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HomeMy WebLinkAbout21022_Brownfields Assessment Report_08.06.2019   Adams Property  Brownfields Assessment Report  510 W Tremont Avenue      F&R Project No. 63X‐0084  Charlotte, North Carolina        August 5, 2019   2  BACKGROUND  The Property consists of an approximate 1.9 acre parcel located at 510 West Tremont Avenue in  Charlotte, North Carolina and identified as Mecklenburg County Parcel No. 119‐164‐21.  F&R  understands that the Property is currently undeveloped.  The Property was historically a salvage  yard  and  quarry,  and  prior  investigations  by  others  identified soil  and  groundwater  contamination consisting of metals and petroleum compounds at the Property.  Based on these  findings, the Property was submitted to the NCDEQ Brownfields Program.    Based on the historical site use and sampling data, preparation of a work plan for additional  sampling of soil, groundwater and soil‐gas was requested Mr. Cody  Cannon of  the NCDEQ  Brownfields Program in June 2019.  Based on the presence of historic trash fill, the NCDEQ also  identified  concern  from  methane  gas  intrusion.  The  purpose  of  the  assessment  was  to  characterize surface soils related to historical site use, determine if there is a risk of methane gas  or vapor intrusion, and to assist in making risk management decisions for inclusion in the  Brownfields Agreement.  The following report details the additional assessment conducted in  accordance  with  the  previously  approved  Work  Plan.  Please  reference  Figure  2  for  sample  locations.  CONFIRMATORY SOIL ANALYSIS  F&R advanced four (4) soil borings at the locations requested by NCDEQ (B‐1, B‐5, B‐6 and B‐9).  The soil borings were installed in order to collect soil samples for the analysis of RCRA metals and  hexavalent chromium, volatile organic compounds (VOCs), and semi‐volatile organic compounds  (SVOCs). In addition, one background sample (B‐10) was collected at the northeast corner of the  Property  (for  RCRA  metals  and  hexavalent  chromium  only).  During  previous  investigations,  metals (including Chromium) were detected above the Residential Preliminary Soil Remediation  Goal (PSRG).  The previous analysis did not differentiate between  hexavalent  and  trivalent  chromium. The chromium detected was believed to be naturally occurring trivalent chromium;  however sampling for hexavalent chromium was conducted during this investigation to determine  the species and concentrations of chromium present.     Sampling was conducted utilizing direct push technology (Geoprobe™).  Direct‐push technology is  a truck or track‐mounted tool that pushes sampling devices into the sub‐surface using hydraulic  pressure.    This  method  creates  little  disturbance,  leaving  only  a  2‐inch  diameter  borehole.   Additionally, one duplicate sample was collected from soil sample location B‐2 for a total of 6 soil  samples.  The soil samples were collected from the 0‐2 foot interval below ground surface (bgs)  at the approximate locations of historic samples SB‐1, SB‐3, the location of the historical quarry,  and one within the proposed footprint of the proposed multi‐family structure, as requested by    Adams Property  Brownfields Assessment Report  510 W Tremont Avenue      F&R Project No. 63X‐0084  Charlotte, North Carolina        August 5, 2019   3  the NCDEQ and shown on the attached Sample Location Plan (Appendix A – Figure 2).  Soil  samples  collected  were  screened  in  the  field with  a  photoionization  detector (PID)  for  the  presence of volatile organic compounds (VOCs) by head space analysis.  PID readings above  background were not identified.  According to the laboratory results of the soil samples submitted for analysis, VOCs were not  detected above laboratory method detection limits, except for acetone, a common laboratory  contaminant.  Acetone concentrations were below its Residential PSRG.  Several SVOCs, including  benzo(a)anthracene,  benzo(a)pyrene,  benzo(b)fluouranthene,  dibenzo(a,h)anthracene,  and  indeno(1,2,3‐cd)pyrene  were  detected  above  their  respective  Residential PSRGs.  The  concentrations detected did not exceed the non‐residential PSRGs.   Arsenic was detected at concentrations ranging from 2.6 to 20 mg/kg, which exceeds the Residential  and  Commercial  PSRGs  of  0.68  and  3.0  mg/kg.    The  concentrations  detected  were  generally  consistent with the concentrations in the background sample (B‐10, 4.5 mg/kg), indicating these  detections are naturally occurring except in sample SB‐1 (from boring B‐1) which was approximately  an order of magnitude greater than the background sample.  Hexavalent chromium was detected  above the Residential PSRG of 0.31 mg/kg, at concentrations of 0.81 mg/kg (in B‐6) and 0.5 and 1.2  mg/kg  (in  B‐9  and  the  duplicate  from  B‐9).    The  concentrations detected  did  not  exceed  the  Commercial PSRG of 6.5 mg/kg.  Hexavalent chromium was also detected in the background sample  at an estimated concentration (‘J’ flag) of 0.29 mg/kg.  The analytical parameters and results are  summarized on Tables 1 and 2 in Appendix B, and shown on Figure 3.  The laboratory report is  included in Appendix C.  The borings were backfilled and abandoned with the soil cuttings upon  completion.  MONITORING WELL INSTALLATION AND GROUNDWATER SAMPLING  Groundwater was previously measured by Mill Creek Environmental in monitoring wells during the  previous groundwater sampling event in February 2017.  The approximate well depths and depths  to groundwater recorded at that time are as shown on the following table:  Monitoring Well  (No.) MW‐1  MW‐2  MW‐3  Depth to Water  February 2017  (ft)  30.82  25.43  28.08  Depth of Well  (ft) 45  40  43    Adams Property  Brownfields Assessment Report  510 W Tremont Avenue      F&R Project No. 63X‐0084  Charlotte, North Carolina        August 5, 2019   4  Previously installed monitoring wells MW‐1, MW‐2, and MW‐3, could not be located and are  presumed destroyed.  Therefore, replacement monitoring wells (MW‐1R, MW‐2R, and MW‐3R)  were installed in the approximate locations of the previous wells using hollow‐stem auger drilling  techniques.  Soils were screened with a PID during drilling.  The wells were installed by a North  Carolina Licensed Well Driller from South Atlantic Environmental Drilling and Construction Company  (SAEDACCO) on July 5, 2019 in accordance with NCAC 2C Well Construction Rules. The wells were  constructed with 2‐inch PVC and 10 feet of screen.  Gravel pack was installed around the screen  to  2’  above  the  top  of  the  screen,  with  a  bentonite  seal  installed  above  the  gravel  pack.    A  cement/bentonite slurry was be placed above the bentonite seal to the ground surface, and the  wells were finished with an approximate 2 foot stick‐up and locking cap.  The wells were developed  and the stick‐ups finished on July 11, 2019.  The wells were allowed to stabilize for at least 24‐ hours after development prior to sampling. F&R measured groundwater levels and conducted a  relative survey of the wells.  The well information is shown on the table below, and a groundwater  flow map is included as Figure 4. Groundwater flow was measured to be generally to the north‐ northeast.  Monitoring Well  (No.) MW‐1R  MW‐2R  MW‐3R  Relative Top of Casing  (TOC) Elevation (ft) 700.00  695.10  695.90  Depth of Well (ft)  38.0  32.5  37.75  Depth to Water from  TOC (ft) 28.10  24.45  29.24  Relative Groundwater  Elevation (ft) 671.90  670.65  666.66  * Top of casing elevation based on a relative survey and assumed benchmark of 700 feet  The well records are included in Appendix D.  MW‐1R is identified as MW‐4R in the well record  prepared by the driller form SAEDACCO.  PID readings above background were not identified  during monitoring well installation or sampling.  