20035_Gastonia Investment_Additional Assessment Report_20180629

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S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-047 Danaher Isley Rd\Soil Sampling 6-19-2018\Additional Soil Assessment Report.docx
Additional Assessment Report Former Apex Tool Facility
Gastonia, North Carolina H&H Job No. FDP-047
Table of Contents

1.0 Introduction ............................................................................................................................ 1
2.0 Assessment Activities ............................................................................................................. 4
2.1 Sampling Procedures and Analysis ...................................................................................... 4
2.2 Sample Analytical Results ................................................................................................... 5
3.0 Summary ................................................................................................................................. 6

List of Tables

Table 1 Summary of Soil Analytical Data
Table 2 Summary of Groundwater Analytical Data

List of Figures
Figure 1 Site Location
Figure 2 Sample Location Map

List of Appendices
Appendix A Laboratory Analytical Data

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S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-047 Danaher Isley Rd\Soil Sampling 6-19-2018\Additional Soil Assessment Report.docx
Additional Assessment Report Former Apex Tool Facility
Gastonia, North Carolina H&H Job No. (FDP-047) 1.0 Introduction

Hart & Hickman, PC (H&H) has prepared this Additional Assessment Report to document
additional sampling conducted at the former Apex Tools (Apex) facility located at 1228 Isley Dr.
in Gastonia, Gaston County, North Carolina (site). A site location map is included as Figure 1.

The subject site is an irregular shaped parcel that is approximately 21.2 acres and is improved with
an approximately 179,000 main building that is vacant and formerly contained office,
manufacturing, and warehouse areas. The main building is primarily one story, however a
basement is located below the far southeastern portion of the building that was used for wastewater
collection and treatment. In addition, second story areas are present in the western portion of the
building (office area) and the eastern portion of the building (mezzanine area). There are also two
smaller one-story buildings (approximately 1,200 sq ft each) in the southeast portion of the site
that were used for paint and other flammable storage and for a boiler. A canopy covered storage
area is also located in the southeast portion of the site. A site plan is provided as Figure 2.

H&H completed a Phase I ESA at the site in December 2015 and conducted follow up inspections
which indicated the following areas of environmental concern at the site:

• Central Yarn and Dye operated at the site from 1965 to 1978 and performed yarn winding,
texturizing, bleaching, and dyeing.

• The site was operated from the late 1970s to 2013 for manufacture of hand tools and
sockets. Operations conducted in association with these activities included, but were not
limited to, stamping metal, degreasing, plating (chromium using hexavalent chromium,
nickel, and tin-cobalt), plating wastewater treatment, painting, and heat treating.
Hazardous wastes generated at the facility during operations included, but were not limited
to, ignitable (D001), corrosive (D002), cadmium (D006), chromium (D007), wastewater
treatment plant sludges from electroplating (F006), spent non-halogenated solvents (F003
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and F005), lead (D008), spent cyanide plating bath solutions (F007), plating bath residues
(F008), spent stripping and cleaning bath solutions from electroplating operations using
cyanide (F009), oil quenching bath residues from metal heat treating in which cyanide was
used (F010), and tetrachloroethene-containing parts washing solvent (D039). The Apex
facility received multiple hazardous waste compliance violations with the North Carolina
Department of Environmental Quality (DEQ) including a Compliance Order with
Administrative Penalty in 2010.

• Metal forming was conducted in the southwestern portion of the building, plating and heat
treating were conducted in the eastern portion of the building, and wastewater collection
and treatment were conducted in the basement area below the eastern portion of the
building. H&H observed residual green colored solids in and near the plating area and the
wastewater treatment area indicative of plating waste. Former above ground storage tank
(ASTs) were located south, east, and north of the building, and a methanol UST was located
northeast of the building.

• H&H observed significant oil staining and pooling throughout the large and small forming
areas in the southwestern portion of the building and, to a lesser extent, in the plating area.
It appears that oil that has accumulated on the ceiling and rafters of these areas is mobilized
by condensation and drips down onto the floor and pools. Significant deterioration of the
epoxy on the floor in the large forming area was also observed.
In August 2016, H&H collected soil and groundwater samples from the site. H&H collected five
soil samples (HH-SB-1 through HH-SB-5) and three groundwater samples (HH-TMW-1 through
HH-TMW-3). The locations of the samples are indicated in Figure 2, and the results of analysis
of the samples are included in Tables 1 and 2.
The results of the soil sample analyses indicated sample HH-SB-2 (0.5-1 ft) from the forming area
contained the chlorinated solvent tetrachloroethylene (PCE) at a concentration of 0.13 mg/kg
which is above the DEQ Protection of Groundwater Preliminary Soil Remediation Goal (PSRG)
of 0.005 mg/kg. In addition, sample HH-SB-4 (0.5-1 ft) collected from degraded concrete in the
basement below the former plating area where wastewater treatment was performed contained
nickel at a concentration of 19,000 mg/kg which is above the Protection of Groundwater,
Residential, and Industrial PSRGs of 130 mg/kg, 300 mg/kg, and 4,400 mg/kg, respectively.
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The results of analysis of the groundwater samples indicated that the chlorinated solvent vinyl
chloride was detected in downgradient sample HH-TMW-3 at 3.7 µg/L which is above the NCAC
2L Groundwater Standard (2L Standard) of 0.03 µg/L. Vinyl chloride is a degradation product of
PCE which was detected in soil at the site as noted above and was also present in parts washing
solvent used by Apex. Concentrations of the chlorinated solvents 1,1-dichloroethane (4.3 µg/L)
and 1,1-dichloroethylene (20 µg/L) were also detected in HH-TMW-3, but the concentrations
detected were below their respective 2L Standards. No other VOC concentrations were detected
in the groundwater samples above laboratory reporting limits. The laboratory analytical results
also indicated that metals were also detected above 2L Standards in the groundwater samples.
Cobalt was detected in all three samples at concentrations ranging from 9.6 µg/L to 38 µg/L, which
are above the DEQ Interim Maximum Allowable Concentration (IMAC) of 1 µg/L. Other metals
detected above 2L Standards or IMACs were chromium and thallium in HH-TMW-2 and
manganese in all three wells. The elevated metals concentrations may have been the result of
turbidity in some samples and/or background conditions.

In June 2018, H&H collected additional soil samples for laboratory analysis from potential areas
of concern at the site. The methods and results of the assessment activities are presented in Section
2.0.

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2.0 Assessment Activities
2.1 Sampling Procedures and Analysis
On June 19, 2018, H&H advanced nine (9) additional borings at the site. The locations of the
borings, labeled HHSB-A through HHSB-I, are indicated in Figure 2. The borings were advanced
in the following locations:

• HHSB-A was advanced in the area of drain in a former exterior drum storage along the
southern portion of the building. The drain appears to be flow to an oil/water separator
south of the drain.
• HHSB-B was advanced in the area of a drain in the former flammable materials/paint
storage building.
• HHSB-C was advanced in a stormwater collection area and outfall in the eastern portion
of the site where historical documents indicate a former nickel spill was also located.
• HHSB-D, HHSB-E, and HHSB-F were advanced in the former metal forming areas in the
southwestern portions of the building where heavy oil staining is present.
• HHSB-G was advanced in the area of one of two drains in the southern portion of the
building.
• HHSB-H and HHSB-I were advanced in the basement area below the former plating area
where wastewater collection and treatment were performed.

H&H advanced the borings at each location using a stainless steel hand auger to depths ranging
from 1 to 3 ft below ground surface (bgs). At each location except HHSB-C in the stormwater
collection area, a concrete core was used to penetrate the concrete and then H&H advanced the
concrete core thorough the cored hole. For the boring locations in the building, ground surface
was considered the point below the bottom of the concrete slab at that location. During boring
advancement, the samples were screened in the field for the presence of odors, staining, and/or
elevated organic vapor utilizing a photoionization detector (PID). All of the samples for laboratory
analysis were collected at 0-1 ft bgs, except the sample from HHSB-D which was collected from
1-2 ft bgs. The depths of the samples submitted for laboratory analysis are indicated in Table 1.

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The samples were submitted for laboratory analyses of the following parameters:
• Samples HHSB-A, HHSB-D, HHSB-E, and HHSB-F were analyzed for volatile organic
compounds (VOCs) by EPA Method 8260 and polynuclear aromatic hydrocarbons (PAHs)
by EPA Method 8270.
• Sample HHSB-B was analyzed for VOCs by EPA Method 8260, and for arsenic, cobalt,
lead, nickel, chromium, and hexavalent chromium by EPA Methods 6020/7196.
• Samples HHSB-C, HHSB-G, HHSB-H, and HHSB-I were analyzed for cobalt, nickel,
chromium, and hexavalent chromium by EPA Methods 6020/7196.

Following completion, the borings located in concrete were backfilled with cuttings and then
grouted to the surface with concrete.

2.2 Sample Analytical Results
The laboratory analytical results of the samples are summarized in Table 1 along with the previous
soil analytical data from August 2016. For ease of reference, the analytical data for the samples
collected in June 2018 are highlighted in blue. The laboratory analytical data are provided in
Appendix A. The results of analysis of the samples were compared to the DEQ Protection of
Groundwater, Residential, and Industrial PSRGs dated February 2018. In addition, metals
concentrations were compared to concentrations in the background sample collected from the site.

The results of analysis of the samples indicate the following:

• Soil sample HHSB-C from the stormwater collection area indicated that nickel (240 mg/kg)
was detected at a concentration above the Protection of Groundwater PSRG of 130 mg/kg.

• Sample HHSB-I collected from below the plating and wastewater treatment basement area
contained nickel at a concentration of 350 mg/kg, which exceeds the Protection of
Groundwater and Residential PSRGs of 130 mg/kg and 310 mg/kg, respectively.

• No other samples contained analyzed compounds above background (for metals) and
PSRGs.

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3.0 Summary

In summary, the results of analysis of soil, sediment, and groundwater samples collected from the
site by H&H in August 2016 and June 2018 indicate the following:

• The chlorinated solvent PCE was detected above the Protection of Groundwater PSRG in
a soil sample below the forming area, and the PCE degradation product vinyl chloride was
detected in groundwater downgradient of the site building.

• Elevated concentrations of nickel are present in soil above PSRGs below the area where
plating and wastewater treatment were performed by Apex. One sample contained a
concentration above the Industrial PSRG.

• An elevated concentration of nickel above the Protection of Groundwater PSRG was
detected in the stormwater collection area in the eastern portion of the site where a
historical nickel release was reported.

