The URL can be used to link to this page

Home My WebLink About22004_Witherspoon Nursery_RevRRPT_20180425April 25, 2018 Mr. Chris Howlett Beacon Properties & Investments 16122 Morehead Drive Chapel Hill, North Carolina 27517 Re: Soil Excavation Activities — Witherspoon Roses Property Heating Oil Aboveground Storage Tank 3312 Watkins Road Durham, Durham County, North Carolina ATC Project No. BEACONAST Dear Mr. Howlett: ;ETC ENVIRONMENTAL • GEOTECHNICAL BUILDING SCIENCES • MATERIALS TESTING ATC Associates of North Carolina, P.C. (ATC) has prepared this letter report regarding soil excavation activities conducted at the Witherspoon Roses property at 3312 Watkins Road in Durham, Durham County, North Carolina. BACKGROUND The property has historically operated as a rose landscaping business and garden supply shop since 1979. In September 2017, Terracon conducted a Phase II Limited Site Investigation for the property. During these activities, a soil sample was collected from the area of an on -site heating oil aboveground storage tank (AST). Laboratory analytical results of the soil sample detected Total Petroleum Hydrocarbon (TPH) — Diesel Range Organics (DRO) at a concentration of 270 milligrams per kilogram (mg/kg), which is above the North Carolina Department of Environmental Quality (NCDEQ) Action Level of 100 mg/kg. SOIL EXCAVATION ACTIVITIES On March 5, 2018, ATC contracted with Eastern Environmental Management (EEM) of Rocky Mount, North Carolina to assist with the excavation of petroleum -impacted soil in proximity to the 280-gallon heating oil aboveground storage tank (AST) (labeled AST-3). The heating oil AST was transported from the property for proper disposal on March 5, 2018. Prior to its removal, approximately 68 gallons of heating oil were removed from the AST. It should be noted underground piping was not encountered during removal of the heating oil AST. The approximate location of the heating oil AST is provided in Attachment I. A copy of the pump out manifest and AST disposal manifest are provided in Attachment II On March 5, 2018, EEM and ATC personnel excavated approximately 5.69 tons of petroleum -impacted soil from the area of AST-3. The AST-3 excavated area measured approximately seven to nine feet in length, seven to nine feet in width, and approximately four feet in depth. The soil was mainly tan to light gray sand with fine to medium gravel to approximately three feet below ground surface (bgs). Groundwater was not encountered during excavation activities. Excavated soils were placed directly into a dump truck and disposed of at Soil Resources, LLC in Pinetops, North Carolina. The soil excavation area, as well as pictures of excavation activities, are provided in Attachment I. The waste manifest for the soil is included in Attachment II. ATC Associates of North Carolina, P.C. 609A Piner Road, Suite115 Wilmington, NC 28409 USA Phone: +1 919 8710999 Fax: +1 737 207 8261 www.atcqs.com s r rTC ® ENVIRONMENTAL• GEOTECHNICAL BUILDING SCIENCES • MATERIALS TESTING April 25, 2018 Page 2 of 2 ATC personnel performed confirmatory soil sampling prior to backfilling the excavated area of AST-3. One soil sample was collected the bottom of the excavation and from each sidewall by hand using clean nitrile gloves between each sampling location. The soil samples were labeled according to their location. These samples were collected to determine the effectiveness of the soil excavation activities. The locations of the confirmatory soil samples are depicted on Attachment I. All samples were collected in laboratory -supplied containers and shipped on ice to Con -test Analytical Laboratory (Con -test) located in East Longmeadow, Massachusetts. Confirmation soil samples collected from excavation area AST-3 utilized Environmental Protection Agency (EPA) Method 8260 and EPA Method 8270. It should be noted one soil sample, AST-3 North (1-2) also was analyzed by Total Petroleum Hydrocarbons-(TPH) — Gasoline Range Organics (GRO) and Diesel Range Organics (DRO) and TCLP Metals for soil disposal purposes. Based on the laboratory analytical results utilizing EPA Method 8260 and EPA Method 8270, target compound concentrations were not detected above Soil -to -Groundwater (STGW) Maximum Contaminant Concentrations (MSCCs) in the soil samples collected from the AST-3 excavation area. Target compound concentration detected above the laboratory method detection limit, but below the STGW-MSCCs, are presented in Attachment III. A copy of the laboratory reports and chains -of -custody documents are provided in Attachment IV. Following completion of excavation activities, the excavated area was backfilled with clean fill material that was obtained from another portion of the property. The approximate area where the clean fill material was obtained is provided on Attachment V. CONCLUSIONS Based on the above activities and subsequent laboratory results, it appears heating oil -impacted soil have been effectively removed from the area of the former heating oil AST and no other activities are warranted at this time. If you have any questions or require additional information, please contact our office at (919) 871-0999. Sincerely, ATC Associates of North dAq.Z Maureen Jackson, P.G. = 231 Senior Project Manager �ma�yy'•, 67(47 , N.C. Licensed GeologisLo t�d6� N 0840611141 Benjamin V. Wilson, P.E. ( = Principle Geotechnical Engineer Attachment I bi I WatklnS.Rd IF AV 609A Piner Road, Suite 115 NkTc Wilmington, North Carolina 28409 ENVIRONMENTAL • GEOTECHNICAL (919) 871-0999 BUILDING SCIENCES - MATERIALS TESTING Project No. DATE: PM: BEACONAST 03/14/2018 Maureen Jackson B�C�C1 Figure 1: Soil Excavation Area Witherspoon Roses Property 3312 Watkins Road Durham, Durham County, North Carolina 0 Photo 1: View of 280-gallon Heating Oil AST (AST-3) prior to removal (looking north). Photo 2: View of Soil Excavation in area of Former Heating Oil AST (AST-3). Witherspoon Roses Property 3312 Watkins Road Durham, North Carolina ATC Project No. BEACONAST Photo 3: View of AST-3 Excavation Backfilled Photo 4: Source location of backfill material (looking west) Witherspoon Roses Property 3312 Watkins Road Durham, North Carolina ATC Project No. BEACONAST Attachment II Eastern Environmental Management P.O. Box 4030 • Rocky Mount, NC 27803 Office (252) 443-2224 (24 Hrs.) • Fax (252) 972-9940 www.eastern-environmental.com NON -HAZARDOUS 1. Generator's US EPA ID No. Manifest 2. Page WASTE MANIFEST I I Document No. of 3. Generator's Name and Mailing Address h of t 6 Pet/ Contact: ba,1-4 W A4-kinS k_ A 4. Generator's Phone 5. Transporter 1 Company Name 6. US EPA ID Number A. State Transporter's ID 600308640 EASTERN ENVIRONMENTAL MANAGEMENT NCR000146456 B. Transporter 1 Phone 252-443-2224 7. Transporter 2 Company Name 8. US EPA ID Number C. State Transporter's ID D. Transporter 2 Phone 9. Designated aco'sility Name and Site Address 10. US EPA ID Number 4 t g E. State Facility's ID V\ e r _ F. Facility's Phone Z�Z-C(3 -Z,Z-Z 11. WASTE DESCRIPTION 12. Containers 13. 14. No. Type Total Quantity Unit Wt./Vol. a. E ViV 'i �� s VAT5" 1 Z GLri v4-i N b E R A T c. O R d. e. f. 15. Special Handling Instructions and Additional Information 16, GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fully and accurately described and are in all respects in proper condition for transport. The materials described on this manifest are not subject to federal hazardous waste regulations. Date Printed/Typed Name Signature Month Day Y TR 17. Transporter 1 Acknowledgment of Receipt of Material Date A O Pr/Typed Na e Sig Month Da Ye r S V`/ � � � p18. Transp rter 2 Acknowledgment of Receipt of Materials Date TPrinted/Typed Name Signature Month Day Year E R I I F 19. Discrepancy Indication Space A c I L 20. F�t Owner or Operator: Certification of receipt of the waste materials cov d y this anif except as noted in item 19. I Date � T Prin / ype Name Signatur th Da Y Y I I ` I /, Soil Resources, LLC N Physical Address: 402 Orchard Road Pinetops, NC Office: 252-904-2457 Mailing Address: PO Box 4005 Rocky Mount, NC 27803 Fax: 252-972-9940 Soil Resources, LLC is operating under the State of North Carolina Contaminated Soil Disposal Permit # SR-0002, hereby acknowledges the receipt of 5.69 tons of soil contaminated with petroleum hydrocarbons and will properly execute the disposal of this soil in the prescribed manner set forth by the North Carolina Department of Environment and Natural Resources, Division of Waste Management, and in accordance with the requirements of SR-0002. Company: Eastern Environmental Management PO Box 4030 Rocky Mount, NC 27803 Generator: Witherspoon Property 3312 Watkins Rd Durham, NC Transporter: Eastern Environmental Management, LLC PO Box 4030 Rocky Mount, NC 27803 Date(s) Received: 03/05/18 (E-09630) Soil Resources, LLC By: cry C. gai�i� Eastern Environmental Management P.O. Box 4030 - Rocky Mount, NC 27803 Office (252) 443-2224 (24 Hrs.) - Fax (252) 972-9940 www.eastem-environmental.com NON -HAZARDOUS 1Generator's US EPA ID No. Manifest 2. Page WASTE MANIFEST Document No. Of 3. Generator's Name and Mailing Address .g6iCq;1 e contact: fklis L 4. Generator's Phone pd.,-L 5. Transporter I Company Name 6. US EPA ID Number A. State Transporter's ID 600308640 EASTERN ENVIRONMENTAL MANAGEMENT I NCR0001 46456 B. Transporter 1 Phone 252-443-2224 7. Transporter 2 Company Name 8. US EPA ID Number C. State Transporter's ID Transporter 2 Phone ID. 9. Designated Facility Name and Site Address 10. US EPA ID Number E. State Facility's ID F. Facility's Phone 1 �11 11. WASTE 6ESCRIPTION 12. Containers 13. 14. No. Type Total Quantity Unit Wt./Vol. a. 14 E N E b. R A T c- 0 d. e. f. 15. Special Handling Instructions and Additional Information ErAW" ""AWNW—AffM MAW AF� MAWMAW, 16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fully and accurately described and are in all respects in proper condition for transport. The materials described on this manifest are not subject to federal hazardous aste regulations. F—Date Pinted/Typmd ame Srainafuria( Month Day Yea 17. Transporter 1 Acknowledgment of Receipt of Material Date Pried yped Na, e Signat Month Day Year 0 R 18. Transporter 2 Ackfiowledgment of Receipt of Materials ,2 Date T Printed/Typed Name Signature Month Day Year E R F 19. Discrepancy Indication Space A C I L )�ility Owner or Operator: Certification of receipt of the waste materials covql;ed_Ja5rthisr`cept as noted in item 19. I Date: T Y PriptegrType Name ��6 1 M th Da Year y Jr� Eastern Environmental Management P.O. Box 4030 - Rocky Mount, NC 27803 Office (252) 443-2224 (24 Hrs.) - Fax (252) 972-9940 www.eastem-environmental.com NON -HAZARDOUS Generator's US EPA ID No. Manifest 2. Page WASTE MANIFEST 11. Document No. of 3. Generator's Name and Mailing Address Contact: J 4. Generator's Phone or� 5. Transporter 1 Company Name 6. US EPA ID Number A. State Transporter's ID 600308640 EASTERN ENVIRONMENTAL MANAGEMENT I NCR0001 46456 B. Transporter 1 Phone 252-443-2224 7. Transporter 2 Company Name 8. US EPA ID Number C. State Transporter's ID Transporter 2 Phone ID. 9. Dpsignated Facility Name and Site Address 10. US EPA ID Number E. State Facility's ID F. Facility's Phone iAl� T 3 1 A/C Z, _7 11. WASTE DESCRIPTION 12. Containers 13. 14. No. Type Total Quantity Unit Wt.1vol. a. G T t- ,_ N b. E R A T c. 0 R d. e. f. 15. Special Handling Instructions and Additional Information IF Aw" AM Aff " WAWW__�W�� AV M 16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fully and accurately described and are in all respects in proper condition for transport. The materials described on this manifest are not subject to federal hazardous waste regulations. Date Printed/Typed Name g u Month D�p Year ft,r,, _5 T 17. Transporter I"Acknowledgment of Receipt-Itif Material Date R A Pr' to I /Typed Na e Si to Month Day Year N S c IY /vk e J P 0 R 18. Trans 2 Acknowledgment of Receipt of Materials Date T Printed/Typed Name Signature Month Day Year E RI F 19. Discrepancy Indication Space A C I L Yity 0 r Operator: Certification of receipt of the waste materials tl;ri �,Kanifest, except as noted in item 19. 20. Fa wnerfo W1 I .4 Date T Printe yp ame Si r Month Day Y I "- 4, W� , I I Eastern Environmental Management, LLC P.O. Box 4030 Rocky Mount, NC 27803 Office (252) 443-2224 (24 Hrs.) Fax (252) 972-9940 www.eastem-environinental.com Cerujicate of disposal Generator: Witherspoon Roses Property 3312 Watkins RD Durham, NC Material Accepted: 1- TT (s)- (68-gal.) — Non -hazardous Material - Petroleum Contact Water 1-DM (s)- (280) — AST fuel oil tank Disposal Method: Waste water treatment Recycle Eastern Environmental Management LLC. Accepted the above materials on 03/05/2018 Eastern Environmental Management LLC has accepted custody of the above referenced non -hazardous material. This material has been determined to be non -hazardous by a material profile, generator knowledge, and/o�Inalytical data provided to Eastern Environmental Management, LLC. CEO. Attachment III Table 1 Soil Excavation Confirmation Laboratory Results Witherspoon Roses Property 3312 Watkins Road Durham, North Carolina ATC Project No. BEACONAST EPA METHOD ANALTYICAL METHOD 8270 Sample Sample ID Date PID Depth .� Sampled (ppm) Q' (feet) � AST-3 Floor 3/5/2018 0.8 3 <0.43 <1.3 AST-3 North (1-2) 3/5/2018 2.9 1-2 <0.41 0.45J AST-3 North (3-4) 3/5/2018 0.0 3-4 <0.40 <1.2 AST-3 South 3/5/2018 0.0 1-2 <0.42 <1.2 AST-3 West 3/5/2018 0.0 1-2 <0.40 <1.2 AST-3 East 3/5/2018 1.2 1-2 <0.43 <1.3 Soil -to -Groundwater MSCCs NE 120 Notes: 1. Concentrations reported in milligrams per kilogram (mg/kg). 2. "<" = not detected at or above the laboratory detection limit. 3. NE denotes Soil -to -Groundwater MSCC has not been established. 4. J value denotes concentration estimated by the laboratory. 5. MSCC denotes Maximum Soil Contaminant Concentration Attachment IV ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 March 13, 2018 Maureen Jackson ATC Group Services LLC - Raleigh NC 2725 East Millbrook Road, Ste 121 Raleigh, NC 27604 Project Location: 3312 Watkins Rd Client Job Number: Project Number: [none] Laboratory Work Order Number: 18C0324 Enclosed are results of analyses for samples received by the laboratory on March 6, 2018. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Page 1 of 94 Table of Contents Table of Contents Sample Summary Hits Only Report Case Narrative Sample Results 18C0324-01 18C0324-02 18C0324-03 18C0324-04 18C0324-05 18C0324-06 18C0324-07 18C0324-08 18C0324-09 18C0324-10 18C0324-11 Sample Preparation Information QC Data Volatile Organic Compounds by GC/MS B 198462 Semivolatile Organic Compounds by GUMS B198559 Petroleum Hydrocarbons Analyses B 198557 B198651 Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 4 5 7 11 11 16 21 26 31 36 41 48 53 58 63 68 70 70 70 75 75 83 83 83 84 Page 2 of 94 Table of Contents Table of Contents (continued) B 198433 TCLP - Metals Analyses B 198629 B 198633 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 84 85 85 85 86 87 91 Page 3 of 94 Table of Contents 40 ,con -testy ANALYTICAL LABORATORY 39 Spruce StreetEast Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 ATC Group Services LLC - Raleigh NC 2725 East Millbrook Road, Ste 121 REPORT DATE: 3/13/2018 Raleigh, NC 27604 PURCHASE ORDER NUMBER: ATTN: Maureen Jackson PROJECT NUMBER: [none] ANALYTICAL SUMMARY WORK ORDER NUMBER: 18CO324 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 3312 Watkins Rd FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB AST-1 Floor 18C0324-01 Soil SM 254OG SW-846 8260B SW-846 8270D AST-1 South 18C0324-02 Soil SM 2540G SW-846 8260B SW-846 8270D AST-1 North 18C0324-03 Soil SM 254OG SW-846 8260B SW-846 8270D AST-1 West 18C0324-04 Soil SM 2540G SW-846 8260B SW-846 8270D AST-1 East 18C0324-05 Soil SM 2540G SW-846 8260B SW-846 8270D AST-3 Floor 18C0324-06 Soil SM 2540G SW-846 8260B SW-846 8270D AST-3 North (1-2) 18C0324-07 Soil SM 2540G SW-846 601OC-D SW-846 7470A SW-846 8015C SW-846 8260B SW-846 8270D AST-3 North (3-4) 18C0324-08 Soil SM 2540G SW-846 8260B SW-846 8270D AST-3 South 18C0324-09 Soil SM 2540G SW-846 8260B SW-846 8270D AST-3 West 18C0324-10 Soil SM 254OG SW-846 8260B SW-846 8270D AST-3 East 18C0324-11 Soil SM 2540G SW-846 8260B SW-846 8270D Page 4 of 94 ,con -testy ANALYTICAL LABORATORY Table of Contents Client ID: AST-1 Floor Analyte Butylbenzylphthalate % Solids Client ID: AST-1 South Analyte % Solids Client ID: AST-1 North Analyte Benzoic Acid % Solids Client ID: AST-1 West Analyte % Solids Client ID: AST-1 East Analyte % Solids Client ID: AST-3 Floor Analyte % Solids Client ID: AST-3 North (1-2) Analyte Benzoic Acid Diesel Range Organics % Solids Barium Lead Mercury Client ID: AST-3 North (3-4) Analyte % Solids Client ID: AST-3 South Analyte % Solids Client ID: AST-3 West Analyte % Solids 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 EXECUTIVE SUMMARY Lab ID: 18C0324-01 Results/Qual DL RL Units Method 0.12 J 0.093 0.39 mg/Kg dry SW-846 8270D 87.0 % Wt SM 2540G Lab ID: 18CO324-02 Results/Qual DL RL Units Method 85.4 % Wt SM 2540G Lab ID: 18CO324-03 Results/Qual DL RL Units Method 0.27 J 0.21 1.2 mg/Kg dry SW-846 8270D 85.4 % Wt SM 2540G Lab ID: 18CO324-04 Results/Qual DL RL Units Method 88.6 % Wt SM 2540G Lab ID: 18C0324-05 Results/Qual DL RL Units Method 84.5 % Wt SM 2540G Lab ID: 18C0324-06 Results/Qual DL RL Units Method 78.4 % Wt SM 2540G Lab ID: 18CO324-07 Results/Qual DL RL Units Method 0.45 1 0.22 1.2 mg/Kg dry SW-846 8270D 1600 23 100 mg/Kg dry SW-846 8015C 82.3 % Wt SM 2540G 0.22 0.0053 0.050 mg/L SW-846 601OC-D 0.14 0.0044 0.010 mg/L SW-846 601OC-D 0.000059 J 0.000034 0.00010 mg/L SW-846 7470A Lab ID: 18CO324-08 Results/Qual DL RL Units Method 84.2 % Wt SM 2540G Lab ID: 18CO324-09 Results/Qual DL RL Units Method 81.5 % Wt SM 2540G Lab ID: 18C0324-10 Results/Qual DL RL Units Method 85.8 % Wt SM 2540G Page 5 of 94 ,con -testy ANALYTICAL LABORATORY Table of Contents Client ID: AST-3 East Analyte % Solids 39 Spruce Street' East Longmeadow, MA 01028' FAX 413/525-6405 ` TEL. 413/525-2332 Lab ID: 18C0324-11 Results/Qual DL RL Units Method 78.3 % Wt SM 2540G Con -Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary section of this report. Users must review this report in its entirety to determine data usability and assessment. Page 6 of 94 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. Page 7 of 94 Table of Contents 40 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 SW-846 6010C-D Qualifications: L-02 Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is on the high side. Analyte & Samples(s) Qualified: Selenium 18C0324-07[AST-3 North (1-2)], B198629-BS1, B198629-BSDI SW-846 8260B Qualifications: L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side. Analyte & Samples(s) Qualified: Chloromethane 18C0324-01[AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor], 18C0324-07[AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-II[AST-3 East], B198462-BLKI, B198462-BS1, B198462-BSD1 SW-846 8270D Qualifications: L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. Analyte & Samples(s) Qualified: Pyridine B 198559-BS 1 MS-09 Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample matrix effects that lead to a low bias for reported result or non -homogeneous sample aliquots cannot be eliminated. Analyte & Samples(s) Qualified: 3,3-Dichlorobenzidine 18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI 4-Chloroaniline 18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI 4-Nitroaniline 18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI Aniline 18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI Benzidine 18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI Pyridine 18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI MS-22 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is within method specified criteria. Analyte & Samples(s) Qualified: 3-Nitroaniline B198559-MSI R-06 Matrix spike duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result for this compound in this sample. Analyte & Samples(s) Qualified: 4-Chloroaniline 18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI Page 8 of 94 ,con-testo ANALYTICAL LABORATORY Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method specified criteria. Reported result is estimated. Analyte & Samples(s) Qualified: Benzidine 18C0324-01[AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor], 18C0324-07[AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI, 13198559-13SI, B198559-BSDI, B198559-MS1, B198559-MSD1 V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. Analyte & Samples(s) Qualified: Aniline 18C0324-OI[AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor], 18C0324-07[AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI, 13198559-13SI, B198559-BSDI, B198559-MS1, B198559-MSD1 Benzidine 18C0324-01[AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor], 18C0324-07[AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI, B198559-BSI, B198559-BSDI, B198559-MS1, B198559-MSD1 Pyridine 18C0324-OI[AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor], 18C0324-07[AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-II[AST-3 East], B198559-BLKI, B198559-BS1, B198559-BSD1, B198559-MS1, B198559-MSD1 V-16 Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. Analyte & Samples(s) Qualified: Pentachloronitrobenzene 18C0324-01[AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor], 18C0324-07[AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI, B198559-BS1, B198559-BSD1, B198559-MS1, B198559-MSD1 V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: 2-Nitroaniline 18C0324-01[AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor], 18C0324-07[AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI, B198559-BS1, B198559-BSD1, B198559-MS1, B198559-MSD1 4-Nitrophenol 18C0324-01[AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor], 18C0324-07[AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-II[AST-3 East], B198559-BLKI, B198559-BS1, B198559-BSD1, B198559-MS1, B198559-MSD1 N-Nitrosodimethylamine 18C0324-01[AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor], 18C0324-07[AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI, B198559-BS1. B198559-BSD1. B198559-MS1. B198559-MSD1 V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. Analyte & Samples(s) Qualified: 4-Chloroaniline B198559-BLKI, 13198559-13SI, B198559-BSDI, B198559-MS1 Page 9 of 94 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 SW-846 601OC/D SW-846 602OA/B For NC, Metals methods SW-846 6010D and SW-846 6020B are followed, and for all other states methods SW-846 6010C and SW-846 6020A are followed. SW-846 8015C Gasoline Range Organics (2-Methylpentane through 1,2,4-Trimethylbenzene) is quantitated against a calibration made with an unleaded gasoline composite standard. Diesel Range Organics (C 10-C28) is quantitated against a calibration made with a #2 fuel oil standard. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Project Manager Page 10 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15 Sample ID: 18C0324-01 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.083 0.019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Acrylonitrile ND 0.0050 0.0021 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF tert-Amyl Methyl Ether (TAME) ND 0.00083 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Benzene ND 0.0017 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Bromobenzene ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Bromochloromethane ND 0.0017 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Bromodichloromethane ND 0.0017 0.00050 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:03 MFF Bromoform ND 0.0017 0.0012 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:03 MFF Bromomethane ND 0.0083 0.0035 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 2-Butanone (MEK) ND 0.033 0.015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF tert-Butyl Alcohol (TBA) ND 0.033 0.017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF n-Butylbenzene ND 0.0017 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF sec-Butylbenzene ND 0.0017 0.00083 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF tert-Butylbenzene ND 0.0017 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00083 0.00050 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Carbon Disulfide ND 0.0050 0.0036 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Carbon Tetrachloride ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Chlombenzene ND 0.0017 0.00058 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:03 MFF Chlorodibromomethane ND 0.0017 0.00058 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:03 MFF Chloroethane ND 0.017 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Chloroform ND 0.0033 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Chloromethane ND 0.0083 0.0053 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 2-Chlorotoluene ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 4-Chlorotoluene ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0017 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,2-Dibromoethane (EDB) ND 0.0017 0.00083 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Dibromomethane ND 0.0017 0.00050 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,2-Dichlorobenzene ND 0.0017 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,3-Dichlorobenzene ND 0.0017 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,4-Dichlorobenzene ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF trans-1,4-Dichloro-2-butene ND 0.0033 0.0017 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:03 MFF Dichlorodifluoromethane (Freon 12) ND 0.017 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,1-Dichloroethane ND 0.0017 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,2-Dichloroethane ND 0.0017 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1, 1 -Dichloroethylene ND 0.0033 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF cis-1,2-Dichloroethylene ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF trans-1,2-Dichloroethylene ND 0.0017 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,2-Dichloropropane ND 0.0017 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,3-Dichloropropane ND 0.00083 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 2,2-Dichloropropane ND 0.0017 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1, 1 -Dichloropropene ND 0.0017 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF cis-1,3-Dichloropropene ND 0.00083 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF trans-1,3-Dichloropropene ND 0.00083 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Diethyl Ether ND 0.017 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Page 11 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15 Sample ID: 18C0324-01 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.00083 0.00050 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,4-Dioxane ND 0.083 0.048 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Ethanol ND 0.17 0.033 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Ethylbenzene ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Hexachlorobutadiene ND 0.0017 0.00083 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 2-Hexanone (MBK) ND 0.017 0.0090 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Isopropylbenzene (Cumene) ND 0.0017 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF p-Isopropyltoluene (p-Cymene) ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0033 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Methylene Chloride ND 0.017 0.0059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 4-Methyl-2-pentanone (MIBK) ND 0.017 0.0063 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Naphthalene ND 0.0033 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF n-Propylbenzene ND 0.0017 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Styrene ND 0.0017 0.00050 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0017 0.0015 mg/Kgdry 1 SW-8468260B 3/8/18 3/8/18 8:03 MFF 1,1,2,2-Tetrachloroethane ND 0.00083 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Tetrachloroethylene ND 0.0017 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Tetrahydrofuran