F&R sampled the monitoring wells on July 18, 2019.  F&R utilized low flow sampling techniques  with a submersible pump and dedicated sampling tubing to attempt to minimize turbidity, with a  turbidity goal of <10 NTU, since sampling for RCRA metals was included in the groundwater  analysis.    Field measurements were recorded including pH, temperature, and conductivity for  stabilization prior to collecting samples in accordance with the workplan.  The groundwater samples  were placed into laboratory provided sample jars for laboratory analysis of VOCs, SVOCs, RCRA  metals, and hexavalent chromium.  Well MW‐3R was still slightly turbid and the turbidity was 10    Adams Property  Brownfields Assessment Report  510 W Tremont Avenue      F&R Project No. 63X‐0084  Charlotte, North Carolina        August 5, 2019   5  NTU after well purging.  Readings obtained for stabilization are shown in the table below:    Time  pH  Temp   (°C)  Conductivity  (µs/cm)  Turbidity  (NTU)  MW‐1R      1105  8.76  22.3  10.3  >100  1120  8.74  21.8  10.2  7.0  1130  8.74  21.7  10.3  5.63  MW‐2R      1030  8.77  21.8  10.1  >100  1040  8.78  21.0  10.3  >100  1050  8.80  20.9  10.3  7.0  MW‐3R      0905  8.80  21.7  10.1  >100  0915  8.82  20.8  10.1  >100  1000  8.82  20.3  10.0  10.0  Note: Monitoring well MW‐3R pumped dry at 0915, adjusted rate and resumed   pumping after ~30 minutes    The groundwater sample collected from MW‐1R detected target compounds (VOCs, SVOCs, and  RCRA metals) above laboratory reporting limits and the North Carolina 2L Groundwater Quality  Standards (NC2LGWQS).  The groundwater sample collected from MW‐2R and MW‐3R and the  duplicate from MW‐2R detected target compounds (VOCs and RCRA metals) above laboratory  reporting limits and the NC2LGWQS.  Results of the sample from MW‐2R were generally consistent  with the duplicate.  The higher turbidity in the sample from MW‐3R may have slightly contributed  to  the  elevated  metals  in  this  sample.    Lead  was  detected  above the NC2LGWQS in all the  groundwater samples, but was also identified above the NC2LGWQS in the field blank and the  laboratory method blank. While total chromium was detected above the NC2LGWQS, speciation  analysis  indicated  that  the  detected  concentrations  were  that  of  trivalent  chromium,  and  are  therefore likely to be naturally occurring.  Table 3 in Appendix B presents a summary of the groundwater analytical results from this event  compared to the NC2LGWQS. The groundwater exceedances are shown on Figure 5. The laboratory  analytical results are provided in Appendix C of this report.           Adams Property  Brownfields Assessment Report  510 W Tremont Avenue      F&R Project No. 63X‐0084  Charlotte, North Carolina        August 5, 2019   6  SOIL‐GAS POINT INSTALLATION AND SAMPLING  F&R advanced via a GeoProbe, seven temporary soil‐gas borings to five feet bgs to screen for  methane with a landfill gas meter.  These borings were installed at the locations of historical  geotechnical borings B‐103A and B‐105A(F&R Borings B‐4 and B‐2), three locations within the  proposed building footprint (F&R Borings B‐7, B‐8 and B‐9), and two locations within the former  quarry operation on the eastern portion of the Property (F&R Borings B‐3 and B‐5), as requested  by the NCDEQ and shown on Figure 2.  Methane concentrations ranged from 0 to 56.8 percent  as shown on Table 4 and Figure 6.    Additionally, three soil‐gas borings were advanced for VOCs analysis via TO‐15 at the locations of  former geotechnical borings B‐103A, B‐105A (B‐4 and B‐2), and the northwest corner of the  proposed building (B‐7) to 20 feet bgs, i.e., a few feet above the water table in accordance with  the NCDEQ Division of Waste Management (DWM) Vapor Intrusion Guidance Document (VIG) dated  March  2018.    Groundwater  levels  in  the  monitoring  wells  were  measured  at  the  time  of  installation  to  determine  of  the  appropriate  depth  for  installation  of  the  soil‐gas  points.   Groundwater was measured between approximately 22 and 27 feet bgs (24 to 29 feet from top  of casing).  The soil‐gas samples were collected by installing an approximate 2‐inch diameter boring to a few  feet above the capillary fringe based on water levels as determined during boring installation and  historic groundwater levels.  The points were installed in accordance with the DEQ DWM Vapor  Intrusion Guidance Document. The points consisted of a 6‐inch vapor sampling probe connected to  dedicated Teflon sampling tubing inserted into the temporary soil‐gas boring points as proposed in  the work plan. A gravel pack filter was installed around the vapor probe to 6 inches to 1 foot above  the  top  of  the  probe,  followed  by  granular  bentonite  to  the  surface,  which  was  hydrated  in  approximate 1‐foot intervals, and packed around the surface to form a seal.  The soil‐gas samples were collected as generally recommended in EPA Soil‐Gas Sampling Operating  Procedure.  The points were allowed to equilibrate for a minimum of 2 hours after installation prior  to sampling.  The tubing was purged in conjunction with the helium leak test (discussed below) for  a minimum of 5 minutes using an air pump at 0.2 L/min maximum (and three sample probe and  tubing volumes) to ensure background air was removed from the tubing in accordance with the DEQ  DWM Vapor Intrusion Guidance and EPA Soil‐Gas Sampling Operating Procedure.  A helium leak test and a shut‐in test was performed to test the integrity of the seals and the soil gas  sampling apparatus.  The helium leak test consisted of filling and sealing a shroud over the sample  point and tubing after the tubing had been placed and sealed.  The shroud was filled to a minimum    Adams Property  Brownfields Assessment Report  510 W Tremont Avenue      F&R Project No. 63X‐0084  Charlotte, North Carolina        August 5, 2019   7  of 50% helium.  A sample was drawn into a tedlar bag from the shroud and the sampling apparatus  using a syringe.  A MGD 2002 helium gas detector was connected to the tedlar bag to check the  helium concentration.  To be considered a good seal the helium concentration at the sample tubing  must be less than 10% of the concentration in the shroud.  Helium concentrations in the sampling  probe and tubing was less than 1% of the concentration in the shroud for the three soil‐gas points.   The soil‐gas samples were collected using 1L batch certified Summa Canisters with flow controller  calibrated at 0.2 L/min (approximately 5 minutes sampling time).  The soil‐gas samples were analyzed for VOCs by Method TO‐15.  Upon completion the tubing was  removed and the soil‐gas points sealed with bentonite.  The soil‐gas samples collected detected multiple VOCs at concentrations above their laboratory  reporting limits.  1,3‐Butadiene exceeded the Residential Soil Gas Screening Level (SGSL) of 14  ug/M3 in sample B‐2 and the duplicate from that location with concentrations of 160 and 72 ug/M3,  respectively. 1,3‐butadiene is typically found in urban areas and is associated with automobile,  cigarette, and manufacturing exhaust, and production of rubber and plastics.  1,3‐butadiene was  not identified in soil or groundwater at the Property.  Sample SB‐4 detected m/p‐xylene above the  Residential SGSL. Other target compounds did not exceed their applicable Residential SGSLs.  Target  compounds did not exceed the Non‐Residential SGSLs.  Table 4 in Appendix B presents a summary  of the soil‐gas analytical results for this event. The Soil‐Gas exceedances are shown on Figure 7.  The  laboratory analytical results are provided in Appendix C of this report.    LABORATORY QA/QC  A total of four soil samples plus a duplicate (5 total) were submitted to an independent North  Carolina certified laboratory for analysis of volatile organic compounds (VOCs) by EPA method  8260, semi‐volatile organic compounds (SVOCs) by EPA Method 8270, RCRA Metals by EPA  Method 6020, and Hexavalent Chromium by EPA Method 7199.  