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HomeMy WebLinkAbout04017_Burlington Mills_Site Assessment Report_LSA_20011108SITE ASSESSMENT REPORT FORMER BURLINGTON INDUSTRIES FACILITY MOORESVILLE, NORTH CAROLINA Prepared For: Cherokee Investment Partners 702 Oberlin Road Suite 150 Raleigh, North Carolina 27605 Prepared By: Mid-Atlantic Associates, P.A. 409 Rogers View Court Raleigh, North Carolina 27610 (919) 250-9918 November 8, 2001 MP?;{\J'r~4NTl<( EngineerinR & Environmental Solutions • • SITE ASSESSMENT REPORT FORMER BURLINGTON INDUSTRIES FACILITY MOORESVILLE, NORTH CAROLINA Prepared For: Cherokee Investment Partners 702 Oberlin Road Suite 150 < Raleigh, North Carolina 27605 Prepared By: Mid-Atlantic Associates, P.A. 409 Rogers View Court Raleigh, North Carolina 27610 (919) 250-9918 November 8, 2001 MP?;{\Jl~~NTl~ Engineering & Enl'irvnmnrtul Solutions • • • Prepared For: MP?~~:fr~4NTl~ Engineering & EnvirOnmental Solutions 409 Rogers View Cmm I Raleigh I North Carolina 127610 800-486-7568/919-250-9918 i919-250-9950 Fanimile www.maaonline.com SITE ASSESSMENT REPORT FORMER BURLINGTON INDUSTRIES FACILITY MOORESVILLE, NORTH CAROLINA Mid-Atlantic Associates Job No. OOOR1127 .00 Prepared By: Cherokee Investment Partners 702 Oberlin Road MID-ATLANTIC ASSOCIATES, P.A. Suite 150 Raleigh, North Carolina 27605 • TABLE OF CONTENTS EXECUTIVE SUMMARY ......................................................................... i 1.0 GENERAL INFORMATION ....................................................................... 1 1 . 1 Introduction and Background ........................................................... 1 1 .2 Previous Environmental Investigations .............................................. 1 2.0 SCOPE OF SERVICES ............................................................................. 2 3.0 SITE GEOLOGY AND HYDROGEOLOGY ................................................... 3 3.1 Site Geology ................................................................................. 3 3.2 Site Hydrogeology ......................................................................... 4 4.0 SUMMARY OF FIELD ACTIVITIES ........................................................... 6 4.1 Hazardous Materials Inventory and Receptors .................................... 6 4.2 Soil Assessment Activities .............................................................. 6 4.3 Groundwater Assessment Activities ................................................. 8 • 4.4 Surface water Sampling Activities ................................................... 9 5.0 SAMPLING RESULTS ............................................................................. 9 5.1 Soil Analytical Results .................................................................... 9 5.1 .1 AST, Garage, and Shop Areas ............................................. 9 5.1 .2 UST Incident Area ............................................................ 10 5.1.3 Transformer Areas ............................................................ 10 5. 1 .4 Railroad Spur Area ........................................................... 1 0 5.2 Groundwater Analytical Results ..................................................... 10 5.2.1 UST Incident Area ............................................................ 11 5.2.2 Southern Portion of Site .................................................... 11 5.2.3 Southeastern Portion of Site .............................................. 11 5.3 Surface Water Sampling Results .................................................... 12 6.0 EVALUATION OF POTENTIAL STREAM IMPACTS ................................... 12 6.1 Surface Water Modeling ............................................................... 12 7.0 CONCLUSIONS AND RECOMMENDATIONS ........................................... 13 8.0 REFERENCES ...................................................................................... 14 • MP?;{\J,~4NTJ~ Engineering & Enl'irunmentul Solutions • • • DRAWINGS Drawing 1.1 Drawing 1.2 Drawing 2.1 Drawing 3.1 Drawing 4.1 Drawing 5.1 Drawing 5.2 Drawing 5.3 Drawing 5.4 TABLES Table 3.1 Table 3.2 Table 4.1 Table 4.2 Table 4.3 Table 4.4 Table 4.5 Table 7.1 APPENDICES Appendix A Appendix B Appendix C Appendix D Appendix E Appendix F Appendix G TABLE OF CONTENTS (CONT.) Topographic Location Map Site Map Potential Contaminant Source and Sample Location Map Estimated Groundwater Flow Map-9/17/01 Receptor Survey Map Summary of Laboratory Results-Soil Samples (Volatile/Semi-Volatile) Summary of Laboratory Results-Soil Samples (Metals) Summary of Laboratory Results -Groundwater Samples (Volatile/Semi-Volatile) Summary of Laboratory Results-Groundwater Samples (Metals) Physical Soil Properties Laboratory Test Data Monitoring Well Casing and Water Elevation Worksheet Summary of Chemical Constituents Detected in Soil Transformer Substation Data Summary of Chemical Constituents Detected in Groundwater Field Measurements Summary of Geochemical Constituents Detected in Groundwater and Soil Evaluation of Potential Environmental Concerns Boring Logs/Headspace Results Soil Grain Size/Bulk Density Analysis Well Construction Records Rising Head Test Receptor Survey Laboratory Analytical Report and Chain-of-Custody Surface Water Modeling Results MP?;~~\~}A{\NTl~ EnHineering & Enl'iranmental Solutions • • • EXECUTIVE SUMMARY The former Burlington Industries facility is located at 476 South Main Street in Mooresville, North Carolina. The site includes a vacant textile manufacturing plant located on 27 acres of land near downtown Mooresville. The site was developed around 1 900 and was used to prepare, weave, dye and finish cotton fiber yarn until it was closed in 2000. A comprehensive assessment of environmental conditions at the site was conducted to support site redevelopment under the North Carolina Brownfield Program. The assessment included the analyses of soil and groundwater samples collected from across the site and in those areas where hazardous materials and petroleum products were used at the facility --a total of 34 soil sampling locations were evaluated and 15 groundwater monitoring wells were installed. The assessment also included an evaluation of potentially sensitive receptors around the former mill. There is a Class C surface water body (the unnamed tributary to Dye Creek) located 200 feet south of the site, but there are no other environmental receptors or groundwater use in the area. In a majority of both the soil and groundwater samples, no contamination was found. Soil contamination was limited to oil staining and low levels of PCBs in several transformer areas and low levels of petroleum constituents in a former underground storage tank (UST) area. Low levels of petroleum constituents were also found in groundwater in the UST area, but at concentrations that will likely require no further action. Three chlorinated solvents (chloroform, 1, 1-dichloroethene and tetrachloroethene) were found in groundwater in the southern portion of the property, but at concentrations that are not expected to pose a threat to either human health or the environment. A separate report entitled Phase I Limited Site Assessment Report and Request for No Further Action has been submitted to the North Carolina Department of Environment and Natural Resources, UST Section, Mooresville Regional Office to close the UST incident. Additional environmental response actions planned in support of the site redevelopment include the following: • • • The remaining coal at the site, the oil/water mixture in the hydraulic jack casings, cooling water towers and any sludge in wastewater tanks, basins or process lines will either be removed or decontaminated as necessary during site demolition and renovation. The existing pad and pole-mounted transformers will be removed and the soil contamination in and around the substations will be excavated and disposed. The low levels of chlorinated solvent contamination in groundwater will be allowed to naturally attenuate as there are no drinking water wells on and around the site and there are no present or expected future impacts to surface water receptors . MP?;{\fl~4-NTJ.~ Enginrrriltf( & Enl'ironmrntal Solutions • • • 1.0 GENERAL INFORMATION 1 .1 Introduction and Background ' ·-"· The former Burlington Industries facility is located at 476 South Main Street in Mooresville, North Carolina (Drawings 1.1 and 1 .2). The site was purchased by Cherokee Mooresville, L.P. (Cherokee) from Burlington Industries (Burlington) in June 2001. The site includes a 1 00-year-old textile plant located on approximately 27 acres of land and several buildings totaling approximately 1 .3 million square feet. The plant has reportedly always been used for yarn manufacturing from cotton fiber and several different dyeing and finishing processes have likely been used at the site. The manufacturing operations were reportedly primarily water-based, associated with cotton products, and not chemical-intensive. The textile plant is currently inactive and the site is scheduled for redevelopment. Prior to purchasing the facility, Cherokee interviewed Burlington employees and the local publicly operated treatment works (POTW) pre-treatment coordinator and reviewed available records regarding the operation of the plant. With the exception of a low-risk underground storage tank (UST) incident, which is expected to be closed without further action, there were no other reported releases or incidents associated with the plant. There was no indication of landfilling or other on-site waste disposal activities. At the time of closing, the facility was listed as a small quantity hazardous waste generator for the operation of the facility by Burlington Industries . The assessment activities presented in this report support redevelopment of the site under the North Carolina Department of Environment and Natural Resources (NCDENR) Brownfields Program. The information contained in this report has also been used, in part, to support a request of no further action for a 1 989 underground storage tank (UST) incident (No. 08171 ). The information supporting incident closure is contained in a separate report prepared by Mid-Atlantic entitled Phase I Limited Site Assessment Report and Request for No Further Action. 1 .2 Previous Environmental Investigations Limited investigations had been conducted at the facility before Cherokee bought it in 2001. These activities included closure of six USTs in 1989 by SPATCO for Burlington Industries. Evidence of soil contamination was discovered during UST closure and was reported to the NCDENR, Mooresville Regional Office. A receptor survey was conducted by Trigon Engineering Consultants, Inc. (Trigon) to support purchase of the property by Cherokee. Mid-Atlantic also prepared a draft preliminary data package that supported a second phase of assessment activities to support limited groundwater modeling. The results contained in the draft data package were reported to the NCDENR Mooresville Regional Office. This report presents the information from all of our assessment activities conducted to date. A list of previous environmental reports are summarized below: MP?;{\:E~4NTJS:. E111-1ineering & Environmental Solutions • • • . Site Assessment Report Former Burlington Industries Facility Mooresville, North Carolina November 8, 2001 Page 2 • Laboratory Results, Soil Samples, Burlington Industries Facility, February 3, 1989. SPA TCO Environmental Services. • Laboratory Results, Soil Samples, Burlington Industries Facility, May 19, 1989. SPA TCO .Environmental Services. • Phase I Environmental Assessment, July 2000. IT Corporation. • Receptor Survey and Review of Environmental Incident, Burlington Industries, January 22, 2001. Trigon Engineering Consultants, Inc. • Draft Preliminary Data Package, Former Burlington Industries Facility, July 17, 2001. Mid-Atlantic Associates, P.A. • Notification of Site Activities, Former Burlington Industries Facility, July 25, 2001. Information of site activities to NCDENR, Division of Water Quality, Mooresville Regional Office. Mid-Atlantic Associates, P.A. • Phase I Limited Site Assessment Report and Request for No Further Action, October 31, 2001. Mid-Atlantic Associates, P.A . 2.0 SCOPE OF SERVICES The objective of our services was to determine the absence or presence of groundwater and soil contamination attributable to previous site operations and potential off-site sources of contamination and potential impacts to receptors. Prior to starting the on-site investigation work, we reviewed the plant operations and visited the site to identify the types, quantities, and location of hazardous material and petroleum products used at the plant. Seventeen locations were initially selected for further assessment (Drawing 2.1 I. The physical testing laboratory (identified as (M) on Drawing 1 .2) was not included in assessment activities after it was discovered that chemicals were not used in laboratory processes. Soil and/or groundwater samples were collected from the remaining areas to determine the absence or presence of contamination at each location. The locations of these seventeen areas and . corresponding sample locations are listed and shown on Drawing 2.1. The assessment information was used to identify and evaluate potential environmental concerns (PECs) and Recommended Response Actions. Activities were conducted to support a Brownfields agreement with the NCDENR Superfund Section and to support site closure of UST incident No. 08171 under the NCDENR UST Section, Mooresville Regional Office. MP?;~J~~~NTl~ Engineerinl( & Enl'ironmenral Solurions • • • Site Assessment Report November 8, 2001 Page 3 Former Burlington Industries Facility Mooresville, North Carolina The scope of services included the following tasks: 3.0 3.1 • Collected soil samples at 34 locations at the 1 6 potential contaminant source areas throughout the site (see Drawing 2.1); • Installed 15 monitoring wells throughout the site (see Drawing 2.1 ); •· Performed rising head tests on selected wells and collected soil samples for grain-size analysis to provide hydraulic conductivity estimates; • Analyzed soil and groundwater samples for one or more of the following; EPA Method 8260 for volatile organic compounds (VOCs), EPA Method 8270 for base neutral and acid extractable semi-volatile organic compounds (SVOCs), Priority Pollutant Metals (13 metals), EPA Method 8082 for PCBs, EPA Method 8015 for total petroleum hydrocarbons (TPH) using preparation method 3550/5030, Massachusetts Department of Environmental Protection (MADEP) Method for volatile petroleum hydrocarbons (VPH) and extractabl.e petroleum hydrocarbons (EPH), EPA Method 9071 for oil and grease, and EPA Method 6010 for lead. Selected soil and groundwater samples were also analyzed for various geochemical parameters to evaluate aquifer conditions; • Identified receptors in and around the plant site; • Collected a surface water sample from an off-site stream to demonstrate it had not been impacted; and • Conducted limited surface water modeling. SITE GEOLOGY AND HYDROGEOLOGY Site Geology The site is located in the Charlotte Belt region of the Piedmont Physiographic Province of North Carolina. The surficial geology consists of residual soils that have weathered in-place from underlying intrusive granite bedrock. The surrounding topography consists of gently rolling land and small drainage features. There were no bedrock outcrops ident~fied at the site; however, according to the Geologic Map of North Carolina, the geologic rock type underlying the site consists of post- tectonic porphyritic granite known as the Mooresville Pluton, which is part of the larger Churchland Plutonic Suite (Goldsmith and others, 1988). Soil logged from the borings in general accordance with the Unified Soil Classification System (USCS, ASTM D 2488-93) revealed predominantly clayey and silty soils from the surface to depths of 5 feet (MW-6) to 45 feet (MW-12) below land surface (BLS). Below the clay and silt, typically fine to coarse sand with varying amounts of silt and mica were encountered. Alluvial material was MP?;~J,~4NTls; Engineering & Enl'ironmental Solutions • • • Site Assessment Report Former Burlington Industries Facility Mooresville, North Carolina November 8, 2001 Page 4 encountered at MW-9 from 0.5 feet to the termination depth of 17 feet and at MW- 13 near the termination depth of 22 feet. Fractured bedrock was encountered at five well locations, while utilizing air-rotary drilling equipment, at depths of 1 8 feet (MW-11) to 38 feet (MW-3) BLS. Refusal, using a truck-mounted Geoprobe® rig, was encountered at 15 soil-boring locations at depths of two feet (L-1 a) to 14.5 feet (L-1 b). No rock samples were obtained in any of the borings. Refer to soil boring logs in Appendix A for a complete description of subsurface materials. Selected soil samples were submitted for laboratory testing of physical soil properties in accordance with appropriate ASTM methods. The laboratory testing was performed to determine hydrogeologic properties for use in site characterization and modeling. The physical tests performed include grain-size distribution (using sieve and hydrometer methods) and dry density. Test results and sample information are summarized in Table 3.1 and complete laboratory reports are included in Appendix B. 3.2 Site Hydrogeology Data from the installation of thirteen Type II, one intermediate Type II and one Type Ill monitoring wells were used to characterize the site hydrogeology. Details about the construction and sampling of these wells are provided in Sections 4.0 and 5.0. The locations of these wells are provided in Drawing 2. 1 and well construction records are provided as Appendix C. Results from our assessment activities indicate that a medium to coarse sand, with varying amounts of silt and clay, typically comprises the surficial aquifer of the site. Partially weathered rock, the transition zone from saprolite to bedrock, and the upper portion of fractured bedrock are also considered part of the surficial aquifer. Groundwater beneath the site is generally present at depths ranging from approximately seven (MW-13) to 41 (MW-6) feet BLS. The surficial aquifer extends to depths of more than 60 feet. The elevations of the top of casing for each of the monitoring wells and the surface water elevation of an adjacent perennial, unnamed tributary to Dye Creek were determined by a Registered Land Surveyor. Groundwater elevation data from monitoring wells MW-1 through MW-13 were determined using the elevation data and depth to groundwater readings (Table 3.2). Results indicate a general southerly groundwater flow direction toward the unnamed tributary to Dye Creek that is located off of the southern portion of the site (Drawing 3.1). Groundwater flow generally mimics the site topography. The elevation of the surface water in the unnamed tributary to Dye Creek also suggests that the water table intersects this streambed . MP?;{\flA{\NTlS:. En8inerring & £1n'ironmrn1al Solution.! • • • Site Assessment Report Former Burlington Industries Facility Mooresville, North Carolina November 8, 2001 Page 5 Horizontal gradients of groundwater flow range from ab.out 0.017 ft/ft in the northwestern part of the site (monitoring well MW-4, main facility area) to about 0.055 ft/ft in the southeastern part of the site (monitoring wells MW-8 and MW-9). The average gradient across the area is about 0.04 ft/ft. Vertical gradients may be approximated by comparing water levels in clustered (nested) wells. Two well clusters exist at the site, monitoring wells MW-4/MW-4s located in the main facility area and MW-8/MW-8i located at the downgradient area of the site (see Figure 3.1 for locations). Using the water-level data in Table 3.2, the vertical gradients at the two cluster locations are as follows: MW-4 858.93 MW-4s 858.79 MW-8 837.20 MW-8i 836.57 Notes: +0.14 -0.63 836.20 25.56 861.76 838.10 1---------1 23.90 814.20 +0.005 -0.026 1 Vertical hydraulic gradient: (-) negative represents downward ( +) positive represents upward flow L Elevation difference between two screen midpoints H Water table elevation difference between two wells in well nest (Hs-H and Hi-H)) The horizontal and vertical gradients are likely affected by the historical use and processing of high volumes of water and the presence of the facility's water reservoir and leakage from subsurface water and water process lines. Aquifer conditions may change once demolition of water and wastewater systems has occurred. Rising head tests for estimating hydraulic conductivity were performed in monitoring wells MW-4s, MW-8 and MW-1 0 with the following results: MP?;~J'~~4NTl9, Engineerinf< & Enl'ironmental Solutions • • • Site Assessment Report Former Burlington Industries Facility Mooresville, North Carolina November 8, 2001 Page 6 Horizontal hydraulic conductivity (k) determined from the field tests range from 4 x 1 o-7 to 6 x 1 o-5 centimeters per second (em/sec). The average hydraulic conductivity is about 2 x 1 o-5 em/sec. This translates to values ranging from 0.001 to 0.2 feet per day (ft/day) with an average value of 0.07 ft/day. This information is indicative of relatively tight soils and reflected in slow groundwater flow rates across the site. Supporting data are included in Appendix D. 4.0 SUMMARY OF FIELD ACTIVITIES 4.1 Hazardous Materials Inventory and Receptors A list of areas where chemicals and petroleum products were used or stored was prepared to develop the assessment scope of work. These locations are shown on Drawing 2.1. A receptor survey was conducted by Trigon Engineering on behalf of Cherokee on December 19, 2000, to identify the presence of sensitive receptors within 1,500 feet of the former Burlington Industries facility. The results of the survey indicate there are no known water-supply wells within 1 ,500 feet of the facility. A copy of the receptor survey is provided in Appendix E. Mid-Atlantic identified two potential receptors within 1,500 feet of the facility. A tributary to Dye Creek is located approximately 200 feet southeast of the southeast property boundary along College Street. The presence of flowing water and the groundwater elevation data provided in Section 3.2 of this report suggests that it is a perennial stream. The stream flows to the west-southwest where it converges with Dye Creek. Another potential receptor may include the on-site, concrete-lined, water supply reservoir that is currently used for the facility's fire protection sprinkler system. Water for this pond was pumped from another water-supply pond located off-site to the south by Dye Creek. 4.2 Soil Assessment Activities Field activities were conducted in June of 2001. Thirty-four soil samples were collected at locations where hazardous materials and petroleum products were utilized at the plant. The borings were advanced either with a truck-mounted Geoprobe"' rig or with a hand auger for difficult access areas. Each boring was advanced until auger refusal or groundwater was encountered. Soil samples were collected at a minimum of five-foot intervals. The samples were visually examined, classified and screened for evidence of contamination. The soil samples were MP?;~~\fl~4NTl~ Engi11eering & En1·ironmenral Solutions • • • Site Assessment Report Former Burlington Industries Facility Mooresville, North Carolina November 8, 2001 Page 7 screened for VOCs using a Flame Ionization Detector (FlO) and the headspace method. Soil samples from selected locations that displayed the greatest indications of potential contamination were submitted for laboratory analysis. Soil boring logs and headspace results are provided in Appendix A. Twenty-one soil samples were collected from boring locations where headspace readings suggested the possible presence of contamination or to verify an apparent lack of contamination. The samples were submitted to Prism Laboratories, Inc. (Prism) of Charlotte for analyses based on historical activities or processes at each location. Ten samples were analyzed for VOCs, eight were analyzed for SVOCs, eight were analyzed for total metals, eight were sampled for PCBs, three were analyzed for oil and grease, three were analyzed for VPH and EPH, three were analyzed for total lead, four were analyzed for diesel range TPH, and three samples were analyzed for gasoline range TPH. The results are summarized in Table 4.1, laboratory test reports are provided in Appendix F, and are discussed in Section 5.1 of this report. Three subsurface, abandoned hydraulic jacks are present at the site. An oil/water mixture was observed in two of the three jacks. Samples of this liquid were collected for laboratory analysis. A physical evaluation of the jacks suggests that the casings are effectively containing the oil/water mixture. The results are summarized in Table 4.1 and the laboratory test reports are provided in Appendix F. A transformer survey was conducted of potential PCB and non-PCB transformer oil soil contamination areas to inventory the number and type of transformer areas exhibiting soil staining. Transformer locations are shown on Drawing 2.1 and specific transformer substation information is summarized in Table 4.2. The survey identified 26 current or former substation and/or transformer locations. There are 1 7 substations with transformers present at the site. There are nine locations where substations were indicated on historic site drawings but no transformers are present. Surface staining was not visible at any of these nine locations. Of the 17 existing transformer sites, nine have visual evidence of staining (see summary table below) . MP?;{\J'~~4-NTPIS: Engineering & En1•ironmental Soltuions • • • Site Assessment Report Former Burlington Industries Facility Mooresville, North Carolina November 8, 2001 Page 8 Shallow soil samples were collected for PCB analysis from five locations where sludge and residue were observed to characterize the type of contamination for disposal purposes. Sample ·depths ranged from 6 to 12-inches below ground surface. Location H-15(N), classified as poor, was not sampled because the area was all concrete. Location H-23(C) was sampled to represent potentially impacted soils from transformer liquids leaking/leaching to adjacent soils. Laboratory test results are provided in Appendix F, summarized in Table 4.1, and discussed in Section 5.1 of this report. 4.3 Groundwater Assessment Activities In June of 2001 Mid-Atlantic installed twelve Type II monitoring wells at the site. These monitoring wells (MW-1 through MW-11, including intermediate well MW-4s) range in total depths of 14 feet BLS for monitoring well MW-8 to 60 feet BLS for monitoring well MW-4. The borings were advanced using 6-inch-diameter, air-rotary drilling techniques. The wells were completed with one-inch diameter, Schedule 40 PVC casing with ten to fifteen feet of 0.01 0-inch mechanically slotted well screen placed in the bottom of each well. Each of the new monitoring wells was subsequently developed to remove fine sediment particles and improve the ' hydraulic connection between the borehole and aquifer. The monitoring well boring logs are included in Appendix A and the well construction records are included in Appendix C. Groundwater samples were collected on June 26, 2001. Depth-to-groundwater readings were collected prior to sample collection. Each well was purged by removing a minimum of three ·well volumes. After each volume purged, pH, electrical conductivity, and temperature were taken. After purging and allowing enough time for the monitoring wells to recover, water samples were collected from each well and analyzed for VOCs, SVOCs, and total metals. Several wells were re-sampled to verify previous results or to obtain additional information. On July 13, 2001, Mid-Atlantic collected a water sample from monitoring well MW-7 for VPH and EPH. On August 7, 2001 Mid-Atlantic collected water samples from monitoring wells MW-4s, MW-8, and MW-1 0. The water sample from MW-4s was analyzed for SVOCs, and the water samples from MW-8 and MW-10 were analyzed-for VOCs. On September 13, 2001, Mid-Atlantic installed four additional monitoring wells in the hydraulically downgradient portion of the site to further define the horizontal and vertical extent of some limited groundwater contamination found in this area. A Type Ill monitoring well (MW-8i) was installed to 35 feet BLS near existing Type II well MW-8. Two additional Type II monitoring wells (MW-12 and MW-13) were installed to depths of 45 and 22 feet BLS (a fourth well installed in the area remains dry and was replaced by MW-12). MP?;{\J',~4NTl<,( Engineerinx & Enl'irunmental SolutionJ • • • Site Assessment Report Former Burlington Industries FactYity Mooresville, North Carolina November 8, 2001 Page 9 During this second round of sampling, ex1st1ng monitoring wells MW-2, MW-8, MW-9, and MW-1 0 were resampled to collect groundwater for geochemical laboratory analysis for aquifer characterization. Monitoring wells MW-Si and MW-13 were also sampled for VOCs at this time. Monitoring well MW-12 was sampled for geochemical parameters and VOCs. Laboratory test results are provided in Appendix F, summarized in Table 4.3, and discussed in Section 5.2. Field measurements for geochemical parameters are provided in Table 4.4 and a summary of agrochemical constituents detected in soil and groundwater to characterize aquifer conditions is provided in Table 4.5. 4.4 Surface water Sampling Activities A surface water sample was collected on September 19, 2001 from the downgradient, unnamed tributary to Dye Creek located approximately 200 feet south of the southern property boundary (Drawings 2.1 and 4.1). The sample was collected to determine the potential impacts of possible .groundwater discharge from the site. The sample was collected during low-flow conditions and was analyzed for VOCs by EPA Method 601. The laboratory test report is provided in Appendix F and summarized in Table 4.3 . 5.0 SAMPLING RESULTS 5.1 Soil Analytical Results No contamination by VOCs or SVOCs was found in a majority of the borings ( 17 of 20) advanced in and around the locations where hazardous materials and petroleum products where utilized at the facility. Only three of the 20 samples exhibited concentrations in excess of regulatory action levels. The following sections summarize the findings of the soil assessment activities relative to applicable action levels. Recommended Response Actions, as described in Table 7.1, are provided for the areas where soil contamination is present in excess of regulatory action levels. A summary of the soil laboratory test results is provided in Table 4.1 and shown with the sample locations on Drawings 5.1 and 5.2. Complete laboratory reports are provided in Appendix F. 5.1.1 AST, Garage, and Shop Areas Concentrations of diesel-range TPH (Sample 1-1 with 33 mg/Kg at the No. 6 oil AST and Sample N-1 with 30 mg/Kg at the garage area) and oil and grease constituents (Sample J-1 with 50 mg/Kg at the maintenance shop) were detected in samples collected from three areas where petroleum products were historically used. The MP?;{\Jl~{\NTl<( EnKineering & £n1•ironmenral So/urions • • • Site Assessment Report Former Burlington Industries Facility Mooresville, North Carolina November 8, 2001 Page 10 TPH concentrations are below the regulatory action level of 40 mg/kg for diesel- range TPH and the oil and grease concentration is below the 250 mg/kg oil and grease action level established in NCDENR's Groundwater Section Guidelines for the Investigation and Remediation of Soil and Groundwater for non-UST releases. 5.1.2 UST Incident Area Concentrations of petroleum-related VOCs and EPH and VPH aromatic and aliphatic fractions and lead were detected in soil sample E-2, which was collected at the former gasoline UST. The organic constituents detected in E-2 are below the lowest soil-to-groundwater and residential Maximum Soil Contaminant Concentrations (MSCC). The lead concentration (270 mg/Kg) is less than NCDENR' s residential soil cleanup level of 400 mg/kg. Because the UST area is an open incident and cannot be addressed within a Brownfield agreement, a separate Phase I Limited Site Assessment Report and Request for No Further Action has been submitted to the NCDENR Mooresville regional office requesting incident closure. 5.1.3 Transformer Areas Two of the five soil samples collected in active or former transformer areas tested positive for PCBs. Samples H-16 (l) and H-26 (A) exhibited PCB concentrations of 9. 3 mg/kg and 5.3 mg/kg, respectively. Although these levels exceed the USEPA Region Ill Risk Based Concentration cleanup guideline of 2.9 mglkg, they are below ·the 50 mglkg threshold level which triggers regulation as a PCB-containing material under the federal Toxic Substances Control Act. Therefore these results indicate that these soils can be addressed as a non-hazardous material. 5.1 .4 Railroad Spur Area With the exception of chromium, no metals were found above the NCDENR residential MSCCs in the seven soil samples collected at this area. Chromium was detected in sample L-3 at a concentration of 58, which just exceeds its residential MSCC of 4 7 mg/Kg. With the exception of chromium, the other metals were detected at concentrations similar to the levels measured in the background sample collected from location BG-1 . The chromium and all other metals are believed to be present at concentrations indicative of urban in-field soils and not associated with a specific release. 5.2 Groundwater Analytical Results No contamination was detected in wells installed along the northwestern boundary of the property (MW-5 and MW-6), in the center of the property where the majority of the manufacturing operations and hazardous material use occurred (MW-1 through MW-4, MW-7 and MW-11) or in the eastern portion of the site MP?;t\f}~~NTl~ EnKineerinx & Enrironmcnta/ Solution.! • • • Site Assessment Report Former Burlington Industries Facility Mooresville, North Carolina November 8, 2001 Page 11 downgradient from the boiler house and large No. 6 fuel oil storage tank (MW-9 and MW-1 3). Three areas of relatively minor VOC and SVOC contamination were observed and some low level contamination by metals was measured that are likely indicative of naturally occurring concentrations. Table 4.3 provides a summary of groundwater laboratory test results and the laboratory test report is included in Appendix F. Drawings 5.3 and 5.4 summarize laboratory test results for each location. 5.2.1 UST Incident Area 1 ,2,4-Trimethylbenzene (7 .1 ug/L) and VPH C5-C8 (200 ug/L) were detected in groundwater sampled from monitoring well MW-7 at concentrations below their respective interim NCGWQS of 350 ug/L and 420 ug/L. As stated in Section 5.1 .3 of this report, the presence of these contaminants has been addressed in a separate report requesting closure of the UST incident. 5.2.2 Southern Portion of Site 1, 1-Dichloroethene (DCE) was detected in MW-1 0 at a concentration of 9. 7 ug/L, above its NCGWQS of 7.0 ug/L. An earlier sample collected from this well contained 6.2 ug/L of DCE, which is just below its NCGWQS. 5.2.3 Southeastern Portion of Site Tetrachloroethene (PCE) and chloroform were detected in MW-8, MW-8i and MW-12 in excess of respective NCGWQS of 0. 7 ug/L and 0.19 ug/L. PCE concentrations ranged from 13 ug/L in well MW-1 2 to 31 ug/L in well MW-8i, and 41 ug/L in MW-8, which is paired with MW-8i and is located just downgradient of well MW-12 along the southeastern property boundary. Chloroform concentrations ranged from 9.0 to 18 ug/L in the wells. These contaminants were not observed in downgradient well MW-9 and in upgradient wells to the northwest or in cross- gradient wells located to the east, suggesting a relatively small groundwater contaminant plume of these compounds. In addition, with respect to the chloroform, there is no record of its use at the facility and it may have been introduced from leaking water supply and sewer lines in the area. According to the United States Agency for Toxic Substances and Disease Registry (ATSDRL treated municipal drinking water typically contains from 2 to 44 ug/L of chloroform. A public water-supply sample (WS-1) collected at the Burlington site contained 9.3 ug/L of chloroform . MP?;{\fl~4NTl~ EnRineering & Enl'ironmen!al Solutions • • • Site Assessment Report Former Burlington Industries Facility Mooresvl1/e, North Carolina November 8, 2001 Page 12 Bis(2-ethylhexyl)phthalate, a common laboratory contaminant, was initially detected in monitoring well MW-4s (24 ug/L) above its NCGWQS of 3 ug/L. Subsequent re- sampling of this well did not indicate its presence above laboratory detection limits. 5.3 Surface Water Sampling Results VOC contamination was not detected in the unnamed tributary to Dye Creek. Table 4.3 provides a summary of surface water test results and the laboratory test report is included in Appendix F. The modeling results provided below, which evaiuated the potential for an adverse impact to the surface water from the site, demcnstrate that it is unlikely that the North Carolina Surface Water Quality Standard (NCSWQS) would ever be exceeded. 6.0 EVALUATION OF POTENTIAL STREAM IMPACTS According to the NCDENR, the on-site reservoir and adjacent unnamed tributary to Dye Creek are Class C surface water bodies. The NCSWQS that apply to the tributary to Dye Creek as a Class C water body for the contaminants detected in groundwater on the southern and southeastern portions of the site are: Note: The NCSWQS for these groundwater contaminants =re reportedly equal to the Human Health Organism Standard as established by the EPA. With the exception of PCE, the maximum concentrations of the groundwater contaminants are below their respective NCSWQS. The fate and transport of these contaminants in groundwater and their potential to impact the nearby stream in excess of respective NCSWQS are discussed in the following section of this report. 6.1 Surface Water Modeling The potential for the stream to be impacted in excess of NCSWQS was evaluated by assuming that contaminated groundwater might eventually discharge into the stream and be diluted as groundwater flows toward and discharges to the stream. MP?;~~\fr~4fiT}<( Engineering & Enl'ironmenta/ Solutions • • • Site Assessment Report Former Burlington Industries Facility MooresvH!e, North Carolina November 8, 2001 Page 13 Mid-Atlantic evaluated the potential for the stream to be impacted by PCE, 1,1- DCE, and chloroform at concentrations in excess of their respective NCSWQS. A one-dimensional screening model, G3CTM, developed by the NCDENR was used. Model results are included in Appendix G. Conservative assumptions were made for the model input values including no biodegradation of the groundwater over time, and low organic carbon content of the aquifer (reflected in low retardation values). The model results indicate that the concentrations of the contaminants would need to be three to four orders of magnitude higher than those observed on-site to impact the stream at concentrations greater than their respective NCSWQS. 7.0 CONCLUSIONS AND RECOMMENDATIONS Assessment results indicate that soil and groundwater contamination in excess of regulatory levels was identified at four on-site areas (The transformers are collectively included as one area). Contamination was not detected in a majority of the areas that were initially identified as potential so.urces of contamination. The lack of contamination is attributed to the historical milling of cotton yarns and the use of water-based dyes which are not typically as chemically"intensive as other textile milling pror:esses. · Table 7 .l provides an evaluation of the PECs at the site where hazardous materials and petroleum products were used or stored (identified in Drawing 2.1 ), a summary of the site assessment findings for each area and Recommended Response Actions, if any. The conclusions and recommendations summarized in Table 7.1 are grouped into five categories to correspond to the way our assessment was conducted and the PECs in each area. These five categories include: • Areas potentially impacted by petroleum and coal fuels • Areas potentially impacted by chlorinated solvents • PCBs • Other potential on-site concerns • Other potential off-site concerns As discussed above in earlier sections of this report and as summarized in Table 7.1, there is only relatively low contamination at the property. In a majority of both the soil and groundwater samples, no contamination was found. According to Cherokee, they plan to implement each of the recommended response actions listed in Table 7.1 and summarized below: • The remaining coal at the site, the oil/water mixture in the hydraulic jack casings, cooling water towers and any sludge in wastewater tanks, basins or process lines will either be removed or decontaminated as necessary during site demolition and renovation. MP?;~Jl~4NTlC( Engineering & F.nl'ironmental Solutions • • • Site Assessment Report Former Burlington Industries Facility Mooresville, North Carolina November 8, 2001 Page 14 • The existing pad and pole-mounted transformers will be removed and the soil contamination in and around the substations will be excavated and disposed of off-site. • The UST incident closure report has been submitted to the Mooresville regional office. Closure of that incident with no further action is anticipated. • The low levels of groundwater chlorinated solvent· contamination will be allowed to naturally attenuate as there are no drinking water use in and around the site and there are no present or expected future impacts to surface water receptors. 8.0 REFERENCES Bouwer, H. and R.C. Rice, 1976, A Slug Test for Determining Hydraulic Conductivity of Unconfined Aquifers with Completely or Partially Penetrating Wells, Water Resources Research, Vol. 12, No. 3, American Geophysical· Union, Washington, DC. · Bouwer, H., 1989, The Bouwer and Rice Slug Test-An Update, Groundwater, Vol. 27, No. 3, National Water Well Association, Dublin, Ohio. Goldsmith, R., D.J. Milton, and J.W. Horton Jr., 1988, Geologic Map of the Charlotte 1 "x2" Quadrangle, North Carolina and South Carolina, United States Geological Survey Miscellaneous Investigations Series Map 1-1 251-E, scale 1:250,000. NCDENR, 1998, Classifications and Water Quality Standards Applicable to the Groundwaters of North Carolina, Division of Water Quality, North Carolina Administrative Code (NCAC) T15A:2L .0100-.0300, Raleigh, North Carolina. NCDENR, 1994, Classifications and Water Quality Standards Applicable to the Surface Waters of North Carolina, Division of Water Quality, North Carolina Administrative Code (NCAC) T15A:2B .0200, Raleigh, North Carolina. NCDENR, 2001, Guidelines For Assessment and Corrective Action, Table 4 Maximum Soil Contaminant Concentrations -Residential Soil Cleanup Levels (mg/kg), North Carolina Underground Storage Tank Program, effective July 1, 2001; U.S. Environmental Protection Agency, 1998, Technical Protocol for Evaluating Natural Attenuation of Chlorinated Solvents in Groundwater, EPAI600/R-98/128, September 1998. MP?;{\fl~4NTl<( En~ineering & E1n'ironmen1al Sol111ions 'i i: :! • NORTH M ID-ATLANTIC ASSOCIATES, P.A • liDgiMtrtiDg & Envimnawr/81 SolutioDs KOORII:SVIILB, NORTH CAROLINA 35080-E7 -lf -024 Dt.h\ 4855 Ill SE-SERIES VB42 1993 COfiiTOUR INTERVAL 10 FEET QUADRANGlE LOCAllON 02-027118 DWG: 1.1 ,; LEGEND lllllllllllllllllllllllllllllllll ---·----·----·------<----<----<------·----·-- .JJ II Mt: -y 115 I ~ i ~ ~ Sl1il!JiT 1-STORY BRICK WAREHOUSE ~ ~~ n -lli<K ~HALTi \ \----..,_ JIJ WATER TANK "" L ~-L ij n ~~ 'llr RAILROAD SPUR FENCE aECTRICAL UNES ABANDONED PROCESS WATER UNES PROPERTY BOUNDARY I ~ ~ ~~w~~~~~~~ DRY CLEANERS [J ~-smEET .s: t:HtHi'r:H ST. INCINERATOR 150,000-GAI..LON NO. 6 FUa OIL TANK ~ 0 0 N 0:: w [JJ :::;; w > 0 z w II~ ;l I STATION I d ... 1 0 200' iii SCALE: 1 • = 200' 0 0 ,..... CD N 0 ~ ,..... ~ ~~~ 0:: 0 ~ ~ 0 0 ~ 0 0 z -[JJ 0 0 <( ...., (.) w< 1-z -::::; Ulo wo:: _J<( _~u CL Gj I < wl-:::; 0:: 0:: oo w oz !::: :::;; -UJIW w_J w_J ~> · oUJ o::W wO:: :r:O uO :::;; U<~ ~ . .g ~~~ rl:i~ z 1';1;1 'ii <E-<ij ~<8 ~u ·~ <o tfl I tl.l "-' 0 z (!) :;: 0 Qt~.:~~ ~< .. ~ ~~ w u z w 0:: w LL.. w 0:: trl LEGEND 0 t.fW-1 +MW-13 Ill t.fW-81 esB-1 eA-1 e BG-1 esw-1 lllllllllllllllllllllllllllllllll -·--·--·--·--·--·---·--·- ~H-24 III H-10 • H-13 MW-10 0 MONITORING WELL LOCATION 'TYPE II MONITORING WELL LOCATION 'TYPE Ill MONITORING WELL LOCATION SOIL BORING LOCATION SOIL BORING/SAMPLE LOCATION BACKGROUND SOIL SAMPLE LOCATION SURFACE WATER SAMPLE LOCATION RAILROAD SPUR F<NCE ELECTRICAL UNES ABANDONED PROCESS WATER UNES PROPERTY BOUNDARY Ulli.JTY POLE W/ TRANSFORMER(S) GROUND TRANSfORMER PREVIOUS TRANSFORMER SITE [;] ® @ eQ-2 ...... UNNAMED TRIBUTARY_:..._·· -SW-1 OF DYE CREEK -.. - 150,000-GALLON NO. 8 RJEL OIL TANK ~ POIENT1AL CONTAMINANT SOURCE INVENTORY TABLE MAP I.D. POTENTlAL CONTAMINANT SOURCE ® WASTEWATER TREATMENT FACIUTY, BASEMENT ® CHEMICAL LAB @ CHEMICAL LAB STORAGE AREA @ FORMER HYDRAUUC UFTS ® FORMER VARSOL., GASOUNE, DIESEL AND WASTE OIL UST/AST AREA ® COAL STORAGE AREA ® DIESEL AST F1RE PUMP ® TRANSFORMER AREAS (SEE LEGEND) CD 150,001l-GAU.ON NO. 8 HEATING OIL AST Q) MAINTENANCE SHOP ® FORMER MAINTENANCE SHOP (b) RAILROAD SPUR, CURRENT AND PREVIOUS ® LABORATORY-PHYSICAL TESTING ® GARAGE NEXT TO GASOUNE UST @ OF1F-SITE LUST/GAS STATION ® OF1F-SITE, FORMER MILL DRY--cLEANERS @ BASEMENT SOILS/STORAGE AREA JjllJI; SOIL BORING AND MONITORING WELL LOCATIONS BY A.G. ZOLITWELLE SuRVEYORS JUNE AND SEPlENBER OF 2001. HORIZONTAL AND VERTICAL POSmONS ARE BASED ON SANirARY SEWER RIM ELEVATIONS AS SHOWN ON THE LAND l1TLE SURVEY BY GERALD V. GRANT AND ASSOCIATES DATlED 12/05/00. 0 200' SCALE: 1"= 200' ~ 0 0 0 0 r-: N N c:t: LJ.J c:t: IIl :::;; 0 0 LJ.J 0 > 0 z 0 z w ~ IIl 0 0 ...., Ol 0 I' N ~ 0 ... 0 < (.J ~ N 0 z ~ :;;= 0 w (.J z LJ.J c:t: LJ.J iJ._ LJ.J c:t: r;1 LEGEND 0MW-1 ~MW-13 Ill MW-81 esw~1 ---·----·----·------·----·----·---__. (818.52') 850.0' .JJ "' ~ MONITORING WEI.J. LOCATION TYPE II MONITORING WELL LOCATION 1YPE Ill MONITORING WELL LOCATION SURFACE WATER SAMPLE LOCATION RAILROADS FENCE ELEC1RICAL UNES PROPERTY BOUNDARY GROUNDWATER FLOW DIRECTION GROUNDWATER EJ.EVATION (AT LOCATION) ESTIMATED GROUNDWATER CONTOUR [;] ® @ ..... ·-9 ........__ _,.. (824.65') UNNAMED TRIBUTARY~ ~ 820.0' OF DYE CREEl< .• -SW-1 (818.52') .. - 825.0' ~ ® ® @ © ® ® @ ()3) CD 0 ® . 0 ~..... 0 0 b 0 r-:r-. ~ N N r: .• a::: ;:: N I --: -wa:::.-t'>") ~ [IJ 0 ~ C'S ::::< 0 Ul ~ 0 0 o-0 .. 0 z 0 z z """ [i] .. (.!) LLI [IJ 0 ~ 0 < 1!5 860.0' 655.0' I'OTENT1AL CONTAMINANT SOURCE INVENTOR\' TABLE WASTEWATER TREATMENT FACJU1Y, BASEMENT CHEMICAL LAB CHEMICAL LAB STORAGE AREA FORMER HYORAUUC UFTS FORMER VAR50L. GASOUNE. DIESEL AND WASTE OIL UST/AST AREA COAL STORAGE AREA DIESEL AST FlRE PUMP TRANSFORMER AREAS 150,000-GALLDN NO. 6 HEATING OIL AST MAINTENANCE SHOP FORMER MAINTENANCE SHOP 0 ...., u ~ ::::< :;: 0 c;: ~~ ~ ~ u a: GJ t:l Ei z a: ~t;i ~t;i < z :::; CLO -c::: r-V\(5 Zz 0::: :5:;: I LLI CL 0 f-1--.--1-a::: ;;!: 0 LLI 0 ::> ......_...J~Z 0 r-. ...J LLI z ~5w>= ::J 'VJ 0::: r-0 mwUz 0::: 0::: LLI ::J (.!) 0 ...J 0 0 w ~ ::::< ~ w Oou ::<a o...J UGJ 0 LLI 0::: U<~ ~. '-1:::2 t....,~=-<;:, (b) . RAILROAD SPUR, CURRENT AND PREVIOUS L"' rn-~ Z r.l a <E-<~ ~<~ ~u ·~ <o~ ® ® @ ® @ LABORATORY-PHYSICAL nESTING GARAGE NEXT TO GASOUNE UST OFF-SITE LUST/GAS STATION. OFF-SITE. FORMER MILL DRY-CLEANERS BASEMENT SOILS/STORAGE AREA 100,.,. ~f'-l-.:l ~<.~ SOIL BORING AND MONITORING WEI.J. LOCATIONS BY A.G. ZOU1WEJ.l.E SUIM:YORS ~l ~~ JUNE AND SEPTEMBER Of 2001. HORIZONTAL AND I/ERT1CAL PosmONS ARE BASED ON SANITARY SEWER RIM EJ.EVATIONS AS SHOWN ON TliE LAND TilLE SURVEY BY G£RAUl V. GRANT AND ASSOCIATES DATED 12/05/DO. 0 0 ........ ILl 0 ........ N ~ (.!) z ~ 0::: 0 ~ 6:: ::J VJ VJ LLI ~ u 0 VJ VJ < .!d r-z li (.!) > g li LLI (.!) w u z LLI 0::: w LL.. w 0::: • M ID-ATLANTIC ASS 0 CIA T E S, P. A. .Eng.ineering &-EnvironmMtal So/uJions 01-112719 4.1 l£GEND eA-1 eac-1 111111111111111111111111111111111 -·--·--·-_, __ , __ ,_ -o-H-24 III H-10 • H-13 _JJ 0 SOIL BORING/SAMPLE LOCATION BACKGROUND SOIL SAIIPL£ LOCATION RAII..ROAil SPUR FENCE EJ.B:IRICAl UNES PROPERTY BOUNDARY UTIUTY POL£ W/ TliANSFORhiER(S) GROUND TRANSFORMER PR~OUS TRANSFORMER SITE I~~H~1~6~(~L)~r===::SAMPLE I.D. (SEE TABL£ 1) (£'ca 1260 9.3 CHEMICAL CONSTITUENT /LASORATCRY TEST RESULT MADEP• MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION (1\NALYTlCAL METHOD) VPH= VOLATIL£ PETROL£UM HYDROCARBONS (mg/kg) EPH= ElCTI!ACTABl£ PETROL£UM HYDROCARBONS (mg/kg) TPH• "TOTAL PETROL£Ut.t HYDROCARBONS (mg/kg) DR= DIESEL RANGE (mg/kg) O&:G• OIL AND GREAS~ (ing/l<g) PCB• POLYCHLORINATED BIPHENYLS (mg/kg) 7r'M;L SAMPl£ LOCATIONS NOT LABaEO INDICATE EITHER NO SAMPL£ TAKEN (NS) OR NO VOLATil£/SEMI-VOLATil£ CONSTITUENTS DETECTED (NO). REFER TO T~ 4.1 FOR A DETAILED SUMtuRf' OF LABORATORY ANALYSES AND METHOD OESCRIPT10NS. ® ...... UNNAWED TRIBUTARY--...:.::..... .. -OF DYE CREEK @ eQ-2 J-1 O&G 50 H-18 H-19 !llliE; E-2 vee's N-BUTYLBENZENE 7.6 SEC-BUTYLBENZENE 17 P-ISOPROPYLTOLUENE 42 N-PROPYLBENZENE 8 1 ,2,4-TRIMETHYLBENZENE 75 1 ,3,5-TRIMETHYLBENZENE 53 EPH and VPH MADEP VPH-C9-C1 2 AUPHATICS 100 VPH-C9-c1 0 AROMA11CS 9.4 EPH-C9-c18 AUPHATlCS 181 EPH-C19-C36 AUPHATICS 130 EPH-C9-c22 AROMATICS 32.4 POTENTlAI.. CONTAMINANT SOURCE INVENTORY TABl£ MAP 1.0. POTENTW. CONTAMINANT SOURCE ® WASTEWATER TREATMENT FACIUTY, BASEMENT ® CHEMICAL LAB © CHEMICAL LAB STORAGE AREA @ FORMER HYDRAUUC UFTS ® FORMER VARSOL., GASOUNE. DIESEL AND WASTE OIL UST/AST AREA ® COAL STORAGE AREA ® DIESEL AST FIRE PUMP ® TRANSFORMER AREAS (SEE l£GEND) CD 1 50,000-GALLON NO. 6 HEATING OIL AST Q) MAINTENANCE SHOP ® FORMER MAINTENANCE SHOP © RAilROAD SPUR, CURRENT AND PREVIOUS ® lABORATORY-PHYSICAL TESTING ® GARAGE NOO' TO GASOUNE UST @ OFF-SITE LUST/GAS STATION ® OFF-SITE, FORMER MILL DRY-cl£ANERS @ BASEMENT SOILS/STORAGE AREA SOIL BORING AND MONITORING WEll. LOCA.llONS B'V AG. ZOUTWEI..lE SURVEYORs JUNE ANO SEPTEMBER OF 2001. HORIZONTAL AND VEJmCAL POSmONS ARE BASED ON SANITARY SEWER RIM ELEVATIONS AS SHOWN ON THE LAND T1Tl£ SURVEY BY GERALD V. GRANT AND ASSOCIATES DATED 1 2/05/00. 0 200' SCAlf: 1·= 200' 0 0 0 0 r--0 N N ~ 0:: ~ r-- w ~ N ~ til 0:: l!) 0 ~ :::;; 0 w 0 > 0 0 z 0 0 z = z w (!) ~ til 0 0 <3 3: 0 ...., Cl ~ '-' "" J: '-' "' c .... "" ~ "" z "' G .. c.. .. ~~ ~~ I VJ :; w~ ::::> ~~-...J VJ WVJ 0 w ...J 0:: j-WO:: ::5 ...J < &Vl ...JU ow§2>I ...J VJ 1-~C.. I We::: o:::::;;:::;;o::o o<w 0 z tilVJVJO ::S...J;)1'w O...JW...J t...VJ-w...J 0 5::..:> oVl >-oo::w 0:: > w 0:: < .._,Io :::;; uo :::;; :::;; ::::> VJ U<~ ~ . ·~ ~~:::t ~~ ~~-a E-o ij ~<~ ~"""!::i u ·~ <o~ I t"-:1 c:ld Qoo ~< .. ~ w u ~~ z w ·§1 0:: w ~ t... w 0:: fJi D-1 iiii BeTNll "CTTiii" N H MD ...Jill '~ L-3 SbTTI ,. 5.1 ![ H IS "-ll--~~I 1 -1 •D-2 © {n A-2 I Q-1 ~ l::aOt: MQ I 0.02 i [;] Q-2 Sb .4 1 H 0.08 r·-·--, ., ~------. H D.004 "), -;1 Nl 3.5 ~ -1&--------.-. ~.l I I ~ 0 0 0 0 ..... "' N N ~ ~ ..... o::w~N~N 0:: ~ . [lJ 0 ~ L{) ::::;; o I w 0 ~ ~ 0 z 0 0 .. z .,.. z r:-l II~ ~ ~ ~ ~ Cl-,(.)0 ~~~~~ I ~ ~ ("' (..) (..) " z ;!: -""' Zlt ~ BkBt: fJ .1.." :·~ ~ ~f.t?" ' ~~ i~~~~~~~ <( wz 1---_J t.tW~ 0 ~~®~~~ '====- ~ LEGEND 0 t.tW-9 •r-1 eaG-1 ---·----·----·------·----·----·--- __,.. .:7'4 EFCP l II -n • MONITORING WEI.i. LOCATION SOIL BORING/SAMPLE LOCATION BACKGROUND SOIL SAMPLE LOCATION RAILROAOS F<NCE ELECTRICAL UNES PROPERTY BOUNDARY I A-2 i SAMPLE 1.0. (SEE TABLE 1) Sb I 1.0 DETECTED METAL/CONCEN1RATION Sb-ANTIMONY Ao-ARSENIC Be-BERYUJUM Cr-CHROt.tiUM Cu-COPPER Pb-LEAO Hg-MERCURY Ni-NICKEL Zn-ZINC All RESULTS REPORTED IN mg/lcg ~FsOIL SAMPLE LOCATIONS NOT LA8El..EO INDICATE EITHER NO SAMPLE TAKEN (NS) OR NO METAL CONSTITUENTS DETECTED (NO). REFER TO TABLE 4.1 FOR A DETAILED SUMMARY OF LABORATORY ANALYSES AND METHOD DESCRIPTIONS. ~ 1 C-1 Sb I B.O 'O ~ ~ MW-9 ..... UNNAMED TRIBUTAIRY ___:_.... •• OF DYE CREEK - _ .. - ~ 66 ' H NS ~ POTENT1Al CONTAMINANT SOURCE INVENTORY TABLE MAP 1.0. POTENT1Al CONTAMINANT SOURCE ® WASTEWATER TREATMENT FAC1UTY, BASEMENT ® CHEMICAL LAB © CHEMICAL LAB STORAGE AREA © FORMER HYORAUUC UFTS ® FORMER VARSOL. GASOUNE. DIESEL AND WASTE OIL UST /AST AREA ® COAL STORAGE AREA @ DIESEL AST FlRE PUMP ® TRANSFORMER AREAS CD 150,000-GAI..LON NO. 6 HEATING OIL AST Q) MAINTENANCE SHOP ® FORMER MAINTENANCE SHOP <D RAil.ROAil SPUR, CURRENT AND PREVIOUS ® LABORATORY-PHYSICAL TESTING ® GARAGE NEXT TO GASOUNE UST @ OFF-ST1E WST/GAS STATION ® OFF-SITE, FORMER MILL DRY-CLEANERS @ BASEMENT SOILS/STURAGE AREA SOIL BORING AND MONITORING WE1.i. LOCATIONS BY A.G. ZOUTWEL.l.E SURVEYORS 0 200' JUNE AND SEPTEMBER OF 2001. HORIZONTAIL AND VERT1CAl POSmONS ARE BASED ON SANITAIRY SEWER RIM ELEVATIONS AS SHOWN ON THE LAND T1Tl.E SURVEY BY GfRAI.D V. GRANT AND ASSOCIATES DATED 12/05/00. SCALE: , • .,. 200' "'Vlo Vl~wo:: ~ ~-'t3 :::Jw:! LLVJ :::;;B;I ow~wl-o:: 0:: >-Vl 0:: 0 ~~~8z :::;;oll..:::;;w ::::;; ';j: ::::;; I --' :::::1 0:: ~ w --' Vlo w5 [lJ --' :>:: Vl <-Ow _] 0 0:: 0:: VJw 0 Io (.)::::;; U<~ ~ . .g ~=--~ ~~ z: 1i <E-<ij ~<El t......'""'~ L"' u -~ < 0 ril I 00 .._. Qoo~ ~<--r ~.~ ~ril w (.) z w 0:: w LL w 0:: [_ ri .JJ ;:! w-1e 0 7=1 u ! n 11 LEGEND eww-1 ~MW-1J Ill MW-81 esw-1 -·--·--·- MONITORING WEll. UOCAllON 1YPE II MONITORING WEll. LOCATION lYPE Ill MONITORING WEll. LOCATION SURFACE WA1£R SAMPLE LOCATION RAILROAD SPUR FENCE -•--•--~:-ElECTRICAL UNES - ---PROPERTY BOUNDARY MW 10 ug/L SAMPLE 1.0. (SEE TABLE 2) 9.7 MW-81 ug/L 9/17/01 PERC J1 CHLOR 18 1 E 6/28/01 8/7/01 SAMPLE DATE '1 DC 6.2 9.7 CHEMICAl. CONSllTUENT/LABORATORY TEST RESULT CHLOR- 1,1-0CE= PERC- 1,2,of-TMB- Blo(2-E)p- CHLOROFORM (ug/L) 1,1-0ICHl.OROEllHENE (ug/L) TETRACHLOROEllHENE (ug7L) 1,2,of-TRIMETlM..BENZENE (ug/L) Blo(2-EllHYHEXYL)PH1HAI.ATE (ug/L) MW-12 ug/L 9/20/01 PERC CHLOR I 11 PERC 2J CHLOR 9.2 ® 41 9.0 .... ~f ·ag~rTORING WELL LOCATIONS NOT t.ABEL.ED INDICATE NO VOLATILE/SENI-\40LA'TILE CONSllTUENTS DETECTED (NO). REFER TO TABLE 2 (TWO) FOR A IJEl'AILED SUMMARY OF LABORATORY ANAL'tSES ANO MEllHOO OESCRIPllONS. UNNAMED TRIBUTARY___:...., OF DYE CREEK •• -SW-:::.1 [;] @ ~ ~ MW-7 ug/L 8/28/01 7/1 J/01 7.1 NS NS 200 POTENl1AL CONTAMINANT SOURCE INVENTORY TABLE MAP 1.0. POTENI1AL CONTAMINANT SOURCE ® WASTEWA1£R TREATMENT FACIUTY, BASENENT ® CHEMICAl. LAS © CHEMICAL LAS STORAGE AREA © FORMER HYORAUUC UFTS ® FORMER VARSOI.., GASOUNE, DIESEl. ANO WASTE 01.. UST/AST AREA ® COAL STORAGE AREA ® O!ESEl. AST FIRE PUMP ® TRANSFORMER AREAS CD 150,000--GAL.LON NO. 6 HEATING OIL AST Q) MAINTENANCE SHOP ® FORMER MAINTENANCE SHOP © RAILROAD SPUR, CURRENT ANO PREV10US @ LABORATORY-PHYSICAl. TESTING ® GARAGE NEXT TO GASOUNE UST © OFF-SITE LUST/GAS STATION ® OFF-SITE, FORMER Mill. CRY-CLEANERS @ IIASENENT SOILS/STORAGE AREA SOIL BORING ANO MONITORING WEll. LOCATIONS BY A.G. ZOUTWEll.E SURVEYORS 0 200' JUNE ANO SEPTEMBER OF 2001. HORIZONTAl ANO VERllCAl. POSIIlONS ARE BAS£D ON SANITARY SEWER RIM ELEVATIONS AS SliOWN ON llHE LANO TITLE SURVEY BY GERALD V. GRANT ANO ASSOCIATES DATED 12/05/00. I SCAlE: 1 ·= 200' ~ 0 0 0 ~I ~ 0 ,.... ~ N N ,.... ct: :: N I "'1 w ~I:: Ill [IJ I~ 01~ o o I .. 0 .. 0 z 0 z z """ w (.!) [IJ 0 :;::: !;,( 0 (5 '= 0 ...., " "' a: c UJ UJ ~ li" ci'ii i .. ci'ii UJ ~ ;;!: a: 0 .. a.. .. i:li'ii ~i'ii I Vl ~ ::::> w< 1-z cn(/)g-:J Ww...JVlo CI::...Jf=Wct: >-~:S...J<( ct:<(O...JU ~Vl>Oii <~'w~ o::~-o::~ o~2ioo Cil<Vloz :S~~=jEw LL.z...lw::J o::::>l-w-o:S~> &~o~~ <( >wet: ::::. ~Io ::::. uo ::::> ::::! Vl U<~ ~ . -~ ~~ {:! ~ rl3' ~ ~'ii E-o ij ~<!3 ~u -~ <o~ lrl.l Qrll~ ~< .. r ~-~ ~~ w u ~ ct: w LL.. w ct: EJi LEGEND i!MW-1 ~MW-13 Ill MW-81 esw-1 ---·----·---·-·------·----·----·--- .JJ ~0 ' MONITORING WELL LOCATION lYPE II MONITORING WELL LOCATION 1YPE Ill MONITORING WELL LOCATION SURFACE WATER SAMPLE LOCATION RAIUROAD SPUR FENCE ELECTRICAL UNES PROPERTY BOUNDARY ~SAMPLE 1.0. (SEE TABLE 2) ~DETECTED METAl/CONCENTRATION Sb-ANTIMONV As-ARSENIC Be-BERYWUM Cd-CAOMIUM Cr-CHROt.tiUM Pb-LEAO H~-MERCURY Ni-NICKEL Zn-ZINC AUl RESULTS REPORTED IN mg/L ~REFER TO TABLE 4.3 FOR A DETAILED SUMMARY OF lABORATORY Ai.!D"'Arw_YSES METHOD DESCHIP110NS. \ ~ [;] • UNNAMED TRIBUTARY is OF DYE CREEK • Sl/::1 ··- .IQII; [U POTENTIAL CONTAMINANT SOURCE INVENTORY TABLE MAP I.D. POTENTIAl. CONTAMINANT SOURCE ® WASTEWATER TREATlotENT FACIUIY, BASEMENT @) CHEMICAL LAB @ . CHEMICAL LAB STORAGE AREA @ FORMER HYDRAUUC UFTS ® FORMER VARSOL, GASOUNE, DIESEL AND WASTE OIL UST /AST AREA ® COAL STORAGE AREA ® DIESEL AST FIRE PUMP ® 1RANSFORMER AREAS CD 150,000-GAU.ON NO. 8 HEATING OIL AST Q) MAINTENANCE SHOP ® FORNER MAINTENANCE SHOP <D RAI~ SPUR, CURRENT AND PRE\IIOUS ® lABORATORY-PHYSICAL TIESTING ® GARAGE NEXT TO GASOUNE UST © OFF-SITE UUST/GAS STATION ® OFF-SITE, FORMER MIUL DRY-cLEANERS @ BASEMENT SOILS/STORAGE AREA SOIL BORING AND MONITORING WELL LOCATIONS BY A.G. ZOlJIWEI..l.E SURVEYORS JUNE AND SEPTEMBER OF 2001. HORIZONTAL AND VERTICAL POSmONS ARE BASED ON SANITARY SEWER RIM ELEVATIONS AS SHOWN ON THE LAND Til\.£ SURVEY BY GERALD V. GRANT AND ASSOCIAlES DATED 12/05/00. 0 200' • SCALE: 1•.,. 200' ~ 0 0 N ~ w (I) ::. w ~ z II •• 0 0 I' ..,. ~ N I' ~ Nl"'\ ~ ~ ~ L!) 0 ~ 0 0 I 0 I .. .. 0 0 z z "'to ....... Ul _~w< ~~1-z _~wUJ_J ::::l ~ 0 Vl .:::S.w cr: w _J <( LL~ Ul_1U o w> 1-_jUJI >-VlCLWI-~ w::. ~·~ <(I-<(00 ;:.>-Vloz ::.~ ::. :::Joe:Jiu.i Ull-1-w::J <<w-~ 3:: :><: > o 0 oVl alZ~w :S ::::lw~ 0 Io ~uo (..') ::. U<!;l ~~ .g ~ ~ z (I)~ ....ollll Jil;l ~ ~Eo-~ ~<El ~u -~ <o [~ I C"'-l ""' QC"'-l~ ~<-~ ~-~ ~-~ l'l ~ w u z w ~ w LL w ~ • • MW-8 13 GS Silty Fine-Medium SAND SM 23.5 MW-8i 12.5-14 ss Silty SAND SM 41.3 MW-10 15 GS Silty Fine-Medium SAND SM 43.8 63.4 MW-13 10-12 ST Sandy CLAY CL (25.2% Silt, 38.2% SB-1 11 .5-13.5 ST Silty SAND SM 24.0 otes: 1 GS = Grab Sample SS = Split Spoon ST = Shelby Tube Unified Soil Classification System Based on Visual-Manual Procedure (ASTM D 2488-93) Percent Passing No. 200 Sieve Lb/Ft3 Not Applicable; Test not Performed • NA 84.4@ 34.5% Moisture NA 45.1@ 36.8% Moisture 16.8% Moisture MW-1 Type II 887.48 22.44 22.71 18-28 865.04 864.77 MW-2 Type II 885.22 19.81 19.97 16.5-31.5 865.41 865.25 MW-3 Type II 896.50 29.11 29.70 23-38 867.39 866.80 MW-4 Intermediate Type II 891.20 32.18 32.27 50-60 859.02 858.93 MW-4s Type II 891.26 32.36 32.47 22-37 858.90 858.79 MW-5 Type II 890.65 22.97 23.60 27-42 867.68 867.05 MW-6 Type II 894.80 24.43 25.00 20-35 870.37 869.80 MW-7 Type II 889.82 38.50 38.92 30-45 851.32 850.90 MW-8 Type II 847.10 9.54 9.90 4-14 837.56 837.20 MW-8i Type Ill 846.70 N/A 10.13 30-35 N/A 836.57 MW-9 Type II 837.13 11.93 12.48 5-15 825.20 824.65 MW-10 Type II 874.56 13.74 14.19 10-20 860.82 860.37 MW-11 Type II 889.43 39.67 40.00 29-44 849.76 849.43 MW-12 Type II 885.58 N/A 40.99 30-45 N/A 844.59 MW-13 Type II 847.26 N/A 6.50 7-22 N/A 840.76 SW-1 N/A N/A N/A N/A N/A N/A 818.52 Notes: Water levels for MW-6 and MW-1 2 were obtained on 9i20!0 1 Shaded box indicates standard exceeded NS Laboratory analysis not requested NO Not detected at or above laboratory Practical Ouantitation Limit (POL) NA Not applicable Sample D·l was obtained from the fanner hydraulic lift jack casing. The sample consisted of a waste oil. The lab diluted the sample to provide a 100,000 ug/L detection limit. Detected concentrations are below this detection limit. (1) North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil Soil • • • Shaded box indicates standard exceeded NS Laboratory analysis not requested NO Not detected at or above laboratory Practical Ouantitation Limit (POL) NA Not applicable (1) North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil I • • • Shaded box indicates standard exceeded NS Laboratory analysis not requested NO Not detected at or above laboratory Practical Ouantitation Limit (POLl NA Not applicable {11 North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil I • • • Shaded box indicates standard exceeded NS Laboratory analysis not requested NO Not detected at or above laboratory Practical Ouantitation Limit (POL) NA Not applicable (1) North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil i I I • • • Shaded box indicates standard exceeded NS Laboratory analysis not requested NO Not detected at or above laboratory Practical Ouantitation Limit (POL) NA Not applicable (11 North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil I • • Total Metals -SW-846 Method 6010 (mg/Kgl Beryllium NO NO NO NS NA Chromium 12 40 NO NS 47 Copper 5.6 83 NO NS NA Lead 15 220 NO 270 400 Mercury-SW-846 Method 7471 (mg/Kg) 0.03 0.12 NO NS NA Nickel 7.0 6.1 NO NS NA Zinc 48 110 7.3 NS NA PCBs -SW-846 Method 8082 (mg/Kgl PCB-1260 NS NS ND NS 2.9 Notes: Shaded box indicates standard exceeded NS Laboratory analysis not requested NO Not detected at or above laboratory Practical Ouantitation Limit (POLl NA Not applicable ( *) Sample D-1 was obtained from the former hydraulic lift jack casing. The sample consisted of ·a waste oil. The lab diluted the sample to provide a 100,000 ug/L detection limit. Detected concentrations are below this detection limit. (11 North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil Contaminant Concentrations -Residential Soil Cleanup Levels (mg/kg). I . Based Soil -I • • • • Total Metals-SW-846 Method 6010 (mg/Kgl Beryllium NS NS NS NS NA Chromium NS NS NS NS 47 Copper NS NS NS NS NA Lead 11 200 NS NS 400 Mercury-SW-846 Method 7471 (mg/Kg) NS NS NS NS NA Nickel NS NS NS NS NA Zinc NS NS NS NS NA PCBs -SW-846 Method 8082 PCB-1260 NS NS NS NS Notes: Shaded box indicates standard exceeded NS Laboratory analysis not requested NO Not detected at or above laboratory Practical Quantitation Limit (POL) NA Not applicable ( 1 I North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil Contaminant Concentrations -Residential Soil Cleanup Levels (mg/kg). US Risk Based. I dated • • • Total Metals -SW-846 Method 6010 (mg/Kg) Beryllium NS NS ND 2.3 NA Chromium NS NS 25 47 Copper NS NS 66 5.1 NA Lead NS NS 160 15 400 Mercury-SW-846 Method 7471 (mg/Kg) NS NS NS NS NA Nickel NS NS 14 14 NA Zinc NS NS 150 130 NA PCBs -SW-846 Method 8082 (mg/Kg) PCB-1260 NS NS NS NS Notes: Shaded box indicates standard exceeded NS Laboratory analysis not requested ND Not detected at or above laboratory Practical Ouantitation limit (POL) NA Not applicable ( 1) North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil Contaminant Concentrations · Residential Soil Cleanup Levels (mg/kg). US I Risk 4/12/99 • Total Metals-SW-846 Method 6010 (mg/Kgl Beryllium Chromium Copper Lead Mercury-SW-846 Method 7471 (mg/Kg) Nickel Zinc PCBs -SW-846 Method 8082 (mg/Kg) PCB-1260 Notes: Shaded box indicates standard exceeded NS Laboratory analysis not requested NO Not detected at or above laboratory Practical Quantitation Limit (POL) NA Not applicable • NS ND NS 30 NS 110 NS 48 NS 0.02 NS 16 NS 120 NS NS 1.9 ND NA 33 22 47 51 31 NA 66 12 400 0.08 0.004 NA 14 3.5 NA 420 51 NA NS NS ( 1) North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil Contaminant Concentrations-Residential Soil Cleanup Levels {mg/kg). · Risk Based Concentration T I dated -Industrial • • • Total Metals-SW-846 Method 6010 lmg/Kg) Beryllium NS NS NS NS NS NA Chromium NS NS NS NS NS 47 Copper NS NS NS NS NS NA Lead NS NS NS NS NS 400 Mercury-SW-846 Method 7471 (mg/Kg) NS NS NS NS NS NA Nickel NS NS NS NS NS NA Zinc NS NS NS NS NA PCBs -SW-846 Method 8082 (mg/Kg) PCB-1260 Notes: Shaded box indicates standard exceeded NS Laboratory analysis not requested NO Not detected at or above laboratory Practical Guantitation Limit (POLl NA Not applicable (1) North Carolina Underground Storage Tank Program, Guidelines For Assessment and Corrective Action, effective July 1, 2001; Table 4 Maximum Soil Contaminant Concentrations -Residential Soil Cleanup Levels (mg/kg). • • ., • Poor= I • 1, 1-Dichl I 1 .2.4· .,._,_ ~ _ ~W OAC I 8P.Q ()lgLll Riol~ r. Tentatively Identified Compounds (ftg/l) Unknown Total Metals -SW-846 Method 3030C (mg/l) I ND ND ND · ND ND NS • I ND ND ND NS ND ND ND NS ND ND ND NS • 0.7 350 (I) NA Antimony ND ND ND ND NA lf-A_rs_e_n_ic _____________ -1'~"'-' 0.013 0.044 0.030 0.050 Beryllium 0.010 0.008 0.005 0.003 NA 18c~ad~m~·~,u~m~============t==~N~D~=l1~~~~~~~-ND ND 0.005 lt~c~hr~oCm=iu=m============J~~~Nmo~!l No ~~~2'i:+---o_.o_5_o __ -J1 Lead ,~,~~~~~~~~~ ,_ ___ 0._0_15 __ -ll Mercury ND ND ND ND 0.0011 Nickel ND ND ND ND 0.100 Zinc ND ND ND ND 2.1 NS Laboratory analysis not requested NA Not available or established ND Not detected at or above laboratory Practical Ouantitation Limit (POL) (I) Interim Standard Shaded values indicate concentration in excess of North Carolina Groundwater .Duality Standards (15NCAC 2L). • Laboratory analysis ncit requested Not available or established Not detected at or above laboratory Practical Ouantitation Limit (POL) Interim Standard in excess of • • • • 1 , 1-Dichloroethene NS Laboratory analysis not requested NA Not available or established NO Not detected. at or above laboratory Practical Ouantitation Limit (POL) Ill Interim Standard Shaded values indicate concentration in excess of North Carolina Groundwater Quality Standards. • Plant water supply used for drill rig decontamination, located near monitoring wells MW-4/45 • • MW-1 5.38 NM 110.7 NM 21.8 NM 6.29 302.0 NM MW-2 5.01 5.41 98.6 56.3 21.5 23.1 5.36 244.0 103 MW-3 4.71 NM 351 NM 22.5 NM 2.00 302.0 NM MW-4 6.18 NM 249 NM 22.6 NM 1.32 280.0 NM MW-4S 5.97 NM 543 NM 22.8 NM 2.87 244.0 NM MW-5 5.07 NM 118.7 NM 21.3 NM 2.39 273.0 NM MW-6 4.87 NM 47.8 NM 23.5 NM 3.76 210.0 NM MW-7 5.60 NM 131.8 NM 21.4 NM 2.24 351.0 NM MW-8 5.26 6.32 720 972 19.0 20.6 4.70 208.0 157 MW-8i NE 6.76 NE 505 NE 20.4 3.96 221.0 NM MW-9 5.36 6.39 466 560 20.5 23.2 18.0 319 MW-10 5.12 6.64 94.6 .2 21.9 7.27 208.0 133 MW-11 4.65 NM 482 NM 25.8 NM 5.17 283.0 NM MW-12* NE 5.99 NE 260.6 NE 20.8 NM NM NM MW-13 NE 6.38 NE 676 NE 20.4 2.29 180.0 NM Notes: su Standard Units EC Electrical conductivity 11S/cm Micro Seimens per centimeter (0-1 ,999) T Temperature oc Degrees Celsius DO Dissolved Oxygen mg/L milligrams per liter NM Not Measured NE Not in Existence at time of sampling • Field Measurements for pH, EC, and T obtained on 9/20/01 -DO, ORP, and C02 not measured . • • • Methane (ug/L) <26 <26 <26 <26 <26 NS NS NS Nitrate (mg/L) 2.8 3.1 <0.10 4.4 2.6 NS NS NS Sulfate (mg/L) 2.7 75 52 1.7 49 NS NS NS Alkalinity (mg/L) <5.0 6.6 97 <5.0 15 NS NS NS Ferrous Iron (mg/L) 0.6 0.2 20 0.2 <0.20 NS NS NS Manganese (mg/L) 1.5 3.1 2.0 0.74 1 . 