15035_Sun Chemical_BAR_20120106

Brownfields Site Assessment Report
Sun Chemical Facility
Charlotte, North Carolina
Brownfields Project No. 15035-11-60

H&H Job No. PPA-038

January 6, 2012
2923 South Tryon Street
Suite 100 Charlotte, NC 28203
704-586-0007
3334 Hillsborough Street
Raleigh, NC 27607 919-847-4241
#C-1269 Engineering #C-245 Geology

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Brownfields Site Assessment Report Sun Chemical Facility
Charlotte, North Carolina
H&H Job No. PPA-038 Table of Contents
Section Page No.

1.0 Introduction and Background ................................................................................................. 1
2.0 Soil and Groundwater Assessment .......................................................................................... 3
2.1 General Field Practices ......................................................................................................... 3
2.2 Soil Sampling Procedures .................................................................................................... 3
2.3 Soil Analytical Results ......................................................................................................... 5
2.4 Temporary Monitoring Well Installation ............................................................................. 6
2.5 Groundwater Flow ................................................................................................................ 7
2.6 Groundwater Sampling Procedures ...................................................................................... 7
2.7 Groundwater Analytical Results .......................................................................................... 8
3.0 Soil Vapor Assessment ............................................................................................................ 11
3.1 Sub-Slab Vapor Sampling Methods ................................................................................... 11
3.2 Sub-Slab Vapor Results ...................................................................................................... 12
3.3 Helium Tracer Gas Testing ................................................................................................ 13
4.0 Summary and Conclusions ..................................................................................................... 14

List of Tables

Table 1 Summary of Soil Analytical Data
Table 2 Summary of Monitoring Well Construction and Groundwater Elevation Data
Table 3 Summary of Groundwater Analytical Data
Table 4 Summary of Historical Groundwater Analytical Data
Table 5 Helium Shroud Readings
Table 6 Summary of Soil Gas Analytical Data

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List of Figures
Figure 1 Site Location Map
Figure 2 Site Map and Sample Locations
Figure 3 Shallow Groundwater Potentiometric Map

List of Appendices

Appendix A Laboratory Analytical Reports
Appendix B Boring Logs
Appendix C Temporary Monitoring Well Construction and Abandonment Records
Appendix D Groundwater Sampling Records

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Brownfields Site Assessment Report Sun Chemical Facility
Charlotte, North Carolina
H&H Job No. PPA-038

1.0 Introduction and Background

This report presents the results of Brownfields site assessment activities conducted by Hart &
Hickman, PC (H&H) at the Sun Chemical Facility located at 1701 Westinghouse Boulevard in
Charlotte, Mecklenburg County, North Carolina. Brownfield assessment activities were
conducted in accordance with H&H’s approved October 20, 2011 Environmental Assessment
Work Plan, an e-mail Work Plan Addendum dated November 17, 2011, and the North Carolina
Department of Environment and Natural Resources (DENR) November 18, 2011 work plan
approval letter. The activities were conducted in support of a Brownfields agreement for the site.
A Site Location Map is included as Figure 1, and a Site Map is included as Figure 2.

The site is approximately 15 acres in area and has historically been used for ink production since
the 1960s. Prior to that time, the site and surrounding area were part of the Charlotte Naval
Ammunition Depot (NAD). The NAD was used during World War II for munitions assembly
and storage. There are known groundwater impacts in portions of the former NAD including an
area located south of the site.

The site contains two main buildings and several smaller buildings. Previous assessment
activities were conducted at the site in the 1990s. Thirteen underground storage tanks (USTs)
were located in the southwestern portion of the site (see Figure 2). The USTs were removed in
1991. Soil and groundwater assessment activities conducted both before and after the USTs
were removed indicated the presence of soil and groundwater impacts in the area of the USTs.
Approximately 600 tons of impacted soil were removed from the UST basin in 1998.

Previous groundwater assessment activities indicated that groundwater impacts were present in
and downgradient of the area of the former USTs. High levels of the compounds acetone,
isopropanol, isopropyl acetate, toluene, and methyl ethyl ketone (MEK or 2-butanone) were

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reported in previous groundwater samples. These compounds were stored in the former USTs.
In addition, the chlorinated solvent tetrachloroethene (PCE) and its degradation products were
detected in the groundwater samples at concentrations above groundwater standards.
Chlorinated solvents were reportedly not stored in the USTs. The locations of the site monitor
wells are included as Figure 2, and the historical groundwater analytical data is provided as
Table 4.

The purpose of the site assessment activities was to 1) determine if there were soil impacts of
potential concern at the site, 2) evaluate current groundwater conditions using the existing
monitor well network and additional temporary monitor wells installed in potential areas of
concern, 3) confirm the direction of shallow groundwater flow, and 4) evaluate the potential for
vapor intrusion concerns by sampling subslab soil vapor. The methods and results of Brownfield
site assessment activities are presented in the following sections of this report.

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2.0 Soil and Groundwater Assessment

Soil and groundwater assessment activities were conducted by H&H at the site between
November 30, 2011 and December 2, 2011. As part of the assessment activities, H&H collected
three soil samples from three borings, installed and sampled four temporary monitoring wells,
and sampled eight existing site monitoring wells. Details of the soil and groundwater assessment
activities are provided in the following sections.

2.1 General Field Practices

Laboratory analyses of soil and groundwater samples were conducted by Pace Analytical
Services, Inc. (Pace) of Huntersville, North Carolina. Pace is a North Carolina certified
laboratory. A chain-of-custody record was completed for samples collected and included the
sample designation, date collected, time collected, matrix, sample container information, and
requested analyses. The completed chain-of-custody record was signed by H&H sampling
personnel and relinquished to laboratory personnel or placed in the cooler, sealed with a custody
seal, and delivered to the laboratory via a courier. The laboratory analytical data reports and
chain-of-custody records are included in Appendix A.

Investigation derived waste (IDW) soil cuttings generated from the installation of the temporary
monitoring wells, and groundwater generated during well development and purging process were
containerized into 55-gallon steel drums and are staged on-site for subsequent off-site treatment
and disposal.

2.2 Soil Sampling Procedures

Three soil borings were advanced at the site on November 30 and December 1, 2011 by hand
auger and direct push technology (DPT) methods. A decontaminated stainless steel hand auger
was used to clear each boring for subsurface utilities to 5 feet (ft) below ground surface (bgs).
Soil samples below 5 ft were collected by DPT using 5-ft long macro-core samplers within an

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acetate sleeve. Soil borings were advanced to an approximate depth of 8 ft bgs or to DPT
refusal.

The approximate soil boring locations, labeled DPT-1 through DPT-3, are depicted on Figure 2.
DPT-1 was collected from the drum/tote storage area in the southwest portion of the site, DPT-2
was collected near the aboveground storage tanks (ASTs) and truck loading area in the south-
central portion of the site, and DPT-3 was collected adjacent to the wastewater pit in the
southeast portion of the site. In addition, one boring (BG) was advanced in the northern portion
of the property to obtain background metal soil concentrations at the site. Boring logs with
lithologic descriptions and field screening results are included in Appendix B.

Following collection, soil samples were described for lithologic purposes, inspected for the
presence of staining and odors, and field-screened for the presence of organic vapors with a
calibrated photo-ionization detector (PID). Because there was no field evidence of soil impact in
the soil samples collected from the borings, samples from each boring were collected from a
depth of 0-2 ft for laboratory analysis. The background sample was also collected from a depth
of 0-2 ft.

The soil samples from DPT-1, DPT-2, and DPT-3 were analyzed for volatile organic compounds
(VOCs) by Environmental Protection Agency (EPA) Method 8260B, semi-VOCs (SVOCs) by
EPA Method 8270C, Hazardous Substance List (HSL) metals by EPA Methods 6010C and
7471B, and hexavalent chromium by EPA Method 7196A. Sample BG was analyzed for HSL
metals and hexavalent chromium only.

After soil sampling was completed, soil borings DPT-1, DPT-2 and BG were abandoned with
hydrated bentonite chips. The surface at DPT-1 was patched with concrete to match the
surrounding surface. Soil boring DPT-3 was converted into temporary monitoring well HH-4.
Temporary monitoring well installation and groundwater sampling are discussed further in
Sections 2.4 and 2.6.

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2.3 Soil Analytical Results

The results of soil sample analyses are summarized in Table 1, and the laboratory analytical data
report is provided in Appendix A. The soil analytical results were compared to the DENR
Inactive Hazardous Sites Branch (IHSB) Residential Health Based Preliminary Soil Remediation
Goals (HBSRGs) and the Industrial HBSRGs. Metal concentrations were also compared to the
site-specific background concentration in sample BG.

Drum/Tote Storage Area
Soil boring DPT-1 was advanced to DPT refusal at 7 ft bgs to assess subsurface conditions in the
drum/tote storage area. Field screening results did not indicate the presence of obvious impacts;
therefore, a soil sample was collected from DPT-1 at 0-2 ft bgs.

No detections of VOCs or SVOCs at concentrations above laboratory reporting limits were
identified in DPT-1. In addition, no metals were detected at concentrations exceeding
Residential and Industrial HBSRGs. Metal detections were similar to concentrations detected in
the background sample collected from the site.

AST and Truck Loading Area
Soil boring DPT-2 was advanced to DPT refusal at 6 ft bgs to assess subsurface conditions near
the AST and truck loading area. Field screening results did not indicate the presence of obvious
impacts; therefore, a soil sample was collected from DPT-2 at 0-2 ft bgs.

Acetone, a common laboratory introduced contaminant, was detected in DPT-2 at a
concentration of 0.169 mg/kg which is below the HBSRGs. The SVOC bis(2-
ethylhexyl)phthalate (DEHP; 1.90 mg/kg) was detected in DPT-2, and this concentration is also
below the HBSRG. No additional VOCs or SVOCs were detected in DPT-2. Concentrations of
total chromium, lead, and manganese appear to be elevated over site-specific background levels.
However, none of the metals concentrations exceeded the SRGs.

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Wastewater Pit
Soil boring DPT-3 was advanced to DPT refusal at 8 ft bgs to assess subsurface conditions
adjacent to the wastewater pit. Field screening results did not indicate the presence of obvious
impacts; therefore, a soil sample was collected from DPT-3 at 0-2 ft bgs.

No detections of VOCs or SVOCs at concentrations above laboratory reporting limits were
identified in DPT-3. In addition, no metals were detected at concentrations exceeding
Residential and Industrial HBSRGs. Metal detections were similar to concentrations detected in
the background sample.

2.4 Temporary Monitoring Well Installation

On November 30, 2011 four shallow temporary monitoring wells were installed by a North
Carolina-licensed well driller at the site. The locations of the temporary wells, labeled HH-1
through HH-4, are indicated in Figure 2. Temporary monitoring well HH-1 was installed to
assess groundwater conditions downgradient of the exterior hazardous waste storage area,
temporary monitoring well HH-2 was installed to assess groundwater conditions in the area of
the former UST basin (where the highest concentrations of compounds were previously detected
in groundwater) and in the area of the current drum and tote storage, HH-3 was installed to
assess groundwater conditions downgradient of the manufacturing building, and HH-4 was
installed to assess groundwater conditions near the cleaning shed and subgrade wastewater
collection pit.

The temporary monitoring wells were planned to be installed utilizing DPT methods with hollow
rods to minimize IDW. However, because of DPT refusal at depths ranging from 6 to 8 ft across
the site, the temporary monitoring wells were installed with the Geoprobe 6620DT rig using 4-
inch hollow-stem augers. The wells were constructed with 2.0-inch PVC riser completed with
10 ft of 0.010-slot screens placed to bracket the water table. A sand filter pack was added to the
well annulus to approximately two feet above the screened interval and a bentonite seal was
installed above the sand filter pack. Following installation, the temporary monitoring wells were

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developed utilizing a decontaminated submersible pump to remove suspended colloidal material
and to improve the hydraulic connectivity between the borehole and the aquifer.

On December 2, 2011, H&H surveyed the tops of casing elevation of the four temporary
monitoring wells using survey techniques, which were referenced to the tops of casing elevation
of existing site monitoring wells. Temporary monitoring well boring logs are provided in
Appendix B, and well construction records are provided in Appendix C.

2.5 Groundwater Flow

The temporary wells were allowed to stabilize two days prior to gauging and sampling. On
December 2, 2011, the depths-to-water in the temporary wells and the existing monitor wells
were obtained using a decontaminated electronic water level probe. Well construction and
groundwater elevation data are summarized in Table 2. Depth-to-water measurements were used
to construct a potentiometric surface map which is included as Figure 3.

The results of the groundwater gauging data indicate that the groundwater flow direction is
generally to the south-southeast as shown on Figure 3. This direction of groundwater flow is
consistent with historical data and topography at the site.

2.6 Groundwater Sampling Procedures

On December 2, 2011, H&H collected groundwater samples from the four temporary monitoring
wells (HH-1 through HH-4) and select existing shallow site monitoring wells G-1, G-3, G-8, G-
9, G-10, G-11, G-12, and G-15. Following depth to groundwater measurements, each well was
purged by low flow methods using a peristaltic pump and new dedicated tubing. Low flow
purging was conducted until field measurements of pH, conductivity, temperature, and turbidity
stabilized. In addition, the four wells from which samples were collected for metals analysis (G-
1, HH-1, HH-3, and HH-4) were purged until turbidity was less than 10 NTU. Groundwater
samples were collected in general accordance with EPA Region 4 Science and Ecosystem
Support Division (SESD) protocols.

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Groundwater samples were collected from each well for laboratory analysis of VOCs by EPA
Method 8260B. In addition, groundwater samples were collected from HH-1, HH-3, HH-4, and
G-1 for analysis of SVOCs by EPA Method 8270C, and HSL Metals by EPA Methods 6010 and
7470. Groundwater sampling records summarizing the field measurements are provided in
Appendix D. After sampling was completed, the temporary monitoring well materials were
removed and the borings were abandoned with cement grout. The surface at each location was
patched with concrete to match the surrounding area. Temporary monitoring well abandonment
records are provided in Appendix C.

2.7 Groundwater Analytical Results

The results of the groundwater analyses are summarized in Table 3. The analytical laboratory
data report is provided in Appendix A. Historical groundwater analytical data is summarized in
Table 4. Groundwater data were compared to North Carolina 2L Standards.

SVOCs
No SVOCs were detected in any of the groundwater samples collected from wells G-1, HH-1,
HH-3, and HH-4.

VOCs
No VOCs were detected in the groundwater samples collected from HH-1, G-1, and G-12 at
concentrations above the laboratory reporting limits. In addition, no VOCs were detected in the
groundwater samples collected from G-3 and G-8 at concentrations above 2L Standards.

The results of laboratory analyses indicate that no VOCs were detected in the upgradient well G-
1 or the well located downgradient of the hazardous waste storage area HH-1. Low
concentrations of benzene and naphthalene were detected in the groundwater sample collected
from temporary monitoring well HH-2 at concentrations that slightly exceed their respective 2L
Standards. Five additional VOCs including acetone, 2-butanone (methyl ethyl ketone),
diisopropyl ether, toluene, and total xylenes were detected above the laboratory reporting limit in

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HH-2, but below their respective 2L Standards. HH-2 was installed to assess current conditions
in the former UST basin where high levels of compounds were detected previously in
groundwater. As indicated in Table 4, high concentrations of acetone, 2-butanone, naphthalene,
and toluene were previously detected in the former UST basin in samples collected in the 1990s;
however, high levels of these compounds were not detected in this area of the site in 2011. The
lack of high detections of these compounds is the result of the fact that the soil impacts were
removed and because the compounds are readily degraded in most groundwater systems.

The laboratory analytical results indicate that PCE and trichloroethene (TCE) were detected in
the groundwater samples collected from monitoring wells HH-3, G-9, G-10, G-11, and G-15 in
the southern portion of the site at concentrations above their respective 2L Standards. In
addition, the PCE and TCE degradation product cis-1,-2-dichloroethene (cis-1,2-DCE) was
detected in monitoring wells G-9, G-10, G-11, and G-15 at concentrations above the laboratory
reporting limit. The presence of PCE in wells G-9, G-10, G-11, and G-15 is consistent with
previous samples collected from these wells in the 1990s; however, the PCE concentrations in
2011 were significantly lower than those detected previously.

Temporary monitoring well HH-4 was installed adjacent to the wastewater collection pit.
Concentrations of cis-1,2-DCE and vinyl chloride were detected in the groundwater sample
collected from HH-4 above their respective 2L Standards. In addition, trans-1,2-dichloroethene
was detected at a concentration above the laboratory reporting limit but below its respective 2L
Standard.

VOC concentrations were also compared to the DENR IHSB vapor intrusion screening levels for
industrial sites. As indicated in Table 3, PCE concentrations in monitoring wells G-9 (259 µg/l),
G-11 (441 µg/l), and G-15 (60.8 µg/l) were above the IHSB Industrial/Commercial Vapor
Intrusion Screening Level for PCE of 29 µg/l.

Metals
The metal manganese was detected in the groundwater samples collected from temporary
monitoring wells HH-1 (65.9 µg/l), HH-3 (269 µg/l), and HH-4 (350 µg/l) at concentrations

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above the 2L Standard of 50 µg/l and the background sample concentration in G-1 of 23 µg/l.
Nickel was detected in the sample collected from HH-3 at a concentration of 64.9 µg/l which is
below its 2L Standard of 100 µg/l. No additional metals were detected in groundwater samples
above laboratory reporting limits.

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3.0 Soil Vapor Assessment
3.1 Sub-Slab Vapor Sampling Methods

On December 1, 2011, H&H collected sub-slab vapor samples from eight locations at the site.
The approximate locations of the vapor monitoring points, labeled SV-1 through SV-8, are
indicated on Figure 2. Sub-slab vapor samples were collected from beneath the building slab
floor at locations inside the western warehouse (SV-1), the northern warehouse (SV-2), inside
the western and main manufacturing areas (SV-3 and SV-4), inside the office area (SV-5), inside
the laboratory building addition (SV-6), inside the cleaning shed (SV-7), and inside the
maintenance building (SV-8).

At each location, H&H drilled through the concrete slab floor using a concrete hammer drill. A
stainless steel AMS dedicated 0.625-inch diameter stainless steel probe with an approximate 1-
inch long soil gas screen fitted with 0.25-inch diameter Teflon® tubing was then installed at each
vapor monitoring point location. The probes were installed through the gravel beneath the
concrete slab and seated in the underlying soil so that the soil gas screen was present in both the
soil and overlying gravel. Filter sand was placed around each soil gas screen to approximately 4
to 5 inches below the top of the concrete slab. Each point was sealed to the surface of the
concrete slab using hydrated bentonite. The soil gas probes were completed at the surface with a
sample valve and Teflon® tubing.

Prior to sampling, a leak check was conducted at each sub-slab sample location by constructing a
shroud around the sampling point and saturating the air within the shroud with helium gas. H&H
utilized a syringe to collect a sample from the gas in the shroud into a Tedlar® bag and analyzed
for helium using a helium gas detector. Vapor from the vapor monitoring point was purged
using a syringe and sampled outside of the shroud into a separate Tedlar® bag and analyzed
using the helium gas detector to ensure that helium concentrations are less than 10% of the
helium concentrations in the shroud. All of the sample points were found to pass the leak check
criteria.

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Following a successful leak check, the sub-slab vapor samples were collected using 6-liter
Summa canisters. The Summa canisters were connected to a one-hour airflow regulator and to
the Teflon® tubing at each point. As part of the sampling effort, H&H also measured ambient
temperature at the beginning, middle, and end of the sample collection period at select sample
locations. Temperatures during sample collection ranged from 63.5° F to 71.3° F at vapor
monitoring point locations. Outside weather conditions during the sampling period were clear
skies with temperatures around 55° F.

In accordance with DENR’s response letter dated November 18, 2011, a helium tracer gas
atmosphere was maintained at the surface of each sub-slab vapor point during the collection of
the vapor sample. The helium gas atmosphere was created by constructing a shroud around the
sampling point and saturating the air within the shroud with helium gas. To ensure a sufficient
helium atmosphere was maintained during sampling, H&H monitored helium levels within the
shroud and added helium as needed to maintain an 80 to 90% helium atmosphere. A record of
helium measurements taken during sampling activities is provided as Table 5.

After sample collection, the regulator valves on the canisters were closed and flow regulators
were removed. The Summa canisters and regulators were placed in laboratory supplied cartons,
properly labeled and were shipped under standard chain-of-custody procedures to Con-Test
Analytical Laboratory in East Longmeadow, MA for analysis of VOCs by EPA Method TO-15
and helium by EPA Method 3C.

3.2 Sub-Slab Vapor Results

The results of the sub-slab vapor sample analyses are summarized in Table 6, and the laboratory
analytical data report is provided in Appendix A. The concentrations of compounds detected in
the sub-slab vapor samples were compared to DENR IHSB Industrial/Commercial Vapor
Intrusion Screening Levels.

As indicated in Table 6, four of the eight sub-slab vapor samples (SV-2, SV-3, SV-5, and SV-8)
contained compound concentrations above the IHSB Industrial/Commercial Vapor Intrusion

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Screening Levels. These samples were located in the northern warehouse, the western
manufacturing area, the office area, and the maintenance building. PCE was detected in vapor
samples SV-2, SV-5, and SV-8 above the IHSB Industrial/Commercial Vapor Intrusion
Screening Levels. In addition, 1,2,4-trimethlybenzene (1,2,4-TMB) was detected in SV-2 and
SV-3 above the IHSB Industrial/Commercial Vapor Intrusion Screening Levels. Multiple other
VOCs were detected in the samples but a concentrations below the IHSB screening levels. No
compounds above the screening levels were detected in the samples from SV-1, SV-4, SV-6, and
SV-7.
3.3 Helium Tracer Gas Testing

The results of the helium tracer gas test performed at each sample point indicate that helium was
not detected above laboratory method detection limits in samples SV-2, SV-4, SV-5, SV-6, and
SV-7. Helium was detected in SV-1 and SV-3 at concentrations less than 10%, and was detected
in SV-8 at a concentration of 25%. The helium concentration in SV-8 is slightly elevated and
may indicate some short-circuiting of ambient air at the surface. However, the PCE
concentration in subslab sample SV-8 was above the IHSB Industrial/Commercial screening
level and therefore the potential short circuiting is not considered significant.

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4.0 Summary and Conclusions

H&H conducted Brownfield site assessment activities at the site from November 30, 2011
through December 2, 2011. The results of the site assessment activities are summarized below.

• No soil impacts above both background (for metals) and Residential and
Commercial/Industrial HBSRGs were detected in the shallow soil samples collected from
the southern portion of the site. As such, there is no evidence of significant soil impacts
in these areas of the site. No soil land use restrictions appear warranted in the
Brownfields agreement for the site.

• Groundwater flow direction across the site is generally to the south-southeast. The
determined direction of groundwater flow is consistent with historical data and
topography at the site.

• Benzene and naphthalene were detected in the groundwater sample collected from
temporary monitoring well HH-2 in the former UST basin at concentrations that slightly
exceed their respective 2L Standards. The high concentrations of compounds such as
acetone, 2-butanone, and toluene detected in and downgradient of the UST basin in
samples collected in the 1990s were not confirmed in the 2011 sampling. The
significantly reduced concentrations are the result of the soil impacts having been
previously removed and because these compounds are readily degraded.

• The chlorinated solvents PCE, TCE, and cis-1,2-DCE were detected above 2L standards
in samples collected from monitoring wells HH-3, HH-4, G-9, G-10, G-11, and G-15 at
concentrations above their respective 2L Standards. The concentrations of PCE detected
in existing wells G-9, G-10, G-11, and G-15 have decreased from the PCE concentrations
detected in the 1990s.

• Manganese was detected in groundwater samples above background levels and the 2L
Standards in samples collected from temporary monitoring wells HH-1, HH-3, and HH-4.

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• PCE was detected in groundwater above the IHSB vapor intrusion screening levels in
samples collected from G-9, G-11, and G-15 located in the southern portion of the site.

• The results of the sub-slab vapor sampling conducted at the property indicate that the
VOCs PCE and/or1,2,4-TMB were detected above the DENR IHSB industrial soil vapor
screening levels in samples SV-2 (northern warehouse), SV-3 (western manufacturing),
SV-5 (office area), and SV-8 (maintenance building). Based upon the results of the sub-
slab soil vapor sampling, H&H recommends that indoor air samples be collected at the
locations and for the compounds that exceeded screening levels at the site to further
evaluate the vapor intrusion pathway.
Table 1
Summary of Soil Analytical Data
Sun Chemical Facility
Charlotte, North Carolina
H&H Job No. PPA-038
S:\AAA-Master Projects\Parker Poe Adams (PPA)\PPA-038 sun chemical selwyn group\Brownfields Assessment\Data Tables1/6/2012
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Loation
Drum/Tote
Storage
AST Farm/Truck
Loading Wastewater Pit
Site Background
Soil Sample
Sample ID DPT-1 DPT-2 DPT-3 BG
Depth (ft bgs)0-2 0-2 0-2 0-2
Sample Date 11/30/2011 11/30/2011 11/30/2011 12/1/2011
Units (mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)
VOCs (8260B)
Acetone <0.119 0.169 <0.0999 ---12,000 100,000
SVOCs (8270C)
bis(2-Ethylhexyl)phthalate <0.465 1.90 <0.379 ---35 120
HSL Metals (6010/7471A/7196)
Arsenic 1.1 1.9 1.3 1.9 0.39 1.6
Beryllium 0.79 0.49 0.76 0.33 32 400
Cadmium 1.2 0.63 <0.094 2.1 14 160
Total Chromium 6.2 40.3 1.9 2.7 NE NE
Hexavalent Chromium <0.51 <0.48 <0.56 <0.47 0.29 5.6
Trivalent Chromium 6.2 40.3 1.9 2.7 24,000 100,000
Copper 8.5 37.0 34.1 21.0 620 8,200
Lead 10.9 173 3.9 3.3 400 800
Manganese 12.6 237 81.3 105 360 4,600
Mercury 0.0081 0.063 <0.0042 0.0079 4.6 62
Nickel 1.5 5.8 1.9 5.3 300 4,000
Selenium 1.1 <1.0 <0.94 <1.1 78 1,000
Thallium <1.0 <1.0 <0.94 1.4 0.16 2
Zinc 9.3 40.4 12.9 41.7 4,600 62,000
Notes:
Soil Remediation Goals (SRGs) from North Carolina Department of Environment and Natural Resources (DENR) Inactive Hazardous Sites Branch (IHSB) Preliminary SRG Table dated August 201
Only those compounds detected in at least one sample (including background) shown above
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; HSL = Hazardous Substance List
NE = not established; --- = Not applicable
mg/kg = milligrams per kilogram
DENR IHSB Residential
Use SRG
DENR IHSB Industrial Use
SRG
Regulatory Screening Levels
Table 2
Summary of Monitoring Well Construction and Groundwater Elevation Data
Sun Chemical Facility
Charlotte, North Carolina
H&H Job No. PPA-038
S:\AAA-Master Projects\Parker Poe Adams (PPA)\PPA-038 sun chemical selwyn group\Brownfields Assessment\Data Tables
1/6/2012
Table 2 (Page 1 of 1)
Hart & Hickman, PC
G-1 Soil 648.80 19.0 10 9.41 639.39 10.22 638.58 10.39 638.41
G-2 Rock 648.85 37.0 5 9.45 639.40 10.23 638.62 10.49 638.36
G-3 Soil 648.52 20.0 10 10.11 638.41 10.78 637.74 10.31 638.21
G-4 Rock 648.53 35.0 5 10.05 638.48 10.89 637.64 10.36 638.17
G-8 Rock 648.31 27.0 5 ----10.58 637.73 10.07 638.24
G-9 Rock 648.64 27.0 5 ----11.25 637.39 10.65 637.99
G-10 Rock 648.76 27.0 5 ----12.58 636.18 10.76 638.00
G-11 Rock 648.29 27.0 5 ----12.08 636.21 11.35 636.94
G-12 Rock 647.11 34.0 5 ----10.10 637.01 9.80 637.31
G-15 ----27.0 10 --------11.53 --
HH-1 Soil 646.04 20.5 10 --------6.80 639.24
HH-2 Soil 648.04 19.0 10 --------9.13 638.91
HH-3 Soil 646.90 22.0 10 --------7.73 639.17
HH-4 Soil 646.11 14.0 10 --------7.49 638.62
-- = information not available
Temporary monitoring wells HH-1 through HH-4 installed on November 30, 2011 and were abandoned on December 2, 2011
TOC elevations for HH-1 through HH-4 referenced to the existing well network.
TOC = top of casing
Well ID
Notes:
TOC
Elevation
(ft)
Depth to
Water
(ft below
TOC)
Total Depth
(ft below
TOC)
Screened
Zone
Ground
Water
Elevation
(ft)
Ground
Water
Elevation
(ft)
Screen
Length
12/2/2011
Ground
Water
Elevation
(ft)
Depth to
Water
(ft below
TOC)
2/29/1988 - 3/3/1988 2/13/1989
Depth to
Water
(ft below
TOC)
Table 3
Summary of Groundwater Analytical Data
Sun Chemical Facility
Charlotte, North Carolina
H&H Job No. PPA-038
S:\AAA-Master Projects\Parker Poe Adams (PPA)\PPA-038 sun chemical selwyn group\Brownfields Assessment\Data Tables
1/6/2012
Table 3 (Page 1 of 1)
Hart & Hickman, PC
Location
Hazardous
Waste Storage
Former UST
Basin
Manufacturing
Bldg Wastewater Pit Background Southern Site Southern Site Southern Site Southern Site Southern Site Southern Site Southern Site
Sample ID HH-1 HH-2 HH-3 HH-4 G-1 G-3 G-8 G-9 G-10 G-11 G-12 G-15
Sample Date 12/2/2011 12/2/2011 12/2/2011 12/2/2011 12/2/2011 12/2/2011 12/2/2011 12/2/2011 12/2/2011 12/2/2011 12/2/2011 12/2/2011
Units (μg/L)(μg/L)(μg/L)(μg/L)(μg/L)(μg/L)(μg/L)(μg/L)(μg/L)(μg/L)(μg/L)(μg/L)(μg/L)(μg/L)
VOCs (8260B)
Acetone <25.0 1,070 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <62.5 <25.0 <25.0 6,000 20,000,000
Benzene <1.0 8.4 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.5 <1.0 <1.0 1 70
2-Butanone (Methyl ethyl ketone)<5.0 64.1 <5.0 <5.0 <5.0 <5.0 <5.0 <10.0 <5.0 <12.5 <5.0 <5.0 4,000 1,900,000
cis-1,2-Dichloroethene <1.0 <2.0 <1.0 76.7 <1.0 <1.0 1.5 45.1 7.8 25.9 <1.0 187 70 140*
trans-1,2-Dichloroethene <1.0 <2.0 <1.0 23.0 <1.0 <1.0 <1.0 6.6 <1.0 <2.5 <1.0 <1.0 100 140
Diisopropyl ether <1.0 39.5 <1.0 <1.0 <1.0 1.5 18.2 <2.0 8.2 4 <1.0 <1.0 NE NE
Naphthalene <1.0 9.5 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.5 <1.0 <1.0 6 140
Tetrachloroethene <1.0 <2.0 10.6 <1.0 <1.0 <1.0 <1.0 259 7.3 441 <1.0 60.8 0.7 29
Toluene <1.0 185 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.5 <1.0 <1.0 600 16000
Trichloroethene <1.0 <2.0 4.8 <1.0 <1.0 <1.0 2.2 52.1 13.2 39.3 <1.0 80.3 3 150
Vinyl chloride <1.0 <2.0 <1.0 6.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.5 <1.0 <1.0 0.03 25
Xylene (Total)<2.0 14.3 <2.0 <2.0 <2.0 <2.0 <2.0 <4.0 <2.0 <5.0 <2.0 <2.0 500 420
SVOCs (8270C)BRL NA BRL BRL BRL NA NA NA NA NA NA NA ------
HSL Metals (6010/7470)
Manganese 65.9 NA 269 350 23.0 NA NA NA NA NA NA NA 50 NE
Nickel <5.0 NA 64.9 <5.0 <5.0 NA NA NA NA NA NA NA 100 NE
Notes:
1. NCAC 2L Groundwater Standards (January 1, 2010)
2. Inactive Hazardous Sites Branch Industrial/Commercial Vapor Intrusion Screening Levels
Only those compounds detected in at least one sample shown above.
Bold indicates concentration above NC 2L Groundwater Standard
Blue highlighting indicates concentrations indicates concentrations above industrial vapor intrusion screening level
Analytical method number follows parameter in parenthesis
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; HSL - Hazardous Substance List
NE = Not established
-- = Not applicable
BRL = All compounds not detected at or above laboratory reporting limit
NA = Not analyzed
μg/L = micrograms per liter
* = screening level for trans-1,2-DCE used as a surrogate for cis-1,2-DCE
IHSB Industrial
Vapor Intrusion
Screening Levels2
NC 2L
Groundwater
Standard¹
Table 4
Summary of Historical Groundwater Analytical Data
Sun Chemical Facility
Charlotte, North Carolina
H&H Job No. PPA-038
S:\AAA-Master Projects\Parker Poe Adams (PPA)\PPA-038 sun chemical selwyn group\Brownfields Assessment\Data Tables
1/6/2012
Table 4 (Page 1 of 1)
Hart & Hickman, PCAcetoneBenzeneCarbon Disulfide1,2-DichloroetheneEthanolEthyl AcetateIsoproponalIsopropyl AcetateMethyl Ethyl KetoneNaphthalenePropyl AcetateTetrachloroethene (PCE)TolueneTrichloroethene (TCE)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)
6,000 1 700 70 NS 3,000 NE NE 4,000 6 NS 0.7 600 3
6/15/1987 10,000 ----------4,000 80 4,000 --3,000 --8,000 --
2/13/1989 46 ----------------------10 --
6/15/1987 40,000 ----------10,000 700 500 --20,000 --200 --
2/13/1989 640 --------------630 ------62 --
6/15/1987 300,000 ----------200,000 2,000,000 30,000 3,000 20,000 --200,000 --
2/13/1989 4,900,000 ----------2,300,000 100,000 --------182,000 --
Mar-88 ----------------4,000 ----------
Dec-91 ----------------------------
Sep-94 ----------------------------
12/2/2011 <25.0 <1.0 --<1.0 --------<5.0 <1.0 --<1.0 <1.0 <1.0
Mar-88 ----------------------------
Dec-91 ----------------------------
Sep-94 ----------------------------
Mar-88 ----------70,000 ------------6 --
Dec-91 310 ----------------------260 --
Sep-94 30,000 ----------------------55,000 --
12/2/2011 <25.0 <1.0 --<1.0 --------<5.0 <1.0 --<1.0 <1.0 <1.0
Mar-88 34,000 6 ------------10,000 ------1,800 --
12/13/1989 18,000 --------------24,000 ------38,000 --
Dec-91 1,500,000 ----------------------240,000 --
Sep-94 910,000 ------70,000 --220,000J ----------170,000 --
G-5 Dec-91 ----------------------------
G-6 Mar-88 ----------------------------
G-7 Mar-88 ------------------------10 --
2/13/1989 ------------8000 --------------
Dec-91 ------------------------4,000 --
Sep-94 230,000 ----------------------84,000 --
12/2/2011 <25.0 <1.0 --<1.0 --------<5.0 <1.0 --<1.0 <1.0 <1.0
2/13/1989 ----------------------------
Dec-91 ------------------------1,500 --
Sep-94 ----------------------530 ----
12/2/2011 <50.0 <2.0 --<2.0 --------<10.0 <2.0 --259 <2.0 52.1
2/13/1989 39 --------------------------
10/26/1989 ----------------------212 --38
Dec-91 ----20 99 --------------------
Sep-94 ----------------------------
12/2/2011 <25.0 <1.0 --<1.0 --------<5.0 <1.0 --7.3 <1.0 13.2
2/13/1989 ----------------------------
Dec-91 ----------------------3,100 ----
Sep-94 ----------------------3,500 ----
12/2/2011 <62.5 <2.5 --<2.5 --------<12.5 <2.5 --441 <2.5 39.3
2/13/1989 ----------------------------
Dec-91 ----8 ----------------------
Sep-94 ----------------------------
12/2/2011 <25.0 <1.0 ------------<5.0 <1.0 --<1.0 <1.0 <1.0
G-13 Dec-91 670,000 ------------------120,000 --120,000 --
G-14 Dec-91 250,000 ----------------------11,000 --
Sep-94 ----------------------1,800 ----
12/2/2011 <25.0 <1.0 --<1.0 --------<5.0 <1.0 --60.8 <1.0 80.3
HH-1 12/2/2011 <25.0 <1.0 --<1.0 --------<5.0 <1.0 --<1.0 <1.0 <1.0
HH-2 12/2/2011 1070 8.4 --<1.0 --------64.1 9.5 --<2.0 185 <2.0
HH-3 12/2/2011 <25.0 <1.0 --<1.0 --------<5.0 <1.0 --10.6 <1.0 4.8
HH-4 12/2/2011 <25.0 <1.0 --<1.0 --------<5.0 <1.0 --<1.0 <1.0 <1.0
Notes:
1) NCAC 2L Groundwater Standards (January 1, 2010)
Bold indicates concentration above the 2L Standard
VOCs= Volatile Organic Compounds
-- = analyte not analyzed for or concentration is below laboratory reporting limit
Historical data obtained from previous tables included in reports completed by other consultants; actual lab data not available for review.
Table does not include all compounds detected in December 2011 sampling event (refer to Table 3)
NE = Not Established
µg/L = micrograms/liter
OW-2
OW-3
G-2
G-4
2L Standards (1)
G-15
G-1
G-3
G-8
G-9
G-11
G-12
G-10
OW-1Well IDSample DateUnits
VOCs
Table 5
Helium Shroud Readings
Sub-Slab Vapor Sampling
Sun Chemical Facility
Charlotte, North Carolina
H&H Project No. PPA-038
S:\AAA-Master Projects\Parker Poe Adams (PPA)\PPA-038 sun chemical selwyn group\Brownfields Assessment\Data Tables
1/6/2012
Table 5
Hart & Hickman, PC
Sample ID Start %He Time %He Time %He Finish %He
SV-1 12:16 86.3%12:36 90.2%12:56 91.3%13:15 87.2%
SV-2 12:11 90.9%12:31 86.1%12:51 85.2%12:10 83.4%
SV-3 12:21 85.0%12:41 90.1%13:01 87.2%13:20 85.2%
SV-4 12:26 89.3%12:46 88.2%13:06 83.2%13:25 84.7%
SV-5 14:11 86.7%14:31 89.9%14:51 83.5%15:10 85.2%
SV-6 14:16 88.7%14:36 86.9%14:56 90.7%15:15 88.0%
SV-7 14:21 85.5%14:41 91.4%15:01 84.2%15:20 85.3%
SV-8 14:26 86.8%14:46 87.3%15:06 90.2%15:25 82.7%
Table 6
Summary of Soil Gas Analytical Data
Sun Chemical Facility
Charlotte, North Carolina
H&H Job No. PPA-038
S:\AAA-Master Projects\Parker Poe Adams (PPA)\PPA-038 sun chemical selwyn group\Brownfields Assessment\Data Tables
1/6/2012
Table 6 (Page 1 of 1)
Hart & Hickman, PC
Location
Western
Warehouse
Northern
Warehouse
Western
Manufacturing
Main
Manufacturing Offices Laboratory Cleaning Shed
Maintenance
Bldg
Sample ID SV-1 SV-2 SV-3 SV-4 SV-5 SV-6 SV-7 SV-8
Sample Date 12/1/2011 12/1/2011 12/1/2011 12/1/2011 12/1/2011 12/1/2011 12/1/2011 12/1/2011
Units (µg/m³)(µg/m³)(µg/m³)(µg/m³)(µg/m³)(µg/m³)(µg/m³)(µg/m³)(µg/m³)(µg/m³)
VOCs (EPA TO-15)
Acetone 260 5,000 410 1300 27 11 110 380 64,000 280,000
Benzene <0.32 2.4 2.8 7.8 0.49 0.12 J <0.32 1.8 31 160
2-Butanone (MEK)16 45 7.3 J 140 6.7 J 2.4 J 1.8 J 21 NE NE
Carbon Disulfide 14 5.1 6.6 7.8 1.2 J 0.48 J 1.2 J 2.0 J 1,460 6,200
Carbon Tetrachloride 0.65 0.42 J 0.54 J <0.63 0.49 J 0.44 J 0.30 J 0.54 J 41 82
Chlorobenzene <0.46 <0.46 0.79 <0.46 <0.46 <0.46 <0.46 <0.46 NE 440
Chloroform 0.36 J <0.49 7.2 <0.49 <0.49 <0.49 3.5 1.1 11 53
Chloromethane <0.21 <0.21 0.43 0.17 J 0.15 J <0.21 0.20 J 0.97 188 780
Cyclohexane <0.34 <0.34 8.7 1.4 <0.34 <0.34 <0.34 1.0 NE NE
1,2-Dichlorobenzene <0.60 0.19 J 2.2 <0.60 <0.60 <0.60 <0.60 <0.60 420 1,760
1,4-Dichlorobenzene <0.60 0.16 J <0.60 <0.60 0.84 <0.60 <0.60 17 22 110
Dichlorodifluoromethane (Freon 12)2.60 2.7 1.6 1.00 2.9 2.9 2.9 2.6 200 880
1,1-Dichloroethane <0.40 0.39 J 0.48 0.68 <0.40 <0.40 <0.40 <0.40 150 770
1,1-Dichloroethylene <0.40 <0.40 18 <0.40 <0.40 <0.40 <0.40 <0.40 420 1,760
cis-1,2-Dichloroethylene <0.40 <0.40 <0.40 1.1 <0.40 <0.40 <0.40 0.24 J NE 520*
trans-1,2-Dichloroethylene <0.40 <0.40 <0.40 0.38 J <0.40 <0.40 <0.40 <0.40 126 520
Ethanol 170 37 480 660 5.2 J 35 140 210 NE NE
Ethyl Acetate 8.3 <0.36 <0.36 <0.36 <0.36 4.9 <0.36 1.6 NE NE
Ethylbezene 56 110 110 26.0 9.2 0.27 J 280 120 97 490
4-Ethyltoluene 0.29 J 61 190 9.0 0.52 <0.49 2.2 4.0 NE NE
Heptane 1.7 0.99 0.98 6.0 0.21 J <0.41 <0.41 4.0 NE NE
Hexane 5.6 J 2.9 J 4.4 J 9.6 J 1.8 J 1.1 J 0.99 J 6.1 J 1,460 6,200
2-Hexanone (MBK)<0.41 2.4 0.56 9.8 0.43 0.25 J 0.28 J <0.41 NE NE
Isopropanol 88 400 790 670 4.3 J 7.1 J 61 80 NE NE
Methyl tert-Butyl Ether (MTBE)<0.36 <0.36 0.62 <0.36 <0.36 <0.36 2.9 <0.36 940 4,700
Methylene Chloride 4.6 12 2.9 J 3.2 J 5.9 4.1 4.2 5.7 520 2,600
4-Methyl-2-pentanone (MIBK)2.1 17 <0.41 12 2.7 <0.41 0.29 J 1.8 6,200 26,000
Propene <6.9 29 <6.9 68 3.7 J 1.4 J <6.9 <6.9 NE NE
Styrene 0.12 J 2.3 0.53 0.37 J 0.14 J <0.43 0.27 J 0.81 2,000 8,800
Tetrachloroethene 0.64 J 340 0.38 J 7.3 1,200 0.58 J 18 510 41 210
Tetrahydrofuran 0.39 <0.29 2.5 <0.29 0.42 0.69 9.1 3.2 NE NE
Toluene 22 79 74 26 2.3 1.2 60 54 10,400 44,000
1,1,1-Trichloroethane <0.55 <0.55 0.68 <0.55 0.19 J <0.55 <0.55 <0.55 10,400 44,000
1,1,2-Trichloroethane <0.55 <0.55 <0.55 <0.55 <0.55 <0.55 <0.55 0.39 J 15 77
Trichloroethene <0.54 <0.54 <0.54 1.2 0.14 J <0.54 <0.54 6.2 120 610
Trichlorofluoromethane (Freon 11)1.5 1.4 0.31 J <0.56 1.1 1.1 1.4 1.4 1,460 6,200
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.54 J 0.52 J <0.77 <0.77 0.54 J 0.58 J 0.58 J 0.54 J 62,000 260,000
1,2,4-Trimethylbenzene 0.61 270 310 30 2.1 <0.49 8.5 10 14.6 62
1,3,5-Trimethylbenzene 0.25 J 190 130 8.5 0.59 <0.49 1.5 3.4 NE NE
Vinyl Chloride <0.26 0.26 0.16 J <0.26 <0.26 <0.26 <0.26 <0.26 16 280
m&p-Xylene 140 400 360 91 40 0.82 J 580 290 200 880
o-Xylene 23 200 140 28 17 0.25 J 190 65 200 880
Helium (EPA 3C)%%%%%%%%
9.4 <0.4 3.3 <0.4 <0.5 <0.4 <0.4 25
Notes:
1. North Carolina Department of Environment and Natural Resources (DENR) Inactive Hazardous Sites Branch (IHSB) Industrial Vapor Intrusion Screening Levels, Acceptable Soil Gas Concentration dated August 2011.
2. DENR IHSB Industrial/ Commercial Vapor Intrusion Screening Levels, Acceptable Soil Gas Concentration dated August 2011.
* = screening level for trans-1,2-DCE used as a surrogate for cis-1,2-DCE
Only those compounds detected in at least one sample shown above
Bold and Highlighting indicates concentration exceeds IHSB Industrial/ Commercial Vapor Intrusion Screening Level.
SV = sub-slab soil gas sample
NE = not established
VOCs = volatile organic compounds
µg/m³ = micrograms per cubic meter
Helium gas was used to perform a leak check on each soil gas point.
Samples were collected into 6-liter Summa canisters. A flow controller was used to collect the samples over a 1-hr period.
Samples were analyzed using EPA Method TO-15.
J flag indicates concentration was detected by the laboratory below the Reporting Limit (lowest calibration standard); therefore, the result is an estimated concentration.
IHSB Residential Vapor
Intrusion Screening Levels¹
Screening Levels
IHSB Industrial/ Commercial Vapor
Intrusion Screening Levels²
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
TITLE
PROJECT
SITE LOCATION MAP
SUN CHEMICAL FACILITY
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
9-21-11 0
1PPA-038
CHARLOTTE WEST, NC 1993
FORT MILL, SC-NC 1993

