MO-88752_91550_CA_IAR_20190806_Initial Abatement Report

Highlands
Environmental
Solutions, Inc. 8410-D Falls ofNeuse Road; Raleigh, NC 27615
Phone: [phone]/Faz: 919-84842651w .highlandsenvitonmental.com
August 6, 2019
Mr. Ron Tarraban
NCDEQ — UST Section
Mooresville Regional Office
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Subject: Submittal of Initial Assessment Report
Hilco Transport, Inc. — Diesel Fuel Release
4293 NC Highway 24/27; Midland, NC
Project #317028
Dear Mr. Tarraban,
On behalf of Hilco Transport, Inc. please find enclosed an original copy of our Initial Assessment Report
for a diesel fuel release incident that occurred near 4293 NC Highway 24/27 in Midland, North Carolina.
The release occurred as a result of a motor vehicle collision. Based on the results of this investigation,
HES concludes that remediation activities successfully remediated the areas impacted by the release.
We do not recommend any additional assessment or remediation activities.
If there are any questions regarding this correspondence, or the project in general, please contact me at
[phone].
Solutions, Inc.
Staff Geologist

Initial Assessment Report
A. Site Investigation
1. Site Identification
Date of Report: August 6. 2019
Facility #: NA Incident Number: NA Site Rank: NA
Site Name: Hilco — Diesel Fuel Release
Site Street Address: 4293 Highway 24/27: Midland NC
City/Town: Midland, NC Zip Code: 28107 County: Cabarrus County
Description of Geographical Data Point (e.g., dispenser): paved/unpaved areas adjacent to highway
24/27
Location Method (GPS, Topographical Map, Other): GPS
Latitude: 35.252417 N Longitude:-80.501862 W
2. Information about Contacts Associated with the Release
AST Owner:_ Hilco Transport Company Attn: Mr. Drew LaHaie
Address: 7700 Kenmont Road: Greensboro, NC 27409 Phone: [phone]
AST Operator: Hilco Transport Company
Address: 7700 Kenmont Road: Greensboro, NC 27409 Phone: [phone]
Other Person Responsible for Release:
Address:
Phone:
Contractor: First Call Environmental
Address: PO BOX 6035, Ashland, VA 23005 Phone: [phone]
Consultant: Highlands Environmental Solutions, Inc
Address: 8410-D Falls of Neuse Road, Raleigh NC 27615 Phone: [phone]
Analytical Laboratory: Con -test Analytical Laboratory
Address: 39 Spruce Street: East Longmeadow, MA Phone: [phone]
3. Information about the Release
Date of Release: 06-24-19 Ca) 03:20 hrs
Estimated Quantity of the Release: Approximately 85 Gallons
Cause of the Release: Accidental release of diesel fuel due to motor vehicle collision
Source of Release (e.g., AST, piping, etc.): Vehicle Saddle Fuel Tank
Sizes and contents of AST System from which the release occurred: Diesel fuel
4. Certification
I, Joe Beaman, P.G.. RSM. a Licensed Geologist for Highlands Environmental Solutions, Inc., do certify
that the information contained in this report is correct and accurate to the best of my knowledge.
Highlands Environmental Solutio CidAicensed to practice Geology in North Carolina. The
certification number of the com
Highlands
Environmental
Solutions, Inc.

Initial Assessment Report — Hiloo Transport Company
August 6, 2019
B. Background and Initial Response Activities
The subject site is located at 4293 NC Hwy 24/27, in Midland, North Carolina. The approximate location
of the site is graphically presented on Figure 1 (included in Appendix A), and is situated at approximate
coordinates 35.252417 N and-80.501862 W. A topographic map of the area is included as Figure 2. An
aerial photo depicting the site and impacted area is included as Figure 3.
Based on information provided to Highlands Environmental Solutions, Inc. (HES) by Hilco Transport, Inc.
(Hilco) personnel regarding a diesel fuel spill occurred that on June 24, 2019 at the subject property. On
June 24, 2019 an accidental release of diesel fuel occurred during an automobile collision at the subject
site. An estimated 85 gallons of diesel fuel were released. The release impacted a stormwater inlet,
adjacent paved surfaces, and adjacent soils. Initial response activities included the abatement of the
release by use of granular sorbent and sorbent pads. Additionally, clean water was utilized to flush the
impacted stormwater inlet, and fluids were recovered using a vacuum truck.
HES was contracted by Hilco to perform remediation activities for the subject site. Upon being notified of
the release, HES dispatched personnel from First Call Environmental (FCE) for emergency response
services. Personnel from HES and FCE mobilized to the site on July 24, 2019 for emergency response
activities. Initial incident response actions included assessing the extent of the petroleum release and
recovering petroleum product using granular sorbent, boom and a vacuum truck. The release impacted
soils adjacent to Highway 24/27 at the subject property. The release area measured approximately 30
feet long by 9 feet wide.
Prior to any on -site remediation activities, HES noted the NC One -Call Center (811) to mark the area for
buried utilities. A site -specific health and safety plan (HASP) was developed by HES for site activities. A
copy of the HASP is included in Appendix B. A UST-62 form was prepared and submitted to the
NCDEQ-Mooresville Regional Office on June 24, 2019.
C. Free Product Investigation and Recovery
As noted in Section B, the released petroleum product impacted soils adjacent to Highway 24/27 at the
incident location. Response personnel mobilized to the site on July 24, 2019, and recovered free product
that was present at the scene. The free liquid was recovered using granular sorbent, boom and a vacuum
truck. Waste materials were containerized in 55-gallon drums, which were transported to the Hazmat
Emergency Response and Remediation (HERR) facility in Whiteville, NC for disposal. Recovered liquids
were transported to Hazmat Emergency Response and Remediation, Inc. (HERR) located in Whiteville,
NC for disposal. Copies of the waste disposal documents are included in Appendix C.
The impacted stormwater system was flushed with clean water. The flushing liquids were recovered
using a vacuum truck, and transported to the CERT facility in Charlotte, NC for disposal. Copies of the
liquid waste disposal documents are also included in Appendix C.
D. Groundwater and Surface Water Investigation
As noted in Section B, the released petroleum product impacted paved surfaces, a stormwater inlet and
underground piping, and adjacent soils. The release did not impact or threaten surface water bodies.
Groundwater was not encountered during soil excavation activities; therefore a groundwater investigation
was not performed during site activities.
E. Initial Response and Abatement Activities
Initial response and abatement actions are summarized in Section B, above.

Initial Assessment Report— Hilco Transport Company
August 6, 2019
F. Excavation of Petroleum Impacted Soil
HES and FCE personnel were on site to conduct soil excavations activities at the impacted area on July
2, 2019. Excavation activities were performed during the day. Selected photographs and response
activities are included in Appendix D.
Personnel from FCE utilized a track excavator to excavate the petroleum -impacted soil. Excavated soil
was loaded into a dump truck and transported off -site for disposal. Excavation began at the East end of
the impacted area. In this area, the track excavator was used to remove petroleum -impacted vegetation
(grass) and surficial soils. As excavation proceeded, the soils were examined for evidence of petroleum
impacts (i.e. staining or odor). During soil excavation, HES personnel collected random soil samples from
the area, and field screened the samples for organic vapors using a photoionization detector (PID —
MiniRae 3000). To field screen the samples, an aliquot of soil was placed in a clean, labeled, zip -lock
bag and allowed to volatilize. At the end of the volatilization period, the sampling probe for the PID was
inserted into the bag to screen for the presence of organic vapors.
In total, five post -excavation confirmation samples (S-1 through S-5) were collected from the excavated
area. The locations of the excavation and the sample collection locations are depicted in Figure 4. Upon
collection, the samples were placed in labeled, pre -preserved, laboratory -supplied containers, and
maintained on ice pending delivery to the analytical laboratory. These samples were shipped via
overnight courier to Con -test Analytical Laboratory for laboratory analysis of diesel range organics (DRO)
and gasoline range organics (GRO). Sufficient sample volume was also collected and submitted for
expanded analysis of volatile organic compounds (VOCs), by Method 8260; and semi -volatile organic
compounds (SVOCs), by Method 8270 if needed. A summary of the soil analytical data is presented in
Table 1 in Appendix E. The complete laboratory analytical data report and chain -of -custody record for
all samples are included in Appendix F.
In addition to the post excavation soil samples, one waste profile soil sample (CHNC0550 Presample)
and one background soil sample (CHNC0550 Background) were collected by FCE on the date of the
incident. The FCE samples were placed in labeled, laboratory supplied containers, maintained on ice,
and transported to Pace Analytical for laboratory analysis of DRO (by Method 8015C); and benzene,
ethylbenzene, toluene, and xylenes (BTEX), by Method 8260D. Laboratory analytical data for these
samples are also summarized on Table 1. A complete copy of the Pace Analytical data report is included
in Appendix F.
During soil remediation activities, approximately 5.55 tons of petroleum -impacted soil were excavated and
transported to EVO Corp, Inc. in Winston Salem, NC for proper disposal via land application. Copies of
the waste manifest documentation, for the petroleum -impacted soil, are included in Appendix C. The
excavated area was not backfilled, upon request of the property owner.
G. Conclusions and Recommendations
The subject site is located at 4293 NC Highway 24/27; Midland, NC. Based on information provided to
Highlands Environmental Solutions, Inc. (HES) personnel by Hilco Transport, Inc., a diesel fuel spill
occurred on July 24, 2019 at the subject property. The release was an accidental release of diesel fuel
that occurred due to an automobile collision. An estimated 85 gallons of diesel fuel were released.
Soil excavation activities associated with the removal of petroleum -impacted soil at the site were
performed on July 2, 2019, with a total of 5.55 tons of petroleum -impacted soil being removed. All
excavated soil was transported to EVO Corp, Inc. in Winston Salem, NC for proper disposal via land
application. Neither groundwater nor surface water were encountered during soil excavation activities.
A total of five post -excavation soil samples were collected from the excavated area of the site for
confirmation analysis. All confirmation soil samples were submitted to Con -test Analytical Laboratory, a
North Carolina -certified laboratory for analysis of DRO and GRO, Laboratory analysis of the post -
excavation samples resulted in the detection of DRO at concentrations at and slightly below the State

Initial Assessment Report — Hilco Transport Company
August 6, 2019
Action Limit of 100 mg/Kg in two soil samples (S-1 and S-2). As such, the two samples containing the
highest concentrations of DRO (S-1 and S-2) were further analyzed for VOCs and SVOCs. Further
analysis of these samples resulted in the detection of target compounds at concentrations less than their
respective MSCCs.
Based on the results of environmental assessment activities, HES concludes that soil excavation
activities successfully remediated the soil impacted by the petroleum release at this site. HES
recommends a No Further Action Required letter be forwarded to Hilco Transport, Inc. for this incident.

APPENDIX A

Blue Baboons
Funtime Events, Inc
P f
Savings Unlimited Q
6D7
Incident Location
i
f Q
INTRAFITT, INC Fifth'
Midland Town Offi Q 4
SFoundation
Specialty
Products & Insitn suing Materials 27
4
2z
Hwj 24
A
Speedway P Sundae Shot-
a
Got P Studio 601
OJO Flowe Grading I
Company
4
Approximate Scale N
0 125 250
feet
Base diagram from Google Maps Site Location Diagram
Drawing / Project Name
Diesel Fuel Release
Highlands Midland, NC
Client
zz
Environmental Hilco Transport, Inc
Project # DB PM Fig.
Solutions, Inc. 317028 AF JB
Scale Date PG PE
As Shown I June 2019 JB

derap
j � 1 !!- J f
/ a Incident Location
_•
ir
��f fit• � � '
N s11 �- tl�__ ! • 36•
i V
gh
a
,\
41
0 ,; •J:
N
Base diagram from USGS Topographic Quadrangle; Concord, NC;
1991 Topographic Location Diagram
Drawing / Project Name
Diesel Fuel Release
Highlands Midland, NC
Client
Environmental Hilco Transport, Inc.
Project # D11 I PM Fig.
Solutions, Inc. 317028 AF JB
Scale Date PG PE 2
Not to Scale I July 2019 JB

Legend
NC Highway 24/27
Parkl'ing Lot
wawing Name
Soil Excavation and Sampling Diagram
Approximate Scale
0 5 10
feet

APPENDIX B

Highlands
Environmental
Solutions, Inc.
Highlands Environmental Solutions, Inc.
HEALTH AND SAFETY PLAN
For Site Activities at:
Soil Remediation Activities
4293 NC Hwy 24/27; Midland, NC
June 2019
Minimum Level of Protection at this site is Level D
Contaminants of Concern are Petroleum Hydrocarbons
Joe Beaman
Project Manager
The information in this HASP is provided solely for the protection of the health and safety of Highlands
Environmental Solutions employees and subcontractors working under the direct supervision and control of
Highlands Environmental Solutions on this project. Highlands Environmental Solutions assumes no liability
for, or responsibility to, any other parties for the accuracy or completeness of the information contained herein
for any use or reliance upon this HASP by any other party.

Streamlined Health and Safety Plan
4293 NC Hwy 24/27; Midland, NC
Page 2
June 2019
SITE EMERGENCY FORM
Contaminants of Concern: Petroleum Hydrocarbons
Minimum Level of Protection: Level D
Do not endanger your life. Survey the situation before taking any action.
Highlands Environmental Solutions Office
[phone]
Telephone:
Site Location Address:
4293 NC Hwy 24/27' Midland, NC
Telephone Located at:
HES Personnel (cellular phone)
EMERGENCY IN THE EVENT OF ANY EMERGENCY, CONTACT PROJECT MANAGER OR
PHONE NUMBERS HEALTH AND SAFETY REPRESENTATIVE
Ambulance:
911
Fire:
911
Police:
911
Hospital Name:
Carolinas Health Care System — Northeast
Hospital Phone:
704-403-3000
Project Manager:
Joe Beaman
Health and Safety Specialist:
Andrew Francis
Client Contact:
Drew Lahaie 336-389-4011
Poison Control:
[phone]
State Agency:
NCDEQ (MRO) 704-663-1699
UTILITY MARKER EMERGENCY TELEPHONE NUMBERS
Utility
Color Code
Telephone Number
Water
Blue
[phone]
Gas
Yellow
[phone]
Electric
Red
[phone]
Telephone
Orange
[phone]
Cable
Orange
[phone]
Sewer
Green
800 632-4949
Dig Safe Telephone Number: [phone]

Streamlined Health and Safety Plan
4293 NC Hwy 24/27; Midland, NC
Page 3
June 2019
HOSPITAL LOCATION MAP
rrMooresville
k ;
Davidson
Corbel lUS
ku
"- �
Huntersville
Charlotte
Gold Hill
KannapoliS
920 CN&ch St N,
Concord 28025
Q Alb
Harrisburg
v
4293 NC-24,
Midland, NC 28107
Mint H.3
Morning Star Acres
Matthews
Pme"lle
Stallings Unionville
Providence Indian Trail
Weddington
Directions: Hospital Information:
Turn left on US 601; bear right on US 601 N bypass; Name: Carolinas Healthcare NE
bear right on US 29 N (Warren Coleman Blvd N; Address: 920 Church Street N
turn right on NC 73; Turn left on Church Street N; City, State: Concord, NC
continue to hospital Phone: 704

Health and Safety Plan
4293 NC Hwy 24/27; Midland, NC
Page 4
June 2019
FIRST AID FOR PETROLEUM HYDROCARBON EMERGENCIES
Ingestion: DO NOT INDUCE VOMITING. Call Poison Control; follow instructions. Administer
cardiopulmonary resuscitation (CPR), if necessary. Seek medical attention.
Inhalation: Remove person from contaminated environment. DO NOT ENTER A CONFINED
SPACE TO RESCUE SOMEONE WHO HAS BEEN OVERCOME UNLESS
PROPERLY EQUIPPED AND A STANDBY PERSON IS PRESENT. Administer
CPR if necessary. Seek medical attention.
Skin Contact: Brush off dry material, remove wet or contaminated clothing. Flush skin thoroughly
with water. Seek medical attention if irritation persists.
Eye Contact: Flush eyes with water for 15 minutes. Seek medical attention.
Exposure Symptoms: Headache, dizziness, nausea, drowsiness, irritation of eyes, nose, throat, breathing
difficulties.
Contingency Plan: Report incident to Project Manager (PM) after emergency procedures have been
implemented.
RESPONDER MUST HAVE A CURRENT CERTIFICATE TO ADMINISTER FIRST AID OR CPR
1. Survey the situation. Do not endanger your own life. DO NOT ENTER A CONFINED SPACE TO
RESCUE SOMEONE WHO HAS BEEN OVERCOME UNLESS PROPERLY EQUIPPED AND A
STANDBY PERSON IS PRESENT.
2. Call 911 (if available) or the fire department IMMEDIATELY. Explain the physical injury, chemical
exposure, fire, or release.
3. Decontaminate the victim without delaying life-saving procedures.
4. If the victim's condition appears to be noncritical, but seems to be more severe than minor cuts,
he/she should be transported to the nearest hospital by trained Emergency Medical Services (EMS)
personnel: let the doctor assume the responsibility for determining the severity of the injury. If the
condition is obviously serious, EMS must transport the victim.
5. Notify the PM.