ND 0.0083 0.0018 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Toluene ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,2,3-Trichlorobenzene ND 0.0017 0.00050 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,2,4-Trichlorobenzene ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,3,5-Trichlorobenzene ND 0.0017 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1, 1, 1 -Trichloroethane ND 0.0017 0.00083 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,1,2-Trichloroethane ND 0.0017 0.00099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Trichloroethylene ND 0.0017 0.00083 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Trichlorofluoromethane (Freon 11) ND 0.0083 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,2,3-Trichloropropane ND 0.0017 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0083 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0017 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF 1,3,5-Trimethylbenzene ND 0.0017 0.00050 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Vinyl Chloride ND 0.0083 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF m+p Xylene ND 0.0033 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF o-Xylene ND 0.0017 0.00058 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:03 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 100 70-130 3/8/18 8:03 Toluene-d8 102 70-130 3/8/18 8:03 4-Bromofluorobenzene 102 70-130 3/8/18 8:03 Page 12 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15 Samnle ID: 18C0324-01 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.19 0.058 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Acenaphthylene ND 0.19 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Acetophenone ND 0.39 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Aniline ND 0.39 0.11 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Anthracene ND 0.19 0.056 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Benzidine ND 0.76 0.49 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Benzo(a)anthracene ND 0.19 0.052 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:06 BGL Benzo(a)pyrene ND 0.19 0.061 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:06 BGL Benzo(b)fluoranthene ND 0.19 0.055 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Benzo(g,h,i)perylene ND 0.19 0.086 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Benzo(k)fluoranthene ND 0.19 0.061 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Benzoic Acid ND 1.1 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Bis(2-chloroethoxy)methane ND 0.39 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Bis(2-chloroethyl)ether ND 0.39 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Bis(2-chloroisopropyl)ether ND 0.39 0.084 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Bis(2-Ethylhexyl)phthalate ND 0.39 0.15 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 4-Bromophenylphenylether ND 0.39 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Butylbenzylphthalate 0.12 0.39 0.093 mg/Kg dry I J SW-846 8270D 3/9/18 3/12/18 13:06 BGL Carbazole ND 0.19 0.050 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:06 BGL 4-Chloroaniline ND 0.76 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 4-Chloro-3-methylphenol ND 0.76 0.084 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2-Chloronaphthalene ND 0.39 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2-Chlorophenol ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 4-Chlorophenylphenylether ND 0.39 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Chrysene ND 0.19 0.061 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Dibenz(a,h)anthracene ND 0.19 0.12 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Dibenzofuran ND 0.39 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Di-n-butylphthalate ND 0.39 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 1,2-Dichlorobenzene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 1,3-Dichlorobenzene ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 1,4-Dichlorobenzene ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 3,3-Dichlorobenzidine ND 0.19 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2,4-Dichlorophenol ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Diethylphthalate ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2,4-Dimethylphenol ND 0.39 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Dimethylphthalate ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 4,6-Dinitro-2-methylphenol ND 0.39 0.37 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2,4-Dinitrophenol ND 0.76 0.22 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2,4-Dinitrotoluene ND 0.39 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2,6-Dinitrotoluene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Di-n-octylphthalate ND 0.39 0.20 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.39 0.063 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:06 BGL Fluoranthene ND 0.19 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Flumene ND 0.19 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Page 13 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15 Samnle ID: 18C0324-01 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Hexachlorobutadiene ND 0.39 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Hexachlorocyclopentadiene ND 0.39 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Hexachloroethane ND 0.39 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Indeno(1,2,3-cd)pyrene ND 0.19 0.14 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Isophorone ND 0.39 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 1-Methylnaphthalene ND 0.19 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2-Methylnaphthalene ND 0.19 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2-Methylphenol ND 0.39 0.097 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 3/4-Methylphenol ND 0.39 0.12 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Naphthalene ND 0.19 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2-Nitroaniline ND 0.39 0.065 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 3-Nitroaniline ND 0.39 0.056 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 4-Nitroaniline ND 0.39 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Nitrobenzene ND 0.39 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2-Nitrophenol ND 0.39 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 4-Nitrophenol ND 0.76 0.085 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 13:06 BGL N-Nitrosodimethylamine ND 0.39 0.25 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 13:06 BGL N-Nitrosodiphenylamine ND 0.39 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL N-Nitrosodi-n-propylamine ND 0.39 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Pentachloronitrobenzene ND 0.39 0.093 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Pentachlorophenol ND 0.39 0.094 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Phenanthrene ND 0.19 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Phenol ND 0.39 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Pyrene ND 0.19 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Pyridine ND 0.39 0.063 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 1,2,4,5-Texachlorobenzene ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 1,2,4-Trichlorobenzene ND 0.39 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2,4,5-Trichlorophenol ND 0.39 0.088 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL 2,4,6-Trichlorophenol ND 0.39 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:06 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 56.9 30-130 3/12/18 13:06 Phenol-d6 57.5 30-130 3/12/18 13:06 Nitrobenzene-d5 79.0 30-130 3/12/18 13:06 2-Fluorobiphenyl 74.0 30-130 3/12/18 13:06 2,4,6-Tribromophenol 79.6 30-130 3/12/18 13:06 p-Terphenyl-dl4 80.9 30-130 3/12/18 13:06 Page 14 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15 Samnle ID: 18C0324-01 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 87.0 % Wt 1 SM 2540G 3/8/18 3/8/18 19:26 DMP Page 15 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 South Sampled: 3/5/2018 10:20 Sample ID: 18C0324-02 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.091 0.021 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Acrylonitrile ND 0.0054 0.0023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF tert-Amyl Methyl Ether (TAME) ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Benzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Bromobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Bromochloromethane ND 0.0018 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Bromodichloromethane ND 0.0018 0.00054 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:30 MFF Bromoform ND 0.0018 0.0013 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:30 MFF Bromomethane ND 0.0091 0.0038 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 2-Butanone (MEK) ND 0.036 0.016 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF tert-Butyl Alcohol (TBA) ND 0.036 0.019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF n-Butylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF sec-Butylbenzene ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF tert-Butylbenzene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00091 0.00054 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Carbon Disulfide ND 0.0054 0.0039 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Carbon Tetrachloride ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Chlombenzene ND 0.0018 0.00064 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:30 MFF Chlorodibromomethane ND 0.0018 0.00064 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:30 MFF Chloroethane ND 0.018 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Chloroform ND 0.0036 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Chloromethane ND 0.0091 0.0058 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 2-Chlorotoluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 4-Chlorotoluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,2-Dibromoethane (EDB) ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Dibromomethane ND 0.0018 0.00054 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,2-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,3-Dichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,4-Dichlorobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF trans-1,4-Dichloro-2-butene ND 0.0036 0.0019 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:30 MFF Dichlorodifluoromethane (Freon 12) ND 0.018 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,1-Dichloroethane ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,2-Dichloroethane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1, 1 -Dichloroethylene ND 0.0036 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF cis-1,2-Dichloroethylene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF trans-1,2-Dichloroethylene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,2-Dichloropropane ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,3-Dichloropropane ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 2,2-Dichloropropane ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1, 1 -Dichloropropene ND 0.0018 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF cis-1,3-Dichloropropene ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF trans-1,3-Dichloropropene ND 0.00091 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Diethyl Ether ND 0.018 0.0016 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Page 16 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 South Sampled: 3/5/2018 10:20 Sample ID: 18C0324-02 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.00091 0.00054 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,4-Dioxane ND 0.091 0.052 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Ethanol ND 0.18 0.036 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Ethylbenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Hexachlorobutadiene ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 2-Hexanone (MBK) ND 0.018 0.0099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Isopropylbenzene (Cumene) ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF p-Isopropyltoluene (p-Cymene) ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0036 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Methylene Chloride ND 0.018 0.0064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 4-Methyl-2-pentanone (MIBK) ND 0.018 0.0069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Naphthalene ND 0.0036 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF n-Propylbenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Styrene ND 0.0018 0.00054 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0018 0.0016 mg/Kg dry 1 SW-8468260B 3/8/18 3/8/18 8:30 MFF 1,1,2,2-Tetrachloroethane ND 0.00091 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Tetrachloroethylene ND 0.0018 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Tetrahydrofuran ND 0.0091 0.0020 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Toluene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,2,3-Trichlorobenzene ND 0.0018 0.00054 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,2,4-Trichlorobenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,3,5-Trichlorobenzene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1, 1, 1 -Trichloroethane ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,1,2-Trichloroethane ND 0.0018 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Trichloroethylene ND 0.0018 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Trichlorofluoromethane (Freon 11) ND 0.0091 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,2,3-Trichloropropane ND 0.0018 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0091 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0018 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF 1,3,5-Trimethylbenzene ND 0.0018 0.00054 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Vinyl Chloride ND 0.0091 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF m+p Xylene ND 0.0036 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF o-Xylene ND 0.0018 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:30 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 100 70-130 3/8/18 8:30 Toluene-d8 98.2 70-130 3/8/18 8:30 4-Bromofluorobenzene 100 70-130 3/8/18 8:30 Page 17 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 South Sampled: 3/5/2018 10:20 Samnle ID: 18C0324-02 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.20 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Acenaphthylene ND 0.20 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Acetophenone ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Aniline ND 0.40 0.11 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Anthracene ND 0.20 0.057 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Benzidine ND 0.77 0.50 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Benzo(a)anthracene ND 0.20 0.053 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:30 BGL Benzo(a)pyrene ND 0.20 0.062 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:30 BGL Benzo(b)fluoranthene ND 0.20 0.056 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Benzo(g,h,i)perylene ND 0.20 0.088 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Benzo(k)fluoranthene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Benzoic Acid ND 1.2 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Bis(2-chloroethoxy)methane ND 0.40 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Bis(2-chloroethyl)ether ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Bis(2-chloroisopropyl)ether ND 0.40 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Bis(2-Ethylhexyl)phthalate ND 0.40 0.15 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 4-Bromophenylphenylether ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Butylbenzylphthalate ND 0.40 0.095 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:30 BGL Carbazole ND 0.20 0.052 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:30 BGL 4-Chloroaniline ND 0.77 0.091 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 4-Chloro-3-methylphenol ND 0.77 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2-Chloronaphthalene ND 0.40 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2-Chlorophenol ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 4-Chlorophenylphenylether ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Chrysene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Dibenz(a,h)anthracene ND 0.20 0.12 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Dibenzofuran ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Di-n-butylphthalate ND 0.40 0.087 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 1,2-Dichlorobenzene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 1,3-Dichlorobenzene ND 0.40 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 1,4-Dichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 3,3-Dichlorobenzidine ND 0.20 0.061 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2,4-Dichlorophenol ND 0.40 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Diethylphthalate ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2,4-Dimethylphenol ND 0.40 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Dimethylphthalate ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 4,6-Dinitro-2-methylphenol ND 0.40 0.38 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2,4-Dinitrophenol ND 0.77 0.23 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2,4-Dinitrotoluene ND 0.40 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2,6-Dinitrotoluene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Di-n-octylphthalate ND 0.40 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.40 0.064 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:30 BGL Fluoranthene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Flumene ND 0.20 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Page 18 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 South Sampled: 3/5/2018 10:20 Samnle ID: 18C0324-02 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Hexachlorobutadiene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Hexachlorocyclopentadiene ND 0.40 0.084 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Hexachloroethane ND 0.40 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Indeno(1,2,3-cd)pyrene ND 0.20 0.14 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Isophorone ND 0.40 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 1-Methylnaphthalene ND 0.20 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2-Methylnaphthalene ND 0.20 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2-Methylphenol ND 0.40 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 3/4-Methylphenol ND 0.40 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Naphthalene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2-Nitroaniline ND 0.40 0.067 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 3-Nitroaniline ND 0.40 0.057 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 4-Nitroaniline ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Nitrobenzene ND 0.40 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2-Nitrophenol ND 0.40 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 4-Nitrophenol ND 0.77 0.087 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 13:30 BGL N-Nitrosodimethylamine ND 0.40 0.25 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 13:30 BGL N-Nitrosodiphenylamine ND 0.40 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL N-Nitrosodi-n-propylamine ND 0.40 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Pentachloronitrobenzene ND 0.40 0.095 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Pentachlorophenol ND 0.40 0.096 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Phenanthrene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Phenol ND 0.40 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Pyrene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Pyridine ND 0.40 0.064 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 1,2,4,5-Texachlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 1,2,4-Trichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2,4,5-Trichlorophenol ND 0.40 0.090 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL 2,4,6-Trichlorophenol ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:30 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 54.7 30-130 3/12/18 13:30 Phenol-d6 53.4 30-130 3/12/18 13:30 Nitrobenzene-d5 76.9 30-130 3/12/18 13:30 2-Fluorobiphenyl 67.5 30-130 3/12/18 13:30 2,4,6-Tribromophenol 67.1 30-130 3/12/18 13:30 p-Terphenyl-dl4 71.1 30-130 3/12/18 13:30 Page 19 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 South Sampled: 3/5/2018 10:20 Samnle ID: 18C0324-02 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 85.4 % Wt 1 SM 2540G 3/8/18 3/8/18 19:27 DMP Page 20 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 North Sampled: 3/5/2018 10:25 Sample ID: 18C0324-03 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.098 0.023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Acrylonitrile ND 0.0059 0.0024 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF tert-Amyl Methyl Ether (TAME) ND 0.00098 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Benzene ND 0.0020 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Bromobenzene ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Bromochloromethane ND 0.0020 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Bromodichloromethane ND 0.0020 0.00059 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:57 MFF Bromoform ND 0.0020 0.0014 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:57 MFF Bromomethane ND 0.0098 0.0041 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 2-Butanone (MEK) ND 0.039 0.017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF tert-Butyl Alcohol (TBA) ND 0.039 0.020 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF n-Butylbenzene ND 0.0020 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF sec-Butylbenzene ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF tert-Butylbenzene ND 0.0020 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00098 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Carbon Disulfide ND 0.0059 0.0042 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Carbon Tetrachloride ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Chlombenzene ND 0.0020 0.00068 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:57 MFF Chlorodibromomethane ND 0.0020 0.00068 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:57 MFF Chloroethane ND 0.020 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Chloroform ND 0.0039 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Chloromethane ND 0.0098 0.0063 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 2-Chlorotoluene ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 4-Chlorotoluene ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0020 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,2-Dibromoethane (EDB) ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Dibromomethane ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,2-Dichlorobenzene ND 0.0020 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,3-Dichlorobenzene ND 0.0020 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,4-Dichlorobenzene ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF trans-1,4-Dichloro-2-butene ND 0.0039 0.0021 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 8:57 MFF Dichlorodifluoromethane (Freon 12) ND 0.020 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,1-Dichloroethane ND 0.0020 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,2-Dichloroethane ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1, 1 -Dichloroethylene ND 0.0039 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF cis-1,2-Dichloroethylene ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF trans-1,2-Dichloroethylene ND 0.0020 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,2-Dichloropropane ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,3-Dichloropropane ND 0.00098 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 2,2-Dichloropropane ND 0.0020 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1, 1 -Dichloropropene ND 0.0020 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF cis-1,3-Dichloropropene ND 0.00098 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF trans-1,3-Dichloropropene ND 0.00098 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Diethyl Ether ND 0.020 0.0018 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Page 21 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 North Sampled: 3/5/2018 10:25 Sample ID: 18C0324-03 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.00098 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,4-Dioxane ND 0.098 0.056 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Ethanol ND 0.20 0.039 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Ethylbenzene ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Hexachlorobutadiene ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 2-Hexanone (MBK) ND 0.020 0.011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Isopropylbenzene (Cumene) ND 0.0020 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF p-Isopropyltoluene (p-Cymene) ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0039 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Methylene Chloride ND 0.020 0.0069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 4-Methyl-2-pentanone (MIBK) ND 0.020 0.0074 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Naphthalene ND 0.0039 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF n-Propylbenzene ND 0.0020 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Styrene ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0020 0.0018 mg/Kg dry 1 SW-8468260B 3/8/18 3/8/18 8:57 MFF 1,1,2,2-Tetrachloroethane ND 0.00098 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Tetrachloroethylene ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Tetrahydrofuran ND 0.0098 0.0022 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Toluene ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,2,3-Trichlorobenzene ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,2,4-Trichlorobenzene ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,3,5-Trichlorobenzene ND 0.0020 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1, 1, 1 -Trichloroethane ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,1,2-Trichloroethane ND 0.0020 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Trichloroethylene ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Trichlorofluoromethane (Freon 11) ND 0.0098 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,2,3-Trichloropropane ND 0.0020 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0098 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0020 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF 1,3,5-Trimethylbenzene ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Vinyl Chloride ND 0.0098 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF m+p Xylene ND 0.0039 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF o-Xylene ND 0.0020 0.00068 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 8:57 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.1 70-130 3/8/18 8:57 Toluene-d8 100 70-130 3/8/18 8:57 4-Bromofluorobenzene 102 70-130 3/8/18 8:57 Page 22 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 North Sampled: 3/5/2018 10:25 Samnle ID: 18C0324-03 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.20 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Acenaphthylene ND 0.20 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Acetophenone ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Aniline ND 0.40 0.11 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Anthracene ND 0.20 0.057 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Benzidine ND 0.77 0.50 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Benzo(a)anthracene