A total of three non‐filtered groundwater samples plus a duplicate (4 total) were submitted to an  independent North Carolina certified laboratory for analysis of VOCs by EPA method 8260, SVOCs  by EPA Method 8270, and RCRA Metals by EPA Method 6020.   A total of three soil‐gas samples plus a duplicate (4 total) were submitted to an independent  NVLAP accredited laboratory for analysis of VOCs by EPA Method TO‐15.    As requested in the NCDEQ May 1, 2019 AAR, Level 2 QA/QC data packages were requested.  F&R  requested that estimated values above the laboratory method detection limit (MDL) but above    Adams Property  Brownfields Assessment Report  510 W Tremont Avenue      F&R Project No. 63X‐0084  Charlotte, North Carolina        August 5, 2019   8  the laboratory reporting limit be reported by the laboratory with a ‘J’ flag.  Level 2 QA/QC data  packages and ‘J’ flags were included in the laboratory data packages as requested.  In addition, a single field and trip blank was collected per cooler for the soil and groundwater  sampling in accordance with the approved work plan.  INVESTIGATION DERIVED WASTE (IDW) MANAGEMENT  The borings were backfilled with the soil cuttings and abandoned upon completion. Since no  obvious indications of contamination were identified based on existing soil sampling data or  during the soil borings or replacement monitoring well installation, soil cuttings were spread  evenly on the land surface around the borings.   Purge water from monitoring wells was filtered through carbon and discharged to the ground  adjacent to the monitoring wells, since obvious contamination such as odors or elevated PID  readings were not identified in the monitoring wells.  RECEPTOR SURVEY The Brownfields receptor survey did not identify sensitive receptors or wells within the applicable  buffer distances. Several underground utilities were identified within 100 feet of the Brownfield  boundary.  Based on the results of Soil‐Gas samples vapors are not anticipated to impact these  receptors.  The Brownfields Receptor Survey is provided in Appendix E of this report.    FINDINGS and CONCLUSIONS  F&R provides the following findings and conclusions based on the limited assessment and sampling  conducted:   Hexavalent chromium was detected in the soils at concentrations above the Residential PSRG  of 0.31 mg/kg, at concentrations of 0.81 mg/kg (in B‐6) and 0.5 and 1.2 mg/kg (in B‐9 and the  duplicate from B‐9).The concentrations detected did not exceed the commercial PSRG of 6.5  mg/kg.  A low level of hexavalent chromium was also detected in the background sample at an  estimated concentration (‘J’ flag) of 0.29 mg/kg.     Arsenic was detected at concentrations ranging from 2.6 to 20 mg/kg,  which  exceeds  its  Residential and Commercial PSRGs.  The concentrations detected were generally consistent with  the concentrations in the background sample (B‐10), indicating these detections are naturally  occurring  except  in  sample  SB‐1  (from  boring  B‐1)  which  was  approximately  an  order  of  magnitude greater than the background sample.     Several  SVOCs,  including  benzo(a)anthracene,  benzo(a)pyrene,  benzo(b)fluouranthene,  dibenzo(a,h)anthracene,  and  indeno(1,2,3‐cd)pyrene  were  detected  above  their  respective    Adams Property  Brownfields Assessment Report  510 W Tremont Avenue      F&R Project No. 63X‐0084  Charlotte, North Carolina        August 5, 2019   9  Residential PSRGs in the soil samples collected.  The concentrations detected did not exceed the  non‐residential PSRGs.    Several VOCs, SVOCs and RCRA metals were detected in the groundwater at concentrations  that exceeded the NC2LGWQS.  Hexavalent chromium was not detected above laboratory  reporting limits.  The target compound concentrations did not exceed the GCLs except for  lead in well MW‐3R.  Sample MW‐3R was noted to be slightly more turbid than the targeted  turbidity of <10 NTU after purging which may have slightly contributed to the elevated metals  in this sample.  Lead was also detected in the field and laboratory method blank.   1,3‐butadiene exceeded the Residential SGSL of 14 ug/M3 at a concentration of 73 and 160  ug/M3 at 15 feet bgs at location B‐2.  1,3‐butadiene is typically found in urban areas and is  associated with automobile, cigarette, and manufacturing exhaust, and production of rubber  and plastics.  Sample SB‐4 detected m/p‐xylene above the Residential SGSL.  1,3‐butadiene and  m/p xylene were not identified in soil or groundwater at the Property.     Methane concentrations raged from 0 to 56.8 percent at the property with the highest  concentrations on the north‐central portion of the Property.         Adams Property  Brownfields Assessment Report  510 W Tremont Avenue      F&R Project No. 63X‐0084  Charlotte, North Carolina        August 5, 2019   10    ACKNOWLEDGMENTS    We appreciate the opportunity to be of service to you on this project.  If you have any questions  regarding this letter, please do not hesitate to contact us.      Sincerely,   FROEHLING & ROBERTSON, INC.,      Brian T. Olin, P.G.     Benjamin Whitley, P.E.  Lead Environmental Scientist    Senior Environmental Professional      Attachments:  Limitations    Appendix A – Figures    Appendix B – Analytical Summary Tables    Appendix C – Laboratory Analytical Report    Appendix D – Monitoring Well Records    Appendix E – Brownfield Receptor Survey      Email Distribution:   David Barringer Smith (Tremont Capital, LLC) david.@barringer‐homes.com                    Cody Cannon(NCDEQ)  cody.cannon@ncdenr.gov         LIMITATIONS    This report has been prepared for the exclusive use of Tremont Capital, LLC c/o Barringer Homes  and or their authorized agents and the NCDEQ.  This report has been prepared in accordance  with generally accepted environmental practices.  No other warranty, expressed or implied, is  made.  Our conclusions and findings are based, in part, upon information provided to us by others  and our site observations.  We have not verified the completeness or accuracy of the information  provided by others. Our observations and findings are based upon conditions readily visible at  the  site  at  the  time  of  our  site  visit,  analytical  tests,  and  upon  current  accepted  industry  standards. The scope of services performed was limited to those requested by the Client.     F&R,  by  virtue  of  providing  the  services  described  in  this  report, does not assume the  responsibility of the person(s) in charge of the site, or otherwise undertake responsibility for  reporting to any local, state, or federal public agencies any conditions at the site that may present  a potential danger to public health, safety, or the environment.  In areas that require notification  of local, state, or federal agencies as required by law, it is the Client’s responsibility to so notify.   Under this scope of services, F&R assumes no responsibility regarding any response actions or  additional studies, which may be required as a result of these findings.  Response actions are the  sole responsibility of the Client and should be conducted in accordance with local, state, and/or  federal requirements, and should be performed by appropriate trained and qualified personnel,  as warranted.                                             