22031_K-Town Furniture Orphan Waste Oil UST Removal_(BPN 22031-18-013)_20190225

Via Email

February 25, 2019

NC DEQ – Brownfields Section
1646 Mail Service Center
Raleigh, NC 27699-1646

Attn: Mr. Bill Schmithorst, PG
Re: Orphan Waste Oil UST Removal
Former K-Town Furniture
Proposed Ballpark and Entertainment Venue
Kannapolis, North Carolina Brownfields Project No. 22031-18-013
H&H Job No. KAN-012

Dear Bill:

On behalf of the City of Kannapolis, Hart & Hickman, PC (H&H) is providing this letter report to
document the discovery and removal of an orphan underground storage tank (UST) at the former
K-Town Furniture (Proposed Ballpark and Entertainment Venue) site located in Kannapolis, North
Carolina (Brownfields Project No. 22031-18-013). The orphan UST was discovered in the
southwest portion of the site on October 5, 2018 during excavation activities associated with the
baseball stadium construction. A site location map is included as Figure 1, and a site map is
included as Figure 2.

On October 5, 2018, H&H was contacted and mobilized to the site to observe the conditions of the
UST and soil in the vicinity of the UST. The UST was approximately 550-gallons in capacity and
contained waste oil. Based on the location of the orphan UST in close proximity to the former gas
station (134 Oak Avenue) and the former auto repair shops (136-138 Oak Avenue), it is likely the
UST was installed for waste oil storage during former automotive sales and service operations
which were conducted on the site between the 1940s and 1970. In accordance with the DEQ
approved Environmental Management Plan (EMP), the DEQ Brownfields Section was notified of
Mr. Bill Schmithorst, PG
February 25, 2019
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the orphan UST discovery via a telephone voice message on October 5, 2018. Upon initial
discovery, H&H worked with the City’s grading contractor to secure the UST area and excavate a
small amount (less than a five cubic yards) of stained soil which was observed in the vicinity of
the tank. In accordance with the approved EMP, the excavated soil was stockpiled on-site in an
area adjacent to the UST location. The stockpiled soil was place on and covered with plastic
sheeting.

On October 8, 2018, approximately 230 gallons of residual liquid was pumped from the UST using
a vacuum truck and the interior of the tank was washed and re-vacuumed. The residual liquid was
transported to EVO Corporation in Winston-Salem, North Carolina for proper off-site
disposal/recycling. Following removal of the residual liquid, the tank was excavated from the
ground using an excavator and transported by truck to Triad Metal Recycling in Yadkinville, North
Carolina for proper off-site disposal/recycling. Copies of the certificate of disposal and non-
hazardous materials manifest for the waste oil and a copy of the certificate of disposal for the tank
are included as Appendix A.

Following removal, the UST was inspected for holes, corrosion, and pitting. Minor pitting and
corrosion were observed on the bottom of the tank. No product or vent piping was encountered
during removal of the UST.

Following removal of the tank, soil in the vicinity of the orphan UST was visually observed for
the presence of staining and odors and field screened using a calibrated photoionization detector
(PID). Excavation of the soil in the vicinity and beneath the tank continued for another
approximate 2 ft below the bottom of the tank until the desired construction grade elevation was
achieved. Suspected impacted soil from this area was segregated and placed in the previously
established soil stockpile. At the conclusion of the field screening and excavation activities, the
soil stockpile was estimated to contain approximately 5 to 10 cubic yards of soil.

Mr. Bill Schmithorst, PG
February 25, 2019
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Following completion of grading activities in the UST area, H&H collected one “at grade” soil
sample (labelled Base 20181008) directly beneath the former UST location and one composite soil
sample (labelled SP 20181008) from the soil stockpile. The approximate locations of the UST and
soil stockpile are depicted on Figure 3. The UST and soil stockpile locations were estimated using
a hand-held global positioning system unit.

The collected soil samples were analyzed for volatile organic compounds (VOCs) by EPA Method
8260B, semi-VOCs (SVOCs) by EPA Method 8270D, Resource Conservation Recovery Act
(RCRA) metals by EPA Methods 6020/7471, and hexavalent chromium by EPA Method 7199.
Soil samples were placed directly into laboratory-supplied glassware, labeled, and placed on ice
in a laboratory-supplied cooler. The cooler was delivered under standard chain of custody
protocols to Pace Analytical (Pace), a North Carolina certified laboratory.

A tabular summary of the soil sample analytical results is presented in Table 1. Copies of the
laboratory analytical reports and chain of custody records are provided in Appendix B. The
laboratory analytical results were compared to the DEQ Inactive Hazardous Sites Branch (IHSB)
Residential Use, Industrial/Commercial Use, and Protection of Groundwater Preliminary Soil
Remedial Goals (PSRGs) dated February 2018. In addition to the PSRGs, metals results were
compared to published concentrations for naturally occurring metals in North Carolina soil and
available site-specific background metals concentrations from other environmental assessments
that have been conducted on nearby properties. Specifically, metals results were compared to
documented concentrations of natural occurring metals on the adjacent former Pillowtex Plant 1
Brownfields Property located to the north of the site and the former Pillowtex/Fieldcrest Cannon
Wastewater Treatment Plant (WWTP) site located approximately 1 mile northwest of the site.

As shown in Table 1, only low concentrations of metals were detected in soil sample
Base 20181008 collected approximately 2 ft below the bottom of the former UST. Of these
detections, only the detected arsenic concentration of 2.66 mg/kg exceeds the DEQ IHSB
Residential Use PSRG of 0.68 mg/kg.
Mr. Bill Schmithorst, PG
February 25, 2019
Page 4
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Low concentrations of VOCs, SVOCs, and several metals were detected in composite soil sample
SP 20181008 collected from the soil stockpile. Of these detections, only the detected
concentrations of 1-methylnaphthalene and arsenic exceed a PSRG. The detected concentration
of 1-methylnaphthalene (0.570 mg/kg) exceeds its Protection of Groundwater PSRG of
0.11 mg/kg, and the detected concentration of arsenic (2.32 mg/kg) exceeds its Residential Use
PSRG of 0.68 mg/kg.

Typical background concentrations of arsenic in North Carolina soils range from 1 to 18 mg/kg,
with a mean concentration of 4.8 mg/kg (Dragun, J. and Chekiri, K. 2005 1). Based on a review
of available site-specific background arsenic data from the adjacent former Pillowtex Plant 1
Brownfields Property and the nearby former Pillowtex/Fieldcrest Cannon WWTP site, typical
background concentrations of arsenic in soils in the site area range from less than 1 to 12.1 mg/kg.
The detected concentrations of arsenic in the soil samples collected beneath the former UST and
the soil stockpile are within published and/or documented nearby area background ranges for
naturally occurring arsenic and are not believed to be anthropogenic.

Based upon the relatively small volume of soil and lack of significant impact, the City requested
that DEQ allow the stockpiled soil associated with the orphan UST to be transported off-site and
placed in the former sediment basin on the adjacent former Pillowtex Plant 1 Brownfields Property
for use as fill. In email correspondence dated October 24, 2018, DEQ approved the request to
transport the soil stockpile associated with the orphan UST to the former sediment basin on the
adjacent Pillowtex Plant 1 Brownfields Property.

On October 25, 2018, approximately 5 to 10 cubic yards of soil stockpiled soil were transported
to the former Pillowtex Plant 1 Brownfields Property for placement in the former sediment basin.
The location of the former sediment basin located on the former Pillowtex Plant 1 Brownfields
Property is depicted on Figure 4.

1 Dragun, J. and Chekiri, K. 2005. Elements in North American Soils.
Mr. Bill Schmithorst, PG
February 25, 2019
Page 5
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Should you have any questions or need additional information, please do not hesitate to contact us
at [phone].

Very truly yours,
Hart & Hickman, PC

Shannon Cottrill
Project Manager
Matt Bramblett, PE
Principal
Attachments

Table 1 (Page 1 of 1)
Summary of UST Soil Characterization Analytical Data
Proposed Baseball Stadium
Kannapolis, North Carolina
H&H Job No. KAN-012
Sample ID Base 20181008 SP 20181008
Date 10/8/2018 10/8/2018
Depth (ft)2 ft below UST Soil Stockpile
VOCs (8260B)
sec-Butylbenzene <0.0016 0.0020 J 4.1 1,600 23,000 ----Ethylbenzene <0.0019 0.0018 J 13 6.1 27 ----p-Isopropyltoluene <0.0017 0.0073 1.24 --------
Naphthalene <0.0012 0.0057 0.39 4.1 18 ----
n-Propylbenzene <0.0017 0.0065 2.6 780 5100 ----
1,2,4-Trimethylbenzene <0.0021 0.0551 12 63 370 ----
1,3,5-Trimethylbenzene <0.0019 0.0219 11 56 320 ----
Xylene (Total)<0.0037 0.0149 9.9 120 530
m&p-Xylene <0.0037 0.0090 9.8 120 500 ----
o-Xylene <0.0020 0.0059 9.8 140 590 ----
SVOCs (8270D)Dibenzofuran <0.0712 0.0766 J 10 15 210 ----bis(2-Ethylhexyl)phthalate <0.119 0.357 J 14 39 160 ----
1-Methylnaphthalene <0.113 0.570 0.11 18 73 ----
2-Methylnaphthalene <0.0936 0.923 3.1 48 600 ----
Naphthalene <0.107 0.357 J 0.39 4.1 18 ----
Phenanthrene <0.0725 0.172 J 134.0 NS NS
RCRA Metals (6020/7471/7199)Range Average
Arsenic 2.66 (5)2.32 (5)5.8 0.68 3.0 1 - 18 4.8
Barium 159 155 580 3,100 47,000 50 - 1,000 356
Cadmium 0.675 <0.0965 3.0 14 200 1 - 10 (4)4.3 (4)
Hexavalent Chromium <0.337 <0.307 3.8 0.31 6.5 ----
Trivalent Chromium 11.3 11.0 360,000 23,000 350,000 ----
Lead 22.9 30.7 270 400 (3)800 (3)ND - 50 16
Mercury 0.0199 J 0.0403 1.0 2.3 9.7 0.03 - 0.52 0.121
Selenium 1.59 1.20 2.1 78 1,200 <0.1 - 0.8 0.42
Silver <0.205 <0.187 3.4 78 1,200 NS NS
Notes:Concentrations are reported in milligrams per kilogram (mg/kg)Laboratory analytical method is shown in parenthesesFor VOCs and SVOCs, only those compounds detected in at least one sample shown above(1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (February 2018)(2) Range and mean values of background metals for North Carolina soils obtained from Elements in North American Soils by Dragun and Chekiri, 2005
(3) Values shown are based on the Environmental Protection Agency (EPA) Regional Screening Levels (RSLs) (November 2018)
(4) Southeastern U.S.A. values are shown, as North Carolina background levels are not specified
(5) Concentration detected is within published background ranges for naturally occurring metals in soil and is not believed to be anthropogenicBold indicates concentration exceeds the Protection of Groundwater PSRG
Underline indicates concentration exceeds the Residential Use PSRG
UST = Underground Storage Tank; VOCs = volatile organic compounds; SVOCs = Semi-VOCs; RCRA = Resource Conservation Recovery Act
-- = Not Applicable; ND = Not Detected; NS = Not Specified
Because J flags were requested, less than concentrations are reported to the laboratory method detection limit
DEQ IHSB
Protection of
Groundwater
PSRGs (1)
DEQ IHSB Residential
Use PSRGs (1)
DEQ IHSB
Industrial /
Commercial
PSRGs (1)
North Carolina
Background Levels (2)
S:\AAA-Master Projects\City of Kannapolis - KAN\KAN-012 Infrastructure, Streetscape, & Baseball Projects\Orphan Waste Oil UST\Tables\Data Table.xlsx
2/19/2019
Table 1 (Page 1 of 1)Hart & Hickman, PC
SITE LOCATION MAP
PROPOSED BALLPARK & ENTERTAINMENT VENUE
OAK AVENUE & W. A STREETKANNAPOLIS, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
11-9-18 0
1KAN-012
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
7.5 MINUTE SERIES (TOPOGRAPHIC)
KANNAPOLIS, NC 1996
SITE
TITLE
PROJECT
REVISION NO. 0
JOB NO. KAN-012
DATE: 11-9-18
FIGURE NO. 2
PROPOSED BALLPARK & ENTERTAINMENT VENUE
OAK AVENUE & W. A STREET
KANNAPOLIS, NORTH CAROLINA
SITE MAP
LEGEND
SITE PROPERTY BOUNDARY
PAD-MOUNTED TRANSFORMER
POLE-MOUNTED TRANSFORMER
ELEVATOR
BOILER ROOM
DUMPSTER
APPROXIMATE AREA SUBJECT TO
EXISTING BROWNFIELDS
AGREEMENT FOR NC RESEARCH
CAMPUS (INCLUDING WATER VAULT)
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
WATSO
N

C
R
I
C
K

D
R
I
V
E
UNDEVELOPED
VACANT
(200 & 206 OAK AVENUE MALL DRIVE)
OAK AVENUE MALL
(318-358 OAK AVENUE MALL DRIVE)
CAROLINAS HEALTHCARE SYSTEM
(201 DALE EARNHARDT BOULEVARD)
FORMER PURITAN/ BOB'S LAUNDRY &
DRY CLEANERS (DEMOLISHED)
(311 WEST A STREET)
VACANT OFFICES
(201 & 203 OAK AVENUE MALL DRIVE)VACANTCROSSFIT
(134 WEST AVENUE)
VIRGINIA'S
(213 WEST A STREET)
ROWAN CABARRUS COMMUNITY COLLEGE
(120 WEST AVENUE)VACANTCAROLINA INTERIORS
(115 OAK AVENUE)
FORMER STAR CLEANERS
(108 WEST AVENUE)
FORMER GOODYEAR
SERVICE GARAGE
(100 WEST AVENUE)
NORTH CAROLINA RESEARCH CAMPUS
(FORMER FIELDCREST CANNON PLANT #1)
(2014 N. MAIN STREET)
LA
U
R
E
A
T
E

W
A
Y
CHES
T
N
U
T

A
V
E
N
U
EWELLNESS WAYOAK AVENUEWEST AVENUES. MAIN STREETW. A
STREET
W.
1
S
T

S
T
R
E
E
T
VACANT RETAIL
(215 W. A. STREET)
W.
B

S
T
R
E
E
T
55-GALLON DRUM OF
WASTE COMPRESSOR OIL
VACANT COMMERCIAL BUILDING (DEMOLISHED)
(134-144 OAK AVENUE)
SOIL STOCKPILES
FORMER WATER VAULT
FORMER WRENN'S CLEANERS
(136 WEST AVENUE)
FORMER GAS STATION W/ THREE USTs
(134 OAK AVENUE)
FORMER AUTO REPAIR SHOPS (DEMOLISHED)
(136-138 OAK AVENUE)
FORMER WASTEWATER
TREATMENT LINES
FORMER DYE
PROCESS AREA
FORMER FIELDCREST CANNON PLANT
NO. 1 BLEACHING BUILDING
FORMER GAS STATION
(400 W. A STREET)
W.
A

S
T
R
E
E
T
S:\AAA-Master Projects\City of Kannapolis - KAN\KAN-012 Infrastructure, Streetscape, & Baseball Projects\Phase II ESA\Figures\Site Map.dwg, FIG 2, 11/9/2018 11:02:28 AM, erichardson
WELLNESS WAY
TMW-5
TMW-7
B-4
SB-15
SB-13
SB-19
SB-20
SB-23
SB-24
SB-25SB-26
FORMER GAS STATION
(400 W. A STREET)
W.
B

S
T
R
E
E
TOAK AVENUEFORMER WRENN'S CLEANERS
(136 WEST AVENUE)
SB-3
SB-4/
TMW-2
SB-5
SB-7
SB-8/
TMW-4
SB-9
SB-10
B-1
B-2
SB-11
B-5B-3
SB-1/
TMW-1
SB-2
SB-6/
TMW-3
TMW-6
SB-17
SB-16
SB-14
SB-18
SB-18A
SB-21
SB-22
SB-12
FORMER AUTO REPAIR SHOPS (DEMOLISHED)
(136-138 OAK AVENUE)
FORMER WATER VAULT
FORMER STAR CLEANERS
(108 WEST AVENUE)
FORMER PURITAN/ BOB'S LAUNDRY &
DRY CLEANERS (DEMOLISHED)
(311 WEST A STREET)
W.
A

S
T
R
E
E
T
CHES
T
N
U
T

A
V
E
N
U
E
LA
U
R
E
A
T
E

W
A
Y
BURIED TIMBER PILINGS W. A
STREET
SB-29
SB-32
SB-28
SB-31
SB-27
SB-30BASE
20181008
SB-21
SB-22
REVISION NO. 0
JOB NO. KAN-012
DATE: 2-18-19
FIGURE NO. 3
PROPOSED BALLPARK & ENTERTAINMENT VENUE
OAK AVENUE & W. A STREET
KANNAPOLIS, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
TEMPORARY MONITORING WELL
LOCATION
TEMPORARY MONITORING WELL/
SOIL BORING LOCATION
SOIL BORING LOCATION
APPROXIMATE AREA SUBJECT TO
EXISTING BROWNFIELDS
AGREEMENT FOR NC RESEARCH
CAMPUS (INCLUDING WATER VAULT)
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
FORMER GAS STATION
(400 W. A STREET)
FORMER AUTO REPAIR SHOPS (DEMOLISHED)
(136-138 OAK AVENUE)
FORMER GAS STATION
W/ THREE USTs
(134 OAK AVENUE)
FORMER STAR CLEANERS
(108 WEST AVENUE)
FORMER PURITAN/ BOB'S LAUNDRY &
DRY CLEANERS (DEMOLISHED)
(311 WEST A STREET)
W.
A