Appendix A
Laboratory Analytical Reports

December 09, 2011
LIMS USE: FR - STEVE HART
LIMS OBJECT ID: 92107622
92107622
Project:
Pace Project No.:
RE:
Mr. Steve HartHart & Hickman2923 South Tryon StreetCharlotte, NC 28203
Sun Chemical Facility PPA-038
Dear Mr. Hart:
Enclosed are the analytical results for sample(s) received by the laboratory on December 02, 2011.
The results relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail] Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357Virginia/VELAP Certification #: 460144
Asheville Certification IDs2225 Riverside Dr., Asheville, NC 28804Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001Virginia Certification #: 00072West Virginia Certification #: 356Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Lab ID Sample ID Matrix Date Collected Date Received
92107622001 DPT-1 (0-2)Solid 11/30/11 10:15 12/02/11 14:30
92107622002 DPT-3 (0-2)Solid 11/30/11 16:50 12/02/11 14:30
92107622003 DPT-2 (0-2)Solid 11/30/11 17:40 12/02/11 14:30
92107622004 BG (0-2)Solid 12/01/11 08:30 12/02/11 14:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92107622001 DPT-1 (0-2)EPA 6010 13 PASI-AJMW
EPA 7471 1 PASI-ASHB
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
EPA 7196 1 PASI-ASDH
92107622002 DPT-3 (0-2)EPA 6010 13 PASI-AJMW
EPA 7471 1 PASI-ASHB
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
EPA 7196 1 PASI-ASDH
92107622003 DPT-2 (0-2)EPA 6010 13 PASI-AJMW
EPA 7471 1 PASI-ASHB
EPA 8270 74 PASI-CPPM
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
EPA 7196 1 PASI-ASDH
92107622004 BG (0-2)EPA 6010 13 PASI-AJMW
EPA 7471 1 PASI-ASHB
ASTM D2974-87 1 PASI-CTNM
EPA 7196 1 PASI-ASDH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-1 (0-2)Lab ID: 92107622001 Collected: 11/30/11 10:15 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 12/07/11 19:11 7440-36-012/06/11 14:500.51
Arsenic 1.1 mg/kg 1 12/07/11 19:11 7440-38-212/06/11 14:500.51
Beryllium 0.79 mg/kg 1 12/07/11 19:11 7440-41-712/06/11 14:500.10
Cadmium 1.2 mg/kg 1 12/07/11 19:11 7440-43-912/06/11 14:500.10
Chromium 6.2 mg/kg 1 12/07/11 19:11 7440-47-312/06/11 14:500.51
Copper 8.5 mg/kg 1 12/07/11 19:11 7440-50-812/06/11 14:500.51
Lead 10.9 mg/kg 1 12/07/11 19:11 7439-92-112/06/11 14:500.51
Manganese 12.6 mg/kg 1 12/07/11 19:11 7439-96-512/06/11 14:500.51
Nickel 1.5 mg/kg 1 12/07/11 19:11 7440-02-012/06/11 14:500.51
Selenium 1.1 mg/kg 1 12/07/11 19:11 7782-49-212/06/11 14:501.0
Silver ND mg/kg 1 12/07/11 19:11 7440-22-412/06/11 14:500.51
Thallium ND mg/kg 1 12/07/11 19:11 7440-28-012/06/11 14:501.0
Zinc 9.3 mg/kg 1 12/07/11 19:11 7440-66-612/06/11 14:501.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.0081 mg/kg 1 12/07/11 12:32 7439-97-612/06/11 18:200.0068
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 12/08/11 17:06 83-32-912/07/11 08:18465
Acenaphthylene ND ug/kg 1 12/08/11 17:06 208-96-812/07/11 08:18465
Aniline ND ug/kg 1 12/08/11 17:06 62-53-312/07/11 08:18465
Anthracene ND ug/kg 1 12/08/11 17:06 120-12-712/07/11 08:18465
Benzo(a)anthracene ND ug/kg 1 12/08/11 17:06 56-55-312/07/11 08:18465
Benzo(a)pyrene ND ug/kg 1 12/08/11 17:06 50-32-812/07/11 08:18465
Benzo(b)fluoranthene ND ug/kg 1 12/08/11 17:06 205-99-212/07/11 08:18465
Benzo(g,h,i)perylene ND ug/kg 1 12/08/11 17:06 191-24-212/07/11 08:18465
Benzo(k)fluoranthene ND ug/kg 1 12/08/11 17:06 207-08-912/07/11 08:18465
Benzoic Acid ND ug/kg 1 12/08/11 17:06 65-85-012/07/11 08:182320
Benzyl alcohol ND ug/kg 1 12/08/11 17:06 100-51-612/07/11 08:18930
4-Bromophenylphenyl ether ND ug/kg 1 12/08/11 17:06 101-55-312/07/11 08:18465
Butylbenzylphthalate ND ug/kg 1 12/08/11 17:06 85-68-712/07/11 08:18465
4-Chloro-3-methylphenol ND ug/kg 1 12/08/11 17:06 59-50-712/07/11 08:18930
4-Chloroaniline ND ug/kg 1 12/08/11 17:06 106-47-812/07/11 08:182320
bis(2-Chloroethoxy)methane ND ug/kg 1 12/08/11 17:06 111-91-112/07/11 08:18465
bis(2-Chloroethyl) ether ND ug/kg 1 12/08/11 17:06 111-44-412/07/11 08:18465
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/08/11 17:06 108-60-112/07/11 08:18465
2-Chloronaphthalene ND ug/kg 1 12/08/11 17:06 91-58-712/07/11 08:18465
2-Chlorophenol ND ug/kg 1 12/08/11 17:06 95-57-812/07/11 08:18465
4-Chlorophenylphenyl ether ND ug/kg 1 12/08/11 17:06 7005-72-312/07/11 08:18465
Chrysene ND ug/kg 1 12/08/11 17:06 218-01-912/07/11 08:18465
Dibenz(a,h)anthracene ND ug/kg 1 12/08/11 17:06 53-70-312/07/11 08:18465
Dibenzofuran ND ug/kg 1 12/08/11 17:06 132-64-912/07/11 08:18465
1,2-Dichlorobenzene ND ug/kg 1 12/08/11 17:06 95-50-112/07/11 08:18465
1,3-Dichlorobenzene ND ug/kg 1 12/08/11 17:06 541-73-112/07/11 08:18465
1,4-Dichlorobenzene ND ug/kg 1 12/08/11 17:06 106-46-712/07/11 08:18465
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 5 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-1 (0-2)Lab ID: 92107622001 Collected: 11/30/11 10:15 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 12/08/11 17:06 91-94-112/07/11 08:182320
2,4-Dichlorophenol ND ug/kg 1 12/08/11 17:06 120-83-212/07/11 08:18465
Diethylphthalate ND ug/kg 1 12/08/11 17:06 84-66-212/07/11 08:18465
2,4-Dimethylphenol ND ug/kg 1 12/08/11 17:06 105-67-912/07/11 08:18465
Dimethylphthalate ND ug/kg 1 12/08/11 17:06 131-11-312/07/11 08:18465
Di-n-butylphthalate ND ug/kg 1 12/08/11 17:06 84-74-212/07/11 08:18465
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/08/11 17:06 534-52-112/07/11 08:18930
2,4-Dinitrophenol ND ug/kg 1 12/08/11 17:06 51-28-512/07/11 08:182320
2,4-Dinitrotoluene ND ug/kg 1 12/08/11 17:06 121-14-212/07/11 08:18465
2,6-Dinitrotoluene ND ug/kg 1 12/08/11 17:06 606-20-212/07/11 08:18465
Di-n-octylphthalate ND ug/kg 1 12/08/11 17:06 117-84-012/07/11 08:18465
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/08/11 17:06 117-81-712/07/11 08:18465
Fluoranthene ND ug/kg 1 12/08/11 17:06 206-44-012/07/11 08:18465
Fluorene ND ug/kg 1 12/08/11 17:06 86-73-712/07/11 08:18465
Hexachloro-1,3-butadiene ND ug/kg 1 12/08/11 17:06 87-68-312/07/11 08:18465
Hexachlorobenzene ND ug/kg 1 12/08/11 17:06 118-74-112/07/11 08:18465
Hexachlorocyclopentadiene ND ug/kg 1 12/08/11 17:06 77-47-412/07/11 08:18465
Hexachloroethane ND ug/kg 1 12/08/11 17:06 67-72-112/07/11 08:18465
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/08/11 17:06 193-39-512/07/11 08:18465
Isophorone ND ug/kg 1 12/08/11 17:06 78-59-112/07/11 08:18465
1-Methylnaphthalene ND ug/kg 1 12/08/11 17:06 90-12-012/07/11 08:18465
2-Methylnaphthalene ND ug/kg 1 12/08/11 17:06 91-57-612/07/11 08:18465
2-Methylphenol(o-Cresol)ND ug/kg 1 12/08/11 17:06 95-48-712/07/11 08:18465
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/08/11 17:0612/07/11 08:18465
Naphthalene ND ug/kg 1 12/08/11 17:06 91-20-312/07/11 08:18465
2-Nitroaniline ND ug/kg 1 12/08/11 17:06 88-74-412/07/11 08:182320
3-Nitroaniline ND ug/kg 1 12/08/11 17:06 99-09-212/07/11 08:182320
4-Nitroaniline ND ug/kg 1 12/08/11 17:06 100-01-612/07/11 08:18930
Nitrobenzene ND ug/kg 1 12/08/11 17:06 98-95-312/07/11 08:18465
2-Nitrophenol ND ug/kg 1 12/08/11 17:06 88-75-512/07/11 08:18465
4-Nitrophenol ND ug/kg 1 12/08/11 17:06 100-02-712/07/11 08:182320
N-Nitrosodimethylamine ND ug/kg 1 12/08/11 17:06 62-75-912/07/11 08:18465
N-Nitroso-di-n-propylamine ND ug/kg 1 12/08/11 17:06 621-64-712/07/11 08:18465
N-Nitrosodiphenylamine ND ug/kg 1 12/08/11 17:06 86-30-612/07/11 08:18465
Pentachlorophenol ND ug/kg 1 12/08/11 17:06 87-86-512/07/11 08:182320
Phenanthrene ND ug/kg 1 12/08/11 17:06 85-01-812/07/11 08:18465
Phenol ND ug/kg 1 12/08/11 17:06 108-95-212/07/11 08:18465
Pyrene ND ug/kg 1 12/08/11 17:06 129-00-012/07/11 08:18465
1,2,4-Trichlorobenzene ND ug/kg 1 12/08/11 17:06 120-82-112/07/11 08:18465
2,4,5-Trichlorophenol ND ug/kg 1 12/08/11 17:06 95-95-412/07/11 08:18465
2,4,6-Trichlorophenol ND ug/kg 1 12/08/11 17:06 88-06-212/07/11 08:18465
Surrogates
Nitrobenzene-d5 (S)47 %1 12/08/11 17:06 4165-60-012/07/11 08:1823-110
2-Fluorobiphenyl (S)52 %1 12/08/11 17:06 321-60-812/07/11 08:1830-110
Terphenyl-d14 (S)58 %1 12/08/11 17:06 1718-51-012/07/11 08:1828-110
Phenol-d6 (S)52 %1 12/08/11 17:06 13127-88-312/07/11 08:1822-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 6 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-1 (0-2)Lab ID: 92107622001 Collected: 11/30/11 10:15 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)58 %1 12/08/11 17:06 367-12-412/07/11 08:1813-110
2,4,6-Tribromophenol (S)52 %1 12/08/11 17:06 118-79-612/07/11 08:1827-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/04/11 16:40 67-64-1119
Benzene ND ug/kg 1 12/04/11 16:40 71-43-25.9
Bromobenzene ND ug/kg 1 12/04/11 16:40 108-86-15.9
Bromochloromethane ND ug/kg 1 12/04/11 16:40 74-97-55.9
Bromodichloromethane ND ug/kg 1 12/04/11 16:40 75-27-45.9
Bromoform ND ug/kg 1 12/04/11 16:40 75-25-25.9
Bromomethane ND ug/kg 1 12/04/11 16:40 74-83-911.9
2-Butanone (MEK)ND ug/kg 1 12/04/11 16:40 78-93-3119
n-Butylbenzene ND ug/kg 1 12/04/11 16:40 104-51-85.9
sec-Butylbenzene ND ug/kg 1 12/04/11 16:40 135-98-85.9
tert-Butylbenzene ND ug/kg 1 12/04/11 16:40 98-06-65.9
Carbon tetrachloride ND ug/kg 1 12/04/11 16:40 56-23-55.9
Chlorobenzene ND ug/kg 1 12/04/11 16:40 108-90-75.9
Chloroethane ND ug/kg 1 12/04/11 16:40 75-00-311.9
Chloroform ND ug/kg 1 12/04/11 16:40 67-66-35.9
Chloromethane ND ug/kg 1 12/04/11 16:40 74-87-311.9
2-Chlorotoluene ND ug/kg 1 12/04/11 16:40 95-49-85.9
4-Chlorotoluene ND ug/kg 1 12/04/11 16:40 106-43-45.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/04/11 16:40 96-12-85.9
Dibromochloromethane ND ug/kg 1 12/04/11 16:40 124-48-15.9
1,2-Dibromoethane (EDB)ND ug/kg 1 12/04/11 16:40 106-93-45.9
Dibromomethane ND ug/kg 1 12/04/11 16:40 74-95-35.9
1,2-Dichlorobenzene ND ug/kg 1 12/04/11 16:40 95-50-15.9
1,3-Dichlorobenzene ND ug/kg 1 12/04/11 16:40 541-73-15.9
1,4-Dichlorobenzene ND ug/kg 1 12/04/11 16:40 106-46-75.9
Dichlorodifluoromethane ND ug/kg 1 12/04/11 16:40 75-71-811.9
1,1-Dichloroethane ND ug/kg 1 12/04/11 16:40 75-34-35.9
1,2-Dichloroethane ND ug/kg 1 12/04/11 16:40 107-06-25.9
1,1-Dichloroethene ND ug/kg 1 12/04/11 16:40 75-35-45.9
cis-1,2-Dichloroethene ND ug/kg 1 12/04/11 16:40 156-59-25.9
trans-1,2-Dichloroethene ND ug/kg 1 12/04/11 16:40 156-60-55.9
1,2-Dichloropropane ND ug/kg 1 12/04/11 16:40 78-87-55.9
1,3-Dichloropropane ND ug/kg 1 12/04/11 16:40 142-28-95.9
2,2-Dichloropropane ND ug/kg 1 12/04/11 16:40 594-20-75.9
1,1-Dichloropropene ND ug/kg 1 12/04/11 16:40 563-58-65.9
cis-1,3-Dichloropropene ND ug/kg 1 12/04/11 16:40 10061-01-55.9
trans-1,3-Dichloropropene ND ug/kg 1 12/04/11 16:40 10061-02-65.9
Diisopropyl ether ND ug/kg 1 12/04/11 16:40 108-20-35.9
Ethylbenzene ND ug/kg 1 12/04/11 16:40 100-41-45.9
Hexachloro-1,3-butadiene ND ug/kg 1 12/04/11 16:40 87-68-35.9
2-Hexanone ND ug/kg 1 12/04/11 16:40 591-78-659.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 7 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-1 (0-2)Lab ID: 92107622001 Collected: 11/30/11 10:15 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Isopropylbenzene (Cumene)ND ug/kg 1 12/04/11 16:40 98-82-85.9
p-Isopropyltoluene ND ug/kg 1 12/04/11 16:40 99-87-65.9
Methylene Chloride ND ug/kg 1 12/04/11 16:40 75-09-223.7
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/04/11 16:40 108-10-159.3
Methyl-tert-butyl ether ND ug/kg 1 12/04/11 16:40 1634-04-45.9
Naphthalene ND ug/kg 1 12/04/11 16:40 91-20-35.9
n-Propylbenzene ND ug/kg 1 12/04/11 16:40 103-65-15.9
Styrene ND ug/kg 1 12/04/11 16:40 100-42-55.9
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/04/11 16:40 630-20-65.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/04/11 16:40 79-34-55.9
Tetrachloroethene ND ug/kg 1 12/04/11 16:40 127-18-45.9
Toluene ND ug/kg 1 12/04/11 16:40 108-88-35.9
1,2,3-Trichlorobenzene ND ug/kg 1 12/04/11 16:40 87-61-65.9
1,2,4-Trichlorobenzene ND ug/kg 1 12/04/11 16:40 120-82-15.9
1,1,1-Trichloroethane ND ug/kg 1 12/04/11 16:40 71-55-65.9
1,1,2-Trichloroethane ND ug/kg 1 12/04/11 16:40 79-00-55.9
Trichloroethene ND ug/kg 1 12/04/11 16:40 79-01-65.9
Trichlorofluoromethane ND ug/kg 1 12/04/11 16:40 75-69-45.9
1,2,3-Trichloropropane ND ug/kg 1 12/04/11 16:40 96-18-45.9
1,2,4-Trimethylbenzene ND ug/kg 1 12/04/11 16:40 95-63-65.9
1,3,5-Trimethylbenzene ND ug/kg 1 12/04/11 16:40 108-67-85.9
Vinyl acetate ND ug/kg 1 12/04/11 16:40 108-05-459.3
Vinyl chloride ND ug/kg 1 12/04/11 16:40 75-01-411.9
Xylene (Total)ND ug/kg 1 12/04/11 16:40 1330-20-711.9
m&p-Xylene ND ug/kg 1 12/04/11 16:40 179601-23-111.9
o-Xylene ND ug/kg 1 12/04/11 16:40 95-47-65.9
Surrogates
Dibromofluoromethane (S)103 %1 12/04/11 16:40 1868-53-770-130
Toluene-d8 (S)104 %1 12/04/11 16:40 2037-26-570-130
4-Bromofluorobenzene (S)93 %1 12/04/11 16:40 460-00-470-130
1,2-Dichloroethane-d4 (S)127 %1 12/04/11 16:40 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 29.0 %1 12/05/11 15:530.10
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 12/05/11 14:03 18540-29-9 M1,N212/05/11 10:470.51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 8 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-3 (0-2)Lab ID: 92107622002 Collected: 11/30/11 16:50 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 12/07/11 19:16 7440-36-012/06/11 14:500.47
Arsenic 1.3 mg/kg 1 12/07/11 19:16 7440-38-212/06/11 14:500.47
Beryllium 0.76 mg/kg 1 12/07/11 19:16 7440-41-712/06/11 14:500.094
Cadmium ND mg/kg 1 12/07/11 19:16 7440-43-912/06/11 14:500.094
Chromium 1.9 mg/kg 1 12/07/11 19:16 7440-47-312/06/11 14:500.47
Copper 34.1 mg/kg 1 12/07/11 19:16 7440-50-812/06/11 14:500.47
Lead 3.9 mg/kg 1 12/07/11 19:16 7439-92-112/06/11 14:500.47
Manganese 81.3 mg/kg 1 12/07/11 19:16 7439-96-512/06/11 14:500.47
Nickel 1.9 mg/kg 1 12/07/11 19:16 7440-02-012/06/11 14:500.47
Selenium ND mg/kg 1 12/07/11 19:16 7782-49-212/06/11 14:500.94
Silver ND mg/kg 1 12/07/11 19:16 7440-22-412/06/11 14:500.47
Thallium ND mg/kg 1 12/07/11 19:16 7440-28-012/06/11 14:500.94
Zinc 12.9 mg/kg 1 12/07/11 19:16 7440-66-612/06/11 14:500.94
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury ND mg/kg 1 12/07/11 12:45 7439-97-612/06/11 18:200.0042
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 12/08/11 17:34 83-32-912/07/11 08:18379
Acenaphthylene ND ug/kg 1 12/08/11 17:34 208-96-812/07/11 08:18379
Aniline ND ug/kg 1 12/08/11 17:34 62-53-312/07/11 08:18379
Anthracene ND ug/kg 1 12/08/11 17:34 120-12-712/07/11 08:18379
Benzo(a)anthracene ND ug/kg 1 12/08/11 17:34 56-55-312/07/11 08:18379
Benzo(a)pyrene ND ug/kg 1 12/08/11 17:34 50-32-812/07/11 08:18379
Benzo(b)fluoranthene ND ug/kg 1 12/08/11 17:34 205-99-212/07/11 08:18379
Benzo(g,h,i)perylene ND ug/kg 1 12/08/11 17:34 191-24-212/07/11 08:18379
Benzo(k)fluoranthene ND ug/kg 1 12/08/11 17:34 207-08-912/07/11 08:18379
Benzoic Acid ND ug/kg 1 12/08/11 17:34 65-85-012/07/11 08:181890
Benzyl alcohol ND ug/kg 1 12/08/11 17:34 100-51-612/07/11 08:18758
4-Bromophenylphenyl ether ND ug/kg 1 12/08/11 17:34 101-55-312/07/11 08:18379
Butylbenzylphthalate ND ug/kg 1 12/08/11 17:34 85-68-712/07/11 08:18379
4-Chloro-3-methylphenol ND ug/kg 1 12/08/11 17:34 59-50-712/07/11 08:18758
4-Chloroaniline ND ug/kg 1 12/08/11 17:34 106-47-812/07/11 08:181890
bis(2-Chloroethoxy)methane ND ug/kg 1 12/08/11 17:34 111-91-112/07/11 08:18379
bis(2-Chloroethyl) ether ND ug/kg 1 12/08/11 17:34 111-44-412/07/11 08:18379
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/08/11 17:34 108-60-112/07/11 08:18379
2-Chloronaphthalene ND ug/kg 1 12/08/11 17:34 91-58-712/07/11 08:18379
2-Chlorophenol ND ug/kg 1 12/08/11 17:34 95-57-812/07/11 08:18379
4-Chlorophenylphenyl ether ND ug/kg 1 12/08/11 17:34 7005-72-312/07/11 08:18379
Chrysene ND ug/kg 1 12/08/11 17:34 218-01-912/07/11 08:18379
Dibenz(a,h)anthracene ND ug/kg 1 12/08/11 17:34 53-70-312/07/11 08:18379
Dibenzofuran ND ug/kg 1 12/08/11 17:34 132-64-912/07/11 08:18379
1,2-Dichlorobenzene ND ug/kg 1 12/08/11 17:34 95-50-112/07/11 08:18379
1,3-Dichlorobenzene ND ug/kg 1 12/08/11 17:34 541-73-112/07/11 08:18379
1,4-Dichlorobenzene ND ug/kg 1 12/08/11 17:34 106-46-712/07/11 08:18379
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 9 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-3 (0-2)Lab ID: 92107622002 Collected: 11/30/11 16:50 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 12/08/11 17:34 91-94-112/07/11 08:181890
2,4-Dichlorophenol ND ug/kg 1 12/08/11 17:34 120-83-212/07/11 08:18379
Diethylphthalate ND ug/kg 1 12/08/11 17:34 84-66-212/07/11 08:18379
2,4-Dimethylphenol ND ug/kg 1 12/08/11 17:34 105-67-912/07/11 08:18379
Dimethylphthalate ND ug/kg 1 12/08/11 17:34 131-11-312/07/11 08:18379
Di-n-butylphthalate ND ug/kg 1 12/08/11 17:34 84-74-212/07/11 08:18379
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/08/11 17:34 534-52-112/07/11 08:18758
2,4-Dinitrophenol ND ug/kg 1 12/08/11 17:34 51-28-512/07/11 08:181890
2,4-Dinitrotoluene ND ug/kg 1 12/08/11 17:34 121-14-212/07/11 08:18379
2,6-Dinitrotoluene ND ug/kg 1 12/08/11 17:34 606-20-212/07/11 08:18379
Di-n-octylphthalate ND ug/kg 1 12/08/11 17:34 117-84-012/07/11 08:18379
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/08/11 17:34 117-81-712/07/11 08:18379
Fluoranthene ND ug/kg 1 12/08/11 17:34 206-44-012/07/11 08:18379
Fluorene ND ug/kg 1 12/08/11 17:34 86-73-712/07/11 08:18379
Hexachloro-1,3-butadiene ND ug/kg 1 12/08/11 17:34 87-68-312/07/11 08:18379
Hexachlorobenzene ND ug/kg 1 12/08/11 17:34 118-74-112/07/11 08:18379
Hexachlorocyclopentadiene ND ug/kg 1 12/08/11 17:34 77-47-412/07/11 08:18379
Hexachloroethane ND ug/kg 1 12/08/11 17:34 67-72-112/07/11 08:18379
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/08/11 17:34 193-39-512/07/11 08:18379
Isophorone ND ug/kg 1 12/08/11 17:34 78-59-112/07/11 08:18379
1-Methylnaphthalene ND ug/kg 1 12/08/11 17:34 90-12-012/07/11 08:18379
2-Methylnaphthalene ND ug/kg 1 12/08/11 17:34 91-57-612/07/11 08:18379
2-Methylphenol(o-Cresol)ND ug/kg 1 12/08/11 17:34 95-48-712/07/11 08:18379
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/08/11 17:3412/07/11 08:18379
Naphthalene ND ug/kg 1 12/08/11 17:34 91-20-312/07/11 08:18379
2-Nitroaniline ND ug/kg 1 12/08/11 17:34 88-74-412/07/11 08:181890
3-Nitroaniline ND ug/kg 1 12/08/11 17:34 99-09-212/07/11 08:181890
4-Nitroaniline ND ug/kg 1 12/08/11 17:34 100-01-612/07/11 08:18758
Nitrobenzene ND ug/kg 1 12/08/11 17:34 98-95-312/07/11 08:18379
2-Nitrophenol ND ug/kg 1 12/08/11 17:34 88-75-512/07/11 08:18379
4-Nitrophenol ND ug/kg 1 12/08/11 17:34 100-02-712/07/11 08:181890
N-Nitrosodimethylamine ND ug/kg 1 12/08/11 17:34 62-75-912/07/11 08:18379
N-Nitroso-di-n-propylamine ND ug/kg 1 12/08/11 17:34 621-64-712/07/11 08:18379
N-Nitrosodiphenylamine ND ug/kg 1 12/08/11 17:34 86-30-612/07/11 08:18379
Pentachlorophenol ND ug/kg 1 12/08/11 17:34 87-86-512/07/11 08:181890
Phenanthrene ND ug/kg 1 12/08/11 17:34 85-01-812/07/11 08:18379
Phenol ND ug/kg 1 12/08/11 17:34 108-95-212/07/11 08:18379
Pyrene ND ug/kg 1 12/08/11 17:34 129-00-012/07/11 08:18379
1,2,4-Trichlorobenzene ND ug/kg 1 12/08/11 17:34 120-82-112/07/11 08:18379
2,4,5-Trichlorophenol ND ug/kg 1 12/08/11 17:34 95-95-412/07/11 08:18379
2,4,6-Trichlorophenol ND ug/kg 1 12/08/11 17:34 88-06-212/07/11 08:18379
Surrogates
Nitrobenzene-d5 (S)60 %1 12/08/11 17:34 4165-60-012/07/11 08:1823-110
2-Fluorobiphenyl (S)62 %1 12/08/11 17:34 321-60-812/07/11 08:1830-110
Terphenyl-d14 (S)67 %1 12/08/11 17:34 1718-51-012/07/11 08:1828-110
Phenol-d6 (S)17 %1 12/08/11 17:34 13127-88-3 1g12/07/11 08:1822-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 10 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-3 (0-2)Lab ID: 92107622002 Collected: 11/30/11 16:50 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)3 %1 12/08/11 17:34 367-12-4 1g12/07/11 08:1813-110
2,4,6-Tribromophenol (S)2 %1 12/08/11 17:34 118-79-6 1g12/07/11 08:1827-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 12/07/11 14:37 67-64-199.9
Benzene ND ug/kg 1 12/07/11 14:37 71-43-25.0
Bromobenzene ND ug/kg 1 12/07/11 14:37 108-86-15.0
Bromochloromethane ND ug/kg 1 12/07/11 14:37 74-97-55.0
Bromodichloromethane ND ug/kg 1 12/07/11 14:37 75-27-45.0
Bromoform ND ug/kg 1 12/07/11 14:37 75-25-25.0
Bromomethane ND ug/kg 1 12/07/11 14:37 74-83-910
2-Butanone (MEK)ND ug/kg 1 12/07/11 14:37 78-93-399.9
n-Butylbenzene ND ug/kg 1 12/07/11 14:37 104-51-85.0
sec-Butylbenzene ND ug/kg 1 12/07/11 14:37 135-98-85.0
tert-Butylbenzene ND ug/kg 1 12/07/11 14:37 98-06-65.0
Carbon tetrachloride ND ug/kg 1 12/07/11 14:37 56-23-55.0
Chlorobenzene ND ug/kg 1 12/07/11 14:37 108-90-75.0
Chloroethane ND ug/kg 1 12/07/11 14:37 75-00-310
Chloroform ND ug/kg 1 12/07/11 14:37 67-66-35.0
Chloromethane ND ug/kg 1 12/07/11 14:37 74-87-310
2-Chlorotoluene ND ug/kg 1 12/07/11 14:37 95-49-85.0
4-Chlorotoluene ND ug/kg 1 12/07/11 14:37 106-43-45.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/07/11 14:37 96-12-85.0
Dibromochloromethane ND ug/kg 1 12/07/11 14:37 124-48-15.0
1,2-Dibromoethane (EDB)ND ug/kg 1 12/07/11 14:37 106-93-45.0
Dibromomethane ND ug/kg 1 12/07/11 14:37 74-95-35.0
1,2-Dichlorobenzene ND ug/kg 1 12/07/11 14:37 95-50-15.0
1,3-Dichlorobenzene ND ug/kg 1 12/07/11 14:37 541-73-15.0
1,4-Dichlorobenzene ND ug/kg 1 12/07/11 14:37 106-46-75.0
Dichlorodifluoromethane ND ug/kg 1 12/07/11 14:37 75-71-810
1,1-Dichloroethane ND ug/kg 1 12/07/11 14:37 75-34-35.0
1,2-Dichloroethane ND ug/kg 1 12/07/11 14:37 107-06-25.0
1,1-Dichloroethene ND ug/kg 1 12/07/11 14:37 75-35-45.0
cis-1,2-Dichloroethene ND ug/kg 1 12/07/11 14:37 156-59-25.0
trans-1,2-Dichloroethene ND ug/kg 1 12/07/11 14:37 156-60-55.0
1,2-Dichloropropane ND ug/kg 1 12/07/11 14:37 78-87-55.0
1,3-Dichloropropane ND ug/kg 1 12/07/11 14:37 142-28-95.0
2,2-Dichloropropane ND ug/kg 1 12/07/11 14:37 594-20-75.0
1,1-Dichloropropene ND ug/kg 1 12/07/11 14:37 563-58-65.0
cis-1,3-Dichloropropene ND ug/kg 1 12/07/11 14:37 10061-01-55.0
trans-1,3-Dichloropropene ND ug/kg 1 12/07/11 14:37 10061-02-65.0
Diisopropyl ether ND ug/kg 1 12/07/11 14:37 108-20-35.0
Ethylbenzene ND ug/kg 1 12/07/11 14:37 100-41-45.0
Hexachloro-1,3-butadiene ND ug/kg 1 12/07/11 14:37 87-68-35.0
2-Hexanone ND ug/kg 1 12/07/11 14:37 591-78-649.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 11 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-3 (0-2)Lab ID: 92107622002 Collected: 11/30/11 16:50 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Isopropylbenzene (Cumene)ND ug/kg 1 12/07/11 14:37 98-82-85.0
p-Isopropyltoluene ND ug/kg 1 12/07/11 14:37 99-87-65.0
Methylene Chloride ND ug/kg 1 12/07/11 14:37 75-09-220.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/07/11 14:37 108-10-149.9
Methyl-tert-butyl ether ND ug/kg 1 12/07/11 14:37 1634-04-45.0
Naphthalene ND ug/kg 1 12/07/11 14:37 91-20-35.0
n-Propylbenzene ND ug/kg 1 12/07/11 14:37 103-65-15.0
Styrene ND ug/kg 1 12/07/11 14:37 100-42-55.0
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/07/11 14:37 630-20-65.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/07/11 14:37 79-34-55.0
Tetrachloroethene ND ug/kg 1 12/07/11 14:37 127-18-45.0
Toluene ND ug/kg 1 12/07/11 14:37 108-88-35.0
1,2,3-Trichlorobenzene ND ug/kg 1 12/07/11 14:37 87-61-65.0
1,2,4-Trichlorobenzene ND ug/kg 1 12/07/11 14:37 120-82-15.0
1,1,1-Trichloroethane ND ug/kg 1 12/07/11 14:37 71-55-65.0
1,1,2-Trichloroethane ND ug/kg 1 12/07/11 14:37 79-00-55.0
Trichloroethene ND ug/kg 1 12/07/11 14:37 79-01-65.0
Trichlorofluoromethane ND ug/kg 1 12/07/11 14:37 75-69-45.0
1,2,3-Trichloropropane ND ug/kg 1 12/07/11 14:37 96-18-45.0
1,2,4-Trimethylbenzene ND ug/kg 1 12/07/11 14:37 95-63-65.0
1,3,5-Trimethylbenzene ND ug/kg 1 12/07/11 14:37 108-67-85.0
Vinyl acetate ND ug/kg 1 12/07/11 14:37 108-05-449.9
Vinyl chloride ND ug/kg 1 12/07/11 14:37 75-01-410
Xylene (Total)ND ug/kg 1 12/07/11 14:37 1330-20-710
m&p-Xylene ND ug/kg 1 12/07/11 14:37 179601-23-110
o-Xylene ND ug/kg 1 12/07/11 14:37 95-47-65.0
Surrogates
Dibromofluoromethane (S)108 %1 12/07/11 14:37 1868-53-770-130
Toluene-d8 (S)100 %1 12/07/11 14:37 2037-26-570-130
4-Bromofluorobenzene (S)95 %1 12/07/11 14:37 460-00-470-130
1,2-Dichloroethane-d4 (S)111 %1 12/07/11 14:37 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 12.9 %1 12/05/11 16:010.10
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 12/05/11 14:03 18540-29-9 N212/05/11 10:470.56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 12 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-2 (0-2)Lab ID: 92107622003 Collected: 11/30/11 17:40 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 12/07/11 19:20 7440-36-012/06/11 14:500.52
Arsenic 1.9 mg/kg 1 12/07/11 19:20 7440-38-212/06/11 14:500.52
Beryllium 0.49 mg/kg 1 12/07/11 19:20 7440-41-712/06/11 14:500.10
Cadmium 0.63 mg/kg 1 12/07/11 19:20 7440-43-912/06/11 14:500.10
Chromium 40.3 mg/kg 1 12/07/11 19:20 7440-47-312/06/11 14:500.52
Copper 37.0 mg/kg 1 12/07/11 19:20 7440-50-812/06/11 14:500.52
Lead 173 mg/kg 1 12/07/11 19:20 7439-92-112/06/11 14:500.52
Manganese 237 mg/kg 1 12/07/11 19:20 7439-96-512/06/11 14:500.52
Nickel 5.8 mg/kg 1 12/07/11 19:20 7440-02-012/06/11 14:500.52
Selenium ND mg/kg 1 12/07/11 19:20 7782-49-212/06/11 14:501.0
Silver ND mg/kg 1 12/07/11 19:20 7440-22-412/06/11 14:500.52
Thallium ND mg/kg 1 12/07/11 19:20 7440-28-012/06/11 14:501.0
Zinc 40.4 mg/kg 1 12/07/11 19:20 7440-66-612/06/11 14:501.0
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.063 mg/kg 1 12/07/11 12:50 7439-97-612/06/11 18:200.0041
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 1 12/06/11 14:36 83-32-912/05/11 13:30380
Acenaphthylene ND ug/kg 1 12/06/11 14:36 208-96-812/05/11 13:30380
Aniline ND ug/kg 1 12/06/11 14:36 62-53-312/05/11 13:30380
Anthracene ND ug/kg 1 12/06/11 14:36 120-12-712/05/11 13:30380
Benzo(a)anthracene ND ug/kg 1 12/06/11 14:36 56-55-312/05/11 13:30380
Benzo(a)pyrene ND ug/kg 1 12/06/11 14:36 50-32-812/05/11 13:30380
Benzo(b)fluoranthene ND ug/kg 1 12/06/11 14:36 205-99-212/05/11 13:30380
Benzo(g,h,i)perylene ND ug/kg 1 12/06/11 14:36 191-24-212/05/11 13:30380
Benzo(k)fluoranthene ND ug/kg 1 12/06/11 14:36 207-08-912/05/11 13:30380
Benzoic Acid ND ug/kg 1 12/06/11 14:36 65-85-012/05/11 13:301900
Benzyl alcohol ND ug/kg 1 12/06/11 14:36 100-51-612/05/11 13:30760
4-Bromophenylphenyl ether ND ug/kg 1 12/06/11 14:36 101-55-312/05/11 13:30380
Butylbenzylphthalate ND ug/kg 1 12/06/11 14:36 85-68-712/05/11 13:30380
4-Chloro-3-methylphenol ND ug/kg 1 12/06/11 14:36 59-50-712/05/11 13:30760
4-Chloroaniline ND ug/kg 1 12/06/11 14:36 106-47-812/05/11 13:301900
bis(2-Chloroethoxy)methane ND ug/kg 1 12/06/11 14:36 111-91-112/05/11 13:30380
bis(2-Chloroethyl) ether ND ug/kg 1 12/06/11 14:36 111-44-412/05/11 13:30380
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/06/11 14:36 108-60-112/05/11 13:30380
2-Chloronaphthalene ND ug/kg 1 12/06/11 14:36 91-58-712/05/11 13:30380
2-Chlorophenol ND ug/kg 1 12/06/11 14:36 95-57-812/05/11 13:30380
4-Chlorophenylphenyl ether ND ug/kg 1 12/06/11 14:36 7005-72-312/05/11 13:30380
Chrysene ND ug/kg 1 12/06/11 14:36 218-01-912/05/11 13:30380
Dibenz(a,h)anthracene ND ug/kg 1 12/06/11 14:36 53-70-312/05/11 13:30380
Dibenzofuran ND ug/kg 1 12/06/11 14:36 132-64-912/05/11 13:30380
1,2-Dichlorobenzene ND ug/kg 1 12/06/11 14:36 95-50-112/05/11 13:30380
1,3-Dichlorobenzene ND ug/kg 1 12/06/11 14:36 541-73-112/05/11 13:30380
1,4-Dichlorobenzene ND ug/kg 1 12/06/11 14:36 106-46-712/05/11 13:30380
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 13 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-2 (0-2)Lab ID: 92107622003 Collected: 11/30/11 17:40 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 1 12/06/11 14:36 91-94-112/05/11 13:301900
2,4-Dichlorophenol ND ug/kg 1 12/06/11 14:36 120-83-212/05/11 13:30380
Diethylphthalate ND ug/kg 1 12/06/11 14:36 84-66-212/05/11 13:30380
2,4-Dimethylphenol ND ug/kg 1 12/06/11 14:36 105-67-912/05/11 13:30380
Dimethylphthalate ND ug/kg 1 12/06/11 14:36 131-11-312/05/11 13:30380
Di-n-butylphthalate ND ug/kg 1 12/06/11 14:36 84-74-212/05/11 13:30380
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/06/11 14:36 534-52-112/05/11 13:30760
2,4-Dinitrophenol ND ug/kg 1 12/06/11 14:36 51-28-512/05/11 13:301900
2,4-Dinitrotoluene ND ug/kg 1 12/06/11 14:36 121-14-212/05/11 13:30380
2,6-Dinitrotoluene ND ug/kg 1 12/06/11 14:36 606-20-212/05/11 13:30380
Di-n-octylphthalate ND ug/kg 1 12/06/11 14:36 117-84-012/05/11 13:30380
bis(2-Ethylhexyl)phthalate 1900 ug/kg 1 12/06/11 14:36 117-81-712/05/11 13:30380
Fluoranthene ND ug/kg 1 12/06/11 14:36 206-44-012/05/11 13:30380
Fluorene ND ug/kg 1 12/06/11 14:36 86-73-712/05/11 13:30380
Hexachloro-1,3-butadiene ND ug/kg 1 12/06/11 14:36 87-68-312/05/11 13:30380
Hexachlorobenzene ND ug/kg 1 12/06/11 14:36 118-74-112/05/11 13:30380
Hexachlorocyclopentadiene ND ug/kg 1 12/06/11 14:36 77-47-412/05/11 13:30380
Hexachloroethane ND ug/kg 1 12/06/11 14:36 67-72-112/05/11 13:30380
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/06/11 14:36 193-39-512/05/11 13:30380
Isophorone ND ug/kg 1 12/06/11 14:36 78-59-112/05/11 13:30380
1-Methylnaphthalene ND ug/kg 1 12/06/11 14:36 90-12-012/05/11 13:30380
2-Methylnaphthalene ND ug/kg 1 12/06/11 14:36 91-57-612/05/11 13:30380
2-Methylphenol(o-Cresol)ND ug/kg 1 12/06/11 14:36 95-48-712/05/11 13:30380
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/06/11 14:3612/05/11 13:30380
Naphthalene ND ug/kg 1 12/06/11 14:36 91-20-312/05/11 13:30380
2-Nitroaniline ND ug/kg 1 12/06/11 14:36 88-74-412/05/11 13:301900
3-Nitroaniline ND ug/kg 1 12/06/11 14:36 99-09-212/05/11 13:301900
4-Nitroaniline ND ug/kg 1 12/06/11 14:36 100-01-612/05/11 13:30760
Nitrobenzene ND ug/kg 1 12/06/11 14:36 98-95-312/05/11 13:30380
2-Nitrophenol ND ug/kg 1 12/06/11 14:36 88-75-512/05/11 13:30380
4-Nitrophenol ND ug/kg 1 12/06/11 14:36 100-02-712/05/11 13:301900
N-Nitrosodimethylamine ND ug/kg 1 12/06/11 14:36 62-75-912/05/11 13:30380
N-Nitroso-di-n-propylamine ND ug/kg 1 12/06/11 14:36 621-64-712/05/11 13:30380
N-Nitrosodiphenylamine ND ug/kg 1 12/06/11 14:36 86-30-612/05/11 13:30380
Pentachlorophenol ND ug/kg 1 12/06/11 14:36 87-86-512/05/11 13:301900
Phenanthrene ND ug/kg 1 12/06/11 14:36 85-01-812/05/11 13:30380
Phenol ND ug/kg 1 12/06/11 14:36 108-95-212/05/11 13:30380
Pyrene ND ug/kg 1 12/06/11 14:36 129-00-012/05/11 13:30380
1,2,4-Trichlorobenzene ND ug/kg 1 12/06/11 14:36 120-82-112/05/11 13:30380
2,4,5-Trichlorophenol ND ug/kg 1 12/06/11 14:36 95-95-412/05/11 13:30380
2,4,6-Trichlorophenol ND ug/kg 1 12/06/11 14:36 88-06-212/05/11 13:30380
Surrogates
Nitrobenzene-d5 (S)34 %1 12/06/11 14:36 4165-60-012/05/11 13:3023-110
2-Fluorobiphenyl (S)35 %1 12/06/11 14:36 321-60-812/05/11 13:3030-110
Terphenyl-d14 (S)43 %1 12/06/11 14:36 1718-51-012/05/11 13:3028-110
Phenol-d6 (S)29 %1 12/06/11 14:36 13127-88-312/05/11 13:3022-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 14 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-2 (0-2)Lab ID: 92107622003 Collected: 11/30/11 17:40 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)22 %1 12/06/11 14:36 367-12-412/05/11 13:3013-110
2,4,6-Tribromophenol (S)41 %1 12/06/11 14:36 118-79-612/05/11 13:3027-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 169 ug/kg 1 12/07/11 14:56 67-64-1 C995.8
Benzene ND ug/kg 1 12/07/11 14:56 71-43-24.8
Bromobenzene ND ug/kg 1 12/07/11 14:56 108-86-14.8
Bromochloromethane ND ug/kg 1 12/07/11 14:56 74-97-54.8
Bromodichloromethane ND ug/kg 1 12/07/11 14:56 75-27-44.8
Bromoform ND ug/kg 1 12/07/11 14:56 75-25-24.8
Bromomethane ND ug/kg 1 12/07/11 14:56 74-83-99.6
2-Butanone (MEK)ND ug/kg 1 12/07/11 14:56 78-93-395.8
n-Butylbenzene ND ug/kg 1 12/07/11 14:56 104-51-84.8
sec-Butylbenzene ND ug/kg 1 12/07/11 14:56 135-98-84.8
tert-Butylbenzene ND ug/kg 1 12/07/11 14:56 98-06-64.8
Carbon tetrachloride ND ug/kg 1 12/07/11 14:56 56-23-54.8
Chlorobenzene ND ug/kg 1 12/07/11 14:56 108-90-74.8
Chloroethane ND ug/kg 1 12/07/11 14:56 75-00-39.6
Chloroform ND ug/kg 1 12/07/11 14:56 67-66-34.8
Chloromethane ND ug/kg 1 12/07/11 14:56 74-87-39.6
2-Chlorotoluene ND ug/kg 1 12/07/11 14:56 95-49-84.8
4-Chlorotoluene ND ug/kg 1 12/07/11 14:56 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 12/07/11 14:56 96-12-84.8
Dibromochloromethane ND ug/kg 1 12/07/11 14:56 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 12/07/11 14:56 106-93-44.8
Dibromomethane ND ug/kg 1 12/07/11 14:56 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 12/07/11 14:56 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 12/07/11 14:56 541-73-14.8
1,4-Dichlorobenzene ND ug/kg 1 12/07/11 14:56 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 12/07/11 14:56 75-71-89.6
1,1-Dichloroethane ND ug/kg 1 12/07/11 14:56 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 12/07/11 14:56 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 12/07/11 14:56 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 12/07/11 14:56 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 12/07/11 14:56 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 12/07/11 14:56 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 12/07/11 14:56 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 12/07/11 14:56 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 12/07/11 14:56 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 12/07/11 14:56 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 12/07/11 14:56 10061-02-64.8
Diisopropyl ether ND ug/kg 1 12/07/11 14:56 108-20-34.8
Ethylbenzene ND ug/kg 1 12/07/11 14:56 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 12/07/11 14:56 87-68-34.8
2-Hexanone ND ug/kg 1 12/07/11 14:56 591-78-647.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 15 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: DPT-2 (0-2)Lab ID: 92107622003 Collected: 11/30/11 17:40 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Isopropylbenzene (Cumene)ND ug/kg 1 12/07/11 14:56 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 12/07/11 14:56 99-87-64.8
Methylene Chloride ND ug/kg 1 12/07/11 14:56 75-09-219.2
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 12/07/11 14:56 108-10-147.9
Methyl-tert-butyl ether ND ug/kg 1 12/07/11 14:56 1634-04-44.8
Naphthalene ND ug/kg 1 12/07/11 14:56 91-20-34.8
n-Propylbenzene ND ug/kg 1 12/07/11 14:56 103-65-14.8
Styrene ND ug/kg 1 12/07/11 14:56 100-42-54.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 12/07/11 14:56 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 12/07/11 14:56 79-34-54.8
Tetrachloroethene ND ug/kg 1 12/07/11 14:56 127-18-44.8
Toluene ND ug/kg 1 12/07/11 14:56 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 12/07/11 14:56 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 12/07/11 14:56 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 12/07/11 14:56 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 12/07/11 14:56 79-00-54.8
Trichloroethene ND ug/kg 1 12/07/11 14:56 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 12/07/11 14:56 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 12/07/11 14:56 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 12/07/11 14:56 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 12/07/11 14:56 108-67-84.8
Vinyl acetate ND ug/kg 1 12/07/11 14:56 108-05-447.9
Vinyl chloride ND ug/kg 1 12/07/11 14:56 75-01-49.6
Xylene (Total)ND ug/kg 1 12/07/11 14:56 1330-20-79.6
m&p-Xylene ND ug/kg 1 12/07/11 14:56 179601-23-19.6
o-Xylene ND ug/kg 1 12/07/11 14:56 95-47-64.8
Surrogates
Dibromofluoromethane (S)109 %1 12/07/11 14:56 1868-53-770-130
Toluene-d8 (S)99 %1 12/07/11 14:56 2037-26-570-130
4-Bromofluorobenzene (S)90 %1 12/07/11 14:56 460-00-470-130
1,2-Dichloroethane-d4 (S)107 %1 12/07/11 14:56 17060-07-070-132
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 12.0 %1 12/05/11 16:010.10
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 12/05/11 14:03 18540-29-9 N212/05/11 10:470.48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 16 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Sample: BG (0-2)Lab ID: 92107622004 Collected: 12/01/11 08:30 Received: 12/02/11 14:30 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 1 12/07/11 19:35 7440-36-012/06/11 14:500.54
Arsenic 1.9 mg/kg 1 12/07/11 19:35 7440-38-212/06/11 14:500.54
Beryllium 0.33 mg/kg 1 12/07/11 19:35 7440-41-712/06/11 14:500.11
Cadmium 2.1 mg/kg 1 12/07/11 19:35 7440-43-912/06/11 14:500.11
Chromium 2.7 mg/kg 1 12/07/11 19:35 7440-47-312/06/11 14:500.54
Copper 21.0 mg/kg 1 12/07/11 19:35 7440-50-812/06/11 14:500.54
Lead 3.3 mg/kg 1 12/07/11 19:35 7439-92-112/06/11 14:500.54
Manganese 105 mg/kg 1 12/07/11 19:35 7439-96-512/06/11 14:500.54
Nickel 5.3 mg/kg 1 12/07/11 19:35 7440-02-012/06/11 14:500.54
Selenium ND mg/kg 1 12/07/11 19:35 7782-49-212/06/11 14:501.1
Silver ND mg/kg 1 12/07/11 19:35 7440-22-412/06/11 14:500.54
Thallium 1.4 mg/kg 1 12/07/11 19:35 7440-28-012/06/11 14:501.1
Zinc 41.7 mg/kg 1 12/07/11 19:35 7440-66-612/06/11 14:501.1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.0079 mg/kg 1 12/07/11 12:53 7439-97-612/06/11 18:200.0054
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 21.0 %1 12/07/11 17:450.10
7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196
Chromium, Hexavalent ND mg/kg 1 12/05/11 14:03 18540-29-9 N212/05/11 10:470.47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 17 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/3906
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples: 92107622001, 92107622002, 92107622003, 92107622004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695573
Associated Lab Samples:92107622001, 92107622002, 92107622003, 92107622004
Matrix: Solid
Analyzed
Mercury mg/kg ND 0.0050 12/07/11 12:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695574LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.066.067 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
695575MATRIX SPIKE SAMPLE:
MSSpike
Result
92107622001
Mercury mg/kg 0.095.087 99 75-1250.0081
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107622002
695576SAMPLE DUPLICATE:
Mercury mg/kg .0026J 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 18 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/9523
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples: 92107622001, 92107622002, 92107622003, 92107622004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695596
Associated Lab Samples:92107622001, 92107622002, 92107622003, 92107622004
Matrix: Solid
Analyzed
Antimony mg/kg ND 0.50 12/07/11 18:26
Arsenic mg/kg ND 0.50 12/07/11 18:26
Beryllium mg/kg ND 0.10 12/07/11 18:26
Cadmium mg/kg ND 0.10 12/07/11 18:26
Chromium mg/kg ND 0.50 12/07/11 18:26
Copper mg/kg ND 0.50 12/07/11 18:26
Lead mg/kg ND 0.50 12/07/11 18:26
Manganese mg/kg ND 0.50 12/07/11 18:26