Health and Safety Plan
4293 NC Hwy 24/27; Midland, NC
Page 5
June 2019
EMERGENCY FIRST AID PROCEDURES
To Stop Bleeding
1. Give medical statement.
2. Assure airway, breathing, and
circulation.
3. Use DIRECT PRESSURE over the
wound with clean dressing or your
hand (use nonpermeable gloves).
Direct pressure will control most
bleeding.
4. Bleeding from an artery or several
injury sites may require DIRECT
PRESSURE on a PRESSURE
POINT. Use pressure points for
30 - 60 seconds to help control
severe bleeding.
5. Continue primary care and seek
medical aid as needed.
CPR
1. Call for help.
2. Arousal: check for consciousness.
3. Open airway with chin -lift.
4. Look, listen, and feel for breathing.
5. If breathing is absent, give 2 slow, full
rescue breaths.
6. Check the pulse for 5 to 10 seconds.
7. If pulse is present, continue rescue
breathing: 1 breath every
5 seconds
8. If pulse is absent, start CPR:
15 compressions, 2 breaths (1 man)

Health and Safety Plan Page 6
4293 NC Hwy 24/27; Midland, NC June 2019
Project and Health and Safety Information
HES will be performing an environmental remediation at the subject site on behalf of Hilco Transport Company
at the subject site.
All work will comply with the Occupational Safety and Health Act (OSHA) standard, "Hazardous Waste
Operations and Emergency Response," (29 CFR 1910.120), and other federal, state and local procedures that
require the development and implementation of a HASP. Generation of this document certifies that the
workplace has been evaluated for the hazards as described. A hazard assessment has been performed and
the adequacy of the personal protective equipment (PPE) selected is hereby certified per 29 CFR 1910.132(d)
and is duly noted by the signature(s) and date appearing on the cover page of this document. If any site
conditions are encountered that are different from typical retail petroleum operations, the field investigator is to
stop work immediately and notify the Project Manager.
This plan addresses the safety issues associated environmental investigation and assessment activities
performed at retail petroleum operations. For this project, site investigation activities will involve the
following (checked items):
Phase I Environmental Site Assessment
Phase II Environmental Site Assessment
x
Spill Response and Abatement
Soil sampling hand auger)
Soil sampling (drilling)
Monitoring well installation
UST removal (requires full HASP
x
Soil excavation
Groundwater sampling/monitoringsampling/monitoring
Groundwater remediation
Drum removal
Site surveying
Soil Gas / VI assess ment/surve
Pump/Slug testing
All activities of this project will be carried out under Level D or Modified Level D. At a minimum, all personnel
will wear the following PPE based on the task to be performed at the site (checked items):
x
Hard Hat
x
Safety Vest
x
Steel Toe Boots
Chemical Boots
x
Nitrile gloves (sampling loves
Heavy Nitrile gloves
x
Safety lasses
Ear plugs/ear muffs sound suppression
White Tyvek
Yellow of coated Tyvek

Health and Safety Plan
4293 NC Hwy 24/27; Midland, NC
Page 7
June 2019
HAZARD IDENTIFICATION AND CONTROL
Precautions must be taken to prevent injuries and exposures to the following potential hazards.
Potential Hazards and Control
Potential Hazard II Control
Exposure to 1. Stand up -wind of petroleum products whenever possible.
Petroleum 2. Minimize contact and contact time with petroleum products.
Products 3. Avoid walking through discolored areas, puddles, leaning on drums, or
contacting anything that is likely to be contaminated.
4. Do not eat, drink, smoke and/or apply cosmetics in the hot or warm zones.
5. Wear gloves when in contact with contaminated surfaces.
6. Safety glasses must be worn at a minimum.
7. Splash goggles must be worn when working with liquids.
8. >25 ppm organic vapors in breathing zone requires upgrade to Level C.
9. >250 ppm organic vapors in breathing zone requires upgrade from
Level C to Level B.
10. If unknown materials are encountered, call the HSS.
Vehicular
1.
Wear traffic safety vest when vehicle hazard exists.
Traffic
2.
Use cones, flags, barricades, and caution tape to define work area.
3.
Use vehicle to block work area.
4.
Engage police detail for high -traffic situations.
Vault Entry
1.
HES Personnel do not perform Confined Space Entry.
Utility Lines
1.
Contact Dig Safe to have utility lines marked prior to excavation/trenching.
Contact
2.
Refer to site drawings or customer interviews if on private property for
utility locations.
3.
Hand dig 3 to 5 feet down and 5 feet each side of utility marker to avoid
breaking utility lines.
Inclement
1.
Stop outdoor work during electrical storms and other extreme weather
Weather
conditions such as extreme heat or cold temperatures.
2.
Take cover indoors or in vehicle.
3.
Listen to local forecasts for warnings about specific weather hazards such
as tornados, hurricanes, and flash floods.
Noise 1. Wear hearing protection when equipment such as a drill rig, jackhammer,
cut saw, air compressor, blower or other heavy equipment is operating on
the site.
2. Wear hearing protection whenever you need to raise your voice above
normal conversational speech due to a loud noise source; this much noise
indicates the need for protection.

Health and Safety Plan
4293 NC Hwy 24/27; Midland, NC
Page 8
June 2019
Potential Hazard II Control
Electric 1. Maintain appropriate distance from overhead utilities;
Shock 20-foot minimum clearance from power lines required;
10-foot minimum clearance from shielded power lines.
2. Use ground -fault circuit interrupters as required.
3. Perform lockout/tagout procedures (Appendix C).
4. Use three -pronged plugs and extension cords.
5. Contact your local underground utility -locating service.
6. Follow code requirements for electrical installations in hazardous
locations.
Physical
1.
Wear hard hats and safety glasses when on -site.
Injury
2.
Maintain visual contact with the equipment operator and wear orange
safety vest when heavy equipment is used on -site.
3.
Avoid loose -fitting clothing (driller and driller's helper).
4.
Prevent slips, trips and falls; keep work area uncluttered.
5.
Keep your hands away from moving parts (i.e., augers).
6.
Test the emergency shutoff switch on the drill rig daily.
Back Injury
1.
Use a mechanical lifting device or a lifting aid where appropriate.
2.
If you must lift, plan the lift before doing it.
3.
Check your route for clearance.
4.
Bend at the knees and use leg muscles when lifting.
5.
Use the buddy system when lifting heavy or awkward objects.
6.
Do not twist your body while lifting.
Heat Stress
1.
Increase water intake while working.
2.
Increase number of rest breaks and/or rotate workers in shorter work
shifts.
3.
Watch for signs and symptoms of heat exhaustion and fatigue.
4.
Plan work for early morning or evening during hot months.
5.
Use ice vests when necessary.
6.
Rest in cool, dry areas.
7.
In the event of heat stroke, bring the victim to a cool environment and
initiate first aid procedures.
Cold Stress
1.
Take breaks in heated shelters when working in extremely cold
temperatures .
2.
Remove the outer layer of clothing and loosen other layers to promote
evaporation of perspiration, upon entering the shelter.
3.
Drink warm liquids to reduce the susceptibility to cold stress.
High Crime
1.
Be aware of surroundings.
Areas
2.
Use the buddy system.
3.
Request police detail when appropriate.
Insects
1.
Tuck pants into socks.
2.
Wear long sleeves.
3.
Use insect repellent.
Poisonous Plants
1.
Don't enter areas infested with poisonous plants.
(Such as Poison
2.
Immediately wash any areas that come into contact with poisonous plants.
Ivv, Oak, etc.)

Health and Safety Plan
4293 NC Hwy 24/27; Midland, NC
Page 9
June 2019
Potential Hazard II Control
Ladders 1. Make sure ladder rungs are sturdy and free of cracks.
2. Use ladders with secure safety feet.
3. Pitch ladders at a 4:1 ratio.
4. Secure ladders at the top when possible.
5. Do not use ladders for access to air stripper towers.
6. Use non-conductive ladders near electrical wires.
Fire Control 1. Smoke only in designated areas.
2. Keep flammable liquids in closed containers.
3. Keep site clean; avoid accumulating combustible debris such as paper.
4. Follow Hot Work Safety Procedures when welding or performing other
activities requiring an open flame.
5. Isolate flammable and combustible materials from ignition sources.
6. Ensure fire safety integrity of equipment installations according to Hazard
Classification Diagram (Appendix G).
Static Electricity 1. Do not create static discharge in flammable atmospheres.
2. Electrically bond and ground pumps transfer vessels, tanks, drums,
bailers and probes, when moving liquids.
3. Electrically bond and ground vacuum trucks and the tanks they are
emptying.
4. Do not splash fill containers with flammable liquids.
Drilling/Boring
1.
Driller and helper must be present during all active operations.
Operations
2.
Driller helper and other site personnel must know location of emergency
shut off switch.
3.
Unauthorized personnel must be kept clear of drilling rig.
4.
Area of drilling operation must be cordoned off/barricaded.
5.
When hazardous conditions are deemed present, operation must be shut
down.
Well Installation,
1.
Wear appropriate PPE to avoid skin, eye, and inhalation contact with
Well
contaminated groundwater and/or soil.
Development,
2.
Stand upwind when conducting tasks and minimize possible inhalation
Well Gauging,
exposure; especially when first opening monitoring wells.
Well Bailing,
3.
Conduct air monitoring to determine level of respiratory protection.
Soil/Ground-
4.
Utilize engineering controls such as portable venturi air movers to draw
water Sampling
away or blow away chemical vapors.
Welding, Cutting,
1.
Before conducting welding at a project site, contact the Project Manager..
Brazing
Cleaning 1. Wear appropriate PPE to avoid skin and eye contact with isopropyl
Equipment alcohol, alconox, or other cleaning materials.
2. Stand upwind to minimize any potential inhalation exposure.
3. Dispose of spent cleanina solutions and rinses accordinalv.
First aid kit, emergency eye wash station, fire extinguisher, and absorbent
pads will be located on -site in the vehicle or site remediation system.

Health and Safety Plan
4293 NC Hwy 24/27; Midland, NC
Page 10
June 2019
Signature Sheet
All persons entering the work zone, or visiting the subject site for the purposes associated with the subject
investigation(s), or activities associated with the subject investigation(s) are required to notify the HES
representative on -site immediately upon arrival. All persons entering the work zone, or visiting the subject site
for the purposes associated with the subject investigation(s), or activities associated with the subject
investigation(s) are required to review appropriate health and safety procedures, and provide a signature
documenting they have been properly briefed on health and safety policies and procedures to be followed
while on -site. HES will not be responsible for personal injuries or death resulting from personal actions that
are considered negligent, or that result from personal activities that are contrary to this health and safety plan.
By my signature, I acknowledge that 1 have been briefed on site specific health and safety procedures,
that 1 am familiar with said health and safety procedures, and that I will follow all indicated health and
safety procedures while on -site.
Name
Signature

APPENDIX C

NON -HAZARDOUS
1 1. Generator ID Number
2. Page 1 of
3. Emergency Response Phone
4. Waste Tracking Number
WASTE MANIFEST
5. Generator's Name and Mailing Address
- Generators Site Address (if different than mailing address)
Generators Phone:
'
6. Transporter 1 Company Name s..
U.S. EPA ID Number
7. Transporter Company Name
U.S. EPA ID Number
8. Designated Facility Name and Site Address
U.S. EPA ID Number
Facil 's Phone:
9. Waste Shipping Name and Description
10. Containers
11. Total
12. Unit
No.
Type
Quantity
Wt.Nol.
1.
wi
W
2.
3.
4.
13. Special Handling Instructions and Additional Information
14. GENERATOR'StOFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by the proper shipping name, and are classified, packaged,
marked and Wbeled/placarded, and an> in all respects in pmper condition for transport according to applicable international and national governmental regulations.
GeneratursKaferors Prinled?yped Nam@
Signature
Month
Day Year
ri
15. International Shipments
❑ Impod to U.S.
❑Expos four, oU.S. Pod ofentry/exit:
Z
Transporter Signature for exports o
Date leaving U.S.:
tit
16. Transporter Acknowledgment of Receipt of Materials
_
¢
Transporter l Printed4ypeci Name
sign .
Month
Day Year
N
r�
Transporter PrintedrTyped Name
Signature
Monts
Day Year
t-
17. Discrepancy
17a. Discrepancy Indication Space ❑ cas ntiy
❑ Type ❑ Residue
El Partial Rejection
I
❑Full
Rejection
Manifest Reference Number:
r
17b. A8emate Facility (or Generator)
U.S. EPA ID Number
J
U
rai
Facklys Plmre:
w
17c. Signature of Alternate Facilely (or Generator)
Month
Day Year
z
0
or
0
18. Designated Facility Caner or Operator. Codification of receipt
of materials covered by the manifest except as noted in Item 17a
Pdmedfyped Nave
Signatu/
Month
Day Year
?, t I
{%
169-BLS-C 5 11979 (Rev. 9/09) GENERATOR'S/SHIPPER'S INITIAL COPY

revo
CORPORATION
1703 Vargrave Street
Wlnalon-Salem, NO 27107
ph 336-725-SB44
fax [phone]
CERTIFICATE OF DISPOSAL
Eva Corporation does hereby certify that 5.55 tons of non -hazardous
contaminated material received on 7/2/2109 from:
Generator: Hilco Transport, Inc.
Originating at: 4293 NC-24
Midland, NC
EC Waste ID #: 071909
has been disposed of by Eva Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Eva Corporation
www.evomrp.netTHE NEXT LEVEL.

NOiFNAZARDOUS
t. Generator ID Number
2. Page i of
3. Emergency Response Phone
4. WastalTmiling Number
WASTE MANIFEST
I
I I,.
5. Generators Name and Mailing Address
Generabys She Address (if &farem ban mailing address)
Gars wri Phone:
6. Transporter i Company Name
U.S. EPA IO Number
7. Transporter Company Name
U.S. EPA ID Number
6. Designated Facility Name and Stle Address
U.S. EPA ID Number
Fang 'a Phone:
B. Waste Shipping Name and Description
10. Candiners
II.TOW
DuaMhy
12. Unit
WLNoI
No.
Type
W
so
2'
J
tl
3.
3
C.
13. Special Handling Instructors and Additional Inbrmaeon
14. GENERATOR'SIOFFEAOR'S CERTIFICATION: I hereby declare
that the contents of Oils consignment arehAly and acantefy described above
by the proper shipping home, and are dassbod, packaged,
marked awCtabeledlplacarded, and are in all respects in proper cond6on For transport according to apoo" international and national gmmmantal regulations.
Genendoesr0aerors Prmtecirryped Name
Swebae
Month Day
Year
LJ 15.Inumational Shipments ❑Import to U.S.
❑evost0an U.S. Pal of erMyfmit:
z Transporter Sionature for exports only):
w 16. Transporter Acknowledgment of Receipt of Materials
Date learn U.S.:
Our
Transporter 1 PrinteElFyped Name
BE
s
Signature
Month Day
Year
ri
Transporter Prntedrlyped Name
Syalure
Month Day
Year
17. Discrepancy
1 17a. Discrepancy Indication Space ❑entity
❑ Type ❑ Residue
❑ Padial Re action
❑ Full Reckon
Manifest Reference Number:
T 17b. Alternate Faciiry, (m Gemrator)
tJ
U.S. EPA ID Number
U
u Facgity's Phone:
0 170. Signature of Alternate Facility (or Generator)
Month Day
Year
2
to
W
O
16. Designated facility Owner or Operator: Certification of receipt of malenals ocuered by the manifest except as noted in Item 17a
Prntedrryped Name r
Signature
Month Day
Year
169-BLS-C 5 11972 (Rev. 9M9) TRANSPORTER #2

63382119
CERTIFIED
AUTOMATED
TRUCK
SCALE
CAT SCALE COMPANY
P.D. BOX 630
WALCOT ,, IA 52773
[phone]
www.catscale.com
THE CAT SCALE GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight- What makes
us different from other scale companies is that we back up our guarantee with cash e
WEIGH WHAT WE SAY OR WE PAY®
If you get an overweight One from the state AEg@ one of our CAT Scales showed a legal weight, we will
Immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight One If our scale is wrong, OR
(2) A representative of CAT Scale Company will appear In court WITH the driver as an expert witness If we
believe our scale was correct
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
11 Post bond and request a court date.
2) Call CAT Scale Company direct 24 hours a day at 1.877-CATSCALE, ext. 7 (Tall Free) or visit www.catwMeguarantes.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department -
DATE:
13: 15 SCALE:
60321911 LOCATION:
PUBLIC WEIGHMASTER'S
CERTIFICATE OF
WEIGHT & MEASURE
WEIGH NUMBER
-L911
•The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale.
7-02-19 STEER AXLE 1. S'720 1 b
DRIVE AXLE 2 1 9 4 0 1 b
405
PILOT 56 TRAILER AXLE 00 1 b
I 85 EXIT 63 GROSS WEIGHT 3-7660 1 b
KANNAPOLIS NC
This Is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy walghmasler, and when property signed and sealed shall be prime facts evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK. PRODUCE. PROPERTY. COMMODITY, ORARncLE wEIGHED FREIGHT ALL KINDS
COMPANY H I LC❑ TRACTOR �, 16219 TRAILER 0000
WEIGHMAS rEH OR TICKET 4 OF
FEE $11.50 WEIGHER SIGNATURE FUL$WEIGH
HEILA CULVE (IFREWENdHi
0 CAT SW a- Reg 3D67711e

Plana esid by J. & KE LER a ASSODATES Na-a.14a�14 MII • V9r,.IadDl �7�•/a�sa��iRWiNkBaraSres
NONd1A7.ANf1OMS
1. Generetar ID Number
2 Page 1 of
& Emergency Response Phone
4. Waste Traddrg Numbst
WASTE MANIFEST'
-
5. Generabfs Name and Malang Address
GeneralMs Site AdSM fit 8 tlan missing address)
WooT�
�o� c rr-\ Nw.1 a` wq
R
M\ar
Geareloye Phora: L
6. Transporter 1 Cgrgany Name
U.S. EPA 9 Menber
\i
"
7. Trereporte2 Conparry Name
U.S. EPA ID NwlDer
8. Desgnated FarB1y, Name aridSite Address U.S. EPA ID Number
39a 59LkG, ����b�
�T11TG.V11\t 1vv
F es Ph" gio— _
10. Containers
11. Total
12. UN
9. Waste Shipping Name and Description
Guaney
WINN.
No.
Type
°
Od5
QM
P
w
2pI� CON I VIAO^ P c.R-W
e C + vo�w. ,
3.
4.
13. Special Nara" Instructors and Additional IMomalm
14. G91 MATORSAFFEAOWS CERTIFICATION: I hereby declare that the patients of 8!s conviowed are hay and accurately described above byme proper shgping name, and are classified, packaged.
marked and IabdedrplacaNed, and we in all respects in
propero,,fton for transportaccardag to appirable mlematioW and national gon mmentai regulations.
Geneato'&OWs Pape0yped Nana
Sgahrta
Month Day Year
°1
U lr
J 15.4denatierd Shprrens Impost to U.S.
❑ E>pmt horn U.S. Pon of etrylexh:
Transporter SWature Pe ns on :
new leanrlo U.S.:
¢ 16. Transporter AWpx7ediment of Receipt of Materials
Month Day Year
Transporter 1 Prtdernypho Name
O
n
2 Pnaedrfyped Name
MaM Day Year
r-
17. Discrepancy
17a. Discrepancy Indcaeon Space ❑ Ouantity
❑ Type ❑ Residue ❑ Parted Rejection
❑ Full Rejection
Manifest Reference Number:
> 171b. Abemae Faciity (or Generatorll
EJ
U.S. EPA ID Number
U
u. FwW. Phone:
0 17c. Signature of AAEmale Faaliy, (or Generator)
Monty Da Year
y
f
z
z
°
N
W
°
18- Designated Fac9dy, Owner or Operator Certification of receipt of maw" covered by the manifest except as noted in Item 17a
PnntedTyped NAa+a--_
Slgnalur
Month Day Year
vedaa cr c �toso yaw„ omol " / DESIGNATED FACILITY TO GENERATOF

APPENDIX D

Highlands
Environmental
Solutions, Inc.
Photograph Number 1: Incident scene during initial abatement activities.
Phntnnrnnh Number 9• Imnactpri arpa of nnrkinn Int rturinn initial ahatpmpnt activities

Highlands
Environmental
Solutions, Inc.
Photograph Number 4: Impacted area of median/shoulder before excavation.