Appendix A  Figures     Drawn: BTO  Scale: As Shown  Project No.: 63X‐0084 Checked: BTO Date: 6/10/2019  Drawing No.: 1 Site Location Map Adams Property Brownfields Project No.: 21022‐17‐060 N Wendys BP Gasoline,  McDonald's Approximate  Brownfields Limit FROEHLING & ROBERTSON, INC. Engineering Stability Since 1881 3300 International Airport Drive, Suite 600 Charlotte, North Carolina  28208 T 704.596.2889 I F 704.596.3784 Replacement Monitoring Well (at approximate locationof historic monitoring wells)MW‐2RMW‐1RMW‐3RB‐10B‐9B‐8B‐7B‐6B‐5B‐4B‐3B‐2B‐1 (SB‐1)FIGURE 2 ‐ SAMPLE LOCATION MAP Replacement Monitoring Well (at approximate locationof historic monitoring wells)B‐8B‐7B‐4B‐3B‐2B‐1 (SB‐1)Benzo(a)pyrene0.21 JArsenic20B‐5Benzo(a)anthracene1.2Benzo(a)pyrene1.8Benzo(b)fluoranthene2.8Dibenzo(a,h)anthracene   1.1Indeno(1,2,3‐cd)pyrene1.1Arsenic2.6B‐6Arsenic7.6Hexavalent Chromium       0.81B‐9Benzo(a)pyrene0.31 JArsenic2.7Hexavalent Chromium       1.22B‐9 (Duplicate)Benzo(a)pyrene0.18 JArsenic3.1Hexavalent Chromium       0.55B‐10 (Background)Arsenic4.5Hexavalent Chromium       0.29 JFIGURE 3 ‐ EXCEEDANCES ONLY SOIL CONCENTRATION MAP Replacement Monitoring Well (at approximate locationof historic monitoring wells)MW‐3R666.66 ftMW‐1R671.90 ftMW‐2R670.65 ft671 ft670 ft667 ft669 ft668 ftApproximate GroundwaterFlow DirectionFIGURE 4 ‐ GROUNDWATER ELEVATION MAP Replacement Monitoring Well (at approximate locationof historic monitoring wells)MW‐2RMW‐1RMW‐3RFIGURE 5 ‐ EXCEEDANCES ONLY GROUNDWATER  CONCENTRATION MAPMW‐3RNaphthalene6.5Arsenic170Barium5,500Cadmium670Selenium190 ASilver20Lead61,000 BMW‐2RNaphthalene6.5Cadmium2.1Lead250 BMW‐2R (Duplicate)Naphthalene6.5Chloromethane11Cadmium2.3Lead230 BMW‐1R1,2‐Dichoroethane0.47 JTetrachoroethylene (PCE)      13Benzo(a)anthracene5.1 JBenzo(a)pyrene4.5 JBenzo(b)fluoranthene6.0 JChrysene5.8 JIndeno(1,2,3‐cd)pyrene8.2 JCadmium3.0Lead290 B Replacement Monitoring Well (at approximate locationof historic monitoring wells)FIGURE 6 ‐ METHANE GAS CONCENTRATION MAPB‐7Methane 56.8 %B‐2Methane 11.7 %B‐3Methane 20.0 %B‐4Methane 40.2 %B‐5Methane 0.0 %B‐8Methane 1.1 %B‐9Methane 3.9 % Replacement Monitoring Well (at approximate locationof historic monitoring wells)FIGURE 7 ‐ EXCEEDANCES ONLY SOIL‐GAS CONCENTRATION MAPB‐4m/p‐xylene             160B‐21,3‐Butadiene       160B‐2 (Duplicate)1,3‐Butadiene       72B‐7No Exceedances                         Appendix B  Tables     TABLE 1 SAMPLE LOCATION AND ANALYTICAL PARAMETERS SUMMARY TABLE ADAMS PROPERTY – BROWNFIELDS PROJECT NO. 21022‐17‐060 510 W TREMONT AVE., CHARLOTTE, NC  Sample IDs Sample Objective Approximate Depth Analytical Method QA/QC/Samples Background Samples Soil B‐1 (SB‐1), B‐5, B‐6, B‐9, and B‐10 (background) Surficial Soil Characterization 0‐2’  VOCS –EPA Method 8260; SVOCs – EPA Method 8270; RCRA Metals – EPA Method 6020 Duplicate, Field Blank, Trip Blank Northeast Corner for RCRA Metals only (B‐10) Groundwater MW‐1R  Groundwater Contaminant Levels ~30’  VOCS –EPA Method 8260; SVOCs – EPA Method 8270; RCRA Metals Duplicate, Field Blank, Trip Blank N/A MW‐2R  ~25’ MW‐3R  ~30’ Soil‐Gas B‐2( near B‐103A), and B‐4 (near B‐105A  Methane‐Prior Fill 5’  Landfill Gas Meter N/A – Field Measurement Background Air – Field Screening B‐7, B‐8, and B‐9  Methane – Proposed Buildings Footprint B‐3, B‐5  Methane – Eastern Portion B‐2, B‐4, and B‐7  Volatile Vapors  ~20’  TO‐15  Duplicate   N/A   Sample ID: SB‐1 B‐5 B‐6 B‐9 B‐9 Dup B‐10#Residential IndustrialSample Date:7/3/2019 7/3/2019 7/3/2019 7/3/2019 7/3/2019 7/3/2019 PSRG PSRGSample Depth:0.5‐2.0' 0.5‐2.0' 0.5‐2.0' 0.5‐2.0' 0.5‐2.0' 0‐1.0'Concentration:mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/Kg mg/KgVolatile Organic Compounds (VOCs)Acetone0.1 0.023 0.036 J 0.21 0.031 NA 12,000140,000Semi‐Volatile Organic Compounds (SVOCs)2‐Methylnaphthalene0.18 J ND ND ND ND NA 48 600Acenaphthylene ND 0.27 J ND ND ND NA 720 9,000Benzo(a)anthracene 0.24 J1.2ND 0.32 J 0.17 J NA 1.1 21.0Benzo(a)pyrene0.21 J 1.8ND0.31 J 0.18 JNA 0.11 2.1Benzo(b)flouranthene 0.30 J2.8ND 0.44 J 0.26 J NA 1.1 21.0Benzo(g,h,i)perylene ND 1.0 ND 0.20 J ND NA ‐ ‐Chrysene  0.25 J 0.83 ND 0.31 J ND NA 110 2,100Dibenzo(a,h)anthracene ND1.1ND ND ND NA 0.11 2.1Fluoranthene 0.51 J 0.26 J ND 0.63 J 0.24 J NA 480 6,000Indeno(1,2,3‐cd)pyrene ND1.1ND 0.22 J ND NA 1.1 21Phenanthrene 0.40 J ND ND 0.28 J ND NA ‐ ‐Pyrene 0.40 J 1.8 ND 0.53 J 0.29 J NA 360 4,500RCRA Metals Mercury0.16 0.15 0.045 J 0.29 0.045 J 0.065 2.3 9.7Arsenic20 2.6 7.6 2.7 3.1 4.50.68 3Barium63 68 66 84 91 100 3,100 47,000Cadmium0.21 J 0.17 J 1.8 0.18 J 0.29 J 1.1 110 3.0Chromium * 33 35 47 33 49 57 0.31 6.5Hexavalent Chromium 0.20 J ND0.81 1.2 0.550.29 J 0.31 6.5Lead 54 100 170 210 82 220 ‐ ‐Selenium 1.2 J 1.2 1.0 J 1.4 1.8 2.0 78 1,200Silver ND ND ND ND ND 0.18 J 78 1,200Data reported in Milligrams per kilogram (mg/Kg)PSRG = NCDEQ Innactive Hazardous Site Branch Preliminary Soil Remediation Goals (February 2018A complete list of target compounds is provided in the laboratory reportCompounds not listed were not detected during sampling in 2017.  Historical exceedances were limited to petroleum compounds addressed through a NORP and did not exceed Residential MSCCsSample SB‐1 was collected from boring B‐1.ND = Not Detected (below reporting limits)NA = Not AnalyzedJ = Estimated concentration.  Compound detected below laboratory reporting limit‐ = No Standard* Standard based on hexavalent chromium, lowest standard for trivalent chromium is 24,000 mg/kg# Backgorund sample for comparison purposes.Bold values exceed the Residential PSRG.Table 2Adams Property ‐ July 2019 Soil Sampling Summary510 West Tremont AvenueCharlotte, North CarolinaF&R Project No. 63X‐0084 Sample ID: MW‐1R MW‐2R MW‐2R (Dup) MW‐3R Field Blank NC2LGWQS NC GCLs Sample Date:7/18/2019 7/18/2019 7/18/2019 7/18/2019 7/18/2019 Concentration:ug/L ug/L ug/L ug/L ug/L ug/L ug/L 1,2‐Dichloroethane 0.47 J ND ND ND ND 0.4 400 Chloroform 0.5 ND ND ND ND 70 70,000 Isopropyl Ether 0.61 ND ND ND ND 70 70,000 Methyl Isobutyl Ketone (MIBK)ND ND 0.37 J 0.31 J ND 100 100,000 Methyl‐tert‐Butyl Ether (MTBE)16 0.57 0.48 J 0.45 J ND 20 20,000 Tetrachloroethylene (PCE)13 ND ND ND ND 0.7 700 Trichloroethylene (TCE)0.73 ND ND ND ND 3 3,000 1,2,4‐Trimethylbenzene ND 14 14 15 ND 400 28,500 1,3,5‐Trimethylbenzene ND 6.7 6.1 6.7 ND 400 28,500 4‐Isopropyltoluene ND 3.9 3.6 3.9 ND 25 11,700 Acetone *ND 8.4 8.7 35 18 6,000 6,000,000 Carbon Disulfide ND 3.9 J ND ND ND 700 590,000 Chloromethane ND ND 11 ND ND 3 3,000 Isopropylbenzene (cumene)ND 1.5 1.4 1.5 ND 70 25,000 Naphthalene ND 6.5 6.5 6.5 0.53 J 6 6,000 n‐butylbenzene ND 2.9 2.6 3.1 ND 70 6,900 n‐propylbenzene ND 3.5 3.2 3.6 ND 70 30,000 sec‐butylbenzene ND 5.2 4.7 5.3 ND 70 8,500 tert‐butylbenzene ND 1.7 1.5 1.6 ND 70 15,000 Benzo(a)anthracene 5.1 J ND ND ND ND 0.05 4.7 Benzo(a)pyrene 4.5 J ND ND ND ND 0.0005 0.81 Benzo(b)fluoranthene 6.0 J ND ND ND ND 0.05 0.75 Chrysene 5.8 J ND ND ND ND 5 5 Fluoranthene 17 ND ND ND ND 300 300 Indeno(1,2,3‐cd)pyrene 8.2 J ND ND ND ND 0.05 0.05 Pyrene 14 ND ND ND ND 200 200 Arsenic 9.5 7.5 7.5 170 ND 10 ‐ Barium 220 430 430 5,500 ND 700 700,000 Cadmium 3.0 2.1 2.3 670 ND 2 ‐ Chromium** 65 21 22 2,500 0.94 J 10 10,000 Hexavalent Chromium ND ND ND ND ND 10 10,000 Selenium 4.4 J 1.1 J 1.3 J 190 A ND 20 ‐ Silver 0.54 J ND ND 20 ND 20 20,000 Mercury 0.00036 J ND 0.00017 J ND ND 1 ‐ Lead 290 B 230 B 250 B 61,000 B 78 B 15 15,000 Data reported in Micrograms per liter (ug/L) NC2LGWQS = North Carolina 2L Grounwater Quality Standard A complete list of target compounds is provided in the laboratory report. Compounds not listed were not detected. J ‐ Detected but below the Laboratory Reporting Limit; therefore, result is an estimated concentration B ‐ Analyte is found in the associated laboratory blank at a concentration >1/2 RL A ‐ LLICV standard recovery (74%) is less than the lower control limit (80%).  Result might have a slight low bias * For acetone, the results were below control limits but within method parameters. A standard at or below the RL was analyzed and found acceptable.    