• Chromium, cobalt, manganese, and thallium were also detected above 2L Standards or
IMACs, although the presence of the metals could be related to turbidity and/or
background conditions.

Table 1 (Page 1 of 1)
Summary of Soil and Sediment Analytical Data
Former Apex Tools/ Danaher Facility
Gastonia, North Carolina
H&H Job No. FDP-047
Sample Area
Wastewater
Treatment Outside Drain Small Building
Drain
Stormwater
Collection
Southern
Portion of
Building
Background
Sample ID HH-SB-1 HH-SB-2 HHSB-D HHSB-E HHSB-F HH-SB-3 HH-SB-4 HH-SB-5 HHSB-H HHSB-I HHSB-A HHSB-B HHSB-C HHSB-G HH-BG-1
Depth (ft bgs)0.5-1 0.5-1 1-2 0-1 0-1 0.5-1 0.5-1 0.5-1 0-1 0-1 0-1 0-1 0-1 0-1 14-15
Sample Date 8/29/2016 8/29/2016 6/19/2018 6/19/2018 6/19/2018 8/29/2016 8/29/2016 8/29/2016 6/19/2018 6/19/2018 6/19/2018 6/19/2018 6/19/2018 6/19/2018 8/29/2016 Protection of
Ground Water Residential Industrial
Units (mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)
VOCs (8260B)
Tetrachloroethylene <0.0023 0.13 <0.0023 <0.0021 <0.0025 <0.0037 <0.0031 <0.0028 NA NA <0.0027 <0.0025 NA <0.0022 NA 0.0063 17 82
Toluene <0.0023 <0.0075 <0.00092 0.0019 J 0.0017 J <0.0037 <0.0031 <0.0028 NA NA <0.0011 <0.0010 NA <0.00086 NA 8.3 990 9700
m,p-Xylene <0.0092 <0.15 <0.0020 0.0021 J <0.0021 <0.015 <0.012 <0.011 NA NA <0.0023 <0.0022 NA <0.0018 NA 9.8 120 500
o-Xylene <0.0046 <0.075 <0.00081 0.00075 J <0.00088 <0.0074 <0.0061 <0.0055 NA NA <0.00093 <0.00089 NA <0.00075 NA 9.8 140 590
SVOCs/PAHs (8270C)BRL BRL BRL*BRL*BRL*BRL BRL BRL NA NA BRL*NA NA NA BRL ------
HSL Metals (6020/7471/71961)
Antimony <2.9 <2.9 NA NA NA <3.4 <3.3 <3.8 NA NA NA NA NA NA <3.4 0.90 6.2 94
Arsenic 4.1 1.7 NA NA NA 1.8 3.3 3.9 NA NA NA 1.4 NA NA 3.1 5.8 0.68 3.0
Beryllium <0.37 <3.7 NA NA NA 0.71 0.6 0.48 NA NA NA NA NA NA 1.5 63 31 470
Cadmium <0.52 <0.52 NA NA NA <0.59 <0.58 <0.67 NA NA NA NA NA NA <0.61 3.0 14.0 200
Cobalt <2.5 15 NA NA NA 3.9 10 3.5 4.9 3.9 NA 11 11 3.3 33 0.9 4.7 70
Copper 13 16 NA NA NA <7.8 29 13 NA NA NA NA NA NA 34 700 630 9,300
Lead 7.6 20 NA NA NA 24 23 19 NA NA NA 16 NA NA 17 270 400 800
Manganese 47 410 NA NA NA 170 320 150 NA NA NA NA NA NA 560 65 380 5,600
Mercury <0.026 <0.027 NA NA NA <0.030 0.042 0.06 NA NA NA NA NA NA <0.030 1.0 2.3 9.7
Nickel <6.8 B 16 B NA NA NA 39 B 19,000 B 37 B 8.1 350 NA 14 240 4.4 J 44 B 130 310 4,700
Selenimum <1.1 <1.1 NA NA NA <1.3 <1.3 <1.5 NA NA NA NA NA NA <1.3 2.1 78 1,200
Silver <0.12 0.18 NA NA NA <0.14 <0.13 <0.15 NA NA NA NA NA NA <0.14 3.4 78 1,200
Thallium 0.088 0.61 NA NA NA 0.5 0.25 0.37 NA NA NA NA NA NA 0.74 0.28 0.16 2.3
Tin <5.3 <5.3 NA NA NA <5.9 <6.3 <6.5 NA NA NA NA NA NA <5.9 10,000 9,400 140,000
Zinc <14 88 NA NA NA 49 67 30 NA NA NA NA NA NA 130 1,200 4,700 70,000
Total Chromium 12 28 NA NA NA 23 91 37 21 27 NA 36 96 16 62
Hexavalent Chromium <0.16 <0.83 NA NA NA <0.19 <0.40 <0.40 <0.11 <0.24 NA <0.27 <0.25 <0.26 NA 3.8 0.31 6.5
Trivalent Chromium 12 28 NA NA NA 23 91 37 21 27 NA 36 96 16 62 360,000 23,000 350,000
Cyanide (9014)
Cyanide NA NA NA NA NA <0.58 <0.59 <0.60 NA NA NA NA NA NA NA 14 1 2.4
Notes:
1) Mercury analyzed by EPA Method 7471 and hexavalent chromium analyzed by EPA Method 7196. Al other metals analyzed by EPA Method 6020.
Only those VOCs detected in at least one sample shown above
Bold indicates concentration exceeds the Protection of Groundwater PSRG and site-specific background levels in the case of metals
Highlighted indicates concentration exceeds the Industrial PSRG and site-specific background levels in the case of metals
Method number follows parameter in parenthesis
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; * = samples analyzed for PAH SVOCs only
NA = not analyzed; -- = Not applicable; BRL = Constituent not detected at or above laboratory reporting limit
mg/kg = milligrams per kilogram
B = Analyte is found in the associated blank as well as in the sample.
J = Detected but below the reporting limit; therefore, result is an estimated concentration.
Blue highlighting denotes samples collected in June 2018.
Underlined indicates concentration exceeds the Residential PSRG and site-specific background levels in the case of metals
Forming Areas Basement/Plating Area
NC DEQ Preliminary Soil Remedial Goals
(PSRGs)
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Table 1 (Page 1 of 1)
Hart & Hickman, PC
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
GASTONIA NORTH, NORTH CAROLINA, 2002
TITLE
PROJECT
SITE LOCATION MAP
FORMER APEX TOOL FACILITY1228 ISLEY DRIVEGASTONIA, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
6-24-11 0
1FDP-001
HHTW-1
HHTW-2
HHTW-3
HHBG-1
HHSB-1
HHSB-2
HHSB-3
HHSB-4
HHSB-5
HHSB-A
HHSB-C
HHSB-G
HHSB-H
HHSB-I
HHSB-D
HHSB-E
HHSB-F
HHSB-B
REVISION NO. 0DATE: 6-28-18
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
JOB NO. FDP-047 FIGURE NO. 2
FORMER APEX TOOL FACILITY
1228 ISLEY DRIVE
GASTONIA, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
FORMER ABOVEGROUND
STORAGE TANK AREA
TEMPORARY MONITORING WELL
LOCATION
SOIL BORING LOCATION
STREAM
INTERMITTENT STREAM /
DRAINAGE FEATURE
PACKAGING
WAREHOUSE
BELT DRIVE
S
M
A
L
L
F
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M
I
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HEAT TREAT
LA
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F
O
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M
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VIBRATORY
TOOL FACTORY
TI
D
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F
L
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(1
9
1
9

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S
T
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P
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)
TALLENT DRUM CO.
(1709 INDUSTRIAL PIKE)
MULTI-TENANT WAREHOSE
(FORMER CRS FACILITY)
(1224 ISLEY DRIVE)
RWM CASTERS
(1225 ISLEY DRIVE)ISLEY DRIVEWOODED
PARKING
PLATINGLAB
OFFICES
(TWO STORIES)
WOODED
BASEMENT BELOW
WASTEWATER TREATMENT
VACANT,
WOODED
LAND
IN
D
U
S
T
R
I
A
L

P
I
K
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D
R
I
V
E
BESSEMER CITY ROADFORMER METHANOL UST
FORMER DYEHOUSE
SUBSTATIONS
STORMWATER
COLLECTION
DRUM STORAGE
OIL / WATER
SEPARATOR PAINT STORGE
S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-047 Danaher Isley Rd\Figures\Sample Location Map.dwg, FIG 2, 6/28/2018 3:51:29 PM, erichardson