S
T
R
E
E
T
W.
B

S
T
R
E
E
TOAK AVENUEWELLNESS WAY
CHES
T
N
U
T

A
V
E
N
U
E
LA
U
R
E
A
T
E

W
A
Y
FORMER GOODYEAR
SERVICE GARAGE
(100 WEST AVENUE)
BURIED TIMBER PILINGS
FORMER WRENN'S CLEANERS
(136 WEST AVENUE)
FORMER 550-GALLON
WASTE OIL UST
FORMER UST SOIL
STOCKPILE
S:\AAA-Master Projects\City of Kannapolis - KAN\KAN-012 Infrastructure, Streetscape, & Baseball Projects\Phase II ESA\Figures\Sample Location Map.dwg, FIG 1 UST, 2/18/2019 2:16:25 PM, amckenzie
JOB NO. KAN-012
REVISION NO. 0DATE: 2-18-19
FIGURE NO. 4
LEGEND
NCRC PROPERTY BOUNDARY
PROPOSED BALLPARK & ENTERTAINMENT VENUE OAK AVENUE & W. A STREET
KANNAPOLIS, NORTH CAROLINA
FILL PLACEMENT AREA MAP
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
APPROXIMATE FORMER
SEDIMENT BASIN
(FILL PLACEMENT AREA)
NORTH CAROLINA RESEARCH CAMPUS
LOOP R
O
A
D

N
O
R
T
HCHURCH AVENUEPOPLAR AVENUEN WALNUT STREETBIOTECHNOLOGY LANEOAK CIR
C
L
E
CHARLES BABBAGE LANE AVENUE
FOREST
NOTE:
IMAGERY TAKEN FROM GOOGLE EARTH
(2018)
ROWAN CABARRUS COMMUNITY
COLLEGE AT NCRC
(399 BIOTECHNOLOGY LANE)
DATA CHAMBERS
(465 CHARLES BABBAGE LANE)S:\AAA-Master Projects\City of Kannapolis - KAN\KAN-012 Infrastructure, Streetscape, & Baseball Projects\Phase II ESA\Figures\Sample Location Map.dwg, 8.5x11 Size Portrait, 2/18/2019 2:15:47 PM, amckenzie

Appendix A
Copies of Certificate of Disposal and Non-Hazardous Materials Manifest (Waste Oil) and Certificate of Disposal (Tank)