Nickel mg/kg ND 0.50 12/07/11 18:26
Selenium mg/kg ND 1.0 12/07/11 18:26
Silver mg/kg ND 0.50 12/07/11 18:26
Thallium mg/kg ND 1.0 12/07/11 18:26
Zinc mg/kg ND 1.0 12/07/11 18:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695597LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 46.450 93 80-120
Arsenic mg/kg 48.350 97 80-120
Beryllium mg/kg 50.050 100 80-120
Cadmium mg/kg 47.650 95 80-120
Chromium mg/kg 48.050 96 80-120
Copper mg/kg 47.650 95 80-120
Lead mg/kg 48.850 98 80-120
Manganese mg/kg 47.350 95 80-120
Nickel mg/kg 47.050 94 80-120
Selenium mg/kg 47.550 95 80-120
Silver mg/kg 24.125 96 80-120
Thallium mg/kg 46.050 92 80-120
Zinc mg/kg 48.550 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
695598MATRIX SPIKE SAMPLE:
MSSpike
Result
92107555001
Antimony mg/kg 44.347.2 94 75-125ND
Arsenic mg/kg 46.347.2 98 75-125ND
Beryllium mg/kg 47.747.2 101 75-125ND
Cadmium mg/kg 45.247.2 96 75-125ND
Chromium mg/kg 46.547.2 97 75-1250.778 ug/g
Copper mg/kg 74.447.2 98 75-12528.0 ug/g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 19 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
695598MATRIX SPIKE SAMPLE:
MSSpike
Result
92107555001
Lead mg/kg 46.347.2 98 75-125ND
Manganese mg/kg 52.747.2 95 75-1257.97 ug/g
Nickel mg/kg 88.847.2 96 75-12543.5 ug/g
Selenium mg/kg 45.747.2 96 75-125ND
Silver mg/kg 23.023.6 97 75-125ND
Thallium mg/kg 43.547.2 92 75-125ND
Zinc mg/kg 49.347.2 98 75-1252.89 ug/g
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107555002
695599SAMPLE DUPLICATE:
Antimony mg/kg ND 20ND
Arsenic mg/kg ND 20ND
Beryllium mg/kg .036J 20ND
Cadmium mg/kg ND 20ND
Chromium mg/kg .035J 20ND
Copper mg/kg .44J 200.440 ug/g
Lead mg/kg ND 20ND
Manganese mg/kg ND 20ND
Nickel mg/kg ND 20ND
Selenium mg/kg ND 20ND
Silver mg/kg .076J 20ND
Thallium mg/kg ND 20ND
Zinc mg/kg ND 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 20 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/17530
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92107622001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695184
Associated Lab Samples:92107622001
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.6 12/04/11 11:04
1,1,1-Trichloroethane ug/kg ND 4.6 12/04/11 11:04
1,1,2,2-Tetrachloroethane ug/kg ND 4.6 12/04/11 11:04
1,1,2-Trichloroethane ug/kg ND 4.6 12/04/11 11:04
1,1-Dichloroethane ug/kg ND 4.6 12/04/11 11:04
1,1-Dichloroethene ug/kg ND 4.6 12/04/11 11:04
1,1-Dichloropropene ug/kg ND 4.6 12/04/11 11:04
1,2,3-Trichlorobenzene ug/kg ND 4.6 12/04/11 11:04
1,2,3-Trichloropropane ug/kg ND 4.6 12/04/11 11:04
1,2,4-Trichlorobenzene ug/kg ND 4.6 12/04/11 11:04
1,2,4-Trimethylbenzene ug/kg ND 4.6 12/04/11 11:04
1,2-Dibromo-3-chloropropane ug/kg ND 4.6 12/04/11 11:04
1,2-Dibromoethane (EDB)ug/kg ND 4.6 12/04/11 11:04
1,2-Dichlorobenzene ug/kg ND 4.6 12/04/11 11:04
1,2-Dichloroethane ug/kg ND 4.6 12/04/11 11:04
1,2-Dichloropropane ug/kg ND 4.6 12/04/11 11:04
1,3,5-Trimethylbenzene ug/kg ND 4.6 12/04/11 11:04
1,3-Dichlorobenzene ug/kg ND 4.6 12/04/11 11:04
1,3-Dichloropropane ug/kg ND 4.6 12/04/11 11:04
1,4-Dichlorobenzene ug/kg ND 4.6 12/04/11 11:04
2,2-Dichloropropane ug/kg ND 4.6 12/04/11 11:04
2-Butanone (MEK)ug/kg ND 92.4 12/04/11 11:04
2-Chlorotoluene ug/kg ND 4.6 12/04/11 11:04
2-Hexanone ug/kg ND 46.2 12/04/11 11:04
4-Chlorotoluene ug/kg ND 4.6 12/04/11 11:04
4-Methyl-2-pentanone (MIBK) ug/kg ND 46.2 12/04/11 11:04
Acetone ug/kg ND 92.4 12/04/11 11:04
Benzene ug/kg ND 4.6 12/04/11 11:04
Bromobenzene ug/kg ND 4.6 12/04/11 11:04
Bromochloromethane ug/kg ND 4.6 12/04/11 11:04
Bromodichloromethane ug/kg ND 4.6 12/04/11 11:04
Bromoform ug/kg ND 4.6 12/04/11 11:04
Bromomethane ug/kg ND 9.2 12/04/11 11:04
Carbon tetrachloride ug/kg ND 4.6 12/04/11 11:04
Chlorobenzene ug/kg ND 4.6 12/04/11 11:04
Chloroethane ug/kg ND 9.2 12/04/11 11:04
Chloroform ug/kg ND 4.6 12/04/11 11:04
Chloromethane ug/kg ND 9.2 12/04/11 11:04
cis-1,2-Dichloroethene ug/kg ND 4.6 12/04/11 11:04
cis-1,3-Dichloropropene ug/kg ND 4.6 12/04/11 11:04
Dibromochloromethane ug/kg ND 4.6 12/04/11 11:04
Dibromomethane ug/kg ND 4.6 12/04/11 11:04
Dichlorodifluoromethane ug/kg ND 9.2 12/04/11 11:04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 21 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695184
Associated Lab Samples:92107622001
Matrix: Solid
Analyzed
Diisopropyl ether ug/kg ND 4.6 12/04/11 11:04
Ethylbenzene ug/kg ND 4.6 12/04/11 11:04
Hexachloro-1,3-butadiene ug/kg ND 4.6 12/04/11 11:04
Isopropylbenzene (Cumene) ug/kg ND 4.6 12/04/11 11:04
m&p-Xylene ug/kg ND 9.2 12/04/11 11:04
Methyl-tert-butyl ether ug/kg ND 4.6 12/04/11 11:04
Methylene Chloride ug/kg ND 18.5 12/04/11 11:04
n-Butylbenzene ug/kg ND 4.6 12/04/11 11:04
n-Propylbenzene ug/kg ND 4.6 12/04/11 11:04
Naphthalene ug/kg ND 4.6 12/04/11 11:04
o-Xylene ug/kg ND 4.6 12/04/11 11:04
p-Isopropyltoluene ug/kg ND 4.6 12/04/11 11:04
sec-Butylbenzene ug/kg ND 4.6 12/04/11 11:04
Styrene ug/kg ND 4.6 12/04/11 11:04
tert-Butylbenzene ug/kg ND 4.6 12/04/11 11:04
Tetrachloroethene ug/kg ND 4.6 12/04/11 11:04
Toluene ug/kg ND 4.6 12/04/11 11:04
trans-1,2-Dichloroethene ug/kg ND 4.6 12/04/11 11:04
trans-1,3-Dichloropropene ug/kg ND 4.6 12/04/11 11:04
Trichloroethene ug/kg ND 4.6 12/04/11 11:04
Trichlorofluoromethane ug/kg ND 4.6 12/04/11 11:04
Vinyl acetate ug/kg ND 46.2 12/04/11 11:04
Vinyl chloride ug/kg ND 9.2 12/04/11 11:04
Xylene (Total)ug/kg ND 9.2 12/04/11 11:04
1,2-Dichloroethane-d4 (S)%131 70-132 12/04/11 11:04
4-Bromofluorobenzene (S)%101 70-130 12/04/11 11:04
Dibromofluoromethane (S)%109 70-130 12/04/11 11:04
Toluene-d8 (S)%100 70-130 12/04/11 11:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695185LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 63.651.1 124 70-131
1,1,1-Trichloroethane ug/kg 60.751.1 119 70-141
1,1,2,2-Tetrachloroethane ug/kg 62.651.1 122 70-130
1,1,2-Trichloroethane ug/kg 55.851.1 109 70-132
1,1-Dichloroethane ug/kg 56.351.1 110 70-143
1,1-Dichloroethene ug/kg 67.651.1 132 70-137
1,1-Dichloropropene ug/kg 53.451.1 104 70-135
1,2,3-Trichlorobenzene ug/kg 57.851.1 113 69-153
1,2,3-Trichloropropane ug/kg 57.851.1 113 70-130
1,2,4-Trichlorobenzene ug/kg 56.751.1 111 55-171
1,2,4-Trimethylbenzene ug/kg 55.751.1 109 70-149
1,2-Dibromo-3-chloropropane ug/kg 70.751.1 138 68-141
1,2-Dibromoethane (EDB)ug/kg 60.151.1 118 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 22 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695185LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 55.151.1 108 70-140
1,2-Dichloroethane ug/kg 69.051.1 135 70-137
1,2-Dichloropropane ug/kg 54.151.1 106 70-133
1,3,5-Trimethylbenzene ug/kg 55.851.1 109 70-143
1,3-Dichlorobenzene ug/kg 55.351.1 108 70-144
1,3-Dichloropropane ug/kg 61.651.1 120 70-132
1,4-Dichlorobenzene ug/kg 56.751.1 111 70-142
2,2-Dichloropropane ug/kg 61.251.1 120 68-152
2-Butanone (MEK)ug/kg 124102 121 70-149
2-Chlorotoluene ug/kg 58.851.1 115 70-141
2-Hexanone ug/kg 149102 145 70-149
4-Chlorotoluene ug/kg 59.751.1 117 70-149
4-Methyl-2-pentanone (MIBK) ug/kg 136102 133 70-153
Acetone ug/kg 130102 127 70-157
Benzene ug/kg 52.051.1 102 70-130
Bromobenzene ug/kg 60.351.1 118 70-141
Bromochloromethane ug/kg 54.351.1 106 70-149
Bromodichloromethane ug/kg 62.251.1 122 70-130
Bromoform ug/kg 52.551.1 103 70-131
Bromomethane ug/kg 63.951.1 125 64-136
Carbon tetrachloride ug/kg 63.451.1 124 70-154
Chlorobenzene ug/kg 58.551.1 114 70-135
Chloroethane ug/kg 58.251.1 114 68-151
Chloroform ug/kg 58.951.1 115 70-130
Chloromethane ug/kg 57.051.1 111 70-132
cis-1,2-Dichloroethene ug/kg 56.851.1 111 70-140
cis-1,3-Dichloropropene ug/kg 57.051.1 111 70-137
Dibromochloromethane ug/kg 62.651.1 123 70-130
Dibromomethane ug/kg 63.251.1 124 70-136
Dichlorodifluoromethane ug/kg 57.751.1 113 36-148
Diisopropyl ether ug/kg 61.351.1 120 70-139
Ethylbenzene ug/kg 58.951.1 115 70-137
Hexachloro-1,3-butadiene ug/kg 53.951.1 105 70-145
Isopropylbenzene (Cumene) ug/kg 60.951.1 119 70-141
m&p-Xylene ug/kg 117102 114 70-140
Methyl-tert-butyl ether ug/kg 67.151.1 131 45-150
Methylene Chloride ug/kg 70.7 L351.1 138 70-133
n-Butylbenzene ug/kg 56.151.1 110 65-155
n-Propylbenzene ug/kg 55.651.1 109 70-148
Naphthalene ug/kg 61.151.1 119 70-148
o-Xylene ug/kg 59.051.1 115 70-141
p-Isopropyltoluene ug/kg 56.251.1 110 70-148
sec-Butylbenzene ug/kg 55.051.1 108 70-145
Styrene ug/kg 58.151.1 114 70-138
tert-Butylbenzene ug/kg 54.451.1 106 70-143
Tetrachloroethene ug/kg 55.351.1 108 70-140
Toluene ug/kg 52.351.1 102 70-130
trans-1,2-Dichloroethene ug/kg 62.251.1 122 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 23 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695185LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 59.151.1 116 70-138
Trichloroethene ug/kg 55.751.1 109 70-132
Trichlorofluoromethane ug/kg 70.1 L351.1 137 69-134
Vinyl acetate ug/kg 108102 106 24-161
Vinyl chloride ug/kg 60.751.1 119 55-140
Xylene (Total)ug/kg 176153 115 70-141
1,2-Dichloroethane-d4 (S)%127 70-132
4-Bromofluorobenzene (S)%104 70-130
Dibromofluoromethane (S)%108 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
695219MATRIX SPIKE SAMPLE:
MSSpike
Result
92107622001
1,1-Dichloroethene ug/kg 59.160.4 98 49-180ND
Benzene ug/kg 53.160.4 88 50-166ND
Chlorobenzene ug/kg 38.960.4 64 43-169ND
Toluene ug/kg 46.360.4 77 52-163ND
Trichloroethene ug/kg 47.860.4 79 49-167ND
1,2-Dichloroethane-d4 (S)%104 70-132
4-Bromofluorobenzene (S)%98 70-130
Dibromofluoromethane (S)%104 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107358004
695218SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 24 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107358004
695218SAMPLE DUPLICATE:
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK) ug/kg ND 30ND
Acetone ug/kg 125 C92530162
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene) ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 25 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107358004
695218SAMPLE DUPLICATE:
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%104 14129
4-Bromofluorobenzene (S)%105 12100
Dibromofluoromethane (S)%106 7106
Toluene-d8 (S)%103 10101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 26 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/17555
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92107622002, 92107622003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 696361
Associated Lab Samples:92107622002, 92107622003
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.7 12/07/11 13:37
1,1,1-Trichloroethane ug/kg ND 4.7 12/07/11 13:37
1,1,2,2-Tetrachloroethane ug/kg ND 4.7 12/07/11 13:37
1,1,2-Trichloroethane ug/kg ND 4.7 12/07/11 13:37
1,1-Dichloroethane ug/kg ND 4.7 12/07/11 13:37
1,1-Dichloroethene ug/kg ND 4.7 12/07/11 13:37
1,1-Dichloropropene ug/kg ND 4.7 12/07/11 13:37
1,2,3-Trichlorobenzene ug/kg ND 4.7 12/07/11 13:37
1,2,3-Trichloropropane ug/kg ND 4.7 12/07/11 13:37
1,2,4-Trichlorobenzene ug/kg ND 4.7 12/07/11 13:37
1,2,4-Trimethylbenzene ug/kg ND 4.7 12/07/11 13:37
1,2-Dibromo-3-chloropropane ug/kg ND 4.7 12/07/11 13:37
1,2-Dibromoethane (EDB)ug/kg ND 4.7 12/07/11 13:37
1,2-Dichlorobenzene ug/kg ND 4.7 12/07/11 13:37
1,2-Dichloroethane ug/kg ND 4.7 12/07/11 13:37
1,2-Dichloropropane ug/kg ND 4.7 12/07/11 13:37
1,3,5-Trimethylbenzene ug/kg ND 4.7 12/07/11 13:37
1,3-Dichlorobenzene ug/kg ND 4.7 12/07/11 13:37
1,3-Dichloropropane ug/kg ND 4.7 12/07/11 13:37
1,4-Dichlorobenzene ug/kg ND 4.7 12/07/11 13:37
2,2-Dichloropropane ug/kg ND 4.7 12/07/11 13:37
2-Butanone (MEK)ug/kg ND 94.3 12/07/11 13:37
2-Chlorotoluene ug/kg ND 4.7 12/07/11 13:37
2-Hexanone ug/kg ND 47.2 12/07/11 13:37
4-Chlorotoluene ug/kg ND 4.7 12/07/11 13:37
4-Methyl-2-pentanone (MIBK) ug/kg ND 47.2 12/07/11 13:37
Acetone ug/kg ND 94.3 12/07/11 13:37
Benzene ug/kg ND 4.7 12/07/11 13:37
Bromobenzene ug/kg ND 4.7 12/07/11 13:37
Bromochloromethane ug/kg ND 4.7 12/07/11 13:37
Bromodichloromethane ug/kg ND 4.7 12/07/11 13:37
Bromoform ug/kg ND 4.7 12/07/11 13:37
Bromomethane ug/kg ND 9.4 12/07/11 13:37
Carbon tetrachloride ug/kg ND 4.7 12/07/11 13:37
Chlorobenzene ug/kg ND 4.7 12/07/11 13:37
Chloroethane ug/kg ND 9.4 12/07/11 13:37
Chloroform ug/kg ND 4.7 12/07/11 13:37
Chloromethane ug/kg ND 9.4 12/07/11 13:37
cis-1,2-Dichloroethene ug/kg ND 4.7 12/07/11 13:37
cis-1,3-Dichloropropene ug/kg ND 4.7 12/07/11 13:37
Dibromochloromethane ug/kg ND 4.7 12/07/11 13:37
Dibromomethane ug/kg ND 4.7 12/07/11 13:37
Dichlorodifluoromethane ug/kg ND 9.4 12/07/11 13:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 27 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 696361
Associated Lab Samples:92107622002, 92107622003
Matrix: Solid
Analyzed
Diisopropyl ether ug/kg ND 4.7 12/07/11 13:37
Ethylbenzene ug/kg ND 4.7 12/07/11 13:37
Hexachloro-1,3-butadiene ug/kg ND 4.7 12/07/11 13:37
Isopropylbenzene (Cumene) ug/kg ND 4.7 12/07/11 13:37
m&p-Xylene ug/kg ND 9.4 12/07/11 13:37
Methyl-tert-butyl ether ug/kg ND 4.7 12/07/11 13:37
Methylene Chloride ug/kg ND 18.9 12/07/11 13:37
n-Butylbenzene ug/kg ND 4.7 12/07/11 13:37
n-Propylbenzene ug/kg ND 4.7 12/07/11 13:37
Naphthalene ug/kg ND 4.7 12/07/11 13:37
o-Xylene ug/kg ND 4.7 12/07/11 13:37
p-Isopropyltoluene ug/kg ND 4.7 12/07/11 13:37
sec-Butylbenzene ug/kg ND 4.7 12/07/11 13:37
Styrene ug/kg ND 4.7 12/07/11 13:37
tert-Butylbenzene ug/kg ND 4.7 12/07/11 13:37
Tetrachloroethene ug/kg ND 4.7 12/07/11 13:37
Toluene ug/kg ND 4.7 12/07/11 13:37
trans-1,2-Dichloroethene ug/kg ND 4.7 12/07/11 13:37
trans-1,3-Dichloropropene ug/kg ND 4.7 12/07/11 13:37
Trichloroethene ug/kg ND 4.7 12/07/11 13:37
Trichlorofluoromethane ug/kg ND 4.7 12/07/11 13:37
Vinyl acetate ug/kg ND 47.2 12/07/11 13:37
Vinyl chloride ug/kg ND 9.4 12/07/11 13:37
Xylene (Total)ug/kg ND 9.4 12/07/11 13:37
1,2-Dichloroethane-d4 (S)%98 70-132 12/07/11 13:37
4-Bromofluorobenzene (S)%101 70-130 12/07/11 13:37
Dibromofluoromethane (S)%101 70-130 12/07/11 13:37
Toluene-d8 (S)%98 70-130 12/07/11 13:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
696362LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 49.748.8 102 70-131
1,1,1-Trichloroethane ug/kg 46.048.8 94 70-141
1,1,2,2-Tetrachloroethane ug/kg 51.448.8 105 70-130
1,1,2-Trichloroethane ug/kg 51.748.8 106 70-132
1,1-Dichloroethane ug/kg 47.548.8 97 70-143
1,1-Dichloroethene ug/kg 45.548.8 93 70-137
1,1-Dichloropropene ug/kg 44.948.8 92 70-135
1,2,3-Trichlorobenzene ug/kg 54.548.8 112 69-153
1,2,3-Trichloropropane ug/kg 48.848.8 100 70-130
1,2,4-Trichlorobenzene ug/kg 52.148.8 107 55-171
1,2,4-Trimethylbenzene ug/kg 51.148.8 105 70-149
1,2-Dibromo-3-chloropropane ug/kg 56.848.8 116 68-141
1,2-Dibromoethane (EDB)ug/kg 51.948.8 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 28 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
696362LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 52.648.8 108 70-140
1,2-Dichloroethane ug/kg 48.448.8 99 70-137
1,2-Dichloropropane ug/kg 48.948.8 100 70-133
1,3,5-Trimethylbenzene ug/kg 51.848.8 106 70-143
1,3-Dichlorobenzene ug/kg 51.548.8 105 70-144
1,3-Dichloropropane ug/kg 50.548.8 103 70-132
1,4-Dichlorobenzene ug/kg 51.948.8 106 70-142
2,2-Dichloropropane ug/kg 47.548.8 97 68-152
2-Butanone (MEK)ug/kg 66.6J L097.7 68 70-149
2-Chlorotoluene ug/kg 51.748.8 106 70-141
2-Hexanone ug/kg 10997.7 112 70-149
4-Chlorotoluene ug/kg 54.248.8 111 70-149
4-Methyl-2-pentanone (MIBK) ug/kg 10997.7 112 70-153
Acetone ug/kg 93.5J97.7 96 70-157
Benzene ug/kg 46.148.8 94 70-130
Bromobenzene ug/kg 52.348.8 107 70-141
Bromochloromethane ug/kg 52.148.8 107 70-149
Bromodichloromethane ug/kg 50.048.8 102 70-130
Bromoform ug/kg 52.148.8 107 70-131
Bromomethane ug/kg 51.848.8 106 64-136
Carbon tetrachloride ug/kg 48.148.8 98 70-154
Chlorobenzene ug/kg 49.548.8 101 70-135
Chloroethane ug/kg 58.648.8 120 68-151
Chloroform ug/kg 49.848.8 102 70-130
Chloromethane ug/kg 52.948.8 108 70-132
cis-1,2-Dichloroethene ug/kg 47.348.8 97 70-140
cis-1,3-Dichloropropene ug/kg 50.148.8 103 70-137
Dibromochloromethane ug/kg 49.348.8 101 70-130
Dibromomethane ug/kg 50.148.8 103 70-136
Dichlorodifluoromethane ug/kg 46.548.8 95 36-148
Diisopropyl ether ug/kg 47.948.8 98 70-139
Ethylbenzene ug/kg 49.148.8 101 70-137
Hexachloro-1,3-butadiene ug/kg 48.948.8 100 70-145
Isopropylbenzene (Cumene) ug/kg 50.448.8 103 70-141
m&p-Xylene ug/kg 95.697.7 98 70-140
Methyl-tert-butyl ether ug/kg 50.748.8 104 45-150
Methylene Chloride ug/kg 46.948.8 96 70-133
n-Butylbenzene ug/kg 50.248.8 103 65-155
n-Propylbenzene ug/kg 52.248.8 107 70-148
Naphthalene ug/kg 60.448.8 124 70-148
o-Xylene ug/kg 49.348.8 101 70-141
p-Isopropyltoluene ug/kg 52.948.8 108 70-148
sec-Butylbenzene ug/kg 50.648.8 104 70-145
Styrene ug/kg 49.348.8 101 70-138
tert-Butylbenzene ug/kg 51.448.8 105 70-143
Tetrachloroethene ug/kg 43.748.8 89 70-140
Toluene ug/kg 47.148.8 96 70-130
trans-1,2-Dichloroethene ug/kg 44.148.8 90 70-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 29 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
696362LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 53.048.8 109 70-138
Trichloroethene ug/kg 44.348.8 91 70-132
Trichlorofluoromethane ug/kg 51.348.8 105 69-134
Vinyl acetate ug/kg 71.997.7 74 24-161
Vinyl chloride ug/kg 57.048.8 117 55-140
Xylene (Total)ug/kg 145146 99 70-141
1,2-Dichloroethane-d4 (S)%101 70-132
4-Bromofluorobenzene (S)%94 70-130
Dibromofluoromethane (S)%102 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 30 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/15763
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92107622003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695365
Associated Lab Samples:92107622003
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 332 12/06/11 11:49
1,2-Dichlorobenzene ug/kg ND 332 12/06/11 11:49
1,3-Dichlorobenzene ug/kg ND 332 12/06/11 11:49
1,4-Dichlorobenzene ug/kg ND 332 12/06/11 11:49
1-Methylnaphthalene ug/kg ND 332 12/06/11 11:49
2,4,5-Trichlorophenol ug/kg ND 332 12/06/11 11:49
2,4,6-Trichlorophenol ug/kg ND 332 12/06/11 11:49
2,4-Dichlorophenol ug/kg ND 332 12/06/11 11:49
2,4-Dimethylphenol ug/kg ND 332 12/06/11 11:49
2,4-Dinitrophenol ug/kg ND 1660 12/06/11 11:49
2,4-Dinitrotoluene ug/kg ND 332 12/06/11 11:49
2,6-Dinitrotoluene ug/kg ND 332 12/06/11 11:49
2-Chloronaphthalene ug/kg ND 332 12/06/11 11:49
2-Chlorophenol ug/kg ND 332 12/06/11 11:49
2-Methylnaphthalene ug/kg ND 332 12/06/11 11:49
2-Methylphenol(o-Cresol)ug/kg ND 332 12/06/11 11:49
2-Nitroaniline ug/kg ND 1660 12/06/11 11:49
2-Nitrophenol ug/kg ND 332 12/06/11 11:49
3&4-Methylphenol(m&p Cresol) ug/kg ND 332 12/06/11 11:49
3,3'-Dichlorobenzidine ug/kg ND 1660 12/06/11 11:49
3-Nitroaniline ug/kg ND 1660 12/06/11 11:49
4,6-Dinitro-2-methylphenol ug/kg ND 664 12/06/11 11:49
4-Bromophenylphenyl ether ug/kg ND 332 12/06/11 11:49
4-Chloro-3-methylphenol ug/kg ND 664 12/06/11 11:49
4-Chloroaniline ug/kg ND 1660 12/06/11 11:49
4-Chlorophenylphenyl ether ug/kg ND 332 12/06/11 11:49
4-Nitroaniline ug/kg ND 664 12/06/11 11:49
4-Nitrophenol ug/kg ND 1660 12/06/11 11:49
Acenaphthene ug/kg ND 332 12/06/11 11:49
Acenaphthylene ug/kg ND 332 12/06/11 11:49
Aniline ug/kg ND 332 12/06/11 11:49
Anthracene ug/kg ND 332 12/06/11 11:49
Benzo(a)anthracene ug/kg ND 332 12/06/11 11:49
Benzo(a)pyrene ug/kg ND 332 12/06/11 11:49
Benzo(b)fluoranthene ug/kg ND 332 12/06/11 11:49
Benzo(g,h,i)perylene ug/kg ND 332 12/06/11 11:49
Benzo(k)fluoranthene ug/kg ND 332 12/06/11 11:49
Benzoic Acid ug/kg ND 1660 12/06/11 11:49
Benzyl alcohol ug/kg ND 664 12/06/11 11:49
bis(2-Chloroethoxy)methane ug/kg ND 332 12/06/11 11:49
bis(2-Chloroethyl) ether ug/kg ND 332 12/06/11 11:49
bis(2-Chloroisopropyl) ether ug/kg ND 332 12/06/11 11:49
bis(2-Ethylhexyl)phthalate ug/kg ND 332 12/06/11 11:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 31 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695365
Associated Lab Samples:92107622003
Matrix: Solid
Analyzed
Butylbenzylphthalate ug/kg ND 332 12/06/11 11:49
Chrysene ug/kg ND 332 12/06/11 11:49
Di-n-butylphthalate ug/kg ND 332 12/06/11 11:49
Di-n-octylphthalate ug/kg ND 332 12/06/11 11:49
Dibenz(a,h)anthracene ug/kg ND 332 12/06/11 11:49
Dibenzofuran ug/kg ND 332 12/06/11 11:49
Diethylphthalate ug/kg ND 332 12/06/11 11:49
Dimethylphthalate ug/kg ND 332 12/06/11 11:49
Fluoranthene ug/kg ND 332 12/06/11 11:49
Fluorene ug/kg ND 332 12/06/11 11:49
Hexachloro-1,3-butadiene ug/kg ND 332 12/06/11 11:49
Hexachlorobenzene ug/kg ND 332 12/06/11 11:49
Hexachlorocyclopentadiene ug/kg ND 332 12/06/11 11:49
Hexachloroethane ug/kg ND 332 12/06/11 11:49
Indeno(1,2,3-cd)pyrene ug/kg ND 332 12/06/11 11:49
Isophorone ug/kg ND 332 12/06/11 11:49
N-Nitroso-di-n-propylamine ug/kg ND 332 12/06/11 11:49
N-Nitrosodimethylamine ug/kg ND 332 12/06/11 11:49
N-Nitrosodiphenylamine ug/kg ND 332 12/06/11 11:49
Naphthalene ug/kg ND 332 12/06/11 11:49
Nitrobenzene ug/kg ND 332 12/06/11 11:49
Pentachlorophenol ug/kg ND 1660 12/06/11 11:49
Phenanthrene ug/kg ND 332 12/06/11 11:49
Phenol ug/kg ND 332 12/06/11 11:49
Pyrene ug/kg ND 332 12/06/11 11:49
2,4,6-Tribromophenol (S)%69 27-110 12/06/11 11:49
2-Fluorobiphenyl (S)%68 30-110 12/06/11 11:49
2-Fluorophenol (S)%66 13-110 12/06/11 11:49
Nitrobenzene-d5 (S)%66 23-110 12/06/11 11:49
Phenol-d6 (S)%66 22-110 12/06/11 11:49
Terphenyl-d14 (S)%76 28-110 12/06/11 11:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695366LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12101670 73 39-101
1,2-Dichlorobenzene ug/kg 11401670 68 36-110
1,3-Dichlorobenzene ug/kg 11301670 68 35-110
1,4-Dichlorobenzene ug/kg 11201670 67 35-110
1-Methylnaphthalene ug/kg 10901670 66 45-105
2,4,5-Trichlorophenol ug/kg 11001670 66 48-109
2,4,6-Trichlorophenol ug/kg 12601670 75 45-111
2,4-Dichlorophenol ug/kg 11801670 71 51-116
2,4-Dimethylphenol ug/kg 11401670 68 42-103
2,4-Dinitrophenol ug/kg 48708330 58 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 32 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695366LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 12101670 72 46-114
2,6-Dinitrotoluene ug/kg 11201670 67 48-112
2-Chloronaphthalene ug/kg 11601670 70 44-105
2-Chlorophenol ug/kg 10701670 64 36-110
2-Methylnaphthalene ug/kg 10901670 65 39-112
2-Methylphenol(o-Cresol)ug/kg 9481670 57 39-101
2-Nitroaniline ug/kg 20803330 62 44-111
2-Nitrophenol ug/kg 10901670 65 41-100
3&4-Methylphenol(m&p Cresol) ug/kg 9841670 59 43-103
3,3'-Dichlorobenzidine ug/kg 19403330 58 10-150
3-Nitroaniline ug/kg 21703330 65 35-110
4,6-Dinitro-2-methylphenol ug/kg 23103330 69 38-118
4-Bromophenylphenyl ether ug/kg 12601670 76 47-115
4-Chloro-3-methylphenol ug/kg 22303330 67 43-127
4-Chloroaniline ug/kg 22103330 66 34-109
4-Chlorophenylphenyl ether ug/kg 11901670 72 44-115
4-Nitroaniline ug/kg 22903330 69 37-111
4-Nitrophenol ug/kg 58208330 70 21-152
Acenaphthene ug/kg 10701670 64 38-117
Acenaphthylene ug/kg 11401670 69 46-107
Aniline ug/kg 10101670 60 29-110
Anthracene ug/kg 11301670 68 50-110
Benzo(a)anthracene ug/kg 11701670 70 47-116
Benzo(a)pyrene ug/kg 11201670 67 47-106
Benzo(b)fluoranthene ug/kg 11501670 69 47-109
Benzo(g,h,i)perylene ug/kg 11401670 68 39-115
Benzo(k)fluoranthene ug/kg 12101670 73 45-117
Benzoic Acid ug/kg 30808330 37 16-110
Benzyl alcohol ug/kg 21103330 63 38-105
bis(2-Chloroethoxy)methane ug/kg 11501670 69 39-110
bis(2-Chloroethyl) ether ug/kg 10901670 66 19-119
bis(2-Chloroisopropyl) ether ug/kg 8291670 50 21-110
bis(2-Ethylhexyl)phthalate ug/kg 10601670 64 35-116
Butylbenzylphthalate ug/kg 10201670 61 38-110
Chrysene ug/kg 11301670 68 49-110
Di-n-butylphthalate ug/kg 11901670 71 43-109
Di-n-octylphthalate ug/kg 9521670 57 37-109
Dibenz(a,h)anthracene ug/kg 11701670 70 43-116
Dibenzofuran ug/kg 11801670 71 45-106
Diethylphthalate ug/kg 11801670 71 41-114
Dimethylphthalate ug/kg 11401670 69 43-110
Fluoranthene ug/kg 11901670 72 50-114
Fluorene ug/kg 11501670 69 46-114
Hexachloro-1,3-butadiene ug/kg 12901670 77 28-111
Hexachlorobenzene ug/kg 12201670 73 46-120
Hexachlorocyclopentadiene ug/kg 12901670 78 18-119
Hexachloroethane ug/kg 10301670 62 33-110
Indeno(1,2,3-cd)pyrene ug/kg 11701670 70 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 33 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695366LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 12201670 73 44-109
N-Nitroso-di-n-propylamine ug/kg 11101670 67 43-104
N-Nitrosodimethylamine ug/kg 10901670 66 29-110
N-Nitrosodiphenylamine ug/kg 12401670 74 48-113
Naphthalene ug/kg 10901670 65 41-110
Nitrobenzene ug/kg 11901670 72 38-110
Pentachlorophenol ug/kg 27603330 83 32-128
Phenanthrene ug/kg 11101670 66 50-110
Phenol ug/kg 11801670 71 28-106
Pyrene ug/kg 10401670 63 45-114
2,4,6-Tribromophenol (S)%74 27-110
2-Fluorobiphenyl (S)%66 30-110
2-Fluorophenol (S)%64 13-110
Nitrobenzene-d5 (S)%68 23-110
Phenol-d6 (S)%64 22-110
Terphenyl-d14 (S)%70 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
695367MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107622003
695368
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1910 35 18-11931 10 301910ND662 598
1,2-Dichlorobenzene ug/kg M0,M119103050-11028 7 301910ND566 527
1,3-Dichlorobenzene ug/kg 1910 29 27-11027 6 301910ND554 520
1,4-Dichlorobenzene ug/kg 1910 28 28-11028 1 301910ND536 530
1-Methylnaphthalene ug/kg 1910 35 24-11631 10 301910ND662 596
2,4,5-Trichlorophenol ug/kg 1910 37 28-11034 7 301910ND700 652
2,4,6-Trichlorophenol ug/kg 1910 43 17-11740 8 301910ND824 762
2,4-Dichlorophenol ug/kg 1910 39 21-12832 20 301910ND749 612
2,4-Dimethylphenol ug/kg 1910 30 10-12026 17 301910ND579 491
2,4-Dinitrophenol ug/kg M0,M195401210-1079 309540ND1170J 821J
2,4-Dinitrotoluene ug/kg 1910 41 36-10937 10 301910ND782 710
2,6-Dinitrotoluene ug/kg 1910 37 32-11035 7 301910ND712 661
2-Chloronaphthalene ug/kg 1910 36 30-10734 7 301910ND692 642
2-Chlorophenol ug/kg 1910 28 14-10625 12 301910ND543 482
2-Methylnaphthalene ug/kg 1910 34 10-13530 13 301910ND654 572
2-Methylphenol(o-Cresol) ug/kg 1910 26 10-12422 18 301910ND494 412
2-Nitroaniline ug/kg 3820 36 26-11632 303820ND1360J 1240J
2-Nitrophenol ug/kg 1910 31 28-10328 12 301910ND595 527
3&4-Methylphenol(m&pCresol)ug/kg 1910 29 10-10925 13 301910ND550 481
3,3'-Dichlorobenzidine ug/kg 3820 24 10-15029 303820ND919J 1110J
3-Nitroaniline ug/kg 3820 34 22-11033 303820ND1310J 1250J
4,6-Dinitro-2-methylphenol ug/kg 3820 27 13-12123 16 303820ND1050 891
4-Bromophenylphenyl ether ug/kg 1910 43 31-10941 5 301910ND827 784
4-Chloro-3-methylphenol ug/kg 3820 37 13-12832 16 303820ND1430 1220
4-Chloroaniline ug/kg 3820 28 18-10228 303820ND1080J 1050J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 34 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
695367MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107622003
695368
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/kg 1910 39 29-11237 7 301910ND747 699
4-Nitroaniline ug/kg 3820 34 16-11132 8 303820ND1300 1200
4-Nitrophenol ug/kg 9540 37 14-13535 6 309540ND3520 3320
Acenaphthene ug/kg 1910 35 26-11433 5 301910ND663 630
Acenaphthylene ug/kg 1910 37 32-10835 5 301910ND703 665
Aniline ug/kg 1910 38 10-10736 7 301910ND731 681
Anthracene ug/kg 1910 39 32-11138 3 301910ND740 717
Benzo(a)anthracene ug/kg 1910 39 25-11737 4 301910ND744 714
Benzo(a)pyrene ug/kg 1910 36 25-10634 5 301910ND679 643
Benzo(b)fluoranthene ug/kg 1910 36 24-11034 7 301910ND695 646
Benzo(g,h,i)perylene ug/kg 1910 38 19-11235 6 301910ND720 676
Benzo(k)fluoranthene ug/kg 1910 38 24-11437 2 301910ND721 703
Benzoic Acid ug/kg M0,M19540210-1102 309540ND228J 154J
Benzyl alcohol ug/kg 3820 29 24-10626 12 303820ND1110 987
bis(2-Chloroethoxy)methane ug/kg 1910 34 13-11931 10 301910ND645 584
bis(2-Chloroethyl) ether ug/kg 1910 56 10-13452 7 301910ND1070 995
bis(2-Chloroisopropyl) ether ug/kg 1910 24 10-11322 10 301910ND467 422
bis(2-Ethylhexyl)phthalate ug/kg M0,M1,R1191014810-12565 40 30191019004730 3140
Butylbenzylphthalate ug/kg 1910 37 18-11048 22 301910ND813 1010
Chrysene ug/kg 1910 37 30-11037 2 301910ND713 696
Di-n-butylphthalate ug/kg 1910 40 19-11237 6 301910ND1020 967
Di-n-octylphthalate ug/kg 1910 36 17-10533 7 301910ND678 635
Dibenz(a,h)anthracene ug/kg 1910 38 23-11136 7 301910ND730 680
Dibenzofuran ug/kg 1910 38 35-10336 6 301910ND731 686
Diethylphthalate ug/kg 1910 41 27-11339 4 301910ND778 750
Dimethylphthalate ug/kg 1910 39 26-11136 8 301910ND743 688
Fluoranthene ug/kg 1910 38 33-10937 3 301910ND724 701
Fluorene ug/kg 1910 38 32-11336 5 301910ND723 686
Hexachloro-1,3-butadiene ug/kg 1910 38 16-11636 6 301910ND721 680
Hexachlorobenzene ug/kg 1910 41 27-12039 4 301910ND776 748
Hexachlorocyclopentadiene ug/kg 1910 33 10-10827 20 301910ND632 518
Hexachloroethane ug/kg 1910 28 10-11726 6 301910ND525 495
Indeno(1,2,3-cd)pyrene ug/kg 1910 37 10-12236 5 301910ND713 678
Isophorone ug/kg 1910 40 28-11436 12 301910ND771 687
N-Nitroso-di-n-propylamine ug/kg 1910 36 27-11331 17 301910ND694 582
N-Nitrosodimethylamine ug/kg 1910 24 10-10923 7 301910ND467 434
N-Nitrosodiphenylamine ug/kg 1910 41 10-12840 3 301910ND780 759
Naphthalene ug/kg 1910 32 25-11030 9 301910ND620 569
Nitrobenzene ug/kg 1910 33 18-11431 6 301910ND631 597
Pentachlorophenol ug/kg 3820 51 10-12247 303820ND1950 1800J
Phenanthrene ug/kg 1910 38 30-11436 5 301910ND727 691
Phenol ug/kg 1910 31 11-10226 21 301910ND600 487
Pyrene ug/kg 1910 36 25-11634 4 301910ND686 658
2,4,6-Tribromophenol (S) %43 27-11041
2-Fluorobiphenyl (S)%33 30-11031
2-Fluorophenol (S)%25 13-11022
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 35 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
695367MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107622003
695368
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrobenzene-d5 (S)%31 23-11029
Phenol-d6 (S)%28 22-11023
Terphenyl-d14 (S)%39 28-11037
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 36 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/15791
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92107622001, 92107622002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 696145
Associated Lab Samples:92107622001, 92107622002
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 12/08/11 16:10
1,2-Dichlorobenzene ug/kg ND 330 12/08/11 16:10
1,3-Dichlorobenzene ug/kg ND 330 12/08/11 16:10
1,4-Dichlorobenzene ug/kg ND 330 12/08/11 16:10
1-Methylnaphthalene ug/kg ND 330 12/08/11 16:10
2,4,5-Trichlorophenol ug/kg ND 330 12/08/11 16:10
2,4,6-Trichlorophenol ug/kg ND 330 12/08/11 16:10
2,4-Dichlorophenol ug/kg ND 330 12/08/11 16:10
2,4-Dimethylphenol ug/kg ND 330 12/08/11 16:10
2,4-Dinitrophenol ug/kg ND 1650 12/08/11 16:10
2,4-Dinitrotoluene ug/kg ND 330 12/08/11 16:10
2,6-Dinitrotoluene ug/kg ND 330 12/08/11 16:10
2-Chloronaphthalene ug/kg ND 330 12/08/11 16:10
2-Chlorophenol ug/kg ND 330 12/08/11 16:10
2-Methylnaphthalene ug/kg ND 330 12/08/11 16:10
2-Methylphenol(o-Cresol)ug/kg ND 330 12/08/11 16:10
2-Nitroaniline ug/kg ND 1650 12/08/11 16:10
2-Nitrophenol ug/kg ND 330 12/08/11 16:10
3&4-Methylphenol(m&p Cresol) ug/kg ND 330 12/08/11 16:10
3,3'-Dichlorobenzidine ug/kg ND 1650 12/08/11 16:10
3-Nitroaniline ug/kg ND 1650 12/08/11 16:10
4,6-Dinitro-2-methylphenol ug/kg ND 660 12/08/11 16:10
4-Bromophenylphenyl ether ug/kg ND 330 12/08/11 16:10
4-Chloro-3-methylphenol ug/kg ND 660 12/08/11 16:10
4-Chloroaniline ug/kg ND 1650 12/08/11 16:10
4-Chlorophenylphenyl ether ug/kg ND 330 12/08/11 16:10
4-Nitroaniline ug/kg ND 660 12/08/11 16:10
4-Nitrophenol ug/kg ND 1650 12/08/11 16:10
Acenaphthene ug/kg ND 330 12/08/11 16:10
Acenaphthylene ug/kg ND 330 12/08/11 16:10
Aniline ug/kg ND 330 12/08/11 16:10
Anthracene ug/kg ND 330 12/08/11 16:10
Benzo(a)anthracene ug/kg ND 330 12/08/11 16:10
Benzo(a)pyrene ug/kg ND 330 12/08/11 16:10
Benzo(b)fluoranthene ug/kg ND 330 12/08/11 16:10
Benzo(g,h,i)perylene ug/kg ND 330 12/08/11 16:10
Benzo(k)fluoranthene ug/kg ND 330 12/08/11 16:10
Benzoic Acid ug/kg ND 1650 12/08/11 16:10
Benzyl alcohol ug/kg ND 660 12/08/11 16:10
bis(2-Chloroethoxy)methane ug/kg ND 330 12/08/11 16:10
bis(2-Chloroethyl) ether ug/kg ND 330 12/08/11 16:10
bis(2-Chloroisopropyl) ether ug/kg ND 330 12/08/11 16:10
bis(2-Ethylhexyl)phthalate ug/kg ND 330 12/08/11 16:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 37 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 696145
Associated Lab Samples:92107622001, 92107622002
Matrix: Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 12/08/11 16:10
Chrysene ug/kg ND 330 12/08/11 16:10
Di-n-butylphthalate ug/kg ND 330 12/08/11 16:10
Di-n-octylphthalate ug/kg ND 330 12/08/11 16:10
Dibenz(a,h)anthracene ug/kg ND 330 12/08/11 16:10
Dibenzofuran ug/kg ND 330 12/08/11 16:10
Diethylphthalate ug/kg ND 330 12/08/11 16:10
Dimethylphthalate ug/kg ND 330 12/08/11 16:10
Fluoranthene ug/kg ND 330 12/08/11 16:10
Fluorene ug/kg ND 330 12/08/11 16:10
Hexachloro-1,3-butadiene ug/kg ND 330 12/08/11 16:10
Hexachlorobenzene ug/kg ND 330 12/08/11 16:10
Hexachlorocyclopentadiene ug/kg ND 330 12/08/11 16:10
Hexachloroethane ug/kg ND 330 12/08/11 16:10
Indeno(1,2,3-cd)pyrene ug/kg ND 330 12/08/11 16:10
Isophorone ug/kg ND 330 12/08/11 16:10
N-Nitroso-di-n-propylamine ug/kg ND 330 12/08/11 16:10
N-Nitrosodimethylamine ug/kg ND 330 12/08/11 16:10
N-Nitrosodiphenylamine ug/kg ND 330 12/08/11 16:10
Naphthalene ug/kg ND 330 12/08/11 16:10
Nitrobenzene ug/kg ND 330 12/08/11 16:10
Pentachlorophenol ug/kg ND 1650 12/08/11 16:10
Phenanthrene ug/kg ND 330 12/08/11 16:10
Phenol ug/kg ND 330 12/08/11 16:10
Pyrene ug/kg ND 330 12/08/11 16:10
2,4,6-Tribromophenol (S)%57 27-110 12/08/11 16:10
2-Fluorobiphenyl (S)%54 30-110 12/08/11 16:10
2-Fluorophenol (S)%62 13-110 12/08/11 16:10
Nitrobenzene-d5 (S)%62 23-110 12/08/11 16:10
Phenol-d6 (S)%54 22-110 12/08/11 16:10
Terphenyl-d14 (S)%68 28-110 12/08/11 16:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
696146LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11601670 69 39-101
1,2-Dichlorobenzene ug/kg 10901670 65 36-110
1,3-Dichlorobenzene ug/kg 11201670 67 35-110
1,4-Dichlorobenzene ug/kg 11401670 69 35-110
1-Methylnaphthalene ug/kg 9431670 57 45-105
2,4,5-Trichlorophenol ug/kg 9961670 60 48-109
2,4,6-Trichlorophenol ug/kg 11701670 70 45-111
2,4-Dichlorophenol ug/kg 10101670 61 51-116
2,4-Dimethylphenol ug/kg 10101670 61 42-103
2,4-Dinitrophenol ug/kg 35208330 42 28-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 38 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
696146LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 11801670 71 46-114
2,6-Dinitrotoluene ug/kg 11601670 70 48-112
2-Chloronaphthalene ug/kg 12201670 73 44-105
2-Chlorophenol ug/kg 10601670 64 36-110
2-Methylnaphthalene ug/kg 9551670 57 39-112
2-Methylphenol(o-Cresol)ug/kg 8141670 49 39-101
2-Nitroaniline ug/kg 24803330 74 44-111
2-Nitrophenol ug/kg 11001670 66 41-100
3&4-Methylphenol(m&p Cresol) ug/kg 7551670 45 43-103
3,3'-Dichlorobenzidine ug/kg 21203330 64 10-150
3-Nitroaniline ug/kg 22703330 68 35-110
4,6-Dinitro-2-methylphenol ug/kg 17403330 52 38-118
4-Bromophenylphenyl ether ug/kg 12001670 72 47-115
4-Chloro-3-methylphenol ug/kg 17203330 52 43-127
4-Chloroaniline ug/kg 18803330 56 34-109
4-Chlorophenylphenyl ether ug/kg 11201670 67 44-115
4-Nitroaniline ug/kg 20403330 61 37-111
4-Nitrophenol ug/kg 46108330 55 21-152
Acenaphthene ug/kg 11501670 69 38-117
Acenaphthylene ug/kg 11101670 67 46-107
Aniline ug/kg 9031670 54 29-110
Anthracene ug/kg 11901670 71 50-110
Benzo(a)anthracene ug/kg 11701670 70 47-116
Benzo(a)pyrene ug/kg 11901670 71 47-106
Benzo(b)fluoranthene ug/kg 11901670 71 47-109
Benzo(g,h,i)perylene ug/kg 11201670 67 39-115
Benzo(k)fluoranthene ug/kg 12901670 77 45-117
Benzoic Acid ug/kg 24308330 29 16-110
Benzyl alcohol ug/kg 16803330 50 38-105
bis(2-Chloroethoxy)methane ug/kg 10401670 63 39-110
bis(2-Chloroethyl) ether ug/kg 11201670 67 19-119
bis(2-Chloroisopropyl) ether ug/kg 10301670 62 21-110
bis(2-Ethylhexyl)phthalate ug/kg 13801670 83 35-116
Butylbenzylphthalate ug/kg 13901670 83 38-110
Chrysene ug/kg 12401670 75 49-110
Di-n-butylphthalate ug/kg 12501670 75 43-109
Di-n-octylphthalate ug/kg 11801670 71 37-109
Dibenz(a,h)anthracene ug/kg 10701670 64 43-116
Dibenzofuran ug/kg 11501670 69 45-106
Diethylphthalate ug/kg 11801670 71 41-114
Dimethylphthalate ug/kg 11701670 70 43-110
Fluoranthene ug/kg 10801670 65 50-114
Fluorene ug/kg 11201670 67 46-114
Hexachloro-1,3-butadiene ug/kg 12101670 73 28-111
Hexachlorobenzene ug/kg 12101670 72 46-120
Hexachlorocyclopentadiene ug/kg 14401670 86 18-119
Hexachloroethane ug/kg 11101670 67 33-110
Indeno(1,2,3-cd)pyrene ug/kg 11001670 66 42-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 39 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
696146LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 10401670 62 44-109
N-Nitroso-di-n-propylamine ug/kg 7581670 45 43-104
N-Nitrosodimethylamine ug/kg 10801670 65 29-110
N-Nitrosodiphenylamine ug/kg 12901670 77 48-113
Naphthalene ug/kg 11101670 66 41-110
Nitrobenzene ug/kg 11901670 71 38-110
Pentachlorophenol ug/kg 18803330 56 32-128
Phenanthrene ug/kg 11601670 70 50-110
Phenol ug/kg 9931670 60 28-106
Pyrene ug/kg 12701670 76 45-114
2,4,6-Tribromophenol (S)%66 27-110
2-Fluorobiphenyl (S)%69 30-110
2-Fluorophenol (S)%66 13-110
Nitrobenzene-d5 (S)%66 23-110
Phenol-d6 (S)%57 22-110
Terphenyl-d14 (S)%77 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
696147MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107622002
696148
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1890 54 18-11960 11 301880ND1020 1130
1,2-Dichlorobenzene ug/kg 1890 53 50-11056 5 301880ND1000 1060
1,3-Dichlorobenzene ug/kg 1890 54 27-11057 6 301880ND1010 1080
1,4-Dichlorobenzene ug/kg 1890 53 28-11057 7 301880ND1000 1080
1-Methylnaphthalene ug/kg 1890 45 24-11646 1 301880ND857 868
2,4,5-Trichlorophenol ug/kg M0,M11890028-1102 301880NDND ND
2,4,6-Trichlorophenol ug/kg M0,M11890017-1170 301880NDND ND
2,4-Dichlorophenol ug/kg M0,M11890521-1285 301880ND90J 92.7J
2,4-Dimethylphenol ug/kg 1890 49 10-12051 4 301880ND919 958
2,4-Dinitrophenol ug/kg M0,M19470010-1070 309420NDND ND
2,4-Dinitrotoluene ug/kg R118907336-109101 32 301880ND1380 1900
2,6-Dinitrotoluene ug/kg 1890 63 32-11081 24 301880ND1200 1530
2-Chloronaphthalene ug/kg 1890 57 30-10760 4 301880ND1080 1120
2-Chlorophenol ug/kg M0,M11890714-1067 301880ND125J 131J
2-Methylnaphthalene ug/kg 1890 47 10-13548 1 301880ND888 899
2-Methylphenol(o-Cresol) ug/kg 1890 33 10-12434 4 301880ND622 647
2-Nitroaniline ug/kg 3790 64 26-11676 16 303770ND2420 2840
2-Nitrophenol ug/kg M0,M11890328-1034 301880NDND ND
3&4-Methylphenol(m&pCresol)ug/kg 1890 27 10-10929 7 301880ND506 545
3,3'-Dichlorobenzidine ug/kg 3790 69 10-15067 3 303770ND2690 2620