1 NS NS NS Carbon Dioxide* (mg/L) 103 157 319 133 NS NS NS NS Total Carbon NS NS NS NS NS 510 770 < 1.0 Relative Well Location Upgradient Plume Leading Edge Plume Fringe Leading Edge Upgradient Plume Interior Notes: ug/L micrograms per liter mg/L milligrams per liter mg/kg milligrams per kilogram NO Not detected NS Not Sampled NM Not Measured • • E -Former varsol, gasoline, diesel, and waste G -Diesel AST fire pump H -Transformer areas i petroleum products and polycyclic aromatic hydrocarbons iPAHs) from coal storage and from the No. 6 heating oil AST and a former gasoline UST. The UST release was reported in 1989, but not closed with state regulators. • former hydraulic lifts are present. jacks have been removed and two of the three subsurface casings contain an oil/water mixture. No ground-water low concentrations of groundwater contamination from USTs. No evidence of petroleum found. No evidence of petroleum contamination found. 17 active transformer substations and 9 locations where substations were located. Nine of the 17 have ground oil staining. Low concentration of PCBs in two locations no incident. None None • Excavate a"nd dispose contaminated soils off-site. No.6 None and previous action levels. Oil & grease at low concentrations (50 ppm) None -oil and grease action level is 250 No evidence of petroleum contamination. None No evidence contamin Slightly elevated chromium concentration associated with former railroad Remove overlying concrete and residual fill material from former railroad spur. Note: ( *) -The letter designation in front of each potential contaminant source corresponds to the potential contaminant sources provided in Drawing 2. 1. • treatment Site wide groundwater contamination groundwater near the machine shops (maintenance shop) and the wastewater treatment facility in the basement of the finishing mill. • No evidence of petroleum contamination. No evidence of petroleum contamination. chlorinated solvent No of chlorinated solvent No evidence of chlorinated solvent contamination. chlorinated solvent No evidence of chlorinated solvent contamination. No of chlorinated solvent No of chlorinated solvent Chloroform, tetrachloroethene, and 1,1- dichloroethene were detected in groundwater in wells on southern and southeastern portions of the site. No drinking water wells in the area and no environmental impacts expected. • None None None None None None None None None None Allow for natural attenuation of relatively low concentrations of groundwater contaminants. • Potential PCB is present in soils in each of the areas where electrical lhH:;-:_-=r;;;;;:~;:;;;;:;;;;-;;a;;:re;;:a;;:s;;----j transformers were previously or currently located --30 transformer areas. area This category includes the stained soils in the basements of "process buildings, potential impacts from cooling towers, potential impacts from coal ash lf-:---=---::----,---------i handling, and closure of the L-Railroad spur wastewater facility. 0 -Basement soils/storage area from abandoned to site soils • Nine of the 17 have ground oil staining. Low concentration of PCBs in two locations below 50 ppm which defines it as non- non-TSCA. Assessment results indicated slightly elevated metal concentrations above background levels but at concentrations expected for urban in-field setting. These soils are located under a concrete slab. (8 Assessment results indicated slightly elevated metal concentrations above background levels that may be associated with the transport and handling of coal, coal-ash and textile materials. (2.3 ppm Assessment results indicated slightly elevated metal concentrations above background levels that may be associated with prior wastewater and sludge handling processes. (8.4 ppm arsenic) Unlikely and of soil • contaminated soils off-site. detected metal are below one or more of the regulatory standards that may be applied for residential/industrial/commercial use. No The detected metal concentrations are below one or more of the regulatory standards that may be applied to the site for residential/industrial/commercial use. No action recommended. The detected metal concentrations are below one or more of the regulatory standards that may be applied to the site for residential/industrial/commercial use. No action recommended. Addressed during building demolition renovation as of the closure • station This category includes both off- site potential sources of I~>:Qii-;;!t.;:!i(;;"~;;-;:;;;!l-i contamination and off-site II P-mill migration of groundwater dry-cleaners contamination originating from the site. \J<)It~~~m~i~g~raattiio~n~~---J groundwater contamination Other off-site waste handling • • No groundwater contamination in vicinity of None. coal ash area. Process equipment cleaned by Burlington Remove and decontaminate as needed prior to plant clo~ure. Some potential for during site demolition. i I or groundwater contamin and decontaminate as needed No evidence that groundwater contamination from this site has migrated onto the There is no evidence that the dry-cleaning activities conducted at this site have the No impact to the off-site unnamed tributary of Dye Creek is expected. No other off-site activities, either from former site activities or adjacent properties, were identified that could be potential sources of contamination. demolition. None None Concentrations below other risk-based cleanup target levels that could be applied to the site. Allow for natural attenuation of relatively low concentrations of groundwater None • APPENDIX A • BORING LOGS/HEADS PACE RESULTS • MP?;{\Jl~4NTl9 En11inet•ring ,(: Enl'ironmental Solution.r • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number A-2 Project Name Cherokee-Mooresville Site Project No. RJ127.00 Geologist J. Reuscher Start Date 6/14101 Water Level Information R.P. =Reference Point • Complete Date Depth From-To (0'-0.5, BLS (2.5'-3.0' BLS .L. = Water Level Purpose Soil Assessment Contractor Mid-Atlantic Associates, P .A. Registration No. NIA DriUer J. Reuscher 6/14101 Equipment Soil/ Rock Description I Comments brown micaceous , with quartz fragments and brown micaceous sandy SILT. more mica and FID I PID (ppm) 0.4 · Soil Sample collected for laboratory analysis from 1-1.5 feet: A-2 (1-1.5). 1 boring did not encounter soil. Concrete/gravel only for -2' to 2.5' TBM = Temporary MSL =Mean Sea Level • Boring 1W ell Construction Log L D. Number Project Name Project No. Geologist Start Date Mid-Atlantic Associates, P.A. BG-1 (15'SofMW-6) Cherokee-Mooresville Site Rl/27.00 C. Lundgren 6126/01 Complete Date Deptb From-To R.P. ~ Reference Point • W.L. ~Water Purpose Contractor Registration No. Driller 612610/ Equipment Soil Assessment Mid-Atlantic Associates, P A. ~ NIA C. Lundgren FID /PID (ppm) Soil /-Rock /Comments @ Depth (ft.) NM NM TBM ~ Temporary BenchMark MSL ~Mean Sea • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number BG-IA (25' E ofMW-6) Purpose Project Name Cherokee-Mooresville Site Contractor Project No. RII27.00 Registration No. Geologist C. Lundgren Driller Start Date 6/26101 Complete Date 6126101 Equipment Subsurface descriptions based on formation cuttings BLS = Below Land Surface Well Construction Deptb From-To Water Level Information R.P. R.P. =Reference Point WL. = Water Level TBM = Temporary BenchMark • Soil Assessment Mid-Atlantic Associates, P.A. NIA C. Lundgren with FID /PID (ppm) @ Depth (ft.) NM MSL =Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number C-1 Project Name Cherokee-Mooresville Site Project No. Rl127.00 Geologist J. Resucher Start Date 6/13/0/ Complete Date Subsurface descriptions BLS~ Below Well Construction Depth Purpose Soil Assessment Contractor Mid-Atlantic Associates, P.A. Registration No. NIA Driller 6/13/01 Equipment Soil/ Rock J Reuscher /Comments FID/PID (ppm) @ Depth (ft.) brown, auger ND on rock or Note: Soil Sample collected for laboratory analysis .from 0-0.5 feet: C-1 (0-0.5) R.P. ~ Point W.L. ~ Water Level TBM ~ Temporary BenchMark MSL ~Mean Sea Level • ·! . • Boring 1W ell Construction Log Mid-Atlantic Associates, P.A. I. D. Number E-1 Project Name Cherokee-Mooresville Site Project No. R1127.00 Geologist J Reuscher Start Date 6/11101 Complete Date Subsurface descriptions based BLS ~ Below Land Surface Well Construction Depth (4'-8) BLS (8'-9.5/ BLS Water Level Information .R.P. ~ Reference Point W.L. ~Water Level Purpose Soil Assessment Contractor Geotek Drilling Registration No. N!A Driller 6111101 Equipment tannish white in color with quartz lenses. Probe 9.5'. No odors FID/PID (ppm) (ft.) ND ND TBM ~ Temporary BenchMark MSL ~Mean Sea Li?Vel • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number E-2 Purpose Soil Assessment Project N arne Cherokee-Mooresville Site Contractor Geotek Drilling Project No. Rll27.00 Registration No. NIA Geologist J. Resucher Driller Start Date 6111101 Complete Date 6111101 Equipment based on formation FID/PID Depth (ppm) Soil/ Rock /Comments @ Depth (ft.) BLS asphalt, some apparently (4'-7? BLS ND Note: Water Level Information . ~ Reference Point WL. ~ Water Level TBM ~Temporary BenchMark MSL ~Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. I. D. Number E-3 Purpose Soil Assessment Project NDme Cherokee-Mooresville Site Contractor Geotek Drilling Project No. Rl127.00 Registration No. NIA Geologist J. Reuscher Driller Start Date 6111101 Complete Date 6/11101 Equipment Ill!; u~ . Subsurface descriptions based on formation cuttings BLS ~ Below Land Surface FID I PID Well Construction Deptb (ppm) Information From-To Soil/ Rock Description I Comments @ Depth (ft.) 'Dia. NA (0'-4/ BLS .• , , 1 over(ving an orangish red, silty CLAY. ND I RiserTVOe Ni. lso~e quartz and mica fragments with moisture. No Ni. odors. tTWe Ni. (4'-7.5/ BLS Orange, silty CLAY grading to orangish red u' ND Ni. I with relict features. Lenses of weathered quartz, I Riser Ni. 1 .r ' ' and mica noted. No odors or moisture Ni. Probe refusal at 7.5'. I Slot Size Ni. Note: Soil sample collected for .. 0 imalysisfrom 7-7.5 feel: E-3 {7-7.5) !Grout Tvne f.iA NA 'Tvne NA. Ni. I Filter Pack Ni. Ni. ITowDeDtb Nli la.P. Nli Nli Water~ Date W.L. Below R.P . • 7 ~Reference Point WL. ~ Water Level TBM = Temporary BenchMark MSL ~Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number E-4 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Geotek Drilling Project No. Rll27.00 Registration No. NIA Geologist J. Reuscher Driller Start Date . 6111101 Complete Date 6/11101 Equipment ~ Comments cu: ::r:: based on} .. , ""' BLS ~ Below Land Surface FIDIPID Well Deptb (ppm) Information From-To Soil I Rock Description I Comments @ Deptb (ft.) :Dia NA (0'-4? BLS r;,_,., asphalt, some soil in upper one foot interval. No ND ~ NA odors. Grading to a reddish brown CL4 Y to about three NA feet then to a SILT with saprolite, weathered mica and ~ NA ~~oted. '"'' and relict features. No odors or moisture NA IRi~~ NA. (4'-8) BLS Weatherd bedrock section with quartz lenses, white to Nli Is~~;; NA. tannish brown. Relict features with quartz and mica I~ Ni. lenses. No odors or · . Probe-refusal at 8'. lc~;rtTVO; Ni. Ni. ~ Nii NA ~ NA. NA. ~ NA. IR:P. NA. NA water Level •mu• n;;t; W.L. Below R.P . • 'Ju;: ~Reference Point WL. ~ Water Level TBM ~ Temporary Benchi\Iark MSL ~Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number E-5 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Geotek Drilling Project No. R1127.00 Registration No. N!A Geologist J. Reuscher Driller Start Date 6111101 Complete Date 6//J/01 Equipment based on formation cuttings BLS ~ Land Surface Well Construction Depth (8'-11 ') BLS P. = Reference Point W.L. =Water Y grading to a re<ta"m brown SILT to saprolitic section with lenses of weathered quartz Jpred<>minm1t. Some pebbles of quartz indicating partial(v rock with No odors noted. above, grading to a whitish pink, granitic, partially lw••athrere>drock with large quartz weathered zones. No TBM= BenchA1ark FID/PID (ppm) ND ND • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number E-6 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Geotek Drilling Project No. Rll27.00 Registration No. NIA Geologist J. Reuscher Driller Start Date 6/11101 Complete Date 6111101 Equipment "!; "1 "'f ~onj BLS ~~Surface FID/PID Well Construction Deptb (ppm) Information From-To Soil/ Rock I Comments @ Deptb (ft) ;rn;: }fA (0'-4~ BLS l,i rum.~ 'with brown silty CLAY. 0.4 ~Tvne NA In NA (4'-8~ BLS IRed CLAY. Very stiff with some weathered rock ND 1 Type }fA No odors. -Ni (8'-10~ BLS IRed CLAY grading to a reddish brown saprolitic clayey ND Riser }fA lsi LT. Weathered rock fragments and small percent of NA '"~• Probe refUsal at 10'. No odors I Slot Size NA Note: Soil Sample collected for laboratory analysis from 0-2 feet: E-6 (0-2) ~Tvne NA NA 'Tvne NA NA I Filter Pack NA NA IT.rtaJ Deptb NA IR.P. -NA. }fA Water Level Information Date ~ ~~ ~ Reftrence Point WL. ~ Water Level TBM ~ Temporary BenchMark MSL ~ .'vfean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number E-7 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Geotek Drilling Project No. Rl127.00 Registration No. NIA Geologist J.Reuscher Driller Start Date 6/11101 Complete Date 6/11101 Equipment ~ ~r Subsurface descriptions based on formation cuttings · BLS = Below Land Surface FID/PID Well Construction . Depth (ppm) Information From-To Soil/ Rock Description I Comments @ Depth (ft.) :Dia. NA (0'-2.25? BLS Top soil, black organic material, coal. Grading to reddish 0.7 Riser Type NA orange, silty CLAY, with moisture and no apparent NA 1Type NA (2.25'-6.50? BLS ·o· wy •• with relict structures, lenses of ND NA weathered quartz and mica. Dry to feel. Upper portion Riser NA lis more clay with little partially weathered rock features. NA INo odors detected. Slot Size NA (6.5'-10.5? BLS Orangish-red saprolite with relict structures. Higher 0.3 I Type NA of mica than quartz and higher percent of CLAY. NA !Moist. No odors detected. Probe .r.. •1 at 10.5'. :Type NA NA !Filter Pack NA NA I Total Depth NA IR.P. NA tuawm NA Water Level ,u., I<Ot;nn Date W.L. Below R.P. . . -Reference Point W:L. -Water Level TBM-Temporary BenchMark iv!SL =}dean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. !'lumber F-1 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Geotek Drilling Project No. RI127.00 Registration No. NIA Geologist J. Reuscher Driller Start Date 6/12101 Complete Date 6112101 Equipment Subsurface descriptions based on formation cuttings BLS ~ Below Land Surface Well Construction Depth FID/PID (ppm) (ft.) Point From-To (4'-8~ BLS (8'-12} BLS Soil/ Rock I Comments orange SILT with quartz grains and mafic structures, iron lenses. above grading to a red sandy SILT, with grain of lmtartz and mica. Lenses of tan clay noted in section. No Jmt>isture as in above section. Weathered rock lenses and structures noted. ND 4.5 (12'-12.5~ BLS above. More relict structures and partially weathered ND Probe at 12.5 '. Note: Soil Sample collected for laboratory analysis from 11-12feet: F-1 (11-12) W.L. ~ Water Level TBM ~ Temporary BenchMark MSL ~Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number Project Name Project No. Geologist Start Date G-1 Cherokee-Mooresville Site Rll27.00 J. Resucher 6/12101 Complete Date Depth From-To (4'-8') BLS Water Level Information W.L. Purpose Soil Assessment Contractor Geotek Drilling Registration No. NIA Driller 6/12101 Equipment Soil/ Rock Description I Comments soil first 1'. to an lc/ovev SiLT. Quartz fragments noted; no mica. Very stiff No ·odors. above. Grading into a sandy, clayey SILT, with relict lfe.otw•es, quartz fragments. Lenses of whitish grey clay weathered rock. No mica or odors. Probe refusal at FID/PID (ppm) (ft.) 0.4 R.P. ~Reference Point W.L. ~ Water Level TBM ~ Temporary BenchMark MSL ~Mean Sea Level • "'! • Boring IW ell Co1;1struction Log Mid-Atlantic Associates, P.A. L D. Number G-2 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Geotek Drilling Project No. Rll27.00 Registration No. NIA Geologist J. Resucher Driller Start Date 6112101 Complete Date 6112101 Equipment IJriJling ·r Subsurface descriptions based on formation cuttings BLS Below Land. FID/PID Well Construction Depth (ppm) Information From-To Soil/ Rock Description I Comments @ Depth (ft.) ,Dja. NA (0~-4') BLS Upper I' gravel, black clayey SILT, with some ND ru•erType NA lgrey clay lenses. Grading into an orange-reddish grey, NA isilry CLAY; very stiff, dry. Some lenses of weathered 1 Type NA I quartz, little ma/ics. NA (4'-6.5') BLS Orangish brown, silry to sandy CLAY. White clay mottles ND Riser NA and quartz fragments. No mica noted. Very stiff, dry. ro. "~Type NA !Probe refusal at 6.5'. NA Note: Soil ~-•1• collected for laboratory analysis from 0-2 feet: G-2 (0-2) 'Type NA NA Filter Pack NA NA ~al Depth NA ~-NA NA Water Level Information Date W.L. Below R.P. R.P. -Re erence Point W.L. -Water Level TBM-Tem ora p ry BenchMark MSL -Mean Sea Level • • Boring IW ell Construction Log L D. Number Project Name Project No. Geologist Start Date Mid-Atlantic Associates, P.A. 1-1 Cherokee-Mooresville Site R1 127.00 J. Reuscher 6112101 Complete Date Subsurface Depth Purpose Soil Assessment Contractor Geotek Drilling Registration No. NIA Driller 6112101 Equipment 2' is IGJ,aa1ne to partially weathered rock section with mottles mafic relict features. Terminated boring at '. Not refusal but into simi/or weathered materail as 1- and1-3. FID/PID (ppm) (ft.) Note: Soil Sample collected for laboratory analysis .from 0-2feet: 1-1 (0-2} Water Level Information = Reference Point W.L. = Water Level TBM = Temporary BenchMark =}.Jean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number Project Name Project No. Geologist Start Date 1·2 Cherokee-Mooresville Site Rll27.00 J. Reuscher 6112101 Complete Date Subsurface descriptions on Depth From -To (0'-4? BLS (4'-8? BLS Water Level Information ··Purpose Soil Assessment Contractor Geotek Drilling Registration No. NIA DriUer 61!2101 Equipment Soil I Rock Description I Comments and gravel top I' grading to a with ·oc!t fr.ag~n"'rls of quartz. Last I' is apparent partially weathered rock with lenses of mafic minerals (biotite, FIDIPID (ppm) @ Depth (ft.) ND ND .•. P. =Reference Point W.L = Water Level = Temporary BenchMark MSL =Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. I. D. Number I-3 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Geotek Drilling Project No. RJ127.00 Registration No. NIA Geologist J Reuscher Driller Start Date 6112101 Complete Date 6112101 Equipment based on formation cuttings ~Below Land Well Construction Depth (4'-8') BLS Point W.L. = Water Level Appears to be all .fill. Grades to partially weathered with quartz fragments, mafic lenses and relict lfe~1tw·es. High percent of mica and quartz, with some weathered rock with large quartz fragments, lm<>ilh>d relict strui:tures. High percent ofma.fics in lenses TBM = Temporary MSL =Mean FID/PID (ppm) (ft.) ND. Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number J-1 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Mid-Atlantic Associates, P.A. Project No. Rl/27.00 Registration No. NIA Geologist J. Resucher Driller Start Date 6//3/0/ Complete Date 6//310/ Equipment based on formation ~ Below Land Surface Well Construction Depth From-To R.P. ~Reference Point W.L. ~ Water Level • and mica, some quartz weathered. No odors or evidence FID /PID (ppm) @ Depth (ft.) ND above. Terminated boring at 3'. Becoming lighter in 0.6 color with more apparent weathered quartz lenses-relict · Soil Sample collected for laboratory analysis from 0.5-/.5 feel: J-1 (0.5-/.5) TBM~ BenchMark MSL ~Mean Sea Level • Boring IW ell Construction Log L D. Number Project Name Project No. Geologist Start Date Comments Mid-Atlantic Associates, P.A. L-/a Cherokee-Mooresvi//e Site RI/27.00 J. Reuscher 6//2/0/ Complete Date 61/2/0/ based on formation cuttings with locking expansion cap and 2' x BLS ~ Below Land Surface Well Deptb Information From. To Purpose Contractor Registration No. Driller Equipment in first I, grading to a Soil Assessment Geotek Dri//ing NIA . Pieces of coal, gravel and greenish sandy lenses iaooarent. Appears to be fi//, debris. No odors apparent. Water Level Information • R.P. ~Reference Point W.L. ~ Water Level TBM ~ Temporary BenchMark MSL~ FID/PID (ppm) (ft.) Sea Level • Boring 1W ell Construction Log L D. Number Project Name Project No. Geologist Start Date Mid-Atlantic Associates, P.A. L-Ib Purpose Soil Assessment Cherokee-Mooresville Site Contractor Geotek Drilling R1127.00 Registration No. NIA J Resucher Driller 6/12101 Complete Date 6/12101 Equipment Subsurface descriptions based on formation cuttings Depth From-To (0'-4') BLS (4'-8') BLS (8'-12') BLS Soil/ Rock I Comments FID/PID (ppm) (ft.) ND ND (12'-14.5') BLS sandy SILT. and partially weathered rock. ND With high percent ofmafics (mica), and quartz Probe at 14.5'. Note: Soil Sample collected for laboratory 1-3 feet: L-Ib (1-3) R.P. =Reference Point W.L. = Water Level TBM = Temporary BenchN!ark MSL = Mean Sea Level • • Boring 1W ell Construction Log Mid-Atlantic Associates, P.A. L D. Number L-2 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor· Geotek Drilling Project No. Rl127.00 Registration No. NIA Geologist J. Resucher Driller Start Date 6112101 Complete Date 6112101 Equipment '( 7 "J' do 'based on BLS = Below Land, FID/PID Well Construction Depth (ppm) Information From-To Soil/ Rock Description I Comments @ Depth (ft.) : Dia. NA (0'-4) BLS Top 1 'gravel, dark, black, silty CLAY, with moisture. ND Riser Type !VA r. •6 into a red clayey SILT, with mottling of NA ~f}!fz /ens~s. No odors. 1 Type NA (4'-7) BLS As above, grading to an orangish red, clayey SILT ND NA ,J .. fiLA with weathered quartz lenses and more mica. Riser NA ,Some quartz fragments. No apparent odors. Probe Type NA .r.. at 7'. NA :Type NA NA Filter Pack NA NA Total Depth NA 'R.P. NA NA water Level .... Date W.L. Below R.P. R.P. -Reference Point W:L. -Water Level TBM-Temporary BenchMark MSL =Mean Sea Level • • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. - I. D. Number L-3 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Geotek Drilling Project No. Rll27.00 Registration No. NIA Geologist J. Resucher Driller Start Date 6112101 Complete Date 6112101 Equipment "!; Ujo I"· <U: ~ons based on formation "1 BLS Below Land FID/PID Well Construction Deptb (ppm) Information From-To Soil/ Rock Description I Comments @ Depth (ft.) ;rna:-NA (0'-4) BLS 1 brown silty CLAY. Very stiff, small quartz ND !Riser Tvne Nli . Grading to an orange-reddish brown clayey Nli !siLT, with more rock (quartz) fragments. No mica or o Tvoe Nli I odors Nli (4'-8) BLS 1A-s-above. Grading to a pink and white mottled, partially ND I Riser NA 'rock section with large weathered lenses of IGroutTvoe NA !quartz and feldspar. No appareniodors. Relic/features NA lwithsomemaficlenses ;-:rv;;; NA ~ ~ ND NA Note: Soil---,;. "r collected for laboratory analysis from 5-6 feet: L-3 (5-6) IFil~ NA NA !Tot~ NA IR.P. f.iA f.iA u:I" Level Information Date -~. R.P. ~Reference Point WL. ~ Water Level TBM ~ Temporary BenchMark MSL ~Mean Sea Level • • Boring 1W ell Construction Log Mid-Atlantic Associates, P.A. LD. Number N-1 Purpose Soil Assessment Project Name Cherokee-Mooresville Site Contractor Geotek Drilling Project No. Rl/27.00 Registration No. NIA Geologist J. Resucher Driller Start Date 6113101 Complete Date 6113/01 Equipment ~ Subsurface ., based on formation cuttings BLS • Below Land FID /PID Well Construction Depth (ppm) Information From-To Soil/ Rock I Comments @ Depth (ft.) : Dia. NA (0'-4? BLS u• u ... / silt and gravel 1' r, •0 to an orange, 0.4 ~_Type NA -r, SILT, then to an orangish brown saprolitic NA purua/ly weathered rock section. Quartz lenses and some .ype NA relict/'· No odors. NA (4'-8? BLS Weathered rock interval. Exhibits lenses of weathered ND Riser NA q!!~rtz and iron staining. No mica noted as lenses. :Type NA f"'nh A. eh tan to white. Relict No odors. NA Note: Soil Sample collected for laboratory ana~vsisfrom 0-4 feet: N-1 (0-4) :Type NA NA Filter Pack NA NA !Total Depth NA iR.P. NA I Datum NA Water Level .. :. Date W.L. Below R.P. R.P. -Re ere nee Point W:L. ~ Water Level TBM~ Tern ora p ry BenchMark MSL ~Mean Sea Level • •Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number MW-1 Project Name Cherokee-Mooresville Site Project No. RIJ27.00 Geologist C. Lundgren Start Date 6118/01 Complete Date 6119101 Of/N! taken from head space Subsurface descriptions based on formation Set flush-moun/ cover with locking expansion cap and 2' x 2' Surface Purpose Contractor Registration No. Driller Equipment pad Groundwater Assessment Richard Simmons Drilling 2933 Tom Tryhuba Torqmaster Foremost CT250 OVM (ppm) Soil/ Rock Description I Comments R.P. =Reference Point W.L. = Water Level .OVJ\1 =Organic Vapor Measurement TBM = Temporary BenchMark MSL =Mean Sea Level •Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number MW-2 Purpose Groundwater Assessment Project NDme Cherokee-Mooresville Site Contractor Richard Simmons Drilling Project No. Rll27.00 Registration No. 2933 Geologist C.Lundgren Driller Tom Tryhuba Start Date 6/18/01 Complete Date 6/21101 Equipment Torqmaster Foremost CT250 OVM taken from head space offonnation cuttings collected at noted depths. Subsurface descriptions based on formation cuttings pad Well Construction Information Depth From -To Soil/ Rock Description I Comments @ OVM (ppm) (ft.) (30? BLS ND R.P. =Reference Point W.L. = Water .VJI,f =Organic Vapor Measurement TBM = Temporary BenchMark MSL =Mean Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number MW-3 Purpose Project Name Cherokee-Mooresville Site Contractor Project No. Rll27.00 Registration No. Geologist C. Lundgren Driller Start Date 6/19101 Complete Date 6120/01 Equipment noted depths. Deptb R.P. ~Reference Point W.L. ~ Water Level • OVM ~Organic Vapor Measurement TBM ~ Temporary BenchMark Groundwater Assessment Richard Simmons Drilling 2933 Tom Tryhuba Torqmaster Foremost CT250 OVM (ppm) (ft.) 7 8.5 MSL ~Mean Sea Level •Boring 1W ell Construction Log L D. Number Project Name Project No. Geologist Start Date Mid-Atlantic Associates, P.A. lv!W-4 Cherokee-Mooresville Site R1127.00 C. Lundgren 6118101 Complete Date 6/19101 OVM taken from head space of formation cuttings collected Subsurface descriptions based on formation cuttings · Purpose Contractor Registration No. Driller Equipment depths. Set flush-mount cover with locking cap and 2' x 2' pad BLS ~Below Well Construction Depth Groundwater Assessment Richard Simmons Drilling 2933 Tom Tryhuba Torqmaster Foremost CT250 OVM Soil I Rock /Comments 0.5 R.P. ~Reference Point W.L. ~ Water Level .OVM ~Organic Vapor Measurement TBM ~ Temporary BenchMark MSL ~Mean Sea Level •Boring IW ell Construction Log LD. Number Project Name Project No. Geologist Start Date Mid-Atlantic Associates, P.A. MW-4s Purpose Cherokee-Mooresville Site Contractor R1 127.00 Registration No. C.Lundgren Driller 6119/01 Complete Date 6121101 Equipment OVA1 taken from head space of formation cuttings collected at noted depths. Subsurface descriptions based cap and 2' x 2' concrete pad Groundwater Assessment Richard Simmons Drilling 2933 Tom Tryhuba Torqmaster Foremost CT250 Well Construction Information Depth From-To Soil/ Rock Description I Comments OVM (ppm) @Depth (ft.) Water Level Information R.P. =Reference Point W.L. = Water .VA1 =Organic Vapor Measurement TBM = Temporary BenchMark MSL =Mean Sea Level •Boring /Well Construction Log Mid-Atlantic Associates, P.A. L D. Number MW-6 Purpose Project Name Cherokee-Mooresville Site Contractor Project No. Rll27.00 Registration No. Geologist C. Lundgren Driller Start Date 6121101 Complete Date 6121/01 Equipment OVM taken from head space of formation cuttings collected at noted depths. Subsurface descriptions based on formation cuttings Set flush-moun/ cover with Well Construction Information Deptb From-To R.P. ~Reference Point WL. ~ Water .VM ~ Organic Vapor Measurement and 2' x 2' concrete pad ~ Temporary BenchMark Groundwater Assessment Richard Simmons Drilling 2933 Tom Tryhuba Torqmaster Foremost CT250 OVM (ppm) @ Depth (ft.) MSL ~Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. LD. Number MW-7 Purpose Groundwater Assessment Project Name Cherokee-Mooresville Site Contractor Richard Simmons Drilling Project No. Rll27.00 Registration No. 2933 Geologist C. Lundgren Start Date 6/21101 Complete Date Driller 6/21101 Equipment cuttings collected at cuttings cover with locking expansion cap and 2' x 2' concrete pa{i Land Surface Information From -To Soil/ Rock R.P. ~Reference Point WL. ~ Water Level .VM ~Organic Vapor }vfeasurement · TBM ~ Temporary BenchMark Tom Tryhuba Torqmaster Foremost CT250 I Comments OVM (ppm) (ft.) MSL ~ Alean Sea Level •Boring /Well Construction Log Mid-Atlantic Associates, P.A. · L D. Number AB-1 (NearMW-7) Project Name Cherokee-Mooresville Site Project No. RJ/27.00 Geologist C. Lundgren Start Date 61/9/0/ Well Construction Information Complete Date Depth From -To (40') BLS R.P. =Reference Point W.L. = Water Level .VM =Organic Vapor Measurement . Purpose · Contractor Registration No. Driller 6/2//0/ Equipment Groundwater Assessment Richard Simmons Drilling 2933 Tom Tryhuba Torqmaster Foremost CT250 OVM (ppm) Soil/ Rock Description I Comments @ Depth (ft.) , grading to orange brown, micaceous, silty, fine to coarse SAND; w/ a diesel odor, caved in to 35' NA NA 20 20 Severe cave-in while drilling from 30'-40' prevented well installation. Borehole OVM readings from 500 to 1000 ppm while drilling from 30'-40~ Cave-in may be backfill from previous tank excavations. Boring abandoned with bentonite (0'-40'). TBM = Temporary BenchMark =Mean Sea • Boring IW ell Construction Log L D. Number Project Name Project No. Geologist Start Date Mid-Atlantic Associates, P.A. MW-8 Cherokee-Mooresville Site Rl127.00 C. Lundgren 612110/ Complete Date 612110/ cullings on formation cuttings cap Well Construction Depth Purpose Groundwater Assessment Contractor Richard Simmons Drilling Registration No. 2933 Driller Tom Tryhuba Equipment Torqmaster Foremost CT250 Information From -To Soil/ Rock I Comments OVM (ppm) (ft.) tenninated at 14' significant water while drilling at 12'. MSL =Mean Sea Level R.P. =Reference Point WL. = Water Level • OVM =Organic Vapor Measurement TBM = Temporary BenchMark •Boring /Well Construction Log Mid-Atlantic Associates, P.A. L D. Number MW-8i Purpose Project Name Cherokee-Mooresville Site Contractor Project No. R1127.00 Registration No. Geologist C. Lundgren Driller Start Date 9/12101 Complete Date 9/13/01 Equipment OVM taken from head space of formation cuttings collected at noted depths. Subsurface descriptions based on formation cuttings Set flush-mount cover with locking expansion cap and 2' x 2' concrete pad Well Construction Information Depth From-To R.P. =Reference Point W.L. = Water Level .Of-M =Organic Vapor Measurement TBM = Temporary BenchMark Groundwater Assessment McCall Brothers 2909 Elliot Ford Canterra D-10 OVM (ppm) @ Depth (ft.) 0.7 MSL =Mean Sea Level • Boring 1W ell Construction Log Mid-Atlantic Associates, P.A. I. D. Number MW-9 Project Name Cherokee-Mooresville Site Project No. Rll27.00 Geologist C. Lundgren Start Date 6120/01 Complete Date 6/20/01 OVMtakenfrom head space cuttings Purpose Contractor Registration No. Driller Equipment noted depths. Groundwater Assessment Richard Simmons Drilling 2933 Tom Tryhuba Torqmaster Foremost CT250 OVM (ppm) Well Construction Information Depth From-To Soil/ Rock Description/ Comments @ Depth (ft.) 5 17. 0 to keep boring open. R.P. ~Reference Point .L. ~ Water Level • OVM ~ Organic Vapor Measurement TBM ~ Temporary BenchMark MSL ~Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number MW-10 Purpose Groundwater Assessment Project Name Cherokee-Mooresville Site Contractor Richard Simmons Drilling Project No. Rl/27.00 Registration No. 2933 Geologist C. Lundgren Driller Tom Tryhuba Start Date 6/18/01 Complete Date 6118101 Equipment Torqmaster Foremost CT250 -.. 5"Air OVM taken from head space of formation cuttings collected at noted depths. Subsurface descriptions based on formation cuttings Set flush-mount cover with expansion cap and 2' x 2' pad BLS ~ Below Land Surface OVM Well Construction Depth (ppm) Information From-To Soil/ Rock /Comments @ Depth (ft_) 'Dia. 5" (0'-8') BLS No NM I Riser Type SCH40PVC (10'-15') BLS ~· w"o"" brown, slightly silty, fine to coarse SAND, with ND I" wave/ (moist) 1 Type SCH40PVC (15'-18') BLS 'lrnngi•h brown, slightly silty, fine to coarse SAND, with NM 1" gruvel (wet) Riser 0'-10' (20') BLS 'R,_;, NM 10'-20' . Note: 1) OVMfrom borehole: :Slot Size 0.010" (7'-8') BLS ~15 ppm tType (10'-15') BLS ~ 70 ppm 0'-6' 2) Initial boring attempted 6' to the east. Drilled through lop of concrete :Type storm drain pipe at 4' BLS. Terminated at bottom of drain pipe (7' BLS). 6'-8' Patched with concrete. !Filter Pack #2 8'-20' I Total Depth 20' iRP. Land iDah1m TOC Water Level Information Date W.L. Below RP. UUl/Ul !3.65' R.P. ~Reference Pomt W.L. ~ Water Level • OVM ~Organic Vapor Measurement TB!vf ~ Temporary BenchMark MSL ~Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. I. D. Number MW-11 Purpose Groundwater Assessment Project Name Cherokee-Mooresville Site Contractor Richard Simmons Drilling Project No. RJJ27.00 Registration No. 2933 Geologist C. Lundgren Driller Tom Tryhuba Start Date 6119101 Complete Date 6120/01 Equipment Torqmaster Foremost CT250 OVM taken from head space of formation cuttings collected at noted depths. Subsurface descriptions based on formation cuttings covi!r with locking expansion cap and 2' X 2' Well Construction Information Water Level Deptb From-To (15'-18') BLS (18'-25') BLS (30'-45') BLS • R.P. ~Reference Point WL. ~ Water Level OVM ~Organic Vapor Measurement Soil/ Rock /Comments clayey, slightly sandy SILT, moist towards bottom IU<>rK<?r brown, highly fractured section; moist •uc~;•·uu• little discernible minerals •m·uwu,, fine, sandy, very micaceous, SILT (moist at 35') OVM (ppm) @ Depth (ft.) 0.410.4 1.5 TBM ~ Temporary BenchMark MSL ~Mean Sea Level • Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number MW-12 Purpose Groundwater Assessment Project Name Cherokee-Mooresville Site Project No. RJJ27.00 Geologist C. Lundgren Start Date 6119101 Well Construction Information Complete Date Deptb From-To 5'-,30') BLS (33.5'-35') BLS Contractor McCall Brothers Registration No. 2909 Driller Elliot Ford 6/20/01 Equipment Buck Rogers D0-2 pad Soil/ Rock Description I Comments whitish, brownish, grey, fine to coarse, very lmicac:emts, sandy SILT, with larger rock fragments and @ OVM (ppm) NM NM (38.5'-40') BLS Whitish, brownish, grey, very micaceous, fine to coarse, NM with and • R.P. ~Reference Point WL. ~ Water Level OVM ~Organic Vapor Measurement TBM ~ Temporary_ BenchMark MSL ~Mean Sea Level •Boring 1W ell Construction Log Mid-Atlantic Associates, P.A. L D. Number MW-12S Project Name Cherokee-Mooresville Site Project No. Rl/27.00 Geologist C. Lundgren Start Date 9/14/01 Well Construction Information Complete Date Deptb From-To (20? BLS (25? BLS R.P. ~Reference Point .L. ~ Water Level .OVM ~Organic Vapor Measurement Purpose Groundwater Assessment Contractor McCall Brothers Registration No. 2909 Driller Elliot Ford 91/410/ Equipment Buck Rogers D0-2 cuttings collected at noted depths. cuttings cap and 2' x 2' concrete pad Soil/ Rock /Comments micaceous, sandy SILT, with quartz and rockfrags micaceous, sandy SILT. with quartz and s/ight(v and terminated OVM (ppm) @ Deptb (ft.) NM NM TBM ~ Temporary BenchMark MSL ~Mean Sea Level • Boring 1W ell Construction Log Mid-Atlantic Associates, P.A. L D. Number AB-2 (near MW-1 2) Purpose Project Name Cherokee-Mooresville Site Contractor Project No. R1127.00 Registration No. Geologist C. Lundgren Driller Start Date 9/13/01 Complete Date 9/13/01 Equipment OVM taken from head space of formation cuttings collected at noted depths. Subsurface descriptions based on formation cuttings with locking expansion cap and 2' x 2' Well Construction Groundwater Assessment McCall Brothers 2909 Elliot Ford Canterra D-10 OVM (ppm) Information From -To Soil/ Rock I Comments @ Depth (ft.) R.P. ~ Reference Point WL. ~ Level .v,V ~Organic Vapor Measurement •Boring IW ell Construction Log Mid-Atlantic Associates, P.A. L D. Number kfW-13 Project Name Cherokee-Mooresville Site· Project No. Rll27.00 Geologist C. Lundgren Start Date 9/13101 Well Construction. Information Complete Date Depth From-To R.P. ~Reference Point W.L. ~ Water Level .VJ\.1' ~Organic Vapor Measurement Purpose Contractor Registration No. Driller 9/13101 Equipment Groundwater Assessment McCa/l Brothers 2909 Elliot Ford Buck Rogers D0-2 OVM (ppm) Soil/ Rock Description I Comments @ Depth (ft.) brown, micaceous, silty SAND, with moisture; 6.6 Tube taken at 10'-12' TBM ~ Temporary BenchMark MSL ~Mean Sea Level • • APPENDIX B SOIL GRAIN SIZE/BULK DENSITY ANALYSIS • MP?;~\fl~4NTJ~ E11ginrering & £1!1'/ronmrntal Solutions • •... :.c.· M!J?;{\Jlt~N!l~ Eng in ee ring & Environ m enra I So lu ti on ... ; Client: Project Name: Project No.: P.O.#/Billing Reference: Sample Collection Date: Sample No.: Depth: Test Date: Lab Sample ID: MAAJob No.: PARTICLE-SIZE ANALYSIS REPORT Mid-Atlantic Associates Cherokee-Mooresville Site R1127 NA NA MW-10 15' 08/30/01 R1127(MW-1 0)(15') R1127 • Total Sample Weight ~...-___ ___:1:..:1....:;4.:.::JSI Grams U.S. Standard U.S. Standard Cumulative Weight Sieve Openings Weight Passing (g) Sieve Sizes Retained (g) (mm) 3/4" 19.000 114.8 0.0 3/8" 9.500 114.8 0.0 #4 4.750 114.8 0.0 #10 2.000 111.7 3.1 #20 0.850 99.4 15.4 #40 0.425 84.2 30.6 #60 0.250 73.5 41.3 #100 0.150 61.8 53.0 #200 0.075 50.3 64.5 • Percent Passing 100.0 100.0 100.0 97.3 86.6 73.3 64.0 53.8 43.8 Note: Particle-size analysis performed in accordance with ASTM D 422. Page 1 of2 MP?;~J~~~NTlS:. Engi,eering & £n,·ironmeutal So/ution.'i Gradation Curve U.S. Standard Sieve Qpeninas in Inches " U.S. Standard Sieve Numbers Hvdrometer "' ,.. • " " " " "' "' 100 ··-----------------------------------------e:;· ----------------------t .. ----1-----1---------------------· ------·-· -------···------ ~ 9) ' p E 80 R c l\ E N 70 T " F 00· ----- I " N E &l R • 40 y " 3J E I G H 20 T 10 a 1000 100 10 1 0.1 0.01 0.001 Grain Size In Millimeters Client: Mtd-AIIank Associates Classtneatlan %Gravel %Send %Silt/Clay Sample Date: NA Project: Cherokee-Mooresvlle Site 0.0 562 43.8 Test Date: 0813001 Maxlnun size 4.75-fml. 2.7% Coarse Sand, 24.0% Meclll.m Sand, 29.5% Fine Sand Project No.; R1127 labiD: R1127(M'N-10)(15') Sample No.: MW-10 Atterberg Limits MAAJobNo.: R1127 Depth: 15' Ucp.id Urm (Ll) = Plsstlc umt {Pl) = Plllstidty Index (PI) = Page 2 of 2 • • • • M!J?;{\:flA4-NTJ~ Engineering & Environmental SoluTions Client: Project Name: Project No.: P.O.#/Billing Reference: Sample Collection Date: Sample No.: Depth: Test Date: Lab Sample ID: MAAJobNo.: PARTICLE-SIZE ANALYSIS REPORT Mid-Atlantic Associates Cherokee-Mooresville Site R1127 NA NA MW-8 13' 08/30/01 R1127(MW-8)(13') R1127 • Total Sample Weight L._ ___ ___;1c..:.0.:.;9.c:..J71 Grams U.S. Standard U.S. Standard Cumulative Weight Sieve Openings Weight Passing (g) Sieve Sizes Retained (g) (mm) 3/4" 19.000 109.7 0.0 3/8" 9.500 109.7 0.0 #4 4.750 107.0 2.7 #10 2.000 92.1 17.6 #20 0.850 75.4 34.3 #40 0.425 59.1 50.6 #60 0.250 46.3 63.4 #100 0.150 34.6 75.1 #200 0.075 25.8 83.9 • Percent· Passing 100.0 100.0 97.5 84.0 68.7 53.9 42.2 31.5 23.5 Note: Particle-size analysis performed in accordance with ASTM 0 422. Page 1 of2 MP?;~J~~~NTl9. Engineerirr~: (.t: Environmental Solutions Gradation Curve U.S. Standard Sieve Ooeninas in Inches U.S. §!!!ndard §ieve Numbers Hvdrometer ,. ,.. • " " " " '"' '"' 100 ··-· -----------------------1-------------.. ··----I ------1·-----I----------------... -----------·······--· '" so p "" • 80 ['\.. R .""' c • N 70 T F 60 I N \ • 50 R B 40 f\ v " 30 ~ • " I. G H 20 T 10 0 1000 100 10 1 0.1 O.Q1 0.001 Grain Size In Millimeters Client: Mld-AIIsnlc Associates Classlfleatlon %Gran! %S.nd %SliUCiay Sample Date: NA Project: ~Mo«esVVIe Site 2.5 74.0 235 Test Data: 081300' MIU!mUn stze 9_5-fml. 13.5% Coarse Sand, 30.1 % MedliTl send, 30 4% Ane Sand Project No.: R1127 labiD: R1127(MW-8X13') S.mpleNo.: MW-8 Atterberg Limits MAAJob No.: R1127 Depth: ,. U~Urril:(ll)= Plastlclifrit(Pl)= Pltlsldtj Index (PI)" Page2of2 • •• • • M!J?;{\JI~4NTl~ Enginee_ring & Environmental Solutit)ns Client: Project Name: Project No.: P.O.#/Billing Reference: Sample Collection Date: Sample No.: Depth: Test Date: Lab Sample ID: MAA Job No.:. PARTICLE-SIZE ANALYSIS REPORT Mid-Atlantic Associates Cherokee-Mooresville Site R1127.01 NA 08/12/01 MW-8i 12.5'-14' 09/24/01 R1127.01 (MW-8i)(12.5-14) R1127.01 Undisturbed Dry Density: 84.4 lb/ft3 @ 34.5 % Moisture • Total Sample Weight .__ ____ ...:..7.:.:9.=2lGrams U.S. Standard U.S. Standard . Cumulative Weight Sieve Openings Weight Passing (g) · Sieve Sizes (mm) Retained (g) 3/4" 19.000 79.2 0.0 3/8" 9.500 79.2 0.0 #4 4.750 79.2 0.0 #10 2.000 79.2 0.0 #20 0.850 78.7 0.5 #40 0.425 77.3 1.9 #60 0.250 73.9 5.3 #100 0.150 60.8 18.4 #200 0.075 32.7 46.5 • Note: Particle-size analysis (w/ washed #200 sieve) perfonned in accordance with ASTM D 422. Percent Passing 100.0 100.0 100.0 100.0 99.4 97.6 93.3 76.8 41.3 Page 1 of 2 . : ~ ... ' ... -~!· Engineering & Enl'ironmellTal Solutions Gradation Curve U.S. Standard Sieve Ooeninas In Inches U.S. standard Sieve NumbefS Hvdrometer "' ,.. • " " .. " "' "' 100 ········· ..... ···-··-·· ....... ········f·· ·+····· I ~ .... -·· . ......... ....... .... ........ t--~ 00 p 1\ E 80 R \ c E N 70 \ T F 60 I I N E 50 R • 40 y w 30 E I G H 20 T 10 0 1000 100 10 1 0.1 0.01 0.001 Grain Size In Millimeters Client: MIG--Atlanac Associates Classification (ASTM 024881VIsuai-Manual Procedure) %Gravel %Sand %Slit/Clay Sample Date: 08/121{)1 Project: Oe"okee-MooreN!e Site Silly SAND (SM)-Maldnvn size 2.0D-mn 0% Coarse Sand, 2.4% Medl.rn sand, 56.3% 00 ,., 41.3 THIDate: 09124.()1 ProJect No.: R1127.01 F""Sond labiD: R1127.01{MW-al)(12.5-14) Sample No.: _., Atterberg Limits MAAJobNo.: R1127.01 Depth: 12.5'-14' U~ Unjt {LL): Pltlsllc Urrit (PL): Plaslldty Index {PI) = Page 2 ot 2 • • • • M!J?~{\Jl~4N!J~ Engineering & Environmenta·l Solutions Client: Project Name: Project No.: P.O.#/Billing Reference: Sample Collection Date: Sample No.: Depth: Test Date: Lab Sample ID: MAA Job No.: - PARTICLE-SIZE ANALYSIS REPORT Mid-Atlantic Associates Cherokee-Mooresville Site R1127.01 NA 08/13/01 MW-13 1 0'-12' 09/24/01 R1127.01(MW-13)(10-12) · R1127.01 Undisturbed Dry Density: 45.1-lb/ft3 @ 36.8 % Moisture e-rotal Sample Weight '-----"-----..:.7..:.4.=31 Grams U.S. Standard U.S. Standard . Cumulative Weight Sieve Openings Weight Passing (g) Sieve Sizes {rl!ml Retained {g) 3/4" 19.000 74.3 0.0 3/8" 9.500 74.3 0.0 #4 4]50 73.9 0.4 #10 2.000 ~2 5.1 #20 0.850 65.6 8.7 #40 0.425 60.2 14.1 #60 0.250 55.9 18.4 #100 0.150 51.8 22.5 #200 QJJ7_9_ 47.1 27.2 -O.Q29 -- -0.019 -- -0.010 ~ - -0.008 -- -0.006 -- -0.003 -- II -0.001 -- Note: Particle-size analysis (w/ hydrometer) perfonned in accordance with ASTM 0 422. Percent Passing 100.0 100.0 99.5 93.1 88.3 81.0 75.2 69.7 63.4 56.1 51.6 44.9 42.7 40.4 _33.7 26.9 . Page 1 of 2 • • • MP?;t\E~4NTJ~ Engineering & l::nl•inHimeutal Solution.,· ' Gradation Curve U.S. Standard Sieve Qpeninas in Inches U.S. Sl!ndard Sig,y! ~umbe[l! Hvdrometer "' ,. • 10 " .. " "" '"" 100 ---· -------· ----------------------------------.. -----.... , ... ---+------···I --------------------------------....... -------,____ ~ 90 .______ p E R 80 c I'-E ' 1'-._ N 70 T ---.._ F 80 I ,____ ~ N E 9:J R ~ • 4J y ~ '-i'---E 3J '---.. I G H 20 T 10 0 1000 100 10 1 0.1 0.01 0.001 Grain Size In Mlllbneters Client: Mld-Allsnllc Associates Classffiution (ASTM D2488Nisuai-Manual Proc:edure) %GI'IIvel 'I. Sand %Slit %Clay Sample Data: 08113101. Projttet: O'lerokeo-Mooresvile Site Stlndy ClAY (Cl)-MaxirrUn $1ze 9.5-frm. 6.4% Coarse Sand, 12.1 % Med~n~sand, 17.6% 05 36.1. 25.2 38.2 Test Date: 09f.!4/01 Project No.: R1127.01 Fine Sand labiD: R1127.01(MW-13X11).12) Sample No.: MW-13 Atterberg Limits MAAJobNo.: R1127.01 Depth: 10'-12' U(f.idl..ini1(ll)c Plaslicumt(PL); Plrlslldty Index {PI) = Page 2 of 2 • ', M!J?;{\JlA4Ii!l~ Engineering & Environmental Solutions Client: Project Name: Project No.: P.O.#/Billing Reference: Sample Collection Date: Sample No.: Depth: Test Date: Lab Sample ID: MAAJob No.: PARTICLE-SIZE ANALYSIS REPORT Mid-Atlantic Associates Cherokee-Mooresville Site R1127.01 NA 08/12/01 SB-1 11.5'-13.5' 09/24/01 R1127.01 (SB-1 )(11.5-13.5) R1127.01 Undisturbed Dry Density: 106.31btfe@ 16.8% Moisture • Total Sampie Weight '------..:..11-'-9..:...8'-'l Grams U.S. Standard U.S. Standard Cumulative Weight Sieve Openings Weight Passing (g) Sieve Sizes Retained (g) , (mm) 3/4" 19.000 119.8 0.0 3/8" 9.500 119.8 0.0 #4 4.750 106.7 13.1 #10 2.000 85.9 33.9 #20 0.850 64.9 54.9 #40 0.425 51.3 68.5 #60 0.250 44.0 75.8 #100 0.150 36.9 82.9 #200 0.075 28.7 91.1 • Note: Particle-size analysis (w/ washed #200 sieve) performed in accordance with ASTM D 422. Percent, Passing 100.0 100.0 89.1 71.7 54.2 42.8 36.7 30.8 24.0 Page 1 of 2 MP?;t\f~~4NTJ~ Engineerin-g & En\•iroumenral Solutions Gradation Curve U.S. Standard Sieve Qpeninqs in Inches U.S. Standard Sieve Numbers Hvdrometer "' ,. • " " " " "' "' 100 -------------------------------------------------------t-----------------------... ... ---·1 -----··1·-----. I -----------------. ----------------------------- 9J I' p [\ E 80 R 1\ c E N 70 '\ T F 80 I N E 50 R ]\ • 40 y ~ w 3) "" E " I G H 20 T 10 0 100J 100 10 1 0.1 O.D1 0.001 Grain Size In Millimeters Client: Mld-A!Iantlc Associates Ctasslflcatlon (ASTM 02488/Vtsuai-Manuel Proc:edure) % Gr.vel %Sand %Silt/Clay Sample~te: 0811Ul1 Project: ~MOOfeSY!Ie Site SlllySAND(SM)-Maxlnunslze9.50-mm. 17.4% Coarse Sand, 28.9% Med~m Sand, 18.8 1D.9 65.1 24.0 Tnt Date: 091Z4Jtl1 Project No.: R1127.01 % """""" LabiD: R1127.01(SB-1)(11.>13.5) Sample No.: SB-1 Atterberg Limits MAAJob No.: R1127.01 O.pth; 11.5'-13.5' U~ Umlt {LL) = Plesflc urnt (Pl) = Ptlls11dty Index (PI)= Page 2 of 2 • • • • APPENDIX C • WELL CONSTRUCTION RECORDS • MP?;*-Jl~~NTl~ HngincerinR & Enl'irollmentol Solutions FROM RSD CAROLINAS PHONE NO. 704 552 0578 J~l. 31 2001 10:24AM P2 North CatQJina • Oepartmenr r::l Environment and Nalural R.oureae. Oi'Jiticln Of Weter Quality .. Groundwater SectiOn 1638 Mail Service Canter. Rale1gh. NC 276$&-1e36 Phone (919)T.l3·3221 • WELL CONSTRUCTION RI!CORQ WeU ld~n#: MW·1 1. WI!U. LOCATION: (Sr-sketol> or the location below) WELL CONTRACTOR~ Rietaard SimtnQO$ Orfflina ot NC: WELL CONTRACTOR CERTIFICATION# 2933 STATE WELL CONSTUCTION PERMIT II: - NeeiYlSI Tewn: t.tqorm)(l!e Counly: .::lredeii="'------ Sooth Main Stralll OEf'Tli QRIU.!NG LOG Fcrn"ttllon Cet.cnP:IOn 2. OWNER:C- AOORESS: Sou!!! Main stJ!I!! ~MR411!111No~ l!ootpille NC 3. DATE DRILL!D: §l1Ml1 4. TOTA~DEPTH: K II. CUTTING COU.!!CTEC: No $. OOES WEU. REPI.ACE EXISTING WEl.l.? 7. STATIC WATER i.EVEL Selow • Tep Of casing; cv .. -...· ir......., To>~ •f C:•tiflt) No 8. TOP OF CASING IS Q FT. Above L.snd SUrfiiC8" 0 CIU!Qi'~lllliwbi.Dwllndlll'l'&eillllllgaillilaM I~~· · "'-'::inaa.o.an:.Wtnw.~2e.~,, eu, (gprn): MeT HOC OF T!!ST: --- 10. WATER ZONES (depth): 11. CHLORINATION Type: Amount: ----- 12. CASING: O<l!)th Fran 0 To 18 A. From To Ft. Fran To Fl. 13. GROUT: Deptll Fran 0 To 16 1"1. Fran To Ft. 14. SCREEN: Oeptll From 18 To 28 Ft. Fran To Ft. Fran To Fl. 15. SANDIGRAVEL I'ACK: Oeplh 28 Fl. ___ Ft. l'ran 16 To ~-To 16. REMARKS: Wall Thickness DiSI"'''.eeUlr or W<Mghll!'t , .. Malllrial Cement iBentalite Diarnet:er" , .. Size 112 SICll Size " .Q10 Mat«ial Sand MaN!rial ~ Mechod T-.nie Material e& ,.:;rom To LQCATION SKETCH t6howdil'el:l!on an" d~~&an.;o fNm llltut M S\ate R~.SS, or Offttt MID referenC:t Defttt) W. Wllltort Ave NC·2t • 100 HEREBY C!ERTIFV~TV4~WM~ON1Tl!Ut.."T&CIN~ WI'!'Ji l5A NCAC 2C, ~U eoNST~!JCTION S'T'~A.C9, A"CTW\T 4 COPYOFTI-f'!l RECORe H.U tEI!iN MOIJIDEO TO TK[ 'M:I.L.OIIt1tlfll; ~ . .JJ.Q (i) s;:r-.-.,. ~ ·Q DATI! stGNAltiU£ OF Cdl'lllU.CTOR 0 R AGiiNT ?r,Q/01 Slbnlori!Piiti:J OIYI:don oiE~ Lt..,......,.AI'I:I al!lll =••"-"· FROM RSD CAROLINAS PHONE ~10. 704 652 0678 Ju I. 31 2001 10: 25RM ·P3 North Catalina~ Oegartment ~ Environment and Natural Resources OJ>o~icrcrt of W.acet Qua lit~ -Groundwater Sect ion 1636 MailS~ Center· i'laleigh, NC 27699-1636 Pi'oone (919)733-3221 • WI!LL CONISTRUCJION RECORD Well-cation Ill; MW-2 1. WI!LL LOCATION: (S~ akelch of tile location boicw) WELL CONTRACTOR; ~jcbard SlmmQM Qri/lina of NC WE~~ CONTRACTOR CERTIFICATIONjO .!!m STATe WE~ CONSTUCTION PERMIT,__ N-1 Town: Mgqn!s'lillf: County: -'lrada""'"'"'------ South Main SII'Gel QI'!I~ING LOG Form;rtimD~ 2. OWNER: Charola!a ADORess:isO::a;;UtfirT.ur.:.,r.:. ""sa:,-=----- l&hllll 011'10~ ftlo,) -ville NC -3. OA '!'!! ORI~!C: !li.W!li 4. TOTAL CEPTH: 31.5 5. CUTTING CO~ECTEC: No 6. DOES WELL REPlACE EXISTING WELL? 7. STATIC WATiiR WiVIiL Below· '!'ap of Casing: {lJM'.,'II'&bo· ... Topof::lll~ NO 8. TOP OF CASING IS Q F'!'. Ab""" Land Surla:e • . • C&tifiiiT~af'ot'*"wiiM~ illllfQalritt~o•.,..11Mce It .& ftac.caA:&MoaWIII1~ NCI.C~ .0118 ~ (gpm): __ METHOO OF TI!ST: --- 10. WATER ZONI!S (d<lfth): 11: CH~ORINA TION Ty)le: 12. CASING: Oepth From 0 To Fran To Fran To 13. GROt.,'T: Oaplh Fran 0 To From To 14. SCREEN: From /Oeplh 18, '7 '!'o Prom To From To 15. SAND/GRAVEL PACK: Depth From 14 To Ptom T'o 16. REMARKS: 18 Ft F~. Ft. 14 Ft. Ft. 31.5 Ft. Ft. Ft 31.5 Ft. ___ Ft. Amount Wall Thickness Oiameter or WeighVFI. 1' Malana Cernern /Bentonile Oiameler" 1' Size 102 slots~· .010 Malarial Saoo Material PVC MOinod Tremmie Material F'VC From To ~OCAJ!ON SKETCH tSI'Ie!W diectfdl"' atld etancD tun i~tll!aa•t'tM:I &Wte Roads. or otl'ls-ffi8ll rarerenca ponUs) W. WIIIOn Ave NC-21 • J 00 i-IEREBY CEtmF'f n;,.;r WELL WAS CONSiRUCTfD INArxc:lROAII!C:E IDM 1SA W"..AC 2C. 'A'EI.~ CCWS":'Ruc1"JOH $TAioiDARDS. AND 'THio.T A COPV OPTkiS AiiCORO H.t.a BGEi"' PlfCMO!ttl TO '!'H~ WEI.~ OIMI'~ O f.,..,. -ff\a~a FROM RSD CAROLI~S PHONE NO. 704 662 0678 Jul. 31 2001 10:26AM North Carolina-Department of Environment and Natt.Jrat Resources Division of Watar Quality-Gtoundwatar Saetion 1636 Mail Serllic:e Center • Raleigh, NC 276911-1636 Phono (919)73~32.21 • WELL COHSTRYCTION RE!CORO WELL CONTRACTOR: R;cham Sjmmons Drilling pf NC WEU. CONTRACTOR .;~:RT;F:CATION# ~ STATE WEW. CONSTUCTION P~:;RMrT "' 1. WEU. LOCATION: (Shew sl<elci1 ~til~ location below) Nearest Ta..n: f;!OQ!!!!IIIill!! county·. .:.:lrecl=ei=------DEPTH DRILLING LOG Formalion 0.~ South Main Snet: 3. DATE ORIL.I.EO: E!11Ml1 4. TOTAL DEPTH: i[ 5, CUTTING COU.ECTEC: No 6. POESWELL REPLACE EX1$TII\IG WELL7 7. STATIC WATER LSVEL Belew-Top of Casing: (UM "1"' r AL10Vt Top Ql CIWI;I No 8. TOI" OF CASING IS Q Fr. Abcw<t Land Su.fooa' ' Cllfll 'l'armllll!ld' lt/Ortlet:N lind sutfa it ii!!CIIilriiM 11 ~ i~ ~~aaoD ... wthiSAN~2C.II118 .,ELD (gpm): __ METHOD OF TEST: __ _ 10. WATER ZONES (de!lll'l): 11. CHLORINATION~ Am~unt 12. CASING: Wal Thicllness Doptn 0-or Wefgtn!Ft. F..., 0 To 23 Fl. 1" From io Ft. From To Fl. 13. GROUT: Depth Mote<ial From 0 To :!1 Ft. Cernant 19ontanilo From To 14. SCREEN: Oepth From ____R._ To Fran To F"'"' To 15. SANOIGRAVE~ F'ACK; t:le!llh Fnom 21 To from To 15. REMARKS: Ft. 36 Ft. Fl. Fl. 38 Ft. ___ Ft. Oi..,eler" 1" Size 1(2 Slot Size • .010 MGlelial 1'1/C Mt!lhod Trammie ~lal PVC From To LQCATION SK!!TCH (Show alrtction and d~ froM .alleatt two .(MN R<ledt, or other w.p re~oarer~ce po~r~:ta) 'N. WkortAYIII NC-2, • l DO HliReBV CI!M!NfHAf\\'£LL VIM. CONSTR!JO'l'f!D IN AOCORc.ucd WT!-115.\ "&CAC X:. Wii.J. CONSTRUCTION sr.t.NOAROG..Ahtl '!'MAT A COPYOFiHI!j, ~CORD HA6III!EH PROYIOEQ TO THE MLI. CWNIA •• ~ .. ~~~&~~ 713Q/01 '·'· . FROM RSD CRROLI NAS . PHONE t-10. 71:14 662 1<1678 Jul. 31 21ala1 11a:26AM PS· North Carolina· Oepmment of E;nvirt~nment and Natural Resources Division of Weier Quality. GroundWater Section 1638 Mall Sentica Cenl"' • Rale•gh. NC 27699·1638 Phone (919)733-3221 • WELL CONSTRUCTION RECORD WEll CONTRACTOR: ~iehj!t!! Simmons Drilling g! NC WEU CONTRACTOR CERTIFICATION# g STATE WELLCONSTUCTION PERMIT., Wall klentlllaltlon #: M- 2. OWNER: Cherokee ADDRESS: SruttJ Main Street i'Sn.~rRO&M~) MDillliSville NC Crt,'or'T!MI'I .... 3. DATE tlRILLE!l: !ll:1J!iQ1 4. TOTAL DEPTH: fm: .. c ... 5. CUTTING COLI.E:C'TED: No 8. DOES WIILL REPLACE EXISTING WELL? O!PTH F"•·o:n To No "DRILLINQ LQ@ FaM'atlan Ol!sa1pt10n 7. STATIC WATER LEVEL Below· Top of Casing: tU• • ..,.It AJ»w 'l'Coul CMitloj B. TO~ OF CASING IS 10. WATER ZONI!.S (depth): 11. CHLORINATION Tl'l)e: 12. CASING: Depth From 0 To From To From To 13. GROUT: Depth From 0 To From To 14. SCREEN: Oeptil FIQ'II so To Frcm To Fram To 15. SANOIGRAVELPACK: Oopth · Frorn .a To Fn:rn To 16. REMARKS: • FT. Allow! land Surface· ~0 Ft. Ft._ Ft 48 Ft. Ft eo Ft. Ft. Ft. 60 Fl ~--Ft. Amount: Wall Thickness Oiameler or W oight.l't !" Material Cement /Bentonite Olametor .. t" sa.. #2 Slot Sil&' .010 fl---.1 PVC -Trammie Matetial PVC l,Q!;WON SKETCH ~SfWJW ~ ~nd c:!stanOII!I l':om M -.t No SCCICe Rc.aes, or Olfter map ~rv:. oolms) W. Wltaor: Ave 1 00 I"IERESY CERnFYT~AT W£L!. ~ CONSTPUC":EC 1~ I<CO~E 'MTH 1-Yt NCAC ,J;. YEU. COHiTA.VC"J'tOH $'I'J,N~RC$. ANO THAT AtoP'V 0~ THIS RECORD~ 69~lPMCI.IIOOC 'TC l'"IE 'MI.I.QWNE!A c--.:Jl\i o~· Q SIGNA\1,/Fte OF CQfolmA(.fOR OR AG&&I Wmit Ofi;lr~ Ill OMIIM~Jf £--.-...1.\lmtai~J~Mt at11J co~ !o .... !I'MW. -· FROM RSD CAROL!NI'lS PHJNE NO. 704 662 0678 Jul. 31 2001 10:27AM P6 North Carotina -~artment of Envtronment and Natural R•t~urces Division ot Wat91 Quality-Groundwater Section 1e36 Mall S8!Vice Center· Ra~h. NC 276119-1636 Phone (919)733-3221 • WELL CONSTRUCTION RECORD WELL CONTRACTOR: Ricturd SjmmO!l$ DrJ!jnq d NC Wallldonllflcatlon Cl: MW..&a WELL CONTRACTOR CERTI FICA TICN# a!!ilil STATE WEI.l CONSTUCTION PEFlMIT 11: 1. WELL lOCATION: (Sh.,.. sla!lch ollhe loeaticln balow) NeoresiTown: Moo!!SlOlle County: .!Ciredel~:!!l _____ _ DEPTH DRILLING LOG flormation O..Crtpti~ South Main S!J!Ol .2.0WNER;~ AOORESS: South Mliin Streot {Vntloro'IQIMNt:l.) MQO!!!IIIIe NC 3. DATE ORIL.I.ED·. ~ 4. TOTAL DEPTH: £ 5. CUTTING COLJ..ECTEO: No 6. OOES WELL REPLACE EXISTING WELL.? No 7. STATIC WATI!R LBVEL. BelOW· Tcii ot Casing: (o. ... fAI».,..TopQI~ a TOP OF CASING IS 10. WATER :!ONES (d&J>th); 11. CHLORINATION Type: 12. CASING: CG!IIh From 0 To From To From To 13. ClROllr: Oopth From 0 To From To 14. SCREEN: Cepit1 From 22 To From To From To 15. SANOIGRAVEL. PACK: Oopth Fr'QTl 20 To From To 18. REMARKS; • ll FT. Abowlland s Ulface • Amount: WallihiCI<noss Oiam-orWo>.lhtn't. 2~ Ft. 1" Fl Ft Molenel 20 Ft. c...-!Berllonile Fl. Diameter" Slot St:e'" 37 fl. 1" .010 Ft Ft. 37 Ft. ___ Ft. M-ial I'VC Mathod Tremmie Marerial PVC LOCATION sKgTCH (SI\ow airaeticln .and diStance tram at leaSt two 5lllta ROOIC;Is, ct other mep r~ points) W. WllaanAw 1 g()Hef\EB'I'Ciarl'rfTiiAT'M!LL"""'I ;~~IWCT!i.OlN~o;:>AQ,It.te& ~ 1!1ol. NCN! :<;:, 'MlLLCOI'O&TIIt\.iC'!'ION ST.a.No.ul06, MO TH.t.T 4 COPY OF' 'THIS RI:QORC riA$ BEEN PRO'IJg&O TO'!""£ WElL OVIINI.It (;"-.~ ~-~ ~ !SJdiltATIJR& OP CON'fi\ACTOR 6l X!ENf $b'N::1Jlllllll!ti:IOi~cr e.Mtvi'J'MI'IItl Ml~tnel:~\1:1 .,...,o_. 7130101 blti n.-u= FROM RSD CAROLINAS PHONE NO. 704 662 0678 Jul. 31 2001 !0:27AM P7 North CargJha · Oepartment of Envkonment ar'ld Natural Resources Oivision r:A Water Quality. Groundwater s.ction 11336 Mai/Sorvice Center· Raleigh, NC 27699-1636 Phone (919)73$.:1221 • WELL CONSTRUCTION RECORD WELL CONTRACTOR: Bi!l!!J!i!lSjmmon& Drilling or NC WEU. CONTRACTOR CERTIFICATION# ;!!!.'!il Wallldontlflcation ill: MW-5 STATE! WELL CONSTUCTION PERMIT#: I. WELL LOCATION: (Snew &1<1111:11 aflhe kx:aion below) Nearest Town: Mooroo,;lle C<>unty: ""lredo=:ou _____ _ DRILLING L.OG Fomaticm Cetcrtpdon SOUIII Main Slreet 2. OWNER: Cherokee AODRESS:.;;S;:;out!J'5;"i;Mi:iai"'n ... S"'I1MI=----- (;n. or Rellll Nt.) Moo""'ville NC ..... 3. DATE DRlll.ED: l!l2l!2l 4. TOTAL OEPTl-1: :!2: 5. CUTTING COLI.ECTSO: No . 6. OOES WI!LL REPLACE SXJSTING WELL? 7. STATIC WATER b!!III!L Bilow· Tcp of Caolng: (IJM ••• if'Abcio~i0!:141 Culna. No 8. TOP OF CASING IS Q FT. Ab<Mt Land Surlace' • c.qT~abr--lllndNtA'Ititlie811.._•.,.,•'*it • JI'I ....... WII\1!.1.~3C.Jl11l ELO (gprn): __ METHOD OF TEST: --- 10. WATER ZONES (depth): 11. CHLORlNATION Type: 1:Z. CASING: Depth From 0 To From To From To· 13. GROUT: Depth From 0 To From To 14. SCREEN: Oeptll F""" 27 To Frorn To Fran To 15. SANDIGRAVE\. PACK: ~h From 2S To Frtm To 16. REMARKS: • 27 Ft Ft Ft. ·~ Ft. Ft. 42 Ft Ft. Ft. .02 F1. ___ Fl. Amount Wall 1'111ckness Cil:rn-or Weight/Ft. 1' Material Cement !Banlonite Diometar" 1"' Sial Si>e" .010 Materiel Sj!!!d Material PVC Method TI'1WflmtP. MMrial PVC From To \.OC/1 TlON SKETCH ~.Show dito:tbrt and dlstalce trom Cit lie&9l. two Sla!B RcDdS, or Olher map toterence ~a) NC-21 W. Wii&CI'l AltO 7130/01 bAli FROM RSD CAROLINAS PHONE NO. 704 662 0678 J~l. 31 2001 10:28AM P8 Netth C•rol/na -Department of Erwironmffl"lt and Natl.lral R:t1'$outee& DMsioo of Water Quality -Qroundwatal' Sactton 1636 MoiiServiceCen!et· Raloligh, NC 27699-1636 Phorte (919)733-322' • WEbb CONSTRUCTION RECORD WELL CCNTRACTOR: Richotd Simmons Onllin9llf NC WELL CO:-JTRACTOR CERTIFICATION# Z!!;l;1 Wen Identification"' MW-0 STATE WEUCONSTUCTION PERMIT j: 1. WELL. L.OCATION: (Shovv lleeloh of the location baiOw) ,.,_ITOMl: Moonosyjlle Counly; .!llr:;:ecl~e::_ll _____ _ DEPTH QBIUINGLOG fonmtiOn o.aaiplion South Main Street 2. OWNER: 3. OATE CRIUEC: §l.6lQ1 4. TOTAL DEPTH; ;jl! 5. CUTTING COLLECTED: No 6. DOES WELL REPLACE SXISTING WELL? 7. STATlCWATERL.EVEL-·TopoiCaoing: (Ua"·-t~T-OfCMiriQ) NO 8. TOP OF CASING IS .Q FT. Abawa Land Surface" 10. WATER ZONES (depth): 11. CH!.ORINATION 'Tyl>e: 12. CASING: Depth From Q To From To From To 13. GROUT: 00¢1 From 0 To Frcm To 14. SCREEN: o..th F""" 20 To Frcm To From To 15. SANO/GRAVEL PACK: ~h From 18 To '!=rom To 2Q Ft Ft. Fl. 18 Ft. Ft. 35 FL Ft. Ft. :::=36==Ft Fl . Amount Wall Thickneu Diametet or Weight/Ft. 1" Material Cement /Bentanite 0/omeler" 1' Size 112 Sic! Sl!e" .010 Material t.and Material PVC Methcd TremmMt Malerial F'VC FrDm To LOCATION SKE!TCH <Snow m~on ano d~ ~at: least two Sl&te R08CI. « othcf" ~ l'8f8Mn.C.e polm&l W. WUSanAva NC..21 • 1 00 HERED'I' l:;&ii:ITIFV TH.l.T WELL WA$ CONST'RI.Jl..,-ED IN AI:GOiiD.~oJrK:E W7111~ HeAl: :K:, 'J.'II.L CONfiT::wc:Ttof\1 STMCINI:P$, ANPTHII'T' A CCP'IQF1"1-Q8 RECORD"'"* I'J!EN PROVIDIO TOTI'~e V,ct.L 0'.\NER .,~·~~~<><~ 0 7/30101 OAii FROM RSD CAROLINAS PHONE NO. 704 652 0578 Jed. 31 2001 10: 2BAM P9 .. North Carolina • Department o' Environment ano Natural Resources Division of Wetef Quality-Grcundwater Section 1636 Mail SeMca Center. Raleig~. NC 27699-1636 Phcne (919)733-3221 • WEl.L CONSTRUCTION R!!CORD WELL CONTRACTOR: Richard Sir'ntnM$ Or~ling of N~ WELl. CONTRACTOR CERTIFICA TIONII Oi!!iY won tdenttflcatian"' --7 STATE WEI.!. CONSTUC'T'ION PERMIT II: sklltch of the looation bebN) -~~lin County: -'!111!<1=•"~----DEPTH i=rom Tc DRILLING L.OG Fomation Des~ 3. OATE DRILLED: §I2Ull.1 4. TOTAL DEPTH: !a: 5. CVTTING COU.ECTED: No 6. DOES WELl. REPLACE EXISTING WELl.? 7. STATIC WATER LEV&L BelOw· Top of Casing: 1\JM •.o• WAblaW Top ot c.lnGt No 8. TOP OP CASING IS g, . FT. Abc-ooe Land Surlaca • . • ~T•""'...wc~Mior........,..,_MIII_'-~-.... u ... •• .In ·~wt~11t.HON:;I2C .0111 -LD (gpm): __ METHOD OF TEST: --- 10. WATER ZONE$ (depln): 11. CHLORINATIONType: 12. CASING: Depth From 0 To From To From To 13. GROUT: Deptt1 From 0 To From To 14-SC"!!N: Depth Fr001 30 TO From To F""" To 15. SANCIGRAVEL PACK: Dopth Prom 28 To From To 16. REMARKS: 30 Pt. Ft. Fl. 28 Ft. Ft -4-5 Ft. Ft. Ft. 4S FL ___ Ft. Amount: Woii'T'hickness Oiamecer or Weig~riFl. 1" !'.lalatial Cement /Bentonite Oiameter" 1" Slot Size • .010 Material Send Moten a! PVC Meth<d Tr'E'Mmia MateriOI PVC LOCAI!ON SKEJCH (Snow diree~ien and dlstarv:. frrolmat Ust two State RoM~. or IJCh .. r map Nllerenoll jXMta} W. WJI&on AVIt NC-21 • I gQ HERES 'I' ctATII'YTJ'II,T\WLL VWSeOI't$TfiVr;:'l!LIIN ACOOftOAIII~C V'~TH 1111'. ~C.O.G" 2¢, 'Ml.I.CONI'TRUCTI¢N OT~M.~CT·:~G~~~~c;;;:o 7f.l0101 DJtiE FROM RSD CAROLINAS PHONE NO. 704 662 06?8 J~l. 31 2001 10:29RM P10 Nortn Carolina-Department of En ¥'ironment and Natural Resoorcas Division of Water Quality-Groundwaler Section te3Q Ma;l Sentica Center-Raloigh. NC 27699-1636 Phone (9191733-3221 • WELL CONSTRUCTION RECORD Wellldentlllcalion 1/o MW·8 1. WELL LOCATION: (Sh<>N sketch ar the 10c:a1ion below) WELL CONTRI'.CTOR: Richard S1mmons Dral!ng gt NC WELl. CONTRACTOR CERTIFICATION# ~ STATE WELL CONSTUCTION PERMIT II: NearesiTOM1; MP91!!!!vilk! Coonty; .::'.-n=C...------DRIWNGLOG FOI'TI1IIIion O.~iOn Soulh Main Slreet 2. OWNER: Cher"""" AOO~ESS: SouthjAaifi §!reet ('lrwtorRtNnt No.) Mooresyil!e NC 3. DATE DRIUJiO: ~ 4. TOTAUlEI"TH: .1£ 5. CUTTING COLLECTED: Ng e. OOE;S WELL REPLACE I!XISTING WELL? 7.' STATIC WAT6R LEVEL Selcw· T011 of casing: (\.hill'+' it AbovtTOOOfCMifl;) 8. TOP OF CASING IS • eu~T~~rtort*w~tnc~•~c.iflt;liiii'IIIN•wn-b 6::-W ... """' 20 01 II (gj>m): -METHOD OF TEST; 10. WATER ZONES (depth): 11. C.HLORINATION Type: Amount: 1Z. CASING: Oe¢1 Oiame~et Frcm 0 To 4 FL ,. From To Ft. From To Ft. 13. GROUT: Oeplh Maleriol No Wall Thickne$9 ot Weighi/Ft. From 0 To 2 Ft. Cement /Bentonila From To 14. SCREEN: Oe!>lh Pnotn .. To From To fi()ITl To 15. SAND/GRAVEL PACK: tleptll From 2 To ,_ To 1 e. REMARKS: • Ft. 14 Ft. Ft. Ft. '4 Ft ___ Ft. Diameter" Slot SWI .. , .. .010 Maerlal PVC Method Tremmie Matertal PVC Fre-m l'o LOCATION SKEICH (SIIGW :trectioo and d~ fl'om" leal two S&at:a Road8, ot oeter ITWll) rftlreMe pohta; W. Wl!aonAw 7130/01 bATE SENT BY: 10-26-1 :10:01AM ;MID-ATL~NTIC ASSOC. ~ 3132508850:# 2/ 5 'u" ; IU/:ib/~1 4:54PM;Iftfu /1705;Page 2/3 _,.., o" •J , m._~ ... .._. Y! '-'I, !ICI ::ll North c:...ailoll· O.p&Mtom of.,...,.,,...,.. an~ Nllutal " ... .._-DM.Io~of W-Cuolly·--1111- IIUIM&U S.Nial c._.-AUOWI. N.C.I7UII-1 aa.'"-(111)7lWII1 .WELL CONSTRUCTION RECORD WELL CONTRACTOR: keet\-\\ !"-~} €i<eff f6ttp iJ • WI'LLCON1'RACTOR C£Rt'IFICA'I'IOfill!_=--.. cr.._q7fi...l_~lj.,;,_L.-___ _ f'ff[J10 ~~ t'\\\J 31. IITATE\¥!!LLCONSTRIJC110NPI!RMI'Tt: 1 . WELL U~ol< Ajl~llc:oaJ• ll6o)l flallidenaal 0 Munkipal 0 lncsuslrtal 0 AgrlculluraJ 0 Monlt.a.1n; !B'"" Racowry D Hear Pump Water II!Jeallc>n 0 011111 D II OU.ar, uacu•: ------------ !. RB!U!NCI l.CG 3. ~-To o-J.r: liy181"Tihrtl Sllle 4. CATEDRILLEO !:3-f)t 5. TCTALCEP'nrl ~ · ------ 6, CUTTINGS COLLECTED YES ~NOQ 7. OOES WELL REF'LACE EXISnNGWEU? YEs 0 N0~------- 8. · STA11C WAT£1'1 LEVELSelowTQCI aiCa.llnQ: Plf_ Fr. 11 IIJM'•'I-TIIp .. Cooii'ICII. a, .TOP OF CASING IS fltt FT. AbDWI..an!l Surface• "'Tr:ap ci Cl ... Mnalnal.ltd d'ar bMDIIII' ._ ~"-~ r~~qultil1 • nrar.. In IAIIQP doNoWIIIIIIIAIICAC~~I · -------- 10, YIELD (gprll): ~ MET'~C OF TE:ST -------------- 11. WATEFI ZONiiS (deplti):.IU(II;,r:!f::.~------------------- QEPn! •. CHLORINATION: 1)pi1 1/lf Arr<Junl II U$11anal apace Ia 11eodood ... -ril"""' 13. C.IISING: --· Q C.p!h I'L cj!!_'"' s;rw 'tl.t. From To :iQ Frcxn To PL """"' Tc Fl 14. CiROVT: , Cep1h Ft8e~t~~ ~'7 Fl<lm 'to \q From ___ To ___ ·Fl.--------- 1 5. SCREEN: 2 .1'1 DIPih Diarneler SIOI Size ~tellal Pram ~To .3£. 1'1 _J__ n. d2J1L ln. /Y.~ FrCIII --TQ-Fl._ Itt __ tn. ---- From __ To-FL_. in. __ ln.---- 1 II. SANCIGRAVS.. PAC!<: Coplh .Siu FrOm 4,8 T<1 3o Fl#?,. LOCAJION §K§ICH {~ dAc1ion llld dllw.-.. _ lllulol-Sw,. Aollda, or ollie INtO noflrer-m PQIPICI) .,~tJJ 18 8 i ~ from To Ft. 1 11'. FIEMARI<S: f.g .V.fiPtJ lf4!-1q-.:2f J <j'l tiki !