108 64.0-132 01/14/2018 16:08 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00738 0.0380 1 01/19/2018 00:46 WG1062710 Acenaphthylene U 0.00772 0.0380 1 01/19/2018 00:46 WG1062710 Anthracene U 0.00727 0.0380 1 01/19/2018 00:46 WG1062710 Benzidine U J4 0.0733 0.383 1 01/19/2018 00:46 WG1062710 Benzo(a)anthracene U 0.00492 0.0380 1 01/19/2018 00:46 WG1062710 Benzo(b)fluoranthene U 0.00799 0.0380 1 01/19/2018 00:46 WG1062710 Benzo(k)fluoranthene U 0.00669 0.0380 1 01/19/2018 00:46 WG1062710 Benzo(g,h,i)perylene U 0.00829 0.0380 1 01/19/2018 00:46 WG1062710 Benzo(a)pyrene U 0.00630 0.0380 1 01/19/2018 00:46 WG1062710 Bis(2-chlorethoxy)methane U 0.00886 0.383 1 01/19/2018 00:46 WG1062710 Bis(2-chloroethyl)ether U 0.0103 0.383 1 01/19/2018 00:46 WG1062710 Bis(2-chloroisopropyl)ether U 0.00874 0.383 1 01/19/2018 00:46 WG1062710 4-Bromophenyl-phenylether U 0.0131 0.383 1 01/19/2018 00:46 WG1062710 2-Chloronaphthalene U 0.00735 0.0380 1 01/19/2018 00:46 WG1062710 4-Chlorophenyl-phenylether U 0.00721 0.383 1 01/19/2018 00:46 WG1062710 Chrysene U 0.00638 0.0380 1 01/19/2018 00:46 WG1062710 Dibenz(a,h)anthracene U 0.00944 0.0380 1 01/19/2018 00:46 WG1062710 3,3-Dichlorobenzidine U 0.0913 0.383 1 01/19/2018 00:46 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 39 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 39 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11 L963090 RF-3 Collected date/time: 01/11/18 14:50 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00698 0.383 1 01/19/2018 00:46 WG1062710 2,6-Dinitrotoluene U 0.00848 0.383 1 01/19/2018 00:46 WG1062710 Fluoranthene 0.112 0.00571 0.0380 1 01/19/2018 00:46 WG1062710 Fluorene U 0.00784 0.0380 1 01/19/2018 00:46 WG1062710 Hexachlorobenzene U 0.00985 0.383 1 01/19/2018 00:46 WG1062710 Hexachloro-1,3-butadiene U 0.0115 0.383 1 01/19/2018 00:46 WG1062710 Hexachlorocyclopentadiene U J0 0.0675 0.383 1 01/19/2018 00:46 WG1062710 Hexachloroethane U 0.0154 0.383 1 01/19/2018 00:46 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00888 0.0380 1 01/19/2018 00:46 WG1062710 Isophorone U 0.00600 0.383 1 01/19/2018 00:46 WG1062710 Naphthalene U 0.0102 0.0380 1 01/19/2018 00:46 WG1062710 Nitrobenzene U 0.00799 0.383 1 01/19/2018 00:46 WG1062710 n-Nitrosodimethylamine U 0.0744 0.383 1 01/19/2018 00:46 WG1062710 n-Nitrosodiphenylamine U 0.00683 0.383 1 01/19/2018 00:46 WG1062710 n-Nitrosodi-n-propylamine U 0.0104 0.383 1 01/19/2018 00:46 WG1062710 Phenanthrene U 0.00607 0.0380 1 01/19/2018 00:46 WG1062710 Benzylbutyl phthalate U 0.0118 0.383 1 01/19/2018 00:46 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0138 0.383 1 01/19/2018 00:46 WG1062710 Di-n-butyl phthalate U 0.0125 0.383 1 01/19/2018 00:46 WG1062710 Diethyl phthalate U 0.00795 0.383 1 01/19/2018 00:46 WG1062710 Dimethyl phthalate U 0.00621 0.383 1 01/19/2018 00:46 WG1062710 Di-n-octyl phthalate U 0.0104 0.383 1 01/19/2018 00:46 WG1062710 Pyrene U 0.0141 0.0380 1 01/19/2018 00:46 WG1062710 1,2,4-Trichlorobenzene U 0.0101 0.383 1 01/19/2018 00:46 WG1062710 4-Chloro-3-methylphenol U 0.00549 0.383 1 01/19/2018 00:46 WG1062710 2-Chlorophenol U 0.00956 0.383 1 01/19/2018 00:46 WG1062710 2,4-Dichlorophenol U 0.00858 0.383 1 01/19/2018 00:46 WG1062710 2,4-Dimethylphenol U 0.0542 0.383 1 01/19/2018 00:46 WG1062710 4,6-Dinitro-2-methylphenol U 0.143 0.383 1 01/19/2018 00:46 WG1062710 2,4-Dinitrophenol U 0.113 0.383 1 01/19/2018 00:46 WG1062710 2-Nitrophenol U 0.0150 0.383 1 01/19/2018 00:46 WG1062710 4-Nitrophenol U J0 0.0604 0.383 1 01/19/2018 00:46 WG1062710 Pentachlorophenol U 0.0552 0.383 1 01/19/2018 00:46 WG1062710 Phenol U 0.00799 0.383 1 01/19/2018 00:46 WG1062710 2,4,6-Trichlorophenol U 0.00896 0.383 1 01/19/2018 00:46 WG1062710 (S) 2-Fluorophenol 60.4 20.0-120 01/19/2018 00:46 WG1062710 (S) Phenol-d5 52.8 20.0-120 01/19/2018 00:46 WG1062710 (S) Nitrobenzene-d5 50.0 18.0-125 01/19/2018 00:46 WG1062710 (S) 2-Fluorobiphenyl 55.4 28.0-120 01/19/2018 00:46 WG1062710 (S) 2,4,6-Tribromophenol 72.6 17.0-137 01/19/2018 00:46 WG1062710 (S) p-Terphenyl-d14 39.4 13.0-131 01/19/2018 00:46 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 40 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 40 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12 L963090 BF12 2-3 Collected date/time: 01/11/18 09:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 89.5 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.101 0.00313 0.0223 1 01/17/2018 21:28 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 1.62 J 0.726 2.23 1 01/16/2018 03:07 WG1062607 Barium 27.7 0.190 0.559 1 01/16/2018 03:07 WG1062607 Cadmium U 0.0782 0.559 1 01/16/2018 03:07 WG1062607 Chromium 15.9 0.156 1.12 1 01/16/2018 03:07 WG1062607 Lead 2.65 0.212 0.559 1 01/16/2018 03:07 WG1062607 Selenium U 0.827 2.23 1 01/16/2018 03:07 WG1062607 Silver U 0.313 1.12 1 01/16/2018 03:07 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0112 0.0559 1 01/14/2018 16:56 WG1062672 Acrylonitrile U 0.00200 0.0112 1 01/14/2018 16:56 WG1062672 Benzene U 0.000302 0.00112 1 01/14/2018 16:56 WG1062672 Bromobenzene U 0.000317 0.00112 1 01/14/2018 16:56 WG1062672 Bromodichloromethane U 0.000284 0.00112 1 01/14/2018 16:56 WG1062672 Bromoform U 0.000474 0.00112 1 01/14/2018 16:56 WG1062672 Bromomethane U 0.00150 0.00559 1 01/14/2018 16:56 WG1062672 n-Butylbenzene U 0.000288 0.00112 1 01/14/2018 16:56 WG1062672 sec-Butylbenzene U 0.000225 0.00112 1 01/14/2018 16:56 WG1062672 tert-Butylbenzene U 0.000230 0.00112 1 01/14/2018 16:56 WG1062672 Carbon tetrachloride U 0.000367 0.00112 1 01/14/2018 16:56 WG1062672 Chlorobenzene U 0.000237 0.00112 1 01/14/2018 16:56 WG1062672 Chlorodibromomethane U 0.000417 0.00112 1 01/14/2018 16:56 WG1062672 Chloroethane U 0.00106 0.00559 1 01/14/2018 16:56 WG1062672 Chloroform U 0.000256 0.00559 1 01/14/2018 16:56 WG1062672 Chloromethane U 0.000419 0.00279 1 01/14/2018 16:56 WG1062672 2-Chlorotoluene U 0.000336 0.00112 1 01/14/2018 16:56 WG1062672 4-Chlorotoluene U 0.000268 0.00112 1 01/14/2018 16:56 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00117 0.00559 1 01/14/2018 16:56 WG1062672 1,2-Dibromoethane U 0.000383 0.00112 1 01/14/2018 16:56 WG1062672 Dibromomethane U 0.000427 0.00112 1 01/14/2018 16:56 WG1062672 1,2-Dichlorobenzene U 0.000341 0.00112 1 01/14/2018 16:56 WG1062672 1,3-Dichlorobenzene U 0.000267 0.00112 1 01/14/2018 16:56 WG1062672 1,4-Dichlorobenzene U 0.000253 0.00112 1 01/14/2018 16:56 WG1062672 Dichlorodifluoromethane U 0.000797 0.00559 1 01/14/2018 16:56 WG1062672 1,1-Dichloroethane U 0.000222 0.00112 1 01/14/2018 16:56 WG1062672 1,2-Dichloroethane U 0.000296 0.00112 1 01/14/2018 16:56 WG1062672 1,1-Dichloroethene U 0.000339 0.00112 1 01/14/2018 16:56 WG1062672 cis-1,2-Dichloroethene U 0.000263 0.00112 1 01/14/2018 16:56 WG1062672 trans-1,2-Dichloroethene U 0.000295 0.00112 1 01/14/2018 16:56 WG1062672 1,2-Dichloropropane U 0.000400 0.00112 1 01/14/2018 16:56 WG1062672 1,1-Dichloropropene U 0.000354 0.00112 1 01/14/2018 16:56 WG1062672 1,3-Dichloropropane U 0.000231 0.00112 1 01/14/2018 16:56 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 41 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 41 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12 L963090 BF12 2-3 Collected date/time: 01/11/18 09:00 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000293 0.00112 1 01/14/2018 16:56 WG1062672 trans-1,3-Dichloropropene U 0.000298 0.00112 1 01/14/2018 16:56 WG1062672 2,2-Dichloropropane U 0.000312 0.00112 1 01/14/2018 16:56 WG1062672 Di-isopropyl ether U 0.000277 0.00112 1 01/14/2018 16:56 WG1062672 Ethylbenzene U 0.000332 0.00112 1 01/14/2018 16:56 WG1062672 Hexachloro-1,3-butadiene U 0.000382 0.00112 1 01/14/2018 16:56 WG1062672 Isopropylbenzene U 0.000272 0.00112 1 01/14/2018 16:56 WG1062672 p-Isopropyltoluene U 0.000228 0.00112 1 01/14/2018 16:56 WG1062672 2-Butanone (MEK)U 0.00523 0.0112 1 01/14/2018 16:56 WG1062672 Methylene Chloride U 0.00112 0.00559 1 01/14/2018 16:56 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00210 0.0112 1 01/14/2018 16:56 WG1062672 Methyl tert-butyl ether U 0.000237 0.00112 1 01/14/2018 16:56 WG1062672 Naphthalene U 0.00112 0.00559 1 01/14/2018 16:56 WG1062672 n-Propylbenzene U 0.000230 0.00112 1 01/14/2018 16:56 WG1062672 Styrene U 0.000261 0.00112 1 01/14/2018 16:56 WG1062672 1,1,1,2-Tetrachloroethane U 0.000295 0.00112 1 01/14/2018 16:56 WG1062672 1,1,2,2-Tetrachloroethane U 0.000408 0.00112 1 01/14/2018 16:56 WG1062672 Tetrachloroethene U 0.000308 0.00112 1 01/14/2018 16:56 WG1062672 Toluene U 0.000485 0.00559 1 01/14/2018 16:56 WG1062672 1,2,3-Trichlorobenzene U 0.000342 0.00112 1 01/14/2018 16:56 WG1062672 1,2,4-Trichlorobenzene U 0.000434 0.00112 1 01/14/2018 16:56 WG1062672 1,1,1-Trichloroethane U 0.000320 0.00112 1 01/14/2018 16:56 WG1062672 1,1,2-Trichloroethane U 0.000310 0.00112 1 01/14/2018 16:56 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000408 0.00112 1 01/14/2018 16:56 WG1062672 Trichloroethene U 0.000312 0.00112 1 01/14/2018 16:56 WG1062672 Trichlorofluoromethane U 0.000427 0.00559 1 01/14/2018 16:56 WG1062672 1,2,3-Trichloropropane U 0.000828 0.00279 1 01/14/2018 16:56 WG1062672 1,2,4-Trimethylbenzene U 0.000236 0.00112 1 01/14/2018 16:56 WG1062672 1,3,5-Trimethylbenzene U 0.000297 0.00112 1 01/14/2018 16:56 WG1062672 Vinyl chloride U 0.000325 0.00112 1 01/14/2018 16:56 WG1062672 Xylenes, Total U 0.000780 0.00335 1 01/14/2018 16:56 WG1062672 (S) Toluene-d8 93.5 80.0-120 01/14/2018 16:56 WG1062672 (S) Dibromofluoromethane 104 74.0-131 01/14/2018 16:56 WG1062672 (S) 4-Bromofluorobenzene 97.4 64.0-132 01/14/2018 16:56 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00717 0.0369 1 01/19/2018 01:09 WG1062710 Acenaphthylene U 0.00750 0.0369 1 01/19/2018 01:09 WG1062710 Anthracene U 0.00706 0.0369 1 01/19/2018 01:09 WG1062710 Benzidine U J4 J6 0.0712 0.372 1 01/19/2018 01:09 WG1062710 Benzo(a)anthracene U 0.00478 0.0369 1 01/19/2018 01:09 WG1062710 Benzo(b)fluoranthene U 0.00777 0.0369 1 01/19/2018 01:09 WG1062710 Benzo(k)fluoranthene U 0.00650 0.0369 1 01/19/2018 01:09 WG1062710 Benzo(g,h,i)perylene U 0.00806 0.0369 1 01/19/2018 01:09 WG1062710 Benzo(a)pyrene U 0.00612 0.0369 1 01/19/2018 01:09 WG1062710 Bis(2-chlorethoxy)methane U 0.00860 0.372 1 01/19/2018 01:09 WG1062710 Bis(2-chloroethyl)ether U 0.0100 0.372 1 01/19/2018 01:09 WG1062710 Bis(2-chloroisopropyl)ether U 0.00849 0.372 1 01/19/2018 01:09 WG1062710 4-Bromophenyl-phenylether U 0.0127 0.372 1 01/19/2018 01:09 WG1062710 2-Chloronaphthalene U 0.00714 0.0369 1 01/19/2018 01:09 WG1062710 4-Chlorophenyl-phenylether U 0.00701 0.372 1 01/19/2018 01:09 WG1062710 Chrysene U 0.00620 0.0369 1 01/19/2018 01:09 WG1062710 Dibenz(a,h)anthracene U 0.00917 0.0369 1 01/19/2018 01:09 WG1062710 3,3-Dichlorobenzidine U 0.0887 0.372 1 01/19/2018 01:09 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 42 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 42 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12 L963090 BF12 2-3 Collected date/time: 01/11/18 09:00 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00678 0.372 1 01/19/2018 01:09 WG1062710 2,6-Dinitrotoluene U 0.00824 0.372 1 01/19/2018 01:09 WG1062710 Fluoranthene U 0.00554 0.0369 1 01/19/2018 01:09 WG1062710 Fluorene U 0.00762 0.0369 1 01/19/2018 01:09 WG1062710 Hexachlorobenzene U 0.00957 0.372 1 01/19/2018 01:09 WG1062710 Hexachloro-1,3-butadiene U 0.0112 0.372 1 01/19/2018 01:09 WG1062710 Hexachlorocyclopentadiene U J0 0.0656 0.372 1 01/19/2018 01:09 WG1062710 Hexachloroethane U 0.0150 0.372 1 01/19/2018 01:09 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00863 0.0369 1 01/19/2018 01:09 WG1062710 Isophorone U 0.00583 0.372 1 01/19/2018 01:09 WG1062710 Naphthalene U 0.00993 0.0369 1 01/19/2018 01:09 WG1062710 Nitrobenzene U 0.00777 0.372 1 01/19/2018 01:09 WG1062710 n-Nitrosodimethylamine U 0.0723 0.372 1 01/19/2018 01:09 WG1062710 n-Nitrosodiphenylamine U 0.00664 0.372 1 01/19/2018 01:09 WG1062710 n-Nitrosodi-n-propylamine U 0.0101 0.372 1 01/19/2018 01:09 WG1062710 Phenanthrene U 0.00590 0.0369 1 01/19/2018 01:09 WG1062710 Benzylbutyl phthalate U 0.0115 0.372 1 01/19/2018 01:09 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0134 0.372 1 01/19/2018 01:09 WG1062710 Di-n-butyl phthalate U 0.0122 0.372 1 01/19/2018 01:09 WG1062710 Diethyl phthalate U 0.00772 0.372 1 01/19/2018 01:09 WG1062710 Dimethyl phthalate U 0.00603 0.372 1 01/19/2018 01:09 WG1062710 Di-n-octyl phthalate U 0.0101 0.372 1 01/19/2018 01:09 WG1062710 Pyrene U 0.0137 0.0369 1 01/19/2018 01:09 WG1062710 1,2,4-Trichlorobenzene U 0.00979 0.372 1 01/19/2018 01:09 WG1062710 4-Chloro-3-methylphenol U 0.00533 0.372 1 01/19/2018 01:09 WG1062710 2-Chlorophenol U 0.00929 0.372 1 01/19/2018 01:09 WG1062710 2,4-Dichlorophenol U 0.00834 0.372 1 01/19/2018 01:09 WG1062710 2,4-Dimethylphenol U 0.0526 0.372 1 01/19/2018 01:09 WG1062710 4,6-Dinitro-2-methylphenol U 0.139 0.372 1 01/19/2018 01:09 WG1062710 2,4-Dinitrophenol U 0.110 0.372 1 01/19/2018 01:09 WG1062710 2-Nitrophenol U 0.0145 0.372 1 01/19/2018 01:09 WG1062710 4-Nitrophenol U J0 J3 J6 0.0587 0.372 1 01/19/2018 01:09 WG1062710 Pentachlorophenol U 0.0536 0.372 1 01/19/2018 01:09 WG1062710 Phenol U 0.00777 0.372 1 01/19/2018 01:09 WG1062710 2,4,6-Trichlorophenol U 0.00871 0.372 1 01/19/2018 01:09 WG1062710 (S) 2-Fluorophenol 68.2 20.0-120 01/19/2018 01:09 WG1062710 (S) Phenol-d5 61.2 20.0-120 01/19/2018 01:09 WG1062710 (S) Nitrobenzene-d5 53.0 18.0-125 01/19/2018 01:09 WG1062710 (S) 2-Fluorobiphenyl 62.0 28.0-120 01/19/2018 01:09 WG1062710 (S) 2,4,6-Tribromophenol 87.2 17.0-137 01/19/2018 01:09 WG1062710 (S) p-Terphenyl-d14 46.0 13.0-131 01/19/2018 01:09 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 43 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 43 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13 L963090 BF12 4-6 Collected date/time: 01/11/18 09:10 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 90.9 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0123 B J 0.00308 0.0220 1 01/17/2018 21:31 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic U 0.715 2.20 1 01/16/2018 03:10 WG1062607 Barium 36.6 0.187 0.550 1 01/16/2018 03:10 WG1062607 Cadmium U 0.0770 0.550 1 01/16/2018 03:10 WG1062607 Chromium 17.7 0.154 1.10 1 01/16/2018 03:10 WG1062607 Lead 5.51 0.209 0.550 1 01/16/2018 03:10 WG1062607 Selenium U 0.814 2.20 1 01/16/2018 03:10 WG1062607 Silver U 0.308 1.10 1 01/16/2018 03:10 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0110 0.0550 1 01/14/2018 17:16 WG1062672 Acrylonitrile U 0.00197 0.0110 1 01/14/2018 17:16 WG1062672 Benzene U 0.000297 0.00110 1 01/14/2018 17:16 WG1062672 Bromobenzene U 0.000313 0.00110 1 01/14/2018 17:16 WG1062672 Bromodichloromethane U 0.000280 0.00110 1 01/14/2018 17:16 WG1062672 Bromoform U 0.000467 0.00110 1 01/14/2018 17:16 WG1062672 Bromomethane U 0.00147 0.00550 1 01/14/2018 17:16 WG1062672 n-Butylbenzene U 0.000284 0.00110 1 01/14/2018 17:16 WG1062672 sec-Butylbenzene U 0.000221 0.00110 1 01/14/2018 17:16 WG1062672 tert-Butylbenzene U 0.000227 0.00110 1 01/14/2018 17:16 WG1062672 Carbon tetrachloride U 0.000361 0.00110 1 01/14/2018 17:16 WG1062672 Chlorobenzene U 0.000233 0.00110 1 01/14/2018 17:16 WG1062672 Chlorodibromomethane U 0.000411 0.00110 1 01/14/2018 17:16 WG1062672 Chloroethane U 0.00104 0.00550 1 01/14/2018 17:16 WG1062672 Chloroform U 0.000252 0.00550 1 01/14/2018 17:16 WG1062672 Chloromethane U 0.000413 0.00275 1 01/14/2018 17:16 WG1062672 2-Chlorotoluene U 0.000331 0.00110 1 01/14/2018 17:16 WG1062672 4-Chlorotoluene U 0.000264 0.00110 1 01/14/2018 17:16 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00116 0.00550 1 01/14/2018 17:16 WG1062672 1,2-Dibromoethane U 0.000378 0.00110 1 01/14/2018 17:16 WG1062672 Dibromomethane U 0.000420 0.00110 1 01/14/2018 17:16 WG1062672 1,2-Dichlorobenzene U 0.000336 0.00110 1 01/14/2018 17:16 WG1062672 1,3-Dichlorobenzene U 0.000263 0.00110 1 01/14/2018 17:16 WG1062672 1,4-Dichlorobenzene U 0.000249 0.00110 1 01/14/2018 17:16 WG1062672 Dichlorodifluoromethane U 0.000785 0.00550 1 01/14/2018 17:16 WG1062672 1,1-Dichloroethane U 0.000219 0.00110 1 01/14/2018 17:16 WG1062672 1,2-Dichloroethane U 0.000292 0.00110 1 01/14/2018 17:16 WG1062672 1,1-Dichloroethene U 0.000333 0.00110 1 01/14/2018 17:16 WG1062672 cis-1,2-Dichloroethene U 0.000259 0.00110 1 01/14/2018 17:16 WG1062672 trans-1,2-Dichloroethene U 0.000291 0.00110 1 01/14/2018 17:16 WG1062672 1,2-Dichloropropane U 0.000394 0.00110 1 01/14/2018 17:16 WG1062672 1,1-Dichloropropene U 0.000349 0.00110 1 01/14/2018 17:16 WG1062672 1,3-Dichloropropane U 0.000228 0.00110 1 01/14/2018 17:16 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 44 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 44 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13 L963090 BF12 4-6 Collected date/time: 01/11/18 09:10 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000288 0.00110 1 01/14/2018 17:16 WG1062672 trans-1,3-Dichloropropene U 0.000294 0.00110 1 01/14/2018 17:16 WG1062672 2,2-Dichloropropane U 0.000307 0.00110 1 01/14/2018 17:16 WG1062672 Di-isopropyl ether U 0.000273 0.00110 1 01/14/2018 17:16 WG1062672 Ethylbenzene U 0.000327 0.00110 1 01/14/2018 17:16 WG1062672 Hexachloro-1,3-butadiene U 0.000376 0.00110 1 01/14/2018 17:16 WG1062672 Isopropylbenzene U 0.000267 0.00110 1 01/14/2018 17:16 WG1062672 p-Isopropyltoluene U 0.000225 0.00110 1 01/14/2018 17:16 WG1062672 2-Butanone (MEK)U 0.00515 0.0110 1 01/14/2018 17:16 WG1062672 Methylene Chloride U 0.00110 0.00550 1 01/14/2018 17:16 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00207 0.0110 1 01/14/2018 17:16 WG1062672 Methyl tert-butyl ether U 0.000233 0.00110 1 01/14/2018 17:16 WG1062672 Naphthalene U 0.00110 0.00550 1 01/14/2018 17:16 WG1062672 n-Propylbenzene U 0.000227 0.00110 1 01/14/2018 17:16 WG1062672 Styrene U 0.000258 0.00110 1 01/14/2018 17:16 WG1062672 1,1,1,2-Tetrachloroethane U 0.000291 0.00110 1 01/14/2018 17:16 WG1062672 1,1,2,2-Tetrachloroethane U 0.000402 0.00110 1 01/14/2018 17:16 WG1062672 Tetrachloroethene U 0.000304 0.00110 1 01/14/2018 17:16 WG1062672 Toluene U 0.000478 0.00550 1 01/14/2018 17:16 WG1062672 1,2,3-Trichlorobenzene U 0.000337 0.00110 1 01/14/2018 17:16 WG1062672 1,2,4-Trichlorobenzene U 0.000427 0.00110 1 01/14/2018 17:16 WG1062672 1,1,1-Trichloroethane U 0.000315 0.00110 1 01/14/2018 17:16 WG1062672 1,1,2-Trichloroethane U 0.000305 0.00110 1 01/14/2018 17:16 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000402 0.00110 1 01/14/2018 17:16 WG1062672 Trichloroethene U 0.000307 0.00110 1 01/14/2018 17:16 