3-Nitroaniline ug/kg 3790 62 22-11079 23 303770ND2350 2960
4,6-Dinitro-2-methylphenol ug/kg M0,M13790013-1210 303770NDND ND
4-Bromophenylphenyl ether ug/kg 1890 56 31-10955 2 301880ND1050 1030
4-Chloro-3-methylphenol ug/kg 3790 37 13-12841 12 303770ND1390 1560
4-Chloroaniline ug/kg 3790 41 18-10240 303770ND1570J 1490J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 40 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
696147MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107622002
696148
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Chlorophenylphenyl ether ug/kg 1890 55 29-11266 16 301880ND1050 1240
4-Nitroaniline ug/kg 3790 83 16-111110 28 303770ND3130 4150
4-Nitrophenol ug/kg M0,M19470014-1350 309420NDND ND
Acenaphthene ug/kg 1890 54 26-11459 9 301880ND1020 1110
Acenaphthylene ug/kg 1890 54 32-10857 5 301880ND1030 1080
Aniline ug/kg 1890 39 10-10735 11 301880ND740 665
Anthracene ug/kg 1890 70 32-11172 2 301880ND1320 1350
Benzo(a)anthracene ug/kg 1890 69 25-11773 4 301880ND1320 1370
Benzo(a)pyrene ug/kg 1890 68 25-10670 2 301880ND1290 1320
Benzo(b)fluoranthene ug/kg 1890 63 24-11066 3 301880ND1250 1290
Benzo(g,h,i)perylene ug/kg 1890 63 19-11265 3 301880ND1250 1280
Benzo(k)fluoranthene ug/kg 1890 67 24-11469 2 301880ND1330 1360
Benzoic Acid ug/kg M0,M19470010-1100 309420NDND ND
Benzyl alcohol ug/kg 3790 40 24-10641 2 303770ND1510 1550
bis(2-Chloroethoxy)methane ug/kg 1890 50 13-11953 7 301880ND940 1010
bis(2-Chloroethyl) ether ug/kg 1890 51 10-13455 7 301880ND968 1040
bis(2-Chloroisopropyl) ether ug/kg 1890 49 10-11351 3 301880ND936 967
bis(2-Ethylhexyl)phthalate ug/kg 1890 80 10-12580 2 301880ND1520 1500
Butylbenzylphthalate ug/kg 1890 76 18-11077 0 301880ND1440 1450
Chrysene ug/kg 1890 70 30-11073 3 301880ND1330 1370
Di-n-butylphthalate ug/kg 1890 88 19-11285 3 301880ND1660 1610
Di-n-octylphthalate ug/kg 1890 70 17-10575 6 301880ND1330 1420
Dibenz(a,h)anthracene ug/kg 1890 63 23-11164 2 301880ND1230 1260
Dibenzofuran ug/kg 1890 56 35-10363 11 301880ND1060 1180
Diethylphthalate ug/kg 1890 68 27-11389 26 301880ND1300 1680
Dimethylphthalate ug/kg 1890 62 26-11174 17 301880ND1170 1390
Fluoranthene ug/kg 1890 86 33-10983 4 301880ND1640 1570
Fluorene ug/kg 1890 56 32-11368 18 301880ND1070 1280
Hexachloro-1,3-butadiene ug/kg 1890 53 16-11659 11 301880ND999 1110
Hexachlorobenzene ug/kg 1890 63 27-12062 2 301880ND1190 1170
Hexachlorocyclopentadiene ug/kg 1890 51 10-10854 5 301880ND960 1010
Hexachloroethane ug/kg 1890 51 10-11754 6 301880ND957 1020
Indeno(1,2,3-cd)pyrene ug/kg 1890 63 10-12264 1 301880ND1240 1260
Isophorone ug/kg 1890 49 28-11452 5 301880ND937 988
N-Nitroso-di-n-propylamine ug/kg 1890 36 27-11337 3 301880ND683 702
N-Nitrosodimethylamine ug/kg 1890 55 10-10957 4 301880ND1040 1080
N-Nitrosodiphenylamine ug/kg 1890 64 10-12862 4 301880ND1210 1160
Naphthalene ug/kg 1890 53 25-11056 5 301880ND996 1050
Nitrobenzene ug/kg 1890 58 18-11462 6 301880ND1090 1160
Pentachlorophenol ug/kg M0,M13790010-1220 303770NDND ND
Phenanthrene ug/kg 1890 66 30-11468 2 301880ND1260 1280
Phenol ug/kg 1890 19 11-10220 301880ND361J 372J
Pyrene ug/kg 1890 66 25-11670 4 301880ND1260 1310
2,4,6-Tribromophenol (S) %1g127-1102
2-Fluorobiphenyl (S)%49 30-11050
2-Fluorophenol (S)%1g213-1103
Nitrobenzene-d5 (S)%54 23-11058
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 41 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
696147MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107622002
696148
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol-d6 (S)%1g1522-11016
Terphenyl-d14 (S)%66 28-11067
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 42 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4362
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92107622001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107263001
694955SAMPLE DUPLICATE:
Percent Moisture %13.2 15 2515.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107622001
694956SAMPLE DUPLICATE:
Percent Moisture %28.9 0 2529.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 43 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4364
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92107622002, 92107622003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107622002
695292SAMPLE DUPLICATE:
Percent Moisture %16.7 R1262512.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107569001
695293SAMPLE DUPLICATE:
Percent Moisture %19.1 R1352527.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 44 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/4369
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92107622004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107622004
696153SAMPLE DUPLICATE:
Percent Moisture %22.2 6 2521.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107720019
696154SAMPLE DUPLICATE:
Percent Moisture %22.5 1 2522.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 45 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/11119
EPA 7196
EPA 7196
7196 Chromium, Hexavalent
Associated Lab Samples: 92107622001, 92107622002, 92107622003, 92107622004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695239
Associated Lab Samples:92107622001, 92107622002, 92107622003, 92107622004
Matrix: Solid
Analyzed
Chromium, Hexavalent mg/kg ND 5.0 N212/05/11 14:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695240LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 51.8 N250104 90-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
695242MATRIX SPIKE SAMPLE:
MSSpike
Result
92107622001
Chromium, Hexavalent mg/kg ND M1,N26.1 -2 75-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107622001
695241SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg .11J N220ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 46 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92107622
Sun Chemical Facility PPA-038
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from samplere-extraction and re-analysis).1g
Common Laboratory Contaminant.C9
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/09/2011 05:04 PM Page 47 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
December 12, 2011
LIMS USE: FR - STEVE HART
LIMS OBJECT ID: 92107636
92107636
Project:
Pace Project No.:
RE:
Mr. Steve HartHart & Hickman2923 South Tryon StreetCharlotte, NC 28203
Sun Chemical Facility PPA-038
Dear Mr. Hart:
Enclosed are the analytical results for sample(s) received by the laboratory on December 02, 2011.
The results relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail] Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357Virginia/VELAP Certification #: 460144
Asheville Certification IDs2225 Riverside Dr., Asheville, NC 28804Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030North Carolina Drinking Water Certification #: 37712North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001Virginia Certification #: 00072West Virginia Certification #: 356Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Lab ID Sample ID Matrix Date Collected Date Received
92107636001 HH-4 Water 12/02/11 09:10 12/02/11 16:30
92107636002 HH-3 Water 12/02/11 09:40 12/02/11 16:30
92107636003 HH-1 Water 12/02/11 10:24 12/02/11 16:30
92107636004 G-1 Water 12/02/11 11:34 12/02/11 16:30
92107636005 HH-2 Water 12/02/11 11:04 12/02/11 16:30
92107636006 G-8 Water 12/02/11 12:20 12/02/11 16:30
92107636007 G-11 Water 12/02/11 12:44 12/02/11 16:30
92107636008 G-15 Water 12/02/11 13:14 12/02/11 16:30
92107636009 G-10 Water 12/02/11 13:46 12/02/11 16:30
92107636010 G-12 Water 12/02/11 14:26 12/02/11 16:30
92107636011 G-9 Water 12/02/11 15:06 12/02/11 16:30
92107636012 G-3 Water 12/02/11 15:46 12/02/11 16:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92107636001 HH-4 EPA 6010 13 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 74 PASI-CBPJ
EPA 8260 64 PASI-CMCK
92107636002 HH-3 EPA 6010 13 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 74 PASI-CBPJ
EPA 8260 64 PASI-CMCK
92107636003 HH-1 EPA 6010 13 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 74 PASI-CBPJ
EPA 8260 64 PASI-CMCK
92107636004 G-1 EPA 6010 13 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 74 PASI-CBPJ
EPA 8260 64 PASI-CMCK
92107636005 HH-2 EPA 8260 64 PASI-CMCK
92107636006 G-8 EPA 8260 64 PASI-CMCK
92107636007 G-11 EPA 8260 64 PASI-CMCK
92107636008 G-15 EPA 8260 64 PASI-CMCK
92107636009 G-10 EPA 8260 64 PASI-CMCK
92107636010 G-12 EPA 8260 64 PASI-CMCK
92107636011 G-9 EPA 8260 64 PASI-CMCK
92107636012 G-3 EPA 8260 64 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-4 Lab ID: 92107636001 Collected: 12/02/11 09:10 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 1 12/08/11 16:00 7440-36-012/07/11 11:505.0
Arsenic ND ug/L 1 12/08/11 16:00 7440-38-212/07/11 11:505.0
Beryllium ND ug/L 1 12/08/11 16:00 7440-41-712/07/11 11:501.0
Cadmium ND ug/L 1 12/08/11 16:00 7440-43-912/07/11 11:501.0
Chromium ND ug/L 1 12/08/11 16:00 7440-47-312/07/11 11:505.0
Copper ND ug/L 1 12/08/11 16:00 7440-50-812/07/11 11:505.0
Lead ND ug/L 1 12/08/11 16:00 7439-92-112/07/11 11:505.0
Manganese 350 ug/L 1 12/08/11 16:00 7439-96-512/07/11 11:505.0
Nickel ND ug/L 1 12/08/11 16:00 7440-02-012/07/11 11:505.0
Selenium ND ug/L 1 12/08/11 16:00 7782-49-212/07/11 11:5010.0
Silver ND ug/L 1 12/08/11 16:00 7440-22-412/07/11 11:505.0
Thallium ND ug/L 1 12/08/11 16:00 7440-28-012/07/11 11:5010.0
Zinc ND ug/L 1 12/08/11 16:00 7440-66-612/07/11 11:5010.0
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 1 12/08/11 11:55 7439-97-6 M112/07/11 16:450.20
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 12/08/11 18:28 83-32-912/06/11 08:3010.0
Acenaphthylene ND ug/L 1 12/08/11 18:28 208-96-812/06/11 08:3010.0
Aniline ND ug/L 1 12/08/11 18:28 62-53-312/06/11 08:3010.0
Anthracene ND ug/L 1 12/08/11 18:28 120-12-712/06/11 08:3010.0
Benzo(a)anthracene ND ug/L 1 12/08/11 18:28 56-55-312/06/11 08:3010.0
Benzo(a)pyrene ND ug/L 1 12/08/11 18:28 50-32-812/06/11 08:3010.0
Benzo(b)fluoranthene ND ug/L 1 12/08/11 18:28 205-99-212/06/11 08:3010.0
Benzo(g,h,i)perylene ND ug/L 1 12/08/11 18:28 191-24-212/06/11 08:3010.0
Benzo(k)fluoranthene ND ug/L 1 12/08/11 18:28 207-08-912/06/11 08:3010.0
Benzoic Acid ND ug/L 1 12/08/11 18:28 65-85-012/06/11 08:3050.0
Benzyl alcohol ND ug/L 1 12/08/11 18:28 100-51-612/06/11 08:3020.0
4-Bromophenylphenyl ether ND ug/L 1 12/08/11 18:28 101-55-312/06/11 08:3010.0
Butylbenzylphthalate ND ug/L 1 12/08/11 18:28 85-68-712/06/11 08:3010.0
4-Chloro-3-methylphenol ND ug/L 1 12/08/11 18:28 59-50-712/06/11 08:3020.0
4-Chloroaniline ND ug/L 1 12/08/11 18:28 106-47-812/06/11 08:3020.0
bis(2-Chloroethoxy)methane ND ug/L 1 12/08/11 18:28 111-91-112/06/11 08:3010.0
bis(2-Chloroethyl) ether ND ug/L 1 12/08/11 18:28 111-44-412/06/11 08:3010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 12/08/11 18:28 108-60-112/06/11 08:3010.0
2-Chloronaphthalene ND ug/L 1 12/08/11 18:28 91-58-712/06/11 08:3010.0
2-Chlorophenol ND ug/L 1 12/08/11 18:28 95-57-812/06/11 08:3010.0
4-Chlorophenylphenyl ether ND ug/L 1 12/08/11 18:28 7005-72-312/06/11 08:3010.0
Chrysene ND ug/L 1 12/08/11 18:28 218-01-912/06/11 08:3010.0
Dibenz(a,h)anthracene ND ug/L 1 12/08/11 18:28 53-70-312/06/11 08:3010.0
Dibenzofuran ND ug/L 1 12/08/11 18:28 132-64-912/06/11 08:3010.0
1,2-Dichlorobenzene ND ug/L 1 12/08/11 18:28 95-50-112/06/11 08:3010.0
1,3-Dichlorobenzene ND ug/L 1 12/08/11 18:28 541-73-112/06/11 08:3010.0
1,4-Dichlorobenzene ND ug/L 1 12/08/11 18:28 106-46-712/06/11 08:3010.0
3,3'-Dichlorobenzidine ND ug/L 1 12/08/11 18:28 91-94-112/06/11 08:3020.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 5 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-4 Lab ID: 92107636001 Collected: 12/02/11 09:10 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2,4-Dichlorophenol ND ug/L 1 12/08/11 18:28 120-83-212/06/11 08:3010.0
Diethylphthalate ND ug/L 1 12/08/11 18:28 84-66-212/06/11 08:3010.0
2,4-Dimethylphenol ND ug/L 1 12/08/11 18:28 105-67-912/06/11 08:3010.0
Dimethylphthalate ND ug/L 1 12/08/11 18:28 131-11-312/06/11 08:3010.0
Di-n-butylphthalate ND ug/L 1 12/08/11 18:28 84-74-212/06/11 08:3010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 12/08/11 18:28 534-52-112/06/11 08:3020.0
2,4-Dinitrophenol ND ug/L 1 12/08/11 18:28 51-28-512/06/11 08:3050.0
2,4-Dinitrotoluene ND ug/L 1 12/08/11 18:28 121-14-212/06/11 08:3010.0
2,6-Dinitrotoluene ND ug/L 1 12/08/11 18:28 606-20-212/06/11 08:3010.0
Di-n-octylphthalate ND ug/L 1 12/08/11 18:28 117-84-012/06/11 08:3010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 12/08/11 18:28 117-81-712/06/11 08:306.0
Fluoranthene ND ug/L 1 12/08/11 18:28 206-44-012/06/11 08:3010.0
Fluorene ND ug/L 1 12/08/11 18:28 86-73-712/06/11 08:3010.0
Hexachloro-1,3-butadiene ND ug/L 1 12/08/11 18:28 87-68-312/06/11 08:3010.0
Hexachlorobenzene ND ug/L 1 12/08/11 18:28 118-74-112/06/11 08:3010.0
Hexachlorocyclopentadiene ND ug/L 1 12/08/11 18:28 77-47-412/06/11 08:3010.0
Hexachloroethane ND ug/L 1 12/08/11 18:28 67-72-112/06/11 08:3010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 12/08/11 18:28 193-39-512/06/11 08:3010.0
Isophorone ND ug/L 1 12/08/11 18:28 78-59-112/06/11 08:3010.0
1-Methylnaphthalene ND ug/L 1 12/08/11 18:28 90-12-012/06/11 08:3010.0
2-Methylnaphthalene ND ug/L 1 12/08/11 18:28 91-57-612/06/11 08:3010.0
2-Methylphenol(o-Cresol)ND ug/L 1 12/08/11 18:28 95-48-712/06/11 08:3010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 12/08/11 18:2812/06/11 08:3010.0
Naphthalene ND ug/L 1 12/08/11 18:28 91-20-312/06/11 08:3010.0
2-Nitroaniline ND ug/L 1 12/08/11 18:28 88-74-412/06/11 08:3050.0
3-Nitroaniline ND ug/L 1 12/08/11 18:28 99-09-212/06/11 08:3050.0
4-Nitroaniline ND ug/L 1 12/08/11 18:28 100-01-612/06/11 08:3020.0
Nitrobenzene ND ug/L 1 12/08/11 18:28 98-95-312/06/11 08:3010.0
2-Nitrophenol ND ug/L 1 12/08/11 18:28 88-75-512/06/11 08:3010.0
4-Nitrophenol ND ug/L 1 12/08/11 18:28 100-02-712/06/11 08:3050.0
N-Nitrosodimethylamine ND ug/L 1 12/08/11 18:28 62-75-912/06/11 08:3010.0
N-Nitroso-di-n-propylamine ND ug/L 1 12/08/11 18:28 621-64-712/06/11 08:3010.0
N-Nitrosodiphenylamine ND ug/L 1 12/08/11 18:28 86-30-612/06/11 08:3010.0
Pentachlorophenol ND ug/L 1 12/08/11 18:28 87-86-512/06/11 08:3025.0
Phenanthrene ND ug/L 1 12/08/11 18:28 85-01-812/06/11 08:3010.0
Phenol ND ug/L 1 12/08/11 18:28 108-95-212/06/11 08:3010.0
Pyrene ND ug/L 1 12/08/11 18:28 129-00-012/06/11 08:3010.0
1,2,4-Trichlorobenzene ND ug/L 1 12/08/11 18:28 120-82-112/06/11 08:3010.0
2,4,5-Trichlorophenol ND ug/L 1 12/08/11 18:28 95-95-412/06/11 08:3010.0
2,4,6-Trichlorophenol ND ug/L 1 12/08/11 18:28 88-06-212/06/11 08:3010.0
Surrogates
Nitrobenzene-d5 (S)32 %1 12/08/11 18:28 4165-60-012/06/11 08:3021-110
2-Fluorobiphenyl (S)42 %1 12/08/11 18:28 321-60-812/06/11 08:3027-110
Terphenyl-d14 (S)60 %1 12/08/11 18:28 1718-51-012/06/11 08:3031-107
Phenol-d6 (S)17 %1 12/08/11 18:28 13127-88-312/06/11 08:3010-110
2-Fluorophenol (S)24 %1 12/08/11 18:28 367-12-412/06/11 08:3012-110
2,4,6-Tribromophenol (S)55 %1 12/08/11 18:28 118-79-612/06/11 08:3027-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 6 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-4 Lab ID: 92107636001 Collected: 12/02/11 09:10 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 12/09/11 21:00 67-64-125.0
Benzene ND ug/L 1 12/09/11 21:00 71-43-21.0
Bromobenzene ND ug/L 1 12/09/11 21:00 108-86-11.0
Bromochloromethane ND ug/L 1 12/09/11 21:00 74-97-51.0
Bromodichloromethane ND ug/L 1 12/09/11 21:00 75-27-41.0
Bromoform ND ug/L 1 12/09/11 21:00 75-25-21.0
Bromomethane ND ug/L 1 12/09/11 21:00 74-83-92.0
2-Butanone (MEK)ND ug/L 1 12/09/11 21:00 78-93-35.0
Carbon tetrachloride ND ug/L 1 12/09/11 21:00 56-23-51.0
Chlorobenzene ND ug/L 1 12/09/11 21:00 108-90-71.0
Chloroethane ND ug/L 1 12/09/11 21:00 75-00-31.0
Chloroform ND ug/L 1 12/09/11 21:00 67-66-31.0
Chloromethane ND ug/L 1 12/09/11 21:00 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/09/11 21:00 95-49-81.0
4-Chlorotoluene ND ug/L 1 12/09/11 21:00 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 12/09/11 21:00 96-12-85.0
Dibromochloromethane ND ug/L 1 12/09/11 21:00 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 12/09/11 21:00 106-93-41.0
Dibromomethane ND ug/L 1 12/09/11 21:00 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 12/09/11 21:00 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 12/09/11 21:00 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 12/09/11 21:00 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 12/09/11 21:00 75-71-81.0
1,1-Dichloroethane ND ug/L 1 12/09/11 21:00 75-34-31.0
1,2-Dichloroethane ND ug/L 1 12/09/11 21:00 107-06-21.0
1,1-Dichloroethene ND ug/L 1 12/09/11 21:00 75-35-41.0
cis-1,2-Dichloroethene 76.7 ug/L 1 12/09/11 21:00 156-59-21.0
trans-1,2-Dichloroethene 23.0 ug/L 1 12/09/11 21:00 156-60-51.0
1,2-Dichloropropane ND ug/L 1 12/09/11 21:00 78-87-51.0
1,3-Dichloropropane ND ug/L 1 12/09/11 21:00 142-28-91.0
2,2-Dichloropropane ND ug/L 1 12/09/11 21:00 594-20-71.0
1,1-Dichloropropene ND ug/L 1 12/09/11 21:00 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 12/09/11 21:00 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 12/09/11 21:00 10061-02-61.0
Diisopropyl ether ND ug/L 1 12/09/11 21:00 108-20-31.0
Ethylbenzene ND ug/L 1 12/09/11 21:00 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 12/09/11 21:00 87-68-31.0
2-Hexanone ND ug/L 1 12/09/11 21:00 591-78-65.0
p-Isopropyltoluene ND ug/L 1 12/09/11 21:00 99-87-61.0
Methylene Chloride ND ug/L 1 12/09/11 21:00 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 12/09/11 21:00 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 12/09/11 21:00 1634-04-41.0
Naphthalene ND ug/L 1 12/09/11 21:00 91-20-31.0
Styrene ND ug/L 1 12/09/11 21:00 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 12/09/11 21:00 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 12/09/11 21:00 79-34-51.0
Tetrachloroethene ND ug/L 1 12/09/11 21:00 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 7 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-4 Lab ID: 92107636001 Collected: 12/02/11 09:10 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 12/09/11 21:00 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 12/09/11 21:00 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 12/09/11 21:00 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 12/09/11 21:00 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 12/09/11 21:00 79-00-51.0
Trichloroethene ND ug/L 1 12/09/11 21:00 79-01-61.0
Trichlorofluoromethane ND ug/L 1 12/09/11 21:00 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/09/11 21:00 96-18-41.0
Vinyl acetate ND ug/L 1 12/09/11 21:00 108-05-42.0
Vinyl chloride 6.0 ug/L 1 12/09/11 21:00 75-01-41.0
Xylene (Total)ND ug/L 1 12/09/11 21:00 1330-20-72.0
m&p-Xylene ND ug/L 1 12/09/11 21:00 179601-23-12.0
o-Xylene ND ug/L 1 12/09/11 21:00 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)95 %1 12/09/11 21:00 460-00-470-130
Dibromofluoromethane (S)105 %1 12/09/11 21:00 1868-53-770-130
1,2-Dichloroethane-d4 (S)104 %1 12/09/11 21:00 17060-07-070-130
Toluene-d8 (S)95 %1 12/09/11 21:00 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 8 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-3 Lab ID: 92107636002 Collected: 12/02/11 09:40 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 1 12/08/11 16:07 7440-36-012/07/11 11:505.0
Arsenic ND ug/L 1 12/08/11 16:07 7440-38-212/07/11 11:505.0
Beryllium ND ug/L 1 12/08/11 16:07 7440-41-712/07/11 11:501.0
Cadmium ND ug/L 1 12/08/11 16:07 7440-43-912/07/11 11:501.0
Chromium ND ug/L 1 12/08/11 16:07 7440-47-312/07/11 11:505.0
Copper ND ug/L 1 12/08/11 16:07 7440-50-812/07/11 11:505.0
Lead ND ug/L 1 12/08/11 16:07 7439-92-112/07/11 11:505.0
Manganese 269 ug/L 1 12/08/11 16:07 7439-96-512/07/11 11:505.0
Nickel 64.9 ug/L 1 12/08/11 16:07 7440-02-012/07/11 11:505.0
Selenium ND ug/L 1 12/08/11 16:07 7782-49-212/07/11 11:5010.0
Silver ND ug/L 1 12/08/11 16:07 7440-22-412/07/11 11:505.0
Thallium ND ug/L 1 12/08/11 16:07 7440-28-012/07/11 11:5010.0
Zinc ND ug/L 1 12/08/11 16:07 7440-66-612/07/11 11:5010.0
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 1 12/08/11 12:11 7439-97-6 M112/07/11 16:450.20
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 12/08/11 19:00 83-32-912/06/11 08:3010.0
Acenaphthylene ND ug/L 1 12/08/11 19:00 208-96-812/06/11 08:3010.0
Aniline ND ug/L 1 12/08/11 19:00 62-53-312/06/11 08:3010.0
Anthracene ND ug/L 1 12/08/11 19:00 120-12-712/06/11 08:3010.0
Benzo(a)anthracene ND ug/L 1 12/08/11 19:00 56-55-312/06/11 08:3010.0
Benzo(a)pyrene ND ug/L 1 12/08/11 19:00 50-32-812/06/11 08:3010.0
Benzo(b)fluoranthene ND ug/L 1 12/08/11 19:00 205-99-212/06/11 08:3010.0
Benzo(g,h,i)perylene ND ug/L 1 12/08/11 19:00 191-24-212/06/11 08:3010.0
Benzo(k)fluoranthene ND ug/L 1 12/08/11 19:00 207-08-912/06/11 08:3010.0
Benzoic Acid ND ug/L 1 12/08/11 19:00 65-85-012/06/11 08:3050.0
Benzyl alcohol ND ug/L 1 12/08/11 19:00 100-51-612/06/11 08:3020.0
4-Bromophenylphenyl ether ND ug/L 1 12/08/11 19:00 101-55-312/06/11 08:3010.0
Butylbenzylphthalate ND ug/L 1 12/08/11 19:00 85-68-712/06/11 08:3010.0
4-Chloro-3-methylphenol ND ug/L 1 12/08/11 19:00 59-50-712/06/11 08:3020.0
4-Chloroaniline ND ug/L 1 12/08/11 19:00 106-47-812/06/11 08:3020.0
bis(2-Chloroethoxy)methane ND ug/L 1 12/08/11 19:00 111-91-112/06/11 08:3010.0
bis(2-Chloroethyl) ether ND ug/L 1 12/08/11 19:00 111-44-412/06/11 08:3010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 12/08/11 19:00 108-60-112/06/11 08:3010.0
2-Chloronaphthalene ND ug/L 1 12/08/11 19:00 91-58-712/06/11 08:3010.0
2-Chlorophenol ND ug/L 1 12/08/11 19:00 95-57-812/06/11 08:3010.0
4-Chlorophenylphenyl ether ND ug/L 1 12/08/11 19:00 7005-72-312/06/11 08:3010.0
Chrysene ND ug/L 1 12/08/11 19:00 218-01-912/06/11 08:3010.0
Dibenz(a,h)anthracene ND ug/L 1 12/08/11 19:00 53-70-312/06/11 08:3010.0
Dibenzofuran ND ug/L 1 12/08/11 19:00 132-64-912/06/11 08:3010.0
1,2-Dichlorobenzene ND ug/L 1 12/08/11 19:00 95-50-112/06/11 08:3010.0
1,3-Dichlorobenzene ND ug/L 1 12/08/11 19:00 541-73-112/06/11 08:3010.0
1,4-Dichlorobenzene ND ug/L 1 12/08/11 19:00 106-46-712/06/11 08:3010.0
3,3'-Dichlorobenzidine ND ug/L 1 12/08/11 19:00 91-94-112/06/11 08:3020.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 9 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-3 Lab ID: 92107636002 Collected: 12/02/11 09:40 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2,4-Dichlorophenol ND ug/L 1 12/08/11 19:00 120-83-212/06/11 08:3010.0
Diethylphthalate ND ug/L 1 12/08/11 19:00 84-66-212/06/11 08:3010.0
2,4-Dimethylphenol ND ug/L 1 12/08/11 19:00 105-67-912/06/11 08:3010.0
Dimethylphthalate ND ug/L 1 12/08/11 19:00 131-11-312/06/11 08:3010.0
Di-n-butylphthalate ND ug/L 1 12/08/11 19:00 84-74-212/06/11 08:3010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 12/08/11 19:00 534-52-112/06/11 08:3020.0
2,4-Dinitrophenol ND ug/L 1 12/08/11 19:00 51-28-512/06/11 08:3050.0
2,4-Dinitrotoluene ND ug/L 1 12/08/11 19:00 121-14-212/06/11 08:3010.0
2,6-Dinitrotoluene ND ug/L 1 12/08/11 19:00 606-20-212/06/11 08:3010.0
Di-n-octylphthalate ND ug/L 1 12/08/11 19:00 117-84-012/06/11 08:3010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 12/08/11 19:00 117-81-712/06/11 08:306.0
Fluoranthene ND ug/L 1 12/08/11 19:00 206-44-012/06/11 08:3010.0
Fluorene ND ug/L 1 12/08/11 19:00 86-73-712/06/11 08:3010.0
Hexachloro-1,3-butadiene ND ug/L 1 12/08/11 19:00 87-68-312/06/11 08:3010.0
Hexachlorobenzene ND ug/L 1 12/08/11 19:00 118-74-112/06/11 08:3010.0
Hexachlorocyclopentadiene ND ug/L 1 12/08/11 19:00 77-47-412/06/11 08:3010.0
Hexachloroethane ND ug/L 1 12/08/11 19:00 67-72-112/06/11 08:3010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 12/08/11 19:00 193-39-512/06/11 08:3010.0
Isophorone ND ug/L 1 12/08/11 19:00 78-59-112/06/11 08:3010.0
1-Methylnaphthalene ND ug/L 1 12/08/11 19:00 90-12-012/06/11 08:3010.0
2-Methylnaphthalene ND ug/L 1 12/08/11 19:00 91-57-612/06/11 08:3010.0
2-Methylphenol(o-Cresol)ND ug/L 1 12/08/11 19:00 95-48-712/06/11 08:3010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 12/08/11 19:0012/06/11 08:3010.0
Naphthalene ND ug/L 1 12/08/11 19:00 91-20-312/06/11 08:3010.0
2-Nitroaniline ND ug/L 1 12/08/11 19:00 88-74-412/06/11 08:3050.0
3-Nitroaniline ND ug/L 1 12/08/11 19:00 99-09-212/06/11 08:3050.0
4-Nitroaniline ND ug/L 1 12/08/11 19:00 100-01-612/06/11 08:3020.0
Nitrobenzene ND ug/L 1 12/08/11 19:00 98-95-312/06/11 08:3010.0
2-Nitrophenol ND ug/L 1 12/08/11 19:00 88-75-512/06/11 08:3010.0
4-Nitrophenol ND ug/L 1 12/08/11 19:00 100-02-712/06/11 08:3050.0
N-Nitrosodimethylamine ND ug/L 1 12/08/11 19:00 62-75-912/06/11 08:3010.0
N-Nitroso-di-n-propylamine ND ug/L 1 12/08/11 19:00 621-64-712/06/11 08:3010.0
N-Nitrosodiphenylamine ND ug/L 1 12/08/11 19:00 86-30-612/06/11 08:3010.0
Pentachlorophenol ND ug/L 1 12/08/11 19:00 87-86-512/06/11 08:3025.0
Phenanthrene ND ug/L 1 12/08/11 19:00 85-01-812/06/11 08:3010.0
Phenol ND ug/L 1 12/08/11 19:00 108-95-212/06/11 08:3010.0
Pyrene ND ug/L 1 12/08/11 19:00 129-00-012/06/11 08:3010.0
1,2,4-Trichlorobenzene ND ug/L 1 12/08/11 19:00 120-82-112/06/11 08:3010.0
2,4,5-Trichlorophenol ND ug/L 1 12/08/11 19:00 95-95-412/06/11 08:3010.0
2,4,6-Trichlorophenol ND ug/L 1 12/08/11 19:00 88-06-212/06/11 08:3010.0
Surrogates
Nitrobenzene-d5 (S)53 %1 12/08/11 19:00 4165-60-012/06/11 08:3021-110
2-Fluorobiphenyl (S)68 %1 12/08/11 19:00 321-60-812/06/11 08:3027-110
Terphenyl-d14 (S)68 %1 12/08/11 19:00 1718-51-012/06/11 08:3031-107
Phenol-d6 (S)22 %1 12/08/11 19:00 13127-88-312/06/11 08:3010-110
2-Fluorophenol (S)36 %1 12/08/11 19:00 367-12-412/06/11 08:3012-110
2,4,6-Tribromophenol (S)72 %1 12/08/11 19:00 118-79-612/06/11 08:3027-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 10 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-3 Lab ID: 92107636002 Collected: 12/02/11 09:40 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 12/09/11 21:25 67-64-125.0
Benzene ND ug/L 1 12/09/11 21:25 71-43-21.0
Bromobenzene ND ug/L 1 12/09/11 21:25 108-86-11.0
Bromochloromethane ND ug/L 1 12/09/11 21:25 74-97-51.0
Bromodichloromethane ND ug/L 1 12/09/11 21:25 75-27-41.0
Bromoform ND ug/L 1 12/09/11 21:25 75-25-21.0
Bromomethane ND ug/L 1 12/09/11 21:25 74-83-92.0
2-Butanone (MEK)ND ug/L 1 12/09/11 21:25 78-93-35.0
Carbon tetrachloride ND ug/L 1 12/09/11 21:25 56-23-51.0
Chlorobenzene ND ug/L 1 12/09/11 21:25 108-90-71.0
Chloroethane ND ug/L 1 12/09/11 21:25 75-00-31.0
Chloroform ND ug/L 1 12/09/11 21:25 67-66-31.0
Chloromethane ND ug/L 1 12/09/11 21:25 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/09/11 21:25 95-49-81.0
4-Chlorotoluene ND ug/L 1 12/09/11 21:25 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 12/09/11 21:25 96-12-85.0
Dibromochloromethane ND ug/L 1 12/09/11 21:25 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 12/09/11 21:25 106-93-41.0
Dibromomethane ND ug/L 1 12/09/11 21:25 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 12/09/11 21:25 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 12/09/11 21:25 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 12/09/11 21:25 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 12/09/11 21:25 75-71-81.0
1,1-Dichloroethane ND ug/L 1 12/09/11 21:25 75-34-31.0
1,2-Dichloroethane ND ug/L 1 12/09/11 21:25 107-06-21.0
1,1-Dichloroethene ND ug/L 1 12/09/11 21:25 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 12/09/11 21:25 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 12/09/11 21:25 156-60-51.0
1,2-Dichloropropane ND ug/L 1 12/09/11 21:25 78-87-51.0
1,3-Dichloropropane ND ug/L 1 12/09/11 21:25 142-28-91.0
2,2-Dichloropropane ND ug/L 1 12/09/11 21:25 594-20-71.0
1,1-Dichloropropene ND ug/L 1 12/09/11 21:25 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 12/09/11 21:25 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 12/09/11 21:25 10061-02-61.0
Diisopropyl ether ND ug/L 1 12/09/11 21:25 108-20-31.0
Ethylbenzene ND ug/L 1 12/09/11 21:25 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 12/09/11 21:25 87-68-31.0
2-Hexanone ND ug/L 1 12/09/11 21:25 591-78-65.0
p-Isopropyltoluene ND ug/L 1 12/09/11 21:25 99-87-61.0
Methylene Chloride ND ug/L 1 12/09/11 21:25 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 12/09/11 21:25 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 12/09/11 21:25 1634-04-41.0
Naphthalene ND ug/L 1 12/09/11 21:25 91-20-31.0
Styrene ND ug/L 1 12/09/11 21:25 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 12/09/11 21:25 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 12/09/11 21:25 79-34-51.0
Tetrachloroethene 10.6 ug/L 1 12/09/11 21:25 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 11 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-3 Lab ID: 92107636002 Collected: 12/02/11 09:40 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 12/09/11 21:25 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 12/09/11 21:25 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 12/09/11 21:25 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 12/09/11 21:25 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 12/09/11 21:25 79-00-51.0
Trichloroethene 4.8 ug/L 1 12/09/11 21:25 79-01-61.0
Trichlorofluoromethane ND ug/L 1 12/09/11 21:25 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/09/11 21:25 96-18-41.0
Vinyl acetate ND ug/L 1 12/09/11 21:25 108-05-42.0
Vinyl chloride ND ug/L 1 12/09/11 21:25 75-01-41.0
Xylene (Total)ND ug/L 1 12/09/11 21:25 1330-20-72.0
m&p-Xylene ND ug/L 1 12/09/11 21:25 179601-23-12.0
o-Xylene ND ug/L 1 12/09/11 21:25 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)93 %1 12/09/11 21:25 460-00-470-130
Dibromofluoromethane (S)109 %1 12/09/11 21:25 1868-53-770-130
1,2-Dichloroethane-d4 (S)105 %1 12/09/11 21:25 17060-07-070-130
Toluene-d8 (S)94 %1 12/09/11 21:25 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 12 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-1 Lab ID: 92107636003 Collected: 12/02/11 10:24 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 1 12/08/11 16:23 7440-36-012/07/11 11:505.0
Arsenic ND ug/L 1 12/08/11 16:23 7440-38-212/07/11 11:505.0
Beryllium ND ug/L 1 12/08/11 16:23 7440-41-712/07/11 11:501.0
Cadmium ND ug/L 1 12/08/11 16:23 7440-43-912/07/11 11:501.0
Chromium ND ug/L 1 12/08/11 16:23 7440-47-312/07/11 11:505.0
Copper ND ug/L 1 12/08/11 16:23 7440-50-812/07/11 11:505.0
Lead ND ug/L 1 12/08/11 16:23 7439-92-112/07/11 11:505.0
Manganese 65.9 ug/L 1 12/08/11 16:23 7439-96-512/07/11 11:505.0
Nickel ND ug/L 1 12/08/11 16:23 7440-02-012/07/11 11:505.0
Selenium ND ug/L 1 12/08/11 16:23 7782-49-212/07/11 11:5010.0
Silver ND ug/L 1 12/08/11 16:23 7440-22-412/07/11 11:505.0
Thallium ND ug/L 1 12/08/11 16:23 7440-28-012/07/11 11:5010.0
Zinc ND ug/L 1 12/08/11 16:23 7440-66-612/07/11 11:5010.0
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 1 12/08/11 12:19 7439-97-612/07/11 16:450.20
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 12/08/11 19:32 83-32-912/06/11 08:3010.0
Acenaphthylene ND ug/L 1 12/08/11 19:32 208-96-812/06/11 08:3010.0
Aniline ND ug/L 1 12/08/11 19:32 62-53-312/06/11 08:3010.0
Anthracene ND ug/L 1 12/08/11 19:32 120-12-712/06/11 08:3010.0
Benzo(a)anthracene ND ug/L 1 12/08/11 19:32 56-55-312/06/11 08:3010.0
Benzo(a)pyrene ND ug/L 1 12/08/11 19:32 50-32-812/06/11 08:3010.0
Benzo(b)fluoranthene ND ug/L 1 12/08/11 19:32 205-99-212/06/11 08:3010.0
Benzo(g,h,i)perylene ND ug/L 1 12/08/11 19:32 191-24-212/06/11 08:3010.0
Benzo(k)fluoranthene ND ug/L 1 12/08/11 19:32 207-08-912/06/11 08:3010.0
Benzoic Acid ND ug/L 1 12/08/11 19:32 65-85-012/06/11 08:3050.0
Benzyl alcohol ND ug/L 1 12/08/11 19:32 100-51-612/06/11 08:3020.0
4-Bromophenylphenyl ether ND ug/L 1 12/08/11 19:32 101-55-312/06/11 08:3010.0
Butylbenzylphthalate ND ug/L 1 12/08/11 19:32 85-68-712/06/11 08:3010.0
4-Chloro-3-methylphenol ND ug/L 1 12/08/11 19:32 59-50-712/06/11 08:3020.0
4-Chloroaniline ND ug/L 1 12/08/11 19:32 106-47-812/06/11 08:3020.0
bis(2-Chloroethoxy)methane ND ug/L 1 12/08/11 19:32 111-91-112/06/11 08:3010.0
bis(2-Chloroethyl) ether ND ug/L 1 12/08/11 19:32 111-44-412/06/11 08:3010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 12/08/11 19:32 108-60-112/06/11 08:3010.0
2-Chloronaphthalene ND ug/L 1 12/08/11 19:32 91-58-712/06/11 08:3010.0
2-Chlorophenol ND ug/L 1 12/08/11 19:32 95-57-812/06/11 08:3010.0
4-Chlorophenylphenyl ether ND ug/L 1 12/08/11 19:32 7005-72-312/06/11 08:3010.0
Chrysene ND ug/L 1 12/08/11 19:32 218-01-912/06/11 08:3010.0
Dibenz(a,h)anthracene ND ug/L 1 12/08/11 19:32 53-70-312/06/11 08:3010.0
Dibenzofuran ND ug/L 1 12/08/11 19:32 132-64-912/06/11 08:3010.0
1,2-Dichlorobenzene ND ug/L 1 12/08/11 19:32 95-50-112/06/11 08:3010.0
1,3-Dichlorobenzene ND ug/L 1 12/08/11 19:32 541-73-112/06/11 08:3010.0
1,4-Dichlorobenzene ND ug/L 1 12/08/11 19:32 106-46-712/06/11 08:3010.0
3,3'-Dichlorobenzidine ND ug/L 1 12/08/11 19:32 91-94-112/06/11 08:3020.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 13 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-1 Lab ID: 92107636003 Collected: 12/02/11 10:24 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2,4-Dichlorophenol ND ug/L 1 12/08/11 19:32 120-83-212/06/11 08:3010.0
Diethylphthalate ND ug/L 1 12/08/11 19:32 84-66-212/06/11 08:3010.0
2,4-Dimethylphenol ND ug/L 1 12/08/11 19:32 105-67-912/06/11 08:3010.0
Dimethylphthalate ND ug/L 1 12/08/11 19:32 131-11-312/06/11 08:3010.0
Di-n-butylphthalate ND ug/L 1 12/08/11 19:32 84-74-212/06/11 08:3010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 12/08/11 19:32 534-52-112/06/11 08:3020.0
2,4-Dinitrophenol ND ug/L 1 12/08/11 19:32 51-28-512/06/11 08:3050.0
2,4-Dinitrotoluene ND ug/L 1 12/08/11 19:32 121-14-212/06/11 08:3010.0
2,6-Dinitrotoluene ND ug/L 1 12/08/11 19:32 606-20-212/06/11 08:3010.0
Di-n-octylphthalate ND ug/L 1 12/08/11 19:32 117-84-012/06/11 08:3010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 12/08/11 19:32 117-81-712/06/11 08:306.0
Fluoranthene ND ug/L 1 12/08/11 19:32 206-44-012/06/11 08:3010.0
Fluorene ND ug/L 1 12/08/11 19:32 86-73-712/06/11 08:3010.0
Hexachloro-1,3-butadiene ND ug/L 1 12/08/11 19:32 87-68-312/06/11 08:3010.0
Hexachlorobenzene ND ug/L 1 12/08/11 19:32 118-74-112/06/11 08:3010.0
Hexachlorocyclopentadiene ND ug/L 1 12/08/11 19:32 77-47-412/06/11 08:3010.0
Hexachloroethane ND ug/L 1 12/08/11 19:32 67-72-112/06/11 08:3010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 12/08/11 19:32 193-39-512/06/11 08:3010.0
Isophorone ND ug/L 1 12/08/11 19:32 78-59-112/06/11 08:3010.0
1-Methylnaphthalene ND ug/L 1 12/08/11 19:32 90-12-012/06/11 08:3010.0
2-Methylnaphthalene ND ug/L 1 12/08/11 19:32 91-57-612/06/11 08:3010.0
2-Methylphenol(o-Cresol)ND ug/L 1 12/08/11 19:32 95-48-712/06/11 08:3010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 12/08/11 19:3212/06/11 08:3010.0
Naphthalene ND ug/L 1 12/08/11 19:32 91-20-312/06/11 08:3010.0
2-Nitroaniline ND ug/L 1 12/08/11 19:32 88-74-412/06/11 08:3050.0
3-Nitroaniline ND ug/L 1 12/08/11 19:32 99-09-212/06/11 08:3050.0
4-Nitroaniline ND ug/L 1 12/08/11 19:32 100-01-612/06/11 08:3020.0
Nitrobenzene ND ug/L 1 12/08/11 19:32 98-95-312/06/11 08:3010.0
2-Nitrophenol ND ug/L 1 12/08/11 19:32 88-75-512/06/11 08:3010.0
4-Nitrophenol ND ug/L 1 12/08/11 19:32 100-02-712/06/11 08:3050.0
N-Nitrosodimethylamine ND ug/L 1 12/08/11 19:32 62-75-912/06/11 08:3010.0
N-Nitroso-di-n-propylamine ND ug/L 1 12/08/11 19:32 621-64-712/06/11 08:3010.0
N-Nitrosodiphenylamine ND ug/L 1 12/08/11 19:32 86-30-612/06/11 08:3010.0
Pentachlorophenol ND ug/L 1 12/08/11 19:32 87-86-512/06/11 08:3025.0
Phenanthrene ND ug/L 1 12/08/11 19:32 85-01-812/06/11 08:3010.0
Phenol ND ug/L 1 12/08/11 19:32 108-95-212/06/11 08:3010.0
Pyrene ND ug/L 1 12/08/11 19:32 129-00-012/06/11 08:3010.0
1,2,4-Trichlorobenzene ND ug/L 1 12/08/11 19:32 120-82-112/06/11 08:3010.0
2,4,5-Trichlorophenol ND ug/L 1 12/08/11 19:32 95-95-412/06/11 08:3010.0
2,4,6-Trichlorophenol ND ug/L 1 12/08/11 19:32 88-06-212/06/11 08:3010.0
Surrogates
Nitrobenzene-d5 (S)32 %1 12/08/11 19:32 4165-60-012/06/11 08:3021-110
2-Fluorobiphenyl (S)36 %1 12/08/11 19:32 321-60-812/06/11 08:3027-110
Terphenyl-d14 (S)65 %1 12/08/11 19:32 1718-51-012/06/11 08:3031-107
Phenol-d6 (S)17 %1 12/08/11 19:32 13127-88-312/06/11 08:3010-110
2-Fluorophenol (S)24 %1 12/08/11 19:32 367-12-412/06/11 08:3012-110
2,4,6-Tribromophenol (S)54 %1 12/08/11 19:32 118-79-612/06/11 08:3027-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 14 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-1 Lab ID: 92107636003 Collected: 12/02/11 10:24 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 12/09/11 21:51 67-64-125.0
Benzene ND ug/L 1 12/09/11 21:51 71-43-21.0
Bromobenzene ND ug/L 1 12/09/11 21:51 108-86-11.0
Bromochloromethane ND ug/L 1 12/09/11 21:51 74-97-51.0
Bromodichloromethane ND ug/L 1 12/09/11 21:51 75-27-41.0
Bromoform ND ug/L 1 12/09/11 21:51 75-25-21.0
Bromomethane ND ug/L 1 12/09/11 21:51 74-83-92.0
2-Butanone (MEK)ND ug/L 1 12/09/11 21:51 78-93-35.0
Carbon tetrachloride ND ug/L 1 12/09/11 21:51 56-23-51.0
Chlorobenzene ND ug/L 1 12/09/11 21:51 108-90-71.0
Chloroethane ND ug/L 1 12/09/11 21:51 75-00-31.0
Chloroform ND ug/L 1 12/09/11 21:51 67-66-31.0
Chloromethane ND ug/L 1 12/09/11 21:51 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/09/11 21:51 95-49-81.0
4-Chlorotoluene ND ug/L 1 12/09/11 21:51 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 12/09/11 21:51 96-12-85.0
Dibromochloromethane ND ug/L 1 12/09/11 21:51 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 12/09/11 21:51 106-93-41.0
Dibromomethane ND ug/L 1 12/09/11 21:51 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 12/09/11 21:51 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 12/09/11 21:51 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 12/09/11 21:51 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 12/09/11 21:51 75-71-81.0
1,1-Dichloroethane ND ug/L 1 12/09/11 21:51 75-34-31.0
1,2-Dichloroethane ND ug/L 1 12/09/11 21:51 107-06-21.0
1,1-Dichloroethene ND ug/L 1 12/09/11 21:51 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 12/09/11 21:51 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 12/09/11 21:51 156-60-51.0
1,2-Dichloropropane ND ug/L 1 12/09/11 21:51 78-87-51.0
1,3-Dichloropropane ND ug/L 1 12/09/11 21:51 142-28-91.0
2,2-Dichloropropane ND ug/L 1 12/09/11 21:51 594-20-71.0
1,1-Dichloropropene ND ug/L 1 12/09/11 21:51 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 12/09/11 21:51 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 12/09/11 21:51 10061-02-61.0