Appendix B Laboratory Analytical Reports
#=CL#
October 18, 2018
LIMS USE: FR - SHANNON COTTRILL
LIMS OBJECT ID: 92402530
92402530
Project:
Pace Project No.:
RE:
Mr. Shannon Cottrill
Hart & Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
Kannapolis, NC Site (KAN-012)
Dear Mr. Cottrill:
Enclosed are the analytical results for sample(s) received by the laboratory on October 08, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
Per client request, report revised 10/18/18 to include MDL and J-Flags.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
cc: Nick Hotzelt, Hart & Hickman
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 39
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Lab ID Sample ID Matrix Date Collected Date Received
92402530001 Base-20181008 Solid 10/08/18 13:00 10/08/18 14:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92402530001 Base-20181008 EPA 8270D 74 PASI-CBPJ
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Sample: Base-20181008 Lab ID: 92402530001 Collected: 10/08/18 13:00 Received: 10/08/18 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 10/15/18 12:49 83-32-910/11/18 18:43435 100 1
Acenaphthylene ND ug/kg 10/15/18 12:49 208-96-810/11/18 18:43435 103 1
Aniline ND ug/kg 10/15/18 12:49 62-53-310/11/18 18:43435 117 1
Anthracene ND ug/kg 10/15/18 12:49 120-12-710/11/18 18:43435 97.6 1
Benzo(a)anthracene ND ug/kg 10/15/18 12:49 56-55-310/11/18 18:43435 80.4 1
Benzo(a)pyrene ND ug/kg 10/15/18 12:49 50-32-810/11/18 18:43435 83.1 1
Benzo(b)fluoranthene ND ug/kg 10/15/18 12:49 205-99-210/11/18 18:43435 75.2 1
Benzo(g,h,i)perylene ND ug/kg 10/15/18 12:49 191-24-210/11/18 18:43435 111 1
Benzo(k)fluoranthene ND ug/kg 10/15/18 12:49 207-08-910/11/18 18:43435 85.7 1
Benzoic Acid ND ug/kg 10/15/18 12:49 65-85-010/11/18 18:432180 79.1 1
Benzyl alcohol ND ug/kg 10/15/18 12:49 100-51-610/11/18 18:43870 87.0 1
4-Bromophenylphenyl ether ND ug/kg 10/15/18 12:49 101-55-310/11/18 18:43435 79.1 1
Butylbenzylphthalate ND ug/kg 10/15/18 12:49 85-68-710/11/18 18:43435 92.3 1
4-Chloro-3-methylphenol ND ug/kg 10/15/18 12:49 59-50-710/11/18 18:43870 89.7 1
4-Chloroaniline ND ug/kg 10/15/18 12:49 106-47-810/11/18 18:432180 121 1
bis(2-Chloroethoxy)methane ND ug/kg 10/15/18 12:49 111-91-110/11/18 18:43435 102 1
bis(2-Chloroethyl) ether ND ug/kg 10/15/18 12:49 111-44-410/11/18 18:43435 111 1
2-Chloronaphthalene ND ug/kg 10/15/18 12:49 91-58-710/11/18 18:43435 85.7 1
2-Chlorophenol ND ug/kg 10/15/18 12:49 95-57-810/11/18 18:43435 119 1
4-Chlorophenylphenyl ether ND ug/kg 10/15/18 12:49 7005-72-310/11/18 18:43435 89.7 1
Chrysene ND ug/kg 10/15/18 12:49 218-01-910/11/18 18:43435 58.0 1
Dibenz(a,h)anthracene ND ug/kg 10/15/18 12:49 53-70-310/11/18 18:43435 92.3 1
Dibenzofuran ND ug/kg 10/15/18 12:49 132-64-910/11/18 18:43435 71.2 1
1,2-Dichlorobenzene ND ug/kg 10/15/18 12:49 95-50-110/11/18 18:43435 116 1
1,3-Dichlorobenzene ND ug/kg 10/15/18 12:49 541-73-110/11/18 18:43435 98.9 1
1,4-Dichlorobenzene ND ug/kg 10/15/18 12:49 106-46-710/11/18 18:43435 123 1
3,3'-Dichlorobenzidine ND ug/kg 10/15/18 12:49 91-94-110/11/18 18:432180 95.0 1
2,4-Dichlorophenol ND ug/kg 10/15/18 12:49 120-83-210/11/18 18:43435 95.0 1
Diethylphthalate ND ug/kg 10/15/18 12:49 84-66-210/11/18 18:43435 67.3 1
2,4-Dimethylphenol ND ug/kg 10/15/18 12:49 105-67-910/11/18 18:43435 171 1
Dimethylphthalate ND ug/kg 10/15/18 12:49 131-11-310/11/18 18:43435 88.4 1
Di-n-butylphthalate ND ug/kg 10/15/18 12:49 84-74-210/11/18 18:43435 71.2 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/15/18 12:49 534-52-110/11/18 18:43870 87.0 1
2,4-Dinitrophenol ND ug/kg 10/15/18 12:49 51-28-510/11/18 18:432180 71.2 1
2,4-Dinitrotoluene ND ug/kg 10/15/18 12:49 121-14-210/11/18 18:43435 81.8 1
2,6-Dinitrotoluene ND ug/kg 10/15/18 12:49 606-20-210/11/18 18:43435 91.0 1
Di-n-octylphthalate ND ug/kg 10/15/18 12:49 117-84-010/11/18 18:43435 91.0 1
bis(2-Ethylhexyl)phthalate ND ug/kg 10/15/18 12:49 117-81-710/11/18 18:43435 119 1
Fluoranthene ND ug/kg 10/15/18 12:49 206-44-010/11/18 18:43435 63.3 1
Fluorene ND ug/kg 10/15/18 12:49 86-73-710/11/18 18:43435 89.7 1
Hexachloro-1,3-butadiene ND ug/kg 10/15/18 12:49 87-68-310/11/18 18:43435 75.2 1
Hexachlorobenzene ND ug/kg 10/15/18 12:49 118-74-110/11/18 18:43435 55.4 1
Hexachlorocyclopentadiene ND ug/kg 10/15/18 12:49 77-47-410/11/18 18:43435 80.4 1
Hexachloroethane ND ug/kg 10/15/18 12:49 67-72-110/11/18 18:43435 115 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/15/18 12:49 193-39-510/11/18 18:43435 89.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Sample: Base-20181008 Lab ID: 92402530001 Collected: 10/08/18 13:00 Received: 10/08/18 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 10/15/18 12:49 78-59-110/11/18 18:43435 97.6 1
1-Methylnaphthalene ND ug/kg 10/15/18 12:49 90-12-010/11/18 18:43435 113 1
2-Methylnaphthalene ND ug/kg 10/15/18 12:49 91-57-610/11/18 18:43435 93.6 1
2-Methylphenol(o-Cresol)ND ug/kg 10/15/18 12:49 95-48-710/11/18 18:43435 132 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/15/18 12:49 15831-10-410/11/18 18:43435 171 1
Naphthalene ND ug/kg 10/15/18 12:49 91-20-310/11/18 18:43435 107 1
2-Nitroaniline ND ug/kg 10/15/18 12:49 88-74-410/11/18 18:432180 135 1
3-Nitroaniline ND ug/kg 10/15/18 12:49 99-09-210/11/18 18:432180 119 1
4-Nitroaniline ND ug/kg 10/15/18 12:49 100-01-610/11/18 18:43870 123 1
Nitrobenzene ND ug/kg 10/15/18 12:49 98-95-310/11/18 18:43435 119 1
2-Nitrophenol ND ug/kg 10/15/18 12:49 88-75-510/11/18 18:43435 106 1
4-Nitrophenol ND ug/kg 10/15/18 12:49 100-02-710/11/18 18:432180 77.8 1
N-Nitrosodimethylamine ND ug/kg 10/15/18 12:49 62-75-910/11/18 18:43435 141 1
N-Nitroso-di-n-propylamine ND ug/kg 10/15/18 12:49 621-64-710/11/18 18:43435 83.1 1
N-Nitrosodiphenylamine ND ug/kg 10/15/18 12:49 86-30-610/11/18 18:43435 129 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/15/18 12:49 108-60-1 L110/11/18 18:43435 116 1
Pentachlorophenol ND ug/kg 10/15/18 12:49 87-86-510/11/18 18:432180 79.1 1
Phenanthrene ND ug/kg 10/15/18 12:49 85-01-810/11/18 18:43435 72.5 1
Phenol ND ug/kg 10/15/18 12:49 108-95-210/11/18 18:43435 131 1
Pyrene ND ug/kg 10/15/18 12:49 129-00-010/11/18 18:43435 73.9 1
1,2,4-Trichlorobenzene ND ug/kg 10/15/18 12:49 120-82-110/11/18 18:43435 84.4 1
2,4,5-Trichlorophenol ND ug/kg 10/15/18 12:49 95-95-410/11/18 18:43435 135 1
2,4,6-Trichlorophenol ND ug/kg 10/15/18 12:49 88-06-210/11/18 18:43435 96.3 1
Surrogates
Nitrobenzene-d5 (S)41 %10/15/18 12:49 4165-60-010/11/18 18:4323-110 1
2-Fluorobiphenyl (S)40 %10/15/18 12:49 321-60-810/11/18 18:4330-110 1
Terphenyl-d14 (S)72 %10/15/18 12:49 1718-51-010/11/18 18:4328-110 1
Phenol-d6 (S)40 %10/15/18 12:49 13127-88-310/11/18 18:4322-110 1
2-Fluorophenol (S)38 %10/15/18 12:49 367-12-410/11/18 18:4313-110 1
2,4,6-Tribromophenol (S)52 %10/15/18 12:49 118-79-610/11/18 18:4327-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone ND ug/kg 10/11/18 15:15 67-64-110/11/18 09:15103 10.3 1
Benzene ND ug/kg 10/11/18 15:15 71-43-210/11/18 09:155.1 1.6 1
Bromobenzene ND ug/kg 10/11/18 15:15 108-86-110/11/18 09:155.1 2.1 1
Bromochloromethane ND ug/kg 10/11/18 15:15 74-97-510/11/18 09:155.1 1.7 1
Bromodichloromethane ND ug/kg 10/11/18 15:15 75-27-410/11/18 09:155.1 2.0 1
Bromoform ND ug/kg 10/11/18 15:15 75-25-210/11/18 09:155.1 2.4 1
Bromomethane ND ug/kg 10/11/18 15:15 74-83-910/11/18 09:1510.3 2.6 1
2-Butanone (MEK)ND ug/kg 10/11/18 15:15 78-93-310/11/18 09:15103 3.0 1
n-Butylbenzene ND ug/kg 10/11/18 15:15 104-51-810/11/18 09:155.1 1.9 1
sec-Butylbenzene ND ug/kg 10/11/18 15:15 135-98-810/11/18 09:155.1 1.6 1
tert-Butylbenzene ND ug/kg 10/11/18 15:15 98-06-610/11/18 09:155.1 2.1 1
Carbon tetrachloride ND ug/kg 10/11/18 15:15 56-23-510/11/18 09:155.1 2.7 1
Chlorobenzene ND ug/kg 10/11/18 15:15 108-90-710/11/18 09:155.1 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Sample: Base-20181008 Lab ID: 92402530001 Collected: 10/08/18 13:00 Received: 10/08/18 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 10/11/18 15:15 75-00-310/11/18 09:1510.3 2.5 1
Chloroform ND ug/kg 10/11/18 15:15 67-66-310/11/18 09:155.1 1.6 1
Chloromethane ND ug/kg 10/11/18 15:15 74-87-310/11/18 09:1510.3 2.5 1
2-Chlorotoluene ND ug/kg 10/11/18 15:15 95-49-810/11/18 09:155.1 1.7 1
4-Chlorotoluene ND ug/kg 10/11/18 15:15 106-43-410/11/18 09:155.1 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/11/18 15:15 96-12-810/11/18 09:155.1 3.7 1
Dibromochloromethane ND ug/kg 10/11/18 15:15 124-48-110/11/18 09:155.1 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 10/11/18 15:15 106-93-410/11/18 09:155.1 1.9 1
Dibromomethane ND ug/kg 10/11/18 15:15 74-95-310/11/18 09:155.1 2.6 1
1,2-Dichlorobenzene ND ug/kg 10/11/18 15:15 95-50-110/11/18 09:155.1 2.0 1
1,3-Dichlorobenzene ND ug/kg 10/11/18 15:15 541-73-110/11/18 09:155.1 2.1 1
1,4-Dichlorobenzene ND ug/kg 10/11/18 15:15 106-46-710/11/18 09:155.1 1.7 1
Dichlorodifluoromethane ND ug/kg 10/11/18 15:15 75-71-810/11/18 09:1510.3 3.7 1
1,1-Dichloroethane ND ug/kg 10/11/18 15:15 75-34-310/11/18 09:155.1 1.5 1
1,2-Dichloroethane ND ug/kg 10/11/18 15:15 107-06-210/11/18 09:155.1 2.3 1
1,1-Dichloroethene ND ug/kg 10/11/18 15:15 75-35-410/11/18 09:155.1 1.9 1
cis-1,2-Dichloroethene ND ug/kg 10/11/18 15:15 156-59-210/11/18 09:155.1 1.4 1
trans-1,2-Dichloroethene ND ug/kg 10/11/18 15:15 156-60-510/11/18 09:155.1 2.0 1
1,2-Dichloropropane ND ug/kg 10/11/18 15:15 78-87-510/11/18 09:155.1 1.7 1
1,3-Dichloropropane ND ug/kg 10/11/18 15:15 142-28-910/11/18 09:155.1 2.0 1
2,2-Dichloropropane ND ug/kg 10/11/18 15:15 594-20-710/11/18 09:155.1 1.7 1
1,1-Dichloropropene ND ug/kg 10/11/18 15:15 563-58-610/11/18 09:155.1 1.5 1
cis-1,3-Dichloropropene ND ug/kg 10/11/18 15:15 10061-01-510/11/18 09:155.1 1.9 1
trans-1,3-Dichloropropene ND ug/kg 10/11/18 15:15 10061-02-610/11/18 09:155.1 1.5 1
Diisopropyl ether ND ug/kg 10/11/18 15:15 108-20-310/11/18 09:155.1 1.7 1
Ethylbenzene ND ug/kg 10/11/18 15:15 100-41-410/11/18 09:155.1 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 10/11/18 15:15 87-68-310/11/18 09:155.1 2.1 1
2-Hexanone ND ug/kg 10/11/18 15:15 591-78-610/11/18 09:1551.5 4.0 1
Isopropylbenzene (Cumene)ND ug/kg 10/11/18 15:15 98-82-810/11/18 09:155.1 2.0 1
p-Isopropyltoluene ND ug/kg 10/11/18 15:15 99-87-610/11/18 09:155.1 1.7 1
Methylene Chloride ND ug/kg 10/11/18 15:15 75-09-210/11/18 09:1520.6 3.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/11/18 15:15 108-10-110/11/18 09:1551.5 3.8 1
Methyl-tert-butyl ether ND ug/kg 10/11/18 15:15 1634-04-410/11/18 09:155.1 1.5 1
Naphthalene ND ug/kg 10/11/18 15:15 91-20-310/11/18 09:155.1 1.2 1
n-Propylbenzene ND ug/kg 10/11/18 15:15 103-65-110/11/18 09:155.1 1.7 1
Styrene ND ug/kg 10/11/18 15:15 100-42-510/11/18 09:155.1 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/11/18 15:15 630-20-610/11/18 09:155.1 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/11/18 15:15 79-34-510/11/18 09:155.1 2.0 1
Tetrachloroethene ND ug/kg 10/11/18 15:15 127-18-410/11/18 09:155.1 1.7 1
Toluene ND ug/kg 10/11/18 15:15 108-88-310/11/18 09:155.1 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 10/11/18 15:15 87-61-610/11/18 09:155.1 2.3 1
1,2,4-Trichlorobenzene ND ug/kg 10/11/18 15:15 120-82-110/11/18 09:155.1 1.6 1
1,1,1-Trichloroethane ND ug/kg 10/11/18 15:15 71-55-610/11/18 09:155.1 1.9 1
1,1,2-Trichloroethane ND ug/kg 10/11/18 15:15 79-00-510/11/18 09:155.1 2.2 1
Trichloroethene ND ug/kg 10/11/18 15:15 79-01-610/11/18 09:155.1 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Sample: Base-20181008 Lab ID: 92402530001 Collected: 10/08/18 13:00 Received: 10/08/18 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 10/11/18 15:15 75-69-410/11/18 09:155.1 2.3 1
1,2,3-Trichloropropane ND ug/kg 10/11/18 15:15 96-18-410/11/18 09:155.1 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 10/11/18 15:15 95-63-610/11/18 09:155.1 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 10/11/18 15:15 108-67-810/11/18 09:155.1 1.9 1
Vinyl acetate ND ug/kg 10/11/18 15:15 108-05-410/11/18 09:1551.5 9.1 1
Vinyl chloride ND ug/kg 10/11/18 15:15 75-01-410/11/18 09:1510.3 1.9 1
Xylene (Total)ND ug/kg 10/11/18 15:15 1330-20-710/11/18 09:1510.3 3.7 1
m&p-Xylene ND ug/kg 10/11/18 15:15 179601-23-110/11/18 09:1510.3 3.7 1
o-Xylene ND ug/kg 10/11/18 15:15 95-47-610/11/18 09:155.1 2.0 1
Surrogates
Toluene-d8 (S)104 %10/11/18 15:15 2037-26-510/11/18 09:1570-130 1
4-Bromofluorobenzene (S)101 %10/11/18 15:15 460-00-410/11/18 09:1570-130 1
1,2-Dichloroethane-d4 (S)86 %10/11/18 15:15 17060-07-010/11/18 09:1570-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.9 %10/09/18 14:130.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435679
EPA 5035A
EPA 8260B
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92402530001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2397689
Associated Lab Samples:92402530001
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 6.1 10/11/18 12:192.6
1,1,1-Trichloroethane ug/kg ND 6.1 10/11/18 12:192.2
1,1,2,2-Tetrachloroethane ug/kg ND 6.1 10/11/18 12:192.3
1,1,2-Trichloroethane ug/kg ND 6.1 10/11/18 12:192.6
1,1-Dichloroethane ug/kg ND 6.1 10/11/18 12:191.8
1,1-Dichloroethene ug/kg ND 6.1 10/11/18 12:192.2
1,1-Dichloropropene ug/kg ND 6.1 10/11/18 12:191.8
1,2,3-Trichlorobenzene ug/kg ND 6.1 10/11/18 12:192.7
1,2,3-Trichloropropane ug/kg ND 6.1 10/11/18 12:192.0
1,2,4-Trichlorobenzene ug/kg ND 6.1 10/11/18 12:192.0
1,2,4-Trimethylbenzene ug/kg ND 6.1 10/11/18 12:192.4
1,2-Dibromo-3-chloropropane ug/kg ND 6.1 10/11/18 12:194.4
1,2-Dibromoethane (EDB)ug/kg ND 6.1 10/11/18 12:192.2
1,2-Dichlorobenzene ug/kg ND 6.1 10/11/18 12:192.3
1,2-Dichloroethane ug/kg ND 6.1 10/11/18 12:192.7
1,2-Dichloropropane ug/kg ND 6.1 10/11/18 12:192.1
1,3,5-Trimethylbenzene ug/kg ND 6.1 10/11/18 12:192.2
1,3-Dichlorobenzene ug/kg ND 6.1 10/11/18 12:192.4
1,3-Dichloropropane ug/kg ND 6.1 10/11/18 12:192.3
1,4-Dichlorobenzene ug/kg ND 6.1 10/11/18 12:192.1
2,2-Dichloropropane ug/kg ND 6.1 10/11/18 12:192.1
2-Butanone (MEK)ug/kg ND 122 10/11/18 12:193.5
2-Chlorotoluene ug/kg ND 6.1 10/11/18 12:192.1
2-Hexanone ug/kg ND 61.1 10/11/18 12:194.8
4-Chlorotoluene ug/kg ND 6.1 10/11/18 12:192.2
4-Methyl-2-pentanone (MIBK)ug/kg ND 61.1 10/11/18 12:194.5
Acetone ug/kg ND 122 10/11/18 12:1912.2
Benzene ug/kg ND 6.1 10/11/18 12:192.0
Bromobenzene ug/kg ND 6.1 10/11/18 12:192.4
Bromochloromethane ug/kg ND 6.1 10/11/18 12:192.1
Bromodichloromethane ug/kg ND 6.1 10/11/18 12:192.3
Bromoform ug/kg ND 6.1 10/11/18 12:192.8
Bromomethane ug/kg ND 12.2 10/11/18 12:193.1
Carbon tetrachloride ug/kg ND 6.1 10/11/18 12:193.2
Chlorobenzene ug/kg ND 6.1 10/11/18 12:192.3
Chloroethane ug/kg ND 12.2 10/11/18 12:192.9
Chloroform ug/kg ND 6.1 10/11/18 12:192.0
Chloromethane ug/kg ND 12.2 10/11/18 12:192.9
cis-1,2-Dichloroethene ug/kg ND 6.1 10/11/18 12:191.7
cis-1,3-Dichloropropene ug/kg ND 6.1 10/11/18 12:192.2