Appendix A
Laboratory Analytical Data

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
June 26, 2018
Steve Hart
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
Project Location: Gastonia, NC
Client Job Number:
Project Number: FDP-047
Laboratory Work Order Number: 18F0987
Enclosed are results of analyses for samples received by the laboratory on June 19, 2018. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 51
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
18F0987-01 5
18F0987-02 9
18F0987-03 13
18F0987-04 15
18F0987-05 19
18F0987-06 23
18F0987-07 27
18F0987-08 31
18F0987-09 33
Sample Preparation Information 35
QC Data 36
Volatile Organic Compounds by GC/MS 36
B206280 36
Semivolatile Organic Compounds by GC/MS 41
B206337 41
Metals Analyses (Total) 43
B206425 43
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 44
B206519 44
Flag/Qualifier Summary 45
Certifications 46
Chain of Custody/Sample Receipt 49
Page 2 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
6/26/2018
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
ATTN: Steve Hart
FDP-047
18F0987
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Gastonia, NC
HHSB-A (0-1)18F0987-01 Soil SM 2540G
SW-846 8260B
SW-846 8270D
HHSB-B (0-1)18F0987-02 Soil SM 2540G
SW-846 6020A-B
SW-846 7196A
SW-846 8260B
HHSB-C (0-1)18F0987-03 Soil SM 2540G
SW-846 6020A-B
SW-846 7196A
HHSB-D (1-2)18F0987-04 Soil SM 2540G
SW-846 8260B
SW-846 8270D
HHSB-E (0-1)18F0987-05 Soil SM 2540G
SW-846 8260B
SW-846 8270D
HHSB-F (0-1)18F0987-06 Soil SM 2540G
SW-846 8260B
SW-846 8270D
HHSB-G (0-1)18F0987-07 Soil SM 2540G
SW-846 6020A-B
SW-846 7196A
SW-846 8260B
HHSB-H (0-1)18F0987-08 Soil SM 2540G
SW-846 6020A-B
SW-846 7196A
HHSB-I (0-1)18F0987-09 Soil SM 2540G
SW-846 6020A-B
SW-846 7196A
[TOC_1]Sample Summary[TOC]
Page 3 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6020, all 5X soil dilutions were performed as per standard operating procedure. 20X dilutions were performed due to exeedance of LDR.
For method 8270, only PAHs were requested and reported.
[TOC_1]Case Narrative[TOC]
SW-846 7196A
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Hexavalent Chromium
18F0987-02[HHSB-B (0-1)], 18F0987-03[HHSB-C (0-1)], 18F0987-07[HHSB-G (0-1)], 18F0987-08[HHSB-H (0-1)], 18F0987-09[HHSB-I (0-1)], B206519-BS1
SW-846 8260B
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Acetone
B206280-BS1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Chloroethane
18F0987-01[HHSB-A (0-1)], 18F0987-02[HHSB-B (0-1)], 18F0987-04[HHSB-D (1-2)], 18F0987-05[HHSB-E (0-1)], 18F0987-06[HHSB-F (0-1)], 18F0987-07[HHSB-G
(0-1)], B206280-BLK1, B206280-BS1, B206280-BSD1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
Bromomethane
B206280-BS1, B206280-BSD1, S024536-CCV1
Dichlorodifluoromethane (Freon 12)
B206280-BS1, B206280-BSD1, S024536-CCV1
SW-846 6010C/D SW-846 6020A/B
For NC, Metals methods SW-846 6010D and SW-846 6020B are followed, and for all other states methods SW-846 6010C and SW-846 6020A are followed.
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 4 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-01
Field Sample #: HHSB-A (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 11:40
[TOC_2]18F0987-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 6/21/18 10:34 MFFmg/Kg dry0.031 6/21/18SW-846 8260B1Acetone
ND 0.0080 6/21/18 10:34 MFFmg/Kg dry0.0033 6/21/18SW-846 8260B1Acrylonitrile
ND 0.0013 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1Benzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Bromobenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0019 6/21/18SW-846 8260B1Bromochloromethane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00080 6/21/18SW-846 8260B1Bromodichloromethane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0019 6/21/18SW-846 8260B1Bromoform
ND 0.013 6/21/18 10:34 MFFmg/Kg dry0.0056 6/21/18SW-846 8260B1Bromomethane
ND 0.053 6/21/18 10:34 MFFmg/Kg dry0.023 6/21/18SW-846 8260B12-Butanone (MEK)
ND 0.053 6/21/18 10:34 MFFmg/Kg dry0.028 6/21/18SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1n-Butylbenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1sec-Butylbenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1tert-Butylbenzene
ND 0.0013 6/21/18 10:34 MFFmg/Kg dry0.00080 6/21/18SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0080 6/21/18 10:34 MFFmg/Kg dry0.0057 6/21/18SW-846 8260B1Carbon Disulfide
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Carbon Tetrachloride
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1Chlorobenzene
ND 0.0013 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1Chlorodibromomethane
ND 0.027 6/21/18 10:34 MFFmg/Kg dry0.0020 6/21/18SW-846 8260B1R-05Chloroethane
ND 0.0053 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1Chloroform
ND 0.013 6/21/18 10:34 MFFmg/Kg dry0.0085 6/21/18SW-846 8260B1Chloromethane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B12-Chlorotoluene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B14-Chlorotoluene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 6/21/18 10:34 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00080 6/21/18SW-846 8260B1Dibromomethane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B11,2-Dichlorobenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B11,3-Dichlorobenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,4-Dichlorobenzene
ND 0.0053 6/21/18 10:34 MFFmg/Kg dry0.0028 6/21/18SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.027 6/21/18 10:34 MFFmg/Kg dry0.0017 6/21/18SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B11,1-Dichloroethane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0017 6/21/18SW-846 8260B11,2-Dichloroethane
ND 0.0053 6/21/18 10:34 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B11,1-Dichloroethylene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0017 6/21/18SW-846 8260B11,2-Dichloropropane
ND 0.0013 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B11,3-Dichloropropane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B12,2-Dichloropropane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,1-Dichloropropene
ND 0.0013 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0013 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1trans-1,3-Dichloropropene
ND 0.027 6/21/18 10:34 MFFmg/Kg dry0.0024 6/21/18SW-846 8260B1Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 5 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-01
Field Sample #: HHSB-A (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 11:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 6/21/18 10:34 MFFmg/Kg dry0.00080 6/21/18SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.13 6/21/18 10:34 MFFmg/Kg dry0.077 6/21/18SW-846 8260B11,4-Dioxane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Ethylbenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1Hexachlorobutadiene
ND 0.027 6/21/18 10:34 MFFmg/Kg dry0.014 6/21/18SW-846 8260B12-Hexanone (MBK)
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0053 6/21/18 10:34 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.027 6/21/18 10:34 MFFmg/Kg dry0.0094 6/21/18SW-846 8260B1Methylene Chloride
ND 0.027 6/21/18 10:34 MFFmg/Kg dry0.010 6/21/18SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0053 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1Naphthalene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1n-Propylbenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00080 6/21/18SW-846 8260B1Styrene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0024 6/21/18SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0013 6/21/18 10:34 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0017 6/21/18SW-846 8260B1Tetrachloroethylene
ND 0.013 6/21/18 10:34 MFFmg/Kg dry0.0029 6/21/18SW-846 8260B1Tetrahydrofuran
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Toluene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00080 6/21/18SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,1,1-Trichloroethane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0016 6/21/18SW-846 8260B11,1,2-Trichloroethane
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1Trichloroethylene
ND 0.013 6/21/18 10:34 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B11,2,3-Trichloropropane
ND 0.013 6/21/18 10:34 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00080 6/21/18SW-846 8260B11,3,5-Trimethylbenzene
ND 0.013 6/21/18 10:34 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B1Vinyl Chloride
ND 0.0053 6/21/18 10:34 MFFmg/Kg dry0.0023 6/21/18SW-846 8260B1m+p Xylene
ND 0.0027 6/21/18 10:34 MFFmg/Kg dry0.00093 6/21/18SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 96.3 6/21/18 10:3470-130
Toluene-d8 101 6/21/18 10:3470-130
4-Bromofluorobenzene 103 6/21/18 10:3470-130
Page 6 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-01
Field Sample #: HHSB-A (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 11:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.061 6/21/18SW-846 8270D1Acenaphthene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.068 6/21/18SW-846 8270D1Acenaphthylene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.059 6/21/18SW-846 8270D1Anthracene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.054 6/21/18SW-846 8270D1Benzo(a)anthracene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.064 6/21/18SW-846 8270D1Benzo(a)pyrene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.058 6/21/18SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.090 6/21/18SW-846 8270D1Benzo(g,h,i)perylene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.064 6/21/18SW-846 8270D1Benzo(k)fluoranthene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.064 6/21/18SW-846 8270D1Chrysene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.12 6/21/18SW-846 8270D1Dibenz(a,h)anthracene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.067 6/21/18SW-846 8270D1Fluoranthene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.066 6/21/18SW-846 8270D1Fluorene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.15 6/21/18SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.071 6/21/18SW-846 8270D12-Methylnaphthalene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.10 6/21/18SW-846 8270D1Naphthalene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.11 6/21/18SW-846 8270D1Phenanthrene
ND 0.20 6/22/18 18:11 CDTmg/Kg dry0.067 6/21/18SW-846 8270D1Pyrene
Surrogates % Recovery Recovery Limits Flag/Qual
Nitrobenzene-d5 67.2 6/22/18 18:1130-130
2-Fluorobiphenyl 62.3 6/22/18 18:1130-130
p-Terphenyl-d14 74.6 6/22/18 18:1130-130
Page 7 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-01
Field Sample #: HHSB-A (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 11:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
83.1 6/21/18 8:29 BLM% Wt 6/20/18SM 2540G1% Solids
Page 8 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-02
Field Sample #: HHSB-B (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 13:55
[TOC_2]18F0987-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 6/21/18 11:02 MFFmg/Kg dry0.030 6/21/18SW-846 8260B1Acetone
ND 0.0076 6/21/18 11:02 MFFmg/Kg dry0.0032 6/21/18SW-846 8260B1Acrylonitrile
ND 0.0013 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1Benzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1Bromobenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0018 6/21/18SW-846 8260B1Bromochloromethane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00076 6/21/18SW-846 8260B1Bromodichloromethane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0018 6/21/18SW-846 8260B1Bromoform
ND 0.013 6/21/18 11:02 MFFmg/Kg dry0.0053 6/21/18SW-846 8260B1Bromomethane
ND 0.051 6/21/18 11:02 MFFmg/Kg dry0.022 6/21/18SW-846 8260B12-Butanone (MEK)