Diisopropyl ether ND ug/L 1 12/09/11 21:51 108-20-31.0
Ethylbenzene ND ug/L 1 12/09/11 21:51 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 12/09/11 21:51 87-68-31.0
2-Hexanone ND ug/L 1 12/09/11 21:51 591-78-65.0
p-Isopropyltoluene ND ug/L 1 12/09/11 21:51 99-87-61.0
Methylene Chloride ND ug/L 1 12/09/11 21:51 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 12/09/11 21:51 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 12/09/11 21:51 1634-04-41.0
Naphthalene ND ug/L 1 12/09/11 21:51 91-20-31.0
Styrene ND ug/L 1 12/09/11 21:51 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 12/09/11 21:51 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 12/09/11 21:51 79-34-51.0
Tetrachloroethene ND ug/L 1 12/09/11 21:51 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 15 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-1 Lab ID: 92107636003 Collected: 12/02/11 10:24 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 12/09/11 21:51 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 12/09/11 21:51 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 12/09/11 21:51 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 12/09/11 21:51 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 12/09/11 21:51 79-00-51.0
Trichloroethene ND ug/L 1 12/09/11 21:51 79-01-61.0
Trichlorofluoromethane ND ug/L 1 12/09/11 21:51 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/09/11 21:51 96-18-41.0
Vinyl acetate ND ug/L 1 12/09/11 21:51 108-05-42.0
Vinyl chloride ND ug/L 1 12/09/11 21:51 75-01-41.0
Xylene (Total)ND ug/L 1 12/09/11 21:51 1330-20-72.0
m&p-Xylene ND ug/L 1 12/09/11 21:51 179601-23-12.0
o-Xylene ND ug/L 1 12/09/11 21:51 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)94 %1 12/09/11 21:51 460-00-470-130
Dibromofluoromethane (S)110 %1 12/09/11 21:51 1868-53-770-130
1,2-Dichloroethane-d4 (S)106 %1 12/09/11 21:51 17060-07-070-130
Toluene-d8 (S)93 %1 12/09/11 21:51 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 16 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-1 Lab ID: 92107636004 Collected: 12/02/11 11:34 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 1 12/08/11 16:26 7440-36-012/07/11 11:505.0
Arsenic ND ug/L 1 12/08/11 16:26 7440-38-212/07/11 11:505.0
Beryllium ND ug/L 1 12/08/11 16:26 7440-41-712/07/11 11:501.0
Cadmium ND ug/L 1 12/08/11 16:26 7440-43-912/07/11 11:501.0
Chromium ND ug/L 1 12/08/11 16:26 7440-47-312/07/11 11:505.0
Copper ND ug/L 1 12/08/11 16:26 7440-50-812/07/11 11:505.0
Lead ND ug/L 1 12/08/11 16:26 7439-92-112/07/11 11:505.0
Manganese 23.0 ug/L 1 12/08/11 16:26 7439-96-512/07/11 11:505.0
Nickel ND ug/L 1 12/08/11 16:26 7440-02-012/07/11 11:505.0
Selenium ND ug/L 1 12/08/11 16:26 7782-49-212/07/11 11:5010.0
Silver ND ug/L 1 12/08/11 16:26 7440-22-412/07/11 11:505.0
Thallium ND ug/L 1 12/08/11 16:26 7440-28-012/07/11 11:5010.0
Zinc ND ug/L 1 12/08/11 16:26 7440-66-612/07/11 11:5010.0
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 1 12/08/11 12:22 7439-97-612/07/11 16:450.20
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 1 12/08/11 20:05 83-32-912/06/11 08:3010.0
Acenaphthylene ND ug/L 1 12/08/11 20:05 208-96-812/06/11 08:3010.0
Aniline ND ug/L 1 12/08/11 20:05 62-53-312/06/11 08:3010.0
Anthracene ND ug/L 1 12/08/11 20:05 120-12-712/06/11 08:3010.0
Benzo(a)anthracene ND ug/L 1 12/08/11 20:05 56-55-312/06/11 08:3010.0
Benzo(a)pyrene ND ug/L 1 12/08/11 20:05 50-32-812/06/11 08:3010.0
Benzo(b)fluoranthene ND ug/L 1 12/08/11 20:05 205-99-212/06/11 08:3010.0
Benzo(g,h,i)perylene ND ug/L 1 12/08/11 20:05 191-24-212/06/11 08:3010.0
Benzo(k)fluoranthene ND ug/L 1 12/08/11 20:05 207-08-912/06/11 08:3010.0
Benzoic Acid ND ug/L 1 12/08/11 20:05 65-85-012/06/11 08:3050.0
Benzyl alcohol ND ug/L 1 12/08/11 20:05 100-51-612/06/11 08:3020.0
4-Bromophenylphenyl ether ND ug/L 1 12/08/11 20:05 101-55-312/06/11 08:3010.0
Butylbenzylphthalate ND ug/L 1 12/08/11 20:05 85-68-712/06/11 08:3010.0
4-Chloro-3-methylphenol ND ug/L 1 12/08/11 20:05 59-50-712/06/11 08:3020.0
4-Chloroaniline ND ug/L 1 12/08/11 20:05 106-47-812/06/11 08:3020.0
bis(2-Chloroethoxy)methane ND ug/L 1 12/08/11 20:05 111-91-112/06/11 08:3010.0
bis(2-Chloroethyl) ether ND ug/L 1 12/08/11 20:05 111-44-412/06/11 08:3010.0
bis(2-Chloroisopropyl) ether ND ug/L 1 12/08/11 20:05 108-60-112/06/11 08:3010.0
2-Chloronaphthalene ND ug/L 1 12/08/11 20:05 91-58-712/06/11 08:3010.0
2-Chlorophenol ND ug/L 1 12/08/11 20:05 95-57-812/06/11 08:3010.0
4-Chlorophenylphenyl ether ND ug/L 1 12/08/11 20:05 7005-72-312/06/11 08:3010.0
Chrysene ND ug/L 1 12/08/11 20:05 218-01-912/06/11 08:3010.0
Dibenz(a,h)anthracene ND ug/L 1 12/08/11 20:05 53-70-312/06/11 08:3010.0
Dibenzofuran ND ug/L 1 12/08/11 20:05 132-64-912/06/11 08:3010.0
1,2-Dichlorobenzene ND ug/L 1 12/08/11 20:05 95-50-112/06/11 08:3010.0
1,3-Dichlorobenzene ND ug/L 1 12/08/11 20:05 541-73-112/06/11 08:3010.0
1,4-Dichlorobenzene ND ug/L 1 12/08/11 20:05 106-46-712/06/11 08:3010.0
3,3'-Dichlorobenzidine ND ug/L 1 12/08/11 20:05 91-94-112/06/11 08:3020.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 17 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-1 Lab ID: 92107636004 Collected: 12/02/11 11:34 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2,4-Dichlorophenol ND ug/L 1 12/08/11 20:05 120-83-212/06/11 08:3010.0
Diethylphthalate ND ug/L 1 12/08/11 20:05 84-66-212/06/11 08:3010.0
2,4-Dimethylphenol ND ug/L 1 12/08/11 20:05 105-67-912/06/11 08:3010.0
Dimethylphthalate ND ug/L 1 12/08/11 20:05 131-11-312/06/11 08:3010.0
Di-n-butylphthalate ND ug/L 1 12/08/11 20:05 84-74-212/06/11 08:3010.0
4,6-Dinitro-2-methylphenol ND ug/L 1 12/08/11 20:05 534-52-112/06/11 08:3020.0
2,4-Dinitrophenol ND ug/L 1 12/08/11 20:05 51-28-512/06/11 08:3050.0
2,4-Dinitrotoluene ND ug/L 1 12/08/11 20:05 121-14-212/06/11 08:3010.0
2,6-Dinitrotoluene ND ug/L 1 12/08/11 20:05 606-20-212/06/11 08:3010.0
Di-n-octylphthalate ND ug/L 1 12/08/11 20:05 117-84-012/06/11 08:3010.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 12/08/11 20:05 117-81-712/06/11 08:306.0
Fluoranthene ND ug/L 1 12/08/11 20:05 206-44-012/06/11 08:3010.0
Fluorene ND ug/L 1 12/08/11 20:05 86-73-712/06/11 08:3010.0
Hexachloro-1,3-butadiene ND ug/L 1 12/08/11 20:05 87-68-312/06/11 08:3010.0
Hexachlorobenzene ND ug/L 1 12/08/11 20:05 118-74-112/06/11 08:3010.0
Hexachlorocyclopentadiene ND ug/L 1 12/08/11 20:05 77-47-412/06/11 08:3010.0
Hexachloroethane ND ug/L 1 12/08/11 20:05 67-72-112/06/11 08:3010.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 12/08/11 20:05 193-39-512/06/11 08:3010.0
Isophorone ND ug/L 1 12/08/11 20:05 78-59-112/06/11 08:3010.0
1-Methylnaphthalene ND ug/L 1 12/08/11 20:05 90-12-012/06/11 08:3010.0
2-Methylnaphthalene ND ug/L 1 12/08/11 20:05 91-57-612/06/11 08:3010.0
2-Methylphenol(o-Cresol)ND ug/L 1 12/08/11 20:05 95-48-712/06/11 08:3010.0
3&4-Methylphenol(m&p Cresol)ND ug/L 1 12/08/11 20:0512/06/11 08:3010.0
Naphthalene ND ug/L 1 12/08/11 20:05 91-20-312/06/11 08:3010.0
2-Nitroaniline ND ug/L 1 12/08/11 20:05 88-74-412/06/11 08:3050.0
3-Nitroaniline ND ug/L 1 12/08/11 20:05 99-09-212/06/11 08:3050.0
4-Nitroaniline ND ug/L 1 12/08/11 20:05 100-01-612/06/11 08:3020.0
Nitrobenzene ND ug/L 1 12/08/11 20:05 98-95-312/06/11 08:3010.0
2-Nitrophenol ND ug/L 1 12/08/11 20:05 88-75-512/06/11 08:3010.0
4-Nitrophenol ND ug/L 1 12/08/11 20:05 100-02-712/06/11 08:3050.0
N-Nitrosodimethylamine ND ug/L 1 12/08/11 20:05 62-75-912/06/11 08:3010.0
N-Nitroso-di-n-propylamine ND ug/L 1 12/08/11 20:05 621-64-712/06/11 08:3010.0
N-Nitrosodiphenylamine ND ug/L 1 12/08/11 20:05 86-30-612/06/11 08:3010.0
Pentachlorophenol ND ug/L 1 12/08/11 20:05 87-86-512/06/11 08:3025.0
Phenanthrene ND ug/L 1 12/08/11 20:05 85-01-812/06/11 08:3010.0
Phenol ND ug/L 1 12/08/11 20:05 108-95-212/06/11 08:3010.0
Pyrene ND ug/L 1 12/08/11 20:05 129-00-012/06/11 08:3010.0
1,2,4-Trichlorobenzene ND ug/L 1 12/08/11 20:05 120-82-112/06/11 08:3010.0
2,4,5-Trichlorophenol ND ug/L 1 12/08/11 20:05 95-95-412/06/11 08:3010.0
2,4,6-Trichlorophenol ND ug/L 1 12/08/11 20:05 88-06-212/06/11 08:3010.0
Surrogates
Nitrobenzene-d5 (S)33 %1 12/08/11 20:05 4165-60-012/06/11 08:3021-110
2-Fluorobiphenyl (S)38 %1 12/08/11 20:05 321-60-812/06/11 08:3027-110
Terphenyl-d14 (S)62 %1 12/08/11 20:05 1718-51-012/06/11 08:3031-107
Phenol-d6 (S)15 %1 12/08/11 20:05 13127-88-312/06/11 08:3010-110
2-Fluorophenol (S)22 %1 12/08/11 20:05 367-12-412/06/11 08:3012-110
2,4,6-Tribromophenol (S)41 %1 12/08/11 20:05 118-79-612/06/11 08:3027-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 18 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-1 Lab ID: 92107636004 Collected: 12/02/11 11:34 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 12/09/11 07:23 67-64-125.0
Benzene ND ug/L 1 12/09/11 07:23 71-43-21.0
Bromobenzene ND ug/L 1 12/09/11 07:23 108-86-11.0
Bromochloromethane ND ug/L 1 12/09/11 07:23 74-97-51.0
Bromodichloromethane ND ug/L 1 12/09/11 07:23 75-27-41.0
Bromoform ND ug/L 1 12/09/11 07:23 75-25-21.0
Bromomethane ND ug/L 1 12/09/11 07:23 74-83-92.0
2-Butanone (MEK)ND ug/L 1 12/09/11 07:23 78-93-35.0
Carbon tetrachloride ND ug/L 1 12/09/11 07:23 56-23-51.0
Chlorobenzene ND ug/L 1 12/09/11 07:23 108-90-71.0
Chloroethane ND ug/L 1 12/09/11 07:23 75-00-31.0
Chloroform ND ug/L 1 12/09/11 07:23 67-66-31.0
Chloromethane ND ug/L 1 12/09/11 07:23 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/09/11 07:23 95-49-81.0
4-Chlorotoluene ND ug/L 1 12/09/11 07:23 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 12/09/11 07:23 96-12-85.0
Dibromochloromethane ND ug/L 1 12/09/11 07:23 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 12/09/11 07:23 106-93-41.0
Dibromomethane ND ug/L 1 12/09/11 07:23 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 12/09/11 07:23 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 12/09/11 07:23 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 12/09/11 07:23 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 12/09/11 07:23 75-71-81.0
1,1-Dichloroethane ND ug/L 1 12/09/11 07:23 75-34-31.0
1,2-Dichloroethane ND ug/L 1 12/09/11 07:23 107-06-21.0
1,1-Dichloroethene ND ug/L 1 12/09/11 07:23 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 12/09/11 07:23 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 12/09/11 07:23 156-60-51.0
1,2-Dichloropropane ND ug/L 1 12/09/11 07:23 78-87-51.0
1,3-Dichloropropane ND ug/L 1 12/09/11 07:23 142-28-91.0
2,2-Dichloropropane ND ug/L 1 12/09/11 07:23 594-20-71.0
1,1-Dichloropropene ND ug/L 1 12/09/11 07:23 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 12/09/11 07:23 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 12/09/11 07:23 10061-02-61.0
Diisopropyl ether ND ug/L 1 12/09/11 07:23 108-20-31.0
Ethylbenzene ND ug/L 1 12/09/11 07:23 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 12/09/11 07:23 87-68-31.0
2-Hexanone ND ug/L 1 12/09/11 07:23 591-78-65.0
p-Isopropyltoluene ND ug/L 1 12/09/11 07:23 99-87-61.0
Methylene Chloride ND ug/L 1 12/09/11 07:23 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 12/09/11 07:23 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 12/09/11 07:23 1634-04-41.0
Naphthalene ND ug/L 1 12/09/11 07:23 91-20-31.0
Styrene ND ug/L 1 12/09/11 07:23 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 12/09/11 07:23 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 12/09/11 07:23 79-34-51.0
Tetrachloroethene ND ug/L 1 12/09/11 07:23 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 19 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-1 Lab ID: 92107636004 Collected: 12/02/11 11:34 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 12/09/11 07:23 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 12/09/11 07:23 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 12/09/11 07:23 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 12/09/11 07:23 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 12/09/11 07:23 79-00-51.0
Trichloroethene ND ug/L 1 12/09/11 07:23 79-01-61.0
Trichlorofluoromethane ND ug/L 1 12/09/11 07:23 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/09/11 07:23 96-18-41.0
Vinyl acetate ND ug/L 1 12/09/11 07:23 108-05-42.0
Vinyl chloride ND ug/L 1 12/09/11 07:23 75-01-41.0
Xylene (Total)ND ug/L 1 12/09/11 07:23 1330-20-72.0
m&p-Xylene ND ug/L 1 12/09/11 07:23 179601-23-12.0
o-Xylene ND ug/L 1 12/09/11 07:23 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)95 %1 12/09/11 07:23 460-00-470-130
Dibromofluoromethane (S)106 %1 12/09/11 07:23 1868-53-770-130
1,2-Dichloroethane-d4 (S)103 %1 12/09/11 07:23 17060-07-070-130
Toluene-d8 (S)96 %1 12/09/11 07:23 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 20 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-2 Lab ID: 92107636005 Collected: 12/02/11 11:04 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone 1070 ug/L 20 12/11/11 10:20 67-64-1500
Benzene 8.4 ug/L 2 12/09/11 22:16 71-43-22.0
Bromobenzene ND ug/L 2 12/09/11 22:16 108-86-12.0
Bromochloromethane ND ug/L 2 12/09/11 22:16 74-97-52.0
Bromodichloromethane ND ug/L 2 12/09/11 22:16 75-27-42.0
Bromoform ND ug/L 2 12/09/11 22:16 75-25-22.0
Bromomethane ND ug/L 2 12/09/11 22:16 74-83-94.0
2-Butanone (MEK)64.1 ug/L 2 12/09/11 22:16 78-93-310.0
Carbon tetrachloride ND ug/L 2 12/09/11 22:16 56-23-52.0
Chlorobenzene ND ug/L 2 12/09/11 22:16 108-90-72.0
Chloroethane ND ug/L 2 12/09/11 22:16 75-00-32.0
Chloroform ND ug/L 2 12/09/11 22:16 67-66-32.0
Chloromethane ND ug/L 2 12/09/11 22:16 74-87-32.0
2-Chlorotoluene ND ug/L 2 12/09/11 22:16 95-49-82.0
4-Chlorotoluene ND ug/L 2 12/09/11 22:16 106-43-42.0
1,2-Dibromo-3-chloropropane ND ug/L 2 12/09/11 22:16 96-12-810.0
Dibromochloromethane ND ug/L 2 12/09/11 22:16 124-48-12.0
1,2-Dibromoethane (EDB)ND ug/L 2 12/09/11 22:16 106-93-42.0
Dibromomethane ND ug/L 2 12/09/11 22:16 74-95-32.0
1,2-Dichlorobenzene ND ug/L 2 12/09/11 22:16 95-50-12.0
1,3-Dichlorobenzene ND ug/L 2 12/09/11 22:16 541-73-12.0
1,4-Dichlorobenzene ND ug/L 2 12/09/11 22:16 106-46-72.0
Dichlorodifluoromethane ND ug/L 2 12/09/11 22:16 75-71-82.0
1,1-Dichloroethane ND ug/L 2 12/09/11 22:16 75-34-32.0
1,2-Dichloroethane ND ug/L 2 12/09/11 22:16 107-06-22.0
1,1-Dichloroethene ND ug/L 2 12/09/11 22:16 75-35-42.0
cis-1,2-Dichloroethene ND ug/L 2 12/09/11 22:16 156-59-22.0
trans-1,2-Dichloroethene ND ug/L 2 12/09/11 22:16 156-60-52.0
1,2-Dichloropropane ND ug/L 2 12/09/11 22:16 78-87-52.0
1,3-Dichloropropane ND ug/L 2 12/09/11 22:16 142-28-92.0
2,2-Dichloropropane ND ug/L 2 12/09/11 22:16 594-20-72.0
1,1-Dichloropropene ND ug/L 2 12/09/11 22:16 563-58-62.0
cis-1,3-Dichloropropene ND ug/L 2 12/09/11 22:16 10061-01-52.0
trans-1,3-Dichloropropene ND ug/L 2 12/09/11 22:16 10061-02-62.0
Diisopropyl ether 39.5 ug/L 2 12/09/11 22:16 108-20-32.0
Ethylbenzene ND ug/L 2 12/09/11 22:16 100-41-42.0
Hexachloro-1,3-butadiene ND ug/L 2 12/09/11 22:16 87-68-32.0
2-Hexanone ND ug/L 2 12/09/11 22:16 591-78-610.0
p-Isopropyltoluene ND ug/L 2 12/09/11 22:16 99-87-62.0
Methylene Chloride ND ug/L 2 12/09/11 22:16 75-09-24.0
4-Methyl-2-pentanone (MIBK)ND ug/L 2 12/09/11 22:16 108-10-110.0
Methyl-tert-butyl ether ND ug/L 2 12/09/11 22:16 1634-04-42.0
Naphthalene 9.5 ug/L 2 12/09/11 22:16 91-20-32.0
Styrene ND ug/L 2 12/09/11 22:16 100-42-52.0
1,1,1,2-Tetrachloroethane ND ug/L 2 12/09/11 22:16 630-20-62.0
1,1,2,2-Tetrachloroethane ND ug/L 2 12/09/11 22:16 79-34-52.0
Tetrachloroethene ND ug/L 2 12/09/11 22:16 127-18-42.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 21 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: HH-2 Lab ID: 92107636005 Collected: 12/02/11 11:04 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene 185 ug/L 2 12/09/11 22:16 108-88-32.0
1,2,3-Trichlorobenzene ND ug/L 2 12/09/11 22:16 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 2 12/09/11 22:16 120-82-12.0
1,1,1-Trichloroethane ND ug/L 2 12/09/11 22:16 71-55-62.0
1,1,2-Trichloroethane ND ug/L 2 12/09/11 22:16 79-00-52.0
Trichloroethene ND ug/L 2 12/09/11 22:16 79-01-62.0
Trichlorofluoromethane ND ug/L 2 12/09/11 22:16 75-69-42.0
1,2,3-Trichloropropane ND ug/L 2 12/09/11 22:16 96-18-42.0
Vinyl acetate ND ug/L 2 12/09/11 22:16 108-05-44.0
Vinyl chloride ND ug/L 2 12/09/11 22:16 75-01-42.0
Xylene (Total)14.3 ug/L 2 12/09/11 22:16 1330-20-74.0
m&p-Xylene ND ug/L 2 12/09/11 22:16 179601-23-14.0
o-Xylene 11.1 ug/L 2 12/09/11 22:16 95-47-62.0
Surrogates
4-Bromofluorobenzene (S)94 %2 12/09/11 22:16 460-00-470-130
Dibromofluoromethane (S)101 %2 12/09/11 22:16 1868-53-770-130
1,2-Dichloroethane-d4 (S)103 %2 12/09/11 22:16 17060-07-070-130
Toluene-d8 (S)97 %2 12/09/11 22:16 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 22 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-8 Lab ID: 92107636006 Collected: 12/02/11 12:20 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 12/09/11 11:38 67-64-125.0
Benzene ND ug/L 1 12/09/11 11:38 71-43-21.0
Bromobenzene ND ug/L 1 12/09/11 11:38 108-86-11.0
Bromochloromethane ND ug/L 1 12/09/11 11:38 74-97-51.0
Bromodichloromethane ND ug/L 1 12/09/11 11:38 75-27-41.0
Bromoform ND ug/L 1 12/09/11 11:38 75-25-21.0
Bromomethane ND ug/L 1 12/09/11 11:38 74-83-92.0
2-Butanone (MEK)ND ug/L 1 12/09/11 11:38 78-93-35.0
Carbon tetrachloride ND ug/L 1 12/09/11 11:38 56-23-51.0
Chlorobenzene ND ug/L 1 12/09/11 11:38 108-90-71.0
Chloroethane ND ug/L 1 12/09/11 11:38 75-00-31.0
Chloroform ND ug/L 1 12/09/11 11:38 67-66-31.0
Chloromethane ND ug/L 1 12/09/11 11:38 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/09/11 11:38 95-49-81.0
4-Chlorotoluene ND ug/L 1 12/09/11 11:38 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 12/09/11 11:38 96-12-85.0
Dibromochloromethane ND ug/L 1 12/09/11 11:38 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 12/09/11 11:38 106-93-41.0
Dibromomethane ND ug/L 1 12/09/11 11:38 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 12/09/11 11:38 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 12/09/11 11:38 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 12/09/11 11:38 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 12/09/11 11:38 75-71-81.0
1,1-Dichloroethane ND ug/L 1 12/09/11 11:38 75-34-31.0
1,2-Dichloroethane ND ug/L 1 12/09/11 11:38 107-06-21.0
1,1-Dichloroethene ND ug/L 1 12/09/11 11:38 75-35-41.0
cis-1,2-Dichloroethene 1.5 ug/L 1 12/09/11 11:38 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 12/09/11 11:38 156-60-51.0
1,2-Dichloropropane ND ug/L 1 12/09/11 11:38 78-87-51.0
1,3-Dichloropropane ND ug/L 1 12/09/11 11:38 142-28-91.0
2,2-Dichloropropane ND ug/L 1 12/09/11 11:38 594-20-71.0
1,1-Dichloropropene ND ug/L 1 12/09/11 11:38 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 12/09/11 11:38 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 12/09/11 11:38 10061-02-61.0
Diisopropyl ether 18.2 ug/L 1 12/09/11 11:38 108-20-31.0
Ethylbenzene ND ug/L 1 12/09/11 11:38 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 12/09/11 11:38 87-68-31.0
2-Hexanone ND ug/L 1 12/09/11 11:38 591-78-65.0
p-Isopropyltoluene ND ug/L 1 12/09/11 11:38 99-87-61.0
Methylene Chloride ND ug/L 1 12/09/11 11:38 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 12/09/11 11:38 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 12/09/11 11:38 1634-04-41.0
Naphthalene ND ug/L 1 12/09/11 11:38 91-20-31.0
Styrene ND ug/L 1 12/09/11 11:38 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 12/09/11 11:38 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 12/09/11 11:38 79-34-51.0
Tetrachloroethene ND ug/L 1 12/09/11 11:38 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 23 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-8 Lab ID: 92107636006 Collected: 12/02/11 12:20 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 12/09/11 11:38 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 12/09/11 11:38 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 12/09/11 11:38 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 12/09/11 11:38 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 12/09/11 11:38 79-00-51.0
Trichloroethene 2.2 ug/L 1 12/09/11 11:38 79-01-61.0
Trichlorofluoromethane ND ug/L 1 12/09/11 11:38 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/09/11 11:38 96-18-41.0
Vinyl acetate ND ug/L 1 12/09/11 11:38 108-05-42.0
Vinyl chloride ND ug/L 1 12/09/11 11:38 75-01-41.0
Xylene (Total)ND ug/L 1 12/09/11 11:38 1330-20-72.0
m&p-Xylene ND ug/L 1 12/09/11 11:38 179601-23-12.0
o-Xylene ND ug/L 1 12/09/11 11:38 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)96 %1 12/09/11 11:38 460-00-470-130
Dibromofluoromethane (S)108 %1 12/09/11 11:38 1868-53-770-130
1,2-Dichloroethane-d4 (S)107 %1 12/09/11 11:38 17060-07-070-130
Toluene-d8 (S)97 %1 12/09/11 11:38 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 24 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-11 Lab ID: 92107636007 Collected: 12/02/11 12:44 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 2.5 12/09/11 19:43 67-64-162.5
Benzene ND ug/L 2.5 12/09/11 19:43 71-43-22.5
Bromobenzene ND ug/L 2.5 12/09/11 19:43 108-86-12.5
Bromochloromethane ND ug/L 2.5 12/09/11 19:43 74-97-52.5
Bromodichloromethane ND ug/L 2.5 12/09/11 19:43 75-27-42.5
Bromoform ND ug/L 2.5 12/09/11 19:43 75-25-22.5
Bromomethane ND ug/L 2.5 12/09/11 19:43 74-83-95.0
2-Butanone (MEK)ND ug/L 2.5 12/09/11 19:43 78-93-312.5
Carbon tetrachloride ND ug/L 2.5 12/09/11 19:43 56-23-52.5
Chlorobenzene ND ug/L 2.5 12/09/11 19:43 108-90-72.5
Chloroethane ND ug/L 2.5 12/09/11 19:43 75-00-32.5
Chloroform ND ug/L 2.5 12/09/11 19:43 67-66-32.5
Chloromethane ND ug/L 2.5 12/09/11 19:43 74-87-32.5
2-Chlorotoluene ND ug/L 2.5 12/09/11 19:43 95-49-82.5
4-Chlorotoluene ND ug/L 2.5 12/09/11 19:43 106-43-42.5
1,2-Dibromo-3-chloropropane ND ug/L 2.5 12/09/11 19:43 96-12-812.5
Dibromochloromethane ND ug/L 2.5 12/09/11 19:43 124-48-12.5
1,2-Dibromoethane (EDB)ND ug/L 2.5 12/09/11 19:43 106-93-42.5
Dibromomethane ND ug/L 2.5 12/09/11 19:43 74-95-32.5
1,2-Dichlorobenzene ND ug/L 2.5 12/09/11 19:43 95-50-12.5
1,3-Dichlorobenzene ND ug/L 2.5 12/09/11 19:43 541-73-12.5
1,4-Dichlorobenzene ND ug/L 2.5 12/09/11 19:43 106-46-72.5
Dichlorodifluoromethane ND ug/L 2.5 12/09/11 19:43 75-71-82.5
1,1-Dichloroethane ND ug/L 2.5 12/09/11 19:43 75-34-32.5
1,2-Dichloroethane ND ug/L 2.5 12/09/11 19:43 107-06-22.5
1,1-Dichloroethene ND ug/L 2.5 12/09/11 19:43 75-35-42.5
cis-1,2-Dichloroethene 25.9 ug/L 2.5 12/09/11 19:43 156-59-22.5
trans-1,2-Dichloroethene ND ug/L 2.5 12/09/11 19:43 156-60-52.5
1,2-Dichloropropane ND ug/L 2.5 12/09/11 19:43 78-87-52.5
1,3-Dichloropropane ND ug/L 2.5 12/09/11 19:43 142-28-92.5
2,2-Dichloropropane ND ug/L 2.5 12/09/11 19:43 594-20-72.5
1,1-Dichloropropene ND ug/L 2.5 12/09/11 19:43 563-58-62.5
cis-1,3-Dichloropropene ND ug/L 2.5 12/09/11 19:43 10061-01-52.5
trans-1,3-Dichloropropene ND ug/L 2.5 12/09/11 19:43 10061-02-62.5
Diisopropyl ether 4.0 ug/L 2.5 12/09/11 19:43 108-20-32.5
Ethylbenzene ND ug/L 2.5 12/09/11 19:43 100-41-42.5
Hexachloro-1,3-butadiene ND ug/L 2.5 12/09/11 19:43 87-68-32.5
2-Hexanone ND ug/L 2.5 12/09/11 19:43 591-78-612.5
p-Isopropyltoluene ND ug/L 2.5 12/09/11 19:43 99-87-62.5
Methylene Chloride ND ug/L 2.5 12/09/11 19:43 75-09-25.0
4-Methyl-2-pentanone (MIBK)ND ug/L 2.5 12/09/11 19:43 108-10-112.5
Methyl-tert-butyl ether ND ug/L 2.5 12/09/11 19:43 1634-04-42.5
Naphthalene ND ug/L 2.5 12/09/11 19:43 91-20-32.5
Styrene ND ug/L 2.5 12/09/11 19:43 100-42-52.5
1,1,1,2-Tetrachloroethane ND ug/L 2.5 12/09/11 19:43 630-20-62.5
1,1,2,2-Tetrachloroethane ND ug/L 2.5 12/09/11 19:43 79-34-52.5
Tetrachloroethene 441 ug/L 2.5 12/09/11 19:43 127-18-42.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 25 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-11 Lab ID: 92107636007 Collected: 12/02/11 12:44 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 2.5 12/09/11 19:43 108-88-32.5
1,2,3-Trichlorobenzene ND ug/L 2.5 12/09/11 19:43 87-61-62.5
1,2,4-Trichlorobenzene ND ug/L 2.5 12/09/11 19:43 120-82-12.5
1,1,1-Trichloroethane ND ug/L 2.5 12/09/11 19:43 71-55-62.5
1,1,2-Trichloroethane ND ug/L 2.5 12/09/11 19:43 79-00-52.5
Trichloroethene 39.3 ug/L 2.5 12/09/11 19:43 79-01-62.5
Trichlorofluoromethane ND ug/L 2.5 12/09/11 19:43 75-69-42.5
1,2,3-Trichloropropane ND ug/L 2.5 12/09/11 19:43 96-18-42.5
Vinyl acetate ND ug/L 2.5 12/09/11 19:43 108-05-45.0
Vinyl chloride ND ug/L 2.5 12/09/11 19:43 75-01-42.5
Xylene (Total)ND ug/L 2.5 12/09/11 19:43 1330-20-75.0
m&p-Xylene ND ug/L 2.5 12/09/11 19:43 179601-23-15.0
o-Xylene ND ug/L 2.5 12/09/11 19:43 95-47-62.5
Surrogates
4-Bromofluorobenzene (S)94 %2.5 12/09/11 19:43 460-00-470-130
Dibromofluoromethane (S)109 %2.5 12/09/11 19:43 1868-53-770-130
1,2-Dichloroethane-d4 (S)106 %2.5 12/09/11 19:43 17060-07-070-130
Toluene-d8 (S)97 %2.5 12/09/11 19:43 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 26 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-15 Lab ID: 92107636008 Collected: 12/02/11 13:14 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 12/11/11 15:04 67-64-125.0
Benzene ND ug/L 1 12/11/11 15:04 71-43-21.0
Bromobenzene ND ug/L 1 12/11/11 15:04 108-86-11.0
Bromochloromethane ND ug/L 1 12/11/11 15:04 74-97-51.0
Bromodichloromethane ND ug/L 1 12/11/11 15:04 75-27-41.0
Bromoform ND ug/L 1 12/11/11 15:04 75-25-21.0
Bromomethane ND ug/L 1 12/11/11 15:04 74-83-92.0
2-Butanone (MEK)ND ug/L 1 12/11/11 15:04 78-93-35.0
Carbon tetrachloride ND ug/L 1 12/11/11 15:04 56-23-51.0
Chlorobenzene ND ug/L 1 12/11/11 15:04 108-90-71.0
Chloroethane ND ug/L 1 12/11/11 15:04 75-00-31.0
Chloroform ND ug/L 1 12/11/11 15:04 67-66-31.0
Chloromethane ND ug/L 1 12/11/11 15:04 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/11/11 15:04 95-49-81.0
4-Chlorotoluene ND ug/L 1 12/11/11 15:04 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 12/11/11 15:04 96-12-85.0
Dibromochloromethane ND ug/L 1 12/11/11 15:04 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 12/11/11 15:04 106-93-41.0
Dibromomethane ND ug/L 1 12/11/11 15:04 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 12/11/11 15:04 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 12/11/11 15:04 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 12/11/11 15:04 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 12/11/11 15:04 75-71-81.0
1,1-Dichloroethane ND ug/L 1 12/11/11 15:04 75-34-31.0
1,2-Dichloroethane ND ug/L 1 12/11/11 15:04 107-06-21.0
1,1-Dichloroethene ND ug/L 1 12/11/11 15:04 75-35-41.0
cis-1,2-Dichloroethene 187 ug/L 1 12/11/11 15:04 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 12/11/11 15:04 156-60-51.0
1,2-Dichloropropane ND ug/L 1 12/11/11 15:04 78-87-51.0
1,3-Dichloropropane ND ug/L 1 12/11/11 15:04 142-28-91.0
2,2-Dichloropropane ND ug/L 1 12/11/11 15:04 594-20-71.0
1,1-Dichloropropene ND ug/L 1 12/11/11 15:04 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 12/11/11 15:04 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 12/11/11 15:04 10061-02-61.0
Diisopropyl ether ND ug/L 1 12/11/11 15:04 108-20-31.0
Ethylbenzene ND ug/L 1 12/11/11 15:04 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 12/11/11 15:04 87-68-31.0
2-Hexanone ND ug/L 1 12/11/11 15:04 591-78-65.0
p-Isopropyltoluene ND ug/L 1 12/11/11 15:04 99-87-61.0
Methylene Chloride ND ug/L 1 12/11/11 15:04 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 12/11/11 15:04 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 12/11/11 15:04 1634-04-41.0
Naphthalene ND ug/L 1 12/11/11 15:04 91-20-31.0
Styrene ND ug/L 1 12/11/11 15:04 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 12/11/11 15:04 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 12/11/11 15:04 79-34-51.0
Tetrachloroethene 60.8 ug/L 1 12/11/11 15:04 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 27 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-15 Lab ID: 92107636008 Collected: 12/02/11 13:14 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 12/11/11 15:04 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 12/11/11 15:04 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 12/11/11 15:04 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 12/11/11 15:04 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 12/11/11 15:04 79-00-51.0
Trichloroethene 80.3 ug/L 1 12/11/11 15:04 79-01-61.0
Trichlorofluoromethane ND ug/L 1 12/11/11 15:04 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/11/11 15:04 96-18-41.0
Vinyl acetate ND ug/L 1 12/11/11 15:04 108-05-42.0
Vinyl chloride ND ug/L 1 12/11/11 15:04 75-01-41.0
Xylene (Total)ND ug/L 1 12/11/11 15:04 1330-20-72.0
m&p-Xylene ND ug/L 1 12/11/11 15:04 179601-23-12.0
o-Xylene ND ug/L 1 12/11/11 15:04 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)93 %1 12/11/11 15:04 460-00-470-130
Dibromofluoromethane (S)107 %1 12/11/11 15:04 1868-53-770-130
1,2-Dichloroethane-d4 (S)110 %1 12/11/11 15:04 17060-07-070-130
Toluene-d8 (S)97 %1 12/11/11 15:04 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 28 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-10 Lab ID: 92107636009 Collected: 12/02/11 13:46 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 12/09/11 07:49 67-64-125.0
Benzene ND ug/L 1 12/09/11 07:49 71-43-21.0
Bromobenzene ND ug/L 1 12/09/11 07:49 108-86-11.0
Bromochloromethane ND ug/L 1 12/09/11 07:49 74-97-51.0
Bromodichloromethane ND ug/L 1 12/09/11 07:49 75-27-41.0
Bromoform ND ug/L 1 12/09/11 07:49 75-25-21.0
Bromomethane ND ug/L 1 12/09/11 07:49 74-83-92.0
2-Butanone (MEK)ND ug/L 1 12/09/11 07:49 78-93-35.0
Carbon tetrachloride ND ug/L 1 12/09/11 07:49 56-23-51.0
Chlorobenzene ND ug/L 1 12/09/11 07:49 108-90-71.0
Chloroethane ND ug/L 1 12/09/11 07:49 75-00-31.0
Chloroform ND ug/L 1 12/09/11 07:49 67-66-31.0
Chloromethane ND ug/L 1 12/09/11 07:49 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/09/11 07:49 95-49-81.0
4-Chlorotoluene ND ug/L 1 12/09/11 07:49 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 12/09/11 07:49 96-12-85.0
Dibromochloromethane ND ug/L 1 12/09/11 07:49 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 12/09/11 07:49 106-93-41.0
Dibromomethane ND ug/L 1 12/09/11 07:49 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 12/09/11 07:49 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 12/09/11 07:49 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 12/09/11 07:49 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 12/09/11 07:49 75-71-81.0
1,1-Dichloroethane ND ug/L 1 12/09/11 07:49 75-34-31.0
1,2-Dichloroethane ND ug/L 1 12/09/11 07:49 107-06-21.0
1,1-Dichloroethene ND ug/L 1 12/09/11 07:49 75-35-41.0
cis-1,2-Dichloroethene 7.8 ug/L 1 12/09/11 07:49 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 12/09/11 07:49 156-60-51.0
1,2-Dichloropropane ND ug/L 1 12/09/11 07:49 78-87-51.0
1,3-Dichloropropane ND ug/L 1 12/09/11 07:49 142-28-91.0
2,2-Dichloropropane ND ug/L 1 12/09/11 07:49 594-20-71.0
1,1-Dichloropropene ND ug/L 1 12/09/11 07:49 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 12/09/11 07:49 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 12/09/11 07:49 10061-02-61.0
Diisopropyl ether 8.2 ug/L 1 12/09/11 07:49 108-20-31.0
Ethylbenzene ND ug/L 1 12/09/11 07:49 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 12/09/11 07:49 87-68-31.0
2-Hexanone ND ug/L 1 12/09/11 07:49 591-78-65.0
p-Isopropyltoluene ND ug/L 1 12/09/11 07:49 99-87-61.0
Methylene Chloride ND ug/L 1 12/09/11 07:49 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 12/09/11 07:49 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 12/09/11 07:49 1634-04-41.0
Naphthalene ND ug/L 1 12/09/11 07:49 91-20-31.0
Styrene ND ug/L 1 12/09/11 07:49 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 12/09/11 07:49 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 12/09/11 07:49 79-34-51.0
Tetrachloroethene 7.3 ug/L 1 12/09/11 07:49 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 29 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-10 Lab ID: 92107636009 Collected: 12/02/11 13:46 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 12/09/11 07:49 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 12/09/11 07:49 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 12/09/11 07:49 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 12/09/11 07:49 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 12/09/11 07:49 79-00-51.0
Trichloroethene 13.2 ug/L 1 12/09/11 07:49 79-01-61.0
Trichlorofluoromethane ND ug/L 1 12/09/11 07:49 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/09/11 07:49 96-18-41.0
Vinyl acetate ND ug/L 1 12/09/11 07:49 108-05-42.0
Vinyl chloride ND ug/L 1 12/09/11 07:49 75-01-41.0
Xylene (Total)ND ug/L 1 12/09/11 07:49 1330-20-72.0
m&p-Xylene ND ug/L 1 12/09/11 07:49 179601-23-12.0
o-Xylene ND ug/L 1 12/09/11 07:49 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)93 %1 12/09/11 07:49 460-00-470-130
Dibromofluoromethane (S)106 %1 12/09/11 07:49 1868-53-770-130
1,2-Dichloroethane-d4 (S)105 %1 12/09/11 07:49 17060-07-070-130
Toluene-d8 (S)97 %1 12/09/11 07:49 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 30 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-12 Lab ID: 92107636010 Collected: 12/02/11 14:26 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 12/09/11 08:14 67-64-125.0
Benzene ND ug/L 1 12/09/11 08:14 71-43-21.0
Bromobenzene ND ug/L 1 12/09/11 08:14 108-86-11.0
Bromochloromethane ND ug/L 1 12/09/11 08:14 74-97-51.0
Bromodichloromethane ND ug/L 1 12/09/11 08:14 75-27-41.0
Bromoform ND ug/L 1 12/09/11 08:14 75-25-21.0
Bromomethane ND ug/L 1 12/09/11 08:14 74-83-92.0
2-Butanone (MEK)ND ug/L 1 12/09/11 08:14 78-93-35.0
Carbon tetrachloride ND ug/L 1 12/09/11 08:14 56-23-51.0
Chlorobenzene ND ug/L 1 12/09/11 08:14 108-90-71.0
Chloroethane ND ug/L 1 12/09/11 08:14 75-00-31.0
Chloroform ND ug/L 1 12/09/11 08:14 67-66-31.0
Chloromethane ND ug/L 1 12/09/11 08:14 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/09/11 08:14 95-49-81.0
4-Chlorotoluene ND ug/L 1 12/09/11 08:14 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 12/09/11 08:14 96-12-85.0
Dibromochloromethane ND ug/L 1 12/09/11 08:14 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 12/09/11 08:14 106-93-41.0
Dibromomethane ND ug/L 1 12/09/11 08:14 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 12/09/11 08:14 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 12/09/11 08:14 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 12/09/11 08:14 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 12/09/11 08:14 75-71-81.0
1,1-Dichloroethane ND ug/L 1 12/09/11 08:14 75-34-31.0
1,2-Dichloroethane ND ug/L 1 12/09/11 08:14 107-06-21.0
1,1-Dichloroethene ND ug/L 1 12/09/11 08:14 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 12/09/11 08:14 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 12/09/11 08:14 156-60-51.0
1,2-Dichloropropane ND ug/L 1 12/09/11 08:14 78-87-51.0
1,3-Dichloropropane ND ug/L 1 12/09/11 08:14 142-28-91.0
2,2-Dichloropropane ND ug/L 1 12/09/11 08:14 594-20-71.0
1,1-Dichloropropene ND ug/L 1 12/09/11 08:14 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 12/09/11 08:14 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 12/09/11 08:14 10061-02-61.0
Diisopropyl ether ND ug/L 1 12/09/11 08:14 108-20-31.0
Ethylbenzene ND ug/L 1 12/09/11 08:14 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 12/09/11 08:14 87-68-31.0
2-Hexanone ND ug/L 1 12/09/11 08:14 591-78-65.0
p-Isopropyltoluene ND ug/L 1 12/09/11 08:14 99-87-61.0
Methylene Chloride ND ug/L 1 12/09/11 08:14 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 12/09/11 08:14 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 12/09/11 08:14 1634-04-41.0
Naphthalene ND ug/L 1 12/09/11 08:14 91-20-31.0
Styrene ND ug/L 1 12/09/11 08:14 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 12/09/11 08:14 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 12/09/11 08:14 79-34-51.0
Tetrachloroethene ND ug/L 1 12/09/11 08:14 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 31 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-12 Lab ID: 92107636010 Collected: 12/02/11 14:26 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 12/09/11 08:14 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 12/09/11 08:14 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 12/09/11 08:14 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 12/09/11 08:14 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 12/09/11 08:14 79-00-51.0
Trichloroethene ND ug/L 1 12/09/11 08:14 79-01-61.0
Trichlorofluoromethane ND ug/L 1 12/09/11 08:14 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/09/11 08:14 96-18-41.0
Vinyl acetate ND ug/L 1 12/09/11 08:14 108-05-42.0
Vinyl chloride ND ug/L 1 12/09/11 08:14 75-01-41.0
Xylene (Total)ND ug/L 1 12/09/11 08:14 1330-20-72.0
m&p-Xylene ND ug/L 1 12/09/11 08:14 179601-23-12.0
o-Xylene ND ug/L 1 12/09/11 08:14 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)93 %1 12/09/11 08:14 460-00-470-130
Dibromofluoromethane (S)109 %1 12/09/11 08:14 1868-53-770-130
1,2-Dichloroethane-d4 (S)106 %1 12/09/11 08:14 17060-07-070-130
Toluene-d8 (S)94 %1 12/09/11 08:14 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 32 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-9 Lab ID: 92107636011 Collected: 12/02/11 15:06 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 2 12/09/11 12:28 67-64-150.0
Benzene ND ug/L 2 12/09/11 12:28 71-43-22.0
Bromobenzene ND ug/L 2 12/09/11 12:28 108-86-12.0
Bromochloromethane ND ug/L 2 12/09/11 12:28 74-97-52.0
Bromodichloromethane ND ug/L 2 12/09/11 12:28 75-27-42.0
Bromoform ND ug/L 2 12/09/11 12:28 75-25-22.0
Bromomethane ND ug/L 2 12/09/11 12:28 74-83-94.0
2-Butanone (MEK)ND ug/L 2 12/09/11 12:28 78-93-310.0
Carbon tetrachloride ND ug/L 2 12/09/11 12:28 56-23-52.0
Chlorobenzene ND ug/L 2 12/09/11 12:28 108-90-72.0
Chloroethane ND ug/L 2 12/09/11 12:28 75-00-32.0
Chloroform ND ug/L 2 12/09/11 12:28 67-66-32.0
Chloromethane ND ug/L 2 12/09/11 12:28 74-87-32.0
2-Chlorotoluene ND ug/L 2 12/09/11 12:28 95-49-82.0
4-Chlorotoluene ND ug/L 2 12/09/11 12:28 106-43-42.0
1,2-Dibromo-3-chloropropane ND ug/L 2 12/09/11 12:28 96-12-810.0
Dibromochloromethane ND ug/L 2 12/09/11 12:28 124-48-12.0
1,2-Dibromoethane (EDB)ND ug/L 2 12/09/11 12:28 106-93-42.0
Dibromomethane ND ug/L 2 12/09/11 12:28 74-95-32.0
1,2-Dichlorobenzene ND ug/L 2 12/09/11 12:28 95-50-12.0
1,3-Dichlorobenzene ND ug/L 2 12/09/11 12:28 541-73-12.0
1,4-Dichlorobenzene ND ug/L 2 12/09/11 12:28 106-46-72.0
Dichlorodifluoromethane ND ug/L 2 12/09/11 12:28 75-71-82.0
1,1-Dichloroethane ND ug/L 2 12/09/11 12:28 75-34-32.0
1,2-Dichloroethane ND ug/L 2 12/09/11 12:28 107-06-22.0