MIN Highlands
Environmental
Solutions, Inc.
a�.
• f _c
.%f'�,k.�C �!N�.' �.? r . ! •''.,M �ne t.`tn �' a.._ f � � � sy
Photooraph Number 5: Photo of the beainnina of the excavation
Photograph Number 6: Photo of the excavation area

Highlands
Environmental
Solutions, Inc.
;'a T
R.r r
Photograph Number 8: Photo of excavation area

Highlands
EnvlronmeMal
Solutions, Ine.
Photograph Number 9: Photo of final excavation area (property owner backfilled and provided
sod cover).

APPENDIX E

Table 1
Hilco Transport Company
Diesel Fuel Release Incident - Intersection of NC24/27 & US Hwy 601; Midland, NC
HES Project #317028
Summary of Analytical Data
(Soil Samples)
Analytical Method (e.g., VOC by EPA 8260B) 0
Field
5035 / 8015
8260D (mg/Kg)
8270E (mg/Kg)
Constituent of Concern
01
m
m
R y
(n
°
tea,
V
'c
o
C
'o
`o
d
Q.
L
C
47
N
R C
Sample ID Number
p
d a
c Y
rn
x
a
y
c
°
`m °
Collection
Sample
° a
E rn
a, rn°
N
07
°
c °-
I:
-
t
m
H>
CO x
c
R
E
Date
Depth (ft.
p
o
y 0
a� O
Q
.•
O o
o
L
U
o
>
a
w
O o
BGS)
d
C)
O
_ V
Q
N
N
T
LL
_ V
Q
m
CO
W
CHNC0550 Background
06/24/19
Surface
na
7.4
ND
ND
na
na
na
na
na
na
ND
CHNC 0550 Presample
06/24/19
Surface
na
289
ND
ND
na
na
na
na
na
na
ND
S-1
7/2/19
0.50
0.10
ND
93
0.042J
ND
0.13J
ND
ND
ND
ND
ND
ND
S-2
7/2/19
0.50
0.00
ND
100
0.083j
ND
0.21J
0.14
0.15J
0.14J
0.14J
0.14J
ND
S-3
7/2/19
0.50
0.00
ND
67
na
na
na
na
----na7
na
na
na
na
S-4
7/2/19
0.50
0.00
ND
54
na
na
na
na
na
na
na
na
na
S-5
7/2/19
0.50
0.00
ND
13
na
na
na
na
na
na
na
na
na
NCDEQ State Action Limit (mg/kg)
50
100
NCDEQ Soil -to -Water MSCC (mg/kg)
24
cs
1.2
6400
6.6
39
290
270
cs
Notes: "ND" denotes not detected. "cs" denotes compound specific. "J" denotes estimated value. "na" denotes not analyzed.
Bold denotes concentration equal to or greater than State Action Limits or Soil to Water MSCC.
1 of 1

APPENDIX F

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
July 16, 2019
Joe Beaman
Highlands Environmental Solutions, Inc.
8410-D Falls of Neuse
Raleigh, NC 27615
Project Location: Midland, NC
Client Job Number:
Project Number: 317028
Laboratory Work Order Number: 19GO278
Enclosed are results of analyses for samples received by the laboratory on July 5, 2019. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 22

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
19GO278-01
19GO278-02
19GO278-03
19GO278-04
19GO278-05
Sample Preparation Information
QC Data
Petroleum Hydrocarbons Analyses
B234917
B235063
B235508
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
7
9
11
13
15
16
16
16
16
16
18
19
20
Page 2 of 22

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Highlands Environmental Solutions, Inc.
8410-D Falls of Neuse REPORT DATE: 7/16/2019
Raleigh, NC 27615 PURCHASE ORDER NUMBER:
ATTN: Joe Beaman
PROJECT NUMBER: 317028
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 19GO278
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: Midland, NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
S-1
19GO278-01
Soil
SM 254OG
SW-846 8015C
S-2
19GO278-02
Soil
SM 2540G
SW-846 8015C
S-3
19GO278-03
Soil
SM 254OG
SW-846 8015C
S-4
19GO278-04
Soil
SM 254OG
SW-846 8015C
S-5
19GO278-05
Soil
SM 2540G
SW-846 8015C
Page 3 of 22

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
SW-846 8015C
Qualifications:
MS-22
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is
within method specified criteria.
Analyte & Samples(s) Qualified:
Diesel Range Organics
B234917-MSI
Z-01
Results in the diesel range organics do not appear to be petroleum related.
Analyte & Samples(s) Qualified:
Diesel Range Organics
19G0278-01RE1[S-1]
SW-846 8015C
Gasoline Range Organics (2-Methylpentane through 1,2,4-Trimethylbenzene) is quantitated against a calibration made with an unleaded gasoline composite standard.
Diesel Range Organics (C10-C28) is quantitated against a calibration made with a #2 fuel oil standard.
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
d�
Lisa A. Worthington
Technical Representative
Page 4 of 22

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-1 Sampled: 7/2/2019 10:15
Sample ID: 19G0278-01
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 1.3 1.3 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 15:39 KMB
Diesel Range Organics 93 9.8 3.5 mg/Kg dry 1 Z-01 SW-846 8015C 7/15/19 7/16/19 9:58 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 109 70-130 7/9/19 15:39
2-Fluorobiphenyl 62.0 40-140 7/16/19 9:58
Page 5 of 22

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-1 Sampled: 7/2/2019 10:15
Sample ID: 19G0278-01
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 84.4 % Wt 1
SM 2540G 7/8/19 7/9/19 8:01 JDN
Page 6 of 22

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-2 Sampled: 7/2/2019 10:20
Sample ID: 19G0278-02
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 0.94 0.91 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 16:14 KMB
Diesel Range Organics 100 9.8 3.5 mg/Kg dry 1 SW-846 8015C 7/6/19 7/12/19 23:53 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 108 70-130 7/9/19 16:14
2-Fluorobiphenyl 55.7 40-140 7/12/19 23:53
Page 7 of 22

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-2 Sampled: 7/2/2019 10:20
Sample ID: 19G0278-02
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 84.8 % Wt 1
SM 2540G 7/8/19 7/9/19 8:01 JDN
Page 8 of 22

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-3 Sampled: 7/2/2019 10:30
Sample ID: 19G0278-03
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 1.5 1.4 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 16:49 KMB
Diesel Range Organics 67 10 3.6 mg/Kg dry 1 SW-846 8015C 7/6/19 7/13/19 0:34 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 113 70-130 7/9/19 16:49
2-Fluorobiphenyl 50.1 40-140 7/13/19 0:34
Page 9 of 22

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-3 Sampled: 7/2/2019 10:30
Sample ID: 19GO278-03
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 83.2 % Wt 1
SM 2540G 7/8/19 7/9/19 8:01 JDN
Page 10 of 22

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-4 Sampled: 7/2/2019 10:45
Sample ID: 19G0278-04
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 1.3 1.3 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 17:24 KMB
Diesel Range Organics 54 46 17 mg/Kg dry 5 SW-846 8015C 7/6/19 7/12/19 23:53 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 113 70-130 7/9/19 17:24
2-Fluorobiphenyl 61.0 40-140 7/12/19 23:53
Page 11 of 22

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-4 Sampled: 7/2/2019 10:45
Sample ID: 19G0278-04
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 90.0 % Wt 1
SM 2540G 7/8/19 7/9/19 8:02 JDN
Page 12 of 22

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-5 Sampled: 7/2/2019 11:00
Sample ID: 19G0278-05
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 1.3 1.3 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 17:59 KMB
Diesel Range Organics 13 9.3 3.4 mg/Kg dry 1 SW-846 8015C 7/6/19 7/13/19 0:14 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 109 70-130 7/9/19 17:59
2-Fluorobiphenyl 51.3 40-140 7/13/19 0:14
Page 13 of 22

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-5 Sampled: 7/2/2019 11:00
Sample ID: 19G0278-05
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 89.3 % Wt 1
SM 2540G 7/8/19 7/9/19 8:02 JDN
Page 14 of 22

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]
Batch
Date
19G0278-01 [S-1]
B234960
07/08/19
19G0278-02[S-2]
B234960
07/08/19
19G0278-03[S-3]
B234960
07/08/19
19G0278-04[S-4]
B234960
07/08/19
19G0278-05 [S-5]
B234960
07/08/19
Prep Method: SW-846 3546-SW-846 8015C
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
19G0278-02[S-2]
B234917
30.0
1.00
07/06/19
19G0278-03 [S-3]
B234917
30.1
1.00
07/06/19
19G0278-04[S-4]
B234917
30.2
1.00
07/06/19
19G0278-05[S-5]
B234917
30.0
1.00
07/06/19
Prep Method: SW-846 5030B-SW-846 8015C
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
19G0278-01[S-1]
B235063
5.10
5.80
07/09/19
19G0278-02[S-2]
B235063
7.80
6.20
07/09/19
19G0278-03[S-3]
B235063
4.70
5.80
07/09/19
19G0278-04[S-4]
B235063
4.70
5.50
07/09/19
19G0278-05[S-5]
B235063
4.70
5.50
07/09/19
Prep Method: SW-846 3546-SW-846 8015C
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
19G0278-01RE1 [S-1]
B235508
30.2
1.00
07/15/19
Page 15 of 22

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B234917 - SW-846 3546
Blank (B234917-BLK1)
Prepared: 07/06/19 Analyzed: 07/09/19
Diesel Range Organics
ND
8.3
mg/Kg wet
Surrogate:2-Fluorobiphenyl
LCS (B234917-BS1)
2.00
mg/Kg wet
3.33 60.0
Prepared: 07/06/19 Analyzed: 07/09/19
40-140
Diesel Range Organics
25.7
8.3
mg/Kg wet
33.3 77.1
40-140
Surrogate:2-Fluorobiphenyl
LCS Dup (B234917-BSD1)
2.73
mg/Kg wet
3.33 82.0
Prepared: 07/06/19 Analyzed: 07/09/19
40-140
Diesel Range Organics
25.0
8.3
mg/Kg wet
33.3 74.9
40-140 2.94
Surrogate:2-Fluorobiphenyl
Matrix Spike (B234917-MS1)
2.67 mg/Kg wet
Source: 19GO278-02
3.33 80.2
Prepared: 07/06/19 Analyzed: 07/13/19
40-140
Diesel Range Organics
105
9.8
mg/Kg dry
39.2 103 6.83 *
40-140 MS-22
Surrogate: 2-Fluorobiphenyl
Matrix Spike Dup (B234917-MSD1)
1.72 mg/Kg dry
Source: 19GO278-02
3.92 43.8
Prepared: 07/06/19 Analyzed: 07/13/19
40-140
Diesel Range Organics
120
9.8
mg/Kg dry
39.2 103 42.9
40-140 12.6 30
Surrogate:2-Fluorobiphenyl
Batch B235063 - SW-846 5030B
2.12
mg/Kg dry
3.92 54.0
40-140
Blank (B235063-BLK1)
Prepared & Analyzed: 07/09/19
Gasoline Range Organics (GRO)
ND
1.0
mg/Kg wet
Surrogate: 1-Chloro-3-fluorobenzene
LCS (B235063-BS1)
16.6
µg/L
15.0 ill
Prepared & Analyzed: 07/09/19
70-130
Gasoline Range Organics (GRO)
0.251
0.010
mg/Kg wet
0.250 100
80-120
Surrogate: 1-Chloro-3-fluorobenzene
LCS Dup (B235063-BSD1)
16.6
µg/L
15.0 ill
Prepared & Analyzed: 07/09/19
70-130
Gasoline Range Organics (GRO)
0.252
0.010
mg/Kg wet
0.250 101
80-120 0.309 30
Surrogate:l-Chloro-3-fluorobenzene
Batch B235508 - SW-846 3546
17.2
µg/L
15.0 114
70-130
Blank (B235508-BLK1)
Prepared: 07/15/19 Analyzed: 07/16/19
Diesel Range Organics
ND
8.3
mg/Kg wet
Surrogate:2-Fluorobiphenyl
LCS (B235508-BS1)
3.47
mg/Kg wet
3.33 104
Prepared: 07/15/19 Analyzed: 07/16/19
40-140
Diesel Range Organics
24.0
8.3
mg/Kg wet
33.3 71.9
40-140
Surrogate:2-Fluorobiphenyl
3.35
mg/Kg wet
3.33 101
40-140
Page 16 of 22

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235508 - SW-846 3546
LCS Dup (B235508-BSD1) Prepared: 07/15/19 Analyzed: 07/16/19
Diesel Range Organics 23.3 8.3 mg/Kg wet 33.3 69.9 40-140 2.88
Surrogate:2-Fluorobiphenyl 3.27 mg/Kgwet 3.33 98.0 40-140
Page 17 of 22

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 * FAX [phone] " TEL. [phone]
FLAG/QUALIFIER SUMMARY
* QC result is outside of established limits.
fi Wide recovery limits established for difficult compound.
$ Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
ND Not Detected
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
MS-22 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the
two MS/MSD results is within method specified criteria.
Z-01 Results in the diesel range organics do not appear to be petroleum related.
Page 18 of 22

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8015C in Product/Solid
Diesel Range Organics
NC
SW-846 8015C in Soil
Gasoline Range Organics (GRO)
NY,VA,NH,NC
Diesel Range Organics
NY,VA,NH,NC
SW-846 8015C in Water
Diesel Range Organics
NY,VA,NH,NC
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2005
100033
03/1/2020
MA
Massachusetts DEP
M-MA100
06/30/2020
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY
New York State Department of Health
10899 NELAP
04/1/2020
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2020
RI
Rhode Island Department of Health
LA000112
12/30/2019
NC
North Carolina Div. of Water Quality
652
12/31/2019
NJ
New Jersey DEP
MA007 NELAP
06/30/2020
FL
Florida Department of Health
E871027 NELAP
06/30/2020
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2020
ME
State of Maine
2011028
06/9/2021
VA
Commonwealth of Virginia
460217
12/14/2019
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2020
NC-DW
North Carolina Department of Health
25703
07/31/2019
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2020
Page 19 of 22

Table of Contents
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Table of Contents
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PACKAGING
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SHIP DATE
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Travel History
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Page 21 of 22

Table of Contents
Received By
Date
How were the samples In Cooler received? "` No Cooler
Direct from Sampling
Were samples within By Gun #
Temperature? 2-6°C
Time J r c u
On ice No Ice
Ambient Melted Ice
Actual Temp - S:
By Blank IT Actual Temp -
Was Custody Seal Intact? —_ VA Were Samples Tampered with?
Was COC Relinquished ? �- Does Chain Agree With Samples?
Are there broken/leaking/loose caps on any samples? F -r
Is COC in ink/ Legible? -T-
Did COC include all Client
{
pertinent Information? Project
T-
Are Sample labels filled out and legible?
Are there Lab to Filters?
Are there Rushes?
Are there Short Holds?
Is there enough Volume?
-T-_
Is there Headspace where applicable?
Proper Media/Containers Used?
-�
T
Were trip blanks received?
Do all samples have the proper pH?
�4f
Were samples received within holding time?
Analysis ;- Sampler Name T
ID's Collection Dates/Times t
Who was notified?
Who was notified?
Who was notified?
MS/MSD?
Is splitting samples required?
On COC? 41
Acid r1nen
f

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
July 22, 2019
Joe Beaman
Highlands Environmental Solutions, Inc.
8410-D Falls of Neuse
Raleigh, NC 27615
Project Location: Midland, NC
Client Job Number:
Project Number: 317028
Laboratory Work Order Number: 19GO278
Enclosed are results of analyses for samples received by the laboratory on July 5, 2019. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 45

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
19G0278-01
19G0278-02
19G0278-03
19G0278-04
19G0278-05
Sample Preparation Information
QC Data
Volatile Organic Compounds by GC/ 4S
B235627
Semivolatile Organic Compounds by GUMS
B235621
Petroleum Hydrocarbons Analyses
B234917
B235063
B235508
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
7
7
13
19
21
23
25
26
26
26
31
31
36
36
36
36
38
39
43
Page 2 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Highlands Environmental Solutions, Inc.
8410-D Falls of Neuse REPORT DATE: 7/22/2019
Raleigh, NC 27615 PURCHASE ORDER NUMBER:
ATTN: Joe Beaman
PROJECT NUMBER: 317028
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 19GO278
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: Midland, NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
S-1
19GO278-01
Soil
SM 254OG
SW-846 8015C
SW-846 8260D
SW-846 8270E
S-2
19GO278-02
Soil
SM 254OG
SW-846 8015C
SW-846 8260D
SW-846 8270E
S-3
19GO278-03
Soil
SM 2540G
SW-846 8015C
S-4
19GO278-04
Soil
SM 254OG
SW-846 8015C
S-5
19GO278-05
Soil
SM 254OG
SW-846 8015C
Page 3 of 45