Result is reported but considered estimated. ** Standard based on hexavalent chromium, no standard for trivalent chromium Semi‐Volatile Organic Compounds (SVOCs) RCRA Metals Volatile Organic Compounds (VOCs) Table 3 Adams Property ‐ July 2019 Groundwater Sampling Summary 510 West Tremont Avenue Charlotte, North Carolina F&R Project No. 63X‐0084 Sample ID: B‐2 B‐2 (Dup) B‐3 B‐4 B‐5 B‐7 B‐8 B‐9NC Residential Vapor NC Non‐Residential VaporSample Date:1/4/2018 1/4/2018 1/8/2018 1/8/2018 1/8/2018 1/8/2018 1/8/2018 1/8/2018 Intrusion Soil‐Gas Intrusion Soil‐GasDepth ft. bgs:20 20 5 20 5 20 5 5 Screening Levels Screening LevelsConcentration:ug/M3ug/M3ug/M3ug/M3ug/M3ug/M3ug/M3ug/M3ug/M3ug/M3Methane (Field Screening)Methane (%)11.7 NA 20.0 40.2 0.0 56.8 1.1 3.9 ‐ ‐Volatile Organic Compounds (TO‐15)Acetone370 230 NA ND NA ND NA NA 220,0002,700,000Benzene28 14 NA 9.1 NA 8.6 NA NA 120 1,6001,3‐Butadiene160 72NA ND NA ND NA NA 14 1802‐Butanone (MEK)50 J 43 J NA 22 J NA 30 J NA NA 35,000 440,000Carbon Disulfide110 74 NA 75 NA 110 NA NA 4,900 61,000CyclohexaneND ND NA ND NA 49 NA NA 42,000 530,000Ethanol44 30 J NA 170 NA ND NA NA ‐ ‐Ethyl Acetate130 66 NA 50 NA 25 NA NA 490 6,1004‐Ethyltoluene34 30 NA ND NA ND NA NA ‐ ‐Heptane53 18 NA 25 NA 96 NA NA 2,800 35,000HexaneND ND NA 80 J NA 760 NA NA 4,900 61,000IsopropanolND ND NA ND NA 14 J NA NA 1,400 18,000Methyl tert‐Butyl Ether (MTBE)37 28 NA 72 NA ND NA NA 3,600 47,000Tolune42 21 NA 27 NA 12 NA NA 35,000 440,0001,2,4‐Trimethylbenzene72 85 NA ND NA ND NA NA 420 5,3001,3,5‐Trimethylbenzene23 22 NA ND NA ND NA NA 420 5,300Ethylbenzene16 11 NA 59 NA 68 NA NA 370 4,900Methylene Chloride 5.3 J ND NA ND NA ND NA NA 4,200 53,000Propene4,500 2,000 NA ND NA ND NA NA 21,000 260,000m&p‐Xylene35 32 NA1,400NA 360 NA NA 700 8,800o‐Xylene16 15 NA 530 NA 120 NA NA 700 8,800Data reported in Micrograms per cubic meter (ug/M3)Vapor Intrusion Screening Levels from the NC Divison of Waste Management Vapor Intrusion Screening Levels Dated February 2018Compounds not listed were not detected above the laboratory reporting limits.A complete list of target compounds is provided in the laboratory reportNA = Not AnalyzedND = Not detected (below reporting limits)J = Estimated concentration.  Compound detected below laboratory reporting limit‐ = No StandardBold values exceed the Most Stringent Vapor Intrusion Screening LevelTable 4Adams Property ‐ July 2019 Soil‐Gas Sampling Summary510 West Tremont AvenueCharlotte, North CarolinaF&R Project No. 63X‐0084 Boring ID Latitude LongitudeB‐1 35.21154 ‐80.86862B‐2 35.21157 ‐80.86846B‐3 35.21168 ‐80.86840B‐4 35.21179 ‐80.86852B‐5 35.21197 ‐80.86846B‐6 32.21188 ‐80.86852B‐7 35.21236 ‐80.86880B‐8 35.21206 ‐80.86885B‐9 35.21172 ‐80.86876B‐10 35.21237 ‐80.86848MW‐1R 35.21181 ‐80.86879MW‐2R 35.21192 ‐80.86854MW‐3R 35.21154‐80.86856Location data collected with handheld GPS for informational purposes and is not surveyed or survey grade data.Table 5Sample Location CoordinatesAdam's Property ‐ 510 West Tremont AvenueCharlotte, North CarolinaF&R Project No. 63X‐0084                         Appendix C  Laboratory Analytical Data                                           Soil      This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Case Narrative 7/15/19 13:33 Froehling & Robertson, Inc. (Charlotte) Brian Olin 3300 International Airport Dr., Suite 600 Charlotte, NC 28208 Project: Barringer Homes Lab Submittal Date: 07/05/2019 Prism Work Order: 9070063 This is a Revised Report and supercedes the original laboratory report dated 7/12/19. Client Sample ID B-10: 8260 and 8270 analyses were removed as they were not requested on the Chain of Custody. Narrative Notes: Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. VP Laboratory Services Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash President/Project Manager This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 64 Data Qualifiers Key Reference: CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. HT Sample received and analyzed outside of the hold time. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken. L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken. LH High LCS recovery. Analyte not detected in the sample(s). No further action taken. Method Detection LimitMDL Below Reporting LimitBRL Relative Percent DifferenceRPD *Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 64 Sample Receipt Summary 07/15/2019 Prism Work Order: 9070063 Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received 9070063-01 07/03/19 9:00SB-1 07/05/19 11:05Solid 9070063-02 07/03/19 10:30B-5 07/05/19 11:05Solid 9070063-03 07/03/19 10:45B-6 07/05/19 11:05Solid 9070063-04 07/03/19 11:10B-9 07/05/19 11:05Solid 9070063-05 07/03/19 11:15B-9 Dup 07/05/19 11:05Solid 9070063-06 07/03/19 11:35B-10 07/05/19 11:05Solid 9070063-07 07/03/19 10:00Field Blank 07/05/19 11:05Water 9070063-08 07/03/19 0:00Trip Blank 07/05/19 11:05Water Samples were received in good condition at 5.5 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 64 Client ID ResultParameterMethod UnitsPrism ID Prism Work Order: 9070063 07/15/2019 Summary of Detections 0.18 J mg/kg dry9070063-01 SB-1 2-Methylnaphthalene 8270E 0.24 J mg/kg dry9070063-01 SB-1 Benzo(a)anthracene 8270E 0.21 J mg/kg dry9070063-01 SB-1 Benzo(a)pyrene 8270E 0.30 J mg/kg dry9070063-01 SB-1 Benzo(b)fluoranthene 8270E 0.25 J mg/kg dry9070063-01 SB-1 Chrysene 8270E 0.51 J mg/kg dry9070063-01 SB-1 Fluoranthene 8270E 0.40 J mg/kg dry9070063-01 SB-1 Phenanthrene 8270E 0.40 J mg/kg dry9070063-01 SB-1 Pyrene 8270E 0.20 J mg/kg dry9070063-01 SB-1 Hexavalent Chromium 7196A 0.16 mg/kg dry9070063-01 SB-1 Mercury 7471B 20 mg/kg dry9070063-01 SB-1 Arsenic 6020B 63 mg/kg dry9070063-01 SB-1 Barium 6020B 0.21 J mg/kg dry9070063-01 SB-1 Cadmium 6020B 33 mg/kg dry9070063-01 SB-1 Chromium 6020B 54 mg/kg dry9070063-01 SB-1 Lead 6020B 1.2 J mg/kg dry9070063-01 SB-1 Selenium 6020B 0.10 mg/kg dry9070063-01 SB-1 Acetone 8260D 0.27 J mg/kg dry9070063-02 B-5 Acenaphthylene 8270E 1.2 mg/kg dry9070063-02 B-5 Benzo(a)anthracene 8270E 1.8 mg/kg dry9070063-02 B-5 Benzo(a)pyrene 8270E 2.8 mg/kg dry9070063-02 B-5 Benzo(b)fluoranthene 8270E 1.0 mg/kg dry9070063-02 B-5 Benzo(g,h,i)perylene 8270E 0.83 mg/kg dry9070063-02 B-5 Benzo(k)fluoranthene 8270E 1.1 mg/kg dry9070063-02 B-5 Chrysene 8270E 0.26 J mg/kg dry9070063-02 B-5 Dibenzo(a,h)anthracene 8270E 1.1 mg/kg dry9070063-02 B-5 Fluoranthene 8270E 1.1 mg/kg dry9070063-02 B-5 Indeno(1,2,3-cd)pyrene 8270E 1.8 mg/kg dry9070063-02 B-5 Pyrene 8270E 0.42 J mg/kg dry9070063-02 B-5 Hexavalent Chromium 7196A 0.15 mg/kg dry9070063-02 B-5 Mercury 7471B 2.6 mg/kg dry9070063-02 B-5 Arsenic 6020B 68 mg/kg dry9070063-02 B-5 Barium 6020B 0.17 J mg/kg dry9070063-02 B-5 Cadmium 6020B 35 mg/kg dry9070063-02 B-5 Chromium 6020B 100 mg/kg dry9070063-02 B-5 Lead 6020B 1.2 mg/kg dry9070063-02 B-5 Selenium 6020B 0.023 mg/kg dry9070063-02 B-5 Acetone 8260D 0.81 mg/kg dry9070063-03 B-6 Hexavalent Chromium 7196A 0.045 J mg/kg dry9070063-03 B-6 Mercury 7471B 7.6 mg/kg dry9070063-03 B-6 Arsenic 6020B 66 mg/kg dry9070063-03 B-6 Barium 6020B 1.8 mg/kg dry9070063-03 B-6 Cadmium 6020B 47 mg/kg dry9070063-03 B-6 Chromium 6020B 170 mg/kg dry9070063-03 B-6 Lead 6020B This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 64 Client ID ResultParameterMethod UnitsPrism ID Prism Work Order: 9070063 07/15/2019 Summary of Detections 1.0 J mg/kg dry9070063-03 B-6 Selenium 6020B 0.036 J mg/kg dry9070063-03 B-6 Acetone 8260D 0.32 J mg/kg dry9070063-04 B-9 Benzo(a)anthracene 8270E 0.31 J mg/kg dry9070063-04 B-9 Benzo(a)pyrene 8270E 0.44 J mg/kg dry9070063-04 B-9 Benzo(b)fluoranthene 8270E 0.20 J mg/kg dry9070063-04 B-9 Benzo(g,h,i)perylene 8270E 0.31 J mg/kg dry9070063-04 B-9 Chrysene 8270E 0.63 J mg/kg dry9070063-04 B-9 Fluoranthene 8270E 0.22 J mg/kg dry9070063-04 B-9 Indeno(1,2,3-cd)pyrene 8270E 0.28 J mg/kg dry9070063-04 B-9 Phenanthrene 8270E 0.53 J mg/kg dry9070063-04 B-9 Pyrene 8270E 1.2 mg/kg dry9070063-04 B-9 Hexavalent Chromium 7196A 0.29 mg/kg dry9070063-04 B-9 Mercury 7471B 2.7 mg/kg dry9070063-04 B-9 Arsenic 6020B 84 mg/kg dry9070063-04 B-9 Barium 6020B 0.18 J mg/kg dry9070063-04 