=Iii /1..5 I DO H!,.I6B'f (;liRTIFV ntJ.T THIS weLl.. W.AS CC"4STRUCTI!O IN ~ORDAHCE WJTH 1 SA NCN: ZC. W&U. CON$'11'1UC'110111 $TANOAAC!l, ANO TH,A.T A COP'f Cl~ THIS ReCOI'IO HAll II~ PI'IOYIOBI TO TH! WI!U. 0\\'NEFI, S;M...,. !M rS-11-01 aiGNATUf'U: Of' I""!R.e!ON ~TfUJCnNCl1'l'ftl' 'Nei.J.. 0..1'1! S•t>nlioriaNIID DNoleo ol Wa~arCIIIIIIy, G...........,_ wllhln 30 days GW•l..V.l*'" .. \ .. ~· , . . , FROM RSD CAROLINAS PHONE NO. 704 662 0678 Jul. 31 2001 10: 29AM PH North CarOlina-Department of Environment and Natural Resources Divisil)11 of Wfi.ftr Quality-Groundwater Sectior'l 1636 Mllll Snce Can!er-Raleigh. NC Z76~1636 Phone (919)733-3221 • WELL CONSTRUCTION RECORD WELL CONTRACTOR: Bk:hard Simmon• Dr!IDng If NI;C WEI.l. CONTRACTOR CERT1Fic.AT10NI ~ Welllclenllflcatton ": MW-9 STATE WEL.L CONSTUCTION PERMIT II: 1. W&LL I.Oc.A TION: (Snow skiiiCil a/ the location bei<NI) N..,....t Town: Moo!'!!Ollile Counly: "lllldel=.,l _____ _ SOlllh Main 8t1eet 2. OWNER:Cher~ ADORESS: SoutliMeill Sini8i (Sfto•ur !WAI ~.) M..,.\lille NC -3. DATE DRILLED: ~ 4. TOTAL CI!F'TH: ~ ,,.,... B. CUTTING COLL!!CTED: No 6. COES WELl. REPLACE EXISTING WELL 1 7. STATIC WATER l.EVI!L Below· Tcp of c .. lng: ,u ... ·~It ADDw 'l'op ~ c.i1tl No 8. TOP CF CASiNG IS Q FT. AblMI Land Suitaoe ' • e..l'lo Ttr'll'i,. .. NMir t:.Miw ~ tulac;al• l.oaiii'IIM• t v¥~W• ~• . -lniMDI'*-Viiiii1151\MCAC2c::.OII3 ~l.D(gr:n): __ METHOOOFTESi: --- 10. WATER ZONES (Oeptll): 11. CHI.ORINATION~: 12. CASING: From From Frcm 13. GROUT: From Frcm 14. SCRE!EN: 0 0 o.pd1 To To To Oopth To To 5 • Amount; WaQ Thioknoss Oiameler cr W flight!Ft. Ft. 1" Ft. Ft. Material Ft. c .... ""' .S.Ontoofte Fl. M-~)L£ Me6locl TI'QfTimie OOplll To To To o,........,... stot s;~" Mat<riol F""" 5 From Fran 15. SANOJGRAVELPACK: Dej)tl1 Fran 3 To From To 16. REMARY.S: 15 Fl ___ Ft ___ Ft 1S Ft ___ Fl. 1" .010 PVC Size Material lf1. S<lnd DEPTH From TO DRILLING LOG •-c-- LOCATION SKE!C::H (Show dirodCcrl and clstance from at -.t t"MJ 8t:at8 Roam, 01 othar map retenmce pXnt•) w. WllaonAn • 1 t)o Ht!RCLW ~!FV TI-'AT 'NI!U. 'tWAS cotor&rllti'CTED ;N A.C;OORDANCS 'MTH 1'14 NCAtl ~.\NELL CONSTI'WCT H:IH ST'-NDA~OS. ~NO TI'Uo.T 4 COP"!" 0,. -,13 REeoAO 11M BIBN PROVIOClOTO'TH' '.\ELL O'Noii!R s~TdR~.0"~o FROM RSD CAROLINRS PHO~IE NO. 704 662 0678 Jul. 31 2001 10!30RM P12 North Carolina. Oepartmont of En'liironment and Natural ~QGoufces Division of Water Quality· Groundw~r sect~ 1e30 Mail Service Center· Raleigh, NC 276119-1635 Ph""" (919)73:1-3221 • weLL, CONSTRUCTION RECORD Wellldemlllcallon #: MW-10 1. WELL LOCATION: (Sho.ll skelch Of the loca1lon below) WELL. CONTRA:TOR: RicNird Simmons Ql'iKing qt NC WELL CONTRACTOR CERTIFICATION# ~ STATE WELL CONSiUCTION PERMIT II: NeareotTe>on: 1\!gorMyile Coufi\Y: ""lr=edal=l _____ _ DEPTH PRlWNG LOG Formation DMCriDtlon South Main Street 1 OWNER:~ ADDRESS: S!iUthM8Jji Slraet · .~arJI.atNo.l Mcon!aviile NC 3. DATE CAILLED: §£1§&1 4. TOTAL DEPTH: 2!I 5. CUTTING COLLECTED: No a. DOES WELL REPLACE EXISTING WELL 7 7. STAnCVVATER LEv"liL. Below· Top of Casing: (U .. '.-if......,.loporc.sr..p No B. TOP OF CASING IS l! FT. Ab"""' Land SUrface • • CIMing ,....,.._. fillet •~~~~•~ ...,. .. l•lllalll ·•• • Wlil!ftOI ~ ' -~~_ ........ ._,!li.~ie.l)'l~8 -LD (gpm): __ METHOD OF TEST: __ _ 10. WATER ZONES (d<lplh): 11. CHLORINATION TYJ)e: 12. CASING: Dopth From 0 To From · To From To 13. GROUT: Depth From 0 To From To 14. SCREEN: Dep(h From 10 To =rem To From To 15. SANOJGRAVEL PACK: Depth From 8 To Frc:m To 10 Fl Fl. Ft. 8 Ft. Ft. 20 Fl FL Ft. 20 Ft ___ Fi. 1\mo"nt: Wall Tllickn .. s Oiameter or WoighiiFt 1" Maleriol c...-,e..-i!a o-· 1" Size 1!2 Slot Size" .0~0 Material Sancl FTOm TO Jr add Ilona! ~ i• noectect use baCk of fam Material LOCATION SKETCH PVC (SnGw c&wo\iM II!WI O!:sWice tun at 6aal tvm stat. RCiild$, Ot ot/\er tnap 1"8ferw1ce painta) Method Tremtni& w. Wilson Aw Material PVC • S.TANOAAD$, .&.NO THAT~ COP'IOPTHS A:ECOA.OHA$:91Uittl PROV!OEtl TOTHEWEU..OWNtfl: ·0 7130101 bAlE .. · '· .. ~;:;;.' ' ." FROM RSD CRROLI NAS PHONE NO. 704 562 0678 Jul. 31 2001 l0:30AM]~{3 North Carolina. Oepat1.ment ct Environment and Nfiural Resources DMsion Cf W~r Quatity .. Groundwator Section 1838 Mail Sllnlice Center. RaleiQ!l, NC 27699-1636 PMr>e (919)733-3221 • WEill CONTRACTOR: WELL CONTR.Io.CTOR WELL CONSTRUCTION RECORD Wallldentlllallion IJ: MW·1 1 STATE WEJ.L CONSTUCTION """'"''T 1. WEJ.L ~OCA TION: (ShC!W okalch of the location betooo) N-Town: Mggreoyj!!a County·. _,lredel"""'"l _____ _ Soutll Main S1!!!!!1 2. OWNI!!R:.->C~h:;-~~=~----­ADDRESS: 5qytll Main St- ~orRovt.No.) · Mogrewflle NC 3. DATE ORIL~O: §llil!ll 4. TOTAL DEPTH: ~ e. CUTTING COI.LECTED: No 6 •. DOES WEI.L REPLACii EXISTING WELl? 7. STATIC WATeR L.EVEL BiloW. TOp ofcasi~9: (1.*"..-a A.l:lllve T'llp at Coli'Q) No 8. lOP OF CASING IS g FT. -1.8nd Surface • 10. WATER ZONES (det)lh): 11. CH~ORINATION T-: ll. CASING: .... Depth From 0 To F.rom To Fran To 13. GROUT: Depth F""' 0 To From To 14. SCREEN: 'j . ~Depth Pram · To F~ To From To 15. SAND/GRAVEL PACK: Dej>th From 28 To Fran To 18. REMARKS: 30 Ft. Ft Ft. 28 Ft. Ft. q'f .A Ft. Ft. Ft 45 Ft. ___ Ft. ArnotJnt: Well Thiokrlesa Olamoter .,w.,;ghUPl. ,. M-"ii Ceme[!! IB!!!tonRa ~ .. 1" Slot Siza" .010 Materilll Sand Material 1"1/C Molhod Tremmie M-PVC DEPTH From To DRilLING LOG Fomlltlon Oelaiplion LOOAIIQN SKSTCH (ShOw 4'ftdlcn and di!l:fanoa li'am at ~ two SteCo Re&da, or 011111r map reflfw\ee .:Qnts) W. Wii&UIAYO NC-21 • I 00 1-tliREBYCERTlFV''l'H~.'I' 'NfU. 'NA.$ CONSTII.:JCT~D IN ACCORDANC'E 'I\1Tll1~ M'AC :C. VI'EU eoNSTRUCT:ON S"r J.NOARD&, AND lHJJ A COPY or i1U AliCOAC ~ I!EN FROVIOED TO Tlolf YIEIJ. OWNER . ~;:~oM•~\)NtRAC~\u~ ~ 7f.llll01 DATii u ...... == SENT BY: _ ...... -J •............................... 10. Q 10-26-1 :1o:02AM :MID-ATL4NTIC ASSOC. , •u~; tU/ob/01 4:55PM;Wru ..... r;: S1 S250SS50; # ~~~;:15 #705; Page 3/3, .-. ~ 1. WELL t.ISii (Chock..,piloable 1ut. Aesldendal 0 illllnldpaJ 0 lndwolrial CJ ~llii..J D -ovary 0 He111 Pump W&lor lnjiiC1len 0 OI!Jr O II OUier, tJal U•: 2. QAIY..INQ LQG F'~Dnt To t~:tr Cflrot r...... 11 -4. DATe CIFIILLEO i-2eP "'f' I ~. TOTALL'.lEPTH 3lR ~ · e. CVTTJNGs COLLECTED veslk:::f NOD ~/ _____ _ 7. DOES WEll RePLACe EXISTING Weu.? YES 0 N0~-------'- 5. m"AllC ~ATEIH.EVELS.lowTopoiCaalng: Jt.fi:...FT. A.. (Uie ···1-Tojoot f;ainQ) 9. TOP Of CASlNG rslltrr FT. AlloYOI..atMI Sllr1oc:u• --'-- -rap of c:.•lnl tWmftM.d lllof blfGIIW taad lwf'flcll'llqY!l'll• • ..... ._ In ..,:.car. IWI<I Willi 11& NC.C ZC ,DJ !I 10. YIELO(opm): ~~OJ" TEST--------~--- 1 1. WATER ZONes (daptn):.tor!B:~-IIUI~------· DEPTH •• CHLORINA TlON: . Type d Amrounr II a.lc!iiJcnal spoca ~ nOOC:ed 111e booli of fc:m. ~:CASING: ' W.UTir- Fram....:IJ::..... _. _0;:'" 39 Fl Oi"lot L'tW m Fram----To---Fl.--- From ---To Ft.--- 14. CJROUT: From ..... o""---~=pt~ ¥> Ft. p, ~r;J From ---To Ft -------- 16. SCREEN: CeJ)Ih Oi.am•ter SlOt S~e ~~ P'll:lm ..3£_ To t{S"' FI_L_ in. ~in. _..~....s-.;:=-­ l'rDII\ _To __ Ft-lo. _,..._ --- \,QCATICN SICETCH (&"""' -tie• .,d diat.-,...., .. IMII-a .... ,...,...,, Of .. , ... """'"'''"""'" poliO) I 00 l'l~f!IV CI!R'III'Y TH.Io.T ntiS WliU. WMO CONSTRLJ::TI!I) II' Ac:CCADAHC:e W1111 I 5A NCAC 2C, WELl. CONSTIIUC'TIQH STAND ARtiS, OND THAT A CCPY OP 'Oil$ M RD HA.S 151li!N PRCMDEDTO THE Wlill OWNER. US!! SICINATUIIlC Ofr PliRIIC:H'I eo.8T~G tHe wwe1.1.. ..-. • ...,.."' !llol,b. "'w-a.oor. ,............., .__, wriiNn ac day• ..... SENT BY: ::i8"'t oy: MC\,;8.1..1. tWU l.fllll'!lo 10-26~ vl ; 10: 02AM :MID-ATL-\_~~~-~ _ASSQC._ -~ ,._. I. Wfi.L USE_J!IIIooiApplloaaho 110¢ flulc!enUaiO Municipal [::J lnduallllll [::J AQrlaullural 0 Monllartng EJ"' I'!ICDVIII\I [J Heat f'ump W&rerlnjectlan (J 01llllt CJ II Olher, 1.1111 Ullll: ----------- 2. WEU.I.OCA TIQI}I: ( ... akstch ¢ 11\t ~tion below) ~111n1Tcwn: OC!CPAs:.cv '!lc. CGun~y: T,ee get k QAIWNGLOO QEp!H 3. Fnn Ta 12 -a,r .. llllt. 4. DATE DFIII..L.ED '=I 1(-p/ s. TOT.IILDEPTH 2-«: 6. CUTTINGS COU!!CTED YES li2f NOD 7. DOES WEI.l fiEPI.AC! I!XlS'!lNG WELL? Yli:S 0 NO(B"': ______ _ &. STATIC WA'TER L.EVEL Belew TOll of Cuing; y;!l. FT. ~ (UM ••• II AtiCJWII 'TDp Of c.Nng) t. TOP OF CASING Ill Mtr FT. AbOV* Land SUrfllle' '"Tap fill czuf,. -~4 ..,.., • .,.land •"""-...;viMia w.,..,.._.,. aa•.,.. dlln•wiUI IU.NCAC:I£.~11 10. YleLO (gpm): MM:._ MV~ OF TEST---------,------ 11. WATEFIZOIIIES (doplh);..l~~~----------------- •• CHLORINATION: T,.-... u-=...:-~"'4"~::::::_-Atn-o_u_nl __ -_-_-_-_-_-_---~n~llld-:-IUa_noi_a-,_..--11-nalded""' -oiiCW'III 13. CASING: --~---_,.~------~--- .WlJI'nllckno .. l"rtlm ~ o;:lh '' . ft_a_.;._ .. _'"'_ .s.trG'· Ncl l'rtlft'li---To Ft.--- From To Ft.--- 14. CIROUT: From ~~ri&J Ft l:llilflll1 H From ___ To ___ Ft.--------- 1$, SCAEEH: Depth Diameter Slot SID ~~~~ F""" ~To~ Fl _j_ ln. &!/£ ln. l'tlf!- Fftlm _To_ Ft. __ ln. _ln.---- FIQITI ...:__To __ F1._ ln. _ln.---- lB. ISANDIGRAIIEL. f'.ACK: 41 Dopth2. .,-~o From Q Tc !2..... Ft. _..2. ~ram To Ft.:r:::--7'7 -:-::""'l!n---- 17. FIEMAAKS: t3e~i:fe. "'h K' LO¢ADON SKifCH ($11oo.. dl!«;Uan ond dlota,..a lmrft alloaai-Slat• fkladl, or oilier map .. r.,.noe po~ll) , J. 'l. S l;lllai-TfiiNI .A> ""'vv J ~ ,..,.,..,., --@ '"' e-rr"' #AJ-., .S/ ~"'Y 11S .. I DO HEIII!&V CERnFY TliAT THIS WEU. WAS CONS~U<:TI!!D Ill ACCOROANC!! WITH IliA NCAA: :ZC, WELL CQNS'J>UJOTION &TANDAAOS, ANO THAT A COPY 01' Till II A!CO!IP HAS !I feN f'RQVII)I;D TO THII! Y/eu. OWN !I'. t.oo;,;tt d....4) Q't-l'i -o I :sGN•c""'e QIIP'I!IISOO' CDNSTIIUCTINIO THii WliL.L. DATG •-111101•11 ta OM-or-· Clollllry. _,., -owllhln 30 day a -·1 fiiY. 12111 ·• SENT BY: iSMt OY~ MC~B~.L 13!'U\.rli!W:t 9192509950:; # <5/ '~ 10-26:} ;1o:o2AM :MID-ATL4_NTIC ASSOC. 4 . -'.' . -C.Oifta -. 0.,--ol 1!/MID ..... nl 111U1 HIJLIIII ---I)MolQ"CJI W-Qllll!y •Grautodnli.r a.cllon 1111111 Mllllllrlio8C..W• Aor.lllll. N.C. 27tii .. IIIS6-I'"""' jiii]?SW211 ·.·.' ···•·. .LL coNsTRUCTION REcoRe w&u.. coNTJtACTOA: HeeA-1\ B~Gtio! ~FL;ptt ~D . i WELl. C:OHT1IACTOR CtlmFICAl10N fl ~!t lf41 0 7 0 L 'il MW -13 STATIIWSLL CONBTIIUCl10N PliRMrrt:_.....&Ao:-...._ __ _ I. Will.&.. US~oo~.AppU .... IO llul> FIMicllnaa/0 Munlm,aJ CJ lnc!YIIIal0 AQrillulrural 0 Monitoring El"' Flec:a .. IV U Hnt l'\lmp W1ter lnJ...,IIDo CJ Olmr CJ II Oll\lr, Ual U.: ----------- ~. QRILL!NG LCQ F""" To (9 -z.. ..... CIII\IIO'Towo &lolo 4. DATI! DAIW:O 9 -(3-Q/ . · !. TOTAI.DePTH g:z:: _,/ 6. C:UTTINGS COLL5CTE'D Y!SL.k1 NOD ;;o------- 7. ooes wa~o. REPLACe EXI8TING wau ves 0 NO~ 8. STATIC WA~ &..!'VEL l!le-Top of CuO.g: lt!Jl=_ Fl'. _-_-_-_-_-_-_-_-_:-_-_--_-_-_-_..., (UM '•' u -Too of C&11"') II. TOP OF CASING IS MA-FT. Ab"'"' I.AIId S..rfoae• ..,.gp of'ee~lll '*""lt41tad atlar ._..,.. .. M surf•• NqUIMI a w.i11.,..1n ua... ---'------- -·-tUNCAC2C_.nJI 10. YlEI.O (gprn): Jl!t:., Me'T~D OP TEST-----------..,-- 11, WATER ~ONeS (dopl~):, .. !i:=:!t_L---------- perTH • CHLORINATION: Ty,e-_..-.:p;:iJSc"~----------------n-1 :::::-: --l-11111-dltionol--1111---~~-ne-oclod-~-okoll""" 1~-CASING: ------~--------- WUITJ\H:I~ .. (J o .. plh a'1,"1' s:rn m I' rom To "2 Ft From To Ft, I'~ To F!. 14. CJIIOI.IT: Deptl\ JZ.~11.riaJ &i.. From a To .:3 Ft. • ttm From To Fl. 18. SCReEN: Depll'l Cl&llletar Sial Sl:e,_~ Fran .::l-To ..l,2__ Ft _...L_ ln. JliJ1. ln. ---'~~!5::..­ Ftarn _To_ 1''--ln. __ ln.---- ft'jR! _To-~"~---tn. _ "'· ---- 1D. 8ANDtGAAVEl PACK: z:-Depth,..~ J.~ !" __ , Ftam V To ~ Fl. ~ !'!._~I Prom To l'l..---:.--.,.....--==---- 17. RE14ARKS: ile.d-,.Mlf".; "$ ~~?- M~ us SIGMit.'n.IR!! P'IIIIII'&)N c::r::w81'AUC1'1NQ JHii w&LJ.. C.,.£ L 8-qnollD -· o/W*Cu...,, o---. wllllln 30 daya .· .... • . :i APPENDIX D • RISING HEAD TEST • MP?;{\flA~NTJ.~ EngineerinN & En1•ironmentul Solutions • Bouwer & Rice Method Version 2.00 6/18/1995 • Calculation Status Bouwer & Rice Method for Calculating Hydraulic Conductivity • Project Name: Cherokee-Mooresville Project No.: ~R~I;-;1:;::2-;7.,----_______ _ Client Name· Cherokee Identification· MW-4s -----Analysis By: CRL Run Date: 9/24/01 10 Riser Pipe Diameter: = = = = ~ = = = = :J: = = = = ~ =: = = = 0.083 feet =: =: J: =:: :!: ::::!::::: Intake Diameter: 0.5 feet ----~----_j_----J----- ----;-----I-----4----- Intake Length: IS feet 0 - - - -~ - - - - -1-- - - -~ - - - - - :I: ----J----_I_----1-----Saturated Column Length: 4.15 feet --I I I :I: Water Table Depth: 32.85 feet -e-~~-11'1 -- I I I .. Aquifer Thickness: 100 feet I I I 1 I _l_ I Line Fit Starting No.: 10 Min I to 0.0001 0.0101 0.0201 0.0301 Line Fit Ending No.: 30 Max22 SpecifY Output Units: 7 I to 9 Time Hyd. Cond., K(h): 3.67E-07 cm./sec. Error of Fit: 0.000 Meas. Time FieldMeas. Drawdown/up Line Fit To Regression On # davs feet feet . -.·.:., LN(Yt) LN(Yt) I) 0.0001736 35.50 2.65 0.975 0.848 2) 0.0003472 35.41 2.56 0.940 0.847 3) 0.0005208 35.38 2.53. 0.928 0.845 4) 0.0008681 35.34 2.49 0.912 0.842 5) 0.0010417 35.30 2.45 0.896 0.840 6) 0.0013889 35.27 2.42 0.884 0.837 7) 0.0017361 35.23 2.38 0.867 0.834 SLUG Result MW-4s Pagel • 8) 9) 10) 11) 12) 13) 14) 15) 16) 17) 18) 19) 20) 21) 22) 0.0020833 0.0024306 0.0027778 0.0034722 0.0041667 0.0048611 0.0055556 0.0062.5 0.0069444 0.0104167 0.0138889 0.0173611 0.0208333 0.0277778 0.0347222 35.21 2.36 35.19 2.34 35.16 2.31 35.13 2.28 35.11 2.26 35.08 2.23 35.06 2.21 35.05 2.20 35.04 2.19 34.97 2.12 34.91 . 2.06 34.85 2.00 34.79 1.94 34.68 1.83 34.56 1.71 • • 0.859 0.831 . 0.850 0.828 i 0.837 0.825 0.824 0.819 0.815 0.812 0.802 0.806 0.793 0.800. 0.788 0.794 0.784 0.787 0.751 0.756 0.723 0.725 0.693 0.693 0.663 0.662 0.604 0.600 0.536 0.537 SLUG Result MW-4s Page2 .. ' • Bouwer & Rice Method Version 2.00 6/I 8/1995 • Calculation Status I Bouwer & Rice Method for Calculating Hydniulic Conductivity Project Name: Cherokee-Mooresville Project No.: RII27 • Client Name· Cherokee Identification· 'MW..,."--;;8c---------- Analysis By: CRL Run Date: -i9'i,;/2c:;4"-u/O"I-------------I Meas .. # I) 2) 3) 4) 5) 6) Riser Pipe Diameter: 0. 083 feet Intake Diameter: 0.5 feet Intake Length: ----~I 0=-feet Saturated Column Length: 4.32 feet Water Table Depth: 9.68 feet Aquifer Thickness: 70 feet Line Fit Starting No.: 4 Min I to Line Fit Ending No.: II Max I8 SpecifY Output Units: 7 I to 9 Hyd. Cond., K(h): 6.4IE-05 cm./sec. Time days 0.0001157 0.0002315 0.000463 0.0005787 0.0006944 0.0008102 0.0009259 Error of Fit: 0. 022 Field Meas. feet 10.51 10.26 10.10 10.00 9.94 9.92 9.91 IX3wdown/up feet · . 0.83 0.58 0.42 0.32 0.26 0.24 0.23 . ... •. . .. ~ . SLUG Result MW-8 100 ~~~~~~~~~~~~~~~~~§§~~~~§§~ ~~~~~~~~~~~~~~~~~s~~~~e~~~ :::J::::1::::r:::~====~=== 10 ::: ::: oo: ~ ::: '= ::: =: 1::: = '= ::: ~ =: '= ::: .,j = =: = =: ~ = :;:: = ~~~3~~~~~~~~~E~~~3~~~~E~~~ ===~====~====~===~====~=== ---I----~----T---I----r--- 1 ~~1§ ~ ~ ~ ~:§ ~ ~ ~ ~ ~ ~ ~ §~ ~ ~ ~~ ~ ~ ~ 0.1 O.Oi 0.0001 0.0006 0.0011 0.0016 0.0021 0.0026 . Ljne Fit To .. LN(Yt) -0.186 . '-0.545 -0.868 ·,1.139 ~1.427 -1.470 .··., Time Regression On LN(Yt) -0.650 -0.776 -1.026 -1.152 -1.277 -1.402 -1.528 Pagel • 7) 8) 9) 10) 11) 12) 13) 14) 15) 16) 17) #REF! 0.0010417 0.0011574 0.0012731 0.0013889 0.0015046 0.0016204 0.0017361 0.0018519 0.0019676 0.0020833 0.0021991 • 9.89 0.21 9.85 0.17 9.82 0.14 9.81 0.13 9.79 O.IJ 9.73 0.05 9.73 0.05 9.76 0.08 9.75 0.07 9.68 0.00 9.68 0.00 #REF! SLUG Result MW-8 • -1.561 -1.653 -1.772 -1.778 -1.966 -1.904 -2.040 -2.029 -2.207 -2.154 -2.996 -2.279 -2.996 -2.405 -2.526 -2.530 -2.659 -2.655 #NUM! -2.781 #NUM! -2.906 #REF! #REF! Page2 • Bouwer & Rice Method Version 2.00 6/18/1995 ©Creative Scientific Applications . • Calculation Status r_"• Bouwer & Rice Method for Calculating Hydraulic Conductivity Project Name: Client Name· Cherokee-Mooresville Project No.: R1127 Cherokee Identification· ""MW~:.o:_coJ-:0--------- Analysis By: CRL Run Date: 9/24/01 100 ~~~~~~~~~§~~~~~~~~~~~§§§ Riser Pipe Diameter: 0.083 feet ~~~~~~~~~~~~~~~~~~~~~~~~ -----~-----~-----·------Intake Diameter: 0.5 feet -----r-----r-----~------ Intake Length: 15 feet 10 ~~~~~~~~~5~~~~5~~~~~222 0 ~~ ~ ~ ~ ~ ~ ~ ~ ~ ~ :~ ~ ~ ~ ~ ~:~ ~ ~ ~ ~ ~ Saturated Column Length: 6.34 feet :I: --:I: ' -----·------ Water Table Depth: 13.66 feet 1 =====~~=~~=~--~===:====~~ Aquifer Thickness: 100 feet ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ :~ = -~ : : = :~= ~ ~ Line Fit Starting No.: 6 . Min I to 0.1 Line Fit Ending No.: 29 Max44 0.0001 0.0101 0.0201 0.0301 SpeCifY Output Units: 7 I to 9 Time Hyd. Cond., K(h): 3.09E-06 cm./sec. Error of Fit: 0.002 Meas. Time Field Meas, . Diawdownlup ·.·_, ·, LineFii To '· ... Regre5sion'On . # days feet feet •. ,· . ... , .\•• 'LN(Yt> .•.· LN(Yt) 0.0001157 17.77 4.11 1.413 1.349 I) 0.0002315 17.72 4.06 1.401 1.341 2) 0.0003472 17.66 4.00 . 1.386 1.333 3) 0.000463 17.59 3.93 1.369 1.325 4) 0.0005787 17.48 3.82 1.340 1.318 5) 0.0006944 17.44 3.78 1.330 1.310 6) 0.0008102 17.38 3.72 1.314 1.302 SLUG Result MW-10 • Page 1 • • • 7) 0.0009259 17.33 3.67 1.300 1.294 8) 0.0010417 17.28 3.62 1.286 1.286 9) 0.0011574 17.25 3.59 1.278 1.278 10) 0.0012731 17.21 3.55 1.267 1.270 II) 0.0013889 17.18 3.52 1.258 1.262 12) 0.0015046 17.14 3.48 1.247 1.255 13) 0.0016204 17.12 3.46 1.241 1.247 14) 0.0017361 17.08 3.42 1.230 1.239 15) 0.0018519 17.05 3.39 1.221 1.231 16) 0.0019676 17.02 3.36 . 1.212 1.223 17) 0.0020833 17.00 3.34 1.206 1.215 18) 0.0023148 16.95 3.29 1.191 1.199 . 19) 0.0025463 16.92 3.26 1.182 1.184 20) 0.0027778 16.88 . 3.22 1.169 1.168 21) 0.0030093 16.84 3.18 1.157 1.152 22) 0.0032407 16.80 3.14 1.144 1.136 23) 0.0034722 16.76 3.10 1.131 1.121 24) 0.0037037 16.71 3.05 1.115 1.105 25) 0.0039352 16.65 2.99 1.095 l.UH9 26) 0.0041667 16.59 2.93 1.075 1.073 27) 0.0043981 16.52 2.86 1.051 1.058 28) 0.0048611 16.44 2.78 1.022 1.026 29) 0.0050926 16.37 2.71 0.997 1.010 30) 0.005787 16.23 2.57 0.944 0.963 . 31) 0.0069444 16.09 . 2.43 . ' 0.888 0.884 32) 0.0076389 15.96 2.30 0.833 0.837 33) 0.0083333 15.85 2.19 0.784 0.790 34) 0.0090278 15.74 2.08 0.732 0.743 35) 0.0097222 15.65 1.99 0.688 0.695 36) 0.0104167 15.54 1.88 0.631 0.648 37) 0.0138889 15.11 1.45 0.372 0.412 SLUG Result MW-10 Page2 • 38) 39) 40) 41) 42) 43) 0.0173611 0.0208333 0.0243056 0.0277778 0.03125 0.0347222 14.83 1.17 14.50 0.84 14.35 0.69 14.21 0.55 14.11 0.45 14.04 0.38 • • 0.157 0.176 . .{).174 .{).061 .{).371 .{).297 .{).598 .{).533 .{).799 .{).770 .{).968 -1.006 SLUG Result MW-10 Page 3 • • APPENDIX E RECEPTOR SURVEY • MP?;{\flA~NTl~ Engineering & Environmentu! Solutions ENGINEERING CONSULTANTS, INC. • • 700 Blue Ridge Road, Suite 101 • Raleigh, NC 27606 • (919) 755-5011 • FAX (919) 755-14l4 January 22, 2001 Mr. John Gallagher Cherokee Environmental Risk Management 702 Oberlin Road, Suite !50 Raleigh, North Carolina 27605 Reference: Dear John: Receptor Survey and Review of Environmental Incidents Burlington Industries-Mooresville, North Caro.lina Trigon Project No. 360-01-007 In accordance with your request, Trigon Engineering Consultants, Inc. performed a receptor survey of the Burlington Industries facility in. Mooresville, North Carolina. The survey included evaluating for the presence of sensitive receptors, including, for example, water supply wells, located within a I ,500-foot radius from the Burlington Industries property (See Figure I for Area). In addition to the survey, we discussed environmental aspects of the operation. of the facility with Town of Mooresville officials, including the wastewater pretreatment coordinator. We found no known sensitive receptors within I ,500 feet of the Burlington Industries facility. There are no apparent private or public water supply wells in the vicinity of the plant site, or other sensitive receptors. The Town of Mooresville has provided public water to the area and all homes in the vicinity of the plant were reportedly connected to the public system at the time of their construction. The Town of Mooresville officials indicated, with the exception of two caustic spills in the early 1990's, that they were aware of no environmental incidents, reported releases or improper chemical handling at the Burlington plant. • • Cherokee Environmental Risk Management Burlington Industries ·Mooresville, NC Methodology January Zl, 2001 Trigmr Project No. 360·01·007 The receptor survey included interviewing Glen Shuler, Superintendent of the Town of Mooresville Utilities Department, Irene Mann, Planning Technician with the Town of Mooresville Planning, Zoning and Engineering Department, Rickie W. Stuts, Pretreatment Coordinator with the Town of Mooresville, and various residents in the neighborhoods surrounding the Burlington Industries property. In addition, Trigon performed a vehicle reconnaissance of the surrounding neighborhoods for evidence of town water meters, well houses and surface waters. Trigon also reviewed maps of the nearest public water lines to these neighborhoods. Trigon representative Charles Wilkins mobilized to the site on December 19, 2001 to perforrn· the receptor survey. Prior the vehicle reconnaissance, Town of Mooresville water supply line maps were reviewed at Mr. Shuler's oflice. Mr. Shuler indicated that these water lines were installed at the time the residential homes were constructed, and that all of the residential homes and light commercial facilities within the area identified on Figure I are supplied with water from the Town of Mooresville. Additional maps were obtained and reviewed· at the Town of Mooresville Planning, Zoning and Engineering Department. It should be noted that this is not an exhaustive survey and is not intended to wholly eliminate the presence of.possible receptors . Vehicle Reconnaissance Following review of the appropriate maps, Trigon performed a vehicle reconnaissance of the property surrounding Burlington Industries. No wells were observed in.this neighborhood. Water meters and fire hydrants were observed in the residential areas around the Burlington Industries facility. Lewis Williams at 514 Ridge Street indicated that he does not know of any wells in the area and that he a!1d his neighbors are on Town of Mooresville water. Trigon observed a decorative well house at the Shoemaker residence located at 527 Ridge Street. According to Jack Benton at 547 Ridge Street, neighbor of the Shoemaker residence, the well house is for decorative purposes and there is no well present. Mr. Benton also stated thar he has lived in the neighborhood since the 1960's and he knows of no wells in the area. An apparent decorative hand pump was observed on Ridge Street next door to 524. No house number was present and there did not appear to be a well present. An additional decorative pump was observed at the Sherills' residence at 214 Pressley Street. According to Sam Corey at 114 East Pressley, no known wells are pres,!nt in the area. According to Betty Burton at 823 Caldwell Street, no knov,11 wells are present in the area. No other evidence of water supply wells was observed during the • vehic!e reconnaissance. Cherokee Environmental Risk Management JanutJry Zl, ZOO/ Burlington Industries~ Mooresville, NC Trigon Project No. 360~01~007 • Review of Environmental Incidents • • Trigon also reviewed the history of environmental incidents with town officials. According to Mr. Stuts, Burlington Industries had two caustic spills in the early 1990's. Mr. Stuts indicated that the State and the US EPA were involved in enforcement actions associated with these incidents. He also indicated that from 1991 to the present, based on his knowledge of operations at the plant and on the inspections he conducted at the Burlington ·facility in his capacity as the town's industrial wastewater pretreatment coordinator, there have been no other environmental incidents at the Burlington Industries facility and that he did not observe misuse or improper storage of chemicals at the facility. Trigon appreciates the opportunity to have provided our environmental consulting services to Cherokee Environmental Risk Management. If you have any questions regarding this report, or if we can be of further assistance, please do not hesitate to contact our office. Sincerely, TRlGON ENGINEERING CONSULTANTS, INC. Charles Wilkins, Jr. Project Manager CGW/NLH:cgw Attachments h:\_ 0360e-l \projects\200 t \03601 007\report.doc ~' .7) -~'?- QUADRANGLE LOCATION TRIGON ENGINEERING CONSULT ANTS. INC ···.~. MOORESVILLE, N. C. 35080-E?-TF-024 PHOTOINSPECTED 1983 1969 Site Location Map Burlington Industries -Mooresville, NC JOB No. 360-01-007 DATE: January 2001 SOURCE: CGW Scale = 1:24,000 Figure 2 • APPENDIX F • LABORATORY ANALYTICAL REPORT AND CHAIN-OF-CUSTODY • MP?;{\fl~4NTlS:. Enginet'ring & Enl'ironmenlal Solutions Lab Report ~ PRISM ~~~@ -J'- .:~~ LABORATOAIES,INC. • Full Serv1ce Analytical & Environmental Solutions 10/1/01 Page 1 of 5 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Attn: Mr. Cliff Lundgren Customer Sample ID: SW-1 PO Box 669004 Prism Sample ID: AC20325 Charlotte, NC 28266 Loqin Group; 3722HZ Sample Collection Date/Time: 9/19/01 17:00 Lab Submittal Date/Time: 9/20/01 11 :17 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME . PARAM~I~~----··--------·· RESULT UNITS --·--LIMIT REFERENCE STARTED ANALYST BROMODICHLOROMETHANE Not detected ug/L EPA 601 9/28/01 09:45 WAD BROMOFORM Not detected ug/L EPA 601 9/28/01 09:45 WAD BROMOMETHANE Not detected ug/L 5 EPA 601 9/28/01 09:45 WAD CARBON TETRACHLORIDE Not detected ug/L EPA 601 9/28/01 09:45 WAD CHLOROBENZENE Not detected ug/L EPA 601 9/28/01 09:45 WAD CHLOROETHANE Not detected ug/L 5 EPA 601 9/28/01 09:45 WAD CHLOROFORM Not detected ug/L EPA 601 9/28/01 09:45 WAD • CHLOROMETHANE Not detected ug/L 5 EPA 601 9/28/01 09:45 WAD DIBROMOCHLOROMETHANE Not detected ug/L EPA 601 9/28/01 09:45 WAD 1.2-DICHLOROBENZENE Not detected ug/L EPA 601 9/28/01 09:45 WAD 1 ,3-DICHLOROBENZENE Not detected ug/L EPA 601 9/28/01 09:45 WAD 1 ,4-DICHL()ROBENZENE Not detected ug/L EPA 601 9/28/01 09:45 WAD DICHLORODIFLUOROMETHANE Not detected ug/L 5 EPA 601 9/28/01 09:45 WAD 1, 1-DICHLOROETHANE Not detected ug/L EPA 601 9/28/01 09:45 WAD 1.2-DICHLOROETHANE Not detected ug/L EPA 601 9/28/01 09:45 WAD 1.1-DICHLOROETHENE Not detected ug/L EPA 601 9/28/01 09:45 WAD TRANS-1,2-DICHLOROETHENE Not detected ug/L EPA 601 9/28/01 09:45 WAD 1,2-DICHLOROPROPANE Not detected ug/L EPA 601 9/28/01 09:45 WAD CIS-1,3-DICHLOROPROPE N E Not detected ug/L EPA 601 9/28/01 09:45 WAD TRANS-1,3-DICHLOROPROPENE Not detected ug/L 5 EPA 601 9/28/01 09:45 WAll EDB Not detected ug/L EPA 601 9/28/01 09:45 WAD METHYLENE CHLORIDE Not detected ug/L 5 EPA 601 9/28/01 09:45 WAD 1.1.2,2-TETRACHLOROETHANE Not detected ug/L EPA 601 9/28/01 09:45 WAD TETRACHLOROETHENE Not detected ug/L EPA 601 9/28/01 09:45 WAD 1,1,1-TRICHLOROETHANE Not detected ug/L EPA 601 9/28/01 09:45 WAD 1,1,2-TRICHLOROETHANE Not detected ug/L EPA 601 9/28/01 09:45 WAD TRICHLOROETHENE Not detected ug/L EPA 601 9/28/01 09:45 WAD • TRICHLOROFLUOROMETHANE Not detected ug/L 5 EPA 601 9/28/01 09:45 WAD VINYL CHLORIDE Not detected ug/L 5 EPA 601 9/28/01 09:45 WAD CIS-1,2-DICHLOROETHENE Not detected ug/L EPA 601 9/28/01 09:45 WAD NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 ..J-4() Springbrook Road .&. P.O. Box 240543..., Churlotte, NC 2H224-ll543 Phune: 704/529-6304 .A. Toll Pree Number: Hm0/52Si-h364 .&. F.t,: 704/525-0-I,l}':J Lab Report PRISM • • • 10/1/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project ID: Customer Sample ID: Prism Samole ID: Looin Group: Sample Collection Date/Time: Lab Submittal Date/Time: " LABORATORIES, INC. . . - Full Service Analytical & Environmental Solutions Page 2 of 5 Cherokee-Mooresville SW-1 AC20325 3722H2 9/19/01 9/20/01 17:00 11 :17 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER Sample Comments: TEST RESULT Angela D. Overcash, V.P. Laboratory Services REPORTING METHOD UNITS LIMIT REFERENCE DATEfTIME STARTED ANALYST NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road A P.O. Bnx ::!40543 A Ch.ulotte. NC 2.822-Hl543 Phone: 704/52Sl-6304 .6.. Toll Free Number: I-800/S29-03h4 A F,1:-..: i04/525-ll4lllJ Lab Report PRISM LABORATORIES, INC . • Full Service Analytical & Environmental Solutions 10/1/01 Page 3 of 5 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Attn: Mr. Cliff Lundgren Customer Sample 10: MW-12 PO Box 669004 Prism Sam ole ID: AC20326 Charlotte, NC 28266 Loqin Group: 3722H2 Sample Collection Date/Time: 9/20/01 09:00 Lab Submittal Date/Time: 9/20/01 11 :17 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST METHANE Less than ug/L 26 8015 9/27/01 12:45 TAl NITRATE 2.6 mg/L 0.10 EPA 300.0 9/20/01 20:55 TAR SULFATE 49 mg/L 10 EPA 300.0 9/20/01 21:14 TAR ALKALINITY, TOTAL 15 mg/L 5.0 SM 2320B 9/24/01 07:21 MLD IRON, FERROUS Less than mg/L 0.20 SM 3500-Fe D 9/24/01 15:10 MBS METALS DIGEST-SURFACE/GROUNDW Completed SW846-3005 9/25/01 13:20 LC2 MANGANESE, TOTAL IN GROUNDWATE 1.1 mg/L 0.05 SW846-6010B 9/26/01 17:51 MSC • .BENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 9/24/01 17:30 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP TERT ·BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 9/24/01 17:30 MP CHLOROFORM 11 ug/L 5.0 SW846-8260B 9/24/01 17:30 MP CHLOROMETHANE Not detected ug/L 10 SW846-8260B 9/24/01 17:30 MP 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-8260B 9/24/01 17:30 MP 1 ,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-8260B 9124101 17:30 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 9124101 17:30 MP 1 ,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9/24101 17:30 MP • 1 ,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9/24101 17:30 MP 1 ,4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9124101 17:30 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-8260B 9124/01 17:30 MP NC Certification No. 402 • SC Cert~ication No. 99012 · NC DrinkinQ Water Cert. No. 37735 • FL Certification No. E87519 44t) Springbrook RonJ .A. P.O. Box 240543 A Charlotte, NC 21'!224-0543 !'hone: 704/52!)~0364 .A Toll Frel' Number: l~H00/52!)-6364 .A F,": 70-t/5::!5-04(}9 Lab Report ~~M ··< • Full Serv1ce Analytical & Environmental Solutions 10/1/01 Page 4 of 5 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Attn: Mr. Cliff Lundgren Customer Sample 10: MW-12 PO Box 669004 Prism Sample ID: AC20326 Charlotte, NC 28266 Looin Group: 3722H2 Sample Collection Date/Time: 9/20/01 09:00 Lab Submittal Date/Time: 9/20/01 11:17 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErriME PARAMETER RESULT. UNITS LIMIT REFERENCE STARTED ANALYST 1,1-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP 1,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP 1,1-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9/24/01 17:30 MP CIS-1 ,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9/24101 17:30 MP TRANS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9124/01 17:30 MP 1,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 9/24101 17:30 MP 1,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 9124101 17:30 MP • 2,2-DICHLOROPROPANE Not detected · ug/L 5.0 SW846-82608 9124/01 17:30 .MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SWB46-82608 9/24101 17:30 . MP ETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-8260B 9124/01 17:30 MP .. ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24101 17:30 MP P-ISOPROPYLTOLUENE Not detected ug/L 5.0 SW846-8260B 9124101 17 ;30 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-8260B 9/24101 17:30 MP NAPHTHALENE Not detected ug/L 5.0 SW846-8260B 9/24101 17:30 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24101 17:30 MP STYRENE Not detected ug/L 5.0 SW846-8260B 9124/01 17:30 MP 1,1,1,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 17:30 MP 1,1,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SWB46-8260B 9/24101 17:30 MP TETRACHLOROETHENE 13 ug/L 5.0 SW846-82608 9/24101 17:30 MP TOLUENE Not detected ug/L 5.0 SW846-82608 9/24101 17:30 MP 1,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9124101 17:30 MP 1.2.4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9/24101 17:30 MP 1,1,1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 9124/01 17:30 MP 1,1,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 9124101 17:30 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9/24/01 17:30 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 9/24101 17:30 MP 1,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 9/24101 17:30 MP • 1,2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP 1,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 17:30 MP NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Rtlt~d .A. 1'.0. Box 240~43 .A. Charlottl', NC 2.H224-0543 Plwne: 704/52t.J-A364 .A. Toll Free Number: l-H00/32Y-fl364 .A. F,1:-;: 704/525-040() Lab Report ~ PRISM • -· • ,~ LABORATORIES, INC, Full Service Analytical & Environmental Solutions 10/1/01 Mid-Atlantic Associates Attn: Mr, Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Page 5 of 5 Customer Project 10: Cherokee-Mooresville Customer Sample 10: MW-12 Prism Sample 10: AC20326 Loqin Group: 3722H2 Sample Collection Datemme: 9/20/01 09:00 Lab Submittal Daterrime: 9/20/01 11 :17 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 9/24/01 17:30 MP TOTAL XYLENES Not detected ug/L S,Q SW846-8260B 9/24/01 17:30 MP cls-1 ,3-DICHLOROPROPENE Not detected ug/L 5,0 SW846-8260B 9/24/0H7:30 MP trans-1 ,3-DiCHLOROPROPENE Not detected ug/L 5,0 SW846-8260B 9/24/01 17:30 MP ACETONE Not detected ug/L so SW846-8260B 9/24/01 17:30 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-8260B 9/24/01 17:30 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 9/24/01 17:30 MP CARBON TETRACHLORIDE Not detected ug/L 5,0 SW846-8260B 9/24/01 17:30 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 9/24/01 17:30 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 9/24/01 17:30 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 9/24/01 17:30 MP ---------- ··-·------·--··-· Sample Comments: Methane subcontracted to NC certified lab #387, Sample for ferrous iron analysis was received beyond EPA recommended holding time, Angela 0, Overcash, V,P, Laboratory Services NC Certification No. 402 -SC Certification No, 99012 -NC Drinkinq Water Cert, No. 37735 -FL Certification No. EB7519 449 Sprin~brook Roe~d .A.. 1'.0. Btlx 240543 .,a,. Charlotte, NC 2H224-0543 Phune: i(l4/529-fi3fi.J. .... Toll Free Numbl'r: l-HOU/52Y-Ii364 .A. F;lx: 704/525-ll40Y ... _., ........ .,..._ --• W'U o 00 o ...... ._,,_.,., A ... Yp ......... TEST AMERICA INC ANALYTICAL REPORT 2960 Foster Creighton Drive 411rhville, Tennessee 37204 ** Original report and a copy of the chain of custody will follow by mail. • • PRISM LABORATORIES 5625 ANGELA OVERCASH P.O. BOX 240543 CHARLOTTE, NC 28224 Sample ID: AC20326 Project: Project Name: Sampler: State Certification: 387 Site I.D.: Lab Number: Ol-Al35537 Date Collected: 9/20/01 Time Collected: 9:00 Date Received: 9/26/01 Time Received: 9:00 Sample Type: Water Report Quan Dil Analysis Analysis Analyte "B.esult Units Limit Limit Factor Date Time Analyst 1-'.ethod Batch "'MISCEU..i.NEOUS cc· P~S* Methane NO ug/1 26. Z6. 9127/0l 12:45 K. Burritt 8015B 8988 HD -Not detected at the report limit. # -Recove~; out5ide Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved·By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric s. Smith, Assistant Technical Director Report Date: 9/27/01 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 'i·;.·: j =e.. ___ r.!I~M .A Full Service Analytical & Environmental Solutions 449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543 I . Client Company Name: f111!;;-A 1 {a--A Ire Report To/Contact Name: {!( I fJ.: /.._ U .• ,.Jf;) {; (2.{.: /V Reporting A~ilr'~;-------------~ CHAIN OF CUstfDY RECORD PAGE _L OF __ QUOTE II TO ENSURE PROP~R .BILLING: . Project Name: /2.//"2. ··1," ( C ?te.· .. l·., ~-.li-:1-·. ,1-l'-' \ t. 1 },(.=.. Short Hold Analysis: ,-_(ye~ (No) UST Project: (Yes) rcfl~D *Please ATTACH any project specific reporting provisions and/or QC Req~lrem~nts Purchase Order No./BIIIIf'!g Reference ------,----- Phone: 7:)J, .g .. t;if-9tr?. Fa' (Yes) (N~): ---;'?'---,,-:>,:--Requested Due Date 0 1 D. ay 0 2 Days D 3 Days 0 4 Day~ 0 5 Days Site Locatlo~/;'a_;: C/;1 ~.,.,_-,f< t.' f!' .. /~W/?<:1. r!& i<.tfZ/.::) f 0 6-9 Days 0 ~tandard 10 days .. Site Location-" y_~cal Address: ----------Samples received after 15:00 will be processed neXt business day. (, ( Turnaround time is based on business days, excluding weekends and holidays. CLIENT SAMPLE DESCRIPTION NPDES: UST: ONC ONC osc osc 0 .0 DATE COLLECTED II lr II TIME COLLECTED MILITARY HOURS '' II Q Prism Field Service 0 MATRIX (SOil, WATER OR SlUDGE) (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) SAMPLE CONTAINER •TYPE SEE BELOW NO. SIZE PRESERVA- TIVES GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA: ONC ONC ONC ONC ONC ONC osc osc osc osc O'SC osc 0 0 0 0 0 0 Samples INTACT upon arrival?/ J '2. o Received ON WET ICE? Temp~ PROPER P,Rf:SEAVATIVES indicated? Recei~~d··\.\'ITHIN HaloiNG TIMES? CUST9DY SE~LS TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Certification: NELAC __ USACE __ FL __ NC_J __ SC OTHER NIA __ · _ WaterCiorinated: YES_ NO~- Sample Iced Upon Collection: YES~ NO_ SUB lAB CERT. IDNO. PRjSM lAB IDNO. PRISM USE ONLY Site Arrival Time: Site Departure Time: Field Tech Fee: Mileage: SEE REVERSE FOR TERMS & CONDITIONS •coNTAINER TYPE CODES: A =Amber C = Clear G = Glass P = Plastic; TL =Teflon-Lined Cap VOA =Volatile Organics Analysis (Zero Head Space) FINAL REPORT COPY Lab Report PRISM • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 LABORATORIES, INC . . ' Full Service Analytical & Environmental Solutions Page 1 of 16 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-2 Prism Samcle 10: AC19784 Loain Grouo: 3599H11 Sample Collection Date/Time: 9/17/01 13:30 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: -~--~--- TEST TEST REPORTING METHOD DATEfTIME .J"t.~AMETER ------------RESULT UNITS LIMIT REFERENCE STARTED _______ ANAL Y~I NITRATE 2.8 mg/L 0.10 EPA 300.0 9/17/01 18:29 TAR SULFATE 2.7 mg/L 1.0 EPA 300.0 9/17/01 18:29 TAR ALKALINITY, TOTAL Less than mg/L 5.0 SM 23208 9/20/01 07:09 MLD IRON, FERROUS 0.6 mg/L 0.20 SM 3500-Fe D 9/17/01 22:30 EHT METALS DIGEST-SURFACE/GROUNDW Completed SW846-3005 9/21/01 12:00 LC2 MANGANESE, TOTAL IN GROUNDWATE 1.5 mg/L 0.05 SW846-6010B 9/24/01 10:45 MSC ·-------------·-·--·-·--- Sample Comments: • Sample for ferrous iron was received beyond EPA recommended holding time. • Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012-NC DrinkinQ WaterCert. No. 37735-FL Certification No. E87519 449 Springbrook Road ..a.. P.O. Box 2-!0543 £ Ch<lr!otte, N~ 2tC24-054~ l'honl..!: 704/52<1-6304 .A. Toll Free Number: 1-800/529-6304 .o1rrr.. F.l.\: 70--l/525-0400 Lab Report ~~PRISM • • • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 , ,• ~~~ LABORATORIES, INC. --... J~.-•• ' -..... Full SeNice Analyttcal & Environmental Solutions Page 2 of 16 Customer Project 10: · Cherokee-Mooresville Site Customer Sample 10: MW-2 Prism Samole 10: AC19785 Loqin Group: 3599H11 Sample Collection Date/Time: 9/17/01 13:10 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER METHANE TEST RESULT Less than UNITS ug/L REPORTING METHOD LIMIT REFERENCE 26 8015 DATE!TIME STARTED 9/25/0111:12 ANALYST TAl ·----··---···-·----------------------------- Sample Comments: Method 8015 subcontracted to NC certified lab# 387 . Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Ro<~d 4 P.O. Box 240543 4 Ch<~rlotte, NC 2R224-0543 Phone: 704/52~-1)364 A Toll Free t\iumbcr: HI00/52Y-6364 A F.1:>:: 704/525-0-Hli.J Lab Report PRISM • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 LABORATORIES, INC. Full Serv1ce Analytical & Environmental Solutions Page 3 of 16 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-8 Prism Sample 10: AC19786 Loqin Group: 3599H11 Sample Collection Date/Time: 9/17/01 10:55 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST NITRATE 3.1 mg/L 0.10 EPA 300.0 9/17/01 18:47 TAR SULFATE 75 mg/L 10 EPA 300.0 9/20/01 00:29 TAR ALKALINITY, TOTAL 6.6 mg/L 5.0 SM 23208 9/20/01 07:10 MLD IRON, FERROUS 0.2 mg/L 0.20 SM 3500-Fe D 9/17/01 22:30 EHT METALS DIGEST-SURFACE/GROUNDW Completed SW846-3005 9/21/01 12:00 LC2 MANGANESE, TOTAL IN GROUNDWATE 3.1 mg/L 0.05 SWB46-6010B 9/24/01 10:50 MSC --~----- Sample Comments: • Sample for ferrous iron was received beyond EPA recommended holding time. • Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. EB7519 -1-49 Springbrook Road • P.O. Box 240543 .A. Charlotte, NC 2~224-!1543 Phnne: 704/52Y-1)31l4 ..a. Till\ FrL'l! Number: 1-!)0()/529-6364 .a. F,l_,: 704/525-tl-!-OlJ . Lab Report • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 4 of 16 Customer Project ID: Cherokee-Mooresville Site Customer Sample 10: MW-8 Prism Samole ID: AC19787 Loqin Group: 3599H11 Sample Collection Date/Time: 9/17/01 10:05 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER METHANE Sample Comments: TEST RESULT Less than UNITS ug/L Method 8015 subcontracted to NC certified lab# 387. REPORTING METHOD LIMIT REFERENCE 26 8015 DATE/TIME STARTED 9/25/0111:19 ANALYST TAl • Angela D. Overcash, V.P. Laboratory Services • NC Certification No. 402 • SC Certification No. 99012 • NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrouk Road .&. 1'.0. Box 240543 .A. Charlotte, NC :!:-\:!24-0543 !'hone: 704/52SI-h364 .A. Toll Free Numb<~r: Hl00/52~-1)364 .A. F<1': 704/525-0..J.OY Lab Report ~\:.· PRISM • • • 9/28/01 ~ • ~ " : LABORATORIES. INC. . . ' -~~ :.· ·_'!:.''> ·_-....: ' Full Service Analytical & Environmental Solutions Page 5 of 16 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-81 Prism Samole 10: AC19788 Loqin Group: 3599H11 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Sample Collection Date/Time: 9/17/01 11:00 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEFfiME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST BENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP. BROMOFORM. Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 9/24/01 15:06 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B . 9/24/01 15:06 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP CHLOR.ODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP CHLOROETHANE Not detected ug/L 10 SW846-82608 9/24/01 15:06 MP CHLOROFORM 18 ug/L 5.0 SW846-8260B 9/24/01 15:06 MP CHLOROMETHANE Not detected ug/L 10 SW846-8260B 9/24/01 15:06 MP 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP 1 ,2-0IBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 9/24/01 15:06 MP 1,2-0IBROMOETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP 1 ,2-0ICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1 ,3-0ICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP 1 ,4-0ICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP OICHLOROOIFLUOROMETHANE Not detected ug/L 10 SW846-8260B 9/24/01 15:06 MP 1, 1-0ICHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1 ,2-0ICHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1, 1-0ICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP CIS-1 ,2-0ICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP TRANS-1 ,2-0ICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1 ,2-0ICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP 1,3-0ICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 -i.t9 Springbrook Roud A P.O. 13ox ~..!0543 ..a.. Churlotte, NC 28224-0543 l'hune: 70-t /52~-1136-t ..a.. Toll Fn .. •e N umbl~r: 1-K00/52':i-(JJ64 .A F.n:: 704/525-040LJ Lab Report PRISM • • • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project ID: Customer Sample ID: Prism Sam ole ID: Loqin Group: Sample Collection Date!Time: Lab Submittal Date!Time: LABORATORIES, INC. Fu!J Service Analytical & Environmental Solutions Page 6 of 16 Cherokee-Mooresville Site MW-81 AC19788 3599H11 9/17/01 11:00 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2.2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1, 1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP ETHYLBENZENE · Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP P-ISOPROPYLTOLUENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP NAPHTHALENE .. Not deteded SW846-82608 9/24/01 15:06 MP ug/L 5.0 N-PROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP· STYRENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1.1, 1.2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1. 1.2.2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP TETRACHLOROETHENE 31 ug/L 5.0 SW846-8260B 9/24/01 15:06 MP TOLUENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1.2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1.2.4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP 1.1.1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1.1.2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-82608 9/24/01 15:06 MP 1.2.3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP 1.2.4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP 1.3.5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP VINYL CHLORIDE Not detected ug/L 10 SW846-82608 9/24/01 15:06 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP cis-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:06 MP trans-1.3-D ICHLOROPROPEN E Not detected ug/L 5.0 SW846-8260B 9/24/01 15:06 MP ACETONE Not detected ug/L 50 SW846-82608 9/24/01 15:06 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-82608 9/24/01 15:06 MP CARBON DISULFIDE Not detected ug/L 50 SW846-82608 9/24/01 15:06 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 44!) Springbrook Roud .&. P.O. Box 240543 .a. Churlottl', NC 28224-0543 Phone: 70.J./52':.l-6364 .&. Tu!l Frel' Number: l-H00/52(j-fiJ64 .a. F.lx: 704/525-0409 Lab Report PRISM • • • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 LABORATORIES. INC. Full Service Analytical & Environmental Solutions Page 7 of 16 Customer Project ID: Cherokee· Mooresville Site Customer Sample ID: MW-81 Prism Samole ID: AC19788 Loqin Group: 3599H11 Sample Collection Date/Time: 9/17/01 11:00 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER CARBON TETRACHLORIDE 2-CHLOROETHYLVINYLETHER 2-HEXANONE 4-METHYL-2-PENTANONE (MIBK) Sample Comments: TEST RESULT Not detected Not detected Not detected Not detected Angela D. Overcash, V.P. Laboratory Services REPORTING UNITS LIMIT ug/L 5.0 ug/L 10 ug/L 10 ug/L 10 METHOD DATEITIME REFERENCE STARTED ANALYST SW846-82608 9/24/01 15:06 MP SW846-82608 9/24/01 15:06 MP SW846-8260B 9/24/01 15:06 MP •q• .. SW846-82608 9/24/01 15:06 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrouk Ro<Jd A P.O. 13o:-.. 240543 .A. Charlotte, NC 2S224-05..!3 Phone: 704/529-636-l A T111l Free Number: l-H00/52<J-6304 ...._ F;lx: 704/525-ll4l)Sl Lab Report ' ~ PRISM • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project ID: Customer Sample ID: Prism Sam ole ID: Loqin Group: Sample Collection Date/Time: Lab Submittal Date/Time: . :~ LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page 8 of 16 Cherokee-Mooresville Site MW-9 AC19789 3599H11 9/17/01 11:40 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST NITRATE Less than mg/L 0.10 EPA 300.0 9/17/01 19:06 TAR SULFATE 52 mg/L 50 EPA 300.0 9/20/01 23:05 TAR ALKALINITY, TOTAL 97 mg/L 5.0 SM 23208 9/20/01 07:12 MLD IRON, FERROUS 20 mg/L 1.0 SM.3500-Fe D 9/17/01 22:30 EHT METALS DIGEST-SURFACE/GROUNDW Completed SW846-3005 9/21/01 12:00 LC2 MANGANESE, TOTAL IN GROUNDWATE 2.0 mg/L 0.05 SW846-6010B 9/24/01 10:55 MSC Sample Comments: • Sample for ferrous iron was received beyond EPA recommended holding time. • Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Sprin~brook RmH.\ A P.O. Box 2..t0543 A. Charlotte, NC 28224-0543 !'hone: 7!l4/52Y-fl364 .A. Toll Free Number: 1-HOO/ 52Y-IJ304 .11111rr.. F.lx: 704/5::?.5-0409 Lab Report PRISM • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Sam ole 10: Loqin Group: Sample Collection Date/Time: Lab Submittal Date/Time: LABORATORIES, INC. I -' Full Serv1c:e Analytical & Environmental Solutions Page 9 of 16 Cherokee-Mooresville Site MW-9 AC19790 3599H11 9/17/01 11 :15 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER METHANE Sample Comments: TEST RESULT Less than UNITS ug/L Method 8015 subcontracted to NC certified lab# 387. REPORTING METHOD , LIMIT REFERENCE 26 8015 DATE/TIME STARTED 9/25/01 11:25 ANALYST TAl • Angela D. Overcash, V.P. Laboratory Services· • NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 -1-·N Springbrook Ro<~d .A. P.O. Box 240543 A Ch<~rlotte, NC 2H224-0543 Phone: 704/529-6304 .a. Tt)ll Free Number: 1-H00/529-6364 .&. F,l.\: 704/525-0409 Lab Report ~·~ PRISM • 9/28/01 Mid-Atlantic Associates· Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project ID: Customer Sample ID: Prism Sam ole ID: Loqin Group: Sample Collection Date/Time: Lab Submittal Date/Time: ~\ LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page 10 of 16 Cherokee-Mooresville Site MW-10 AC19791 3599H11 9/17/01 12:55 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST NITRATE 4.4 mg/L 0.10 EPA 300.0 9/17/01 19:24 TAR SULFATE 1.7 mg/L 1.0 EPA 300.0 9/17/01 19:24 TAR ALKALINITY, TOTAL Less than mg/L 5.0 SM 23208 9/20/01 07:13 ·MLD IRON, FERROUS 0.2 mg/L 0.20 SM 3500-Fe D 9/17/01 22:30 EHT METALS DIGEST-SURFACEIGROUNDW Completed SW846-3005 9/21/01 12:00 LC2 MANGANESE, TOTAL IN GROUNDWATE 0.74 mg/L 0.05 SW846-6010B 9/24/01 11:00 MSC Sample Comments: • Sample for ferrous iron was received beyond EPA recommended holding time. • Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .& f).0. Box 240543 .&. Ch<~rlutte, NC :?.H224-ll543 !'hone: 704 I 52Y-63h4 ... Toll Free Number: 1-fl(JO /529-6364 .A. F.t.\: 704 I 525-0409 Lab Report PRISM • • • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page 11 of 16 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-10 Prism Samcle 10: AC19792 Loqin Group: 3599H11 Sample Collection Date/Time: 9/17/01 12:40 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER METHANE Sample Comments: TEST RESULT Less than UNITS ug/L Method 8015 subcontracted to NC certified lab# 387. Angela D. Overcash, V.P. Laboratory Services REPORTING METHOD LIMIT REFERENCE 26 8015 DATE/TIME STARTED 9/25/01 11:33 ANALYST TAl NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Sprin)..;brook Roud .A. P.O. Box 240543 A C~arlotte, NC 2S22-H)3.J.3 l'lwne: 704/52SI-h3h4 4 Tul! Free Number: 1-800/5::.';:.1)304 .a. 1',1:-.: 70-l 325-0-HJ~l Lab Report PRISM • • • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page12of16 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: MW-13 Prism Sample ID: AC19793 Lo!lin Group: 3599H11 Sample Collection Date/Time: 9/17/01 12:15 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST BENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:53 MP BROMOBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP BROMOFORM Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 9/24/01 15:53 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:53 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-82~08 9/24/01 15:53 MP CHLOROETHANE Not detected ug/L 10 SW846-82608 9/24/01 15:53 MP CHLOROFORM No~t detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP CHLOROMETHANE Not detected ug/L 10 SW846-82608 9/24/01 15:53 MP 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SWB46-82608 9/24/01 15:53 MP 1.2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SWB46-82608 9/24/01 15:53 MP 1.2-DIBROMOETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 9/24/01 15:53 MP 1.3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-8260B 9/24/01 15:53 MP 1.1-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.2-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.1-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP CIS-1.2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP TRANS-1.2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 .t4!J Springbrook Road A P.O. Box 2-t0543 A Charlotte, NC 2S224-0543 l'lwnl': 704/529-fi]h•l A Toll Frel' i\:umbl'r: 1-800/529-6364 ..._ F,r\: 704/5:?.5-0409 Lab Report .~ f.!Y§.JI.l Full Service Analytical & Environmental Solutions • 9/28/01 Page 13 of 16 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Attn: Mr. Cliff Lundgren Customer Sample 10: MW-13 PO Box 669004 Prism Samole 10: AC19793 Charlotte, NC 28266 LoQin Group: 3599H11 Sample Collection Date/Time: 9/17/01 12:15 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfnME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2.2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP P-ISOPROPYL TOLUENE Not detected ug/L 5.0 SW846-B2608 9/24/01 15:53 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SWB46-82608 9/24/01 15:53 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP • N-PROPYLBENZENE Not detected ug/L 5.0 SWB46-82608 9/24/01 15:53 MP STYRENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1,1, 1 ,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1, 1.2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP TETRACHLOROETHENE Not detected ug/L 5.0 SWB46-82608 9/24/01 15:53 MP TOLUENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SWB46-82608 9/24/01 15:53 MP 1.2.4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.1, 1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-B2608 9/24101 15:53 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-82608 9/24101 15:53 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-82608 9/24/01 15:53 MP 1 ,2.3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1.2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP 1 ,3.5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-82608 9/24/01 15:53 MP VINYL CHLORIDE Not detected ug/L 10 SW846-82608 9/24101 15:53 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-82608 9124/01 15:53 MP cis-1.3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 9124/01 15:53 MP trans-1.3-DICHLOROPROPENE Not detected ug/L 5.0 SWB46-82608 9/24101 15:53 MP ACETONE Not detected ug/L 50 SW846-82608 9/24/01 15:53 MP • 2-BUTANONE (MEK) Not detected ug/L 10 SWB46-B2608 9/24/01 15:53 MP CARBON DISULFIDE Not detected ug/L 50 SW846-82608 9/24/01 15:53 MP NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 44Y Springbrook Ro,ld 4 P.O. Box 240543 ..tr.. Charlotte, NC 2t'224-0543 1'h1me: 704 I 52<J-h364 ..a.. Toll Fret: Number: 1-HOO I 52tJ-fiJfl4 A Fa\:: 704/525-040(} Lab Report ,.,.. RISM ~~p • • • 9/28/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 ~ LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page 14 of 16 Customer Project 10:· Cherokee-Mooresville Site Customer Sample 10: MW-13 Prism Sample 10: AC19793 Looin Group: 3599H11 Sample Collection Date/Time: 9/17/01 12:15 Lab Submittal Date/Time: 9/17/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER CARBON TETRACHLORIDE 2-CHLOROETHYLVINYLETHER 2-HEXANONE 4-METHYL-2-PENTANONE (MIBK) Sample Comments: TEST RESULT Not detected Not detected Not detected Not detected Angela D. Overcash, V.P. Laboratory Services UNITS ug/L ug/L ug/L ug/L REPORTING METHOD DATEfTIME LIMIT REFERENCE STARTED ANALYST 5.0 SW846-8260B 9/24/01 15:53 MP 10 SW846-8260B 9/24/01 15:53 MP 10 SW846-82608 9/24/01 15:53 MP 10 SW846-82608 9/24/01 15:53 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 4-19 Springbrook Rund • P.O. Box 240543 .&. Charlottt!, NC 2H224-0543 Phmll': 704/52~-1)364 £Toll Free 1'\!umbcr: J-Hll0/52Sl-6364 .A. F.lx: 704/525-0409 SEP-26-2001 13:09 FROr1: TEST AMERICA TO:B-17045250~ • • • TestAmerica ANALYTICAL REPORT PRISM LABORATORIES 5625 ANGELA OVERCASH P.O. BOX 240543 CHARLOTTE, NC 28224 Project: Project Name: 3599Hll Sampler: ~eport tHCCI~OlA'lCI Qc""' Lab Number: Ol-Al3276l Sample ID: AC19785 Sample Type: Water Site ID: Date Collected: Time Collected: Date Received: Time Received: 9/17/01 13:10 9/21/01 9:00 D1l AllJtlyflb AnAl;v~lR Analytt Rtteult onus Umit l1mit ro.etor Da.to Tlmc AMl.y!'ft. ~l'!'l:hod Ba-:eh -------------------------- *W...SC~EOIJS IX r~S" 1?. rllAI'l.e ND \1~1 26. 26. 9125/0l 11:12 ND-Nat dl!lt~e~ad at tht! tttport limit. , • aac:ovf'.ry Cl\lt."1d:A LAboratory hl.atoricai or :z:athod prascr1bed limit:l. These results relate only to the items tested. This report shall not be reproduced except in fun and with permission of the laboratory. ................ •• Burritt Report Approved By: Report Date: 9/25/01 ··------- 8015!! Paul E. Lane, Jr., Lab Director Gail A. Lagc, Technical Serv. Michael H. Dunn, M.S., Technical .Director Johnny A. Mitchell, Dir. Technical Serv. Eric s. Smith, Assistant Technical Director Glenn L. Norton. Technical Serv. Kelly S. Comstock, Technical Scrv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report . 2960 Fn>""" C•<HlliTON OMovf. 1 NA<HVII.I.•.TN 37204 I 6!5-726-D177 I FAI: 615·7Z6·0954 ( ll01)-76~-D980 7665 SEP-26-2001 13:10 FROM:TEST AMERICA TO:B-17045250409 P.004 • • • Test America ANALYTICAL REPORT PRISM LABORATORIES 5625 ANGELA OVERCASH P.O. BOX 240543 CHARLOTTE, NC 28224 Pro~ect: . ProJeCt Name: 3599Hll Sampler: Lab Number: Ol-Al32762 Sample ID: AC19787 Sample Type: Water Site ID: Date Collected: Time Collected: Date Received: Time Received: 9/17/01 10:05 9121101 9:00 B.e.sult tTnf.u Lil'!l.it Limit Factot Dat~ Time. ~K!SC!U.ANEOU9 GC PARI.METERS• MP.thlUlP. N1) 26. 26. 9125/0l 1J :19 rc. liu:r:dtt 8015M NO • Not 4ate~te4 at tha report 1imit. f .. R~ccvery O!Jt!S~df!' LR.borator.y bi!"tcr1c.ctl or mP.thod p~e"crtbed U111ir.R. These results relate on!y to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane. Jr .. Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric s. Smith, Assistant Technical Director Report Date: 9125101 Gail A. Lage, Technical Serv. Glenn L. Norton. Technical Serv. Kelly s. Comstock, Technical serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report . 2960 FnsTr.t CM~<u:~rnN Dowr./ NMIIVII.I.•.TN 37204/ 615-726-01771 FAX: 615-726-0954/800-765-0980 7665 SEP-26-2001 13:10 FROM:TEST AMERICA TO: 8-17045250409 P.OOS • • • TestAmerica ANALYTICAL REPORT PRISM LABORATORIES 5625 ANGELA OVERCASH P.O. BOX 240543 CHARLOTTE, NC 28224 Project: PrOJect Name: 3599Hll Sampler: R.aault Unita "11ISCELLANE0t1S IX PABAl'IE1"US• Me!hBne ND ug/l Ntl .. Not dot~C~I'}d M the report l1m,:r:. Rorort Lifllit 26. QuM Limit Lab Number: Ol-Al32763 Sample ID: AC19790 Sample Type: Water Site ID: Date Collected: Time Collected: Date Received: Time Received: 9117/01 11:15 9/21/01 9:00 'il Andy!!i$ An.tlyj:lifC Foeo:o:~r DO.tf.l time Andy'.lt; ------------------------------------ 26. ?125/0l lL25 l. B1Jrri tt I • ~ovory OQt~14~ Ldboratory h1~~or1c~l o: ~t.hod prflr.~~ibA4 llmir;~. These results relate only to the items tested. This report shall not be reproduc~d except in full and with permission of the laboratory. Report Approved By: Report Date: 9/25/01 MAr;bod --------- SOil~ Paul E. Lane, Jr., Lab Director . Michael R. Dunn. M.S .. Technical Director .Johnny A. Mitchell, Dir. Technical Serv. E'ic S. Smit.h, Assistant Technical Director Gail A. Lage, Technical Serv . Glenn L. Norton. Technical Serv . Kelly s. Comstock. Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report . 2900 Fn:rrr.• CRtlr.urnN D•••t 1 N•~,Vl~t•.TN 37204 I 6\u-726-0\77 I FAx: 6\5-726-0954 /800-765-0980 Bat::c.h 7665 SEP-26-2001 13:10 FROM:TEST AMERICA TO:S-17045250409 P.006 • • • Test America ANALYTICAL REPORT PRISM LABORATORIES 5625 ANGELA OVERCASH P.O. BOX 240543 CHARLOTTE, NC 28224 Pro~ec t: ProJect Name: 3599Hll Sampler: Lab Number: Ol-Al32764 Sample ID: AC19792 Sample Type: Water Site ID: Date Collected: Time Collected: Date Received: Time Received: 9/17/01 12:40 9/21/01 9:00 Report Quan Dil An&ly~ia Analysia ' Re11ult Unil:& Umir: J.nalyat Kathod Bateh ugll 26. 9/25/01 11:33 X. ~lrritt SOlSM ND • Not d~t~etod at t~ r~~~rt l1m1t. ~ • Rec~ery outa14a Ldbotatory hi~tori~al or mothod pr~aeribod lim1ta. These results relate only to the items tested. This report shall not be t'eprod.uced except in full and with permissiqn of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell. Dir. Technical Serv. Eric S. Smith, Assl.stant Technical Director Report Date: 9/25101 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock. Technical Serv. Pamela A. Langford, Technical Serv. l.aboratory Certification Number: 387 End of Sample Report . 2980 FOOTER C••rcHTON DRIVE I NASHVILLE.TN 37204 I 815-726-0177 IF~~' 615-721\-0954/ 800-785-0980 7665 SEP-26-2001 13:10 FROM:TEST AMERICA TO:S-17045250409 Testi~merica • PROJECT QUALITY CONTROL DATA Project Number: • •~MISC PARAMETERS•• Methane Mathana ~AHISC PARAMR!!RS~• Mathana K~tr1x Spike Raeovnry unito Orig. Val. ogr. 0.103 0\g/L 0.103 HRtr.ix Spike Duplic&tQ uniu Orig. V(\l. ~----··--- LSO Laboratory ContrQl n~~~ MS Vd l..50 1.30 Dul?liC:A.ta .................. 1.30 u.nlu Known Val. AM..i.:n;ed V11.1 • ~•VOA PARA~~s~• Mt!thartC! **HISC PARAHEI!RS~* 11ethane m;q:/1 Laboratory units "''ll 1.33 1.40 ContrQl DA.t:A .,. . ., VOll. AMlJZftd Val -·----·-·· .................... 1.33 1.40 1.33 lOS 40 140 1.33 90 40 140 RPil Lim.1t Q.C. PaA.t:c.h -----------------··· !4 .29 50 7665 ~ Recovery Target Rang~ Q.C. aeteh 105 82 121 7665 ;: aecovery l'uget Range Q.C. 8At:<:h ----------------------........ -... 82 • 121 7665 P.007 7665 01-A134261 7665 0 1· Al3t,26l 2960 Fnsre• Cl"lra!TUN OkiV>: I NASHVII.LE,TN 37204 I 615·726-0177 I Fu: 615-726·09641 600·76G·09{10 SEP-26-2001 13:10 FROM:TEST AMERICA TO:B-17045250409 Test America • PROJECT QUALITY CONTROL DATA Project Number: 81PI.~It Data Bla.dJt VolU('. -~~-·------- Bllm.k 'Oata tnan.l.t. Vf.\luA ------------ •~MISC PARAMETERS•• Mcr.hM.~"­• 0.026 Uniu Q.c. :Batch ------------------- 1JnH::: Q.c. Satt.h. ---------····------ ••IL 7~6~ , .. Value Ol.ltsldP. Labo;ratory hi.::torical or Mthod p.!'A~cribed QC li:ni u . • !nd o.t Report £or rroje~t 253629 • Analysis OAt I'! Anely2iS T1mP: -------······ -----------·· Dlltll M~ly:red Tii<O 1\na.ly:ed -------····-----------···- 9/2$/0l lO:JJ 2960 Fn.,l:o CWOHTON D•1•• I NMHVMr-,TN 37204 I 615·726-0177 I F.x: 615-726-0954 I 800-765-0980 P.008 CHAI~ OF CUSTODY RECORD ;~.n(,;) c1 I PAGE __ OF--QUOtE ~!fl oRliAE PROPS BILLING: Sa'f\;11~3 ttlTACT tJpon arrival? run s..n~oe -'nei¢1cal & t.m~l Solli\II:IM 441 Springbrook Road • P.O. B~ ~ • NC 2~0 \ I Client Company """'"'+...,1F--:1o<!"'"C 'l'~?."'::rl~f:--- ReportTotContact He•~~~~~!i~~~:~c= R rttn •' !'rojecl Name: ~·..2;&1.;:,1. '!E~Z:.iJJtUffL~=--------~-:- Short Hold An3Jysls: (Yes) f."'ai) UST Pro~l: (Yes) (No) RaceM.d ON VIET \CE? TerT.p __ _ PROP~R PRESERVATIVES iM':aled? Reoeivect wmti.N HOLOJMG TlMES? CUSTODY SEALS tNTACT? Test America 2960 Fostec Origltlon R4 Nashville, 1N 37204 VOLATILES rE-e'd WAJUT HEA.OSPAC£? -------·J PHOPi:R CONlA.,NrnS tn!Jd'? BE FILLED IN BY YES NO r~A She Location Name:----=--------&•• Location Physical Address: --------- H.eQUe..st60 UlJe ua.te u , l""Y lJ ~ u;) URys u 4 Deys 0 S Da~ 06-9 ~ J'\Standa.td 10days Samples r£-:E-Ived eha 15:00 d be processed ned lauainu5 d£v. . TUlnaround time is bas~ (!R bg:gnes.s. dayt, exc;fuding weekends end hoii~­ (SEE REVERSE SIDE FOR RUSK 1URNAROUND F££S) Cert1Hc:a~on:. NELAC __ USACE __ FL __ NC SC __ O'THEA ---WA -- WaterCiarlnale<l: YES_ NO_ SA&IPL.E CON'TAJNEfl CUENt swPL£ oesCAJPnON 90' • sc111e 1:1 sc 1:1 sc Q sc () sc 1:1 sc () sc PRESERVA- TIVI!S NPOES: I UST: l GROUNDWATER: I DRJNJ<INGWATER: l SOUDWASTE: ) RCRA:: !:INC ONC l:ll'fC ONC I ONC ONC o___ o___ o o______ o ______ o __ _ g::cLA: I ~grn-L: I g~: 1:1 sc 1:1 sc 1:1 sc Q _____ Q 0~--- 'CONTAINER TYPE CODES: • A ~ Amber C • Clear G = Glass P = Plastic; TL = Tenon-uned Cap VO.olallle Organics Analysis (Zero Heod Space) YES_ NO_ sua LAB JIEMA>lKS CEfiT. IOHO. PRISM lAB IDNO. ·PRISM USE'ONLY Sl!e Am\lal Tm•: . Site Oep2rll!Te T.ims: rtcW l&ch Fftf': Mile&i!O: SEE REVERS£ FOA TEfU.'!S & CONDITiONS OR~ ;,, -~-~!!~~ Full Service Analytical & Environmental Solutions 449 Springbrook Road • P.O. Box 240543 • CharloUe, NC 28224·0543 Phone: 7n"s-"\;.,; -§ \\] Fax §(No): 71("-'-.1'§ -•\11'\ Site Location Name: e..\::_t· (r")\I'P-Mu.,r .... v.\\t ,), r p Site Location Physical Address: ---------- CliENT DATE SAMPlE DESCRIPTION COllECTED v._l\l!u M ~I -'il\ '"'w- M IV- J'I\V-\V (IJ\ '.J-I ;• : 't() (V\W-'1 ·. 15 '.J Fed Ex 1.:.J UPS !J Hand-delivered U Prism Field Service '.J MATRIX (SOIL, WATER OR SLUDGE) CHAIN OF CU.ODY RECORD PAGE _\ _ OF l_ QUOTE I TO ENSURE PROPER BILLING: ------ Project Name: C'.\,er~\..v-1-J. .• whv .\\(• S·.1t Samples INTACT upon arrival? · Received ON WET ICE? Temp~ PAOP~R PRESERVATIVES indicated? Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No) *Please ATTACH any project specific reporting provisions and!$!_ QC R~quirements Invoice To: t \, \'i: \. "·~t>' ( (\ .s Receiv~d WITHIN HOLDING TIMES? __ ----;T' CUSTODY SEALS INTACT? " ------.7""' ---!,L"_ VOLATILES reC'd W/OUT ~t:AUSPACf:? z_JL___;. --=-= PROPER coNTAINERS-Used? ~ Address: ____________________ '----'------~--------------' Purchase Order NoJBilling Reference ~---------­ Request~d Due Date _'0 1 Day 0 2 Days ci 3 Days 0 :4 Days 0 5 Days ~ 0 &-s Days 0 Standard 10 days Samples received alter 15:00 will be processed next business day. Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) SAMPlE CONTAINER NO. SIZE _L '> .., ( -s -~') '> ., ( . '· (, s PRESERVA- TIVES '} '! " ), I ·r ''i TO BE FILLED IN BY PERSONNEL C~rtilication: NELAC __ USACE __ FL __ NC L SC OTHER N/A Water Clorinated: YES NO 'f NO SUB LAB PRISM LAB IDNO. PRISM USE ONLY Site Arrival Tim~: Site Departure Time: Field Tech Fee: Mileage: NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA: LANDFILL: OTHER: ONC ONC ONC ONC osc osc osc osc 0 0 0 [I •coNTAINER TYPE CODES: A = Amber C = Clear G = Glass [INC l:l NC [I sc osc 0 0 P = Plastic; TL =Teflon-Lined Cap ONC [INC ONC osc osc osc 0 [I 0 VOA =Volatile Organics Analysis (Zero Head Space) SEE REVERSE FOR TERMS & CONDITIONS FINAL REPORT COPY P.O.#IBilling Re.t~_re~?~-\ .. f-J. .:-\\-t --1:;..; -\_,,,.,,. -~-(~-"C{i(t:~·J·"f ~'' \...- CHAIN OF CU.ODY RECORD PAGE (· OF 2:__ QUOTE # ----,-------- 449 Springbrook Road .... Charlotte, NC 28217 P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 70415(~~~3t~.)., ~a~: 704/525-0409 REPORT TO: Name ---.\ . - - . -- BILL TO: Address,._\_~'>-, -~~--,; -·;. I ; · -'!-.~,;;\I I , Name---~----~------____ , _____ _ A~dress _ Requested Due Date 0 1 Day 0 2 Days 0 3 Days 0 4 Days Q 5 Days 0 6-9 Days 0 Standard 10 days Samples received after 15:00 will be processed the next business day. Turnaround time is based on business days, excluding weekends and holidays. State Certification Requested FL NC sc Water Chlorinated Yes Sample Iced Upon Collection CMUD NPDES No Yes Other.-. NA -- NA No OTHER. (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) PrOJeCt Name ' _. PRESS DOWN FIRMLY-3 COPIES CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED Mltii'A"iiv HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER PRESERVA- "TYPE TIVES SEE BELOW NO. SIZE ANAL VSES REQUESTED / ·. / ' /, / / /'·. / ,, ' \ ;.J / ,, REMARKS 'J. ·-I .J-_"j l't .'IS ',.j ' . ... ,.,vr ' ~ (_ ·; _', \i '·· \ 1- ------------ 1!;.< II(,;Jt-'ikNI,l- Sampler's Stgnature ~ ------?.----/---- ' 0 Fed Ex 0 UPS 0 Hand-delivered 0 Other. ·-------·-------------- ,\,, ~~.-;~r 1-t,)\-1/i ~ ________ sampledBy(PnntName).-·-···--··---.cl Rpived By: (Signature) I Received By: (Signature) NPDES: UST: GROUNDWATER: DRINKING WATER: , SOLID WASTE: RCRA: ' CERCLA Q NC 0 NC , 0 NC 0 NC \o NC 0 NC 0 NC 0 sc 0 sc 0 sc 0 sc 0 sc 0 sc 0 sc CJ OTHER ' 0 OTHER 0 OTHER o OTHER i 0 OTHER 0 OTHER 0 OTHER . . n'.)-rn &;·1·1· '~­-__ _ Affiliation __ __ __ Additional Comments: -.. , . . . g'}'>::]j _j,;,t· ..... -.. -· !; 'j "'' -' Log-In Group No. LANDFILL OTHER: 0 NC 0 NC - [I sc 0 sc 0 OTHER 0 OTHER SUB LAB CERT. IDNO. PRISM LAB IDNO. ·-----·-1---1 PRISM USE ONLY Site_ArrivallJme:· <;_""'. Site DepartUre Time:·-. .. .-. . Field Tech F_ee: . J Mileage . ' ;_' . SEE REVERSE FOR TERMS & CONDITIONS *CONTAINER TYPE CODES: A =Amber C =Clear G =Glass P =Plastic; TL = Teflon·Uned Cap VOA =Volatile Organics Analysis (Zero Head Space) FINAL REPORT COPY ·--. Lab Report " ~ p f:':, RISM • • • t ~~ ? LABOR~TORIES, INC. Full Service Analytical & Environmental Solutions 9/27/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Page 1 of 3 Customer Project ID: Cherokee-Mooresville Customer Sample ID: MW-8;(11-12.5) Prism Samole 10: AC19409 Looin Grouo: 3546H3 Sample Collection Date/Time: 9/12/01 14:20 Lab Submittal Date/Time: 9/13/01 18:00 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: --·----··--------------------- TEST TEST _f'!I_RAMETER ---·-RESI.JL T ____ _\!_NITS TOTAL ORGANIC CARBON Less than mg/kg Sample Comments: TOC subcontracted to NC certified lab# 539. Angela D. Overcash, V.P. Laboratory Services REPORTING METHOD LIMIT REFERENCE 1.0 SW-846 9060 DATErriME STARTED 9/19/01 12:53 ANALYST PLI NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 44<} Springbrook Ru<ld .&. 1'.0. Box 2-!0543 .4. Charlotte, NC 2~~24-0543 Phune: 704/529-6364 A Toll Free Number: J-):l!l()/529-h3M .A. F,1;.;: 704/325-0.tOY Lab Report ~ PRISM • • • 9/27101 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project ID: Customer Sample ID: Prism Sam ole ID: Loqin Group: Sample Collection Date/Time: Lab Submittal Date/Time: ~:\~ LABORATORIES, INC . .. :~ Full Service Analytical & Environmental Solutions Page 2 of 3 Cherokee-Mooresville SB-1 (13.5-15) AC19410 3546H3 9/13/01 13:20 9/13/01 18:00 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER TOTAL ORGANIC CARBON Sample Comments: TEST RESULT 510 TOC subcontracted to NC certified lab# 539. Angela D. Overcash, V.P. Laboratory Services UNITS mg/kg REPORTING METHOD LIMIT REFERENCE 1.0 SW-846 9060 DATE/TIME STARTED 9/19/01 12:53 ANALYST PLI NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 -1-49 Springbrook Rand A P.O. Box 2-l0543 .A. Ch.Hlottt:, NC ::!~::!24-0.543 l'hLll1l!: 704/529-6364 A Toll Free Numbt>r: 1-HIJ0/529-03()4 A F.1x: 704/525-040lJ Lab Report ~ PRISM • • • 9/27/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 ~{,\ LABORATOAIES,INC. f-,~ ~ -.... Full Serv1ce Analytical & Environmental Solutions Page 3 of 3 Customer Project ID: Cherokee-Mooresville Customer Sample ID: SB-2 (21-22.5) Prism Samole ID: AC19411 Loqin Group: 3546H3 Sample Collection Date/Time: 9/12/01 10:50 Lab Submittal Date/Time: 9/13/01 18:00 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER TOTAL ORGANIC CARBON Sample Comments: TEST RESULT 770 TOC subcontracted to NC certified lab# 539. · Angela D. Overcash, V.P. Laboratory Services UNITS mg/kg REPORTING METHOD LIMIT REFERENCE 1.0 SW-846 9060 DATEfTIME STARTED 9/19/01 12:53 ANALYST PLI NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 44!J Spring-brook RunJ .A. P.O. 13ox 240543 .A. Charlotte, NC 2S2:!4-0543 Phone: 704/52!J-D364 .A. Toll Free Number: 1-H0(}/32SI-hJ64 A. F<l:\: 70-l/525-ll..J.OlJ Sep-26-01 04:07P acces_s ~!'.alytical 803 7Sl. 4303 I·H~~; P.Ol. f·._.,.,c L • ,UCie OverQSb · l'l'ltm Labon.torlea tnc: P.O. Boll 140.143 Cllarlotte, NC 21214 Slle Locallan/Projeot Pcrt.eiU Solids Cartaon, TOIII 011'h~ ACCESS ANALYTICAL, INC. 73.4 IIDL " REPORT COMMENTS: Paa• 1 Se-p~emba-tfi, 1001 a.ipon 1 IOIOOOiill Onkr, ll8239 I i!O.)(A1Tioi·D221 d !1060 (NASI So1ll1l CUOIIfta em IDI 960%3 Mw-s; (il-l'-.;-) SuDple l.D.: AC 19409 Callilch<l: Of/U/01 l4:lD R...ned: Ot/11101 10:00 Colleaeol by: Clialt 0.01 1.0 05tlli/Z001 Qt/l91100l 10:4(1 fV/10 09119/ZOOI 09119/l001 11:.!1 SIIF BDL: In~ Analyr.e i• Below De~ee~ion UA1i1 MEDF: Mllril Efftctec! Dilution Jlaaor Unl.,, odwwiiC! OOtec!. JIIIIICJ deaoreo '"'" wcilhf Unl ... olllerwiiC! DOled in ealY$1 ...,.ion, Ill work porform<d by STL MIAMI. IOUlO USA Today Way, Miramar .PI~ 33025. (9S4) 01·4SSO (South Catolilla Cen 101 !16023) co,,., Al.•l4l180, Ct.•IPHOl17, IU.=IIE270 + E124S, Ky.•ti900B'7, t...•#llfiOI, Md.Dn71, Ma.a~·FUl!­ NO. •IRifil, OK.•19!23, SC. -l!lfi023, T11.•1TNOl826 Unless Ollll:twiiC IIOhOII, umplca lllbmillld fOJ I!PA :SOlS~ oolleclecl,p•..., vorl md ualyzal iD """'rdaDcc • with an med\odoiDJYft<IUircmtW. ~- COIIIpnJ K..,......sadve • 1248 LAKr MURRAY BLVD. ·JRMO. S.C. 29063 !'HONE 1803) 781·4243 ·TOLL FREE 1888) 315-4243 • FAX 1803) 781·4303 • EMAIL: AXSA NAL YT@AOL.COM Sep-26-01 04:08P access analytical . ·-.~ ...... v...,..., ..,...,.,c:..v v.~. J.O·.:>v ru: 803 781 4303 FAX: P.02 • • • Anpe Oven:asll Primo Laborlldri• lae P.O.IIoa:l40543 Cll8rlone, N'C 28%24 Pcrccnl SoliiJ Cutton, Tom.l Orp:n~ lti!PORT COMMENTS: USIJLT IU 510 PAGE 2.-7 Se!>-l ( 1'3S-I$"") !!Mlple I. D.: AC 1!1410 Calleded: Of/13/Gl 13:20 Iecdved: . 09/11101 10:00 Colle<fed by: Cliad UEIBCUON Do\ T£ uwn ar. 0.01 1.0 OQ/18Jltl01 0!1119/l(IC)!IO,.I IV/10 OOJit/2001 09fl91l00S tl:Sl SMP . BDL: 1n••'&ICI Aaai)'IC is Below Daccci= Limit MEDF: Malril< Etfocled Dilullon Faccor Unless Olberwise ncne4, msfKi dumea wet weiJb! Un!ea Olbcrwiac: liiiiCCI ill Ulllyn SCCiioD, all wmt performed by STL MIAMI. 10200 USA Today Way, MiraiDat Flarida 3302S. (9S4) 43HSSO tSowb Clrolllla Cctt 1019602.3) terts: Al.•'41180; Cl.~#PH0217, ICl.=l£!70 + E124S, Ky.•l90087, l.a.=l960l, Md.=ll71, Ma.=fM·Fl.S3' ND. •IR163, OK. ~m2.3, SC. •19602.3, Til. =TI'N02126 Unleu ~ liNd. wapleo oullmilled for EPA 503S wen: c:ollcc!=l,preservcd wllllllyzcd in accorcbua: Willi all -bodOlotY l'eqlliremeDIS . Sep-26-01 04:08P access analytical • ,......._ t'IV.\IVV v~r~o Vl iO·SS !U: 803 781 4303 FAX: P.03 PAGE 3/ 7 • • • ADgle Ov...cash Prtim Laboratotlfs lac P.O. 11m< UOS43 Cllorlolfe, NC ZQ:U Pl:~n:l£olid.s Cartm., Tocal Orcanic REPORT COMMENTS: · 85.5 no llNITS _$8.-2..( '2-/ -22 s) Sample I.D.: AC 19411 CallKicd: 0!1/lliGI 10:50 lteceiwd: 0!1111/61 10:00 Coli""""' bJ': Cllcat 0.01 1.0 091111/2001 0!1111112001 10,.1 IV/IIt) 09J19/2CD1 09/1Mil01 1:l:5l ... f BDL:.I.adicates A11a1yte iJ BeloW DOitClion Limil MEDF: Mamx Etr=ed DU.WO.. F¥101' Unl ... Olberwi& DOled, 1111/X& dc:aorel wet wejpl Uulea Dllw'loiae liOUII ill aaai)'SI=tion. aU wart perfotllled by STL MIAMI. 10200 USA Today WIJ', Milamlr Plorida330%5. (!154) 431-4550 (Soudl CuoliDa Celt !DI9602l) terto• Al.~l41110, Cl ... IPH0217, Ki.•ll!l70 + El245, Ky. •#90087. L&.•19601. Md.•l271. Ma.~IM~PLS3~ ND. •iJR16l, Olt. •19523, SC. al96023, Tn. =ITN02826 Ullleas Olbe<witc DOled, saDiplca mllmiued fat !!Pl. 5035 wme calle<~ed,pme~Ved IIlii 81111y>ed in occoroOIIOC wid! all =cbodolog ~ti...,ems. ,,,..,.... ... · c:::.----"-'::::.----- CGiiiJIIIIJ' lep1 _,--~--PRISM ;~< '. LABOR-ATORIES, IN~. PA~HA~FN OQ~T~~~~.?.~.~~~CORD. _._: -. ·_ --- Full Service Analytical & Environmental Soluti~ms 449 Springbrook Road • P.O. Box ~40543 • Charlotte, NC 28224-0543 Site Location PhysiCal Address: ---oc::-'--------- CLIENT DATE SAMP~E OE~CRIPTION , COLLECTED TIME COLLECTED . ·M.ILITARV HOURS MATRIX (SOIL, WATER OR SLUDGE) 0 Hand-delivered Q Prism Field Service Q Other ProjectName: ('1,-,Ha\.~<-fi'.ourt~v,\\c £;1-e_, Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No) Purchase-Order No./Billing Reference ----------- Requested Due Date 0 1 Day 0 2 Days 0 3 Days 0 4 Days 0 5 Days 0 s--.9 Days dstandard 10 d!'lys Samples received after 15:00 will be processed next b~sin9ss day. Turnaround time is baSed on business days, exclu~ing Vff!!ekEmds and holidays. (SEE -AE~ERSE SIDE FOR FEES) .. SAMPLE CONTAINER "TYPE SEE BELOW NO. I SIZE . PRE.SERVA:·· TIVES NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: _RCRA: CERCLA: LANDFILL: ONC osc o_· __ _ ONC osc o~--- ONC osc Q ____ _ ONC osc o ____ _ ONe' osc o ___ _ ONC osc o_·-~- ONC osc o __ -'-- ONC osc 0 __ '-<- TO BE FILLED IN BY CLIENT/SAMPLING PERSONN,_ Certification: NELAC __ USACE __ FL __ NC __ SC __ OTHER ___ NIA __ WaterCiorinated: YES_ NO_ Samp!e Iced Upon Collection: YES OTHER: ONC osc Q __ _ REMARKS NO SUB lAB CERT. IDNO. PRISM lAB . IDNO. PRISM USE ONLY Site Arrival Time: Site Departure Time: Field Tech Fee: . -'· Mileage: SEE REVERSE FOR TERMS & CONDITIONS *CONTAINER TYPE CODES: A= Amber C = Clear G = Glass P = Plastic; TL =Teflon-Lined Cap VOA =Volatile Organics Analysis (Zero Head Space) FINAL REPORT COPY .- . . -_ Lab Report ~PRISM ~~~~~'!)[QJ • LABORATORI.ES,INC. _,~c..:~ Full Service Analytical & Environmental Solutions • • 8/14/01 Page 1 of9 Mid-Atlantic Associates Customer Project 10:. Cherokee-Mooresville Site Attn: Mr. Cliff Lundgren Customer Sample 10: MW-45 PO Box 669004 Prism Samole 10: AC15359 Charlotte, NC 28266 Loain Group: A0815H3 Sample Collection Date/Time: 8/7/01 11:05 Lab Submittal Date/Time: 8/7/01 15:50 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST PREP. METHOD 3510 Completed SW846-3510 8/10/01 08:30 JDP 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC PHENOL Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 1,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 1,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 1.4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC NITROBENZENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC ISOPHORONE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 8/13/01 22:36 LAC 2.4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BIS(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 1,2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC NAPHTHALENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC HEXACHLOROBUTADIENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 4-CHLOR0-3-METHYL PHENOL· Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC ACENAPHTHYLENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364.., Toll Free Number: t-800/529-6364 .._Fax: 704/525-0409 Lab Report ~~~.JM • • • Full Service Analytical & Environmental Solutions 8/14/01 Page 2 of 9 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Attn: Mr. Cliff Lundgren Customer Sample 10: MW-45 PO Box 669004 Prism Sam ole 10: AC15359 Charlotte, NC 28266 LoQin Group: A0815H3 Sample Collection Date/Time: 8/7/01 11:05 Lab Submittal Date/Time: 8/7/01 15:50 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2,4-DICHLOROPHENOL Not detected ug!L 10 SW846-8270C 8/13/01 22:36 LAC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 2,4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 8/13/01 22:36 LAC 2,4 DINITROTOLUE.NE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC FLUORENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 8/13/01 22:36 LAC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC ANTHRACENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC FLUORANTHENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC PYRENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC CHRYSENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC INDEN0(1,2.3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC BENZO(G.H,I)PERYLENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC PHENANTHRENE Not detected ug/L 10 SW846-8270C 8/13/01 22:36 LAC ---------- NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...., P.O. Box 240543 ...., Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o.. Toll Free Number: l-800/529-6364 ..o.. Fa.x: 704/525-0409 Lab Report .. ~ PRISM • • • 8/14/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Sample 10: Login Group: Sample Collection Date/Time: Lab Submittal Date/Time: ·~ LABORATORIEs; INC. •·F~d~~ · Full Service Analytical & Environmental Solutions Page 3 of 9 Cherokee-Mooresville Site MW-45 AC15359 A0815H3 8/7/01 8/7/01 11:05 15:50 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER Sample Comments: TEST RESULT Angela D. Overcash, V.P. Laboratory Services REPORTING METHOD UNITS LIMIT REFERENCE DATE!TIME STARTED ANALYST NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224~0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 .·., . Lab Report ····~PRISM • • • _ ., LABORATORIES, INC, .. ~If~·> . Full Service Analytical & Environmental Solutions 8/14/01 Page 4 of 9 Mid-Atlantic, Associates Customer Project ID: Cherokee-Mooresville Site Attn: Mr. Cliff Lundgren Customer Sample ID: MW-8 PO Box 669004 Prism Sample ID: AC15360 Charlotte, NC 28266 Lapin Group: A0815H3 Sample Collection Date/Time: 8/7/01 11:25 Lab Submittal Date/Time: 8/7/01 15:50 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST BENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP BROMOFORM· Not detected ·ug/L 5.0 SW846-8260B 8/10/01 20:59 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 8/10/01 20:59 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP SEC-BUTYLBENZENE . Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP CHLOROBENZENE Not detected . ug/L 5.0 SW846-8260B 8/10/01 20:59 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 8/10/01 20:59 MP CHLOROFORM 9.0 ug/L 5.0 SW846-8260B 8/10/01 20:59 MP ' CHLOROMETHANE Not detected ug/L 10 SW846-8260B 8/10/01 20:59 MP 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-8260B 8/10/01 20:59 MP 1 ,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1 ,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846·8260B 8/10/01 20:59 MP 1 ,4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-8260B 8/10/01 20:59 MP 1,1-DICHLOROETHANE Not detected ug/L 5.0 SW846·8260B 8/10/01 20:59 MP 1 ,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,1-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP CIS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP TRANS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1 ,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP NC Certification No. 402 -SC Certification No. 99012 • NC Drinkin~ Water Cert. No. 37735 FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .._Toll Free Number: 1-800/529-6364 .._ Fax: 704/525-0409 Lab Report • • • 8/14/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte. NC 28266 Full Service Analytical & Environmental Solutions Page 5 of 9 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-8 Prism Samcle 10: AC15360 Loqin Group: A0815H3 Sample Collection Date/Time: 8/7/01 11:25 Lab Submittal Date/Time: 8/7/01 15:50 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RES]Lll__. UNITS LIMIT REFERENCE STARTED ANALYST 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP ISOPROPYLBENZENE .. Not detected · ug/L 5.0 SW846-8260B 8/10/01 20:59 MP P-ISOPROPYLTOLUENE Not detected ug/L 5.0 SW846-8260B . 8/10/01 20:59 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP NAPHTHALENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP STYRENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,1,1,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,1,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP TETRACHLOROETHENE 41 ug/L 5.0 SW846-8260B 8/10/01 20:59 MP TOLUENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,2,4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,1,1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,1,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 8/10/01 20:59 MP 1,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP 1,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 8/10/01 20:59 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP cis-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP trans-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 8/10/01 20:59 MP ACETONE Not detected ug/L 50 SW846-8260B 8/10/01 20:59 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-8260B 8/10/01 20:59 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 8/10/01 20:59 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 ------- Lab Report • • • 8/14/01 Mid-Atlantic Associates Attn: Mr. Clift Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 6 of 9 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-8 Prism Sample 10: AC15360 LoQin Grouo: A0815H3 Sample Collection Date/Time: 8/7/01 11:25 Lab Submittal Date/Time: 8/7/01 15:50 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-82608 8/10/01 20:59 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-82608 8/10/01 20:59 MP 2-HEXANONE Not detected ug/L 10 SW846-82608 8/10/01 20:59 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-82608 8/10/01 20:59 MP ·-·-·---- Sample Comments: ~ Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 -149 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: t-800/529-6364 .... Fax: 704/525-0409 Lab Report ~"'~~M • • • Full Service Analytical & Environmental Solutions 8/14/01 Page 7 of 9 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Attn: Mr. Cliff Lundgren Customer Sample 10: MW-10 PO Box 669004 Prism Sam ole 10: AC15361 Charlotte, NC 28266 LoQin Group: A0815H3 Sample Collection Date/Time: 8/7/01 10:50 Lab Submittal Date/Time: 8/7/01 15:50 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST BENZENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP BROMOBENZENE Not detected ug/L 5.0 SW846-82608 8110/01 21:41 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP BROMODICHLOROMETHANE Not detected ugtL 5.0 -SW846-8260B 8/10/01 21:41 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 . MP BROMOMETHANE Not detected ug/L 10 SW846-82608 8/10/01 21:41 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP CHLOROBENZENE. Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 8/10/01 21:41 MP CHLOROFORM Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP CHLOROMETHANE Not detected ug/L 10 SW846-82608 8/10/01 21:41 MP 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 8/10/01 21:41 MP 1 ,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP 1,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP 1,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 1 ,4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-8260B 8/10/01 21:41 MP 1,1-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 1 ,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP 1,1-DICHLOROETHENE 9.7 ug/L 5.0 SW846-8260B 8/10/01 21:41 MP CIS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP TRAN.S-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 1 ,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP 1,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: l-800/529-6364 .... Fax: 704/525-0409 Lab Report ·')~~!~Mo. •• • • -~~~-:·--w·~ Full Service Analytical & Environmental Solutions 8/14/01 Page 8 of 9 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Attn: Mr. Cliff Lundgren Customer Sample 10: MW-10 PO Box 669004 Prism Sample 10: AC15361 Charlotte, NC 28266 LoQin Group: A0815H3 Sample Collection Date/Time: 8/7/01 10:50 Lab Submittal Date/Time: 8/7/01 15:50 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOO DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP P-ISOPROPYLTOLUENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP STYRENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 1,1,1 ,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP 1, 1,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP TETRACHLOROETHENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP TOLUENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 1,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 1.2.4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 1,1,1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP 1,1,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-82608 8/10/01 21:41 MP 1,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP 1 ,2.4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP 1 ,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP VINYL CHLORIDE Not detected ug/L 10 SW846-82608 8/10/01 21:41 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP cis-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP trans-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 8/10/01 21:41 MP ACETONE Not detected ug/L 50 SW846-8260B 8/10/01 21:41 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-8260B 8/10/01 21:41 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 8/10/01 21:41 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 ..... Charlotte, NC 28224-0543 · Phone: 704/529-6364 ..o. Toll Free Number: 1-800/529-6364 ..o. Fax: 704/525-0409 Lab Report PRISM • • • 8/14/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 j _, Customer Project ID: Customer Sample ID: Prism Sample ID: LoQin Group: Sample Collection Date/Time: Lab Submittal Date/Time: LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page 9 of 9 Cherokee-Mooresville Site MW-10 AC15361 A0815H3 8/7/01 8/7/01 10:50 15:50 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 8/10/01 21:41 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 8/10/01 21:41 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 8/10/01 21:41 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 8/10/01 21:41 MP --------- Sample Comments: ~ Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 ... Charlotte, NC 28224-0543 Phone: 704/529-6364 • Toll Free Number: 1-800/529-6364 ... Fax: 704/525-0409 P.O.#/Billing R~terence _ ~--ot ---,-.,,-l-· • --"·f.'V\"-1-C.: .. -1 1.:0ortt.,·J. \\\,' J·"' t.. CHAIN OF CU.ODY RECORD PAGE-~ OF-~ QUOTE#--------- 449 Springbrook Road ..... Charlotte, NC 28217 P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529\f>~M t; Fax: 704/525-0409 ,).:\ ·····"·•'<IU'\ REPORT TO: Name ________ :;. _______ . ____ -- BILL TO: Address -· Name---------- Address_------~----------·--­ Requested Due Date D 1 Day . 0 2 Days 0 3 bays 0 4 Days ~ 5 Days 0 6-9 Days 0 Standard 10 days Samples received after 15:00 will be processed the next business day. Turnaround time is based on business days, excluding weekends and holidays. Requested FL __ --· NC __ Water Chlorinated Yes. Sample Iced Upon Collection CMUD -·--·--NPDES sc -· No Yes Other ___ NA -- --NA __ No OTHER----- Pro:Ject Name _ _ . --_,-,,.:_·_. _ ·':----__ ·~ _ _ (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) PRESS DOWN FIRMLY· 3 COPIES CLIENT SAMPLE DESCRIPTION DATE COLLECTED l'l\ w -1\-~ _'6 n to\ -r~, v.7 -:-t.r --: --r-- ~~ \" :~so ·----v- TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPlE CONTAINER •TYPE SEE BElOW NO. SIZE PRESERVA- TIVES \ ('J ,, "(. :: 'tci·~r -\\t:_I -t -·. ~T·-----~,;----· / \ / / REMARKS l'l.d•l' I j. tJ.--~ . '/1~·~{-"V Y. ·ya.,.,r·-· f"',o~· 1'1)-l<.o).( Sampler's Signature ___ ----~-_ ------:J---------·· Sampled By (Print Name)----~~~.:...--.~/----,1--------·----·--·Affiliation-_---------- Received By: (Signature) Date Military/Hours Additional Comments: Received By: {~ignalure) Date "Ri~f •• o ~iej,;n Laboratocte• By · · t· · V\ tN . ...._ -Method of ShiP(neqt: . -·----------------------'~---v·_ --,;..-,-·--·------ ,1( ·' / ':t Fe<\ Ex 0 UP~::t-Hand-delivered 0 Ot~_er: .. . _ _ / _,.,.,.,.-_ RelinQUished BY: (Signature) ~~fe,\ J···J .• ,.,Iii' .. ,,,i I I . , -" . -!--. l --. Log-In Gro\'q~P, ,.. _ -o..'"'ytr!H:f>··- NPDES: UST: GROUNDWATER: ! DRINKING WATER: SOLID WASTE: RCRA: CERCLA ' LANDFILL OTHER: ' Q NC Q NC Q NC Q NC Q NC i Q NC Q NC I Q NC i Q NC ! I 0 sc [J sc [J sc [J sc [J sc [J sc [J sc [J sc ' [J sc Q OTHER Q OTHER Q OTHER Q OTHER Q OTHER i Q OTHER Q OTHER ' Q OTHER i Q OTHER SUB LAB CERT. IDNO. PRISM LAB IDNO. I) ))C{ l·)';co PRISM USE ONLY Site Arriv~l Tirf!e: _ .. Site Departure Tim~: . ~ieldT~~ F~e: Mileage ·--. . SEE REVERSE FOR TERMS & CONDITIONS 'CONTAINER TYPE CODES: A ~ Amber C = Clear G = Glass P = Plastic; TL = T eflon-Uned Cap VOA = Volatile Organics Analysis (Zero Head Space) FINAL REPORT COPY • • • La~ Report 7/25/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Sample 10: Login Group: Sample Collection Date/Time: PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page 1 of 3 Cherokee Mooresville Site MW-7 AC12895 2046H2 7/13/01 10:10 Lab Submittal Date/Time: 7/13/01 11:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST C5-C8 Aliphatics 200 ug/L 150 MADEP VPH 7/17/01 22:49 JYS C9-C 12 Aliphatics Not detected ug/L 100 MADEP VPH 7/17/01 22:49 JYS C9-C 10 Aromatics Not detected ug/L 50 MADEP VPH 7/17/01 22:49 JYS Surrogate % Recovery-PID: 92 % (70-130) MADEP VPH 7/17/01 22:49 JYS Surrogate% Recovery-FlO 96 % (70-130) MADEP VPH 7/17/01 22:49 JYS Dilution Factor ug/L MADEP VPH 7/17/01 22:49 JYS -------- EXTRACTION FOR EPH Completed MADEP-EPH 7/24/01 19:00 JMK C9-C18 ALIPHATICS Not detected ug/L 250 MADEP-EPH 7/25/01 06:03 KTE C19-C36 ALIPHATICS Not detected ug/L-250 MADEP-EPH 7/25/01 06:03 KTE C11-C22 AROMATICS Not detected ug/L 250 MADEP-EPH 7/25/01 06:03 KTE SURROGATE RECOVERY-ALIPHATIC 78 % (40-140) MADEP-EPH 7/25/01 06:03 KTE SURROGATE RECOVERY-AROMATIC 97 % (40-140) MADEP-EPH 7/25/01 06:03 KTE SURR:2-BROMONAPHTHALENE 76 % (40-140) MADEP-EPH 7/25/01 06:03 KTE SURR:2-FLUOROBIPHENYL 70 % (40-140) MADEP-EPH 7/25/01 06:03 KTE DILUTION FACTOR ug/L MADEP-EPH 7/25/01 06:03 KTE ---------- NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..o. P.O. Box 240543 ..o. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o. Toll Free Number: 1-800/529-6364 ..o. Fax: 704/525-0409 Lab Report "'''"~~,§~ • •• • 7/25/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Sample 10: Login Group: Sample Collection DatefTime: Lab Submittal DatefTime: Full Service Analytical & Environmental Solutions Page 2 of 3 Cherokee Mooresville Site MW-7 AC12895 2046H2 7/13/01 10:10 7/13/01 11:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST PARAMETER Sample Comments: TEST RESULT Angela D. Overcash, V.P. Laboratory Services UNITS REPORTING METHOD LIMIT REFERENCE DATE/TIME STARTED ANALYST NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 ..a.. Charlotte, NC 28224-0543 Phone: 704/529-6364 • Toll Free Number: l-800/529-6364 .._ Fax: 704/525-0409 • • • Lab Report 7/25/01 Mid-Atlantic Associates Attn: Mr. Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project ID: Customer Sample ID: Prism Sample ID: Login Group: Sample Collection Date/Time: . ~~!~Mo.· -··:!'''~= Full Service Analytical & Environmental Solutions Page 3 of 3 Cherokee-Mooresville Site TRIP BLANK AC12932 2046H2 7/13/01 Lab Submittal Date/Time: 7/13/01 11:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST C5-C8 Aliphatics Not detected ug/L 150 MADEP VPH 7118101 01:47 JYS C9-C 12 Aliphatics Not detected ug/L 100 MADEP VPH 7118101 01:47 JYS C9-C10 Aromatics Not detected ug/L 50 MADEP VPH 7118101 01:47 JYS Surrogate% Recovery-PID 98 % (70-130) MADEP VPH 7/18/01 01:47 JYS Surrogate %Recovery-FID 92 % (70-130) . MADEP VPH •7/18/01 01:47 JYS Dilution Factor ug/L MADEP VPH 7/18/01 01:47 JYS ---------- ----·· Sample Comments: ~ Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..._ P.O. Box 240543 ..._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ..._Toll Free Number: 1-800/529-6364 ..._Fax: 704/525-0409 ''· :.... . . . lrl ._..; . • Full Service Analytical &· Environmental Solutions Main Office: 449 Springbrook Road P.O. Box 240543 Charlotte, NC 28224-0543 Phone: 704/529-6364 1/800/529-6364 Fax: 704/525-0409. ·.~.· ~ .. • • CompanyName: -~J_-~ ~--·---,----Date: 1:/z.=r/o!. To:_· _ ___,ClJ?=·=!W-::c._-"'~4· :::·-'-_-'-· 7!'-=:::::..:._-·-----,,.-------Lab Group ID: Z·o'{l,l-f t-- The State of North Carolina requires the enclosed VPH and EPH forms be submitted with our laboratory report. Before submitting these forms to the state, please insert tho: project name and/or site location. TYJk ;tou. ~a.-- Prism LaborJrie~, Inc. Cc: Lab File T:word/vphtonn/siteloca.doc '···· • • VPH (Aiiphatics/Aromatics) Laboratory Reporting Form Client Name Mid-Atlantic Associates Project Name Cherokee-Mooresville Site Site Locaiion Method for Ranges: MADEP VPH VPH Surrogate Standards Aliphatic: 2,5-Dibromotoluene Aromatic: 2,5-Dibromotoluene Hydrocarbon Ranges Units of Measure C5 -CS Aliphatics** ug/L C9-C12 Aliphatics** ug/L C9-C10 Aromatics** ug/L Sample Surrogate Acceptance Range Aliphatic Surrogate % Recovery -FID Aromatic Surrogate % Recovery -PID Laboratory Name NC Certification# (Lab) Sample Matrix Prism Laboratories, Inc 402 Water Sample Information and Analytical Results Sample Identification AC12895 AC12932 Trip Blk Collection Option (for soil)* ·NA NA Date Collected 7/13/01 7/13/01 Date Received 7/13/01 7/13/01 Date Extracted NA NA Date Analyzed 7/17/01 7/18/01 %Dry Solids NA NA Dilution Factor 1 1 MDL RL Blank Sample Results 47 150 <150 200 <150 28 100 <100 <100 <100 10 50 <50 <50 <50 70-130% 70-130% 70-130% 97% 96% 92% 99% 92% 98% * Option 1 -Established fill line on vial Option 2 -Sampling Device (indicate brand, e.g. EnCoreTM) Option 3 -Field weight of soil • •• Unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, and/or concentrations of other ranges that elute within the specified range. MDL = Method Detection Limit RL = Reporting Limit Blank= Laboratory Method Blank or Trip Blank whichever is higher (indicate type) VPH rev. 11/00 Were all performance/acceptance standards for required QA/QC procedures achieved? Were any significant modifications to the VPH method made? C:::=--Y'-e'-s;__-==:::=:>No-Details A C No =:>Yes-Details A • • • EPH (Aiiphatics/Aromatics) Laboratory Reporting Form Client Name Mid-Atlantic Associates Project Name Cherokee-Mooresville Site Site Location Method for Ranges: MADEP EPH EPH Surrogate Standards Aliphatic: 1-Chloro-octadecane Aromatic: o-Terphenyl EPH Fractionation Surrogates #1: 2-Bromonaphthalene #2: 2-Fiuorobiphenyl Laboratory Name NC Certification # (Lab) pample Matrix . Sample Information and Analytical Results Sample Identification AC12895 Date Collected 7/13/01 Date Received 7/13/01 Date Extracted · 7/24/01 Date Analyzed . 7/25/01 %Dry Solids NA Dilution Factor 1 Prism Laboratories, Inc 402 Water Hydrocarbon Ranges Units of Measure MDL RL Blank Sample Results C9 -C18 Aliphatics* ug/L 130 250 <250 <250 C19 -C36 Aliphatics* ug/L 120 250 <250 <250 C11 -C22 Aromatics* ug/L 240 250 <250 <250 Sample Surrogate Acceptance Range 40-140% 40-140% Aliphatic Surrogate% Recovery 56% 78% Aromatic Surrogate% Recovery 84% 97% Fractionation Surrogate Acceptance Range 40-140% 40-140% Fractionation Surrogate #1 % Recovery 68% 76% Fractionation Surrogate #2 % Recovery 70% 70% • Unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, and/or concentrations of other ranges that elute within the specified range. MDL = Method Detection Limit RL = Reporting Limit Blank = Laboratory Method Blank EPH rev. 11/00 Were all performance/acceptance standards for required QA/QC procedures achieved? Was blank correction applied as a significant modification of the method ? Were any significant modifications to the EPH method made? Page 1 ~ No -Details Attached Yes~ QD Yes-Details Attached P.O.#/BIIIIng RFfer~n,. . . " .• 0 , . \' ._.1.. . . ..t·•.ll..lhtt'-1-'·W•~ >V· ,1{' ;,"\€_ ProJect Name~--____ ------------------------ CLIENT SAMPLE DESCRIPTION DATE COLLECTED , i I :SiD\ . II /,1 .:) dr"l:f. Sampler's Signature _____ ~-----~ TIME CQ~~~"'!"~D MILITARY HOURS MATRIX (SOIL, WATER OR , .SLUDGE) CHAIN OF CU.ODY RECORD PAGE _\_ OF _i_ QUOTE # · 449 Springbrook Road .... Charlotte, NC 2821 7 P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 7o4/St(~~3,~~-<t1 ;,~~ 704/525-0409 REPORT TO: Name --·---~---____:_:l_ ---------- Address ---------~------- BILL TO: ·Name-------______ _:__ --- Address _ __ ----· ----------.. Requested Due Date 0 1 Day 0 2 Days 0 3 Days 0 4 Days 0 5 Days 0 6-9 Days,-6' Standard 10 days Samples received after 15:00 will be processed the next business day. Turnaround time i~ based on business days, excluding weekends and holidays. (SEE REVERSE SIDE FOR RUSH TURNA~OUND FEES~-. SAMPLE CONTAINER "TYPE SEE BELOW NO. ' ·' SIZE PRESERVA- TIVES \ / I . --l- ·~ Requesled FL . ;_ NC . . SC . _ Other ~-NA Water Chlorinated Yes Sample Iced Upon Collection CMUD NPDES. No NA Yes No OTHER- PRESS DOWN FIRMLY· 3 COPIES / / REMARKS SUB LAB CERT. IDNO. PRISM LAB IDNO. . ____ /j~'J _,-· " {>· (~-t~~ 1;;,.·, ·(.. Affiliation Date Military/Hours Additional Comments: PRISM USE ONLY M"eihodot-shjpffiiqH --· --· --·----·· 0 Fed Ex 0 UPSXr;.. Hand-delivered a Other: NPDES: Q NC Q sc Q OTHER UST: Q NC Q sc 0 OTHER GROUNDWATER: Q NC Q sc Q OTHER DRINKING WATER: i SOLID WASTE: ONC lONG QSC :osc Q OTHER 0 OTHER RCRA: Q NC 0 sc Q OTHER CERCLA Q NC Q sc Q OTHER Date LANDFILL Q NC Q sc 0 OTHER OTHER: Q NC ~­ Q sc Q OTHER •coNTAINER TYPE CODES: A =Amber C =Clear G =Glass P =Plastic; TL =Teflon-Lined Cap VOA =Volatile Organics Analysis (Zero Head Space) F!eld Tech_fee: .. .' SEE REVERSE FOR TERMS & CONDITIONS FINAL REPORT COPY • • • Lab Report Today's Date: July 12, 2001 Mid-Atlantic Associates Attn: Cliff Lundgren PO Box 669004 Charlotte, NC 28266 PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions REVISED LABORATORY REPORT Client Project ID: Cherokee-Mooresville Site Client Sample ID: MW-7/ Prism Sample ID: AC11550 Prism Login Group: 1695H18 The attached laboratory report is a revision and supersedes our original laboratory report dated July 11, 2001 If you have questions, please call us . Angela D. Overcash, V.P. Laboratory Services Prepared by: Paula Gilleland F:\common\revlab.xls Created 3/16/00 Revised 3/30/00 449 Springbrook Road ..... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report ~~!~M. -...a:5~~ Full Service Analytical & Environmental Solutions 7/12/01 Page 1 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-1 PO Box 669004 Prism Sam ole 10: AC11543 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 09:20 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST METALS DIGESTION/3030C Completed 3030C 6127101 09:30 LC2 SILVER, TOTAL, IN GROUNDWATER Less than mg/L 0.018 6010 6127101 20:38 MSC MERCURY DIGESTION Completed EPA 245.1 712101 09:30 LC2 PREP. METHOD 3510 Completed. SW846-3510 6/28101 08:00 JDP LEAD, TOTAL IN GROUNDWATER 0.051 mg/L 0.015 SW846-6010B 6127/01 20:38 MSC ANTIMONY, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-601 OB 6/27/01 20:38 MSC . ARSENIC, TOTAL IN GROUNDWATER 0.058 mg/L 0.010 SW846-601 OB 6/27/01 20:38 MSC BERYLLIUM, TOTAL IN GROUNDWATER 0.010 mg/L 0.002 SW846-601 OB 6/27/01 20:38 MSC CADMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.005 SW846-6010B 6/27/01 20:38 MSC CHROMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-6010B 6/27/01 20:38 MSC COPPER, TOTAL IN GROUNDWATER Less than mg/L 1.0 SW846-601 OB 6/27/01 20:38 MSC NICKEL, TOTAL IN GROUNDWATER Less than mg/L 0.10 SW846-6010B 6/27/01 20:38 MSC SELENIUM, TOTAL IN GROUNDWATER Less than mg/L 0.01 SW846-6010B 6/27101 20:38 MSC THALLIUM, TOTAL IN GOUNDWATER Less than mg/L 0.05 SW846-601 OB 6/27/01 20:38 MSC ZINC, TOTAL IN GROUNDWATER Less than mg/L 2.0 SW846-6010B 6/27/01 20:38 MSC MERCURY, TOTAL IN GROUNDWATER Less than mg/L 0.0002 SW846-7470 7/3/01 13:30 PRF BENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6129/01 13:42 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 6/29101 13:42 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 6/29/01 13:42 MP CHLOROFORM Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364 """ Toll Free Number: 1-800/529-6364 ...,. Fax: 704/525-0409 • • • Lab Report ~!:!!~M.· .....d""'~~ Full Service Analytical & Environmental Solutions 7/12/01 Page 2 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-1 PO Box 669004 Prism Sample ID: AC11543 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 09:20 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFI;RENCE STARTED ANALYST CHLOROMETHANE Not detected · ug/L 10 SW846-82608 6/29/01 13:42 MP 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP 4-CHLOROTOLUENE Not detected ug/L . 5.0 SW846-82608 6/29/01 13:42 MP . 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 6/29/01 13:42 MP 1,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP· DIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP 1,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP 1 ,3-DICHLOROBENZENE Not detected ug/L s.o SW846-82608 6/29/01 13:42 MP 1.4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP DICHLORODIFLUOROMETHANE Not detected ug/L ~0 SW846-82608 6/29/01 13:42 MP 1, 1-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP 1,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP 1,1-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP CIS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP TRANS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP 1 ,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP 1.3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SWB46-8260B 6/29/01 13:42 MP 1, 1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP ETHYLBENZENE Not deteCted ug/L 5.0 SW846-82608 6/29/01 13:42 MP HEXACHLOROBUTAOIENE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP P-ISOPROPYLTOLUENE Not detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP METHYLENE CHLORIDE Nat detected ug/L 5.0 SW846-8260B 6/29/01 13:42 MP NAPHTHALENE Not detected ug/L 5.0 SWB46-82608 6/29/01 13:42 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP STYRENE Nat detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP 1,1,1,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP 1,1,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP TETRACHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/29/01 13:42 MP NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 ...._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ...._ ToU Free Number: l-800/529-6364 ...._Fax: 704/525-0409 Lab Report ~~i • Full Servk:e Analytical & Environmental Solutions 7/12/01 Page 3 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-1 PO Box 669004 Prism Sam ole ID: AC11543 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 09:20 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEJTIME PARAMETER RESULT . _Ul!LTS> ___ LIMIT REFERENCE STARTED ANALYST TOLUENE Not detected ug/L 5.0 SW846-8260B 6129101 13:42 MP 1,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846·8260B 6129101 13:42 MP 1,2,4-TRICHLOROBENZENE Not detected · ug/L . 5.0 SW846-8260B 6129101 13:42 MP 1,1, 1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6129/01 13:42 MP 1,1,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6129101 13:42 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6129101 13:42 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 6129101 13:42 MP • 1,2;3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 6129101 13:42 MP 1 ,2.4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6129/01 13:42 MP 1 ,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 612910113:42 MP VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 6/29/01 13:42 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-8260B 6129101 13:42 MP cis-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6129101 13:42 MP lrans-1.3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6129101 13:42 MP ACETONE Not detected ug/L 50 SW846-8260B 6129101 13:42 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-8260B 6129/01 13:42 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 6129101 13:42 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 6129101 13:42 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B . 6129/01 13:42 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 6129101 13:42 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 6129101 13:42 MP ---------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6128101 20:50 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6128/01 20:50 HWC PHENOL Not detected ug/L 10 SW846-8270C 6128101 20:50 HWC 1,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6128101 20:50 HWC 1,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6128101 20:50 HWC 1.4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6128101 20:50 HWC • BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6128/01 20:50 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6128/01 20:50 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364""' Toll Free Number: t-800/529-6364""' Fax: 704/525-0409 • • • Lab Report ""'~~~ Full Service Analytical & Environmental Solutions 7/12/01 Page. 4 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-1 PO Box 669004 Prism Sample ID: AC11543 Charlotte, NC 28266 LoQin Group: 1695H18 Sample Collection Date/Time: 6/26/01 09:20 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC ISOPHORONE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/28/01 20:50 HWC 2.4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 815(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 1 ,2.4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/2~/01 20:50 HWC HEXACHLOROBUTADIENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC ACENAPHTHYLENE Not dete.cted ug/L 10 SW846-8270C 6/28/01 20:50 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 2.4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01'20:50 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 2,4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6/28/01 20:50 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC FLUORENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/28/01 20:50 HWC NC Certification No. 402 -SC Cert~ication No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: t -800/529-6364 .... Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 5 of 67 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: MW-1 Prism Samole ID: AC11543 Login Group: 1695H18 Sample Collection Date/Time: 6/26/01 09:20 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC DI·N·BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC PYRENE Not detected ug/L 10 SW846-8270C 6/28/0,1 20:50 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC INDEN0(1 ,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6/28/01 20:50 HWC ·~·------------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..-.. P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .._ Toll Free Number: t -800/529-6364 .._ Fax: 704/525-0409 • • • Lab Report . ~~!~~- _, ......... "!i1 •. ''i;;"~ ...... Full Service Analytical & Environmental Solutions 7/12/01 Page 6 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-2 PO Box 669004 Prism Sam ole ID: AC11544 Charlotte, NC 28266 Looin Group: 1695H18 Sample Collection Date/Time: 6/26/01 09:50 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST METALS DIGESTION/3030C Completed 3030C 6/27/01 09:30 LC2 SILVER, TOTAL, IN GROUNDWATER Less than mg/L 0.018 6010 6/27/01 20:43 MSC MERCURY DIGESTION Completed EPA 245.1 7/2101 09:30 LC2 PREP. METHOD 3510 Completed SW846-3510 6/28/01 08:00 JDP 'lEAD, TOTAL IN GROUNDWATER 0.067 mg/L 0.015 SW846-Q010B 6/27/01 20:43 MSC ANTIMONY, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-6010B 6/27/01 20:43 MSC ARSENIC, TOTAL IN GROUNDWATER 0.013 mg/L 0.010 SW846-Q01 OB 6/27/01 20:43 MSC BERYlLIUM; TOTAL.IN GROUNDWATER· 0.008 mg/L 0.002 SW846-6010B 6/27/01 20:43 MSC CADMIUM, TOTAL IN GROUNDWATER 0.006 mg/L 0.005 SW846-601 OB 6/27/01 20:43 MSC, CHROMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-601 OB . 6/27/01 20:43 MSC COPPER, TOTAL IN GROUNDWATER Less than mg/L 1.0 SW846-60) OB 6/27/01 20:43 MSC NICKEL, TOTAL IN GROUNDWATER Less than mg/L 0.10 SW846-601 OB 6/27/01 20:43 MSC SELENIUM, TOTAL IN GROUNDWATER Less than mg/L 0.01 SW846-6010B 6/27/01 20:43 MSC THALLIUM, TOTAL IN GOUNDWATER Less than mg/L 0.05 SW846-Q010B 6/27/01 20:43 MSC ZINC, TOTAL IN GROUNDWATER Less than mg/L 2.0 SW846-6010B 6/27/01 20:43 MSC MERCURY, TOTAL IN GROUNDWATER Less than mg/L 0.0002 SW846-7470 7/3/0113:33 PRF BENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 14:26 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP CHLORODIBROMOMETHANE . Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 6/29/01 14:26 MP CHLOROFORM Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP CHLOROMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 14:26 MP NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .a.. P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ~Toll Free Number: l-800/529-6364 ~ Fax: 704/525-0409 • • • Lab Report ~ f.!!~Mc. .,....,~.~::;;.,..:: Full Service Analytical & Environmental Solutions 7/12/01 Page 7 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-2 PO Box 669004 Prism Sample 10: AC11544 Charlotte, NC 28266 LoQin Group: 1695H1B Sample Collection Date/Time: 6/26/01 09:50 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNIT§ LIMIT REFE.RENCE STARTED ANALYST 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-B260B 6/29/01 14:26 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 6/29/01 14:26 MP 1 ,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 14:26 MP 1 ,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 14:26 MP 1 ,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 14:26 MP 1.4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 14:26 MP 1.1-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP 1,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP 1.1-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP CIS-1.2-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP TRANS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/29/01 14:26 MP 1.2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP 1,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 14:26 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 14:26 MP P-ISOPROPYLTOLUENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 6/29/01 14:26 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 6/29/01 14:26 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP STYRENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP 1,1, 1,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP TETRACHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29/01 14:26 MP TOLUENE Not detected ug/L 5.0 SW846-82608 6/29/01 14:26 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road..-.. P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o.. Toll Free Number: l-800/529-6364 ..o.. Fax: 704/525-0409 Lab Report ~~~!! • • • Full Service Analytical & Environmental Solutions 7/12/01 Page 8 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-2 PO Box 669004 Prism Sample 10: AC11544 Charlotte, NC 26266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 09:50 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST ·--·-----·---.... 1 ,2,3-TRICHLOROBENZENE Not detected . u9/L 5.0 SW846-82608 6129101 14:26 MP 1 ,2,4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6129101 14:26 MP 1,1, 1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29101 14:26 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6129101 14:26 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6129101 14:26 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 6129101 14:26 MP 1 ,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6129101 14:26 MP 1 ,2,4-TRIMETHYLBENZEN E Not detected ug/L 5.0 SW846-82608 6129/01 14:26 MP. 1 ,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6129101 14:26 MP VINYL CHLORIDE Not detected · ug/L 10 SW846-82608 6/29101 14:26 MP TOTAL XYLENES Not detected ug/L 5,0 SW846-8260B 6129/01 14:26 MP cis-1 ,3-DICHLDROPROPENE Not detected ug/L 5.0 SW846-82608 6129101 14:26 MP trans-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 6129101 14:26 MP ACETONE Not detected ug/L 50 SW846-82608 6129101 14:26 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-82608 6129101 14:26 MP CARBON DISULFIDE Not detected ug/L 50 SW846-82608 6129/01 14:26 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-82608 6129101 14:26 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-82608 6/29/01 14:26 MP 2-HEXANONE Not detected ug/L 10 SW846-82608 6/29/01 14:26 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-82608 6/29/01 14:26 MP ---------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC PHENOL Not detected ug/L 10 SW846-8270C 6/28101 16:26 HWC 1 ,3-DICHLOROBENZENE Not detected · ug/L 10 SW846-8270C 6/28/01 16:26 HWC 1 ,2-DICHLOROBENZENE . Not detected ug/L 10 SW846-8270C . 6/28/01 16:26 HWC 1 ,4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. EB7519 449 Springbrook Road ..._ P.O. Box 240543 ..._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ..._ Toll Free Number: 1-800/529-6364 ..._ Fnx: 704/525-0409 • • • Lab Report -~-~ !:!!~~-,..,e,~. . Full Service Analytical & Environmental Solutions 7/12/01 Page 9 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-2 PO Box 669004 Prism Samole ID: AC11544 Charlotte, NC 28266 Looin Group: 1695H18 Sample Collection Date/Time: 6/26/01 09:50 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED . ANALYST N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 .SW846-8270C 6/28/01 16:26 HWC ISOPHORONE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/28/01 16:26 HWC 2.4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC· BIS(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 1.2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC HEXACHLOROBUTADIENE Not detected . ug/L 10 SW846-8270C 6/28/01 16:26 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 4-CHLOR0-3-METHYL PHENOL Not detected · ug/L 10 SW846-8270C 6/28/01 16:26 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 2,4.6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 2.4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC ACENAPHTHYLENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 2.6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 2.4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 2.4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6/28/01 16:26 HWC 2.4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC FLUORENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/28/01 16:26 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o. Toll Free Number: 1-800/529-6364 ..o. Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project ID: Customer Sample ID: Prism Sample ID: LoQin Group: Sample Collection Date/Time: Lab Submittal Date/Time: Full Service Analytical & Environmental Solutions Page 10 of 67 Cherokee-Mooresville Site MW-2 AC11544 1695H18 6/26/01 09:50 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYS"[ 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 16:26 HWC ANTHRACENE Not detected ug/L 10 -SW846-8270C 6128101 16:26 HWC DI-N-BUTYL PHTHALATE Not -detected ug/L 10 SW846-8270C 6128/01 16:26 HWC FLUORANTHENE Not detected ug/L 10 SW846-8270C 6128101 16:26 HWC PYRENE Not detected ug/L 10 SW846-8270C 6128101 16:26 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28101 16:26 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6128101 16:26 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6128/01 16:26 HWC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/L 10 SW846-8270C 6128101 16:26 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6128101 16:26 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/28101 16:26 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6128/01 16:26 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6128/01 16:26 HWC INDEN0(1 ,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6128101 16:26 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846-8270C 6128101 16:26 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6128/01 16:26 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6128/01 16:26 HWC ··-------- Sample Comments: NC Certification No. 402 -SC Certification No. 99012 -NC Orinkinq Water Cert. No. 37735 FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 ... Charlotte, NC 28224MOS43 Phone: 704/529-6364 ...._ Toll Free Number: l-800/529-6364 ...._ Fax: 704/525-0409 • • • Lab Report ~ .,~ PR .. :. LABORA!~Mc. ~~ Full Service Analytical & Environmental Solutions 7/12/01 Page 11 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-3 PO Box 669004 Prism Samole 10: AC11545 Charlotte, NC 28266 LoQin Group: 1695H18 Sample Collection Date/Time: 6/26/01 15:10 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST METALS DIGESTION/3030C Completed 3030C 6/27/01.09:30 LC2 SILVER. TOTAL, IN GROUNDWATER Less than mg/L 0.018 6010 6/27/01 20:48 MSC MERCURY DIGESTION Completed EPA 245.1 7/2101 09:30 LC2 PREP. METHOD 3510 Completed SW846-3510 6/28/01 08:00 JDP LEAD. TOTAL IN GROUNDWATER 0.12 mg/L O.D15 SW846-601 OB 6/27/01 20:48 MSC ANTIMONY. TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-601 OB 6/27/01 20:48 MSC ARSENIC, TOTAL IN GROUNDWATER 0.044 mg/L 0.010 SW846-601 OB 6/27/01 20:48 MSC BERYLLIUM. TOTAL IN GROUNDWATER 0.005 mg/L · 0.002 SW846-6010B 6/27/01 20:48 MSC CADMIUM. TOTAL IN GROUNDWATER Less than mg/L 0.005 SW846-601 OB 6/27/01 20:48 MSC CHROMIUM. TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-601 OB 6/27101 20:48 MSC COPPER. TOTAL IN GROUNDWATER Less than mg/L '1.0. SW846-6010B 6/27/01 20:48 MSC NICKEL, TOTAL IN GROUNDWATER Less than mg/L 0.10 SW846-6010B 6/27/01 20:48 MSC SELENIUM. TOTAL IN GROUNDWATER Less than mg/L 0.01 SW846-6010B 6/27/01 20:48 MSC THALLIUM, TOTAL IN GOUNDWATER Less than mg/L 0.05 SW846-601 OB 6/27/01 20:48 MSC ZINC, TOTAL IN GROUNDWATER Less than mg/L 2.0 SW846-601 OB 6/27/01 20:48 MSC . MERCURY, TOTAL IN GROUNDWATER Less than mg/L 0.0002 SW846-7470 7/6/01 17:29 PRF BENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 15:22 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 6/29/01 15:22 MP CHLOROFORM Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP CHLOROMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 15:22 MP -NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road A. P.O. Box 240543 ... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..._Toll Free Number: 1-800/529-6364 ..._Fax: 704/525-0409 • • • Lab Report ~· PRISM. LABORATORIES, INC. -dT~ Full Service Analytical & Environmental Solutions 7/12/01 Page 12 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-3 PO Box 669004 Prism Sample 10: AC11545 Charlotte, NC 28266 Looin Group: 1695H18 Sample Collection Date/Time: 6/26/01 15:10 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 6129/01 15:22 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 6/29101 15:22 MP 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 6129101 15:22 MP 1,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-82608 6129/01 15:22 MP DIBROMOMETHANE Not detected ug/L . 5.0 SW846-82608 6129/01 15:22 MP 1,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP 1,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP 1,4-DICHLOROBENZENE Not detected ug/L 5.0 . SW846-82608 6129101 15:22 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-82608 6129101 15:22 MP 1,1-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP 1,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP 1,1-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP CIS-1,2,DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP TRANS-1,2-DICH LOROETHEN E Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP 1,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6129/01 15:22 MP 1,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6/29101 15:22 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-82608 6/29101 15:22 MP ISOPROPYLBENZENE Not detected ug/L 5.0 .SW846-82608 6129101 15:22 MP P-ISOPROPYL TOLUENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP STYRENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP 1,1,1,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP 1,1,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP TETRACHLOROETHENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP TOLUENE Not detected ug/L 5.0 SW846-82608 6129101 15:22 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .., P.O. Box 240543 .., Charlotte, NC 28224-0543 Phone: 704/529-6364 .., Toll Free Number: l-800/529-6364 .., Fax: 704/525-0409 • • • Lab Report ""A.~~ Full Service Analytical & Environmental Solutions 7/12/01 Page 13 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-3 PO Box 669004 Prism Samole ID: AC11545 Charlotte, NC 28266 Looin Group: 1695H18 Sample Collection Date/Time: 6/26/01 15:10 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE . STARTED ANALYST 1 ,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP 1 ,2,4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP - 1, 1, 1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 15:22 MP 1,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 sw 846-8260B 6/29/01 15:22 MP 1 ,2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP 1 ,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 6/29/01 15:22 MP TOTAL XYLENES. Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP cis-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP trans-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP ACETONE Not detected ug/L 50 SW846-8260B 6/29/01 15:22 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-8260B 6/29/01 15:22 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 6/29/01 15:22 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 6/29/01 15:22 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 6129101 15:22 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 6129101 15:22 MP 4-METHYL-2-PENTANONE (MIBK) Not detected . ug/L 10 SW846-8260B 6129101 15:22 MP --------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6128/01 20:02 HWC PHENOL Not detected ug/L 10 SW846-8270C 6128101 20:02 HWC 1 ,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6128101 20:02 HWC 1 ,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/28101 20:02 HWC 1 A-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC 81$(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC 2-METHYL PH~NOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6128101 20:02 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6128/01 20:02 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .., P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364.., Toll Free Number: 1-800/529-6364..,. Fax: 704/525-0409 Lab Report • • • 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 14 of 67 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: MW-3 Prism Sample ID: AC11545 Loqin Group: 1695H 18 Sample Collection Date/Time: 6/26/01 15:10 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST PARAMETER RESULT ---------""~"------ N-NITROSO-DI-N-PROPYLAMINE NITROBENZENE 4-METHYL PHENOL (P CRESOL) ISOPHORONE -2-NITROPHENOL 4-NITROPHENOL 2,4 DIMETHYL PHENOL BIS(2-CHLOROETHOXY)METHANE 1,2,4 TRICHLOROBENZENE NAPHTHALENE HEXACHLOROBUTADIENE 2-METHYL NAPHTHALENE 4-CHLOR0-3-METHYL PHENOL HEXACHLOROCYCLOPENTADIENE 2,4,6 TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2,4,5 TRICHLOROPHENOL ACENAPHTHYLENE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE 2,4-DICHLOROPHENOL ACENAPHTHENE DIBENZOFURAN 2,4 DINITROPHENOL 2,4 DINITROTOLUENE FLUORENE 4-CHLOROPHENYL PHENYL ETHER DIETHYL PHTHALATE 4,6-DINITR0-2-METHYL PHENOL N-NITROSODIPHENYLAMINE Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detecied Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected REPORTING METHOD DATEfTIME UNIT'-'S,__ __ ,LI,M,_,IT ___ _cR,E"'F"ER,_E"'N"'C_,E,c_____,S,_,T_,A"'R-"TE,_,D,_ ug/L. ug/L ug/L ug/L ug/L_ ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 10 10 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 50 10 10 10 10 50 10 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28101 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6128/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 SW846-8270C 6/28/01 20:02 ANALYST HWC HWC HWC HWC HWC- HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC NC Certification No. 402 SC Cert~ication No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ~ P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 .o.. Toll Free Number: 1-800/529-6364 .o.. Fax: 704/525-0409 Lab Report • • • 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 15 of 67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-3 Prism Sample 10: AC11545 Loqin Group: 1695H18 Sample Collection Daterrime: 6/26/01 15:10 Lab Submittal Datemme: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 Hwc- FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC PYRENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC INDEN0(1 ,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6/28/01 20:02 HWC ----------------· Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..o. P.O. Box 240543 ..o. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o. Toll Free Number: t -800/529-6364 ..., Fax: 704/525-0409 Lab Report PRISM. ~ . • • • LABORATORIES, INC. ~ Full Service Analytical & Environment~! Solutions 7/12/01 Page 16 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Clift Lundgren Customer Sample 10: MW-4 PO Box 669004 Prism Samole 10: AC11546 Loqin Group: 1695H18 Charlotte, NC 28266 Sample Collection Date/Time: 6/26/01 11:10 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST METALS DIGESTIONI3030C Completed 3030C 6127101 09:30 LC2 SILVER, TOTAL, IN GROUNDWATER Less than mg/L 0.018 6010 6127101 20:54 MSC MERCURY DIGESTION Completed EPA 245.1 712101 09:30 LC2 PREP. METHOD 3510 Completed SW846·3510 6128101 16:30 JMK LEAD, TOTAL IN GROUNDWATER 0.072 · mg/L 0.015 SW846·601 OB 6127101 20:54 MSC ANTIMONY, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-601 OB 6127/D1 20:54 MSC ARSENIC, TOTAL IN GROUNDWATER D.D3D mg/L 0.010 SW846-6D10B 6127101 20:54 MSC BERYLLIUM, TOTAL IN GROUNDWATER D.DD3 mg/L 0.002 SW846-6010B 6127101 20:54 MSC CADMIUM, TOTAL IN GROUNDWATER Less than mg/L O.D05 SW846-601 OB 61271D1 20:54 MSC CHROMIUM, TOTAL IN GROUNDWATER 0.095 mg/L O.D5 SW846·6010B 6127101 20:54 MSC COPPER, TOTAL IN GROUNDWATER Less than mg/L 1.D SW846-601 DB 61271D1 20:54 MSC NICKEL, TOTAL IN GROUNDWATER Less than mg/L 0.10 SW846-601 DB 61271D1 2D:54 MSC SELENIUM, TOTAL IN GROUNDWATER Less than ing/L 0.01 SW846-!lD10B 6127101 20:54 MSC THALLIUM, TOTAL IN GOUNDWATER Less than mg/L 0.05 SW846-6010B 6127101 2D:54 MSC ZINC, TOTAL IN GROUNDWATER Less than mg/L 2.0 SW846-6010B 6127101 20:54 MSC MERCURY, TOTAL IN GROUNDWATER Less than mg/L 0.0002 SW846-7470 716/D1 17:33 PRF BENZENE Not detected ug/L 5.0 SW846-826DB 6129101 16:16 MP BROMOBENZENE Not detected ug/L 5.D SW846-826DB 6129/D1 16:16 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6129101 16:16 MP BROMODICHLOROMETHANE Not detected ug/L 5.D SW846-8260B 61291D1 16:16 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 6129/D1 16:16 MP BROMOMETHANE Not detected ug/L 10 SW846-826DB 6129/D1 16:16 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6129101-16:16 MP SEC-BUTYLBENZENE Not detected ug/L 5.D SW846-826DB 6/29/D1 16:16 MP TERT-BUTYLBENZENE Not detected ug/L 5.D SW846-8260B 6129101 16:16 MP CHLOROBENZENE Not detected ug/L 5.D SW846-826DB 6129/D1 16:16 MP CHLORODIBROMOMETHANE Not detected ug/L 5.D SW846-8260B 6129101 16:16 MP CHLOROETHANE Not detected ug/L 10 SW846-826DB 6/291D1 16:16 MP CHLOROFORM Not detected ug/L 5.0 SW846-8260B 6129101 16:16 MP CHLOROMETHANE Not detected ug/L '10 SW846-826DB 6129101 16:16 MP NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 ..._ Fax: 704/525-0409 • • • Lab Report ~~!~M. ··•'P 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 -a:··~...