ND 0.051 6/21/18 11:02 MFFmg/Kg dry0.027 6/21/18SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1n-Butylbenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1sec-Butylbenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1tert-Butylbenzene
ND 0.0013 6/21/18 11:02 MFFmg/Kg dry0.00076 6/21/18SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0076 6/21/18 11:02 MFFmg/Kg dry0.0055 6/21/18SW-846 8260B1Carbon Disulfide
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1Carbon Tetrachloride
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1Chlorobenzene
ND 0.0013 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1Chlorodibromomethane
ND 0.025 6/21/18 11:02 MFFmg/Kg dry0.0019 6/21/18SW-846 8260B1R-05Chloroethane
ND 0.0051 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1Chloroform
ND 0.013 6/21/18 11:02 MFFmg/Kg dry0.0081 6/21/18SW-846 8260B1Chloromethane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B12-Chlorotoluene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B14-Chlorotoluene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 6/21/18 11:02 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00076 6/21/18SW-846 8260B1Dibromomethane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B11,2-Dichlorobenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B11,3-Dichlorobenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B11,4-Dichlorobenzene
ND 0.0051 6/21/18 11:02 MFFmg/Kg dry0.0027 6/21/18SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.025 6/21/18 11:02 MFFmg/Kg dry0.0017 6/21/18SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B11,1-Dichloroethane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0017 6/21/18SW-846 8260B11,2-Dichloroethane
ND 0.0051 6/21/18 11:02 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,1-Dichloroethylene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0017 6/21/18SW-846 8260B11,2-Dichloropropane
ND 0.0013 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B11,3-Dichloropropane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B12,2-Dichloropropane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,1-Dichloropropene
ND 0.0013 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0013 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1trans-1,3-Dichloropropene
ND 0.025 6/21/18 11:02 MFFmg/Kg dry0.0023 6/21/18SW-846 8260B1Diethyl Ether
Page 9 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-02
Field Sample #: HHSB-B (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 6/21/18 11:02 MFFmg/Kg dry0.00076 6/21/18SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.13 6/21/18 11:02 MFFmg/Kg dry0.073 6/21/18SW-846 8260B11,4-Dioxane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1Ethylbenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1Hexachlorobutadiene
ND 0.025 6/21/18 11:02 MFFmg/Kg dry0.014 6/21/18SW-846 8260B12-Hexanone (MBK)
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0051 6/21/18 11:02 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.025 6/21/18 11:02 MFFmg/Kg dry0.0090 6/21/18SW-846 8260B1Methylene Chloride
ND 0.025 6/21/18 11:02 MFFmg/Kg dry0.0097 6/21/18SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0051 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1Naphthalene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1n-Propylbenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00076 6/21/18SW-846 8260B1Styrene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0023 6/21/18SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0013 6/21/18 11:02 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0017 6/21/18SW-846 8260B1Tetrachloroethylene
ND 0.013 6/21/18 11:02 MFFmg/Kg dry0.0028 6/21/18SW-846 8260B1Tetrahydrofuran
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1Toluene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00076 6/21/18SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,1,1-Trichloroethane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B11,1,2-Trichloroethane
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1Trichloroethylene
ND 0.013 6/21/18 11:02 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,2,3-Trichloropropane
ND 0.013 6/21/18 11:02 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00076 6/21/18SW-846 8260B11,3,5-Trimethylbenzene
ND 0.013 6/21/18 11:02 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B1Vinyl Chloride
ND 0.0051 6/21/18 11:02 MFFmg/Kg dry0.0022 6/21/18SW-846 8260B1m+p Xylene
ND 0.0025 6/21/18 11:02 MFFmg/Kg dry0.00089 6/21/18SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 97.0 6/21/18 11:0270-130
Toluene-d8 102 6/21/18 11:0270-130
4-Bromofluorobenzene 104 6/21/18 11:0270-130
Page 10 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-02
Field Sample #: HHSB-B (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.4 0.22 6/24/18 15:19 MJHmg/Kg dry0.036 6/22/18SW-846 6020A-B5Arsenic
36 5.5 6/24/18 15:19 MJHmg/Kg dry0.20 6/22/18SW-846 6020A-B5Chromium
11 2.0 6/24/18 15:19 MJHmg/Kg dry0.11 6/22/18SW-846 6020A-B5Cobalt
16 2.2 6/24/18 15:19 MJHmg/Kg dry0.072 6/22/18SW-846 6020A-B5Lead
14 5.5 6/24/18 15:19 MJHmg/Kg dry0.20 6/22/18SW-846 6020A-B5Nickel
ND 0.42 6/24/18 15:19 MJHmg/Kg dry0.014 6/22/18SW-846 6020A-B5Cadmium
Page 11 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-02
Field Sample #: HHSB-B (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 1.1 6/26/18 8:30 LLmg/Kg dry0.27 6/25/18SW-846 7196A5L-07Hexavalent Chromium
74.0 6/21/18 8:29 BLM% Wt 6/20/18SM 2540G1% Solids
Page 12 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-03
Field Sample #: HHSB-C (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 14:40
[TOC_2]18F0987-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
96 5.6 6/24/18 15:22 MJHmg/Kg dry0.20 6/22/18SW-846 6020A-B5Chromium
11 2.1 6/24/18 15:22 MJHmg/Kg dry0.11 6/22/18SW-846 6020A-B5Cobalt
240 22 6/25/18 8:49 MJHmg/Kg dry0.83 6/22/18SW-846 6020A-B20Nickel
Page 13 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-03
Field Sample #: HHSB-C (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 14:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 1.0 6/26/18 8:30 LLmg/Kg dry0.25 6/25/18SW-846 7196A5L-07Hexavalent Chromium
78.4 6/21/18 8:29 BLM% Wt 6/20/18SM 2540G1% Solids
Page 14 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-04
Field Sample #: HHSB-D (1-2)
Sample Matrix: Soil
Sampled: 6/19/2018 17:00
[TOC_2]18F0987-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.12 6/21/18 11:29 MFFmg/Kg dry0.027 6/21/18SW-846 8260B1Acetone
ND 0.0069 6/21/18 11:29 MFFmg/Kg dry0.0029 6/21/18SW-846 8260B1Acrylonitrile
ND 0.0012 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1Benzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B1Bromobenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0016 6/21/18SW-846 8260B1Bromochloromethane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00069 6/21/18SW-846 8260B1Bromodichloromethane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0016 6/21/18SW-846 8260B1Bromoform
ND 0.012 6/21/18 11:29 MFFmg/Kg dry0.0048 6/21/18SW-846 8260B1Bromomethane
ND 0.046 6/21/18 11:29 MFFmg/Kg dry0.020 6/21/18SW-846 8260B12-Butanone (MEK)
ND 0.046 6/21/18 11:29 MFFmg/Kg dry0.024 6/21/18SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1n-Butylbenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1sec-Butylbenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1tert-Butylbenzene
ND 0.0012 6/21/18 11:29 MFFmg/Kg dry0.00069 6/21/18SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0069 6/21/18 11:29 MFFmg/Kg dry0.0050 6/21/18SW-846 8260B1Carbon Disulfide
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B1Carbon Tetrachloride
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1Chlorobenzene
ND 0.0012 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1Chlorodibromomethane
ND 0.023 6/21/18 11:29 MFFmg/Kg dry0.0017 6/21/18SW-846 8260B1R-05Chloroethane
ND 0.0046 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1Chloroform
ND 0.012 6/21/18 11:29 MFFmg/Kg dry0.0074 6/21/18SW-846 8260B1Chloromethane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B12-Chlorotoluene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B14-Chlorotoluene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0012 6/21/18 11:29 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00069 6/21/18SW-846 8260B1Dibromomethane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B11,2-Dichlorobenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B11,3-Dichlorobenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B11,4-Dichlorobenzene
ND 0.0046 6/21/18 11:29 MFFmg/Kg dry0.0024 6/21/18SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.023 6/21/18 11:29 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B11,1-Dichloroethane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B11,2-Dichloroethane
ND 0.0046 6/21/18 11:29 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,1-Dichloroethylene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B11,2-Dichloropropane
ND 0.0012 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B11,3-Dichloropropane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B12,2-Dichloropropane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B11,1-Dichloropropene
ND 0.0012 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0012 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1trans-1,3-Dichloropropene
ND 0.023 6/21/18 11:29 MFFmg/Kg dry0.0021 6/21/18SW-846 8260B1Diethyl Ether
Page 15 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-04
Field Sample #: HHSB-D (1-2)
Sample Matrix: Soil
Sampled: 6/19/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0012 6/21/18 11:29 MFFmg/Kg dry0.00069 6/21/18SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.12 6/21/18 11:29 MFFmg/Kg dry0.066 6/21/18SW-846 8260B11,4-Dioxane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B1Ethylbenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1Hexachlorobutadiene
ND 0.023 6/21/18 11:29 MFFmg/Kg dry0.013 6/21/18SW-846 8260B12-Hexanone (MBK)
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0046 6/21/18 11:29 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.023 6/21/18 11:29 MFFmg/Kg dry0.0082 6/21/18SW-846 8260B1Methylene Chloride
ND 0.023 6/21/18 11:29 MFFmg/Kg dry0.0088 6/21/18SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0046 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1Naphthalene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1n-Propylbenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00069 6/21/18SW-846 8260B1Styrene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0021 6/21/18SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0012 6/21/18 11:29 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B1Tetrachloroethylene
ND 0.012 6/21/18 11:29 MFFmg/Kg dry0.0025 6/21/18SW-846 8260B1Tetrahydrofuran
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B1Toluene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00069 6/21/18SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,1,1-Trichloroethane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,1,2-Trichloroethane
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1Trichloroethylene
ND 0.012 6/21/18 11:29 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,2,3-Trichloropropane
ND 0.012 6/21/18 11:29 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00092 6/21/18SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00069 6/21/18SW-846 8260B11,3,5-Trimethylbenzene
ND 0.012 6/21/18 11:29 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1Vinyl Chloride
ND 0.0046 6/21/18 11:29 MFFmg/Kg dry0.0020 6/21/18SW-846 8260B1m+p Xylene
ND 0.0023 6/21/18 11:29 MFFmg/Kg dry0.00081 6/21/18SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 96.2 6/21/18 11:2970-130
Toluene-d8 101 6/21/18 11:2970-130
4-Bromofluorobenzene 100 6/21/18 11:2970-130
Page 16 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-04