Dibromochloromethane ug/kg ND 6.1 10/11/18 12:192.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2397689
Associated Lab Samples:92402530001
Matrix: Solid
AnalyzedMDL
Dibromomethane ug/kg ND 6.1 10/11/18 12:193.1
Dichlorodifluoromethane ug/kg ND 12.2 10/11/18 12:194.4
Diisopropyl ether ug/kg ND 6.1 10/11/18 12:192.1
Ethylbenzene ug/kg ND 6.1 10/11/18 12:192.2
Hexachloro-1,3-butadiene ug/kg ND 6.1 10/11/18 12:192.4
Isopropylbenzene (Cumene)ug/kg ND 6.1 10/11/18 12:192.3
m&p-Xylene ug/kg ND 12.2 10/11/18 12:194.4
Methyl-tert-butyl ether ug/kg ND 6.1 10/11/18 12:191.8
Methylene Chloride ug/kg ND 24.4 10/11/18 12:193.7
n-Butylbenzene ug/kg ND 6.1 10/11/18 12:192.2
n-Propylbenzene ug/kg ND 6.1 10/11/18 12:192.1
Naphthalene ug/kg ND 6.1 10/11/18 12:191.5
o-Xylene ug/kg ND 6.1 10/11/18 12:192.3
p-Isopropyltoluene ug/kg ND 6.1 10/11/18 12:192.1
sec-Butylbenzene ug/kg ND 6.1 10/11/18 12:192.0
Styrene ug/kg ND 6.1 10/11/18 12:192.2
tert-Butylbenzene ug/kg ND 6.1 10/11/18 12:192.4
Tetrachloroethene ug/kg ND 6.1 10/11/18 12:192.1
Toluene ug/kg ND 6.1 10/11/18 12:192.2
trans-1,2-Dichloroethene ug/kg ND 6.1 10/11/18 12:192.3
trans-1,3-Dichloropropene ug/kg ND 6.1 10/11/18 12:191.8
Trichloroethene ug/kg ND 6.1 10/11/18 12:192.6
Trichlorofluoromethane ug/kg ND 6.1 10/11/18 12:192.7
Vinyl acetate ug/kg ND 61.1 10/11/18 12:1910.8
Vinyl chloride ug/kg ND 12.2 10/11/18 12:192.2
Xylene (Total)ug/kg ND 12.2 10/11/18 12:194.4
1,2-Dichloroethane-d4 (S)%89 70-132 10/11/18 12:19
4-Bromofluorobenzene (S)%103 70-130 10/11/18 12:19
Toluene-d8 (S)%106 70-130 10/11/18 12:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397690LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 55.561.4 90 74-137
1,1,1-Trichloroethane ug/kg 57.161.4 93 67-140
1,1,2,2-Tetrachloroethane ug/kg 48.761.4 79 72-141
1,1,2-Trichloroethane ug/kg 56.261.4 91 78-138
1,1-Dichloroethane ug/kg 56.361.4 92 69-134
1,1-Dichloroethene ug/kg 61.261.4 100 67-138
1,1-Dichloropropene ug/kg 59.761.4 97 69-139
1,2,3-Trichlorobenzene ug/kg 54.761.4 89 70-146
1,2,3-Trichloropropane ug/kg 56.161.4 91 69-144
1,2,4-Trichlorobenzene ug/kg 54.461.4 89 68-148
1,2,4-Trimethylbenzene ug/kg 56.661.4 92 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397690LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 53.661.4 87 65-140
1,2-Dibromoethane (EDB)ug/kg 57.661.4 94 77-135
1,2-Dichlorobenzene ug/kg 56.961.4 93 77-141
1,2-Dichloroethane ug/kg 55.661.4 91 65-137
1,2-Dichloropropane ug/kg 57.961.4 94 72-136
1,3,5-Trimethylbenzene ug/kg 57.661.4 94 76-133
1,3-Dichlorobenzene ug/kg 55.461.4 90 74-138
1,3-Dichloropropane ug/kg 59.161.4 96 71-139
1,4-Dichlorobenzene ug/kg 55.761.4 91 76-138
2,2-Dichloropropane ug/kg 53.261.4 87 68-137
2-Butanone (MEK)ug/kg 109J123 89 58-147
2-Chlorotoluene ug/kg 57.561.4 94 73-139
2-Hexanone ug/kg 105123 85 62-145
4-Chlorotoluene ug/kg 57.461.4 93 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 104123 85 64-149
Acetone ug/kg 96.2J123 78 53-153
Benzene ug/kg 56.861.4 93 73-135
Bromobenzene ug/kg 57.961.4 94 75-133
Bromochloromethane ug/kg 55.661.4 90 73-134
Bromodichloromethane ug/kg 55.461.4 90 71-135
Bromoform ug/kg 52.061.4 85 66-141
Bromomethane ug/kg 57.561.4 94 53-160
Carbon tetrachloride ug/kg 54.161.4 88 60-145
Chlorobenzene ug/kg 54.461.4 89 78-130
Chloroethane ug/kg 64.161.4 104 64-149
Chloroform ug/kg 54.461.4 89 70-134
Chloromethane ug/kg 48.961.4 80 52-150
cis-1,2-Dichloroethene ug/kg 55.361.4 90 70-133
cis-1,3-Dichloropropene ug/kg 55.361.4 90 68-134
Dibromochloromethane ug/kg 56.461.4 92 71-138
Dibromomethane ug/kg 52.461.4 85 74-130
Dichlorodifluoromethane ug/kg 51.761.4 84 40-160
Diisopropyl ether ug/kg 56.461.4 92 69-141
Ethylbenzene ug/kg 56.061.4 91 75-133
Hexachloro-1,3-butadiene ug/kg 53.561.4 87 68-143
Isopropylbenzene (Cumene)ug/kg 56.561.4 92 76-143
m&p-Xylene ug/kg 112123 91 75-136
Methyl-tert-butyl ether ug/kg 59.961.4 97 68-144
Methylene Chloride ug/kg 59.961.4 98 45-154
n-Butylbenzene ug/kg 57.161.4 93 72-137
n-Propylbenzene ug/kg 59.761.4 97 76-136
Naphthalene ug/kg 56.161.4 91 68-151
o-Xylene ug/kg 56.761.4 92 76-141
p-Isopropyltoluene ug/kg 54.961.4 89 76-140
sec-Butylbenzene ug/kg 58.661.4 95 79-139
Styrene ug/kg 54.461.4 89 79-137
tert-Butylbenzene ug/kg 53.361.4 87 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397690LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 50.461.4 82 71-138
Toluene ug/kg 52.661.4 86 74-131
trans-1,2-Dichloroethene ug/kg 57.361.4 93 67-135
trans-1,3-Dichloropropene ug/kg 54.261.4 88 65-146
Trichloroethene ug/kg 62.261.4 101 67-135
Trichlorofluoromethane ug/kg 65.161.4 106 59-144
Vinyl acetate ug/kg 68.1123 55 40-160
Vinyl chloride ug/kg 61.861.4 101 56-141
Xylene (Total)ug/kg 169184 92 76-137
1,2-Dichloroethane-d4 (S)%99 70-132
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397691MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397692
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg M1,R1187270-13037 33 3025.4ND 13.0 9.3
1,1,1-Trichloroethane ug/kg M1188070-13022 3025.4ND 14.4 5.7J
1,1,2,2-Tetrachloroethane ug/kg M1,R1186970-13071 37 3025.4ND 12.5 18.1
1,1,2-Trichloroethane ug/kg M1187370-13067 26 3025.4ND 13.2 17.1
1,1-Dichloroethane ug/kg M1,R1188070-13036 46 3025.4ND 14.4 9.1
1,1-Dichloroethene ug/kg M1188649-18023 3025.4ND 15.4 5.9J
1,1-Dichloropropene ug/kg M1187670-13018 3025.4ND 13.7 4.6J
1,2,3-Trichlorobenzene ug/kg M1183270-13027 17 3025.4ND 5.8 6.9
1,2,3-Trichloropropane ug/kg R1187570-13076 35 3025.4ND 13.6 19.3
1,2,4-Trichlorobenzene ug/kg M1183570-13026 2 3025.4ND 6.4 6.5
1,2,4-Trimethylbenzene ug/kg M1,R1187770-13033 50 3025.4ND 13.8 8.3
1,2-Dibromo-3-
chloropropane ug/kg M1,R1186370-13070 44 3025.4ND 11.4 17.9
1,2-Dibromoethane (EDB) ug/kg M1187070-13059 18 3025.4ND 12.6 15.1
1,2-Dichlorobenzene ug/kg M1186070-13041 4 3025.4ND 10.8 10.3
1,2-Dichloroethane ug/kg R1187270-13070 31 3025.4ND 13.0 17.8
1,2-Dichloropropane ug/kg M1187970-13042 30 3025.4ND 14.2 10.6
1,3,5-Trimethylbenzene ug/kg M1,R1187970-13030 60 3025.4ND 14.3 7.7
1,3-Dichlorobenzene ug/kg M1186370-13035 25 3025.4ND 11.4 8.9
1,3-Dichloropropane ug/kg M1187770-13056 3 3025.4ND 13.9 14.2
1,4-Dichlorobenzene ug/kg M1186170-13034 24 3025.4ND 11.1 8.7
2,2-Dichloropropane ug/kg M1187670-13020 3025.4ND 13.7 5.1J
2-Butanone (MEK)ug/kg M136.1 50 70-13056 3050.8ND 18.2J 28.4J
2-Chlorotoluene ug/kg M1,R1187970-13038 38 3025.4ND 14.2 9.7
2-Hexanone ug/kg M136.1 37 70-13033 3050.8ND 13.4J 16.9J
4-Chlorotoluene ug/kg M1,R1187470-13037 36 3025.4ND 13.4 9.3
4-Methyl-2-pentanone
(MIBK)ug/kg M136.1 67 70-13084 3050.8ND 24.0J 42.6J
Acetone ug/kg M136.1 59 70-130133 3050.818.2J 39.6J 86.0J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397691MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397692
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene ug/kg M1,R1188050-16635 49 3025.4ND 14.5 8.8
Bromobenzene ug/kg M1187670-13044 19 3025.4ND 13.7 11.3
Bromochloromethane ug/kg M1187370-13056 9 3025.4ND 13.1 14.3
Bromodichloromethane ug/kg M1187670-13048 13 3025.4ND 13.8 12.2
Bromoform ug/kg M1185470-13048 21 3025.4ND 9.8 12.1
Bromomethane ug/kg M1188070-13031 3025.4ND 14.5 7.9J
Carbon tetrachloride ug/kg M1188170-13019 3025.4ND 14.5 4.9J
Chlorobenzene ug/kg M1,R1187243-16936 34 3025.4ND 12.9 9.2
Chloroethane ug/kg M1189270-13030 3025.4ND 16.6 7.7J
Chloroform ug/kg M1188170-13047 20 3025.4ND 14.7 12.1
Chloromethane ug/kg M1187070-13023 3025.4ND 12.7 5.7J
cis-1,2-Dichloroethene ug/kg M1187770-13043 24 3025.4ND 14.0 11.0
cis-1,3-Dichloropropene ug/kg M1185670-13031 25 3025.4ND 10.1 7.9
Dibromochloromethane ug/kg M1186570-13047 3 3025.4ND 11.7 12.0
Dibromomethane ug/kg M1187470-13066 22 3025.4ND 13.3 16.7
Dichlorodifluoromethane ug/kg M1187370-13010 3025.4ND 13.2 ND
Diisopropyl ether ug/kg M1187670-13052 3 3025.4ND 13.7 13.3
Ethylbenzene ug/kg M1,R1188070-13030 63 3025.4ND 14.4 7.5
Hexachloro-1,3-butadiene ug/kg M1184470-13015 3025.4ND 7.9 3.8J
Isopropylbenzene (Cumene) ug/kg M1,R1187770-13027 69 3025.4ND 13.9 6.8
m&p-Xylene ug/kg M1,R136.1 78 70-13031 57 3050.8ND 28.3 15.8
Methyl-tert-butyl ether ug/kg R1187470-13072 31 3025.4ND 13.3 18.2
Methylene Chloride ug/kg M1187370-13042 3025.4ND 13.3J 10.6J
n-Butylbenzene ug/kg M1186770-13020 3025.4ND 12.1 5.1J
n-Propylbenzene ug/kg M1,R1188970-13029 75 3025.4ND 16.1 7.3
Naphthalene ug/kg M1184470-13038 20 3025.4ND 8.0 9.7
o-Xylene ug/kg M1,R1187670-13035 43 3025.4ND 13.8 8.9
p-Isopropyltoluene ug/kg M1187270-13022 3025.4ND 13.0 5.6J
sec-Butylbenzene ug/kg M1188270-13023 3025.4ND 14.8 5.9J
Styrene ug/kg M1186070-13032 29 3025.4ND 10.9 8.2
tert-Butylbenzene ug/kg M1,R1187770-13026 71 3025.4ND 13.9 6.6
Tetrachloroethene ug/kg M1187070-13019 3025.4ND 12.7 4.9J
Toluene ug/kg M1,R1187652-16334 46 3025.4ND 13.8 8.7
trans-1,2-Dichloroethene ug/kg M1,R1188670-13030 67 3025.4ND 15.5 7.7
trans-1,3-Dichloropropene ug/kg M1185870-13043 3 3025.4ND 10.5 10.8
Trichloroethene ug/kg M1187849-16722 3025.4ND 14.0 5.5J
Trichlorofluoromethane ug/kg M1189470-13018 3025.4ND 17.0 4.5J
Vinyl acetate ug/kg M136.1 9 70-1307 3050.8ND ND ND
Vinyl chloride ug/kg M1188670-13022 3025.4ND 15.6 5.5J
Xylene (Total)ug/kg MS,RS54.1 78 70-13032 52 3076.2ND 42.1 24.7
1,2-Dichloroethane-d4 (S)%94 70-132131
4-Bromofluorobenzene (S) %98 70-130100
Toluene-d8 (S)%99 70-130105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435704
EPA 3546
EPA 8270D
8270 Solid MSSV Microwave
Associated Lab Samples: 92402530001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2397791
Associated Lab Samples:92402530001
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 327 10/15/18 11:5363.4
1,2-Dichlorobenzene ug/kg ND 327 10/15/18 11:5387.1
1,3-Dichlorobenzene ug/kg ND 327 10/15/18 11:5374.3
1,4-Dichlorobenzene ug/kg ND 327 10/15/18 11:5392.1
1-Methylnaphthalene ug/kg ND 327 10/15/18 11:5385.1
2,2'-Oxybis(1-chloropropane)ug/kg ND 327 10/15/18 11:5387.1
2,4,5-Trichlorophenol ug/kg ND 327 10/15/18 11:53101
2,4,6-Trichlorophenol ug/kg ND 327 10/15/18 11:5372.3
2,4-Dichlorophenol ug/kg ND 327 10/15/18 11:5371.3
2,4-Dimethylphenol ug/kg ND 327 10/15/18 11:53129
2,4-Dinitrophenol ug/kg ND 1630 10/15/18 11:5353.5
2,4-Dinitrotoluene ug/kg ND 327 10/15/18 11:5361.4
2,6-Dinitrotoluene ug/kg ND 327 10/15/18 11:5368.3
2-Chloronaphthalene ug/kg ND 327 10/15/18 11:5364.4
2-Chlorophenol ug/kg ND 327 10/15/18 11:5389.1
2-Methylnaphthalene ug/kg ND 327 10/15/18 11:5370.3
2-Methylphenol(o-Cresol)ug/kg ND 327 10/15/18 11:5399.0
2-Nitroaniline ug/kg ND 1630 10/15/18 11:53101
2-Nitrophenol ug/kg ND 327 10/15/18 11:5379.2
3&4-Methylphenol(m&p Cresol)ug/kg ND 327 10/15/18 11:53129
3,3'-Dichlorobenzidine ug/kg 76.6J 1630 10/15/18 11:5371.3
3-Nitroaniline ug/kg ND 1630 10/15/18 11:5389.1
4,6-Dinitro-2-methylphenol ug/kg ND 653 10/15/18 11:5365.3
4-Bromophenylphenyl ether ug/kg ND 327 10/15/18 11:5359.4
4-Chloro-3-methylphenol ug/kg ND 653 10/15/18 11:5367.3
4-Chloroaniline ug/kg ND 1630 10/15/18 11:5391.1
4-Chlorophenylphenyl ether ug/kg ND 327 10/15/18 11:5367.3
4-Nitroaniline ug/kg ND 653 10/15/18 11:5392.1
4-Nitrophenol ug/kg 265J 1630 10/15/18 11:5358.4
Acenaphthene ug/kg ND 327 10/15/18 11:5375.2
Acenaphthylene ug/kg ND 327 10/15/18 11:5377.2
Aniline ug/kg ND 327 10/15/18 11:5388.1
Anthracene ug/kg ND 327 10/15/18 11:5373.3
Benzo(a)anthracene ug/kg 67.3J 327 10/15/18 11:5360.4
Benzo(a)pyrene ug/kg ND 327 10/15/18 11:5362.4
Benzo(b)fluoranthene ug/kg ND 327 10/15/18 11:5356.4
Benzo(g,h,i)perylene ug/kg ND 327 10/15/18 11:5383.2
Benzo(k)fluoranthene ug/kg ND 327 10/15/18 11:5364.4
Benzoic Acid ug/kg ND 1630 10/15/18 11:5359.4
Benzyl alcohol ug/kg ND 653 10/15/18 11:5365.3
bis(2-Chloroethoxy)methane ug/kg ND 327 10/15/18 11:5376.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2397791
Associated Lab Samples:92402530001
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 327 10/15/18 11:5383.2
bis(2-Ethylhexyl)phthalate ug/kg ND 327 10/15/18 11:5389.1
Butylbenzylphthalate ug/kg ND 327 10/15/18 11:5369.3
Chrysene ug/kg 67.1J 327 10/15/18 11:5343.6
Di-n-butylphthalate ug/kg ND 327 10/15/18 11:5353.5
Di-n-octylphthalate ug/kg ND 327 10/15/18 11:5368.3
Dibenz(a,h)anthracene ug/kg ND 327 10/15/18 11:5369.3
Dibenzofuran ug/kg ND 327 10/15/18 11:5353.5
Diethylphthalate ug/kg ND 327 10/15/18 11:5350.5
Dimethylphthalate ug/kg ND 327 10/15/18 11:5366.3
Fluoranthene ug/kg 58.2J 327 10/15/18 11:5347.5
Fluorene ug/kg ND 327 10/15/18 11:5367.3
Hexachloro-1,3-butadiene ug/kg ND 327 10/15/18 11:5356.4
Hexachlorobenzene ug/kg ND 327 10/15/18 11:5341.6
Hexachlorocyclopentadiene ug/kg ND 327 10/15/18 11:5360.4
Hexachloroethane ug/kg ND 327 10/15/18 11:5386.1
Indeno(1,2,3-cd)pyrene ug/kg ND 327 10/15/18 11:5367.3
Isophorone ug/kg ND 327 10/15/18 11:5373.3
N-Nitroso-di-n-propylamine ug/kg ND 327 10/15/18 11:5362.4
N-Nitrosodimethylamine ug/kg ND 327 10/15/18 11:53106
N-Nitrosodiphenylamine ug/kg ND 327 10/15/18 11:5397.0
Naphthalene ug/kg ND 327 10/15/18 11:5380.2
Nitrobenzene ug/kg ND 327 10/15/18 11:5389.1
Pentachlorophenol ug/kg 97.5J 1630 10/15/18 11:5359.4
Phenanthrene ug/kg ND 327 10/15/18 11:5354.5
Phenol ug/kg ND 327 10/15/18 11:5398.0
Pyrene ug/kg 76.3J 327 10/15/18 11:5355.4
2,4,6-Tribromophenol (S)%91 27-110 10/15/18 11:53
2-Fluorobiphenyl (S)%80 30-110 10/15/18 11:53
2-Fluorophenol (S)%79 13-110 10/15/18 11:53
Nitrobenzene-d5 (S)%85 23-110 10/15/18 11:53
Phenol-d6 (S)%81 22-110 10/15/18 11:53
Terphenyl-d14 (S)%122 28-110 S310/15/18 11:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397792LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13601660 82 36-120
1,2-Dichlorobenzene ug/kg 14001660 85 41-120
1,3-Dichlorobenzene ug/kg 13901660 84 66-120
1,4-Dichlorobenzene ug/kg 14001660 85 42-120
1-Methylnaphthalene ug/kg 16301660 98 40-120
2,2'-Oxybis(1-chloropropane)ug/kg 2200 L11660133 17-120
2,4,5-Trichlorophenol ug/kg 14301660 87 37-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397792LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 15101660 91 40-120
2,4-Dichlorophenol ug/kg 14601660 88 33-120
2,4-Dimethylphenol ug/kg 17001660 102 36-120
2,4-Dinitrophenol ug/kg 67508280 82 22-121
2,4-Dinitrotoluene ug/kg 15801660 95 60-120
2,6-Dinitrotoluene ug/kg 16501660 100 54-120
2-Chloronaphthalene ug/kg 16601660 100 41-120
2-Chlorophenol ug/kg 15401660 93 39-120
2-Methylnaphthalene ug/kg 16801660 102 26-120
2-Methylphenol(o-Cresol)ug/kg 16001660 97 41-120
2-Nitroaniline ug/kg 32703310 99 45-120
2-Nitrophenol ug/kg 14201660 86 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 16401660 99 35-120
3,3'-Dichlorobenzidine ug/kg 31403310 95 16-125
3-Nitroaniline ug/kg 31103310 94 45-120
4,6-Dinitro-2-methylphenol ug/kg 31203310 94 46-120
4-Bromophenylphenyl ether ug/kg 16501660 100 36-120
4-Chloro-3-methylphenol ug/kg 32103310 97 37-120
4-Chloroaniline ug/kg 28803310 87 35-120
4-Chlorophenylphenyl ether ug/kg 15601660 95 30-120
4-Nitroaniline ug/kg 30103310 91 48-120