-:~ Full Service Analytical & Environmental Solutions Page 17 of 67 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: MW-4 Prism SamoleiD: AC11546 Loqin Group: 1695H18 Sample Collection DatefTime: 6/26/01 11:10 Lab Submittal DatefTime: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER 2-CHLOROTOLUENE 4-CHLOROTOLUENE 1.2-DIBROM0-3-CHLOROPROPANE 1.2-DIBROMOETHANE DIBROMOMETHANE 1.2-DICHLOROBENZENE 1.3-DICHLOROBENZENE 1.4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1.1-DICHLOROETHANE 1.2-DICHLOROETHANE 1, 1-DICHLOROETHENE CIS-1.2-DICHLOROETHENE TRANS-1.2-DICHLOROETHENE 1.2-DICHLOROPROPANE 1.3-DICHLOROPROPANE 2,2-DICHLOROPROPANE 1, 1-DICHLOROPROPENE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE P-ISOPROPYL TOLUENE METHYLENE CHLORIDE NAPHTHALENE N-PROPYLBENZENE STYRENE 1.1. 1.2-TETRACHLOROETHANE 1.1.2.2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE TEST RESULT Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected UNITS ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L REPORTING METHOD DATE!TIME STARTED LIMIT REFERENCE 5.0 5.0 10 5.0 5.0 5.0 5.0 5.0 10 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 SW846-82608 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-82608 6/29/01 16:16 SWB46-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-82608 6/29/01 16:16 SW846-8260B 6/29/01 16:16 SW846-82608 6/29/01 16:16 ANALYST MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364""" Toll Free Number: 1-800/529-6364""" Fax: 704/525-0409 • • • Lab Report -~~~ Full Service Analytical & Environmental Solutions 7/12/01 Page 18 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-4 PO Box 669004 Prism Sam ole 10: AC11546 Charlotte, NC 28266 Looin Group: 1695H18 Sample Collection Date/Time: 6/26/01 11:10 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 1,2,3-TRICHLOROBENZENE ·Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP 1,2,4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP 1,1,1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP 1,1,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 16:16 MP 1,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP 1,2.4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP 1.3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 6/29/01 16:16 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP cis-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP trans-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP ACETONE Not detected ug/L 50 SW846-8260B 6/29/01 16:16 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-8260B 6/29/01 16:16 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 6/29/01 16:16 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 6/29/01 16:16 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 6/29/01 16:16 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 6/29/01 16:16 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 6/29/01 16:16 MP ---------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 1,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 1,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 1.4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6/29/0116:50 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..o.. P.O. Box 240543 ..o.. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o.. Toll Free Number: l-800/529-6364 ..o.. Fax: 704/525-0409 • • • Lab Report ~PRISM LABORATORIES, INC, ~..,.;til~.;~~ .... ~ . Full Service Analytical & Environmental Solutions 7/12/01 Page 19 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-4 PO Box 669004 Prism Samole ID: AC11546 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 11:10 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME . PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC . ISOPHORONE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 16:50 HWC 2.4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC BIS(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 1 ,2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC HEXACHLOROBUTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW 846-8270C 6/29/01 16:50 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC ACENAPHTHYLENE Nat detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 2.4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 2,4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 16:50 HWC 2.4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC FLUORENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/29/01 16:50 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC NC Certification No. 402 SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..., P.O. Box 240543 ..., Charlotte, NC 28224-0543 Phone: 704/529-6364 ..., Toll Free Number: 1-800/529-6364..., Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full SeNice Analytical & Environmental Solutions Page 20 of 67 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: MW-4 Prism Samcle ID: AC11546 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 11:10 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST ------·--- 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC FLUORANTHENE Not detected ug/L 10 SWB46-8270C 6/29/01 16:50 HWC PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC BIS(2-ETHYLHEXYL)PHTHALA TE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SWB46-8270C 6/29/01 16:50 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SWB46-8270C 6/29/01 16:50 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 16:50 HWC INDEN0(1 ,2,3-C,O)PYRENE Not detected ug/L 10 SWB46-8270C 6/29/01 16:50 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SWB46-8270C 6/29/01 16:50 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-B270C 6/29/01 16:50 HWC PHENANTHRENE Not detected ug/L 10 SWB46-8270C 6/29/01 16:50 HWC --------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .-.. P.O. Box 240543 .-.. Charlotte, NC 28224-0543 Phone: 704/529-6364 ... Toll Free Number: l-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 21 of 67 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: MW-45 Prism Sample ID: AC11547 LoQin Group: 1695H 18 Sample Collection DatefTime: 6/26/01 10:40 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER METALS DIGESTION/3030C SILVER, TOTAL, IN GROUNDWATER MERCURY DIGESTION PREP. METHOD 3510 TEST RESULT Completed Less than Completed Completed LEAD, TOTAL IN GROUNDWATER 0.082 ANTIMONY, TOTAL IN GROUNDWATER Less than ARSENIC, TOTAL IN GROUNDWATER 0.018 BERYLLIUM, TOTAL IN GROUNDWATER 0.004 CADMIUM, TOTAL IN GROUNDWATER 0.018 CHROMIUM, TOTAL IN GROUNDWATER Less than COPPER, TOTAL IN GROUNDWATER Less than NICKEL, TOTAL IN GROUNDWATER Less than THALLIUM, TOTAL IN GOUNDWATER Less than ZINC, TOTAL IN GROUNDWATER Less than SELENIUM, TOTAL IN GROUNDWATER Less than MERCURY, TOTAL IN GROUNDWATER 0.0008 BENZENE Not detected BROMOBENZENE Not detected BROMOCHLOROMETHANE Not detected BROMODICHLOROMETHANE Not detected BROMOFORM Not detected BROMOMETHANE Not detected N-BUTYLBENZENE Not detected SEC-BUTYLBENZENE Not detected TERT-BUTYLBENZENE Not detected CHLOROBENZENE Not detected CHLORODIBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE Nat detected Not detected Not detected Not detected UNITS mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L REPORTING METHOD DATEfTIME STARTED LIMIT REFERENCE 0.018 0.015 0.05 0.010 0.002 0.005 0.05 1.0 0.10 0.05 2.0 0.01 0.0002 5.0 5.0 5.0 5.0 5.0 10 5.0 5.0 5.0 5.0 5.0 10 5.0 10 3030C 6010 EPA 245.1 SW846-3510 6/27/01 09:30 6/27/01 20:59 7/2/01 09:30 6/28/01 16:30 SW846-60108 6/27/01 20:59 SW846-60108 6/27/01 20:59 SW846-60108 6/27/01 20:59 SW846-60108 6/27/01 20:59 SW846-60108 6/27/01 20:59 SW846-60108 6/27/01 20:59 SW846-6010B 6/27/01 20:59 SW846-6010B 6/27/01 20:59 SW846-60108 6/27/01 20:59 SW846-60108 6/27/01 20:59 SW846-60108 6/27/01 20:59 SW846-7470 7/6/01 17:37 SW846-82608 6/29/01 17:00 SW846-82608 6/29/01 17:00 SW846-82608 6/29/01 17:00 SW846-8260B 6/29/01 17:00 SW846-82608 6/29/01 17:00 SW846-8260B 6/29/01 17:00 SW846-82608 6/29/01 17:00 SW846-82608 6/29/01 17:00 SW846-82608 6/29/01 17:00 SW846-82608 6/29/01 17:00 SW846-82608 6/29/01 17:00 SW846-8260B 6/29/01 17:00 SW846-82608 6/29/01 17:00 SW846-82608 6/29/01 17:00 ANALYST LC2 MSC LC2 JMK MSC MSC MSC MSC MSC MSC MSC MSC MSC MSC MSC PRF MP MP MP MP MP MP MP MP MP MP MP MP MP MP NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 ... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..., Toll Free Number: 1-800/529-6364 ..., Fax: 704/525-0409 • • • Lab Report ~r.!!~M. .-oor~ ~.... ... ' . Full Service Analytical & Environmental Solutions 7/12/01 Page 22 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-45 PO Box 669004 Prism Sam ole 10: AC11547 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 10:40 Lab Submittal Date/Time: 6/27/01 07:55 The follow.ing analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMU~~--· RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2·CHLOROTOLUENE Not detected ug/L 5.0 SWB46·8260B 6/29/01 17:00 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 6/29/01 17:00 MP 1.2-DIBROMOETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:00 MP 1,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1 ,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1,4-D.ICHLOROBENZENE Not detected ug/L 5.0 SW846-B2608 6/29/01 17:00 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-82608 6/29/01 17:00 MP 1,1-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6i29/01 17:00 MP 1 ,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1, 1-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:00 MP CIS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP TRANS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1 ,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 . SW846-82608 6/29/01 17:00 MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:00 MP P-ISOPROPYLTOLUENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:00 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 '6/29/01 17:00 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP STYRENE Not detected ug/L 5.0 SWB46-82608 6/29/01 17:00 MP 1,1, 1 ,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1,1,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP TETRACHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:00 MP TOLUENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:00 MP NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..., P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..., Toll Free Number: 1-800/529-6364 ..., Fax: 704/525-0409 • • • Lab Report ,,.~~!~Mo. *''"""""-il-' ./t:> . Full Service Analytical & Environmental Solutions 7/12/01 Page 23 of67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-45 PO Box 669004 Prism Samole 10: AC11547 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 10:40 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 1 .2.3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1 .2.4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1,1. 1 -TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP TRICHLOROETHENE Not detected ug/L 5.0. SW846-82608 6/29/01 17:00 MP .\. TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-82608 6/29/01 17:00 MP 1 .2.3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP 1 ,2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP i.3.5-TRIMETHYLBENZENE Not detected · ug/L 5.0· SW846-82608 6/29/01 17:00 MP VINYL CHLORIDE Not detected ug/L 10 SW846-82608 6/29/01 17:00 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP. cis-1 .3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 6/29/01 17:00 MP trans-1 .3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:00 MP ACETONE Not detected ug/L 50 SW846-82608 6/29/01 17:00 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-82608 6/29/01 17:00 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 6/29/01 17:00 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:00 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 6/29/01 17:00 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 6/29/01 17:00 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 6/29/01 17:00 MP ---------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 1 ,3·DICHLOROBENZENE Nat detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 1 .2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 1.4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..,. P.O. Box 240543 ..,. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..,. Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report ___,~w~~ Fun ·Service Analytical & Environmental Solutions 7/12/01 Page 24 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-4S PO Box 669004 Prism Samcle 10: AC11547 Charlotte, NC 28266 Looin Group: 1695H18 Sample Collection Date/Time: 6/26/01 10:40 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSO·DI·N·PROPYLAMINE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC ISOPHORONE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 4-NITROPHENOL Not detected ug/L 50 SW846·8270C 6/29/01 17:38 HWC 2,4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC BIS(2·CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 1 ,2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC NAPHTHALENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC HEXACHLOROBUTADIENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846·8270C 6/29/0.1 17:38 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC ACENAPHTHYLENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 2,4-DICHLOROPHENOL Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC ACENAPHTHENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC DIBENZOFURAN Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC 2,4 DINITROPHENOL Not detected ug/L 50 . SW846-8270C 6/29/01 17:38 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC FLUORENE Nat detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846·8270C 6/29/01 17:38 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC NC Certification No. 402 • SC Certification No. 99012 • NC Drinkino Water Cert. No. 37735 • FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364.., Toll Free Number: l-800/529·6364.., Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 25 of 67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-45 Prism Sample 10: AC11547 Lopin Group: 1695H18 Sample Collection Date/Time: 6/26/01 10:40 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMEJER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC FLUORANTHENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC PYRENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC CHRYSENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC 815(2-ETHYLHEXYL)PHTHALATE 24 ug/L 10 SW846·8270C 6/29/01 17:38 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 .HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 17:38 HWC INDENO( 1,2,3-C,D)PYRENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC PHENANTHRENE Not detected ug/L 10 SW846·8270C 6/29/01 17:38 HWC ···------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 • SC Certification No. 99012 • NC Drinking Water Cart. No. 37735 • FL Certification No. E87519 449 Springbrook Road ..o.. P.O. Box 240543 ..o.. Charlotte, NC 28224-0543 Phone: 704/529·6364 ..o.. Toll Free Number: 1-800/529-6364 ..o.. Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solut!ons Page 26 of 67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-5 Prism Sample 10: AC11548 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 15:40 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER METALS DIGESTION/3030C SILVER, TOTAL, IN GROUNDWATER MERCURY DIGESTION PREP. METHOD 3510 TEST RESULT Completed Less than Completed Completed LEAD, TOTAL IN GROUNDWATER 0.031 ANTIMONY, TOTAL IN GROUNDWATER Less than ARSENIC, TOTAL IN GROUNDWATER Less than BERYLLIUM, TOTAL IN GROUNDWATER 0.12 CADMIUM, TOTAL IN GROUNDWATER Less than CHROMIUM, TOTAL IN GROUNDWATER Less than COPPER, TOTAL IN GROUNDWATER Less than NICKEL, TOTAL IN GROUNDWATER Less than ZINC, TOTAL IN GROUNDWATER Less than THALLIUM, TOTAL IN GOUNDWATER Less than SELENIUM, TOTAL IN GROUNDWATER Less than MERCURY, TOTAL IN GROUNDWATER Less than BENZENE Not detected BROMOBENZENE Not detected BROMOCHLOROMETHANE Not detected BROMODICHLOROMETHANE Not detected BROMOFORM Not detected BROMOMETHANE Not detected N-BUTYLBENZENE Not detected SEC-BUTYLBENZENE Not detected TERT-BUTYLBENZENE Not detected CHLOROBENZENE Not detected CHLORODIBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE Not dete9ted Not detected Not detected Not detected UNITS mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L REPORTING METHOD DATEfTIME STARTED LIMIT REFERENCE 0.018 0.015 0.05 0.010 0.002 0.005 0.05 1.0 0.10 2.0 0.05 0.01 0.0002 5.0 5.0 5.0 5.0 5.0 10 5.0 5.0 5.0 5.0 5.0 10 5.0 10 3030C 6010 EPA 245.1 SW846-3510 6/27/01 09:30 6/27/01 21:14 7/2/01 09:30 6/28/01 16:30 SW846-6010B 6/27/01 21:14 SW846-6010B 6/27/01 21:14 SW846-6010B 6/27/01 21:14 SW846-6010B. 6/27/01 21:14 SW846-6010B 6/27/01 21:14 SW846-6010B 6/27/01 21:14 SW846-6010B 6/27/01 21:14 SW846-6010B 6/27/01 21:14 SW846-6010B 6/27/01 21:14 SW846-6010B 6/27/01 21:14 SW846-6010B 6/27/01 21:14 SW846-7470 7/6/01 17:41 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-8260B 6/29/01 17:43 SW846-82608 6/29/01 17:43 SW846-82608 6/29/01 17:43 SW846-8260B 6/29/01 17:43 ANALYST LC2 MSC LC2 JMK MSC MSC MSC MSC MSC MSC MSC· MSC MSC MSC MSC PRF MP MP MP MP MP MP MP MP MP MP MP MP MP MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .., P.O. Box 240543 .., Charlotte, NC 28224-0543 Phone: 704/529-6364.., Toll Free Number: t-800/529-6364.., Fax: 704/525-0409 • • • Lab Report FuJI Service Analytical & Environmental Solutions 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Page 27 of 67 Customer Project ID: ·Cherokee-Mooresville Site Customer Sample ID: MW-5 Prism Sample ID: AC11548 LoQin Group: 1695H18 Sample Collection Date/Time: 6/26/01 15:40 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME STARTED PARAM~_,_T,ER"-----,----------'R"'E"'S"'U"'L"-T __ _,_UN'-"1"-T"-S __ _:L,IM,_IT'---'---'R"'E"-'F-"E"'R"'E"'N"'C"'-E 2-CHLOROTOLUENE 4-CHLOROTOLUENE 1 ,2-DIBROM0-3-CHLOROPROPANE 1,2-DIBROMOETHANE DIBROMOMETHANE 1 ,2-DICHLOROBENZENE 1 ,3-DICHLOROBENZENE 1 A-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1, 1-DICHLOROETHANE 1 ,2-DICHLOROETHANE . 1, 1-DICHLOROETHENE CIS-1,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1 ,2-DICHLOROPROPANE 1,3-DICHLOROPROPANE 2,2-DICHLOROPROPANE 1, 1-DICHLOROPROPENE ETHYLBENZENE HEXACHLOROBUTADIENE ISOPROPYLBENZENE P-ISOPROPYL TOLUENE METHYLENE CHLORIDE NAPHTHALENE N-PROPYLBENZENE STYRENE 1,1, 1,2-TETRACHLOROETHANE 1,1 ,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE Not detected Not detected Not detected Not detected · Not detected Not detected Not detected ug/L ug/L ug/L ug/L ug/L ug/L ug/L Not detected : ug/l: Not detected ug/L Not detected ug/L Not detected -ug/L Not detected ug/L Not detected -ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected ug/L Not detected Not detected ug/L ug/L 5.0 5.0 10 5.0 5.0 5.0 5.0 5.0. 10 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-8260B 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-8260B 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-8260B 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-8260B 6129101 17:43 SW846-82608 6129101 17:43 SW846-8260B 6129101 17:43 SW846-8260B 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 SW846-82608 6129101 17:43 ANALYST MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .._ P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364 ""' Toll Free Number: 1-800/529-6364 ""' Fax: 704/525-0409 • • • Lab Report PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions 7112101 Page 28 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-5 PO Box 669004 Prism Sam ole ID: AC11548 Charlotte, NC ·28266 Looin Group: 1695H18 Sample Collection Date/Time: 6126/01 15:40 Lab Submittal Date/Time: 6127101 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 1 ,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:43 MP 1 ,2,4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:43 MP 1,1,1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:43 MP 1,1,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:43 MP TRICHLOROETHENE · Not detected ug/L 5.0 SW846-8260B 6f29/01 17"1! MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 17:43 MP 1,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:43 MP 1 ,2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01.17:43 MP 1,3,5-TRIMETHYLBENZENE . Not detected ug/L 5.0 sw 846-8260B 6/29/01 17:43 MP VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 6/29/01 17:43 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-8260B 6/29/01 17:43 MP. cis-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:43 MP trans-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/29/01 17:43 MP ACETONE Not detected ug/L 50 SW846-8260B 6/29/01 17:43 MP 2-BUTANONE (MEK) Not detected .ug/L 10 SW846-8260B 6/29/01 17:43 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 6/29/01 17:43 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 sw 846-8260B 6/29/01 17:43 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 6/29/01 17:43 MP 2-HEXANONE Not detected ug/L 10 SW 846-8260B 6/29/01 17:43 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 6/29/01 17:43 MP ---------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC PHENOL Not detected ug/L 10 SW 846-8270C 6/29/01 18:27 HWC 1,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 1,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 1 A-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: t-800/529-6364.., Fax: 704/525-0409 • • • Lab Report ~A~A! Fu!l Service Analytical & Environmental Solutions 7/12/01 Page 29 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-5 PO Box 669004 Prism Sample ID: AC11548 Charlotte, NC 28266 l.ooin Group: 1695H18 Sample Collection Date/Time: 6/26/01 15:40 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErriME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC ISOPHORONE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 18:27 HWC 2,4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC BIS(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 1,2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC HEXACHLOROBUTADIENE Not detected ug/L 10 SW84S-8270C 6/29/01 18:27 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 -SW846-8270C 6/29/01 18:27 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 _18:27 HWC ACENAPHTHYLENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 2,4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 2,4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 18:27 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC FLUORENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C · 6/29/01 18:27 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/29/01 18:27 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road _.. P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364.., Toll Free Number: 1-800/529-6364.., Fax: 704/525-0409 • • • Lab Report ... 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Samole 10: LoQin Group: Sample Collection DatefTime: Lab Submittal DatefTime: Full Service Analytical & .Env\ronmental Solutions Page 30 of 67 Cherokee-Mooresville Site MW-5 AC11548 1695H18 6/26/01 6/27/01 15:40 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC DI-N-BUTYL PHTHALATE Not detected · ug/L 10 SW846-8270C 6/29/01 18:27 HWC FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC . BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C · 6/29/01 18:27 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC BIS(2-ETHYLHEXYL)PHTHALA TE Not detected ug/L 10 SW846-8270C. 6/29/01 18:27 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC INDEN0(1 ,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6/29101 18:27 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6/29/01 18:27 HWC ---------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ... Toll Free Number: l-800/529-6364 ... Fax: 704/525-0409 Lab Report PRISM LABORATORIES, INC. • Full Service Analytical & Environmental Solutions 7/12/01 Page 31 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-6 PO Box 669004 Prism Samole 10: AC11549 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 16:00 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST METALS DIGESTION/3030C Completed 3030C 6/27/01 09:30 LC2 SILVER, TOTAL, IN GROUNDWATER Less than mg/L 0.018 6010 6/27/01 21:20 MSC MERCURY DIGESTION Completed EPA 245.1 7/2/01 09:30 LC2 PREP. METHOD 3510 Completed SW846-3510 6/28/01 16:30 JMK -LEAD, TOTAL IN GROUNDWATER 0.031' mg/L 0.015. SW846-601 OB 6/27/01 21:20 MSC ANTIMONY, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-601 OB 6/27/01 21:20 MSC ARSENIC, TOTAL IN GROUNDWATER 0.027 mg/L 0.010 SW846-601 OB 6/27/01 21:20 MSC • BERYLLIUM, TOTAL IN GROUNDWATER 0.003 . mg/L 0.002 SW846-6010B 6/27/01 21:20 MSC CADMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.005 SW846-6010B 6/27/01 21:20 MSC CHROMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-6010B 6/27/01 21:20 MSC COPPER, TOTAL IN GROUNDWATER Less than mg/L 1.0 SW846-601 OB 6/27/01 21:20 MSC NICKEL, TOTAL IN GRO.UNDWATER Less than mg/L 0.10. SW846-6010B 6/27/0121:20 MSC ZINC, TOTAL IN GROUNDWATER Less than mg/L 2.0 SW846-6010B 6/27/01 21:20 MSC THALLIUM, TOTAL IN GOUNDWATER Less than mg/L 0.05 SW846-6010B 6/27/01 21:20 MSC SELENIUM, TOTAL IN GROUNDWATER Less than mg/L 0.01 SW846-6010B 6/27/01 21:20 MSC MERCURY, TOTAL IN GROUNDWATER Less than mg/L 0.0002 SW846-7470 7/6/01 17:45 PRF BENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP BROMDMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 18:27 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP CHLDRODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP • CHLOROETHANE Not detected ug/L 10 SW846-8260B 6/29/01 18:27 MP CHLOROFORM Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP CHLOROMETHANE Not detected ug/L 10 SW646-8260B 6/29/01 18:27 MP NC Certification No. 402 • SC Certification No. 99012 • NC DrinkinQ Water Cert. No. 37735 • FL Certification No. EB7519 449 Springbrook Road ..a.. P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report '· PRISM LABORATORIES; IN~. Full Service Analytical & Environmental Solutions 7/12/01 ·Page 32 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-6 PO Box 669004 Prism Sam ole 10: AC11549 Charlotte, NC 28266 LoQin Group: 1695H18 Sample Collection Date/Time: 6/26/01 16:00 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the.indicated sample which was submitted to this laboratory: TEST. TEST REPORTING METHOD DATE/TIME PARAMETER --__ , ____ , ___ ~-----RESULT .UNITS LIMIT REFERENCE STARTED ANALYSe 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 6/29/01 18:27 MP 1,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-82608 6/29101 18:27 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP 1,2-DICHLOROBENZENE NOt detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP 1 ,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP 1,4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 'MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-82608 6/29/01 18:27 MP 1, 1-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP 1,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP 1.1-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP · CIS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 • 6/29/01 18:27 MP TRANS-1, 2-DICH LOROETHENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP 1 ,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846·82608 6/29/01 18:27 MP 1,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6/29/01 .18:27 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846·82608 6/29/01 18:27 MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP P-I SO PROPYL TOLUENE Not detec_ted ug/L 5.0 SW846·82608 6/29/01 18:27 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP STYRENE Nat detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP 1,1, 1,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP 1,1,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP TETRACHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/29/01 18:27 MP TOLUENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 ...-. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: l-800/529-6364 ....,. Fax: 704/525-0409 • • • Lab Report .PRISM LABORATORIES, INC. Ful! Service Analytical & Environmental Solutions 7/12/01 Page 33 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-6 PO Box 669004 Prism Samole 10: AC11549 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 16:00 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS . LIMIT REFERENCE STARTED ANALYST 1,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP 1,2,4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP 1,1, 1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP TRICHLOROETHENE Not detected · . ug/L 5.0 SW846-8260B 6/29101 18:27 . MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 6/29/01 18:27 MP 1,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP 1,2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP 1,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 6/29/01 18:27 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP Cis-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27 MP trans-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6129/01 18:27 MP ACETONE Not detected ug/L 50 SW846-8260B 6/29/01 18:27 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-8260B 6/29/01 18:27 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 6/29/01 18:27 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 6/29/01 18:27-MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 6/29/01 18:27 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 6/29/01 18:27 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 6/29101 18:27 MP ---------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 1,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 1,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 1 ,4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364..., Toll Free Number: l-800/529-6364..., Fax: 704/525-0409 • • • Lab Report ~PRISM LABORATORIES, INC. ~.¥~~ Full Service Analytical & Environmental Solutions 7/12/01 Page 34 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-6 PO Box 669004 Prism Sam ole 10: AC11549 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date!Time: 6/26/01 16:00 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for.the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC ISOPHORONE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 19:15 HWC 2,4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 815(2-CHLOROETHOXY)METHANE · Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 1,2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC HEXACHLOROBUTADIENE Not detected .ug/L 10 SW846-8270C 6/29/01 19:15 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC HEXACHLOROCYCLOPENTADIENE. Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC ACENAPHTHYLENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 2,4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/29/0119:15 HWC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 2,4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 19:15 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC FLUORENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/29/01 19:15 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road...._ P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: l-800/529-6364 ..., Fax: 704/525-0409 Lab Report • • • 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 35 of 67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-6 Prism Samole 10: AC11549 Loqin Group: 1695H 18 Sample Collection Date/Time: 6/26/01 16:00 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYS' 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C .. 6/29/01 19:15 HWC FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC BIS(2-ETHYLHEXYL)PHTHALA TE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC INDEN0(1,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6/29/01 19:15 HWC ---------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364.-.. Toll Free Number: 1-800/529-6364 ....._Fax: 704/525-0409 • • • Lab Report '~~!~Mo. ~_;.:i:.:.<.._,b Fun Service Analytical & Environmental Solutions 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Page 36 of 67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-7/( Prism Sample 10: AC11550 LoQin Group: 1695H18 Sample Collection Date/Time: 6/26/01 14:35 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME STARTED -'P'-'A_,R_,A_,M,E:T.c;E,_R,_ ________ -'R_,E~S,.,U,.,L"-T __ __,UecN"-IT,_,S-_ __ LIMIT REFERENCE METALS DIGESTION/3030C SILVER, TOTAL, IN GROUNDWATER TICs BY SEMIVOLATILE GC/MS Completed Less than mg/L 0.018 625/8270 Tentatively Identified Compounds (lO-largest TICs): <Identification Class> <Closest Spectral Fit> ================================= ====================== Unknown (Unknown) MERCURY DIGESTION PREP. METHOD 3510 Completed Completed LEAD, TOTAL IN GROUNDWATER 0.12 ANTIMONY, TOTAL IN GROUNDWATER Less than ARSENIC, TOTAL IN GROUNDWATER 0.016 BERYLLIUM, TOTAL IN GROUNDWATER 0.026 CADMIUM, TOTAL IN GROUNDWATER Less than CHROMIUM, TOTAL IN GROUNDWATER Less than COPPER, TOTAL IN GROUNDWATER Less than NICKEL, TOTAL IN GROUNDWATER Less than SELENIUM, TOTAL IN GROUNDWATER Less than THALLIUM, TOTAL IN GOUNDWATER Less than ZINC, TOTAL IN GROUNDWATER Less than MERCURY, TOTAL IN GROUNDWATER Less than BENZENE Not detected BROMOBENZENE Not detected BROMOCHLOROMETHANE Not detected BROMODICHLOROMETHANE Not detected BROMOFORM Not detected BROMOMETHANE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE Not detected Not detected Not detected Noi detected mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 0.015 0.05 0.010 0.002 0.005 0.05 1.0 0.10 0.01 0.05 2.0 0.0002 5.0 5.0 5.0 5.0 5.0 10 5.0 5.0 5.0 3030C 6010 625/8270 <Est. Cone.> ============ 87 ug/L EPA 245.1 SW846-3510 6/27/01 09:30 6/27/01 21:25 6/29/01 20:03 7/2/01 09:30 6/28/01 16:30 SW846-6010B 6/27/01 21:25 SW846-6010B 6/27/01 21:25 SW846-6010B 6/27/01 21:25 SW846-60108 6/27/01 21:25 SWB46-6010B 6/27/01 21:25 SW846-60108 6/27/01 21:25 SW846-6010B 6/27/01 21:25 SWB46-6010B 6/27/01 21:25 SW846-Q0108 6/27/01 21:25 SWB46-6010B 6/27/01 21:25 SW846-6010B 6/27/01 21:25 SWB46-7470 7/6/0117:49 SW846-B2608 6/29/01 19:11 SW846-B260B 6/29/01 19:11 SWB46-8260B 6/29/0119:11 SWB46-8260B 6/29/01 19:11 ' S W846-8260B 6/29/01 19:11 SW846-8260B 6/29/01 19:11 SWB46-8260B 6/29/01 19:11 SWB46-8260B 6/29/01 19:11 SW346-8260B 6/29/01 19:11 ANALYST LC2 MSC HWC LC2 JMK MSC MSC MSC MSC MSC MSC MSC MSC MSC MSC MSC PRF MP MP MP MP MP MP MP MP MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 ...... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o. Toll Free Number: t -800/529-6364 ..o. Fax: 704/525-0409 • • • Lab Report -<~!'.!IJ~ Full Service Analytical & Environmental Solutions 7/12/01 Page 37 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-7/f PO Box 669004 Prism Sample ID: AC11550 Charlotte, NC 28266 Looin Group: 1695H18 Sample Collection Date/Time: 6/26/01 14:35 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6129101 19:11 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 6/29/01 19:11 MP CHLOROETHANE Not detected ug/L 10 SW846-82608 6129101 19:11 MP CHLOROFORM Not detected ug/L 5.0 SW846-8260B 6129101 19:11 MP CHLOROMETHANE Not detected ugll 10 SW846-8260B 6129101 19:11 MP 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 6129101 19:11 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846·82608 6129101 19:11 MP 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 612910119:11 MP 1,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-82608 6129101 19:11 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846·8260B 6/29101 19:11 MP 1,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846·8260B 612910119:11 MP 1,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6129101 19:11 MP 1,4-DICHLOROBENZENE Not detected ug/L 5.0 SW846·8260B 612910119:11 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-82608 612910119:11 MP 1,1-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6129101 19:11 MP 1,2-DICHLOROETHANE Not detected ug/L 5.0 SW846·82608 612910119:11 MP 1,1-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6/29101 19:11 MP CIS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 6129101 19:11 MP TRANS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SWB46·8260B 6/29101 19:11 MP 1,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 612910119:11 MP 1,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6129101 19:11 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SWB46·82608 6129101 19:11 MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 6/29101 19:11 MP ETHYLBENZENE Not detected ug/L 5.0 SWB46·82608 612910119:11 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SWB46-82608 6129101 19:11 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-82608 6/29101 19:11 MP P-ISOPROPYL TOLUENE Not detected ug/L 5.0 SW846·8260B 6129101 19:11 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 6129101 19:11 MP NAPHTHALENE Not detected ug/L 5.0 SW846·82608 6129101 19:11 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 612910119:11 MP NC Certification No. 402 • SC Certification No. 99012 • NC DrinkinQ Water Cert. No. 37735 . FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: t-800/529-6364 ..... Fax: 704/525-0409 • • • Lab Report --~f.!!~M. .:-rt"l·., X "', ~ .<?::> . Full ServiCe Analytical & Environmental Solutions 7/12/01 Page 38 of67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Clift Lundgren Customer Sample 10: MW-7/{ PO Box 669004 Prism Samole 10: AC11550 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 14:35 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST STYRENE Not detected ug/L 5.0 SW846-8260B 6129101 19:11 MP 1, 1,1 ,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846·8260B 6129101 19:11 MP 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6129101 19:11 MP TETRACHLOROETHENE Not detected ug/L 5-Q SW846·8260B 6129101 19:11 MP TOLUENE Not detected ug/L 5.0 SW846-8260B 612910119:11 MP 1,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SWB46-8260B 6129101 19:11 MP 1, 2.4· TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6129/01 19:11 MP 1, 1, 1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-B260B 6129101 19:11 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6129101 19:11 MP TRICHLOROETHENE Not detected ug/L 5-Q SW846·8260B 6129101 19:11 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846·8260B 6129101 19:11 MP 1 ,2,3-TRICHLOROPROPANE Not detected ug/L 5-Q SWB46-8260B 612910119:11 MP 1 ,2,4-TRIMETHYLBENZENE 7.1 ug/L 5-Q SW846-8260B 612910119:11 MP 1 ,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 6129101 19:11 MP VINYL CHLORIDE Not detected ug/L 10 SW846-82608 6129101 19:11 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-8260B 6129101 19:11 MP cis-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846·8260B 6/29101 19:11 MP trans-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846·8260B 6/29101 19:11 MP ACETONE Not detected ug/L 50 SW846-8260B 612910119:11 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846·8260B 6129101 19:11 MP CARBON DISULFIDE Not detected ug/L 50 SW846·8260B 6129101 19:11 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846·8260B 612910119:11 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846·8260B 6129101 19:11 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 6129101 19:11 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846·8260B 6129101 19:11 MP --------- 2-CHLOROPHENOL Not detected ug/L 10 SWB46-8270C 6129101 20:03 HWC BIS(2·CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6129101 20:03 HWC PHENOL Not detected ug/L 10 SW846-8270C 6129101 20:03 HWC 1 ,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6129/01 20:03 HWC NC Certification No. 402 • SC Certification No. 99012 • NC Drinkinq Water Cert. No. 37735 • FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: t-800/529-6364 ...._Fax: 704/525-0409 Lab Report -~~!\! ~~~ • Full Service Analytical & Environmental Solutions 7/12/01 Page 39 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-7/( PO Box 669004 Prism Sample 10: AC11550 Charlotte, NC 28266 Loain Group: 1695H18 Sample Collection Date/Time: 6/26/01 14:35 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 1 ,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 1 ,4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 815(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC • ISOPHORONE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 20:03 HWC 2,4 DIMETHYL PHENOL Not detected ug/L 10 SW 846-8270C 6/29/01 20:03 HWC BIS(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 1 ,2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC HEXACHLOROBUTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 2-CHLORONAPHTHALENE Nat detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC ACENAPHTHYLENE Nat detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 2,4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC ACENAPHTHENE Not detected ug/L 10 SW 846-8270C 6/29/01 20:03 HWC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC • 2,4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 20:03 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224·0543 Phone: 704/529-6364 ...._Toll Free Number: l-800/529-6364 ..... Fax: 704/525-0409 • • • Lab Report PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions 7/12/01 Page 40 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-71( PO Box 669004 Prism Sam ole 10: AC11550 Charlotte, NC 28266 LoQin Group: 1695H18 Sample Collection DatefTime: 6/26/01 14:35 Lab Submittal DatefTime: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOO DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST FLUORENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/29/01 20:03 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC HEXACHLOROBENZENE Not detected ug/L 10 SWB46-8270C 6/29/01 20:03 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C · 6/29/01 20:03 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC BIS(2-ETHYLHEXYL)PHTHALA TE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC INDEN0(1,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SWB46-8270C 6/29/01 20:03 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6/29/01 20:03 HWC ---------- NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..., P.O. Box 240543 ..., Charlotte, NC 28224-0543 Phone: 704/529-6364 ..., Toll Free Number: 1-800/529-6364 ..., Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page 41 of 67 Customer Project 10: Cherokee-Mooresville Site ... Customer Sample 10: MW-7/( Prism Samole 10: AC11550 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 14:35 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER Sample Comments: TEST RESULT REPORTING METHOD UNITS LIMIT REFERENCE This report is a revision and supersedes our original laboratory report dated 7/11/01. Angela D . DATE/TIME STARTED ANALYST NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ......_ P.O. Box 240543 ._ Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: l-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report ,.,,~~!~Mo. ~;..t:.t:l!.l.Ui...;.,.~ Full Service Analytical & Environmental Solutions 7/12/01 Page 42 of67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-8 PO Box 669004 Prism Sam ole 10: AC11551 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 14:15 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST METALS DIGESTION13030C Completed 3030C 6127101 09:30 LC2 SILVER. TOTAL. IN GROUNDWATER Less than mg/L 0.018 6010 6127101 21:30 MSC MERCURY DIGESTION Completed EPA 245.1 71210110:40 LC2 PREP. METHOD 3510 Completed SW846-3510 6128101 16:30 JMK LEAD. TOTAL IN GROUNDWATER 0.028 mg/L 0.015 SW846-6010B 6127101 21:30 MSC ANTIMONY. TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-6010B 6127101 21:30 MSC ARSENIC. TOTAL IN GROUNDWATER 0.013 mg/L 0.010 SW846-6010B 6127101 21:30 MSC · BERYLLIUM. TOTAL IN GROUNDWATER 0.008 mg/L 0.002 SW846-601 OB 6127101 21:30 . MSC CADMIUM. TOTAL IN GROUNDWATER Less than mg/L 0.005 SW846-601 OB 6127101 21:30 MSC CHROMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-Q010B 6127101 21:30 MSC COPPER. TOTAL IN GROUNDWATER Less than mg/L 1.0 SW846-Q010B 6127101 21:30 MSC NICKEL. TOTAL IN GROUNDWATER Less than mg/L 0.10 SW846-6010B 6127101 21:30 MSC SELENIUM. TOTAL IN GROUNDWATER Less than mg/L 0.01 SW846-6010B 6127101 21:30 MSC THALLIUM, TOTAL IN GOUNDWATER Less than mg/L 0.05 SW846-6010B 6127101 21:30 MSC ZINC. TOTAL IN GROUNDWATER Less than mg/L 2.0 SW846-601 OB 6127101 21:30 MSC MERCURY. TOTAL IN GROUNDWATER Less than mg/L 0.0002 SW846-7470 716101 13:01 PRF BENZENE Not detected ug/L 5.0 SWB46-8260B 712101 12:49 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 71210112:49 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 712101 12:49 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 712101 12:49 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 712101 12:49 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 712101 12:49 MP N-BUTYLBENZENE· Not detected ug/L 5.0 SW846-8260B 712/01 12:49 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 712101 12:49 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 712101 12:49 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 712101 12:49 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 712101 12:49 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 712101 12:49 MP CHLOROFORM 9.2 ug/L 5.0 SW846-8260B 712101 12:49 MP CHLOROMETHANE Not detected ug/L 10 SW846-8260B 7/210112:49 MP NC Certification No. 402 SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364"""' Toll Free Number: t-800/529-6364..,. Fax: 704/525-0409 • • • Lab Report ~~li Full Service Analytical & Environmental Solutions 7/12/01 Page 43 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-8 PO Box 669004 Prism Sample 10: AC11551 Charlotte, NC 28266 Loain Group: 1695H18 Sample Collection Date/Time: 6/26/01 14:15 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 7/2101 12:49 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 7/2/01 12:49 MP 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected · ug/L 10 SW846-82608 7/2/01 12:49 MP 1 ,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-S260B 7/2101 12:49 MP 1 ,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP 1,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP 1,4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 7/2101 12:49 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-82608 7/2/01 12:49 MP 1, 1-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/2101 12:49 MP 1 ,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP 1, 1-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP CIS-1 ,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 7/2101 12:49 MP TRANS-1 ,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP 1 ,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 7/2/01 12:49 MP 1 ,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP 1, 1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-82608 7/2/0112:49 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-82608 7/2/0112:49 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP P-ISOPROPYL TOLUENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP STYRENE Not detected ug/L 5.0 SW846-82608 7/2/0112:49 MP 1, 1,1 ,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/210112:49 MP 1,1 ,2.2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP 'TETRACHLOROETHENE 23 ug/L 5.0 SW846-82608 7/2/0112:49 MP TOLUENE Not detected ug/L 5.0 SW846-82608 7/2101 12:49 MP NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..._ P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o.. Toll Free Number: l-800/529-6364,.. Fax: 704/525-0409 • • • Lab Report ,-~~!~Mo. ~~;~J.< .. ' Full Service Analytical & Environmental Solutions 7112101 Page 44 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-8 PO Box 669004 Prism Sample ID: AC11551 Charlotte, NC 28266 Looin Grouo: 1695H18 Sample Collection Date/Time: 6126/01 14:15 Lab Submittal Date/Time: 6127/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 1.2.3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP 1.2.4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 712101 12:49 MP 1.1.1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 7/2/01 12:49 MP 1,1.2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 12:49 MP TRICHLOROETHENE Nat detected ug/L 5.0 SW846-8260B 7/2/01 12:49 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-82608 712101 12:49 MP 1,2.3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 712101 12:49 MP 1,2.4· TRI METHYLBENZENE Not detected ug/L 5.0 SW846·82608 712101 12:49 MP 1.3.5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-82608 712101 12:49 MP VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 712101 12:49 MP TOTAL XYLENES Nat detected ug/L 5.0 SW846-82608 7/2101 12:49 MP cis-1.3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 7/2101 12:49 MP trans-1,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 7/2/01 12:49 MP ACETONE Not detected ug/L 50 SW846-82608 7/210112:49 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-82608 7/2101 12:49 MP CARBON DISULFIDE Not detected ug/L 50 SW846-82608 7/2101 12:49 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 7/2/01 12:49 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-82608 7/210112:49 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 712/01 12:49 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 712/01 12:49 MP ---------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6129101 20:51 HWC BIS(2·CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6129101 20:51 HWC PHENOL Not detected ug/L 10 SW846-8270C 6129101 20:51 HWC 1,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6129/01 20:51 HWC 1.2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6129/01 20:51 HWC 1.4·DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6129101 20:51 HWC BIS(2·CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6129101 20:51 HWC 2·METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6129101 20:51 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846·8270C 6129/01 20:51 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364 • Toll Free Number: 1-800/529-6364 • Fax: 704/525-0409 • • • Lab Report PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions 7/12/01 Page 45 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-8 PO Box 669004 Prism Sample ID: AC11551 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 14:15 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC ISOPHORONE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 20:51 HWC 2,4 DIMETHYL PHENOL Not detected ug/L 10 . SW846-8270C 6/29/01 20:51 HWC BIS(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC 1 ,2,4 TRICHLOROBENZENE Nat detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6129/01 20:51 HWC HEXACHLOROBUTADIENE Not detected . ug/L 10 SW846-8270C 6/29/01 20:51 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6129/01 20:51 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846-8270C 6129/01 20:51 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC 2,4,6 TRICHLOROPHENOL Not detected ugtL 10 SW846-8270C 6/29/01 20:51 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29101 20:51 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC ACENAPHTHYLENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SWB46-8270C 6/29/01 20:51 HWC 2,4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC DIBENZOFURAN Not detected ug/L 10 SWB46-8270C 6/29101 20:51 HWC 2,4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6129/01 20:51 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6129101 20:51 HWC FLUORENE Not detected ug/L 10 SW846-8270C 6129/01 20:51 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/29/01 20:51 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .., P.O. Box 240543 .., Charlotte, NC 28224-0543 Phone: 704/529-6364.., Toll Free Number: 1-800/529-6364.., Fax: 704/525-0409 • • • ·'·· .. • Lab Report Full Service Analytical & Environmental Solutions 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Page 46 of67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-8 Prism Sample 10: AC11551 Looin Grouo: 1695H18 Sample Collection Date/Time: 6/26/01 14:15 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC BIS(2-ETHYLH EXYL)PHTHALA TE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC INDEN0(1 ,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6/29/01 20:51 HWC ---------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ....._ P.O. Box 240543 ....._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o,. Toll Free Number: l-800/529-6364 ...... Fax: 704/525-0409 • • • lab Report ~A~~ Full Service Analytical & Environmental Solutions 7/12/01 Page 47 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW·9 PO Box 669004 Prism Samole ID: AC11552 Charlotte, NC 28266 Looin Grouo: 1695H18 Sample Collection Date/Time: 6/26/01 13:50 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErriME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST METALS DIGESTION/3030C Complet~d 3030C 6/27/01 09:30 LC2 SILVER, TOTAL, IN GROUNDWATER Less than mg/L O.Q18 6010 6/27/01 20:23 MSC MERCURY DIGESTION Completed. EPA 245.1 7/2101 10:40 LC2 PREP. METHOD 3510 Completed SW846-3510 6/28/01 16:30 JMK LEAD, TOTAL IN GROUNDWATER 0.019 mg/L 0.015 SW846-6010B 6/27/01 20:23 MSC ANTIMONY. TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-6010B 6/27/01 20:23 MSC ARSENIC, TOTAL IN GROUNDWATER 0.011 mg/L 0.010 SW846-6010B 6/27/01 20:23 MSC BERYLLIUM, TOTAL IN GROUNDWATER 0.003 mg/L 0.002 SW846-601 OB 6/27/01 20:23 MSC CADMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.005 SW846-6010B 6/27/01 20:23 MSC CHROMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-6010B 6/27/01 20:23 MSC COPPER. TOTAL IN GROUNDWATER Less than mg/L 1.0 SW846-601 OB 6/27/01 20:23 MSC NICKEL. TOTAL IN GROUNDWATER Less than mg/L 0.10 SW846-6010B 6/27/01 20:23 MSC SELENIUM, TOTAL IN GROUNDWATER Less than mg/L 0.01 SW846-6010B 6/27/01 20:23 MSC THALLIUM. TOTAL IN GOUNDWATER Less than mg/L 0.05 SW846-6010B 6/27/01 20:23 MSC ZINC, TOTAL IN GROUNDWATER Less than· mg/L 2.0 SW846-601 OB 6/27/01 20:23 MSC MERCURY, TOTAL IN GROUNDWATER Less than mg/L 0.0002 SW846-7470 7/6/0113:05 PRF BENZENE Not detected ug/L 5.0 SW846-8260B 7/2/0113:33 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 7/2101 13:33 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 7/2/0113:33 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 7/2/0113:33 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 7/2101 13:33 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 7/2/01 13:33 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/210113:33 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 712101 13:33 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 712101 13:33 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 712101 13:33 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 7/2101 13:33 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 71210113:33 MP CHLOROFORM Not detected ug/L 5.0 SW846-8260B 712101 13:33 MP CHLOROMETHANE Not detected ug/L 10 SW846-8260B 712101 13:33 MP NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 7041529-6364 ..oo. Toll Free Number: 1-800/529-6364 ...._Fax: 7041525-0409 • • • Lab Report ~~~!~M. ~~ Full Service Analytical & Environmental Solutions 7/12/01 Page 48 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-9 PO Box 669004 Prism Sam ole ID: AC11552 Charlotte, NC 28266 LoQin Group: 1695H18 Sample Collection Date/Time: 6/26/01 13:50 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have· been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 7/2/01 13:33 MP 1.2-DIBROMOETHANE Not detected ug/L 5.0 SW846-82608 7/2101 13:33 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-82608 7/2101 13:33 MP 1,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 7/2101 13:33 MP 1,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP 1.4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 7/2/0113:33 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-8260B 7/2101 13:33 MP 1,1-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 7/2101 13:33 MP 1.2-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP 1, 1-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP CIS-1.2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 712101 13:33 MP TRANS-1.2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP 1 ,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP 1.3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP 2.2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 7/2101 13:33 MP 1.1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP P-ISOPROPYL TOLUENE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-82608 7/2101 13:33 MP STYRENE Not detected ug/L 5.0 SW846-82608 7/2101 13:33 MP 1, 1,1 ,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 13:33 MP TETRACHLOROETHENE Not detected ug/L 5.0 SW846-82608 7/2101 13:33 MP TOLUENE Not detected ug/L 5.0 SW846-82608 7/2/0113:33 MP NC Certification No. 402 -SC Certrrication No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 .... Charlotte, NC 18224-0543 Phone: 704/529-6364 • Toll Free Number: t-800/529-6364 ... Fax: 704/525-0409 • • • Lab Report ~~!~~!" ~~ Full Service Analytical & Environmental Solutions 7/12/01 Page 49 of67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-9 PO Box 669004 Prism Sam ole 10: AC11552 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection DatefTime: 6/26/01 13:50 Lab Submittal DatefTime: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED · ANALYSe 1 ,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP 1 ,2,4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP 1,1, I-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 7/2/0113:33 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 7/2/0113:33 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 7/2/01 13:33 MP 1 ,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 7/2/0113:33 MP 1 ,2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP 1 ,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 7/2/01 13:33 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-8260B 7/2/0113:33 MP cis-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP trans-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 7/2/01 13:33 MP ACETONE Not detected ug/L 50 SW846-8260B 7/2/0113:33 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-8260B 7/2/01 13:33 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 7/2/01 13:33 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 7/2/0113:33 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 7/2/01 13:33 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 7/2/01 13:33 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 7/2/01 13:33 MP ---------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 1 ,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 1 ,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 2'1:39 HWC 1,4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529·6364 ..o. Toll Free Number: 1-800/529-6364...,. Fax: 704/525-0409 • • • ,;j· Lab Report ~~!~~-.~~ .. , Full Service Analytical & Environmental Solutions 7/12/01 Page 50 of67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-9 PO Box 669004 Prism Samcle 10: AC11552 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Daterrime: 6/26/01 13:50 Lab Submittal Daterrime: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC NITROBENZENE Not detected ugiL 10 SW846-8270C 6/29/01 21:39 HWC 4-METHYL PHENOL(P CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC ISOPHORONE Nol detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 21:39 HWC 2,4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC BIS(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 1 ,2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC HEXACHLOROBUTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 2.4.6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 2.4.5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC ACENAPHTHYLENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 21 :39 HWC 2,4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC 2.4 DINITROPHENOL Not detected ug/L 50 SW846-8270C -6/29/01 21:39 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 21:39 HWC FLUORENE Not detected ug/L 10 SW846-8270C 6129/01 21:39 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29101 21:39 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6129/01 21:39 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6129101 21:39 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/29101 21:39 HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook R~ad .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o. Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 51 of 67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-9 Prism Samole 10: AC11552 Looin Grouo: 1695H18 Sample Collection Date/Time: 6/26/01 13:50 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 4-BROMOPHENYL PHENYL ETHER Not detected ug/L io SW846-8270C 6129101 21:39 HWC HEXACHLOROBENZENE Nat detected ug/L 10 SW846-8270C 6129101 21:39 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29101 21:39 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC FLUORANTHENE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC PYRENE Not detected ug/L 10 SW846-8270C 6129/01 21:39 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/L 10 SW846-8270C 6/29101 21:39 HWC DI-N-OCTYL PHTHALATE Not delected ug/L 10 SW846-8270C 6129101 21:39 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 sw 846-8270C 6129101 21:39 . HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC INDEN0(1 ,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6129101 21:39 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6129/01 21:39 HWC ---------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .a P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: 1-800/529-6364 ..... Fax: 704/525-0409 • • • Lab Report ..... • --~~!~Mo.· ..,ckl~ Full Service Analytical & Environmental Solutions 7/12/01 Page 52 of67 Mid-Atlantic Associates Customer Project tD: Cherokee-Mooresvilte Site Cliff Lundgren Customer Sample ID: MW-10 PO Box 669004 Prism Samole ID: AC11553 Charlotte, NC 28266 Looin Group: 1695H18 Sample Collection Date/Time: 6/26/01 10:20 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST· REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT .REFERENCE STARTED ANALYST METALS DIGESTION/3030C Completed 3030C 6/27/01 15:40 LC2 SILVER, TOTAL, IN GROUNDWATER Less than mg/L 0.018 6010 6/29/01 23:00 MSC MERCURY DIGESTION Completed EPA 245.1 7/210110:40 LC2 PREP. METHOD 3510 Completed SW846-3510 6/28/01 16:30 JMK LEAD, TOTAL IN GROUNDWATER 0.057 mg/L 0.015 SW846-6010B 6/29/01 23:00 MSC ANTIMONY, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-6010B 6/29/01 23:00 MSC ARSENIC, TOTAL IN GROUNDWATER 0.054 mg/L 0.010 SW846-6010B 6/29/01 23:00 MSC BERYLLIUM, TOTAL IN GROUNDWATER 0.035 mg/L 0.002 SW846-6010B 6/29/01 23:00 MSC CADMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.005 SW846-6010B 6/29/01 23:00 MSC CHROMIUM, TOTAL IN GROUNDWATER 0.060 mg/L 0.05 SW846-6010B 6/29/01 23:00 MSC COPPER, TOTAL IN GROUNDWATER Less than mg/L 1.0 SW846-6010B 6/29/01 23:00 'MSC NICKEL, TOTAL IN GROUNDWATER Less than mg/L 0.10 SW846-6010B 6/29/01 23:00 MSC SELENIUM, TOTAL IN GROUNDWATER Less than mg/L O.Q1 SW846-6010B 6/29/01 23:00 MSC THALLIUM, TOTAL IN GOUNDWATER Less than mg/L 0.05 SW846-6010B 6/29/01 23:00 MSC ZINC, TOTAL IN GROUNDWATER Less than mg/L 2.0 SW846-601 OB 6/29/01 23:00 MSC MERCURY, TOTAL IN GROUNDWATER Less than mg/L 0.0002 SW846-7470 7/6/01 13:09 PRF BENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 14:16 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 7/2101 14:16 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 7/2/01 14:16 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 7/2/01 14:16 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 7/2101 14:16 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 7/2/01 14:16 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2101 14:16 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 14:16 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 14:16 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 14:16 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 7/2/01 14:16 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 7/2101 14:16 MP CHLOROFORM Not detected ug/L 5.0 SW846-8260B 7/2101 14:16 MP CHLOROMETHANE Not detected ug/L 10 SW846-8260B 7/2/01 14:16 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224~0543 Phone: 704/529-6364 ..o. Toll Free Number: 1-800/529-6364 ..... Fax: 704/525-0409 Lab Report ~~!