1,1-Dichloroethene ND ug/L 2 12/09/11 12:28 75-35-42.0
cis-1,2-Dichloroethene 45.1 ug/L 2 12/09/11 12:28 156-59-22.0
trans-1,2-Dichloroethene 6.6 ug/L 2 12/09/11 12:28 156-60-52.0
1,2-Dichloropropane ND ug/L 2 12/09/11 12:28 78-87-52.0
1,3-Dichloropropane ND ug/L 2 12/09/11 12:28 142-28-92.0
2,2-Dichloropropane ND ug/L 2 12/09/11 12:28 594-20-72.0
1,1-Dichloropropene ND ug/L 2 12/09/11 12:28 563-58-62.0
cis-1,3-Dichloropropene ND ug/L 2 12/09/11 12:28 10061-01-52.0
trans-1,3-Dichloropropene ND ug/L 2 12/09/11 12:28 10061-02-62.0
Diisopropyl ether ND ug/L 2 12/09/11 12:28 108-20-32.0
Ethylbenzene ND ug/L 2 12/09/11 12:28 100-41-42.0
Hexachloro-1,3-butadiene ND ug/L 2 12/09/11 12:28 87-68-32.0
2-Hexanone ND ug/L 2 12/09/11 12:28 591-78-610.0
p-Isopropyltoluene ND ug/L 2 12/09/11 12:28 99-87-62.0
Methylene Chloride ND ug/L 2 12/09/11 12:28 75-09-24.0
4-Methyl-2-pentanone (MIBK)ND ug/L 2 12/09/11 12:28 108-10-110.0
Methyl-tert-butyl ether ND ug/L 2 12/09/11 12:28 1634-04-42.0
Naphthalene ND ug/L 2 12/09/11 12:28 91-20-32.0
Styrene ND ug/L 2 12/09/11 12:28 100-42-52.0
1,1,1,2-Tetrachloroethane ND ug/L 2 12/09/11 12:28 630-20-62.0
1,1,2,2-Tetrachloroethane ND ug/L 2 12/09/11 12:28 79-34-52.0
Tetrachloroethene 259 ug/L 2 12/09/11 12:28 127-18-42.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 33 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-9 Lab ID: 92107636011 Collected: 12/02/11 15:06 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 2 12/09/11 12:28 108-88-32.0
1,2,3-Trichlorobenzene ND ug/L 2 12/09/11 12:28 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 2 12/09/11 12:28 120-82-12.0
1,1,1-Trichloroethane ND ug/L 2 12/09/11 12:28 71-55-62.0
1,1,2-Trichloroethane ND ug/L 2 12/09/11 12:28 79-00-52.0
Trichloroethene 52.1 ug/L 2 12/09/11 12:28 79-01-62.0
Trichlorofluoromethane ND ug/L 2 12/09/11 12:28 75-69-42.0
1,2,3-Trichloropropane ND ug/L 2 12/09/11 12:28 96-18-42.0
Vinyl acetate ND ug/L 2 12/09/11 12:28 108-05-44.0
Vinyl chloride ND ug/L 2 12/09/11 12:28 75-01-42.0
Xylene (Total)ND ug/L 2 12/09/11 12:28 1330-20-74.0
m&p-Xylene ND ug/L 2 12/09/11 12:28 179601-23-14.0
o-Xylene ND ug/L 2 12/09/11 12:28 95-47-62.0
Surrogates
4-Bromofluorobenzene (S)97 %2 12/09/11 12:28 460-00-470-130
Dibromofluoromethane (S)110 %2 12/09/11 12:28 1868-53-770-130
1,2-Dichloroethane-d4 (S)107 %2 12/09/11 12:28 17060-07-070-130
Toluene-d8 (S)97 %2 12/09/11 12:28 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 34 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-3 Lab ID: 92107636012 Collected: 12/02/11 15:46 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 12/11/11 14:13 67-64-125.0
Benzene ND ug/L 1 12/11/11 14:13 71-43-21.0
Bromobenzene ND ug/L 1 12/11/11 14:13 108-86-11.0
Bromochloromethane ND ug/L 1 12/11/11 14:13 74-97-51.0
Bromodichloromethane ND ug/L 1 12/11/11 14:13 75-27-41.0
Bromoform ND ug/L 1 12/11/11 14:13 75-25-21.0
Bromomethane ND ug/L 1 12/11/11 14:13 74-83-92.0
2-Butanone (MEK)ND ug/L 1 12/11/11 14:13 78-93-35.0
Carbon tetrachloride ND ug/L 1 12/11/11 14:13 56-23-51.0
Chlorobenzene ND ug/L 1 12/11/11 14:13 108-90-71.0
Chloroethane ND ug/L 1 12/11/11 14:13 75-00-31.0
Chloroform ND ug/L 1 12/11/11 14:13 67-66-31.0
Chloromethane ND ug/L 1 12/11/11 14:13 74-87-31.0
2-Chlorotoluene ND ug/L 1 12/11/11 14:13 95-49-81.0
4-Chlorotoluene ND ug/L 1 12/11/11 14:13 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 12/11/11 14:13 96-12-85.0
Dibromochloromethane ND ug/L 1 12/11/11 14:13 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 12/11/11 14:13 106-93-41.0
Dibromomethane ND ug/L 1 12/11/11 14:13 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 12/11/11 14:13 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 12/11/11 14:13 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 12/11/11 14:13 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 12/11/11 14:13 75-71-81.0
1,1-Dichloroethane ND ug/L 1 12/11/11 14:13 75-34-31.0
1,2-Dichloroethane ND ug/L 1 12/11/11 14:13 107-06-21.0
1,1-Dichloroethene ND ug/L 1 12/11/11 14:13 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 12/11/11 14:13 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 12/11/11 14:13 156-60-51.0
1,2-Dichloropropane ND ug/L 1 12/11/11 14:13 78-87-51.0
1,3-Dichloropropane ND ug/L 1 12/11/11 14:13 142-28-91.0
2,2-Dichloropropane ND ug/L 1 12/11/11 14:13 594-20-71.0
1,1-Dichloropropene ND ug/L 1 12/11/11 14:13 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 12/11/11 14:13 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 12/11/11 14:13 10061-02-61.0
Diisopropyl ether 1.5 ug/L 1 12/11/11 14:13 108-20-31.0
Ethylbenzene ND ug/L 1 12/11/11 14:13 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 12/11/11 14:13 87-68-31.0
2-Hexanone ND ug/L 1 12/11/11 14:13 591-78-65.0
p-Isopropyltoluene ND ug/L 1 12/11/11 14:13 99-87-61.0
Methylene Chloride ND ug/L 1 12/11/11 14:13 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 12/11/11 14:13 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 12/11/11 14:13 1634-04-41.0
Naphthalene ND ug/L 1 12/11/11 14:13 91-20-31.0
Styrene ND ug/L 1 12/11/11 14:13 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 12/11/11 14:13 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 12/11/11 14:13 79-34-51.0
Tetrachloroethene ND ug/L 1 12/11/11 14:13 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 35 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Sample: G-3 Lab ID: 92107636012 Collected: 12/02/11 15:46 Received: 12/02/11 16:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 12/11/11 14:13 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 12/11/11 14:13 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 12/11/11 14:13 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 12/11/11 14:13 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 12/11/11 14:13 79-00-51.0
Trichloroethene ND ug/L 1 12/11/11 14:13 79-01-61.0
Trichlorofluoromethane ND ug/L 1 12/11/11 14:13 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 12/11/11 14:13 96-18-41.0
Vinyl acetate ND ug/L 1 12/11/11 14:13 108-05-42.0
Vinyl chloride ND ug/L 1 12/11/11 14:13 75-01-41.0
Xylene (Total)ND ug/L 1 12/11/11 14:13 1330-20-72.0
m&p-Xylene ND ug/L 1 12/11/11 14:13 179601-23-12.0
o-Xylene ND ug/L 1 12/11/11 14:13 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)94 %1 12/11/11 14:13 460-00-470-130
Dibromofluoromethane (S)114 %1 12/11/11 14:13 1868-53-770-130
1,2-Dichloroethane-d4 (S)113 %1 12/11/11 14:13 17060-07-070-130
Toluene-d8 (S)94 %1 12/11/11 14:13 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 36 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/3907
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples: 92107636001, 92107636002, 92107636003, 92107636004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695577
Associated Lab Samples:92107636001, 92107636002, 92107636003, 92107636004
Matrix: Water
Analyzed
Mercury ug/L ND 0.20 12/08/11 11:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695578LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.22.5 90 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
695579MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107636001
695580
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M12.5 63 75-12563 1 252.5ND 1.6 1.6
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
695581MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107636002
695582
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M12.5 73 75-12573 1 252.5ND 1.9 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 37 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/9531
EPA 3010
EPA 6010
6010 MET
Associated Lab Samples: 92107636001, 92107636002, 92107636003, 92107636004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 696238
Associated Lab Samples:92107636001, 92107636002, 92107636003, 92107636004
Matrix: Water
Analyzed
Antimony ug/L ND 5.0 12/08/11 15:53
Arsenic ug/L ND 5.0 12/08/11 15:53
Beryllium ug/L ND 1.0 12/08/11 15:53
Cadmium ug/L ND 1.0 12/08/11 15:53
Chromium ug/L ND 5.0 12/08/11 15:53
Copper ug/L ND 5.0 12/08/11 15:53
Lead ug/L ND 5.0 12/08/11 15:53
Manganese ug/L ND 5.0 12/08/11 15:53
Nickel ug/L ND 5.0 12/08/11 15:53
Selenium ug/L ND 10.0 12/08/11 15:53
Silver ug/L ND 5.0 12/08/11 15:53
Thallium ug/L ND 10.0 12/08/11 15:53
Zinc ug/L ND 10.0 12/08/11 15:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
696239LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 472500 94 80-120
Arsenic ug/L 477500 95 80-120
Beryllium ug/L 470500 94 80-120
Cadmium ug/L 478500 96 80-120
Chromium ug/L 480500 96 80-120
Copper ug/L 469500 94 80-120
Lead ug/L 478500 96 80-120
Manganese ug/L 465500 93 80-120
Nickel ug/L 473500 95 80-120
Selenium ug/L 475500 95 80-120
Silver ug/L 239250 96 80-120
Thallium ug/L 466500 93 80-120
Zinc ug/L 480500 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
696240MATRIX SPIKE SAMPLE:
MSSpike
Result
92107636001
Antimony ug/L 500500 100 75-125ND
Arsenic ug/L 515500 103 75-125ND
Beryllium ug/L 479500 96 75-125ND
Cadmium ug/L 476500 95 75-125ND
Chromium ug/L 485500 97 75-125ND
Copper ug/L 493500 98 75-125ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 38 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
696240MATRIX SPIKE SAMPLE:
MSSpike
Result
92107636001
Lead ug/L 461500 92 75-125ND
Manganese ug/L 807500 91 75-125350
Nickel ug/L 471500 93 75-125ND
Selenium ug/L 492500 98 75-125ND
Silver ug/L 248250 99 75-125ND
Thallium ug/L 445500 88 75-125ND
Zinc ug/L 503500 100 75-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92107636002
696241SAMPLE DUPLICATE:
Antimony ug/L ND 20ND
Arsenic ug/L ND 20ND
Beryllium ug/L ND 20ND
Cadmium ug/L ND 20ND
Chromium ug/L ND 20ND
Copper ug/L 2.9J 20ND
Lead ug/L ND 20ND
Manganese ug/L 276 3 20269
Nickel ug/L 66.7 3 2064.9
Selenium ug/L ND 20ND
Silver ug/L ND 20ND
Thallium ug/L ND 20ND
Zinc ug/L ND 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 39 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/17570
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92107636004, 92107636006, 92107636009, 92107636010, 92107636011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 697290
Associated Lab Samples:92107636004, 92107636006, 92107636009, 92107636010, 92107636011
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 12/09/11 01:53
1,1,1-Trichloroethane ug/L ND 1.0 12/09/11 01:53
1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/09/11 01:53
1,1,2-Trichloroethane ug/L ND 1.0 12/09/11 01:53
1,1-Dichloroethane ug/L ND 1.0 12/09/11 01:53
1,1-Dichloroethene ug/L ND 1.0 12/09/11 01:53
1,1-Dichloropropene ug/L ND 1.0 12/09/11 01:53
1,2,3-Trichlorobenzene ug/L ND 1.0 12/09/11 01:53
1,2,3-Trichloropropane ug/L ND 1.0 12/09/11 01:53
1,2,4-Trichlorobenzene ug/L ND 1.0 12/09/11 01:53
1,2-Dibromo-3-chloropropane ug/L ND 5.0 12/09/11 01:53
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/09/11 01:53
1,2-Dichlorobenzene ug/L ND 1.0 12/09/11 01:53
1,2-Dichloroethane ug/L ND 1.0 12/09/11 01:53
1,2-Dichloropropane ug/L ND 1.0 12/09/11 01:53
1,3-Dichlorobenzene ug/L ND 1.0 12/09/11 01:53
1,3-Dichloropropane ug/L ND 1.0 12/09/11 01:53
1,4-Dichlorobenzene ug/L ND 1.0 12/09/11 01:53
2,2-Dichloropropane ug/L ND 1.0 12/09/11 01:53
2-Butanone (MEK)ug/L ND 5.0 12/09/11 01:53
2-Chlorotoluene ug/L ND 1.0 12/09/11 01:53
2-Hexanone ug/L ND 5.0 12/09/11 01:53
4-Chlorotoluene ug/L ND 1.0 12/09/11 01:53
4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 12/09/11 01:53
Acetone ug/L ND 25.0 12/09/11 01:53
Benzene ug/L ND 1.0 12/09/11 01:53
Bromobenzene ug/L ND 1.0 12/09/11 01:53
Bromochloromethane ug/L ND 1.0 12/09/11 01:53
Bromodichloromethane ug/L ND 1.0 12/09/11 01:53
Bromoform ug/L ND 1.0 12/09/11 01:53
Bromomethane ug/L ND 2.0 12/09/11 01:53
Carbon tetrachloride ug/L ND 1.0 12/09/11 01:53
Chlorobenzene ug/L ND 1.0 12/09/11 01:53
Chloroethane ug/L ND 1.0 12/09/11 01:53
Chloroform ug/L ND 1.0 12/09/11 01:53
Chloromethane ug/L ND 1.0 12/09/11 01:53
cis-1,2-Dichloroethene ug/L ND 1.0 12/09/11 01:53
cis-1,3-Dichloropropene ug/L ND 1.0 12/09/11 01:53
Dibromochloromethane ug/L ND 1.0 12/09/11 01:53
Dibromomethane ug/L ND 1.0 12/09/11 01:53
Dichlorodifluoromethane ug/L ND 1.0 12/09/11 01:53
Diisopropyl ether ug/L ND 1.0 12/09/11 01:53
Ethylbenzene ug/L ND 1.0 12/09/11 01:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 40 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 697290
Associated Lab Samples:92107636004, 92107636006, 92107636009, 92107636010, 92107636011
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 12/09/11 01:53
m&p-Xylene ug/L ND 2.0 12/09/11 01:53
Methyl-tert-butyl ether ug/L ND 1.0 12/09/11 01:53
Methylene Chloride ug/L ND 2.0 12/09/11 01:53
Naphthalene ug/L ND 1.0 12/09/11 01:53
o-Xylene ug/L ND 1.0 12/09/11 01:53
p-Isopropyltoluene ug/L ND 1.0 12/09/11 01:53
Styrene ug/L ND 1.0 12/09/11 01:53
Tetrachloroethene ug/L ND 1.0 12/09/11 01:53
Toluene ug/L ND 1.0 12/09/11 01:53
trans-1,2-Dichloroethene ug/L ND 1.0 12/09/11 01:53
trans-1,3-Dichloropropene ug/L ND 1.0 12/09/11 01:53
Trichloroethene ug/L ND 1.0 12/09/11 01:53
Trichlorofluoromethane ug/L ND 1.0 12/09/11 01:53
Vinyl acetate ug/L ND 2.0 12/09/11 01:53
Vinyl chloride ug/L ND 1.0 12/09/11 01:53
Xylene (Total)ug/L ND 2.0 12/09/11 01:53
1,2-Dichloroethane-d4 (S)%102 70-130 12/09/11 01:53
4-Bromofluorobenzene (S)%95 70-130 12/09/11 01:53
Dibromofluoromethane (S)%105 70-130 12/09/11 01:53
Toluene-d8 (S)%94 70-130 12/09/11 01:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
697291LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.250 104 70-130
1,1,1-Trichloroethane ug/L 44.250 88 70-130
1,1,2,2-Tetrachloroethane ug/L 49.250 98 70-130
1,1,2-Trichloroethane ug/L 51.550 103 70-130
1,1-Dichloroethane ug/L 41.650 83 70-130
1,1-Dichloroethene ug/L 39.650 79 70-132
1,1-Dichloropropene ug/L 41.950 84 70-130
1,2,3-Trichlorobenzene ug/L 53.350 107 70-135
1,2,3-Trichloropropane ug/L 46.950 94 70-130
1,2,4-Trichlorobenzene ug/L 51.850 104 70-134
1,2-Dibromo-3-chloropropane ug/L 51.450 103 70-130
1,2-Dibromoethane (EDB)ug/L 47.850 96 70-130
1,2-Dichlorobenzene ug/L 52.450 105 70-130
1,2-Dichloroethane ug/L 44.550 89 70-130
1,2-Dichloropropane ug/L 46.150 92 70-130
1,3-Dichlorobenzene ug/L 50.550 101 70-130
1,3-Dichloropropane ug/L 46.250 92 70-130
1,4-Dichlorobenzene ug/L 51.150 102 70-130
2,2-Dichloropropane ug/L 35.850 72 58-145
2-Butanone (MEK)ug/L 81.4100 81 70-145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 41 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
697291LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorotoluene ug/L 51.150 102 70-130
2-Hexanone ug/L 93.5 F310093 70-144
4-Chlorotoluene ug/L 51.850 104 70-130
4-Methyl-2-pentanone (MIBK) ug/L 103100 103 70-140
Acetone ug/L 90.2 F310090 50-175
Benzene ug/L 45.050 90 70-130
Bromobenzene ug/L 47.850 96 70-130
Bromochloromethane ug/L 44.050 88 70-130
Bromodichloromethane ug/L 51.650 103 70-130
Bromoform ug/L 45.550 91 70-130
Bromomethane ug/L 35.150 70 54-130
Carbon tetrachloride ug/L 55.150 110 70-132
Chlorobenzene ug/L 50.550 101 70-130
Chloroethane ug/L 37.850 76 64-134
Chloroform ug/L 46.150 92 70-130
Chloromethane ug/L 39.650 79 64-130
cis-1,2-Dichloroethene ug/L 41.650 83 70-131
cis-1,3-Dichloropropene ug/L 49.450 99 70-130
Dibromochloromethane ug/L 52.350 105 70-130
Dibromomethane ug/L 49.850 100 70-131
Dichlorodifluoromethane ug/L 38.4 F35077 56-130
Diisopropyl ether ug/L 42.650 85 70-130
Ethylbenzene ug/L 50.350 101 70-130
Hexachloro-1,3-butadiene ug/L 48.350 97 70-130
m&p-Xylene ug/L 103100 103 70-130
Methyl-tert-butyl ether ug/L 45.350 91 70-130
Methylene Chloride ug/L 45.750 91 63-130
Naphthalene ug/L 48.950 98 70-138
o-Xylene ug/L 51.550 103 70-130
p-Isopropyltoluene ug/L 54.050 108 70-130
Styrene ug/L 52.950 106 70-130
Tetrachloroethene ug/L 45.550 91 70-130
Toluene ug/L 50.150 100 70-130
trans-1,2-Dichloroethene ug/L 39.850 80 70-130
trans-1,3-Dichloropropene ug/L 50.250 100 70-132
Trichloroethene ug/L 45.850 92 70-130
Trichlorofluoromethane ug/L 40.250 80 62-133
Vinyl acetate ug/L 41.8 L010042 66-157
Vinyl chloride ug/L 45.550 91 69-130
Xylene (Total)ug/L 154150 103 70-130
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%102 70-130
Dibromofluoromethane (S)%92 70-130
Toluene-d8 (S)%104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 42 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
697328MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107802007
697329
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 105 70-166104 0 30500.64J 53.0 52.9
Benzene ug/L 50 113 70-148115 1 3050ND56.5 57.4
Chlorobenzene ug/L 50 110 70-146112 2 3050ND55.1 56.0
Toluene ug/L 50 112 70-155114 2 3050ND55.9 57.0
Trichloroethene ug/L 50 113 69-151118 2 305063.0 119 122
1,2-Dichloroethane-d4 (S) %105 70-130105
4-Bromofluorobenzene (S) %99 70-13097
Dibromofluoromethane (S) %104 70-130103
Toluene-d8 (S)%102 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 43 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/17579
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92107636001, 92107636002, 92107636003, 92107636005, 92107636007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 697865
Associated Lab Samples:92107636001, 92107636002, 92107636003, 92107636005, 92107636007
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 12/09/11 15:03
1,1,1-Trichloroethane ug/L ND 1.0 12/09/11 15:03
1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/09/11 15:03
1,1,2-Trichloroethane ug/L ND 1.0 12/09/11 15:03
1,1-Dichloroethane ug/L ND 1.0 12/09/11 15:03
1,1-Dichloroethene ug/L ND 1.0 12/09/11 15:03
1,1-Dichloropropene ug/L ND 1.0 12/09/11 15:03
1,2,3-Trichlorobenzene ug/L ND 1.0 12/09/11 15:03
1,2,3-Trichloropropane ug/L ND 1.0 12/09/11 15:03
1,2,4-Trichlorobenzene ug/L ND 1.0 12/09/11 15:03
1,2-Dibromo-3-chloropropane ug/L ND 5.0 12/09/11 15:03
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/09/11 15:03
1,2-Dichlorobenzene ug/L ND 1.0 12/09/11 15:03
1,2-Dichloroethane ug/L ND 1.0 12/09/11 15:03
1,2-Dichloropropane ug/L ND 1.0 12/09/11 15:03
1,3-Dichlorobenzene ug/L ND 1.0 12/09/11 15:03
1,3-Dichloropropane ug/L ND 1.0 12/09/11 15:03
1,4-Dichlorobenzene ug/L ND 1.0 12/09/11 15:03
2,2-Dichloropropane ug/L ND 1.0 12/09/11 15:03
2-Butanone (MEK)ug/L ND 5.0 12/09/11 15:03
2-Chlorotoluene ug/L ND 1.0 12/09/11 15:03
2-Hexanone ug/L ND 5.0 12/09/11 15:03
4-Chlorotoluene ug/L ND 1.0 12/09/11 15:03
4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 12/09/11 15:03
Acetone ug/L ND 25.0 12/09/11 15:03
Benzene ug/L ND 1.0 12/09/11 15:03
Bromobenzene ug/L ND 1.0 12/09/11 15:03
Bromochloromethane ug/L ND 1.0 12/09/11 15:03
Bromodichloromethane ug/L ND 1.0 12/09/11 15:03
Bromoform ug/L ND 1.0 12/09/11 15:03
Bromomethane ug/L ND 2.0 12/09/11 15:03
Carbon tetrachloride ug/L ND 1.0 12/09/11 15:03
Chlorobenzene ug/L ND 1.0 12/09/11 15:03
Chloroethane ug/L ND 1.0 12/09/11 15:03
Chloroform ug/L ND 1.0 12/09/11 15:03
Chloromethane ug/L ND 1.0 12/09/11 15:03
cis-1,2-Dichloroethene ug/L ND 1.0 12/09/11 15:03
cis-1,3-Dichloropropene ug/L ND 1.0 12/09/11 15:03
Dibromochloromethane ug/L ND 1.0 12/09/11 15:03
Dibromomethane ug/L ND 1.0 12/09/11 15:03
Dichlorodifluoromethane ug/L ND 1.0 12/09/11 15:03
Diisopropyl ether ug/L ND 1.0 12/09/11 15:03
Ethylbenzene ug/L ND 1.0 12/09/11 15:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 44 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 697865
Associated Lab Samples:92107636001, 92107636002, 92107636003, 92107636005, 92107636007
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 12/09/11 15:03
m&p-Xylene ug/L ND 2.0 12/09/11 15:03
Methyl-tert-butyl ether ug/L ND 1.0 12/09/11 15:03
Methylene Chloride ug/L ND 2.0 12/09/11 15:03
Naphthalene ug/L ND 1.0 12/09/11 15:03
o-Xylene ug/L ND 1.0 12/09/11 15:03
p-Isopropyltoluene ug/L ND 1.0 12/09/11 15:03
Styrene ug/L ND 1.0 12/09/11 15:03
Tetrachloroethene ug/L ND 1.0 12/09/11 15:03
Toluene ug/L ND 1.0 12/09/11 15:03
trans-1,2-Dichloroethene ug/L ND 1.0 12/09/11 15:03
trans-1,3-Dichloropropene ug/L ND 1.0 12/09/11 15:03
Trichloroethene ug/L ND 1.0 12/09/11 15:03
Trichlorofluoromethane ug/L ND 1.0 12/09/11 15:03
Vinyl acetate ug/L ND 2.0 12/09/11 15:03
Vinyl chloride ug/L ND 1.0 12/09/11 15:03
Xylene (Total)ug/L ND 2.0 12/09/11 15:03
1,2-Dichloroethane-d4 (S)%105 70-130 12/09/11 15:03
4-Bromofluorobenzene (S)%95 70-130 12/09/11 15:03
Dibromofluoromethane (S)%110 70-130 12/09/11 15:03
Toluene-d8 (S)%93 70-130 12/09/11 15:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
697866LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 58.450 117 70-130
1,1,1-Trichloroethane ug/L 52.750 105 70-130
1,1,2,2-Tetrachloroethane ug/L 49.350 99 70-130
1,1,2-Trichloroethane ug/L 50.850 102 70-130
1,1-Dichloroethane ug/L 48.850 98 70-130
1,1-Dichloroethene ug/L 50.950 102 70-132
1,1-Dichloropropene ug/L 52.250 104 70-130
1,2,3-Trichlorobenzene ug/L 55.650 111 70-135
1,2,3-Trichloropropane ug/L 47.850 96 70-130
1,2,4-Trichlorobenzene ug/L 56.150 112 70-134
1,2-Dibromo-3-chloropropane ug/L 55.850 112 70-130
1,2-Dibromoethane (EDB)ug/L 54.550 109 70-130
1,2-Dichlorobenzene ug/L 55.950 112 70-130
1,2-Dichloroethane ug/L 52.750 105 70-130
1,2-Dichloropropane ug/L 52.650 105 70-130
1,3-Dichlorobenzene ug/L 53.750 107 70-130
1,3-Dichloropropane ug/L 50.650 101 70-130
1,4-Dichlorobenzene ug/L 54.550 109 70-130
2,2-Dichloropropane ug/L 53.450 107 58-145
2-Butanone (MEK)ug/L 85.0 F310085 70-145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 45 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
697866LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorotoluene ug/L 55.550 111 70-130
2-Hexanone ug/L 98.7100 99 70-144
4-Chlorotoluene ug/L 55.250 110 70-130
4-Methyl-2-pentanone (MIBK) ug/L 91.7100 92 70-140
Acetone ug/L 94.2 F310094 50-175
Benzene ug/L 52.650 105 70-130
Bromobenzene ug/L 49.850 100 70-130
Bromochloromethane ug/L 53.050 106 70-130
Bromodichloromethane ug/L 58.950 118 70-130
Bromoform ug/L 50.450 101 70-130
Bromomethane ug/L 30.550 61 54-130
Carbon tetrachloride ug/L 60.650 121 70-132
Chlorobenzene ug/L 54.950 110 70-130
Chloroethane ug/L 28.7 L05057 64-134
Chloroform ug/L 56.250 112 70-130
Chloromethane ug/L 42.450 85 64-130
cis-1,2-Dichloroethene ug/L 49.250 98 70-131
cis-1,3-Dichloropropene ug/L 56.450 113 70-130
Dibromochloromethane ug/L 59.850 120 70-130
Dibromomethane ug/L 56.450 113 70-131
Dichlorodifluoromethane ug/L 51.3 F350103 56-130
Diisopropyl ether ug/L 45.950 92 70-130
Ethylbenzene ug/L 54.350 109 70-130
Hexachloro-1,3-butadiene ug/L 55.650 111 70-130
m&p-Xylene ug/L 111100 111 70-130
Methyl-tert-butyl ether ug/L 49.750 99 70-130
Methylene Chloride ug/L 51.650 103 63-130
Naphthalene ug/L 51.550 103 70-138
o-Xylene ug/L 54.650 109 70-130
p-Isopropyltoluene ug/L 58.950 118 70-130
Styrene ug/L 55.650 111 70-130
Tetrachloroethene ug/L 53.950 108 70-130
Toluene ug/L 53.550 107 70-130
trans-1,2-Dichloroethene ug/L 49.250 98 70-130
trans-1,3-Dichloropropene ug/L 54.950 110 70-132
Trichloroethene ug/L 54.950 110 70-130
Trichlorofluoromethane ug/L 52.150 104 62-133
Vinyl acetate ug/L 75.4 F310075 66-157
Vinyl chloride ug/L 50.650 101 69-130
Xylene (Total)ug/L 166150 110 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%99 70-130
Dibromofluoromethane (S)%98 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 46 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
697867MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107584004
697868
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 111 70-166112 1 3050ND55.4 56.1
Benzene ug/L 50 112 70-148112 0 3050ND55.9 56.1
Chlorobenzene ug/L 50 114 70-146111 3 3050ND57.1 55.5
Toluene ug/L 50 105 70-155107 1 3050ND52.7 53.5
Trichloroethene ug/L 50 116 69-151117 1 3050ND58.0 58.5
1,2-Dichloroethane-d4 (S) %106 70-130110
4-Bromofluorobenzene (S) %105 70-13098
Dibromofluoromethane (S) %107 70-130112
Toluene-d8 (S)%93 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 47 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/17597
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92107636008, 92107636012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 698249
Associated Lab Samples:92107636008, 92107636012
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 12/11/11 12:31
1,1,1-Trichloroethane ug/L ND 1.0 12/11/11 12:31
1,1,2,2-Tetrachloroethane ug/L ND 1.0 12/11/11 12:31
1,1,2-Trichloroethane ug/L ND 1.0 12/11/11 12:31
1,1-Dichloroethane ug/L ND 1.0 12/11/11 12:31
1,1-Dichloroethene ug/L ND 1.0 12/11/11 12:31
1,1-Dichloropropene ug/L ND 1.0 12/11/11 12:31
1,2,3-Trichlorobenzene ug/L ND 1.0 12/11/11 12:31
1,2,3-Trichloropropane ug/L ND 1.0 12/11/11 12:31
1,2,4-Trichlorobenzene ug/L ND 1.0 12/11/11 12:31
1,2-Dibromo-3-chloropropane ug/L ND 5.0 12/11/11 12:31
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/11/11 12:31
1,2-Dichlorobenzene ug/L ND 1.0 12/11/11 12:31
1,2-Dichloroethane ug/L ND 1.0 12/11/11 12:31
1,2-Dichloropropane ug/L ND 1.0 12/11/11 12:31
1,3-Dichlorobenzene ug/L ND 1.0 12/11/11 12:31
1,3-Dichloropropane ug/L ND 1.0 12/11/11 12:31
1,4-Dichlorobenzene ug/L ND 1.0 12/11/11 12:31
2,2-Dichloropropane ug/L ND 1.0 12/11/11 12:31
2-Butanone (MEK)ug/L ND 5.0 12/11/11 12:31
2-Chlorotoluene ug/L ND 1.0 12/11/11 12:31
2-Hexanone ug/L ND 5.0 12/11/11 12:31
4-Chlorotoluene ug/L ND 1.0 12/11/11 12:31
4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 12/11/11 12:31
Acetone ug/L ND 25.0 12/11/11 12:31
Benzene ug/L ND 1.0 12/11/11 12:31
Bromobenzene ug/L ND 1.0 12/11/11 12:31
Bromochloromethane ug/L ND 1.0 12/11/11 12:31
Bromodichloromethane ug/L ND 1.0 12/11/11 12:31
Bromoform ug/L ND 1.0 12/11/11 12:31
Bromomethane ug/L ND 2.0 12/11/11 12:31
Carbon tetrachloride ug/L ND 1.0 12/11/11 12:31
Chlorobenzene ug/L ND 1.0 12/11/11 12:31
Chloroethane ug/L ND 1.0 12/11/11 12:31
Chloroform ug/L ND 1.0 12/11/11 12:31
Chloromethane ug/L ND 1.0 12/11/11 12:31
cis-1,2-Dichloroethene ug/L ND 1.0 12/11/11 12:31
cis-1,3-Dichloropropene ug/L ND 1.0 12/11/11 12:31
Dibromochloromethane ug/L ND 1.0 12/11/11 12:31
Dibromomethane ug/L ND 1.0 12/11/11 12:31
Dichlorodifluoromethane ug/L ND 1.0 12/11/11 12:31
Diisopropyl ether ug/L ND 1.0 12/11/11 12:31
Ethylbenzene ug/L ND 1.0 12/11/11 12:31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 48 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 698249
Associated Lab Samples:92107636008, 92107636012
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 12/11/11 12:31
m&p-Xylene ug/L ND 2.0 12/11/11 12:31
Methyl-tert-butyl ether ug/L ND 1.0 12/11/11 12:31
Methylene Chloride ug/L ND 2.0 12/11/11 12:31
Naphthalene ug/L ND 1.0 12/11/11 12:31
o-Xylene ug/L ND 1.0 12/11/11 12:31
p-Isopropyltoluene ug/L ND 1.0 12/11/11 12:31
Styrene ug/L ND 1.0 12/11/11 12:31
Tetrachloroethene ug/L ND 1.0 12/11/11 12:31
Toluene ug/L ND 1.0 12/11/11 12:31
trans-1,2-Dichloroethene ug/L ND 1.0 12/11/11 12:31
trans-1,3-Dichloropropene ug/L ND 1.0 12/11/11 12:31
Trichloroethene ug/L ND 1.0 12/11/11 12:31
Trichlorofluoromethane ug/L ND 1.0 12/11/11 12:31
Vinyl acetate ug/L ND 2.0 12/11/11 12:31
Vinyl chloride ug/L ND 1.0 12/11/11 12:31
Xylene (Total)ug/L ND 2.0 12/11/11 12:31
1,2-Dichloroethane-d4 (S)%110 70-130 12/11/11 12:31
4-Bromofluorobenzene (S)%95 70-130 12/11/11 12:31
Dibromofluoromethane (S)%114 70-130 12/11/11 12:31
Toluene-d8 (S)%89 70-130 12/11/11 12:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
698250LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.750 107 70-130
1,1,1-Trichloroethane ug/L 50.550 101 70-130
1,1,2,2-Tetrachloroethane ug/L 48.550 97 70-130
1,1,2-Trichloroethane ug/L 50.450 101 70-130
1,1-Dichloroethane ug/L 47.950 96 70-130
1,1-Dichloroethene ug/L 50.050 100 70-132
1,1-Dichloropropene ug/L 50.450 101 70-130
1,2,3-Trichlorobenzene ug/L 50.750 101 70-135
1,2,3-Trichloropropane ug/L 45.950 92 70-130
1,2,4-Trichlorobenzene ug/L 50.750 101 70-134
1,2-Dibromo-3-chloropropane ug/L 54.750 109 70-130
1,2-Dibromoethane (EDB)ug/L 51.750 103 70-130
1,2-Dichlorobenzene ug/L 51.750 103 70-130
1,2-Dichloroethane ug/L 52.450 105 70-130
1,2-Dichloropropane ug/L 52.050 104 70-130
1,3-Dichlorobenzene ug/L 50.850 102 70-130
1,3-Dichloropropane ug/L 49.250 98 70-130
1,4-Dichlorobenzene ug/L 50.650 101 70-130
2,2-Dichloropropane ug/L 51.550 103 58-145
2-Butanone (MEK)ug/L 99.8100 100 70-145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 49 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
698250LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorotoluene ug/L 53.950 108 70-130
2-Hexanone ug/L 106100 106 70-144
4-Chlorotoluene ug/L 53.850 108 70-130
4-Methyl-2-pentanone (MIBK) ug/L 101100 101 70-140
Acetone ug/L 117100 117 50-175
Benzene ug/L 49.950 100 70-130
Bromobenzene ug/L 52.650 105 70-130
Bromochloromethane ug/L 49.050 98 70-130
Bromodichloromethane ug/L 55.750 111 70-130
Bromoform ug/L 49.550 99 70-130
Bromomethane ug/L 34.550 69 54-130
Carbon tetrachloride ug/L 62.850 126 70-132
Chlorobenzene ug/L 51.350 103 70-130
Chloroethane ug/L 35.450 71 64-134
Chloroform ug/L 53.850 108 70-130
Chloromethane ug/L 51.650 103 64-130
cis-1,2-Dichloroethene ug/L 46.450 93 70-131
cis-1,3-Dichloropropene ug/L 55.150 110 70-130
Dibromochloromethane ug/L 55.250 110 70-130
Dibromomethane ug/L 51.050 102 70-131
Dichlorodifluoromethane ug/L 41.350 83 56-130
Diisopropyl ether ug/L 47.050 94 70-130
Ethylbenzene ug/L 51.350 103 70-130
Hexachloro-1,3-butadiene ug/L 52.150 104 70-130
m&p-Xylene ug/L 104100 104 70-130
Methyl-tert-butyl ether ug/L 47.350 95 70-130
Methylene Chloride ug/L 56.550 113 63-130
Naphthalene ug/L 55.250 110 70-138
o-Xylene ug/L 52.550 105 70-130
p-Isopropyltoluene ug/L 55.050 110 70-130
Styrene ug/L 53.050 106 70-130
Tetrachloroethene ug/L 49.450 99 70-130
Toluene ug/L 51.550 103 70-130
trans-1,2-Dichloroethene ug/L 48.250 96 70-130
trans-1,3-Dichloropropene ug/L 55.050 110 70-132
Trichloroethene ug/L 50.650 101 70-130
Trichlorofluoromethane ug/L 46.050 92 62-133
Vinyl acetate ug/L 77.0100 77 66-157
Vinyl chloride ug/L 50.450 101 69-130
Xylene (Total)ug/L 156150 104 70-130
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%99 70-130
Dibromofluoromethane (S)%100 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 50 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
698251MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92107743003
698252
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 89 70-166110 20 3050ND44.6 54.8
Benzene ug/L 50 91 70-148109 18 3050ND45.4 54.4
Chlorobenzene ug/L 50 86 70-146101 17 3050ND42.8 50.7
Toluene ug/L 50 85 70-155102 19 3050ND42.3 51.2
Trichloroethene ug/L 50 88 69-151106 19 3050ND44.1 53.2
1,2-Dichloroethane-d4 (S) %112 70-130111
4-Bromofluorobenzene (S) %94 70-13094
Dibromofluoromethane (S) %112 70-130115
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 51 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/15772
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples: 92107636001, 92107636002, 92107636003, 92107636004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695564
Associated Lab Samples:92107636001, 92107636002, 92107636003, 92107636004
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 12/08/11 17:24
1,2-Dichlorobenzene ug/L ND 10.0 12/08/11 17:24
1,3-Dichlorobenzene ug/L ND 10.0 12/08/11 17:24
1,4-Dichlorobenzene ug/L ND 10.0 12/08/11 17:24
1-Methylnaphthalene ug/L ND 10.0 12/08/11 17:24
2,4,5-Trichlorophenol ug/L ND 10.0 12/08/11 17:24
2,4,6-Trichlorophenol ug/L ND 10.0 12/08/11 17:24
2,4-Dichlorophenol ug/L ND 10.0 12/08/11 17:24
2,4-Dimethylphenol ug/L ND 10.0 12/08/11 17:24
2,4-Dinitrophenol ug/L ND 50.0 12/08/11 17:24
2,4-Dinitrotoluene ug/L ND 10.0 12/08/11 17:24
2,6-Dinitrotoluene ug/L ND 10.0 12/08/11 17:24
2-Chloronaphthalene ug/L ND 10.0 12/08/11 17:24
2-Chlorophenol ug/L ND 10.0 12/08/11 17:24
2-Methylnaphthalene ug/L ND 10.0 12/08/11 17:24
2-Methylphenol(o-Cresol)ug/L ND 10.0 12/08/11 17:24
2-Nitroaniline ug/L ND 50.0 12/08/11 17:24
2-Nitrophenol ug/L ND 10.0 12/08/11 17:24
3&4-Methylphenol(m&p Cresol) ug/L ND 10.0 12/08/11 17:24
3,3'-Dichlorobenzidine ug/L ND 20.0 12/08/11 17:24
3-Nitroaniline ug/L ND 50.0 12/08/11 17:24
4,6-Dinitro-2-methylphenol ug/L ND 20.0 12/08/11 17:24
4-Bromophenylphenyl ether ug/L ND 10.0 12/08/11 17:24
4-Chloro-3-methylphenol ug/L ND 20.0 12/08/11 17:24
4-Chloroaniline ug/L ND 20.0 12/08/11 17:24
4-Chlorophenylphenyl ether ug/L ND 10.0 12/08/11 17:24
4-Nitroaniline ug/L ND 20.0 12/08/11 17:24
4-Nitrophenol ug/L ND 50.0 12/08/11 17:24
Acenaphthene ug/L ND 10.0 12/08/11 17:24
Acenaphthylene ug/L ND 10.0 12/08/11 17:24
Aniline ug/L ND 10.0 12/08/11 17:24
Anthracene ug/L ND 10.0 12/08/11 17:24
Benzo(a)anthracene ug/L ND 10.0 12/08/11 17:24
Benzo(a)pyrene ug/L ND 10.0 12/08/11 17:24
Benzo(b)fluoranthene ug/L ND 10.0 12/08/11 17:24
Benzo(g,h,i)perylene ug/L ND 10.0 12/08/11 17:24
Benzo(k)fluoranthene ug/L ND 10.0 12/08/11 17:24
Benzoic Acid ug/L ND 50.0 12/08/11 17:24
Benzyl alcohol ug/L ND 20.0 12/08/11 17:24
bis(2-Chloroethoxy)methane ug/L ND 10.0 12/08/11 17:24
bis(2-Chloroethyl) ether ug/L ND 10.0 12/08/11 17:24
bis(2-Chloroisopropyl) ether ug/L ND 10.0 12/08/11 17:24
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 12/08/11 17:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 52 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 695564
Associated Lab Samples:92107636001, 92107636002, 92107636003, 92107636004
Matrix: Water
Analyzed
Butylbenzylphthalate ug/L ND 10.0 12/08/11 17:24
Chrysene ug/L ND 10.0 12/08/11 17:24
Di-n-butylphthalate ug/L ND 10.0 12/08/11 17:24
Di-n-octylphthalate ug/L ND 10.0 12/08/11 17:24
Dibenz(a,h)anthracene ug/L ND 10.0 12/08/11 17:24
Dibenzofuran ug/L ND 10.0 12/08/11 17:24
Diethylphthalate ug/L ND 10.0 12/08/11 17:24
Dimethylphthalate ug/L ND 10.0 12/08/11 17:24
Fluoranthene ug/L ND 10.0 12/08/11 17:24
Fluorene ug/L ND 10.0 12/08/11 17:24
Hexachloro-1,3-butadiene ug/L ND 10.0 12/08/11 17:24
Hexachlorobenzene ug/L ND 10.0 12/08/11 17:24
Hexachlorocyclopentadiene ug/L ND 10.0 12/08/11 17:24
Hexachloroethane ug/L ND 10.0 12/08/11 17:24
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 12/08/11 17:24
Isophorone ug/L ND 10.0 12/08/11 17:24
N-Nitroso-di-n-propylamine ug/L ND 10.0 12/08/11 17:24
N-Nitrosodimethylamine ug/L ND 10.0 12/08/11 17:24
N-Nitrosodiphenylamine ug/L ND 10.0 12/08/11 17:24
Naphthalene ug/L ND 10.0 12/08/11 17:24
Nitrobenzene ug/L ND 10.0 12/08/11 17:24
Pentachlorophenol ug/L ND 25.0 12/08/11 17:24
Phenanthrene ug/L ND 10.0 12/08/11 17:24
Phenol ug/L ND 10.0 12/08/11 17:24
Pyrene ug/L ND 10.0 12/08/11 17:24
2,4,6-Tribromophenol (S)%66 27-110 12/08/11 17:24
2-Fluorobiphenyl (S)%58 27-110 12/08/11 17:24
2-Fluorophenol (S)%41 12-110 12/08/11 17:24
Nitrobenzene-d5 (S)%50 21-110 12/08/11 17:24
Phenol-d6 (S)%25 10-110 12/08/11 17:24
Terphenyl-d14 (S)%77 31-107 12/08/11 17:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695565LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 23.450 47 10-110
1,2-Dichlorobenzene ug/L 25.550 51 10-110
1,3-Dichlorobenzene ug/L 24.750 49 10-110
1,4-Dichlorobenzene ug/L 24.750 49 10-110
1-Methylnaphthalene ug/L 28.550 57 21-110
2,4,5-Trichlorophenol ug/L 25.150 50 23-116
2,4,6-Trichlorophenol ug/L 28.850 58 21-114
2,4-Dichlorophenol ug/L 28.450 57 22-120
2,4-Dimethylphenol ug/L 29.450 59 15-109
2,4-Dinitrophenol ug/L 82.2250 33 10-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 53 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695565LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/L 36.350 73 24-119
2,6-Dinitrotoluene ug/L 34.050 68 25-116
2-Chloronaphthalene ug/L 28.050 56 18-110
2-Chlorophenol ug/L 31.650 63 10-104
2-Methylnaphthalene ug/L 27.950 56 16-110
2-Methylphenol(o-Cresol)ug/L 25.050 50 13-110
2-Nitroaniline ug/L 53.6100 54 20-117
2-Nitrophenol ug/L 29.850 60 16-108
3&4-Methylphenol(m&p Cresol) ug/L 24.450 49 14-110
3,3'-Dichlorobenzidine ug/L 72.5100 72 13-131
3-Nitroaniline ug/L 71.5100 71 15-117
4,6-Dinitro-2-methylphenol ug/L 59.8100 60 13-119
4-Bromophenylphenyl ether ug/L 28.750 57 23-120
4-Chloro-3-methylphenol ug/L 59.3100 59 21-119
4-Chloroaniline ug/L 62.7100 63 10-122
4-Chlorophenylphenyl ether ug/L 28.850 58 22-112
4-Nitroaniline ug/L 78.5100 79 14-118
4-Nitrophenol ug/L 67.2250 27 10-110
Acenaphthene ug/L 29.550 59 20-105
Acenaphthylene ug/L 28.750 57 23-106
Aniline ug/L 27.950 56 10-110
Anthracene ug/L 31.150 62 25-120
Benzo(a)anthracene ug/L 35.150 70 21-128
Benzo(a)pyrene ug/L 33.850 68 25-116
Benzo(b)fluoranthene ug/L 32.150 64 23-117
Benzo(g,h,i)perylene ug/L 34.150 68 17-128
Benzo(k)fluoranthene ug/L 33.150 66 25-127
Benzoic Acid ug/L 33.5J250 13 10-110
Benzyl alcohol ug/L 56.0100 56 10-101
bis(2-Chloroethoxy)methane ug/L 27.850 56 19-107
bis(2-Chloroethyl) ether ug/L 30.350 61 10-108
bis(2-Chloroisopropyl) ether ug/L 28.350 57 10-108
bis(2-Ethylhexyl)phthalate ug/L 35.750 71 16-123
Butylbenzylphthalate ug/L 36.050 72 20-118
Chrysene ug/L 35.650 71 24-125
Di-n-butylphthalate ug/L 35.450 71 23-115
Di-n-octylphthalate ug/L 36.850 74 20-115
Dibenz(a,h)anthracene ug/L 34.150 68 18-131
Dibenzofuran ug/L 30.150 60 23-106
Diethylphthalate ug/L 32.750 65 24-115
Dimethylphthalate ug/L 30.150 60 22-113
Fluoranthene ug/L 34.950 70 24-125
Fluorene ug/L 30.550 61 24-114
Hexachloro-1,3-butadiene ug/L 18.450 37 10-110
Hexachlorobenzene ug/L 30.550 61 22-127
Hexachlorocyclopentadiene ug/L 21.050 42 10-110
Hexachloroethane ug/L 23.450 47 10-110
Indeno(1,2,3-cd)pyrene ug/L 33.750 67 18-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 54 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
695565LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/L 27.550 55 23-114
N-Nitroso-di-n-propylamine ug/L 28.650 57 21-114
N-Nitrosodimethylamine ug/L 23.350 47 10-110
N-Nitrosodiphenylamine ug/L 30.250 60 24-123
Naphthalene ug/L 26.550 53 14-110
Nitrobenzene ug/L 24.250 48 16-106
Pentachlorophenol ug/L 45.3100 45 10-123
Phenanthrene ug/L 29.150 58 25-119
Phenol ug/L 17.050 34 10-110
Pyrene ug/L 32.150 64 22-127
2,4,6-Tribromophenol (S)%67 27-110
2-Fluorobiphenyl (S)%52 27-110
2-Fluorophenol (S)%42 12-110
Nitrobenzene-d5 (S)%47 21-110
Phenol-d6 (S)%27 10-110
Terphenyl-d14 (S)%66 31-107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 55 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92107636
Sun Chemical Facility PPA-038
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside thelaboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/12/2011 04:43 PM Page 56 of 56
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
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Appendix B
Boring Logs