ND 0.20 0.053 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Benzo(a)pyrene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Benzo(b)fluoranthene ND 0.20 0.056 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Benzo(g,h,i)perylene ND 0.20 0.088 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Benzo(k)fluoranthene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Benzoic Acid 0.27 1.2 0.21 mg/Kg dry 1 J SW-846 8270D 3/9/18 3/12/18 13:53 BGL Bis(2-chloroethoxy)methane ND 0.40 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Bis(2-chloroethyl)ether ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Bis(2-chloroisopropyl)ether ND 0.40 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Bis(2-Ethylhexyl)phthalate ND 0.40 0.15 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 4-Bromophenylphenylether ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Butylbenzylphthalate ND 0.40 0.095 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:53 BGL Carbazole ND 0.20 0.052 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:53 BGL 4-Chloroaniline ND 0.77 0.091 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 4-Chloro-3-methylphenol ND 0.77 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2-Chloronaphthalene ND 0.40 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2-Chlorophenol ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 4-Chlorophenylphenylether ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Chrysene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Dibenz(a,h)anthracene ND 0.20 0.12 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Dibenzofuran ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Di-n-butylphthalate ND 0.40 0.087 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 1,2-Dichlorobenzene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 1,3-Dichlorobenzene ND 0.40 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 1,4-Dichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 3,3-Dichlorobenzidine ND 0.20 0.061 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2,4-Dichlorophenol ND 0.40 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Diethylphthalate ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2,4-Dimethylphenol ND 0.40 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Dimethylphthalate ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 4,6-Dinitro-2-methylphenol ND 0.40 0.38 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2,4-Dinitrophenol ND 0.77 0.23 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2,4-Dinitrotoluene ND 0.40 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2,6-Dinitrotoluene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Di-n-octylphthalate ND 0.40 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.40 0.064 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 13:53 BGL Fluoranthene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Flumene ND 0.20 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Page 23 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 North Sampled: 3/5/2018 10:25 Samnle ID: 18C0324-03 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Hexachlorobutadiene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Hexachlorocyclopentadiene ND 0.40 0.084 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Hexachloroethane ND 0.40 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Indeno(1,2,3-cd)pyrene ND 0.20 0.14 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Isophorone ND 0.40 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 1-Methylnaphthalene ND 0.20 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2-Methylnaphthalene ND 0.20 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2-Methylphenol ND 0.40 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 3/4-Methylphenol ND 0.40 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Naphthalene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2-Nitroaniline ND 0.40 0.067 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 3-Nitroaniline ND 0.40 0.057 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 4-Nitroaniline ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Nitrobenzene ND 0.40 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2-Nitrophenol ND 0.40 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 4-Nitrophenol ND 0.77 0.087 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 13:53 BGL N-Nitrosodimethylamine ND 0.40 0.25 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 13:53 BGL N-Nitrosodiphenylamine ND 0.40 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL N-Nitrosodi-n-propylamine ND 0.40 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Pentachloronitrobenzene ND 0.40 0.095 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Pentachlorophenol ND 0.40 0.096 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Phenanthrene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Phenol ND 0.40 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Pyrene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Pyridine ND 0.40 0.064 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 1,2,4,5-Texachlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 1,2,4-Trichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2,4,5-Trichlorophenol ND 0.40 0.090 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL 2,4,6-Trichlorophenol ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 13:53 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 59.3 30-130 3/12/18 13:53 Phenol-d6 59.8 30-130 3/12/18 13:53 Nitrobenzene-d5 82.1 30-130 3/12/18 13:53 2-Fluorobiphenyl 76.6 30-130 3/12/18 13:53 2,4,6-Tribromophenol 80.9 30-130 3/12/18 13:53 p-Terphenyl-dl4 84.4 30-130 3/12/18 13:53 Page 24 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 North Sampled: 3/5/2018 10:25 Samnle ID: 18C0324-03 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 85.4 % Wt 1 SM 2540G 3/8/18 3/8/18 19:27 DMP Page 25 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 West Sampled: 3/5/2018 10:30 Sample ID: 18C0324-04 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.11 0.026 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Acrylonitrile ND 0.0065 0.0027 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF tert-Amyl Methyl Ether (TAME) ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Benzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Bromobenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Bromochloromethane ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Bromodichloromethane ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Bromoform ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Bromomethane ND 0.011 0.0046 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 2-Butanone (MEK) ND 0.044 0.019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF tert-Butyl Alcohol (TBA) ND 0.044 0.023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF n-Butylbenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF sec-Butylbenzene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF tert-Butylbenzene ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0011 0.00065 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Carbon Disulfide ND 0.0065 0.0047 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Carbon Tetrachloride ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Chlombenzene ND 0.0022 0.00076 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 9:25 MFF Chlorodibromomethane ND 0.0022 0.00076 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 9:25 MFF Chloroethane ND 0.022 0.0016 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Chloroform ND 0.0044 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Chloromethane ND 0.011 0.0070 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 2-Chlorotoluene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 4-Chlorotoluene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,2-Dibromoethane (EDB) ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Dibromomethane ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,2-Dichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,3-Dichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,4-Dichlorobenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF trans-1,4-Dichloro-2-butene ND 0.0044 0.0023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Dichlorodifluoromethane (Freon 12) ND 0.022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,1-Dichloroethane ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,2-Dichloroethane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1, 1 -Dichloroethylene ND 0.0044 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF cis-1,2-Dichloroethylene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF trans-1,2-Dichloroethylene ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,2-Dichloropropane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,3-Dichloropropane ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 2,2-Dichloropropane ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1, 1 -Dichloropropene ND 0.0022 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF cis-1,3-Dichloropropene ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF trans-1,3-Dichloropropene ND 0.0011 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Diethyl Ether ND 0.022 0.0020 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Page 26 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 West Sampled: 3/5/2018 10:30 Sample ID: 18C0324-04 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0011 0.00065 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,4-Dioxane ND 0.11 0.063 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Ethanol ND 0.22 0.044 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Ethylbenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Hexachlorobutadiene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 2-Hexanone (MBK) ND 0.022 0.012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Isopropylbenzene (Cumene) ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF p-Isopropyltoluene (p-Cymene) ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0044 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Methylene Chloride ND 0.022 0.0077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 4-Methyl-2-pentanone (MIBK) ND 0.022 0.0083 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Naphthalene ND 0.0044 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF n-Propylbenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Styrene ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0022 0.0020 mg/Kg dry 1 SW-8468260B 3/8/18 3/8/18 9:25 MFF 1,1,2,2-Tetrachloroethane ND 0.0011 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Tetrachloroethylene ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Tetrahydrofuran ND 0.011 0.0024 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Toluene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,2,3-Trichlorobenzene ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,2,4-Trichlorobenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,3,5-Trichlorobenzene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1, 1, 1 -Trichloroethane ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,1,2-Trichloroethane ND 0.0022 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Trichloroethylene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Trichlorofluoromethane (Freon 11) ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,2,3-Trichloropropane ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.011 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0022 0.00087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF 1,3,5-Trimethylbenzene ND 0.0022 0.00065 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Vinyl Chloride ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF m+p Xylene ND 0.0044 0.0019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF o-Xylene ND 0.0022 0.00076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:25 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 98.2 70-130 3/8/18 9:25 Toluene-d8 101 70-130 3/8/18 9:25 4-Bromofluorobenzene 102 70-130 3/8/18 9:25 Page 27 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 West Sampled: 3/5/2018 10:30 Samnle ID: 18C0324-04 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.19 0.057 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Acenaphthylene ND 0.19 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Acetophenone ND 0.38 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Aniline ND 0.38 0.11 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Anthracene ND 0.19 0.055 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Benzidine ND 0.74 0.47 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Benzo(a)anthracene ND 0.19 0.050 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Benzo(a)pyrene ND 0.19 0.059 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Benzo(b)fluoranthene ND 0.19 0.054 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Benzo(g,h,i)perylene ND 0.19 0.084 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Benzo(k)fluoranthene ND 0.19 0.059 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Benzoic Acid ND 1.1 0.20 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Bis(2-chloroethoxy)methane ND 0.38 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Bis(2-chloroethyl)ether ND 0.38 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Bis(2-chloroisopropyl)ether ND 0.38 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Bis(2-Ethylhexyl)phthalate ND 0.38 0.15 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 4-Bromophenylphenylether ND 0.38 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Butylbenzylphthalate ND 0.38 0.091 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 14:16 BGL Carbazole ND 0.19 0.049 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 14:16 BGL 4-Chloroaniline ND 0.74 0.087 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 4-Chloro-3-methylphenol ND 0.74 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2-Chloronaphthalene ND 0.38 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2-Chlorophenol ND 0.38 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 4-Chlorophenylphenylether ND 0.38 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Chrysene ND 0.19 0.059 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Dibenz(a,h)anthracene ND 0.19 0.12 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Dibenzofuran ND 0.38 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Di-n-butylphthalate ND 0.38 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 1,2-Dichlorobenzene ND 0.38 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 1,3-Dichlorobenzene ND 0.38 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 1,4-Dichlorobenzene ND 0.38 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 3,3-Dichlorobenzidine ND 0.19 0.058 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2,4-Dichlorophenol ND 0.38 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Diethylphthalate ND 0.38 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2,4-Dimethylphenol ND 0.38 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Dimethylphthalate ND 0.38 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 4,6-Dinitro-2-methylphenol ND 0.38 0.36 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2,4-Dinitrophenol ND 0.74 0.22 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2,4-Dinitrotoluene ND 0.38 0.061 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2,6-Dinitrotoluene ND 0.38 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Di-n-octylphthalate ND 0.38 0.20 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.38 0.061 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 14:16 BGL Fluoranthene ND 0.19 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Flumene ND 0.19 0.061 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Page 28 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 West Sampled: 3/5/2018 10:30 Samnle ID: 18C0324-04 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.38 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Hexachlorobutadiene ND 0.38 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Hexachlorocyclopentadiene ND 0.38 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Hexachloroethane ND 0.38 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Indeno(1,2,3-cd)pyrene ND 0.19 0.14 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Isophorone ND 0.38 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 1-Methylnaphthalene ND 0.19 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2-Methylnaphthalene ND 0.19 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2-Methylphenol ND 0.38 0.095 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 3/4-Methylphenol ND 0.38 0.12 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Naphthalene ND 0.19 0.097 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2-Nitroaniline ND 0.38 0.064 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 3-Nitroaniline ND 0.38 0.055 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 4-Nitroaniline ND 0.38 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Nitrobenzene ND 0.38 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2-Nitrophenol ND 0.38 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 4-Nitrophenol ND 0.74 0.083 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 14:16 BGL N-Nitrosodimethylamine ND 0.38 0.24 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 14:16 BGL N-Nitrosodiphenylamine ND 0.38 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL N-Nitrosodi-n-propylamine ND 0.38 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Pentachloronitrobenzene ND 0.38 0.091 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Pentachlorophenol ND 0.38 0.092 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Phenanthrene ND 0.19 0.098 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Phenol ND 0.38 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Pyrene ND 0.19 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Pyridine ND 0.38 0.061 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 1,2,4,5-Texachlorobenzene ND 0.38 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 1,2,4-Trichlorobenzene ND 0.38 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2,4,5-Trichlorophenol ND 0.38 0.086 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL 2,4,6-Trichlorophenol ND 0.38 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:16 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 59.6 30-130 3/12/18 14:16 Phenol-d6 60.8 30-130 3/12/18 14:16 Nitrobenzene-d5 86.9 30-130 3/12/18 14:16 2-Fluorobiphenyl 81.4 30-130 3/12/18 14:16 2,4,6-Tribromophenol 84.6 30-130 3/12/18 14:16 p-Terphenyl-dl4 88.8 30-130 3/12/18 14:16 Page 29 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 West Sampled: 3/5/2018 10:30 Samnle ID: 18C0324-04 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 88.6 % Wt 1 SM 2540G 3/8/18 3/8/18 19:27 DMP Page 30 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 East Sampled: 3/5/2018 10:35 Sample ID: 18C0324-05 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.10 0.024 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Acrylonitrile ND 0.0062 0.0026 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF tert-Amyl Methyl Ether (TAME) ND 0.0010 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Benzene ND 0.0021 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Bromobenzene ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Bromochloromethane ND 0.0021 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Bromodichloromethane ND 0.0021 0.00062 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Bromoform ND 0.0021 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Bromomethane ND 0.010 0.0043 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 2-Butanone (MEK) ND 0.041 0.018 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF tert-Butyl Alcohol (TBA) ND 0.041 0.021 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF n-Butylbenzene ND 0.0021 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF sec-Butylbenzene ND 0.0021 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF tert-Butylbenzene ND 0.0021 0.00092 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0010 0.00062 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Carbon Disulfide ND 0.0062 0.0044 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Carbon Tetrachloride ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Chlombenzene ND 0.0021 0.00072 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 9:52 MFF Chlorodibromomethane ND 0.0021 0.00072 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 9:52 MFF Chloroethane ND 0.021 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Chloroform ND 0.0041 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Chloromethane ND 0.010 0.0066 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 2-Chlorotoluene ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 4-Chlorotoluene ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,2-Dibromoethane (EDB) ND 0.0021 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Dibromomethane ND 0.0021 0.00062 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,2-Dichlorobenzene ND 0.0021 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,3-Dichlorobenzene ND 0.0021 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,4-Dichlorobenzene ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF trans-1,4-Dichloro-2-butene ND 0.0041 0.0022 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Dichlorodifluoromethane (Freon 12) ND 0.021 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,1-Dichloroethane ND 0.0021 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,2-Dichloroethane ND 0.0021 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1, 1 -Dichloroethylene ND 0.0041 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF cis-1,2-Dichloroethylene ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF trans-1,2-Dichloroethylene ND 0.0021 0.00092 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,2-Dichloropropane ND 0.0021 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,3-Dichloropropane ND 0.0010 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 2,2-Dichloropropane ND 0.0021 0.00092 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1, 1 -Dichloropropene ND 0.0021 0.00092 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF cis-1,3-Dichloropropene ND 0.0010 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF trans-1,3-Dichloropropene ND 0.0010 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Diethyl Ether ND 0.021 0.0018 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Page 31 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 East Sampled: 3/5/2018 10:35 Sample ID: 18C0324-05 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0010 0.00062 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,4-Dioxane ND 0.10 0.059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Ethanol ND 0.21 0.041 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Ethylbenzene ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Hexachlorobutadiene ND 0.0021 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 2-Hexanone (MBK) ND 0.021 0.011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Isopropylbenzene (Cumene) ND 0.0021 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF p-Isopropyltoluene (p-Cymene) ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0041 0.00092 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Methylene Chloride ND 0.021 0.0073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 4-Methyl-2-pentanone (MIBK) ND 0.021 0.0078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Naphthalene ND 0.0041 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF n-Propylbenzene ND 0.0021 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Styrene ND 0.0021 0.00062 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0021 0.0018 mg/Kg dry 1 SW-8468260B 3/8/18 3/8/18 9:52 MFF 1,1,2,2-Tetrachloroethane ND 0.0010 0.00092 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Tetrachloroethylene ND 0.0021 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Tetrahydrofuran ND 0.010 0.0023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Toluene ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,2,3-Trichlorobenzene ND 0.0021 0.00062 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,2,4-Trichlorobenzene ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,3,5-Trichlorobenzene ND 0.0021 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1, 1, 1 -Trichloroethane ND 0.0021 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,1,2-Trichloroethane ND 0.0021 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Trichloroethylene ND 0.0021 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Trichlorofluoromethane (Freon 11) ND 0.010 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,2,3-Trichloropropane ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.010 0.00092 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0021 0.00082 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF 1,3,5-Trimethylbenzene ND 0.0021 0.00062 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Vinyl Chloride ND 0.010 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF m+p Xylene ND 0.0041 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF o-Xylene ND 0.0021 0.00072 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 9:52 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.2 70-130 3/8/18 9:52 Toluene-d8 99.4 70-130 3/8/18 9:52 4-Bromofluorobenzene 101 70-130 3/8/18 9:52 Page 32 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 East Sampled: 3/5/2018 10:35 Samnle ID: 18C0324-05 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.20 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Acenaphthylene ND 0.20 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Acetophenone ND 0.40 0.079 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Aniline ND 0.40 0.11 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Anthracene ND 0.20 0.058 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Benzidine ND 0.78 0.50 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Benzo(a)anthracene ND 0.20 0.053 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 14:38 BGL Benzo(a)pyrene ND 0.20 0.063 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 14:38 BGL Benzo(b)fluoranthene ND 0.20 0.057 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Benzo(g,h,i)perylene ND 0.20 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Benzo(k)fluoranthene ND 0.20 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Benzoic Acid ND 1.2 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Bis(2-chloroethoxy)methane ND 0.40 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Bis(2-chloroethyl)ether ND 0.40 0.079 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Bis(2-chloroisopropyl)ether ND 0.40 0.086 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Bis(2-Ethylhexyl)phthalate ND 0.40 0.16 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 4-Bromophenylphenylether ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Butylbenzylphthalate ND 0.40 0.096 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 14:38 BGL Carbazole ND 0.20 0.052 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 14:38 BGL 4-Chloroaniline ND 0.78 0.092 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 4-Chloro-3-methylphenol ND 0.78 0.086 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2-Chloronaphthalene ND 0.40 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2-Chlorophenol ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 4-Chlorophenylphenylether ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Chrysene ND 0.20 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Dibenz(a,h)anthracene ND 0.20 0.12 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Dibenzofuran ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Di-n-butylphthalate ND 0.40 0.088 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 