~Me. ~..:z::,..:: • Full Service Analytical & Environmental Solutions 7/12/01 Page 53 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-10 PO Box 669004 Prism Sample 10: AC11553 Charlotte, NC 28266 Loain Group: 1695H18 . Sample Collection Date/Time: 6/26/01 10:20 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 7/2/01 14:16 MP 1,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP !:"" .. 1,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP 1.3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 7/2/0114:16 MP • 1.4-DICHlOROBENZENE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW646-82608 7/2101 14:16 MP 1, 1-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP 1,2-DICHLOROETHANE Not defected ug/L 5.0 SW846-82608 7/2101 14:16 MP 1,1-DICHLOROETHENE 6.2 ug/L 5.0 SW846-82608 7/2/01 14:16 MP CIS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP TRANS-1,2-01 CH LOROETHENE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP 1,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP 1,3-DICHLOROPROPANE Not detected ug/L 5.0 . SW646-82608 7/2101 14:16 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SW646-82608 7/2101 14:16 MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP P-ISOPROPYL TOLUENE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP STYRENE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP 1,1,1,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP 1,1,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP • TETRACHLOROETHENE Not detected ug/L 5.0 SW846-82608 7/2/01 14:16 MP TOLUENE Not detected ug/L 5.0 SW846-82608 7/2101 14:16 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o. Toll Free Number: 1-800/529-6364 ..o. Fax: 704/525-0409 • • • Lab Report ,··:;f~~ ·---~f.!!~&: ~.~ ; Full Service Analytical & Environmental Solutions ~ 7/12/01 Page 54 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-10 PO Box 669004 Prism Sample ID: AC11553 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date!Time: 6/26/01 10:20 Lab Submittal Date!Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 1 ,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 sw 846-82608 712101 14:16 MP 1 ,2,4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 712101 14:16 MP 1,1, 1-TRICHLOROETHANE Not detected ug/L. 5.0 SW846-8260B 712101 14:16 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 712101 14:16 MP TRICHLOROETHENE No't detected ug/L 5.0 SW846-8260B 712101 14:16 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 712101 14:16 MP 1 ,2, 3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 712101 14:16 MP 1,2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 712101 14:16 MP 1 ,3,5-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 712101 14:16 MP VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 712101 14:16 MP TOTAL XYLENES Not detected ug/L 5.0 SW846-82608 712101 14:16 MP cis-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 712101 14:16 MP trans~ 1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 . SW846-8260B 712101 14:16 MP ACETONE Not detected ug/L 50 SW846-8260B 712101 14:16 MP 2-BUTANONE (MEK) Not detected ug/L 10 SWB46-8260B 712101 14:16 MP CARBON DISULFIDE Not detected ug/L 50 SW846-8260B 712101 14:16 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 712101 14:16 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 712101 14:16 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 712101 14:16 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 712/01 14:16 MP --------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6129101 22:28 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L 10 SW846-8270C 6129101 22:28 HWC PHENOL Not detected ug/L 10 SW846-8270C 6129101 22:28 HWC 1 ,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6129101 22:28 HWC 1 ,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6129/01 22:28 HWC 1 ,4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6129101 22:28 HWC BIS(2·CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6/29101 22:28 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6129101 22:28 HWC HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6129101 22:28 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road,... P.O. Box 240543 ...._ Charlotte, NC 28224·0543 Phone: 704/529-6364..., Toll Free Number: t-800/529-6364..., Fax: 704/525-0409 • • • ·<~ Lab Report ~ ,, P1usti --"' LABORAT~RIES,INC. _...as!f'Sl' f'l~lk> . Full Service Analytical & Environmental Solutions 7/12101 Page 55 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-10 PO Box 669004 Prism Sample 10: AC11553 Charlotte, NC 28266 LoQin Group: 1695H18 Sample Collection Date/Time: 6/26/01 10:20 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC ISOPHORONE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 2-NITROPHENOL Not detected ug/L 10 · SW846-8270C 6/29/0122:28 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 22:28 HWC 2,4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC BIS(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 1 ,2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC HEXACHLOROBUTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC ACENAPHTHYLENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 2,4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 2,4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 22:28 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC FLUORENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/29/01 22:28 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...,. P.O. Box 240543 ..... Charlotte, NC :!8224-0543 Phone: 704/529-6364 ..o. Toll Free Number: 1-800/529-6364 ..o. Fax: 704/525-0409 Lab Report • • • 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project ID: Customer Sample ID: Prism Samole ID: LoQin Group: Sample Collection Date/Time: Lab Submittal Date/Time: Full Service Analytical & Environmental Solutions Page 56 of 67 Cherokee-Mooresville Site MW-10 AC11553 1695H18 6/26/01 10:20 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC DI-N-BUTYL PHTHALATE Not detected ugiL 10' SW846-8270C 6/29/01 22:28 HWC FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C .. 6/29/01 22:28 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC INDEN0(1 ,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC DIBENZO(A,H)ANTHRACENE. Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6/29/01 22:28 HWC --------- Sample Comments: ~ \,. Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 • SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 • Toll Free Number: 1-800/529-6364 ..._ Fax: 704/525-0409 ,, . Lab Report ~PRisM • • • • ,LABORA;OAIES, INC. --··~ ~· . FuJI Service Analytical & Environmental Solutions 7/12/01 Page 57 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-11 PO Box 669004 Prism Sam ole 10: AC11554 Charlotte, NC 28266 LoQin Group: 1695H18 Sample Collection Date/Time: 6/26/01 11:30 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST METALS DIGESTION/3030C Completed 3030C 6/27/01 15:40 LC2 SILVER, TOTAL, IN GROUNDWATER Less than mg/L 0.018 6010 6/29/01 23:05 MSC MERCURY DIGESTION Completed EPA 245.1. 7/2/01 10:40 LC2 PREP. METHOD 3510 Completed SW846-3510 6/28/01 16:30 JMK LEAD, TOTAL IN GROUNDWATER 0.073 mg/L 0.015 SW846-601 OB 6/29/01 23:05 .MSC ANTIMONY, TOTAL IN GROUNDWATER Less than mg/L 0.05 SW846-6010B 6/29/01 23:05 MSC ARSENIC, TOTAL IN GROUNDWATER 0.017 mg/L 0.010 SW846-6010B 6/29/01 23:05 MSC BERYLLIUM, TOTAL IN GROUNDWATER 0.017 mg/L 0.002 SW846-6010B 6/29/01 23:05 MSC. CADMIUM, TOTAL IN GROUNDWATER Less than mg/L 0.005 SW846-6010B 6/29/01 23:05 MSC CHROMIUM, TOTAL IN GROUNDWATER 0.16 mg/L 0.05 SW846-8010B 6/29/01 23:05 MSC COPPER, TOTAL IN GROUNDWATER Less than .mg/L 1.0 SW846-601 OB 6/29/01 23:05 MSC NICKEL, TOTAL IN GROUNDWATER 0.18 mg/L 0.10 SW846-601 OB 6/29/01 23:05 MSC SELENIUM, TOTAL IN GROUNDWATER Less than mg/L 0.01 SW846-6010B 6/29/01 23:05 MSC THALLIUM, TOTAL IN GOUNDWATER Less than mg/L 0.05 SW846-6010B 6/29/01 23:05 MSC ZINC, TOTAL IN GROUNDWATER Less than mg/L 2.0 SW846-601 OB 6/29/01 23:05 MSC MERCURY, TOTAL IN GROUNDWATER Less than mg/L 0.0002 SW846-7470 7/6/0113:12 PRF BENZENE Not detected ug/L 5.0 SW846-8260B 7/2/0115:00 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 7/2/0115:00 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 7/2/0115:00 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 7/2/01 15:00 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/0115:00 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 7/210115:00 MP CHLORODIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 7/210115:00 MP CHLOROFORM Not detected ug/L 5.0 SW846-8260B 7/210115:00 MP CHLOROMETHANE Not detected ug/L 10 SW846-8260B 7/2101 15:00 MP NC Certification No. 402 SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..._ P.O. Box 240543 ..._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ..._Toil Free Number: 1-800/529-6364 ..._Fax: 704/525-0409 Lab Report ~PRISM· • • • LABORATORIES, INC.· -&~ Full Service Analytical & Environmental Solutions 7/12/01 Page 58 of 67 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: MW-11 PO Box 669004 Prism Sam ole ID: AC11554 Charlotte, NC 28266 LoQin Group: 1695H18 Sample Collection Daterrime: 6/26/01 11:30 Lab Submittal Daterrime: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-8260B 7/2101 15:00 MP 1,2-DIBROMOETHANE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP 1,2-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP 1,3-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP 1 ,4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-8260B 7/2101 15:00 MP 1,1-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP 1,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP 1,1-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP CIS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP TRANS-1,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP 1,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 7/210115:00 MP 1,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-8260B 7/2/0115:00 MP 1,1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP P-ISOPROPYL TOLUENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP NAPHTHALENE Not detected ug/L 5.0 SW846-8260B 7/2/0115:00 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP STYRENE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP 1,1,1,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP 1,1,2,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-8260B 7/2/01 15:00 MP TETRACHLOROETHENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP TOLUENE Not detected ug/L 5.0 SW846-8260B 7/2101 15:00 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529·6364 • Toll Free Number: 1-800/529-6364 • Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 ·'' ~ !:!!~~. _.-·d~ . Full Service Analytlcal &-Environmental Solutions Page 59 of67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: MW-11 Prism Samole 10: AC11554 Loqin Group: 1695H18 Sample Collection Daternme: 6/26/01 11 :30 Lab Submittal Date!Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER 1,2,3-TRICHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE . TRICHLOROETHENE TRICHLOROFLUOROMETHANE 1,2.3-TRICHLOROPROPANE 1 ,2.4-TRIMETHYLBENZENE 1,3,5-TRIMETHYLBENZEN E VINYL CHLORIDE TOTAL XYLENES · cis-1,3-DICHLOROPROPENE trans-1,3-DICHLOROPROPENE ACETONE 2-BUTANONE (MEK) CARBON DISULFIDE CARBON TETRACHLORIDE 2-CHLOROETHYLVINYLETHER 2-HEXANONE 4-METHYL-2-PENTANONE (MIBK) 2-CHLOROPHENOL 81S(2-CHLOROETHYL)ETHER PHENOL 1,3-DICHLOR08ENZENE 1 ,2-DICHLOR08ENZENE 1.4-DICHLOR08ENZENE 81S(2-CHLOROISOPROPYL)ETHER 2-METHYL PHENOL (0 CRESOL) HEXACHLOROETHANE TEST RESULT Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected UNITS ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L REPORTING METHOD DATEfTIME STARTED LIMIT REFERENCE 5.0 5.0 5.0 5.0 5.0 10 5.0 5.0 5.0 10 5.0 ·5.0 5.0 50 10 50 5.0 10 10 10 10 10 10 10 10 10 10 10 10 SW846-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/210115:00 SW846-8260B 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-8260B 7/2/01 15:00 SW646-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-8260B 7/2/01 15:00 SW846-8260B 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/2/01 15:00 SW846-82608 7/2/0115:00 SW846-8270C 6/29/01 23:15 SW846-8270C 6/29/01 23:15 SW846-8270C 6/29/01 23:15 SW846-8270C 6/29/01 23:15 SW846-8270C 6/29/01 23:15 SW846-8270C 6/29/01 23:15 SW846-8270C 6/29/01 23:15 SW846-8270C 6/29/01 23:15 SW646-8270C 6/29/01 23:15 ANALYST MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP MP HWC HWC HWC HWC HWC HWC HWC HWC HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .., P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364.., Toll Free Number: t-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report ··~~!~Mo. -~?]:~ Full Service Analytical & Environmental Solutions 7/12/01 Page 60 of 67 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: MW-11 PO Box 669004 Prism Sample 10: AC11554 Charlotte, NC 28266 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 11:30 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErrtME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC ISOPHORONE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 23:15 HWC 2,4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC BIS(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 1 ,2,4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/29/01 23:·15 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC HEXACHLOROBUTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC ACENAPHTHYLENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 2,4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC DIBENZDFURAN Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 2,4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6/29/01 23:15 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC FLUORENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC DIETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6129101 23:15 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/29/01 23:15 HWC N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC NC Certification No. 402 • SC Certification No. 99012 • NC Drinking Water Cert. No. 37735 • FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28i24-0543 Phone: 704/529-6364 • Toll Free Number: 1-800/529-6364 ..... Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Sam ole 10: Looin Group: Sample Collection OatefTime: Lab Submittal DatefTime: '! ·, ~ ~!~&~ ~;~ ·. Full Service Analytical 8. Environmental Solutions Page 61 of 67 .. Cherokee-Mooresville Site MW-11 AC11554 1695H18 6/26/01 11 :30 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SWB46-8270C 6/29/01 23:15 HWC HEXACHLOROBENZENE Not detected ug/L 10 SWB46-8270C 6/29/01 23:15 HWC PENTACHLOROPHENOL Not detected ug/L 10 SWB46-8270C 6/29/01 23:15 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC FLUDRANTHENE Not detected ug/L 10 SWB46-8270C 6/29/01 23:15 HWC PYRENE Not detected ug/L 10 SWB46-8270C . 6/29/01 23:15 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29i01 23:15 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/L 10 SWB46-8270C 6/29/01 23:15 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SWB46-8270C 6/29/01 23:15 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC INDEN0(1,2,3-C.D)PYRENE Not detected ug/L 10 SWB46-8270C 6/29/01 23:15 HWC DIBENZO(A.H)ANTHRACENE Not detected ug/L 10 SWB46-8270C 6/29/01 23:15 HWC BENZO(G.H.I)PERYLENE Not detected ug/L 10 SW846-B270C 6/29/01 23:15 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6/29/01 23:15 HWC ····-···· Sample Comments: ~ \.. NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 ...._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ...._Toll Free Number: 1-800/529-6364 ...._Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 . .,\ ,; ' PRISM LABORATORIES. INC. Full Service Analytical & Environmental Solutions Page 62 of 67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: BG-1.o!(4.0) Prism Sample 10: AC11555 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 Lab Submittal Date/Time: 6/27/01 13:00 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 77 %DRYWT. 0.01 SM 2540 G 6129101 17:45 JLW METALS DIGESTION METHOD 3050 Completed SW846-3050 6127101 12:00 LC2 ANTIMONY, TOTAL 1.5 mg/kg 1.0 SW846-601 OB 6128101 00:08 MSC ARSENIC, TOTAL 3.1 mg/kg 1.0 SW846-601 OB 6128101 00:08 MSC BERYLLIUM, TOTAL Less than mg/kg 1.0 SW846-6010B 6128101 00:08 MSC CADMIUM, TOTAL Less than mg/kg 1.0 SW846-6010B 6128101 00:08 MSC CHROMIUM, TOTAL 22 mg/kg 1.0 SW846-601 OB 6128101 00:08 MSC COPPER, TOTAL 31 mg/kg 2.0 SW846-6010B 6128101 OO:D8 MSC LEAD, TOTAL 12 mg/kg 1.D SW846-6D1 DB 6128101 OD:D8 MSC NICKEL, TOTAL 3.5 mg/kg 1.D SW846-6D1DB 61281D1 DO:D8 MSC SELENIUM, TOTAL Less than mg/kg 2.D SW846-6010B 6128101 DD:D8 MSC SILVER. TOTAL Less than mg/kg 2.D SW846-601DB 6128/01 OO:D8 MSC THALLIUM, TOTAL Less than mg/kg 0.5 SW846-601 DB 61281D1 D0:08 MSC ZINC, TOTAL 51 mg/kg 1.0 SW846-6D1 DB 6/28/D1 DD:D8 MSC MERCURY, TOTAL D.04 mg/kg D.03 SW846-7471 6128101 14:46 PRF MERCURY DIGESTION Completed SW846-7471 6/271D1 12:30 LC2 -~~·· Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road & P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364 .a. Toll Free Number: 1-800/529-6364 .a. Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 PRISM LABoRATORIES, INC . . •·; Full SeNice Analytical & Environmental Solutions Page 63 of 67 Customer Project 10: Cherokee-Mooresville Sit~ Customer Sample 10: H-1(0) (0.5) Prism Samole 10: AC11556 Loqin Group: 1695H18 Sample Collection Datemme: 6/26/01 13:15 Lab Submittal Daterrime: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 93 %DRYWT. 0.01 SM 2540 G 6/28/01 15:30 JLW PREP. METHOD J550 Completed SW846-3550 7/3/01 18:00 JLW PCB-1016 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:11 CWA PCB-1221 Not detected mg/kg 1.0 SW846-8082 7/5/01 21:11 CWA PCB-1232 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:11 CWA PCB-1242 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:11 CWA PCB-1248 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:11 CWA PCB-1254 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:11 CWA PCB-1260 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:11 CWA PCB-1262 Not detected mg/kg 0.50 SW846-8082 7/5/0121:11 CWA PCB-1268 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:11 CWA ---------- ---~-~··- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..o. P.O. Box 240543 ..o. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o. Toll Free Number: t -800/529-6364 ..o. Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 ~ ~!~A. ~;7~ Full Service Analytical a Environmental Solutions Page 64 of 67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: H-8(F)(1.0) Prism SamoleiO: AC11557 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 13:30 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 80 . %DRYWT. . 0.01 SM 2540 G 6/28/01 15:30 JLW PREP. METHOD 3550 Comple1ed SW846-3550 7/3/01 18:00 JLW PCB-1016 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:56 CWA PCB-1221 Not detected mg/kg 1.0 SW846-8082 7/5/01 21:56 CWA PCB-1232 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:56 CWA PCB-1242 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:56 CWA PCB-1248 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:56 CWA PCB-1254 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:56 CWA PCB-1260 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:56 CWA PCB-1262 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:56 CWA PCB-1268 Not detected mg/kg 0.50 SW846-8082 7/5/01 21:56 CWA ---------- ·-·-·--------- Sample Comments: Analysis note for SW846-8082: Detection limits for this sample raised 1 Ox due to 1 Ox dilution made prior to analysis for matrix interference. Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 ...._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ...._Toil Free Number: 1-800/529-6364 ...._Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 65 of 67 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: H-26(A) (1.0) Prism Samole 10: AC11558 Loqin Group: 1695H 18 Sample Collection Date/Time: 6/26/01 13:40 Lab Submittal Date/Time: 6/27/01 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOO DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 94 % DRYWT. 0.01 SM-2540 G 6/28/01 15:30 JLW PREP. METHOD 3550 Completed SW846-3550 7/3/01 18:00 JLW PCB-1016 Not detected mglkg 0.50 SW846-8082 7/5/01 22:41 CWA PCB-1221 Not detected mg/kg 1.0 SW846-8082 7/5/01 22:41 CWA PCB-1232 Not detected mg/kg 0.50 SW846-8082 7/5/01 22:41 CWA PCB-1242 Not detected mg/kg 0.50 SW846-8082 7/5/01 22:41 CWA PCB-1248 Not detected mglkg 0.50 SW846-8082 7/5/01 22:41 CWA PCB-1254 Not detected mg!kg 0.50 SW846-8082 7/5/01 22:41 CWA PCB-1260 5.3 mg/kg 0.50 SW846-8082 7/5/01 22:41 CWA PCB-1262 Not detected mg/kg 0.50 SW846-8082 7/5/01 22:41 CWA PCB-1268 Not detected mg/kg 0.50 SW846-8082 7/5/01 22:41 CWA --------·-·-----·· --·----·---· Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ...._Toll Free Number: 1-800/529-6364 ...._Fax: 704/525-0409 • • • Lab Report 7112101 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte; NC 28266 Customer Project ID: Customer Sample ID: Prism Sample 10: Loain Group: Sample Collection Date/Time: Lab Submittal Date/Time: Full Service Analytical & Environmental Solutions Page 66 of 67 Cherokee-Mooresville Site H-16(L) !11 { 0, 7) AC11559 1695H18 6126101 6127/01 14:00 07:55 The following analytical results have been obtained for the indicated sampl~ which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 92 %DRYWT. O.Q1 SM 2540 G 6/28/01 15:30 JLW PREP. METHOD 3550 Completed SW846-3550 7/3/01 18:00 JLW PCB-1016 Not detected mg/kg 5.0 SW846-8082 7/6/01 23:05 CWA PCB-1221 Not detected mglkg 10 SW846-8082 7/6/01 23:05 CWA PCB-1232 Not detected mg/kg 5.0 SW846-8082 7/6/01 23:05 CWA PCB-1242 Not detected mg/kg 5.0 SW846-8082 7/6/01 23:05 CWA PCB-1248 Not detected mg/kg 5.0 SW846-8082 7/6/01 23:05 CWA PCB-1254 Not detected mg/kg 5.0 SW846-8082 7/6/01 23:05 CWA PCB-1260 9.3 mg/kg 5.0 SW846-8082 7/6/01 23:05 CWA PCB-1262 Not detected mg/kg 5.0 SW846-8082 7/6/01 23:05 CWA PCB-1268 Not detected mg/kg 5.0 SW846-8082 7/6/01 23:05 CWA ·--------------··-·------·. -·------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road...._ P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 .-.. Toll Free Number: 1-800/529-6364 .-.. Fax: 704/525-0409 • • • Lab Report 7/12/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 67 of67 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: H-23(C) (1.0) Prism Samole ID: AC11560 Loqin Group: 1695H18 Sample Collection Date/Time: 6/26/01 Lab Submittal Date/Time: 6/27/01 14:30 07:55 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME _!>.t,RAMETER RESULT UNITS LIMIT REFEflENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 83 %DRYWT. 0.01 SM 2540 G 6/28/01 15:30 JLW PREP. METHOD 3550 Completed SW846-3550 7/3/0118:00 JLW PCB-1016 Not detected mg/kg 0.50 SW846-8082 7/6/01 00:10 CWA PCB-1221 Not detected mg/kg 1.0 SW846-8082 7/6/01 00:10 CWA PCB-1232 Not detected mg/kg 0.50 SW846-8082 7/6/01 00:10 CWA PCB-1242 Not detected mg/kg 0.50 SW846-8082 7/6/01 00:10 CWA PCB-1248 Not detected mg/kg 0.50 SW846-8082 7/6/01 00:10 CWA PCB-1254 Not detected mg/kg 0.50 SW846-8082 7/6/01 00:10 CWA PCB-1260 Not detected mg/kg 0.50 SW846-8082 7/6/01 00:10 CWA PCB-1262 Not detected rrig/kg 0.50 SW846-8082 7/6/01 00:10 CWA PCB-1268 Not detected mg/kg 0.50 SW846-8082 7/6/01 00:10 CWA ---------·-----·-----·· Sample Comments: Analysis note for SW846-8082: Detection limits for this sample raised 1 Ox due to 1 Ox dilution made prior to analysis for matrix interference. Angela D . NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .a. P.O. Box 240543 ....._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ...._ Toll Free Number: I -800/529-6364 ...._ Fax: 704/525-0409 CHAIN OF CU.ODY RECORD Full Service Analytical & Environmental Solutions '''\) . :\ ......... ' _, \; \' ...... '' '' . ' ~~:::c.~ Add;~:~.'~.~~ 't-;-:f ':',\~)\~;. (;i .-:~;~,t---== ------11", -<s~;:; ':" ;: : -: --·,~,;.·, ---\--;--~ -::-·m··\·------ Phone____ Fax P.O.#/Billing R~f~~~~ce1:, -, • f':. '·" .· 'r• Project Name _____ ~ · ~-______ _ ~L PAGE OF QUOTE#----~----- 449 Springbrook Road ..... Charlotte, NC 2821 7 P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Fax: 704/525-0409 ·. . '.' ·:· · .. :~ .... -" .. ,-; REPORT TO: Name BILL TO: Address ~-~:-;;--~-~~-T7'S~.T:-· ---,-------- Name ----__ _ Address ___ -------------___ :__ ____ _ Requested Due Date 0 _1 Day 0 2 Days 0 3 Days 0 4 Days 0 5 Days 0 6-9 Days 0 Standard 10 days Samples received after 15:00 will be processed the next business day. Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) NC Water Chlorinated Yes Sample Iced uPon C?ltection CMUD NPDES SC ---Other_---NA -- No NA Yes No OTHER PRESS DOWN FIRMLY • 3 COPIES TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED SUB1 lAB CERT. IDNO. CLIENT DATE COL~~CT~D SAMPLE DESCRIPTION COLLECTED MILITARY HOURS ' ... -...J --I. (1 ' ( b/i; I ::_ -:, ,. f·'· ·,., . c. I . :1·1 I :~\ \ 'J . -s r.. T,-q--I I ,:-. i'J,_,_., -4S I ~ ; . " ') JV\ \",: -. i\\': t··\ ' ... ...--L I \_-~ Ji. \v -1 r.-~ . 't) I ;· \·)·-'' I 'j -' '· TI\\J :-q-.. ·-·. {· ' ·~::;-c- {I•'· :~, ...1 •• ~'-' (SOil, WATER OR SlUDGE) 'v.h,•?.- __ J I I I -{, •TYPE SEE BELOW , .. _. NO. ·-,_, ... SIZE PRESERVA- TIVES ;; ' -·1·:1:. ' ' ___ , ----- ' I i L ! -. _j --- I • j I . . ., --~------\L--·---~-V----~- ~-' .... / ~, /' ·:, ' ') l i I ' 1 ' I I ' I I I I I I I I ) \ I I I I w--,y- Sampler's Signature _ --~---__ 1 \ _ ' . IJ/. ;-~•·.;.--:\. ·x; .. u-..r· • _ ________ Sampled By (Prrnt Name) -------1-----f--------- Received By: (Signature) -• ·--·---.-· -Received BY: ~Sigrlature) Aelinq~ished By: (Signature) ·----R~;~J, F~ir, Prlsffi L&boritofes \3y - - -- 1. tl;\ ... v~-.,J·--· · :: -... _'b:~\. ----------·,---/ ______ .) __ _ Meth"""Od or shipment:/ -------·-- - r:J Fed Ex 0 UPS P Hand-delivered CJ Other: NPDES: 0 NC CJ sc 0 OTHER UST: 0 NC 0 sc 0 OTHER I GROUNDWATER: 0 NC 0 sc 0 OTHER -;._ ,• DRINKING WATER: • 1 SOLID WASTE: CJNC 'ONC osc osc 0 OTHER •CJ OTHER c' RCRA: 0 NC 0 sc CJ OTHER CERCLA 0 NC 0 sc 0 OTHER Date Date LANDFILL 0 NC .0 sc 0 OTHER --.: ., ··-~· / / / REMARKS ._ PRISM lAB IDNO. \~~~~·:)~'' -.. ----- - {~ ·, ;.J. \ ' (. ·, ', :,l.' ___ Affiliation __ ·· _ . · ·- Military/Hours OTHER: 0 NC 0 sc 0 OTHER Additional Comments: [,c __ <{\. ~-~ --:---:r " dj\" : . ----~ . ':_ :·:.,•Ft . ·'· · ! 1 r ,.'\.(; _, -. ((\_ 't<;t)1 Site Arrival T!me: · ,,: Field Tech fee; ~ileage ··, · ;;,-·. SEE REVERSE FOR - TERMS & CONUITIONS ·coNTAINER TYPE CODES: A =Amber C =Clear G =Glass P =Plastic; TL =Teflon-Lined Cap VOA =Volatile Organics Analysis {Zero Head Space) FINAL REPORT COPY CHAIN OF CU.ODY RECORD . ' I J. -~ .. '. '" • .. ' ( • Client \(~ \;S::' C;[_.·, G;l~"', Physical Address. lo:·'. ' f•. (~' /. (~~ \·;::,.=.\.- ----=·-'-"tv:~----:\(.-~ ~·\<t. -·-----!'i:A:-:: :_('". r:.:-'f\t-<1 ______ _ Phone Fax P.O.#/BIIIing R~f~~-~l]c,~-,..__~: \' F'· ,J.;~ f, :>--~ '\,' -!:-.: :... ~- ' ' PAGE OF QUOTE#--------- 449 Springbrook Road .... Charlotte, NC 282 I 7 P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Fax: 704/525·0409 ·:.-.-~ ,. \~~---·.·)'·· i· f.i REPORT TO: Name Bill TO: Address:.\/\ .. , \~" ;_~ '"-, :~~\'i'_I­ Name ------------ Address Requested Due Date 0 1 Day 0 2 Days 0 3 Days 0 4 Days Q 5 Days CJ 6-9 Days 0 Standard 10 days Samples received after 15:00 will be processed the next business day. Turnaround time is based on business days, exc!uding weekends and holi~ays. NC sc Other NA. Water Chlorinated Yes No NA Sample Iced Upon Collection Yes No CMUD NPDES OTHER Project Name _ _ _ _ ___ ---·-· __ -------·-- (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES} PRESS DOWN FIRMLY· 3 COPIES TIME CliENT DATE COLL~c;:TEO SAMPLE DESCRIPTION COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER ~TYPE SEE BELOW NO. SIZE PRESERVA- TIVES REMARKS ,'.'\ \./ ~ i ') b i7_[;{;)\ : .. (t'• '·J, ... :'r '\,' . ' I· ~ ?, (.. . i ~. (1 . ·.' i\ ~ il; Sampler's Signature , ' ' ii . . ';.t: itJ· ? c· ; I ..... · _.} ' .)/ (~ .·. --v. '- ·.'=~--I / ' ' .. i ., ·-~· 1.~( 0 ., ·-j.~ ... ~-:, o-~ ---·---· --· ,;:; :-_:.'l ·~~' (.J-::. 1'"1 "Jtc) l·r· ;. __ _ __ .Sampled By (Print Name). Received By: (Signature) Received By: (Signature) Affiliation Date Mililary/Hours Date ~ ; I -----------:--!----i---\-----R,l:lceiVe~ f,or Pnsm Labdrrones By ------------~--qai~--j-· , j-··-:j I ,;(t i: <. MethOdOFShipmeilt.J -. .'------------- (\\}7iv'~.'v•/y~ ... -~-__)1~~-\ -------,.---J----,.-)-' .. _:.. r -!·.; ~ . ----·----~-· -'-·1--·-· . -· -----·-· Log-In Gro~~ N_.P·:-·· , .. , 'J i'·--'' 1 -~ n 1 r~ Ci Fed Ex r:.J UPS ~Hand-delivered CJ Other: , __ _ NPDES: UST: GROUNDWATER: DRINKING WATER: '· SOLID WASTE: RCRA: I CERCLA lANDFILL OTHER: Cl NC 0 NC 0 NC 0 NC i 0 NC 0 NC 0 NC 0 NC 0 NC 0 sc 0 sc 0 sc 0 sc :0 sc 0 sc (I sc 0 sc r:. SC 0 OTHER 0 OTHER 0 OTHER Cl OTHER :0 OTHER 0 OTHER 0 OTHER 0 OTHER Cl OTHER ·•·· ... I .. H.; k,.,..; Additional Com;;;8nts: SUB LAB CERT. IDNO. Field Tech Fee: -. Mileage PRISM, LAB ' IDNO. t, ( c:::·· . ./ /_/ ,,,;,;,:; /lj~~i SEE REVERSE FOR~ TERMS & CONDITIONS 'CONTAINER TYPE CODES: A = Amber C = Clear G =Glass P =Plastic; TL = Teflon-Lined Cap VOA =Volatile Organics Analysis,(Zero Head Space) FINAL REPORT COPY PrusM . LABORATORIES, INC. Clienl M;J-!\.,.\,.~\-"-!\~>"' ;"\~~ Physical Address ~0 ~> 1-b t '\ 00~ t-""'-r\o~e._, tv'-((l.(,b-'I!JO'\ PhonelO'l-3~•-1\1( Fax 70'1--''1~-'ill'\: P.O.#/BIIIIng Reference CHAIN OF C.TODY RECORD PAGE _l_ OF l.. QUOTE # --------- 449 Springbrook Road ..... Charlotte, NC 2821 7 P.O. Box 240543 ...,. Charlotte, NC 28224-0543 Phone: 704/529-QJ64 ..,... Fax: 704/525-0409 REPORT TO: Name ~u\..1'\ \\e_ u.._~;Jv\.e_( Address ~ Name 'l.o\" \'-<.~'0><\-.e_( BILL TO: Address Requested Due Dale f_J 1 Day i.J 2 Days \.J 3 Days ·.J 4 Days .J 5 Days • 1.J 6-9 Days ·J Standard 10 days Samples received alter 15:00 will be processed the nexl business day. Turnaround time is based on business days, eKcluding weekends and tlolldays. Sarllples INTACT upon arrival? ;:: 1 ~ Received ON WET ICE? Temp !;b_J PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOlA TILES rec'd W/OUT HEAOSPACE? PROPER CONTAINERS used? Requesled FL Waler Chlorinated NC /sc Yes No Sample Iced Upon Collecllon Yes CMUD NPDES Olher NA No OTHER NA ProjectNamo (\...u...:.~tl -/'V\o••1 h.t·.\\~ ~-•'h! .. (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) PRESS DOWN FIRMLY • 3 COPIES CLIENT DATE SAMPLE DESCRIPTION COLLECTED ~v-I 6 IGI../b 1 f'/1 1,/-l. fv\W-) /"\...,-'1- MI,./-4-S Mw-S" M""-(, f'l\ W-l f1 ~w-co {V\ ¥I-'\ R~uish d By: (Signatute) '{1/. t,.~-"k. .. ..,....-- Retinquished By: (S~;e) (/ Relinquished By: (Signature) Method ol Shipmen~· -.J Fed E• .J UPS Hand-delivered .J Other: TIME COLLECTED MILITARY HOURS '"\ ,lO q_·.so \5. I D \I·. 10 10'.'\{) I ... Ll.i\ ) . -,v lb'.OO 1'\ ·.y) 1'\:'.'5 1 ',' ':>u MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER •TYPE SEE BELOW NO. G" b 6 b b b b 6 b b SIZE PRESERVA- TIVES I~Ll /WD.111., } ' Sampled By (Prinl Name) '1}1 • ~(...'-'t I Received By: (Signature) NPDES: UST: -...J NC I...J NC GROUNDWATER: 0 NC DRINKING WATER: SOLID WASTE: :.J NC :.J NC RCRA: I.J NC usc CERCLA I.J NC usc -' sc .J sc '.J sc :.J sc ,_. sc -' OTHER -' OTHER '.J OTHER -' OTHER ._, OTHER U OTHER U OTHER ANALYSES REQUESTED ,..,v ~~=['\~!~~~~ I , , i I REMARKS Date Additional Comments: Date LANDFILL -' NC -' sc -' OTHER OTHER: -' NC -' sc -' OTHER •cONTAINER TYPE CODES: A =Amber C =Clear G =Glass P =Plastic; TL =Teflon-lined Cap VOA = Volalile Organics Analysis (Zero Hnact Spacnl SUB LAB CERT. IONO. PRISM . LAB IONO. c lt/~~3- /1)~'-1 (I SitS ItS""!{ ~ ll'i>H /IS<JV 1151-11 1/~c; 0 /l'i'i I 1/'iSl- PRISM USE ONLY Site ArrtvaJ Time: Site Departure Time: Fteld Tech Fee: . SEE REVERSE fOR TERMS & CONDITIONS PRisM LABORATORIES, INC. Full Service Analytical & Environmental Solutions P.O.#/Billlng Relerence CHAIN OF C.TODY RECORD . PAGE -.3:_ OF l QUOTE I--------- 449 Springbrook Road ... Charloue. NC 28217 P.O. Box 240543 ... Charlolle, NC 28224-0543 Phone: 704/529-63(i4 ... Fax: 704/525-0409 REPORTTO: Name '::,o~" \\e-"~Lh l ( Address Name ':-.c\_~ \\tVI.'><-\..e.r BILL TO: Address Requested Due Date U 1 Day [J 2 Days U 3 Days ..J 4 Days ..J 5 Days · U 6-9 Days i.J Standard 10 days Samples received alter 15:00 will be processed the next business day. TUrnaround time is based on business days, excluding weekends and holidays Samples INTACT upon arrival? fi.:} 1 j Received ON WET ICE? Temp'-'-- PROPER PRESERVATIVES incticated? ..! Received WITHIN HOLDING TIMES? j / CUSTODY SEALS INTACT? VOLATILES rec'd WIOUT HEADSPACE? ./ PROPER CONTAINERS used? .I Requested FL NC sc Other NA Waler Chlorinated Yes No NA Sample Iced Upon Colteclion Yes No CMUD NPDES OTHER (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) Pmject Name t..\.e<o\<..~( Moor i<,..l."t ~:"\ <-PRESS DOWN FIRMLY • 3 COPIES CLIENT SAMPLE DESCRIPTION DATE COLLECTED PRESERVA· TIVES TIME MATRIX SAMPLE CONTAINER ANALYSES REOUESTE~ ::"\ COLLECTED (SOIL, " ...._-, 1.) Q { MILITARY WATER OR •TYPE ,U '\'-' of'" u -<; Q,'.f. fl:' REMARKS PRISM LAB IDNO. NO. SIZE b VG<r\e":! ~~Li,>INO.;_I'(,.~ HOURS SLUDGE) SEE BELOW l.t...J" '\.1 ..f 4 ~'::/.. 0.. .t1 J:' Q..'u p======+===p===l~;===k7~;==~~=1===1"'T.~S;"'~j=~--~ ·~o ~o~= •~-1 f >.>-,.__,\.•,· ·.~· '"~\· l t ~ • I >QI<~v.i~.J~~~ M\J-10 b /~/0\ 1 o·. ro V'--'.>.,er \\<,}-r V(,~ SUB LAB CERT. IONO. l'5'i3 It; r;t./ 1/.;s.; /lt;')t, (t\v..l-\\ .v \t'.)U .v 6 -¥ ~ I $oz. - I 8 c·,_ I Bo<-. I g o-z. . - { e uz..... I Co-z.. EG-IA (tf.o') i1-Lt(or (3,: /)'0 JOIL (1 H-ICb) (o. ~') t~~j; c:S:ts-$P•'-G lf-e(f)~o·) ( 3: 3<> .SetL 4 lf-U,(A.) l.o ') ~~Of (1.;<-{o ~-i'-(, /HfQCt.)~'') ~jzif:'t t'f.'(JV So(L (~ Jt-2-$CC) (L"J ~12..4>/0f /f:3o JorL. 4 Sampler's Signature ftA. < tc t-r Yo---• Sampled By (Print Name) -..) 1 Received By: (Signature) Aellnq/fi/.8~~~ Relinquished By: {Signatu~---7 Relinquished By: {Signature) Method ol Shit:oment .J Fed El( .J UPS Hand-delivered .J Other: NPDES: . .J NC •.J sc .J OTHER UST: ·.J NC .J sc .J OTHER GROUNDWATER: DRINKING WATER: SOLID WASTE: UNC UNC '.JNC t:JSC 'JSC ..JSC '.J OTHER U OTHER .J OTHER RCRA: W NC .J sc '.J OTHER CERCLA U NC •.J sc· . .J OTHER Date LANDFILL .J NC .J sc .J OTHER IV"' ' I/"-: . I~~ I ~~ ;,yl I 1 ,_I I ,/' I ' I •, Affiliation ("\: OTHER: .J NC .J sc .J OTHER Additional Comments: "CONTAINER TYPE CODES: A =Amber C =Clear G =Glass P =Plastic: TL = Teflon·Lined Cap VOA =Volatile Organics Analys1s (Zero Hean Spar:ol tS57 II~~ /1'}')'1 !6h0 PRISM USE ONLY Site Arrival Ttme: Site Departure Time: Field Tech Fee: SEE REVERSE FOR TERMS & CONDITIONS • • • Lab Report .,.;~ !l,!~M. [Rj[Z;~J;®~]fm ~~--... -·-· .... ~ ' Full Service Analytical & Environmental Solutions 6/22/01 Page 1 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: WS-1 PO Box 669004 Prism Sam ole 10: AC10513 Charlotte, NC 28266 Loqin Group: MK621H5 Sample Collection Date/Time: 6/14/01 11:00 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErriME PARAM.~TER RESULT UNIT§. __ LIMIT REFERENCE STARTED ANALYST METALS DIGESTION Completed EPA 200.7 6/18/01 12:20 LC2 ANTIMONY, TOTAL 0.007 mg/L 0.002 EPA 200.7 6/19/0111:35 MSP ARSENIC,.TOTAL Less than mg/L 0.010 EPA 200.7 6/19/01 11:35 MSP BERYLLIUM, TOTAL Less than mg/L 0.001 EPA 200.7 6/19/01 11:35 MSP CADMIUM, TOTAL Less than mg/L 0.005 EPA 200.7 6/19/0111:35 MSP CHROMIUM, TOTAL Less than mg/L 0.005 EPA 200.7 6/19/0111:35 MSP COPPER, TOTAL Less than mg/L 0.010 EPA 200.7 6/19/01 11:35 MSP LEAD, TOTAL Less than mg/L 0.005 EPA 200.7 6/19/0111:35 MSP NICKEL, TOTAL Less than mg/L 0.010 EPA 200.7 6/19/01 11:35 MSP SELENIUM, TOTAL Less than mg/L 0.010 EPA 200.7 6/19/01 11 :35 MSP SILVER, TOTAL Less than mg/L 0.005 EPA 200.7 6/19/0111:35 MSP THALLIUM, TOTAL Less than mg/L 0.01 EPA 200.7 6/19/01 11:35 MSP ZINC, TOTAL 0.077 mg/L 0.010 EPA 200.7 6/19/01 11:35 MSP MERCURY, TOTAL Less than mg/L 0.0002 EPA 245.1 6/21/01 15:55 PRF MERCURY DIGESTION Completed EPA 245.1 6/20/01 11:50 LC2 PREP. METHOD 3510 Completed SW846-3510 6/19/01 07:00 JDP BENZENE Nat detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP BROMOBENZENE Not detected ug/L 5.0 SW846-8260B 6/19/0116:59 MP BROMOCHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6/19/0116:59 MP BROMODICHLOROMETHANE Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP BROMOFORM Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP BROMOMETHANE Not detected ug/L 10 SW846-8260B 6/19/01 16:59 MP N-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP SEC-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP TERT-BUTYLBENZENE Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP CHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP CHLOROOIBROMOMETHANE Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP CHLOROETHANE Not detected ug/L 10 SW846-8260B 6/19/0116:59 MP CHLOROFORM 9.3 ug/L 5.0 SW846-8260B 6/19/01 16:59 MP NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: 1-800/529-6364 ..... Fax: 704/525-0409 • • • Lab Report PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions 6/22/01 Page 2 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: WS-1 PO Box 669004 Prism Sam ole 10: AC10513 Charlotte, NC 28266 LoQin Group: MK621H5 Sample Collection Date/Time: 6/14/01 11:00 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESU_I,T ______ !!NITS LIMIT REFERENCE STARTED ANALYST CHLOROMETHANE Not detected .ug/L 10 SW846-82608 6/19/01 16:59 MP 2-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 4-CHLOROTOLUENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 10 SW846-82608 6/19/0t 16:59 MP 1 ,2-DIBROMOETHANE Not detected ug/L ·5.0 SW846-82608 6/19/01 16:59 MP DIBROMOMETHANE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1 ,2-D\CHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1 ,3-DICHLOROBENZENE Not detected ug/L . 5.0 · SW846-82608 6/19/01 16:59 MP 1 ,4-DICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP DICHLORODIFLUOROMETHANE Not detected ug/L 10 SW846-82608 6/19/01 16:59 MP 1, 1-D\CHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1 ,2-DICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1, 1-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP CIS-1 ,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP TRANS-1 ,2-DICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1 ,2-DICHLOROPROPANE Not detected ug/L 5.0 sw 846-82608 6/19/01 16:59 MP 1 ,3-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 2,2-DICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1, 1-DICHLOROPROPENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP ETHYLBENZENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP HEXACHLOROBUTADIENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP ISOPROPYLBENZENE Not detected ug/L 5.0 SW846-82608. 6/19/01 16:59 MP P-ISOPROPYL TOLUENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP METHYLENE CHLORIDE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP NAPHTHALENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP N-PROPYLBENZENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP STYRENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1,1, 1 ,2-TETRACHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1,1 .2,2-TETRACHLOROETHANE Not detected _ug/L 5.0 SW846-82608 6/19/01 16:59 MP TETRACHLOROETHENE Not detected ug/L 5.0 SW846:82608 6/19/01 16:59 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...,. P.O. Box 240543 ....._ Charlotte, NC 28224-0543 Phone: 704/529-6364 .., Toll Free Number: 1-800/529-6364 .., Fax: 704/525-0409 • • • Lab Report A~~~ Full Service Analytical & Environmental Solutions 6/22/01 Page 3 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: WS-1 PO Box 669004 Prism Samole 10: AC10513 Charlotte, NC 28266 Loain Group: MK621H5 · Sample Collection Date/Time: 6/14/01 . 11:00 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEffiME PARAMET.E!L_ __ RESULT UNITS LIMIT REFERENCE STARTED ANALYST TOLUENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1 ,2,3-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP· 1 ,2,4-TRICHLOROBENZENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1, 1, 1-TRICHLOROETHANE Not detected ug/L 5.0 SW846-82608 6/19/0116:59 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP TRICHLOROETHENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP TRICHLOROFLUOROMETHANE Not detected ug/L 10 SW846-8260B 6/19/01 16:59 MP 1,2,3-TRICHLOROPROPANE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1 ,2,4-TRIMETHYLBENZENE Not detected ug/L 5.0 SW846-82608 6/19/01 16:59 MP 1 ,3,5-TRIMETHYLBENZENE Not detected ug/L-5.0 SW846-82608 6/19/01 16:59 MP · VINYL CHLORIDE Not detected ug/L 10 SW846-8260B 6119101 16:59 MP TOTAL XYLENES Not detected ug/L s.o SW846-82608 6/19/01 16:59 MP cis-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/19/01 16:59 MP trans-1 ,3-DICHLOROPROPENE Not detected ug/L 5.0 SW846-8260B 6/19/0116:59 MP ACETONE Not detected ug/L 50 SW846-8260B 6/19/01 16:59 MP 2-BUTANONE (MEK) Not detected ug/L 10 SW846-82608 6/19/01 16:59 MP CARBON DISULFIDE Not detected ug/L 50 SW846-82608 6/19/01 16:59 MP CARBON TETRACHLORIDE Not detected ug/L 5.0 SW846-8260B 6/19/0116:59 MP 2-CHLOROETHYLVINYLETHER Not detected ug/L 10 SW846-8260B 6/19/01 16:59 MP 2-HEXANONE Not detected ug/L 10 SW846-8260B 6/19/01 16:59 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/L 10 SW846-8260B 6/19/01 16:59 MP -------- 2-CHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/20101 19:16 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/L tO SW846-8270C 6/20/01 19:16 HWC PHENOL Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 1,3-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/20101. 19:16 HWC 1,2-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 612010119:16 HWC 1.4-DICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/L 10 SW846-8270C 6120/01 19:16 HWC 2-METHYL PHENOL (0 CRESOL) Not detected ug/L 10 SW846-8270C 6/20/0119:16 HWC NC Certification No. 402 ~C Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report .~f.!!~~.· ~·-~ Full Service Analytical & Environmental Solutions 6/22/01 Page 4 of 29 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: WS-1 PO Box.669004 Prism Sam ole ID: AC10513 Charlotte, NC 28266 Looin Group: MK621H5 Sample Collection Date/Time: 6/14/01 11:00 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST HEXACHLOROETHANE Not detected ug/L 10 SW846-8270C 6/20/01 19: 16 HWC N-NITROSO-DI-N-PROPYLAMINE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC NITROBENZENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 4-METHYL PHENOL (P CRESOL) Not detected ug/L 10 SWB46·8270C 6/20/01 19:16 HWC ISOPHORONE Not detected ug/L io SW846-8270C 6/20/01 19:16 HWC 2-NITROPHENOL Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 4-NITROPHENOL Not detected ug/L 50 SW846-8270C 6/20/01 19:16 HWC 2,4 DIMETHYL PHENOL Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 815(2-CHLOROETHOXY)METHANE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 1 ,2.4 TRICHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC HEXACHLOROBUTADIENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 2-METHYL NAPHTHALENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 4-CHLOR0-3-METHYL PHENOL Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 2,4,6 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 2-CHLORONAPHTHALENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 2,4,5 TRICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC ACENAPHTHYLENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC DIMETHYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 2,6-DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 2.4-DICHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC ACENAPHTHENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC DIBENZOFURAN Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC 2.4 DINITROPHENOL Not detected ug/L 50 SW846-8270C 6/20/01 19:16 HWC 2,4 DINITROTOLUENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC FLUORENE Not detected ug/L .10 SW846-8270C 6/20/01 19:16 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC DIETHYL PHTHALATE Not detected ug/L . 10 SW846-8270C 6/20/01 19:16 HWC 4,6-DINITR0-2-METHYL PHENOL Not detected ug/L 50 SW846-8270C 6/20/01 19:16 HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..., P.O. Box 240543 ..., Charlotte, NC 28224-0543 Phone: 704/529-6364 ..., Toll Free Number: 1-800/529·6364 ..., Fax: 704/525-0409 • • • Lab Report 6/22/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project tO: Customer Sam pte ID: Prism Sample ID: LoQin Grouo: Sample Collection Date/Time: Lab Submittal Date/Time: Full Service Analytical & Environmental Solutions Page 5 of 29 Cherokee-Mooresville Site WS·1 AC10513 MK621H5 6/14/01 11 :00 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST N-NITROSODIPHENYLAMINE Not detected ug/L 10 SW846·8270C 6/20/01 19:16 HWC 4-BROMOPHENYL PHENYL ETHER Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC HEXACHLOROBENZENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC PENTACHLOROPHENOL Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC ANTHRACENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC DI-N-BUTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC PYRENE ,·, Not detected ug/L 10 SW846:8270C 6/20/01 19:16 HWC BUTYL BENZYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC CHRYSENE Not detected ug/L 10 SW846-8270C 6/20/0119:16 HWC BENZO(A)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC DI-N-OCTYL PHTHALATE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC BENZO(B)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC BENZO(K)FLUORANTHENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC BENZO(A)PYRENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC INDEN0(1 ,2,3-C,D)PYRENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/L 10 SW846-8270C 6/20/01 19:16 HWC BENZO(G,H,I)PERYLENE Not detected ug/L 10 SW846-8270C 6/20/0119:16 HWC PHENANTHRENE Not detected ug/L 10 SW846-8270C 6/2010119:16 HWC --------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report 6/22/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental SOlutions Page 6 of 29 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: A-2 {1-1.5) Prism Samole 10: AC10514 LoQin Group: MK621 H5 Sample Collection Oaterrime: 6/14/01 12:30 Lab Submittal Daterrime: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 79 %DRYWT. O.Q1 SM 2540G 6/19/01 17:05 JLW METALS DIGESTION METHOD 3050 Completed SW846-3050 6/15/01 13:15 LC2 PREP. METHOD 3550 Completed SW846-3550B 6/18/01 20:00 JLW ANTIMONY, TOTAL 1.0 mg/kg 1.0 SW846-6010B 6/18/01 21:14 MSP ARSENIC, TOTAL 4.4 . mg/kg 1.0 . SW846-6010B . 6/18/01 21:14 MSP BERYLLIUM, TOTAL Less than mg/kg 1.0 SW846-6010B 6/18/01 21:14 MSP CADMIUM, TOTAL Less than mg/kg 1.0 SW846-6010B 6/18/01 21:14 MSP CHROMIUM, TOTAL 12 mg/kg 1.0 SW846-6010B 6/18/01 21:14 MSP COPPER, TOTAL 5.6 mg/kg 2.0 SW846·6010B 6/18/01 21:14 MSP LEAD, TOTAL 15 mg/kg 1.0 SW846-601 OB 6/18/01 21:14 MSP NICKEL, TOTAL 7.0 mg/kg 1.0 SW846-601 OB 6/18/01 21:14 . MSP SELENIUM, TOTAL Less than mg/kg 2.0 SW846·601 OB 6/18/01 21:14 MSP SILVER, TOTAL Less than mg/kg 2.0 SW846·601 OB 6/18/01 21:14 MSP THALLIUM, TOTAL Less than mg/kg 0.5 SW846·601 OB 6/18/01 21:14 MSP ZINC, TOTAL 48 mg/kg 1.0 SW846·601 OB 6/18/01 21:14 MSP MERCURY, TOTAL 0.03 mg/kg 0.03 SW846-7471 6/21/01 14:48 PRF MERCURY DIGESTION Completed SW846-7471 6/20/01 10:40 LC2 BENZENE Not detected ug/kg 6.0 SW846·8260B 6/20/01 01:35 CMB BROMOBENZENE Not detected ug/kg 6.0 SW846·8260B 6/20/01 01:35 CMB BROMOCHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB BROMODICHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB BROMOFORM Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB BROMO METHANE Not detected ug/kg 12.0 SW846-8260B 6/20/01 01:35 CMB N-BUTYLBENZENE Not detected ug/kg 6.0 SW846·8260B 6/20/01 01:35 CMB SEC-BUTYLBENZENE Not detected ug/kg 6.0 SW846·8260B 6/20/01 01:35 CMB TERT-BUTYLBENZENE Not detected uglkg 6.0 SW846-8260B 6/20/01 01:35 CMB CARBON TETRACHLORIDE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB CHLORODIBROMOMETHANE Not detected ug/kg 6.0 SW846·8260B 6/20/01 01:35 CMB CHLOROETHANE Not detected ug/kg 12.0 SW846-8260B 6/20/01 01:35 CMB NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..o.. P.O. Box 240543 ..o.. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o.. Toll Free Number: 1·800/529·6364 ..o.. Fax: 704/525-0409 -------- • • • ........ Lab Report ~;~~~ Full Service Analytical & Environmental Solutions 6/22/01 Page 7 of29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: A-2 (1-1.5) PO Box 669004 Prism Samole 10: AC10514 Charlotte. NC 28266 LoQin Group: MK621H5 Sample Collection Date/Time: 6/14/01 12:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CHLOROFORM Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB CHLOROMETHANE Not detected ug/kg 12.0 SW846-82608 6/20/01 01:35 CMB 2-CHLOROTOLUENE Not detected uglkg 6.0 SW846-82608 6/20/01 01:35 CMB 4-CHLDROTOLUENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/kg 12:0 SW846-82608 6/20/01 01:35 CMB 1,2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB DIBROMOMETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB 1,2-DICHLOROBENZENE Not detected uglkg 6.0 SW846-S260B 6/20/01 01:35 CMB 1,3-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB 1,4-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB 1,1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB 1,2-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB 1,1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB CIS-1,2'DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB TRANS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB 1,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB 1,3-DICHLOROPROPANE Not detected uglkg 6.0 SW846-82608 6/20/01 01:35 CMB 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB 1,1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB ETHYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB HEXACHLOROBUTADIENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB ISOPROPYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB P-ISOPROPYLTOLUENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-8260B 6/20/01 01:35 CMB NAPHTHALENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB STYRENE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB 1,1,1,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 01:35 CMB 1,1,2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 01:35 CMB NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..._ P.O. Box 240543 ..._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ..._Toll Free Number: 1-800/529-6364 ..._Fax: 704/525-0409 -·::·~'"! • ,1_\' Lab Report -~~~!~h. . .-r:'l}!j'~:-~ • Full Service Analytical & Environmental Solutions 6/22/01 Page 8 of 29 Mid-Atlantic Associates Customer Project tO: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: A-2 (1-1.5) PO Box 669004 Prism Sam ole 10: AC10514 Charlotte, NC 28266 Looin Group: MK621H5 Sample Collection Date!Time: 6/14/01 12:30 Lab Submittal Date!Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST TETRACHLOROETHENE Not detected ug/kg 6.0 SW846·8260B 6120101 01:35 CMB TOLUENE Not detected ug/kg 6.0 SWB46·8260B 6120101 01:35 CMB 1 ,2,3-TRICHLOROB.ENZENE Not detected ug/kg 6.0 SW846-8260B 6120101 01:35 CMB 1.2.4-TRICHLOROBENZENE Not detected ug/kg 6.0 SWB46-8260B 6120101 01:35 CMB 1,1, 1·TRICHLOROETHANE Not detected ug/kg 6.0 SWB46-8260B 6120101 01 :35 CMB 1, 1.2-TRICHLOROETHANE Not detected ug/kg 6.0 SWB46-8260B 6120101 01:35 CMB TRICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6120101 01:35 CMB TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6120101 01:35 CMB • 1 ,2,3· TRICHLOROPROPANE Not detected ug/kg 6.0 SWB46-8260B 6/20101 01:35 CMB 1 ,2.4-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6120101 01:35 CMB 1.3,S-TRIMETHYLBENZEN E Not detected ug/kg 6.0 SW846·8260B · 6/20/01 01:35 CMB VINYL CHLORIDE Not detected ug/kg 12.0 SW846-8260B 6120101 01:35 CMB 'TOTAL XYLENES Not detected ug/kg 6.0 SW846·8260B 6120101 01:35 CMB 2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-8260B 6120101 01:35 CMB 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 SWB46-8260B 6120101 01:35 CMB 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-82SOB 6120101 01:35 CMB ACETONE Not detected ug/kg 120.0 SW846-8260B 6120101 01:35 CMB CARBON DISULFIDE Not detected ug/kg 120.0 SWB46-8260B 6120101 01:35 CMB VINYL ACETATE Not detected ug/kg 60.0 SWB46-8260B 6120/01 01:35 CMB CIS-1 ,3-DICHLOROPROPENE Not detected ug/kg 6.0 SWB46-8260B 6120101 01:35 CMB TRANS-1 ,3-DICHLOROPROPENE Not detected ug/kg 6.0 SWB46-8260B 6120101 01:35 CMB 2-HEXANONE Not detected ug/kg 60.0 SWB46-8260B 6/20101 01:35 CMB IPE Not detected ug/kg 6.0 SW846-8260B 6120101 01:35 CMB MTBE Not detected ug/kg 6.0 SW846-8260B 6120/01 01:35 CMB SURR:DIBROMOFLUOROMETHANE 114 % 70-130 SW846-8260B 6120101 01:35 CMB SURR:TOLUENE-DB 116 % 70-130 SW846-8260B 6120101 01:35 CMB SURR:BROMOFLUOROBENZENE 107 % 70-130 SW846-8260B 6120101 01:35 CMB ----------• ACENAPHTHENE Not detected ug/kg 420 SW846-8270C 6120101 02:59 HWC ACENAPHTHYLENE Not detected ug/kg 420 SWB46-8270C 6/20/01 02:59 HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 ...._ Charlotte, NC 28224-0543 Phone: 704/529-6364 .o. Toll Free Number: 1-800/529-6364 .o. Fax: 704/525-0409 Lab Report ::.~!~{:· . ··., PRISM LA~ATORIE~,INC. • Full Service Analytical & Environmental Solutions 6/22/01 Page 9 of 29 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: A-2 (1-1.5) PO Box 669004 Prism Samole ID: AC10514 Charlotte, NC 28266 Loqin Group: MK621H5 Sample Collection Date/Time: 6/14/01 12:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST ANTHRACENE Not detected ug/kg . 420 SW846-8270C 6/20/01 02:59 HWC 8ENZO(A)ANTHRACENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 8ENZ0(8)FLUORANTHENE . Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 8ENZO(K)FLUORANTHENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 8ENZO(A)PYRENE Not detected uglkg 420 SW846-8270C 6/20/01 02:59 HWC 8ENZO(GHI)PERYLENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 81S(2-CHLOROETHOXY)METHANE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 81S(2-CHLOROETHYL)ETHER Not detected uglkg 420 SW846-827o"C 6/20/01 02:59 HWC • 81S(2-CHLOROISOPROPYL)ETHER Not detected uglkg 420 SW846-8270C 6/20/01 02:59 HWC 81S(2-ETHYLHEXYL)PHTHALA TE Not detected uglkg 420 SW846-8270C 6/20'01 02:59 HWC 4-8ROMOPHENYL PHENYL ETHER Not detected · uglkg 420 SW846-8270C 6/20/01 02:59 HWC 8UTYL8ENZYLPHTHALATE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 4-CHLOR0-3-METHYLPHENOL Not detected uglkg 420 SW846-8270C 6/20/01 02:59 HWC 2-CHLORONAPHTHALENE Not detected uglkg 420 SW846-8270C 6/20/01 02:59 HWC 2-CHLOROPHENOL Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 420" SW846-8270C 6/20/01 02:59 HWC CHRYSENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC DI8ENZO(A,H)ANTHRACENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC D18ENZOFURAN Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC DI-N-8UTYLPHTHALA TE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 1,2-DICHLOR08ENZENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 1,3-DICHLOR08ENZENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 1 .4-DICHLOR08ENZENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 2,4-DICHLOROPHENOL Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC DIETHYL PHTHALATE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 2,4-DIMETHYLPHENOL Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC DIMETHYL PHTHALATE Not detected uglkg 420 SW846-8270C 6/20/01 02:59 HWC 2,4-DINITROPHENOL Not detected ug/kg 2100 SW846-8270C 6/20/01 02:59 HWC • 2.4-DINITROTOLUENE Not detected ug/kg 420 SW646-8270C 6/20/01 02:59 HWC 2.6-DINITROTOLUENE Not detected ug/kg 420 SW646-8270C 6/20/01 02:59 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..a.. P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o.. Toll Free Number: 1-800/529-6364 ..o.. Fax: 704/525-0409 • • • Lab Report 6/22101 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 ... '-. , .... ''{"t.J!' ~ ~!;.~. d •• ..r(i~. Full Servica Analytical & Environmental Solutions Page 10 of 29 Customer Project 10: Cherokee-Mooresville Site Customer Sample _10: A-2 (1-1.5) Prism Samcle 10: AC10514 Loqin Group: MK621 H5 Sample Collection Date/Time: 6/14/01 12:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT · REFERENCE STARTED ANALYST - DI-N-OCTYLPHTHALATE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC FLUORANTHENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC FLUORENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC HEXACHLOROBENZENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC HEXACHLOROBUTADIENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC HEXACHLOROETHANE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC INDEN0(1 ,2,3-CD)PYRENE Not detected ug/kg 420 SW84S-8270C 6/20/01 02:59 HWC ISOPHORONE Not detected ug/kg 420 SW646-8270C 6/20/01 02:59 HWC 2-METHYL-4,6-DINITROPHENOL Not detected ug/kg 2100 SW646-8270C 6/20/01 02:59 HWC 2-METHYL NAPHTHALENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 2-METHYL-PHENOL Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 4-METHYL-PHENOL Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC NAPHTHALENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC NITROBENZENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 2-NITROPHENOL Not detected ug/kg 420 SW846-8270C 6/20i01 02:59 HWC 4-NITROPHENOL Not detected ug/kg 2100 SW846-8270C 6/20/01 02:59 HWC N-NITROSODIPHENYLAMINE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC N-NITROSODI-N-PROPYLAMINE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC PENTACHLOROPHENOL Not detected ug/kg 2100 SW846-8270C 6/20/01 02:59 HWC PHENANTHRENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC PHENOL Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC PYRENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 1.2,4-TRICHLOROBENZENE Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 2,4,5-TRICHLOROPHENOL Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC 2.4,6-TRICHLOROPHENOL Not detected ug/kg 420 SW846-8270C 6/20/01 02:59 HWC ---------- NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ....._ P.O. Box 240543 .... Charlotte, NC 28224MOS43 Phone' 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report 6/22/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 11 of 29 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: A-2 (1-1.5) Prism Sample 10: AC10514 Looin Group: MK621 H5 Sample Collection Date/Time: 6/14/01 12:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER Sample Comments: TEST RESULT Angela D. Overcash, V.P. Laboratory Services ·. ~ . REPORTING METHOD . UNITS LIMIT REFERENCE DATEfTIME STARTED ANALYST NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 .... Charlotte, NC 28224~0543 Phone: 704/529-6364 ~Toll Free Number: 1-800/529-6364 ~Fax: 704/525-0409 • • • Lab Report 6/22/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page 12of29 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: Q-1 Prism Samole 10: AC10515 Looin Group: MK621 H5 Sample Collection Date/Time: 6/14/01 13:00 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER . CALCULATIONS BASED ON DRY WT. METALS DIGESTION METHOD 3050 PREP. METHOD 3550-PCB PREP. METHOD 3550 ANTIMONY, TOTAL ARSENIC, TOTAL BERYLLIUM, TOTAL CADMIUM, TOTAL CHROMIUM, TOTAL COPPER, TOTAL LEAD, TOTAL NICKEL, TOTAL SELENIUM, TOTAL SILVER, TOTAL THALLIUM, TOTAL ZINC, TOTAL MERCURY, TOTAL MERCURY DIGESTION PCB-1016. PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 PCB-1262 PCB-1268 BENZENE BROMOBENZENE TEST RESULT 82 Completed Completed Completed 3.2 8.4 Less than Less than 30 110 48 16 Less than Less than Less than 120 0.02 Completed Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected UNITS %DRYWT. mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg . mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg uglkg ug/kg REPORTING METHOD DATEfTIME STARTED LIMIT REFERENCE 0.01 1.0 1.0 1.0 1.0 1.0 2.0 ·1.0 1.0 2.0 2.0 0.5 1.0 0.02 5.0 10 5.0 5.0 5.0 5.0 5.0 5.0 5.0 6.0 6.0 SM 2540 G 6/19/01 17:05 SW846-3050 6/15/0113:15 SW846-3550 6/15/01 12:00 SW846-3550B 6/18/01 20:00 SW846-6010B ' 6i1S/01 21:21 SW846-6010B 6/18/01 21:21 SW846-60108 6/18/01 21:21 SW846-60108 6/18/01 21:21 SW846-6010B 6/18/01 21:21 SW846-6010B 6/18/01 21:21 SW846-6010B 6/18/01 21:21 SW846-6010B 6/18/01 21:21 SW846-6010B 6/18/01 21:21 SW846-6010B 6/18/01 21:21 SW846-6010B 6/18/01 21:21. SW846-601 08 6/20/01 13:29 SW846-7471 6/21/01 14:59 SW846-7471 SW846-8082 SW846-8082 SW846-8082 SW846-8082 SW846-8082 SW846-8082 SW846-8082 SW846-8082 SW846-8082 6/20/01 10:40 6/22/01 09:54 6/22/01 09:54 6/22/01 09:54 6/22/01 09:54 6/22/01 09:54 6/22/01 09:54 6/22/01 09:54 6/22/01 09:54 6/22/01 09:54 SW846-8260B 6/20/01 02:20 SW846-82608 6/20/01 02:20 ANALYST JLW LC2 ·JMV JLW MSP MSP MSP MSP MSP MSP MSP MSP MSP MSP MSP MSP PRF LC2 CWA CWA CWA CWA CWA CWA CWA CWA CWA CMB CMB NC Certification No. 402 SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... ToU Free Number: l-800/529-6364 .... Fax: 704/525-0409 • • • .:~~·. Lab Report ~.·.~~JM -" ' :::::..;::" Full Service Analytical & Environmental Solutions 6/22/01 Page 13 of29 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: Q-1 PO Box 669004 Prism Sam ole ID: AC10515 Charlotte, NC 28266 Loqin Group: MK621H5 Sample Collection Date/Time: 6/14/01 13:00 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESUlT UNITS LIMIT REFERENCE STARTED ANALYST BROMOCHLOROMETHANE · Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB BROMODICHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB BROMOFORM Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB BROMOMETHANE Not detected ug/kg 12.0 SW846-8260B · 6120101 02:20 CMB N-BUTYLBENZENE Not detected ug/kg 6.0 . SW846-8260B 6120101 02:20 CMB SEC-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB TERT-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB CARBON TETRACHLORIDE · Not detected ug/kg · ·6.0 SW846-8260B 6120101 02:20 CMB CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB CHLORODIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB CHLOROETHANE Not detected ug/kg 12.0 SW846-8260B 6120101 02:20 CMB CHLOROFORM Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB CHLOROMETHANE Not detected ug/kg 12.0 SW846-8260B 6120101 02:20 CMB 2-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 4-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-8260B 6120101 02:20 CMB 1 ,2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB DIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 1 ,2-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 1 ,3-DICHLOROBENZENE Not detected · ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 1 A-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6120101.02:20 CMB DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 1, 1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 1 ,2-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 1, 1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB CIS-1 ,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB TRANS-1 ,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 1 ,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 1 ,3-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6120101 02:20 CMB NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ......_ P.O. Box 240543 ......_ Charlotte, NC 28224·0543 Phone: 704/529-6364 .... Toll Free Number: t -800/529-6364 ...,. Fax: 704/525-0409 ' ··'•• Lab Report --<~~,§i • Full Service Analytical & Environmental Solutions 6/22/01 Page 14 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: Q-1 PO Box 669004 Prism Sam ole 10: AC10515 Charlotte, NC 28266 Looin Group: MK621H5 Sample Collection Date/Time: 6/14/01 13:00 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 1, 1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB ETHYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB HEXACHLOROBUTADIENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 02:20 CMB ISOPROPYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB P-ISOPROPYLTOLUENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 02:20 CMB METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-82608 6/20/01 02:20 CMB NAPHTHALENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB • STYRENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB 1,1, 1 ,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB TETRACHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB TOLUENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 02:20 CMB 1 ,2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB 1 ,2,4-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6120101 02:20 CMB 1,1, 1-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB 1,1 ,2-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB TRICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB 1 ,2,3-TRICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 02:20 CMB 1 ,2,4-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-82608 6120101 02:20 CMB 1 ,3,5-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB VINYL CHLORIDE Not detected ug/kg 12.0 SW846-82608 6/20/01 02:20 CMB TOTAL XYLENE$ Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CMB 2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-8260B 6/20/01 02:20 CMB 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 SW846-82608 6/20/01 02:20 CMB 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260B 6/20/01 02:20 CMB ACETONE Not detected ug/kg 120.0 SW846-8260B 6/20/01 02:20 CMB • CARBON DISULFIDE Not detected ug/kg 120.0 SW846-82608 6/20/01 02:20 CMB VINYL ACETATE Not detected ug/kg 60.0 SW846-82608 6/20/01 02:20 CMB NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road A. P.O. Box 240543 A. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o.. Toll Free Number: t-800/529-6364 ..o.. Fax: 704/525-0409 Lab Report 'PRISM • • • LABORATORIES, INC. Full Service Analytical & Environmental Solutions 6/22101 Page 15 of 29 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: Q-1 PO Box 669004 Prism Sample ID: AC10515 Charlotte, NC 28266 LoQin Group: MK621H5 Sample Collection Date/Time: 6/14/01 13:00. Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CIS-1 ,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CM8 TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CM8 2-HEXANONE Not detected ug/kg 60.0 SW846·82608 6/20/01 02:20 CM8 IPE Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CM8 MT8E Not detected ug/kg 6.0 SW846-82608 6/20/01 02:20 CM8 SURR:DI8ROMOFLUOROMETHANE 125 % 70-130 SW846-82608 6/20/01 02:20 CM8 SURR:TOLUENE-DB 119 % 70-130 SW846·82608 6/20/01 02:20 CM8 SURR:8ROMOFLUOR08ENZENE 129 % 70-130 SW846-82608 6/20/01 02:20 CM8 ~-------- ACENAPHTHENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC ACENAPHTHYLENE Not detected ug/kg 2000 SW846·8270C 6/20/01 03:44 HWC ANTHRACENE Not detected ug/kg 2000 SW846·8270C 6/20/01 03:44 HWC 8ENZO(A)ANTHRACENE Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 8ENZ0(8)FLUORANTHENE Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 8ENZO(K)FLUORANTHENE Not detected ug/kg 2000 5W846·8270C 6/20/01 03:44 HWC 8ENZO(A)PYRENE Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 8ENZO(GHI)PERYLENE Not detected ug/kg 2000 5W846·8270C 6/20/01 03:44 HWC 815(2-CHLOROETHOXY)METHANE Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 815(2-CHLOROETHYL)ETHER Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 815(2-CHLOR0150PROPYL)ETHER Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 815(2-ETHYLHEXYL)PHTHALATE Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 4-8ROMOPHENYL PHENYL ETHER Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 8UTYL8ENZYLPHTHALATE Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 4-CHLOR0-3-METHYLPHENOL Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 2-CHLORONAPHTHALENE Not detected ug/kg 2000 5W846·8270C 6/20/01 03:44 HWC 2-CHLOROPHENOL Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC CHRYSENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC DI8ENZO(A,H)ANTHRACENE Not detected ug/kg 2000 5W846·8270C 6/20/01 03:44 HWC DI8ENZOFURAN Not detected ug/kg 2000 5W846-8270C 6/20/01 03:44 HWC NC Certification No. 402 -5C Certification No. 99012 • NC Drinking Water Cert. No. 37735 • FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ...._Toll Free Number: 1-800/529-6364 ...._Fax: 704/525-0409 • • • Lab Report -~~~~!! Full Service Analytical & Environmental Solutions 6/22/01 Page 16 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: Q-1 PO Box 669004 Prism Sam ole 10: AC10515 Charlotte, NC 28266 LoQin Group: MK621H5 Sample Collection Date/Time: 6/14/01 13:00 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST DI-N-BUTYLPHTHALATE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC 1,2-DICHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC 1,3-DICHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC 1,4·DICHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC 2,4-DICHLOROPHENOL Not detected ug/kg 2000 SW846·8270C 6/20/01 03:44 HWC DIETHYL PHTHALATE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC 2,4-DIMETHYLPHENOL Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC DIMETHYL PHTHALATE Not detected ug/kg 2000 SW846·8270C 6/20/01 03:44 HWC 2.4-DINITROPHENOL Not detected ug/kg 10000 SW846-8270C 6/20/01 03:44 HWC 2,4-DINITROTOLUENE Not detected uglkg 2000 SW846·8270C 6/20/01 03:44 HWC 2,6-DINITROTOLUENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC DI-N-OCTYLPHTHALA TE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC FLUORANTHENE Not detected ug!kg 2000 SWB46-8270C 6/20/01 03:44 HWC FLUORENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC HEXACHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC HEXACHLOROBUTADIENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC HEXACHLOROETHANE Not detected ug/kg 2000 SW846·B270C 6/20/01 03:44 HWC INDEN0(1,2,3·CD)PYRENE Not detected ug/kg 2000 SWB46-8270C 6/20/01 03:44 HWC ISOPHORONE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC 2-METHYL-4,6-DINITROPHENOL Not detected ug/kg 10000 SW846-8270C 6/20/01 03:44 HWC 2·METHYL NAPHTHALENE Not detected ug/kg 2000 SWB46-8270C 6/20/01 03:44 HWC 2-METHYL-PHENOL Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC 4·METHYL·PHENOL Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC NAPHTHALENE Not detected ug/kg 2000 SW846·8270C 6/20/01 03:44 HWC NITROBENZENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC 2-NITROPHENOL Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC 4-NITROPHENOL Not detected ug/kg 10000 SWB46-8270C 6/20/01 03:44 HWC N-NITROSODIPHENYLAMINE Not detected ug/kg 2000 SW846·8270C 6/20/01 03:44 HWC N-NITROSODI·N-PROPYLAMINE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 HWC NC Certification No. 402 • SC Certification No. 99012 • NC DrinkinQ Water Cert. No. 37735 • FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o. Toll Free Number: 1-800/529-6364 ..o. Fax: 704/525·0409 Lab Report • • • Full Service Analytical & Environmental Solutions 6/22/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Page 17 of 29 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: Q-1 Prism Samole 10: AC10515 Loqin Group: MK621 H5 Sample Collection Date/Time: 6/14/01 13:00 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST PENTACHLOROPHENOL Not detected ug/kg 10000 SW846·8270C 6/20/01 03:44 PHENANTHRENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 PHENOL Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 PYRENE Not detected ug/kg 2000 SWB46-8270C 6/20/01 03:44 1 ,2,4-TRICHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 2,4,5-TRICHLOROPHENOL Not detected ug/kg 2000 SW846-8270C 6/20/01 03:44 2,4,6-TRICHLOROPHENOL Not detected ug/kg 2000 SWB46-8270C 6/20/01 03:44 --------- Sample Comments: Analysis note for SW-846/8270: MDLs for this sample were raised due to dilutions made to sample prior to analysis. Sample was analyzed at a (1 :5) dilution, therefore MDLs were raised 5 times. Sample had thick oil matrix. Analysis note for SW-846/8082: No surrogate recovery possible due to 1 OOx dilution made prior to analysis. Detection limits raise 1 OOx due to matrix interference. Angela D. Overcash, V.P. Laboratory Services HWC HWC HWC HWC HWC. HWC HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 · 449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364 • Toll Free Number: t-800/529-6364 ..._ Fax: 704/525-0409 • • • Lab· Report --" ~ ~,J.;\1 Full Service Analytical & Environmental Solutions 6/22/01 Page 18 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: Q-2 PO Box 669004 Prism Samcle 10: AC10516 Charlotte, NC 28266 Loqin Group: MK621H5 Sample Collection Date/Time: 6/14/01 13:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 91 %DRYWT. 0.01 SM 2540 G 6/19/01 17:05 JLW METALS DIGESTION METHOD 3050 Completed SW846-3050 6/15/01 13:15 LC2 PREP. METHOD 355D-PCB Completed SW846-3550 6/15/D1 12:0D JMV PREP. METHOD 355D Completed SW846-355DB 6/18/D1 20:00 JLW ANTIMONY, TOTAL 2.4 mg/kg 1.0 SW846-601DB 6/18/D1 21:27 MSP ARSENIC, TOTAL 5.1 mg/kg 1.0 SW846-6D1 DB 6/18/D1 21:27 MSP BERYLLIUM, TOTAL 1.9 mg/kg 1.0 SW846-6D1DB 6/18/D1 21:27 MSP CADMIUM, TOTAL Less than mg/kg 1.0 SW846-6D1DB 6/18/D1 21:27 MSP CHROMIUM, TOTAL 33 mg/kg 1.D SW846-6D1DB 6/18/D1 21:27 MSP COPPER, TOTAL 51 mg/kg 2.0 SW846-6D1 DB 6/18/01 21:27 MSP LEAD, TOTAL 66 mg/kg 1.D SW846-6D1DB 6/18/D1 21:27 MSP NICKEL, TOTAL 14 mg/kg 1.0 SW846-6D1DB 6/18/D1 21:27 MSP SELENIUM, TOTAL Less than mg/kg 2.D SW846-6D1 DB 6/18/01 21:27 MSP SILVER, TOTAL Less than mg/kg 2.0 SW846-6D10B 6/18/D1 21:27 MSP THALLIUM, TOTAL Less than mg/kg 0.5 SW846-6D1DB 6/18/D1 21:27. MSP ZINC, TOTAL 42D mg/kg 10 SW846-6D1DB 612D/D1 13:19 MSP MERCURY, TOTAL · O.D8 mg/kg D.D2 SW846-7471 6121/D1 15:03 PRF MERCURY DIGESTION Completed SW846-7471 6/2D/D1 1 0:4D LC2 PCB-1016 Not detected mg/kg 5.0 SW846-8082 6/22/01 1D:39 CWA PCB-1221 Not detected mg/kg 10 SW846-8D82 6/22/D1 1 D:39 CWA PCB-1232 Not detected mg/kg 5.0 SW846-8D82 6/22/D1 10:39 CWA PCB-1242 Not detected mg/kg S.D SW846-8D82 6/22/D1 1D:39 CWA PCB-1248 Not detected mg/kg S.D SW846-8D82 6t221D1 ·1D:39 CWA PCB-1254 Not detected mg/kg 5.0 SW846-8082 6/22/01 10:39 CWA PCB-126D Not detected mg/kg S.D SW846-8082 6/22/01 10:39 CWA PCB-1262 Not detected mg/kg S.D SW846-8D82 6/22/D1 1D:39 CWA PCB-1268 Not detected mg/kg S.D SW846-8D82 6/22/D1 1D:39 CWA ·--------- BENZENE Not detected ug/kg S.D SW846-826DB 6/2D/D1 D3:05 CMB BROMOBENZENE Not detected uglkg S.D SW846-826DB 6/2D/D1 D3:05 CMB NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364...., Toll Free Number: 1-800/529-6364 ..... Fax: 704/525-0409 • • • Lab Report 6/22/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Sample 10: .Loqin Group: Sample Collection Oate!Time: Lab Submittal Oate!Time: ,\> • ~~~}! . .-.c(~<~b.:.: Full Service Analytical & Environmental Solutions Page 19 of29 Cherokee-Mooresville Site Q-2 AC10516 MK621H5 6/14/01 13:30 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON TETRACHLORIDE CHLOROBENZENE CHLORODIBROMOMETHANE CHLOROETHANE CHLOROFORM CHLOROMETHANE 2-CHLOROTOLUENE 4-CHLOROTOLUENE 1 ,2-DIBROM0-3-CHLOROPROPANE 1 ,2-DIBROMOETHANE DIBROMOMETHANE 1 ,2-DICHLOROBENZENE 1 ,3-DICHLOROBENZENE 1.4-DICHLOROBENZENE DICHLORODIFLUOROMETHANE 1, 1-DICHLOROETHANE 1 ,2-DICHLOROETHANE 1, 1-DICHLOROETHENE CIS-1 ,2-DICHLOROETHENE TRANS-1,2-DICHLOROETHENE 1 ,2-DICHLOROPROPANE 1 ,3-DICHLOROPROPANE 2.2-DICHLOROPROPANE TEST RESULT UNITS Not detected ug/kg Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected ug/kg ug/kg ug/kg ug/kg ug/kg uglkg ug/kg · uglkg uglkg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected uglkg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected ug/kg Not detected Not detected uglkg ug/kg REPORTING METHOD DATEfTIME STARTED LIMIT REFERENCE 5.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 5.0 10.0 5.0 5.0 10.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 SW846-8260B . 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-8260B 6/20/01 03:05 ·SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW84S-8260B 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-82608 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 SW846-8260B 6/20/01 03:05 ANALYST CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..a.. P.O. Box 240543 ..a.. Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report -·8~~A! Full Service Analytical & Environmental Solutions 6/22/01 Page 20 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: Q-2 PO Box 669004 Prism Samole 10: AC10516 Charlotte, NC 28266 Looin Group: MK621H5 Sample Collection Date/Time: 6/14/01 13:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 1,1-DICHLOROPROPENE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 . CMB ETHYLBENZENE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB HEXACHLOROBUTADIENE Not detected ug/kg 5.0 SWB46-B2608 6/20/01 03:05 CMB ISOPROPYLBENZENE Not detected ug/kg 5.0 SWB46-82608 6/20/01 03:05. CMB P-ISOPROPYL TOLUENE Not detect~ ug/kg 5.0 SWB46-82608 6/20/01 03:05 CMB METHYLENE CHLORIDE Not detected ug/kg 100.0 SW846-82608 6/20/01 03:05 CMB NAPHTHALENE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB N-PROPYLBENZENE Not detected ug/kg 5.0 SW846-82~0B 6/20/01 03:05 CMB STYRENE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB 1,1, 1,2-TETRACHLOROETHANE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB TETRACHLOROETHENE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB TOLUENE Not detected ug/kg 5.0 SWB46-B2608 6/20/01 03:05 CMB 1,2.3-TRICHLOROBENZENE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB 1,2,4-TRICHLOROBENZENE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB 1, 1,1-TRICHLOROETHANE Not detected ug/kg 5.0 SWB46-8260B 6/20/01 03:05 CMB 1, 1,2-TRICHLOROETHANE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB TRICHLOROETHENE Not detected ug/kg 5.0 SW846-B2608 6/20/01 03:05 CMB TRICHLOROFLUOROMETHANE Not detected ug/kg 5.0 SW846-82608 6/20/01 03:05 CMB 1 ,2,3-TRICHLOROPROPANE Not detected ug/kg 5.0 SWB46-B2608 6/20/01 03:05 CMB 1,2,4-TRIMETHYLBENZENE Not detected uglkg 5.0 SWB46-82608 6/20/01 03:05 CMB 1,3,5-TRIMETHYLBENZENE Not detected uglkg 5.0 SWB46-82608 6/20/01 03:05 CMB VINYL CHLORIDE Not detected ug/kg 10.0 SW846-82608 6/20/01 03:05 CMB TOTAL XYLENES Not detected ug/kg 5.0 SWB46-82608 6/20/01 03:05 CMB 2-BUTANONE (MEK) Not detected ug/kg 50.0 SWB46-82608 6/20/01 03:05 CMB 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 10.0 SWB46-B2608 6/20/01 03:05 CMB 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 50.0 SW846-82608 6/20/01 03:05 CMB ACETONE Not detected ug/kg 100.0 SW846-B2608 6/20/01 03:05 CMB CARBON DISULFIDE Not detected ug/kg 100.0 SWB46-82608 6/20/01 03:05 CMB VINYL ACETATE Not detected ug/kg 50.0 SWB46-8260B 6/20/01 03:05 CMB NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -·FL Certification No. E87519 449 Springbrook Road A. P.O. Box 240543 A. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..., Toll Free Number: l-800/529-6364 ..... Fax: 704/525-0409 • • • Lab Report ~ .. A-~~ Full Service Analytical & Environmental Solutions 6/22/01 Page 21 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: Q-2 PO Box 669004 Prism Samcle 10: AC10516 Charlotte, NC 28266 Looin Group: MK621H5 Sample Collection Date/Time: 6/14/01 13:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS. LIMIT REFERENCE STARTED ANALYST CIS-1,3-DICHLOROPROPENE Not detected ug/kg 5.0 SW846-8260B 6120101 03:05 CMB TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 5.0 SW846-8260B 6/20/01 03:05 CMB 2-HEXANONE Not detected ug/kg 50.0 SW846-8260B 6120101 03:05 CMB IPE Not detected ug/kg 5.0 SW846-8260B 6120101 03:05 CMB MTBE Not detected ug/kg . 5.0 SW846-8260B 6/20101 03:05 CMB SURR:DIBROMOFLUOROMETHANE 135. % 70-130 SW846-8260B 6120101 03:05 CMB SURR:TOLUENE-D8 130 % 70-130 SW846-8260B 6120/01 03:05 CMB SURR:BROMOFLUOROBENZENE 120 % 70-130 SW846-8260B 6/20101 03:05 CMB ---------- ACENAPHTHENE Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC ACENAPHTHYLENE Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC ANTHRACENE Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC BENZO(A)ANTHRACENE Not detected ug/kg 1800 SW846-8270C 6120/01 04:30 HWC BENZO(B)FLUORANTHENE Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC BENZO(K)FLUORANTHENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC BENZO(A)PYRENE Not detected ug/kg 1800 SW846-8270C 6120/01 04:30 HWC BENZO(GHI)PERYLENE Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC BIS(2-CHLOROETHOXY)METHANE Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/kg 1800 SW846-8270C 6/20101 04:30 HWC BIS(2-CHLOROISOPROPYL)ETHER Nat detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 4-BROMOPHENYL PHENYL ETHER Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC BUTYL BENZYL PHTHALATE Not detected ug/kg 1800 SW846-8270C 6/20101 04:30 HWC 4-CHLOR0-3-METHYLPHENOL Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC 2-CHLORONAPHTHALENE Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC 2-CHLOROPHENOL Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 1800 SW846-8270C 6/20101 04:30 HWC CHRYSENE Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC DIBENZOFURAN Not detected ug/kg 1800 SW846-8270C 6120101 04:30 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364.., Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report -~\..!1¥}~ Full Service Analytical & Environmental Solutions 6/22/01 Page 22 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: Q-2 PO Box 669004 Prism Sample 10: AC10516 Charlotte, NC 28266 Looin Group: MK621H5 Sample Collection Date/Time: 6/14/01 13:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST DI-N-BUTYLPHTHALATE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 1 ,2-DICHLOROBENZENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 1 ,3-DICHLOROBENZENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 1 ,4-DICHLOROBENZENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 2,4-DICHLOROPHENOL Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30. HWC DIETHYL PHTHALATE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 2,4-DIMETHYLPHENOL Not detected uglkg 1800 SW846-8270C 6/20/01 04:30 HWC DIMETHYl PHTHALATE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 2,4-DINITROPHENOL Not detected ug/kg 9000 SW846-8270C 6/20/01 04:30 HWC 2,4-DINITROTOLUENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 2,6-DINITROTOLUENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC DI-N-OCTYLPHTHALA TE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC FLUORANTHENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC FLUORENE Not detected uglkg 1800 SW846-8270C 6/20/01 04:30 HWC HEXACHLOROBENZENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC HEXACHLOROBUTADIENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC HEXACHLOROETHANE Not detected uglkg 1800 SW846-8270C 6/20/01 04:30 HWC INDEN0(1,2,3-CD)PYRENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC ISOPHORONE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 2-METHYL-4,6-DINITROPHENOL Not detected uglkg 9000 SW846-8270C 6/20/01 04:30 HWC 2-METHYL NAPHTHALENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 2-METHYL-PHENOL Not detected uglkg 1800 SW846-8270C 6/20/01 04:30 HWC 4-METHYL-PHENOL Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC NAPHTHALENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC NITROBENZENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 2-NITROPHENOL Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC 4-NITROPHENOL Not detected ug/kg 9000 SW846-8270C 6/20/01 04:30 HWC N-NITROSODIPHENYLAMINE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC N-NITROSODI-N-PROPYLAMINE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 HWC NC Certification No. 402 -SC Certification No. 99012 -NC OrinkinQ Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road .-. P.O. Box 240543 .... Charlotte, NC 28224·0543 Phone: 704/529-6364 ... Toll Free Number: 1-800/529-6364 ... Fax: 704/525-0409 • • • Lab Report PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions 6/22/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Sample 10: Looin Group: Sample Collection Date/Time: Lab Submittal Date/Time: Page 23 of 29 Cherokee-Mooresville Site Q-2 AC10516 MK621H5 6/14/01 6/14/01 13:30 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST PENTACHLOROPHENOL Not detected ug/kg 9000 SW846-8270C 6/20/01 04:30 PHENANTHRENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 PHENOL Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 PYRENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 1 ,2,4-TRICHLOROBENZENE Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 2,4,5-TRICHLOROPHENOL Not detected ug/kg 1800 SW846-8270C 6/20/01 04:30 2,4,6-TRICHLOROPHENOL Not detected uglkg 1800 SW846-8270C 6/20/01 04:30 ------------------ Sample Comments: Analysis note for SW-846/8270: MDLs for this sample were raised due to dilutions made· to sample prior to analysis: Sample was analyzed at a (1 :5) dilution, therefore MDLs were raised 5 times. Sample had thick oil matrix. Analysis note for SW-846/8082: No surrogate recovery possible due to 1 OOx dilution made prior to analysis. Detection limits raised 1 OOx due to matrix interference. 8260-• Surrogate recovery above QC limits. Matrix interference is suspected. Angela D. Overcash, V.P. Laboratory Services HWC HWC HWC HWC HWC HWC HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364..., Toll Free Number: 1-800/529-6364 ..._Fax: 704/525-0409 • • • ·1.1~--.• Lab Report . ~!'.!'Ji .r; ~..c.-..:: Full Service Analytical & Environmental Solutions 6/22/01 _Page 24 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren · Customer Sample 10: D-1 PO Box 669004 Prism Sample 10: AC10517 Charlotte, NC 28266 Looin Group: MK621H5 Sample Collection Date/Time: 6/14/01 14:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST PCBs in Oil, Preparation Completed 358013665 6121101 20:00 CWA WASTE DILUTION PREPARATION Completed SW-846, 3580 6120101 15:00 HC METALS DIGESTION METHOD 3050 Completed SW846-3050 6120101 10:15 LC2 ANTIMONY, TOTAL Less than mg/kg 1.0 SW846-6010B 6120101 20:48 MSP ARSENIC, TOTAL Less than mg/kg 1.0 SW846-6010B 6120101 20:48 MSP BERYLLIUM, TOTAL Less than mg/kg 1.0 SW846-6010B 6120101 20:48 MSP CADMIUM, TOTAL Less than mg/kg 1.0 SW846-6010B 6120101 20:48 MSP CHROMIUM, TOTAL Less than mg/kg 1.0 SW846-6010B 6120101 20:48 MSP COPPER, TOTAL Less than mg/kg 2.0 SW846-6010B 6120101 20:48 MSP LEAD, TOTAL Less than mg/kg 1.0 SW846-6010B 6120101 20:48 MSP NICKEL, TOTAL Less than mg/kg 1.0 SW846-601 08 . 6120101 20:48 MSP SELENIUM, TOTAL Less than mg/kg 0.20 SW846-601 08 6120101 20:48 MSP SILVER, TOTAL Less than mg/kg 2.0 SW846-601 08 6120101 20:48 MSP THALLIUM, TOTAL Less than mg/kg 0.5 SW846-60108 6120101 20:48 MSP ZINC, TOTAL 7.3 mg/kg 1.0 SW846-60108 6/20/01 20:48 MSP MERCURY, TOTAL Less than mg/kg 0.02 SW846-7471 6121101.15:07 PRF MERCURY DIGESTION Completed SW846-7471 6120/01 10:40 LC2 PC8-1016 Not detected mg/kg 5.0 SW846-8082 6122/01 12:00 CWA PCB-1221 Not detected mg/kg 10 SW846-8082 6/22101 12:00 CWA PCB-1232 Not detected mg/kg 5.0 SWB46-8082 6122/01 12:00 CWA PCB-1242 Not detected mg/kg 5.0 SW846-8082 6122101 12:00 CWA PCB-1248 Not detected mg/kg 5.0 SW846-8082 6122101 12:00 CWA PCB-1254 Not detected mg/kg 5.0 SW846-8082 6122101 12:00 CWA PCB-1260 Not detected mg/kg 5.0 SW846-8082 6122101 12:00 CWA PCB-1262 Not detected mg/kg 5.0 SW846-8082 6122101 12:00 CWA PCB-1268 Not detected mg/kg 5.0 SW846-8082 6122101 12:00 CWA ---------- BENZENE Not detected ug/kg 10000 SW846-82608 6119101 19:15 MP BROMOBENZENE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP BROMOCHLOROMETHANE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 ...._ Charlotte, NC 28224-0543 Phone: 704/529-6364 .,. Toll Free Number: 1-800/529-6364 .,. Fax: 704/525-0409 • • • ~:v.t·, ,. Lab Report ----=~~~ Full Service Analytical & Environmental Solutions 6/22/01 Page 25 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Clift Lundgren Customer Sample 10: 0-1 PO Box 669004 Prism Samcle 10: AC10517 Charlotte, NC 28266 Looin Grouo: MK621H5 Sample Collection Date/Time: 6/14/01 14:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST BROMODICHLOROMETHANE Not detected ug/kg 10000 SW846·8260B 6/19/01 19:15 MP BROMOFORM Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP BROMOMETHANE Not detected ug/kg 20000 SW846-8260B 6/19/01 19:15 MP N-BUTYLBENZENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP SEC-BUTYLBENZENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP TERT-BUTYLBENZENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP CARBON TETRACHLORIDE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP CHLOROBENZENE, Not detected .. ug/kg 10000 SW846-8260B 6/19/01 19:15 MP CHLORODIBROMOMETHANE Not detected ug/kg 10000 SW846:8260B 6/19i01 19:15 MP CHLOROETHANE Not detected ug/kg 20000 SW846·8260B 6/19/01 19:15 MP CHLOROFORM Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP CHLOROMETHANE Not detected ug/kg 20000 SW846·8260B 6/19/01 19:15 MP . 2-CHLOROTOLUENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP 4-CHLOROTOLUENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected ug/kg 20000 SW846·8260B 6/19/01 19:15 MP 1 ,2-DIBROMOETHANE Not detected ug/kg 10000 SW846-8260B 6/19/0119:15 MP DIBROMOMETHANE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP 1 ,2-DICHLOROBENZENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP 1,3-DICHLOROBENZENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP 1,4-DICHLOROBENZENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP DICHLORODIFLUOROMETHANE Not detected ug/kg 10000 SW846-8260B 6/19/0119:15 MP 1,1-DICHLOROETHANE Not detected uglkg 10000 SW846-8260B 6/19/01 19:15 MP 1,2-DICHLOROETHANE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP 1,1-DICHLOROETHENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP CIS-1,2-DICHLOROETHENE Not detected ug/kg 10000 SW846·8260B 6/19/01 19:15 MP TRANS-1,2-DICHLOROETHENE Not detected ug/kg 10000 SW846·8260B 6/19/01 19:15 MP 1,2-DICHLOROPROPANE Not detected ug/kg 10000 SW846·8260B 6/19/01 19:15 MP 1,3-DICHLOROPROPANE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP 2,2-DICHLOROPROPANE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP 1,1-DICHLOROPROPENE Not detected ug/kg 10000 SW846-8260B 6/19/01 19:15 MP NC Certification No. 402 • SC Certification No. 99012 • NC DrinkinQ Water Cert. No. 37735 • FL Certification No. E87519 449 Springbrook Road ..., P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 ..., Fax: 704/525-0409 • • • Lab Report ~e>~~~~ Full Service Analytical & Environmental Solutions 6/22/01 Page 26 of 29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: D-1 PO Box 669004 Prism Samole 10: AC10517 Charlotte, NC 28266 Looin Group: MK621H5 Sample Collection Date/Time: 6/14/01 14:30 Lab Submittal Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST ETHYLBENZENE Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP HEXACHLOROBUTADIENE Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP ISOPROPYLBENZENE Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP P-ISOPROPYLTOLUENE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP METHYLENE CHLORIDE Not detected ug/kg 200000 SWB46-8260B 6119101 19:15 MP NAPHTHALENE Not detected ug/kg 10000 SWB46-8260B 611910119:15 MP N-PROPYLBENZENE Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP STYRENE Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP 1,1, 1 ,2-TETRACHLOROETHANE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP TETRACHLOROETHENE Not detected ug/kg 10000 SW846-8260B 6119101-19:15 MP TOLUENE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP 1,2,3-TRICHLOROBENZENE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP 1 ,2,4-TRICHLOROBENZENE Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP 1,1, 1-TRICHLOROETHANE NOt detected ug/kg 10000 SW846-8260B 6119101 19:15 MP 1,1 ,2-TRICHLOROETHANE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP TRICHLOROETHENE Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP TRICHLOROFLUOROMETHANE Not detected ug/kg 10000 1 SW846-8260B 611910119:15 MP 1,2,3-TRICHLOROPROPANE Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP 1,2,4-TRIMETHYLBENZENE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP 1 ,3,5-TRIMETHYLBENZENE Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP VINYL CHLORIDE Not detected ug/kg 20000 SW846-8260B 6119101 19:15 MP TOTAL XYLENES Not detected ug/kg 10000 SWB46-8260B 6119101 19:15 MP 2-BUTANONE (MEK) Not detected ug/kg 100000 SWB46-8260B 6119101 19:15 MP 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 20000 SW846-8260B 6119101 19:15 MP 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 100000 SWB46-8260B 6119101 19:15 MP ACETONE Not detected ug/kg 200000 SW846-8260B 6119101 19:15 MP CARBON DISULFIDE Not detected ug/kg 200000 SW846-8260B 6119101 19:15 MP VINYL ACETATE Not detected ug/kg 100000 SW846-8260B 611910119:15 MP CIS-1 ,3-DICHLOROPROPENE Not detected ug/kg 10000 SW846-8260B 6119101 19:15 MP NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..o. P.O. Box 240543 ..o. Charlotte, NC 28224-0543 Phone: 7041529-6364 ..o. Toll Free Number: 1-8001529-6364 ..o. Fax: 704/525-0409 • • • '-!·•. ~·. ,: Lab Report ~Plus~ lABORATORIES, IN~. --.a~ . Full Service Analytical & Environmental Solutions 6/22/01 Page 27 of29 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: D-1 PO Box 669004 Prism Samcle 10: AC10517 Charlotte, NC 28266 Looin Group: MK621H5 Sample Collection Date/Time: 6/14/01 14:30 Lab Submittal-Date/Time: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST TRAN5-1,3-DICHLOROPROPENE Not detected ug/kg 10000 5W846-82608 6/19/01 19:15 MP 2-HEXANONE Not detected ug/kg 100000 5W846-82608 6/19/01 19:15 MP IPE Not detected uglkg 10000 5W846-82608 6/19/01 19:15 MP MT8E Not detected uglkg 10000 5W846-82608 6/19/01 19:15 MP 5URR:DI8ROMOFLUOROMETHANE 106 % 70-130 5W846-82608 6/19/01 19:15 MP 5URR:TOLUENE-D8 98 % 70-130 5W846-82608 6/19/01 19:15 MP 5URR:8ROMOFLUOR08ENZENE 123 % 70-130 5W846-82608 6/19/01 19:15 MP ~-·-··· . ACENAPHTHENE Not detected ug/kg 100000 5W846-8270C . 6/20/01 18:29 HWC ACENAPHTHYLENE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC ANTHRACENE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 8ENZO(A)ANTHRACENE Not detected ug/kg 100000 5W846·8270C 6/20/01 18:29 HWC 8ENZ0(8)FLUORANTHENE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 8ENZO(K)FLUORANTHENE Not detected ug/kg 100000 5W846·8270C 6/20/01 18:29 HWC 8ENZO(A)PYRENE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 8ENZO(GHI)PERYLENE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 815(2-CHLOROETHOXY)METHANE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 815(2-CHLOROETHYL)ETHER Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 815(2-CHLOROI50PROPYL)ETHER Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 815(2-ETHYLHEXYL)PHTHALATE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 4-8ROMOPHENYL PHENYL ETHER Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 8UTYL8ENZYLPHTHALATE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 4-CHLOR0-3-METHYLPHENOL Not detected ug/kg 100000 5W846:8270C 6/20/01 18:29 HWC 2-CHLORONAPHTHALENE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC 2-CHLOROPHENOL Not detected ug/kg 100000 SW846·8270C 6/20/01 18:29 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 100000 5W846·8270C 6/20/01 18:29 HWC CHRY5ENE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC D18ENZO(A,H)ANTHRACENE Not detected ug/kg 100000 5W846·8270C 6/20/01 18:29 HWC DI8ENZOFURAN Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC DI·N·8UTYLPHTHALATE Not detected ug/kg 100000 5W846-8270C 6/20/01 18:29 HWC NC Certification No. 402 -SC Certification No. 99012 • NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .-.. Toll Free Number: 1-800/529-6364 ..._ Fax: 704/525-0409 • • • Lab Report 6/22/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Samole 10: Loqin Group: Sample Collection Date/Time: Lab Submittal Date/Time: Full Service Analytical & Environmental Solutions Page 28 of29 Cherokee-Mooresville Site D-1 AC10517 MK621H5 6/14/01 14:30 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1 ,4-DICHLOROBENZENE 2,4-DICHLOROPHENOL DIETHYL PHTHALATE 2,4-DIMETHYLPHENOL DIMETHYL PHTHALATE 2,4-DINITROPHENOL 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE DI-N-OCTYLPHTHALA TE FLUORANTHENE FLUORENE HEXACHLOROBENZENE HEXACHLOROBUTADIENE HEXACHLOROCYCLOPENTADIENE HEXACHLOROETHANE INDEN0(1 ,2,3-CD)PYRENE ISOPHORONE 2-METHYL-4,6-0INITROPHENOL 2-METHYL NAPHTHALENE 2-METHYL-PHENOL 4-METHYL-PHENOL NAPHTHALENE NITROBENZENE 2-NITROPHENOL 4-NITROPHENOL N-NITROSODIPHENYLAMINE N-NITROSODI-N-PROPYLAMINE PENTACHLOROPHENOL TEST RESULT Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected UNITS ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg REPORTING METHOD DATE/TIME STARTED LIMIT REFERENCE tooooo 100000 100000 100000 100000 100000 100000 500000 100000 100000 100000 100000 100000 100000 100000 100000 100000 100000 100000 500000 100000 100000 100000 100000 100000 100000 500000 100000 100000 500000 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 SW846-8270C 6/20/01 18:29 ANALYST HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .._ P.O. Box 240543 .._ Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report Full Service Analytical & Environmental Solutions 6/22/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Page 29 of 29 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: D-1 Prism Sample 10: AC10517 LoQin Group: MK621 H5 Sample Collection DatefTime: 6/14/01 14:30 Lab Submittal DatefTime: 6/14/01 16:45 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST -------- PHENANTHRENE Not detected ug/kg 100000 SW846-8270C 6/20/01 18:29 HWC PHENOL Not detected ug/kg 100000 SW846-8270C 6/20/01 18:29 HWC PYRENE Not detected ug/kg 100000 SW846-8270C 6/20/01 18:29 HWC 1 ,2,4-TRICHLOROBENZENE Not detected ug/kg 100000 SW846-8270C 6/20/01 18:29 HWC 2,4,5-TRICHLOROPHENOL Not detected ug/kg 100000 SW846-8270C 6/20/01 18:29 HWC 2,4,6-TRICHLOROPHENOL Not detected ug/kg 100000 SW846-8270C 6/20/01 18:29 HWC -------- Sample Comments: Note for 8260: Sample diluted due to matrix (oil). Analysis note for SW-846/3580 for 8270: This sample was analyzed as a waste dilution. A dilution of 1g- 1 OmL was used for analysis, therefore MDLs were raised to a detection limit of 100000 ug/kg. Sample matrix was waste oil. Analysis note for SW-846/8082: No surrogate recovery possible due to 100x dilution made prior to analysis. Detection limits raised 1 OOx due to matrix interference. · Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Cert~ication No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 _. Toll Free Number: 1-800/529-6364 _. Fax: 704/525-0409 J I /}/•/ ,. '\-,,· ft /d -n t.;::rv(.., ·c I' ·.::, .... (:< . . ... Client , 1 , -h =::_ --~c T ,, .,. , _;::J(,--_ _ , --r '--t <7-·~ 1.:< c.l '1. , · C-· · f'~ It I< o--· Ph"!'•¥•' Addrf.•• .1 /. -.--'-J {I~ --J ; t.----., f~ _, c ,., -~-'ft: /(,('}. . ... .... 1.· ... ~(} ~' --... -,..." ?. t} CHAI~ 017 CU.ODY RECORD . PAGE _1_ OF_/_'_ QUOTE#--------- 449 Springbrook Road .. Charlotte, NC 2821 7 P.O. Box 240543 .. Charlotte, NC 28224-0543 Phone: 704/52~J~J,P4./~-!l:'~~ !.~4/525-0409 REPORT TO: ~arne . . --! . BILL TO: Address --·.-----:_.;;-··· --7fN'c3'f.¥-9N=----. --'-r!J'i--~\'lJ-~9//'(- Phone ____________ ~--,-;--J---7 Fax ____ _ Requested Due Date 0 1 Day 0 2 Days 0 3 Days 0 4 Days 0 5 Days 0 6-~ Days 0 Standard 10 days · ,-\ ' ( ,..., . P.O.#/BIIIing R~rpnce 1 ;.,.{ ., ~. · //,_, (·_ .~~~-..._rrc.--w .r:ec~ --1v uu.-·c..: th, '"t'"' _), ~ ' Samples received after 15:00 will be processed the next business day. Turnaround time is based on business days, excluding weekends and holidays. State Certification ... v Requested FL __ _ NC --SC Water Chlorinated Yes Sample Iced Upon Collection CMUD NPDES Other ___ NA __ No NA Yes No_ OTHER----- Project Name _______ . _______ . ----------___ ... __ ·-------- (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) PRESS DOWN FIRMLY • 3 COPIES CLIENT . SAMPLE DESCRIPTION t.vS-1 DATE ColLECTED ~-ILl-v{ --------------- Relinquished By: (Signature) Relinquished By: (Signature) TIME cq~~~~-.:~D MILITARY HOURS !100 MATRIX (SOIL, WATER OR SLUDGE) ' . SAMPLE CONTAINER i) f,'ALYS~}REQU~STED PRESEAVA· ft.y /11\1 1 ~~,~ / ,. ,....-/ "TYPE T1VES / < / 'b '~> /--(/ ' SEE BELOW NO. SIZE _ /';l, ·/' (() /if:'/ i <~" /' (J< ~ .3 ;;_ ~3-----~""""?~~. i'. ·;u; . _,_ -t r ; I •'1 ~~ .. . I T / / -~ ' I --I -- -•] ""'· ' / REMARKS I / / . f ~ .~;t-" ! ~ 1 -:;• • _ .~~( ........ -• .f--f--,--./£"/ ,"/,..,.:..j~ ----~~L~r''·;r-t-'t-J,(~.....--.... t<)itiJf-.1.,___1_'::/.·r·~:-,·~-· ~.,,vl\ Ov;(\(' I· • ,...-,.~-------·-/---_sampledBy(PnntNamO) ______ ------------_______ J-· Afftllatton ___ . _ _ ___ Received By: (Signature) Date Militaryfl-iours Additional Comments: NPDES: 0 NC 0 sc UST: 0 NC 0 sc GROUNDWATER: 0 NC DRINKING WATER: 0 NC I SOLID WASTE: 0 NC RCRA: 0 NC 0 sc CERCLA 0 NC 0 sc LANDFILL 0 NC OTHER:' 0 NC __ _ 0 OTHER 0 OTHER 0 sc 0 OTHER 0 sc 0 OTHER i 0 sc ! 0 OTHER 0 OTHER 0 OTHER 0 sc 0 OTHER 0 sc 0 OTHER SUB LAB CEAT. IDNO. .. ,, Site Arrival_}j~e: •. :- PRISM LAB IDNO. SEE REVERSE FOR TERMS & CONDITIONS *CONTAINER TYPE CODES: A =Amber C =Clear G =Glass P =Plast-ic; Tl =Teflon-tined Cap VOA = Volatile,Organics Analysis (Zero Head Space) FINAL REPORT COPY • • • Lub Report ~~Ai [g]~~~w~~[Q) c:tt:ffW'.?s; Futt Service Analytical & Environmental Solutions 6/21/01 Page 1 of 8 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: N-1 (0-4) PO Box 669004 Prism Sam ole ID: AC10432 Charlotte, NC 28266 Loqin Group: MK621H38 Sample Collection Date/Time: 6/13/01 10:40 Lab Submittal Date/Time: 6/14/01 11:20 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER .. ___ 13ESULT . UNITS LIMIT -REFERENCE _STARTED ANALYST TPH • DIESEL RANGE -30 mg/kg 10 8015MOD/3550 6/18/01 10:13 GRR TPH-GASOLINE RANGE Less than mg/kg 1.0 8015MOD/5030 6/15/01 18:33 KC OIL & GREASE. HYDROCARBONS Less than mg/kg 50 9071/silica 6/19/01 09:00 GRR CALCULATIONS BASED ON DRY WT. 85 %DRYWT. 0.01 SM 2540 G 6/18/01 17:00 JLW PREP. METHOD 3550 Completed SW846-3550 6/15/01 09:30 JMV ·-------·- . Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..._Toll Free Number: 1-800/529-6364 ..._Fax: 704/525-0409 • • • Lab Report 6/21/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 2 of 8 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: J-1 (.5-1.5) Prism Samole ID: AC10433 LoQin Group: MK621 H3B Sample Collection Date/Time: 6/13/01 11:30 Lab Submittal Date/Time: 6/14/01 11:20 The following analytical results have been obtained for ttle indicated sample which was submitted to this laboratory:. TEST TEST REPORTING METHOD DATE!TIME PARAMET!O_R_ RESULT UNITS LIMIT REFEREN_CE STARTED ANALYST TPH • DIESEL RANGE Less than mg/kg 10 8015MOD/3550 6/18/01 12:18 GRR TPH-GASOLINE RANGE Less than mg/kg 1.0 8015MOD/5030 6/15/01 19:10 KC OIL & GREASE, HYDROCARBONS 50 . mg/kg 50 9071/silica 6/19/01 09:00 GRR CALCULATIONS BASED ON DRY WT: 79 %DRYWT. ·0.01 SM 2540 G 6/19/01 17:05 JLW PREP. METHOD 3550 Completed SW846-3550 6/15/01 09:30 JMV Sample CPmments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 ...._ Charlotte, NC 28224-0543 . Phone: 704/529-6364 ...._ Toll Free Number: 1-800/529-6364 :.... Fax: 704/525-0409 • • • Lab Report ,.t~~~( PRISM LABORATORIES, INC. ' Full Service Analytical & Environmental Solutions 6/21/01 Page 3 of 8 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: C-1 {0-.5) PO Box 669004 Prism Sample 10: AC10434 Charlotte, NC 28266 Looin Group: MK621H3B Sample Collection Date/Time: 6/13/01 14:10 Lab Submittal Date/Time: 6/14/01 11:20 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 85 %DRYWT. 0.01 SM 2540 G 6/19/01 17:05 JLW METALS DIGESTION METHOD 3050 Completed SW846-3050 6/15/01 13:15 LC2 PREP. METHOD 3550 Completed SW846-3550B 6/18/01 20:00 JLW ANTIMONY, TOTAL 8.0 mg/kg 1.0 SW846-601 OB 6/18/01 20:56 MSP ARSENIC, TOTAL 4.0 mg/kg 1.0 SW846-601 OB 6/18/01 20:56 MSP BERYLLIUM, TOTAL Less than mg/kg 1.0 SW846-601 OB 6/18/01 20:56 MSP CADMIUM. TOTAL Less than mg/kg 1.0 SW846-6010B 6/18/01 20:56 MSP ..... CHROMIUM. TOTAL 40 mg/kg 1.0 SW846-601 OB 6/18/01 20:56 MSP COPPER. TOTAL 83 mg/kg 2.0 SW846-601 OB 6/18/01 20:56 MSP LEAD. TOTAL 220 mg/kg 2.0 SW846-6010B 6/21/01 12:34 MSP NICKEL. TOTAL 6.1 mg/kg 1.0 SW846-601 OB 6/18/01 20:56 MSP SELENIUM. TOTAL Less than mg/kg 2.0 SW846-60 1 OB 6/18/01 20:56 MSP SILVER. TOTAL Less than mg/kg 2.0 SW846-601 OB 6/18/01 20:56 MSP THALLIUM. TOTAL Less than mg/kg 0.5 SW846-601 OB 6/18/01 20:56 MSP ZINC, TOTAL 110 mg/kg 1.0 SW846-6010B 6/18/01 20:56 MSP MERCURY. TOTAL 0.12 mg/kg 0.02 SW846-7471 6/19/01 13:34 PRF MERCURY DIGESTION Completed SW846-7471 6/18/01 12:00 LC2 BENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB BROMOBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB BROMOCHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB BROMODICHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB BROMOFORM Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB BROMOMETHANE Not detected ug/kg 12.0 SW846-8260B 6/20/01 00:50 CMB N-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB SEC-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB TERT-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB CARBON TETRACHLORIDE Not detected uglkg 6.0 SW846-82608 6/20/01 00:50 CMB CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB CHLORODIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB CHLOROETHANE Not detected ug/kg 12.0 SW846-8260B 6/20/01 00:50 CMB NC Certification No. 402 -SC Certification No. 99012 -NC Drink/no Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road..., P.O. Box 240543 a Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 . ' • • • Lab Report ~ PR •li? .<olfii,~ LABO~A!~~- Full Service Analytical & Environmental Solutions 6/21/01 Page 4 of 8 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: C-1 (0-.5) PO Box 669004 Prism Sample 10: AC10434 Charlotte, NC 28266 Loain Group: MK621H38 Sample Collection Date/Time: 6/13/01 14:10 Lab Submittal Date/Time: 6/14/01 11:20 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED. ANALYST CHLOROFORM Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB CHLOROMETHANE Not detected ug/kg 12.0 SW846-82608 6/20/01 00:50 CMB 2-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-82608 . 6/20/01 00:50 CMB 4-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-82608 6/20/01 oo:5o CMB 1.2-DIBROM0-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-82608 6/20/01 00:50 CMB 1 ,2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB DIBROMOMETHANE Not detected . ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB 1 ,2-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB 1.3-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 1.4-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB 1, 1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB 1.2-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 1, 1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB CIS-1.2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB TRANS-1.2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB 1,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB 1.3-DICHLOROPROPANE . Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB 1, 1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB ETHYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB HEXACHLOROBUTADIENE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB ISOPROPYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB P-ISOPROPYL TOLUENE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-82608 6/20/01 00:50 CMB NAPHTHALENE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB STYRENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 1.1.1,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB 1.1.2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 00:50 CMB NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .._Toll Free Number: 1-800/529-6364 .._Fax: 704/525-0409 • • • ', ',\>'' Lab Report ~ <o' PRisM: ..-LABORATORIES,INC . .....,;;,-~~ ' ' Full Service Analytical & Environmental Solutions 6/21/01 Page 5 of 8 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: C-1 (0-.5) PO Box 669004 Prism Sample ID: AC10434 Charlotte, NC 28266 Loqin Group: MK621H3B Sample Collection Date/Time: 6/13/01 14:10 Lab Submittal Date/Time: 6/14/01 11 ::20 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST ···------- TETRACHLOROETHENE Not detected " ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB TOLUENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 1 ,2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B _ 6/20/01 00:50 CMB 1 ,2,4-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB ·1,1, 1-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B -6/20/01 00:50 CMB- 1,1 ,2-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB TRICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 1,2,3-TRICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 1 ,2,4-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 1,3,5-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB VINYL CHLORIDE Not detected ug/kg 12.0 SW846-8260B 6/20/01 00:50 CMB TOTAL XYLENES Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-8260B 6/20/01 00:50 CMB 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 SW846-8260B 6/20/01 00:50 CMB 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260B 6/20/01 00:50 CMB ACE~ONE Not detected ug/kg 120.0 SW846-8260B 6/20/01 00:50 CMB CARBON DISULFIDE Not detected ug/kg 120.0. SW846-8260B 6/20/01 00:50 CMB VINYL ACETATE Not detected ug/kg 60.0 SW846-8260B 6/20/01 00:50 CMB CIS-1 ,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB TRANS-1 ,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB 2-HEXANONE Not detected ug/kg 60.0 SW846-8260B 6/20/01 00:50 CMB IPE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB MTBE Not detected ug/kg 6.0 SW846-8260B 6/20/01 00:50 CMB SURR:DIBROMOFLUOROMETHANE 105 % 70-130 SW846-8260B 6/20/01 00:50 CMB SURR:TOLUENE-D8 118 % 70-130 SW846-8260B 6/20/01 00:50 CMB SURR:BROMOFLUOROBENZENE 109 % 70-130 SW846-8260B 6/20/01 00:50 CMB M~-------- ACENAPHTHENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC ACENAPHTHYLENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert No. 37735 -FL Certification No. E87519 449 Springbrook Road ... P.O. Box 240543 ... Charlotte, NC 28224-0543 Phone: 704/529-6364 _... Toll Free Number: 1-800/529-6364 _... Fax: 704/525-0409 • • • Lab Report ~ "''h PRISM LABORATORIES, INC. ~c~ . Full Service Analytical & Environmental Solutions 6/21/01 Page 6 of 8 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: C-1 (0-.5) PO Box 669004 Prism Sam ole ID: AC10434 Charlotte, NC 28266 Looin Group: MK621H3B Sample Collection Date/Time: 6/13/01 14:10 Lab Submittal Date/Time: 6/14/01 11:20 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST ANTHRACENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 8ENZO(A)ANTHRACENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 8ENZ0(8)FLUORANTHENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 8ENZO(K)FLUORANTHENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 8ENZO(A)PYRENE Not detected ug/kg 1900 SW846·8270C 6/20/01 01:29 HWC BENZO(GHI)PERYLENE Not detected ug/kg 1900 SW846·8270C 6/20/01 01:29 HWC 81S(2-CHLOROETHOXY)METHANE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 81S(2-CHLOROETHYL)ETHER Not detected ug/kg 1900 SW846·8270C 6/20/01 01:29 HWC 81S(2·CHLOROISOPROPYL)ETHER Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 81S(2-ETHYLHEXYL)PHTHALA TE Not detected ug/kg 1900 SW846-8270C 6/20/01 01 :29 HWC 4-8ROMOPHENYL PHENYL ETHER Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 8UTYL8ENZYLPHTHALATE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 4-CHLOR0-3-METHYLPHENOL Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 2-CHLORONAPHTHALENE Not detected ug/kg 1900 SW846·8270C 6/20/01 01:29 HWC 2-CHLOROPHENOL Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC CHRYSENE Not detected ug/kg 1900 SW846·8270C 6/20/01 01:29 HWC D18ENZO(A.H)ANTHRACENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC DI8ENZOFURAN Not detected ug/kg 1900 SW846·8270C 6/20/01 01:29 HWC DI-N-8UTYLPHTHALA TE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 1,2-DICHLOR08ENZENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 1.3-DICHLOR08ENZENE Not detected ug/kg 1900 SW846·8270C 6/20/01 01 :29 HWC 1 ,4-DICHLOR08ENZENE Not detected ug/kg 1900 SW846·8270C 6/20/01 01:29 HWC 2.4-DICHLOROPHENOL Not detected ug/kg 1900 SW846-8270C 6/20/01 01 :29 HWC DIETHYL PHTHALATE Not detected ug/kg· 1900 SW846·8270C 6/20/01 01:29 HWC 2,4-DIMETHYLPHENOL Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC DIMETHYL PHTHALATE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 2,4-DINITROPHENOL Not detected ug/kg 9500 SW846-8270C 6/20/01 01:29 HWC 2,4-DINITROTOLUENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 2.6-DINITROTOLUENE Not detected ug/kg 1900 SW846·8270C 6/20/01 01:29 HWC NC Certification No. 402 • SC Certification No. 99012 -NC Drinking Water Cart. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: t-800/529-6364 ..... Fax: 704/525·0409 • • • Lab Report PRisM· LAaoRATOAIES, INC. "' Full Service Analytical & Environmental Solutions 6/21/01 Page 7 of 8 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: C-1 (0-.5) PO Box 669004 Prism Sample 10: AC10434 Charlotte, NC 28266 Loqin Group: MK621H3B Sample Collection Date/Time: 6/13/01 14:10 Lab Submittal Date/Time: 6/14/01 11:20 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST DI-N-OCTYLPHTHALATE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC FLUORANTHENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC FLUORENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC HEXACHLOROBENZENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC HEXACHLOROBUTADIENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC HEXACHLOROETHANE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC INDEN0(1,2,3-CD)PYRENE Not detected ug/kg 1900 SW846·8270C 6/20/01 01:29 HWC ISOPHORONE Not detected ug/kg 1900 SW846-8270C 6/20/01 01 :29 HWC 2-METHYL-4,6-DINITROPHENOL Not detected ug/kg 9500 SW846-8270C 6/20/01 01:29 HWC 2-METHYL NAPHTHALENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 2·METHYL·PHENOL Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 4-METHYL-PHENOL Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC NAPHTHALENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC NITROBENZENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 2-NITROPHENOL Not detected -ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 4-NITROPHENOL Not detected ug/kg 9500 SW846-8270C 6/20/01 01 :;!9 HWC N-NITROSODIPHENYLAMINE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC N-NITROSODI-N-PROPYLAMINE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC PENTACHLOROPHENOL Not detected . ug/kg 9500 SW846-8270C 6/20/01 01:29 HWC PHENANTHRENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC PHENOL Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC PYRENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 1,2,4-TRICHLOROBENZENE Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 2,4,5-TRICHLOROPHENOL Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC 2,4,6-TRICHLOROPHENOL Not detected ug/kg 1900 SW846-8270C 6/20/01 01:29 HWC ---------- NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 2405H ...._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ...._Toll Free Number: 1-800/529-6364 ..... Fax: 704/525-0409 • Lab Report 6/21/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 8 of 8 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: C-1 (0·.5) Prism Sample ID: AC10434 LoQin Group: MK621 H3B Sample Collection Date/Time: 6/13/01 14:10 Lab Submittal Date/Time: 6/14/01 11:20 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER Sample Comments: TEST RESULT UNITS REPORTING METHOD LIMIT REFERENCE DATE/TIME STARTED ANALYST Analysis note for SW-846/8270: MDLs for this sample were raised due to dilutions made to sample prior to analysis. Sample was analyzed at a (1:5) dilution, therefore MDLs were raised·5 times. Sample had thick oil matrix. • Angela D. Overcash, V.P. Laboratory Services • NC Certification No. 402 • SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 ... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 CHAIN Ot;' CU._QI.)Y RECORD ) I /'1/fi,, .... ,.,/ Full Se!Vice Analytical & Environmental Solutions . n1.ci_,d.J(«.·J., r1ssoc-,-,, Chen~ -·· -qrno--i:. ,,c: a ;-r{-.v:.rk-,(;/~--·~7~c•) 1Jit•••c:~~;j;;Ue-itk-J.J"iJ.o·so------· - -----715'/-3.:fJ -·.::itt ):1 ---------,,)-.. f--=--~.:F?J~--:-97~~~-­ Phone __ -----· ----!{ rt·-1.-=~X ------------ P.O.#/Billing R?l•ence ,~-. __ :_~ --,-J _______ •1. ----· .-:_-.·~----"-~--.~:.) j{-1( -fV1-t:J.:: .• ~/5-J:t . .N' '\j IT Project Name . _ __ _ __ __ _ _ _ _ ~----__ _ PAGE __ OF __ QUOTE# __ _. I (. tP{,·(~:-!.,.,, 449 Springbrook Road :.. Charlotte, NC 2821 7 P.O. Box 240543 ...... Charlotte, NC 28224-0543 Phone: 704/5~9,~~3,6J ~r~~.f/2~~525-0409 REPORT TO: Name -~-~-------------~~---~---___ _ _ -- Address -,<1-i--.-;.;:=-,?-J----. -.l:.·?l·~r,.~--=----· c_., " • -, 1-·-~ ..... •' v ' BILL TO: Name ./ -- / ;:;---·-Address __ --· Requested Due Date 0 1 Day 0 2 Days 0 3 Days 0 4 Days 0 5 Days 0 6-9 Days 0 Standard 10 days Samples received after 15:00 will be processed the next business day. Turnaround time is based on business days, excluding weekends and holidays, (SEE . SIDE FOR RUSH TURNAROUND FEES) SAMPLE CLIENT SAMPlE DESCRIPTION DATE COllECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) "TYPE SEE BElOW NO. SIZE PRESERVA- TIVES NPDES: u NC 0 sc w OTHER UST: 0 NC 0 sc 0 OTHER -0) /.cJ</J i/.30 i.j ~;-(;~ GROUNDWATER: 0 NC I 0 SC (.:. {;- ,, DRINKING WATER: 0 NC 0 sc \>OLIO WASTE: 0 NC 0 sc 0 OTHER '0 OTHER 0 OTHER li 1.• CERCLA '6 NC 0 sc 0 OTHER NC--·-SC -·- . No -d .:__,_,....,.._· Other-----NA --· NA Water Chlorinated Yes . Sample Iced Upon Collection CMUD -_ -·-· NPDES . Yes No . -----· OTHER. _____ _ I I I Affiliation OTHER: 0 NC 0 sc 0 OTHER Additional Comments: \/ t. ).;,.,_..f I r.''";'-1./i'/t.'l.i. ,, ,<}--( bc;-,,_.;71 ,!//•~.~{/ .d: ~-s-·:,1 / i ·. PRISM LAB IDNO. PRISM USE ONLY -·--,' ' Mile~ge -· .... - SEE REVERSE FOR TERMS & CONDITIONS '•CONTAINER TYPE CODES: A =Amber C =Clear G =Glass P =Plastic; TL = Teflon-li~ed Cap VOA =Volatile Organics Analysis (Zero Head Space) FINAL REPORT COPY • • • Lab Report PRISM LAaoFiATORIES,INC. Fu!l Service Analytical & Environmental Solutions 6/20/01 Page 1 of 17 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: F-1 (11-12) PO Box 669004 Prism Sample 10: AC10370 Charlotte, NC 28266 Loqin Group: MK620H5 Sample Collection Date/Time: 6/12/01 10:10 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: ··--··-·----· .~ TEST TEST REPORTING METHOD DATEITIME .J'.ARAMETER RESULT UNITS LIMIT REFERENCE STARTED ... __ _!INAL Y~ CALCULATIONS BASED ON DRY WT. 82 % DRYWT. 0.01 SM 2540 G 6/19/01 17:05 JLW PREP. METHOD 3550 Completed SW846-35508 6/18/01 20:00 JLW ACENAPHTHENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC ACENAPHTHYLENE Not detected ug/kg 400 SW846·8270C 6/19/01 23:12 HWC ANTHRACENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BENZO(A)ANTHRACENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BENZO(B)FLUORANTHENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BENZO(K)FLUORANTHENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BENZO(A)PYRENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BENZO(GHI)PERYLENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BIS(2·CHLOROETHOXY)METHANE · Not detected . ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BIS(2·CHLOROETHYL)ETHER Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BIS(2·CHLOROISOPROPYL)ETHER Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BIS(2·ETHYLHEXYL)PHTHALATE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 4-BROMOPHENYL PHENYL ETHER Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC BUTYL BENZYL PHTHALATE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 4-CHLOR0-3-METHYLPHENOL Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 2-CHLORONAPHTHALENE Not detected ug/kg 400 SW 846-8270C 6/19/01 23:12 HWC 2-CHLOROPHENOL Not detected ug/kg 400 SW846·8270C 6/19/01 23:12 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC CHRYSENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC DIBENZOFURAN Not detected ug/kg 400 SW846·8270C 6/19/01 23:12 HWC DI·N·BUTYLPHTHALATE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 1,2-DICHLOROBENZENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 1 ,3-DICHLOROBENZENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 1 ,4-DICHLOROBENZENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 2,4-DICHLOROPHENOL Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC DIETHYL PHTHALATE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 2,4-DIMETHYLPHENOL Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC NC Certification No. 402 • SC Certification No. 99012 • NC DrinkinQ Water Cert. No. 37735 • FL Certification No. E87519 449 Springbrook Road """ P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364""" Toll Free Number: 1-800/529-6364 ...,. Fax: 704/525-0409 • • • Lab Report ~~,J~ Full Service Analytical & Environmental Solutions ' 6/20/01 Page 2 of 17 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample·ID: F-1 (11-12) PO Box 669004 Prism Sample ID: AC10370 Charlotte, NC 28266 Loqin Group: MK620H5 Sample Collection Date/Time: 6/12/01 10:10 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST DIMETHYL PHTHALATE Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC 2,4-DINITROPHENOL Not detected ug/kg 2000 SWB46-8270C 6/19/01 23:12 HWC 2,4-DINITROTOLUENE Not detected ug/kg 400 SWB46-B270C 6/19/01 23:12 HWC 2,6-DINITROTOLUENE Not detected ug/kg 400 SWB46-B270C 6/19/01 23:12 HWC DI-N-OCTYLPHTHALATE Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC FLUORANTHENE Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC FLUORENE Not detected ug/kg 400 SW846-B270C 6/19/01 23:12 HWC HEXACHLOROBENZENE. Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC HEXACHLOROBUTADIENE Not detected ug/kg 400 SWB46-B270C 6/19/01 23:12 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC HEXACHLOROETHANE Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC INDEN0(1 ,2,3-CD)PYRENE Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC ISOPHORONE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 2-METHYL-4,6-DINITROPHENOL Not detected ug/kg 2000 SWB46-8270C 6/19/01 23:12 HWC 2-METHYL NAPHTHALENE Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC 2-METHYL-PHENOL Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 4-METHYL-PHENOL Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC NAPHTHALENE Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC NITROBENZENE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC 2-NITROPHENOL Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC 4-NITROPHENOL Not detected ug/kg 2000 SWB46-B270C 6/19/01 23:12 HWC N-NITROSODIPHENYLAMINE Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC N-NITROSODI·N-PROPYLAMINE Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC PENTACHLOROPHENOL Not detected ug/kg 2000 SWB46-8270C 6/19/01 23:12 HWC PHENANTHRENE Not detected ug/kg 400 SWB46-B270C 6/19/01 23:12 HWC PHENOL Not detected ug/kg 400 SW846-8270C 6/19/01 23:12 HWC PYRENE Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC 1 ,2,4-TRICHLOROBENZENE Not detected ug/kg 400 SWB46-B270C 6/19/01 23:12 HWC 2,4,5-TRICHLOROPHENOL Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC 2,4,6-TRICHLOROPHENOL Not detected ug/kg 400 SWB46-8270C 6/19/01 23:12 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 ...,. Toll Free Number: 1-800/529-6364...,. Fax: 704/525-0409 • • • Lab Report 6/20/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Customer Project 10: Customer Sample 10: Prism Sam ole 10: LOQin Group: Sample Collection Date/Time: Lab Submittal Date/Time: ~ r.i!~Mc. --·$A Full Service Analytical & Environmental Solutions Page 3 of 17 Cherokee-Mooresville Site F-1 (11-12) AC10370 MK620H5 6/12/01 10:10 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER Sample Comments: TEST RESULT Angela D. Overcash, V.P. Laboratory Services UNITS REPORTING METHOD LIMIT REFERENCE DATE!TIME STARTED ANALYST NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: 1-800/529-6364 ..... Fax: 704/525-0409 • • • Lab Report 6/20/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 4 of 17 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: 1-1 (0-2) Prism Sample 10: AC10371 Looin Grouo: MK620H5 Sample Collection Date/Time: 6/12/01 11:50 Lab Submittal Date/Time: 6/13/01 15:40 . The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST TPH -DIESEL RANGE · 33 mg/kg 10 80 15MOD/3550 6/18/01 09:31 GRR OIL & GREASE, HYDROCARBONS Less than mg/kg 50 9071/silica 6/19/01 09:00 GRR CALCULATIONS BASED ON DRY WT. 87 %DRYWT. 0.01 SM 2540 G 6/18/01 17:00 JLW PREP. METHOD 3550 · Completed SW846-3550 6/15/01 09:30 JMV Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ WaterCert. No. 37735-FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .._Toil Free Number: 1-800/529-6364 ... Fax: 704/525-0409 Lab Report ~A~M. • Full Service Analytical & Enviroomental Solutions 6/20/01 b Page 5 of 17 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: L-1 ( (1-3) PO Box 669004 Prism Sample 10: AC10372 Charlotte, NC 28266 Loqin Group: MK620H5 Sample Collection Daterrime: 6/12101 13:55 Lab Submittal Daterrime: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CALCULATIONS BASED ON DRY WT. 89 % DRYWT. 0.01 SM 2540 G 6/19/01 17:05 JLW METALS DIGESTION METHOD 3050 Completed SW846-3050 6/15/01 13:15 LC2 PREP. METHOD 3550 Completed SW846-3550B 6/18/01 20:00 JLW ANTIMONY, TOTAL 1.4 mg/kg 1.0 SW846-60.10B 6/18101 20:35 MSP ARSENIC, TOTAL 2.9 mg/kg 1.0 SW846-601 OB 6/18/01 20:35 MSP BERYLLIUM, TOTAL Less than mg/kg 1.0 SW846-6010B 6/18/01 20:35 MSP CADMIUM, TOTAL Less than mg/kg 1.0 SW846-601 OB 6/18/01 20:35 MSP • CHROMIUM, TOTAL 25 mg/kg 1.0 SW846-601 OB 6118101 20:35 MSP COPPER, TOTAL 66 mg/kg 2.0 SW846-601 OB 6118101 20:35 MSP LEAD, TOTAL 160 mg/kg 2.0 SW846-601 OB 6120/01 13:45 MSP NICKEL, TOTAL 14 mg/kg 1.0 SW846-601 OB 6/18/01 20:35 MSP SELENIUM, TOTAL Less than mg/kg 2.0 SW846-6010B 6/18/01 20:35 MSP SILVER, TOTAL Less than mg/kg 2.0 SW846-6010B 6/18/01 20:35 MSP THALLIUM, TOTAL Less than mg/kg 0.50 SW846-601 OB 6/18/01 20:35 MSP ZINC, TOTAL 150 mg/kg 2.0 SW846-601 OB 6/20101 13:45 MSP MERCURY, TOTAL Less than mg/kg 0.02 SW846-7471 6119/01 13:31 PRF MERCURY DIGESTION Completed SW846-7471 6/18/01 12:00 LC2 BENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB BROMOBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB BROMOCHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB BROMODICHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB BROMOFORM Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB BROMOMETHANE Not detected ug/kg 12.0 SW846-8260B 6/19/01 23:21 CMB N-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB SEC-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19101 23:21 CMB TERT-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19101 23:21 CMB CARBON TETRACHLORIDE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB • CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19101 23:21 CMB CHLORODIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB CHLOROETHANE Not detected ug/kg 12.0 SW846-8260B 6/19/01 23:21 CMB NC Certification No. 402 SC Certification No. 99012 -NC Drinking Water Cart. No. 37735 -FL Certification No. EB7519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: t-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report _A.~.M· Full Service Analytical & Environmental Solutions 6/20/01 b Page 6 of 17 Mid-Atlantic Associates Customer Project 10: Ch~kee-Mooresville Site Cliff Lundgren Customer Sample 10: L-1 (1-3) PO Box 669004 Prism Sam ole 10: AC10372 Charlotte, NC 28266 Loain Grouo: MK620H5 Sample Collection Date/Time: 6/12/01 13:55 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST ·-~·-~~~· CHLOROFORM Not detected ug/kg 6,0 SW846-8260B 6/19/01 23:21 CMB CHLOROMETHANE Not detected ug/kg 12.0 SW846-8260B 6/19/01 23:21 CMB 2-CHLOROTOLUENE Not detected . ug/kg 6.0 SW846-82608 6/19/01 23:21 CMB 4-CHLOROTOLUENE Not detected ug/kg 6.0 SW846.-8260B 6/19/01 23:21 CMB 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-8260B 6/19/01 23:21 CMB 1 ,2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB DIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1,2-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/19/01 23:21 CMB 1,3-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1 ,4-DICHLOROBENZENE Not detected · ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1, 1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/19/01 23:21 CMB 1,2-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1, 1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB CIS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB TRANS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1,3-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1,1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB ETHYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB HEXACHLOROBUTADIENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB ISOPROPYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB P-ISOPROPYLTOLUENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-8260B 6/19/01 23:21 CMB NAPHTHALENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB STYRENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1,1, 1,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..., P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364..., Fax: 704/525-0409 • • • ... Lab Report . ' -.PRISM LABDiiATORJES,INC. :~· Full Service Analytical & Environmental Solutions 6/20/01 b Page 7 of 17 Mid-Atlantic Associates Customer Project 10: Chtkee-Mooresville Site Cliff Lundgren Customer Sample 10: L-1 (1-3) PO Box 669004 Prism Sam ole 10: AC10372 Charlotte, NC 28266 Loqin Group: MK620H5 Sample Collection Date/Time: 6/12/01 13:55 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST TETRACHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/19/01 23:21 CMB TOLUENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1 ,2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21-CMB 1 ,2.4-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1, 1,1-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1,1 ,2-TRICHLDROETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB TRICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1,2,3-TRICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1 ,2,4-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 1 ,3,5-TRIMETHYLBENZENE Not detected ug/kg. 6.0 SW846-8260B 6/19/01 23:21 CMB VINYL CHLORIDE Not detected ug/kg 12.0 SW846-8260B 6/19/01 23:21 CMB TOTAL XYLENES Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-82608 6/19/01 23:21 CMB. 