WG1062672 Trichlorofluoromethane U 0.000420 0.00550 1 01/14/2018 17:16 WG1062672 1,2,3-Trichloropropane U 0.000816 0.00275 1 01/14/2018 17:16 WG1062672 1,2,4-Trimethylbenzene U 0.000232 0.00110 1 01/14/2018 17:16 WG1062672 1,3,5-Trimethylbenzene U 0.000293 0.00110 1 01/14/2018 17:16 WG1062672 Vinyl chloride U 0.000320 0.00110 1 01/14/2018 17:16 WG1062672 Xylenes, Total U 0.000768 0.00330 1 01/14/2018 17:16 WG1062672 (S) Toluene-d8 95.3 80.0-120 01/14/2018 17:16 WG1062672 (S) Dibromofluoromethane 106 74.0-131 01/14/2018 17:16 WG1062672 (S) 4-Bromofluorobenzene 96.4 64.0-132 01/14/2018 17:16 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00707 0.0363 1 01/19/2018 02:19 WG1062710 Acenaphthylene U 0.00739 0.0363 1 01/19/2018 02:19 WG1062710 Anthracene U 0.00696 0.0363 1 01/19/2018 02:19 WG1062710 Benzidine U J4 0.0701 0.367 1 01/19/2018 02:19 WG1062710 Benzo(a)anthracene U 0.00471 0.0363 1 01/19/2018 02:19 WG1062710 Benzo(b)fluoranthene U 0.00765 0.0363 1 01/19/2018 02:19 WG1062710 Benzo(k)fluoranthene U 0.00641 0.0363 1 01/19/2018 02:19 WG1062710 Benzo(g,h,i)perylene U 0.00794 0.0363 1 01/19/2018 02:19 WG1062710 Benzo(a)pyrene U 0.00603 0.0363 1 01/19/2018 02:19 WG1062710 Bis(2-chlorethoxy)methane U 0.00848 0.367 1 01/19/2018 02:19 WG1062710 Bis(2-chloroethyl)ether U 0.00986 0.367 1 01/19/2018 02:19 WG1062710 Bis(2-chloroisopropyl)ether U 0.00837 0.367 1 01/19/2018 02:19 WG1062710 4-Bromophenyl-phenylether U 0.0125 0.367 1 01/19/2018 02:19 WG1062710 2-Chloronaphthalene U 0.00703 0.0363 1 01/19/2018 02:19 WG1062710 4-Chlorophenyl-phenylether U 0.00690 0.367 1 01/19/2018 02:19 WG1062710 Chrysene U 0.00611 0.0363 1 01/19/2018 02:19 WG1062710 Dibenz(a,h)anthracene U 0.00904 0.0363 1 01/19/2018 02:19 WG1062710 3,3-Dichlorobenzidine U 0.0874 0.367 1 01/19/2018 02:19 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 45 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 45 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13 L963090 BF12 4-6 Collected date/time: 01/11/18 09:10 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00668 0.367 1 01/19/2018 02:19 WG1062710 2,6-Dinitrotoluene U 0.00811 0.367 1 01/19/2018 02:19 WG1062710 Fluoranthene U 0.00546 0.0363 1 01/19/2018 02:19 WG1062710 Fluorene U 0.00751 0.0363 1 01/19/2018 02:19 WG1062710 Hexachlorobenzene U 0.00942 0.367 1 01/19/2018 02:19 WG1062710 Hexachloro-1,3-butadiene U 0.0110 0.367 1 01/19/2018 02:19 WG1062710 Hexachlorocyclopentadiene U J0 0.0646 0.367 1 01/19/2018 02:19 WG1062710 Hexachloroethane U 0.0147 0.367 1 01/19/2018 02:19 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00850 0.0363 1 01/19/2018 02:19 WG1062710 Isophorone U 0.00575 0.367 1 01/19/2018 02:19 WG1062710 Naphthalene U 0.00978 0.0363 1 01/19/2018 02:19 WG1062710 Nitrobenzene U 0.00765 0.367 1 01/19/2018 02:19 WG1062710 n-Nitrosodimethylamine U 0.0712 0.367 1 01/19/2018 02:19 WG1062710 n-Nitrosodiphenylamine U 0.00654 0.367 1 01/19/2018 02:19 WG1062710 n-Nitrosodi-n-propylamine U 0.00997 0.367 1 01/19/2018 02:19 WG1062710 Phenanthrene U 0.00581 0.0363 1 01/19/2018 02:19 WG1062710 Benzylbutyl phthalate U 0.0113 0.367 1 01/19/2018 02:19 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0132 0.367 1 01/19/2018 02:19 WG1062710 Di-n-butyl phthalate U 0.0120 0.367 1 01/19/2018 02:19 WG1062710 Diethyl phthalate U 0.00761 0.367 1 01/19/2018 02:19 WG1062710 Dimethyl phthalate U 0.00594 0.367 1 01/19/2018 02:19 WG1062710 Di-n-octyl phthalate U 0.00998 0.367 1 01/19/2018 02:19 WG1062710 Pyrene U 0.0135 0.0363 1 01/19/2018 02:19 WG1062710 1,2,4-Trichlorobenzene U 0.00964 0.367 1 01/19/2018 02:19 WG1062710 4-Chloro-3-methylphenol U 0.00525 0.367 1 01/19/2018 02:19 WG1062710 2-Chlorophenol U 0.00915 0.367 1 01/19/2018 02:19 WG1062710 2,4-Dichlorophenol U 0.00821 0.367 1 01/19/2018 02:19 WG1062710 2,4-Dimethylphenol U 0.0518 0.367 1 01/19/2018 02:19 WG1062710 4,6-Dinitro-2-methylphenol U 0.136 0.367 1 01/19/2018 02:19 WG1062710 2,4-Dinitrophenol U 0.108 0.367 1 01/19/2018 02:19 WG1062710 2-Nitrophenol U 0.0143 0.367 1 01/19/2018 02:19 WG1062710 4-Nitrophenol U J0 0.0578 0.367 1 01/19/2018 02:19 WG1062710 Pentachlorophenol U 0.0528 0.367 1 01/19/2018 02:19 WG1062710 Phenol U 0.00765 0.367 1 01/19/2018 02:19 WG1062710 2,4,6-Trichlorophenol U 0.00857 0.367 1 01/19/2018 02:19 WG1062710 (S) 2-Fluorophenol 80.0 20.0-120 01/19/2018 02:19 WG1062710 (S) Phenol-d5 70.0 20.0-120 01/19/2018 02:19 WG1062710 (S) Nitrobenzene-d5 61.4 18.0-125 01/19/2018 02:19 WG1062710 (S) 2-Fluorobiphenyl 71.0 28.0-120 01/19/2018 02:19 WG1062710 (S) 2,4,6-Tribromophenol 94.0 17.0-137 01/19/2018 02:19 WG1062710 (S) p-Terphenyl-d14 57.2 13.0-131 01/19/2018 02:19 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 46 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 46 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14 L963090 BF12 9-11 Collected date/time: 01/11/18 09:20 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 86.6 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.00723 B J 0.00323 0.0231 1 01/17/2018 21:33 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic U 0.750 2.31 1 01/16/2018 03:20 WG1062607 Barium 32.1 0.196 0.577 1 01/16/2018 03:20 WG1062607 Cadmium 0.0954 J 0.0808 0.577 1 01/16/2018 03:20 WG1062607 Chromium 3.51 0.162 1.15 1 01/16/2018 03:20 WG1062607 Lead 11.0 0.219 0.577 1 01/16/2018 03:20 WG1062607 Selenium U 0.854 2.31 1 01/16/2018 03:20 WG1062607 Silver U 0.323 1.15 1 01/16/2018 03:20 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0115 0.0577 1 01/14/2018 17:35 WG1062672 Acrylonitrile U 0.00207 0.0115 1 01/14/2018 17:35 WG1062672 Benzene 0.00695 0.000312 0.00115 1 01/14/2018 17:35 WG1062672 Bromobenzene U 0.000328 0.00115 1 01/14/2018 17:35 WG1062672 Bromodichloromethane U 0.000293 0.00115 1 01/14/2018 17:35 WG1062672 Bromoform U 0.000489 0.00115 1 01/14/2018 17:35 WG1062672 Bromomethane U 0.00155 0.00577 1 01/14/2018 17:35 WG1062672 n-Butylbenzene U 0.000298 0.00115 1 01/14/2018 17:35 WG1062672 sec-Butylbenzene U 0.000232 0.00115 1 01/14/2018 17:35 WG1062672 tert-Butylbenzene U 0.000238 0.00115 1 01/14/2018 17:35 WG1062672 Carbon tetrachloride U 0.000379 0.00115 1 01/14/2018 17:35 WG1062672 Chlorobenzene U 0.000245 0.00115 1 01/14/2018 17:35 WG1062672 Chlorodibromomethane U 0.000431 0.00115 1 01/14/2018 17:35 WG1062672 Chloroethane U 0.00109 0.00577 1 01/14/2018 17:35 WG1062672 Chloroform U 0.000264 0.00577 1 01/14/2018 17:35 WG1062672 Chloromethane U 0.000433 0.00289 1 01/14/2018 17:35 WG1062672 2-Chlorotoluene U 0.000347 0.00115 1 01/14/2018 17:35 WG1062672 4-Chlorotoluene U 0.000277 0.00115 1 01/14/2018 17:35 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00121 0.00577 1 01/14/2018 17:35 WG1062672 1,2-Dibromoethane U 0.000396 0.00115 1 01/14/2018 17:35 WG1062672 Dibromomethane U 0.000441 0.00115 1 01/14/2018 17:35 WG1062672 1,2-Dichlorobenzene U 0.000352 0.00115 1 01/14/2018 17:35 WG1062672 1,3-Dichlorobenzene U 0.000276 0.00115 1 01/14/2018 17:35 WG1062672 1,4-Dichlorobenzene U 0.000261 0.00115 1 01/14/2018 17:35 WG1062672 Dichlorodifluoromethane U 0.000823 0.00577 1 01/14/2018 17:35 WG1062672 1,1-Dichloroethane U 0.000230 0.00115 1 01/14/2018 17:35 WG1062672 1,2-Dichloroethane U 0.000306 0.00115 1 01/14/2018 17:35 WG1062672 1,1-Dichloroethene U 0.000350 0.00115 1 01/14/2018 17:35 WG1062672 cis-1,2-Dichloroethene 0.00396 0.000271 0.00115 1 01/14/2018 17:35 WG1062672 trans-1,2-Dichloroethene U 0.000305 0.00115 1 01/14/2018 17:35 WG1062672 1,2-Dichloropropane U 0.000413 0.00115 1 01/14/2018 17:35 WG1062672 1,1-Dichloropropene U 0.000366 0.00115 1 01/14/2018 17:35 WG1062672 1,3-Dichloropropane U 0.000239 0.00115 1 01/14/2018 17:35 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 47 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 47 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14 L963090 BF12 9-11 Collected date/time: 01/11/18 09:20 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000302 0.00115 1 01/14/2018 17:35 WG1062672 trans-1,3-Dichloropropene U 0.000308 0.00115 1 01/14/2018 17:35 WG1062672 2,2-Dichloropropane U 0.000322 0.00115 1 01/14/2018 17:35 WG1062672 Di-isopropyl ether U 0.000286 0.00115 1 01/14/2018 17:35 WG1062672 Ethylbenzene 0.00185 0.000343 0.00115 1 01/14/2018 17:35 WG1062672 Hexachloro-1,3-butadiene U 0.000395 0.00115 1 01/14/2018 17:35 WG1062672 Isopropylbenzene 0.000597 J 0.000280 0.00115 1 01/14/2018 17:35 WG1062672 p-Isopropyltoluene U 0.000235 0.00115 1 01/14/2018 17:35 WG1062672 2-Butanone (MEK)U 0.00540 0.0115 1 01/14/2018 17:35 WG1062672 Methylene Chloride U 0.00115 0.00577 1 01/14/2018 17:35 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00217 0.0115 1 01/14/2018 17:35 WG1062672 Methyl tert-butyl ether U 0.000245 0.00115 1 01/14/2018 17:35 WG1062672 Naphthalene U 0.00115 0.00577 1 01/14/2018 17:35 WG1062672 n-Propylbenzene 0.000467 J 0.000238 0.00115 1 01/14/2018 17:35 WG1062672 Styrene U 0.000270 0.00115 1 01/14/2018 17:35 WG1062672 1,1,1,2-Tetrachloroethane U 0.000305 0.00115 1 01/14/2018 17:35 WG1062672 1,1,2,2-Tetrachloroethane U 0.000421 0.00115 1 01/14/2018 17:35 WG1062672 Tetrachloroethene U 0.000319 0.00115 1 01/14/2018 17:35 WG1062672 Toluene 0.000814 J 0.000501 0.00577 1 01/14/2018 17:35 WG1062672 1,2,3-Trichlorobenzene U 0.000353 0.00115 1 01/14/2018 17:35 WG1062672 1,2,4-Trichlorobenzene U 0.000448 0.00115 1 01/14/2018 17:35 WG1062672 1,1,1-Trichloroethane U 0.000330 0.00115 1 01/14/2018 17:35 WG1062672 1,1,2-Trichloroethane U 0.000320 0.00115 1 01/14/2018 17:35 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000421 0.00115 1 01/14/2018 17:35 WG1062672 Trichloroethene U 0.000322 0.00115 1 01/14/2018 17:35 WG1062672 Trichlorofluoromethane U 0.000441 0.00577 1 01/14/2018 17:35 WG1062672 1,2,3-Trichloropropane U 0.000855 0.00289 1 01/14/2018 17:35 WG1062672 1,2,4-Trimethylbenzene U 0.000244 0.00115 1 01/14/2018 17:35 WG1062672 1,3,5-Trimethylbenzene U 0.000307 0.00115 1 01/14/2018 17:35 WG1062672 Vinyl chloride U 0.000336 0.00115 1 01/14/2018 17:35 WG1062672 Xylenes, Total 0.00395 0.000806 0.00346 1 01/14/2018 17:35 WG1062672 (S) Toluene-d8 94.3 80.0-120 01/14/2018 17:35 WG1062672 (S) Dibromofluoromethane 106 74.0-131 01/14/2018 17:35 WG1062672 (S) 4-Bromofluorobenzene 96.0 64.0-132 01/14/2018 17:35 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00741 0.0381 1 01/19/2018 02:42 WG1062710 Acenaphthylene U 0.00774 0.0381 1 01/19/2018 02:42 WG1062710 Anthracene U 0.00729 0.0381 1 01/19/2018 02:42 WG1062710 Benzidine U J4 0.0735 0.384 1 01/19/2018 02:42 WG1062710 Benzo(a)anthracene U 0.00494 0.0381 1 01/19/2018 02:42 WG1062710 Benzo(b)fluoranthene U 0.00802 0.0381 1 01/19/2018 02:42 WG1062710 Benzo(k)fluoranthene U 0.00672 0.0381 1 01/19/2018 02:42 WG1062710 Benzo(g,h,i)perylene U 0.00832 0.0381 1 01/19/2018 02:42 WG1062710 Benzo(a)pyrene U 0.00633 0.0381 1 01/19/2018 02:42 WG1062710 Bis(2-chlorethoxy)methane U 0.00889 0.384 1 01/19/2018 02:42 WG1062710 Bis(2-chloroethyl)ether U 0.0103 0.384 1 01/19/2018 02:42 WG1062710 Bis(2-chloroisopropyl)ether U 0.00877 0.384 1 01/19/2018 02:42 WG1062710 4-Bromophenyl-phenylether U 0.0132 0.384 1 01/19/2018 02:42 WG1062710 2-Chloronaphthalene U 0.00738 0.0381 1 01/19/2018 02:42 WG1062710 4-Chlorophenyl-phenylether U 0.00724 0.384 1 01/19/2018 02:42 WG1062710 Chrysene U 0.00641 0.0381 1 01/19/2018 02:42 WG1062710 Dibenz(a,h)anthracene U 0.00948 0.0381 1 01/19/2018 02:42 WG1062710 3,3-Dichlorobenzidine U 0.0916 0.384 1 01/19/2018 02:42 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 48 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 48 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14 L963090 BF12 9-11 Collected date/time: 01/11/18 09:20 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.00701 0.384 1 01/19/2018 02:42 WG1062710 2,6-Dinitrotoluene U 0.00851 0.384 1 01/19/2018 02:42 WG1062710 Fluoranthene U 0.00573 0.0381 1 01/19/2018 02:42 WG1062710 Fluorene U 0.00787 0.0381 1 01/19/2018 02:42 WG1062710 Hexachlorobenzene U 0.00988 0.384 1 01/19/2018 02:42 WG1062710 Hexachloro-1,3-butadiene U 0.0115 0.384 1 01/19/2018 02:42 WG1062710 Hexachlorocyclopentadiene U J0 0.0678 0.384 1 01/19/2018 02:42 WG1062710 Hexachloroethane U 0.0155 0.384 1 01/19/2018 02:42 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00891 0.0381 1 01/19/2018 02:42 WG1062710 Isophorone U 0.00603 0.384 1 01/19/2018 02:42 WG1062710 Naphthalene U 0.0103 0.0381 1 01/19/2018 02:42 WG1062710 Nitrobenzene U 0.00802 0.384 1 01/19/2018 02:42 WG1062710 n-Nitrosodimethylamine U 0.0747 0.384 1 01/19/2018 02:42 WG1062710 n-Nitrosodiphenylamine U 0.00686 0.384 1 01/19/2018 02:42 WG1062710 n-Nitrosodi-n-propylamine U 0.0105 0.384 1 01/19/2018 02:42 WG1062710 Phenanthrene U 0.00609 0.0381 1 01/19/2018 02:42 WG1062710 Benzylbutyl phthalate U 0.0119 0.384 1 01/19/2018 02:42 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0139 0.384 1 01/19/2018 02:42 WG1062710 Di-n-butyl phthalate U 0.0126 0.384 1 01/19/2018 02:42 WG1062710 Diethyl phthalate U 0.00798 0.384 1 01/19/2018 02:42 WG1062710 Dimethyl phthalate U 0.00623 0.384 1 01/19/2018 02:42 WG1062710 Di-n-octyl phthalate U 0.0105 0.384 1 01/19/2018 02:42 WG1062710 Pyrene U 0.0142 0.0381 1 01/19/2018 02:42 WG1062710 1,2,4-Trichlorobenzene U 0.0101 0.384 1 01/19/2018 02:42 WG1062710 4-Chloro-3-methylphenol U 0.00551 0.384 1 01/19/2018 02:42 WG1062710 2-Chlorophenol U 0.00959 0.384 1 01/19/2018 02:42 WG1062710 2,4-Dichlorophenol U 0.00861 0.384 1 01/19/2018 02:42 WG1062710 2,4-Dimethylphenol U 0.0544 0.384 1 01/19/2018 02:42 WG1062710 4,6-Dinitro-2-methylphenol U 0.143 0.384 1 01/19/2018 02:42 WG1062710 2,4-Dinitrophenol U 0.113 0.384 1 01/19/2018 02:42 WG1062710 2-Nitrophenol U 0.0150 0.384 1 01/19/2018 02:42 WG1062710 4-Nitrophenol U J0 0.0606 0.384 1 01/19/2018 02:42 WG1062710 Pentachlorophenol U 0.0554 0.384 1 01/19/2018 02:42 WG1062710 Phenol U 0.00802 0.384 1 01/19/2018 02:42 WG1062710 2,4,6-Trichlorophenol U 0.00899 0.384 1 01/19/2018 02:42 WG1062710 (S) 2-Fluorophenol 77.2 20.0-120 01/19/2018 02:42 WG1062710 (S) Phenol-d5 66.0 20.0-120 01/19/2018 02:42 WG1062710 (S) Nitrobenzene-d5 61.4 18.0-125 01/19/2018 02:42 WG1062710 (S) 2-Fluorobiphenyl 69.6 28.0-120 01/19/2018 02:42 WG1062710 (S) 2,4,6-Tribromophenol 90.4 17.0-137 01/19/2018 02:42 WG1062710 (S) p-Terphenyl-d14 54.6 13.0-131 01/19/2018 02:42 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 49 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 49 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15 L963090 BF13 1-3 Collected date/time: 01/11/18 09:40 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 79.0 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0181 B J 0.00354 0.0253 1 01/17/2018 21:36 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 0.925 J 0.823 2.53 1 01/16/2018 03:23 WG1062607 Barium 107 0.215 0.633 1 01/16/2018 03:23 WG1062607 Cadmium 0.101 J 0.0886 0.633 1 01/16/2018 03:23 WG1062607 Chromium 27.3 0.177 1.27 1 01/16/2018 03:23 WG1062607 Lead 4.21 0.241 0.633 1 01/16/2018 03:23 WG1062607 Selenium U 0.937 2.53 1 01/16/2018 03:23 WG1062607 Silver U 0.354 1.27 1 01/16/2018 03:23 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0127 0.0633 1 01/14/2018 17:55 WG1062672 Acrylonitrile U 0.00227 0.0127 1 01/14/2018 17:55 WG1062672 Benzene U 0.000342 0.00127 1 01/14/2018 17:55 WG1062672 Bromobenzene U 0.000360 0.00127 1 01/14/2018 17:55 WG1062672 Bromodichloromethane U 0.000322 0.00127 1 01/14/2018 17:55 WG1062672 Bromoform U 0.000537 0.00127 1 01/14/2018 17:55 WG1062672 Bromomethane U 0.00170 0.00633 1 01/14/2018 17:55 WG1062672 n-Butylbenzene U 0.000327 0.00127 1 01/14/2018 17:55 WG1062672 sec-Butylbenzene U 0.000254 0.00127 1 01/14/2018 17:55 WG1062672 tert-Butylbenzene U 0.000261 0.00127 1 01/14/2018 17:55 WG1062672 Carbon tetrachloride U 0.000415 0.00127 1 01/14/2018 17:55 WG1062672 Chlorobenzene U 0.000268 0.00127 1 01/14/2018 17:55 WG1062672 Chlorodibromomethane U 0.000472 0.00127 1 01/14/2018 17:55 WG1062672 Chloroethane U 0.00120 0.00633 1 01/14/2018 17:55 WG1062672 Chloroform U 0.000290 0.00633 1 01/14/2018 17:55 WG1062672 Chloromethane U 0.000475 0.00316 1 01/14/2018 17:55 WG1062672 2-Chlorotoluene U 0.000381 0.00127 1 01/14/2018 17:55 WG1062672 4-Chlorotoluene U 0.000304 0.00127 1 01/14/2018 17:55 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00133 0.00633 1 01/14/2018 17:55 WG1062672 1,2-Dibromoethane U 0.000434 0.00127 1 01/14/2018 17:55 WG1062672 Dibromomethane U 0.000484 0.00127 1 01/14/2018 17:55 WG1062672 1,2-Dichlorobenzene U 0.000386 0.00127 1 01/14/2018 17:55 WG1062672 1,3-Dichlorobenzene U 0.000303 0.00127 1 01/14/2018 17:55 WG1062672 1,4-Dichlorobenzene U 0.000286 0.00127 1 01/14/2018 17:55 WG1062672 Dichlorodifluoromethane U 0.000903 0.00633 1 01/14/2018 17:55 WG1062672 1,1-Dichloroethane U 0.000252 0.00127 1 01/14/2018 17:55 WG1062672 1,2-Dichloroethane U 0.000335 0.00127 1 01/14/2018 17:55 WG1062672 1,1-Dichloroethene U 0.000384 0.00127 1 01/14/2018 17:55 WG1062672 cis-1,2-Dichloroethene U 0.000297 0.00127 1 01/14/2018 17:55 WG1062672 trans-1,2-Dichloroethene U 0.000334 0.00127 1 01/14/2018 17:55 WG1062672 1,2-Dichloropropane U 0.000453 0.00127 1 01/14/2018 17:55 WG1062672 1,1-Dichloropropene U 0.000401 0.00127 1 01/14/2018 17:55 WG1062672 1,3-Dichloropropane U 0.000262 0.00127 1 01/14/2018 17:55 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 50 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 50 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15 L963090 BF13 1-3 Collected date/time: 01/11/18 09:40 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000332 0.00127 1 01/14/2018 17:55 WG1062672 trans-1,3-Dichloropropene U 0.000338 0.00127 1 01/14/2018 17:55 WG1062672 2,2-Dichloropropane U 0.000353 0.00127 1 01/14/2018 17:55 WG1062672 Di-isopropyl ether U 0.000314 0.00127 1 01/14/2018 17:55 WG1062672 Ethylbenzene U 0.000376 0.00127 1 01/14/2018 17:55 WG1062672 Hexachloro-1,3-butadiene U 0.000433 0.00127 1 01/14/2018 17:55 WG1062672 Isopropylbenzene U 0.000308 0.00127 1 01/14/2018 17:55 WG1062672 p-Isopropyltoluene U 0.000258 0.00127 1 01/14/2018 17:55 WG1062672 2-Butanone (MEK)U 0.00592 0.0127 1 01/14/2018 17:55 WG1062672 Methylene Chloride U 0.00127 0.00633 1 01/14/2018 17:55 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00238 0.0127 1 01/14/2018 17:55 WG1062672 Methyl tert-butyl ether U 0.000268 0.00127 1 01/14/2018 17:55 WG1062672 Naphthalene U 0.00127 0.00633 1 01/14/2018 17:55 WG1062672 n-Propylbenzene U 0.000261 0.00127 1 01/14/2018 17:55 WG1062672 Styrene U 0.000296 0.00127 1 01/14/2018 17:55 WG1062672 1,1,1,2-Tetrachloroethane U 0.000334 0.00127 1 01/14/2018 