4-Nitrophenol ug/kg 72108280 87 43-120
Acenaphthene ug/kg 15801660 95 46-120
Acenaphthylene ug/kg 15901660 96 46-120
Aniline ug/kg 14101660 85 33-120
Anthracene ug/kg 16101660 97 63-120
Benzo(a)anthracene ug/kg 15401660 93 61-120
Benzo(a)pyrene ug/kg 16101660 97 59-120
Benzo(b)fluoranthene ug/kg 16701660 101 55-120
Benzo(g,h,i)perylene ug/kg 16301660 98 57-120
Benzo(k)fluoranthene ug/kg 16401660 99 56-120
Benzoic Acid ug/kg 70208280 85 13-120
Benzyl alcohol ug/kg 33803310 102 34-120
bis(2-Chloroethoxy)methane ug/kg 18501660 112 21-120
bis(2-Chloroethyl) ether ug/kg 17001660 103 25-120
bis(2-Ethylhexyl)phthalate ug/kg 16301660 98 56-123
Butylbenzylphthalate ug/kg 16101660 97 57-120
Chrysene ug/kg 15501660 93 64-120
Di-n-butylphthalate ug/kg 16201660 98 58-120
Di-n-octylphthalate ug/kg 18101660 109 47-121
Dibenz(a,h)anthracene ug/kg 16601660 100 56-120
Dibenzofuran ug/kg 16001660 97 43-120
Diethylphthalate ug/kg 15101660 91 55-120
Dimethylphthalate ug/kg 14301660 86 54-120
Fluoranthene ug/kg 14701660 89 61-120
Fluorene ug/kg 16201660 98 51-120
Hexachloro-1,3-butadiene ug/kg 14701660 89 22-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397792LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 15301660 92 53-120
Hexachlorocyclopentadiene ug/kg 15401660 93 18-150
Hexachloroethane ug/kg 15401660 93 39-120
Indeno(1,2,3-cd)pyrene ug/kg 16201660 98 58-120
Isophorone ug/kg 14901660 90 38-120
N-Nitroso-di-n-propylamine ug/kg 17501660 106 30-120
N-Nitrosodimethylamine ug/kg 16901660 102 32-120
N-Nitrosodiphenylamine ug/kg 15801660 95 50-120
Naphthalene ug/kg 15401660 93 38-120
Nitrobenzene ug/kg 15901660 96 37-120
Pentachlorophenol ug/kg 25603310 77 10-120
Phenanthrene ug/kg 15701660 95 62-120
Phenol ug/kg 17301660 105 37-120
Pyrene ug/kg 15701660 95 63-120
2,4,6-Tribromophenol (S)%91 27-110
2-Fluorobiphenyl (S)%83 30-110
2-Fluorophenol (S)%88 13-110
Nitrobenzene-d5 (S)%89 23-110
Phenol-d6 (S)%94 22-110
Terphenyl-d14 (S)%109 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397793MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397794
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1770 50 18-11942 18 301750ND885 740
1,2-Dichlorobenzene ug/kg M117705150-11041 21 301750ND894 721
1,3-Dichlorobenzene ug/kg 1770 49 27-11041 21 301750ND871 708
1,4-Dichlorobenzene ug/kg 1770 50 28-11041 23 301750ND893 710
1-Methylnaphthalene ug/kg 1770 59 24-11654 9 301750ND1040 944
2,2'-Oxybis(1-chloropropane) ug/kg 1770 72 50-15059 22 301750ND1270 1030
2,4,5-Trichlorophenol ug/kg 1770 59 28-11057 5 301750ND1040 986
2,4,6-Trichlorophenol ug/kg 1770 61 17-11758 7 301750ND1080 1010
2,4-Dichlorophenol ug/kg 1770 53 21-12848 11 301750ND942 845
2,4-Dimethylphenol ug/kg 1770 48 10-12049 0 301750ND851 852
2,4-Dinitrophenol ug/kg 8850 34 10-10736 4 308720ND2970 3100
2,4-Dinitrotoluene ug/kg 1770 60 36-10962 1 301750ND1060 1080
2,6-Dinitrotoluene ug/kg 1770 62 32-11062 1 301750ND1090 1080
2-Chloronaphthalene ug/kg 1770 55 30-10751 8 301750ND969 898
2-Chlorophenol ug/kg 1770 54 14-10643 23 301750ND947 755
2-Methylnaphthalene ug/kg 1770 59 10-13554 11 301750ND1050 942
2-Methylphenol(o-Cresol) ug/kg 1770 53 10-12445 18 301750ND944 789
2-Nitroaniline ug/kg 3540 60 26-11659 3 303490ND2120 2060
2-Nitrophenol ug/kg 1770 49 28-10342 18 301750ND871 726
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397793MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397794
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/kg 1770 51 10-10947 9 301750ND895 816
3,3'-Dichlorobenzidine ug/kg 3540 47 10-15052 303490ND1660J 1810
3-Nitroaniline ug/kg 3540 54 22-11058 5 303490ND1920 2030
4,6-Dinitro-2-methylphenol ug/kg 3540 53 13-12161 12 303490ND1880 2110
4-Bromophenylphenyl ether ug/kg 1770 69 31-10969 2 301750ND1230 1200
4-Chloro-3-methylphenol ug/kg 3540 59 13-12859 2 303490ND2100 2050
4-Chloroaniline ug/kg 3540 48 18-10246 303490ND1680J 1610J
4-Chlorophenylphenyl ether ug/kg 1770 60 29-11260 2 301750ND1060 1040
4-Nitroaniline ug/kg 3540 54 16-11159 8 303490ND1900 2070
4-Nitrophenol ug/kg 8850 50 14-13557 10 308720ND4460 4950
Acenaphthene ug/kg 1770 58 26-11458 2 301750ND1020 1010
Acenaphthylene ug/kg 1770 58 32-10858 1 301750ND1030 1010
Aniline ug/kg 1770 39 10-10735 12 301750ND690 614
Anthracene ug/kg 1770 63 32-11163 1 301750ND1120 1100
Benzo(a)anthracene ug/kg 1770 57 25-11759 2 301750ND1010 1030
Benzo(a)pyrene ug/kg 1770 62 25-10663 1 301750ND1090 1100
Benzo(b)fluoranthene ug/kg 1770 59 24-11060 0 301750ND1050 1050
Benzo(g,h,i)perylene ug/kg 1770 62 19-11264 2 301750ND1100 1130
Benzo(k)fluoranthene ug/kg 1770 61 24-11461 1 301750ND1080 1070
Benzoic Acid ug/kg 8850 22 10-11020 308720ND1920 1720J
Benzyl alcohol ug/kg 3540 58 24-10650 16 303490ND2060 1760
bis(2-Chloroethoxy)methane ug/kg 1770 60 13-11953 15 301750ND1070 924
bis(2-Chloroethyl) ether ug/kg 1770 57 10-13449 17 301750ND1010 852
bis(2-Ethylhexyl)phthalate ug/kg 1770 59 10-12561 2 301750ND1040 1060
Butylbenzylphthalate ug/kg 1770 58 18-11058 1 301750ND1020 1010
Chrysene ug/kg 1770 58 30-11059 0 301750ND1020 1030
Di-n-butylphthalate ug/kg 1770 64 19-11264 1 301750ND1130 1120
Di-n-octylphthalate ug/kg 1770 65 17-10568 3 301750ND1150 1190
Dibenz(a,h)anthracene ug/kg 1770 66 23-11167 0 301750ND1170 1170
Dibenzofuran ug/kg 1770 60 35-10361 1 301750ND1070 1060
Diethylphthalate ug/kg 1770 58 27-11359 1 301750ND1030 1040
Dimethylphthalate ug/kg 1770 57 26-11156 2 301750ND1000 977
Fluoranthene ug/kg 1770 61 33-10960 2 301750ND1080 1050
Fluorene ug/kg 1770 61 32-11361 0 301750ND1070 1070
Hexachloro-1,3-butadiene ug/kg 1770 54 16-11646 17 301750ND959 809
Hexachlorobenzene ug/kg 1770 66 27-12065 3 301750ND1170 1140
Hexachlorocyclopentadiene ug/kg 1770 41 10-10833 23 301750ND720 574
Hexachloroethane ug/kg 1770 54 10-11743 23 301750ND955 754
Indeno(1,2,3-cd)pyrene ug/kg 1770 64 10-12265 1 301750ND1130 1140
Isophorone ug/kg 1770 51 28-11447 8 301750ND895 829
N-Nitroso-di-n-propylamine ug/kg 1770 57 27-11351 13 301750ND1010 882
N-Nitrosodimethylamine ug/kg 1770 55 10-10943 25 301750ND969 755
N-Nitrosodiphenylamine ug/kg 1770 64 10-12864 1 301750ND1130 1120
Naphthalene ug/kg 1770 54 25-11046 18 301750ND956 800
Nitrobenzene ug/kg 1770 52 18-11445 16 301750ND916 781
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397793MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397794
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pentachlorophenol ug/kg 3540 45 10-12252 303490ND1600J 1810
Phenanthrene ug/kg 1770 63 30-11464 1 301750ND1110 1110
Phenol ug/kg 1770 54 11-10247 16 301750ND960 814
Pyrene ug/kg 1770 55 25-11655 0 301750ND965 968
2,4,6-Tribromophenol (S)%73 27-11073
2-Fluorobiphenyl (S)%55 30-11050
2-Fluorophenol (S)%50 13-11040
Nitrobenzene-d5 (S)%51 23-11043
Phenol-d6 (S)%52 22-11044
Terphenyl-d14 (S)%74 28-11071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435049
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92402530001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92402531001
2395073SAMPLE DUPLICATE:
Percent Moisture %17.6 2 2517.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92402529002
2395097SAMPLE DUPLICATE:
Percent Moisture %22.5 3 2523.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 39
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
RPD value was outside control limits.R1
The RPD value in one of the constituent analytes was outside the control limits.RS
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 39
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92402530
Kannapolis, NC Site (KAN-012)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92402530001 435704 436214Base-20181008 EPA 3546 EPA 8270D
92402530001 435679 435689Base-20181008 EPA 5035A EPA 8260B
92402530001 435049Base-20181008 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:43 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 39
Page 23 of 39
Page 24 of 39
Page 25 of 39
ANALYTICAL REPORT
October 16, 2018
Pace Analytical - Huntersville, NC
Sample Delivery Group:L1032789
Samples Received:10/09/2018
Project Number:92402530
Description:Kannapolis, NC Site
Report To:Kevin Godwin
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By:
October 16, 2018
[Preliminary Report]
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Nationalis performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
October 16, 2018
Jason Romer
Project Manager
Page 26 of 39
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
BASE-20181008 L1032789-01 5
Qc: Quality Control Summary 6
Total Solids by Method 2540 G-2011 6
Wet Chemistry by Method 7199 7
Mercury by Method 7471B 8
Metals (ICPMS) by Method 6020B 9
Gl: Glossary of Terms 11
Al: Accreditations & Locations 12
Sc: Sample Chain of Custody 13
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 27 of 39
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
BASE-20181008 L1032789-01 Solid 10/08/18 13:00 10/09/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1178913 1 10/11/18 10:46 10/11/18 10:53 KDW
Wet Chemistry by Method 7199 WG1179761 1 10/12/18 16:14 10/12/18 21:13 GB
Mercury by Method 7471B WG1178441 1 10/09/18 18:40 10/11/18 12:23 ABL
Metals (ICPMS) by Method 6020B WG1178442 5 10/10/18 10:36 10/11/18 00:10 JDG
Metals (ICPMS) by Method 6020B WG1178442 5 10/10/18 10:36 10/11/18 03:00 JDG
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 28 of 39
ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Nancy McLain
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Huntersville, NC 92402530 L1032789 10/16/18 10:59 4 of 14
Jason Romer
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Pace Analytical - Huntersville, NC 92402530 L1032789 10/16/18 12:14 4 of 14
Page 29 of 39
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1032789
BASE-20181008
Collected date/time: 10/08/18 13:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 75.8 1 10/11/2018 10:53 WG1178913
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium U 0.337 1.32 1 10/12/2018 21:13 WG1179761
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0199 J 0.00369 0.0264 1 10/11/2018 12:23 WG1178441
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.66 0.0165 0.660 5 10/11/2018 00:10 WG1178442
Barium 159 0.211 1.32 5 10/11/2018 00:10 WG1178442
Cadmium 0.675 0.106 0.660 5 10/11/2018 00:10 WG1178442
Chromium 11.3 0.356 1.32 5 10/11/2018 00:10 WG1178442
Lead 22.9 0.158 0.660 5 10/11/2018 00:10 WG1178442
Selenium 1.59 0.251 0.660 5 10/11/2018 03:00 WG1178442
Silver U 0.205 0.660 5 10/11/2018 00:10 WG1178442
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1178913
Total Solids by Method 2540 G-2011 L1032789-01
Method Blank (MB)
(MB) R3349987-1 10/11/18 10:53
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1032611-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1032611-03 10/11/18 10:53 • (DUP) R3349987-3 10/11/18 10:53
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 88.0 87.0 1 1.11 10
Laboratory Control Sample (LCS)
(LCS) R3349987-2 10/11/18 10:53
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1179761
Wet Chemistry by Method 7199 L1032789-01
Method Blank (MB)
(MB) R3350745-1 10/12/18 19:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1032837-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1032837-01 10/12/18 21:19 • (DUP) R3350745-8 10/12/18 21:25
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium U 0.000 1 0.000 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3350745-2 10/12/18 19:46 • (LCSD) R3350745-3 10/12/18 19:52
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 10.0 9.95 10.0 99.5 100 80.0-120 0.809 20
L1032035-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1032035-01 10/12/18 20:11 • (MS) R3350745-4 10/12/18 20:17 • (MSD) R3350745-5 10/12/18 20:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 20.0 9.41 30.2 29.5 104 100 1 75.0-125 2.43 20
L1032035-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1032035-01 10/12/18 20:11 • (MS) R3350745-6 10/12/18 20:29
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 720 9.41 648 90.0 50 75.0-125
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1178441
Mercury by Method 7471B L1032789-01
Method Blank (MB)
(MB) R3349732-1 10/11/18 11:31
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.00280 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3349732-2 10/11/18 11:34 • (LCSD) R3349732-3 10/11/18 11:37
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.281 0.270 93.6 90.1 80.0-120 3.83 20
L1032550-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1032550-01 10/11/18 11:39 • (MS) R3349732-4 10/11/18 11:42 • (MSD) R3349732-5 10/11/18 11:44
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.0192 0.267 0.250 82.7 76.8 1 75.0-125 6.83 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1178442
Metals (ICPMS) by Method 6020B L1032789-01
Method Blank (MB)
(MB) R3349772-1 10/10/18 23:00
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.0125 0.500
Barium U 0.160 1.00
Cadmium U 0.0800 0.500
Chromium U 0.270 1.00
Lead U 0.120 0.500
Silver U 0.155 0.500
Method Blank (MB)
(MB) R3349772-8 10/11/18 02:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Selenium U 0.190 0.500
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3349772-2 10/10/18 23:04 • (LCSD) R3349772-3 10/10/18 23:08
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Arsenic 100 97.7 96.7 97.7 96.7 80.0-120 0.961 20
Barium 100 94.9 94.8 94.9 94.8 80.0-120 0.0777 20
Cadmium 100 100 100 100 100 80.0-120 0.203 20
Chromium 100 99.5 98.2 99.5 98.2 80.0-120 1.32 20
Lead 100 94.7 95.4 94.7 95.4 80.0-120 0.760 20
Silver 20.0 20.2 20.2 101 101 80.0-120 0.405 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3349772-9 10/11/18 02:10 • (LCSD) R3349772-10 10/11/18 02:14
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Selenium 100 93.3 96.7 93.3 96.7 80.0-120 3.53 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 34 of 39
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1178442
Metals (ICPMS) by Method 6020B L1032789-01
L1032452-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1032452-02 10/10/18 23:12 • (MS) R3349772-6 10/10/18 23:24 • (MSD) R3349772-7 10/10/18 23:28
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 20.0 2.00 94.3 102 92.3 99.8 5 75.0-125 7.60 20
Barium 20.0 36.0 125 130 89.1 94.2 5 75.0-125 4.02 20
Cadmium 20.0 0.225 97.2 103 96.9 103 5 75.0-125 5.90 20
Chromium 20.0 5.06 99.2 107 94.2 102 5 75.0-125 7.84 20
Lead 20.0 11.8 102 106 90.2 94.6 5 75.0-125 4.23 20
Silver 4.00 U 19.7 20.6 98.3 103 5 75.0-125 4.90 20
L1032452-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1032452-02 10/11/18 02:18 • (MS) R3349772-13 10/11/18 02:30 • (MSD) R3349772-14 10/11/18 02:34
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Selenium 20.0 0.263 93.7 97.7 93.5 97.4 5 75.0-125 4.11 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 35 of 39
ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 36 of 39