B-9 Cadmium 6020B 33 mg/kg dry9070063-04 B-9 Chromium 6020B 210 mg/kg dry9070063-04 B-9 Lead 6020B 1.4 mg/kg dry9070063-04 B-9 Selenium 6020B 0.21 mg/kg dry9070063-04 B-9 Acetone 8260D 0.17 J mg/kg dry9070063-05 B-9 Dup Benzo(a)anthracene 8270E 0.18 J mg/kg dry9070063-05 B-9 Dup Benzo(a)pyrene 8270E 0.26 J mg/kg dry9070063-05 B-9 Dup Benzo(b)fluoranthene 8270E 0.24 J mg/kg dry9070063-05 B-9 Dup Fluoranthene 8270E 0.29 J mg/kg dry9070063-05 B-9 Dup Pyrene 8270E 0.55 mg/kg dry9070063-05 B-9 Dup Hexavalent Chromium 7196A 0.045 J mg/kg dry9070063-05 B-9 Dup Mercury 7471B 3.1 mg/kg dry9070063-05 B-9 Dup Arsenic 6020B 91 mg/kg dry9070063-05 B-9 Dup Barium 6020B 0.29 J mg/kg dry9070063-05 B-9 Dup Cadmium 6020B 49 mg/kg dry9070063-05 B-9 Dup Chromium 6020B 82 mg/kg dry9070063-05 B-9 Dup Lead 6020B 1.8 mg/kg dry9070063-05 B-9 Dup Selenium 6020B 0.031 mg/kg dry9070063-05 B-9 Dup Acetone 8260D 0.29 J mg/kg dry9070063-06 B-10 Hexavalent Chromium 7196A 0.065 mg/kg dry9070063-06 B-10 Mercury 7471B 4.5 mg/kg dry9070063-06 B-10 Arsenic 6020B 100 mg/kg dry9070063-06 B-10 Barium 6020B 1.1 mg/kg dry9070063-06 B-10 Cadmium 6020B 57 mg/kg dry9070063-06 B-10 Chromium 6020B 220 mg/kg dry9070063-06 B-10 Lead 6020B 2.0 mg/kg dry9070063-06 B-10 Selenium 6020B 0.18 J mg/kg dry9070063-06 B-10 Silver 6020B 14 ug/L9070063-07 Field Blank Acetone 8260D 4.0 J ug/L9070063-08 Trip Blank Acetone 8260D This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 64 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: SB-1 Prism Sample ID: 9070063-01 Prism Work Order: 9070063 Time Collected: 07/03/19 09:00 Time Submitted: 07/05/19 11:05 General Chemistry Parameters 80.8 SM2540 G P9G014110.100 7/10/19 9:20 KBS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.141,2,4-Trichlorobenzene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.131,2-Dichlorobenzene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.121,3-Dichlorobenzene BRL 8270E P9G012110.41 7/8/19 21:24 JMVmg/kg dry 0.131,4-Dichlorobenzene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.171-Methylnaphthalene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.172,4,5-Trichlorophenol BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.202,4,6-Trichlorophenol BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.162,4-Dichlorophenol BRL 8270E P9G012110.41 7/8/19 21:24 JMVmg/kg dry 0.172,4-Dimethylphenol BRL 8270E P9G012111.9 7/8/19 21:24 JMVmg/kg dry 0.482,4-Dinitrophenol BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.222,4-Dinitrotoluene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.212,6-Dinitrotoluene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.202-Chloronaphthalene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.162-Chlorophenol 0.18 8270E P9G012110.82 7/8/19 21:24 JMVJmg/kg dry 0.162-Methylnaphthalene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.162-Methylphenol BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.142-Nitrophenol BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.163,3’-Dichlorobenzidine BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.183/4-Methylphenol BRL 8270E P9G012111.9 7/8/19 21:24 JMVmg/kg dry 0.454,6-Dinitro-2-methylphenol BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.194-Bromophenyl phenyl ether BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.164-Chloro-3-methylphenol BRL 8270E P9G012110.41 7/8/19 21:24 JMVmg/kg dry 0.0994-Chloroaniline BRL 8270E P9G012111.2 7/8/19 21:24 JMVmg/kg dry 0.254-Chlorophenyl phenyl ether BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.204-Nitrophenol BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.20Acenaphthene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.22Acenaphthylene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.22Anthracene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.17Azobenzene 0.24 8270E P9G012110.82 7/8/19 21:24 JMVJmg/kg dry 0.17Benzo(a)anthracene 0.21 8270E P9G012110.82 7/8/19 21:24 JMVJmg/kg dry 0.18Benzo(a)pyrene 0.30 8270E P9G012110.82 7/8/19 21:24 JMVJmg/kg dry 0.19Benzo(b)fluoranthene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.16Benzo(g,h,i)perylene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.18Benzo(k)fluoranthene BRL 8270E P9G012112.5 7/8/19 21:24 JMVmg/kg dry 0.68Benzoic Acid BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.15Benzyl alcohol BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.16bis(2-Chloroethoxy)methane BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.13Bis(2-Chloroethyl)ether BRL 8270E P9G012110.41 7/8/19 21:24 JMVmg/kg dry 0.15Bis(2-chloroisopropyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: SB-1 Prism Sample ID: 9070063-01 Prism Work Order: 9070063 Time Collected: 07/03/19 09:00 Time Submitted: 07/05/19 11:05 BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.18Bis(2-Ethylhexyl)phthalate BRL 8270E P9G012110.41 7/8/19 21:24 JMVmg/kg dry 0.14Butyl benzyl phthalate 0.25 8270E P9G012110.82 7/8/19 21:24 JMVJmg/kg dry 0.18Chrysene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.23Dibenzo(a,h)anthracene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.22Dibenzofuran BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.21Diethyl phthalate BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.20Dimethyl phthalate BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.20Di-n-butyl phthalate BRL 8270E P9G012110.41 7/8/19 21:24 JMVmg/kg dry 0.21Di-n-octyl phthalate 0.51 8270E P9G012110.82 7/8/19 21:24 JMVJmg/kg dry 0.21Fluoranthene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.24Fluorene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.18Hexachlorobenzene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.18Hexachlorobutadiene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.28Hexachlorocyclopentadiene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.13Hexachloroethane BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.15Indeno(1,2,3-cd)pyrene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.18Isophorone BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.16Naphthalene BRL 8270E P9G012110.41 7/8/19 21:24 JMVmg/kg dry 0.17Nitrobenzene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.19N-Nitroso-di-n-propylamine BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.22N-Nitrosodiphenylamine BRL 8270E P9G012111.2 7/8/19 21:24 JMVmg/kg dry 0.52Pentachlorophenol 0.40 8270E P9G012110.82 7/8/19 21:24 JMVJmg/kg dry 0.21Phenanthrene BRL 8270E P9G012110.82 7/8/19 21:24 JMVmg/kg dry 0.13Phenol 0.40 8270E P9G012110.82 7/8/19 21:24 JMVJmg/kg dry 0.19Pyrene BRL 8270E P9G012110.41 7/8/19 21:24 JMVmg/kg dry 0.078Pyridine Surrogate Recovery Control Limits 39-13284 %2,4,6-Tribromophenol 44-11578 %2-Fluorobiphenyl 35-11579 %2-Fluorophenol 37-12267 %Nitrobenzene-d5 34-12177 %Phenol-d5 54-12776 %Terphenyl-d14 Total Metals 0.20 7196A P9G012210.49 7/9/19 0:00 BMSJmg/kg dry 0.12Hexavalent Chromium 0.16 7471B P9G013110.060 7/9/19 12:10 JABmg/kg dry 0.021Mercury 20 6020B P9G0166101.3 7/12/19 0:26 JABmg/kg dry 0.41Arsenic 63 6020B P9G016610137/12/19 0:26 JABmg/kg dry 0.43Barium 0.21 6020B P9G0166100.63 7/12/19 0:26 JABJmg/kg dry 0.12Cadmium 33 6020B P9G0166101.3 7/12/19 0:26 JABmg/kg dry 0.33Chromium 54 6020B P9G0166101.3 7/12/19 0:26 JABmg/kg dry 0.24Lead 1.2 6020B P9G0166101.3 7/12/19 0:26 JABJmg/kg dry 0.34Selenium This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: SB-1 Prism Sample ID: 9070063-01 Prism Work Order: 9070063 Time Collected: 07/03/19 09:00 Time Submitted: 07/05/19 11:05 BRL 6020B P9G0166100.63 7/12/19 0:26 JABmg/kg dry 0.15Silver Volatile Organic Compounds by GC/MS BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000721,1,1,2-Tetrachloroethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000861,1,1-Trichloroethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000431,1,2,2-Tetrachloroethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000631,1,2-Trichloroethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00111,1-Dichloroethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00111,1-Dichloroethylene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000901,1-Dichloropropylene BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.000841,2,3-Trichlorobenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000671,2,3-Trichloropropane BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.000561,2,4-Trichlorobenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000621,2,4-Trimethylbenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000521,2-Dibromoethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000651,2-Dichlorobenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000701,2-Dichloroethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000881,2-Dichloropropane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000741,3,5-Trimethylbenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000731,3-Dichlorobenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000491,3-Dichloropropane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000741,4-Dichlorobenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000732,2-Dichloropropane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000792-Chlorotoluene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.000674-Chlorotoluene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00154-Isopropyltoluene 0.10 8260D P9G014310.023 7/9/19 19:49 JLBmg/kg dry 0.0015Acetone BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00091Benzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00081Bromobenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00096Bromochloromethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00056Bromodichloromethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00045Bromoform BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.0029Bromomethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.0012Carbon Tetrachloride BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00092Chlorobenzene BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.0011Chloroethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00072Chloroform BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.0018Chloromethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00092cis-1,2-Dichloroethylene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00058cis-1,3-Dichloropropylene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00039Dibromochloromethane BRL 8260D P9G014310.012 7/9/19 19:49 JLBCCVmg/kg dry 0.0017Dichlorodifluoromethane BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00088Ethylbenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00086Isopropyl Ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: SB-1 Prism Sample ID: 9070063-01 Prism Work Order: 9070063 Time Collected: 07/03/19 09:00 Time Submitted: 07/05/19 11:05 BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00068Isopropylbenzene (Cumene) BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.0015m,p-Xylenes BRL 8260D P9G014310.023 7/9/19 19:49 JLBmg/kg dry 0.00041Methyl Butyl Ketone (2-Hexanone) BRL 8260D P9G014310.023 7/9/19 19:49 JLBmg/kg dry 0.0014Methyl Ethyl Ketone (2-Butanone) BRL 8260D P9G014310.023 7/9/19 19:49 JLBmg/kg dry 0.00048Methyl Isobutyl Ketone BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00095Methylene Chloride BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00082Methyl-tert-Butyl Ether BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.00059Naphthalene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00055n-Butylbenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00085n-Propylbenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00062o-Xylene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00063sec-Butylbenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00057Styrene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00070tert-Butylbenzene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.0011Tetrachloroethylene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00093Toluene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.0011trans-1,2-Dichloroethylene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.00050trans-1,3-Dichloropropylene BRL 8260D P9G014310.0059 7/9/19 19:49 JLBmg/kg dry 0.0011Trichloroethylene BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.0016Trichlorofluoromethane BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.00064Vinyl acetate BRL 8260D P9G014310.012 7/9/19 19:49 JLBmg/kg dry 0.0012Vinyl chloride BRL 8260D P9G014310.018 7/9/19 19:49 JLBmg/kg dry 0.0021Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 84-123109 %Dibromofluoromethane 76-12996 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-5 Prism Sample ID: 9070063-02 Prism Work Order: 9070063 Time Collected: 07/03/19 10:30 Time Submitted: 07/05/19 11:05 General Chemistry Parameters 82.4 SM2540 G P9G014110.100 7/10/19 9:20 KBS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.141,2,4-Trichlorobenzene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.131,2-Dichlorobenzene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.121,3-Dichlorobenzene BRL 8270E P9G012110.40 7/8/19 21:47 JMVmg/kg dry 0.131,4-Dichlorobenzene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.171-Methylnaphthalene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.172,4,5-Trichlorophenol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.192,4,6-Trichlorophenol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.162,4-Dichlorophenol BRL 8270E P9G012110.40 7/8/19 21:47 JMVmg/kg dry 0.172,4-Dimethylphenol BRL 8270E P9G012111.8 7/8/19 21:47 JMVmg/kg dry 0.472,4-Dinitrophenol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.212,4-Dinitrotoluene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.212,6-Dinitrotoluene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.202-Chloronaphthalene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.152-Chlorophenol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.162-Methylnaphthalene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.152-Methylphenol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.132-Nitrophenol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.163,3’-Dichlorobenzidine BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.173/4-Methylphenol BRL 8270E P9G012111.8 7/8/19 21:47 JMVmg/kg dry 0.444,6-Dinitro-2-methylphenol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.194-Bromophenyl phenyl ether BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.154-Chloro-3-methylphenol BRL 8270E P9G012110.40 7/8/19 21:47 JMVmg/kg dry 0.0974-Chloroaniline BRL 8270E P9G012111.2 7/8/19 21:47 JMVmg/kg dry 0.244-Chlorophenyl phenyl ether BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.204-Nitrophenol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.19Acenaphthene 0.27 8270E P9G012110.80 7/8/19 21:47 JMVJmg/kg dry 0.22Acenaphthylene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.22Anthracene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.17Azobenzene 1.2 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.17Benzo(a)anthracene 1.8 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.18Benzo(a)pyrene 2.8 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.19Benzo(b)fluoranthene 1.0 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.16Benzo(g,h,i)perylene 0.83 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.17Benzo(k)fluoranthene BRL 8270E P9G012112.4 7/8/19 21:47 JMVmg/kg dry 0.66Benzoic Acid BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.15Benzyl alcohol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.15bis(2-Chloroethoxy)methane BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.13Bis(2-Chloroethyl)ether BRL 8270E P9G012110.40 7/8/19 21:47 JMVmg/kg dry 