1,2-Dichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 1,3-Dichlorobenzene ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 1,4-Dichlorobenzene ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 3,3-Dichlorobenzidine ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2,4-Dichlorophenol ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Diethylphthalate ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2,4-Dimethylphenol ND 0.40 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Dimethylphthalate ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 4,6-Dinitro-2-methylphenol ND 0.40 0.38 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2,4-Dinitrophenol ND 0.78 0.23 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2,4-Dinitrotoluene ND 0.40 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2,6-Dinitrotoluene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Di-n-octylphthalate ND 0.40 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.40 0.065 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 14:38 BGL Fluoranthene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Flumene ND 0.20 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Page 33 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 East Sampled: 3/5/2018 10:35 Samnle ID: 18C0324-05 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Hexachlorobutadiene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Hexachlorocyclopentadiene ND 0.40 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Hexachloroethane ND 0.40 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Indeno(1,2,3-cd)pyrene ND 0.20 0.14 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Isophorone ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 1-Methylnaphthalene ND 0.20 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2-Methylnaphthalene ND 0.20 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2-Methylphenol ND 0.40 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 3/4-Methylphenol ND 0.40 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Naphthalene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2-Nitroaniline ND 0.40 0.067 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 3-Nitroaniline ND 0.40 0.058 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 4-Nitroaniline ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Nitrobenzene ND 0.40 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2-Nitrophenol ND 0.40 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 4-Nitrophenol ND 0.78 0.088 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 14:38 BGL N-Nitrosodimethylamine ND 0.40 0.25 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 14:38 BGL N-Nitrosodiphenylamine ND 0.40 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL N-Nitrosodi-n-propylamine ND 0.40 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Pentachloronitrobenzene ND 0.40 0.096 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Pentachlorophenol ND 0.40 0.097 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Phenanthrene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Phenol ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Pyrene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Pyridine ND 0.40 0.065 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 1,2,4,5-Texachlorobenzene ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 1,2,4-Trichlorobenzene ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2,4,5-Trichlorophenol ND 0.40 0.091 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL 2,4,6-Trichlorophenol ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 14:38 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 60.9 30-130 3/12/18 14:38 Phenol-d6 60.6 30-130 3/12/18 14:38 Nitrobenzene-d5 86.5 30-130 3/12/18 14:38 2-Fluorobiphenyl 78.4 30-130 3/12/18 14:38 2,4,6-Tribromophenol 79.6 30-130 3/12/18 14:38 p-Terphenyl-dl4 82.4 30-130 3/12/18 14:38 Page 34 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-1 East Sampled: 3/5/2018 10:35 Samnle ID: 18C0324-05 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 84.5 % Wt 1 SM 2540G 3/8/18 3/8/18 19:27 DMP Page 35 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00 Sample ID: 18C0324-06 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.12 0.029 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Acrylonitrile ND 0.0073 0.0031 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF tert-Amyl Methyl Ether (TAME) ND 0.0012 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Benzene ND 0.0024 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Bromobenzene ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Bromochloromethane ND 0.0024 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Bromodichloromethane ND 0.0024 0.00073 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 10:21 MFF Bromoform ND 0.0024 0.0017 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 10:21 MFF Bromomethane ND 0.012 0.0051 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 2-Butanone (MEK) ND 0.049 0.021 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF tert-Butyl Alcohol (TBA) ND 0.049 0.026 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF n-Butylbenzene ND 0.0024 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF sec-Butylbenzene ND 0.0024 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF tert-Butylbenzene ND 0.0024 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0012 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Carbon Disulfide ND 0.0073 0.0053 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Carbon Tetrachloride ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Chlombenzene ND 0.0024 0.00085 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 10:21 MFF Chlorodibromomethane ND 0.0024 0.00085 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 10:21 MFF Chloroethane ND 0.024 0.0018 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Chloroform ND 0.0049 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Chloromethane ND 0.012 0.0078 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 2-Chlorotoluene ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 4-Chlorotoluene ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0024 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,2-Dibromoethane (EDB) ND 0.0024 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Dibromomethane ND 0.0024 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,2-Dichlorobenzene ND 0.0024 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,3-Dichlorobenzene ND 0.0024 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,4-Dichlorobenzene ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF trans-1,4-Dichloro-2-butene ND 0.0049 0.0026 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Dichlorodifluoromethane (Freon 12) ND 0.024 0.0016 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,1-Dichloroethane ND 0.0024 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,2-Dichloroethane ND 0.0024 0.0016 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1, 1 -Dichloroethylene ND 0.0049 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF cis-1,2-Dichloroethylene ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF trans-1,2-Dichloroethylene ND 0.0024 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,2-Dichloropropane ND 0.0024 0.0016 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,3-Dichloropropane ND 0.0012 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 2,2-Dichloropropane ND 0.0024 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1, 1 -Dichloropropene ND 0.0024 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF cis-1,3-Dichloropropene ND 0.0012 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF trans-1,3-Dichloropropene ND 0.0012 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Diethyl Ether ND 0.024 0.0022 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Page 36 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00 Sample ID: 18C0324-06 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0012 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,4-Dioxane ND 0.12 0.070 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Ethanol ND 0.24 0.049 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Ethylbenzene ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Hexachlorobutadiene ND 0.0024 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 2-Hexanone (MBK) ND 0.024 0.013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Isopropylbenzene (Cumene) ND 0.0024 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF p-Isopropyltoluene (p-Cymene) ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0049 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Methylene Chloride ND 0.024 0.0087 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 4-Methyl-2-pentanone (MIBK) ND 0.024 0.0093 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Naphthalene ND 0.0049 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF n-Propylbenzene ND 0.0024 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Styrene ND 0.0024 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0024 0.0022 mg/Kgdry 1 SW-8468260B 3/8/18 3/8/18 10:21 MFF 1,1,2,2-Tetrachloroethane ND 0.0012 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Tetrachloroethylene ND 0.0024 0.0016 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Tetrahydrofuran ND 0.012 0.0027 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Toluene ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,2,3-Trichlorobenzene ND 0.0024 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,2,4-Trichlorobenzene ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,3,5-Trichlorobenzene ND 0.0024 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1, 1, 1 -Trichloroethane ND 0.0024 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,1,2-Trichloroethane ND 0.0024 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Trichloroethylene ND 0.0024 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Trichlorofluoromethane (Freon 11) ND 0.012 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,2,3-Trichloropropane ND 0.0024 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.012 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0024 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF 1,3,5-Trimethylbenzene ND 0.0024 0.00073 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Vinyl Chloride ND 0.012 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF m+p Xylene ND 0.0049 0.0021 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF o-Xylene ND 0.0024 0.00085 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:21 MFF Surrogates % Recovery Recovery Limits Flag/Qaal 1,2-Dichloroethane-d4 100 70-130 3/8/18 10:21 Toluene-d8 97.8 70-130 3/8/18 10:21 4-Bromofluorobenzene 102 70-130 3/8/18 10:21 Page 37 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00 Samnle ID: 18C0324-06 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.22 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Acenaphthylene ND 0.22 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Acetophenone ND 0.43 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Aniline ND 0.43 0.12 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Anthracene ND 0.22 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Benzidine ND 0.84 0.54 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Benzo(a)anthracene ND 0.22 0.057 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:01 BGL Benzo(a)pyrene ND 0.22 0.068 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:01 BGL Benzo(b)fluoranthene ND 0.22 0.061 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Benzo(g,h,i)perylene ND 0.22 0.096 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Benzo(k)fluoranthene ND 0.22 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Benzoic Acid ND 1.3 0.23 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Bis(2-chloroethoxy)methane ND 0.43 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Bis(2-chloroethyl)ether ND 0.43 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Bis(2-chloroisopropyl)ether ND 0.43 0.093 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Bis(2-Ethylhexyl)phthalate ND 0.43 0.17 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 4-Bromophenylphenylether ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Butylbenzylphthalate ND 0.43 0.10 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:01 BGL Carbazole ND 0.22 0.056 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:01 BGL 4-Chloroaniline ND 0.84 0.099 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 4-Chloro-3-methylphenol ND 0.84 0.093 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2-Chloronaphthalene ND 0.43 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2-Chlorophenol ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 4-Chlorophenylphenylether ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Chrysene ND 0.22 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Dibenz(a,h)anthracene ND 0.22 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Dibenzofuran ND 0.43 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Di-n-butylphthalate ND 0.43 0.094 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 1,2-Dichlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 1,3-Dichlorobenzene ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 1,4-Dichlorobenzene ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 3,3-Dichlorobenzidine ND 0.22 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2,4-Dichlorophenol ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Diethylphthalate ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2,4-Dimethylphenol ND 0.43 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Dimethylphthalate ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 4,6-Dinitro-2-methylphenol ND 0.43 0.41 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2,4-Dinitrophenol ND 0.84 0.25 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2,4-Dinitrotoluene ND 0.43 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2,6-Dinitrotoluene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Di-n-octylphthalate ND 0.43 0.23 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.43 0.070 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:01 BGL Fluoranthene ND 0.22 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Flumene ND 0.22 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Page 38 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00 Samnle ID: 18C0324-06 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Hexachlorobutadiene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Hexachlorocyclopentadiene ND 0.43 0.092 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Hexachloroethane ND 0.43 0.087 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Indeno(1,2,3-cd)pyrene ND 0.22 0.16 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Isophorone ND 0.43 0.084 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 1-Methylnaphthalene ND 0.22 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2-Methylnaphthalene ND 0.22 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2-Methylphenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 3/4-Methylphenol ND 0.43 0.14 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Naphthalene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2-Nitroaniline ND 0.43 0.073 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 3-Nitroaniline ND 0.43 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 4-Nitroaniline ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Nitrobenzene ND 0.43 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2-Nitrophenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 4-Nitrophenol ND 0.84 0.094 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 15:01 BGL N-Nitrosodimethylamine ND 0.43 0.27 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 15:01 BGL N-Nitrosodiphenylamine ND 0.43 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL N-Nitrosodi-n-propylamine ND 0.43 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Pentachloronitrobenzene ND 0.43 0.10 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Pentachlorophenol ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Phenanthrene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Phenol ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Pyrene ND 0.22 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Pyridine ND 0.43 0.070 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 1,2,4,5-Texachlorobenzene ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 1,2,4-Trichlorobenzene ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2,4,5-Trichlorophenol ND 0.43 0.098 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL 2,4,6-Trichlorophenol ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:01 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 63.6 30-130 3/12/18 15:01 Phenol-d6 63.6 30-130 3/12/18 15:01 Nitrobenzene-d5 94.9 30-130 3/12/18 15:01 2-Fluorobiphenyl 78.5 30-130 3/12/18 15:01 2,4,6-Tribromophenol 82.8 30-130 3/12/18 15:01 p-Terphenyl-dl4 84.8 30-130 3/12/18 15:01 Page 39 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00 Samnle ID: 18C0324-06 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 78.4 % Wt 1 SM 2540G 3/8/18 3/8/18 19:27 DMP Page 40 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15 Sample ID: 18C0324-07 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.11 0.026 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Acrylonitrile ND 0.0066 0.0028 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF tert-Amyl Methyl Ether (TAME) ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Benzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Bromobenzene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Bromochloromethane ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Bromodichloromethane ND 0.0022 0.00066 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 10:48 MFF Bromoform ND 0.0022 0.0015 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 10:48 MFF Bromomethane ND 0.011 0.0046 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 2-Butanone (MEK) ND 0.044 0.019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF tert-Butyl Alcohol (TBA) ND 0.044 0.023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF n-Butylbenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF sec-Butylbenzene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF tert-Butylbenzene ND 0.0022 0.00099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0011 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Carbon Disulfide ND 0.0066 0.0047 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Carbon Tetrachloride ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Chlombenzene ND 0.0022 0.00077 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 10:48 MFF Chlorodibromomethane ND 0.0022 0.00077 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 10:48 MFF Chloroethane ND 0.022 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Chloroform ND 0.0044 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Chloromethane ND 0.011 0.0071 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 2-Chlorotoluene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 4-Chlorotoluene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,2-Dibromoethane (EDB) ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Dibromomethane ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,2-Dichlorobenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,3-Dichlorobenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,4-Dichlorobenzene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF trans-1,4-Dichloro-2-butene ND 0.0044 0.0023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Dichlorodifluoromethane (Freon 12) ND 0.022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,1-Dichloroethane ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,2-Dichloroethane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1, 1 -Dichloroethylene ND 0.0044 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF cis-1,2-Dichloroethylene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF trans-1,2-Dichloroethylene ND 0.0022 0.00099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,2-Dichloropropane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,3-Dichloropropane ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 2,2-Dichloropropane ND 0.0022 0.00099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1, 1 -Dichloropropene ND 0.0022 0.00099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF cis-1,3-Dichloropropene ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF trans-1,3-Dichloropropene ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Diethyl Ether ND 0.022 0.0020 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Page 41 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15 Sample ID: 18C0324-07 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0011 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,4-Dioxane ND 0.11 0.063 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Ethanol ND 0.22 0.044 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Ethylbenzene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Hexachlorobutadiene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 2-Hexanone (MBK) ND 0.022 0.012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Isopropylbenzene (Cumene) ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF p-Isopropyltoluene (p-Cymene) ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0044 0.00099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Methylene Chloride ND 0.022 0.0078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 4-Methyl-2-pentanone (MIBK) ND 0.022 0.0084 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Naphthalene ND 0.0044 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF n-Propylbenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Styrene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0022 0.0020 mg/Kg dry 1 SW-8468260B 3/8/18 3/8/18 10:48 MFF 1,1,2,2-Tetrachloroethane ND 0.0011 0.00099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Tetrachloroethylene ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Tetrahydrofuran ND 0.011 0.0024 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Toluene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,2,3-Trichlorobenzene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,2,4-Trichlorobenzene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,3,5-Trichlorobenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1, 1, 1 -Trichloroethane ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,1,2-Trichloroethane ND 0.0022 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Trichloroethylene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Trichlorofluoromethane (Freon 11) ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,2,3-Trichloropropane ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.011 0.00099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF 1,3,5-Trimethylbenzene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Vinyl Chloride ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF m+p Xylene ND 0.0044 0.0019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF o-Xylene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 10:48 MFF Surrogates % Recovery Recovery Limits Flag/Qaal 1,2-Dichloroethane-d4 100 70-130 3/8/18 10:48 Toluene-d8 99.0 70-130 3/8/18 10:48 4-Bromofluorobenzene 99.8 70-130 3/8/18 10:48 Page 42 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15 Samnle ID: 18C0324-07 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.21 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Acenaphthylene ND 0.21 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Acetophenone ND 0.41 0.081 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Aniline ND 0.41 0.12 mg/Kg dry 1 MS-09, V-05 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Anthracene ND 0.21 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Benzidine ND 0.80 0.52 mg/Kg dry 1 MS-09, V-04, V-05 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Benzo(a)anthracene ND 0.21 0.055 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Benzo(a)pyrene ND 0.21 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Benzo(b)fluoranthene ND 0.21 0.058 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Benzo(g,h,i)perylene ND 0.21 0.091 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Benzo(k)fluoranthene ND 0.21 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Benzoic Acid 0.45 1.2 0.22 mg/Kg dry 1 J SW-846 8270D 3/9/18 3/12/18 15:24 BGL Bis(2-chloroethoxy)methane ND 0.41 0.079 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Bis(2-chloroethyl)ether ND 0.41 0.081 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Bis(2-chloroisopropyl)ether ND 0.41 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Bis(2-Ethylhexyl)phthalate ND 0.41 0.16 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 4-Bromophenylphenylether ND 0.41 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Butylbenzylphthalate ND 0.41 0.098 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:24 BGL Carbazole ND 0.21 0.053 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 4-Chloroaniline ND 0.80 0.095 mg/Kg dry 1 MS-09, R-06 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 4-Chloro-3-methylphenol ND 0.80 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2-Chloronaphthalene ND 0.41 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2-Chlorophenol ND 0.41 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 4-Chlorophenylphenylether ND 0.41 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Chrysene ND 0.21 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Dibenz(a,h)anthracene ND 0.21 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Dibenzofuran ND 0.41 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Di-n-butylphthalate ND 0.41 0.090 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 1,2-Dichlorobenzene ND 0.41 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 1,3-Dichlorobenzene ND 0.41 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 1,4-Dichlorobenzene ND 0.41 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 3,3-Dichlorobenzidine ND 0.21 0.063 mg/Kg dry 1 MS-09 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2,4-Dichlorophenol ND 0.41 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Diethylphthalate ND 0.41 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2,4-Dimethylphenol ND 0.41 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Dimethylphthalate ND 0.41 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 4,6-Dinitro-2-methylphenol ND 0.41 0.39 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2,4-Dinitrophenol ND 0.80 0.24 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2,4-Dinitrotoluene ND 0.41 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2,6-Dinitrotoluene ND 0.41 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Di-n-octylphthalate ND 0.41 0.22 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.41 0.067 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:24 BGL Fluoranthene ND 0.21 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Flumene ND 0.21 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Page 43 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15 Samnle ID: 18C0324-07 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.41 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Hexachlorobutadiene ND 0.41 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Hexachlorocyclopentadiene ND 0.41 0.087 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Hexachloroethane ND 0.41 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Indeno(1,2,3-cd)pyrene ND 0.21 0.15 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Isophorone ND 0.41 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 1-Methylnaphthalene ND 0.21 0.079 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2-Methylnaphthalene ND 0.21 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2-Methylphenol