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
REVISED REPORT - 7/16/2019 - Samples 19GO278-01 & -02 analyzed for VOCs & SVOCs per client's request.
Page 4 of 45

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ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
SW-846 8015C
Qualifications
MS-22
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is
within method specified criteria.
Analyte & Samples(s) Qualified:
Diesel Range Organics
B234917-MSI
Z-01
Results in the diesel range organics do not appear to be petroleum related.
Analyte & Samples(s) Qualified:
Diesel Range Organics
19G0278-01RE1[S-1]
SW-846 8260D
Qualifications:
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
tert-Butyl Alcohol (TBA)
B235627-BSI, B235627-BSDI
V-16
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported
result.
Analyte & Samples(s) Qualified:
1,4-Dioxane
19G0278-01[S-1], 19G0278-02[S-2], B235627-BLK1, B235627-BSI, B235627-BSDI
V-20
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
Bromodichloromethane
B235627-BS1, B235627-BSD1, 5038163-CCVI
Bromomethane
B235627-BS1, B235627-BSD1, 5038163-CCVI
tert-Butyl Alcohol (TBA)
B235627-BSI, B235627-BSDI, S038163-CCVI
Tetrachloroethylene
B235627-BSI, B235627-BSDI, S038163-CCVI
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
Bromomethane
19G0278-01[S-1], 19G0278-02[S-2], B235627-BLKI, B235627-BSI, B235627-BSDI, S038163-CCVI
V-35
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
Acetone
B235627-BSI, B235627-BSDI, S038163-CCVI
SW-846 8270E
Qualifications:
Page 5 of 45

,con-testo
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] ` TEL. [phone]
V-04
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
2,4-Dinitrophenol
19G0278-01[S-1], 19G0278-02[S-2], S038306-CCVI
Benzidine
19G0278-01[S-1], 19G0278-02[S-2], B235621-BLKI, B235621-BSI, B235621-BSD1, 5038218-CCVI, S038306-CCVI
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
Benzidine
19G0278-01[S-1], 19G0278-02[S-2], B235621-BLKI, B235621-BSI, B235621-BSD1, 5038218-CCVI, S038306-CCVI
Hexachlorocyclopentadiene
B235621-BLKI, B235621-BSI, B235621-BSD1, S038218-CCVI
V-16
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported
result.
Analyte & Samples(s) Qualified:
Pentachloronitrobenzene
B235621-BLKI, B235621-BSI, B235621-BSD1, S038218-CCVI
V-20
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
2,4-Dinitrophenol
19G0278-01[S-1], 19G0278-02[S-2], S038306-CCVI
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
3,3-Dichlorobenzidine
B235621-BLKI, B235621-BSI, B235621-BSDI, S038218-CCVI
4-Chloroaniline
19G0278-01[S-1], 19G0278-02[S-2], B235621-BLKI, B235621-BSI, B235621-BSD1, 5038218-CCVI, S038306-CCVI
V-35
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
2-Nitroaniline
19G0278-01[S-1], 19G0278-02[S-2], S038306-CCVI
SW-846 8015C
Gasoline Range Organics (2-Methylpentane through 1,2,4-Trimethylbenzene) is quantitated against a calibration made with an unleaded gasoline composite standard.
Diesel Range Organics (C10-C28) is quantitated against a calibration made with a #2 fuel oil standard.
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
d�
Lisa A. Worthington
Technical Representative
Page 6 of 45

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-1 Sampled: 7/2/2019 10:15
Sample ID: 19GO278-01
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
0.042
0.11
0.0092
mg/Kg dry
1 J
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Acrylonitrile
ND
0.0066
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0011
0.00033
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Benzene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Bromobenzene
ND
0.0022
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Bromochloromethane
ND
0.0044
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Bromodichloromethane
ND
0.0022
0.00055
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Bromoform
ND
0.0044
0.00077
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Bromomethane
ND
0.011
0.0012
mg/Kg dry
1 V-34
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
2-Butanone (MEK)
ND
0.044
0.0060
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
tert-Butyl Alcohol (TBA)
ND
0.044
0.0049
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
n-Butylbenzene
ND
0.0022
0.00055
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
sec-Butylbenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
tert-Butylbenzene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0011
0.00022
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Carbon Disulfide
ND
0.0066
0.0059
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Carbon Tetrachloride
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Chlorobenzene
ND
0.0022
0.00055
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Chlorodibromomethane
ND
0.0022
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Chloroethane
ND
0.022
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Chloroform
ND
0.0044
0.00055
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Chloromethane
ND
0.011
0.00077
mg/Kg dry
I
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
2-Chlorotoluene
ND
0.0022
0.00033
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
4-Chlorotoluene
ND
0.0022
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0022
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,2-Dibromoethane (EDB)
ND
0.0011
0.00077
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Dibromomethane
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,2-Dichlorobenzene
ND
0.0022
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,3-Dichlorobenzene
ND
0.0022
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,4-Dichlorobenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
trans-1,4-Dichloro-2-butene
ND
0.0044
0.00066
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.022
0.0012
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,1-Dichloroethane
ND
0.0022
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,2-Dichloroethane
ND
0.0022
0.00055
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,1-Dichloroethylene
ND
0.0044
0.00077
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
cis-1,2-Dichloroethylene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
trans-1,2-Dichloroethylene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,2-Dichloropropane
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,3-Dichloropropane
ND
0.0011
0.00055
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
2,2-Dichloropropane
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,1-Dichloropropene
ND
0.0044
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
cis-1,3-Dichloropropene
ND
0.0011
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
trans-1,3-Dichloropropene
ND
0.0011
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Diethyl Ether
ND
0.022
0.00077
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Page 7 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-1 Sampled: 7/2/2019 10:15
Sample ID: 19GO278-01
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPS)
ND
0.0011
0.00022
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,4-Dioxane
ND
0.11
0.0058
mg/Kg dry
1 V-16
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Ethylbenzene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Hexachlorobutadiene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
2-Hexanone (MBK)
ND
0.022
0.0022
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Isopropylbenzene (Cumene)
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0022
0.00055
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0044
0.00033
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Methylene Chloride
ND
0.022
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.022
0.0027
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Naphthalene
ND
0.011
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
n-Propylbenzene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Styrene
ND
0.0022
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0022
0.0011
mg/Kg dry
1
SW-8468260D
7/16/19
7/16/19 15:21
MFF
1,1,2,2-Tetrachloroethane
ND
0.0011
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Tetrachloroethylene
ND
0.0022
0.0013
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Tetrahydrofirran
ND
0.011
0.0012
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Toluene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,2,3-Trichlorobenzene
ND
0.0022
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,2,4-Trichlorobenzene
ND
0.0022
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,3,5-Trichlorobenzene
ND
0.0022
0.00033
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1, 1, 1 -Trichloroethane
ND
0.0022
0.00055
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,1,2-Trichloroethane
ND
0.0022
0.00044
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Trichloroethylene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Trichlorofluoromethane (Freon 11)
ND
0.011
0.00077
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,2,3-Trichloropropane
ND
0.0044
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
0.011
0.00088
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
0.0022
0.00033
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
1,3,5-Trimethylbenzene
ND
0.0022
0.00055
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Vinyl Chloride
ND
0.011
0.00099
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
m+p Xylene
ND
0.0044
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
o-Xylene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:21
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
98.8
70-130
7/16/19 15:21
Toluene-d8
99.2
70-130
7/16/19 15:21
4-Bromofluorobenzene
101
70-130
7/16/19 15:21
Page 8 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-1 Sampled: 7/2/2019 10:15
Samnle ID: 19GO278-01
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Acenaphthylene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Acetophenone
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Aniline
ND
0.40
0.095
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Anthracene
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Benzidine
ND
0.78
0.21
mg/Kg dry
1 V-04, V-05
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Benzo(a)anthracene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Benzo(a)pyrene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Benzo(b)fluoranthene
0.13
0.20
0.13
mg/Kg dry
1 J
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Benzo(g,h,i)perylene
ND
0.20
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Benzo(k)fluoranthene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Benzoic Acid
ND
1.2
0.70
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Bis(2-chloroethoxy)methane
ND
0.40
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Bis(2-chloroethyl)ether
ND
0.40
0.20
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Bis(2-chloroisopropyl)ether
ND
0.40
0.27
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
4-Bromophenylphenylether
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Butylbenzylphthalate
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Carbazole
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
4-Chloroaniline
ND
0.78
0.17
mg/Kg dry
1 V-34
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
4-Chloro-3-methylphenol
ND
0.78
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2-Chloronaphthalene
ND
0.40
0.12
mg/Kg dry
I
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2-Chlorophenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
4-Chlorophenylphenylether
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Chrysene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Dibenz(a,h)anthracene
ND
0.20
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Dibenzofman
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Di-n-butylphthalate
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
1,2-Dichlorobenzene
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
1,3-Dichlorobenzene
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
1,4-Dichlorobenzene
ND
0.40
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
3,3-Dichlorobenzidine
ND
0.20
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2,4-Dichlorophenol
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Diethylphthalate
ND
0.40
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2,4-Dimethylphenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Dimethylphthalate
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
4,6-Dinitro-2-methylphenol
ND
0.40
0.35
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2,4-Dinitrophenol
ND
0.78
0.54
mg/Kg dry
1 V-04, V-20
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2,4-Dinitrotoluene
ND
0.40
0.19
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2,6-Dinitrotoluene
ND
0.40
0.19
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Di-n-octylphthalate
ND
0.40
0.18
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
1,2-Diphenylhydrazine/Azobenzene
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Flumanthene
ND
0.20
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Flumene
ND
0.20
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Page 9 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-1 Sampled: 7/2/2019 10:15
Samnle ID: 19GO278-01
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.40
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Hexachlorobutadiene
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Hexachlorocyclopentadiene
ND
0.40
0.33
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Hexachloroethane
ND
0.40
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Indeno(1,2,3-cd)pyrene
ND
0.20
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Isophorone
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
1-Methylnaphthalene
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2-Methylnaphthalene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2-Methylphenol
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
3/4-Methylphenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Naphthalene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2-Nitroaniline
ND
0.40
0.24
mg/Kg dry
1 V-35
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
3-Nitroaniline
ND
0.40
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
4-Nitroaniline
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Nitrobenzene
ND
0.40
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2-Nitrophenol
ND
0.40
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
4-Nitrophenol
ND
0.78
0.28
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
N-Nitrosodimethylamine
ND
0.40
0.21
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
N-Nitrosodiphenylamine/Diphenylamine
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
N-Nitrosodi-n-propylamine
ND
0.40
0.18
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Pentachloronitrobenzene
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Pentachlorophenol
ND
0.40
0.27
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Phenanthrene
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Phenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Pyrene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Pyridine
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
1,2,4,5-Tetrachlorobenzene
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
1,2,4-Trichlorobenzene
ND
0.40
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2,4,5-Trichlorophenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
2,4,6-Trichlorophenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:21
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
41.1
30-130
7/19/19 13:21
Phenol-d6
53.6
30-130
7/19/19 13:21
Nitrobenzene-d5
78.3
30-130
7/19/19 13:21
2-Fluorobiphenyl
84.2
30-130
7/19/19 13:21
2,4,6-Tribromophenol
43.8
30-130
7/19/19 13:21
p-Terphenyl-dl4
88.1
30-130
7/19/19 13:21
Page 10 of 45

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-1 Sampled: 7/2/2019 10:15
Sample ID: 19G0278-01
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 1.3 1.3 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 15:39 KMB
Diesel Range Organics 93 9.8 3.5 mg/Kg dry 1 Z-01 SW-846 8015C 7/15/19 7/16/19 9:58 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 109 70-130 7/9/19 15:39
2-Fluorobiphenyl 62.0 40-140 7/16/19 9:58
Page 11 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-1 Sampled: 7/2/2019 10:15
Sample ID: 19G0278-01
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 84.4 % Wt 1
SM 2540G 7/8/19 7/9/19 8:01 JDN
Page 12 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-2 Sampled: 7/2/2019 10:20
Sample ID: 19GO278-02
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
0.083
0.14
0.012
mg/Kg dry
1 J
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Acrylonitrile
ND
0.0084
0.0014
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0014
0.00042
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Benzene
ND
0.0028
0.00084
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Bromobenzene
ND
0.0028
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Bromochloromethane
ND
0.0056
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Bromodichloromethane
ND
0.0028
0.00070
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Bromoform
ND
0.0056
0.00098
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Bromomethane
ND
0.014
0.0015
mg/Kg dry
1 V-34
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
2-Butanone (MEK)
ND
0.056
0.0077
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
tert-Butyl Alcohol (TBA)
ND
0.056
0.0063
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
n-Butylbenzene
ND
0.0028
0.00070
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
sec-Butylbenzene
ND
0.0028
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
tert-Butylbenzene
ND
0.0028
0.00084
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0014
0.00028
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Carbon Disulfide
ND
0.0084
0.0075
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Carbon Tetrachloride
ND
0.0028
0.00098
mg/Kg dry
I
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Chlorobenzene
ND
0.0028
0.00070
mg/Kg dry
I
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Chlorodibromomethane
ND
0.0028
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Chloroethane
ND
0.028
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Chloroform
ND
0.0056
0.00070
mg/Kg dry
I
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Chloromethane
ND
0.014
0.00098
mg/Kg dry
I
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
2-Chlorotoluene
ND
0.0028
0.00042
mg/Kg dry
I
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
4-Chlorotoluene
ND
0.0028
0.00056
mg/Kg dry
I
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0028
0.0014
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,2-Dibromoethane (EDB)
ND
0.0014
0.00098
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Dibromomethane
ND
0.0028
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,2-Dichlorobenzene
ND
0.0028
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,3-Dichlorobenzene
ND
0.0028
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,4-Dichlorobenzene
ND
0.0028
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
trans-1,4-Dichloro-2-butene
ND
0.0056
0.00084
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.028
0.0015
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,1-Dichloroethane
ND
0.0028
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,2-Dichloroethane
ND
0.0028
0.00070
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1, 1 -Dichloroethylene
ND
0.0056
0.00098
mg/Kg dry
1
SW-8468260D
7/16/19
7/16/19 15:48
MFF
cis-1,2-Dichloroethylene
ND
0.0028
0.00098
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
trans-1,2-Dichloroethylene
ND
0.0028
0.00084
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,2-Dichloropropane
ND
0.0028
0.0011
mg/Kg dry
I
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,3-Dichloropropane
ND
0.0014
0.00070
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
2,2-Dichloropropane
ND
0.0028
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,1-Dichloropropene
ND
0.0056
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
cis-1,3-Dichloropropene
ND
0.0014
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
trans-1,3-Dichloropropene
ND
0.0014
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Diethyl Ether
ND
0.028
0.00098
mg/Kg dry
I
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Page 13 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-2 Sampled: 7/2/2019 10:20
Sample ID: 19GO278-02
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPS)
ND
0.0014
0.00028
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,4-Dioxane
ND
0.14
0.0074
mg/Kg dry
1 V-16
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Ethylbenzene
ND
0.0028
0.00084
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Hexachlorobutadiene
ND
0.0028
0.00098
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
2-Hexanone (MBK)
ND
0.028
0.0028
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Isopropylbenzene (Cumene)
ND
0.0028
0.00084
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0028
0.00070
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0056
0.00042
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Methylene Chloride
ND
0.028
0.0014
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.028
0.0035
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Naphthalene
ND
0.014
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
n-Propylbenzene
ND
0.0028
0.00084
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Styrene
ND
0.0028
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0028
0.0014
mg/Kg dry
1
SW-8468260D
7/16/19
7/16/19 15:48
MFF
1,1,2,2-Tetrachloroethane
ND
0.0014
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Tetrachloroethylene
ND
0.0028
0.0017
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Tetrahydrofirran
ND
0.014
0.0015
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Toluene
ND
0.0028
0.00084
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,2,3-Trichlorobenzene
ND
0.0028
0.0014
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,2,4-Trichlorobenzene
ND
0.0028
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,3,5-Trichlorobenzene
ND
0.0028
0.00042
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1, 1, 1 -Trichloroethane
ND
0.0028
0.00070
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,1,2-Trichloroethane
ND
0.0028
0.00056
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Trichloroethylene
ND
0.0028
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Trichlorofluoromethane (Freon 11)
ND
0.014
0.00098
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,2,3-Trichloropropane
ND
0.0056
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
0.014
0.0011
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
0.0028
0.00042
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
1,3,5-Trimethylbenzene
ND
0.0028
0.00070
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Vinyl Chloride
ND
0.014
0.0013
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
m+p Xylene
ND
0.0056
0.0014
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
o-Xylene
ND
0.0028
0.00084
mg/Kg dry
1
SW-846 8260D
7/16/19
7/16/19 15:48
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
98.7
70-130
7/16/19 15:48
Toluene-d8
97.3
70-130
7/16/19 15:48
4-Bromofluorobenzene
97.0
70-130
7/16/19 15:48
Page 14 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-2 Sampled: 7/2/2019 10:20
Samnle ID: 19GO278-02
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Acenaphthylene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Acetophenone
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Aniline
ND
0.40
0.094
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Anthracene
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Benzidine
ND
0.78
0.21
mg/Kg dry
1 V-04, V-05
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Benzo(a)anthracene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Benzo(a)pyrene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Benzo(b)fluoranthene
0.21
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Benzo(g,h,i)perylene
0.14
0.20
0.12
mg/Kg dry
1 J
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Benzo(k)fluoranthene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Benzoic Acid
ND
1.2
0.70
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Bis(2-chloroethoxy)methane
ND
0.40
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Bis(2-chloroethyl)ether
ND
0.40
0.20
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Bis(2-chloroisopropyl)ether
ND
0.40
0.27
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Bis(2-Ethylhexyl)phthalate
0.15
0.40
0.12
mg/Kg dry
1 J
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
4-Bromophenylphenylether
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Butylbenzylphthalate
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Carbazole
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
4-Chloroaniline
ND
0.78
0.17
mg/Kg dry
1 V-34
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
4-Chloro-3-methylphenol
ND
0.78
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2-Chloronaphthalene
ND
0.40
0.12
mg/Kg dry
I
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2-Chlorophenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
4-Chlorophenylphenylether
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Chrysene
0.14
0.20
0.13
mg/Kg dry
1 J
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Dibenz(a,h)anthracene
ND
0.20
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Dibenzofman
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Di-n-butylphthalate
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
1,2-Dichlorobenzene
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
1,3-Dichlorobenzene
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
1,4-Dichlorobenzene
ND
0.40
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
3,3-Dichlorobenzidine
ND
0.20
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2,4-Dichlorophenol
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Diethylphthalate
ND
0.40
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2,4-Dimethylphenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Dimethylphthalate
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
4,6-Dinitro-2-methylphenol
ND
0.40
0.35
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2,4-Dinitrophenol
ND
0.78
0.54
mg/Kg dry
1 V-04, V-20
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2,4-Dinitrotoluene
ND
0.40
0.19
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2,6-Dinitrotoluene
ND
0.40
0.19
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Di-n-octylphthalate
ND
0.40
0.18
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
1,2-Diphenylhydrazine/Azobenzene
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Flumanthene
0.14
0.20
0.12
mg/Kg dry
1 J
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Flumene
ND
0.20
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Page 15 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-2 Sampled: 7/2/2019 10:20
Samnle ID: 19GO278-02
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.40
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Hexachlorobutadiene
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Hexachlorocyclopentadiene
ND
0.40
0.33
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Hexachloroethane
ND
0.40
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Indeno(1,2,3-cd)pyrene
ND
0.20
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Isophorone
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
1-Methylnaphthalene
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2-Methylnaphthalene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2-Methylphenol
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
3/4-Methylphenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Naphthalene
ND
0.20
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2-Nitroaniline
ND
0.40
0.24
mg/Kg dry
1 V-35
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
3-Nitroaniline
ND
0.40
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
4-Nitroaniline
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Nitrobenzene
ND
0.40
0.17
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2-Nitrophenol
ND
0.40
0.17
mg/Kg dry
I
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
4-Nitrophenol
ND
0.78
0.28
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
N-Nitrosodimethylamine
ND
0.40
0.21
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
N-Nitrosodiphenylamine/Diphenylamine
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
N-Nitrosodi-n-propylamine
ND
0.40
0.18
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Pentachloronitrobenzene
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Pentachlorophenol
ND
0.40
0.27
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Phenanthrene
ND
0.20
0.11
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Phenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Pyrene
0.14
0.20
0.13
mg/Kg dry
1 J
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Pyridine
ND
0.40
0.12
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
1,2,4,5-Tetrachlorobenzene
ND
0.40
0.15
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
1,2,4-Trichlorobenzene
ND
0.40
0.13
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2,4,5-Trichlorophenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
2,4,6-Trichlorophenol
ND
0.40
0.14
mg/Kg dry
1
SW-846 8270E
7/16/19
7/19/19 13:47
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
46.3
30-130
7/19/19 13:47
Phenol-d6
54.8
30-130
7/19/19 13:47
Nitrobenzene-d5
70.3
30-130
7/19/19 13:47
2-Fluorobiphenyl
74.2
30-130
7/19/19 13:47
2,4,6-Tribromophenol
55.6
30-130
7/19/19 13:47
p-Terphenyl-dl4
77.8
30-130
7/19/19 13:47
Page 16 of 45