17:55 WG1062672 1,1,2,2-Tetrachloroethane U 0.000462 0.00127 1 01/14/2018 17:55 WG1062672 Tetrachloroethene U 0.000349 0.00127 1 01/14/2018 17:55 WG1062672 Toluene U 0.000549 0.00633 1 01/14/2018 17:55 WG1062672 1,2,3-Trichlorobenzene U 0.000387 0.00127 1 01/14/2018 17:55 WG1062672 1,2,4-Trichlorobenzene U 0.000491 0.00127 1 01/14/2018 17:55 WG1062672 1,1,1-Trichloroethane U 0.000362 0.00127 1 01/14/2018 17:55 WG1062672 1,1,2-Trichloroethane U 0.000351 0.00127 1 01/14/2018 17:55 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000462 0.00127 1 01/14/2018 17:55 WG1062672 Trichloroethene U 0.000353 0.00127 1 01/14/2018 17:55 WG1062672 Trichlorofluoromethane U 0.000484 0.00633 1 01/14/2018 17:55 WG1062672 1,2,3-Trichloropropane U 0.000938 0.00316 1 01/14/2018 17:55 WG1062672 1,2,4-Trimethylbenzene U 0.000267 0.00127 1 01/14/2018 17:55 WG1062672 1,3,5-Trimethylbenzene U 0.000337 0.00127 1 01/14/2018 17:55 WG1062672 Vinyl chloride U 0.000368 0.00127 1 01/14/2018 17:55 WG1062672 Xylenes, Total U 0.000884 0.00380 1 01/14/2018 17:55 WG1062672 (S) Toluene-d8 92.9 80.0-120 01/14/2018 17:55 WG1062672 (S) Dibromofluoromethane 110 74.0-131 01/14/2018 17:55 WG1062672 (S) 4-Bromofluorobenzene 99.5 64.0-132 01/14/2018 17:55 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.162 0.836 20 01/19/2018 05:02 WG1062710 Acenaphthylene U 0.170 0.836 20 01/19/2018 05:02 WG1062710 Anthracene U 0.160 0.836 20 01/19/2018 05:02 WG1062710 Benzidine U J4 1.61 8.43 20 01/19/2018 05:02 WG1062710 Benzo(a)anthracene U 0.108 0.836 20 01/19/2018 05:02 WG1062710 Benzo(b)fluoranthene U 0.176 0.836 20 01/19/2018 05:02 WG1062710 Benzo(k)fluoranthene U 0.147 0.836 20 01/19/2018 05:02 WG1062710 Benzo(g,h,i)perylene U 0.182 0.836 20 01/19/2018 05:02 WG1062710 Benzo(a)pyrene U 0.139 0.836 20 01/19/2018 05:02 WG1062710 Bis(2-chlorethoxy)methane U 0.195 8.43 20 01/19/2018 05:02 WG1062710 Bis(2-chloroethyl)ether U 0.227 8.43 20 01/19/2018 05:02 WG1062710 Bis(2-chloroisopropyl)ether U 0.192 8.43 20 01/19/2018 05:02 WG1062710 4-Bromophenyl-phenylether U 0.289 8.43 20 01/19/2018 05:02 WG1062710 2-Chloronaphthalene U 0.162 0.836 20 01/19/2018 05:02 WG1062710 4-Chlorophenyl-phenylether U 0.158 8.43 20 01/19/2018 05:02 WG1062710 Chrysene U 0.141 0.836 20 01/19/2018 05:02 WG1062710 Dibenz(a,h)anthracene U 0.208 0.836 20 01/19/2018 05:02 WG1062710 3,3-Dichlorobenzidine U 2.01 8.43 20 01/19/2018 05:02 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 51 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 51 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15 L963090 BF13 1-3 Collected date/time: 01/11/18 09:40 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.153 8.43 20 01/19/2018 05:02 WG1062710 2,6-Dinitrotoluene U 0.186 8.43 20 01/19/2018 05:02 WG1062710 Fluoranthene U 0.126 0.836 20 01/19/2018 05:02 WG1062710 Fluorene U 0.172 0.836 20 01/19/2018 05:02 WG1062710 Hexachlorobenzene U 0.216 8.43 20 01/19/2018 05:02 WG1062710 Hexachloro-1,3-butadiene U 0.253 8.43 20 01/19/2018 05:02 WG1062710 Hexachlorocyclopentadiene U J0 1.48 8.43 20 01/19/2018 05:02 WG1062710 Hexachloroethane U 0.339 8.43 20 01/19/2018 05:02 WG1062710 Indeno(1,2,3-cd)pyrene U 0.195 0.836 20 01/19/2018 05:02 WG1062710 Isophorone U 0.132 8.43 20 01/19/2018 05:02 WG1062710 Naphthalene U 0.225 0.836 20 01/19/2018 05:02 WG1062710 Nitrobenzene U 0.176 8.43 20 01/19/2018 05:02 WG1062710 n-Nitrosodimethylamine U 1.63 8.43 20 01/19/2018 05:02 WG1062710 n-Nitrosodiphenylamine U 0.151 8.43 20 01/19/2018 05:02 WG1062710 n-Nitrosodi-n-propylamine U 0.229 8.43 20 01/19/2018 05:02 WG1062710 Phenanthrene U 0.134 0.836 20 01/19/2018 05:02 WG1062710 Benzylbutyl phthalate U 0.261 8.43 20 01/19/2018 05:02 WG1062710 Bis(2-ethylhexyl)phthalate U 0.304 8.43 20 01/19/2018 05:02 WG1062710 Di-n-butyl phthalate U 0.276 8.43 20 01/19/2018 05:02 WG1062710 Diethyl phthalate U 0.175 8.43 20 01/19/2018 05:02 WG1062710 Dimethyl phthalate U 0.137 8.43 20 01/19/2018 05:02 WG1062710 Di-n-octyl phthalate U 0.229 8.43 20 01/19/2018 05:02 WG1062710 Pyrene U 0.311 0.836 20 01/19/2018 05:02 WG1062710 1,2,4-Trichlorobenzene U 0.222 8.43 20 01/19/2018 05:02 WG1062710 4-Chloro-3-methylphenol U 0.121 8.43 20 01/19/2018 05:02 WG1062710 2-Chlorophenol U 0.210 8.43 20 01/19/2018 05:02 WG1062710 2,4-Dichlorophenol U 0.189 8.43 20 01/19/2018 05:02 WG1062710 2,4-Dimethylphenol U 1.19 8.43 20 01/19/2018 05:02 WG1062710 4,6-Dinitro-2-methylphenol U 3.14 8.43 20 01/19/2018 05:02 WG1062710 2,4-Dinitrophenol U 2.48 8.43 20 01/19/2018 05:02 WG1062710 2-Nitrophenol U 0.329 8.43 20 01/19/2018 05:02 WG1062710 4-Nitrophenol U J0 1.33 8.43 20 01/19/2018 05:02 WG1062710 Pentachlorophenol U 1.22 8.43 20 01/19/2018 05:02 WG1062710 Phenol U 0.176 8.43 20 01/19/2018 05:02 WG1062710 2,4,6-Trichlorophenol U 0.197 8.43 20 01/19/2018 05:02 WG1062710 (S) 2-Fluorophenol 52.4 J7 20.0-120 01/19/2018 05:02 WG1062710 (S) Phenol-d5 53.2 J7 20.0-120 01/19/2018 05:02 WG1062710 (S) Nitrobenzene-d5 44.0 J7 18.0-125 01/19/2018 05:02 WG1062710 (S) 2-Fluorobiphenyl 59.0 J7 28.0-120 01/19/2018 05:02 WG1062710 (S) 2,4,6-Tribromophenol 61.6 J7 17.0-137 01/19/2018 05:02 WG1062710 (S) p-Terphenyl-d14 43.2 J7 13.0-131 01/19/2018 05:02 WG1062710 Sample Narrative: L963090-15 WG1062710: Dilution due to matrix 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 52 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 52 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16 L963090 BF13 4-5 Collected date/time: 01/11/18 09:50 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 84.7 1 01/17/2018 10:09 WG1063380 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.00757 B J 0.00331 0.0236 1 01/17/2018 21:39 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic U 0.767 2.36 1 01/16/2018 03:27 WG1062607 Barium 68.8 0.201 0.590 1 01/16/2018 03:27 WG1062607 Cadmium U 0.0826 0.590 1 01/16/2018 03:27 WG1062607 Chromium 36.2 0.165 1.18 1 01/16/2018 03:27 WG1062607 Lead 5.85 0.224 0.590 1 01/16/2018 03:27 WG1062607 Selenium U 0.874 2.36 1 01/16/2018 03:27 WG1062607 Silver U 0.331 1.18 1 01/16/2018 03:27 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 1.18 5.90 100 01/14/2018 19:33 WG1062672 Acrylonitrile U 0.211 1.18 100 01/14/2018 19:33 WG1062672 Benzene U 0.0319 0.118 100 01/14/2018 19:33 WG1062672 Bromobenzene U 0.0335 0.118 100 01/14/2018 19:33 WG1062672 Bromodichloromethane U 0.0300 0.118 100 01/14/2018 19:33 WG1062672 Bromoform U 0.0501 0.118 100 01/14/2018 19:33 WG1062672 Bromomethane U 0.158 0.590 100 01/14/2018 19:33 WG1062672 n-Butylbenzene 0.670 0.0305 0.118 100 01/14/2018 19:33 WG1062672 sec-Butylbenzene 0.235 0.0237 0.118 100 01/14/2018 19:33 WG1062672 tert-Butylbenzene U 0.0243 0.118 100 01/14/2018 19:33 WG1062672 Carbon tetrachloride U 0.0387 0.118 100 01/14/2018 19:33 WG1062672 Chlorobenzene U 0.0250 0.118 100 01/14/2018 19:33 WG1062672 Chlorodibromomethane U 0.0440 0.118 100 01/14/2018 19:33 WG1062672 Chloroethane U 0.112 0.590 100 01/14/2018 19:33 WG1062672 Chloroform U 0.0270 0.590 100 01/14/2018 19:33 WG1062672 Chloromethane U 0.0443 0.295 100 01/14/2018 19:33 WG1062672 2-Chlorotoluene U 0.0355 0.118 100 01/14/2018 19:33 WG1062672 4-Chlorotoluene U 0.0283 0.118 100 01/14/2018 19:33 WG1062672 1,2-Dibromo-3-Chloropropane U 0.124 0.590 100 01/14/2018 19:33 WG1062672 1,2-Dibromoethane U 0.0405 0.118 100 01/14/2018 19:33 WG1062672 Dibromomethane U 0.0451 0.118 100 01/14/2018 19:33 WG1062672 1,2-Dichlorobenzene U 0.0360 0.118 100 01/14/2018 19:33 WG1062672 1,3-Dichlorobenzene U 0.0282 0.118 100 01/14/2018 19:33 WG1062672 1,4-Dichlorobenzene U 0.0267 0.118 100 01/14/2018 19:33 WG1062672 Dichlorodifluoromethane U 0.0842 0.590 100 01/14/2018 19:33 WG1062672 1,1-Dichloroethane U 0.0235 0.118 100 01/14/2018 19:33 WG1062672 1,2-Dichloroethane U 0.0313 0.118 100 01/14/2018 19:33 WG1062672 1,1-Dichloroethene U 0.0358 0.118 100 01/14/2018 19:33 WG1062672 cis-1,2-Dichloroethene U 0.0277 0.118 100 01/14/2018 19:33 WG1062672 trans-1,2-Dichloroethene U 0.0312 0.118 100 01/14/2018 19:33 WG1062672 1,2-Dichloropropane U 0.0423 0.118 100 01/14/2018 19:33 WG1062672 1,1-Dichloropropene U 0.0374 0.118 100 01/14/2018 19:33 WG1062672 1,3-Dichloropropane U 0.0244 0.118 100 01/14/2018 19:33 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 53 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 53 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16 L963090 BF13 4-5 Collected date/time: 01/11/18 09:50 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.0309 0.118 100 01/14/2018 19:33 WG1062672 trans-1,3-Dichloropropene U 0.0315 0.118 100 01/14/2018 19:33 WG1062672 2,2-Dichloropropane U 0.0329 0.118 100 01/14/2018 19:33 WG1062672 Di-isopropyl ether U 0.0293 0.118 100 01/14/2018 19:33 WG1062672 Ethylbenzene 0.539 0.0351 0.118 100 01/14/2018 19:33 WG1062672 Hexachloro-1,3-butadiene U 0.0404 0.118 100 01/14/2018 19:33 WG1062672 Isopropylbenzene 0.261 0.0287 0.118 100 01/14/2018 19:33 WG1062672 p-Isopropyltoluene 0.0734 J 0.0241 0.118 100 01/14/2018 19:33 WG1062672 2-Butanone (MEK)U 0.552 1.18 100 01/14/2018 19:33 WG1062672 Methylene Chloride U 0.118 0.590 100 01/14/2018 19:33 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.222 1.18 100 01/14/2018 19:33 WG1062672 Methyl tert-butyl ether U 0.0250 0.118 100 01/14/2018 19:33 WG1062672 Naphthalene 0.169 J 0.118 0.590 100 01/14/2018 19:33 WG1062672 n-Propylbenzene 1.33 0.0243 0.118 100 01/14/2018 19:33 WG1062672 Styrene U 0.0276 0.118 100 01/14/2018 19:33 WG1062672 1,1,1,2-Tetrachloroethane U 0.0312 0.118 100 01/14/2018 19:33 WG1062672 1,1,2,2-Tetrachloroethane U 0.0431 0.118 100 01/14/2018 19:33 WG1062672 Tetrachloroethene U 0.0326 0.118 100 01/14/2018 19:33 WG1062672 Toluene U 0.0512 0.590 100 01/14/2018 19:33 WG1062672 1,2,3-Trichlorobenzene U 0.0361 0.118 100 01/14/2018 19:33 WG1062672 1,2,4-Trichlorobenzene U 0.0458 0.118 100 01/14/2018 19:33 WG1062672 1,1,1-Trichloroethane U 0.0338 0.118 100 01/14/2018 19:33 WG1062672 1,1,2-Trichloroethane U 0.0327 0.118 100 01/14/2018 19:33 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.0431 0.118 100 01/14/2018 19:33 WG1062672 Trichloroethene U 0.0329 0.118 100 01/14/2018 19:33 WG1062672 Trichlorofluoromethane U 0.0451 0.590 100 01/14/2018 19:33 WG1062672 1,2,3-Trichloropropane U 0.0875 0.295 100 01/14/2018 19:33 WG1062672 1,2,4-Trimethylbenzene 2.85 0.0249 0.118 100 01/14/2018 19:33 WG1062672 1,3,5-Trimethylbenzene 1.10 0.0314 0.118 100 01/14/2018 19:33 WG1062672 Vinyl chloride U 0.0344 0.118 100 01/14/2018 19:33 WG1062672 Xylenes, Total 0.391 0.0824 0.354 100 01/14/2018 19:33 WG1062672 (S) Toluene-d8 100 80.0-120 01/14/2018 19:33 WG1062672 (S) Dibromofluoromethane 100 74.0-131 01/14/2018 19:33 WG1062672 (S) 4-Bromofluorobenzene 99.3 64.0-132 01/14/2018 19:33 WG1062672 Sample Narrative: L963090-16 WG1062672: Non-target compounds too high to run at a lower dilution. Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00758 0.0390 1 01/19/2018 03:05 WG1062710 Acenaphthylene U 0.00792 0.0390 1 01/19/2018 03:05 WG1062710 Anthracene U 0.00746 0.0390 1 01/19/2018 03:05 WG1062710 Benzidine U J4 0.0752 0.393 1 01/19/2018 03:05 WG1062710 Benzo(a)anthracene U 0.00505 0.0390 1 01/19/2018 03:05 WG1062710 Benzo(b)fluoranthene U 0.00820 0.0390 1 01/19/2018 03:05 WG1062710 Benzo(k)fluoranthene U 0.00687 0.0390 1 01/19/2018 03:05 WG1062710 Benzo(g,h,i)perylene U 0.00851 0.0390 1 01/19/2018 03:05 WG1062710 Benzo(a)pyrene U 0.00647 0.0390 1 01/19/2018 03:05 WG1062710 Bis(2-chlorethoxy)methane U 0.00909 0.393 1 01/19/2018 03:05 WG1062710 Bis(2-chloroethyl)ether U 0.0106 0.393 1 01/19/2018 03:05 WG1062710 Bis(2-chloroisopropyl)ether U 0.00897 0.393 1 01/19/2018 03:05 WG1062710 4-Bromophenyl-phenylether U 0.0135 0.393 1 01/19/2018 03:05 WG1062710 2-Chloronaphthalene U 0.00754 0.0390 1 01/19/2018 03:05 WG1062710 4-Chlorophenyl-phenylether U 0.00740 0.393 1 01/19/2018 03:05 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 54 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 54 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16 L963090 BF13 4-5 Collected date/time: 01/11/18 09:50 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Chrysene U 0.00655 0.0390 1 01/19/2018 03:05 WG1062710 Dibenz(a,h)anthracene U 0.00969 0.0390 1 01/19/2018 03:05 WG1062710 3,3-Dichlorobenzidine U 0.0937 0.393 1 01/19/2018 03:05 WG1062710 2,4-Dinitrotoluene U 0.00717 0.393 1 01/19/2018 03:05 WG1062710 2,6-Dinitrotoluene U 0.00870 0.393 1 01/19/2018 03:05 WG1062710 Fluoranthene U 0.00586 0.0390 1 01/19/2018 03:05 WG1062710 Fluorene U 0.00805 0.0390 1 01/19/2018 03:05 WG1062710 Hexachlorobenzene U 0.0101 0.393 1 01/19/2018 03:05 WG1062710 Hexachloro-1,3-butadiene U 0.0118 0.393 1 01/19/2018 03:05 WG1062710 Hexachlorocyclopentadiene U J0 0.0693 0.393 1 01/19/2018 03:05 WG1062710 Hexachloroethane U 0.0158 0.393 1 01/19/2018 03:05 WG1062710 Indeno(1,2,3-cd)pyrene U 0.00911 0.0390 1 01/19/2018 03:05 WG1062710 Isophorone U 0.00616 0.393 1 01/19/2018 03:05 WG1062710 Naphthalene 0.193 0.0105 0.0390 1 01/19/2018 03:05 WG1062710 Nitrobenzene U 0.00820 0.393 1 01/19/2018 03:05 WG1062710 n-Nitrosodimethylamine U 0.0764 0.393 1 01/19/2018 03:05 WG1062710 n-Nitrosodiphenylamine U 0.00701 0.393 1 01/19/2018 03:05 WG1062710 n-Nitrosodi-n-propylamine U 0.0107 0.393 1 01/19/2018 03:05 WG1062710 Phenanthrene U 0.00623 0.0390 1 01/19/2018 03:05 WG1062710 Benzylbutyl phthalate U 0.0122 0.393 1 01/19/2018 03:05 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0142 0.393 1 01/19/2018 03:05 WG1062710 Di-n-butyl phthalate U 0.0129 0.393 1 01/19/2018 03:05 WG1062710 Diethyl phthalate U 0.00816 0.393 1 01/19/2018 03:05 WG1062710 Dimethyl phthalate U 0.00637 0.393 1 01/19/2018 03:05 WG1062710 Di-n-octyl phthalate U 0.0107 0.393 1 01/19/2018 03:05 WG1062710 Pyrene U 0.0145 0.0390 1 01/19/2018 03:05 WG1062710 1,2,4-Trichlorobenzene U 0.0103 0.393 1 01/19/2018 03:05 WG1062710 4-Chloro-3-methylphenol U 0.00563 0.393 1 01/19/2018 03:05 WG1062710 2-Chlorophenol U 0.00981 0.393 1 01/19/2018 03:05 WG1062710 2,4-Dichlorophenol U 0.00881 0.393 1 01/19/2018 03:05 WG1062710 2,4-Dimethylphenol U 0.0556 0.393 1 01/19/2018 03:05 WG1062710 4,6-Dinitro-2-methylphenol U 0.146 0.393 1 01/19/2018 03:05 WG1062710 2,4-Dinitrophenol U 0.116 0.393 1 01/19/2018 03:05 WG1062710 2-Nitrophenol U 0.0153 0.393 1 01/19/2018 03:05 WG1062710 4-Nitrophenol U J0 0.0620 0.393 1 01/19/2018 03:05 WG1062710 Pentachlorophenol U 0.0567 0.393 1 01/19/2018 03:05 WG1062710 Phenol U 0.00820 0.393 1 01/19/2018 03:05 WG1062710 2,4,6-Trichlorophenol U 0.00920 0.393 1 01/19/2018 03:05 WG1062710 (S) 2-Fluorophenol 76.0 20.0-120 01/19/2018 03:05 WG1062710 (S) Phenol-d5 69.4 20.0-120 01/19/2018 03:05 WG1062710 (S) Nitrobenzene-d5 59.4 18.0-125 01/19/2018 03:05 WG1062710 (S) 2-Fluorobiphenyl 66.4 28.0-120 01/19/2018 03:05 WG1062710 (S) 2,4,6-Tribromophenol 100 17.0-137 01/19/2018 03:05 WG1062710 (S) p-Terphenyl-d14 54.8 13.0-131 01/19/2018 03:05 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 55 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 55 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17 L963090 BF13 8-10 Collected date/time: 01/11/18 10:00 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 62.9 1 01/17/2018 10:33 WG1063382 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.00822 B J 0.00445 0.0318 1 01/17/2018 21:41 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic U 1.03 3.18 1 01/16/2018 03:30 WG1062607 Barium 182 0.270 0.795 1 01/16/2018 03:30 WG1062607 Cadmium 0.180 J 0.111 0.795 1 01/16/2018 03:30 WG1062607 Chromium 22.2 0.222 1.59 1 01/16/2018 03:30 WG1062607 Lead 2.83 0.302 0.795 1 01/16/2018 03:30 WG1062607 Selenium U 1.18 3.18 1 01/16/2018 03:30 WG1062607 Silver U 0.445 1.59 1 01/16/2018 03:30 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.397 1.99 25 01/14/2018 19:52 WG1062672 Acrylonitrile U 0.0712 0.397 25 01/14/2018 19:52 WG1062672 Benzene 0.339 0.0107 0.0397 25 01/14/2018 19:52 WG1062672 Bromobenzene U 0.0113 0.0397 25 01/14/2018 19:52 WG1062672 Bromodichloromethane U 0.0101 0.0397 25 01/14/2018 19:52 WG1062672 Bromoform U 0.0168 0.0397 25 01/14/2018 19:52 WG1062672 Bromomethane U 0.0532 0.199 25 01/14/2018 19:52 WG1062672 n-Butylbenzene U 0.0102 0.0397 25 01/14/2018 19:52 WG1062672 sec-Butylbenzene U 0.00798 0.0397 25 01/14/2018 19:52 WG1062672 tert-Butylbenzene U 0.00818 0.0397 25 01/14/2018 19:52 WG1062672 Carbon tetrachloride U 0.0130 0.0397 25 01/14/2018 19:52 WG1062672 Chlorobenzene U 0.00842 0.0397 25 01/14/2018 19:52 WG1062672 Chlorodibromomethane U 0.0148 0.0397 25 01/14/2018 19:52 WG1062672 Chloroethane U 0.0375 0.199 25 01/14/2018 19:52 WG1062672 Chloroform U 0.00909 0.199 25 01/14/2018 19:52 WG1062672 Chloromethane U 0.0149 0.0993 25 01/14/2018 19:52 WG1062672 2-Chlorotoluene U 0.0119 0.0397 25 01/14/2018 19:52 WG1062672 4-Chlorotoluene U 0.00953 0.0397 25 01/14/2018 19:52 WG1062672 1,2-Dibromo-3-Chloropropane U 0.0416 0.199 25 01/14/2018 19:52 WG1062672 1,2-Dibromoethane U 0.0136 0.0397 25 01/14/2018 19:52 WG1062672 Dibromomethane U 0.0152 0.0397 25 01/14/2018 19:52 WG1062672 1,2-Dichlorobenzene U 0.0121 0.0397 25 01/14/2018 19:52 WG1062672 1,3-Dichlorobenzene U 0.00950 0.0397 25 01/14/2018 19:52 WG1062672 1,4-Dichlorobenzene U 0.00898 0.0397 25 01/14/2018 19:52 WG1062672 Dichlorodifluoromethane U 0.0283 0.199 25 01/14/2018 19:52 WG1062672 1,1-Dichloroethane U 0.00791 0.0397 25 01/14/2018 19:52 WG1062672 1,2-Dichloroethane U 0.0105 0.0397 25 01/14/2018 19:52 WG1062672 1,1-Dichloroethene U 0.0120 0.0397 25 01/14/2018 19:52 WG1062672 cis-1,2-Dichloroethene U 0.00934 0.0397 25 01/14/2018 19:52 WG1062672 trans-1,2-Dichloroethene U 0.0105 0.0397 25 01/14/2018 19:52 WG1062672 1,2-Dichloropropane U 0.0142 0.0397 25 01/14/2018 19:52 WG1062672 1,1-Dichloropropene U 0.0126 0.0397 25 01/14/2018 19:52 WG1062672 1,3-Dichloropropane U 0.00823 0.0397 25 01/14/2018 19:52 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 56 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 56 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17 L963090 BF13 8-10 Collected date/time: 01/11/18 10:00 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.0104 0.0397 25 01/14/2018 19:52 WG1062672 trans-1,3-Dichloropropene U 0.0106 0.0397 25 01/14/2018 19:52 WG1062672 2,2-Dichloropropane U 0.0111 0.0397 25 01/14/2018 19:52 WG1062672 Di-isopropyl ether U 0.00985 0.0397 25 01/14/2018 19:52 WG1062672 Ethylbenzene 0.0203 J 0.0118 0.0397 25 01/14/2018 19:52 WG1062672 Hexachloro-1,3-butadiene U 0.0136 0.0397 25 01/14/2018 19:52 WG1062672 Isopropylbenzene 0.0180 J 0.00966 0.0397 25 01/14/2018 19:52 WG1062672 p-Isopropyltoluene U 0.00810 0.0397 25 01/14/2018 19:52 WG1062672 2-Butanone (MEK)U 0.186 0.397 25 01/14/2018 19:52 WG1062672 Methylene Chloride U 0.0397 0.199 25 01/14/2018 19:52 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.0747 0.397 25 01/14/2018 19:52 WG1062672 Methyl tert-butyl ether U 0.00842 0.0397 25 01/14/2018 19:52 WG1062672 Naphthalene U 0.0397 0.199 25 01/14/2018 19:52 WG1062672 n-Propylbenzene 0.00945 J 0.00818 0.0397 25 01/14/2018 19:52 WG1062672 Styrene U 0.00930 0.0397 25 01/14/2018 19:52 WG1062672 1,1,1,2-Tetrachloroethane U 0.0105 0.0397 25 01/14/2018 19:52 WG1062672 1,1,2,2-Tetrachloroethane U 0.0145 0.0397 25 01/14/2018 19:52 WG1062672 Tetrachloroethene U 0.0110 0.0397 25 01/14/2018 19:52 WG1062672 Toluene 0.0785 J 0.0172 0.199 25 01/14/2018 19:52 WG1062672 1,2,3-Trichlorobenzene U 0.0122 0.0397 25 01/14/2018 19:52 WG1062672 1,2,4-Trichlorobenzene U 0.0154 0.0397 25 01/14/2018 19:52 WG1062672 1,1,1-Trichloroethane U 0.0114 0.0397 25 01/14/2018 19:52 WG1062672 1,1,2-Trichloroethane U 0.0110 0.0397 25 01/14/2018 19:52 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.0145 0.0397 25 01/14/2018 19:52 WG1062672 Trichloroethene U 0.0111 0.0397 25 01/14/2018 19:52 WG1062672 Trichlorofluoromethane U 0.0152 0.199 25 01/14/2018 19:52 WG1062672 1,2,3-Trichloropropane U 0.0294 0.0993 25 01/14/2018 19:52 WG1062672 1,2,4-Trimethylbenzene 0.0133 J 0.00839 0.0397 25 01/14/2018 19:52 WG1062672 1,3,5-Trimethylbenzene U 0.0106 0.0397 25 01/14/2018 19:52 WG1062672 Vinyl chloride U 0.0116 0.0397 25 01/14/2018 19:52 WG1062672 Xylenes, Total 0.0649 J 0.0277 0.119 25 01/14/2018 19:52 WG1062672 (S) Toluene-d8 100 80.0-120 01/14/2018 19:52 WG1062672 (S) Dibromofluoromethane 97.1 74.0-131 01/14/2018 19:52 WG1062672 (S) 4-Bromofluorobenzene 100 64.0-132 01/14/2018 19:52 WG1062672 Sample Narrative: L963090-17 WG1062672: Non-target compounds too high to run at a lower dilution. Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.0102 0.0524 1 01/19/2018 03:29 WG1062710 Acenaphthylene U 0.0107 0.0524 1 01/19/2018 03:29 WG1062710 Anthracene U 0.0100 0.0524 1 01/19/2018 03:29 WG1062710 Benzidine U J4 0.101 0.529 1 01/19/2018 03:29 WG1062710 Benzo(a)anthracene U 0.00680 0.0524 1 01/19/2018 03:29 WG1062710 Benzo(b)fluoranthene U 0.0110 0.0524 1 01/19/2018 03:29 WG1062710 Benzo(k)fluoranthene U 0.00925 0.0524 1 01/19/2018 03:29 WG1062710 Benzo(g,h,i)perylene U 0.0115 0.0524 1 01/19/2018 03:29 WG1062710 Benzo(a)pyrene U 0.00871 0.0524 1 01/19/2018 03:29 WG1062710 Bis(2-chlorethoxy)methane U 0.0122 0.529 1 01/19/2018 03:29 WG1062710 Bis(2-chloroethyl)ether U 0.0142 0.529 1 01/19/2018 03:29 WG1062710 Bis(2-chloroisopropyl)ether U 0.0121 0.529 1 01/19/2018 03:29 WG1062710 4-Bromophenyl-phenylether U 0.0181 0.529 1 01/19/2018 03:29 WG1062710 2-Chloronaphthalene U 0.0102 0.0524 1 01/19/2018 03:29 WG1062710 4-Chlorophenyl-phenylether U 0.00996 0.529 1 01/19/2018 03:29 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 57 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 57 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17 L963090 BF13 8-10 Collected date/time: 01/11/18 10:00 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Chrysene U 0.00882 0.0524 1 01/19/2018 03:29 WG1062710 Dibenz(a,h)anthracene U 0.0130 0.0524 1 01/19/2018 03:29 WG1062710 3,3-Dichlorobenzidine U 0.126 0.529 1 01/19/2018 03:29 WG1062710 2,4-Dinitrotoluene U 0.00965 0.529 1 01/19/2018 03:29 WG1062710 2,6-Dinitrotoluene U 0.0117 0.529 1 01/19/2018 03:29 WG1062710 Fluoranthene U 0.00788 0.0524 1 01/19/2018 03:29 WG1062710 Fluorene U 0.0108 0.0524 1 01/19/2018 03:29 WG1062710 Hexachlorobenzene U 0.0136 0.529 1 01/19/2018 03:29 WG1062710 Hexachloro-1,3-butadiene U 0.0159 0.529 1 01/19/2018 03:29 WG1062710 Hexachlorocyclopentadiene U J0 0.0933 0.529 1 01/19/2018 03:29 WG1062710 Hexachloroethane U 0.0213 0.529 1 01/19/2018 03:29 WG1062710 Indeno(1,2,3-cd)pyrene U 0.0123 0.0524 1 01/19/2018 03:29 WG1062710 Isophorone U 0.00830 0.529 1 01/19/2018 03:29 WG1062710 Naphthalene U 0.0141 0.0524 1 01/19/2018 03:29 WG1062710 Nitrobenzene U 0.0110 0.529 1 01/19/2018 03:29 WG1062710 n-Nitrosodimethylamine U 0.103 0.529 1 01/19/2018 03:29 WG1062710 n-Nitrosodiphenylamine U 0.00944 0.529 1 01/19/2018 03:29 WG1062710 n-Nitrosodi-n-propylamine U 0.0144 0.529 1 01/19/2018 03:29 WG1062710 Phenanthrene U 0.00839 0.0524 1 01/19/2018 03:29 WG1062710 Benzylbutyl phthalate U 0.0164 0.529 1 01/19/2018 03:29 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0191 0.529 1 01/19/2018 03:29 WG1062710 Di-n-butyl phthalate U 0.0173 0.529 1 01/19/2018 03:29 WG1062710 Diethyl phthalate U 0.0110 0.529 1 01/19/2018 03:29 WG1062710 Dimethyl phthalate U 0.00858 0.529 1 01/19/2018 03:29 WG1062710 Di-n-octyl phthalate U 0.0144 0.529 1 01/19/2018 03:29 WG1062710 Pyrene U 0.0195 0.0524 1 01/19/2018 03:29 WG1062710 1,2,4-Trichlorobenzene U 0.0139 0.529 1 01/19/2018 03:29 WG1062710 4-Chloro-3-methylphenol U 0.00758 0.529 1 01/19/2018 03:29 WG1062710 2-Chlorophenol U 0.0132 0.529 1 01/19/2018 03:29 WG1062710 2,4-Dichlorophenol U 0.0119 0.529 1 01/19/2018 03:29 WG1062710 2,4-Dimethylphenol U 0.0748 0.529 1 01/19/2018 03:29 WG1062710 4,6-Dinitro-2-methylphenol U 0.197 0.529 1 01/19/2018 03:29 WG1062710 2,4-Dinitrophenol U 0.156 0.529 1 01/19/2018 03:29 WG1062710 2-Nitrophenol U 0.0207 0.529 1 01/19/2018 03:29 WG1062710 4-Nitrophenol U J0 0.0834 0.529 1 01/19/2018 03:29 WG1062710 Pentachlorophenol U 0.0763 0.529 1 01/19/2018 03:29 WG1062710 Phenol U 0.0110 0.529 1 01/19/2018 03:29 WG1062710 2,4,6-Trichlorophenol U 0.0124 0.529 1 01/19/2018 03:29 WG1062710 (S) 2-Fluorophenol 72.8 20.0-120 01/19/2018 03:29 WG1062710 (S) Phenol-d5 65.2 20.0-120 01/19/2018 03:29 WG1062710 (S) Nitrobenzene-d5 58.4 18.0-125 01/19/2018 03:29 WG1062710 (S) 2-Fluorobiphenyl 65.0 28.0-120 01/19/2018 03:29 WG1062710 (S) 2,4,6-Tribromophenol 87.0 17.0-137 01/19/2018 03:29 WG1062710 (S) p-Terphenyl-d14 60.6 13.0-131 01/19/2018 03:29 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 58 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 58 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18 L963090 BF6 0.5-1.5 Collected date/time: 01/11/18 08:50 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 86.2 1 01/17/2018 10:33 WG1063382 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.0134 B J 0.00325 0.0232 1 01/17/2018 21:44 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic 0.845 J 0.754 2.32 1 01/16/2018 03:33 WG1062607 Barium 103 0.197 0.580 1 01/16/2018 03:33 WG1062607 Cadmium 0.0918 J 0.0812 0.580 1 01/16/2018 03:33 WG1062607 Chromium 25.1 0.162 1.16 1 01/16/2018 03:33 WG1062607 Lead 5.15 0.221 0.580 1 01/16/2018 03:33 WG1062607 Selenium U 0.859 2.32 1 01/16/2018 03:33 WG1062607 Silver U 0.325 1.16 1 01/16/2018 03:33 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone 0.0320 J 0.0116 0.0580 1 01/14/2018 18:15 WG1062672 Acrylonitrile U 0.00208 0.0116 1 01/14/2018 18:15 WG1062672 Benzene U 0.000313 0.00116 1 01/14/2018 18:15 WG1062672 Bromobenzene U 0.000330 0.00116 1 01/14/2018 18:15 WG1062672 Bromodichloromethane U 0.000295 0.00116 1 01/14/2018 18:15 WG1062672 Bromoform U 0.000492 0.00116 1 01/14/2018 18:15 WG1062672 Bromomethane U 0.00156 0.00580 1 01/14/2018 18:15 WG1062672 n-Butylbenzene U 0.000299 0.00116 1 01/14/2018 18:15 WG1062672 sec-Butylbenzene U 0.000233 0.00116 1 01/14/2018 18:15 WG1062672 tert-Butylbenzene U 0.000239 0.00116 1 01/14/2018 18:15 WG1062672 Carbon tetrachloride U 0.000381 0.00116 1 01/14/2018 18:15 WG1062672 Chlorobenzene U 0.000246 0.00116 1 01/14/2018 18:15 WG1062672 Chlorodibromomethane U 0.000433 0.00116 1 01/14/2018 18:15 WG1062672 Chloroethane U 0.00110 0.00580 1 01/14/2018 18:15 WG1062672 Chloroform U 0.000266 0.00580 1 01/14/2018 18:15 WG1062672 Chloromethane U 0.000435 0.00290 1 01/14/2018 18:15 WG1062672 2-Chlorotoluene U 0.000349 0.00116 1 01/14/2018 18:15 WG1062672 4-Chlorotoluene U 0.000279 0.00116 1 01/14/2018 18:15 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00122 0.00580 1 01/14/2018 18:15 WG1062672 1,2-Dibromoethane U 0.000398 0.00116 1 01/14/2018 18:15 WG1062672 Dibromomethane U 0.000443 0.00116 1 01/14/2018 18:15 WG1062672 1,2-Dichlorobenzene U 0.000354 0.00116 1 01/14/2018 18:15 WG1062672 1,3-Dichlorobenzene U 0.000277 0.00116 1 01/14/2018 18:15 WG1062672 1,4-Dichlorobenzene U 0.000262 0.00116 1 01/14/2018 18:15 WG1062672 Dichlorodifluoromethane U 0.000828 0.00580 1 01/14/2018 18:15 WG1062672 1,1-Dichloroethane U 0.000231 0.00116 1 01/14/2018 18:15 WG1062672 1,2-Dichloroethane U 0.000308 0.00116 1 01/14/2018 18:15 WG1062672 1,1-Dichloroethene U 0.000352 0.00116 1 01/14/2018 18:15 WG1062672 cis-1,2-Dichloroethene U 0.000273 0.00116 1 01/14/2018 18:15 WG1062672 trans-1,2-Dichloroethene U 0.000306 0.00116 1 01/14/2018 18:15 WG1062672 1,2-Dichloropropane U 0.000416 0.00116 1 01/14/2018 18:15 WG1062672 1,1-Dichloropropene U 0.000368 0.00116 1 01/14/2018 18:15 WG1062672 1,3-Dichloropropane U 0.000240 0.00116 1 01/14/2018 18:15 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 59 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 59 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18 L963090 BF6 0.5-1.5 Collected date/time: 01/11/18 08:50 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000304 0.00116 1 01/14/2018 18:15 WG1062672 trans-1,3-Dichloropropene U 0.000310 0.00116 1 01/14/2018 18:15 WG1062672 2,2-Dichloropropane U 0.000324 0.00116 1 01/14/2018 18:15 WG1062672 Di-isopropyl ether U 0.000288 0.00116 1 01/14/2018 18:15 WG1062672 Ethylbenzene U 0.000345 0.00116 1 01/14/2018 18:15 WG1062672 Hexachloro-1,3-butadiene U 0.000397 0.00116 1 01/14/2018 18:15 WG1062672 Isopropylbenzene U 0.000282 0.00116 1 01/14/2018 18:15 WG1062672 p-Isopropyltoluene U 0.000237 0.00116 1 01/14/2018 18:15 WG1062672 2-Butanone (MEK)0.00545 J 0.00543 0.0116 1 01/14/2018 18:15 WG1062672 Methylene Chloride U 0.00116 0.00580 1 01/14/2018 18:15 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00218 0.0116 1 01/14/2018 18:15 WG1062672 Methyl tert-butyl ether U 0.000246 0.00116 1 01/14/2018 18:15 WG1062672 Naphthalene U 0.00116 0.00580 1 01/14/2018 18:15 WG1062672 n-Propylbenzene U 0.000239 0.00116 1 01/14/2018 18:15 WG1062672 Styrene U 0.000272 0.00116 1 01/14/2018 18:15 WG1062672 1,1,1,2-Tetrachloroethane U 0.000306 0.00116 1 01/14/2018 18:15 WG1062672 1,1,2,2-Tetrachloroethane U 0.000424 0.00116 1 01/14/2018 18:15 WG1062672 Tetrachloroethene U 0.000320 0.00116 1 01/14/2018 18:15 WG1062672 Toluene U 0.000504 0.00580 1 01/14/2018 18:15 WG1062672 1,2,3-Trichlorobenzene U 0.000355 0.00116 1 01/14/2018 18:15 WG1062672 1,2,4-Trichlorobenzene U 0.000450 0.00116 1 01/14/2018 18:15 WG1062672 1,1,1-Trichloroethane U 0.000332 0.00116 1 01/14/2018 18:15 WG1062672 1,1,2-Trichloroethane U 0.000322 0.00116 1 01/14/2018 18:15 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000424 0.00116 1 01/14/2018 18:15 WG1062672 Trichloroethene U 0.000324 0.00116 1 01/14/2018 18:15 WG1062672 Trichlorofluoromethane U 0.000443 0.00580 1 01/14/2018 18:15 WG1062672 1,2,3-Trichloropropane U 0.000860 0.00290 1 01/14/2018 18:15 WG1062672 1,2,4-Trimethylbenzene U 0.000245 0.00116 1 01/14/2018 18:15 WG1062672 1,3,5-Trimethylbenzene U 0.000309 0.00116 1 01/14/2018 18:15 WG1062672 Vinyl chloride U 0.000338 0.00116 1 01/14/2018 18:15 WG1062672 Xylenes, Total U 0.000810 0.00348 1 01/14/2018 18:15 WG1062672 (S) Toluene-d8 92.2 80.0-120 01/14/2018 18:15 WG1062672 (S) Dibromofluoromethane 110 74.0-131 01/14/2018 18:15 WG1062672 (S) 4-Bromofluorobenzene 95.5 64.0-132 01/14/2018 18:15 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.149 0.766 20 01/19/2018 04:38 WG1062710 Acenaphthylene U 0.156 0.766 20 01/19/2018 04:38 WG1062710 Anthracene U 0.146 0.766 20 01/19/2018 04:38 WG1062710 Benzidine U J4 1.47 7.73 20 01/19/2018 04:38 WG1062710 Benzo(a)anthracene U 0.0994 0.766 20 01/19/2018 04:38 WG1062710 Benzo(b)fluoranthene U 0.161 0.766 20 01/19/2018 04:38 WG1062710 Benzo(k)fluoranthene U 0.135 0.766 20 01/19/2018 04:38 WG1062710 Benzo(g,h,i)perylene U 0.167 0.766 20 01/19/2018 04:38 WG1062710 Benzo(a)pyrene U 0.128 0.766 20 01/19/2018 04:38 WG1062710 Bis(2-chlorethoxy)methane U 0.179 7.73 20 01/19/2018 04:38 WG1062710 Bis(2-chloroethyl)ether U 0.208 7.73 20 01/19/2018 04:38 WG1062710 Bis(2-chloroisopropyl)ether U 0.176 7.73 20 01/19/2018 04:38 WG1062710 4-Bromophenyl-phenylether U 0.265 7.73 20 01/19/2018 04:38 WG1062710 2-Chloronaphthalene U 0.149 0.766 20 01/19/2018 04:38 WG1062710 4-Chlorophenyl-phenylether U 0.145 7.73 20 01/19/2018 04:38 WG1062710 Chrysene U 0.129 0.766 20 01/19/2018 04:38 WG1062710 Dibenz(a,h)anthracene U 0.190 0.766 20 01/19/2018 04:38 WG1062710 3,3-Dichlorobenzidine U 1.85 7.73 20 01/19/2018 04:38 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 60 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 60 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18 L963090 BF6 0.5-1.5 Collected date/time: 01/11/18 08:50 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time 2,4-Dinitrotoluene U 0.140 7.73 20 01/19/2018 04:38 WG1062710 2,6-Dinitrotoluene U 0.171 7.73 20 01/19/2018 04:38 WG1062710 Fluoranthene U 0.115 0.766 20 01/19/2018 04:38 WG1062710 Fluorene 1.14 0.158 0.766 20 01/19/2018 04:38 WG1062710 Hexachlorobenzene U 0.198 7.73 20 01/19/2018 04:38 WG1062710 Hexachloro-1,3-butadiene U 0.232 7.73 20 01/19/2018 04:38 WG1062710 Hexachlorocyclopentadiene U J0 1.36 7.73 20 01/19/2018 04:38 WG1062710 Hexachloroethane U 0.311 7.73 20 01/19/2018 04:38 WG1062710 Indeno(1,2,3-cd)pyrene U 0.179 0.766 20 01/19/2018 04:38 WG1062710 Isophorone U 0.121 7.73 20 01/19/2018 04:38 WG1062710 Naphthalene 4.49 0.207 0.766 20 01/19/2018 04:38 WG1062710 Nitrobenzene U 0.161 7.73 20 01/19/2018 04:38 WG1062710 n-Nitrosodimethylamine U 1.50 7.73 20 01/19/2018 04:38 WG1062710 n-Nitrosodiphenylamine U 0.138 7.73 20 01/19/2018 04:38 WG1062710 n-Nitrosodi-n-propylamine U 0.210 7.73 20 01/19/2018 04:38 WG1062710 Phenanthrene 0.126 J 0.123 0.766 20 01/19/2018 04:38 WG1062710 Benzylbutyl phthalate U 0.239 7.73 20 01/19/2018 04:38 WG1062710 Bis(2-ethylhexyl)phthalate U 0.279 7.73 20 01/19/2018 04:38 WG1062710 Di-n-butyl phthalate U 0.253 7.73 20 01/19/2018 04:38 WG1062710 Diethyl phthalate U 0.160 7.73 20 01/19/2018 04:38 WG1062710 Dimethyl phthalate U 0.125 7.73 20 01/19/2018 04:38 WG1062710 Di-n-octyl phthalate U 0.210 7.73 20 01/19/2018 04:38 WG1062710 Pyrene U 0.286 0.766 20 01/19/2018 04:38 WG1062710 1,2,4-Trichlorobenzene U 0.203 7.73 20 01/19/2018 04:38 WG1062710 4-Chloro-3-methylphenol U 0.111 7.73 20 01/19/2018 04:38 WG1062710 2-Chlorophenol U 0.193 7.73 20 01/19/2018 04:38 WG1062710 2,4-Dichlorophenol U 0.173 7.73 20 01/19/2018 04:38 WG1062710 2,4-Dimethylphenol U 1.09 7.73 20 01/19/2018 04:38 WG1062710 4,6-Dinitro-2-methylphenol U 2.88 7.73 20 01/19/2018 04:38 WG1062710 2,4-Dinitrophenol U 2.27 7.73 20 01/19/2018 04:38 WG1062710 2-Nitrophenol U 0.302 7.73 20 01/19/2018 04:38 WG1062710 4-Nitrophenol U J0 1.22 7.73 20 01/19/2018 04:38 WG1062710 Pentachlorophenol U 1.11 7.73 20 01/19/2018 04:38 WG1062710 Phenol U 0.161 7.73 20 01/19/2018 04:38 WG1062710 2,4,6-Trichlorophenol U 0.181 7.73 20 01/19/2018 04:38 WG1062710 (S) 2-Fluorophenol 66.2 J7 20.0-120 01/19/2018 04:38 WG1062710 (S) Phenol-d5 60.0 J7 20.0-120 01/19/2018 04:38 WG1062710 (S) Nitrobenzene-d5 97.6 J7 18.0-125 01/19/2018 04:38 WG1062710 (S) 2-Fluorobiphenyl 62.4 J7 28.0-120 01/19/2018 04:38 WG1062710 (S) 2,4,6-Tribromophenol 65.6 J7 17.0-137 01/19/2018 04:38 WG1062710 (S) p-Terphenyl-d14 57.2 J7 13.0-131 01/19/2018 04:38 WG1062710 Sample Narrative: L963090-18 WG1062710: Dilution due to matrix 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 61 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 61 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19 L963090 BF6 4-5 Collected date/time: 01/11/18 08:55 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 75.4 1 01/17/2018 10:33 WG1063382 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.00988 B J 0.00372 0.0265 1 01/17/2018 21:46 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic U 0.863 2.65 1 01/16/2018 03:37 WG1062607 Barium 44.1 0.226 0.664 1 01/16/2018 03:37 WG1062607 Cadmium U 0.0929 0.664 1 01/16/2018 03:37 WG1062607 Chromium 25.1 0.186 1.33 1 01/16/2018 03:37 WG1062607 Lead 6.81 0.252 0.664 1 01/16/2018 03:37 WG1062607 Selenium U 0.982 2.65 1 01/16/2018 03:37 WG1062607 Silver U 0.372 1.33 1 01/16/2018 03:37 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 2.65 13.3 200 01/14/2018 20:12 WG1062672 Acrylonitrile U 0.475 2.65 200 01/14/2018 20:12 WG1062672 Benzene U 0.0717 0.265 200 01/14/2018 20:12 WG1062672 Bromobenzene U 0.0754 0.265 200 01/14/2018 20:12 WG1062672 Bromodichloromethane U 0.0674 0.265 200 01/14/2018 20:12 WG1062672 Bromoform U 0.113 0.265 200 01/14/2018 20:12 WG1062672 Bromomethane U 0.356 1.33 200 01/14/2018 20:12 WG1062672 n-Butylbenzene 0.188 J 0.0685 0.265 200 01/14/2018 20:12 WG1062672 sec-Butylbenzene 0.0806 J 0.0534 0.265 200 01/14/2018 20:12 WG1062672 tert-Butylbenzene U 0.0547 0.265 200 01/14/2018 20:12 WG1062672 Carbon tetrachloride U 0.0871 0.265 200 01/14/2018 20:12 WG1062672 Chlorobenzene U 0.0563 0.265 200 01/14/2018 20:12 WG1062672 Chlorodibromomethane U 0.0990 0.265 200 01/14/2018 20:12 WG1062672 Chloroethane U 0.251 1.33 200 01/14/2018 20:12 WG1062672 Chloroform U 0.0608 1.33 200 01/14/2018 20:12 WG1062672 Chloromethane U 0.0995 0.664 200 01/14/2018 20:12 WG1062672 2-Chlorotoluene U 0.0799 0.265 200 01/14/2018 20:12 WG1062672 4-Chlorotoluene U 0.0637 0.265 200 01/14/2018 20:12 WG1062672 1,2-Dibromo-3-Chloropropane U 0.279 1.33 200 01/14/2018 20:12 WG1062672 1,2-Dibromoethane U 0.0910 0.265 200 01/14/2018 20:12 WG1062672 Dibromomethane U 0.101 0.265 200 01/14/2018 20:12 WG1062672 1,2-Dichlorobenzene U 0.0810 0.265 200 01/14/2018 20:12 WG1062672 1,3-Dichlorobenzene U 0.0634 0.265 200 01/14/2018 20:12 WG1062672 1,4-Dichlorobenzene U 0.0600 0.265 200 01/14/2018 20:12 WG1062672 Dichlorodifluoromethane U 0.190 1.33 200 01/14/2018 20:12 WG1062672 1,1-Dichloroethane U 0.0528 0.265 200 01/14/2018 20:12 WG1062672 1,2-Dichloroethane U 0.0703 0.265 200 01/14/2018 20:12 WG1062672 1,1-Dichloroethene U 0.0804 0.265 200 01/14/2018 20:12 WG1062672 cis-1,2-Dichloroethene U 0.0624 0.265 200 01/14/2018 20:12 WG1062672 trans-1,2-Dichloroethene U 0.0701 0.265 200 01/14/2018 20:12 WG1062672 1,2-Dichloropropane U 0.0950 0.265 200 01/14/2018 20:12 WG1062672 1,1-Dichloropropene U 0.0841 0.265 200 01/14/2018 20:12 WG1062672 1,3-Dichloropropane U 0.0549 0.265 200 01/14/2018 20:12 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 62 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 62 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19 L963090 BF6 4-5 Collected date/time: 01/11/18 08:55 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.0695 0.265 200 01/14/2018 20:12 WG1062672 trans-1,3-Dichloropropene U 0.0709 0.265 200 01/14/2018 20:12 WG1062672 2,2-Dichloropropane U 0.0741 0.265 200 01/14/2018 20:12 WG1062672 Di-isopropyl ether U 0.0658 0.265 200 01/14/2018 20:12 WG1062672 Ethylbenzene 0.526 0.0788 0.265 200 01/14/2018 20:12 WG1062672 Hexachloro-1,3-butadiene U 0.0908 0.265 200 01/14/2018 20:12 WG1062672 Isopropylbenzene 0.185 J 0.0645 0.265 200 01/14/2018 20:12 WG1062672 p-Isopropyltoluene 0.0627 J 0.0541 0.265 200 01/14/2018 20:12 WG1062672 2-Butanone (MEK)U 1.24 2.65 200 01/14/2018 20:12 WG1062672 Methylene Chloride U 0.265 1.33 200 01/14/2018 20:12 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.499 2.65 200 01/14/2018 20:12 WG1062672 Methyl tert-butyl ether U 0.0563 0.265 200 01/14/2018 20:12 WG1062672 Naphthalene 0.692 J 0.265 1.33 200 01/14/2018 20:12 WG1062672 n-Propylbenzene 0.528 0.0547 0.265 200 01/14/2018 20:12 WG1062672 Styrene U 0.0621 0.265 200 01/14/2018 20:12 WG1062672 1,1,1,2-Tetrachloroethane U 0.0701 0.265 200 01/14/2018 20:12 WG1062672 1,1,2,2-Tetrachloroethane U 0.0969 0.265 200 01/14/2018 20:12 WG1062672 Tetrachloroethene U 0.0733 0.265 200 01/14/2018 20:12 WG1062672 Toluene 0.140 J 0.115 1.33 200 01/14/2018 20:12 WG1062672 1,2,3-Trichlorobenzene U 0.0812 0.265 200 01/14/2018 20:12 WG1062672 1,2,4-Trichlorobenzene U 0.103 0.265 200 01/14/2018 20:12 WG1062672 1,1,1-Trichloroethane U 0.0759 0.265 200 01/14/2018 20:12 WG1062672 1,1,2-Trichloroethane U 0.0735 0.265 200 01/14/2018 20:12 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.0969 0.265 200 01/14/2018 20:12 WG1062672 Trichloroethene U 0.0741 0.265 200 01/14/2018 20:12 WG1062672 Trichlorofluoromethane U 0.101 1.33 200 01/14/2018 20:12 WG1062672 1,2,3-Trichloropropane U 0.196 0.664 200 01/14/2018 20:12 WG1062672 1,2,4-Trimethylbenzene 1.84 0.0560 0.265 200 01/14/2018 20:12 WG1062672 1,3,5-Trimethylbenzene 0.645 0.0706 0.265 200 01/14/2018 20:12 WG1062672 Vinyl chloride U 0.0772 0.265 200 01/14/2018 20:12 WG1062672 Xylenes, Total 1.80 0.186 0.796 200 01/14/2018 20:12 WG1062672 (S) Toluene-d8 99.3 80.0-120 01/14/2018 20:12 WG1062672 (S) Dibromofluoromethane 103 74.0-131 01/14/2018 20:12 WG1062672 (S) 4-Bromofluorobenzene 98.8 64.0-132 01/14/2018 20:12 WG1062672 Sample Narrative: L963090-19 WG1062672: Non-target compounds too high to run at a lower dilution. Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00852 0.0438 1 01/19/2018 03:52 WG1062710 Acenaphthylene U 0.00891 0.0438 1 01/19/2018 03:52 WG1062710 Anthracene U 0.00839 0.0438 1 01/19/2018 03:52 WG1062710 Benzidine U J4 0.0845 0.442 1 01/19/2018 03:52 WG1062710 Benzo(a)anthracene U 0.00568 0.0438 1 01/19/2018 03:52 WG1062710 Benzo(b)fluoranthene U 0.00922 0.0438 1 01/19/2018 03:52 WG1062710 Benzo(k)fluoranthene U 0.00772 0.0438 1 01/19/2018 03:52 WG1062710 Benzo(g,h,i)perylene U 0.00957 0.0438 1 01/19/2018 03:52 WG1062710 Benzo(a)pyrene U 0.00727 0.0438 1 01/19/2018 03:52 WG1062710 Bis(2-chlorethoxy)methane U 0.0102 0.442 1 01/19/2018 03:52 WG1062710 Bis(2-chloroethyl)ether U 0.0119 0.442 1 01/19/2018 03:52 WG1062710 Bis(2-chloroisopropyl)ether U 0.0101 0.442 1 01/19/2018 03:52 WG1062710 4-Bromophenyl-phenylether U 0.0151 0.442 1 01/19/2018 03:52 WG1062710 2-Chloronaphthalene U 0.00848 0.0438 1 01/19/2018 03:52 WG1062710 4-Chlorophenyl-phenylether U 0.00832 0.442 1 01/19/2018 03:52 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 63 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 63 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19 L963090 BF6 4-5 Collected date/time: 01/11/18 08:55 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Chrysene U 0.00737 0.0438 1 01/19/2018 03:52 WG1062710 Dibenz(a,h)anthracene U 0.0109 0.0438 1 01/19/2018 03:52 WG1062710 3,3-Dichlorobenzidine U 0.105 0.442 1 01/19/2018 03:52 WG1062710 2,4-Dinitrotoluene U 0.00806 0.442 1 01/19/2018 03:52 WG1062710 2,6-Dinitrotoluene U 0.00978 0.442 1 01/19/2018 03:52 WG1062710 Fluoranthene U 0.00658 0.0438 1 01/19/2018 03:52 WG1062710 Fluorene U 0.00905 0.0438 1 01/19/2018 03:52 WG1062710 Hexachlorobenzene U 0.0114 0.442 1 01/19/2018 03:52 WG1062710 Hexachloro-1,3-butadiene U 0.0133 0.442 1 01/19/2018 03:52 WG1062710 Hexachlorocyclopentadiene U J0 0.0779 0.442 1 01/19/2018 03:52 WG1062710 Hexachloroethane U 0.0178 0.442 1 01/19/2018 03:52 WG1062710 Indeno(1,2,3-cd)pyrene U 0.0102 0.0438 1 01/19/2018 03:52 WG1062710 Isophorone U 0.00693 0.442 1 01/19/2018 03:52 WG1062710 Naphthalene 1.91 0.118 0.438 10 01/19/2018 16:19 WG1062710 Nitrobenzene U 0.00922 0.442 1 01/19/2018 03:52 WG1062710 n-Nitrosodimethylamine U 0.0859 0.442 1 01/19/2018 03:52 WG1062710 n-Nitrosodiphenylamine U 0.00788 0.442 1 01/19/2018 03:52 WG1062710 n-Nitrosodi-n-propylamine U 0.0120 0.442 1 01/19/2018 03:52 WG1062710 Phenanthrene U 0.00701 0.0438 1 01/19/2018 03:52 WG1062710 Benzylbutyl phthalate U 0.0137 0.442 1 01/19/2018 03:52 WG1062710 Bis(2-ethylhexyl)phthalate U 0.0159 0.442 1 01/19/2018 03:52 WG1062710 Di-n-butyl phthalate U 0.0145 0.442 1 01/19/2018 03:52 WG1062710 Diethyl phthalate U 0.00917 0.442 1 01/19/2018 03:52 WG1062710 Dimethyl phthalate U 0.00717 0.442 1 01/19/2018 03:52 WG1062710 Di-n-octyl phthalate U 0.0120 0.442 1 01/19/2018 03:52 WG1062710 Pyrene U 0.0163 0.0438 1 01/19/2018 03:52 WG1062710 1,2,4-Trichlorobenzene U 0.0116 0.442 1 01/19/2018 03:52 WG1062710 4-Chloro-3-methylphenol U 0.00633 0.442 1 01/19/2018 03:52 WG1062710 2-Chlorophenol U 0.0110 0.442 1 01/19/2018 03:52 WG1062710 2,4-Dichlorophenol U 0.00990 0.442 1 01/19/2018 03:52 WG1062710 2,4-Dimethylphenol U 0.0625 0.442 1 01/19/2018 03:52 WG1062710 4,6-Dinitro-2-methylphenol U 0.165 0.442 1 01/19/2018 03:52 WG1062710 2,4-Dinitrophenol U 0.130 0.442 1 01/19/2018 03:52 WG1062710 2-Nitrophenol U 0.0173 0.442 1 01/19/2018 03:52 WG1062710 4-Nitrophenol U J0 0.0697 0.442 1 01/19/2018 03:52 WG1062710 Pentachlorophenol U 0.0637 0.442 1 01/19/2018 03:52 WG1062710 Phenol U 0.00922 0.442 1 01/19/2018 03:52 WG1062710 2,4,6-Trichlorophenol U 0.0103 0.442 1 01/19/2018 03:52 WG1062710 (S) 2-Fluorophenol 64.0 20.0-120 01/19/2018 03:52 WG1062710 (S) 2-Fluorophenol 60.2 20.0-120 01/19/2018 16:19 WG1062710 (S) Phenol-d5 67.0 20.0-120 01/19/2018 03:52 WG1062710 (S) Phenol-d5 59.8 20.0-120 01/19/2018 16:19 WG1062710 (S) Nitrobenzene-d5 57.6 18.0-125 01/19/2018 03:52 WG1062710 (S) Nitrobenzene-d5 55.8 18.0-125 01/19/2018 16:19 WG1062710 (S) 2-Fluorobiphenyl 58.0 28.0-120 01/19/2018 03:52 WG1062710 (S) 2-Fluorobiphenyl 47.6 28.0-120 01/19/2018 16:19 WG1062710 (S) 2,4,6-Tribromophenol 54.2 17.0-137 01/19/2018 16:19 WG1062710 (S) 2,4,6-Tribromophenol 88.6 17.0-137 01/19/2018 03:52 WG1062710 (S) p-Terphenyl-d14 43.2 13.0-131 01/19/2018 16:19 WG1062710 (S) p-Terphenyl-d14 46.0 13.0-131 01/19/2018 03:52 WG1062710 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 64 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 64 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20 L963090 BF6 14-15 Collected date/time: 01/11/18 08:45 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte %date / time Total Solids 87.1 1 01/17/2018 10:33 WG1063382 Mercury by Method 7471B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Mercury 0.00365 B J 0.00321 0.0230 1 01/17/2018 21:49 WG1062912 Metals (ICP) by Method 6010D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Arsenic U 0.746 2.30 1 01/16/2018 03:40 WG1062607 Barium 26.7 0.195 0.574 1 01/16/2018 03:40 WG1062607 Cadmium U 0.0803 0.574 1 01/16/2018 03:40 WG1062607 Chromium 1.57 0.161 1.15 1 01/16/2018 03:40 WG1062607 Lead 1.49 0.218 0.574 1 01/16/2018 03:40 WG1062607 Selenium U 0.849 2.30 1 01/16/2018 03:40 WG1062607 Silver U 0.321 1.15 1 01/16/2018 03:40 WG1062607 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acetone U 0.0115 0.0574 1 01/14/2018 18:34 WG1062672 Acrylonitrile U 0.00205 0.0115 1 01/14/2018 18:34 WG1062672 Benzene 0.0807 0.000310 0.00115 1 01/14/2018 18:34 WG1062672 Bromobenzene U 0.000326 0.00115 1 01/14/2018 18:34 WG1062672 Bromodichloromethane U 0.000292 0.00115 1 01/14/2018 18:34 WG1062672 Bromoform U 0.000487 0.00115 1 01/14/2018 18:34 WG1062672 Bromomethane U 0.00154 0.00574 1 01/14/2018 18:34 WG1062672 n-Butylbenzene 0.000323 J 0.000296 0.00115 1 01/14/2018 18:34 WG1062672 sec-Butylbenzene 0.000366 J 0.000231 0.00115 1 01/14/2018 18:34 WG1062672 tert-Butylbenzene U 0.000236 0.00115 1 01/14/2018 18:34 WG1062672 Carbon tetrachloride U 0.000376 0.00115 1 01/14/2018 18:34 WG1062672 Chlorobenzene U 0.000243 0.00115 1 01/14/2018 18:34 WG1062672 Chlorodibromomethane U 0.000428 0.00115 1 01/14/2018 18:34 WG1062672 Chloroethane U 0.00109 0.00574 1 01/14/2018 18:34 WG1062672 Chloroform U 0.000263 0.00574 1 01/14/2018 18:34 WG1062672 Chloromethane U 0.000430 0.00287 1 01/14/2018 18:34 WG1062672 2-Chlorotoluene U 0.000345 0.00115 1 01/14/2018 18:34 WG1062672 4-Chlorotoluene U 0.000275 0.00115 1 01/14/2018 18:34 WG1062672 1,2-Dibromo-3-Chloropropane U 0.00121 0.00574 1 01/14/2018 18:34 WG1062672 1,2-Dibromoethane U 0.000394 0.00115 1 01/14/2018 18:34 WG1062672 Dibromomethane U 0.000438 0.00115 1 01/14/2018 18:34 WG1062672 1,2-Dichlorobenzene U 0.000350 0.00115 1 01/14/2018 18:34 WG1062672 1,3-Dichlorobenzene U 0.000274 0.00115 1 01/14/2018 18:34 WG1062672 1,4-Dichlorobenzene U 0.000259 0.00115 1 01/14/2018 18:34 WG1062672 Dichlorodifluoromethane U 0.000818 0.00574 1 01/14/2018 18:34 WG1062672 1,1-Dichloroethane U 0.000228 0.00115 1 01/14/2018 18:34 WG1062672 1,2-Dichloroethane U 0.000304 0.00115 1 01/14/2018 18:34 WG1062672 1,1-Dichloroethene U 0.000348 0.00115 1 01/14/2018 18:34 WG1062672 cis-1,2-Dichloroethene U 0.000270 0.00115 1 01/14/2018 18:34 WG1062672 trans-1,2-Dichloroethene U 0.000303 0.00115 1 01/14/2018 18:34 WG1062672 1,2-Dichloropropane U 0.000411 0.00115 1 01/14/2018 18:34 WG1062672 1,1-Dichloropropene U 0.000364 0.00115 1 01/14/2018 18:34 WG1062672 1,3-Dichloropropane U 0.000238 0.00115 1 01/14/2018 18:34 WG1062672 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 65 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 65 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20 L963090 BF6 14-15 Collected date/time: 01/11/18 08:45 Volatile Organic Compounds (GC/MS) by Method 8260B Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time cis-1,3-Dichloropropene U 0.000301 0.00115 1 01/14/2018 18:34 WG1062672 trans-1,3-Dichloropropene U 0.000306 0.00115 1 01/14/2018 18:34 WG1062672 2,2-Dichloropropane U 0.000320 0.00115 1 01/14/2018 18:34 WG1062672 Di-isopropyl ether U 0.000285 0.00115 1 01/14/2018 18:34 WG1062672 Ethylbenzene 0.0676 0.000341 0.00115 1 01/14/2018 18:34 WG1062672 Hexachloro-1,3-butadiene U 0.000393 0.00115 1 01/14/2018 18:34 WG1062672 Isopropylbenzene 0.00294 0.000279 0.00115 1 01/14/2018 18:34 WG1062672 p-Isopropyltoluene U 0.000234 0.00115 1 01/14/2018 18:34 WG1062672 2-Butanone (MEK)U 0.00537 0.0115 1 01/14/2018 18:34 WG1062672 Methylene Chloride U 0.00115 0.00574 1 01/14/2018 18:34 WG1062672 4-Methyl-2-pentanone (MIBK)U 0.00216 0.0115 1 01/14/2018 18:34 WG1062672 Methyl tert-butyl ether U 0.000243 0.00115 1 01/14/2018 18:34 WG1062672 Naphthalene 0.00134 J 0.00115 0.00574 1 01/14/2018 18:34 WG1062672 n-Propylbenzene 0.00686 0.000236 0.00115 1 01/14/2018 18:34 WG1062672 Styrene U 0.000269 0.00115 1 01/14/2018 18:34 WG1062672 1,1,1,2-Tetrachloroethane U 0.000303 0.00115 1 01/14/2018 18:34 WG1062672 1,1,2,2-Tetrachloroethane U 0.000419 0.00115 1 01/14/2018 18:34 WG1062672 Tetrachloroethene U 0.000317 0.00115 1 01/14/2018 18:34 WG1062672 Toluene 0.289 0.0124 0.143 25 01/17/2018 17:52 WG1062672 1,2,3-Trichlorobenzene U 0.000351 0.00115 1 01/14/2018 18:34 WG1062672 1,2,4-Trichlorobenzene U 0.000445 0.00115 1 01/14/2018 18:34 WG1062672 1,1,1-Trichloroethane U 0.000328 0.00115 1 01/14/2018 18:34 WG1062672 1,1,2-Trichloroethane U 0.000318 0.00115 1 01/14/2018 18:34 WG1062672 1,1,2-Trichlorotrifluoroethane U 0.000419 0.00115 1 01/14/2018 18:34 WG1062672 Trichloroethene 0.000820 J 0.000320 0.00115 1 01/14/2018 18:34 WG1062672 Trichlorofluoromethane U 0.000438 0.00574 1 01/14/2018 18:34 WG1062672 1,2,3-Trichloropropane U 0.000850 0.00287 1 01/14/2018 18:34 WG1062672 1,2,4-Trimethylbenzene 0.0317 0.000242 0.00115 1 01/14/2018 18:34 WG1062672 1,3,5-Trimethylbenzene 0.0107 0.000305 0.00115 1 01/14/2018 18:34 WG1062672 Vinyl chloride U 0.000334 0.00115 1 01/14/2018 18:34 WG1062672 Xylenes, Total 0.304 0.000801 0.00344 1 01/14/2018 18:34 WG1062672 (S) Toluene-d8 97.4 80.0-120 01/14/2018 18:34 WG1062672 (S) Toluene-d8 107 80.0-120 01/17/2018 17:52 WG1062672 (S) Dibromofluoromethane 105 74.0-131 01/14/2018 18:34 WG1062672 (S) Dibromofluoromethane 94.1 74.0-131 01/17/2018 17:52 WG1062672 (S) 4-Bromofluorobenzene 101 64.0-132 01/14/2018 18:34 WG1062672 (S) 4-Bromofluorobenzene 97.7 64.0-132 01/17/2018 17:52 WG1062672 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Acenaphthene U 0.00737 0.0379 1 01/15/2018 19:44 WG1062000 Acenaphthylene U 0.00770 0.0379 1 01/15/2018 19:44 WG1062000 Anthracene U 0.00725 0.0379 1 01/15/2018 19:44 WG1062000 Benzidine U J3 J4 0.0731 0.382 1 01/15/2018 19:44 WG1062000 Benzo(a)anthracene U 0.00491 0.0379 1 01/15/2018 19:44 WG1062000 Benzo(b)fluoranthene U 0.00798 0.0379 1 01/15/2018 19:44 WG1062000 Benzo(k)fluoranthene U 0.00668 0.0379 1 01/15/2018 19:44 WG1062000 Benzo(g,h,i)perylene U 0.00828 0.0379 1 01/15/2018 19:44 WG1062000 Benzo(a)pyrene U 0.00629 0.0379 1 01/15/2018 19:44 WG1062000 Bis(2-chlorethoxy)methane U 0.00884 0.382 1 01/15/2018 19:44 WG1062000 Bis(2-chloroethyl)ether U 0.0103 0.382 1 01/15/2018 19:44 WG1062000 Bis(2-chloroisopropyl)ether U 0.00872 0.382 1 01/15/2018 19:44 WG1062000 4-Bromophenyl-phenylether U 0.0131 0.382 1 01/15/2018 19:44 WG1062000 2-Chloronaphthalene U 0.00733 0.0379 1 01/15/2018 19:44 WG1062000 4-Chlorophenyl-phenylether U 0.00720 0.382 1 01/15/2018 19:44 WG1062000 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 66 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 66 of 98 ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20 L963090 BF6 14-15 Collected date/time: 01/11/18 08:45 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch Analyte mg/kg mg/kg mg/kg date / time Chrysene U 0.00637 0.0379 1 01/15/2018 19:44 WG1062000 Dibenz(a,h)anthracene U 0.00942 0.0379 1 01/15/2018 19:44 WG1062000 3,3-Dichlorobenzidine U 0.0911 0.382 1 01/15/2018 19:44 WG1062000 2,4-Dinitrotoluene U 0.00697 0.382 1 01/15/2018 19:44 WG1062000 2,6-Dinitrotoluene U 0.00846 0.382 1 01/15/2018 19:44 WG1062000 Fluoranthene U 0.00569 0.0379 1 01/15/2018 19:44 WG1062000 Fluorene U 0.00783 0.0379 1 01/15/2018 19:44 WG1062000 Hexachlorobenzene U 0.00982 0.382 1 01/15/2018 19:44 WG1062000 Hexachloro-1,3-butadiene U 0.0115 0.382 1 01/15/2018 19:44 WG1062000 Hexachlorocyclopentadiene U 0.0674 0.382 1 01/15/2018 19:44 WG1062000 Hexachloroethane U 0.0154 0.382 1 01/15/2018 19:44 WG1062000 Indeno(1,2,3-cd)pyrene U 0.00886 0.0379 1 01/15/2018 19:44 WG1062000 Isophorone U 0.00599 0.382 1 01/15/2018 19:44 WG1062000 Naphthalene U 0.0102 0.0379 1 01/15/2018 19:44 WG1062000 Nitrobenzene U 0.00798 0.382 1 01/15/2018 19:44 WG1062000 n-Nitrosodimethylamine U 0.0743 0.382 1 01/15/2018 19:44 WG1062000 n-Nitrosodiphenylamine U 0.00682 0.382 1 01/15/2018 19:44 WG1062000 n-Nitrosodi-n-propylamine U 0.0104 0.382 1 01/15/2018 19:44 WG1062000 Phenanthrene U 0.00606 0.0379 1 01/15/2018 19:44 WG1062000 Benzylbutyl phthalate U 0.0118 0.382 1 01/15/2018 19:44 WG1062000 Bis(2-ethylhexyl)phthalate U 0.0138 0.382 1 01/15/2018 19:44 WG1062000 Di-n-butyl phthalate U 0.0125 0.382 1 01/15/2018 19:44 WG1062000 Diethyl phthalate U 0.00793 0.382 1 01/15/2018 19:44 WG1062000 Dimethyl phthalate U 0.00620 0.382 1 01/15/2018 19:44 WG1062000 Di-n-octyl phthalate U 0.0104 0.382 1 01/15/2018 19:44 WG1062000 Pyrene U 0.0141 0.0379 1 01/15/2018 19:44 WG1062000 1,2,4-Trichlorobenzene U 0.0101 0.382 1 01/15/2018 19:44 WG1062000 4-Chloro-3-methylphenol U 0.00547 0.382 1 01/15/2018 19:44 WG1062000 2-Chlorophenol U 0.00954 0.382 1 01/15/2018 19:44 WG1062000 2,4-Dichlorophenol U 0.00856 0.382 1 01/15/2018 19:44 WG1062000 2,4-Dimethylphenol U 0.0541 0.382 1 01/15/2018 19:44 WG1062000 4,6-Dinitro-2-methylphenol U 0.142 0.382 1 01/15/2018 19:44 WG1062000 2,4-Dinitrophenol U 0.112 0.382 1 01/15/2018 19:44 WG1062000 2-Nitrophenol U 0.0149 0.382 1 01/15/2018 19:44 WG1062000 4-Nitrophenol U 0.0603 0.382 1 01/15/2018 19:44 WG1062000 Pentachlorophenol U 0.0551 0.382 1 01/15/2018 19:44 WG1062000 Phenol U 0.00798 0.382 1 01/15/2018 19:44 WG1062000 2,4,6-Trichlorophenol U 0.00894 0.382 1 01/15/2018 19:44 WG1062000 (S) 2-Fluorophenol 58.2 20.0-120 01/15/2018 19:44 WG1062000 (S) Phenol-d5 58.7 20.0-120 01/15/2018 19:44 WG1062000 (S) Nitrobenzene-d5 57.3 18.0-125 01/15/2018 19:44 WG1062000 (S) 2-Fluorobiphenyl 60.5 28.0-120 01/15/2018 19:44 WG1062000 (S) 2,4,6-Tribromophenol 75.3 17.0-137 01/15/2018 19:44 WG1062000 (S) p-Terphenyl-d14 58.2 13.0-131 01/15/2018 19:44 WG1062000 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 67 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 67 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1063379 Total Solids by Method 2540 G-2011 L963090-01,02,03,04,05,06 Method Blank (MB) (MB) R3279959-1 01/17/18 09:47 MB Result MB Qualifier MB MDL MB RDL Analyte %%% Total Solids 0 L963090-01 Original Sample (OS) • Duplicate (DUP) (OS) L963090-01 01/17/18 09:47 • (DUP) R3279959-3 01/17/18 09:47 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte %%%% Total Solids 75.0 75.3 1 0 5 Laboratory Control Sample (LCS) (LCS) R3279959-2 01/17/18 09:47 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte %%%% Total Solids 50.0 50.0 100 85-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 68 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 68 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1063380 Total Solids by Method 2540 G-2011 L963090-07,08,09,10,11,12,13,14,15,16 Method Blank (MB) (MB) R3279971-1 01/17/18 10:09 MB Result MB Qualifier MB MDL MB RDL Analyte %%% Total Solids 0 L963090-16 Original Sample (OS) • Duplicate (DUP) (OS) L963090-16 01/17/18 10:09 • (DUP) R3279971-3 01/17/18 10:09 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte %%%% Total Solids 84.7 85.0 1 0 5 Laboratory Control Sample (LCS) (LCS) R3279971-2 01/17/18 10:09 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte %%%% Total Solids 50.0 50.0 100 85-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 69 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 69 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1063382 Total Solids by Method 2540 G-2011 L963090-17,18,19,20 Method Blank (MB) (MB) R3279985-1 01/17/18 10:33 MB Result MB Qualifier MB MDL MB RDL Analyte %%% Total Solids 0 L963090-17 Original Sample (OS) • Duplicate (DUP) (OS) L963090-17 01/17/18 10:33 • (DUP) R3279985-3 01/17/18 10:33 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte %%%% Total Solids 62.9 63.9 1 1 5 Laboratory Control Sample (LCS) (LCS) R3279985-2 01/17/18 10:33 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte %%%% Total Solids 50.0 50.0 100 85-115 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 70 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 70 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062912 Mercury by Method 7471B L963090-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3279921-1 01/17/18 20:35 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Mercury 0.00464 J 0.0028 0.0200 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3279921-2 01/17/18 20:38 • (LCSD) R3279921-3 01/17/18 20:40 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Mercury 0.300 0.288 0.285 96 95.1 80-120 0.992 20 L963090-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L963090-01 01/17/18 20:43 • (MS) R3279921-4 01/17/18 20:45 • (MSD) R3279921-5 01/17/18 20:55 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Mercury 0.400 0.0360 0.411 0.408 93.7 93 1 75-125 0.72 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 71 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 71 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062607 Metals (ICP) by Method 6010D L963090-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3279495-1 01/16/18 02:03 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Arsenic U 0.65 2.00 Barium U 0.17 0.500 Cadmium U 0.07 0.500 Chromium U 0.14 1.00 Lead U 0.19 0.500 Selenium U 0.74 2.00 Silver U 0.28 1.