ND 0.41 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 3/4-Methylphenol ND 0.41 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Naphthalene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2-Nitroaniline ND 0.41 0.069 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 3-Nitroaniline ND 0.41 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 4-Nitroaniline ND 0.41 0.069 mg/Kg dry 1 MS-09 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Nitrobenzene ND 0.41 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2-Nitrophenol ND 0.41 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 4-Nitrophenol ND 0.80 0.090 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 15:24 BGL N-Nitrosodimethylamine ND 0.41 0.26 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 15:24 BGL N-Nitrosodiphenylamine ND 0.41 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL N-Nitrosodi-n-propylamine ND 0.41 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Pentachloronitrobenzene ND 0.41 0.098 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Pentachlorophenol ND 0.41 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Phenanthrene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Phenol ND 0.41 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Pyrene ND 0.21 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Pyridine ND 0.41 0.067 mg/Kg dry 1 MS-09, V-05 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 1,2,4,5-Texachlorobenzene ND 0.41 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 1,2,4-Trichlorobenzene ND 0.41 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2,4,5-Trichlorophenol ND 0.41 0.094 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL 2,4,6-Trichlorophenol ND 0.41 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:24 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 53.8 30-130 3/12/18 15:24 Phenol-d6 53.4 30-130 3/12/18 15:24 Nitrobenzene-d5 79.5 30-130 3/12/18 15:24 2-Fluorobiphenyl 65.6 30-130 3/12/18 15:24 2,4,6-Tribromophenol 77.4 30-130 3/12/18 15:24 p-Terphenyl-dl4 85.7 30-130 3/12/18 15:24 Page 44 of 94 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15 Samnle ID: 18C0324-07 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Gasoline Range Organics (GRO) ND 1.2 1.2 mg/Kg dry 1 SW-846 8015C 3/12/18 3/12/18 17:01 EEH Diesel Range Organics 1600 100 23 mg/Kg dry 10 SW-846 8015C 3/9/18 3/11/18 18:45 PJG Surrogates % Recovery Recovery Limits Flag/Qual 1-Chloro-3-fluorobenzene 104 70-130 3/12/18 17:01 o-Terphenyl 71.8 40-140 3/11/18 18:45 Page 45 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15 Samnle ID: 18C0324-07 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 82.3 % Wt 1 SM 2540G 3/8/18 3/8/18 19:16 DMP Page 46 of 94 Table of Contents icon-te w ANALYTICAL LABORATORY Project Location: 3312 Watkins Rd Date Received: 3/6/2018 Field Sample #: AST-3 North (1-2) Samnle ID: 18C0324-07 Samnle Matrix: Soil 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Sample Description: Sampled: 3/5/2018 11:15 Work Order: 18C0324 TCLP - Metals Analyses Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Arsenic ND 0.010 0.0080 mg/L 1 SW-846 601OC-D 3/12/18 3/12/18 18:41 QNW Mercury 0.000059 0.00010 0.000034 1119/1- 1 J SW-846 7470A 3/12/18 3/12/18 11:59 EJB Barium 0.22 0.050 0.0053 mg/L 1 SW-846 601OC-D 3/12/18 3/12/18 18:41 QNW Cadmium ND 0.0040 0.00090 mg/L 1 SW-846 601OC-D 3/12/18 3/12/18 18:41 QNW Chromium ND 0.010 0.0061 mg/L 1 SW-846 601OC-D 3/12/18 3/12/18 18:41 QNW Lead 0.14 0.010 0.0044 mg/L 1 SW-846 601OC-D 3/12/18 3/12/18 18:41 QNW Selenium ND 0.050 0.034 mg/L 1 L-02 SW-846 601OC-D 3/12/18 3/12/18 18:41 QNW Silver ND 0.0050 0.0049 mg/L 1 SW-846 601OC-D 3/12/18 3/13/18 13:12 QNW Page 47 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35 Sample ID: 18C0324-08 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.13 0.030 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Acrylonitrile ND 0.0078 0.0033 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF tert-Amyl Methyl Ether (TAME) ND 0.0013 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Benzene ND 0.0026 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Bromobenzene ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Bromochloromethane ND 0.0026 0.0018 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Bromodichloromethane ND 0.0026 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Bromoform ND 0.0026 0.0018 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Bromomethane ND 0.013 0.0055 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 2-Butanone (MEK) ND 0.052 0.023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF tert-Butyl Alcohol (TBA) ND 0.052 0.027 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF n-Butylbenzene ND 0.0026 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF sec-Butylbenzene ND 0.0026 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF tert-Butylbenzene ND 0.0026 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0013 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Carbon Disulfide ND 0.0078 0.0056 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Carbon Tetrachloride ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Chlombenzene ND 0.0026 0.00091 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 11:17 MFF Chlorodibromomethane ND 0.0026 0.00091 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 11:17 MFF Chloroethane ND 0.026 0.0020 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Chloroform ND 0.0052 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Chloromethane ND 0.013 0.0083 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 2-Chlorotoluene ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 4-Chlorotoluene ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0026 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,2-Dibromoethane (EDB) ND 0.0026 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Dibromomethane ND 0.0026 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,2-Dichlorobenzene ND 0.0026 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,3-Dichlorobenzene ND 0.0026 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,4-Dichlorobenzene ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF trans-1,4-Dichloro-2-butene ND 0.0052 0.0027 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Dichlorodifluoromethane (Freon 12) ND 0.026 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,1-Dichloroethane ND 0.0026 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,2-Dichloroethane ND 0.0026 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1, 1 -Dichloroethylene ND 0.0052 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF cis-1,2-Dichloroethylene ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF trans-1,2-Dichloroethylene ND 0.0026 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,2-Dichloropropane ND 0.0026 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,3-Dichloropropane ND 0.0013 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 2,2-Dichloropropane ND 0.0026 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1, 1 -Dichloropropene ND 0.0026 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF cis-1,3-Dichloropropene ND 0.0013 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF trans-1,3-Dichloropropene ND 0.0013 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Diethyl Ether ND 0.026 0.0023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Page 48 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35 Sample ID: 18C0324-08 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0013 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,4-Dioxane ND 0.13 0.075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Ethanol ND 0.26 0.052 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Ethylbenzene ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Hexachlorobutadiene ND 0.0026 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 2-Hexanone (MBK) ND 0.026 0.014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Isopropylbenzene (Cumene) ND 0.0026 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF p-Isopropyltoluene (p-Cymene) ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0052 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Methylene Chloride ND 0.026 0.0092 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 4-Methyl-2-pentanone (MIBK) ND 0.026 0.0099 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Naphthalene ND 0.0052 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF n-Propylbenzene ND 0.0026 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Styrene ND 0.0026 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0026 0.0023 mg/Kg dry 1 SW-8468260B 3/8/18 3/8/18 11:17 MFF 1,1,2,2-Tetrachloroethane ND 0.0013 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Tetrachloroethylene ND 0.0026 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Tetrahydrofuran ND 0.013 0.0029 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Toluene ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,2,3-Trichlorobenzene ND 0.0026 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,2,4-Trichlorobenzene ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,3,5-Trichlorobenzene ND 0.0026 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1, 1, 1 -Trichloroethane ND 0.0026 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,1,2-Trichloroethane ND 0.0026 0.0016 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Trichloroethylene ND 0.0026 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Trichlorofluoromethane (Freon 11) ND 0.013 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,2,3-Trichloropropane ND 0.0026 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.013 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0026 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF 1,3,5-Trimethylbenzene ND 0.0026 0.00078 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Vinyl Chloride ND 0.013 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF m+p Xylene ND 0.0052 0.0022 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF o-Xylene ND 0.0026 0.00091 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:17 MFF Surrogates % Recovery Recovery Limits Flag/Qaal 1,2-Dichloroethane-d4 98.5 70-130 3/8/18 11:17 Toluene-d8 99.0 70-130 3/8/18 11:17 4-Bromofluorobenzene 100 70-130 3/8/18 11:17 Page 49 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35 Samnle ID: 18C0324-08 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.20 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Acenaphthylene ND 0.20 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Acetophenone ND 0.40 0.079 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Aniline ND 0.40 0.11 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Anthracene ND 0.20 0.058 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Benzidine ND 0.78 0.50 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Benzo(a)anthracene ND 0.20 0.053 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Benzo(a)pyrene ND 0.20 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Benzo(b)fluoranthene ND 0.20 0.057 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Benzo(g,h,i)perylene ND 0.20 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Benzo(k)fluoranthene ND 0.20 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Benzoic Acid ND 1.2 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Bis(2-chloroethoxy)methane ND 0.40 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Bis(2-chloroethyl)ether ND 0.40 0.079 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Bis(2-chloroisopropyl)ether ND 0.40 0.086 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Bis(2-Ethylhexyl)phthalate ND 0.40 0.16 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 4-Bromophenylphenylether ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Butylbenzylphthalate ND 0.40 0.096 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:46 BGL Carbazole ND 0.20 0.052 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:46 BGL 4-Chloroaniline ND 0.78 0.092 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 4-Chloro-3-methylphenol ND 0.78 0.086 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2-Chloronaphthalene ND 0.40 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2-Chlorophenol ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 4-Chlorophenylphenylether ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Chrysene ND 0.20 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Dibenz(a,h)anthracene ND 0.20 0.12 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Dibenzofuran ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Di-n-butylphthalate ND 0.40 0.088 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 1,2-Dichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 1,3-Dichlorobenzene ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 1,4-Dichlorobenzene ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 3,3-Dichlorobenzidine ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2,4-Dichlorophenol ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Diethylphthalate ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2,4-Dimethylphenol ND 0.40 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Dimethylphthalate ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 4,6-Dinitro-2-methylphenol ND 0.40 0.38 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2,4-Dinitrophenol ND 0.78 0.23 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2,4-Dinitrotoluene ND 0.40 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2,6-Dinitrotoluene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Di-n-octylphthalate ND 0.40 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.40 0.065 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 15:46 BGL Fluoranthene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Flumene ND 0.20 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Page 50 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35 Samnle ID: 18C0324-08 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Hexachlorobutadiene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Hexachlorocyclopentadiene ND 0.40 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Hexachloroethane ND 0.40 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Indeno(1,2,3-cd)pyrene ND 0.20 0.14 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Isophorone ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 1-Methylnaphthalene ND 0.20 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2-Methylnaphthalene ND 0.20 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2-Methylphenol ND 0.40 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 3/4-Methylphenol ND 0.40 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Naphthalene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2-Nitroaniline ND 0.40 0.067 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 3-Nitroaniline ND 0.40 0.058 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 4-Nitroaniline ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Nitrobenzene ND 0.40 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2-Nitrophenol ND 0.40 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 4-Nitrophenol ND 0.78 0.088 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 15:46 BGL N-Nitrosodimethylamine ND 0.40 0.25 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 15:46 BGL N-Nitrosodiphenylamine ND 0.40 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL N-Nitrosodi-n-propylamine ND 0.40 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Pentachloronitrobenzene ND 0.40 0.096 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Pentachlorophenol ND 0.40 0.097 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Phenanthrene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Phenol ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Pyrene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Pyridine ND 0.40 0.065 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 1,2,4,5-Texachlorobenzene ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 1,2,4-Trichlorobenzene ND 0.40 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2,4,5-Trichlorophenol ND 0.40 0.091 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL 2,4,6-Trichlorophenol ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 15:46 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 61.4 30-130 3/12/18 15:46 Phenol-d6 61.0 30-130 3/12/18 15:46 Nitrobenzene-d5 84.3 30-130 3/12/18 15:46 2-Fluorobiphenyl 81.2 30-130 3/12/18 15:46 2,4,6-Tribromophenol 82.4 30-130 3/12/18 15:46 p-Terphenyl-dl4 92.8 30-130 3/12/18 15:46 Page 51 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35 Samnle ID: 18C0324-08 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 84.2 % Wt 1 SM 2540G 3/8/18 3/8/18 19:17 DMP Page 52 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 South Sampled: 3/5/2018 11:20 Sample ID: 18C0324-09 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.11 0.026 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Acrylonitrile ND 0.0066 0.0028 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF tert-Amyl Methyl Ether (TAME) ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Benzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Bromobenzene ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Bromochloromethane ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Bromodichloromethane ND 0.0022 0.00066 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 11:46 MFF Bromoform ND 0.0022 0.0015 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 11:46 MFF Bromomethane ND 0.011 0.0046 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 2-Butanone (MEK) ND 0.044 0.019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF tert-Butyl Alcohol (TBA) ND 0.044 0.023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF n-Butylbenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF sec-Butylbenzene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF tert-Butylbenzene ND 0.0022 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0011 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Carbon Disulfide ND 0.0066 0.0048 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Carbon Tetrachloride ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Chlombenzene ND 0.0022 0.00077 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 11:46 MFF Chlorodibromomethane ND 0.0022 0.00077 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 11:46 MFF Chloroethane ND 0.022 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Chloroform ND 0.0044 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Chloromethane ND 0.011 0.0071 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 2-Chlorotoluene ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 4-Chlorotoluene ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,2-Dibromoethane (EDB) ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Dibromomethane ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,2-Dichlorobenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,3-Dichlorobenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,4-Dichlorobenzene ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF trans-1,4-Dichloro-2-butene ND 0.0044 0.0023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Dichlorodifluoromethane (Freon 12) ND 0.022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,1-Dichloroethane ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,2-Dichloroethane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1, 1 -Dichloroethylene ND 0.0044 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF cis-1,2-Dichloroethylene ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF trans-1,2-Dichloroethylene ND 0.0022 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,2-Dichloropropane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,3-Dichloropropane ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 2,2-Dichloropropane ND 0.0022 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1, 1 -Dichloropropene ND 0.0022 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF cis-1,3-Dichloropropene ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF trans-1,3-Dichloropropene ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Diethyl Ether ND 0.022 0.0020 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Page 53 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 South Sampled: 3/5/2018 11:20 Sample ID: 18C0324-09 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0011 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,4-Dioxane ND 0.11 0.064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Ethanol ND 0.22 0.044 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Ethylbenzene ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Hexachlorobutadiene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 2-Hexanone (MBK) ND 0.022 0.012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Isopropylbenzene (Cumene) ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF p-Isopropyltoluene (p-Cymene) ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0044 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Methylene Chloride ND 0.022 0.0079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 4-Methyl-2-pentanone (MIBK) ND 0.022 0.0084 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Naphthalene ND 0.0044 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF n-Propylbenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Styrene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0022 0.0020 mg/Kg dry 1 SW-8468260B 3/8/18 3/8/18 11:46 MFF 1,1,2,2-Tetrachloroethane ND 0.0011 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Tetrachloroethylene ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Tetrahydrofuran ND 0.011 0.0024 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Toluene ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,2,3-Trichlorobenzene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,2,4-Trichlorobenzene ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,3,5-Trichlorobenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1, 1, 1 -Trichloroethane ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,1,2-Trichloroethane ND 0.0022 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Trichloroethylene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Trichlorofluoromethane (Freon 11) ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,2,3-Trichloropropane ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.011 0.0010 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0022 0.00089 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF 1,3,5-Trimethylbenzene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Vinyl Chloride ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF m+p Xylene ND 0.0044 0.0019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF o-Xylene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 11:46 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 97.5 70-130 3/8/18 11:46 Toluene-d8 99.2 70-130 3/8/18 11:46 4-Bromofluorobenzene 102 70-130 3/8/18 11:46 Page 54 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 South Sampled: 3/5/2018 11:20 Samnle ID: 18C0324-09 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.21 0.063 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Acenaphthylene ND 0.21 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Acetophenone ND 0.42 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Aniline ND 0.42 0.12 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Anthracene ND 0.21 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Benzidine ND 0.81 0.52 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Benzo(a)anthracene ND 0.21 0.055 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:09 BGL Benzo(a)pyrene ND 0.21 0.065 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:09 BGL Benzo(b)fluoranthene ND 0.21 0.059 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Benzo(g,h,i)perylene ND 0.21 0.092 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Benzo(k)fluoranthene ND 0.21 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Benzoic Acid ND 1.2 0.22 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Bis(2-chloroethoxy)methane ND 0.42 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Bis(2-chloroethyl)ether ND 0.42 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Bis(2-chloroisopropyl)ether ND 0.42 0.090 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Bis(2-Ethylhexyl)phthalate ND 0.42 0.16 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 4-Bromophenylphenylether ND 0.42 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Butylbenzylphthalate ND 0.42 0.099 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:09 BGL Carbazole ND 0.21 0.054 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:09 BGL 4-Chloroaniline ND 0.81 0.096 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 4-Chloro-3-methylphenol ND 0.81 0.090 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2-Chloronaphthalene ND 0.42 0.079 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2-Chlorophenol ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 4-Chlorophenylphenylether ND 0.42 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Chrysene ND 0.21 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Dibenz(a,h)anthracene ND 0.21 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Dibenzofuran ND 0.42 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Di-n-butylphthalate ND 0.42 0.091 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 1,2-Dichlorobenzene ND 0.42 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 1,3-Dichlorobenzene ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 1,4-Dichlorobenzene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 3,3-Dichlorobenzidine ND 0.21 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2,4-Dichlorophenol ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Diethylphthalate ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2,4-Dimethylphenol ND 0.42 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Dimethylphthalate ND 0.42 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 4,6-Dinitro-2-methylphenol ND 0.42 0.40 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2,4-Dinitrophenol ND 0.81 0.24 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2,4-Dinitrotoluene ND 0.42 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2,6-Dinitrotoluene ND 0.42 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Di-n-octylphthalate ND 0.42 0.22 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.42 0.067 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:09 BGL Fluoranthene ND 0.21 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Flumene ND 0.21 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Page 55 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 South Sampled: 3/5/2018 11:20 Samnle ID: 18C0324-09 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.42 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Hexachlorobutadiene ND 0.42 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Hexachlorocyclopentadiene ND 0.42 0.088 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Hexachloroethane ND 0.42 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Indeno(1,2,3-cd)pyrene ND 0.21 0.15 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Isophorone ND 0.42 0.081 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 1-Methylnaphthalene ND 0.21 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2-Methylnaphthalene ND 0.21 0.072 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2-Methylphenol ND 0.42 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 3/4-Methylphenol ND 0.42 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Naphthalene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2-Nitroaniline ND 0.42 0.070 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 3-Nitroaniline ND 0.42 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 4-Nitroaniline ND 0.42 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Nitrobenzene ND 0.42 0.079 