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-2 Sampled: 7/2/2019 10:20
Sample ID: 19G0278-02
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 0.94 0.91 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 16:14 KMB
Diesel Range Organics 100 9.8 3.5 mg/Kg dry 1 SW-846 8015C 7/6/19 7/12/19 23:53 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 108 70-130 7/9/19 16:14
2-Fluorobiphenyl 55.7 40-140 7/12/19 23:53
Page 17 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-2 Sampled: 7/2/2019 10:20
Sample ID: 19G0278-02
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 84.8 % Wt 1
SM 2540G 7/8/19 7/9/19 8:01 JDN
Page 18 of 45

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-3 Sampled: 7/2/2019 10:30
Sample ID: 19G0278-03
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 1.5 1.4 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 16:49 KMB
Diesel Range Organics 67 10 3.6 mg/Kg dry 1 SW-846 8015C 7/6/19 7/13/19 0:34 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 113 70-130 7/9/19 16:49
2-Fluorobiphenyl 50.1 40-140 7/13/19 0:34
Page 19 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19GO278
Date Received: 7/5/2019
Field Sample #: S-3 Sampled: 7/2/2019 10:30
Sample ID: 19GO278-03
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 83.2 % Wt 1
SM 2540G 7/8/19 7/9/19 8:01 JDN
Page 20 of 45

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-4 Sampled: 7/2/2019 10:45
Sample ID: 19G0278-04
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 1.3 1.3 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 17:24 KMB
Diesel Range Organics 54 46 17 mg/Kg dry 5 SW-846 8015C 7/6/19 7/12/19 23:53 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 113 70-130 7/9/19 17:24
2-Fluorobiphenyl 61.0 40-140 7/12/19 23:53
Page 21 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-4 Sampled: 7/2/2019 10:45
Sample ID: 19G0278-04
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 90.0 % Wt 1
SM 2540G 7/8/19 7/9/19 8:02 JDN
Page 22 of 45