Soil
Dry to slightly moist, brown, loose, sandy SILT
Bottom of borehole at 2.0 feet.
GB
DRAWN BY:
BORING COMPLETED:12/1/11
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:N/A / Hand Auger
SAMPLING METHOD:Hand Auger Soil samples collected from 0-2 ft bgs.
BORING STARTED:12/1/11
LOGGED BY:JRS
TOTAL DEPTH: 2 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER BG
PROJECT:Sun Chemical Facility
JOB NUMBER:PPA-038
LOCATION:1701 Westnghouse Blvd. Charlotte, NC
BORING LOG - HART HICKMAN.GDT - 12/19/11 16:52 - S:\AAA-MASTER GINT PROJECTS\PPA-038.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
1
2
3
0
1
2
3
0.4
0.5
0.3
0.1
Concrete
Slightly moist, greenish gray, stiff, CLAY
Slightly moist, light brown and gray, loose, silty SAND w/ abundant
gravels
Refusal at 7.0 feet.
Bottom of borehole at 7.0 feet.
0
0
0
0
GB
DRAWN BY:
BORING COMPLETED:11/30/11
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / DPT
SAMPLING METHOD:Hand Auger / Macro-Core Hand auger to 5 ft bgs. Soil samplescollected from 0-2 ft bgs.
BORING STARTED:11/30/11
LOGGED BY:JRS
TOTAL DEPTH: 7 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER DPT-1
PROJECT:Sun Chemical Facility
JOB NUMBER:PPA-038
LOCATION:1701 Westnghouse Blvd. Charlotte, NC
BORING LOG - HART HICKMAN.GDT - 12/19/11 16:52 - S:\AAA-MASTER GINT PROJECTS\PPA-038.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
7.5
10.0
0.0
2.5
5.0
7.5
10.0
0.1
0.1
0.1
Soil
Slightly moist, dark brown, loose, sandy SILT
Slightly moist, light brown, loose, sandy SILT
Slightly moist, light brown and gray, medium, sandy CLAY
Dry to slightly moist, light brown, loose, SAND
Refusal at 6.0 feet.
Bottom of borehole at 6.0 feet.
0
0
0
GB
DRAWN BY:
BORING COMPLETED:11/30/11
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / DPT
SAMPLING METHOD:Hand Auger / Macro-Core Hand auge to 5 ft bgs. Soil samplescollected from 0-2 ft bgs.
BORING STARTED:11/30/11
LOGGED BY:JRS
TOTAL DEPTH: 6 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER DPT-2
PROJECT:Sun Chemical Facility
JOB NUMBER:PPA-038
LOCATION:1701 Westnghouse Blvd. Charlotte, NC
BORING LOG - HART HICKMAN.GDT - 12/19/11 16:52 - S:\AAA-MASTER GINT PROJECTS\PPA-038.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
7.5
10.0
0.0
2.5
5.0
7.5
10.0
2.1
0.9
0.3
0.1
Concrete
Slightly moist, greenish gray, stiff, CLAY
Slightly moist, brown, moist, sandy CLAY
Dry to slightly moist, brown, loose, silty SAND
Dry to slightly moist, orangish brown, loose, silty SAND w/ mica
Saturated, orangish brown, loose, silty SAND w/ mica
Saturated, orangish brown, loose, silty SAND w/ mica and abundantgravels
Refusal at 20.5 feet.
Bottom of borehole at 20.5 feet.
0
0
0
0
2" PVC
Riser
Bentonite
#2 FilterSand
0.01" Slotted
PVC Screen
DRAWN BY:
BORING COMPLETED:11/30/11
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / HSA
SAMPLING METHOD:Hand Auger / Auger Cuttings Hand auger to 5 ft bgs. Temporarymonitoring well abandoned followingcollection of groundwater samples.
BORING STARTED:11/30/11
LOGGED BY:JRS
TOTAL DEPTH: 20.5 ft.
TOP OF CASING ELEV: 0 ft.
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER HH-1
PROJECT:Sun Chemical Facility
JOB NUMBER:PPA-038
LOCATION:1701 Westnghouse Blvd. Charlotte, NC
BORING LOG - HART HICKMAN.GDT - 12/19/11 16:52 - S:\AAA-MASTER GINT PROJECTS\PPA-038.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
0
5
10
15
20
4.1
45.9
4.5
0.3
Concrete
Slightly moist, greenish gray, loose, sandy CLAY
Slightly moist, gray and tan, loose, gravelly SAND w/ trace of silt and
clay
Slightly moist, light brown, loose, SAND
Moist, tan and gray, loose, sandy SILT w/ abundant gravels andminor clay clasts
Saturated, greenish gray and tan, loose, gravelly SAND w/ clayclasts
Bottom of borehole at 19.0 feet.
0
0
0
0
2" PVCRiser
BentoniteSeal
#2 SandPack
0.01" SlotPVC Screen
DRAWN BY:
BORING COMPLETED:11/30/11
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / HSA
SAMPLING METHOD:Hand Auger / Auger Cuttings Hand auger to 5 ft bgs. Temporarymonitoring well abandoned followingcollection of groundwater samples.
BORING STARTED:11/30/11
LOGGED BY:JRS
TOTAL DEPTH: 19 ft.
TOP OF CASING ELEV: 0 ft.
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER HH-2
PROJECT:Sun Chemical Facility
JOB NUMBER:PPA-038
LOCATION:1701 Westnghouse Blvd. Charlotte, NC
BORING LOG - HART HICKMAN.GDT - 12/19/11 16:52 - S:\AAA-MASTER GINT PROJECTS\PPA-038.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
0
5
10
15
20
0.1
0.2
0.2
0.1
Concrete
Gravel fill
Slightly moist, greenish gray, stiff, CLAY
Dry, orangish brown, loose, silty SAND
Moist, orangish brown, loose, sandy SILT
Saturated, brown, loose, sandy SILT w/ few small gravels
Bottom of borehole at 23.0 feet.
0
0
0
0
2" PVC
Riser
Bentonite
Seal
#2 FilterSand
0.01" SlotPVC Screen
DRAWN BY:
BORING COMPLETED:11/30/11
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / HSA
SAMPLING METHOD:Hand Auger / Auger Cuttings Hand auger to 5 ft bgs. Temporarymonitoring well abandoned followingcollection of groundwater samples.
BORING STARTED:11/30/11
LOGGED BY:JRS
TOTAL DEPTH: 23 ft.
TOP OF CASING ELEV: 0 ft.
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER HH-3
PROJECT:Sun Chemical Facility
JOB NUMBER:PPA-038
LOCATION:1701 Westnghouse Blvd. Charlotte, NC
BORING LOG - HART HICKMAN.GDT - 12/19/11 16:52 - S:\AAA-MASTER GINT PROJECTS\PPA-038.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
0
5
10
15
20
25
Concrete
Gravel fill
Dry, gray, loose, SAND w/ trace of silt
Moist, greenish gray, medium, CLAY w/ trace of sand
Moist, brown, loose, silty SAND
Saturated, gray, loose, sandy SILT w/ abundant gravels
Refusal at 15.0 feet.
Bottom of borehole at 15.0 feet.
GB
2" PVC
Riser
Bentoniteseal
#2 SandPack
0.01" SlotPVC Screen
DRAWN BY:
BORING COMPLETED:11/30/11
DRILLING CONTRACTOR:Probe Technology Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / DPT / HSA
SAMPLING METHOD:Hand Auger / Macro-Core Hand auger to 5 ft bgs. Soil samplescollected from 0-2 ft bgs. Temporarymonitoring well abandoned following
collection of groundwater samples.
BORING STARTED:11/30/11
LOGGED BY:JRS
TOTAL DEPTH: 15 ft.
TOP OF CASING ELEV: 0 ft.
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER HH-4 / DPT-3
PROJECT:Sun Chemical Facility
JOB NUMBER:PPA-038
LOCATION:1701 Westnghouse Blvd. Charlotte, NC
BORING LOG - HART HICKMAN.GDT - 12/19/11 16:52 - S:\AAA-MASTER GINT PROJECTS\PPA-038.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
7.5
10.0
12.5
15.0
0.0
2.5
5.0
7.5
10.0
12.5
15.0