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2-Nitrophenol ND 0.42 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 4-Nitrophenol ND 0.81 0.091 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 16:09 BGL N-Nitrosodimethylamine ND 0.42 0.26 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 16:09 BGL N-Nitrosodiphenylamine ND 0.42 0.086 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL N-Nitrosodi-n-propylamine ND 0.42 0.086 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Pentachloronitrobenzene ND 0.42 0.099 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Pentachlorophenol ND 0.42 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Phenanthrene ND 0.21 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Phenol ND 0.42 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Pyrene ND 0.21 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Pyridine ND 0.42 0.067 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 1,2,4,5-Texachlorobenzene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 1,2,4-Trichlorobenzene ND 0.42 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2,4,5-Trichlorophenol ND 0.42 0.094 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL 2,4,6-Trichlorophenol ND 0.42 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:09 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 60.4 30-130 3/12/18 16:09 Phenol-d6 62.0 30-130 3/12/18 16:09 Nitrobenzene-d5 89.3 30-130 3/12/18 16:09 2-Fluorobiphenyl 85.2 30-130 3/12/18 16:09 2,4,6-Tribromophenol 88.1 30-130 3/12/18 16:09 p-Terphenyl-dl4 92.6 30-130 3/12/18 16:09 Page 56 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 South Sampled: 3/5/2018 11:20 Samnle ID: 18C0324-09 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 81.5 % Wt 1 SM 2540G 3/8/18 3/8/18 19:17 DMP Page 57 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 West Sampled: 3/5/2018 11:25 Sample ID: 18C0324-10 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.098 0.023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Acrylonitrile ND 0.0059 0.0025 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF tert-Amyl Methyl Ether (TAME) ND 0.00098 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Benzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Bromobenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Bromochloromethane ND 0.0020 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Bromodichloromethane ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Bromoform ND 0.0020 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Bromomethane ND 0.0098 0.0041 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 2-Butanone (MEK) ND 0.039 0.017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF tert-Butyl Alcohol (TBA) ND 0.039 0.021 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF n-Butylbenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF sec-Butylbenzene ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF tert-Butylbenzene ND 0.0020 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00098 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Carbon Disulfide ND 0.0059 0.0042 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Carbon Tetrachloride ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Chlombenzene ND 0.0020 0.00069 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 12:14 MFF Chlorodibromomethane ND 0.0020 0.00069 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 12:14 MFF Chloroethane ND 0.020 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Chloroform ND 0.0039 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Chloromethane ND 0.0098 0.0063 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 2-Chlorotoluene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 4-Chlorotoluene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0020 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,2-Dibromoethane (EDB) ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Dibromomethane ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,2-Dichlorobenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,3-Dichlorobenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,4-Dichlorobenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF trans-1,4-Dichloro-2-butene ND 0.0039 0.0021 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Dichlorodifluoromethane (Freon 12) ND 0.020 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,1-Dichloroethane ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,2-Dichloroethane ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1, 1 -Dichloroethylene ND 0.0039 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF cis-1,2-Dichloroethylene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF trans-1,2-Dichloroethylene ND 0.0020 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,2-Dichloropropane ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,3-Dichloropropane ND 0.00098 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 2,2-Dichloropropane ND 0.0020 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1, 1 -Dichloropropene ND 0.0020 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF cis-1,3-Dichloropropene ND 0.00098 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF trans-1,3-Dichloropropene ND 0.00098 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Diethyl Ether ND 0.020 0.0018 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Page 58 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 West Sampled: 3/5/2018 11:25 Sample ID: 18C0324-10 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.00098 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,4-Dioxane ND 0.098 0.057 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Ethanol ND 0.20 0.039 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Ethylbenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Hexachlorobutadiene ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 2-Hexanone (MBK) ND 0.020 0.011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Isopropylbenzene (Cumene) ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF p-Isopropyltoluene (p-Cymene) ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0039 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Methylene Chloride ND 0.020 0.0070 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 4-Methyl-2-pentanone (MIBK) ND 0.020 0.0075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Naphthalene ND 0.0039 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF n-Propylbenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Styrene ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0020 0.0018 mg/Kg dry 1 SW-8468260B 3/8/18 3/8/18 12:14 MFF 1,1,2,2-Tetrachloroethane ND 0.00098 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Tetrachloroethylene ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Tetrahydrofuran ND 0.0098 0.0022 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Toluene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,2,3-Trichlorobenzene ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,2,4-Trichlorobenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,3,5-Trichlorobenzene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1, 1, 1 -Trichloroethane ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,1,2-Trichloroethane ND 0.0020 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Trichloroethylene ND 0.0020 0.00098 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Trichlorofluoromethane (Freon 11) ND 0.0098 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,2,3-Trichloropropane ND 0.0020 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.0098 0.00088 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0020 0.00079 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF 1,3,5-Trimethylbenzene ND 0.0020 0.00059 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Vinyl Chloride ND 0.0098 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF m+p Xylene ND 0.0039 0.0017 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF o-Xylene ND 0.0020 0.00069 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:14 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.5 70-130 3/8/18 12:14 Toluene-d8 101 70-130 3/8/18 12:14 4-Bromofluorobenzene 101 70-130 3/8/18 12:14 Page 59 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 West Sampled: 3/5/2018 11:25 Samnle ID: 18C0324-10 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.20 0.059 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Acenaphthylene ND 0.20 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Acetophenone ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Aniline ND 0.40 0.11 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Anthracene ND 0.20 0.057 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Benzidine ND 0.77 0.49 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Benzo(a)anthracene ND 0.20 0.052 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:34 BGL Benzo(a)pyrene ND 0.20 0.062 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:34 BGL Benzo(b)fluoranthene ND 0.20 0.056 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Benzo(g,h,i)perylene ND 0.20 0.087 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Benzo(k)fluoranthene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Benzoic Acid ND 1.2 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Bis(2-chloroethoxy)methane ND 0.40 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Bis(2-chloroethyl)ether ND 0.40 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Bis(2-chloroisopropyl)ether ND 0.40 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Bis(2-Ethylhexyl)phthalate ND 0.40 0.15 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 4-Bromophenylphenylether ND 0.40 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Butylbenzylphthalate ND 0.40 0.094 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:34 BGL Carbazole ND 0.20 0.051 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:34 BGL 4-Chloroaniline ND 0.77 0.091 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 4-Chloro-3-methylphenol ND 0.77 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2-Chloronaphthalene ND 0.40 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2-Chlorophenol ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 4-Chlorophenylphenylether ND 0.40 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Chrysene ND 0.20 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Dibenz(a,h)anthracene ND 0.20 0.12 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Dibenzofuran ND 0.40 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Di-n-butylphthalate ND 0.40 0.086 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 1,2-Dichlorobenzene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 1,3-Dichlorobenzene ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 1,4-Dichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 3,3-Dichlorobenzidine ND 0.20 0.060 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2,4-Dichlorophenol ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Diethylphthalate ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2,4-Dimethylphenol ND 0.40 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Dimethylphthalate ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 4,6-Dinitro-2-methylphenol ND 0.40 0.38 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2,4-Dinitrophenol ND 0.77 0.23 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2,4-Dinitrotoluene ND 0.40 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2,6-Dinitrotoluene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Di-n-octylphthalate ND 0.40 0.21 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.40 0.064 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:34 BGL Fluoranthene ND 0.20 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Flumene ND 0.20 0.064 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Page 60 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 West Sampled: 3/5/2018 11:25 Samnle ID: 18C0324-10 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Hexachlorobutadiene ND 0.40 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Hexachlorocyclopentadiene ND 0.40 0.084 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Hexachloroethane ND 0.40 0.079 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Indeno(1,2,3-cd)pyrene ND 0.20 0.14 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Isophorone ND 0.40 0.077 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 1-Methylnaphthalene ND 0.20 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2-Methylnaphthalene ND 0.20 0.069 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2-Methylphenol ND 0.40 0.099 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 3/4-Methylphenol ND 0.40 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Naphthalene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2-Nitroaniline ND 0.40 0.066 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 3-Nitroaniline ND 0.40 0.057 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 4-Nitroaniline ND 0.40 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Nitrobenzene ND 0.40 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2-Nitrophenol ND 0.40 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 4-Nitrophenol ND 0.77 0.086 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 16:34 BGL N-Nitrosodimethylamine ND 0.40 0.25 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 16:34 BGL N-Nitrosodiphenylamine ND 0.40 0.081 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL N-Nitrosodi-n-propylamine ND 0.40 0.081 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Pentachloronitrobenzene ND 0.40 0.094 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Pentachlorophenol ND 0.40 0.095 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Phenanthrene ND 0.20 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Phenol ND 0.40 0.067 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Pyrene ND 0.20 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Pyridine ND 0.40 0.064 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 1,2,4,5-Texachlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 1,2,4-Trichlorobenzene ND 0.40 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2,4,5-Trichlorophenol ND 0.40 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL 2,4,6-Trichlorophenol ND 0.40 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:34 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 65.3 30-130 3/12/18 16:34 Phenol-d6 65.3 30-130 3/12/18 16:34 Nitrobenzene-d5 91.9 30-130 3/12/18 16:34 2-Fluorobiphenyl 86.7 30-130 3/12/18 16:34 2,4,6-Tribromophenol 87.0 30-130 3/12/18 16:34 p-Terphenyl-dl4 96.4 30-130 3/12/18 16:34 Page 61 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 West Sampled: 3/5/2018 11:25 Samnle ID: 18C0324-10 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 85.8 % Wt 1 SM 2540G 3/8/18 3/8/18 19:18 DMP Page 62 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 East Sampled: 3/5/2018 11:30 Sample ID: 18C0324-11 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.11 0.025 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Acrylonitrile ND 0.0064 0.0027 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF tert-Amyl Methyl Ether (TAME) ND 0.0011 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Benzene ND 0.0021 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Bromobenzene ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Bromochloromethane ND 0.0021 0.0015 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Bromodichloromethane ND 0.0021 0.00064 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 12:41 MFF Bromoform ND 0.0021 0.0015 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 12:41 MFF Bromomethane ND 0.011 0.0045 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 2-Butanone (MEK) ND 0.043 0.019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF tert-Butyl Alcohol (TBA) ND 0.043 0.022 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF n-Butylbenzene ND 0.0021 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF sec-Butylbenzene ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF tert-Butylbenzene ND 0.0021 0.00096 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0011 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Carbon Disulfide ND 0.0064 0.0046 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Carbon Tetrachloride ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Chlombenzene ND 0.0021 0.00075 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 12:41 MFF Chlorodibromomethane ND 0.0021 0.00075 mg/Kg dry I SW-846 8260B 3/8/18 3/8/18 12:41 MFF Chloroethane ND 0.021 0.0016 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Chloroform ND 0.0043 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Chloromethane ND 0.011 0.0069 mg/Kg dry 1 L-04 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 2-Chlorotoluene ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 4-Chlorotoluene ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0021 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,2-Dibromoethane (EDB) ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Dibromomethane ND 0.0021 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,2-Dichlorobenzene ND 0.0021 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,3-Dichlorobenzene ND 0.0021 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,4-Dichlorobenzene ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF trans-1,4-Dichloro-2-butene ND 0.0043 0.0023 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Dichlorodifluoromethane (Freon 12) ND 0.021 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,1-Dichloroethane ND 0.0021 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,2-Dichloroethane ND 0.0021 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1, 1 -Dichloroethylene ND 0.0043 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF cis-1,2-Dichloroethylene ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF trans-1,2-Dichloroethylene ND 0.0021 0.00096 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,2-Dichloropropane ND 0.0021 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,3-Dichloropropane ND 0.0011 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 2,2-Dichloropropane ND 0.0021 0.00096 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1, 1 -Dichloropropene ND 0.0021 0.00096 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF cis-1,3-Dichloropropene ND 0.0011 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF trans-1,3-Dichloropropene ND 0.0011 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Diethyl Ether ND 0.021 0.0019 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Page 63 of 94 Table of Contents icon-te w ANALYTICAL LA8ORATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 East Sampled: 3/5/2018 11:30 Sample ID: 18C0324-11 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0011 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,4-Dioxane ND 0.11 0.062 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Ethanol ND 0.21 0.043 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Ethylbenzene ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Hexachlorobutadiene ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 2-Hexanone (MBK) ND 0.021 0.012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Isopropylbenzene (Cumene) ND 0.0021 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF p-Isopropyltoluene (p-Cymene) ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0043 0.00096 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Methylene Chloride ND 0.021 0.0076 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 4-Methyl-2-pentanone (MIBK) ND 0.021 0.0081 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Naphthalene ND 0.0043 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF n-Propylbenzene ND 0.0021 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Styrene ND 0.0021 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0021 0.0019 mg/Kgdry 1 SW-8468260B 3/8/18 3/8/18 12:41 MFF 1,1,2,2-Tetrachloroethane ND 0.0011 0.00096 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Tetrachloroethylene ND 0.0021 0.0014 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Tetrahydrofuran ND 0.011 0.0024 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Toluene ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,2,3-Trichlorobenzene ND 0.0021 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,2,4-Trichlorobenzene ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,3,5-Trichlorobenzene ND 0.0021 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1, 1, 1 -Trichloroethane ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,1,2-Trichloroethane ND 0.0021 0.0013 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Trichloroethylene ND 0.0021 0.0011 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Trichlorofluoromethane (Freon 11) ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,2,3-Trichloropropane ND 0.0021 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.011 0.00096 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0021 0.00086 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF 1,3,5-Trimethylbenzene ND 0.0021 0.00064 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Vinyl Chloride ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF m+p Xylene ND 0.0043 0.0018 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF o-Xylene ND 0.0021 0.00075 mg/Kg dry 1 SW-846 8260B 3/8/18 3/8/18 12:41 MFF Surrogates % Recovery Recovery Limits Flag/Qaal 1,2-Dichloroethane-d4 101 70-130 3/8/18 12:41 Toluene-d8 100 70-130 3/8/18 12:41 4-Bromofluorobenzene 102 70-130 3/8/18 12:41 Page 64 of 94 Table of Contents icon-te w ANALYTICAL LABQRATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 East Sampled: 3/5/2018 11:30 Samnle ID: 18C0324-11 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.22 0.065 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Acenaphthylene ND 0.22 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Acetophenone ND 0.43 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Aniline ND 0.43 0.12 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Anthracene ND 0.22 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Benzidine ND 0.84 0.54 mg/Kg dry 1 V-04, V-05 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Benzo(a)anthracene ND 0.22 0.057 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:56 BGL Benzo(a)pyrene ND 0.22 0.068 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:56 BGL Benzo(b)fluoranthene ND 0.22 0.061 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Benzo(g,h,i)perylene ND 0.22 0.096 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Benzo(k)fluoranthene ND 0.22 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Benzoic Acid ND 1.3 0.23 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Bis(2-chloroethoxy)methane ND 0.43 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Bis(2-chloroethyl)ether ND 0.43 0.085 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Bis(2-chloroisopropyl)ether ND 0.43 0.093 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Bis(2-Ethylhexyl)phthalate ND 0.43 0.17 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 4-Bromophenylphenylether ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Butylbenzylphthalate ND 0.43 0.10 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:56 BGL Carbazole ND 0.22 0.056 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:56 BGL 4-Chloroaniline ND 0.84 0.099 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 4-Chloro-3-methylphenol ND 0.84 0.093 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2-Chloronaphthalene ND 0.43 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2-Chlorophenol ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 4-Chlorophenylphenylether ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Chrysene ND 0.22 0.068 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Dibenz(a,h)anthracene ND 0.22 0.13 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Dibenzofuran ND 0.43 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Di-n-butylphthalate ND 0.43 0.094 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 1,2-Dichlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 1,3-Dichlorobenzene ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 1,4-Dichlorobenzene ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 3,3-Dichlorobenzidine ND 0.22 0.066 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2,4-Dichlorophenol ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Diethylphthalate ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2,4-Dimethylphenol ND 0.43 0.080 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Dimethylphthalate ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 4,6-Dinitro-2-methylphenol ND 0.43 0.41 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2,4-Dinitrophenol ND 0.84 0.25 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2,4-Dinitrotoluene ND 0.43 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2,6-Dinitrotoluene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Di-n-octylphthalate ND 0.43 0.23 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.43 0.070 mg/Kg dry I SW-846 8270D 3/9/18 3/12/18 16:56 BGL Fluoranthene ND 0.22 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Flumene ND 0.22 0.070 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Page 65 of 94 Table of Contents icon-te w ANALYTICAL LABQRATIDRY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 East Sampled: 3/5/2018 11:30 Samnle ID: 18C0324-11 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Hexachlorobutadiene ND 0.43 0.076 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Hexachlorocyclopentadiene ND 0.43 0.092 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Hexachloroethane ND 0.43 0.087 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Indeno(1,2,3-cd)pyrene ND 0.22 0.16 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Isophorone ND 0.43 0.084 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 1-Methylnaphthalene ND 0.22 0.083 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2-Methylnaphthalene ND 0.22 0.075 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2-Methylphenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 3/4-Methylphenol ND 0.43 0.14 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Naphthalene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2-Nitroaniline ND 0.43 0.073 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 3-Nitroaniline ND 0.43 0.062 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 4-Nitroaniline ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Nitrobenzene ND 0.43 0.082 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2-Nitrophenol ND 0.43 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 4-Nitrophenol ND 0.84 0.094 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 16:56 BGL N-Nitrosodimethylamine ND 0.43 0.27 mg/Kg dry 1 V-20 SW-846 8270D 3/9/18 3/12/18 16:56 BGL N-Nitrosodiphenylamine ND 0.43 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL N-Nitrosodi-n-propylamine ND 0.43 0.089 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Pentachloronitrobenzene ND 0.43 0.10 mg/Kg dry 1 V-16 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Pentachlorophenol ND 0.43 0.10 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Phenanthrene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Phenol ND 0.43 0.074 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Pyrene ND 0.22 0.071 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Pyridine ND 0.43 0.070 mg/Kg dry 1 V-05 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 1,2,4,5-Texachlorobenzene ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 1,2,4-Trichlorobenzene ND 0.43 0.078 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2,4,5-Trichlorophenol ND 0.43 0.098 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL 2,4,6-Trichlorophenol ND 0.43 0.073 mg/Kg dry 1 SW-846 8270D 3/9/18 3/12/18 16:56 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 64.5 30-130 3/12/18 16:56 Phenol-d6 