Table of Contents
icon-tes w .
40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-5 Sampled: 7/2/2019 11:00
Sample ID: 19G0278-05
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 1.3 1.3 mg/Kg dry 1 SW-846 8015C 7/9/19 7/9/19 17:59 KMB
Diesel Range Organics 13 9.3 3.4 mg/Kg dry 1 SW-846 8015C 7/6/19 7/13/19 0:14 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 109 70-130 7/9/19 17:59
2-Fluorobiphenyl 51.3 40-140 7/13/19 0:14
Page 23 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Midland, NC Sample Description: Work Order: 19G0278
Date Received: 7/5/2019
Field Sample #: S-5 Sampled: 7/2/2019 11:00
Sample ID: 19G0278-05
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 89.3 % Wt 1
SM 2540G 7/8/19 7/9/19 8:02 JDN
Page 24 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]
Batch
Date
19G0278-01 [S-1]
B234960
07/08/19
19G0278-02[S-2]
B234960
07/08/19
19G0278-03[S-3]
B234960
07/08/19
19G0278-04[S-4]
B234960
07/08/19
19G0278-05 [S-5]
B234960
07/08/19
Prep Method: SW-846 3546-SW-846 8015C
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
19G0278-02[S-2]
B234917
30.0
1.00
07/06/19
19G0278-03 [S-3]
B234917
30.1
1.00
07/06/19
19G0278-04[S-4]
B234917
30.2
1.00
07/06/19
19G0278-05[S-5]
B234917
30.0
1.00
07/06/19
Prep Method: SW-846 5030B-SW-846 8015C
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
19G0278-01[S-1]
B235063
5.10
5.80
07/09/19
19G0278-02[S-2]
B235063
7.80
6.20
07/09/19
19G0278-03[S-3]
B235063
4.70
5.80
07/09/19
19G0278-04[S-4]
B235063
4.70
5.50
07/09/19
19G0278-05[S-5]
B235063
4.70
5.50
07/09/19
Prep Method: SW-846 3546-SW-846 8015C
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
19G0278-01RE1 [S-1]
B235508
30.2
1.00
07/15/19
Prep Method: SW-846 5035-SW-846 8260D
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
19G0278-01[S-1]
B235627
5.41
10.0
07/16/19
19G0278-02[S-2]
B235627
4.23
10.0
07/16/19
Prep Method: SW-846 3546-SW-846 8270E
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
19G0278-01[S-1]
B235621
30.1
1.00
07/16/19
19G0278-02[S-2]
B235621
30.0
1.00
07/16/19
Page 25 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235627 - SW-846 5035
Blank (B235627-BLK1) Prepared & Analyzed: 07/16/19
Acetone
ND
0.10
mg/Kg wet
Acrylonitrile
ND
0.0060
mg/Kg wet
tert-Amyl Methyl Ether (TAME)
ND
0.0010
mg/Kg wet
Benzene
ND
0.0020
mg/Kg wet
Bromobenzene
ND
0.0020
mg/Kg wet
Bromochloromethane
ND
0.0020
mg/Kg wet
Bromodichloromethane
ND
0.0020
mg/Kg wet
Bromoform
ND
0.0020
mg/Kg wet
Bromomethane
ND
0.010
mg/Kg wet
2-Butanone (MEK)
ND
0.040
mg/Kg wet
tert-Butyl Alcohol (TBA)
ND
0.040
mg/Kg wet
n-Butylbenzene
ND
0.0020
mg/Kg wet
sec-Butylbenzene
ND
0.0020
mg/Kg wet
tert-Butylbenzene
ND
0.0020
mg/Kg wet
tert-Butyl Ethyl Ether (TBEE)
ND
0.0010
mg/Kg wet
Carbon Disulfide
ND
0.0060
mg/Kg wet
Carbon Tetrachloride
ND
0.0020
mg/Kg wet
Chlorobenzene
ND
0.0020
mg/Kg wet
Chlorodibromomethane
ND
0.0010
mg/Kg wet
Chloroethane
ND
0.020
mg/Kg wet
Chloroform
ND
0.0040
mg/Kg wet
Chloromethane
ND
0.010
mg/Kg wet
2-Chlorotoluene
ND
0.0020
mg/Kg wet
4-Chlorotoluene
ND
0.0020
mg/Kg wet
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0020
mg/Kg wet
1,2-Dibromoethane (EDB)
ND
0.0010
mg/Kg wet
Dibromomethane
ND
0.0020
mg/Kg wet
1,2-Dichlorobenzene
ND
0.0020
mg/Kg wet
1,3-Dichlorobenzene
ND
0.0020
mg/Kg wet
1,4-Dichlorobenzene
ND
0.0020
mg/Kg wet
trans-1,4-Dichloro-2-butene
ND
0.0040
mg/Kg wet
Dichlorodifluoromethane (Freon 12)
ND
0.020
mg/Kg wet
1,1-Dichloroethane
ND
0.0020
mg/Kg wet
1,2-Dichloroethane
ND
0.0020
mg/Kg wet
1,1-Dichloroethylene
ND
0.0040
mg/Kg wet
cis-1,2-Dichloroethylene
ND
0.0020
mg/Kg wet
trans-1,2-Dichloroethylene
ND
0.0020
mg/Kg wet
1,2-Dichloropropane
ND
0.0020
mg/Kg wet
1,3-Dichloropropane
ND
0.0010
mg/Kg wet
2,2-Dichloropropane
ND
0.0020
mg/Kg wet
1,1-Dichloropropene
ND
0.0020
mg/Kg wet
cis-1,3-Dichloropropene
ND
0.0010
mg/Kg wet
trans-1,3-Dichloropropene
ND
0.0010
mg/Kg wet
Diethyl Ether
ND
0.020
mg/Kg wet
Diisopropyl Ether (RIPE)
ND
0.0010
mg/Kg wet
1,4-Dioxane
ND
0.10
mg/Kg wet
Ethylbenzene
ND
0.0020
mg/Kg wet
Hexachlorobutadiene
ND
0.0020
mg/Kg wet
2-Hexanone (MBK)
ND
0.020
mg/Kg wet
Isopropylbenzene (Cumene)
ND
0.0020
mg/Kg wet
p-Isopropyltoluene (p-Cymene)
ND
0.0020
mg/Kg wet
Methyl tert-Butyl Ether (MTBE)
ND
0.0040
mg/Kg wet
V-34
\TAa
Page 26 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
malyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235627 - SW-846 5035
Blank (B235627-BLK1)
Prepared & Analyzed: 07/16/19
Methylene Chloride
0.0020
0.020
mg/Kg wet J
4-Methyl-2-pentanone (MIBK)
ND
0.020
mg/Kg wet
Naphthalene
ND
0.0040
mg/Kg wet
n-Propylbenzene
ND
0.0020
mg/Kg wet
Styrene
ND
0.0020
mg/Kg wet
1, 1, 1,2-Tetrachloroethane
ND
0.0020
mg/Kg wet
1,1,2,2-Tetrachloroethane
ND
0.0010
mg/Kg wet
Tetrachloroethylene
ND
0.0020
mg/Kg wet
Tetrahydrofuran
ND
0.010
mg/Kg wet
Toluene
ND
0.0020
mg/Kg wet
1,2,3-Trichlorobenzene
ND
0.0020
mg/Kg wet
1,2,4-Trichlorobenzene
ND
0.0020
mg/Kg wet
1,3,5-Trichlorobenzene
ND
0.0020
mg/Kg wet
1, 1, 1 -Trichloroethane
ND
0.0020
mg/Kg wet
1,1,2-Trichloroethane
ND
0.0020
mg/Kg wet
Trichloroethylene
ND
0.0020
mg/Kg wet
Trichlorofluoromethane (Freon 11)
ND
0.010
mg/Kg wet
1,2,3-Trichloropropane
ND
0.0020
mg/Kg wet
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0.010
mg/Kg wet
113)
1,2,4-Trimethylbenzene
ND
0.0020
mg/Kg wet
1,3,5-Trimethylbenzene
ND
0.0020
mg/Kg wet
Vinyl Chloride
ND
0.010
mg/Kg wet
m+p Xylene
ND
0.0040
mg/Kg wet
o-Xylene
ND
0.0020
mg/Kg wet
Surrogate: 1,2-Dichloroethane-d4 0.0452 mg/Kg wet 0.0500 90.5 70-130
Surrogate: Toluene-d8 0.0487 mg/Kg wet 0.0500 97.5 70-130
Surrogate:4-Bromofluorobenzene 0.0531 mg/Kg wet 0.0500 106 70-130
LCS (B235627-BS1) Prepared & Analyzed: 07/16/19
Acetone
0.236
0.10
mg/Kg wet
0.200
118
70-160
Acrylonitrile
0.0198
0.0060
mg/Kg wet
0.0200
98.8
70-130
tert-Amyl Methyl Ether (TAME)
0.0215
0.0010
mg/Kg wet
0.0200
107
70-130
Benzene
0.0189
0.0020
mg/Kg wet
0.0200
94.3
70-130
Bromobenzene
0.0191
0.0020
mg/Kg wet
0.0200
95.6
70-130
Bromochloromethane
0.0213
0.0020
mg/Kg wet
0.0200
107
70-130
Bromodichloromethane
0.0241
0.0020
mg/Kg wet
0.0200
121
70-130
Bromoform
0.0197
0.0020
mg/Kg wet
0.0200
98.6
70-130
Bromomethane
0.0141
0.010
mg/Kg wet
0.0200
70.7
40-130
2-Butanone (MEK)
0.216
0.040
mg/Kg wet
0.200
108
70-160
tert-Butyl Alcohol (TBA)
0.264
0.040
mg/Kg wet
0.200
132 *
40-130
n-Butylbenzene
0.0170
0.0020
mg/Kg wet
0,0200
85.2
70-130
sec-Butylbenzene
0.0194
0.0020
mg/Kg wet
0.0200
97.1
70-130
tert-Butylbenzene
0.0169
0.0020
mg/Kg wet
0.0200
84.7
70-160
tert-Butyl Ethyl Ether (TBEE)
0.0206
0.0010
mg/Kg wet
0,0200
103
70-130
Carbon Disulfide
0.0216
0.0060
mg/Kg wet
0.0200
108
70-130
Carbon Tetrachloride
0.0211
0.0020
mg/Kg wet
0.0200
106
70-130
Chlorobenzene
0.0194
0.0020
mg/Kg wet
0,0200
96.8
70-130
Chlorodibromomethane
0.0239
0.0010
mg/Kg wet
0.0200
119
70-130
Chloroethane
0.0188
0.020
mg/Kg wet
0.0200
93.8
70-130
Chloroform
0.0197
0.0040
mg/Kg wet
0,0200
98.4
70-130
Chloromethane
0.0163
0.010
mg/Kg wet
0.0200
81.3
70-130
2-Chlorotoluene
0.0202
0.0020
mg/Kg wet
0.0200
101
70-130
V-35 t
V-20
V-20, V-34 t
t
L-02, V-20 t
t
Page 27 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
\nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235627 - SW-846 5035
LCS (B235627-BSI)
Prepared &Analyzed:07/16/19
4-Chlorotoluene
0.0210
0.0020
mg/Kg wet
0.0200
105
70-130
1,2-Dibromo-3-chloropropane (DBCP)
0.0178
0.0020
mg/Kg wet
0.0200
89.0
70-130
1,2-Dibromoethane (EDB)
0.0231
0.0010
mg/Kg wet
0.0200
116
70-130
Dibromomethane
0.0230
0.0020
mg/Kg wet
0.0200
115
70-130
1,2-Dichlorobenzene
0.0179
0.0020
mg/Kg wet
0.0200
89.3
70-130
1,3-Dichlorobenzene
0.0178
0.0020
mg/Kg wet
0.0200
89.2
70-130
1,4-Dichlorobenzene
0.0170
0.0020
mg/Kg wet
0.0200
84.9
70-130
trans-1,4-Dichloro-2-butene
0.0198
0.0040
mg/Kg wet
0.0200
99.0
70-130
Dichlorodifluoromethane(Freon 12)
0.0162
0.020
mg/Kg wet
0.0200
81.0
40-160
1,1-Dichloroethane
0.0211
0.0020
mg/Kg wet
0.0200
105
70-130
1,2-Dichloroethane
0.0238
0.0020
mg/Kg wet
0.0200
119
70-130
1,1-Dichloroethylene
0.0203
0.0040
mg/Kg wet
0.0200
102
70-130
cis-1,2-Dichloroethylene
0.0213
0.0020
mg/Kg wet
0.0200
107
70-130
trans-1,2-Dichloroethylene
0.0211
0.0020
mg/Kg wet
0.0200
106
70-130
1,2-Dichloropropane
0.0211
0.0020
mg/Kg wet
0.0200
105
70-130
1,3-Dichloropropane
0.0217
0.0010
mg/Kg wet
0.0200
108
70-130
2,2-Dichloropropane
0.0202
0.0020
mg/Kg wet
0.0200
101
70-130
1,1-Dichloropropene
0.0199
0.0020
mg/Kg wet
0.0200
99.6
70-130
cis-1,3-Dichloropropene
0.0229
0.0010
mg/Kg wet
0.0200
115
70-130
trans-1,3-Dichloropropene
0.0222
0.0010
mg/Kg wet
0.0200
ill
70-130
Diethyl Ether
0.0213
0.020
mg/Kg wet
0.0200
107
70-130
Diisopropyl Ether (DIPE)
0.0208
0.0010
mg/Kg wet
0.0200
104
70-130
1,4-Dioxane
0.229
0.10
mg/Kg wet
0.200
114
40-160
Ethylbenzene
0.0192
0.0020
mg/Kg wet
0.0200
95.8
70-130
Hexachlorobutadiene
0.0218
0.0020
mg/Kg wet
0.0200
109
70-160
2-Hexanone (MBK)
0.228
0.020
mg/Kg wet
0.200
114
70-160
Isopropylbenzene (Cumene)
0.0195
0.0020
mg/Kg wet
0.0200
97.4
70-130
p-Isopropyltoluene (p-Cymene)
0.0180
0.0020
mg/Kg wet
0.0200
89.8
70-130
Methyl tert-Butyl Ether (MTBE)
0.0217
0.0040
mg/Kg wet
0.0200
108
70-130
Methylene Chloride
0.0208
0.020
mg/Kg wet
0.0200
104
40-160
4-Methyl-2-pentanone (MIBK)
0.229
0.020
mg/Kg wet
0.200
115
70-160
Naphthalene
0.0159
0.0040
mg/Kg wet
0.0200
79.4
40-130
n-Propylbenzene
0.0196
0.0020
mg/Kg wet
0.0200
98.1
70-130
Styrene
0.0192
0.0020
mg/Kg wet
0.0200
96.0
70-130
1, 1, 1,2-Tetrachloroethane
0.0223
0.0020
mg/Kg wet
0.0200
112
70-130
1,1,2,2-Tetrachloroethane
0.0197
0.0010
mg/Kg wet
0.0200
98.4
70-130
Tetrachloroethylene
0.0249
0.0020
mg/Kg wet
0.0200
124
70-130
Tetrahydrofuran
0.0206
0.010
mg/Kg wet
0.0200
103
70-130
Toluene
0.0206
0.0020
mg/Kg wet
0.0200
103
70-130
1,2,3-Trichlorobenzene
0.0186
0.0020
mg/Kg wet
0.0200
93.1
70-130
1,2,4-Trichlorobenzene
0.0181
0.0020
mg/Kg wet
0.0200
90.5
70-130
1,3,5-Trichlorobenzene
0.0185
0.0020
mg/Kg wet
0.0200
92.3
70-130
1, 1, 1 -Trichloroethane
0.0204
0.0020
mg/Kg wet
0.0200
102
70-130
1,1,2-Trichloroethane
0.0224
0.0020
mg/Kg wet
0.0200
112
70-130
Trichloroethylene
0.0221
0.0020
mg/Kg wet
0.0200
ill
70-130
Trichlorofluoromethane (Freon 11)
0.0200
0.010
mg/Kg wet
0.0200
99.8
70-130
1,2,3-Trichloropropane
0.0194
0.0020
mg/Kg wet
0.0200
97.1
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.0211
0.010
mg/Kg wet
0.0200
106
70-130
113)
1,2,4-Trimethylbenzene
0.0171
0.0020
mg/Kg wet
0.0200
85.4
70-130
1,3,5-Trimethylbenzene
0.0198
0.0020
mg/Kg wet
0.0200
99.0
70-130
Vinyl Chloride
0.0179
0.010
mg/Kg wet
0,0200
89.7
40-130
J f
V-16 f
t
f
t
t
V-20
Page 28 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235627 - SW-846 5035
LCS (B235627-BSI) Prepared & Analyzed: 07/16/19
m+p Xylene 0.0389 0.0040 mg/Kg wet 0.0400 97.2 70-130
o-Xylene 0.0192 0.0020 mg/Kg wet 0.0200 95.8 70-130
Surrogate:l,2-Dichloroethane-d4
Surrogate: Toluene-d8
Surrogate:4-Bromofluorobenzene
LCS Dup (B235627-BSD1)
0.0436
0.0502
0.0527
mg/Kg wet
mg/Kg wet
mg/Kg wet
0.0500 87.3
0.0500 100
0.0500 105
Prepared & Analyzed: 07/16/19
70-130
70-130
70-130
Acetone
0.231
0.10
mg/Kg wet
0.200
116
70-160
1.93
Acrylonitrile
0.0194
0.0060
mg/Kg wet
0.0200
97.2
70-130
1.63
tert-Amyl Methyl Ether (TAME)
0.0209
0.0010
mg/Kg wet
0.0200
104
70-130
2.74
Benzene
0.0191
0.0020
mg/Kg wet
0.0200
95.3
70-130
1.05
Bromobenzene
0.0185
0.0020
mg/Kg wet
0.0200
92.5
70-130
3.30
Bromochloromethane
0.0205
0.0020
mg/Kg wet
0.0200
103
70-130
3.82
Bromodichloromethane
0.0252
0.0020
mg/Kg wet
0.0200
126
70-130
4.14
Bromoform
0.0202
0.0020
mg/Kg wet
0.0200
101
70-130
2.50
Bromomethane
0.0161
0.010
mg/Kg wet
0.0200
80.7
40-130
13.2
2-Butanone (MEK)
0.204
0.040
mg/Kg wet
0.200
102
70-160
5.62
tert-Butyl Alcohol (TBA)
0.261
0.040
mg/Kg wet
0.200
131
* 40-130
0.953
n-Butylbenzene
0.0174
0.0020
mg/Kg wet
0.0200
86.8
70-130
1.86
sec-Butylbenzene
0.0184
0.0020
mg/Kg wet
0.0200
92.2
70-130
5.18
tert-Butylbenzene
0.0173
0.0020
mg/Kg wet
0.0200
86.4
70-160
1.99
tert-Butyl Ethyl Ether (TBEE)
0.0209
0.0010
mg/Kg wet
0.0200
105
70-130
1.54
Carbon Disulfide
0.0207
0.0060
mg/Kg wet
0.0200
104
70-130
4.25
Carbon Tetrachloride
0.0216
0.0020
mg/Kg wet
0.0200
108
70-130
2.25
Chlorobenzene
0.0192
0.0020
mg/Kg wet
0.0200
96.0
70-130
0.830
Chlorodibromomethane
0.0220
0.0010
mg/Kg wet
0.0200
110
70-130
8.29
Chloroethane
0.0201
0.020
mg/Kg wet
0.0200
100
70-130
6.70
Chloroform
0.0197
0.0040
mg/Kg wet
0.0200
98.3
70-130
0.102
Chloromethane
0.0164
0.010
mg/Kg wet
0.0200
81.8
70-130
0.613
2-Chlorotoluene
0.0195
0.0020
mg/Kg wet
0.0200
97.6
70-130
3.23
4-Chlorotoluene
0.0196
0.0020
mg/Kg wet
0.0200
97.9
70-130
7.00
1,2-Dibromo-3-chloropropane (DBCP)
0.0183
0.0020
mg/Kg wet
0.0200
91.4
70-130
2.66
1,2-Dibromoethane (EDB)
0.0221
0.0010
mg/Kg wet
0.0200
110
70-130
4.42
Dibromomethane
0.0218
0.0020
mg/Kg wet
0.0200
109
70-130
5.54
1,2-Dichlorobenzene
0.0177
0.0020
mg/Kg wet
0.0200
88.5
70-130
0.900
1,3-Dichlorobenzene
0.0180
0.0020
mg/Kg wet
0.0200
90.0
70-130
0.893
1,4-Dichlorobenzene
0.0172
0.0020
mg/Kg wet
0.0200
86.0
70-130
1.29
trans-1,4-Dichloro-2-butene
0.0184
0.0040
mg/Kg wet
0.0200
91.8
70-130
7.55
Dichlorodifluoromethane(Freon 12)
0.0157
0.020
mg/Kg wet
0.0200
78.5
40-160
3.13
1, 1 -Dichloroethane
0.0215
0.0020
mg/Kg wet
0.0200
108
70-130
2.25
1,2-Dichloroethane
0.0230
0.0020
mg/Kg wet
0.0200
115
70-130
3.50
1,1-Dichloroethylene
0.0208
0.0040
mg/Kg wet
0.0200
104
70-130
2.53
cis-1,2-Dichloroethylene
0.0213
0.0020
mg/Kg wet
0.0200
107
70-130
0.0938
trans-1,2-Dichloroethylene
0.0211
0.0020
mg/Kg wet
0.0200
106
70-130
0.0947
1,2-Dichloropropane
0.0216
0.0020
mg/Kg wet
0.0200
108
70-130
2.44
1,3-Dichloropropane
0.0209
0.0010
mg/Kg wet
0.0200
105
70-130
3.57
2,2-Dichloropropane
0.0194
0.0020
mg/Kg wet
0.0200
96.9
70-130
4.04
1,1-Dichloropropene
0.0195
0.0020
mg/Kg wet
0.0200
97.7
70-130
1.93
cis-1,3-Dichloropropene
0.0218
0.0010
mg/Kg wet
0.0200
109
70-130
5.10
trans-1,3-Dichloropropene
0.0219
0.0010
mg/Kg wet
0.0200
110
70-130
1.45
Diethyl Ether
0.0199
0.020
mg/Kg wet
0.0200
99.5
70-130
6.98
Diisopropyl Ether (DIPE)
0.0206
0.0010
mg/Kg wet
0.0200
103
70-130
0.968
25 V-35 t
25
25
25
25
25
25 V-20
25
25 V-20, V-34 f
25 t
25 L-02, V-20 t
25
25
25 t
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25 J t
25
25
25
25
25
25
25
25
25
25
25
25 1
25
Page 29 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235627 - SW-846 5035
LCS Dup (B235627-BSD1)
Prepared & Analyzed: 07/16/19
1,4-Dioxane
0.213
0.10
mg/Kgwet
0.200
106
40-160
7.30
50
V-16 t t
Ethylbenzene
0.0189
0.0020
mg/Kg wet
0.0200
94.5
70-130
1.37
25
Hexachlorobutadiene
0.0204
0.0020
mg/Kg wet
0.0200
102
70-160
6.55
25
2-Hexanone (MBK)
0.215
0.020
mg/Kg wet
0.200
107
70-160
6.15
25
t
Isopropylbenzene (Cumene)
0.0184
0.0020
mg/Kg wet
0.0200
92.1
70-130
5.59
25
p-Isopropyltoluene(p-Cymene)
0.0175
0.0020
mg/Kg wet
0.0200
87.5
70-130
2.59
25
Methyl tert-Butyl Ether (MTBE)
0.0217
0.0040
mg/Kg wet
0.0200
109
70-130
0.184
25
Methylene Chloride
0.0213
0.020
mg/Kg wet
0.0200
106
40-160
2.28
25
f
4-Methyl-2-pentanone (MIBK)
0.218
0.020
mg/Kg wet
0.200
109
70-160
5.16
25
t
Naphthalene
0.0155
0.0040
mg/Kg wet
0.0200
77.3
40-130
2.68
25
f
n-Propylbenzene
0.0194
0.0020
mg/Kg wet
0.0200
96.8
70-130
1.33
25
Styrene
0.0189
0.0020
mg/Kg wet
0.0200
94.7
70-130
1.36
25
1, 1, 1,2-Tetrachloroethane
0.0210
0.0020
mg/Kg wet
0.0200
105
70-130
6.19
25
1,1,2,2-Tetrachloroethane
0.0198
0.0010
mg/Kg wet
0.0200
98.8
70-130
0.406
25
Tetrachloroethylene
0.0235
0.0020
mg/Kg wet
0.0200
117
70-130
5.96
25
V-20
Tetrahydrofuran
0.0211
0.010
mg/Kg wet
0.0200
105
70-130
2.31
25
Toluene
0.0205
0.0020
mg/Kg wet
0.0200
102
70-130
0.487
25
1,2,3-Trichlorobenzene
0.0190
0.0020
mg/Kg wet
0.0200
95.1
70-130
2.13
25
1,2,4-Trichlorobenzene
0.0175
0.0020
mg/Kg wet
0.0200
87.5
70-130
3.37
25
1,3,5-Trichlorobenzene
0.0194
0.0020
mg/Kg wet
0.0200
97.2
70-130
5.17
25
1, 1, 1 -Trichloroethane
0.0211
0.0020
mg/Kg wet
0.0200
106
70-130
3.76
25
1,1,2-Trichloroethane
0.0198
0.0020
mg/Kg wet
0.0200
98.8
70-130
12.7
25
Trichloroethylene
0.0211
0.0020
mg/Kg wet
0.0200
105
70-130
4.91
25
Trichlorofluoromethane (Freon 11)
0.0206
0.010
mg/Kg wet
0.0200
103
70-130
3.16
25
1,2,3-Trichloropropane
0.0190
0.0020
mg/Kg wet
0.0200
94.8
70-130
2.40
25
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.0224
0.010
mg/Kg wet
0.0200
112
70-130
5.70
25
113)
1,2,4-Trimethylbenzene
0.0169
0.0020
mg/Kg wet
0.0200
84.4
70-130
1.18
25
1,3,5-Trimethylbenzene
0.0191
0.0020
mg/Kg wet
0.0200
95.7
70-130
3.39
25
Vinyl Chloride
0.0174
0.010
mg/Kg wet
0.0200
86.9
40-130
3.17
25
t
m+p Xylene
0.0383
0.0040
mg/Kg wet
0.0400
95.8
70-130
1.45
25
o-Xylene
0.0187
0.0020
mg/Kg wet
0.0200
93.5
70-130
2.43
25
Surrogate: 1,2-Dichloroethane-d4
0.0440
mg/Kg wet
0.0500
88.1
70-130
Surrogate: Toluene-d8
0.0501
mg/Kg wet
0.0500
100
70-130
Surrogate:4-Bromofluorobenzene
0.0526
mg/Kg wet
0.0500
105
70-130
Page 30 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235621 - SW-846 3546
Blank (B235621-BLK1) Prepared: 07/16/19 Analyzed: 07/17/19
Acenaphthene
ND
0.17
mg/Kg wet
Acenaphthylene
ND
0.17
mg/Kg wet
Acetophenone
ND
0.34
mg/Kg wet
Aniline
ND
0.34
mg/Kg wet
Anthracene
ND
0.17
mg/Kg wet
Benzidine
ND
0.66
mg/Kg wet
Benzo(a)anthracene
ND
0.17
mg/Kg wet
Benzo(a)pyrene
ND
0.17
mg/Kg wet
Benzo(b)fluoranthene
ND
0.17
mg/Kg wet
Benzo(g,h,i)perylene
ND
0.17
mg/Kg wet
Benzo(b)fluoranthene
ND
0.17
mg/Kg wet
Benzoic Acid
ND
1.0
mg/Kg wet
Bis(2-chloroethoxy)methane
ND
0.34
mg/Kg wet
Bis(2-chloroethyl)ether
ND
0.34
mg/Kg wet
Bis(2-chloroisopropyl)ether
ND
0.34
mg/Kg wet
Bis(2-Ethylhexyl)phthalate
ND
0.34
mg/Kg wet
4-Bromophenylphenylether
ND
0.34
mg/Kg wet
Butylbenzylphthalate
ND
0.34
mg/Kg wet
Carbazole
ND
0.17
mg/Kg wet
4-Chloroaniline
ND
0.66
mg/Kg wet
4-Chloro-3-methylphenol
ND
0.66
mg/Kg wet
2-Chloronaphthalene
ND
0.34
mg/Kg wet
2-Chlorophenol
ND
0.34
mg/Kg wet
4-Chlorophenylphenylether
ND
0.34
mg/Kg wet
Chrysene
ND
0.17
mg/Kg wet
Dibenz(a,h)anthracene
ND
0.17
mg/Kg wet
Dibenzofuran
ND
0.34
mg/Kg wet
Di-n-butylphthalate
ND
0.34
mg/Kg wet
1,2-Dichlorobenzene
ND
0.34
mg/Kg wet
1,3-Dichlorobenzene
ND
0.34
mg/Kg wet
1,4-Dichlorobenzene
ND
0.34
mg/Kg wet
3,3-Dichlorobenzidine
ND
0.17
mg/Kg wet
2,4-Dichlorophenol
ND
0.34
mg/Kg wet
Diethylphthalate
ND
0.34
mg/Kg wet
2,4-Dimethylphenol
ND
0.34
mg/Kg wet
Dimethylphthalate
ND
0.34
mg/Kg wet
4,6-Dinitro-2-methylphenol
ND
0.34
mg/Kg wet
2,4-Dinitrophenol
ND
0.66
mg/Kg wet
2,4-Dinitrotoluene
ND
0.34
mg/Kg wet
2,6-Dinitrotoluene
ND
0.34
mg/Kg wet
Di-n-octylphthalate
ND
0.34
mg/Kg wet
1,2-Diphenylhydrazine/Azobenzene
ND
0.34
mg/Kg wet
Fluoranthene
ND
0.17
mg/Kg wet
Fluorene
ND
0.17
mg/Kg wet
Hexachlorobenzene
ND
0.34
mg/Kg wet
Hexachlorobutadiene
ND
0.34
mg/Kg wet
Hexachlorocyclopentadiene
ND
0.34
mg/Kg wet
Hexachloroethane
ND
0.34
mg/Kg wet
Indeno(1,2,3-cd)pyrene
ND
0.17
mg/Kg wet
Isophorone
ND
0.34
mg/Kg wet
1-Methylnaphthalene
ND
0.17
mg/Kg wet
2-Methylnaphthalene
ND
0.17
mg/Kg wet
V-04, V-05
V-34
V-34
V-05
Page 31 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
\nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235621 - SW-846 3546
Blank (B235621-BLK1)
Prepared: 07/16/19 Analyzed: 07/17/19
2-Methylphenol
ND
0.34
mg/Kg wet
3/4-Methylphenol
ND
0.34
mg/Kg wet
Naphthalene
ND
0.17
mg/Kg wet
2-Nitroaniline
ND
0.34
mg/Kg wet
3-Nitroaniline
ND
0.34
mg/Kg wet
4-Nitroaniline
ND
0.34
mg/Kg wet
Nitrobenzene
ND
0.34
mg/Kg wet
2-Nitrophenol
ND
0.34
mg/Kg wet
4-Nitrophenol
ND
0.66
mg/Kg wet
N-Nitrosodimethylamine
ND
0.34
mg/Kg wet
N-Nitrosodiphenylamine/Diphenylamine
ND
0.34
mg/Kg wet
N-Nitrosodi-n-propylamine
ND
0.34
mg/Kg wet
Pentachloronitrobenzene
ND
0.34
mg/Kg wet
V-16
Pentachlorophenol
ND
0.34
mg/Kg wet
Phenanthrene
ND
0.17
mg/Kg wet
Phenol
ND
0.34
mg/Kg wet
Pyrene
ND
0.17
mg/Kg wet
Pyridine
ND
0.34
mg/Kg wet
1,2,4,5-Tetrachlorobenzene
ND
0.34
mg/Kg wet
1,2,4-Trichlorobenzene
ND
0.34
mg/Kg wet
2,4,5-Trichlorophenol
ND
0.34
mg/Kg wet
2,4,6-Trichlorophenol
ND
0.34
mg/Kg wet
Surrogate:2-Fluorophenol
3.99
mg/Kg wet
6.67
59.9
30-130
Surrogate: Phenol-d6
4.19
mg/Kg wet
6.67
62.9
30-130
Surrogate: Nitrobenzene-d5
2.19
mg/Kg wet
3.33
65.6
30-130
Surrogate:2-Fluorobiphenyl
2.20
mg/Kg wet
3.33
66.1
30-130
Surrogate: 2,4,6-Tribromophenol
4.51
mg/Kg wet
6.67
67.7
30-130
Surrogate: p-Terphenyl-d14
2.38
mg/Kg wet
3.33
71.3
30-130
LCS (B235621-BSI)
Prepared: 07/16/19 Analyzed: 07/17/19
Acenaphthene
1.16
0.17
mg/Kg wet
1.67
69.5
40-140
Acenaphthylene
1.23
0.17
mg/Kg wet
1.67
73.9
40-140
Acetophenone
1.08
0.34
mg/Kg wet
1.67
64.8
40-140
Aniline
0.975
0.34
mg/Kg wet
1.67
58.5
10-140
Anthracene
1.26
0.17
mg/Kg wet
1.67
75.8
40-140
Benzidine
1.85
0.66
mg/Kg wet
1.67
111
40-140
Benzo(a)anthracene
1.24
0.17
mg/Kg wet
1.67
74.2
40-140
Benzo(a)pyrene
1.30
0.17
mg/Kg wet
1.67
77.8
40-140
Benzo(b)fluoranthene
1.21
0.17
mg/Kg wet
1.67
72.8
40-140
Benzo(g,h,i)perylene
1.18
0.17
mg/Kg wet
1.67
70.5
40-140
Benzo(k)fluoranthene
1.23
0.17
mg/Kg wet
1.67
73.9
40-140
Benzoic Acid
1.03
1.0
mg/Kg wet
1.67
61.9
30-130
Bis(2-chloroethoxy)methane
1.29
0.34
mg/Kg wet
1.67
77.6
40-140
Bis(2-chloroethyl)ether
1.11
0.34
mg/Kg wet
1.67
66.8
40-140
Bis(2-chloroisopropyl)ether
1.22
0.34
mg/Kg wet
1.67
73.4
40-140
Bis(2-Ethylhexyl)phthalate
1.28
0.34
mg/Kg wet
1.67
77.0
40-140
4-Bromophenylphenylether
1.10
0.34
mg/Kg wet
1.67
65.8
40-140
Butylbenzylphthalate
1.24
0.34
mg/Kg wet
1.67
74.4
40-140
Carbazole
1.27
0.17
mg/Kg wet
1.67
76.2
40-140
4-Chloroaniline
0.839
0.66
mg/Kg wet
1.67
50.3
10-140
4-Chloro-3-methylphenol
1.25
0.66
mg/Kg wet
1.67
75.0
30-130
2-Chloronaphthalene
1.01
0.34
mg/Kg wet
1.67
60.4
40-140
t
V-04, V-05
V-34
Page 32 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
\nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235621 - SW-846 3546
LCS (B235621-BS1)
Prepared: 07/16/19 Analyzed: 07/17/19
2-Chlorophenol
1.13
0.34
mg/Kg wet
1.67
67.6
30-130
4-Chlorophenylphenylether
1.16
0.34
mg/Kg wet
1.67
69.8
40-140
Chrysene
1.23
0.17
mg/Kg wet
1.67
74.0
40-140
Dibenz(a,h)anthracene
1.15
0.17
mg/Kg wet
1.67
69.2
40-140
Dibenzofuran
1.22
0.34
mg/Kg wet
1.67
73.4
40-140
Di-n-butylphthalate
1.18
0.34
mg/Kg wet
1.67
70.6
40-140
1,2-Dichlorobenzene
0.954
0.34
mg/Kg wet
1.67
57.2
40-140
1,3-Dichlorobenzene
0.928
0.34
mg/Kg wet
1.67
55.7
40-140
1,4-Dichlorobenzene
0.943
0.34
mg/Kg wet
1.67
56.6
40-140
3,3-Dichlorobenzidine
0.885
0.17
mg/Kg wet
1.67
53.1
20-140 V-34 t
2,4-Dichlorophenol
1.17
0.34
mg/Kg wet
1.67
70.1
30-130
Diethylphthalate
1.21
0.34
mg/Kg wet
1.67
72.6
40-140
2,4-Dimethylphenol
1.16
0.34
mg/Kg wet
1.67
69.6
30-130
Dimethylphthalate
1.21
0.34
mg/Kg wet
1.67
72.8
40-140
4,6-Dinitro-2-methylphenol
1.23
0.34
mg/Kg wet
1.67
74.0
30-130
2,4-Dinitrophenol
0.995
0.66
mg/Kg wet
1.67
59.7
30-130
2,4-Dinitrotoluene
1.36
0.34
mg/Kg wet
1.67
81.9
40-140
2,6-Dinitrotoluene
1.42
0.34
mg/Kg wet
1.67
84.9
40-140
Di-n-octylphthalate
1.24
0.34
mg/Kg wet
1.67
74.4
40-140
1,2-Diphenylhydrazine/Azobenzene
1.20
0.34
mg/Kg wet
1.67
71.8
40-140
Fluoranthene
1.28
0.17
mg/Kg wet
1.67
76.9
40-140
Fluorene
1.27
0.17
mg/Kg wet
1.67
76.4
40-140
Hexachlorobenzene
1.14
0.34
mg/Kg wet
1.67
68.3
40-140
Hexachlorobutadiene
0.971
0.34
mg/Kg wet
1.67
58.3
40-140
Hexachlorocyclopentadiene
0.829
0.34
mg/Kg wet
1.67
49.7
40-140 V-05
Hexachloroethane
0.958
0.34
mg/Kg wet
1.67
57.5
40-140
Indeno(1,2,3-cd)pyrene
1.27
0.17
mg/Kg wet
1.67
76.0
40-140
Isophorone
1.23
0.34
mg/Kg wet
1.67
73.9
40-140
1-Methylnaphthalene
1.14
0.17
mg/Kg wet
1.67
68.3
40-140
2-Methylnaphthalene
1.26
0.17
mg/Kg wet
1.67
75.4
40-140
2-Methylphenol
0.998
0.34
mg/Kg wet
1.67
59.9
30-130
3/4-Methylphenol
1.18
0.34
mg/Kg wet
1.67
71.0
30-130
Naphthalene
1.11
0.17
mg/Kg wet
1.67
66.7
40-140
2-Nitroaniline
1.42
0.34
mg/Kg wet
1.67
85.1
40-140
3-Nitroaniline
1.23
0.34
mg/Kg wet
1.67
73.9
30-140 t
4-Nitroaniline
1.54
0.34
mg/Kg wet
1.67
92.2
40-140
Nitrobenzene
1.17
0.34
mg/Kg wet
1.67
70.3
40-140
2-Nitrophenol
1.29
0.34
mg/Kg wet
1.67
77.3
30-130
4-Nitrophenol
1.35
0.66
mg/Kg wet
1.67
81.1
30-130
N-Nitrosodimethylamine
1.00
0.34
mg/Kg wet
1.67
60.2
40-140
N-Nitrosodiphenylamine/Diphenylamine
1.22
0.34
mg/Kg wet
1.67
72.9
40-140
N-Nitrosodi-n-propylamine
1.09
0.34
mg/Kg wet
1.67
65.5
40-140
Pentachloronitrobenzene
1.20
0.34
mg/Kg wet
1.67
71.8
40-140 V-16
Pentachlorophenol
0.940
0.34
mg/Kg wet
1.67
56.4
30-130
Phenanthrene
1.26
0.17
mg/Kg wet
1.67
75.8
40-140
Phenol
1.18
0.34
mg/Kg wet
1.67
70.8
30-130
Pyrene
1.24
0.17
mg/Kg wet
1.67
74.4
40-140
Pyridine
0.661
0.34
mg/Kg wet
1.67
39.6
30-140
1,2,4,5-Tetrachlorobenzene
1.09
0.34
mg/Kg wet
1.67
65.2
40-140
1,2,4-Trichlorobenzene
1.04
0.34
mg/Kg wet
1.67
62.2
40-140
2,4,5-Trichlorophenol
1.18
0.34
mg/Kg wet
1.67
70.5
30-130
2,4,6-Trichlorophenol
1.19
0.34
mg/Kg wet
1.67
71.4
30-130
Page 33 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235621 - SW-846 3546
LCS (B235621-BSI)
Prepared: 07/16/19 Analyzed: 07/17/19
Surrogate:2-Fluorophenol
4.64
mg/Kg wet
6.67
69.6
30-130
Surrogate: Phenol-&
4.85
mg/Kg wet
6.67
72.8
30-130
Surrogate: Nitrobenzene-d5
2.58
mg/Kg wet
3.33
77.3
30-130
Surrogate:2-Fluorobiphenyl
2.52
mg/Kg wet
3.33
75.7
30-130
Surrogate: 2,4,6-Tribromophenol
5.22
mg/Kg wet
6.67
78.3
30-130
Surrogate:p-Terphenyl-d14
2.60
mg/Kg wet
3.33
77.9
30-130
LCS Dup (B235621-BSD1)
Prepared: 07/16/19 Analyzed: 07/17/19
Acenaphthene
1.23
0.17
mg/Kg wet
1.67
74.0
40-140
6.30
30
Acenaphthylene
1.28
0.17
mg/Kg wet
1.67
76.7
40-140
3.77
30
Acetophenone
1.17
0.34
mg/Kg wet
1.67
70.4
40-140
8.26
30
Aniline
1.04
0.34
mg/Kg wet
1.67
62.6
10-140
6.74
50 $ #
Anthracene
1.34
0.17
mg/Kg wet
1.67
80.1
40-140
5.54
30
Benzidine
2.07
0.66
mg/Kg wet
1.67
124
40-140
11.2
30 V-04,V-05
Benzo(a)anthracene
1.27
0.17
mg/Kg wet
1.67
76.2
40-140
2.61
30
Benzo(a)pyrene
1.37
0.17
mg/Kg wet
1.67
82.0
40-140
5.26
30
Benzo(b)fluoranthene
1.29
0.17
mg/Kg wet
1.67
77.3
40-140
5.97
30
Benzo(g,h,i)perylene
1.13
0.17
mg/Kg wet
1.67
67.6
40-140
4.23
30
Benzo(k)fluoranthene
1.31
0.17
mg/Kg wet
1.67
78.5
40-140
6.14
30
Benzoic Acid
1.06
1.0
mg/Kg wet
1.67
63.3
30-130
2.27
50 $
Bis(2-chloroethoxy)methane
1.31
0.34
mg/Kg wet
1.67
78.8
40-140
1.51
30
Bis(2-chloroethyl)ether
1.17
0.34
mg/Kg wet
1.67
70.4
40-140
5.22
30
Bis(2-chloroisopropyl)ether
1.30
0.34
mg/Kg wet
1.67
78.0
40-140
6.05
30
Bis(2-Ethylhexyl)phthalate
1.32
0.34
mg/Kg wet
1.67
79.2
40-140
2.82
30
4-Bromophenylphenylether
1.20
0.34
mg/Kg wet
1.67
72.2
40-140
9.36
30
Butylbenzylphthalate
1.25
0.34
mg/Kg wet
1.67
74.9
40-140
0.696
30
Carbazole
1.34
0.17
mg/Kg wet
1.67
80.6
40-140
5.53
30
4-Chloroaniline
0.954
0.66
mg/Kg wet
1.67
57.2
10-140
12.8
30 V-34 t
4-Chloro-3-methylphenol
1.29
0.66
mg/Kg wet
1.67
77.1
30-130
2.76
30
2-Chloronaphthalene
1.08
0.34
mg/Kg wet
1.67
64.9
40-140
7.28
30
2-Chorophenol
1.20
0.34
mg/Kg wet
1.67
72.2
30-130
6.70
30
4-Chlorophenylphenylether
1.25
0.34
mg/Kg wet
1.67
75.2
40-140
7.53
30
Chrysene
1.28
0.17
mg/Kg wet
1.67
76.5
40-140
3.40
30
Dibenz(a,h)anthracene
1.11
0.17
mg/Kg wet
1.67
66.8
40-140
3.62
30
Dibenzofuran
1.29
0.34
mg/Kg wet
1.67
77.5
40-140
5.46
30
Di-n-butylphthalate
1.26
0.34
mg/Kg wet
1.67
75.8
40-140
7.02
30
1,2-Dichlorobenzene
1.05
0.34
mg/Kg wet
1.67
63.1
40-140
9.71
30
1,3-Dichlorobenzene
1.02
0.34
mg/Kg wet
1.67
61.2
40-140
9.45
30
1,4-Dichlorobenzene
1.04
0.34
mg/Kg wet
1.67
62.1
40-140
9.33
30
3,3-Dichlorobenzidine
0.924
0.17
mg/Kg wet
1.67
55.4
20-140
4.35
50 V-34 t #
2,4-Dichlorophenol
1.25
0.34
mg/Kg wet
1.67
75.3
30-130
7.13
30
Diethylphthalate
1.26
0.34
mg/Kg wet
1.67
75.6
40-140
4.05
30
2,4-Dimethylphenol
1.17
0.34
mg/Kg wet
1.67
70.1
30-130
0.802
30
Dimethylphthalate
1.27
0.34
mg/Kg wet
1.67
76.3
40-140
4.72
30
4,6-Dinitro-2-methylphenol
1.31
0.34
mg/Kg wet
1.67
78.5
30-130
5.98
30
2,4-Dinitrophenol
1.05
0.66
mg/Kg wet
1.67
63.2
30-130
5.67
30
2,4-Dinitrotoluene
1.48
0.34
mg/Kg wet
1.67
89.0
40-140
8.31
30
2,6-Dinitrotoluene
1.45
0.34
mg/Kg wet
1.67
87.3
40-140
2.74
30
Di-n-octylphthalate
1.30
0.34
mg/Kg wet
1.67
78.1
40-140
4.88
30
1,2-Diphenylhydrazine/Azobenzene
1.23
0.34
mg/Kg wet
1.67
74.0
40-140
3.13
30
Fluoranthene
1.37
0.17
mg/Kg wet
1.67
82.4
40-140
6.83
30
Fluorene
1.32
0.17
mg/Kg wet
1.67
79.2
40-140
3.65
30
Page 34 of 45