Field Sample #: HHSB-D (1-2)
Sample Matrix: Soil
Sampled: 6/19/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.060 6/21/18SW-846 8270D1Acenaphthene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.067 6/21/18SW-846 8270D1Acenaphthylene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.058 6/21/18SW-846 8270D1Anthracene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.053 6/21/18SW-846 8270D1Benzo(a)anthracene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.062 6/21/18SW-846 8270D1Benzo(a)pyrene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.056 6/21/18SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.088 6/21/18SW-846 8270D1Benzo(g,h,i)perylene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.062 6/21/18SW-846 8270D1Benzo(k)fluoranthene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.062 6/21/18SW-846 8270D1Chrysene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.12 6/21/18SW-846 8270D1Dibenz(a,h)anthracene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.066 6/21/18SW-846 8270D1Fluoranthene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.065 6/21/18SW-846 8270D1Fluorene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.14 6/21/18SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.069 6/21/18SW-846 8270D12-Methylnaphthalene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.10 6/21/18SW-846 8270D1Naphthalene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.10 6/21/18SW-846 8270D1Phenanthrene
ND 0.20 6/22/18 18:38 CDTmg/Kg dry0.066 6/21/18SW-846 8270D1Pyrene
Surrogates % Recovery Recovery Limits Flag/Qual
Nitrobenzene-d5 66.2 6/22/18 18:3830-130
2-Fluorobiphenyl 63.8 6/22/18 18:3830-130
p-Terphenyl-d14 80.4 6/22/18 18:3830-130
Page 17 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-04
Field Sample #: HHSB-D (1-2)
Sample Matrix: Soil
Sampled: 6/19/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
84.7 6/21/18 8:29 BLM% Wt 6/20/18SM 2540G1% Solids
Page 18 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-05
Field Sample #: HHSB-E (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 16:15
[TOC_2]18F0987-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.11 6/21/18 11:56 MFFmg/Kg dry0.025 6/21/18SW-846 8260B1Acetone
ND 0.0064 6/21/18 11:56 MFFmg/Kg dry0.0027 6/21/18SW-846 8260B1Acrylonitrile
ND 0.0011 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Benzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B1Bromobenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B1Bromochloromethane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00064 6/21/18SW-846 8260B1Bromodichloromethane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B1Bromoform
ND 0.011 6/21/18 11:56 MFFmg/Kg dry0.0045 6/21/18SW-846 8260B1Bromomethane
ND 0.043 6/21/18 11:56 MFFmg/Kg dry0.019 6/21/18SW-846 8260B12-Butanone (MEK)
ND 0.043 6/21/18 11:56 MFFmg/Kg dry0.022 6/21/18SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1n-Butylbenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1sec-Butylbenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00096 6/21/18SW-846 8260B1tert-Butylbenzene
ND 0.0011 6/21/18 11:56 MFFmg/Kg dry0.00064 6/21/18SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0064 6/21/18 11:56 MFFmg/Kg dry0.0046 6/21/18SW-846 8260B1Carbon Disulfide
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B1Carbon Tetrachloride
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Chlorobenzene
ND 0.0011 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Chlorodibromomethane
ND 0.021 6/21/18 11:56 MFFmg/Kg dry0.0016 6/21/18SW-846 8260B1R-05Chloroethane
ND 0.0043 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Chloroform
ND 0.011 6/21/18 11:56 MFFmg/Kg dry0.0068 6/21/18SW-846 8260B1Chloromethane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B12-Chlorotoluene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B14-Chlorotoluene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0011 6/21/18 11:56 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00064 6/21/18SW-846 8260B1Dibromomethane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,2-Dichlorobenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,3-Dichlorobenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B11,4-Dichlorobenzene
ND 0.0043 6/21/18 11:56 MFFmg/Kg dry0.0022 6/21/18SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.021 6/21/18 11:56 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,1-Dichloroethane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,2-Dichloroethane
ND 0.0043 6/21/18 11:56 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,1-Dichloroethylene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00096 6/21/18SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,2-Dichloropropane
ND 0.0011 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,3-Dichloropropane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00096 6/21/18SW-846 8260B12,2-Dichloropropane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00096 6/21/18SW-846 8260B11,1-Dichloropropene
ND 0.0011 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0011 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1trans-1,3-Dichloropropene
ND 0.021 6/21/18 11:56 MFFmg/Kg dry0.0019 6/21/18SW-846 8260B1Diethyl Ether
Page 19 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-05
Field Sample #: HHSB-E (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 16:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0011 6/21/18 11:56 MFFmg/Kg dry0.00064 6/21/18SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.11 6/21/18 11:56 MFFmg/Kg dry0.061 6/21/18SW-846 8260B11,4-Dioxane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B1Ethylbenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Hexachlorobutadiene
ND 0.021 6/21/18 11:56 MFFmg/Kg dry0.012 6/21/18SW-846 8260B12-Hexanone (MBK)
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0043 6/21/18 11:56 MFFmg/Kg dry0.00096 6/21/18SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.021 6/21/18 11:56 MFFmg/Kg dry0.0076 6/21/18SW-846 8260B1Methylene Chloride
ND 0.021 6/21/18 11:56 MFFmg/Kg dry0.0081 6/21/18SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0043 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Naphthalene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1n-Propylbenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00064 6/21/18SW-846 8260B1Styrene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0019 6/21/18SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0011 6/21/18 11:56 MFFmg/Kg dry0.00096 6/21/18SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B1Tetrachloroethylene
ND 0.011 6/21/18 11:56 MFFmg/Kg dry0.0023 6/21/18SW-846 8260B1Tetrahydrofuran
0.0019 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B1JToluene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00064 6/21/18SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,1,1-Trichloroethane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,1,2-Trichloroethane
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Trichloroethylene
ND 0.011 6/21/18 11:56 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,2,3-Trichloropropane
ND 0.011 6/21/18 11:56 MFFmg/Kg dry0.00096 6/21/18SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00085 6/21/18SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00064 6/21/18SW-846 8260B11,3,5-Trimethylbenzene
ND 0.011 6/21/18 11:56 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1Vinyl Chloride
0.0021 0.0043 6/21/18 11:56 MFFmg/Kg dry0.0018 6/21/18SW-846 8260B1Jm+p Xylene
0.00075 0.0021 6/21/18 11:56 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Jo-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.0 6/21/18 11:5670-130
Toluene-d8 103 6/21/18 11:5670-130
4-Bromofluorobenzene 102 6/21/18 11:5670-130
Page 20 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-05
Field Sample #: HHSB-E (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 16:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.067 6/21/18SW-846 8270D1Acenaphthene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.075 6/21/18SW-846 8270D1Acenaphthylene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.064 6/21/18SW-846 8270D1Anthracene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.059 6/21/18SW-846 8270D1Benzo(a)anthracene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.069 6/21/18SW-846 8270D1Benzo(a)pyrene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.063 6/21/18SW-846 8270D1Benzo(b)fluoranthene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.098 6/21/18SW-846 8270D1Benzo(g,h,i)perylene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.069 6/21/18SW-846 8270D1Benzo(k)fluoranthene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.069 6/21/18SW-846 8270D1Chrysene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.14 6/21/18SW-846 8270D1Dibenz(a,h)anthracene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.073 6/21/18SW-846 8270D1Fluoranthene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.072 6/21/18SW-846 8270D1Fluorene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.16 6/21/18SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.077 6/21/18SW-846 8270D12-Methylnaphthalene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.11 6/21/18SW-846 8270D1Naphthalene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.12 6/21/18SW-846 8270D1Phenanthrene
ND 0.22 6/22/18 19:04 CDTmg/Kg dry0.073 6/21/18SW-846 8270D1Pyrene
Surrogates % Recovery Recovery Limits Flag/Qual
Nitrobenzene-d5 62.3 6/22/18 19:0430-130
2-Fluorobiphenyl 59.7 6/22/18 19:0430-130
p-Terphenyl-d14 73.2 6/22/18 19:0430-130
Page 21 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-05
Field Sample #: HHSB-E (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 16:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
76.4 6/21/18 8:30 BLM% Wt 6/20/18SM 2540G1% Solids
Page 22 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-06
Field Sample #: HHSB-F (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 15:35
[TOC_2]18F0987-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 6/21/18 12:23 MFFmg/Kg dry0.029 6/21/18SW-846 8260B1Acetone
ND 0.0075 6/21/18 12:23 MFFmg/Kg dry0.0031 6/21/18SW-846 8260B1Acrylonitrile
ND 0.0013 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1Benzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1Bromobenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0018 6/21/18SW-846 8260B1Bromochloromethane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Bromodichloromethane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0018 6/21/18SW-846 8260B1Bromoform
ND 0.013 6/21/18 12:23 MFFmg/Kg dry0.0053 6/21/18SW-846 8260B1Bromomethane
ND 0.050 6/21/18 12:23 MFFmg/Kg dry0.022 6/21/18SW-846 8260B12-Butanone (MEK)
ND 0.050 6/21/18 12:23 MFFmg/Kg dry0.026 6/21/18SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1n-Butylbenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1sec-Butylbenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1tert-Butylbenzene
ND 0.0013 6/21/18 12:23 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0075 6/21/18 12:23 MFFmg/Kg dry0.0054 6/21/18SW-846 8260B1Carbon Disulfide
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1Carbon Tetrachloride
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1Chlorobenzene
ND 0.0013 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1Chlorodibromomethane
ND 0.025 6/21/18 12:23 MFFmg/Kg dry0.0019 6/21/18SW-846 8260B1R-05Chloroethane
ND 0.0050 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1Chloroform