64.5 30-130 3/12/18 16:56 Nitrobenzene-d5 84.1 30-130 3/12/18 16:56 2-Fluorobiphenyl 78.1 30-130 3/12/18 16:56 2,4,6-Tribromophenol 85.2 30-130 3/12/18 16:56 p-Terphenyl-dl4 87.5 30-130 3/12/18 16:56 Page 66 of 94 Table of Contents icon-te w ANALYTICAL LAaORATC]RY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324 Date Received: 3/6/2018 Field Sample #: AST-3 East Sampled: 3/5/2018 11:30 Samnle ID: 18C0324-11 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 78.3 % Wt 1 SM 2540G 3/8/18 3/8/18 19:18 DMP Page 67 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: % Solids-SM 2540G Lab Number [Field ID] Batch Date 18C0324-01 [AST-1 Floor] B198433 03/08/18 18C0324-02 [AST-1 South] B198433 03/08/18 18C0324-03 [AST-1 North] B198433 03/08/18 18C0324-04 [AST-1 West] B198433 03/08/18 18C0324-05 [AST-1 East] B198433 03/08/18 18C0324-06 [AST-3 Floor] B198433 03/08/18 18C0324-07 [AST-3 North (1-2)] B198433 03/08/18 18C0324-08 [AST-3 North (3-4)] B198433 03/08/18 18C0324-09 [AST-3 South] B198433 03/08/18 18C0324-10 [AST-3 West] B198433 03/08/18 18C0324-11 [AST-3 East] B198433 03/08/18 Prep Method: SW-846 3010A-SW-846 6010C-D Leachates were extracted on 3/8/2018 per SW-846 1311 in Batch B198451 Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 18C0324-07 [AST-3 North (1-2)] B198629 50.0 50.0 03/12/18 Prep Method: SW-846 7470A Prep-SW-846 7470A Leachates were extracted on 3/8/2018 per SW-846 1311 in Batch B198451 Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 18C0324-07 [AST-3 North (1-2)] B198633 6.00 6.00 03/12/18 Prep Method: SW-846 3546-SW-846 8015C Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18C0324-07 [AST-3 North (1-2)] B198557 30.1 1.00 03/09/18 Prep Method: SW-846 5035/5030B-SW-846 8015C Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18C0324-07 [AST-3 North (1-2)] B198651 5.90 6.00 03/12/18 Prep Method: SW-846 5035-SW-846 8260B Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18C0324-01 [AST-1 Floor] B198462 6.93 10.0 03/08/18 18C0324-02 [AST-1 South] B198462 6.45 10.0 03/08/18 18C0324-03 [AST-1 North] B198462 5.99 10.0 03/08/18 18C0324-04 [AST-1 West] B198462 5.17 10.0 03/08/18 18C0324-05 [AST-1 East] B198462 5.77 10.0 03/08/18 18C0324-06 [AST-3 Floor] B198462 5.22 10.0 03/08/18 18C0324-07 [AST-3 North (1-2)] B198462 5.51 10.0 03/08/18 18C0324-08 [AST-3 North (3-4)] B198462 4.56 10.0 03/08/18 18C0324-09 [AST-3 South] B198462 5.54 10.0 03/08/18 18C0324-10 [AST-3 West] B198462 5.93 10.0 03/08/18 18C0324-11 [AST-3 East] B198462 5.96 10.0 03/08/18 Page 68 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 3546-SW-846 8270D Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18C0324-01 [AST-1 Floor] B198559 30.1 1.00 03/09/18 18C0324-02 [AST-1 South] B198559 30.0 1.00 03/09/18 18C0324-03 [AST-1 North] B198559 30.0 1.00 03/09/18 18C0324-04 [AST-1 West] B198559 30.3 1.00 03/09/18 18C0324-05 [AST-1 East] B198559 30.0 1.00 03/09/18 18C0324-06 [AST-3 Floor] B198559 30.0 1.00 03/09/18 18C0324-07 [AST-3 North (1-2)] B198559 30.0 1.00 03/09/18 18C0324-08 [AST-3 North (3-4)] B198559 30.1 1.00 03/09/18 18C0324-09 [AST-3 South] B198559 30.0 1.00 03/09/18 18C0324-10 [AST-3 West] B198559 30.1 1.00 03/09/18 18C0324-11 [AST-3 East] B198559 30.1 1.00 03/09/18 Page 69 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198462 - SW-846 5035 Blank (B198462-BLK1) Prepared & Analyzed: 03/08/18 Acetone ND 0.10 mg/Kg wet Acrylonitrile ND 0.0060 mg/Kg wet tert-Amyl Methyl Ether (TAME) ND 0.0010 mg/Kg wet Benzene ND 0.0020 mg/Kg wet Bromobenzene ND 0.0020 mg/Kg wet Bromochloromethane ND 0.0020 mg/Kg wet Bromodichloromethane ND 0.0020 mg/Kg wet Bromoform ND 0.0020 mg/Kg wet Bromomethane ND 0.010 mg/Kg wet 2-Butanone (MEK) ND 0.040 mg/Kg wet tert-Butyl Alcohol (TBA) ND 0.040 mg/Kg wet n-Butylbenzene ND 0.0020 mg/Kg wet sec-Butylbenzene ND 0.0020 mg/Kg wet tert-Butylbenzene ND 0.0020 mg/Kg wet tert-Butyl Ethyl Ether (TBEE) ND 0.0010 mg/Kg wet Carbon Disulfide ND 0.0060 mg/Kg wet Carbon Tetrachloride ND 0.0020 mg/Kg wet Chlorobenzene ND 0.0020 mg/Kg wet Chlorodibromomethane ND 0.0010 mg/Kg wet Chloroethane ND 0.020 mg/Kg wet Chloroform ND 0.0040 mg/Kg wet Chloromethane ND 0.010 mg/Kg wet 2-Chlorotoluene ND 0.0020 mg/Kg wet 4-Chlorotoluene ND 0.0020 mg/Kg wet 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0020 mg/Kg wet 1,2-Dibromoethane (EDB) ND 0.0010 mg/Kg wet Dibromomethane ND 0.0020 mg/Kg wet 1,2-Dichlorobenzene ND 0.0020 mg/Kg wet 1,3-Dichlorobenzene ND 0.0020 mg/Kg wet 1,4-Dichlorobenzene ND 0.0020 mg/Kg wet trans-1,4-Dichloro-2-butene ND 0.0040 mg/Kg wet Dichlorodifluoromethane (Freon 12) ND 0.020 mg/Kg wet 1,1-Dichloroethane ND 0.0020 mg/Kg wet 1,2-Dichloroethane ND 0.0020 mg/Kg wet 1,1-Dichloroethylene ND 0.0040 mg/Kg wet cis-1,2-Dichloroethylene ND 0.0020 mg/Kg wet trans-1,2-Dichloroethylene ND 0.0020 mg/Kg wet 1,2-Dichloropropane ND 0.0020 mg/Kg wet 1,3-Dichloropropane ND 0.0010 mg/Kg wet 2,2-Dichloropropane ND 0.0020 mg/Kg wet 1,1-Dichloropropene ND 0.0020 mg/Kg wet cis-1,3-Dichloropropene ND 0.0010 mg/Kg wet trans-1,3-Dichloropropene ND 0.0010 mg/Kg wet Diethyl Ether ND 0.020 mg/Kg wet Diisopropyl Ether (RIPE) ND 0.0010 mg/Kg wet 1,4-Dioxane ND 0.10 mg/Kg wet Ethanol ND 0.20 mg/Kg wet Ethylbenzene ND 0.0020 mg/Kg wet Hexachlorobutadiene ND 0.0020 mg/Kg wet 2-Hexanone (MBK) ND 0.020 mg/Kg wet Isopropylbenzene (Cumene) ND 0.0020 mg/Kg wet p-Isopropyltoluene (p-Cymene) ND 0.0020 mg/Kg wet L-04 Page 70 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD \nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198462 - SW-846 5035 Blank (B198462-BLK1) Prepared & Analyzed: 03/08/18 Methyl tert-Butyl Ether (MTBE) ND 0.0040 mg/Kg wet Methylene Chloride ND 0.020 mg/Kg wet 4-Methyl-2-pentanone (MIBK) ND 0.020 mg/Kg wet Naphthalene ND 0.0040 mg/Kg wet n-Propylbenzene ND 0.0020 mg/Kg wet Styrene ND 0.0020 mg/Kg wet 1, 1, 1,2-Tetrachloroethane ND 0.0020 mg/Kg wet 1,1,2,2-Tetrachloroethane ND 0.0010 mg/Kg wet Tetrachloroethylene ND 0.0020 mg/Kg wet Tetrahydrofuran ND 0.010 mg/Kg wet Toluene ND 0.0020 mg/Kg wet 1,2,3-Trichlorobenzene ND 0.0020 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.0020 mg/Kg wet 1,3,5-Trichlorobenzene ND 0.0020 mg/Kg wet 1, 1, 1 -Trichloroethane ND 0.0020 mg/Kg wet 1,1,2-Trichloroethane ND 0.0020 mg/Kg wet Trichloroethylene ND 0.0020 mg/Kg wet Trichlorofluoromethane (Freon 11) ND 0.010 mg/Kg wet 1,2,3-Trichloropropane ND 0.0020 mg/Kg wet 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.010 mg/Kg wet 113) 1,2,4-Trimethylbenzene ND 0.0020 mg/Kg wet 1,3,5-Trimethylbenzene ND 0.0020 mg/Kg wet Vinyl Chloride ND 0.010 mg/Kg wet m+p Xylene ND 0.0040 mg/Kg wet o-Xylene ND 0.0020 mg/Kg wet Surrogate:l,2-Dichloroethane-d4 0.0489 mg/Kg wet 0.0500 97.8 70-130 Surrogate: Toluene-d8 0.0488 mg/Kg wet 0.0500 97.6 70-130 Surrogate:4-Bromofluorobenzene 0.0502 mg/Kg wet 0.0500 100 70-130 LCS (B198462-BSI) Prepared & Analyzed: 03/08/18 Acetone 0.182 0.10 mg/Kg wet 0.200 91.2 70-160 f Acrylonitrile 0.0205 0.0060 mg/Kg wet 0.0200 103 70-130 tert-Amyl Methyl Ether (TAME) 0.0180 0.0010 mg/Kg wet 0.0200 89.9 70-130 Benzene 0.0178 0.0020 mg/Kgwet 0.0200 88.9 70-130 Bromobenzene 0.0193 0.0020 mg/Kg wet 0.0200 96.5 70-130 Bromochloromethane 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 Bromodichloromethane 0.0183 0.0020 mg/Kgwet 0.0200 91.5 70-130 Bromoform 0.0203 0.0020 mg/Kg wet 0.0200 102 70-130 Bromomethane 0.00892 0.010 mg/Kg wet 0.0200 44.6 40-130 J t 2-Butanone (MEK) 0.215 0.040 mg/Kg wet 0.200 107 70-160 f tert-Butyl Alcohol (TBA) 0.200 0.040 mg/Kg wet 0.200 100 40-130 t n-Butylbenzene 0.0193 0.0020 mg/Kg wet 0.0200 96.6 70-130 sec-Butylbenzene 0.0188 0.0020 mg/Kgwet 0.0200 94.0 70-130 tert-Butylbenzene 0.0178 0.0020 mg/Kg wet 0,0200 89.1 70-160 t tert-Butyl Ethyl Ether (TBEE) 0.0180 0.0010 mg/Kg wet 0.0200 90.2 70-130 Carbon Disulfide 0.0168 0.0060 mg/Kg wet 0.0200 84.1 70-130 Carbon Tetrachloride 0.0193 0.0020 mg/Kg wet 0,0200 96.5 70-130 Chlorobenzene 0.0190 0.0020 mg/Kg wet 0.0200 94.8 70-130 Chlorodibromomethane 0.0211 0.0010 mg/Kgwet 0.0200 105 70-130 Chloroethane 0.0158 0.020 mg/Kg wet 0,0200 78.8 70-130 J Chloroform 0.0180 0.0040 mg/Kg wet 0.0200 90.1 70-130 Chloromethane 0.0138 0.010 mg/Kg wet 0.0200 69.0 * 70-130 L-04 Page 71 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD \nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198462 - SW-846 5035 LCS (B198462-BSI) Prepared & Analyzed: 03/08/18 2-Chlorotoluene 0.0190 0.0020 mg/Kg wet 0.0200 95.1 70-130 4-Chlorotoluene 0.0198 0.0020 mg/Kg wet 0.0200 98.8 70-130 1,2-Dibromo-3-chloropropane (DBCP) 0.0198 0.0020 mg/Kg wet 0.0200 98.9 70-130 1,2-Dibromoethane (EDB) 0.0202 0.0010 mg/Kg wet 0.0200 101 70-130 Dibromomethane 0.0204 0.0020 mg/Kg wet 0.0200 102 70-130 1,2-Dichlorobenzene 0.0191 0.0020 mg/Kg wet 0.0200 95.7 70-130 1,3-Dichlorobenzene 0.0194 0.0020 mg/Kg wet 0.0200 97.2 70-130 1,4-Dichlorobenzene 0.0186 0.0020 mg/Kg wet 0.0200 92.9 70-130 trans-1,4-Dichloro-2-butene 0.0212 0.0040 mg/Kg wet 0.0200 106 70-130 Dichlorodifluoromethane(Freon 12) 0.00922 0.020 mg/Kg wet 0.0200 46.1 40-160 J t 1,1-Dichloroethane 0.0190 0.0020 mg/Kg wet 0.0200 95.2 70-130 1,2-Dichloroethane 0.0192 0.0020 mg/Kg wet 0.0200 95.8 70-130 1,1-Dichloroethylene 0.0168 0.0040 mg/Kg wet 0.0200 83.9 70-130 cis-1,2-Dichloroethylene 0.0195 0.0020 mg/Kg wet 0.0200 97.6 70-130 trans-1,2-Dichloroethylene 0.0182 0.0020 mg/Kg wet 0.0200 91.1 70-130 1,2-Dichloropropane 0.0179 0.0020 mg/Kg wet 0.0200 89.3 70-130 1,3-Dichloropropane 0.0192 0.0010 mg/Kg wet 0.0200 96.2 70-130 2,2-Dichloropropane 0.0192 0.0020 mg/Kg wet 0.0200 95.9 70-130 1,1-Dichloropropene 0.0174 0.0020 mg/Kg wet 0.0200 87.0 70-130 cis-1,3-Dichloropropene 0.0183 0.0010 mg/Kg wet 0.0200 91.6 70-130 trans-1,3-Dichloropropene 0.0209 0.0010 mg/Kg wet 0.0200 104 70-130 Diethyl Ether 0.0204 0.020 mg/Kg wet 0.0200 102 70-130 Diisopropyl Ether (DIPE) 0.0195 0.0010 mg/Kg wet 0.0200 97.7 70-130 1,4-Dioxane 0.217 0.10 mg/Kg wet 0.200 108 40-160 t Ethanol 0.183 0.20 mg/Kgwet 0.200 91.4 40-160 J Ethylbenzene 0.0184 0.0020 mg/Kg wet 0.0200 92.0 70-130 Hexachlorobutadiene 0.0181 0.0020 mg/Kg wet 0.0200 90.3 70-160 2-Hexanone (MBK) 0.219 0.020 mg/Kg wet 0.200 110 70-160 t Isopropylbenzene (Cumene) 0.0213 0.0020 mg/Kg wet 0.0200 106 70-130 p-Isopropyltoluene(p-Cymene) 0.0189 0.0020 mg/Kg wet 0.0200 94.4 70-130 Methyl tert-Butyl Ether (MTBE) 0.0199 0.0040 mg/Kg wet 0.0200 99.4 70-130 Methylene Chloride 0.0197 0.020 mg/Kg wet 0.0200 98.5 40-160 J t 4-Methyl-2-pentanone (MIBK) 0.218 0.020 mg/Kg wet 0.200 109 70-160 t Naphthalene 0.0176 0.0040 mg/Kg wet 0.0200 88.1 40-130 t n-Propylbenzene 0.0193 0.0020 mg/Kg wet 0.0200 96.4 70-130 Styrene 0.0200 0.0020 mg/Kg wet 0.0200 99.8 70-130 1, 1, 1,2-Tetrachloroethane 0.0201 0.0020 mg/Kg wet 0.0200 100 70-130 1,1,2,2-Tetrachloroethane 0.0210 0.0010 mg/Kg wet 0.0200 105 70-130 Tetrachloroethylene 0.0195 0.0020 mg/Kg wet 0.0200 97.4 70-130 Tetrahydrofuran 0.0177 0.010 mg/Kg wet 0.0200 88.3 70-130 Toluene 0.0186 0.0020 mg/Kg wet 0.0200 93.1 70-130 1,2,3-Trichlorobenzene 0.0179 0.0020 mg/Kg wet 0.0200 89.6 70-130 1,2,4-Trichlorobenzene 0.0181 0.0020 mg/Kg wet 0.0200 90.5 70-130 1,3,5-Trichlorobenzene 0.0181 0.0020 mg/Kg wet 0.0200 90.3 70-130 1, 1, 1 -Trichloroethane 0.0177 0.0020 mg/Kg wet 0.0200 88.4 70-130 1,1,2-Trichloroethane 0.0204 0.0020 mg/Kg wet 0.0200 102 70-130 Trichloroethylene 0.0179 0.0020 mg/Kg wet 0.0200 89.3 70-130 Trichlorofluoromethane (Freon 11) 0.0167 0.010 mg/Kg wet 0.0200 83.4 70-130 1,2,3-Trichloropropane 0.0214 0.0020 mg/Kg wet 0.0200 107 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.0170 0.010 mg/Kg wet 0.0200 85.0 70-130 113) 1,2,4-Trimethylbenzene 0.0179 0.0020 mg/Kg wet 0,0200 89.5 70-130 Page 72 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD \nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198462 - SW-846 5035 LCS (B198462-BSI) Prepared & Analyzed: 03/08/18 1,3,5-Trimethylbenzene 0.0197 0.0020 mg/Kg wet 0.0200 98.5 70-130 Vinyl Chloride 0.0143 0.010 mg/Kgwet 0.0200 71.6 40-130 t m+p Xylene 0.0358 0.0040 mg/Kg wet 0.0400 89.6 70-130 o-Xylene 0.0189 0.0020 mg/Kg wet 0.0200 94.5 70-130 Surrogate: 1,2-Dichloroethane-d4 0.0492 mg/Kg wet 0.0500 98.4 70-130 Surrogate: Toluene-d8 0.0494 mg/Kg wet 0.0500 98.8 70-130 Surrogate: 4-Bromofluorobenzene 0.0518 mg/Kg wet 0.0500 104 70-130 LCS Dup (B198462-BS131) Prepared & Analyzed: 03/08/18 Acetone 0.184 0.10 mg/Kg wet 0.200 91.9 70-160 0.798 25 t Acrylonitrile 0.0210 0.0060 mg/Kg wet 0.0200 105 70-130 2.31 25 tert-Amyl Methyl Ether (TAME) 0.0189 0.0010 mg/Kg wet 0.0200 94.7 70-130 5.20 25 Benzene 0.0184 0.0020 mg/Kg wet 0.0200 91.8 70-130 3.21 25 Bromobenzene 0.0204 0.0020 mg/Kg wet 0.0200 102 70-130 5.54 25 Bromochloromethane 0.0226 0.0020 mg/Kg wet 0.0200 113 70-130 11.3 25 Bromodichloromethane 0.0196 0.0020 mg/Kg wet 0.0200 97.9 70-130 6.76 25 Bromoform 0.0216 0.0020 mg/Kg wet 0.0200 108 70-130 5.82 25 Bromomethane 0.00994 0.010 mg/Kg wet 0.0200 49.7 40-130 10.8 25 1 t 2-Butanone (MEK) 0.218 0.040 mg/Kg wet 0.200 109 70-160 1.41 25 t tert-Butyl Alcohol (TBA) 0.216 0.040 mg/Kg wet 0.200 108 40-130 7.77 25 t n-Butylbenzene 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 4.65 25 sec-Butylbenzene 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 6.98 25 tert-Butylbenzene 0.0187 0.0020 mg/Kg wet 0.0200 93.7 70-160 5.03 25 t tert-Butyl Ethyl Ether (TBEE) 0.0185 0.0010 mg/Kg wet 0.0200 92.7 70-130 2.73 25 Carbon Disulfide 0.0169 0.0060 mg/Kg wet 0.0200 84.5 70-130 0.474 25 Carbon Tetrachloride 0.0195 0.0020 mg/Kg wet 0.0200 97.7 70-130 1.24 25 Chlorobenzene 0.0200 0.0020 mg/Kg wet 0.0200 100 70-130 5.44 25 Chlorodibromomethane 0.0220 0.0010 mg/Kg wet 0.0200 110 70-130 4.09 25 Chloroethane 0.0160 0.020 mg/Kg wet 0.0200 80.0 70-130 1.51 25 1 Chloroform 0.0180 0.0040 mg/Kg wet 0.0200 90.0 70-130 0.111 25 Chloromethane 0.0140 0.010 mg/Kg wet 0.0200 69.8 * 70-130 1.15 25 L-04 2-Chlorotoluene 0.0191 0.0020 mg/Kg wet 0.0200 95.6 70-130 0.524 25 4-Chlorotoluene 0.0203 0.0020 mg/Kg wet 0.0200 101 70-130 2.50 25 1,2-Dibromo-3-chloropropane (DBCP) 0.0217 0.0020 mg/Kg wet 0.0200 108 70-130 9.07 25 1,2-Dibromoethane (EDB) 0.0211 0.0010 mg/Kg wet 0.0200 106 70-130 4.45 25 Dibromomethane 0.0215 0.0020 mg/Kg wet 0.0200 107 70-130 4.97 25 1,2-Dichlorobenzene 0.0207 0.0020 mg/Kg wet 0.0200 104 70-130 8.02 25 1,3-Dichlorobenzene 0.0207 0.0020 mg/Kg wet 0.0200 104 70-130 6.47 25 1,4-Dichlorobenzene 0.0196 0.0020 mg/Kg wet 0.0200 98.1 70-130 5.45 25 trans-1,4-Dichloro-2-butene 0.0225 0.0040 mg/Kg wet 0.0200 113 70-130 6.22 25 Dichlorodifluoromethane (Freon 12) 0.00936 0.020 mg/Kg wet 0.0200 46.8 40-160 1.51 25 1 t 1,1-Dichloroethane 0.0191 0.0020 mg/Kg wet 0.0200 95.6 70-130 0.419 25 1,2-Dichloroethane 0.0196 0.0020 mg/Kg wet 0.0200 98.0 70-130 2.27 25 1,1-Dichloroethylene 0.0175 0.0040 mg/Kg wet 0.0200 87.5 70-130 4.20 25 cis-1,2-Dichloroethylene 0.0198 0.0020 mg/Kg wet 0.0200 99.1 70-130 1.53 25 trans-1,2-Dichloroethylene 0.0188 0.0020 mg/Kg wet 0.0200 93.9 70-130 3.03 25 1,2-Dichloropropane 0.0191 0.0020 mg/Kg wet 0.0200 95.7 70-130 6.92 25 1,3-Dichloropropane 0.0207 0.0010 mg/Kg wet 0.0200 103 70-130 7.21 25 2,2-Dichloropropane 0.0195 0.0020 mg/Kg wet 0.0200 97.5 70-130 1.65 25 1,1-Dichloropropene 0.0185 0.0020 mg/Kg wet 0.0200 92.4 70-130 6.02 25 cis-1,3-Dichloropropene 0.0191 0.0010 mg/Kg wet 0.0200 95.7 70-130 4.38 25 trans-1,3-Dichloropropene 0.0215 0.0010 mg/Kg wet 0.0200 108 70-130 3.02 25 Page 73 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198462 - SW-846 5035 LCS Dup (B198462-BSD1) Prepared & Analyzed: 03/08/18 Diethyl Ether 0.0189 0.020 mg/Kg wet 0.0200 94.5 70-130 7.73 25 J Diisopropyl Ether (DIPE) 0.0197 0.0010 mg/Kg wet 0.0200 98.7 70-130 1.02 25 1,4-Dioxane 0.211 0.10 mg/Kg wet 0.200 106 40-160 2.48 50 t $ Ethanol 0.172 0.20 mg/Kg wet 0.200 86.1 40-160 5.95 25 J Ethylbenzene 0.0195 0.0020 mg/Kg wet 0.0200 97.3 70-130 5.60 25 Hexachlorobutadiene 0.0207 0.0020 mg/Kg wet 0.0200 104 70-160 13.7 25 2-Hexanone (MBK) 0.232 0.020 mg/Kg wet 0.200 116 70-160 5.68 25 f Isopropylbenzene (Cumene) 0.0216 0.0020 mg/Kg wet 0.0200 108 70-130 1.49 25 p-Isopropyltoluene (p-Cymene) 0.0197 0.0020 mg/Kg wet 0.0200 98.6 70-130 4.35 25 Methyl tert-Butyl Ether (MTBE) 0.0196 0.0040 mg/Kg wet 0.0200 97.8 70-130 1.62 25 Methylene Chloride 0.0190 0.020 mg/Kg wet 0.0200 95.1 40-160 3.51 25 J t 4-Methyl-2-pentanone (MIBK) 0.228 0.020 mg/Kg wet 0.200 114 70-160 4.62 25 t Naphthalene 0.0192 0.0040 mg/Kg wet 0.0200 96.1 40-130 8.69 25 f n-Propylbenzene 0.0197 0.0020 mg/Kg wet 0.0200 98.5 70-130 2.15 25 Styrene 0.0201 0.0020 mg/Kg wet 0.0200 101 70-130 0.898 25 1, 1, 1,2-Tetrachloroethane 0.0208 0.0020 mg/Kg wet 0.0200 104 70-130 3.72 25 1,1,2,2-Tetrachloroethane 0.0222 0.0010 mg/Kg wet 0.0200 ill 70-130 5.38 25 Tetrachloroethylene 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 5.69 25 Tetrahydrofuran 0.0207 0.010 mg/Kg wet 0.0200 104 70-130 15.9 25 Toluene 0.0194 0.0020 mg/Kg wet 0.0200 97.2 70-130 4.31 25 1,2,3-Trichlorobenzene 0.0194 0.0020 mg/Kg wet 0.0200 96.9 70-130 7.83 25 1,2,4-Trichlorobenzene 0.0199 0.0020 mg/Kg wet 0.0200 99.6 70-130 9.57 25 1,3,5-Trichlorobenzene 0.0198 0.0020 mg/Kg wet 0.0200 98.9 70-130 9.09 25 1, 1, 1 -Trichloroethane 0.0178 0.0020 mg/Kg wet 0.0200 89.1 70-130 0.789 25 1,1,2-Trichloroethane 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 0.780 25 Trichloroethylene 0.0183 0.0020 mg/Kg wet 0.0200 91.3 70-130 2.21 25 Trichlorofluoromethane (Freon 11) 0.0174 0.010 mg/Kg wet 0.0200 86.8 70-130 4.00 25 1,2,3-Trichloropropane 0.0232 0.0020 mg/Kg wet 0.0200 116 70-130 7.97 25 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.0168 0.010 mg/Kg wet 0.0200 83.8 70-130 1.42 25 113) 1,2,4-Trimethylbenzene 0.0191 0.0020 mg/Kg wet 0,0200 95.7 70-130 6.70 25 1,3,5-Trimethylbenzene 0.0201 0.0020 mg/Kg wet 0.0200 100 70-130 1.91 25 Vinyl Chloride 0.0145 0.010 mg/Kg wet 0.0200 72.5 40-130 1.25 25 t m+p Xylene 0.0394 0.0040 mg/Kg wet 0,0400 98.6 70-130 9.57 25 o-Xylene 0.0198 0.0020 mg/Kg wet 0.0200 99.2 70-130 4.85 25 Surrogate:l,2-Dichloroethane-d4 0.0497 mg/Kg wet 0.0500 99.4 70-130 Surrogate: Toluene-d8 0.0495 mg/Kg wet 0.0500 99.1 70-130 Surrogate:4-Bromofluorobenzene 0.0505 mg/Kg wet 0.0500 101 70-130 Page 74 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198559 - SW-846 3546 Blank (B198559-BLK1) Prepared: 03/09/18 Analyzed: 03/12/18 Acenaphthene ND 0.17 mg/Kg wet Acenaphthylene ND 0.17 mg/Kg wet Acetophenone ND 0.34 mg/Kg wet Aniline ND 0.34 mg/Kg wet Anthracene ND 0.17 mg/Kg wet Benzidine ND 0.66 mg/Kg wet Benzo(a)anthracene ND 0.17 mg/Kg wet Benzo(a)pyrene ND 0.17 mg/Kg wet Benzo(b)fluoranthene ND 0.17 mg/Kg wet Benzo(g,h,i)perylene ND 0.17 mg/Kg wet Benzo(b)fluoranthene ND 0.17 mg/Kg wet Benzoic Acid ND 1.0 mg/Kg wet Bis(2-chloroethoxy)methane ND 0.34 mg/Kg wet Bis(2-chloroethyl)ether ND 0.34 mg/Kg wet Bis(2-chloroisopropyl)ether ND 0.34 mg/Kg wet Bis(2-Ethylhexyl)phthalate ND 0.34 mg/Kg wet 4-Bromophenylphenylether ND 0.34 mg/Kg wet Butylbenzylphthalate ND 0.34 mg/Kg wet Carbazole ND 0.17 mg/Kg wet 4-Chloroaniline ND 0.66 mg/Kg wet 4-Chloro-3-methylphenol ND 0.66 mg/Kg wet 2-Chloronaphthalene ND 0.34 mg/Kg wet 2-Chlorophenol ND 0.34 mg/Kg wet 4-Chlorophenylphenylether ND 0.34 mg/Kg wet Chrysene ND 0.17 mg/Kg wet Dibenz(a,h)anthracene ND 0.17 mg/Kg wet Dibenzofuran ND 0.34 mg/Kg wet Di-n-butylphthalate ND 0.34 mg/Kg wet 1,2-Dichlorobenzene ND 0.34 mg/Kg wet 1,3-Dichlorobenzene ND 0.34 mg/Kg wet 1,4-Dichlorobenzene ND 0.34 mg/Kg wet 3,3-Dichlorobenzidine ND 0.17 mg/Kg wet 2,4-Dichlorophenol ND 0.34 mg/Kg wet Diethylphthalate ND 0.34 mg/Kg wet 2,4-Dimethylphenol ND 0.34 mg/Kg wet Dimethylphthalate ND 0.34 mg/Kg wet 4,6-Dinitro-2-methylphenol ND 0.34 mg/Kg wet 2,4-Dinitrophenol ND 0.66 mg/Kg wet 2,4-Dinitrotoluene ND 0.34 mg/Kg wet 2,6-Dinitrotoluene ND 0.34 mg/Kg wet Di-n-octylphthalate ND 0.34 mg/Kg wet 1,2-Diphenylhydrazine (as Azobenzene) ND 0.34 mg/Kg wet Fluoranthene ND 0.17 mg/Kg wet Fluorene ND 0.17 mg/Kg wet Hexachlorobenzene ND 0.34 mg/Kg wet Hexachlorobutadiene ND 0.34 mg/Kg wet Hexachlorocyclopentadiene ND 0.34 mg/Kg wet Hexachloroethane ND 0.34 mg/Kg wet Indeno(1,2,3-cd)pyrene ND 0.17 mg/Kg wet Isophorone ND 0.34 mg/Kg wet 1-Methylnaphthalene ND 0.17 mg/Kg wet 2-Methylnaphthalene ND 0.17 mg/Kg wet V-05 V-04, V-05 V-34 Page 75 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198559 - SW-846 3546 Blank (B198559-BLK1) Prepared: 03/09/18 Analyzed: 03/12/18 2-Methylphenol ND 0.34 mg/Kg wet 3/4-Methylphenol ND 0.34 mg/Kg wet Naphthalene ND 0.17 mg/Kg wet 2-Nitroaniline ND 0.34 mg/Kg wet V-20 3-Nitroaniline ND 0.34 mg/Kg wet 4-Nitroaniline ND 0.34 mg/Kg wet Nitrobenzene ND 0.34 mg/Kg wet 2-Nitrophenol ND 0.34 mg/Kg wet 4-Nitrophenol ND 0.66 mg/Kg wet V-20 N-Nitrosodimethylamine ND 0.34 mg/Kg wet V-20 N-Nitrosodiphenylamine ND 0.34 mg/Kg wet N-Nitrosodi-n-propylamine ND 0.34 mg/Kg wet Pentachloronitrobenzene ND 0.34 mg/Kg wet V-16 Pentachlorophenol ND 0.34 mg/Kg wet Phenanthrene ND 0.17 mg/Kg wet Phenol ND 0.34 mg/Kg wet Pyrene ND 0.17 mg/Kg wet Pyridine ND 0.34 mg/Kg wet V-05 1,2,4,5-Tetrachlorobenzene ND 0.34 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.34 mg/Kg wet 2,4,5-Trichlorophenol ND 0.34 mg/Kg wet 2,4,6-Trichlorophenol ND 0.34 mg/Kg wet Surrogate:2-Fluorophenol 3.71 mg/Kg wet 6.67 55.6 30-130 Surrogate: Phenol-d6 3.75 mg/Kg wet 6.67 56.2 30-130 Surrogate: Nitrobenzene-d5 2.55 mg/Kg wet 3.33 76.6 30-130 Surrogate:2-Fluorobiphenyl 2.24 mg/Kg wet 3.33 67.2 30-130 Surrogate: 2,4,6-Tribromophenol 4.60 mg/Kg wet 6.67 68.9 30-130 Surrogate: p-Terphenyl-dl4 2.26 mg/Kg wet 3.33 67.9 30-130 LCS (B198559-BS1) Prepared: 03/09/18 Analyzed: 03/12/18 Acenaphthene 0.963 0.17 mg/Kg wet 1.67 57.8 40-140 Acenaphthylene 0.997 0.17 mg/Kg wet 1.67 59.8 40-140 Acetophenone 0.897 0.34 mg/Kg wet 1.67 53.8 40-140 Aniline 0.676 0.34 mg/Kg wet 1.67 40.6 10-140 V-05 t Anthracene 0.917 0.17 mg/Kg wet 1.67 55.0 40-140 Benzidine 1.43 0.66 mg/Kg wet 1.67 86.1 40-140 V-04,V-05 Benzo(a)anthracene 0.990 0.17 mg/Kg wet 1.67 59.4 40-140 Benzo(a)pyrene 1.01 0.17 mg/Kg wet 1.67 60.7 40-140 Benzo(b)fluoranthene 0.964 0.17 mg/Kg wet 1.67 57.8 40-140 Benzo(g,h,i)perylene 1.04 0.17 mg/Kg wet 1.67 62.1 40-140 Benzo(k)fluoranthene 0.989 0.17 mg/Kg wet 1.67 59.3 40-140 Benzoic Acid 0.517 1.0 mg/Kg wet 1.67 31.0 30-130 1 Bis(2-chloroethoxy)methane 1.06 0.34 mg/Kg wet 1.67 63.3 40-140 Bis(2-chloroethyl)ether 0.829 0.34 mg/Kg wet 1.67 49.8 40-140 Bis(2-chloroisopropyl)ether 0.941 0.34 mg/Kg wet 1.67 56.5 40-140 Bis(2-Ethylhexyl)phthalate 1.23 0.34 mg/Kg wet 1.67 73.6 40-140 4-Bromophenylphenylether 1.01 0.34 mg/Kg wet 1.67 60.7 40-140 Butylbenzylphthalate 1.19 0.34 mg/Kg wet 1.67 71.4 40-140 Carbazole 0.961 0.17 mg/Kg wet 1.67 57.6 40-140 4-Chloroaniline 0.744 0.66 mg/Kg wet 1.67 44.6 10-140 V-34 4-Chloro-3-methylphenol 1.13 0.66 mg/Kg wet 1.67 67.7 30-130 2-Chloronaphthalene 0.872 0.34 mg/Kg wet 1.67 52.3 40-140 Page 76 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD walyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198559 - SW-846 3546 LCS (B198559-BSI) Prepared: 03/09/18 Analyzed:03/12/18 2-Chlorophenol 0.768 0.34 mg/Kg wet 1.67 46.1 30-130 4-Chlorophenylphenylether 1.05 0.34 mg/Kg wet 1.67 63.0 40-140 Chrysene 0.984 0.17 mg/Kg wet 1.67 59.0 40-140 Dibenz(a,h)anthracene 1.02 0.17 mg/Kg wet 1.67 61.3 40-140 Dibenzofuran 1.10 0.34 mg/Kg wet 1.67 65.9 40-140 Di-n-butylphthalate 1.10 0.34 mg/Kg wet 1.67 66.1 40-140 1,2-Dichlorobenzene 0.724 0.34 mg/Kg wet 1.67 43.4 40-140 1,3-Dichlorobenzene 0.709 0.34 mg/Kg wet 1.67 42.5 40-140 1,4-Dichlorobenzene 0.700 0.34 mg/Kg wet 1.67 42.0 40-140 3,3-Dichlorobenzidine 0.827 0.17 mg/Kg wet 1.67 49.6 20-140 2,4-Dichlorophenol 0.891 0.34 mg/Kg wet 1.67 53.5 30-130 Diethylphthalate 1.18 0.34 mg/Kg wet 1.67 70.9 40-140 2,4-Dimethylphenol 0.981 0.34 mg/Kg wet 1.67 58.9 30-130 Dimethylphthalate 1.06 0.34 mg/Kg wet 1.67 63.3 40-140 4,6-Dinitro-2-methylphenol 0.754 0.34 mg/Kg wet 1.67 45.2 30-130 2,4-Dinitrophenol 0.604 0.66 mg/Kg wet 1.67 36.2 30-130 2,4-Dinitrotoluene 0.986 0.34 mg/Kg wet 1.67 59.1 40-140 2,6-Dinitrotoluene 1.02 0.34 mg/Kg wet 1.67 61.1 40-140 Di-n-octylphthalate 1.20 0.34 mg/Kg wet 1.67 71.8 40-140 1,2-Diphenylhydrazine (as Azobenzene) 1.22 0.34 mg/Kg wet 1.67 73.3 40-140 Fluoranthene 0.949 0.17 mg/Kg wet 1.67 57.0 40-140 Fluorene 1.02 0.17 mg/Kg wet 1.67 61.1 40-140 Hexachlorobenzene 0.908 0.34 mg/Kg wet 1.67 54.5 40-140 Hexachlorobutadiene 0.966 0.34 mg/Kg wet 1.67 57.9 40-140 Hexachlorocyclopentadiene 0.815 0.34 mg/Kg wet 1.67 48.9 40-140 Hexachloroethane 0.813 0.34 mg/Kg wet 1.67 48.8 40-140 Indeno(1,2,3-cd)pyrene 1.01 0.17 mg/Kg wet 1.67 60.6 40-140 Isophorone 1.11 0.34 mg/Kg wet 1.67 66.8 40-140 1-Methylnaphthalene 0.934 0.17 mg/Kg wet 1.67 56.0 40-140 2-Methylnaphthalene 0.928 0.17 mg/Kg wet 1.67 55.7 40-140 2-Methylphenol 0.853 0.34 mg/Kg wet 1.67 51.2 30-130 3/4-Methylphenol 0.939 0.34 mg/Kg wet 1.67 56.3 30-130 Naphthalene 0.841 0.17 mg/Kg wet 1.67 50.5 40-140 2-Nitroaniline 1.32 0.34 mg/Kg wet 1.67 78.9 40-140 3-Nitroaniline 0.904 0.34 mg/Kg wet 1.67 54.3 30-140 4-Nitroaniline 0.989 0.34 mg/Kg wet 1.67 59.3 40-140 Nitrobenzene 1.04 0.34 mg/Kg wet 1.67 62.4 40-140 2-Nitrophenol 0.839 0.34 mg/Kg wet 1.67 50.3 30-130 4-Nitrophenol 1.23 0.66 mg/Kg wet 1.67 73.8 30-130 N-Nitrosodimethylarnme 0.972 0.34 mg/Kg wet 1.67 58.3 40-140 N-Nitrosodiphenylamine 1.26 0.34 mg/Kg wet 1.67 75.3 40-140 N-Nitrosodi-n-propylamine 0.982 0.34 mg/Kg wet 1.67 58.9 40-140 Pentachloronitrobenzene 0.954 0.34 mg/Kg wet 1.67 57.2 40-140 Pentachlorophenol 0.815 0.34 mg/Kg wet 1.67 48.9 30-130 Phenanthrene 0.920 0.17 mg/Kg wet 1.67 55.2 40-140 Phenol 0.785 0.34 mg/Kg wet 1.67 47.1 30-130 Pyrene 0.993 0.17 mg/Kg wet 1.67 59.6 40-140 Pyridine 0.491 0.34 mg/Kg wet 1.67 29.4 * 30-140 1,2,4,5-Tetrachlorobenzene 1.04 0.34 mg/Kg wet 1.67 62.5 40-140 1,2,4-Trichlorobenzene 0.855 0.34 mg/Kg wet 1.67 51.3 40-140 2,4,5-Trichlorophenol 1.10 0.34 mg/Kg wet 1.67 66.1 30-130 2,4,6-Trichlorophenol 1.09 0.34 mg/Kg wet 1.67 65.1 30-130 t J V-20 f V-20 V-20 V-16 L-07, V-05 Page 77 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198559 - SW-846 3546 LCS (B198559-BSI) Prepared: 03/09/18 Analyzed: 03/12/18 Surrogate:2-Fluorophenol 3.23 mg/Kg wet 6.67 48.4 30-130 Surrogate: Phenol-d6 3.44 mg/Kg wet 6.67 51.6 30-130 Surrogate: Nitrobenzene-d5 2.30 mg/Kg wet 3.33 68.9 30-130 Surrogate:2-Fluorobiphenyl 2.33 mg/Kg wet 3.33 69.8 30-130 Surrogate: 2,4,6-Tribromophenol 4.74 mg/Kg wet 6.67 71.1 30-130 Surrogate:p-Terphenyl-dl4 2.20 mg/Kg wet 3.33 66.1 30-130 LCS Dup (B198559-BSD1) Prepared: 03/09/18 Analyzed: 03/12/18 Acenaphthene 0.973 0.17 mg/Kg wet 1.67 58.4 40-140 0.998 30 Acenaphthylene 0.989 0.17 mg/Kg wet 1.67 59.3 40-140 0.873 30 Acetophenone 1.01 0.34 mg/Kg wet 1.67 60.7 40-140 12.0 30 Aniline 0.686 0.34 mg/Kg wet 1.67 41.2 10-140 1.52 50 V-05 f # Anthracene 0.949 0.17 mg/Kg wet 1.67 56.9 40-140 3.43 30 Benzidine 1.45 0.66 mg/Kg wet 1.67 87.1 40-140 1.18 30 V-04,V-05 Benzo(a)anthracene 1.02 0.17 mg/Kg wet 1.67 61.3 40-140 3.11 30 Benzo(a)pyrene 0.989 0.17 mg/Kg wet 1.67 59.4 40-140 2.30 30 Benzo(b)fluoranthene 1.00 0.17 mg/Kg wet 1.67 60.0 40-140 3.70 30 Benzo(g,h,i)perylene 1.06 0.17 mg/Kg wet 1.67 63.8 40-140 2.73 30 Benzo(k)fluoranthene 0.998 0.17 mg/Kg wet 1.67 59.9 40-140 0.906 30 Benzoic Acid 0.523 1.0 mg/Kg wet 1.67 31.4 30-130 1.22 50 J $ Bis(2-chloroethoxy)methane 1.13 0.34 mg/Kg wet 1.67 67.8 40-140 6.77 30 Bis(2-chloroethyl)ether 0.938 0.34 mg/Kg wet 1.67 56.3 40-140 12.3 30 Bis(2-chloroisopropyl)ether 1.05 0.34 mg/Kg wet 1.67 62.8 40-140 10.6 30 Bis(2-Ethylhexyl)phthalate 1.17 0.34 mg/Kg wet 1.67 70.2 40-140 4.65 30 4-Bromophenylphenylether 1.07 0.34 mg/Kg wet 1.67 64.2 40-140 5.57 30 Butylbenzylphthalate 1.17 0.34 mg/Kg wet 1.67 69.9 40-140 2.12 30 Carbazole 0.959 0.17 mg/Kg wet 1.67 57.6 40-140 0.139 30 4-Chloroaniline 0.656 0.66 mg/Kg wet 1.67 39.4 10-140 12.5 30 V-34, J f 4-Chloro-3-methylphenol 1.13 0.66 mg/Kg wet 1.67 67.7 30-130 0.0295 30 2-Chloronaphthalene 0.816 0.34 mg/Kg wet 1.67 48.9 40-140 6.68 30 2-Chorophenol 0.878 0.34 mg/Kg wet 1.67 52.7 30-130 13.4 30 4-Chlorophenylphenylether 1.09 0.34 mg/Kg wet 1.67 65.2 40-140 3.43 30 Chrysene 0.980 0.17 mg/Kg wet 1.67 58.8 40-140 0.407 30 Dibenz(a,h)anthracene 1.13 0.17 mg/Kg wet 1.67 67.7 40-140 9.98 30 Dibenzofuran 1.08 0.34 mg/Kg