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235621 - SW-846 3546
LCS Dup (B235621-BSD1) Prepared: 07/16/19 Analyzed: 07/17/19
Hexachlorobenzene
1.22
0.34
mg/Kg wet
1.67
73.3
40-140
7.01
30
Hexachlorobutadiene
1.10
0.34
mg/Kg wet
1.67
65.8
40-140
12.1
30
Hexachlorocyclopentadiene
0.910
0.34
mg/Kg wet
1.67
54.6
40-140
9.35
30 V-05
Hexachloroethane
1.04
0.34
mg/Kg wet
1.67
62.4
40-140
8.27
30
Indeno(1,2,3-cd)pyrene
1.22
0.17
mg/Kg wet
1.67
73.4
40-140
3.45
30
Isophorone
1.26
0.34
mg/Kg wet
1.67
75.9
40-140
2.70
30
1-Methylnaphthalene
1.17
0.17
mg/Kg wet
1.67
70.5
40-140
3.14
30
2-Methylnaphthalene
1.30
0.17
mg/Kg wet
1.67
78.2
40-140
3.70
30
2-Methylphenol
1.07
0.34
mg/Kg wet
1.67
64.5
30-130
7.43
30
3/4-Methylphenol
1.24
0.34
mg/Kg wet
1.67
74.2
30-130
4.38
30
Naphthalene
1.20
0.17
mg/Kg wet
1.67
71.8
40-140
7.33
30
2-Nitroaniline
1.40
0.34
mg/Kg wet
1.67
84.2
40-140
1.16
30
3-Nitroaniline
1.30
0.34
mg/Kg wet
1.67
78.0
30-140
5.35
30 f
4-Nitroaniline
1.59
0.34
mg/Kg wet
1.67
95.6
40-140
3.68
30
Nitrobenzene
1.20
0.34
mg/Kg wet
1.67
72.1
40-140
2.58
30
2-Nitrophenol
1.33
0.34
mg/Kg wet
1.67
79.7
30-130
3.01
30
4-Nitrophenol
1.43
0.66
mg/Kg wet
1.67
85.7
30-130
5.54
50
N-Nitrosodimethylamine
1.03
0.34
mg/Kg wet
1.67
61.7
40-140
2.56
30
N-Nitrosodiphenylamine/Diphenylamine
1.29
0.34
mg/Kg wet
1.67
77.4
40-140
5.96
30
N-Nitrosodi-n-propylamine
1.16
0.34
mg/Kg wet
1.67
69.6
40-140
5.98
30
Pentachloronitrobenzene
1.24
0.34
mg/Kg wet
1.67
74.4
40-140
3.53
30 V-16
Pentachlorophenol
1.00
0.34
mg/Kg wet
1.67
60.1
30-130
6.38
30
Phenanthrene
1.34
0.17
mg/Kg wet
1.67
80.2
40-140
5.61
30
Phenol
1.24
0.34
mg/Kg wet
1.67
74.1
30-130
4.61
30
Pyrene
1.28
0.17
mg/Kg wet
1.67
77.0
40-140
3.49
30
Pyridine
0.693
0.34
mg/Kg wet
1.67
41.6
30-140
4.73
30 t
1,2,4,5-Tetrachlorobenzene
1.17
0.34
mg/Kg wet
1.67
70.1
40-140
7.30
30
1,2,4-Trichlorobenzene
1.13
0.34
mg/Kg wet
1.67
68.0
40-140
8.94
30
2,4,5-Trichlorophenol
1.26
0.34
mg/Kg wet
1.67
75.5
30-130
6.80
30
2,4,6-Trichlorophenol
1.27
0.34
mg/Kg wet
1.67
76.3
30-130
6.61
30
Surrogate:2-Fluorophenol
4.92
mg/Kg wet
6.67
73.8
30-130
Surrogate: Phenol-d6
4.99
mg/Kg wet
6.67
74.9
30-130
Surrogate: Nitrobenzene-d5
2.60
mg/Kg wet
3.33
78.1
30-130
Surrogate: 2-Fluorobiphenyl
2.68
mg/Kg wet
3.33
80.3
30-130
Surrogate: 2,4,6-Tribromophenol
5.43
mg/Kg wet
6.67
81.4
30-130
Surrogate: p-Terphenyl-d14
2.67
mg/Kg wet
3.33
80.1
30-130
Page 35 of 45