ND 0.013 6/21/18 12:23 MFFmg/Kg dry0.0080 6/21/18SW-846 8260B1Chloromethane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B12-Chlorotoluene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B14-Chlorotoluene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 6/21/18 12:23 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Dibromomethane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B11,2-Dichlorobenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B11,3-Dichlorobenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B11,4-Dichlorobenzene
ND 0.0050 6/21/18 12:23 MFFmg/Kg dry0.0026 6/21/18SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.025 6/21/18 12:23 MFFmg/Kg dry0.0016 6/21/18SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B11,1-Dichloroethane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0016 6/21/18SW-846 8260B11,2-Dichloroethane
ND 0.0050 6/21/18 12:23 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,1-Dichloroethylene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0016 6/21/18SW-846 8260B11,2-Dichloropropane
ND 0.0013 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B11,3-Dichloropropane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B12,2-Dichloropropane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,1-Dichloropropene
ND 0.0013 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0013 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1trans-1,3-Dichloropropene
ND 0.025 6/21/18 12:23 MFFmg/Kg dry0.0023 6/21/18SW-846 8260B1Diethyl Ether
Page 23 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-06
Field Sample #: HHSB-F (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 15:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 6/21/18 12:23 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.13 6/21/18 12:23 MFFmg/Kg dry0.072 6/21/18SW-846 8260B11,4-Dioxane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1Ethylbenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1Hexachlorobutadiene
ND 0.025 6/21/18 12:23 MFFmg/Kg dry0.014 6/21/18SW-846 8260B12-Hexanone (MBK)
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0050 6/21/18 12:23 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.025 6/21/18 12:23 MFFmg/Kg dry0.0089 6/21/18SW-846 8260B1Methylene Chloride
ND 0.025 6/21/18 12:23 MFFmg/Kg dry0.0095 6/21/18SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0050 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1Naphthalene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1n-Propylbenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Styrene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0023 6/21/18SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0013 6/21/18 12:23 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0016 6/21/18SW-846 8260B1Tetrachloroethylene
ND 0.013 6/21/18 12:23 MFFmg/Kg dry0.0028 6/21/18SW-846 8260B1Tetrahydrofuran
0.0017 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B1JToluene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,1,1-Trichloroethane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B11,1,2-Trichloroethane
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B1Trichloroethylene
ND 0.013 6/21/18 12:23 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,2,3-Trichloropropane
ND 0.013 6/21/18 12:23 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.0010 6/21/18SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,3,5-Trimethylbenzene
ND 0.013 6/21/18 12:23 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B1Vinyl Chloride
ND 0.0050 6/21/18 12:23 MFFmg/Kg dry0.0021 6/21/18SW-846 8260B1m+p Xylene
ND 0.0025 6/21/18 12:23 MFFmg/Kg dry0.00088 6/21/18SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 96.5 6/21/18 12:2370-130
Toluene-d8 101 6/21/18 12:2370-130
4-Bromofluorobenzene 103 6/21/18 12:2370-130
Page 24 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-06
Field Sample #: HHSB-F (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 15:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.072 6/21/18SW-846 8270D1Acenaphthene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.081 6/21/18SW-846 8270D1Acenaphthylene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.069 6/21/18SW-846 8270D1Anthracene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.064 6/21/18SW-846 8270D1Benzo(a)anthracene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.075 6/21/18SW-846 8270D1Benzo(a)pyrene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.068 6/21/18SW-846 8270D1Benzo(b)fluoranthene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.11 6/21/18SW-846 8270D1Benzo(g,h,i)perylene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.075 6/21/18SW-846 8270D1Benzo(k)fluoranthene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.075 6/21/18SW-846 8270D1Chrysene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.15 6/21/18SW-846 8270D1Dibenz(a,h)anthracene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.079 6/21/18SW-846 8270D1Fluoranthene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.078 6/21/18SW-846 8270D1Fluorene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.17 6/21/18SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.083 6/21/18SW-846 8270D12-Methylnaphthalene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.12 6/21/18SW-846 8270D1Naphthalene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.12 6/21/18SW-846 8270D1Phenanthrene
ND 0.24 6/22/18 19:31 CDTmg/Kg dry0.079 6/21/18SW-846 8270D1Pyrene
Surrogates % Recovery Recovery Limits Flag/Qual
Nitrobenzene-d5 60.9 6/22/18 19:3130-130
2-Fluorobiphenyl 59.4 6/22/18 19:3130-130
p-Terphenyl-d14 71.8 6/22/18 19:3130-130
Page 25 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-06
Field Sample #: HHSB-F (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 15:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
70.7 6/21/18 8:30 BLM% Wt 6/20/18SM 2540G1% Solids
Page 26 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-07
Field Sample #: HHSB-G (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 15:10
[TOC_2]18F0987-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.11 6/21/18 12:51 MFFmg/Kg dry0.025 6/21/18SW-846 8260B1Acetone
ND 0.0065 6/21/18 12:51 MFFmg/Kg dry0.0027 6/21/18SW-846 8260B1Acrylonitrile
ND 0.0011 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Benzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B1Bromobenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B1Bromochloromethane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00065 6/21/18SW-846 8260B1Bromodichloromethane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0015 6/21/18SW-846 8260B1Bromoform
ND 0.011 6/21/18 12:51 MFFmg/Kg dry0.0045 6/21/18SW-846 8260B1Bromomethane
ND 0.043 6/21/18 12:51 MFFmg/Kg dry0.019 6/21/18SW-846 8260B12-Butanone (MEK)
ND 0.043 6/21/18 12:51 MFFmg/Kg dry0.023 6/21/18SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1n-Butylbenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1sec-Butylbenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00097 6/21/18SW-846 8260B1tert-Butylbenzene
ND 0.0011 6/21/18 12:51 MFFmg/Kg dry0.00065 6/21/18SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0065 6/21/18 12:51 MFFmg/Kg dry0.0046 6/21/18SW-846 8260B1Carbon Disulfide
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B1Carbon Tetrachloride
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Chlorobenzene
ND 0.0011 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Chlorodibromomethane
ND 0.022 6/21/18 12:51 MFFmg/Kg dry0.0016 6/21/18SW-846 8260B1R-05Chloroethane
ND 0.0043 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Chloroform
ND 0.011 6/21/18 12:51 MFFmg/Kg dry0.0069 6/21/18SW-846 8260B1Chloromethane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B12-Chlorotoluene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B14-Chlorotoluene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0011 6/21/18 12:51 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00065 6/21/18SW-846 8260B1Dibromomethane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,2-Dichlorobenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,3-Dichlorobenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B11,4-Dichlorobenzene
ND 0.0043 6/21/18 12:51 MFFmg/Kg dry0.0023 6/21/18SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.022 6/21/18 12:51 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,1-Dichloroethane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,2-Dichloroethane
ND 0.0043 6/21/18 12:51 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,1-Dichloroethylene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00097 6/21/18SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B11,2-Dichloropropane
ND 0.0011 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,3-Dichloropropane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00097 6/21/18SW-846 8260B12,2-Dichloropropane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00097 6/21/18SW-846 8260B11,1-Dichloropropene
ND 0.0011 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0011 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1trans-1,3-Dichloropropene
ND 0.022 6/21/18 12:51 MFFmg/Kg dry0.0019 6/21/18SW-846 8260B1Diethyl Ether
Page 27 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-07
Field Sample #: HHSB-G (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 15:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0011 6/21/18 12:51 MFFmg/Kg dry0.00065 6/21/18SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.11 6/21/18 12:51 MFFmg/Kg dry0.062 6/21/18SW-846 8260B11,4-Dioxane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B1Ethylbenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Hexachlorobutadiene
ND 0.022 6/21/18 12:51 MFFmg/Kg dry0.012 6/21/18SW-846 8260B12-Hexanone (MBK)
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0043 6/21/18 12:51 MFFmg/Kg dry0.00097 6/21/18SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.022 6/21/18 12:51 MFFmg/Kg dry0.0076 6/21/18SW-846 8260B1Methylene Chloride
ND 0.022 6/21/18 12:51 MFFmg/Kg dry0.0082 6/21/18SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0043 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1Naphthalene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1n-Propylbenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00065 6/21/18SW-846 8260B1Styrene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0019 6/21/18SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0011 6/21/18 12:51 MFFmg/Kg dry0.00097 6/21/18SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0014 6/21/18SW-846 8260B1Tetrachloroethylene
ND 0.011 6/21/18 12:51 MFFmg/Kg dry0.0024 6/21/18SW-846 8260B1Tetrahydrofuran
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B1Toluene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00065 6/21/18SW-846 8260B11,2,3-Trichlorobenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B11,2,4-Trichlorobenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B11,1,1-Trichloroethane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0013 6/21/18SW-846 8260B11,1,2-Trichloroethane
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0011 6/21/18SW-846 8260B1Trichloroethylene
ND 0.011 6/21/18 12:51 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B11,2,3-Trichloropropane
ND 0.011 6/21/18 12:51 MFFmg/Kg dry0.00097 6/21/18SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00086 6/21/18SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00065 6/21/18SW-846 8260B11,3,5-Trimethylbenzene
ND 0.011 6/21/18 12:51 MFFmg/Kg dry0.0012 6/21/18SW-846 8260B1Vinyl Chloride
ND 0.0043 6/21/18 12:51 MFFmg/Kg dry0.0018 6/21/18SW-846 8260B1m+p Xylene
ND 0.0022 6/21/18 12:51 MFFmg/Kg dry0.00075 6/21/18SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.4 6/21/18 12:5170-130
Toluene-d8 101 6/21/18 12:5170-130
4-Bromofluorobenzene 102 6/21/18 12:5170-130
Page 28 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-07
Field Sample #: HHSB-G (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 15:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