Appendix C
Temporary Monitoring Well Construction and Abandonment Records

UNON RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # ___________________________
1. WELL CONTRACTOR:
_________________________________________________________
Well Contractor (Individual) Name
_________________________________________________________
Well Contractor Company Name
_________________________________________________________
Street Address
_________________________________________________________
City or Town State Zip Code
(_______) __________________________
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#______________________________
OTHER ASSOCIATED PERMIT#(if applicable)______________________
SITE WELL ID #(if applicable)______________________________
3. WELL USE (Check One Box) Monitoring ഋ Municipal/Public ഋ
Industrial/Commercial ഋ Agricultural ഋ Recovery ഋ Injection ഋ
Irrigationഋ Other ഋ (list use) ____________________________
DATE DRILLED_____________________
4. WELL LOCATION:
_________________________________________________________
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: ____________________________ COUNTY________________
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
ഋSlope ഋValley ഋFlat ഋRidge ഋOther___________________
LATITUDE ______°____'_________" DMS OR _____________ DD
LONGITUDE _____°____'_________" DMS OR _____________ DD
Latitude/longitude source: ഋGPS ഋTopographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
_________________________________________________________
Facility Name Facility ID# (if applicable)
_________________________________________________________
Street Address
_________________________________________________________
City or Town State Zip Code
_________________________________________________________
Contact Name
_________________________________________________________
Mailing Address
_________________________________________________________
City or Town State Zip Code
(_______) __________________________
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH:___________________
b. DOES WELL REPLACE EXISTING WELL?YES ഋ NOഋ
c. WATER LEVEL Below Top of Casing: _______________FT.
(Use “+” if Above Top of Casing)
d. TOP OF CASING IS _____________ FT. Above Land Surface*
*Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): ___________ METHOD OF TEST______________
f. DISINFECTION: Type_______________ Amount ____________
g. WATER ZONES (depth):
Top_________ Bottom_________ Top_________ Bottom_________
Top_________ Bottom_________ Top_________ Bottom_________
Top_________ Bottom_________ Top_________ Bottom_________
Thickness/
7. CASING: Depth Diameter Weight Material
Top_______ Bottom_______ Ft.________ _______ ___________
Top_______ Bottom_______ Ft.________ _______ ___________
Top_______ Bottom_______ Ft.________ _______ ___________
8. GROUT: Depth Material Method
Top_______ Bottom_______ Ft.______________ ______________
Top_______ Bottom_______ Ft.______________ ______________
Top_______ Bottom_______ Ft.______________ ______________
9. SCREEN: Depth Diameter Slot Size Material
Top_______ Bottom_______ Ft.______in. ______ in. ____________
Top_______ Bottom_______ Ft.______in. ______ in. ____________
Top_______ Bottom_______ Ft.______in. ______ in. ____________
10. SAND/GRAVEL PACK:
Depth Size Material
Top________Bottom_______ Ft.________ ______________________
Top________Bottom_______ Ft.________ ______________________
Top________Bottom_______ Ft.________ ______________________
11.DRILLING LOG
Top Bottom Formation Description
12. REMARKS:
_________________________________________________________
_________________________________________________________
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
__________________________________________ ___________
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
__________________________________________________
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
Submit within 30 days of completion to: Division of Water Quality -Information Processing,
1617 Mail Service Center, Raleigh, NC 27699-161, Phone : [phone]
2736-A
Chris Bost
Probe Technology,Inc.
4537 OrphanageRd
Concord NC 28027
704 933-5538
HH-1
✔
temporary mw
11-30-11
1701Westinghouse Blvd,28273
Charlotte Mecklenburg
✔
35 7 28.6470 3x.xxxxxxxxx
80 56 14.7160 7x.xxxxxxxxx
✔
Sun Chemical
1701Westinghouse Blvd
Charlotte NC 28273
1701Westinghouse Blvd
Charlotte NC 28273
20.5 ft
✔
7.5
-0.5
N/A none
none N/A
8 20.5
0.5 10.5 2" Sch40 PVC
5 8 bentonite gravity
10.5 20.5 2" 0.010 PVC
8 20.5 #2 silica sand
See Geologist's log
12-8-11
Chris Bost 2736-A
UNON RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # ___________________________
1. WELL CONTRACTOR:
_________________________________________________________
Well Contractor (Individual) Name
_________________________________________________________
Well Contractor Company Name
_________________________________________________________
Street Address
_________________________________________________________
City or Town State Zip Code
(_______) __________________________
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#______________________________
OTHER ASSOCIATED PERMIT#(if applicable)______________________
SITE WELL ID #(if applicable)______________________________
3. WELL USE (Check One Box) Monitoring ഋ Municipal/Public ഋ
Industrial/Commercial ഋ Agricultural ഋ Recovery ഋ Injection ഋ
Irrigationഋ Other ഋ (list use) ____________________________
DATE DRILLED_____________________
4. WELL LOCATION:
_________________________________________________________
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: ____________________________ COUNTY________________
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
ഋSlope ഋValley ഋFlat ഋRidge ഋOther___________________
LATITUDE ______°____'_________" DMS OR _____________ DD
LONGITUDE _____°____'_________" DMS OR _____________ DD
Latitude/longitude source: ഋGPS ഋTopographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
_________________________________________________________
Facility Name Facility ID# (if applicable)
_________________________________________________________
Street Address
_________________________________________________________
City or Town State Zip Code
_________________________________________________________
Contact Name
_________________________________________________________
Mailing Address
_________________________________________________________
City or Town State Zip Code
(_______) __________________________
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH:___________________
b. DOES WELL REPLACE EXISTING WELL?YES ഋ NOഋ
c. WATER LEVEL Below Top of Casing: _______________FT.
(Use “+” if Above Top of Casing)
d. TOP OF CASING IS _____________ FT. Above Land Surface*
*Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): ___________ METHOD OF TEST______________
f. DISINFECTION: Type_______________ Amount ____________
g. WATER ZONES (depth):
Top_________ Bottom_________ Top_________ Bottom_________
Top_________ Bottom_________ Top_________ Bottom_________
Top_________ Bottom_________ Top_________ Bottom_________
Thickness/
7. CASING: Depth Diameter Weight Material
Top_______ Bottom_______ Ft.________ _______ ___________
Top_______ Bottom_______ Ft.________ _______ ___________
Top_______ Bottom_______ Ft.________ _______ ___________
8. GROUT: Depth Material Method
Top_______ Bottom_______ Ft.______________ ______________
Top_______ Bottom_______ Ft.______________ ______________
Top_______ Bottom_______ Ft.______________ ______________
9. SCREEN: Depth Diameter Slot Size Material
Top_______ Bottom_______ Ft.______in. ______ in. ____________
Top_______ Bottom_______ Ft.______in. ______ in. ____________
Top_______ Bottom_______ Ft.______in. ______ in. ____________
10. SAND/GRAVEL PACK:
Depth Size Material
Top________Bottom_______ Ft.________ ______________________
Top________Bottom_______ Ft.________ ______________________
Top________Bottom_______ Ft.________ ______________________
11.DRILLING LOG
Top Bottom Formation Description
12. REMARKS:
_________________________________________________________
_________________________________________________________
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
__________________________________________ ___________
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
__________________________________________________
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
Submit within 30 days of completion to: Division of Water Quality -Information Processing,
1617 Mail Service Center, Raleigh, NC 27699-161, Phone : [phone]
2736-A
Chris Bost
Probe Technology,Inc.
4537 OrphanageRd
Concord NC 28027
704 933-5538
HH-2
✔
temporary mw
11-30-11
1701Westinghouse Blvd,28273
Charlotte Mecklenburg
✔
35 7 28.1050 3x.xxxxxxxxx
80 56 13.9960 7x.xxxxxxxxx
✔
Sun Chemical
1701Westinghouse Blvd
Charlotte NC 28273
1701Westinghouse Blvd
Charlotte NC 28273
19 ft
✔
9
1
N/A none
none N/A
819
+1 9 2" Sch40 PVC
5 7 bentonite gravity
9 19 2" 0.010 PVC
719#2 silica sand
See Geologist's log
Chris Bost 2736-A
UNON RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # ___________________________
1. WELL CONTRACTOR:
_________________________________________________________
Well Contractor (Individual) Name
_________________________________________________________
Well Contractor Company Name
_________________________________________________________
Street Address
_________________________________________________________
City or Town State Zip Code
(_______) __________________________
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#______________________________
OTHER ASSOCIATED PERMIT#(if applicable)______________________
SITE WELL ID #(if applicable)______________________________
3. WELL USE (Check One Box) Monitoring ഋ Municipal/Public ഋ
Industrial/Commercial ഋ Agricultural ഋ Recovery ഋ Injection ഋ
Irrigationഋ Other ഋ (list use) ____________________________
DATE DRILLED_____________________
4. WELL LOCATION:
_________________________________________________________
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: ____________________________ COUNTY________________
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
ഋSlope ഋValley ഋFlat ഋRidge ഋOther___________________
LATITUDE ______°____'_________" DMS OR _____________ DD
LONGITUDE _____°____'_________" DMS OR _____________ DD
Latitude/longitude source: ഋGPS ഋTopographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
_________________________________________________________
Facility Name Facility ID# (if applicable)
_________________________________________________________
Street Address
_________________________________________________________
City or Town State Zip Code
_________________________________________________________
Contact Name
_________________________________________________________
Mailing Address
_________________________________________________________
City or Town State Zip Code
(_______) __________________________
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH:___________________
b. DOES WELL REPLACE EXISTING WELL?YES ഋ NOഋ
c. WATER LEVEL Below Top of Casing: _______________FT.
(Use “+” if Above Top of Casing)
d. TOP OF CASING IS _____________ FT. Above Land Surface*
*Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): ___________ METHOD OF TEST______________
f. DISINFECTION: Type_______________ Amount ____________
g. WATER ZONES (depth):
Top_________ Bottom_________ Top_________ Bottom_________
Top_________ Bottom_________ Top_________ Bottom_________
Top_________ Bottom_________ Top_________ Bottom_________
Thickness/
7. CASING: Depth Diameter Weight Material
Top_______ Bottom_______ Ft.________ _______ ___________
Top_______ Bottom_______ Ft.________ _______ ___________
Top_______ Bottom_______ Ft.________ _______ ___________
8. GROUT: Depth Material Method
Top_______ Bottom_______ Ft.______________ ______________
Top_______ Bottom_______ Ft.______________ ______________
Top_______ Bottom_______ Ft.______________ ______________
9. SCREEN: Depth Diameter Slot Size Material
Top_______ Bottom_______ Ft.______in. ______ in. ____________
Top_______ Bottom_______ Ft.______in. ______ in. ____________
Top_______ Bottom_______ Ft.______in. ______ in. ____________
10. SAND/GRAVEL PACK:
Depth Size Material
Top________Bottom_______ Ft.________ ______________________
Top________Bottom_______ Ft.________ ______________________
Top________Bottom_______ Ft.________ ______________________
11.DRILLING LOG
Top Bottom Formation Description
12. REMARKS:
_________________________________________________________
_________________________________________________________
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
__________________________________________ ___________
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
__________________________________________________
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
Submit within 30 days of completion to: Division of Water Quality -Information Processing,
1617 Mail Service Center, Raleigh, NC 27699-161, Phone : [phone]
2736-A
Chris Bost
Probe Technology,Inc.
4537 OrphanageRd
Concord NC 28027
704 933-5538
HH-3
✔
temporary mw
11-30-11
1701Westinghouse Blvd,28273
Charlotte Mecklenburg
✔
35 7 29.5570 3x.xxxxxxxxx
80 56 12.5220 7x.xxxxxxxxx
✔
Sun Chemical
1701Westinghouse Blvd
Charlotte NC 28273
1701Westinghouse Blvd
Charlotte NC 28273
22 ft
✔
9
1
N/A none
none N/A
822
+1 12 2" Sch40 PVC
6 8 bentonite gravity
12 22 2" 0.010 PVC
822#2 silica sand
See Geologist's log
12-8-11
Chris Bost 2736-A
UNON RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # ___________________________
1. WELL CONTRACTOR:
_________________________________________________________
Well Contractor (Individual) Name
_________________________________________________________
Well Contractor Company Name
_________________________________________________________
Street Address
_________________________________________________________
City or Town State Zip Code
(_______) __________________________
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#______________________________
OTHER ASSOCIATED PERMIT#(if applicable)______________________
SITE WELL ID #(if applicable)______________________________
3. WELL USE (Check One Box) Monitoring ഋ Municipal/Public ഋ
Industrial/Commercial ഋ Agricultural ഋ Recovery ഋ Injection ഋ
Irrigationഋ Other ഋ (list use) ____________________________
DATE DRILLED_____________________
4. WELL LOCATION:
_________________________________________________________
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: ____________________________ COUNTY________________
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
ഋSlope ഋValley ഋFlat ഋRidge ഋOther___________________
LATITUDE ______°____'_________" DMS OR _____________ DD
LONGITUDE _____°____'_________" DMS OR _____________ DD
Latitude/longitude source: ഋGPS ഋTopographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
_________________________________________________________
Facility Name Facility ID# (if applicable)
_________________________________________________________
Street Address
_________________________________________________________
City or Town State Zip Code
_________________________________________________________
Contact Name
_________________________________________________________
Mailing Address
_________________________________________________________
City or Town State Zip Code
(_______) __________________________
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH:___________________
b. DOES WELL REPLACE EXISTING WELL?YES ഋ NOഋ
c. WATER LEVEL Below Top of Casing: _______________FT.
(Use “+” if Above Top of Casing)
d. TOP OF CASING IS _____________ FT. Above Land Surface*
*Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): ___________ METHOD OF TEST______________
f. DISINFECTION: Type_______________ Amount ____________
g. WATER ZONES (depth):
Top_________ Bottom_________ Top_________ Bottom_________
Top_________ Bottom_________ Top_________ Bottom_________
Top_________ Bottom_________ Top_________ Bottom_________
Thickness/
7. CASING: Depth Diameter Weight Material
Top_______ Bottom_______ Ft.________ _______ ___________
Top_______ Bottom_______ Ft.________ _______ ___________
Top_______ Bottom_______ Ft.________ _______ ___________
8. GROUT: Depth Material Method
Top_______ Bottom_______ Ft.______________ ______________
Top_______ Bottom_______ Ft.______________ ______________
Top_______ Bottom_______ Ft.______________ ______________
9. SCREEN: Depth Diameter Slot Size Material
Top_______ Bottom_______ Ft.______in. ______ in. ____________
Top_______ Bottom_______ Ft.______in. ______ in. ____________
Top_______ Bottom_______ Ft.______in. ______ in. ____________
10. SAND/GRAVEL PACK:
Depth Size Material
Top________Bottom_______ Ft.________ ______________________
Top________Bottom_______ Ft.________ ______________________
Top________Bottom_______ Ft.________ ______________________
11.DRILLING LOG
Top Bottom Formation Description
12. REMARKS:
_________________________________________________________
_________________________________________________________
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
__________________________________________ ___________
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
__________________________________________________
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
______/_________ ___________________________
Submit within 30 days of completion to: Division of Water Quality -Information Processing,
1617 Mail Service Center, Raleigh, NC 27699-161, Phone : [phone]
2736-A
Chris Bost
Probe Technology,Inc.
4537 OrphanageRd
Concord NC 28027
704 933-5538
HH-4
✔
temporary mw
11-30-11
1701Westinghouse Blvd,28273
Charlotte Mecklenburg
✔
35 7 29.2640 3x.xxxxxxxxx
80 56 11.0100 7x.xxxxxxxxx
✔
Sun Chemical
1701Westinghouse Blvd
Charlotte NC 28273
1701Westinghouse Blvd
Charlotte NC 28273
14 ft
✔
9
1
N/A none
none N/A
814
+1 4 2" Sch40 PVC
1 2 bentonite gravity
4 14 2" 0.010 PVC
214#2 silica sand
See Geologist's log
12-8-11
Chris Bost 2736-A
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION #___________________________
1. WELL CONTRACTOR:
______________________________________________________
Well Contractor (Individual) Name
______________________________________________________
Well Contractor Company Name
STREET ADDRESS ____________________________________
______________________________________________________
City or Town State Zip Code
(_______) - _____________________
Area code - Phone number
2. WELL INFORMATION:
SITE WELL ID #(if applicable)____________________________________
STATE WELL PERMIT #(if applicable)____________________________
COUNTY WELL PERMIT# (if applicable)_________________________
DWQ or OTHER PERMIT #(if applicable)__________________________
WELL USE (Check applicable use):ട Monitoring ട Residential
ട Municipal/Public ട Industrial/Commercial ട Agricultural
ട Recovery ട Injection ട Irrigation
ട Other (list use) _________________________________________
3. WELL LOCATION:
COUNTY______________ QUADRANGLE NAME _______________
NEAREST TOWN: __________________________________________
___________________________________________________________
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHIC / LAND SETTING:
ട Slope ട Valley ട Flat ട Ridge ട Other_____________________
(Check appropriate setting)
LATITUDE ___ ___ _____________
LONGITUDE ___ ___ _____________
Latitude/longitude source:ട GPS ട Topographic map
(Location of well must be shown on a USGS topo map and
attached to this form if not using GPS.)
4a. FACILITY-The name of the business where the well is located. Complete 4a and4b.
(If a residential well, skip 4a; complete 4b, well owner information only.)
FACILITY ID #(if applicable) _________________________________
NAME OF FACILITY_________________________________________
STREET ADDRESS __________________________________________
___________________________________________________________
City or Town State Zip Code
4b. CONTACT PERSON/WELL OWNER:
NAME ____________________________________________________
STREET ADDRESS_________________________________________
5. WELL DETAILS:
a.Total Depth:____________ ft. Diameter:____________ in.
b. Water Level (Below Measuring Point): _________ ft.
Measuring point is _________ ft. above land surface.
6. CASING:Length Diameter
a. Casing Depth (if known): __________ ft. ________ in.
b. Casing Removed: __________ ft. ________ in.
7. DISINFECTION:_____________________
(Amount of 65%-75% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement _________ lb. Cement_________ lb.
Water___________ gal. Water___________gal.
Bentonite
Bentonite lb.
Type:ട Slurry ടPellets
Water______________ gal.
Other
Type material _________________________________
Amount _____________________________________
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
____________________________________________________________
____________________________________________________________
____________________________________________________________
____________________________________________________________
10. WELL DIAGRAM: Draw a detailed sketch of the well on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materials used.
11. DATE WELL ABANDONED ______________________________
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
_______________________________________________________
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
______________________________________________________
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
(The private well owner must be an individual who personally abandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
________________________________________________________________________
PRINTED NAME OF PERSON ABANDONING THE WELL
Submit a copy to the owner and the original to the Division of Water Quality within 30 days.Form GW-30
Attn: Information Management, 1617 Mail Service Center – Raleigh, NC 27699-1617, Phone No. [phone] ext 568.Rev. 5/06
May be in degrees,
minutes, seconds, or in a
decimal format
2725-A
Mike Tynan
Probe Technology, Inc.
4537 Orphanage Rd
Concord NC 28027
704 933-5538
HH-1
✔
Mecklenburg
Charlotte
1701 Westinghouse Blvd, 28273
✔
35 07 28.647
80 56 14.716
✔
Sun Chemical
1701 Westinghouse Blvd
Charlotte NC 28273
Same as above
20.5 2
8
0
10 2
02
none
94
6.5
Filled MW from bottom to top through rigid tremmie
pipe with cement/bentonite grout. Surface pavement
completed with concrete.
12/2/11
12-8-11
Mike Tynan
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION #___________________________
1. WELL CONTRACTOR:
______________________________________________________
Well Contractor (Individual) Name
______________________________________________________
Well Contractor Company Name
STREET ADDRESS ____________________________________
______________________________________________________
City or Town State Zip Code
(_______) - _____________________
Area code - Phone number
2. WELL INFORMATION:
SITE WELL ID #(if applicable)____________________________________
STATE WELL PERMIT #(if applicable)____________________________
COUNTY WELL PERMIT# (if applicable)_________________________
DWQ or OTHER PERMIT #(if applicable)__________________________
WELL USE (Check applicable use):ട Monitoring ട Residential
ട Municipal/Public ട Industrial/Commercial ട Agricultural
ട Recovery ട Injection ട Irrigation
ട Other (list use) _________________________________________
3. WELL LOCATION:
COUNTY______________ QUADRANGLE NAME _______________
NEAREST TOWN: __________________________________________
___________________________________________________________
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHIC / LAND SETTING:
ട Slope ട Valley ട Flat ട Ridge ട Other_____________________
(Check appropriate setting)
LATITUDE ___ ___ _____________
LONGITUDE ___ ___ _____________
Latitude/longitude source:ട GPS ട Topographic map
(Location of well must be shown on a USGS topo map and
attached to this form if not using GPS.)
4a. FACILITY-The name of the business where the well is located. Complete 4a and4b.
(If a residential well, skip 4a; complete 4b, well owner information only.)
FACILITY ID #(if applicable) _________________________________
NAME OF FACILITY_________________________________________
STREET ADDRESS __________________________________________
___________________________________________________________
City or Town State Zip Code
4b. CONTACT PERSON/WELL OWNER:
NAME ____________________________________________________
STREET ADDRESS_________________________________________
5. WELL DETAILS:
a.Total Depth:____________ ft. Diameter:____________ in.
b. Water Level (Below Measuring Point): _________ ft.
Measuring point is _________ ft. above land surface.
6. CASING:Length Diameter
a. Casing Depth (if known): __________ ft. ________ in.
b. Casing Removed: __________ ft. ________ in.
7. DISINFECTION:_____________________
(Amount of 65%-75% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement _________ lb. Cement_________ lb.
Water___________ gal. Water___________gal.
Bentonite
Bentonite lb.
Type:ട Slurry ടPellets
Water______________ gal.
Other
Type material _________________________________
Amount _____________________________________
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
____________________________________________________________
____________________________________________________________
____________________________________________________________
____________________________________________________________
10. WELL DIAGRAM: Draw a detailed sketch of the well on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materials used.
11. DATE WELL ABANDONED ______________________________
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
_______________________________________________________
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
______________________________________________________
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
(The private well owner must be an individual who personally abandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
________________________________________________________________________
PRINTED NAME OF PERSON ABANDONING THE WELL
Submit a copy to the owner and the original to the Division of Water Quality within 30 days.Form GW-30
Attn: Information Management, 1617 Mail Service Center – Raleigh, NC 27699-1617, Phone No. [phone] ext 568.Rev. 5/06
May be in degrees,
minutes, seconds, or in a
decimal format
2725-A
Mike Tynan
Probe Technology, Inc.
4537 Orphanage Rd
Concord NC 28027
704 933-5538
HH-2
✔
Mecklenburg
Charlotte
1701 Westinghouse Blvd, 28273
✔
35 07 28.105
80 56 13.996
✔
Sun Chemical
1701 Westinghouse Blvd
Charlotte NC 28273
Same as above
19 2
8
0
92
92
none
94
6.5
Filled MW from bottom to top through rigid tremmie
pipe with cement/bentonite grout. Surface pavement
completed with concrete.
Removed all screen & riser.
12/2/11
Mike Tynan
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION #___________________________
1. WELL CONTRACTOR:
______________________________________________________
Well Contractor (Individual) Name
______________________________________________________
Well Contractor Company Name
STREET ADDRESS ____________________________________
______________________________________________________
City or Town State Zip Code
(_______) - _____________________
Area code - Phone number
2. WELL INFORMATION:
SITE WELL ID #(if applicable)____________________________________
STATE WELL PERMIT #(if applicable)____________________________
COUNTY WELL PERMIT# (if applicable)_________________________
DWQ or OTHER PERMIT #(if applicable)__________________________
WELL USE (Check applicable use):ട Monitoring ട Residential
ട Municipal/Public ട Industrial/Commercial ട Agricultural
ട Recovery ട Injection ട Irrigation
ട Other (list use) _________________________________________
3. WELL LOCATION:
COUNTY______________ QUADRANGLE NAME _______________
NEAREST TOWN: __________________________________________
___________________________________________________________
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHIC / LAND SETTING:
ട Slope ട Valley ട Flat ട Ridge ട Other_____________________
(Check appropriate setting)
LATITUDE ___ ___ _____________
LONGITUDE ___ ___ _____________
Latitude/longitude source:ട GPS ട Topographic map
(Location of well must be shown on a USGS topo map and
attached to this form if not using GPS.)
4a. FACILITY-The name of the business where the well is located. Complete 4a and4b.
(If a residential well, skip 4a; complete 4b, well owner information only.)
FACILITY ID #(if applicable) _________________________________
NAME OF FACILITY_________________________________________
STREET ADDRESS __________________________________________
___________________________________________________________
City or Town State Zip Code
4b. CONTACT PERSON/WELL OWNER:
NAME ____________________________________________________
STREET ADDRESS_________________________________________
5. WELL DETAILS:
a.Total Depth:____________ ft. Diameter:____________ in.
b. Water Level (Below Measuring Point): _________ ft.
Measuring point is _________ ft. above land surface.
6. CASING:Length Diameter
a. Casing Depth (if known): __________ ft. ________ in.
b. Casing Removed: __________ ft. ________ in.
7. DISINFECTION:_____________________
(Amount of 65%-75% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement _________ lb. Cement_________ lb.
Water___________ gal. Water___________gal.
Bentonite
Bentonite lb.
Type:ട Slurry ടPellets
Water______________ gal.
Other
Type material _________________________________
Amount _____________________________________
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
____________________________________________________________
____________________________________________________________
____________________________________________________________
____________________________________________________________
10. WELL DIAGRAM: Draw a detailed sketch of the well on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materials used.
11. DATE WELL ABANDONED ______________________________
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
_______________________________________________________
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
______________________________________________________
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
(The private well owner must be an individual who personally abandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
________________________________________________________________________
PRINTED NAME OF PERSON ABANDONING THE WELL
Submit a copy to the owner and the original to the Division of Water Quality within 30 days.Form GW-30
Attn: Information Management, 1617 Mail Service Center – Raleigh, NC 27699-1617, Phone No. [phone] ext 568.Rev. 5/06
May be in degrees,
minutes, seconds, or in a
decimal format
2725-A
Mike Tynan
Probe Technology, Inc.
4537 Orphanage Rd
Concord NC 28027
704 933-5538
HH-3
✔
Mecklenburg
Charlotte
1701 Westinghouse Blvd, 28273
✔
35 07 29.557
80 56 12.522
✔
Sun Chemical
1701 Westinghouse Blvd
Charlotte NC 28273
Same as above
22 2
8
0
12 2
12 2
none
94
6.5
Filled MW from bottom to top through rigid tremmie
pipe with cement/bentonite grout. Surface pavement
completed with concrete.
Removed all screen & riser.
12/2/11
12-8-11
Mike Tynan
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION #___________________________
1. WELL CONTRACTOR:
______________________________________________________
Well Contractor (Individual) Name
______________________________________________________
Well Contractor Company Name
STREET ADDRESS ____________________________________
______________________________________________________
City or Town State Zip Code
(_______) - _____________________
Area code - Phone number
2. WELL INFORMATION:
SITE WELL ID #(if applicable)____________________________________
STATE WELL PERMIT #(if applicable)____________________________
COUNTY WELL PERMIT# (if applicable)_________________________
DWQ or OTHER PERMIT #(if applicable)__________________________
WELL USE (Check applicable use):ട Monitoring ട Residential
ട Municipal/Public ട Industrial/Commercial ട Agricultural
ട Recovery ട Injection ട Irrigation
ട Other (list use) _________________________________________
3. WELL LOCATION:
COUNTY______________ QUADRANGLE NAME _______________
NEAREST TOWN: __________________________________________
___________________________________________________________
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHIC / LAND SETTING:
ട Slope ട Valley ട Flat ട Ridge ട Other_____________________
(Check appropriate setting)
LATITUDE ___ ___ _____________
LONGITUDE ___ ___ _____________
Latitude/longitude source:ട GPS ട Topographic map
(Location of well must be shown on a USGS topo map and
attached to this form if not using GPS.)
4a. FACILITY-The name of the business where the well is located. Complete 4a and4b.
(If a residential well, skip 4a; complete 4b, well owner information only.)
FACILITY ID #(if applicable) _________________________________
NAME OF FACILITY_________________________________________
STREET ADDRESS __________________________________________
___________________________________________________________
City or Town State Zip Code
4b. CONTACT PERSON/WELL OWNER:
NAME ____________________________________________________
STREET ADDRESS_________________________________________
5. WELL DETAILS:
a.Total Depth:____________ ft. Diameter:____________ in.
b. Water Level (Below Measuring Point): _________ ft.
Measuring point is _________ ft. above land surface.
6. CASING:Length Diameter
a. Casing Depth (if known): __________ ft. ________ in.
b. Casing Removed: __________ ft. ________ in.
7. DISINFECTION:_____________________
(Amount of 65%-75% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement _________ lb. Cement_________ lb.
Water___________ gal. Water___________gal.
Bentonite
Bentonite lb.
Type:ട Slurry ടPellets
Water______________ gal.
Other
Type material _________________________________
Amount _____________________________________
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
____________________________________________________________
____________________________________________________________
____________________________________________________________
____________________________________________________________
10. WELL DIAGRAM: Draw a detailed sketch of the well on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materials used.
11. DATE WELL ABANDONED ______________________________
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
_______________________________________________________
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
______________________________________________________
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
(The private well owner must be an individual who personally abandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
________________________________________________________________________
PRINTED NAME OF PERSON ABANDONING THE WELL
Submit a copy to the owner and the original to the Division of Water Quality within 30 days.Form GW-30
Attn: Information Management, 1617 Mail Service Center – Raleigh, NC 27699-1617, Phone No. [phone] ext 568.Rev. 5/06
May be in degrees,
minutes, seconds, or in a
decimal format
2725-A
Mike Tynan
Probe Technology, Inc.
4537 Orphanage Rd
Concord NC 28027
704 933-5538
HH-4
✔
Mecklenburg
Charlotte
1701 Westinghouse Blvd, 28273
✔
35 07 29.264
80 56 11.010
✔
Sun Chemical
1701 Westinghouse Blvd
Charlotte NC 28273
Same as above
14 2
8
0
42
42
none
60
4.5
Filled MW from bottom to top through rigid tremmie
pipe with cement/bentonite grout. Surface pavement
completed with concrete.
Removed all casing (4 ft)
12/2/11
12-8-11
Mike Tynan

Appendix D Groundwater Sampling Records