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B234917 - SW-846 3546
Blank (B234917-BLK1)
Prepared: 07/06/19 Analyzed: 07/09/19
Diesel Range Organics
ND
8.3
mg/Kg wet
Surrogate:2-Fluorobiphenyl
LCS (B234917-BS1)
2.00
mg/Kg wet
3.33 60.0
Prepared: 07/06/19 Analyzed: 07/09/19
40-140
Diesel Range Organics
25.7
8.3
mg/Kg wet
33.3 77.1
40-140
Surrogate:2-Fluorobiphenyl
LCS Dup (B234917-BSD1)
2.73
mg/Kg wet
3.33 82.0
Prepared: 07/06/19 Analyzed: 07/09/19
40-140
Diesel Range Organics
25.0
8.3
mg/Kg wet
33.3 74.9
40-140 2.94
Surrogate:2-Fluorobiphenyl
Matrix Spike (B234917-MS1)
2.67 mg/Kg wet
Source: 19GO278-02
3.33 80.2
Prepared: 07/06/19 Analyzed: 07/13/19
40-140
Diesel Range Organics
105
9.8
mg/Kg dry
39.2 103 6.83 *
40-140 MS-22
Surrogate: 2-Fluorobiphenyl
Matrix Spike Dup (B234917-MSD1)
1.72 mg/Kg dry
Source: 19GO278-02
3.92 43.8
Prepared: 07/06/19 Analyzed: 07/13/19
40-140
Diesel Range Organics
120
9.8
mg/Kg dry
39.2 103 42.9
40-140 12.6 30
Surrogate:2-Fluorobiphenyl
Batch B235063 - SW-846 5030B
2.12
mg/Kg dry
3.92 54.0
40-140
Blank (B235063-BLK1)
Prepared & Analyzed: 07/09/19
Gasoline Range Organics (GRO)
ND
1.0
mg/Kg wet
Surrogate: 1-Chloro-3-fluorobenzene
LCS (B235063-BS1)
16.6
µg/L
15.0 ill
Prepared & Analyzed: 07/09/19
70-130
Gasoline Range Organics (GRO)
0.251
0.010
mg/Kg wet
0.250 100
80-120
Surrogate: 1-Chloro-3-fluorobenzene
LCS Dup (B235063-BSD1)
16.6
µg/L
15.0 ill
Prepared & Analyzed: 07/09/19
70-130
Gasoline Range Organics (GRO)
0.252
0.010
mg/Kg wet
0.250 101
80-120 0.309 30
Surrogate:l-Chloro-3-fluorobenzene
Batch B235508 - SW-846 3546
17.2
µg/L
15.0 114
70-130
Blank (B235508-BLK1)
Prepared: 07/15/19 Analyzed: 07/16/19
Diesel Range Organics
ND
8.3
mg/Kg wet
Surrogate:2-Fluorobiphenyl
LCS (B235508-BS1)
3.47
mg/Kg wet
3.33 104
Prepared: 07/15/19 Analyzed: 07/16/19
40-140
Diesel Range Organics
24.0
8.3
mg/Kg wet
33.3 71.9
40-140
Surrogate:2-Fluorobiphenyl
3.35
mg/Kg wet
3.33 101
40-140
Page 36 of 45

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B235508 - SW-846 3546
LCS Dup (B235508-BSD1) Prepared: 07/15/19 Analyzed: 07/16/19
Diesel Range Organics 23.3 8.3 mg/Kg wet 33.3 69.9 40-140 2.88
Surrogate:2-Fluorobiphenyl 3.27 mg/Kgwet 3.33 98.0 40-140
Page 37 of 45

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 * FAX [phone] " TEL. [phone]
FLAG/QUALIFIER SUMMARY
* QC result is outside of established limits.
fi Wide recovery limits established for difficult compound.
$ Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
ND Not Detected
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
L-02 Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
MS-22 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the
two MS/MSD results is within method specified criteria.
V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-05 Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-16 Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may
be associated with reported result.
V-20 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-35 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this
compound. Reported result is estimated.
Z-01 Results in the diesel range organics do not appear to be petroleum related.
Page 38 of 45

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ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8015C in Product/Solid
Diesel Range Organics
NC
SW-846 8015C in Soil
Gasoline Range Organics (GRO)
NY,VA,NH,NC
Diesel Range Organics
NY,VA,NH,NC
SW-846 8015C in Water
Diesel Range Organics
NY,VA,NH,NC
SW-846 8260D in Soil
Acetone
NC
Acrylonitrile
NC
tert-Amyl Methyl Ether (TAME)
NC
Benzene
NC
Bromobenzene
NC
Bromochloromethane
NC
Bromodichloromethane
NC
Bromoform
NC
Bromomethane
NC
2-Butanone (MEK)
NC
tert-Butyl Alcohol (TBA)
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
tert-Butyl Ethyl Ether (TBEE)
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorodibromomethane
NC
Chloroethane
NC
Chloroform
NC
Chloromethane
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibromo-3-chloropropane (DBCP)
NC
1,2-Dibromoethane (EDB)
NC
Dibromomethane
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
trans-1,4-Dichloro-2-butene
NC
Dichlorodifluoromethane (Freon 12)
NC
1,1-Dichloroethane
NC
1,2-Dichloroethane
NC
1,1-Dichloroethylene
NC
cis-1,2-Dichloroethylene
NC
trans-1,2-Dichloroethylene
NC
1,2-Dichloropropane
NC
1,3-Dichloropropane
NC
Page 39 of 45

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ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8260D in Soil
2,2-Dichloropropane
NC
1,1-Dichloropropene
NC
cis-1,3-Dichloropropene
NC
trans-1,3-Dichloropropene
NC
Diethyl Ether
NC
Diisopropyl Ether (DIPE)
NC
1,4-Dioxane
NC
Ethylbenzene
NC
Hexachlorobutadiene
NC
2-Hexanone (MBK)
NC
Isopropylbenzene (Cumene)
NC
p-Isopropyltoluene (p-Cymene)
NC
Methyl tert-Butyl Ether (MTBE)
NC
Methylene Chloride
NC
4-Methyl-2-pentanone (MIBK)
NC
Naphthalene
NC
n-Propylbenzene
NC
Styrene
NC
1, 1, 1,2-Tetrachloroethane
NC
1,1,2,2-Tetrachloroethane
NC
Tetrachloroethylene
NC
Tetrahydrofuran
NC
Toluene
NC
1,2,3-Trichlorobenzene
NC
1,2,4-Trichlorobenzene
NC
1,3,5-Trichlorobenzene
NC
1, 1, 1 -Trichloroethane
NC
1,1,2-Trichloroethane
NC
Trichloroethylene
NC
Trichlorofluoromethane (Freon 11)
NC
1,2,3-Trichloropropane
NC
1,1,2-Trichloro-1,2,2-ttifluoroethane (Freon 113)
NC
1,2,4-Trimethylbenzene
NC
1,3,5-Trimethylbenzene
NC
Vinyl Chloride
NC
m+p Xylene
NC
o-Xylene
NC
SW-846 8270E in Soil
Acenaphthene
CT,NY,NH,ME,NC,VA
Acenaphthylene
CT,NY,NH,ME,NC,VA
Acetophenone
NY,NH,ME,NC,VA
Aniline
NY,NH,ME,NC,VA
Anthracene
CT,NY,NH,ME,NC,VA
Benzidine
CT,NY,NH,ME,NC,VA
Benzo(a)anthracene
CT,NY,NH,ME,NC,VA
Benzo(a)pyrene
CT,NY,NH,ME,NC,VA
Page 40 of 45

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ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270E in Soil
Benzo(b)fluoranthene
CTNY,NH,ME,NC,VA
Benzo(g,h,i)perylene
CTNY,NH,ME,NC,VA
Benzo(k)fluoranthene
CTNY,NH,ME,NC,VA
Benzoic Acid
NY,NH,ME,NC,VA
Bis(2-chloroethoxy)methane
CTNY,NH,ME,NC,VA
Bis(2-chloroethyl)ether
CTNY,NH,ME,NC,VA
Bis(2-chloroisopropyl)ether
CTNY,NH,ME,NC,VA
Bis(2-Ethylhexyl)phthalate
CTNY,NH,ME,NC,VA
4-Bromophenylphenylether
CTNY,NH,ME,NC,VA
Butylbenzylphthalate
CTNY,NH,ME,NC,VA
Carbazole
NC
4-Chloroaniline
CTNY,NH,ME,NC,VA
4-Chloro-3-methylphenol
CTNY,NH,ME,NC,VA
2-Chloronaphthalene
CTNY,NH,NC,VA
2-Chlorophenol
CTNY,NH,ME,NC,VA
4-Chlorophenylphenylether
CTNY,NH,ME,NC,VA
Chrysene
CTNY,NH,ME,NC,VA
Dibenz(a,h)anthracene
CTNY,NH,ME,NC,VA
Dibenzofuran
CTNY,NH,ME,NC,VA
Di-n-butylphthalate
CT,NY,NH,ME,NC,VA
1,2-Dichlorobenzene
NY,NH,ME,NC,VA
1,3-Dichlorobenzene
NY,NH,ME,NC,VA
1,4-Dichlorobenzene
NY,NH,ME,NC,VA
3,3-Dichlorobenzidine
CTNY,NH,ME,NC,VA
2,4-Dichlorophenol
CTNY,NH,ME,NC,VA
Diethylphthalate
CTNY,NH,ME,NC,VA
2,4-Dimethylphenol
CTNY,NH,ME,NC,VA
Dimethylphthalate
CTNY,NH,ME,NC,VA
4,6-Dinitro-2-methylphenol
CTNY,NH,ME,NC,VA
2,4-Dinitrophenol
CTNY,NH,ME,NC,VA
2,4-Dinitrotoluene
CTNY,NH,ME,NC,VA
2,6-Dinitrotoluene
CTNY,NH,ME,NC,VA
Di-n-octylphthalate
CTNY,NH,ME,NC,VA
1,2-Diphenylhydrazine/Azobenzene
NY,NH,ME,NC,VA
Fluoranthene
CTNY,NH,ME,NC,VA
Fluorene
NY,NH,ME,NC,VA
Hexachlorobenzene
CTNY,NH,ME,NC,VA
Hexachlorobutadiene
CTNY,NH,ME,NC,VA
Hexachlorocyclopentadiene
CTNY,NH,ME,NC,VA
Hexachloroethane
CTNY,NH,ME,NC,VA
Indeno(1,2,3-cd)pyrene
CTNY,NH,ME,NC,VA
Isophorone
CTNY,NH,ME,NC,VA
1-Methylnaphthalene
NC
2-Methylnaphthalene
CTNY,NH,ME,NC,VA
2-Methylphenol
CTNY,NH,ME,NC,VA
3/4-Methylphenol
CTNY,NH,ME,NC,VA
Naphthalene
CTNY,NH,ME,NC,VA
Page 41 of 45

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8270E in Soil
2-Nitroaniline
CT,NY,NH,ME,NC,VA
3-Nitroaniline
CT,NY,NH,ME,NC,VA
4-Nitroaniline
CT,NY,NH,ME,NC,VA
Nitrobenzene
CT,NY,NH,ME,NC,VA
2-Nitrophenol
CT,NY,NH,ME,NC,VA
4-Nitrophenol
CT,NY,NH,ME,NC,VA
N-Nitrosodimethylamine
CT,NY,NH,ME,NC,VA
N-Nitrosodi-n-propylamine
CT,NY,NH,ME,NC,VA
Pentachloronitrobenzene
NY,NC
Pentachlorophenol
CT,NY,NH,ME,NC,VA
Phenanthrene
CT,NY,NH,ME,NC,VA
Phenol
CT,NY,NH,ME,NC,VA
Pyrene
CT,NY,NH,ME,NC,VA
Pyridine
CT,NY,NH,ME,NC,VA
1,2,4,5-Tetrachlorobenzene
NY,NC
1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA
2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA
2,4,6-Trichlorophenol
CT,NY,NH,ME,NC,VA
2-Fluorophenol
NC
The CON -TEST Environmental
Laboratory operates under the following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2005
100033
03/1/2020
MA
Massachusetts DEP
M-MA100
06/30/2020
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY
New York State Department of Health
10899 NELAP
04/1/2020
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2020
RI
Rhode Island Department of Health
LA000112
12/30/2019
NC
North Carolina Div. of Water Quality
652
12/31/2019
NJ
New Jersey DEP
MA007 NELAP
06/30/2020
FL
Florida Department of Health
E871027 NELAP
06/30/2020
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2020
ME
State of Maine
2011028
06/9/2021
VA
Commonwealth of Virginia
460217
12/14/2019
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW
Vermont Department of Health Drinking
Water
VT-255716
06/12/2020
NC-DW
North Carolina Department of Health
25703
07/31/2019
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2020
Page 42 of 45

Table of Contents
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7/6/2019 Track your package or shipment with FedEx Tracking
Table of Contents
%7764.E081 636 � �=
Delivered
Saturday 7/Q6%2-19 at 11:00 a
DELIVERED
Signed for by: M.POVEST
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
FROM TO
Ralcigli, NC US PAST LO��Giv1UADOln�, MA US
Orygin Tennina! [-::,,l!H non l_ocation
RALEIGH, NC WINDSOR LOCKS, CT
Shipment Facts
TRACKING NUM13ER
SERVICE
WEIGHT
//564g0816s6
FedEx Priority Overnight
15 €bs i 6.8 kas
DIMENSIONS
DELIVERED TO
TOTAL PIECES
18x11 xis In.
Shiphi�iglRec ivincd
1
TOTAL SHIPMENT WEIGHT
TERMS
SHIPPER REFERENCE
15) lbs / 6 g k9s
I bird Party
80
PACKAGING
SPECIAL HANDLING SECTION
STANDARD TRANSIT
Your Packaging
SeiIUfday Delivery, Additional Handling
Surcharge
71"W2019 by 12 001p1m,
SHIP DATE
ACTUAL DELIVERY
0
Sat 7/06/2019 11.00 anj
Fri //05/ 2019
Travel History
Saturday,7/06/2019
11:00 am EAST LONGMEADOW, MA Delivered
&21 am WINDSOR LOCKS, CT On FedEx vehicle for delivery
https:/Iwww.fedex,com/apps/fodextrack/?action=track&trackingnumber=775644081636&cntry_code=us&locale=en US
Local Scan Time `1/
Page 44 of 45

Table of Contents
Received By
Date
How were the samples In Cooler received? "` No Cooler
Direct from Sampling
Were samples within By Gun #
Temperature? 2-6°C
Time J r c u
On ice No Ice
Ambient Melted Ice
Actual Temp - S:
By Blank IT Actual Temp -
Was Custody Seal Intact? —_ VA Were Samples Tampered with?
Was COC Relinquished ? �- Does Chain Agree With Samples?
Are there broken/leaking/loose caps on any samples? F -r
Is COC in ink/ Legible? -T-
Did COC include all Client
{
pertinent Information? Project
T-
Are Sample labels filled out and legible?
Are there Lab to Filters?
Are there Rushes?
Are there Short Holds?
Is there enough Volume?
-T-_
Is there Headspace where applicable?
Proper Media/Containers Used?
-�
T
Were trip blanks received?
Do all samples have the proper pH?
�4f
Were samples received within holding time?
Analysis ;- Sampler Name T
ID's Collection Dates/Times t
Who was notified?
Who was notified?
Who was notified?
MS/MSD?
Is splitting samples required?
On COC? 41
Acid r1nen
f