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 SW846-8260B 6/19/01 23:21 CMB. 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260B 6/19/01 23:21 CMB ACETONE Not detected ug/kg 120.0 SW846-8260B 6/19/01 23:21 CMB CARBON DISULFIDE Not detected ug/kg 120.0 SW846-8260B 6/19/01 23:21 CMB VINYL ACETATE Not detected ug/kg 60.0 SW846-8260B 6/19/01 23:21 CMB CIS-1 ,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 23:21 CMB 2-HEXANONE Not detected ug/kg 60.0 SW846-8260B 6/19/01 23:21 CMB IPE Not detected ug/kg 6.0 SW846-82608 6/19/01 23:21 CMB MTBE Not detected ug/kg 6.0 SW846-82608 6/19/01 23:21 CMB SURR:DIBROMOFLUOROMETHANE 130 % 70-130 SW846-8260B 6/19/01 23:21 CMB SURR:TOLUENE-DB 139. % 70-130 SW846-8260B 6/19/01 23:21 CMB SURR:BROMOFLUOROBENZENE 121 % 70-130 SW846-8260B 6/19/01 23:21 CMB --------- ACENAPHTHENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC ACENAPHTHYLENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road...., P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone; 704/529-6364...., Toll Free Number: t-800/529-6364...., Fax: 704/525-0409 • • • Lab Report ~ l'Rffi~ . ~ -LABOR_~TORIES, INC~ -"""'-"'~ Full Service Analytical & Environmental Solutions 6/20/01 £ Page8of17 Mid-Atlantic Associates Customer Project 10: Ch~kee-Mooresville Site Cliff Lundgren Customer Sample 10: L·1 (1·3) PO Box 669004 Prism Sam ole 10: AC10372 Charlotte, NC 28266 Looin Grouo: MK620H5 Sample Collection Daterrime: 6/12/01 13:55 Lab Submittal Daterrime: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST ANTHRACENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC BENZO(A)ANTHRACENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC BENZO(B)FLUORANTHENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC BENZO(K)FLUORANTHENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 . HWC BENZO(A)PYRENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC BENZO(GHI)PERYLENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC BIS(2-CHLOROETHOXY)METHANE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC BIS(2-CHLOROETHYL)ETHER Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 4-BROMOPHENYL PHENYL ETHER Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC BUTYL BENZYL PHTHALATE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 4-CHLOR0-3-METHYLPHENOL Not detected uglkg 1900 SW846-8270C 6/19/01 23:58 HWC 2-CHLORONAPHTHALENE Not detected ug/kg · 1900 SW846-8270C 6/19/01 23:58 HWC 2-CHLOROPHENOL Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC CHRYSENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC DIBENZO(A,H)ANTHRACENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC DIBENZOFURAN Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC Dt-N-BUTYLPHTHALATE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 1,2-DICHLOROBENZENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 1,3-DICHLOROBENZENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 1,4-DICHLQROBENZENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58. HWC 2,4-DICHLOROPHENOL Not delected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC DIETHYL PHTHALATE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 2,4-DIMETHYLPHENOL Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC DIMETHYL PHTHALATE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 2,4-DINITROPHENOL Not detected ug/kg 9500 SW846-8270C 6/19/01 23:58 HWC 2,4-DINITROTOLUENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 2,6-DINITROTOLUENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrjnkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road....._ P.O. Box 240543 .... Charlotte, NC ~8224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • ,,, Lab Report .~~A Full Service Analytical & Environmental Solutions 6/20/01 ~ Page 9 of 17 Mid-Atlantic Associates Customer Project ID: Ch~kee-Mooresville Site Cliff Lundgren Customer Sample ID: L-1 (1-3) PO Box 669004 Prism Sample ID:· AC10372 Charlotte, NC 28266 Loqin Group: MK620H5 Sample Collection Date/Time: 6/12/01 13:55 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST DI-N-OCTYLPHTHALATE Not detected ug/kg 1900· SW846-8270C 6119101 23:58 HWC FLUORANTHENE Nat detected ug/kg 1900 SW846-8270C 6119101 23:58 HWC FLUORENE Not detected ug/kg 1900 SW846-8270C 6119101 23:58 HWC HEXACHLOROBENZENE Not detected ug/kg 1900 SW846-8270C 6119101 23:58 HWC HEXACHLOROBUTADIENE Not detected ug/kg 1900 SW846-8270C 6119101 23:58 HWC HEXACHLOROCYCLOPENTADIENE Nat detected ug/kg 1900 SW846-8270C 6119101 23:58 HWC HEXACHLOROETHANE Not detected ug/kg 1900 SW846-8270C 6119/01 23:58 HWC I NDEN0(1,2,3-CD)PYRENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC ISOPHORONE Not detected ug/kg 1900 SW846-8270C 6/19101 23:58 HWC 2-METHYL-4,6-DINITROPHENOL Nat detected ug/kg 9500 SW846-8270C 6/19/01 23:58 HWC 2-METHYL NAPHTHALENE Not detec_ted ug/kg 1900 SW846-8270C 6/19/0J 23:58 HWC 2-METHYL-PHENOL Not detected ug/kg. 1900 SW846-8270C 6/19/01 23:58 HWC 4-METHYL-PHENOL Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC NAPHTHALENE Not detected ug/kg 1900. SW846-8270C 6/19/01.23:58 HWC NITROBENZENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 2-NITROPHENOL Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 4-NITROPHENOL Not detected ug/kg 9500 SW846-8270C 6/19/01 23:58 HWC N-NITROSODIPHENYLAMINE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC N-NITROSODI-N-PROPYLAMINE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC PENTACHLOROPHENOL Not detected ug/kg 9500 SW846-8270C 6/19/01 23:58 HWC PHENANTHRENE Nat detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC PHENOL Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC PYRENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 1,2,4-TRICHLOROBENZENE Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 2,4,5-TRICHLOROPHENOL Not detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC 2,4,6-TRICHLOROPHENOL Nat detected ug/kg 1900 SW846-8270C 6/19/01 23:58 HWC -------- NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .-..Toll Free Number: 1-800/529-6364.., Fax: 704/525-0409 • • • ~~:·· ·.~ Lab Report .,A.~N. 6/20/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Customer Project 10: Customer Sample 10: b Page 10 of 17 Chejkee-Mooresville Site L-1~~-3) , Prism Sample 10: AC10372 Loqin Group: MK620H5 Sample Collection Date/Time: 6/12/01 13:55 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER Sample Comments: TEST RESULT "UNITS REPORTING METHOD .DATEITIME LIMIT REFERENCE · STARTED ANALYST Analysis note for SW-846/8270: MDLs for this sample were raised due to dilutions made to sample prior to analysis. Sample was analyzed at a (1 :5) dilution, therefore MDLs were raised 5 times. Sample had thick oil matrix. Note for 8260: Surrogate recovery outside QC control limits . Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report 6/20/01 Mid-Atlaniic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 PRISM LABORATORIES, INC . Full Service Analytical & Environmental Solutions Page 11 of 17 Customer Project ID: ·Cherokee-Mooresville Site Customer Sample ID: G-2 (0-2) Prism Samole ID: AC10373 Loqin Group: MK620H5 Sample Collection Date/Time: 6/12/01 16:1 0 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST TPH -DIESEL RANGE Less than mg/kg 10 8015MOD/3550 6/18/01 08:50 GRR TPH-GASOLINE RANGE Less than mg/kg 1.0 8015MOD/5030 6/15/01 17:56 KC CALCULATIONS BASED ON DRY WT. 86 %DRYWT. 0.01 SM 2540 G 6/19/01 17:05 JLW PREP. METH_OD 3550 Completed SW846-3550 6115/01 09:30 JMV Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. EB7519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 _...Fax: 704/525-0409 • • • Lab Report 6/20/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 12 of 17 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: L•3'(5-6)_ Prism Samole 10: AC10374 Loqin Group: MK620H5 Sample Collection Date/Time: 6/12/01 16:55 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER CALCULATIONS BASED ON DRY WT. METALS DIGESTION METHOD 3050 PREP. METHOD 3550 ANTIMONY, TOTAL ARSENIC, TOTAL BERYLLIUM, TOTAL CADMIUM, TOTAL CHROMIUM, TOTAL COPPER, TOTAL LEAD, TOTAL NICKEL, TOTAL SELENIUM, TOTAL SILVER, TOTAL THALLIUM, TOTAL ZINC, TOTAL MERCURY, TOTAL MERCURY DIGESTION BENZENE BROMOBENZENE BROMOCHLOROMETHANE BROMODICHLOROMETHANE BROMOFORM BROMOMETHANE N-BUTYLBENZENE SEC-BUTYLBENZENE TERT-BUTYLBENZENE CARBON TETRACHLORIDE CHLOROBENZENE CHLORODIBROMOMETHANE CHLOROETHANE TEST RESULT 75 Completed Completed 3.4 5.1 2.3 Less than 58 5.1 15 14 Less than Less than Less than 130 0.03 Completed Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not detected Not d8tected Not detected Not detected Not detected Not detected UNITS % DRYWT. mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg uglkg REPORTING METHOD DATE!TIME STARTED LIMIT REFERENCE 0.01 1.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 2.0 2.0 0.5 1.0 0.03 6.0 6.0 6.0 6.0 6.0 12.0 6.0 6.0 6.0 6.0 6.0 6.0 12.0 SM 2540 G 6/19/01 17:05 SWB46-3050 6/15/01 13:15 SWB46-3550B 6/18/01 20:00 SW846-6010B 6/18/01 20:51 SWB46-6010B 6/18/01 20:5i SWB46-6010B 6/18/01 20:51 SWB46-6010B 6/18/01 20:51 SW846-6010B 6/18/01 20:51 SW846-6010B · 6/18/01 20:51 SWB46-6010B 6/18/01 20:51 SWB46-6010B 6/18/01 20:51 SWB46-6010B 6118101 20:51 SW846-6010B 6118101 20:51 SW846-6010B 6118101 20:51 SWB46-6010B 6/18101 20:51 SW846-7471 6119101 13:19 SWB46-7471 6118101 12:00 SWB46-8260B 6120101 11:57 SWB46-8260B 6/20101 11:57 SWB46-8260B 6120101 11:57 SWB46-8260B 6120101 11:57 SW846-8260B 6120/01 11:57 SW846-8260B 6/20101 11:57 SW846-8260B 6120101 11:57 SWB46-8260B 6120101 11:57 SWB46-8260B 6120101 11:57 SWB46-8260B 6120101 11:57 SWB46-8260B 6120/01 11:57 SWB46-8260B 6120101 11:57 SWB46-8260B 6120/01 11:57 ANALYST JLW LC2 JLW MSP MSP MSP MSP 'MSP MSP MSP MSP MSP MSP MSP MSP PRF LC2 CMB CMB CMB CMB CMB CMB CMB CMB CMB CMB. CMB CMB CMB NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .., P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364.., ToU Free Number: 1-800/529-6364.., Fax: 704/525-0409 • • • ·*!:~ ~ .:J.t~. ' Lab Report ~~!~M.· ~ Full Service Analytical & Environmental Solutions 6/20/01 Page 13 of 17 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: L-3 (5-6) PO Box 669004 Prism Sample 10: AC10374 Charlotte, NC 28266 Loqin Group: MK620H5 Sample Collection Date/Time: 6/12/01 16:55 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST CHLOROFORM Not detected ug/kg 6.0 SW846-8260B 6/20/01 11 :57 CMB CHLOROMETHANE Not detected ug/kg 12.0 SW846-8260B 6/20/01 11:57 CMB 2-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 4-CHLOROTOLUENE Not detected ug/kg . 6.0 SW846-8260B 6/20/01 11:57 CMB 1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-8260B 6/20/01 11:57 CMB 1 ,2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB DIBROMOMETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 11:57 CMB 1,2-DICHLOROBENZENE Not detected ug/kg 6.0 · SW846-82608 6/20/01 11:57 CMB 1 ,3-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 1 ,4-DICHLOROBENZENE Not deteCted ug/kg 6.0 SW846-82608 6/20/01 11:57 CMB DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 11:57 CMB 1, 1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 11:57 CMB 1 ,2-DICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 11:57 CMB 1, 1-DICHLOROETHENE " .. Not detected ug/kg 6.0 SW846-82608 6/20/01 11:57 CMB CIS-1 ,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/20/01 11:57 CMB TRANS-1 ,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/20/01 11:57 CMB 1,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 1 ,3-DICHLOROPROPANE Not detected ug/kg 6:0 SW846-82608 6/20/01 11:57 CMB 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 1, 1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11 :57 CMB ETHYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB HEXACHLOROBUTADIENE Not detected ug/kg 6.0 SW846-8260B 6120101 11 :57 CMB ISOPROPYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB P-ISOPROPYL TOLUENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-8260B 6/20/01 11:57 CMB NAPHTHALENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB . N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB STYRENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 1, 1,1 ,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/20/01 11:57 CMB NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. EB7519 449 Springbrook Road ...._ P.O. Box 240543 ...._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ...._ Toll Free Number: 1-800/529-6364 ...._ Fax: 704/525-0409 • • • Lab Report ~Pit': LABORA!~M.· .,..;;:::-~ . . ; Full Service Analytical & Environmental Solutions · 6/20/01 Page 14 of 17 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: L-3 (5-6) PO Box 669004 Prism Samole ID: AC10374 Charlotte, NC 28266 Loqin Group: MK620H5 Sample Collection Daterrime: 6/12/01 16:55 Lab Submittal Daterrime: 6/13/01 15:40. The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEffiME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST TETRACHLOROETHENE Not detected ug/kg . 6.0 SW846'82SOB 6/20/01 11:57 CMB TOLUENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 1,2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 1,2,4-TRICHLOROBENZENE Not detected .ug/kg 6.0 SW~46-8260B 6/20/01 11:57 CMB 1, 1,1•TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 1,1 ,2-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB TRICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 . SW846-8260B 6/20/01 11:57 CMB 1,2,3-TRICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB ' 1 ,2,4-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/20/01. 11:57 CMB 1,3,5-TRIMETHYLBENZENE · Not detected . ug/kg 6.0 SW846-8260B 6/20/01 11:57 . CMB VINYL CHLORIDE Not detected ug/kg 12.0 SW846-8260B 6/20/01 11:57 CMB TOTAL XYLENES Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-8260B 6/20/01 11:57 CMB 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 SW846-8260B 6/20/01 11:57 CMB- 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260B 6/20/01 11:57 CMB ACETONE Not detected ug/kg 120.0 SW846-8260B 6/20/01 11:57 CMB CARBON DISULFIDE Not detected ug/kg 120.0 SW846-8260B 6/20/01 11:57 CMB VINYL ACETATE Not detected ug/kg 60.0 SW846-8260B 6/20/01 11:57 CMB CIS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB 2-HEXANONE Not detected ug/kg 60.0 SW846-8260B 6/20/01 11:57 CMB IPE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB MTBE Not detected ug/kg 6.0 SW846-8260B 6/20/01 11:57 CMB SURR:DIBROMOFLUOROMETHANE 112 % 70-130 SW846-8260B 6/20/01 11:57 CMB SURR:TOLUENE-D8 119 % 70-130 SW846-8260B 6/20/01 11:57 CMB SURR:BROMOFLUOROBENZENE 94 % 70-130 · SW846-8260B 6/20/01 11:57 CMB --------- ACENAPHTHENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC ACENAPHTHYLENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...,. P.O. Box 240543 ..-.. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..o.. Toll Free Number: 1-800/529-6364 ..o.. Fax: 704/525-0409 • • • .. ' . " . -.. ~~:~·· Lab Report . -~ ~f.!!~~i _..,.~ Full Service Analytical & Environmental Solutions 6/20/01 Page 15 of 17 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: L-3 (5-6) PO Box 669004 Prism Sam ole 10: AC10374 Charlotte, NC 28266 Loqin Group: MK620H5 Sample Collection Date/Time: 6/12/01 16:55 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST ANTHRACENE Not detected ug/kg 440 SW846-8270C 6120101 00:43 HWC 8ENZO(A)ANTHRACENE Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC' 8ENZ0(8)FLUORANTHENE Not-detected ug!kg 440 SW846-8270C 6/20/01 00:43 HWC 8ENZO(K)FLUORANTHENE Not detected ug/kg 440 SW846-8270C 6/20101 00:43 HWC 8ENZO(A)PYRENE Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC 8ENZO(GHI)PERYLENE Not detected ug/kg . · 440 SW846-8270C 6120101 00:43 HWC 81S(2·CHLOROETHOXY)METHANE Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC 81S(2-CHLOROETHYL)ETHER Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC 81S(2-CHLOROISOPROPYL)ETHER Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC 81S(2-ETHYLHEXYL)PHTHALATE Not detected ug/kg 440 SW846-8270C 6120101 00:43 HWC 4-BROMOPHENYL PHENYL ETHER Not detected ug/kg 440' SW846-8270C 6/20/01 00:43 HWC 8UTYL8ENZYLPHTHALATE Not detected ug/kg 440 SW846-8270C 6120101 00:43 HWC 4-CHLOR0-3-METHYLPHENOL Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC 2-CHLORONAPHTHALENE · Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC 2-CHLOROPHENOL Not detected ug/kg 440 SW846-8270C 6120101 00:43 HWC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 440 SW846-8270C 6120101 00:43 HWC CHRYSENE Not detected ug/kg 440 SW846-8270C 6/20101 00:43 HWC DI8ENZO(A,H)ANTHRACENE Not detected ug/kg 440 SW846-8270C 6120101 00:43 HWC DI8ENZOFURAN Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC DI-N-8UTYLPHTHALATE Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC 1,2-DICHLOR08ENZENE Not detected ug/kg 440 SW846-8270C 6120101 00:43 HWC 1,3-DICHLOR08ENZENE Not detected ug/kg 440 SWB46-8270C 6120101 00:43 HWC 1.4-DICHLOR08ENZENE Not detected ug/kg 440 SW846-8270C 6/20101 00:43 HWC 2.4-DICHLOROPHENOL Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC DIETHYL PHTHALATE Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC 2,4-DIMETHYLPHENOL Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC DIMETHYL PHTHALATE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC 2.4-DINITROPHENOL Not detected ug/kg 2200 SW846-8270C 6120/01 00:43 HWC 2,4-DINITROTOLUENE Not detected ug/kg 440 SW846-8270C 6120/01 00:43 HWC 2,6-DINITROTOLUENE Not detected ug/kg 440 SW846-8270C 6120101 00:43 HWC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364""" Toll Free Number: t-800/529-6364""" Fax: 704/525-0409 Lab Report • • • 6/20/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 16 of 17 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: L-3 (5-6) Prism Sa mole 10: AC1 037 4 Looin Group: MK620H5 Sample Collection Date/Time: 6/12/01 16:55 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE!TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST DI-N-OCTYLPHTHALATE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC FLUORANTHENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC FLUORENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC HEXACHLOROBENZENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC HEXACHLOROBUTADIENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC HEXACHLOROCYCLOPENTADIENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC HEXACHLOROETHANE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC INDEN0(1,2,3-CD)PYRENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC ISOPHORONE Not detected ug/kg 440 SWB46-8270C 6/20/01 00:43 HWC 2-METHYL-4,6-DINITROPHENOL Not detected ug/kg 2200 SW846-8270C "6/20/01 00:43 HWC .2-METHYL NAPHTHALENE NOt detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC 2-METHYL-PHENOL Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC 4-METHYL-PHENOL Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC .NAPHTHALENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC NITROBENZENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC 2-NITROPHENOL Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC 4-NITROPHENOL Not detected ug/kg 2200 SW846-8270C 6/20/01 00:43 HWC N-NITROSODIPHENYLAMINE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC N-NITROSODI-N-PROPYLAMINE Not detected ug/kg 440 SWB46-8270C 6/20/01 00:43 HWC PENTACHLOROPHENOL Not detected ug/kg 2200 SW846-8270C 6/20/01 00:43 HWC PHENANTHRENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC PHENOL Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC PYRENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC 1 ,2,4-TRICHLOROBENZENE Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC 2,4,5-TRICHLOROPHENOL Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC 2,4,6-TRICHLOROPHENOL Not detected ug/kg 440 SW846-8270C 6/20/01 00:43 HWC ---------- NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 ...._ Charlotte, NC 28224-0543 Phone: 704/529-6364 ...._ Toll Free Number: l-800/529-6364 ...._ Fax: 704/525-0409 • • • Lab Report 6/20/01 Mid-Atlantic Associates Clift Lundgren PO Box 669004 Charlotte, NC 28266 ~--~: PRISM LABORATOAtES, INC. Full Service Analytical & Environmental Solutions Page 17 of 17 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: L-3 (5-6) Prism Sample 10: AC10374 LoQin Group: MK620H5 Sample Collection Date/Time: 6/12/01 16:55 Lab Submittal Date/Time: 6/13/01 15:40 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST PARAMETER Sample Comments: TEST RESULT Angela D. Overcash, V.P. Laboratory Services REPORTING METHOD UNITS LIMIT REFERENCE DATEITIME STARTED ANALYST NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ... Toll Free Number: l-800/529-6364 .., Fax: 704/525-0409 CHAIN OF CU~5~!,<P~~f10RD PAGE _!__ OF _f_ QUOTE I L . Full Service Analytical & Environmental Solutions . !Yl:a' -/IN~· ,, /. 1 <. A -: . .soc . ~;::~aJ~-"JJ----y:-~_f o:~?:;~_.'!_z,~_~c-t_-~~:--_. ,--5,-_•'(:._;;_1-:_-- ~':)"fe. , o :1 (.....1'1 ~' / !t-l~l 1 /~-"---t7-J oJ......-:) ---,D~r:.-_3q,y--=-t7J;---;;c--~)9----::;·'l'<J--=-9/~ Phone __ ------J?·;r~"''-jax ------------ P.O.#/Billing R ... rence -•·f'a--•" -----~(;n-<:-'-'-1·.-·.----L,.,t~.r.o"" <. -/n [l.{:!ll!.S!..I' ,_, ... _. 1 Project Name _ _ _. _ _ __ _ .. _ TIME MATRIX CLIENT DATE CQbb~-I~~ (SOIL, SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 449 Springbrook Road .... Charlotte, NC 28217 P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 70415?!;?~~ ~}}'J/~~(525-0409 REPORT TO: Name ___ __ _ . -~ .. -· --. Add,.ss,-.1-/-f'¥---'--"z·· ··--· ·-~----t.-· ',., ·r "'-;,;'•,.·c.:.• :1 .-:-.. , ·Name ..... __ _ BILLTO: · Address / Requested Due Date 0 1 Day 0 2 Days 0 3 Days 0 4 Days 0 5 Days 0 6-9 Days 0 Standard.10 days Samples receiVed after 15:00 will be processed the next busifless day. Turnaround time is based on busir:tess days, excluding weekends and holidays. SAMPLE CONTAINER PAESER~A- 'TYPE TIVES HOURS SLUDGE) SEE BELOW NO. SIZE NPDES: 0 NG a SG UST: 0 NG a SG "·· L ··' 6· L II ,, /, I; -_,,.-- .',' u / ( .... ~---~-" GROUNDWATER: 0 NG a sG 1 DRINKING WATER: . 0 NG 'a SG ,,. " -'•;. ... ~) 1 SOLID WASTE: ! 0 NC ~a SG J.)o.•- ., .. I I ,, I RCRA: I CERCLA I LANDFILL OSG· OSG OSG LAB USE ONLY . State Certification \-.,./ Requested FL ___ NG SG -. Other-NA - Water Chlorinated Yes No NA Sample Iced Upon Collection GMUD ---_ NPDES -- REMARKS I I OTHER: 0 NG - a SG ... .: .. ~-·/J.. lj. ' . •. .,) f"'\"-pA_ ;...t . ~, , _;(.·· .. -_,.., ;::_~ L L ; 8JJ { ___ ---------- PRISM USE ONLY •. ·\_ .. · ;• J -. ·:·--... 0 OTHER' 0 OTHER 0 OTHER 0 OTHER I 0 OTHER ONG lONG 1 aNG 0 OTHER 0 OTHER I ' 0 OTHER I 0 OTHER SEE REVERSE FOR TERMS & CONDITIONS *CONTAINER TYPE CODES: A =Amber C =Clear G,= Glass P =Plastic; TL =Teflon-Lined Cap VOA :=Volatile Organics Analysis (Zero Head Space) FINAL REPORT COPY ''·· Lab Report PRISM • • •• Today's Date: June 27, 2001 Mid-Atlantic Associates Attn: Cliff Lundgren PO Box 669004 Charlotte, NC 28266 LABORATORIES, INC. Full Service Analytical & Environmental Solutions REVISED LABORATORY REPORT Client Project ID: Cherokee-Mooresville Site Client Sample ID: E-2 (1-2) Prism Sample ID: AC10191 Prism LoginGroup: MK619H4 The attached laboratory report is a revision and supersedes our original laboratory report dated June 19, 2001 If you have questions, please call us . Angela D. Overcash, V.P. Laboratory Services Prepared by: Paula Gilleland F:lcommonlrevlab.xls Created 3/16/00 Revised 3/30/00 449 Springbrook Road ..oo. P.O. Box 240543 ..oo. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..oo. Toll Free Number: 1-800/529-6364 ..oo. Fax: 704/525-0409 • • • Lab Report PRISM LABORATORIES, INC. Full Service Analytical & Environmental Solutions 6/27/01 Page 1 of 13 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: E-3 (7-7.5) PO Box 669004 Prism Sam ole 10: AC10190 Charlotte, NC 28266 Looin Grouo: MK619H4 Sample Collection Date/Time: 6/11/01 13:45 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST C5-C8 Aliphatics Not detected mg/kg 7 MADEP VPH 6119101 02:39 KC C9-C12 Aliphatlcs Not detected mg/kg 6 MADEP VPH 6/19101 02:39 KC C9-C 10 Aromatics Not detected mg/kg 2 MADEP VPH 6119/01 02:39 KC Surrogate % Recovery-PID 90 % (70-130) MADEP VPH 6119101 02:39 KC Surrogate% Recovery-FlO 86 % (70-130) MADEP VPH 6119101 02:39 KC Dilution Factor mg/kg MADEP VPH 6119101 02:39 KC Dry Weight Received 14.23 g mg/kg MADEP VPH 6119101 02:39 KC ---------- CALCULATIONS BASED ON DRY WT. 79 % DRYWT. 0.01 SM 2540 G 6112101 16:25 JLW METALS DIGESTION METHOD 3050 Completed SW846-3050 611310115:30 LC2 LEAD. TOTAL 11 mg/kg 1.0 SW846-6010B 6114101 13:57 MSP BENZENE Not detected · ug/kg 6.0. SW846-8260B 6118101 07:30 CMB BROMOBENZENE Not detected ug/kg 6.0 SW846-82608 6118101 07:30 CMB BROMOCHLOROMETHANE Not detected ug/kg 6.0 SW846-82608 6118101 07:30 CMB BROMODICHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6118101 07:30 CMB BROMOFORM Not detected ug/kg 6.0 SW846-8260B 6118101 07:30 CMB BROMOMETHANE Not detected ug/kg 12.0 SW846-8260B 6118101 07:30 CMB N-BUTYLBENZENE Not detected ug/kg 6.0 SW846-82608 6118/01 07:30 CMB . SEC-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6118101 07:30 CMB TERT-BUTYLBENZENE Not detected ug/kg 6.0 SWB46-8260B 6/18/01 07:30 CMB CARBON TETRACHLORIDE Not detected ug/kg 6.0 SW846-8260B 6118101 07:30 CMB CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6118101 07:30 CMB CHLORODIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260B 6118101 07:30 CMB CHLOROETHANE Not detected ug/kg 12.0 SW846-8260B 6118/01 07:30 CMB CHLOROFORM Not detected ug/kg 6.0 SW846-8260B 6118101 07:30 CMB CHLOROMETHANE Not detected ug/kg 12.0 SW846-8260B 6118101 07:30 CMB 2-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260B 6118101 07:30 CMB 4-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-8260B 6118101 07:30 CMB 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-8260B 6118/01 07:30 CMB 1.2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-8260B 6/18101 07:30 CMB NC Certification No. 402 SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 • FL Certification No. EB7519 449 Springbrook Road ...._ P.O. Box 240543 ...._ Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... F.X: 704/525-0409 · • • • Lab Report ~~!.! Full ServiCe Analytical & Environmental Solutions 6/27/01 Page 2 of 13 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: E-3 (7-7.5) PO Box 669004 Prism Sample 10: AC10190 Charlotte, NC 28266 Loqin Group: MK619H4 Sample Collection Date/Time: 6/11/01 13:45 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErriME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST DIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB 1 ,2-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB 1 ,3-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB 1 .4-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB 1, 1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB 1,2-DICHLOROETHANE Not detected ug/kg 6.0 SW848-8260B 6/18/01 07:30 CMB 1, 1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB CIS-1 ,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB TRANS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB 1 ,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB 1.3-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB 1,1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB ETHYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB .. HEXACHLOROBUTADIENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB ISOPROPYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB P-ISOPROPYL TOLUENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-8260B 6/18/01 07:30 CMB NAPHTHALENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB STYRENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB 1, 1,1 ,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB TETRACHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB TOLUENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB 1 ,2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB 1,2,4-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 07:30 CMB 1.1.1-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 5/18/01 07:30 CMB 1, 1,2-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cart . .No. 37735 -FL Certification No. E87519 449 Springbrook Road ..,. P.O. Box 240543 .._ Charlotte, NC 28224~0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 Lab Report PRISM • •· 6/27/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC. 28266 LABORATORIES, INC. Full Service Analytical & Environmental Solutions Page 3 of 13 Customer Project ID: Cherokee-Mooresville Site Customer Sample ID: E-3 (7-7.5) Prism Sample ID: AC10190 LoQin Group: MK619H4 Sample Collection Date/Time: 6/11/01 13:45 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST TRICHLOROETHENE Not detected ug/kg 6.0 SWB46-8260B 6/18/01 07:30 CMB TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SWB46-8260B 6/18/01 07:30 CMB 1 ,2,3· TRICHLOROPROPANE Not detected ug/kg 6.0 SW846·8260B 6/18/01 07:30 CMB 1 ,2.4· TRI METHYLBENZENE Not detected ug/kg 6.0 SW846-8260B' 6/18/01 07:30 CMB 1 ,3,5· TRIME!HYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB -VINYL CHLORIDE Not detected ug/kg 12.0 SWB46-8260B 6/18/01 07:30 CMB TOTAL XYLENES Not detected ug/kg 6.0 SWB46-8260B 6/18/01 07:30 CMB 2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-8260B 6/18/01 07:30 CMB 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 SW846-8260B ot18to1 07:3o CMB 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260B 6/18/01 07:30 CMB ACETONE Not detected ug/kg 120.0 SW846-8260B 6/18/01 07:30 CMB CARBON DISULFIDE Not detected ug/kg 120.0 SW846-8260B 6/18/01 07:30 CMB VINYL ACETATE Not detected ug/kg 60.0 SW846-8260B 6/18/01 07:30 CMB CIS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB 2-HEXANONE Not detected ug/kg 60.0. SW846-8260B 6/18/01 07:30 CMB IPE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB MTBE Not detected ug/kg 6.0 SW846-8260B 6/18/01 07:30 CMB SURR:DIBROMOFLUOROMETHANE 120 % 70-130 SW846-8260B 6/18/01 07:30 CMB SURR:TOLUENE-D8 119 % 70-130 SWB46-8260B 6/18/01 07:30 CMB SURR:BROMOFLUOROBENZENE 121 % 70-130 SW846-8260B 6/18/01 07:30 CMB --------- Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 ·-FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: 1-800/529-6364 .... Fax: 704/525-0409 • • • Lab Report ~""~ E!IJ.M Full Service Analytical & Environmental Solutions 6/27/01 Page 4 of 13 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: E-2 (1-2) PO Box 669004 Prism Sam ole 10: AC10191 Charlotte, NC 28266 Loqin Group: MK619H4 Sample Collection Date/Time: 6/11/01 17:30 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST C5-C8 Aliphatics Not detected mg/kg 7 MADEP VPH 6119101 03:38 KC C9-C12 Aliphatics 100 mg/kg 6 MADEP VPH 6/19/01 03:38 KC C9-C10 Aromatics 9.4 mg/kg 2 MADEP VPH 6/19/01 03:38 KC Surrogate'% RecoVery-PID 81 % (70-130) MADEP VPH 6/19/01 03:38 KC Surrogate % Recovery -Fl D 87 % (70-130) MADEP VPH 6/19/01 03:38 KC Dilution Factor mg/kg MADEP VPH 6/19/01 03:38 KC· Dry Weight Received 17.25 9 mg/kg MADEP VPH 6/19/01 03:38 KC -------- EXTRACTION FOR EPH Completed ·MADEP-EPH 6/21/01 09:45 JMV C9-C18 ALIPHATICS 81 mg/kg 40 MADEP-EPH 6/22/01 19:46 KTE C19-C36 ALIPHATICS 130 mg/kg 20 MADEP-EPH 6/22/01 19:46 KTE C1 1-C22 AROMATICS 23 mg/kg 20 MADEP-EPH 6/22/01 19:46 KTE SURROGATE RECOVERY -ALIPHATIC 67 % (40-140) MADEP-EPH 6/22/01 19:46 KTE SURROGATE RECOVERY-AROMATIC 61 % (40-140) MADEP-EPH 6/22/01 19:46 KTE SURR:2-BROMONAPHTHALENE 72 '% (40-140) MADEP-EPH 6/22/01 19:46 KTE SURR:2-FLUOROBIPHENYL 82 % (40-140) MADEP-EPH 6/22101 19:46 KTE DILUTION FACTOR mg/kg MADEP-EPH 6/22/01 19:46 KTE DRY WEIGHT 8.3 9 mg/kg MADEP-EPH 6/22/01 19:46 KTE ---------- CALCULATIONS BASED ON DRY WT. 83 % DRYWT. O.D1 SM 2540 G 6/12/01 16:25 JLW METALS DIGESTION METHOD 3050 Completed SW846-3050 6/13/01 15:30 LC2 PREP. METHOD 3550 Completed SW846-35508 6/21/01 14:30 JMV LEAD, TOTAL 270 mg/kg 2.0 SW846-60108 6/18/01 13:55 MSP BENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB BROMOBENZENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 08:15 CMB BROMOCHLOROMETHANE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB BROMODICHLOROMETHANE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB BROMOFORM Not detected ug/kg 6.0 SW846-8260B 6/18/01 08:15 CMB BROMOMETHANE Not detected ug/kg 12.0 SW846-8260B 6/18/01 08:15 CMB N-BUTYLBENZENE 7.8 ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB NC Certification No. 402 SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: t -800/529-6364 .... Fax: 704/525-0409 • • • Lab Report ~·-~~~ Full Service Analytical & Environmental Solutions 6/27/01 Page 5 of 13 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: E-2 (1-2) PO Box 669004 . . Prism Sam ole ID: AC10191 Charlotte, NC 28266 Looin Grouo: MK619H4 Sample Collection Date/Time: 6/11/01 17:30 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST SEC-BUTYLBENZENE 17 ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB TERT-BUTYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB CARBON TETRACHLORIDE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 08:15 CMB CHLORODIBROMOMETHANE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB CHLOROETHANE Not detected ug/kg 12.0 SW846-8260B 6/18/01 08:15 CMB CHLOROFORM Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB CHLOROMETHANE Not detected ug/kg '12.0 SW846·82608 6/18/01 08:15 CMB 2-CHLOROTOLUENE Not detected ug/kg· 6.0 SW846-82608 6/18/01 08:15 CMB 4-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB 1 )-DIBROM0-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-82608 6/18/01 08:15 CMB 1 ,2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB DIBROMOMETHANE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB 1 ,2-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB 1 ,3-DICHLOROBENZENE Not detected ug/kg 6·.o SW846-82608 6/18/01 08:15 CMB 1 ,4-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB DICHLDRODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB 1, 1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6/18/01 08:15 CMB 1 ,2-DICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB 1, 1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB CIS-1 ,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB TRANS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB 1 ,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB 1 ,3-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-8260B 6/18/01 08:15 CMB 1, 1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846·8260B 6/18/01 08:15 CMB ETHYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB HEXACHLOROBUTADIENE Not detected ug/kg 6.0 SW846-8260B 6/18/01 08:15 CMB ISOPROPYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB P-ISOPROPYL TOLUENE 42 ug/kg 6.0 SW846-82608 6/18/01 08:15 CMB NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .._ P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: 1-800/529-6364 ..... Fa.~: 704/525-0409 • • • Lab Report . ~PRISM · LABORATORIES, INC. --€~~ FuJI Service Analytical & Environmental Solutions 6/27/01 Page 6 of 13 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: E-2 (1-2) PO Box 669004 Prism Sample 10: AC10191 Charlotte, NC 28266 Loqin Group: MK619H4 Sample Collection Date/Time: 6/11/01 17:30 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST . METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-82608 6118101 08:15 CMB NAPHTHALENE Not detected ug/kg 6.0 SW846-82608 6118101 08:15 CMB N-PROPYLBENZENE 8.0 ug/kg 6.0 SW846-82608 6118101 08:15 CMB STYRENE Not detected ug/kg 6.0 SW846-82608 6118101 08:15 CMB 1,1,1,2-TETR....eHLOROETHANE Not dete~ted ug/kg 6.0 SW846-8260B 6118101 08:15 CMB 1,1,2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-8260B 6118101 08:15 CMB TETRACHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6118101 08:15 CMB TOLUENE Not detected ug/kg 6.0 SW846-8260B 611!il01 08:15 CMB 1,2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/18101 08:15 CMB 1,2,4-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6118101 08:15 CMB 1,1,1-TRICHLOROETHANE Not detected ug/kg .6.0 SW846-8260B 6118101 08:15 CMB 1,1,2-TRICHLOROETHANE Not detected • ug/kg· 6.0 . SW846-82608 6118101 08:15 CMB TRICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6118101 08:15 CMB TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SW846-82606 6118101 08:15 CMB 1,2,3-TRICHLOROPROPANE Not detected ug/kg 6.0 SW846-82606 6118101 08:15 CMB 1,2,4-TRIMETHYLBENZENE 75 ug/kg 6.0 SW846-8260B 6118101 08:15 CMB 1,3,5-TRIMETHYLBENZENE 63 ug/kg 6.0 SW846-8260B 6118101 08:15 CMB VINYL CHLORIDE Not detected ug/kg 12.0 SW846-8260B 6118101 08:15 CMB TOTAL XYLENES Not detected ug/kg 6.0 SW846-8260B 6118101 08:15 CMB 2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-8260B 6118/01 08:15 CMB 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 . SW846-8260B 6118101 08:15 CMB 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260B 6118101 08:15 CMB ACETONE Not detected ug/kg 120.0 SW846-8260B 6118101 08:15 CMB CARBON DISULFIDE Not detected uglkg 120.0 SW846-8260B 6118101 08:15 CMB VINYL ACETATE Not detected -uglkg 60.0 SW846-8260B 6/18101 08:15 CMB CIS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6118101 08:15 CMB TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6118101 08:15 CMB 2-HEXANONE Not detected ug/kg 60.0 SW846-8260B 6118101 08:15 CMB IPE Not detected ug/kg 6.0 SW846-8260B 6118/01 08:15 CMB MTBE Not detected ug/kg 6.0 SW846-8260B 6118101 08:15 CMB NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQWater Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224·0543 Phone: 704/529-6364 ...._ Toll Free Number: 1-800/529-6364 ..... Fax: 704/525-0409 • • • Lab Report ~~~A! Full Service Analytical & Environmental Solutions 6/27/01 Page 7 of 13 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: E-2 (1-2) PO Box 669004 Prism Sample ID: AC10191 Charlotte, NC 28266 Loqin Group: MK619H4 Sample Collection DatefTime: 6/11/01 17:30 Lab Submittal DatefTime: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST SURR:DIBROMOFLUOROMETHANE 89 % 70-130 SW846-8260B 6/18/01 08:15 CMB SURR:TOLUENE-D8 135. % 70-130 SW846-8260B 6/18/01 08:15 CMB SURR:BROMOFLUOROBENZENE 143. % 70-130 SW846-8260B 6/18/01 08:15 CMB --------- ACENAPHTHENE Not detected ug/kg 2000 SW846-8270C. 6/26/01 10:41 .LAC. ACENAPHTHYLENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC ANTHRACENE Not detected ug/kg 2000 SW 846-8270C 6/26/01 10:41 LAC 'BENZO(A)ANTHRACENE Not detected . ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC BENZO(B)FLUORANTHENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC BENZO(K)FLUORANTHENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC BENZO(A)PYRENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC BENZO(GHI)PERYLENE Not detected ug/kg . 2000' SW846-8270C 6/26/01 10:41 LAC BIS(2-CHLOROETHOXY)METHANE Not detected ug/kg 2000 SW846-8270C 6/26/0110:41 LAC BIS(2-CHLOROETHYL)ETHER Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC BIS(2-CHLOROISOPROPYL)ETHER Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC BIS(2-ETHYLHEXYL)PHTHALATE Not detected ug/kg 2000 SW846-8270C · 6/26/01 10:41 LAC 4-BROMOPHENYL PHENYL ETHER Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC BUTYL BENZYL PHTHALATE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 4-CHLOR0-3-METHYLPHENOL Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 2-CHLORONAPHTHALENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 2-CHLOROPHENOL Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 4-CHLOROPHENYL PHENYL ETHER Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC CHRYSENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC DIBENZO(A.H)ANTHRACENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC DIBENZOFURAN Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC DI-N-BUTYLPHTHALA TE Not detected ug/kg 2000 SW846·8270C 6/26/01 10:41 LAC 1 ,2-DICHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 1,3-DICHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 1,4-DICHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 2,4-DICHLOROPHENOL Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC NC Certification No. 402 -SC Certification No. 99012 -NC Drinkinq Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .... P.O. Box 240543 .... Charlotte, NC 28224-0543 Phone: 704/529-6364 • Toll Free Number: 1-800/529-6364 • Fax: 704/525·0409 • • • Lab Report ~!:!!if>! Full Service Analytical & Environmental Solutions 6/27/01 Page 8 of 13 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: E-2 (1-2) PO Box 669004 Prism Sample ID: AC10191 Charlotte, NC 28266 Loqin Group: MK619H4 Sample Collection Date/Time: 6/11/01 17:30 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT .REFERENCE STARTED ANALYST DIETHYL PHTHALATE Not detected ug/kg 2000 SW846-8270C 6/26/0110:41 LAC 2,4-DIMETHYLPHENOL Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC DIMETHYL PHTHALATE Not detected ug/kg · 2000 SW846-8270C 6/26/01 10:41 LAC 2,4-DINITROPHENOL Not detected ug/kg 10000 SW846-8270C 6/26/01 10:41 LAC 2,4-DINITROTOLUENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 2,6-DINITROTOLUENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC DI-N-OCTYLPHTHALA TE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC . FLUORANTHENE Not detected ug/kg 2000 SW846:8270C 6/26/0110:41 LAC FLUORENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC HEXACHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC HEXACHLOROBUTADIENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC HEXACHLOROCYCLOPENTADIENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC HEXACHLOROETHANE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC INDEN0(1 ,2,3-CD)PYRENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC ISOPHORONE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 2-METHYL-4,6-DINITROPHENOL Not detected ug/kg 10000 SW846-8270C 6/26/0110:41. LAC 2-METHYL NAPHTHALENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 2-METHYL-PHENOL Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 4'METHYL-PHENOL Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC NAPHTHALENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC NITROBENZENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 2-NITROPHENOL Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 4-NITROPHENOL Not detected ug/kg 10000 SW846-8270C 6/26/01 10:41 LAC N-NITROSODIPHENYLAMINE Not detected ug/kg 2000. SW846-8270C 6/26/01 10:41 LAC N-NITROSODI-N-PROPYLAMINE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC PENTACHLOROPHENOL Not detected ug/kg 10000 SW846-8270C 6/26/01 10:41 LAC PHENANTHRENE Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC PHENOL Not detected uglkg 2000 SW846-8270C 6/26/01 10:41 LAC PYRENE Not detected ug!kg 2000 SW846-8270C 6/26/01 10:41. LAC 1,2,4-TRICHLOROBENZENE Not detected ug/kg 2000 SW846-8270C 6/26/0110:41 LAC NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..... P.O. Box 240543 ..o. Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: 1-800/529-6364 ..o. Fax: 704/525-0409 • • Lab Report Full Service Analytical & Environmental Solutions 6/27/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Page 9 of 13 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: E-2 (1-2) Prism Sample 10: AC10191 Looin Group: MK619H4 Sample Collection Date/Time: 6/11/01 17:30 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME ·.PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST 2,4,5-TRICHLOROPHENOL Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC 2.4,6-TRICHLOROPHENOL Not detected ug/kg 2000 SW846-8270C 6/26/01 10:41 LAC ---------- Sample Comments: · Note for 8260: Surrogate recovery outside QC control limits due to matrix interference. Analysis note for SW846-S8270: MDLs for this sample were raised by a factor of5 due to (1 :5) dilution made prior to analysis. Sample had black, oily matrix. · Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ...._ P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364 .., Toll Free Number: l-800/529-6364 .., Fax: 704/525-0409 , Lab Report .,, . PRisM· • • • lABORATORIES, INC. Full Service Analytical & Environmental Solutions 6/27/01 Page10of13 Mid-Atlantic Associates Customer Project ID: Cherokee-Mooresville Site Cliff Lundgren Customer Sample ID: E-6(0-2) PO Box 669004 Prism Sample ID: AC10192 Charlotte, NC 28266 Loqin Group: MK619H4 Sample Collection Date/Time: 6/11/01 18:00 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEITIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST. C5-C8 Aliphatics Not detected mg/kg 7 MADEP VPH 6/19/01 04:37 KC C9-C 12 Aliphatics Not detected mg/kg 6 MADEPVPH 6/19/01 04:37 KC C9-C10 Aromatics Not detected mg/kg 2 MADEP VPH 6/19/01 04:37 KC Surrogate % Recovery-PID 90 % (70-130) MADEP VPH 6/19/01 04:37 KC Surrogate% Recovery-FlO 96 ·% (70-130) MADEPVPH 6/19/01 04:37 KC Dilution Factor mg/kg MADEP VPH 6/19/01 04:37 Kc· Dry Weight Received 15.42 g mg/kg MADEP VPH 6/19/01 04:37 KC ---------- CALCULATIONS BASED ON DRY WT. 85 %DRYWT. 0.01 SM 2540 G 6/12/01 16:25 JLW METALS DIGESTION METHOD 3050 Completed SW846-3050 6/13/01 15:30 LC2 LEAD, TOTAL 200 mg/kg 2.0 SW846-601 OB 6/18/01 14:01 MSP BENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB BROMOBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB BROMOCHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB BROMODICHLOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB BROMOFORM Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB BROMOMETHANE Not detected ug/kg 12.0 SW846-8260B 6/19/01 02:59 CMB N-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB SEC-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB TERT-BUTYLBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB CARBON TETRACHLORIDE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB CHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB CHLORODIBROMOMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB CHLOROETHANE Not detected ug/kg 12.0 SW846-82608 6/19/01 02:59 CMB CHLOROFORM Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB CHLOROMETHANE Not detected ug/kg 12.0 SW846-8260B 6/19/01 02:59 CMB 2-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 4-CHLOROTOLUENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1 ,2-DIBROM0-3-CHLOROPROPANE Not detected ug/kg 12.0 SW846-82608 6/19/01 02:59 CMB 1,2-DIBROMOETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 ..-.. Charlotte, NC 28224-0543 Phone: 704/529-6364 .... Toll Free Number: l-800/529-6364 .... ·Fax: 704/525-0409 Lab Report .PRisM ~ ··.·.· • • • at;~~ . ~BORA TORIES, INC. Full Service Analytical & Environmental Solutions 6/27/01 Page 11 of 13 Mid-Atlantic Associates Customer Project 10: Cherokee-Mooresville Site Cliff Lundgren Customer Sample 10: E-6(0-2) PO Box 669004 Prism Samole 10: AC10192 Charlotte, NC 28266 LoQin Group: MK619H4 Sample Collection Date/Time: 6/11/01 18:00 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT· UNITS LIMIT REFERENCE STARTED ANALYST DIBROMOMETHANE Not detected ug/kg 6.0 SWB46-B2608 6/19/01 02:59 CMB 1 ,2-DICHLOROBENZENE Nat detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1 ,3-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB. 1 ,4-DICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02;59 CMB DICHLORODIFLUOROMETHANE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB 1, 1-DICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1 ,2-DICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1, 1-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB CIS-1 ,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB TRANS-1,2-DICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,2-DICHLOROPROPANE Not detected ug/kg 6.0 . SW846-82608 6/19/0102:59 CMB 1,3-DICHLOROPROPANE Not detected ug/kg 6.0 SWB46-82608 6/19/01 02:59 CMB 2,2-DICHLOROPROPANE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1, 1-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB ETHYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB HEXACHLOROBUTADIENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB ISOPROPYLBENZENE. Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB P-ISOPROPYLTOLUENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB METHYLENE CHLORIDE Not detected ug/kg 120.0 SW846-82608 6/19/01 02:59 CMB NAPHTHALENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB N-PROPYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB STYRENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,1, 1 ,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,1 ,2,2-TETRACHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB TETRACHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB TOLUENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,2,3-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,2,4-TRICHLOROBENZENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,1, 1-TRICHLOROETHANE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,1 ,2-TRICHLOROETHANE Not detected ug/kg 6.0 SWB46-8260B 6/19/01 02:59 CMB NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543 Phone: 704/529-6364..., Toll Free Number: 1-800/529-6364..., Fax: 704/525-0409 Lab Report • • • 6/27/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 Full Service Analytical & Environmental Solutions Page 12 of 13 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: E-6(0-2) Prism Samole 10: AC10192 Loqin Group: . MK619H4 Sample Collection Date/Time: 6/11/01 18:00 Lab Submittal Date/Time: 6/12/01 14:30 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATErrlME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST TRICHLOROETHENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB TRICHLOROFLUOROMETHANE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,2,3-TRICHLOROPROPANE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,2,4-TRIMETHYLBENZENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 1,3,5-TRI METHYLBENZENE · Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB VINYL CHLORIDE Not detected ug/kg 12.0 SW846-8260B 6/19/01 02:59 CMB TOTAL XYLENES Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 2-BUTANONE (MEK) Not detected ug/kg 60.0 SW846-82608 . 6/19/01 02:59 CMB 2-CHLOROETHYL VINYL ETHER Not detected ug/kg 12.0 SW846-82608 6/19/01 02:59 CMB 4-METHYL-2-PENTANONE (MIBK) Not detected ug/kg 60.0 SW846-8260B 6/19/01 02:59 CMB ACETONE Not detected ug/kg 120.0 SW846~82608 6/19/01 02:59 CMB CARBON DISULFIDE Not detected ug/kg 120.0 SW846-82608 6/19/01 02:59 CMB VINYL ACETATE Not detected ug/kg 60.0 SW846-82608 6/19/01 02:59 CMB CIS-1 ,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-8260B 6/19/01 02:59 CMB TRANS-1,3-DICHLOROPROPENE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB 2-HEXANONE Not detected ug/kg 60.0 SW846-82608 6/19/01 02:59 CMB IPE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB MTBE Not detected ug/kg 6.0 SW846-82608 6/19/01 02:59 CMB SURR:DIBROMOFLUOROMETHANE 119 % 70-130 SWB46-8260B 6/19/01 02:59 CMB SURR:TOLUENE-DB 141 • % 70-130 SW846-82608 6/19/01 02:59 CMB SURR:BROMOFLUOROBENZENE 129 % 70-130 SW846-82608 6/19/01 02:59 CMB -------------- Sample Comments: Note for 8260: Surrogate recovery outside QC control limits. Sample was re-analyzed with no improvement in surrogate recovery . Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road ..., P.O. Box 240543 ..., Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Toll Free Number: 1'800/529-6364 ..., Fax: 704/525-0409 • • • Lab Report 6/27/01 Mid-Atlantic Associates Cliff Lundgren PO Box 669004 Charlotte, NC 28266 k ··• -~ . .·;>·.,. ~· PRISM ~·'<':C~ LABORATORIES,INC: FuJI Service Analytical & Environmental Solutions Page 13 of 13 Customer Project 10: Cherokee-Mooresville Site Customer Sample 10: TRIP BLANK Prism Samole 10: AC10193 Looin Grouo: MK619H4 Sample Collection Date/Time: 6/11/01 13:00 Lab Submittal Date/Time: 6/12/01 14:30 . The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST C5-C8 Aliphatics Not detected mg/L 7 MADEP VPH 6/19/01 01:40 KC C9-C 12 Aliphalics Not detected mg/L 6 MADEP VPH 6/19/01 01:40 KC C9·C 1 0 Aromatics Not detected mg/L 2 MADEP.VPH 6/19/01 01:40 KC Surrogate % Recovery-PID 84 % (70-130) . MADEP VPH 6/19/01 01:40 KC Surrogate% Recovery-FlO 83 % (70-130) MADEP VPH 6/19/01 01:40 KC Dilution Factor mg/L MADEP VPH 6/19/01 01:40 KC ---------- ···-·--·-·---···~-·---··-·---· Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 -SC Certification No. 99012 -NC Drinkin~ Water Cert. No. 37735 -FL Certification No. E87519 449 Springbrook Road .., P.O. Box 240543 .., Charlotte, NC 28224-0543 Phone: 704/529·6364.., Toll Free Number: l-800/529-6364.., Fax: 704/525-0409 Full Service Analytical & Environmental Solutions Client t12,".,/ -t4i/.r"t//c ,4ss~L. Physical Address .J./ .;./_;}I) -~~~ ti il.tJ, ?'.~ {..~."('.: k" ~;.i · <-le 1{)/i Chu r/rolh. . J.}(~ .;; d'.;! OJ-' C!lo~IN, 2F C~,DY RECORD· 449 Springbrook Road ..... Charlotte, NC 2821 7 P.O. Box 240543 ..... Charlotte, NC 28224-0543 Phone: 704/529-6364 ..... Fax: 704/525-0409 PRESS DOWN FIRMLY - 3 COPIES Address -c-----:,-------,.-------- Requested Due Date /, -· • --:~ ~-· .1 / (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) ), . LAB USE ONLY ._ ·satnpreS iNTACT. upon cirrival? ·. -· 1 .I "'·" · A~~iVJci ON:We{lce?-re~p:_l_· · · ~ .... -·~-.·--_;; ":~l' --~·-,·. -.-; -~-rAf>PE~-~.!AE~EfiYATIY~~ i~!cB:ted? Received WITHIN'HOLDING TIMES? ·, -cUSrOo~:SiiA·Ls-INTACT? · .. c~ ·· ""':--<. 't ,f VOLATILES rec'd W/OUT HEADSPACE? 'PAbPeA CorflAINeAs-used? ~~ -. . -' YES/ NO 'N(A ___u!_: _,_ •. _ . _._ . d' ·"'-.' ,, ~::-: ~ : ~-~~~-~ .-2 State Certification Requested / NC ~ SC __ Other __ NA __ Water Chlorinated Yes __ No __ NA __ Sample Iced Upon Collection Yes __ No __ CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER 1YPE SEE BELOW NO. SIZE PRESERVA- TIVES SUB LAB CERT. IDNO. PRISM LAB IONO. f!--7 ti-:Z) li--·ii·DI ·' 7.3<-' -~<.;.;.) / ".:.. (l ,:, /. //J .:J. c-& co -;z.) ./ 300 ' I j ~-, :j Li,~.-L L ·' . I l' ., 11aJ . .._,L I I :z / f ..t:. ' ~rYi I ' I .... l.. ~":l .. .I 1---------t----+-------1----j------·---:-1-·--c-----1-----~.--· ----1--l--c-----'--+----------1--+-------1 1---~---1------1----1---1'------1------1--------------1--:------------------'--1------+--1------1 """::> Sampled By (Print Name) -cc~! s_OLC'.Li"-''-'· J_.L,._·,~"~"":::.~-·..:.i.=l.,_(.,_io.cl"::_··._;,..o(~----Affiliation _..<:L!CL<='----------------• " .. : f Re~nquished By: (~t:v~ -f/1~~&/ Received By: (Signature) /J.i!.:lt -, Date Military/Hours /./' ' X. ,, ( I / //:. . ··-· U"b/ZCJ ''h)' ' .... - Additional Comments Relinquished By: {SignallJre) ' Received By: (Signature) ~ I ' Date ' ) ' Relinquished By: (Signature) A""f_Y .. Receiv~ For Prisrift.aboratOries By: Date ?/i ,.£·} 'r ,_.:·_·>.~~.-:··· -' ·: i::· l-/Yu,.4~ --~--·:>1 (:.(I _I }L! ---~:.D• -~ ~ _ __,..,_....._ . ' Method of Shipment / . ------· log·'n Group No . I"· ,:~ II '! . ' ' I ~-, I' {I 1~ '1 if, ~~! ~ 1~.-, " . NPDES NC UST: NC v·· GROUNDWATER: NC DRINKING WATER: NC SOLID WASTE: NC / OTHER: NC sc sc ---sc __ _ OTHER __ sc __ _ OTHER. __ sc sc =--OTHER__ OTHER __ OTHER____ OTHER __ _ •coNTAINER TYPE CODES: A= Amber C = Clear G =Glass P = Plastic; TL =Teflon-Lined Cap VOA = Volatile Organi~s Analysis (Zero Head Space) SEE REVERSE FOR TERMS & CONDITIONS FINAL REPORT COPY • • • Full Service Analytical.& Environmental Solutions ..-~.:..;·.·~ '·j~N{; ··'':" . Main Office: 449 Springbrook Road .. P.O. Box 240543 Charlotte, NC 28224-0543 Phone: 704/529-6364 1/800/529-6364 Fax: 704/525-0409 Company Name:_L.,/JZ'-L/-<e/!'L..:.--t.H.I...L/2!1!.1a!Llfl'{.-f.u;<;o..-~&"':.s~s:!::~.::c:..=' ~~/i_:e..;;,s~------'-'· Date: 6 -:U-N · To: _ __,Ct=..t· _!,. rl....!.~-~L::::!.-t!Ltniii:~;l-Lc__r.t.c.J.n~--------Lab Group ID: /114(/, ltli1 The State ofNo.rth Carolina requires the enclosed VPH and EPH form~ be submitted with · our laboratory report. Before submitting these forms to the state, please insert the project name · and/or site location. · · Thank you. edlr-&#~ ~#"Laboratories, Inc. . . Cc: Lab File T:wordlvphformlsiteloca.dcic • • • VPH (Aiiphatics/Aromatics) Laboratory Reporting Form Continued Client Name Mid-Atlantic Associates Laboratory Name PRISM LABORATORIES, INC. Project Name Cherokee-Mooresville Site Site Location INCLUDE APPROPRIATE UNITS Sample Identification AC10190 Sample Matrix Soil Collection Option (for soil)* 1 Date Collected 6/11/01 Date Received 6/12/01 Date Extracted 6/18/01 Date Analyzed 6/19/01 Dry Weight 14.23 g Dilution Factor 1 C5 -CS Aliphatics•• <7 mg/kg C9 -C12 Aliphatics•• <6 mg/kg C9-C10 Aromatics•• <2 mg/kg Surrogate % Recovery -PID 90% Surrogate % Recovery -FID 86% NC Certification# (Lab) ...:4c::0.::2 ___________ _ '~ AC10191 AC10192 AC10193 Soil Soil Trip Blank 1 1 NA 6/11/01 6/11/01 . 6/11101 6/12/01 6/12/01 6/12/01 6/18/01 6/18/01" 6/18/01 6/19/01 6/19/01 6/19/01 17.25 g 15.42 g NA 1 1 1 <7 mg/kg <7 mg/kg <7 mg/L 100 mg/kg <6 mg/kg <6 mg/L 9.4 mg/kg <2 mg/kg <2 mg/L 81% 90% 84% 87% 96% 83% *Option 1 = Established fill line on v1al Option 2 = Sampling Dev1ce (1nd1cate brand, e.g. EnCore) Opt1on 3 = F1eld we1ght of so1l ** Unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, ancllor concentrations of other ranges that elute within the specified range. AC10190 AC10191 AC10192 AC10193 Percent -Fortified Blank Relative Percent Difference-PID N/A N/A . 3.0% Percent -Fortified Blank 96% 92% N/A Difference-FID 4.0% 6.0% N/A Page 1 Revision 5/6/98 • • • Page 2 Mid-Atlantic Associates Proj: Cherokee-Mooresville Site Attachment 2 VPH Laboratory Reporting Form Initial Calibration Date 6/4/01 Calibration Ranges and Limits ~~~LE"~ CS -C8 Aliphatics 2.0 mg/kg 5.2 mg/kg 7.0 mg/kg C9 • C12 Aliphatics 1.3 mg/kg 4.1 mg/kg 6.0 mg/kg C9 -C10 Aromatics 0.4 mg/kg 1.3 mg/kg 2.0 mg/kg NOTE: Please 1nclude un1ts as appropnate Method of Quantitation (circle one): Curve ~rage Response Factor:::> Calibration Concentration Levels C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics NOTE: Please indicate units as appropriate. Calibration Check Date Calibration Check 6/18/01 14% 12% 19% ~Ef:~~~ CS -C8 Aliphatics C9-C12 Aliphatics C9 -C10 Aromatics MDL = Method Detection Limit ML = Mimimum Limit RL = Reportable Limit 375 ug/L 275 ug/L 50 ug/L AC10190 AC10191 AC10192 AC10193 6.0% 6.0% 15% RPD = Relative Percent Difference %RSD = Percent Relative Standard Deviation CCC = Correlation Coefficient .of Curve Revision 5/6/98 • Full Service Analytical & Environmental Solutions Main Office: 449 Springbrook Road P.O. Box 240543 Charlotte, NC 28224-0543 Phone: 704/529-6364 . 1/800/529-6364 Fax: 704/525-0409 • • Date: {; },.q ':f} 0 ( . r . , To:_-=t_.·~-+:-fA--· 4/-~..l,;._A-'--vul!;-· --11-~L=!{__,/=------Lab Group ID:!Yl( (pI q lft The State of North Carolina requires the enclosed VPH and EPH forms be submitted with our laboratory report. Before submitting these forms to the state, please insert the project name and/or site location. . Thank you. t GAte -fuJ!W/JiJj_) Prism Laboratories, Inc. Cc: Lab File T:word/vphfonn/sireloca.doc · • EPH (Aiiphatics/Aromatics~aboratory Reporting Form • Client Name Mid-Atlantic Asscoiates Project Name Cherokee-Mooresville Site Site Location Matrix Date Collected Date Received Date Extracted Dilution Factor C9-C18 C11-C22 Aromatics* %Recovery %Recove Fractionation Su Fractionation Su Laboratory Name Prism Laboratories, Inc. NC Certification# (Lab) ___ ....:.4:::02=------------ Soil 6/11/01 6/12/01 **6/21/01 6/22/01 8.3 1 81 130 23 67% 61% 72% 82% • Unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, and/or concentrations of other ranges that elute within the specified range. •• Sample for EPH was extracted outside of hold time at client's request. AC10191 Percent Recovery-Fortified Blank (Spike) 56% 60% 89% Relative Percent Difference -Sample Duplicates 9.0% 6.0% 16% Page 1 Revision 5/6/98 • • • Page 2 -Mid-Atlantic Asscoiates Proj: Cherokee-Mooresville Site EPH Laboratory Reporting Form Initial Calibration Date 6/4/01 (All) 5/23/01 (ARO) Calibration Ranges and Limits ~~~~ C9 -C18 Aliphatics 10 mg/kg 32 mg/kg 40 mg/kg C19-C36 Aliphatics 5.7 mg/kg 18 mg/kg 20 mg/kg C11 -C22 Aromatics 16 mg/kg 20 mg/kg 20 mg/kg NOTE: Please Include un1ts as appropnate Method of Quantitation (circle one): Curve Average Response Factor Calibration Concentration Levels C9-C18 Aliphatics 5.0% C19 -C36 Aliphatics C11-C22 Aromatics Calibration Check Date Calibration Check MDL = Method Detection Limit ML = Minimum Limit RL = Reportable Limit AC10191 6/22/01 .7.0% 4.0% RPD = Relative Percent Difference %RSD = Percent Relative Standard Deviation CCC = Correlation Coefficient of Curve Revision 5/6/98 • • APPENDIX G SURFACE WATER MODELING RESULTS • MP?;t\fl~~NTl<; En[?ineering & Enrironmenral Solutions • • • DATAFILE NAME: A:CHLOROFORM North Caroline Department of Environment and Natural Resources Risk Assessment, Category G-3, Method II G-3 Groundwater Contaminant Transport model INPUT PARAMETERS: CONTAMINANT CHEMICAL NAME SURFACE WATER CHEMICAL STANDARD (mg/1) DISTANCE FROM P.L.E. TO SURFACE-WATER BODY (Feet) (P.L.E. = PLUME LEADING EDGE) AQUIFER HYDRAULIC CONDUCTIVITY AQUIFER GROUNDWATER GRADIENT AQUIFER EFFECTIVE POROSITY AQUIFER DISPERSION COEFFICIENT CHEMICAL RETARDATION FACTOR CHEMICAL BIODEGRADATION DECAY RATE LENGTH OF CONTAMINANT PLUME THICKNESS OF SURFICIAL AQUIFER WIDTH OF CONTAMINANT PLUME 7Ql0 OF RIVER OR STREAM UP-STREAM CHEMICAL CONCENTRATION MODELING RESULTS: (Feet/Day) (Feet/ Feet I (unitless) (Feet'2/Day) (unitless) (1/Day) (Feet) (Feet). (Feet) (Feet'3/Second) (rng/1) chloroform 0.47 250 .064 .04 .2 10 1 0 200 25 400 0.1 0 Maximum Groundwater Contaminant Concentration at Surface Water Boundary occurs at Time = 0.4492E+02 years . with Groundwater Concentration C/Csource = 0.2993E+OO where Csource Maximum Source· Concentration Maximum Groundwater source Concentration·= 0.5316E+03 ·mg/l for the chemical chloroform • • • DATAFILE NAME: A:DCE North Caroline Department of Environment and Natural Resources Risk Assessment, Category G-3, Method II G-3 Groundwater Contaminant Transport model INPUT PARAMETERS: CONTAMINANT CHEMICAL NAME SURFACE WATER CHEMICAL STANDARD (mg/1) DISTANCE FROM P.L.E. TO SURFACE WATER BODY (Feet) (P.L.E. = PLUME LEADING EDGE) AQUIFER HYDRAULIC CONDUCTIVITY AQUIFER GROUNDWATER GRADIENT AQUIFER EFFECTIVE POROSITY AQUIFER DISPERSION COEFFICIENT CHEMICAL RETARDATION FACTOR CHEMICAL BIODEGRADATION DECAY RATE LENGTH OF CONTAMINANT PLUME THICKNESS OF SURFICIAL AQUIFER WIDTH OF CONTAMINANT PLUME 7Ql0 OF RIVER OR STREAM UP-STREAM CHEMICAL CONCENTRATION MODELING RESULTS: (Feet/Day) (Feet/ Feet I (unitlessl (FeetA2/Day) (unitlessl (1/Day) (Feet) (Feet) (Feet) (FeetA3/Second) (mg/1) DCE 0.00885 sao . 064 .04 .2 10 1.5 0 200 25 200 0 .1 0 Maximum Groundwater Contaminant Concentration at Surface Water Boundary occurs at Time = 0.8449E+02 years with Groundwater Concentration C/Csource = 0.1991E+00 where Csource Maximum Squrce Concentration Maximum Groundwater source Concentration= 0.3004E+02 for the chemical DCE mg/l • • • DATAFILE NAME: A:PCE North Caroline Department of Environment and Natural Resources Risk Assessment, Category G-3, Method II G-3 Groundwater Contaminant Transport model INPUT PARAMETERS: CONTAMINANT CHEMICAL NAME SURFACE WATER CHEMICAL STANDARD (mg/1) DISTANCE FROM ·P.L.E. TO SURFACE WATER BODY (Feet) (P.L.E. = PLUME LEADING EDGE) AQUIFER HYDRAULIC CONDUCTIVITY AQUIFER GROUNDWATER GRADIENT AQUIFER EFFECTIVE POROSITY AQUIFER DISPERSION COEFFICIENT CHEMICAL RETARDATION FACTOR CHEMICAL BIODEGRADATION DECAY RATE LENGTH OF CONTAMINANT PLUME THICKNESS OF SURFICIAL AQUIFER WIDTH OF CONTAMINANT PLUME 7Q10 OF RIVER OR STREAM UP-STREAM CHEMICAL CONCENTRATION MODELING RESULTS: (Feet/Day) (Feet/Feet) (unitless) (Feet'2/Day) (unitless) (1/Day) (Feet) (Feet) (Feet) (Feet'3/Second) (mg/11 PCE 0.018 250 . 064 .04 .2 10 1.5 0 200 25 400 0.1 0 Maximum Groundwater Contaminant Concentration at Surface Water Boundary occurs at Time= 0.6738E+02 years with Groundwater Concentration C/Csource = 0.2993E+00 where Csource = Maximum Source Concentration Maximum Groundwater Source Concentration = 0.2036E+02 mg/1 for the chemical PCE