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T 104704245-17-14
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Page 37 of 39
Page 38 of 39
Page 39 of 39
#=CL#
October 18, 2018
LIMS USE: FR - SHANNON COTTRILL
LIMS OBJECT ID: 92402528
92402528
Project:
Pace Project No.:
RE:
Mr. Shannon Cottrill
Hart & Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
Kannapolis, NC Site (KAN-012)
Dear Mr. Cottrill:
Enclosed are the analytical results for sample(s) received by the laboratory on October 08, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
Per client request, report revised 10/18/18 to include MDL and J-Flags.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
cc: Nick Hotzelt, Hart & Hickman
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 39
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Lab ID Sample ID Matrix Date Collected Date Received
92402528001 SP-20181008 Solid 10/08/18 11:20 10/08/18 14:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92402528001 SP-20181008 EPA 8270D 74 PASI-CBPJ
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Sample: SP-20181008 Lab ID: 92402528001 Collected: 10/08/18 11:20 Received: 10/08/18 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 10/15/18 12:21 83-32-910/11/18 18:43388 89.3 1
Acenaphthylene ND ug/kg 10/15/18 12:21 208-96-810/11/18 18:43388 91.7 1
Aniline ND ug/kg 10/15/18 12:21 62-53-310/11/18 18:43388 105 1
Anthracene ND ug/kg 10/15/18 12:21 120-12-710/11/18 18:43388 87.0 1
Benzo(a)anthracene ND ug/kg 10/15/18 12:21 56-55-310/11/18 18:43388 71.7 1
Benzo(a)pyrene ND ug/kg 10/15/18 12:21 50-32-810/11/18 18:43388 74.0 1
Benzo(b)fluoranthene ND ug/kg 10/15/18 12:21 205-99-210/11/18 18:43388 67.0 1
Benzo(g,h,i)perylene ND ug/kg 10/15/18 12:21 191-24-210/11/18 18:43388 98.7 1
Benzo(k)fluoranthene ND ug/kg 10/15/18 12:21 207-08-910/11/18 18:43388 76.4 1
Benzoic Acid ND ug/kg 10/15/18 12:21 65-85-010/11/18 18:431940 70.5 1
Benzyl alcohol ND ug/kg 10/15/18 12:21 100-51-610/11/18 18:43776 77.6 1
4-Bromophenylphenyl ether ND ug/kg 10/15/18 12:21 101-55-310/11/18 18:43388 70.5 1
Butylbenzylphthalate ND ug/kg 10/15/18 12:21 85-68-710/11/18 18:43388 82.3 1
4-Chloro-3-methylphenol ND ug/kg 10/15/18 12:21 59-50-710/11/18 18:43776 79.9 1
4-Chloroaniline ND ug/kg 10/15/18 12:21 106-47-810/11/18 18:431940 108 1
bis(2-Chloroethoxy)methane ND ug/kg 10/15/18 12:21 111-91-110/11/18 18:43388 90.5 1
bis(2-Chloroethyl) ether ND ug/kg 10/15/18 12:21 111-44-410/11/18 18:43388 98.7 1
2-Chloronaphthalene ND ug/kg 10/15/18 12:21 91-58-710/11/18 18:43388 76.4 1
2-Chlorophenol ND ug/kg 10/15/18 12:21 95-57-810/11/18 18:43388 106 1
4-Chlorophenylphenyl ether ND ug/kg 10/15/18 12:21 7005-72-310/11/18 18:43388 79.9 1
Chrysene ND ug/kg 10/15/18 12:21 218-01-910/11/18 18:43388 51.7 1
Dibenz(a,h)anthracene ND ug/kg 10/15/18 12:21 53-70-310/11/18 18:43388 82.3 1
Dibenzofuran 76.6J ug/kg 10/15/18 12:21 132-64-910/11/18 18:43388 63.5 1
1,2-Dichlorobenzene ND ug/kg 10/15/18 12:21 95-50-110/11/18 18:43388 103 1
1,3-Dichlorobenzene ND ug/kg 10/15/18 12:21 541-73-110/11/18 18:43388 88.1 1
1,4-Dichlorobenzene ND ug/kg 10/15/18 12:21 106-46-710/11/18 18:43388 109 1
3,3'-Dichlorobenzidine ND ug/kg 10/15/18 12:21 91-94-110/11/18 18:431940 84.6 1
2,4-Dichlorophenol ND ug/kg 10/15/18 12:21 120-83-210/11/18 18:43388 84.6 1
Diethylphthalate ND ug/kg 10/15/18 12:21 84-66-210/11/18 18:43388 59.9 1
2,4-Dimethylphenol ND ug/kg 10/15/18 12:21 105-67-910/11/18 18:43388 153 1
Dimethylphthalate ND ug/kg 10/15/18 12:21 131-11-310/11/18 18:43388 78.7 1
Di-n-butylphthalate ND ug/kg 10/15/18 12:21 84-74-210/11/18 18:43388 63.5 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/15/18 12:21 534-52-110/11/18 18:43776 77.6 1
2,4-Dinitrophenol ND ug/kg 10/15/18 12:21 51-28-510/11/18 18:431940 63.5 1
2,4-Dinitrotoluene ND ug/kg 10/15/18 12:21 121-14-210/11/18 18:43388 72.9 1
2,6-Dinitrotoluene ND ug/kg 10/15/18 12:21 606-20-210/11/18 18:43388 81.1 1
Di-n-octylphthalate ND ug/kg 10/15/18 12:21 117-84-010/11/18 18:43388 81.1 1
bis(2-Ethylhexyl)phthalate 357J ug/kg 10/15/18 12:21 117-81-710/11/18 18:43388 106 1
Fluoranthene ND ug/kg 10/15/18 12:21 206-44-010/11/18 18:43388 56.4 1
Fluorene ND ug/kg 10/15/18 12:21 86-73-710/11/18 18:43388 79.9 1
Hexachloro-1,3-butadiene ND ug/kg 10/15/18 12:21 87-68-310/11/18 18:43388 67.0 1
Hexachlorobenzene ND ug/kg 10/15/18 12:21 118-74-110/11/18 18:43388 49.4 1
Hexachlorocyclopentadiene ND ug/kg 10/15/18 12:21 77-47-410/11/18 18:43388 71.7 1
Hexachloroethane ND ug/kg 10/15/18 12:21 67-72-110/11/18 18:43388 102 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/15/18 12:21 193-39-510/11/18 18:43388 79.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Sample: SP-20181008 Lab ID: 92402528001 Collected: 10/08/18 11:20 Received: 10/08/18 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Isophorone ND ug/kg 10/15/18 12:21 78-59-110/11/18 18:43388 87.0 1
1-Methylnaphthalene 570 ug/kg 10/15/18 12:21 90-12-010/11/18 18:43388 101 1
2-Methylnaphthalene 923 ug/kg 10/15/18 12:21 91-57-610/11/18 18:43388 83.4 1
2-Methylphenol(o-Cresol)ND ug/kg 10/15/18 12:21 95-48-710/11/18 18:43388 118 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/15/18 12:21 15831-10-410/11/18 18:43388 153 1
Naphthalene 357J ug/kg 10/15/18 12:21 91-20-310/11/18 18:43388 95.2 1
2-Nitroaniline ND ug/kg 10/15/18 12:21 88-74-410/11/18 18:431940 120 1
3-Nitroaniline ND ug/kg 10/15/18 12:21 99-09-210/11/18 18:431940 106 1
4-Nitroaniline ND ug/kg 10/15/18 12:21 100-01-610/11/18 18:43776 109 1
Nitrobenzene ND ug/kg 10/15/18 12:21 98-95-310/11/18 18:43388 106 1
2-Nitrophenol ND ug/kg 10/15/18 12:21 88-75-510/11/18 18:43388 94.0 1
4-Nitrophenol ND ug/kg 10/15/18 12:21 100-02-710/11/18 18:431940 69.3 1
N-Nitrosodimethylamine ND ug/kg 10/15/18 12:21 62-75-910/11/18 18:43388 126 1
N-Nitroso-di-n-propylamine ND ug/kg 10/15/18 12:21 621-64-710/11/18 18:43388 74.0 1
N-Nitrosodiphenylamine ND ug/kg 10/15/18 12:21 86-30-610/11/18 18:43388 115 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/15/18 12:21 108-60-1 L110/11/18 18:43388 103 1
Pentachlorophenol ND ug/kg 10/15/18 12:21 87-86-510/11/18 18:431940 70.5 1
Phenanthrene 172J ug/kg 10/15/18 12:21 85-01-810/11/18 18:43388 64.6 1
Phenol ND ug/kg 10/15/18 12:21 108-95-210/11/18 18:43388 116 1
Pyrene ND ug/kg 10/15/18 12:21 129-00-010/11/18 18:43388 65.8 1
1,2,4-Trichlorobenzene ND ug/kg 10/15/18 12:21 120-82-110/11/18 18:43388 75.2 1
2,4,5-Trichlorophenol ND ug/kg 10/15/18 12:21 95-95-410/11/18 18:43388 120 1
2,4,6-Trichlorophenol ND ug/kg 10/15/18 12:21 88-06-210/11/18 18:43388 85.8 1
Surrogates
Nitrobenzene-d5 (S)72 %10/15/18 12:21 4165-60-010/11/18 18:4323-110 1
2-Fluorobiphenyl (S)72 %10/15/18 12:21 321-60-810/11/18 18:4330-110 1
Terphenyl-d14 (S)85 %10/15/18 12:21 1718-51-010/11/18 18:4328-110 1
Phenol-d6 (S)63 %10/15/18 12:21 13127-88-310/11/18 18:4322-110 1
2-Fluorophenol (S)60 %10/15/18 12:21 367-12-410/11/18 18:4313-110 1
2,4,6-Tribromophenol (S)84 %10/15/18 12:21 118-79-610/11/18 18:4327-110 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone ND ug/kg 10/11/18 18:40 67-64-110/11/18 09:1585.1 8.5 1
Benzene ND ug/kg 10/11/18 18:40 71-43-210/11/18 09:154.3 1.4 1
Bromobenzene ND ug/kg 10/11/18 18:40 108-86-110/11/18 09:154.3 1.7 1
Bromochloromethane ND ug/kg 10/11/18 18:40 74-97-510/11/18 09:154.3 1.4 1
Bromodichloromethane ND ug/kg 10/11/18 18:40 75-27-410/11/18 09:154.3 1.6 1
Bromoform ND ug/kg 10/11/18 18:40 75-25-210/11/18 09:154.3 2.0 1
Bromomethane ND ug/kg 10/11/18 18:40 74-83-910/11/18 09:158.5 2.1 1
2-Butanone (MEK)ND ug/kg 10/11/18 18:40 78-93-310/11/18 09:1585.1 2.5 1
n-Butylbenzene ND ug/kg 10/11/18 18:40 104-51-810/11/18 09:154.3 1.5 1
sec-Butylbenzene 2.0J ug/kg 10/11/18 18:40 135-98-810/11/18 09:154.3 1.4 1
tert-Butylbenzene ND ug/kg 10/11/18 18:40 98-06-610/11/18 09:154.3 1.7 1
Carbon tetrachloride ND ug/kg 10/11/18 18:40 56-23-510/11/18 09:154.3 2.2 1
Chlorobenzene ND ug/kg 10/11/18 18:40 108-90-710/11/18 09:154.3 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Sample: SP-20181008 Lab ID: 92402528001 Collected: 10/08/18 11:20 Received: 10/08/18 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Chloroethane ND ug/kg 10/11/18 18:40 75-00-310/11/18 09:158.5 2.0 1
Chloroform ND ug/kg 10/11/18 18:40 67-66-310/11/18 09:154.3 1.4 1
Chloromethane ND ug/kg 10/11/18 18:40 74-87-310/11/18 09:158.5 2.0 1
2-Chlorotoluene ND ug/kg 10/11/18 18:40 95-49-810/11/18 09:154.3 1.4 1
4-Chlorotoluene ND ug/kg 10/11/18 18:40 106-43-410/11/18 09:154.3 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/11/18 18:40 96-12-810/11/18 09:154.3 3.1 1
Dibromochloromethane ND ug/kg 10/11/18 18:40 124-48-110/11/18 09:154.3 1.5 1
1,2-Dibromoethane (EDB)ND ug/kg 10/11/18 18:40 106-93-410/11/18 09:154.3 1.5 1
Dibromomethane ND ug/kg 10/11/18 18:40 74-95-310/11/18 09:154.3 2.1 1
1,2-Dichlorobenzene ND ug/kg 10/11/18 18:40 95-50-110/11/18 09:154.3 1.6 1
1,3-Dichlorobenzene ND ug/kg 10/11/18 18:40 541-73-110/11/18 09:154.3 1.7 1
1,4-Dichlorobenzene ND ug/kg 10/11/18 18:40 106-46-710/11/18 09:154.3 1.4 1
Dichlorodifluoromethane ND ug/kg 10/11/18 18:40 75-71-810/11/18 09:158.5 3.1 1
1,1-Dichloroethane ND ug/kg 10/11/18 18:40 75-34-310/11/18 09:154.3 1.3 1
1,2-Dichloroethane ND ug/kg 10/11/18 18:40 107-06-210/11/18 09:154.3 1.9 1
1,1-Dichloroethene ND ug/kg 10/11/18 18:40 75-35-410/11/18 09:154.3 1.5 1
cis-1,2-Dichloroethene ND ug/kg 10/11/18 18:40 156-59-210/11/18 09:154.3 1.2 1
trans-1,2-Dichloroethene ND ug/kg 10/11/18 18:40 156-60-510/11/18 09:154.3 1.6 1
1,2-Dichloropropane ND ug/kg 10/11/18 18:40 78-87-510/11/18 09:154.3 1.4 1
1,3-Dichloropropane ND ug/kg 10/11/18 18:40 142-28-910/11/18 09:154.3 1.6 1
2,2-Dichloropropane ND ug/kg 10/11/18 18:40 594-20-710/11/18 09:154.3 1.4 1
1,1-Dichloropropene ND ug/kg 10/11/18 18:40 563-58-610/11/18 09:154.3 1.3 1
cis-1,3-Dichloropropene ND ug/kg 10/11/18 18:40 10061-01-510/11/18 09:154.3 1.5 1
trans-1,3-Dichloropropene ND ug/kg 10/11/18 18:40 10061-02-610/11/18 09:154.3 1.3 1
Diisopropyl ether ND ug/kg 10/11/18 18:40 108-20-310/11/18 09:154.3 1.4 1
Ethylbenzene 1.8J ug/kg 10/11/18 18:40 100-41-410/11/18 09:154.3 1.5 1
Hexachloro-1,3-butadiene ND ug/kg 10/11/18 18:40 87-68-310/11/18 09:154.3 1.7 1
2-Hexanone ND ug/kg 10/11/18 18:40 591-78-610/11/18 09:1542.5 3.3 1
Isopropylbenzene (Cumene)ND ug/kg 10/11/18 18:40 98-82-810/11/18 09:154.3 1.6 1
p-Isopropyltoluene 7.3 ug/kg 10/11/18 18:40 99-87-610/11/18 09:154.3 1.4 1
Methylene Chloride ND ug/kg 10/11/18 18:40 75-09-210/11/18 09:1517.0 2.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/11/18 18:40 108-10-110/11/18 09:1542.5 3.1 1
Methyl-tert-butyl ether ND ug/kg 10/11/18 18:40 1634-04-410/11/18 09:154.3 1.3 1
Naphthalene 5.7 ug/kg 10/11/18 18:40 91-20-310/11/18 09:154.3 1.0 1
n-Propylbenzene 6.5 ug/kg 10/11/18 18:40 103-65-110/11/18 09:154.3 1.4 1
Styrene ND ug/kg 10/11/18 18:40 100-42-510/11/18 09:154.3 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/11/18 18:40 630-20-610/11/18 09:154.3 1.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/11/18 18:40 79-34-510/11/18 09:154.3 1.6 1
Tetrachloroethene ND ug/kg 10/11/18 18:40 127-18-410/11/18 09:154.3 1.4 1
Toluene ND ug/kg 10/11/18 18:40 108-88-310/11/18 09:154.3 1.5 1
1,2,3-Trichlorobenzene ND ug/kg 10/11/18 18:40 87-61-610/11/18 09:154.3 1.9 1
1,2,4-Trichlorobenzene ND ug/kg 10/11/18 18:40 120-82-110/11/18 09:154.3 1.4 1
1,1,1-Trichloroethane ND ug/kg 10/11/18 18:40 71-55-610/11/18 09:154.3 1.5 1
1,1,2-Trichloroethane ND ug/kg 10/11/18 18:40 79-00-510/11/18 09:154.3 1.8 1
Trichloroethene ND ug/kg 10/11/18 18:40 79-01-610/11/18 09:154.3 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Sample: SP-20181008 Lab ID: 92402528001 Collected: 10/08/18 11:20 Received: 10/08/18 14:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 10/11/18 18:40 75-69-410/11/18 09:154.3 1.9 1
1,2,3-Trichloropropane ND ug/kg 10/11/18 18:40 96-18-410/11/18 09:154.3 1.4 1
1,2,4-Trimethylbenzene 55.1 ug/kg 10/11/18 18:40 95-63-610/11/18 09:154.3 1.7 1
1,3,5-Trimethylbenzene 21.9 ug/kg 10/11/18 18:40 108-67-810/11/18 09:154.3 1.5 1
Vinyl acetate ND ug/kg 10/11/18 18:40 108-05-410/11/18 09:1542.5 7.5 1
Vinyl chloride ND ug/kg 10/11/18 18:40 75-01-410/11/18 09:158.5 1.5 1
Xylene (Total)14.9 ug/kg 10/11/18 18:40 1330-20-710/11/18 09:158.5 3.1 1
m&p-Xylene 9.0 ug/kg 10/11/18 18:40 179601-23-110/11/18 09:158.5 3.1 1
o-Xylene 5.9 ug/kg 10/11/18 18:40 95-47-610/11/18 09:154.3 1.6 1
Surrogates
Toluene-d8 (S)106 %10/11/18 18:40 2037-26-510/11/18 09:1570-130 1
4-Bromofluorobenzene (S)93 %10/11/18 18:40 460-00-410/11/18 09:1570-130 1
1,2-Dichloroethane-d4 (S)95 %10/11/18 18:40 17060-07-010/11/18 09:1570-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.5 %10/09/18 14:130.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435679
EPA 5035A
EPA 8260B
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92402528001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2397689
Associated Lab Samples:92402528001
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 6.1 10/11/18 12:192.6
1,1,1-Trichloroethane ug/kg ND 6.1 10/11/18 12:192.2
1,1,2,2-Tetrachloroethane ug/kg ND 6.1 10/11/18 12:192.3
1,1,2-Trichloroethane ug/kg ND 6.1 10/11/18 12:192.6
1,1-Dichloroethane ug/kg ND 6.1 10/11/18 12:191.8
1,1-Dichloroethene ug/kg ND 6.1 10/11/18 12:192.2
1,1-Dichloropropene ug/kg ND 6.1 10/11/18 12:191.8
1,2,3-Trichlorobenzene ug/kg ND 6.1 10/11/18 12:192.7
1,2,3-Trichloropropane ug/kg ND 6.1 10/11/18 12:192.0
1,2,4-Trichlorobenzene ug/kg ND 6.1 10/11/18 12:192.0
1,2,4-Trimethylbenzene ug/kg ND 6.1 10/11/18 12:192.4
1,2-Dibromo-3-chloropropane ug/kg ND 6.1 10/11/18 12:194.4
1,2-Dibromoethane (EDB)ug/kg ND 6.1 10/11/18 12:192.2
1,2-Dichlorobenzene ug/kg ND 6.1 10/11/18 12:192.3
1,2-Dichloroethane ug/kg ND 6.1 10/11/18 12:192.7
1,2-Dichloropropane ug/kg ND 6.1 10/11/18 12:192.1
1,3,5-Trimethylbenzene ug/kg ND 6.1 10/11/18 12:192.2
1,3-Dichlorobenzene ug/kg ND 6.1 10/11/18 12:192.4
1,3-Dichloropropane ug/kg ND 6.1 10/11/18 12:192.3
1,4-Dichlorobenzene ug/kg ND 6.1 10/11/18 12:192.1
2,2-Dichloropropane ug/kg ND 6.1 10/11/18 12:192.1
2-Butanone (MEK)ug/kg ND 122 10/11/18 12:193.5
2-Chlorotoluene ug/kg ND 6.1 10/11/18 12:192.1
2-Hexanone ug/kg ND 61.1 10/11/18 12:194.8
4-Chlorotoluene ug/kg ND 6.1 10/11/18 12:192.2
4-Methyl-2-pentanone (MIBK)ug/kg ND 61.1 10/11/18 12:194.5
Acetone ug/kg ND 122 10/11/18 12:1912.2
Benzene ug/kg ND 6.1 10/11/18 12:192.0
Bromobenzene ug/kg ND 6.1 10/11/18 12:192.4
Bromochloromethane ug/kg ND 6.1 10/11/18 12:192.1
Bromodichloromethane ug/kg ND 6.1 10/11/18 12:192.3
Bromoform ug/kg ND 6.1 10/11/18 12:192.8
Bromomethane ug/kg ND 12.2 10/11/18 12:193.1
Carbon tetrachloride ug/kg ND 6.1 10/11/18 12:193.2
Chlorobenzene ug/kg ND 6.1 10/11/18 12:192.3
Chloroethane ug/kg ND 12.2 10/11/18 12:192.9
Chloroform ug/kg ND 6.1 10/11/18 12:192.0