16 5.6 6/24/18 15:26 MJHmg/Kg dry0.20 6/22/18SW-846 6020A-B5Chromium
3.3 2.1 6/24/18 15:26 MJHmg/Kg dry0.11 6/22/18SW-846 6020A-B5Cobalt
4.4 5.6 6/24/18 15:26 MJHmg/Kg dry0.21 6/22/18SW-846 6020A-B5JNickel
Page 29 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-07
Field Sample #: HHSB-G (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 15:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 1.0 6/26/18 8:30 LLmg/Kg dry0.26 6/25/18SW-846 7196A5L-07Hexavalent Chromium
75.6 6/21/18 8:30 BLM% Wt 6/20/18SM 2540G1% Solids
Page 30 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-08
Field Sample #: HHSB-H (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 12:30
[TOC_2]18F0987-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
21 6.0 6/24/18 15:29 MJHmg/Kg dry0.21 6/22/18SW-846 6020A-B5Chromium
4.9 2.2 6/24/18 15:29 MJHmg/Kg dry0.11 6/22/18SW-846 6020A-B5Cobalt
8.1 6.0 6/24/18 15:29 MJHmg/Kg dry0.22 6/22/18SW-846 6020A-B5Nickel
Page 31 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-08
Field Sample #: HHSB-H (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 0.43 6/26/18 8:30 LLmg/Kg dry0.11 6/25/18SW-846 7196A2L-07Hexavalent Chromium
71.8 6/21/18 8:30 BLM% Wt 6/20/18SM 2540G1% Solids
Page 32 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-09
Field Sample #: HHSB-I (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 12:50
[TOC_2]18F0987-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
27 5.4 6/24/18 15:33 MJHmg/Kg dry0.19 6/22/18SW-846 6020A-B5Chromium
3.9 2.0 6/24/18 15:33 MJHmg/Kg dry0.10 6/22/18SW-846 6020A-B5Cobalt
350 22 6/25/18 8:52 MJHmg/Kg dry0.80 6/22/18SW-846 6020A-B20Nickel
Page 33 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/19/2018
Work Order: 18F0987Sample Description:Project Location: Gastonia, NC
Sample ID: 18F0987-09
Field Sample #: HHSB-I (0-1)
Sample Matrix: Soil
Sampled: 6/19/2018 12:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
ND 0.98 6/26/18 8:30 LLmg/Kg dry0.24 6/25/18SW-846 7196A5L-07Hexavalent Chromium
79.1 6/21/18 8:30 BLM% Wt 6/20/18SM 2540G1% Solids
Page 34 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B206214 06/20/1818F0987-01 [HHSB-A (0-1)]
B206214 06/20/1818F0987-02 [HHSB-B (0-1)]
B206214 06/20/1818F0987-03 [HHSB-C (0-1)]
B206214 06/20/1818F0987-04 [HHSB-D (1-2)]
B206214 06/20/1818F0987-05 [HHSB-E (0-1)]
B206214 06/20/1818F0987-06 [HHSB-F (0-1)]
B206214 06/20/1818F0987-07 [HHSB-G (0-1)]
B206214 06/20/1818F0987-08 [HHSB-H (0-1)]
B206214 06/20/1818F0987-09 [HHSB-I (0-1)]
Prep Method: SW-846 3050B-SW-846 6020A-B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B206425 06/22/181.54 50.018F0987-02 [HHSB-B (0-1)]
B206425 06/22/181.42 50.018F0987-03 [HHSB-C (0-1)]
B206425 06/22/181.47 50.018F0987-07 [HHSB-G (0-1)]
B206425 06/22/181.46 50.018F0987-08 [HHSB-H (0-1)]
B206425 06/22/181.46 50.018F0987-09 [HHSB-I (0-1)]
SW-846 7196A
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B206519 06/25/182.54 10018F0987-02 [HHSB-B (0-1)]
B206519 06/25/182.54 10018F0987-03 [HHSB-C (0-1)]
B206519 06/25/182.55 10018F0987-07 [HHSB-G (0-1)]
B206519 06/25/182.57 10018F0987-08 [HHSB-H (0-1)]
B206519 06/25/182.59 10018F0987-09 [HHSB-I (0-1)]
Prep Method: SW-846 5035-SW-846 8260B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B206280 06/21/184.53 10.018F0987-01 [HHSB-A (0-1)]
B206280 06/21/185.31 10.018F0987-02 [HHSB-B (0-1)]
B206280 06/21/185.12 10.018F0987-04 [HHSB-D (1-2)]
B206280 06/21/186.15 10.018F0987-05 [HHSB-E (0-1)]
B206280 06/21/185.64 10.018F0987-06 [HHSB-F (0-1)]
B206280 06/21/186.14 10.018F0987-07 [HHSB-G (0-1)]
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B206337 06/21/1830.1 1.0018F0987-01 [HHSB-A (0-1)]
B206337 06/21/1830.1 1.0018F0987-04 [HHSB-D (1-2)]
B206337 06/21/1830.0 1.0018F0987-05 [HHSB-E (0-1)]
B206337 06/21/1830.0 1.0018F0987-06 [HHSB-F (0-1)]
[TOC_1]Sample Preparation Information[TOC]
Page 35 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B206280 - SW-846 5035
[TOC_3]B206280[TOC]
Blank (B206280-BLK1) Prepared & Analyzed: 06/21/18
Acetone mg/Kg wet0.10ND
Acrylonitrile mg/Kg wet0.0060ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010ND
Benzene mg/Kg wet0.0020ND
Bromobenzene mg/Kg wet0.0020ND
Bromochloromethane mg/Kg wet0.0020ND
Bromodichloromethane mg/Kg wet0.0020ND
Bromoform mg/Kg wet0.0020ND
Bromomethane mg/Kg wet0.010ND
2-Butanone (MEK)mg/Kg wet0.040ND
tert-Butyl Alcohol (TBA)mg/Kg wet0.040ND
n-Butylbenzene mg/Kg wet0.0020ND
sec-Butylbenzene mg/Kg wet0.0020ND
tert-Butylbenzene mg/Kg wet0.0020ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010ND
Carbon Disulfide mg/Kg wet0.0060ND
Carbon Tetrachloride mg/Kg wet0.0020ND
Chlorobenzene mg/Kg wet0.0020ND
Chlorodibromomethane mg/Kg wet0.0010ND
Chloroethane mg/Kg wet0.020 R-05ND
Chloroform mg/Kg wet0.0040ND
Chloromethane mg/Kg wet0.010ND
2-Chlorotoluene mg/Kg wet0.0020ND
4-Chlorotoluene mg/Kg wet0.0020ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020ND
1,2-Dibromoethane (EDB)mg/Kg wet0.0010ND
Dibromomethane mg/Kg wet0.0020ND
1,2-Dichlorobenzene mg/Kg wet0.0020ND
1,3-Dichlorobenzene mg/Kg wet0.0020ND
1,4-Dichlorobenzene mg/Kg wet0.0020ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020ND
1,1-Dichloroethane mg/Kg wet0.0020ND
1,2-Dichloroethane mg/Kg wet0.0020ND
1,1-Dichloroethylene mg/Kg wet0.0040ND
cis-1,2-Dichloroethylene mg/Kg wet0.0020ND
trans-1,2-Dichloroethylene mg/Kg wet0.0020ND
1,2-Dichloropropane mg/Kg wet0.0020ND
1,3-Dichloropropane mg/Kg wet0.0010ND
2,2-Dichloropropane mg/Kg wet0.0020ND
1,1-Dichloropropene mg/Kg wet0.0020ND
cis-1,3-Dichloropropene mg/Kg wet0.0010ND
trans-1,3-Dichloropropene mg/Kg wet0.0010ND
Diethyl Ether mg/Kg wet0.020ND
Diisopropyl Ether (DIPE)mg/Kg wet0.0010ND
1,4-Dioxane mg/Kg wet0.10ND
Ethylbenzene mg/Kg wet0.0020ND
Hexachlorobutadiene mg/Kg wet0.0020ND
2-Hexanone (MBK)mg/Kg wet0.020ND
Isopropylbenzene (Cumene)mg/Kg wet0.0020ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040ND
[TOC_1]QC Data[TOC]
Page 36 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B206280 - SW-846 5035
Blank (B206280-BLK1) Prepared & Analyzed: 06/21/18
Methylene Chloride mg/Kg wet0.020ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020ND
Naphthalene mg/Kg wet0.0040ND
n-Propylbenzene mg/Kg wet0.0020ND
Styrene mg/Kg wet0.0020ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010ND
Tetrachloroethylene mg/Kg wet0.0020ND
Tetrahydrofuran mg/Kg wet0.010ND
Toluene mg/Kg wet0.0020ND
1,2,3-Trichlorobenzene mg/Kg wet0.0020ND
1,2,4-Trichlorobenzene mg/Kg wet0.0020ND
1,3,5-Trichlorobenzene mg/Kg wet0.0020ND
1,1,1-Trichloroethane mg/Kg wet0.0020ND
1,1,2-Trichloroethane mg/Kg wet0.0020ND
Trichloroethylene mg/Kg wet0.0020ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010ND
1,2,3-Trichloropropane mg/Kg wet0.0020ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010ND
1,2,4-Trimethylbenzene mg/Kg wet0.0020ND
1,3,5-Trimethylbenzene mg/Kg wet0.0020ND
Vinyl Chloride mg/Kg wet0.010ND
m+p Xylene mg/Kg wet0.0040ND
o-Xylene mg/Kg wet0.0020ND
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 95.70.0479
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1000.0500
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1020.0508
LCS (B206280-BS1) Prepared & Analyzed: 06/21/18
Acetone mg/Kg wet0.10 0.200 L-0770-160171*0.341
Acrylonitrile mg/Kg wet0.0060 0.0200 70-13096.40.0193
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 70-13088.70.0177
Benzene mg/Kg wet0.0020 0.0200 70-13096.00.0192
Bromobenzene mg/Kg wet0.0020 0.0200 70-1301010.0203
Bromochloromethane mg/Kg wet0.0020 0.0200 70-1301060.0212
Bromodichloromethane mg/Kg wet0.0020 0.0200 70-13096.80.0194
Bromoform mg/Kg wet0.0020 0.0200 70-1301090.0218
Bromomethane mg/Kg wet0.010 0.0200 V-3440-13057.60.0115
2-Butanone (MEK)mg/Kg wet0.040 0.200 70-1601350.269
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 40-1301010.202
n-Butylbenzene mg/Kg wet0.0020 0.0200 70-1301040.0208
sec-Butylbenzene mg/Kg wet0.0020 0.0200 70-1301130.0227
tert-Butylbenzene mg/Kg wet0.0020 0.0200 70-16098.80.0198
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 70-13094.70.0189
Carbon Disulfide mg/Kg wet0.0060 0.0200 70-1301140.0228
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 70-1301070.0213
Chlorobenzene mg/Kg wet0.0020 0.0200 70-1301030.0206
Chlorodibromomethane mg/Kg wet0.0010 0.0200 70-1301050.0210
Chloroethane mg/Kg wet0.020 0.0200 R-0570-1301150.0231
Chloroform mg/Kg wet0.0040 0.0200 70-13098.00.0196
Chloromethane mg/Kg wet0.010 0.0200 70-13099.60.0199
2-Chlorotoluene mg/Kg wet0.0020 0.0200 70-1301020.0204
Page 37 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B206280 - SW-846 5035
LCS (B206280-BS1) Prepared & Analyzed: 06/21/18
4-Chlorotoluene mg/Kg wet0.0020 0.0200 70-1301030.0207
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 70-1301040.0207
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 70-1301020.0204
Dibromomethane mg/Kg wet0.0020 0.0200 70-1301080.0217
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301080.0216
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301080.0216
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301030.0206
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 70-1301100.0219
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 V-34, J40-16081.50.0163
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 70-1301010.0202
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 70-1301040.0209
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 70-1301140.0229
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-1301020.0205
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-1301010.0202
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-1301070.0214
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 70-13097.30.0195
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13099.10.0198
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 70-13091.50.0183
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13094.70.0189
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-1301020.0204
Diethyl Ether mg/Kg wet0.020 0.0200 70-1301010.0202
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 70-13097.00.0194
1,4-Dioxane mg/Kg wet0.10 0.200 40-16080.60.161
Ethylbenzene mg/Kg wet0.0020 0.0200 70-1301040.0209
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 70-1601200.0241
2-Hexanone (MBK)mg/Kg wet0.020 0.200 70-1601270.253
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 70-1301140.0229
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 70-1301090.0218
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 70-13095.60.0191
Methylene Chloride mg/Kg wet0.020 0.0200 J40-16097.40.0195
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 70-1601210.241
Naphthalene mg/Kg wet0.0040 0.0200 40-13099.70.0199
n-Propylbenzene mg/Kg wet0.0020 0.0200 70-1301070.0213
Styrene mg/Kg wet0.0020 0.0200 70-1301040.0209
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 70-1301160.0233
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 70-13099.70.0199
Tetrachloroethylene mg/Kg wet0.0020 0.0200 70-1301190.0238
Tetrahydrofuran mg/Kg wet0.010 0.0200 70-1301070.0214
Toluene mg/Kg wet0.0020 0.0200 70-1301020.0204
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-1301120.0225
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-1301150.0230
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-1301100.0220
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 70-13097.40.0195
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 70-13098.40.0197
Trichloroethylene mg/Kg wet0.0020 0.0200 70-13099.40.0199
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 70-1301010.0202
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 70-1301050.0210
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 70-1301120.0223
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-1301030.0206
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-1301060.0213