wet 1.67 64.8 40-140 1.62 30 Di-n-butylphthalate 1.11 0.34 mg/Kg wet 1.67 66.5 40-140 0.633 30 1,2-Dichlorobenzene 0.830 0.34 mg/Kg wet 1.67 49.8 40-140 13.7 30 1,3-Dichlorobenzene 0.812 0.34 mg/Kg wet 1.67 48.7 40-140 13.6 30 1,4-Dichlorobenzene 0.809 0.34 mg/Kg wet 1.67 48.6 40-140 14.4 30 3,3-Dichlorobenzidine 0.694 0.17 mg/Kg wet 1.67 41.7 20-140 17.4 50 f $ 2,4-Dichlorophenol 0.959 0.34 mg/Kg wet 1.67 57.5 30-130 7.35 30 Diethylphthalate 1.14 0.34 mg/Kg wet 1.67 68.3 40-140 3.65 30 2,4-Dimethylphenol 0.928 0.34 mg/Kg wet 1.67 55.7 30-130 5.55 30 Dimethylphthalate 1.05 0.34 mg/Kg wet 1.67 63.2 40-140 0.0948 30 4,6-Dinitro-2-methylphenol 0.773 0.34 mg/Kg wet 1.67 46.4 30-130 2.58 30 2,4-Dinitrophenol 0.574 0.66 mg/Kg wet 1.67 34.4 30-130 5.10 30 J 2,4-Dinitrotoluene 0.942 0.34 mg/Kg wet 1.67 56.5 40-140 4.53 30 2,6-Dinitrotoluene 1.01 0.34 mg/Kg wet 1.67 60.6 40-140 0.920 30 Di-n-octylphthalate 1.16 0.34 mg/Kg wet 1.67 69.9 40-140 2.71 30 1,2-Diphenylhydrazine (as Azobenzene) 1.23 0.34 mg/Kg wet 1.67 73.5 40-140 0.382 30 Fluoranthene 0.954 0.17 mg/Kg wet 1.67 57.2 40-140 0.490 30 Fluorene 1.00 0.17 mg/Kg wet 1.67 60.0 40-140 1.78 30 Page 78 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD .nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198559 - SW-846 3546 LCS Dup (B198559-BSD1) Prepared: 03/09/18 Analyzed: 03/12/18 Hexachlorobenzene 0.978 0.34 mg/Kg wet 1.67 58.7 40-140 7.49 30 Hexachlorobutadiene 1.08 0.34 mg/Kg wet 1.67 64.6 40-140 10.9 30 Hexachlorocyclopentadiene 0.858 0.34 mg/Kg wet 1.67 51.5 40-140 5.14 30 Hexachloroethane 0.947 0.34 mg/Kg wet 1.67 56.8 40-140 15.2 30 Indeno(1,2,3-cd)pyrene 1.08 0.17 mg/Kg wet 1.67 65.0 40-140 7.13 30 Isophorone 1.18 0.34 mg/Kg wet 1.67 70.9 40-140 6.04 30 I-Methylnaphthalene 0.972 0.17 mg/Kg wet 1.67 58.3 40-140 4.06 30 2-Methylnaphthalene 0.969 0.17 mg/Kg wet 1.67 58.2 40-140 4.39 30 2-Methylphenol 0.938 0.34 mg/Kg wet 1.67 56.3 30-130 9.49 30 3/4-Methylphenol 0.987 0.34 mg/Kg wet 1.67 59.2 30-130 5.02 30 Naphthalene 0.906 0.17 mg/Kg wet 1.67 54.3 40-140 7.40 30 2-Nitroanihne 1.25 0.34 mg/Kg wet 1.67 75.1 40-140 4.91 30 V-20 3-Nitroaniline 0.823 0.34 mg/Kg wet 1.67 49.4 30-140 9.38 30 f 4-Nitroaniline 0.952 0.34 mg/Kg wet 1.67 57.1 40-140 3.81 30 Nitrobenzene 1.12 0.34 mg/Kg wet 1.67 67.0 40-140 7.14 30 2-Nitrophenol 0.900 0.34 mg/Kg wet 1.67 54.0 30-130 7.06 30 4-Nitrophenol 1.25 0.66 mg/Kg wet 1.67 74.7 30-130 1.24 50 V-20 N-Nitrosodimethylamine 1.07 0.34 mg/Kg wet 1.67 64.4 40-140 9.97 30 V-20 N-Nitrosodiphenylamine 1.29 0.34 mg/Kg wet 1.67 77.4 40-140 2.65 30 N-Nitrosodi-n-propylamine 1.07 0.34 mg/Kg wet 1.67 64.2 40-140 8.67 30 Pentachloronitrobenzene 0.964 0.34 mg/Kg wet 1.67 57.9 40-140 1.08 30 V-16 Pentachlorophenol 0.819 0.34 mg/Kg wet 1.67 49.1 30-130 0.531 30 Phenanthrene 0.940 0.17 mg/Kg wet 1.67 56.4 40-140 2.22 30 Phenol 0.884 0.34 mg/Kg wet 1.67 53.0 30-130 11.9 30 Pyrene 1.00 0.17 mg/Kg wet 1.67 60.1 40-140 0.969 30 Pyridine 0.562 0.34 mg/Kg wet 1.67 33.7 30-140 13.6 30 V-05 t 1,2,4,5-Tetrachlorobenzene 1.08 0.34 mg/Kg wet 1.67 65.0 40-140 3.92 30 1,2,4-Trichlorobenzene 0.922 0.34 mg/Kg wet 1.67 55.3 40-140 7.58 30 2,4,5-Trichlorophenol 1.06 0.34 mg/Kg wet 1.67 63.5 30-130 4.14 30 2,4,6-Trichlorophenol 1.07 0.34 mg/Kg wet 1.67 64.2 30-130 1.39 30 Surrogate:2-Fluorophenol 3.75 mg/Kg wet 6.67 56.2 30-130 Surrogate: Phenol-d6 3.88 mg/Kg wet 6.67 58.2 30-130 Surrogate: Nitrobenzene-d5 2.46 mg/Kg wet 3.33 73.9 30-130 Surrogate: 2-Fluorobiphenyl 2.37 mg/Kg wet 3.33 71.2 30-130 Surrogate: 2,4,6-Tribromophenol 4.70 mg/Kg wet 6.67 70.6 30-130 Surrogate:p-Terphenyl-dl4 2.28 mg/Kg wet 3.33 68.3 30-130 Matrix Spike (B198559-MS1) Source: 18CO324-07 Prepared: 03/09/18 Analyzed: 03/12/18 Acenaphthene 1.08 0.21 mg/Kg dry 2.02 ND 53.1 40-140 Acenaphthylene 1.12 0.21 mg/Kg dry 2.02 ND 55.2 40-140 Acetophenone 1.12 0.41 mg/Kg dry 2.02 ND 55.2 40-140 Aniline 0.0506 0.41 mg/Kg dry 2.02 ND 2.50 * 40-140 MS-09, V-05, J Anthracene 1.10 0.21 mg/Kg dry 2.02 ND 54.2 40-140 Benzidine 0.0142 0.80 mg/Kg dry 2.02 ND 0.700 * 40-140 MS-09, V-04, V-05,J Benzo(a)anthracene 1.14 0.21 mg/Kg dry 2.02 ND 56.4 40-140 Benzo(a)pyrene 1.10 0.21 mg/Kg dry 2.02 ND 54.3 40-140 Benzo(b)fluoranthene 1.09 0.21 mg/Kg dry 2.02 ND 53.8 40-140 Benzo(g,h,i)perylene 1.20 0.21 mg/Kg dry 2.02 ND 59.2 40-140 Benzo(k)fluoranthene 1.14 0.21 mg/Kg dry 2.02 ND 56.4 40-140 Benzoic Acid 1.60 1.2 mg/Kg dry 2.02 0.451 56.9 40-140 Bis(2-chloroethoxy)methane 1.28 0.41 mg/Kg dry 2.02 ND 63.3 40-140 Bis(2-chloroethyl)ether 1.06 0.41 mg/Kg dry 2.02 ND 52.3 40-140 Page 79 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD walyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198559 - SW-846 3546 Matrix Spike (B198559-MSI) Source: 18CO324-07 Prepared: 03/09/18 Analyzed: 03/12/18 Bis(2-chloroisopropyl)ether 1.21 0.41 mg/Kg dry 2.02 ND 59.8 40-140 Bis(2-Ethylhexyl)phthalate 1.57 0.41 mg/Kg dry 2.02 ND 77.7 40-140 4-Bromophenylphenylether 1.10 0.41 mg/Kg dry 2.02 ND 54.3 40-140 Butylbenzylphthalate 1.55 0.41 mg/Kg dry 2.02 ND 76.6 40-140 Carbazole 1.20 0.21 mg/Kg dry 2.02 ND 59.1 40-140 4-Chloroaniline 0.210 0.80 mg/Kg dry 2.02 ND 10.4 * 40-140 MS-09, R-06, V-34, J 4-Chloro-3-methylphenol 1.37 0.80 mg/Kg dry 2.02 ND 67.6 30-130 2-Chloronaphthalene 0.896 0.41 mg/Kg dry 2.02 ND 44.3 40-140 2-Chlorophenol 0.977 0.41 mg/Kg dry 2.02 ND 48.3 30-130 4-Chlorophenylphenylether 1.30 0.41 mg/Kg dry 2.02 ND 64.1 40-140 Chrysene 1,14 0.21 mg/Kg dry 2.02 ND 56.4 40-140 Dibenz(a,h)anthracene 1.21 0.21 mg/Kg dry 2.02 ND 59.8 40-140 Dibenzofuran 1.19 0.41 mg/Kg dry 2.02 ND 59.0 40-140 Di-n-butylphthalate 1.34 0.41 mg/Kg dry 2.02 ND 66.2 40-140 1,2-Dichlorobenzene 0.883 0.41 mg/Kg dry 2.02 ND 43.6 40-140 1,3-Dichlorobenzene 0.832 0.41 mg/Kg dry 2.02 ND 41.1 40-140 1,4-Dichlorobenzene 0.838 0.41 mg/Kg dry 2.02 ND 41.4 40-140 3,3-Dichlorobenzidine 0.00648 0.21 mg/Kg dry 2.02 ND 0.320 * 40-140 MS-09, J 2,4-Dichlorophenol 1.08 0.41 mg/Kg dry 2.02 ND 53.3 30-130 Diethylphthalate 1,42 0.41 mg/Kg dry 2.02 ND 69.9 40-140 2,4-Dimethylphenol 1.07 0.41 mg/Kg dry 2.02 ND 53.1 30-130 Dimethylphthalate 1.17 0.41 mg/Kg dry 2.02 ND 57.7 40-140 4,6-Dinitro-2-methylphenol 0.843 0.41 mg/Kg dry 2.02 ND 41.7 30-130 2,4-Dinitrophenol 1.08 0.80 mg/Kg dry 2.02 ND 53.2 30-130 2,4-Dinitrotoluene 1.22 0.41 mg/Kg dry 2.02 ND 60.1 40-140 2,6-Dinitrotoluene 1.16 0.41 mg/Kg dry 2.02 ND 57.5 40-140 Di-n-octylphthalate 1.56 0.41 mg/Kg dry 2.02 ND 76.9 40-140 1,2-Diphenylhydrazine (as Azobenzene) 1.23 0.41 mg/Kg dry 2.02 ND 60.6 40-140 Fluoranthene 1.17 0.21 mg/Kg dry 2.02 ND 58.0 40-140 Fluorene 1.23 0.21 mg/Kg dry 2.02 ND 60.7 40-140 Hexachlorobenzene 1.07 0.41 mg/Kg dry 2.02 ND 52.7 40-140 Hexachlorobutadiene 1,28 0.41 mg/Kg dry 2.02 ND 63.3 40-140 Hexachlorocyclopentadiene 0.904 0.41 mg/Kg dry 2.02 ND 44.7 30-130 Hexachloroethane 0.994 0.41 mg/Kg dry 2.02 ND 49.1 40-140 Indeno(1,2,3-cd)pyrene 1,16 0.21 mg/Kg dry 2.02 ND 57.5 40-140 Isophorone 1.37 0.41 mg/Kg dry 2.02 ND 67.8 40-140 1-Methylnaphthalene 1.16 0.21 mg/Kg dry 2.02 ND 57.3 40-140 2-Methylnaphthalene 1,14 0.21 mg/Kg dry 2.02 ND 56.2 40-140 2-Methylphenol 1.04 0.41 mg/Kg dry 2.02 ND 51.2 30-130 3/4-Methylphenol 1.09 0.41 mg/Kg dry 2.02 ND 53.7 30-130 Naphthalene 1.06 0.21 mg/Kg dry 2.02 ND 52.2 40-140 2-Nitroaniline 1.34 0.41 mg/Kg dry 2.02 ND 66.4 40-140 V-20 3-Nitroaniline 0.724 0.41 mg/Kg dry 2.02 ND 35.8 * 40-140 MS-22 4-Nitroaniline 0.685 0.41 mg/Kg dry 2.02 ND 33.9 * 40-140 MS-09 Nitrobenzene 1.31 0.41 mg/Kg dry 2.02 ND 64.5 40-140 2-Nitrophenol 1.07 0.41 mg/Kg dry 2.02 ND 52.9 30-130 4-Nitrophenol 1.45 0.80 mg/Kg dry 2.02 ND 71.5 30-130 V-20 N-Nitrosodimethylamine 1.13 0.41 mg/Kg dry 2.02 ND 55.9 40-140 V-20 N-Nitrosodiphenylamine 1.34 0.41 mg/Kg dry 2.02 ND 66.2 40-140 N-Nitrosodi-n-propylamine 1,21 0.41 mg/Kg dry 2.02 ND 59.7 40-140 Pentachloronitrobenzene 1.18 0.41 mg/Kg dry 2.02 ND 58.3 40-140 V-16 Pentachlorophenol 1.10 0.41 mg/Kg dry 2.02 ND 54.5 30-130 Page 80 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD walyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198559 - SW-846 3546 Matrix Spike (B198559-MS1) Source: 18CO324-07 Prepared: 03/09/18 Analyzed: 03/12/18 Phenanthrene 1.07 0.21 mg/Kg dry 2.02 ND 52.9 40-140 Phenol 1.00 0.41 mg/Kg dry 2.02 ND 49.6 30-130 Pyrene 1.35 0.21 mg/Kg dry 2.02 ND 66.9 40-140 Pyridine 0.0158 0.41 mg/Kg dry 2.02 ND 0.780 * 40-140 MS-09, V-05, J 1,2,4,5-Tetrachlorobenzene 1.10 0.41 mg/Kg dry 2.02 ND 54.3 40-140 1,2,4-Trichlorobenzene 1.04 0.41 mg/Kg dry 2.02 ND 51.3 40-140 2,4,5-Trichlorophenol 1.12 0.41 mg/Kg dry 2.02 ND 55.4 30-130 2,4,6-Trichlorophenol 1.11 0.41 mg/Kg dry 2.02 ND 55.0 30-130 Surrogate:2-Fluorophenol 4.05 mg/Kg dry 8.10 50.1 30-130 Surrogate: Phenol-d6 4.26 mg/Kg dry 8.10 52.7 30-130 Surrogate: Nitrobenzene-d5 2.89 mg/Kg dry 4.05 71.3 30-130 Surrogate:2-Fluorobiphenyl 2.34 mg/Kg dry 4.05 57.8 30-130 Surrogate: 2,4,6-Tribromophenol 5.89 mg/Kg dry 8.10 72.8 30-130 Surrogate: p-Terphenyl-d14 3.00 mg/Kg dry 4.05 74.0 30-130 Matrix Spike Dup (B198559-MSD1) Source: 18CO324-07 Prepared: 03/09/18 Analyzed: 03/12/18 Acenaphthene 1.08 0.21 mg/Kg dry 2.02 ND 53.7 40-140 0.753 30 Acenaphthylene 1.12 0.21 mg/Kg dry 2.02 ND 55.7 40-140 0.533 30 Acetophenone 1.09 0.41 mg/Kg dry 2.02 ND 54.0 40-140 2.49 30 Aniline 0.0504 0.41 mg/Kg dry 2.02 ND 2.50 * 40-140 30 MS-09, V-05, J Anthracene 1.07 0.21 mg/Kg dry 2.02 ND 53.3 40-140 2.01 30 Benzidine 0.0291 0.80 mg/Kg dry 2.02 ND 1.44 * 40-140 30 MS-09, V-04, V-05,J Benzo(a)anthracene 1.15 0.21 mg/Kg dry 2.02 ND 57.1 40-140 0.865 30 Benzo(a)pyrene 1.17 0.21 mg/Kg dry 2.02 ND 58.1 40-140 6.54 30 Benzo(b)fluoranthene 1.11 0.21 mg/Kg dry 2.02 ND 55.1 40-140 2.20 30 Benzo(g,h,i)perylene 1.14 0.21 mg/Kg dry 2.02 ND 56.4 40-140 5.18 30 Benzo(k)fluoranthene 1.19 0.21 mg/Kg dry 2.02 ND 58.8 40-140 3.84 30 Benzoic Acid 1.67 1.2 mg/Kg dry 2.02 0.451 60.5 40-140 4.21 30 Bis(2-chloroethoxy)methane 1.28 0.41 mg/Kg dry 2.02 ND 63.5 40-140 0.0172 30 Bis(2-chloroethyl)ether 1.01 0.41 mg/Kg dry 2.02 ND 50.2 40-140 4.43 30 Bis(2-chloroisopropyl)ether 1.14 0.41 mg/Kg dry 2.02 ND 56.5 40-140 6.04 30 Bis(2-Ethylhexyl)phthalate 1.61 0.41 mg/Kg dry 2.02 ND 79.9 40-140 2.46 30 4-Bromophenylphenylether 1.17 0.41 mg/Kg dry 2.02 ND 57.8 40-140 5.77 30 Butylbenzylphthalate 1.48 0.41 mg/Kg dry 2.02 ND 78.2 40-140 1.81 30 Carbazole 1.18 0.21 mg/Kg dry 2.02 ND 58.3 40-140 1.73 30 4-Chloroaniline 0.154 0.80 mg/Kg dry 2.02 ND 7.62 * 40-140 30.8 * 30 MS-09, R-06, J 4-Chloro-3-methylphenol 1.29 0.80 mg/Kg dry 2.02 ND 64.1 30-130 5.59 30 2-Chloronaphthalene 0.897 0.41 mg/Kg dry 2.02 ND 44.5 40-140 0.118 30 2-Chorophenol 0.953 0.41 mg/Kg dry 2.02 ND 47.3 30-130 2.47 30 4-Chlorophenylphenylether 1.34 0.41 mg/Kg dry 2.02 ND 66.5 40-140 3.28 30 Chrysene 1.14 0.21 mg/Kg dry 2.02 ND 56.4 40-140 0.333 30 Dibenz(a,h)anthracene 1.15 0.21 mg/Kg dry 2.02 ND 56.9 40-140 5.27 30 Dibenzofuran 1,21 0.41 mg/Kg dry 2.02 ND 60.1 40-140 1.48 30 Di-n-butylphthalate 1.33 0.41 mg/Kg dry 2.02 ND 66.1 40-140 0.454 30 1,2-Dichlorobenzene 0.839 0.41 mg/Kg dry 2.02 ND 41.6 40-140 5.12 30 1,3-Dichlorobenzene 0.826 0.41 mg/Kg dry 2.02 ND 40.9 40-140 0.772 30 1,4-Dichlorobenzene 0.831 0.41 mg/Kg dry 2.02 ND 41.2 40-140 0.914 30 3,3-Dichlorobenzidine 0.00565 0.21 mg/Kg dry 2.02 ND 0.280 * 40-140 30 MS-09, J 2,4-Dichlorophenol 1.09 0.41 mg/Kg dry 2.02 ND 54.2 30-130 1.42 30 Diethylphthalate 1.38 0.41 mg/Kg dry 2.02 ND 68.2 40-140 2.82 30 2,4-Dimethylphenol 1.03 0.41 mg/Kg dry 2.02 ND 51.1 30-130 4.06 30 Dimethylphthalate 1.23 0.41 mg/Kg dry 2.02 ND 60.8 40-140 4.90 30 Page 81 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198559 - SW-846 3546 Matrix Spike Dup (B198559-MSD1) Source: 18CO324-07 Prepared: 03/09/18 Analyzed: 03/12/18 4,6-Dinitro-2-methylphenol 0.800 0.41 mg/Kg dry 2.02 ND 39.6 30-130 5.30 30 2,4-Dinitrophenol 1.14 0.80 mg/Kg dry 2.02 ND 56.7 30-130 6.00 30 2,4-Dinitrotoluene 1.38 0.41 mg/Kg dry 2.02 ND 68.3 40-140 12.6 30 2,6-Dinitrotoluene 1.20 0.41 mg/Kg dry 2.02 ND 59.6 40-140 3.25 30 Di-n-octylphthalate 1.56 0.41 mg/Kg dry 2.02 ND 77.3 40-140 0.290 30 1,2-Diphenylhydrazine (as Azobenzene) 1.10 0.41 mg/Kg dry 2.02 ND 54.7 40-140 10.6 30 Fluoranthene 1.14 0.21 mg/Kg dry 2.02 ND 56.3 40-140 3.34 30 Fluorene 1.28 0.21 mg/Kg dry 2.02 ND 63.4 40-140 3.99 30 Hexachlorobenzene 1.02 0.41 mg/Kg dry 2.02 ND 50.6 40-140 4.32 30 Hexachlorobutadiene 1.27 0.41 mg/Kg dry 2.02 ND 63.0 40-140 0.745 30 Hexachlorocyclopentadiene 0.822 0.41 mg/Kg dry 2.02 ND 40.7 30-130 9.56 30 Hexachloroethane 0.993 0.41 mg/Kg dry 2.02 ND 49.2 40-140 0.129 30 Indeno(1,2,3-cd)pyrene 1.19 0.21 mg/Kg dry 2.02 ND 58.8 40-140 1.80 30 Isophorone 1.33 0.41 mg/Kg dry 2.02 ND 65.8 40-140 3.33 30 1-Methylnaphthalene 1.12 0.21 mg/Kg dry 2.02 ND 55.7 40-140 3.24 30 2-Methylnaphthalene 1.10 0.21 mg/Kg dry 2.02 ND 54.5 40-140 3.40 30 2-Methylphenol 0.979 0.41 mg/Kg dry 2.02 ND 48.5 30-130 5.67 30 3/4-Methylphenol 1.06 0.41 mg/Kg dry 2.02 ND 52.3 30-130 2.94 30 Naphthalene 1.06 0.21 mg/Kg dry 2.02 ND 52.4 40-140 0.0114 30 2-Nitroaniline 1.43 0.41 mg/Kg dry 2.02 ND 70.8 40-140 6.09 30 V-20 3-Nitroaniline 0.831 0.41 mg/Kg dry 2.02 ND 41.2 40-140 13.8 30 4-Nitroaniline 0.600 0.41 mg/Kg dry 2.02 ND 29.7 * 40-140 13.3 30 MS-09 Nitrobenzene 1.27 0.41 mg/Kg dry 2.02 ND 63.0 40-140 2.65 30 2-Nitrophenol 1.06 0.41 mg/Kg dry 2.02 ND 52.3 30-130 1.40 30 4-Nitrophenol 1.63 0.80 mg/Kg dry 2.02 ND 80.6 30-130 11.6 30 V-20 N-Nitrosodimethylamine 1.11 0.41 mg/Kg dry 2.02 ND 55.2 40-140 1.45 30 V-20 N-Nitrosodiphenylamine 1.26 0.41 mg/Kg dry 2.02 ND 62.3 40-140 6.43 30 N-Nitrosodi-n-propylamine 1.15 0.41 mg/Kg dry 2.02 ND 57.0 40-140 5.10 30 Pentachloronitrobenzene 1.09 0.41 mg/Kg dry 2.02 ND 54.2 40-140 7.55 30 V-16 Pentachlorophenol 1.05 0.41 mg/Kg dry 2.02 ND 52.0 30-130 5.03 30 Phenanthrene 1.06 0.21 mg/Kg dry 2.02 ND 52.3 40-140 1.55 30 Phenol 0.964 0.41 mg/Kg dry 2.02 ND 47.8 30-130 4.03 30 Pyrene 1.42 0.21 mg/Kg dry 2.02 ND 70.5 40-140 4.91 30 Pyridine 0.00444 0.41 mg/Kg dry 2.02 ND 0.220 * 40-140 30 MS-09, V-05, J 1,2,4,5-Tetrachlorobenzene 1.10 0.41 mg/Kg dry 2.02 ND 54.5 40-140 0.145 30 1,2,4-Trichlorobenzene 1.07 0.41 mg/Kg dry 2.02 ND 53.0 40-140 3.00 30 2,4,5-Trichlorophenol 1.14 0.41 mg/Kg dry 2.02 ND 56.6 30-130 1.74 30 2,4,6-Trichlorophenol 1.15 0.41 mg/Kg dry 2.02 ND 57.0 30-130 3.35 30 Surrogate:2-Fluorophenol 3.94 mg/Kg dry 8.07 48.8 30-130 Surrogate: Phenol-d6 4.11 mg/Kg dry 8.07 51.0 30-130 Surrogate: Nitrobenzene-d5 2.90 mg/Kg dry 4.04 71.9 30-130 Surrogate:2-Fluorobiphenyl 2.35 mg/Kg dry 4.04 58.1 30-130 Surrogate: 2,4,6-Tribromophenol 6.00 mg/Kg dry 8.07 74.3 30-130 Surrogate: p-Terphenyl-d14 3.26 mg/Kg dry 4.04 80.8 30-130 Page 82 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198557 - SW-846 3546 Blank (B198557-BLK1) Prepared: 03/09/18 Analyzed: 03/11/18 Diesel Range Organics ND 8.3 mg/Kg wet Surrogate:o-Terphenyl LCS (B198557-BS1) 3.37 mg/Kg wet 3.33 101 Prepared: 03/09/18 Analyzed: 03/11/18 40-140 Diesel Range Organics 28.5 8.3 mg/Kg wet 33.3 85.4 40-140 Surrogate:o-Terphenyl LCS Dup (B198557-BSD1) 3.40 mg/Kg wet 3.33 102 Prepared: 03/09/18 Analyzed: 03/11/18 40-140 Diesel Range Organics 27.4 8.3 mg/Kg wet 33.3 82.3 40-140 3.75 Surrogate:o-Terphenyl Batch B198651 - SW-846 5035/5030B 3.27 mg/Kg wet 3.33 98.1 40-140 Blank (B198651-BLKl) Prepared & Analyzed: 03/12/18 Gasoline Range Organics (GRO) ND 1.0 mg/Kg wet Surrogate: 1-Chloro-3-fluorobenzene LCS (B198651-BSI) 16.4 µg/L 15.0 109 Prepared & Analyzed: 03/12/18 70-130 Gasoline Range Organics (GRO) 0.250 0.010 mg/Kg wet 0.250 100 80-120 Surrogate: 1-Chloro-3-fluorobenzene LCS Dup (B198651-BSD1) 19.2 µg/L 15.0 128 Prepared & Analyzed: 03/12/18 70-130 Gasoline Range Organics (GRO) 0.263 0.010 mg/Kg wet 0.250 105 80-120 4.84 30 Surrogate: 1-Chloro-3-fluorobenzene 16.1 µg/L 15.0 107 70-130 Page 83 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198433 - % Solids Blank (B198433-BLK1) Prepared: 03/08/18 Analyzed: 03/09/18 % Solids Blank (B198433-BLK2) 0.00 % Wt Prepared: 03/08/18 Analyzed: 03/09/18 % Solids Blank (B198433-BLK3) 0.00 % Wt Prepared: 03/08/18 Analyzed: 03/09/18 % Solids Blank (B198433-BLK4) 0.00 % Wt Prepared: 03/08/18 Analyzed: 03/09/18 % Solids Blank (B198433-BLK5) 0.00 % Wt Prepared: 03/08/18 Analyzed: 03/09/18 % Solids Duplicate (B198433-DUPB) 0.00 Source: 18CO324-01 % Wt Prepared & Analyzed: 03/08/18 % Solids 86.3 % Wt 87.0 0.865 20 Page 84 of 94 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL TCLP - Metals Analyses - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B198629 - SW-846 3010A Blank (B198629-BLK1) Prepared & Analyzed: 03/12/18 Arsenic ND 0.010 mg/L Barium ND 0.050 mg/L Cadmium ND 0.0040 mg/L Chromium ND 0.010 mg/L Lead ND 0.010 mg/L Selenium ND 0.050 mg/L Silver ND 0.0050 mg/L LCS (B198629-BS1) Prepared & Analyzed: 03/12/18 Arsenic 0.557 0.010 mg/L 0.500 ill 80-120 Barium 0.513 0.050 mg/L 0.500 103 80-120 Cadmium 0.543 0.0040 mg/L 0.500 109 80-120 Chromium 0.508 0.010 mg/L 0.500 102 80-120 Lead 0.486 0.010 mg/L 0.500 97.3 80-120 Selenium 0.635 0.050 mg/L 0.500 127 * 80-120 L-02 Silver 0.552 0.0050 mg/L 0.500 110 80-120 LCS Dup (B198629-BSD1) Prepared & Analyzed: 03/12/18 Arsenic 0.567 0.010 mg/L 0.500 113 80-120 1.90 20 Barium 0.523 0.050 mg/L 0.500 105 80-120 1.97 20 Cadmium 0.555 0.0040 mg/L 0.500 111 80-120 2.15 20 Chromium 0.518 0.010 mg/L 0.500 104 80-120 1.90 20 Lead 0.494 0.010 mg/L 0.500 98.8 80-120 1.55 20 Selenium 0.665 0.050 mg/L 0.500 133 * 80-120 4.55 20 L-02 Silver 0.543 0.0050 mg/L 0.500 109 80-120 1.70 20 Batch B198633 - SW-846 7470A Prep Blank (B198633-BLK1) Prepared & Analyzed: 03/12/18 Mercury 0.000045 0.00010 mg/L J LCS (B198633-BS1) Prepared & Analyzed: 03/12/18 Mercury 0.00197 0.00010 mg/L 0.00200 98.5 80-120 LCS Dup (B198633-BSD1) Prepared & Analyzed: 03/12/18 Mercury 0.00199 0.00010 mg/L 0.00200 99.3 80-120 0.779 20 Page 85 of 94 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-02 Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is on the high side. L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side. L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. MS-09 Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample matrix effects that lead to a low bias for reported result or non -homogeneous sample aliquots cannot be eliminated. MS-22 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is within method specified criteria. R-06 Matrix spike duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result for this compound in this sample. V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method specified criteria. Reported result is estimated. V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. V-16 Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. Page 86 of 94 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 6010C-D in Water Arsenic NY,CT,NC,ME,NH,VA Barium NY,CT,ME,NC,NH,VA Cadmium NY,CT,ME,NC,NH,VA Chromium NY,CT,ME,NC,NH,VA Lead NY,CT,ME,NC,NH,VA Selenium CT,ME,NCNH,NY,VA Silver CT,ME,NCNH,NY,VA SW-846 7470A in Water Mercury CT,ME,NCNH,NY,VA SW-846 801 SC in Soil Gasoline Range Organics (GRO) NY,VA,NH NC Diesel Range Organics NY,VA,NH,NC SW-846 8260B in Soil Acetone NC Acrylonitrile NC tert-Amyl Methyl Ether (TAME) NC Benzene NC Bromobenzene NC Bromochloromethane NC Bromodichloromethane NC Bromoform NC Bromomethane NC 2-Butanone (MEK) NC tert-Butyl Alcohol (TBA) NC n-Butylbenzene NC sec-Butylbenzene NC tert-Butylbenzene NC tert-Butyl Ethyl Ether (TBEE) NC Carbon Disulfide NC Carbon Tetrachloride NC Chlorobenzene NC Chlorodibromomethane NC Chloroethane NC Chloroform NC Chloromethane NC 2-Chlorotoluene NC 4-Chlorotoluene NC 1,2-Dibromo-3-chloropropane (DBCP) NC 1,2-Dibromoethane (EDB) NC Dibromomethane NC 1,2-Dichlorobenzene NC 1,3-Dichlorobenzene NC 1,4-Dichlorobenzene NC trans-1,4-Dichloro-2-butene NC Dichlorodifluoromethane (Freon 12) NC 1,1-Dichloroethane NC Page 87 of 94 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte SW-846 8260B in Soil 1,2-Dichloroethane 1,1-Dichloroethylene cis-1,2-Dichloroethylene trans- l,2-Dichloro ethylene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis- 1,3 -Dichloropropene trans- l,3-Dichloropropene Diethyl Ether Diisopropyl Ether (DIPE) 1,4-Dioxane Ethylbenzene Hexachlorobutadiene 2-Hexanone (MBK) Isopropylbenzene (Cumene) p-Isopropyltoluene (p-Cymene) Methyl tart -Butyl Ether (MTBE) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Tetrahydrofuran Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trichlorobenzene 1, 1, 1 -Trichloroethane 1, 1,2 -Trichloroethane Trichloroethylene Trichlorofluoromethane (Freon 11) 1,2,3-Trichloropropane 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113) 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Chloride m+p Xylene o-Xylene SW-846 8270D in Soil Acenaphthene Acenaphthylene Certifications NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA Page 88 of 94 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Soil Acetophenone NY,NH,ME,NC,VA Aniline NY,NH,ME,NC,VA Anthracene CT,NY,NH,ME,NC,VA Benzidine CT,NY,NH,ME,NC,VA Benzo(a)anthracene CT,NY,NH,ME,NC,VA Benzo(a)pyrene CT,NY,NH,ME,NC,VA Benzo(b)fluoranthene CT,NY,NH,ME,NC,VA Benzo(g,h,i)perylene CT,NY,NH,ME,NC,VA Benzo(k)fluoranthene CT,NY,NH,ME,NC,VA Benzoic Acid NY,NH,ME,NC,VA Bis(2-chloroethoxy)methane CT,NY,NH,ME,NC,VA Bis(2-chloroethyl)ether CT,NY,NH,ME,NC,VA Bis(2-chloroisopropyl)ether CT,NY,NH,ME,NC,VA Bis(2-Ethylhexyl)phthalate CT,NY,NH,ME,NC,VA 4-Bromophenylphenylether CT,NY,NH,ME,NC,VA Butylbenzylphthalate CT,NY,NH,ME,NC,VA Carbazole NC 4-Chloroaniline CT,NY,NH,ME,NC,VA 4-Chloro-3-methylphenol CT,NY,NH,ME,NC,VA 2-Chloronaphthalene CT,NY,NH,NC,VA 2-Chlorophenol CT,NY,NH,ME,NC,VA 4-Chlorophenylphenylether CT,NY,NH,ME,NC,VA Chrysene CT,NY,NH,ME,NC,VA Dibenz(a,h)anthracene CT,NY NH,ME,NC,VA Dibenzofuran CT,NY,NH,ME,NC,VA Di-n-butylphthalate CT,NY,NH,ME,NC,VA 1,2-Dichlorobenzene NY,NH,ME,NC,VA 1,3-Dichlorobenzene NY,NH,ME,NC,VA 1,4-Dichlorobenzene NY,NH,ME,NC,VA 3,3-Dichlorobenzidine CT,NY,NH,ME,NC,VA 2,4-Dichlorophenol CT,NY,NH,ME,NC,VA Diethylphthalate CT,NY,NH,ME,NC,VA 2,4-Dimethylphenol CT,NY,NH,ME,NC,VA Dimethylphthalate CT,NY,NH,ME,NC,VA 4,6-Dinitro-2-methylphenol CT,NY,NH,ME,NC,VA 2,4-Dinitrophenol CT,NY,NH,ME,NC,VA 2,4-Dinitrotoluene CT,NY,NH,ME,NC,VA 2,6-Dinitrotoluene CT,NY,NH,ME,NC,VA Di-n-octylphthalate CT,NY,NH,ME,NC,VA 1,2-Diphenylhydrazine (as Azobenzene) NY,NH,ME,NC,VA Fluoranthene CT,NY,NH,ME,NC,VA Fluorene NY,NH,ME,NC,VA Hexachlorobenzene CT,NY,NH,ME,NC,VA Hexachlorobutadiene CT,NY,NH,ME,NC,VA Hexachlorocyclopentadiene CT,NY,NH,ME,NC,VA Hexachloroethane CT,NY,NH,ME,NC,VA Indeno(1,2,3-cd)pyrene CT,NY,NH,ME,NC,VA Page 89 of 94 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Soil Isophorone CT,NY,NH,ME,NC,VA 1-Methylnaphthalene NC 2-Methylnaphthalene CT,NY,NH,ME,NC,VA 2-Methylphenol CT,NY,NH,ME,NC,VA 3/4-Methylphenol CT,NY,NH,ME,NC,VA Naphthalene CT,NY,NH,ME,NC,VA 2-Nitmaniline CT,NY,NH,ME,NC,VA 3-Nitmaniline CT,NY,NH,ME,NC,VA 4-Nitroaniline CT,NY,NH,ME,NC,VA Nitrobenzene CT,NY,NH,ME,NC,VA 2-Nitrophenol CT,NY,NH,ME,NC,VA 4-Nitrophenol CT,NY,NH,ME,NC,VA N-Nitrosodimethylamine CT,NY,NH,ME,NC,VA N-Nitrosodiphenylamine CT,NY,NH,ME,NC,VA N-Nitrosodi-n-propylamine CT,NY,NH,ME,NC,VA Pentachloronitrobenzene NY,NC Pentachlorophenol CT,NY,NH,ME,NC,VA Phenanthrene CT,NY,NH,ME,NC,VA Phenol CT,NY,NH,ME,NC,VA Pyrene CT,NY,NH,ME,NC,VA Pyridine CT,NY,NH,ME,NC,VA 1,2,4,5-Tetrachlorobenzene NY,NC 1,2,4-Trichlorobenzene CT,NY,NH,ME,NC,VA 2,4,5-Trichlorophenol CT,NY,NH,ME,NC,VA 2,4,6-Trichlorophenol CT,NY,NH,ME,NC,VA 2-Fluorophenol NC The CON -TEST Environmental Laboratory operates under the following certifications and accreditation: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2018 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2018 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2018 NC North Carolina Div. of Water Quality 652 12/31/2018 NJ New Jersey DEP MA007 NELAP 06/30/2018 FL Florida Department of Health E871027 NELAP 06/30/2018 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2018 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2018 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2018 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2018 NC-DW North Carolina Department of Health 25703 07/31/2018 Page 90 of 94 Table of Contents L b � � An OL O o c i 7_ EEE @ S w c3 n C1iO ? m LnN = :m � Nllc Q .11 I ila v�aiOc w=--iznc 4°�= o ¢C 7m > .c�nil-0 cJ N -�0 a11 I Ifj £ [i 13 ii _j . .-.. . 0�VN toO'mO ... 2 Ln m X OQ Q 0 CL cn >.cn 0} El ❑z MMUMEMEMEN ■m■■■. ®®®m®m M®®m®® ❑D T M r El EDD Y �• O m O J E ro S M jM vJ v N p C7 or N p � it) U c C W W F U {AI�I�IL�I T IZ C L= C p I E___9 El D G N C7 to � � ✓ C� Lr U W "-1 d c a Pape 91 of 94 Table of Contents At CO m Q -0 o;c �rnv > -� w �� au co(1111 ` ry_ r.-. . .... _�o.i.t '©L3f NtCUS •963 �US 7,-E . a A'O- 4�. Q-m� 7_a t rL'i—t O O O r VV> V7.8 OQ U. .. h% iro F it 0 .....>a I7 II - it .. �R1.`CCaI�i€ GQOz7 bin>sn-O'0O -.. ❑ ❑p b C O a E C c � _ I O C X s— M V lu au Y ❑ ❑ ❑ G C r,7 D U 0 0 rA a S a p 2 j E U C E E U tit•-•�',�.,: :J E EC- U 2 V C T ^ Pape 92 of 94 Table of Contents 3/7/2018 Track your package or shipment with FedEx Tracking Signed far'by: J.DEIATRAS Travel History Date/Time Activity Location - 3l07r2018 -Wednesday 10:09 am Delivered aril wNcr.+EA❑ow.M", 8:28 am On FedEx vehicle for delivery cr 8:15 am At Incal FedEx fadlity r:a,❑saR LOCXs cT 6:24 am At destination sort facility snsT GRti ,NBY cT 4.43 am Departed FedEx location "J°'AN^'D1'S "` 1 07 am Arrived at FedEx location p {lIAhF OLIS,is - 3/06/2018 - Tuesday 4:22 pm Picked up Ra Lice.Nr 3:02 pm Shipment information sent to FedEx Shipment Facts Tracking Number 771734496441 Service FedEx Priority Overnight Weight 36-6 €bs 1 16.6 kgs Dimensions 24x14x14 in. Delivered To Shipping/Receiving Total pieces 1 Total shipment weight 36.6 Ibs 116.6 kgs Terms Third Party Shipper reference 80 Packaging Your Packaging Special handling Deliver Weekday, Addiliona! Standard 3ID7l2018 by 14:30 am section Handling Surcharge transit OUR COMPANY About FedEx Our Portfolio Investor Relations Careers M. FedEx Blog Corporate Responsibility Newsroom Contact Us MORE FROM FEDEX FedEx Compatible Developer Resource Center FedEx Cross Border Page 93 of 94 hops://www.fedex,comlappslfedextrackl?action=track&tracknumbers=771734496441 &locale=en_US&cntry_code=us Table of Contents Client — Received By How were the samples received? -....... Date In Cooler No Cooler Direct from Sampling Time C On Ice i No Ice Ambient Melted Ice Were samples within - By Gun # i Actual Temp -- Temperature? 2-6'C By lank # Actual Temp - Was Custody Seal Intact? " Were Samples Tampered with? L AA - Was COC Relinquished ? -T Does Chan Agree With Samples? Are there broken/leaking/loose caps on any samples? Is COC in ink/ Legible? i Were samples received within holding time? i Did COC include all Client i Analysis Sampler Name pertinent Information? Project ID's Collection Dates/Times Are Sample labels filled out and legible? i Are there Lab to Filters? Who was notified? Are there Rushes? Who was notified? Are there Short Holds? — Who was notified? Is there enough Volume? Is there Headspace where applicable? MS/MSD? , Proper Media/Containers Used? Is splitting samples required? Were trip blanks received? On COC? Do all samples have the proper pH? Acid Base Unp- 1 Liter Amb. 1 Liter Plastic 16 oz Amb. HCL- -` 5: t 51-,J mL Amb. mil ' 500 mL Plastic —t 8o (Clear Meoh- 1 250 mL Amb. 250 mL Plastic -i 4oz GbZlear Bisulfate- 6�- Col./Bacteria Flashpoint 2oz Am bk0ba> DI- Other Plastic Other Glass Encore Thiosulfate- SOC Kit Plastic Bag Frozen: Sulfuric- I Perchlorate Zir)lock Unp- 1 Liter Amb. 1 Liter Plastic 16 oz Amb. HCL- 500 mL Amb. 500 mL Plastic 8oz Amb/Clear Meoh- 250 mL Amb. 250 mL Plastic 4oz Amb/Clear Bisulfate- Col./Bacteria Flashpoint 2oz Amb/Clear DI- Other Plastic Other Glass Encore Thiosulfate- SOC Kit Plastic Ba Frozen: Sulfuric- Perchlorate Ziolock Attachment V ,r I IF AV 609A Piner Road, Suite 115 ff kTc Wilmington, North Carolina 28409 ENVIRONMENTAL • GEOTECHNICAL (919) 871-0999 BUILDING SCIENCES - MATERIALS TESTING Project No. DATE: PM: BEACONAST 03/14/2018 Maureen Jackson O Location of Backfill for AST-3 Excavation Witherspoon Roses Property 3312 Watkins Road Durham, Durham County, North Carolina