Chloromethane ug/kg ND 12.2 10/11/18 12:192.9
cis-1,2-Dichloroethene ug/kg ND 6.1 10/11/18 12:191.7
cis-1,3-Dichloropropene ug/kg ND 6.1 10/11/18 12:192.2
Dibromochloromethane ug/kg ND 6.1 10/11/18 12:192.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2397689
Associated Lab Samples:92402528001
Matrix: Solid
AnalyzedMDL
Dibromomethane ug/kg ND 6.1 10/11/18 12:193.1
Dichlorodifluoromethane ug/kg ND 12.2 10/11/18 12:194.4
Diisopropyl ether ug/kg ND 6.1 10/11/18 12:192.1
Ethylbenzene ug/kg ND 6.1 10/11/18 12:192.2
Hexachloro-1,3-butadiene ug/kg ND 6.1 10/11/18 12:192.4
Isopropylbenzene (Cumene)ug/kg ND 6.1 10/11/18 12:192.3
m&p-Xylene ug/kg ND 12.2 10/11/18 12:194.4
Methyl-tert-butyl ether ug/kg ND 6.1 10/11/18 12:191.8
Methylene Chloride ug/kg ND 24.4 10/11/18 12:193.7
n-Butylbenzene ug/kg ND 6.1 10/11/18 12:192.2
n-Propylbenzene ug/kg ND 6.1 10/11/18 12:192.1
Naphthalene ug/kg ND 6.1 10/11/18 12:191.5
o-Xylene ug/kg ND 6.1 10/11/18 12:192.3
p-Isopropyltoluene ug/kg ND 6.1 10/11/18 12:192.1
sec-Butylbenzene ug/kg ND 6.1 10/11/18 12:192.0
Styrene ug/kg ND 6.1 10/11/18 12:192.2
tert-Butylbenzene ug/kg ND 6.1 10/11/18 12:192.4
Tetrachloroethene ug/kg ND 6.1 10/11/18 12:192.1
Toluene ug/kg ND 6.1 10/11/18 12:192.2
trans-1,2-Dichloroethene ug/kg ND 6.1 10/11/18 12:192.3
trans-1,3-Dichloropropene ug/kg ND 6.1 10/11/18 12:191.8
Trichloroethene ug/kg ND 6.1 10/11/18 12:192.6
Trichlorofluoromethane ug/kg ND 6.1 10/11/18 12:192.7
Vinyl acetate ug/kg ND 61.1 10/11/18 12:1910.8
Vinyl chloride ug/kg ND 12.2 10/11/18 12:192.2
Xylene (Total)ug/kg ND 12.2 10/11/18 12:194.4
1,2-Dichloroethane-d4 (S)%89 70-132 10/11/18 12:19
4-Bromofluorobenzene (S)%103 70-130 10/11/18 12:19
Toluene-d8 (S)%106 70-130 10/11/18 12:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397690LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 55.561.4 90 74-137
1,1,1-Trichloroethane ug/kg 57.161.4 93 67-140
1,1,2,2-Tetrachloroethane ug/kg 48.761.4 79 72-141
1,1,2-Trichloroethane ug/kg 56.261.4 91 78-138
1,1-Dichloroethane ug/kg 56.361.4 92 69-134
1,1-Dichloroethene ug/kg 61.261.4 100 67-138
1,1-Dichloropropene ug/kg 59.761.4 97 69-139
1,2,3-Trichlorobenzene ug/kg 54.761.4 89 70-146
1,2,3-Trichloropropane ug/kg 56.161.4 91 69-144
1,2,4-Trichlorobenzene ug/kg 54.461.4 89 68-148
1,2,4-Trimethylbenzene ug/kg 56.661.4 92 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397690LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 53.661.4 87 65-140
1,2-Dibromoethane (EDB)ug/kg 57.661.4 94 77-135
1,2-Dichlorobenzene ug/kg 56.961.4 93 77-141
1,2-Dichloroethane ug/kg 55.661.4 91 65-137
1,2-Dichloropropane ug/kg 57.961.4 94 72-136
1,3,5-Trimethylbenzene ug/kg 57.661.4 94 76-133
1,3-Dichlorobenzene ug/kg 55.461.4 90 74-138
1,3-Dichloropropane ug/kg 59.161.4 96 71-139
1,4-Dichlorobenzene ug/kg 55.761.4 91 76-138
2,2-Dichloropropane ug/kg 53.261.4 87 68-137
2-Butanone (MEK)ug/kg 109J123 89 58-147
2-Chlorotoluene ug/kg 57.561.4 94 73-139
2-Hexanone ug/kg 105123 85 62-145
4-Chlorotoluene ug/kg 57.461.4 93 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 104123 85 64-149
Acetone ug/kg 96.2J123 78 53-153
Benzene ug/kg 56.861.4 93 73-135
Bromobenzene ug/kg 57.961.4 94 75-133
Bromochloromethane ug/kg 55.661.4 90 73-134
Bromodichloromethane ug/kg 55.461.4 90 71-135
Bromoform ug/kg 52.061.4 85 66-141
Bromomethane ug/kg 57.561.4 94 53-160
Carbon tetrachloride ug/kg 54.161.4 88 60-145
Chlorobenzene ug/kg 54.461.4 89 78-130
Chloroethane ug/kg 64.161.4 104 64-149
Chloroform ug/kg 54.461.4 89 70-134
Chloromethane ug/kg 48.961.4 80 52-150
cis-1,2-Dichloroethene ug/kg 55.361.4 90 70-133
cis-1,3-Dichloropropene ug/kg 55.361.4 90 68-134
Dibromochloromethane ug/kg 56.461.4 92 71-138
Dibromomethane ug/kg 52.461.4 85 74-130
Dichlorodifluoromethane ug/kg 51.761.4 84 40-160
Diisopropyl ether ug/kg 56.461.4 92 69-141
Ethylbenzene ug/kg 56.061.4 91 75-133
Hexachloro-1,3-butadiene ug/kg 53.561.4 87 68-143
Isopropylbenzene (Cumene)ug/kg 56.561.4 92 76-143
m&p-Xylene ug/kg 112123 91 75-136
Methyl-tert-butyl ether ug/kg 59.961.4 97 68-144
Methylene Chloride ug/kg 59.961.4 98 45-154
n-Butylbenzene ug/kg 57.161.4 93 72-137
n-Propylbenzene ug/kg 59.761.4 97 76-136
Naphthalene ug/kg 56.161.4 91 68-151
o-Xylene ug/kg 56.761.4 92 76-141
p-Isopropyltoluene ug/kg 54.961.4 89 76-140
sec-Butylbenzene ug/kg 58.661.4 95 79-139
Styrene ug/kg 54.461.4 89 79-137
tert-Butylbenzene ug/kg 53.361.4 87 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397690LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 50.461.4 82 71-138
Toluene ug/kg 52.661.4 86 74-131
trans-1,2-Dichloroethene ug/kg 57.361.4 93 67-135
trans-1,3-Dichloropropene ug/kg 54.261.4 88 65-146
Trichloroethene ug/kg 62.261.4 101 67-135
Trichlorofluoromethane ug/kg 65.161.4 106 59-144
Vinyl acetate ug/kg 68.1123 55 40-160
Vinyl chloride ug/kg 61.861.4 101 56-141
Xylene (Total)ug/kg 169184 92 76-137
1,2-Dichloroethane-d4 (S)%99 70-132
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397691MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397692
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg M1,R1187270-13037 33 3025.4ND 13.0 9.3
1,1,1-Trichloroethane ug/kg M1188070-13022 3025.4ND 14.4 5.7J
1,1,2,2-Tetrachloroethane ug/kg M1,R1186970-13071 37 3025.4ND 12.5 18.1
1,1,2-Trichloroethane ug/kg M1187370-13067 26 3025.4ND 13.2 17.1
1,1-Dichloroethane ug/kg M1,R1188070-13036 46 3025.4ND 14.4 9.1
1,1-Dichloroethene ug/kg M1188649-18023 3025.4ND 15.4 5.9J
1,1-Dichloropropene ug/kg M1187670-13018 3025.4ND 13.7 4.6J
1,2,3-Trichlorobenzene ug/kg M1183270-13027 17 3025.4ND 5.8 6.9
1,2,3-Trichloropropane ug/kg R1187570-13076 35 3025.4ND 13.6 19.3
1,2,4-Trichlorobenzene ug/kg M1183570-13026 2 3025.4ND 6.4 6.5
1,2,4-Trimethylbenzene ug/kg M1,R1187770-13033 50 3025.4ND 13.8 8.3
1,2-Dibromo-3-
chloropropane ug/kg M1,R1186370-13070 44 3025.4ND 11.4 17.9
1,2-Dibromoethane (EDB) ug/kg M1187070-13059 18 3025.4ND 12.6 15.1
1,2-Dichlorobenzene ug/kg M1186070-13041 4 3025.4ND 10.8 10.3
1,2-Dichloroethane ug/kg R1187270-13070 31 3025.4ND 13.0 17.8
1,2-Dichloropropane ug/kg M1187970-13042 30 3025.4ND 14.2 10.6
1,3,5-Trimethylbenzene ug/kg M1,R1187970-13030 60 3025.4ND 14.3 7.7
1,3-Dichlorobenzene ug/kg M1186370-13035 25 3025.4ND 11.4 8.9
1,3-Dichloropropane ug/kg M1187770-13056 3 3025.4ND 13.9 14.2
1,4-Dichlorobenzene ug/kg M1186170-13034 24 3025.4ND 11.1 8.7
2,2-Dichloropropane ug/kg M1187670-13020 3025.4ND 13.7 5.1J
2-Butanone (MEK)ug/kg M136.1 50 70-13056 3050.8ND 18.2J 28.4J
2-Chlorotoluene ug/kg M1,R1187970-13038 38 3025.4ND 14.2 9.7
2-Hexanone ug/kg M136.1 37 70-13033 3050.8ND 13.4J 16.9J
4-Chlorotoluene ug/kg M1,R1187470-13037 36 3025.4ND 13.4 9.3
4-Methyl-2-pentanone
(MIBK)ug/kg M136.1 67 70-13084 3050.8ND 24.0J 42.6J
Acetone ug/kg M136.1 59 70-130133 3050.818.2J 39.6J 86.0J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397691MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397692
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene ug/kg M1,R1188050-16635 49 3025.4ND 14.5 8.8
Bromobenzene ug/kg M1187670-13044 19 3025.4ND 13.7 11.3
Bromochloromethane ug/kg M1187370-13056 9 3025.4ND 13.1 14.3
Bromodichloromethane ug/kg M1187670-13048 13 3025.4ND 13.8 12.2
Bromoform ug/kg M1185470-13048 21 3025.4ND 9.8 12.1
Bromomethane ug/kg M1188070-13031 3025.4ND 14.5 7.9J
Carbon tetrachloride ug/kg M1188170-13019 3025.4ND 14.5 4.9J
Chlorobenzene ug/kg M1,R1187243-16936 34 3025.4ND 12.9 9.2
Chloroethane ug/kg M1189270-13030 3025.4ND 16.6 7.7J
Chloroform ug/kg M1188170-13047 20 3025.4ND 14.7 12.1
Chloromethane ug/kg M1187070-13023 3025.4ND 12.7 5.7J
cis-1,2-Dichloroethene ug/kg M1187770-13043 24 3025.4ND 14.0 11.0
cis-1,3-Dichloropropene ug/kg M1185670-13031 25 3025.4ND 10.1 7.9
Dibromochloromethane ug/kg M1186570-13047 3 3025.4ND 11.7 12.0
Dibromomethane ug/kg M1187470-13066 22 3025.4ND 13.3 16.7
Dichlorodifluoromethane ug/kg M1187370-13010 3025.4ND 13.2 ND
Diisopropyl ether ug/kg M1187670-13052 3 3025.4ND 13.7 13.3
Ethylbenzene ug/kg M1,R1188070-13030 63 3025.4ND 14.4 7.5
Hexachloro-1,3-butadiene ug/kg M1184470-13015 3025.4ND 7.9 3.8J
Isopropylbenzene (Cumene) ug/kg M1,R1187770-13027 69 3025.4ND 13.9 6.8
m&p-Xylene ug/kg M1,R136.1 78 70-13031 57 3050.8ND 28.3 15.8
Methyl-tert-butyl ether ug/kg R1187470-13072 31 3025.4ND 13.3 18.2
Methylene Chloride ug/kg M1187370-13042 3025.4ND 13.3J 10.6J
n-Butylbenzene ug/kg M1186770-13020 3025.4ND 12.1 5.1J
n-Propylbenzene ug/kg M1,R1188970-13029 75 3025.4ND 16.1 7.3
Naphthalene ug/kg M1184470-13038 20 3025.4ND 8.0 9.7
o-Xylene ug/kg M1,R1187670-13035 43 3025.4ND 13.8 8.9
p-Isopropyltoluene ug/kg M1187270-13022 3025.4ND 13.0 5.6J
sec-Butylbenzene ug/kg M1188270-13023 3025.4ND 14.8 5.9J
Styrene ug/kg M1186070-13032 29 3025.4ND 10.9 8.2
tert-Butylbenzene ug/kg M1,R1187770-13026 71 3025.4ND 13.9 6.6
Tetrachloroethene ug/kg M1187070-13019 3025.4ND 12.7 4.9J
Toluene ug/kg M1,R1187652-16334 46 3025.4ND 13.8 8.7
trans-1,2-Dichloroethene ug/kg M1,R1188670-13030 67 3025.4ND 15.5 7.7
trans-1,3-Dichloropropene ug/kg M1185870-13043 3 3025.4ND 10.5 10.8
Trichloroethene ug/kg M1187849-16722 3025.4ND 14.0 5.5J
Trichlorofluoromethane ug/kg M1189470-13018 3025.4ND 17.0 4.5J
Vinyl acetate ug/kg M136.1 9 70-1307 3050.8ND ND ND
Vinyl chloride ug/kg M1188670-13022 3025.4ND 15.6 5.5J
Xylene (Total)ug/kg MS,RS54.1 78 70-13032 52 3076.2ND 42.1 24.7
1,2-Dichloroethane-d4 (S)%94 70-132131
4-Bromofluorobenzene (S) %98 70-130100
Toluene-d8 (S)%99 70-130105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435704
EPA 3546
EPA 8270D
8270 Solid MSSV Microwave
Associated Lab Samples: 92402528001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2397791
Associated Lab Samples:92402528001
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 327 10/15/18 11:5363.4
1,2-Dichlorobenzene ug/kg ND 327 10/15/18 11:5387.1
1,3-Dichlorobenzene ug/kg ND 327 10/15/18 11:5374.3
1,4-Dichlorobenzene ug/kg ND 327 10/15/18 11:5392.1
1-Methylnaphthalene ug/kg ND 327 10/15/18 11:5385.1
2,2'-Oxybis(1-chloropropane)ug/kg ND 327 10/15/18 11:5387.1
2,4,5-Trichlorophenol ug/kg ND 327 10/15/18 11:53101
2,4,6-Trichlorophenol ug/kg ND 327 10/15/18 11:5372.3
2,4-Dichlorophenol ug/kg ND 327 10/15/18 11:5371.3
2,4-Dimethylphenol ug/kg ND 327 10/15/18 11:53129
2,4-Dinitrophenol ug/kg ND 1630 10/15/18 11:5353.5
2,4-Dinitrotoluene ug/kg ND 327 10/15/18 11:5361.4
2,6-Dinitrotoluene ug/kg ND 327 10/15/18 11:5368.3
2-Chloronaphthalene ug/kg ND 327 10/15/18 11:5364.4
2-Chlorophenol ug/kg ND 327 10/15/18 11:5389.1
2-Methylnaphthalene ug/kg ND 327 10/15/18 11:5370.3
2-Methylphenol(o-Cresol)ug/kg ND 327 10/15/18 11:5399.0
2-Nitroaniline ug/kg ND 1630 10/15/18 11:53101
2-Nitrophenol ug/kg ND 327 10/15/18 11:5379.2
3&4-Methylphenol(m&p Cresol)ug/kg ND 327 10/15/18 11:53129
3,3'-Dichlorobenzidine ug/kg 76.6J 1630 10/15/18 11:5371.3
3-Nitroaniline ug/kg ND 1630 10/15/18 11:5389.1
4,6-Dinitro-2-methylphenol ug/kg ND 653 10/15/18 11:5365.3
4-Bromophenylphenyl ether ug/kg ND 327 10/15/18 11:5359.4
4-Chloro-3-methylphenol ug/kg ND 653 10/15/18 11:5367.3
4-Chloroaniline ug/kg ND 1630 10/15/18 11:5391.1
4-Chlorophenylphenyl ether ug/kg ND 327 10/15/18 11:5367.3
4-Nitroaniline ug/kg ND 653 10/15/18 11:5392.1
4-Nitrophenol ug/kg 265J 1630 10/15/18 11:5358.4
Acenaphthene ug/kg ND 327 10/15/18 11:5375.2
Acenaphthylene ug/kg ND 327 10/15/18 11:5377.2
Aniline ug/kg ND 327 10/15/18 11:5388.1
Anthracene ug/kg ND 327 10/15/18 11:5373.3
Benzo(a)anthracene ug/kg 67.3J 327 10/15/18 11:5360.4
Benzo(a)pyrene ug/kg ND 327 10/15/18 11:5362.4
Benzo(b)fluoranthene ug/kg ND 327 10/15/18 11:5356.4
Benzo(g,h,i)perylene ug/kg ND 327 10/15/18 11:5383.2
Benzo(k)fluoranthene ug/kg ND 327 10/15/18 11:5364.4
Benzoic Acid ug/kg ND 1630 10/15/18 11:5359.4
Benzyl alcohol ug/kg ND 653 10/15/18 11:5365.3
bis(2-Chloroethoxy)methane ug/kg ND 327 10/15/18 11:5376.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2397791
Associated Lab Samples:92402528001
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 327 10/15/18 11:5383.2
bis(2-Ethylhexyl)phthalate ug/kg ND 327 10/15/18 11:5389.1
Butylbenzylphthalate ug/kg ND 327 10/15/18 11:5369.3
Chrysene ug/kg 67.1J 327 10/15/18 11:5343.6
Di-n-butylphthalate ug/kg ND 327 10/15/18 11:5353.5
Di-n-octylphthalate ug/kg ND 327 10/15/18 11:5368.3
Dibenz(a,h)anthracene ug/kg ND 327 10/15/18 11:5369.3
Dibenzofuran ug/kg ND 327 10/15/18 11:5353.5
Diethylphthalate ug/kg ND 327 10/15/18 11:5350.5
Dimethylphthalate ug/kg ND 327 10/15/18 11:5366.3
Fluoranthene ug/kg 58.2J 327 10/15/18 11:5347.5
Fluorene ug/kg ND 327 10/15/18 11:5367.3
Hexachloro-1,3-butadiene ug/kg ND 327 10/15/18 11:5356.4
Hexachlorobenzene ug/kg ND 327 10/15/18 11:5341.6
Hexachlorocyclopentadiene ug/kg ND 327 10/15/18 11:5360.4
Hexachloroethane ug/kg ND 327 10/15/18 11:5386.1
Indeno(1,2,3-cd)pyrene ug/kg ND 327 10/15/18 11:5367.3
Isophorone ug/kg ND 327 10/15/18 11:5373.3
N-Nitroso-di-n-propylamine ug/kg ND 327 10/15/18 11:5362.4
N-Nitrosodimethylamine ug/kg ND 327 10/15/18 11:53106
N-Nitrosodiphenylamine ug/kg ND 327 10/15/18 11:5397.0
Naphthalene ug/kg ND 327 10/15/18 11:5380.2
Nitrobenzene ug/kg ND 327 10/15/18 11:5389.1
Pentachlorophenol ug/kg 97.5J 1630 10/15/18 11:5359.4
Phenanthrene ug/kg ND 327 10/15/18 11:5354.5
Phenol ug/kg ND 327 10/15/18 11:5398.0
Pyrene ug/kg 76.3J 327 10/15/18 11:5355.4
2,4,6-Tribromophenol (S)%91 27-110 10/15/18 11:53
2-Fluorobiphenyl (S)%80 30-110 10/15/18 11:53
2-Fluorophenol (S)%79 13-110 10/15/18 11:53
Nitrobenzene-d5 (S)%85 23-110 10/15/18 11:53
Phenol-d6 (S)%81 22-110 10/15/18 11:53
Terphenyl-d14 (S)%122 28-110 S310/15/18 11:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397792LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13601660 82 36-120
1,2-Dichlorobenzene ug/kg 14001660 85 41-120
1,3-Dichlorobenzene ug/kg 13901660 84 66-120
1,4-Dichlorobenzene ug/kg 14001660 85 42-120
1-Methylnaphthalene ug/kg 16301660 98 40-120
2,2'-Oxybis(1-chloropropane)ug/kg 2200 L11660133 17-120
2,4,5-Trichlorophenol ug/kg 14301660 87 37-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397792LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 15101660 91 40-120
2,4-Dichlorophenol ug/kg 14601660 88 33-120
2,4-Dimethylphenol ug/kg 17001660 102 36-120
2,4-Dinitrophenol ug/kg 67508280 82 22-121
2,4-Dinitrotoluene ug/kg 15801660 95 60-120
2,6-Dinitrotoluene ug/kg 16501660 100 54-120
2-Chloronaphthalene ug/kg 16601660 100 41-120
2-Chlorophenol ug/kg 15401660 93 39-120
2-Methylnaphthalene ug/kg 16801660 102 26-120
2-Methylphenol(o-Cresol)ug/kg 16001660 97 41-120
2-Nitroaniline ug/kg 32703310 99 45-120
2-Nitrophenol ug/kg 14201660 86 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 16401660 99 35-120
3,3'-Dichlorobenzidine ug/kg 31403310 95 16-125
3-Nitroaniline ug/kg 31103310 94 45-120
4,6-Dinitro-2-methylphenol ug/kg 31203310 94 46-120
4-Bromophenylphenyl ether ug/kg 16501660 100 36-120
4-Chloro-3-methylphenol ug/kg 32103310 97 37-120