Vinyl Chloride mg/Kg wet0.010 0.0200 40-13097.00.0194
Page 38 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B206280 - SW-846 5035
LCS (B206280-BS1) Prepared & Analyzed: 06/21/18
m+p Xylene mg/Kg wet0.0040 0.0400 70-1301030.0411
o-Xylene mg/Kg wet0.0020 0.0200 70-1301010.0201
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 93.00.0465
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1000.0500
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1010.0507
LCS Dup (B206280-BSD1) Prepared & Analyzed: 06/21/18
Acetone mg/Kg wet0.10 0.200 2570-160142 18.50.284
Acrylonitrile mg/Kg wet0.0060 0.0200 2570-13096.4 0.000.0193
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 2570-13092.1 3.760.0184
Benzene mg/Kg wet0.0020 0.0200 2570-13097.1 1.140.0194
Bromobenzene mg/Kg wet0.0020 0.0200 2570-130104 2.920.0209
Bromochloromethane mg/Kg wet0.0020 0.0200 2570-130110 3.610.0220
Bromodichloromethane mg/Kg wet0.0020 0.0200 2570-130107 9.730.0213
Bromoform mg/Kg wet0.0020 0.0200 2570-130123 12.10.0246
Bromomethane mg/Kg wet0.010 0.0200 25 V-3440-13068.4 17.10.0137
2-Butanone (MEK)mg/Kg wet0.040 0.200 2570-160136 1.140.272
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 2540-13096.9 4.100.194
n-Butylbenzene mg/Kg wet0.0020 0.0200 2570-130103 0.7710.0207
sec-Butylbenzene mg/Kg wet0.0020 0.0200 2570-130106 7.120.0211
tert-Butylbenzene mg/Kg wet0.0020 0.0200 2570-16098.9 0.1010.0198
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 2570-13095.9 1.260.0192
Carbon Disulfide mg/Kg wet0.0060 0.0200 2570-130120 5.630.0241
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 2570-130109 2.130.0218
Chlorobenzene mg/Kg wet0.0020 0.0200 2570-130102 0.9770.0204
Chlorodibromomethane mg/Kg wet0.0010 0.0200 2570-130111 5.090.0221
Chloroethane mg/Kg wet0.020 0.0200 25 R-05, J70-13084.2 31.2 *0.0168
Chloroform mg/Kg wet0.0040 0.0200 2570-130101 2.820.0202
Chloromethane mg/Kg wet0.010 0.0200 2570-130100 0.5010.0200
2-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-130103 1.070.0206
4-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-130103 0.4850.0206
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 2570-13098.2 5.450.0196
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 2570-130101 0.5910.0203
Dibromomethane mg/Kg wet0.0020 0.0200 2570-130108 0.000.0217
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130105 2.720.0210
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130108 0.2770.0217
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130101 2.450.0201
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 2570-130122 10.60.0244
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 25 V-34, J40-16085.5 4.790.0171
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130104 2.830.0208
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130104 0.09570.0209
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 2570-130123 6.830.0245
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-130110 6.600.0219
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-130106 5.020.0212
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-130111 3.840.0223
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 2570-13098.8 1.530.0198
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-130101 2.200.0203
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 2570-13097.5 6.350.0195
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13094.2 0.5290.0188
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-130103 1.070.0207
Diethyl Ether mg/Kg wet0.020 0.0200 2570-130107 5.870.0214
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 2570-13099.4 2.440.0199
Page 39 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B206280 - SW-846 5035
LCS Dup (B206280-BSD1) Prepared & Analyzed: 06/21/18
1,4-Dioxane mg/Kg wet0.10 0.200 5040-160128 45.60.257
Ethylbenzene mg/Kg wet0.0020 0.0200 2570-130103 1.740.0205
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 2570-160117 2.860.0234
2-Hexanone (MBK)mg/Kg wet0.020 0.200 2570-160132 3.850.263
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 2570-130114 0.000.0229
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 2570-130105 3.640.0211
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 2570-13098.2 2.680.0196
Methylene Chloride mg/Kg wet0.020 0.0200 2540-160105 7.410.0210
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 2570-160130 7.340.259
Naphthalene mg/Kg wet0.0040 0.0200 2540-130112 11.70.0224
n-Propylbenzene mg/Kg wet0.0020 0.0200 2570-130106 0.1880.0213
Styrene mg/Kg wet0.0020 0.0200 2570-130104 0.000.0209
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 2570-130104 10.90.0209
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 2570-130106 6.310.0212
Tetrachloroethylene mg/Kg wet0.0020 0.0200 2570-130122 2.160.0243
Tetrahydrofuran mg/Kg wet0.010 0.0200 2570-13097.6 9.370.0195
Toluene mg/Kg wet0.0020 0.0200 2570-130102 0.09790.0204
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-130115 2.200.0230
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-130113 1.930.0226
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-130107 2.760.0214
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 2570-13098.3 0.9200.0197
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130102 3.690.0204
Trichloroethylene mg/Kg wet0.0020 0.0200 2570-130101 1.400.0202
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 2570-13095.8 5.280.0192
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 2570-130101 3.780.0202
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 2570-130114 2.040.0228
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-130101 1.860.0202
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-130107 0.4690.0214
Vinyl Chloride mg/Kg wet0.010 0.0200 2540-13097.1 0.1030.0194
m+p Xylene mg/Kg wet0.0040 0.0400 2570-130102 1.030.0407
o-Xylene mg/Kg wet0.0020 0.0200 2570-13098.0 2.620.0196
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 95.30.0477
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1020.0508
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1000.0501
Page 40 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B206337 - SW-846 3546
[TOC_3]B206337[TOC]
Blank (B206337-BLK1) Prepared: 06/21/18 Analyzed: 06/22/18
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Anthracene mg/Kg wet0.17ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Naphthalene mg/Kg wet0.17ND
Phenanthrene mg/Kg wet0.17ND
Pyrene mg/Kg wet0.17ND
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 71.52.38
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 72.42.41
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 78.02.60
LCS (B206337-BS1) Prepared: 06/21/18 Analyzed: 06/22/18
Acenaphthene mg/Kg wet0.17 1.67 40-14063.21.05
Acenaphthylene mg/Kg wet0.17 1.67 40-14064.91.08
Anthracene mg/Kg wet0.17 1.67 40-14067.81.13
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14065.81.10
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14066.91.12
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14065.91.10
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14065.51.09
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14065.21.09
Chrysene mg/Kg wet0.17 1.67 40-14066.11.10
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14063.41.06
Fluoranthene mg/Kg wet0.17 1.67 40-14066.01.10
Fluorene mg/Kg wet0.17 1.67 40-14066.21.10
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14063.71.06
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14067.61.13
Naphthalene mg/Kg wet0.17 1.67 40-14064.41.07
Phenanthrene mg/Kg wet0.17 1.67 40-14066.11.10
Pyrene mg/Kg wet0.17 1.67 40-14064.71.08
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 66.62.22
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 67.12.24
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 70.62.35
Page 41 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B206337 - SW-846 3546
LCS Dup (B206337-BSD1) Prepared: 06/21/18 Analyzed: 06/22/18
Acenaphthene mg/Kg wet0.17 1.67 3040-14065.4 3.391.09
Acenaphthylene mg/Kg wet0.17 1.67 3040-14066.4 2.281.11
Anthracene mg/Kg wet0.17 1.67 3040-14068.1 0.5001.14
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14067.1 1.931.12
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14067.7 1.251.13
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14067.0 1.591.12
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14066.2 1.061.10
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14066.1 1.281.10
Chrysene mg/Kg wet0.17 1.67 3040-14065.3 1.191.09
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14064.5 1.811.08
Fluoranthene mg/Kg wet0.17 1.67 3040-14067.4 2.071.12
Fluorene mg/Kg wet0.17 1.67 3040-14067.0 1.231.12
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14064.8 1.741.08
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14069.0 2.081.15
Naphthalene mg/Kg wet0.17 1.67 3040-14066.7 3.421.11
Phenanthrene mg/Kg wet0.17 1.67 3040-14068.2 3.131.14
Pyrene mg/Kg wet0.17 1.67 3040-14064.8 0.1851.08
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 67.82.26
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 66.42.21
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 68.62.29
Page 42 of 51
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Metals Analyses (Total)[TOC]
Batch B206425 - SW-846 3050B
[TOC_3]B206425[TOC]
Blank (B206425-BLK1) Prepared: 06/22/18 Analyzed: 06/24/18
Arsenic mg/Kg wet0.17ND
Chromium mg/Kg wet4.2ND
Cobalt mg/Kg wet1.5ND
Lead mg/Kg wet1.7ND
Nickel mg/Kg wet4.2ND
Cadmium mg/Kg wet0.32ND
LCS (B206425-BS1) Prepared: 06/22/18 Analyzed: 06/24/18
Arsenic mg/Kg wet2.0 161 83.2-116.899.0159
Chromium mg/Kg wet50 136 82.4-117.6103141
Cobalt mg/Kg wet18 48.2 84.2-115.610852.3
Lead mg/Kg wet20 111 83-117.1103114
Nickel mg/Kg wet50 91.9 82.9-117.510697.1
Cadmium mg/Kg wet3.8 211 83.4-116.698.0207
LCS Dup (B206425-BSD1) Prepared: 06/22/18 Analyzed: 06/24/18
Arsenic mg/Kg wet2.0 161 3083.2-116.898.1 0.874158
Chromium mg/Kg wet49 136 3082.4-117.6101 1.94138
Cobalt mg/Kg wet18 48.2 3084.2-115.6106 2.6350.9
Lead mg/Kg wet20 111 3083-117.199.8 2.78111
Nickel mg/Kg wet49 91.9 3082.9-117.5102 3.9493.3
Cadmium mg/Kg wet3.7 211 3083.4-116.693.3 4.94197
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B206519 - SW-846 7196A
[TOC_3]B206519[TOC]
Blank (B206519-BLK1) Prepared: 06/25/18 Analyzed: 06/26/18
Hexavalent Chromium mg/Kg wet0.16ND
LCS (B206519-BS1) Prepared: 06/25/18 Analyzed: 06/26/18
Hexavalent Chromium mg/Kg wet1.7 63.8 L-0780-12079.9 *51
LCS Dup (B206519-BSD1) Prepared: 06/25/18 Analyzed: 06/26/18
Hexavalent Chromium mg/Kg wet1.7 64.4 2080-12086.5 8.8956
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 6020A-B in Soil
NY,VA,NH,NCArsenic
NY,NCChromium
NY,NCCobalt
NY,NCLead
NY,NCNickel
NY,NCCadmium
SW-846 7196A in Soil
NY,CT,NH,NC,ME,VAHexavalent Chromium
SW-846 8260B in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
[TOC_1]Certifications[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260B in Soil
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
CT,NY,NH,ME,NC,VAAnthracene
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
CT,NY,NH,ME,NC,VAFluoranthene
CT,NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPyrene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2018
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2019
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2019
LAO00112Rhode Island Department of HealthRI 12/30/2018
652North Carolina Div. of Water QualityNC 12/31/2018
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2018
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2018
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2018
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2018
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2018
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