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3279495-2 01/16/18 02:06 • (LCSD) R3279495-3 01/16/18 02:09 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Arsenic 100 97.7 98.6 97.7 98.6 80-120 0.961 20 Barium 100 103 104 103 104 80-120 0.992 20 Cadmium 100 96.2 97.3 96.2 97.3 80-120 1.13 20 Chromium 100 99.9 101 99.9 101 80-120 1.33 20 Lead 100 99.3 100 99.3 100 80-120 1.05 20 Selenium 100 96.0 97.5 96 97.5 80-120 1.64 20 Silver 20.0 18.3 18.6 91.6 92.9 80-120 1.46 20 L963090-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L963090-01 01/16/18 02:12 • (MS) R3279495-6 01/16/18 02:21 • (MSD) R3279495-7 01/16/18 02:25 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Arsenic 133 U 117 115 87.7 86.3 1 75-125 1.63 20 Barium 133 75.5 204 192 96.2 87.7 1 75-125 5.76 20 Cadmium 133 U 122 120 91.8 90.2 1 75-125 1.69 20 Chromium 133 143 264 265 90.2 90.8 1 75-125 0.295 20 Lead 133 3.67 134 132 97.9 96.3 1 75-125 1.52 20 Selenium 133 U 117 115 87.6 85.9 1 75-125 2 20 Silver 26.7 U 23.7 23.2 89 87.1 1 75-125 2.13 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 72 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 72 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062584 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-01,02,03,04,05,06,07 Method Blank (MB) (MB) R3279553-3 01/13/18 23:53 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acetone U 0.0100 0.0500 Acrylonitrile U 0.00179 0.0100 Benzene U 0.000270 0.00100 Bromobenzene U 0.000284 0.00100 Bromodichloromethane U 0.000254 0.00100 Bromoform U 0.000424 0.00100 Bromomethane U 0.00134 0.00500 n-Butylbenzene U 0.000258 0.00100 sec-Butylbenzene U 0.000201 0.00100 tert-Butylbenzene U 0.000206 0.00100 Carbon tetrachloride U 0.000328 0.00100 Chlorobenzene U 0.000212 0.00100 Chlorodibromomethane U 0.000373 0.00100 Chloroethane U 0.000946 0.00500 Chloroform U 0.000229 0.00500 Chloromethane U 0.000375 0.00250 2-Chlorotoluene U 0.000301 0.00100 4-Chlorotoluene U 0.000240 0.00100 1,2-Dibromo-3-Chloropropane U 0.00105 0.00500 1,2-Dibromoethane U 0.000343 0.00100 Dibromomethane U 0.000382 0.00100 1,2-Dichlorobenzene U 0.000305 0.00100 1,3-Dichlorobenzene U 0.000239 0.00100 1,4-Dichlorobenzene U 0.000226 0.00100 Dichlorodifluoromethane U 0.000713 0.00500 1,1-Dichloroethane U 0.000199 0.00100 1,2-Dichloroethane U 0.000265 0.00100 1,1-Dichloroethene U 0.000303 0.00100 cis-1,2-Dichloroethene U 0.000235 0.00100 trans-1,2-Dichloroethene U 0.000264 0.00100 1,2-Dichloropropane U 0.000358 0.00100 1,1-Dichloropropene U 0.000317 0.00100 1,3-Dichloropropane U 0.000207 0.00100 cis-1,3-Dichloropropene U 0.000262 0.00100 trans-1,3-Dichloropropene U 0.000267 0.00100 2,2-Dichloropropane U 0.000279 0.00100 Di-isopropyl ether U 0.000248 0.00100 Ethylbenzene U 0.000297 0.00100 Hexachloro-1,3-butadiene U 0.000342 0.00100 Isopropylbenzene U 0.000243 0.00100 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 73 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 73 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062584 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-01,02,03,04,05,06,07 Method Blank (MB) (MB) R3279553-3 01/13/18 23:53 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg p-Isopropyltoluene U 0.000204 0.00100 2-Butanone (MEK)U 0.00468 0.0100 Methylene Chloride U 0.00100 0.00500 4-Methyl-2-pentanone (MIBK)U 0.00188 0.0100 Methyl tert-butyl ether U 0.000212 0.00100 Naphthalene U 0.00100 0.00500 n-Propylbenzene U 0.000206 0.00100 Styrene U 0.000234 0.00100 1,1,1,2-Tetrachloroethane U 0.000264 0.00100 1,1,2,2-Tetrachloroethane U 0.000365 0.00100 Tetrachloroethene U 0.000276 0.00100 Toluene U 0.000434 0.00500 1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100 1,2,3-Trichlorobenzene U 0.000306 0.00100 1,2,4-Trichlorobenzene U 0.000388 0.00100 1,1,1-Trichloroethane U 0.000286 0.00100 1,1,2-Trichloroethane U 0.000277 0.00100 Trichloroethene U 0.000279 0.00100 Trichlorofluoromethane U 0.000382 0.00500 1,2,3-Trichloropropane U 0.000741 0.00250 1,2,4-Trimethylbenzene U 0.000211 0.00100 1,3,5-Trimethylbenzene U 0.000266 0.00100 Vinyl chloride U 0.000291 0.00100 Xylenes, Total U 0.000698 0.00300 (S) Toluene-d8 105 80.0-120 (S) Dibromofluoromethane 99.1 74.0-131 (S) 4-Bromofluorobenzene 101 64.0-132 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3279553-1 01/13/18 22:50 • (LCSD) R3279553-2 01/13/18 23:10 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Acetone 0.125 0.133 0.122 106 97.3 11.0-160 8.55 23 Acrylonitrile 0.125 0.119 0.121 95.3 96.8 61.0-143 1.54 20 Benzene 0.0250 0.0238 0.0236 95.4 94.2 71.0-124 1.21 20 Bromobenzene 0.0250 0.0248 0.0242 99.3 96.7 78.0-120 2.65 20 Bromodichloromethane 0.0250 0.0240 0.0244 95.8 97.7 75.0-120 1.96 20 Bromoform 0.0250 0.0256 0.0263 102 105 65.0-133 2.70 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 74 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 74 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062584 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-01,02,03,04,05,06,07 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3279553-1 01/13/18 22:50 • (LCSD) R3279553-2 01/13/18 23:10 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Bromomethane 0.0250 0.0247 0.0248 98.9 99.0 26.0-160 0.112 20 n-Butylbenzene 0.0250 0.0278 0.0264 111 106 73.0-126 5.05 20 sec-Butylbenzene 0.0250 0.0260 0.0252 104 101 75.0-121 2.78 20 tert-Butylbenzene 0.0250 0.0260 0.0248 104 99.2 74.0-122 4.70 20 Carbon tetrachloride 0.0250 0.0243 0.0240 97.2 96.1 66.0-123 1.23 20 Chlorobenzene 0.0250 0.0261 0.0250 104 100 79.0-121 4.08 20 Chlorodibromomethane 0.0250 0.0252 0.0248 101 99.0 74.0-128 1.61 20 Chloroethane 0.0250 0.0243 0.0240 97.3 96.1 51.0-147 1.17 20 Chloroform 0.0250 0.0246 0.0246 98.5 98.6 73.0-123 0.0261 20 Chloromethane 0.0250 0.0228 0.0224 91.2 89.7 51.0-138 1.70 20 2-Chlorotoluene 0.0250 0.0253 0.0247 101 99.0 72.0-124 2.32 20 4-Chlorotoluene 0.0250 0.0261 0.0254 104 102 78.0-120 2.56 20 1,2-Dibromo-3-Chloropropane 0.0250 0.0242 0.0250 96.8 100 65.0-126 3.32 20 1,2-Dibromoethane 0.0250 0.0248 0.0248 99.0 99.0 78.0-122 0.0154 20 Dibromomethane 0.0250 0.0252 0.0250 101 99.9 79.0-120 1.03 20 1,2-Dichlorobenzene 0.0250 0.0253 0.0253 101 101 80.0-120 0.120 20 1,3-Dichlorobenzene 0.0250 0.0259 0.0259 104 104 72.0-123 0.0602 20 1,4-Dichlorobenzene 0.0250 0.0247 0.0244 99.0 97.4 77.0-120 1.59 20 Dichlorodifluoromethane 0.0250 0.0241 0.0235 96.2 94.1 49.0-155 2.16 20 1,1-Dichloroethane 0.0250 0.0246 0.0242 98.4 96.8 70.0-128 1.66 20 1,2-Dichloroethane 0.0250 0.0239 0.0241 95.6 96.4 69.0-128 0.776 20 1,1-Dichloroethene 0.0250 0.0247 0.0235 98.9 94.1 63.0-131 4.98 20 cis-1,2-Dichloroethene 0.0250 0.0248 0.0252 99.3 101 74.0-123 1.28 20 trans-1,2-Dichloroethene 0.0250 0.0256 0.0236 102 94.2 72.0-122 8.26 20 1,2-Dichloropropane 0.0250 0.0255 0.0254 102 102 75.0-126 0.0717 20 1,1-Dichloropropene 0.0250 0.0242 0.0239 96.8 95.6 72.0-130 1.23 20 1,3-Dichloropropane 0.0250 0.0240 0.0236 95.9 94.4 80.0-121 1.62 20 cis-1,3-Dichloropropene 0.0250 0.0249 0.0245 99.7 97.9 80.0-125 1.80 20 trans-1,3-Dichloropropene 0.0250 0.0258 0.0254 103 101 75.0-129 1.61 20 2,2-Dichloropropane 0.0250 0.0258 0.0260 103 104 60.0-129 0.824 20 Di-isopropyl ether 0.0250 0.0247 0.0243 98.9 97.0 62.0-133 1.91 20 Ethylbenzene 0.0250 0.0255 0.0249 102 99.8 77.0-120 2.28 20 Hexachloro-1,3-butadiene 0.0250 0.0259 0.0248 104 99.2 68.0-128 4.32 20 Isopropylbenzene 0.0250 0.0251 0.0241 101 96.5 75.0-120 4.13 20 p-Isopropyltoluene 0.0250 0.0268 0.0260 107 104 74.0-125 3.16 20 2-Butanone (MEK)0.125 0.125 0.130 100 104 37.0-159 3.68 20 Methylene Chloride 0.0250 0.0248 0.0226 99.1 90.4 67.0-123 9.17 20 4-Methyl-2-pentanone (MIBK)0.125 0.126 0.124 101 99.6 60.0-144 1.55 20 Methyl tert-butyl ether 0.0250 0.0257 0.0241 103 96.3 66.0-125 6.47 20 Naphthalene 0.0250 0.0243 0.0248 97.1 99.1 64.0-125 1.98 20 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 75 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 75 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062584 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-01,02,03,04,05,06,07 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3279553-1 01/13/18 22:50 • (LCSD) R3279553-2 01/13/18 23:10 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% n-Propylbenzene 0.0250 0.0255 0.0245 102 97.9 78.0-120 4.26 20 Styrene 0.0250 0.0276 0.0271 110 108 78.0-124 1.76 20 1,1,1,2-Tetrachloroethane 0.0250 0.0265 0.0258 106 103 74.0-124 2.55 20 1,1,2,2-Tetrachloroethane 0.0250 0.0242 0.0245 96.6 97.8 73.0-120 1.21 20 Tetrachloroethene 0.0250 0.0258 0.0249 103 99.7 70.0-127 3.55 20 Toluene 0.0250 0.0234 0.0225 93.4 89.9 77.0-120 3.83 20 1,1,2-Trichlorotrifluoroethane 0.0250 0.0245 0.0230 98.0 91.9 64.0-135 6.42 20 1,2,3-Trichlorobenzene 0.0250 0.0264 0.0262 106 105 68.0-126 0.839 20 1,2,4-Trichlorobenzene 0.0250 0.0272 0.0274 109 110 70.0-127 0.759 20 1,1,1-Trichloroethane 0.0250 0.0251 0.0246 100 98.2 69.0-125 2.01 20 1,1,2-Trichloroethane 0.0250 0.0246 0.0242 98.5 96.7 78.0-120 1.77 20 Trichloroethene 0.0250 0.0247 0.0244 98.8 97.8 79.0-120 1.03 20 Trichlorofluoromethane 0.0250 0.0257 0.00848 103 33.9 59.0-136 J3 J4 101 20 1,2,3-Trichloropropane 0.0250 0.0249 0.0260 99.7 104 73.0-124 4.15 20 1,2,4-Trimethylbenzene 0.0250 0.0258 0.0252 103 101 75.0-120 2.35 20 1,3,5-Trimethylbenzene 0.0250 0.0255 0.0246 102 98.2 75.0-120 3.92 20 Vinyl chloride 0.0250 0.0253 0.0246 101 98.3 63.0-134 2.81 20 Xylenes, Total 0.0750 0.0778 0.0752 104 100 77.0-120 3.40 20 (S) Toluene-d8 99.6 97.9 80.0-120 (S) Dibromofluoromethane 97.8 98.5 74.0-131 (S) 4-Bromofluorobenzene 98.7 98.3 64.0-132 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 76 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 76 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062672 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-08,09,10,11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3279544-2 01/14/18 13:11 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acetone U 0.0100 0.0500 Acrylonitrile U 0.00179 0.0100 Benzene U 0.000270 0.00100 Bromobenzene U 0.000284 0.00100 Bromodichloromethane U 0.000254 0.00100 Bromoform U 0.000424 0.00100 Bromomethane U 0.00134 0.00500 n-Butylbenzene U 0.000258 0.00100 sec-Butylbenzene U 0.000201 0.00100 tert-Butylbenzene U 0.000206 0.00100 Carbon tetrachloride U 0.000328 0.00100 Chlorobenzene U 0.000212 0.00100 Chlorodibromomethane U 0.000373 0.00100 Chloroethane U 0.000946 0.00500 Chloroform U 0.000229 0.00500 Chloromethane U 0.000375 0.00250 2-Chlorotoluene U 0.000301 0.00100 4-Chlorotoluene U 0.000240 0.00100 1,2-Dibromo-3-Chloropropane U 0.00105 0.00500 1,2-Dibromoethane U 0.000343 0.00100 Dibromomethane U 0.000382 0.00100 1,2-Dichlorobenzene U 0.000305 0.00100 1,3-Dichlorobenzene U 0.000239 0.00100 1,4-Dichlorobenzene U 0.000226 0.00100 Dichlorodifluoromethane U 0.000713 0.00500 1,1-Dichloroethane U 0.000199 0.00100 1,2-Dichloroethane U 0.000265 0.00100 1,1-Dichloroethene U 0.000303 0.00100 cis-1,2-Dichloroethene U 0.000235 0.00100 trans-1,2-Dichloroethene U 0.000264 0.00100 1,2-Dichloropropane U 0.000358 0.00100 1,1-Dichloropropene U 0.000317 0.00100 1,3-Dichloropropane U 0.000207 0.00100 cis-1,3-Dichloropropene U 0.000262 0.00100 trans-1,3-Dichloropropene U 0.000267 0.00100 2,2-Dichloropropane U 0.000279 0.00100 Di-isopropyl ether U 0.000248 0.00100 Ethylbenzene U 0.000297 0.00100 Hexachloro-1,3-butadiene U 0.000342 0.00100 Isopropylbenzene U 0.000243 0.00100 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 77 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 77 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062672 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-08,09,10,11,12,13,14,15,16,17,18,19,20 Method Blank (MB) (MB) R3279544-2 01/14/18 13:11 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg p-Isopropyltoluene U 0.000204 0.00100 2-Butanone (MEK)U 0.00468 0.0100 Methylene Chloride U 0.00100 0.00500 4-Methyl-2-pentanone (MIBK)U 0.00188 0.0100 Methyl tert-butyl ether U 0.000212 0.00100 Naphthalene U 0.00100 0.00500 n-Propylbenzene U 0.000206 0.00100 Styrene U 0.000234 0.00100 1,1,1,2-Tetrachloroethane U 0.000264 0.00100 1,1,2,2-Tetrachloroethane U 0.000365 0.00100 Tetrachloroethene U 0.000276 0.00100 Toluene U 0.000434 0.00500 1,1,2-Trichlorotrifluoroethane U 0.000365 0.00100 1,2,3-Trichlorobenzene U 0.000306 0.00100 1,2,4-Trichlorobenzene U 0.000388 0.00100 1,1,1-Trichloroethane U 0.000286 0.00100 1,1,2-Trichloroethane U 0.000277 0.00100 Trichloroethene U 0.000279 0.00100 Trichlorofluoromethane U 0.000382 0.00500 1,2,3-Trichloropropane U 0.000741 0.00250 1,2,4-Trimethylbenzene U 0.000211 0.00100 1,3,5-Trimethylbenzene U 0.000266 0.00100 Vinyl chloride U 0.000291 0.00100 Xylenes, Total U 0.000698 0.00300 (S) Toluene-d8 98.6 80.0-120 (S) Dibromofluoromethane 97.0 74.0-131 (S) 4-Bromofluorobenzene 95.6 64.0-132 Laboratory Control Sample (LCS) (LCS) R3279544-1 01/14/18 11:53 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Acetone 0.125 0.129 103 11.0-160 Acrylonitrile 0.125 0.115 92.3 61.0-143 Benzene 0.0250 0.0226 90.5 71.0-124 Bromobenzene 0.0250 0.0226 90.4 78.0-120 Bromodichloromethane 0.0250 0.0240 96.0 75.0-120 Bromoform 0.0250 0.0237 94.8 65.0-133 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 78 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 78 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062672 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-08,09,10,11,12,13,14,15,16,17,18,19,20 Laboratory Control Sample (LCS) (LCS) R3279544-1 01/14/18 11:53 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% Bromomethane 0.0250 0.0283 113 26.0-160 n-Butylbenzene 0.0250 0.0237 94.6 73.0-126 sec-Butylbenzene 0.0250 0.0231 92.5 75.0-121 tert-Butylbenzene 0.0250 0.0238 95.2 74.0-122 Carbon tetrachloride 0.0250 0.0250 100 66.0-123 Chlorobenzene 0.0250 0.0239 95.6 79.0-121 Chlorodibromomethane 0.0250 0.0253 101 74.0-128 Chloroethane 0.0250 0.0276 110 51.0-147 Chloroform 0.0250 0.0251 100 73.0-123 Chloromethane 0.0250 0.0232 92.7 51.0-138 2-Chlorotoluene 0.0250 0.0224 89.7 72.0-124 4-Chlorotoluene 0.0250 0.0233 93.1 78.0-120 1,2-Dibromo-3-Chloropropane 0.0250 0.0236 94.2 65.0-126 1,2-Dibromoethane 0.0250 0.0238 95.2 78.0-122 Dibromomethane 0.0250 0.0241 96.3 79.0-120 1,2-Dichlorobenzene 0.0250 0.0240 96.1 80.0-120 1,3-Dichlorobenzene 0.0250 0.0235 94.1 72.0-123 1,4-Dichlorobenzene 0.0250 0.0231 92.5 77.0-120 Dichlorodifluoromethane 0.0250 0.0260 104 49.0-155 1,1-Dichloroethane 0.0250 0.0237 94.9 70.0-128 1,2-Dichloroethane 0.0250 0.0246 98.5 69.0-128 1,1-Dichloroethene 0.0250 0.0233 93.4 63.0-131 cis-1,2-Dichloroethene 0.0250 0.0239 95.6 74.0-123 trans-1,2-Dichloroethene 0.0250 0.0229 91.5 72.0-122 1,2-Dichloropropane 0.0250 0.0234 93.5 75.0-126 1,1-Dichloropropene 0.0250 0.0235 93.8 72.0-130 1,3-Dichloropropane 0.0250 0.0233 93.3 80.0-121 cis-1,3-Dichloropropene 0.0250 0.0237 95.0 80.0-125 trans-1,3-Dichloropropene 0.0250 0.0240 95.9 75.0-129 2,2-Dichloropropane 0.0250 0.0249 99.4 60.0-129 Di-isopropyl ether 0.0250 0.0244 97.6 62.0-133 Ethylbenzene 0.0250 0.0224 89.4 77.0-120 Hexachloro-1,3-butadiene 0.0250 0.0253 101 68.0-128 Isopropylbenzene 0.0250 0.0225 90.0 75.0-120 p-Isopropyltoluene 0.0250 0.0229 91.5 74.0-125 2-Butanone (MEK)0.125 0.115 92.4 37.0-159 Methylene Chloride 0.0250 0.0250 100 67.0-123 4-Methyl-2-pentanone (MIBK)0.125 0.119 95.2 60.0-144 Methyl tert-butyl ether 0.0250 0.0240 96.1 66.0-125 Naphthalene 0.0250 0.0240 96.1 64.0-125 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 79 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 79 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062672 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-08,09,10,11,12,13,14,15,16,17,18,19,20 Laboratory Control Sample (LCS) (LCS) R3279544-1 01/14/18 11:53 Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier Analyte mg/kg mg/kg %% n-Propylbenzene 0.0250 0.0227 90.7 78.0-120 Styrene 0.0250 0.0241 96.4 78.0-124 1,1,1,2-Tetrachloroethane 0.0250 0.0253 101 74.0-124 1,1,2,2-Tetrachloroethane 0.0250 0.0216 86.2 73.0-120 Tetrachloroethene 0.0250 0.0236 94.3 70.0-127 Toluene 0.0250 0.0221 88.5 77.0-120 1,1,2-Trichlorotrifluoroethane 0.0250 0.0235 93.9 64.0-135 1,2,3-Trichlorobenzene 0.0250 0.0255 102 68.0-126 1,2,4-Trichlorobenzene 0.0250 0.0261 104 70.0-127 1,1,1-Trichloroethane 0.0250 0.0241 96.3 69.0-125 1,1,2-Trichloroethane 0.0250 0.0239 95.5 78.0-120 Trichloroethene 0.0250 0.0234 93.4 79.0-120 Trichlorofluoromethane 0.0250 0.0259 104 59.0-136 1,2,3-Trichloropropane 0.0250 0.0244 97.5 73.0-124 1,2,4-Trimethylbenzene 0.0250 