4-Chloroaniline ug/kg 28803310 87 35-120
4-Chlorophenylphenyl ether ug/kg 15601660 95 30-120
4-Nitroaniline ug/kg 30103310 91 48-120
4-Nitrophenol ug/kg 72108280 87 43-120
Acenaphthene ug/kg 15801660 95 46-120
Acenaphthylene ug/kg 15901660 96 46-120
Aniline ug/kg 14101660 85 33-120
Anthracene ug/kg 16101660 97 63-120
Benzo(a)anthracene ug/kg 15401660 93 61-120
Benzo(a)pyrene ug/kg 16101660 97 59-120
Benzo(b)fluoranthene ug/kg 16701660 101 55-120
Benzo(g,h,i)perylene ug/kg 16301660 98 57-120
Benzo(k)fluoranthene ug/kg 16401660 99 56-120
Benzoic Acid ug/kg 70208280 85 13-120
Benzyl alcohol ug/kg 33803310 102 34-120
bis(2-Chloroethoxy)methane ug/kg 18501660 112 21-120
bis(2-Chloroethyl) ether ug/kg 17001660 103 25-120
bis(2-Ethylhexyl)phthalate ug/kg 16301660 98 56-123
Butylbenzylphthalate ug/kg 16101660 97 57-120
Chrysene ug/kg 15501660 93 64-120
Di-n-butylphthalate ug/kg 16201660 98 58-120
Di-n-octylphthalate ug/kg 18101660 109 47-121
Dibenz(a,h)anthracene ug/kg 16601660 100 56-120
Dibenzofuran ug/kg 16001660 97 43-120
Diethylphthalate ug/kg 15101660 91 55-120
Dimethylphthalate ug/kg 14301660 86 54-120
Fluoranthene ug/kg 14701660 89 61-120
Fluorene ug/kg 16201660 98 51-120
Hexachloro-1,3-butadiene ug/kg 14701660 89 22-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397792LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 15301660 92 53-120
Hexachlorocyclopentadiene ug/kg 15401660 93 18-150
Hexachloroethane ug/kg 15401660 93 39-120
Indeno(1,2,3-cd)pyrene ug/kg 16201660 98 58-120
Isophorone ug/kg 14901660 90 38-120
N-Nitroso-di-n-propylamine ug/kg 17501660 106 30-120
N-Nitrosodimethylamine ug/kg 16901660 102 32-120
N-Nitrosodiphenylamine ug/kg 15801660 95 50-120
Naphthalene ug/kg 15401660 93 38-120
Nitrobenzene ug/kg 15901660 96 37-120
Pentachlorophenol ug/kg 25603310 77 10-120
Phenanthrene ug/kg 15701660 95 62-120
Phenol ug/kg 17301660 105 37-120
Pyrene ug/kg 15701660 95 63-120
2,4,6-Tribromophenol (S)%91 27-110
2-Fluorobiphenyl (S)%83 30-110
2-Fluorophenol (S)%88 13-110
Nitrobenzene-d5 (S)%89 23-110
Phenol-d6 (S)%94 22-110
Terphenyl-d14 (S)%109 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397793MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397794
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1770 50 18-11942 18 301750ND885 740
1,2-Dichlorobenzene ug/kg M117705150-11041 21 301750ND894 721
1,3-Dichlorobenzene ug/kg 1770 49 27-11041 21 301750ND871 708
1,4-Dichlorobenzene ug/kg 1770 50 28-11041 23 301750ND893 710
1-Methylnaphthalene ug/kg 1770 59 24-11654 9 301750ND1040 944
2,2'-Oxybis(1-chloropropane) ug/kg 1770 72 50-15059 22 301750ND1270 1030
2,4,5-Trichlorophenol ug/kg 1770 59 28-11057 5 301750ND1040 986
2,4,6-Trichlorophenol ug/kg 1770 61 17-11758 7 301750ND1080 1010
2,4-Dichlorophenol ug/kg 1770 53 21-12848 11 301750ND942 845
2,4-Dimethylphenol ug/kg 1770 48 10-12049 0 301750ND851 852
2,4-Dinitrophenol ug/kg 8850 34 10-10736 4 308720ND2970 3100
2,4-Dinitrotoluene ug/kg 1770 60 36-10962 1 301750ND1060 1080
2,6-Dinitrotoluene ug/kg 1770 62 32-11062 1 301750ND1090 1080
2-Chloronaphthalene ug/kg 1770 55 30-10751 8 301750ND969 898
2-Chlorophenol ug/kg 1770 54 14-10643 23 301750ND947 755
2-Methylnaphthalene ug/kg 1770 59 10-13554 11 301750ND1050 942
2-Methylphenol(o-Cresol) ug/kg 1770 53 10-12445 18 301750ND944 789
2-Nitroaniline ug/kg 3540 60 26-11659 3 303490ND2120 2060
2-Nitrophenol ug/kg 1770 49 28-10342 18 301750ND871 726
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397793MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397794
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/kg 1770 51 10-10947 9 301750ND895 816
3,3'-Dichlorobenzidine ug/kg 3540 47 10-15052 303490ND1660J 1810
3-Nitroaniline ug/kg 3540 54 22-11058 5 303490ND1920 2030
4,6-Dinitro-2-methylphenol ug/kg 3540 53 13-12161 12 303490ND1880 2110
4-Bromophenylphenyl ether ug/kg 1770 69 31-10969 2 301750ND1230 1200
4-Chloro-3-methylphenol ug/kg 3540 59 13-12859 2 303490ND2100 2050
4-Chloroaniline ug/kg 3540 48 18-10246 303490ND1680J 1610J
4-Chlorophenylphenyl ether ug/kg 1770 60 29-11260 2 301750ND1060 1040
4-Nitroaniline ug/kg 3540 54 16-11159 8 303490ND1900 2070
4-Nitrophenol ug/kg 8850 50 14-13557 10 308720ND4460 4950
Acenaphthene ug/kg 1770 58 26-11458 2 301750ND1020 1010
Acenaphthylene ug/kg 1770 58 32-10858 1 301750ND1030 1010
Aniline ug/kg 1770 39 10-10735 12 301750ND690 614
Anthracene ug/kg 1770 63 32-11163 1 301750ND1120 1100
Benzo(a)anthracene ug/kg 1770 57 25-11759 2 301750ND1010 1030
Benzo(a)pyrene ug/kg 1770 62 25-10663 1 301750ND1090 1100
Benzo(b)fluoranthene ug/kg 1770 59 24-11060 0 301750ND1050 1050
Benzo(g,h,i)perylene ug/kg 1770 62 19-11264 2 301750ND1100 1130
Benzo(k)fluoranthene ug/kg 1770 61 24-11461 1 301750ND1080 1070
Benzoic Acid ug/kg 8850 22 10-11020 308720ND1920 1720J
Benzyl alcohol ug/kg 3540 58 24-10650 16 303490ND2060 1760
bis(2-Chloroethoxy)methane ug/kg 1770 60 13-11953 15 301750ND1070 924
bis(2-Chloroethyl) ether ug/kg 1770 57 10-13449 17 301750ND1010 852
bis(2-Ethylhexyl)phthalate ug/kg 1770 59 10-12561 2 301750ND1040 1060
Butylbenzylphthalate ug/kg 1770 58 18-11058 1 301750ND1020 1010
Chrysene ug/kg 1770 58 30-11059 0 301750ND1020 1030
Di-n-butylphthalate ug/kg 1770 64 19-11264 1 301750ND1130 1120
Di-n-octylphthalate ug/kg 1770 65 17-10568 3 301750ND1150 1190
Dibenz(a,h)anthracene ug/kg 1770 66 23-11167 0 301750ND1170 1170
Dibenzofuran ug/kg 1770 60 35-10361 1 301750ND1070 1060
Diethylphthalate ug/kg 1770 58 27-11359 1 301750ND1030 1040
Dimethylphthalate ug/kg 1770 57 26-11156 2 301750ND1000 977
Fluoranthene ug/kg 1770 61 33-10960 2 301750ND1080 1050
Fluorene ug/kg 1770 61 32-11361 0 301750ND1070 1070
Hexachloro-1,3-butadiene ug/kg 1770 54 16-11646 17 301750ND959 809
Hexachlorobenzene ug/kg 1770 66 27-12065 3 301750ND1170 1140
Hexachlorocyclopentadiene ug/kg 1770 41 10-10833 23 301750ND720 574
Hexachloroethane ug/kg 1770 54 10-11743 23 301750ND955 754
Indeno(1,2,3-cd)pyrene ug/kg 1770 64 10-12265 1 301750ND1130 1140
Isophorone ug/kg 1770 51 28-11447 8 301750ND895 829
N-Nitroso-di-n-propylamine ug/kg 1770 57 27-11351 13 301750ND1010 882
N-Nitrosodimethylamine ug/kg 1770 55 10-10943 25 301750ND969 755
N-Nitrosodiphenylamine ug/kg 1770 64 10-12864 1 301750ND1130 1120
Naphthalene ug/kg 1770 54 25-11046 18 301750ND956 800
Nitrobenzene ug/kg 1770 52 18-11445 16 301750ND916 781
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397793MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402661001
2397794
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pentachlorophenol ug/kg 3540 45 10-12252 303490ND1600J 1810
Phenanthrene ug/kg 1770 63 30-11464 1 301750ND1110 1110
Phenol ug/kg 1770 54 11-10247 16 301750ND960 814
Pyrene ug/kg 1770 55 25-11655 0 301750ND965 968
2,4,6-Tribromophenol (S)%73 27-11073
2-Fluorobiphenyl (S)%55 30-11050
2-Fluorophenol (S)%50 13-11040
Nitrobenzene-d5 (S)%51 23-11043
Phenol-d6 (S)%52 22-11044
Terphenyl-d14 (S)%74 28-11071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435049
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92402528001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92402531001
2395073SAMPLE DUPLICATE:
Percent Moisture %17.6 2 2517.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92402529002
2395097SAMPLE DUPLICATE:
Percent Moisture %22.5 3 2523.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 39
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
RPD value was outside control limits.R1
The RPD value in one of the constituent analytes was outside the control limits.RS
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 39
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92402528
Kannapolis, NC Site (KAN-012)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92402528001 435704 436214SP-20181008 EPA 3546 EPA 8270D
92402528001 435679 435689SP-20181008 EPA 5035A EPA 8260B
92402528001 435049SP-20181008 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2018 09:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 39
Page 23 of 39
Page 24 of 39
Page 25 of 39
ANALYTICAL REPORT
October 16, 2018
Pace Analytical - Huntersville, NC
Sample Delivery Group:L1032837
Samples Received:10/09/2018
Project Number:92402528
Description:Kannapolis, NC Site (Kan-012)
Report To:Kevin Godwin
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By:
October 16, 2018
[Preliminary Report]
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Nationalis performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
October 16, 2018
Jason Romer
Project Manager
Page 26 of 39
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
SP-20181008 L1032837-01 5
Qc: Quality Control Summary 6
Total Solids by Method 2540 G-2011 6
Wet Chemistry by Method 7199 7
Mercury by Method 7471B 8
Metals (ICPMS) by Method 6020B 9
Gl: Glossary of Terms 11
Al: Accreditations & Locations 12
Sc: Sample Chain of Custody 13
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SP-20181008 L1032837-01 Solid 10/08/18 11:20 10/09/18 08:45
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG1179223 1 10/11/18 11:34 10/11/18 11:45 JD
Wet Chemistry by Method 7199 WG1179761 1 10/12/18 16:14 10/12/18 21:19 GB
Mercury by Method 7471B WG1178441 1 10/09/18 18:40 10/11/18 12:26 ABL
Metals (ICPMS) by Method 6020B WG1178442 5 10/10/18 10:36 10/11/18 00:14 JDG
Metals (ICPMS) by Method 6020B WG1178442 5 10/10/18 10:36 10/11/18 03:04 JDG
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Nancy McLain
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Jason Romer
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1032837
SP-20181008
Collected date/time: 10/08/18 11:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.9 1 10/11/2018 11:45 WG1179223
Wet Chemistry by Method 7199
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Hexavalent Chromium U 0.307 1.21 1 10/12/2018 21:19 WG1179761
Mercury by Method 7471B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Mercury 0.0403 0.00338 0.0241 1 10/11/2018 12:26 WG1178441
Metals (ICPMS) by Method 6020B
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Arsenic 2.32 0.0151 0.603 5 10/11/2018 00:14 WG1178442
Barium 155 0.193 1.21 5 10/11/2018 00:14 WG1178442
Cadmium U 0.0965 0.603 5 10/11/2018 00:14 WG1178442
Chromium 11.0 0.326 1.21 5 10/11/2018 00:14 WG1178442
Lead 30.7 0.145 0.603 5 10/11/2018 00:14 WG1178442
Selenium 1.20 0.229 0.603 5 10/11/2018 03:04 WG1178442
Silver U 0.187 0.603 5 10/11/2018 00:14 WG1178442
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1179223
Total Solids by Method 2540 G-2011 L1032837-01
Method Blank (MB)
(MB) R3350007-1 10/11/18 11:45
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1033455-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1033455-01 10/11/18 11:45 • (DUP) R3350007-3 10/11/18 11:45
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 60.6 58.3 1 3.70 10
Laboratory Control Sample (LCS)
(LCS) R3350007-2 10/11/18 11:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1179761
Wet Chemistry by Method 7199 L1032837-01
Method Blank (MB)
(MB) R3350745-1 10/12/18 19:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1032837-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1032837-01 10/12/18 21:19 • (DUP) R3350745-8 10/12/18 21:25
Original Result
(dry)
DUP Result
(dry)Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium U 0.000 1 0.000 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3350745-2 10/12/18 19:46 • (LCSD) R3350745-3 10/12/18 19:52
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 10.0 9.95 10.0 99.5 100 80.0-120 0.809 20
L1032035-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1032035-01 10/12/18 20:11 • (MS) R3350745-4 10/12/18 20:17 • (MSD) R3350745-5 10/12/18 20:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 20.0 9.41 30.2 29.5 104 100 1 75.0-125 2.43 20
L1032035-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1032035-01 10/12/18 20:11 • (MS) R3350745-6 10/12/18 20:29
Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 720 9.41 648 90.0 50 75.0-125
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1178441
Mercury by Method 7471B L1032837-01
Method Blank (MB)
(MB) R3349732-1 10/11/18 11:31
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.00280 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3349732-2 10/11/18 11:34 • (LCSD) R3349732-3 10/11/18 11:37
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.281 0.270 93.6 90.1 80.0-120 3.83 20
L1032550-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1032550-01 10/11/18 11:39 • (MS) R3349732-4 10/11/18 11:42 • (MSD) R3349732-5 10/11/18 11:44
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.300 0.0192 0.267 0.250 82.7 76.8 1 75.0-125 6.83 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1178442
Metals (ICPMS) by Method 6020B L1032837-01
Method Blank (MB)
(MB) R3349772-1 10/10/18 23:00
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.0125 0.500
Barium U 0.160 1.00
Cadmium U 0.0800 0.500
Chromium U 0.270 1.00
Lead U 0.120 0.500
Silver U 0.155 0.500
Method Blank (MB)
(MB) R3349772-8 10/11/18 02:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Selenium U 0.190 0.500
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3349772-2 10/10/18 23:04 • (LCSD) R3349772-3 10/10/18 23:08
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Arsenic 100 97.7 96.7 97.7 96.7 80.0-120 0.961 20
Barium 100 94.9 94.8 94.9 94.8 80.0-120 0.0777 20
Cadmium 100 100 100 100 100 80.0-120 0.203 20
Chromium 100 99.5 98.2 99.5 98.2 80.0-120 1.32 20
Lead 100 94.7 95.4 94.7 95.4 80.0-120 0.760 20
Silver 20.0 20.2 20.2 101 101 80.0-120 0.405 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3349772-9 10/11/18 02:10 • (LCSD) R3349772-10 10/11/18 02:14
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Selenium 100 93.3 96.7 93.3 96.7 80.0-120 3.53 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1178442
Metals (ICPMS) by Method 6020B L1032837-01
L1032452-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1032452-02 10/10/18 23:12 • (MS) R3349772-6 10/10/18 23:24 • (MSD) R3349772-7 10/10/18 23:28
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 20.0 2.00 94.3 102 92.3 99.8 5 75.0-125 7.60 20
Barium 20.0 36.0 125 130 89.1 94.2 5 75.0-125 4.02 20
Cadmium 20.0 0.225 97.2 103 96.9 103 5 75.0-125 5.90 20
Chromium 20.0 5.06 99.2 107 94.2 102 5 75.0-125 7.84 20
Lead 20.0 11.8 102 106 90.2 94.6 5 75.0-125 4.23 20
Silver 4.00 U 19.7 20.6 98.3 103 5 75.0-125 4.90 20
L1032452-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1032452-02 10/11/18 02:18 • (MS) R3349772-13 10/11/18 02:30 • (MSD) R3349772-14 10/11/18 02:34
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Selenium 20.0 0.263 93.7 97.7 93.5 97.4 5 75.0-125 4.11 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T 104704245-17-14
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
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