0.0233 93.3 75.0-120 1,3,5-Trimethylbenzene 0.0250 0.0240 95.9 75.0-120 Vinyl chloride 0.0250 0.0257 103 63.0-134 Xylenes, Total 0.0750 0.0698 93.1 77.0-120 (S) Toluene-d8 98.6 80.0-120 (S) Dibromofluoromethane 103 74.0-131 (S) 4-Bromofluorobenzene 97.8 64.0-132 L963090-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L963090-16 01/14/18 19:33 • (MS) R3279544-3 01/14/18 20:52 • (MSD) R3279544-4 01/14/18 21:11 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Acetone 0.148 U 13.0 13.9 88.3 94.3 100 10.0-160 6.67 36 Acrylonitrile 0.148 U 10.4 11.5 70.6 77.8 100 14.0-160 9.76 33 Benzene 0.0295 U 1.82 1.95 61.7 66.1 100 13.0-146 6.87 27 Bromobenzene 0.0295 U 2.03 2.25 68.9 76.1 100 10.0-149 9.98 33 Bromodichloromethane 0.0295 U 2.10 2.28 71.2 77.3 100 15.0-142 8.19 28 Bromoform 0.0295 U 2.02 2.22 68.6 75.3 100 10.0-147 9.43 31 Bromomethane 0.0295 U 1.73 1.79 58.5 60.8 100 10.0-160 3.93 32 n-Butylbenzene 0.0295 0.670 2.78 2.80 71.4 72.2 100 10.0-154 0.843 37 sec-Butylbenzene 0.0295 0.235 2.27 2.42 68.8 74.0 100 10.0-151 6.44 36 tert-Butylbenzene 0.0295 U 2.14 2.26 72.4 76.4 100 10.0-152 5.41 35 Carbon tetrachloride 0.0295 U 1.99 2.05 67.3 69.6 100 13.0-140 3.36 30 Chlorobenzene 0.0295 U 2.11 2.19 71.4 74.1 100 10.0-149 3.69 31 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 80 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 80 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062672 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-08,09,10,11,12,13,14,15,16,17,18,19,20 L963090-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L963090-16 01/14/18 19:33 • (MS) R3279544-3 01/14/18 20:52 • (MSD) R3279544-4 01/14/18 21:11 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Chlorodibromomethane 0.0295 U 2.22 2.39 75.3 80.9 100 12.0-147 7.17 29 Chloroethane 0.0295 U 1.74 1.90 59.0 64.4 100 10.0-159 8.84 33 Chloroform 0.0295 U 2.14 2.27 72.6 76.8 100 18.0-148 5.64 28 Chloromethane 0.0295 U 1.38 1.42 46.8 48.2 100 10.0-146 3.09 29 2-Chlorotoluene 0.0295 U 2.08 2.18 70.4 73.8 100 10.0-151 4.71 35 4-Chlorotoluene 0.0295 U 2.07 2.15 70.0 73.0 100 10.0-150 4.15 35 1,2-Dibromo-3-Chloropropane 0.0295 U 2.03 2.29 68.9 77.5 100 10.0-149 11.8 34 1,2-Dibromoethane 0.0295 U 2.06 2.18 69.7 74.0 100 14.0-145 5.90 28 Dibromomethane 0.0295 U 1.95 2.20 66.1 74.6 100 18.0-144 12.1 27 1,2-Dichlorobenzene 0.0295 U 2.01 2.23 68.1 75.5 100 10.0-153 10.2 34 1,3-Dichlorobenzene 0.0295 U 2.05 2.24 69.3 75.8 100 10.0-150 8.97 35 1,4-Dichlorobenzene 0.0295 U 2.00 2.12 67.7 72.0 100 10.0-148 6.20 34 Dichlorodifluoromethane 0.0295 U 1.65 1.72 55.8 58.3 100 10.0-160 4.30 30 1,1-Dichloroethane 0.0295 U 1.97 2.16 66.8 73.2 100 19.0-148 9.17 28 1,2-Dichloroethane 0.0295 U 2.09 2.16 70.7 73.2 100 17.0-147 3.36 27 1,1-Dichloroethene 0.0295 U 1.72 1.77 58.4 59.9 100 10.0-150 2.64 31 cis-1,2-Dichloroethene 0.0295 U 2.00 2.13 67.7 72.2 100 16.0-145 6.45 28 trans-1,2-Dichloroethene 0.0295 U 1.61 1.68 54.4 57.0 100 11.0-142 4.68 29 1,2-Dichloropropane 0.0295 U 1.99 2.13 67.4 72.2 100 17.0-148 6.82 28 1,1-Dichloropropene 0.0295 U 1.73 1.83 58.8 61.9 100 10.0-150 5.14 30 1,3-Dichloropropane 0.0295 U 2.07 2.18 70.1 73.9 100 16.0-148 5.29 27 cis-1,3-Dichloropropene 0.0295 U 1.94 2.04 65.7 69.1 100 13.0-150 5.11 28 trans-1,3-Dichloropropene 0.0295 U 2.02 2.09 68.5 70.8 100 10.0-152 3.40 29 2,2-Dichloropropane 0.0295 U 2.03 2.21 68.8 74.9 100 16.0-143 8.49 30 Di-isopropyl ether 0.0295 U 2.09 2.23 70.7 75.6 100 16.0-149 6.63 28 Ethylbenzene 0.0295 0.539 2.40 2.52 63.2 67.3 100 10.0-147 4.85 31 Hexachloro-1,3-butadiene 0.0295 U 2.23 2.23 75.6 75.6 100 10.0-154 0.0901 40 Isopropylbenzene 0.0295 0.261 2.27 2.37 68.0 71.6 100 10.0-147 4.52 33 p-Isopropyltoluene 0.0295 0.0734 2.35 2.44 77.2 80.3 100 10.0-156 3.76 37 2-Butanone (MEK)0.148 U 11.9 12.8 80.6 86.9 100 10.0-160 7.55 33 Methylene Chloride 0.0295 U 1.94 2.12 65.6 71.8 100 16.0-139 9.09 29 4-Methyl-2-pentanone (MIBK)0.148 U 11.6 11.9 78.6 80.7 100 12.0-160 2.62 32 Methyl tert-butyl ether 0.0295 U 2.06 2.31 69.6 78.2 100 21.0-145 11.6 29 Naphthalene 0.0295 0.169 2.12 2.36 66.0 74.1 100 10.0-153 10.7 36 n-Propylbenzene 0.0295 1.33 3.31 3.40 67.2 70.2 100 10.0-151 2.64 34 Styrene 0.0295 U 2.12 2.25 71.8 76.1 100 10.0-155 5.79 34 1,1,1,2-Tetrachloroethane 0.0295 U 2.18 2.34 73.8 79.4 100 10.0-147 7.32 30 1,1,2,2-Tetrachloroethane 0.0295 U 2.00 2.04 67.8 69.0 100 10.0-155 1.67 31 Tetrachloroethene 0.0295 U 1.82 1.92 61.7 65.1 100 10.0-144 5.29 32 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 81 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 81 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062672 Volatile Organic Compounds (GC/MS) by Method 8260B L963090-08,09,10,11,12,13,14,15,16,17,18,19,20 L963090-16 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L963090-16 01/14/18 19:33 • (MS) R3279544-3 01/14/18 20:52 • (MSD) R3279544-4 01/14/18 21:11 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Toluene 0.0295 U 1.82 1.89 61.8 63.9 100 10.0-144 3.39 28 1,1,2-Trichlorotrifluoroethane 0.0295 U 1.86 1.99 63.0 67.5 100 10.0-153 6.77 33 1,2,3-Trichlorobenzene 0.0295 U 2.02 2.16 68.5 73.1 100 10.0-153 6.50 40 1,2,4-Trichlorobenzene 0.0295 U 2.12 2.23 71.8 75.5 100 10.0-156 5.06 40 1,1,1-Trichloroethane 0.0295 U 1.97 2.07 66.8 70.1 100 18.0-145 4.83 29 1,1,2-Trichloroethane 0.0295 U 2.32 2.45 78.6 83.0 100 12.0-151 5.40 28 Trichloroethene 0.0295 U 1.95 2.13 66.1 72.2 100 11.0-148 8.74 29 Trichlorofluoromethane 0.0295 U 1.90 1.95 64.5 66.2 100 10.0-157 2.59 34 1,2,3-Trichloropropane 0.0295 U 2.32 2.47 78.5 83.5 100 10.0-154 6.26 32 1,2,4-Trimethylbenzene 0.0295 2.85 4.84 4.91 67.5 69.8 100 10.0-151 1.37 34 1,3,5-Trimethylbenzene 0.0295 1.10 3.18 3.30 70.6 74.4 100 10.0-150 3.47 33 Vinyl chloride 0.0295 U 1.56 1.62 53.0 54.8 100 10.0-150 3.29 29 Xylenes, Total 0.0885 0.391 6.26 6.52 66.3 69.2 100 10.0-150 4.07 31 (S) Toluene-d8 98.6 96.8 80.0-120 (S) Dibromofluoromethane 99.5 101 74.0-131 (S) 4-Bromofluorobenzene 99.5 98.8 64.0-132 Sample Narrative: OS: Non-target compounds too high to run at a lower dilution. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 82 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 82 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062000 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-20 Method Blank (MB) (MB) R3279450-3 01/15/18 14:57 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acenaphthene U 0.00642 0.0330 Acenaphthylene U 0.00671 0.0330 Anthracene U 0.00632 0.0330 Benzidine U 0.0637 0.333 Benzo(a)anthracene U 0.00428 0.0330 Benzo(b)fluoranthene U 0.00695 0.0330 Benzo(k)fluoranthene U 0.00582 0.0330 Benzo(g,h,i)perylene U 0.00721 0.0330 Benzo(a)pyrene U 0.00548 0.0330 Bis(2-chlorethoxy)methane U 0.00770 0.333 Bis(2-chloroethyl)ether U 0.00896 0.333 Bis(2-chloroisopropyl)ether U 0.00760 0.333 4-Bromophenyl-phenylether U 0.0114 0.333 2-Chloronaphthalene U 0.00639 0.0330 4-Chlorophenyl-phenylether U 0.00627 0.333 Chrysene U 0.00555 0.0330 Dibenz(a,h)anthracene U 0.00821 0.0330 3,3-Dichlorobenzidine U 0.0794 0.333 2,4-Dinitrotoluene U 0.00607 0.333 2,6-Dinitrotoluene U 0.00737 0.333 Fluoranthene U 0.00496 0.0330 Fluorene U 0.00682 0.0330 Hexachlorobenzene U 0.00856 0.333 Hexachloro-1,3-butadiene U 0.0100 0.333 Hexachlorocyclopentadiene U 0.0587 0.333 Hexachloroethane U 0.0134 0.333 Indeno(1,2,3-cd)pyrene U 0.00772 0.0330 Isophorone U 0.00522 0.333 Naphthalene U 0.00889 0.0330 Nitrobenzene U 0.00695 0.333 n-Nitrosodimethylamine U 0.0647 0.333 n-Nitrosodiphenylamine U 0.00594 0.333 n-Nitrosodi-n-propylamine U 0.00906 0.333 Phenanthrene U 0.00528 0.0330 Benzylbutyl phthalate U 0.0103 0.333 Bis(2-ethylhexyl)phthalate U 0.0120 0.333 Di-n-butyl phthalate U 0.0109 0.333 Diethyl phthalate U 0.00691 0.333 Dimethyl phthalate U 0.00540 0.333 Di-n-octyl phthalate U 0.00907 0.333 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 83 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 83 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062000 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-20 Method Blank (MB) (MB) R3279450-3 01/15/18 14:57 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Pyrene U 0.0123 0.0330 1,2,4-Trichlorobenzene U 0.00876 0.333 4-Chloro-3-methylphenol U 0.00477 0.333 2-Chlorophenol U 0.00831 0.333 2,4-Dichlorophenol U 0.00746 0.333 2,4-Dimethylphenol U 0.0471 0.333 4,6-Dinitro-2-methylphenol U 0.124 0.333 2,4-Dinitrophenol U 0.0980 0.333 2-Nitrophenol U 0.0130 0.333 4-Nitrophenol U 0.0525 0.333 Pentachlorophenol U 0.0480 0.333 Phenol U 0.00695 0.333 2,4,6-Trichlorophenol U 0.00779 0.333 (S) Nitrobenzene-d5 74.5 18.0-125 (S) 2-Fluorobiphenyl 67.6 28.0-120 (S) p-Terphenyl-d14 55.3 13.0-131 (S) Phenol-d5 74.4 20.0-120 (S) 2-Fluorophenol 78.9 20.0-120 (S) 2,4,6-Tribromophenol 66.8 17.0-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3279450-1 01/15/18 14:10 • (LCSD) R3279450-2 01/15/18 14:33 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Acenaphthene 0.667 0.489 0.487 73.3 73.1 47.0-120 0.377 21 Acenaphthylene 0.667 0.524 0.518 78.6 77.6 48.0-120 1.25 21 Anthracene 0.667 0.534 0.507 80.0 76.0 46.0-120 5.22 20 Benzidine 0.667 ND ND 0.000 0.000 1.00-120 J4 J4 0.000 36 Benzo(a)anthracene 0.667 0.512 0.483 76.8 72.5 46.0-120 5.74 20 Benzo(b)fluoranthene 0.667 0.533 0.495 79.9 74.3 45.0-120 7.26 22 Benzo(k)fluoranthene 0.667 0.489 0.499 73.2 74.8 45.0-120 2.16 23 Benzo(g,h,i)perylene 0.667 0.489 0.484 73.4 72.6 48.0-120 1.01 21 Benzo(a)pyrene 0.667 0.508 0.500 76.1 75.0 46.0-120 1.51 21 Bis(2-chlorethoxy)methane 0.667 0.429 0.426 64.3 63.8 41.0-120 0.750 22 Bis(2-chloroethyl)ether 0.667 0.503 0.481 75.3 72.1 28.0-120 4.37 28 Bis(2-chloroisopropyl)ether 0.667 0.468 0.453 70.2 68.0 40.0-120 3.16 27 4-Bromophenyl-phenylether 0.667 0.520 0.496 78.0 74.3 45.0-120 4.84 20 2-Chloronaphthalene 0.667 0.475 0.470 71.2 70.4 43.0-120 1.11 22 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 84 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 84 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062000 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3279450-1 01/15/18 14:10 • (LCSD) R3279450-2 01/15/18 14:33 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% 4-Chlorophenyl-phenylether 0.667 0.524 0.509 78.6 76.3 46.0-120 2.90 21 Chrysene 0.667 0.493 0.464 73.8 69.5 46.0-120 6.02 20 Dibenz(a,h)anthracene 0.667 0.523 0.511 78.4 76.6 47.0-120 2.35 22 3,3-Dichlorobenzidine 0.667 0.337 0.377 50.5 56.5 20.0-130 11.1 24 2,4-Dinitrotoluene 0.667 0.551 0.535 82.6 80.2 48.0-122 2.91 21 2,6-Dinitrotoluene 0.667 0.497 0.492 74.5 73.7 46.0-120 1.04 21 Fluoranthene 0.667 0.550 0.516 82.4 77.4 46.0-120 6.28 20 Fluorene 0.667 0.536 0.522 80.3 78.3 47.0-120 2.50 20 Hexachlorobenzene 0.667 0.524 0.514 78.6 77.0 42.0-120 2.00 20 Hexachloro-1,3-butadiene 0.667 0.446 0.432 66.8 64.7 36.0-120 3.24 26 Hexachlorocyclopentadiene 0.667 0.433 0.428 64.9 64.1 20.0-124 1.24 26 Hexachloroethane 0.667 0.479 0.447 71.8 67.0 32.0-120 7.02 31 Indeno(1,2,3-cd)pyrene 0.667 0.518 0.504 77.7 75.6 48.0-120 2.76 21 Isophorone 0.667 0.439 0.435 65.8 65.2 42.0-120 0.930 21 Naphthalene 0.667 0.390 0.388 58.4 58.2 41.0-120 0.380 24 Nitrobenzene 0.667 0.435 0.435 65.3 65.3 36.0-120 0.0186 24 n-Nitrosodimethylamine 0.667 0.482 0.487 72.3 73.1 20.0-120 1.07 31 n-Nitrosodiphenylamine 0.667 0.486 0.463 72.9 69.5 42.0-120 4.78 20 n-Nitrosodi-n-propylamine 0.667 0.511 0.506 76.5 75.9 39.0-120 0.856 23 Phenanthrene 0.667 0.540 0.506 80.9 75.9 45.0-120 6.41 20 Benzylbutyl phthalate 0.667 0.502 0.483 75.3 72.4 41.0-123 3.90 20 Bis(2-ethylhexyl)phthalate 0.667 0.530 0.502 79.5 75.3 41.0-124 5.42 20 Di-n-butyl phthalate 0.667 0.555 0.517 83.3 77.5 44.0-120 7.17 20 Diethyl phthalate 0.667 0.565 0.544 84.8 81.6 46.0-120 3.82 20 Dimethyl phthalate 0.667 0.521 0.496 78.1 74.3 47.0-120 4.98 21 Di-n-octyl phthalate 0.667 0.514 0.502 77.0 75.2 40.0-123 2.33 21 Pyrene 0.667 0.486 0.463 72.8 69.4 45.0-120 4.82 21 1,2,4-Trichlorobenzene 0.667 0.412 0.408 61.7 61.2 40.0-120 0.765 25 4-Chloro-3-methylphenol 0.667 0.456 0.437 68.3 65.4 46.0-120 4.30 20 2-Chlorophenol 0.667 0.481 0.471 72.1 70.6 37.0-120 2.12 27 2,4-Dichlorophenol 0.667 0.425 0.443 63.8 66.4 45.0-120 4.00 21 2,4-Dimethylphenol 0.667 0.422 0.428 63.3 64.2 40.0-120 1.36 22 4,6-Dinitro-2-methylphenol 0.667 0.550 0.527 82.4 79.0 34.0-120 4.15 23 2,4-Dinitrophenol 0.667 0.386 0.375 57.9 56.2 10.0-120 2.96 30 2-Nitrophenol 0.667 0.413 0.413 62.0 61.9 42.0-120 0.203 24 4-Nitrophenol 0.667 0.495 0.467 74.2 70.0 40.0-120 5.93 21 Pentachlorophenol 0.667 0.542 0.558 81.3 83.7 33.0-122 2.86 22 Phenol 0.667 0.485 0.469 72.7 70.3 38.0-120 3.44 25 2,4,6-Trichlorophenol 0.667 0.580 0.547 87.0 82.1 47.0-120 5.87 22 (S) Nitrobenzene-d5 64.4 64.1 18.0-125 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 85 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 85 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062000 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3279450-1 01/15/18 14:10 • (LCSD) R3279450-2 01/15/18 14:33 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% (S) 2-Fluorobiphenyl 67.9 68.0 28.0-120 (S) p-Terphenyl-d14 51.0 50.6 13.0-131 (S) Phenol-d5 68.6 66.6 20.0-120 (S) 2-Fluorophenol 75.2 74.1 20.0-120 (S) 2,4,6-Tribromophenol 70.8 66.8 17.0-137 L963090-20 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L963090-20 01/15/18 19:44 • (MS) R3279450-4 01/15/18 20:07 • (MSD) R3279450-5 01/15/18 20:31 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Acenaphthene 0.766 U 0.579 0.654 75.6 85.5 1 37.0-120 12.3 23 Acenaphthylene 0.766 U 0.631 0.692 82.4 90.4 1 41.0-120 9.27 22 Anthracene 0.766 U 0.622 0.700 81.2 91.4 1 30.0-123 11.8 25 Benzidine 0.766 U 0.128 0.223 16.8 29.2 1 1.00-120 J3 54.0 36 Benzo(a)anthracene 0.766 U 0.599 0.655 78.3 85.6 1 21.0-123 8.92 26 Benzo(b)fluoranthene 0.766 U 0.607 0.696 79.3 90.9 1 20.0-127 13.7 29 Benzo(k)fluoranthene 0.766 U 0.568 0.666 74.2 86.9 1 22.0-123 15.8 28 Benzo(g,h,i)perylene 0.766 U 0.572 0.669 74.8 87.3 1 10.0-120 15.5 32 Benzo(a)pyrene 0.766 U 0.588 0.674 76.8 88.1 1 23.0-120 13.7 27 Bis(2-chlorethoxy)methane 0.766 U 0.506 0.553 66.2 72.3 1 37.0-120 8.86 22 Bis(2-chloroethyl)ether 0.766 U 0.576 0.660 75.2 86.2 1 26.0-120 13.6 27 Bis(2-chloroisopropyl)ether 0.766 U 0.551 0.631 72.0 82.4 1 35.0-120 13.5 25 4-Bromophenyl-phenylether 0.766 U 0.593 0.650 77.4 85.0 1 34.0-120 9.29 23 2-Chloronaphthalene 0.766 U 0.562 0.626 73.4 81.8 1 40.0-120 10.8 22 4-Chlorophenyl-phenylether 0.766 U 0.633 0.701 82.7 91.6 1 37.0-120 10.1 23 Chrysene 0.766 U 0.579 0.635 75.7 83.0 1 19.0-127 9.23 27 Dibenz(a,h)anthracene 0.766 U 0.600 0.695 78.4 90.7 1 10.0-120 14.6 28 3,3-Dichlorobenzidine 0.766 U 0.485 0.585 63.3 76.4 1 10.0-142 18.8 30 2,4-Dinitrotoluene 0.766 U 0.650 0.730 85.0 95.4 1 37.0-129 11.5 24 2,6-Dinitrotoluene 0.766 U 0.582 0.657 76.0 85.8 1 40.0-120 12.2 23 Fluoranthene 0.766 U 0.642 0.718 83.8 93.8 1 20.0-133 11.2 28 Fluorene 0.766 U 0.637 0.715 83.1 93.4 1 35.0-120 11.6 23 Hexachlorobenzene 0.766 U 0.612 0.683 79.9 89.2 1 33.0-120 11.0 24 Hexachloro-1,3-butadiene 0.766 U 0.506 0.561 66.0 73.2 1 33.0-120 10.3 25 Hexachlorocyclopentadiene 0.766 U 0.416 0.456 54.4 59.6 1 10.0-120 9.17 33 Hexachloroethane 0.766 U 0.542 0.612 70.7 80.0 1 21.0-120 12.3 30 Indeno(1,2,3-cd)pyrene 0.766 U 0.596 0.695 77.9 90.8 1 10.0-120 15.3 30 Isophorone 0.766 U 0.517 0.564 67.5 73.7 1 38.0-120 8.73 22 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 86 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 86 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062000 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-20 L963090-20 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L963090-20 01/15/18 19:44 • (MS) R3279450-4 01/15/18 20:07 • (MSD) R3279450-5 01/15/18 20:31 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Naphthalene 0.766 U 0.457 0.499 59.7 65.2 1 37.0-120 8.80 25 Nitrobenzene 0.766 U 0.508 0.555 66.4 72.5 1 32.0-120 8.84 24 n-Nitrosodimethylamine 0.766 U 0.564 0.640 73.6 83.6 1 18.0-120 12.7 27 n-Nitrosodiphenylamine 0.766 U 0.563 0.627 73.5 81.9 1 20.0-125 10.8 25 n-Nitrosodi-n-propylamine 0.766 U 0.611 0.678 79.9 88.6 1 34.0-120 10.3 23 Phenanthrene 0.766 U 0.614 0.686 80.2 89.6 1 24.0-124 11.0 25 Benzylbutyl phthalate 0.766 U 0.605 0.666 79.0 87.0 1 18.0-130 9.65 27 Bis(2-ethylhexyl)phthalate 0.766 U 0.626 0.687 81.8 89.7 1 19.0-127 9.22 28 Di-n-butyl phthalate 0.766 U 0.650 0.718 84.9 93.8 1 29.0-120 10.0 26 Diethyl phthalate 0.766 U 0.665 0.745 86.9 97.3 1 42.0-121 11.3 23 Dimethyl phthalate 0.766 U 0.613 0.682 80.1 89.1 1 42.0-120 10.6 23 Di-n-octyl phthalate 0.766 U 0.610 0.686 79.7 89.6 1 21.0-122 11.8 27 Pyrene 0.766 U 0.571 0.645 74.6 84.3 1 19.0-127 12.2 29 1,2,4-Trichlorobenzene 0.766 U 0.470 0.528 61.5 69.0 1 39.0-120 11.5 25 4-Chloro-3-methylphenol 0.766 U 0.544 0.587 71.0 76.7 1 37.0-121 7.68 23 2-Chlorophenol 0.766 U 0.571 0.649 74.6 84.8 1 34.0-120 12.8 25 2,4-Dichlorophenol 0.766 U 0.535 0.568 69.9 74.1 1 41.0-120 5.90 22 2,4-Dimethylphenol 0.766 U 0.521 0.568 68.1 74.2 1 27.0-120 8.53 25 4,6-Dinitro-2-methylphenol 0.766 U 0.693 0.770 90.5 101 1 10.0-131 10.5 29 2,4-Dinitrophenol 0.766 U 0.593 0.663 77.5 86.6 1 10.0-142 11.1 30 2-Nitrophenol 0.766 U 0.491 0.551 64.2 72.0 1 34.0-124 11.5 27 4-Nitrophenol 0.766 U 0.638 0.666 83.3 87.0 1 26.0-133 4.39 25 Pentachlorophenol 0.766 U 0.786 0.855 103 112 1 15.0-152 8.36 26 Phenol 0.766 U 0.578 0.651 75.5 85.1 1 33.0-120 11.9 24 2,4,6-Trichlorophenol 0.766 U 0.703 0.796 91.8 104 1 40.0-125 12.4 24 (S) Nitrobenzene-d5 64.7 75.7 18.0-125 (S) 2-Fluorobiphenyl 72.6 80.8 28.0-120 (S) p-Terphenyl-d14 55.2 61.1 13.0-131 (S) Phenol-d5 72.0 79.2 20.0-120 (S) 2-Fluorophenol 78.1 92.8 20.0-120 (S) 2,4,6-Tribromophenol 76.9 84.2 17.0-137 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 87 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 87 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062710 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19 Method Blank (MB) (MB) R3280484-3 01/18/18 20:30 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Acenaphthene U 0.00642 0.0330 Acenaphthylene U 0.00671 0.0330 Anthracene U 0.00632 0.0330 Benzidine U 0.0637 0.333 Benzo(a)anthracene U 0.00428 0.0330 Benzo(b)fluoranthene U 0.00695 0.0330 Benzo(k)fluoranthene U 0.00582 0.0330 Benzo(g,h,i)perylene U 0.00721 0.0330 Benzo(a)pyrene U 0.00548 0.0330 Bis(2-chlorethoxy)methane U 0.00770 0.333 Bis(2-chloroethyl)ether U 0.00896 0.333 Bis(2-chloroisopropyl)ether U 0.00760 0.333 4-Bromophenyl-phenylether U 0.0114 0.333 2-Chloronaphthalene U 0.00639 0.0330 4-Chlorophenyl-phenylether U 0.00627 0.333 Chrysene U 0.00555 0.0330 Dibenz(a,h)anthracene U 0.00821 0.0330 3,3-Dichlorobenzidine U 0.0794 0.333 2,4-Dinitrotoluene U 0.00607 0.333 2,6-Dinitrotoluene U 0.00737 0.333 Fluoranthene U 0.00496 0.0330 Fluorene U 0.00682 0.0330 Hexachlorobenzene U 0.00856 0.333 Hexachloro-1,3-butadiene U 0.0100 0.333 Hexachlorocyclopentadiene U 0.0587 0.333 Hexachloroethane U 0.0134 0.333 Indeno(1,2,3-cd)pyrene U 0.00772 0.0330 Isophorone U 0.00522 0.333 Naphthalene U 0.00889 0.0330 Nitrobenzene U 0.00695 0.333 n-Nitrosodimethylamine U 0.0647 0.333 n-Nitrosodiphenylamine U 0.00594 0.333 n-Nitrosodi-n-propylamine U 0.00906 0.333 Phenanthrene U 0.00528 0.0330 Benzylbutyl phthalate U 0.0103 0.333 Bis(2-ethylhexyl)phthalate U 0.0120 0.333 Di-n-butyl phthalate U 0.0109 0.333 Diethyl phthalate U 0.00691 0.333 Dimethyl phthalate U 0.00540 0.333 Di-n-octyl phthalate U 0.00907 0.333 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 88 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 88 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062710 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19 Method Blank (MB) (MB) R3280484-3 01/18/18 20:30 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Pyrene U 0.0123 0.0330 1,2,4-Trichlorobenzene U 0.00876 0.333 4-Chloro-3-methylphenol U 0.00477 0.333 2-Chlorophenol U 0.00831 0.333 2,4-Dichlorophenol U 0.00746 0.333 2,4-Dimethylphenol U 0.0471 0.333 4,6-Dinitro-2-methylphenol U 0.124 0.333 2,4-Dinitrophenol U 0.0980 0.333 2-Nitrophenol U 0.0130 0.333 4-Nitrophenol U 0.0525 0.333 Pentachlorophenol U 0.0480 0.333 Phenol U 0.00695 0.333 2,4,6-Trichlorophenol U 0.00779 0.333 (S) Nitrobenzene-d5 60.6 18.0-125 (S) 2-Fluorobiphenyl 70.0 28.0-120 (S) p-Terphenyl-d14 67.6 13.0-131 (S) Phenol-d5 68.2 20.0-120 (S) 2-Fluorophenol 77.4 20.0-120 (S) 2,4,6-Tribromophenol 96.0 17.0-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3280484-1 01/18/18 19:43 • (LCSD) R3280484-2 01/18/18 20:06 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% Acenaphthene 0.667 0.456 0.444 68.4 66.6 47.0-120 2.68 21 Acenaphthylene 0.667 0.480 0.481 71.9 72.1 48.0-120 0.220 21 Anthracene 0.667 0.530 0.531 79.4 79.6 46.0-120 0.262 20 Benzidine 0.667 ND ND 0.000 0.000 1.00-120 J4 J4 0.000 36 Benzo(a)anthracene 0.667 0.494 0.533 74.0 79.9 46.0-120 7.71 20 Benzo(b)fluoranthene 0.667 0.478 0.482 71.6 72.2 45.0-120 0.814 22 Benzo(k)fluoranthene 0.667 0.465 0.491 69.8 73.6 45.0-120 5.35 23 Benzo(g,h,i)perylene 0.667 0.597 0.610 89.4 91.5 48.0-120 2.27 21 Benzo(a)pyrene 0.667 0.489 0.502 73.2 75.2 46.0-120 2.69 21 Bis(2-chlorethoxy)methane 0.667 0.330 0.320 49.5 48.0 41.0-120 3.11 22 Bis(2-chloroethyl)ether 0.667 0.463 0.391 69.4 58.7 28.0-120 16.8 28 Bis(2-chloroisopropyl)ether 0.667 0.416 0.361 62.4 54.1 40.0-120 14.1 27 4-Bromophenyl-phenylether 0.667 0.508 0.538 76.1 80.6 45.0-120 5.74 20 2-Chloronaphthalene 0.667 0.431 0.416 64.7 62.4 43.0-120 3.56 22 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 89 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 89 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062710 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3280484-1 01/18/18 19:43 • (LCSD) R3280484-2 01/18/18 20:06 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% 4-Chlorophenyl-phenylether 0.667 0.423 0.428 63.4 64.2 46.0-120 1.30 21 Chrysene 0.667 0.503 0.536 75.4 80.4 46.0-120 6.49 20 Dibenz(a,h)anthracene 0.667 0.571 0.596 85.7 89.3 47.0-120 4.12 22 3,3-Dichlorobenzidine 0.667 0.277 0.273 41.5 40.9 20.0-130 1.39 24 2,4-Dinitrotoluene 0.667 0.415 0.443 62.2 66.5 48.0-122 6.60 21 2,6-Dinitrotoluene 0.667 0.447 0.453 67.0 67.9 46.0-120 1.34 21 Fluoranthene 0.667 0.529 0.536 79.3 80.4 46.0-120 1.37 20 Fluorene 0.667 0.429 0.433 64.3 64.9 47.0-120 1.01 20 Hexachlorobenzene 0.667 0.527 0.526 78.9 78.8 42.0-120 0.170 20 Hexachloro-1,3-butadiene 0.667 0.327 0.307 49.0 46.0 36.0-120 6.42 26 Hexachlorocyclopentadiene 0.667 0.364 0.336 54.6 50.4 20.0-124 7.97 26 Hexachloroethane 0.667 0.376 0.327 56.4 49.0 32.0-120 14.0 31 Indeno(1,2,3-cd)pyrene 0.667 0.572 0.597 85.8 89.5 48.0-120 4.16 21 Isophorone 0.667 0.343 0.338 51.4 50.7 42.0-120 1.36 21 Naphthalene 0.667 0.362 0.340 54.3 50.9 41.0-120 6.52 24 Nitrobenzene 0.667 0.374 0.356 56.0 53.3 36.0-120 4.94 24 n-Nitrosodimethylamine 0.667 0.476 0.415 71.4 62.3 20.0-120 13.7 31 n-Nitrosodiphenylamine 0.667 0.483 0.496 72.4 74.3 42.0-120 2.64 20 n-Nitrosodi-n-propylamine 0.667 0.465 0.413 69.6 62.0 39.0-120 11.7 23 Phenanthrene 0.667 0.510 0.521 76.5 78.0 45.0-120 2.00 20 Benzylbutyl phthalate 0.667 0.447 0.486 67.0 72.9 41.0-123 8.54 20 Bis(2-ethylhexyl)phthalate 0.667 0.499 0.547 74.8 82.0 41.0-124 9.17 20 Di-n-butyl phthalate 0.667 0.555 0.566 83.2 84.9 44.0-120 2.00 20 Diethyl phthalate 0.667 0.396 0.408 59.4 61.1 46.0-120 2.82 20 Dimethyl phthalate 0.667 0.431 0.444 64.6 66.6 47.0-120 3.03 21 Di-n-octyl phthalate 0.667 0.512 0.550 76.7 82.5 40.0-123 7.32 21 Pyrene 0.667 0.484 0.528 72.6 79.1 45.0-120 8.52 21 1,2,4-Trichlorobenzene 0.667 0.335 0.305 50.2 45.8 40.0-120 9.26 25 4-Chloro-3-methylphenol 0.667 0.361 0.374 54.1 56.1 46.0-120 3.63 20 2-Chlorophenol 0.667 0.441 0.404 66.1 60.6 37.0-120 8.76 27 2,4-Dichlorophenol 0.667 0.373 0.369 55.9 55.3 45.0-120 1.17 21 2,4-Dimethylphenol 0.667 0.321 0.317 48.2 47.5 40.0-120 1.31 22 4,6-Dinitro-2-methylphenol 0.667 0.543 0.554 81.4 83.1 34.0-120 2.11 23 2,4-Dinitrophenol 0.667 0.401 0.422 60.1 63.3 10.0-120 5.24 30 2-Nitrophenol 0.667 0.368 0.363 55.2 54.4 42.0-120 1.59 24 4-Nitrophenol 0.667 0.388 0.423 58.2 63.4 40.0-120 8.68 21 Pentachlorophenol 0.667 0.456 0.490 68.4 73.4 33.0-122 7.04 22 Phenol 0.667 0.457 0.414 68.5 62.1 38.0-120 9.74 25 2,4,6-Trichlorophenol 0.667 0.434 0.455 65.1 68.3 47.0-120 4.73 22 (S) Nitrobenzene-d5 50.2 43.8 18.0-125 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 90 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 90 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062710 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3280484-1 01/18/18 19:43 • (LCSD) R3280484-2 01/18/18 20:06 Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg %%%%% (S) 2-Fluorobiphenyl 69.8 62.6 28.0-120 (S) p-Terphenyl-d14 61.0 60.2 13.0-131 (S) Phenol-d5 71.6 59.4 20.0-120 (S) 2-Fluorophenol 81.2 63.8 20.0-120 (S) 2,4,6-Tribromophenol 106 100 17.0-137 L963090-12 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L963090-12 01/19/18 01:09 • (MS) R3280484-4 01/19/18 01:33 • (MSD) R3280484-5 01/19/18 01:56 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Acenaphthene 0.745 U 0.528 0.493 70.8 66.1 1 37.0-120 6.89 23 Acenaphthylene 0.745 U 0.550 0.522 73.8 70.1 1 41.0-120 5.17 22 Anthracene 0.745 U 0.564 0.544 75.7 72.9 1 30.0-123 3.74 25 Benzidine 0.745 U ND ND 0.000 0.000 1 1.00-120 J6 J6 0.000 36 Benzo(a)anthracene 0.745 U 0.552 0.553 74.1 74.3 1 21.0-123 0.269 26 Benzo(b)fluoranthene 0.745 U 0.518 0.525 69.5 70.4 1 20.0-127 1.32 29 Benzo(k)fluoranthene 0.745 U 0.506 0.527 67.9 70.8 1 22.0-123 4.13 28 Benzo(g,h,i)perylene 0.745 U 0.453 0.400 60.8 53.7 1 10.0-120 12.5 32 Benzo(a)pyrene 0.745 U 0.524 0.547 70.3 73.4 1 23.0-120 4.34 27 Bis(2-chlorethoxy)methane 0.745 U 0.368 0.350 49.3 46.9 1 37.0-120 5.03 22 Bis(2-chloroethyl)ether 0.745 U 0.463 0.438 62.1 58.8 1 26.0-120 5.46 27 Bis(2-chloroisopropyl)ether 0.745 U 0.436 0.431 58.4 57.9 1 35.0-120 1.02 25 4-Bromophenyl-phenylether 0.745 U 0.565 0.572 75.8 76.7 1 34.0-120 1.18 23 2-Chloronaphthalene 0.745 U 0.486 0.477 65.3 64.0 1 40.0-120 1.93 22 4-Chlorophenyl-phenylether 0.745 U 0.485 0.456 65.0 61.2 1 37.0-120 5.99 23 Chrysene 0.745 U 0.567 0.573 76.1 76.8 1 19.0-127 0.924 27 Dibenz(a,h)anthracene 0.745 U 0.506 0.467 67.9 62.6 1 10.0-120 8.05 28 3,3-Dichlorobenzidine 0.745 U 0.354 0.367 47.5 49.2 1 10.0-142 3.46 30 2,4-Dinitrotoluene 0.745 U 0.483 0.459 64.8 61.6 1 37.0-129 5.03 24 2,6-Dinitrotoluene 0.745 U 0.526 0.487 70.6 65.4 1 40.0-120 7.74 23 Fluoranthene 0.745 U 0.593 0.586 79.6 78.6 1 20.0-133 1.20 28 Fluorene 0.745 U 0.479 0.464 64.2 62.2 1 35.0-120 3.20 23 Hexachlorobenzene 0.745 U 0.580 0.578 77.9 77.6 1 33.0-120 0.403 24 Hexachloro-1,3-butadiene 0.745 U 0.401 0.368 53.8 49.4 1 33.0-120 8.58 25 Hexachlorocyclopentadiene 0.745 U 0.195 0.187 26.2 25.1 1 10.0-120 4.33 33 Hexachloroethane 0.745 U 0.385 0.348 51.6 46.7 1 21.0-120 10.0 30 Indeno(1,2,3-cd)pyrene 0.745 U 0.500 0.456 67.1 61.2 1 10.0-120 9.13 30 Isophorone 0.745 U 0.383 0.361 51.4 48.5 1 38.0-120 5.95 22 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 91 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 91 of 98 ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1062710 Semi Volatile Organic Compounds (GC/MS) by Method 8270D L963090-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19 L963090-12 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L963090-12 01/19/18 01:09 • (MS) R3280484-4 01/19/18 01:33 • (MSD) R3280484-5 01/19/18 01:56 Spike Amount (dry) Original Result (dry)MS Result (dry)MSD Result (dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg %%%%% Naphthalene 0.745 U 0.412 0.392 55.3 52.6 1 37.0-120 4.91 25 Nitrobenzene 0.745 U 0.408 0.386 54.8 51.8 1 32.0-120 5.49 24 n-Nitrosodimethylamine 0.745 U 0.514 0.472 69.0 63.4 1 18.0-120 8.49 27 n-Nitrosodiphenylamine 0.745 U 0.522 0.530 70.1 71.1 1 20.0-125 1.37 25 n-Nitrosodi-n-propylamine 0.745 U 0.466 0.463 62.5 62.1 1 34.0-120 0.575 23 Phenanthrene 0.745 U 0.572 0.551 76.7 73.9 1 24.0-124 3.71 25 Benzylbutyl phthalate 0.745 U 0.484 0.462 64.9 62.0 1 18.0-130 4.67 27 Bis(2-ethylhexyl)phthalate 0.745 U 0.534 0.521 71.7 69.8 1 19.0-127 2.63 28 Di-n-butyl phthalate 0.745 U 0.607 0.579 81.4 77.7 1 29.0-120 4.64 26 Diethyl phthalate 0.745 U 0.446 0.442 59.8 59.3 1 42.0-121 0.925 23 Dimethyl phthalate 0.745 U 0.488 0.468 65.5 62.8 1 42.0-120 4.25 23 Di-n-octyl phthalate 0.745 U 0.604 0.599 81.0 80.4 1 21.0-122 0.718 27 Pyrene 0.745 U 0.511 0.490 68.5 65.8 1 19.0-127 4.10 29 1,2,4-Trichlorobenzene 0.745 U 0.394 0.361 52.9 48.4 1 39.0-120 8.94 25 4-Chloro-3-methylphenol 0.745 U 0.414 0.402 55.5 53.9 1 37.0-121 2.92 23 2-Chlorophenol 0.745 U 0.486 0.472 65.2 63.3 1 34.0-120 2.98 25 2,4-Dichlorophenol 0.745 U 0.437 0.425 58.6 57.0 1 41.0-120 2.72 22 2,4-Dimethylphenol 0.745 U 0.374 0.365 50.2 49.0 1 27.0-120 2.46 25 4,6-Dinitro-2-methylphenol 0.745 U 0.461 0.413 61.8 55.4 1 10.0-131 11.0 29 2,4-Dinitrophenol 0.745 U 0.331 0.257 44.5 34.5 1 10.0-142 25.2 30 2-Nitrophenol 0.745 U 0.447 0.434 59.9 58.2 1 34.0-124 2.97 27 4-Nitrophenol 0.745 U ND 0.462 0.000 62.0 1 26.0-133 J6 J3 200 25 Pentachlorophenol 0.745 U 0.461 0.474 61.8 63.5 1 15.0-152 2.71 26 Phenol 0.745 U 0.480 0.465 64.3 62.4 1 33.0-120 3.10 24 2,4,6-Trichlorophenol 0.745 U 0.514 0.502 69.0 67.4 1 40.0-125 2.31 24 (S) Nitrobenzene-d5 45.4 42.0 18.0-125 (S) 2-Fluorobiphenyl 65.2 61.8 28.0-120 (S) p-Terphenyl-d14 40.4 45.0 13.0-131 (S) Phenol-d5 62.4 61.2 20.0-120 (S) 2-Fluorophenol 71.2 68.0 20.0-120 (S) 2,4,6-Tribromophenol 95.4 45.0 17.0-137 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 92 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 92 of 98 ONE LAB. NATIONWIDE.GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions (dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. MDL (dry)Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. RDL (dry)Reported Detection Limit. Rec.Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Dilution If the sample matrix contains an interfering material, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. Result The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL” (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non-conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control Summary (Qc) This section of the report includes the results of the laboratory quality control analyses required by procedure or analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of Custody (Sc) This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. J The identification of the analyte is acceptable; the reported value is an estimate. J0 J0: Calibration verification outside of acceptance limits. Result is estimated. J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. J7 Surrogate recovery cannot be used for control limit evaluation due to dilution. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 93 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 93 of 98 ONE LAB. NATIONWIDE. ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. * Not all certifications held by the laboratory are applicable to the results reported in the attached report. 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If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. 1 Cp 2Tc 3Ss 4Cn 5Sr 6Qc 7Gl 8Al 9Sc ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:35 94 of 98 ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE: Withers & Ravenel Eng. - Standard 02170761 L963090 01/25/18 13:54 94 of 98 APPENDIX B Boring Logs Boring #Job Name Date Site Loc. WR Rep Driller NC NAD83 Easting: From To 0.0 5.0 Boring ID Sample Depth PID FID BF1 0-5 4.2 0.0 BF2 0-5 3.6 0.4 BF3 0-5 3.5 0.1 BF4 0-5 3.6 0.0 BF5 0-5 3.4 0.0 BF6 0-5 3.1 0.0 BF7 0-5 3.2 0.0 BF8 0-5 3.4 0.0 Note: TOC - Top of Casing BLS - Below land surface Soil Description (Field USCS Classification) 115 MacKenan Drive | Cary, NC 27511 t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832 Cary | Greensboro | Pittsboro | Raleigh | Wilmington Page 1 of 1 See Table 1 Depth in Feet Borings BF1 through BF8 advanced in Buffaloe Landfill obtained fill. Sandy Clay (CL); 60% fines; Fine-Med Sand; low-med plasticity; Red; Moist; No odors SOIL BORING LOG January 11, 2018 Raleigh, NC 02170761.00Job #BF1 through BF8 M. James Quantex NC NAD83 Northing:See Table 1 607 - 617 West South Street Boring #Job Name Date Site Loc. WR Rep Driller NC NAD83 Easting: From To 0.0 2.0 2.0 9.5 9.5 15.0 Boring ID Sample Depth PID FID BF6 0-5 800 3000.0 BF6 5-10 >3000 >15000 BF6 10-15 40 364 Note: TOC - Top of Casing BLS - Below land surface 115 MacKenan Drive | Cary, NC 27511 t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832 Cary | Greensboro | Pittsboro | Raleigh | Wilmington Sand some clay (SC); Coarse Sand; Resembles Saprolite; White; Wet; Petro Odor Sandy Clay (CL); Fill; 60% fines; Fine-Med Sand; low-med plasticity; Red; Moist; No odors Sand some clay (SC); Fill; Med Grain; 30% Fines; Tan / Grey; Moist; Petro Odor; Wet at 8 ft Page 1 of 1 See Table 1 NC NAD83 Northing:See Table 1 Depth in Feet Soil Description (Field USCS Classification) January 11, 2018 Raleigh, NC M. James Quantex SOIL BORING LOG BF6 (Adj to MW-1)607 - 617 West South Street Job #02170761.00 Boring #Job Name Date Site Loc. WR Rep Driller NC NAD83 Easting: From To 0.0 4.0 4.0 9.0 9.0 15.0 Boring ID Sample Depth PID FID BF12 0-5 40 146.0 BF12 5-10 8.0 60 BF12 10-15 6.3 5.1 Note: TOC - Top of Casing BLS - Below land surface Page 1 of 1 115 MacKenan Drive | Cary, NC 27511 t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832 Cary | Greensboro | Pittsboro | Raleigh | Wilmington Sandy Clay (CL); Fill; 60% fines; Fine-Med Sand; low-med plasticity; Red; Moist; No odors Sand some clay (SC); Fill; Med Grain; 30% Fines; Tan / Grey; Moist; Petro Odor; Wet at 8 ft Sand some clay (SC); Coarse Sand; Resembles Saprolite; White; Wet; Petro Odor See Table 1 NC NAD83 Northing:See Table 1 Depth in Feet Soil Description (Field USCS Classification) January 11, 2018 Raleigh, NC M. James Quantex SOIL BORING LOG BF12 607 - 617 West South Street Job #02170761.00 Boring #Job Name Date Site Loc. WR Rep Driller NC NAD83 Easting: From To 0.0 4.0 4.0 5.0 5.0 10.0 Boring ID Sample Depth PID FID BF13 0-5 1000 4000.0 BF13 5-10 1200 6000 Note: TOC - Top of Casing BLS - Below land surface Page 1 of 1 115 MacKenan Drive | Cary, NC 27511 t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832 Cary | Greensboro | Pittsboro | Raleigh | Wilmington Sandy Clay (CL); Fill; 60% fines; Fine-Med Sand; low-med plasticity; Red; Moist; No odors Sand some clay (SC); Fill; Med Grain; 30% Fines; Tan / Grey; Moist; Petro Odor; Wet at 8 ft Silt some sand (MH); 70% fines; Frey; increasing moisture with depth; Petro Odor. See Table 1 NC NAD83 Northing:See Table 1 Depth in Feet Soil Description (Field USCS Classification) January 11, 2018 Raleigh, NC M. James Quantex SOIL BORING LOG BF13 607 - 617 West South Street Job #02170761.00 Boring #Job Name Date Site Loc. WR Rep Driller NC NAD83 Easting: From To 0.0 0.5 0.5 5.0 Boring ID Sample Depth PID FID BF14 0-5 250 1000.0 Note: TOC - Top of Casing BLS - Below land surface Page 1 of 1 115 MacKenan Drive | Cary, NC 27511 t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832 Cary | Greensboro | Pittsboro | Raleigh | Wilmington Sandy Clay (CL); Fill; 60% fines; Fine-Med Sand; low-med plasticity; Red; Moist; No odors Sand some clay (SC); Fill; Med Grain; 30% Fines; Tan / Grey; Moist; Petro Odor; See Table 1 NC NAD83 Northing:See Table 1 Depth in Feet Soil Description (Field USCS Classification) January 11, 2018 Raleigh, NC M. James Quantex SOIL BORING LOG BF14 607 - 617 West South Street Job #02170761.00 Boring #Job Name Date Site Loc. WR Rep Driller NC NAD83 Easting: From To 0.0 0.5 0.5 5.0 Boring ID Sample Depth PID FID BF14 0-5 250 1000 Note: TOC - Top of Casing BLS - Below land surface Page 1 of 1 115 MacKenan Drive | Cary, NC 27511 t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832 Cary | Greensboro | Pittsboro | Raleigh | Wilmington Sandy Clay (CL); Fill; 60% fines; Fine-Med Sand; low-med plasticity; Red; Moist; No odors Sand some clay (SC); Fill; Fine Grain; 30% Fines; Tan / Grey; Moist; Petro Odor; See Table 1 NC NAD83 Northing:See Table 1 Depth in Feet Soil Description (Field USCS Classification) January 11, 2018 Raleigh, NC M. James Quantex SOIL BORING LOG BF15 607 - 617 West South Street Job #02170761.00 Boring #Job Name Date Site Loc. WR Rep Driller NC NAD83 Easting: From To 0.0 0.5 0.5 5.0 Boring ID Sample Depth PID FID BF14 0-5 120 700 Note: TOC - Top of Casing BLS - Below land surface Page 1 of 1 115 MacKenan Drive | Cary, NC 27511 t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832 Cary | Greensboro | Pittsboro | Raleigh | Wilmington Sandy Clay (CL); Fill; 60% fines; Fine-Med Sand; low-med plasticity; Red; Moist; No odors Sand some clay (SC); Fill; Fine Grain; 30% Fines; Tan / Grey; Moist; Petro Odor; See Table 1 NC NAD83 Northing:See Table 1 Depth in Feet Soil Description (Field USCS Classification) January 11, 2018 Raleigh, NC M. James Quantex SOIL BORING LOG BF16 607 - 617 West South Street Job #02170761.00