0.14Bis(2-chloroisopropyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-5 Prism Sample ID: 9070063-02 Prism Work Order: 9070063 Time Collected: 07/03/19 10:30 Time Submitted: 07/05/19 11:05 BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.18Bis(2-Ethylhexyl)phthalate BRL 8270E P9G012110.40 7/8/19 21:47 JMVmg/kg dry 0.14Butyl benzyl phthalate 1.1 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.18Chrysene 0.26 8270E P9G012110.80 7/8/19 21:47 JMVJmg/kg dry 0.23Dibenzo(a,h)anthracene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.22Dibenzofuran BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.21Diethyl phthalate BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.19Dimethyl phthalate BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.20Di-n-butyl phthalate BRL 8270E P9G012110.40 7/8/19 21:47 JMVmg/kg dry 0.21Di-n-octyl phthalate 1.1 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.20Fluoranthene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.24Fluorene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.18Hexachlorobenzene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.18Hexachlorobutadiene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.27Hexachlorocyclopentadiene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.13Hexachloroethane 1.1 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.15Indeno(1,2,3-cd)pyrene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.17Isophorone BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.16Naphthalene BRL 8270E P9G012110.40 7/8/19 21:47 JMVmg/kg dry 0.17Nitrobenzene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.18N-Nitroso-di-n-propylamine BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.22N-Nitrosodiphenylamine BRL 8270E P9G012111.2 7/8/19 21:47 JMVmg/kg dry 0.51Pentachlorophenol BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.21Phenanthrene BRL 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.13Phenol 1.8 8270E P9G012110.80 7/8/19 21:47 JMVmg/kg dry 0.18Pyrene BRL 8270E P9G012110.40 7/8/19 21:47 JMVmg/kg dry 0.076Pyridine Surrogate Recovery Control Limits 39-132101 %2,4,6-Tribromophenol 44-11595 %2-Fluorobiphenyl 35-11587 %2-Fluorophenol 37-12274 %Nitrobenzene-d5 34-12190 %Phenol-d5 54-12788 %Terphenyl-d14 Total Metals 0.42 7196A P9G012210.49 7/9/19 0:00 BMSJmg/kg dry 0.12Hexavalent Chromium 0.15 7471B P9G013110.057 7/9/19 12:15 JABmg/kg dry 0.020Mercury 2.6 6020B P9G0166101.2 7/12/19 0:32 JABmg/kg dry 0.40Arsenic 68 6020B P9G016610127/12/19 0:32 JABmg/kg dry 0.42Barium 0.17 6020B P9G0166100.62 7/12/19 0:32 JABJmg/kg dry 0.12Cadmium 35 6020B P9G0166101.2 7/12/19 0:32 JABmg/kg dry 0.32Chromium 100 6020B P9G0166101.2 7/12/19 0:32 JABmg/kg dry 0.23Lead 1.2 6020B P9G0166101.2 7/12/19 0:32 JABmg/kg dry 0.33Selenium This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-5 Prism Sample ID: 9070063-02 Prism Work Order: 9070063 Time Collected: 07/03/19 10:30 Time Submitted: 07/05/19 11:05 BRL 6020B P9G0166100.62 7/12/19 0:32 JABmg/kg dry 0.15Silver Volatile Organic Compounds by GC/MS BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000621,1,1,2-Tetrachloroethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000741,1,1-Trichloroethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000371,1,2,2-Tetrachloroethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000541,1,2-Trichloroethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000911,1-Dichloroethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000921,1-Dichloroethylene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000781,1-Dichloropropylene BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.000721,2,3-Trichlorobenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000571,2,3-Trichloropropane BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.000481,2,4-Trichlorobenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000531,2,4-Trimethylbenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000451,2-Dibromoethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000561,2-Dichlorobenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000601,2-Dichloroethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000761,2-Dichloropropane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000631,3,5-Trimethylbenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000631,3-Dichlorobenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000421,3-Dichloropropane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000641,4-Dichlorobenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000632,2-Dichloropropane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000682-Chlorotoluene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.000574-Chlorotoluene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00134-Isopropyltoluene 0.023 8260D P9G014310.020 7/9/19 20:19 JLBmg/kg dry 0.0013Acetone BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00079Benzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00070Bromobenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00083Bromochloromethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00048Bromodichloromethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00039Bromoform BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.0025Bromomethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00099Carbon Tetrachloride BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00079Chlorobenzene BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.00096Chloroethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00062Chloroform BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.0015Chloromethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00079cis-1,2-Dichloroethylene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00050cis-1,3-Dichloropropylene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00034Dibromochloromethane BRL 8260D P9G014310.010 7/9/19 20:19 JLBCCVmg/kg dry 0.0014Dichlorodifluoromethane BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00076Ethylbenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00074Isopropyl Ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-5 Prism Sample ID: 9070063-02 Prism Work Order: 9070063 Time Collected: 07/03/19 10:30 Time Submitted: 07/05/19 11:05 BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00059Isopropylbenzene (Cumene) BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.0013m,p-Xylenes BRL 8260D P9G014310.020 7/9/19 20:19 JLBmg/kg dry 0.00035Methyl Butyl Ketone (2-Hexanone) BRL 8260D P9G014310.020 7/9/19 20:19 JLBmg/kg dry 0.0012Methyl Ethyl Ketone (2-Butanone) BRL 8260D P9G014310.020 7/9/19 20:19 JLBmg/kg dry 0.00041Methyl Isobutyl Ketone BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00082Methylene Chloride BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00071Methyl-tert-Butyl Ether BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.00051Naphthalene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00047n-Butylbenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00073n-Propylbenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00054o-Xylene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00054sec-Butylbenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00049Styrene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00060tert-Butylbenzene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00091Tetrachloroethylene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00080Toluene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00097trans-1,2-Dichloroethylene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00043trans-1,3-Dichloropropylene BRL 8260D P9G014310.0050 7/9/19 20:19 JLBmg/kg dry 0.00098Trichloroethylene BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.0014Trichlorofluoromethane BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.00055Vinyl acetate BRL 8260D P9G014310.010 7/9/19 20:19 JLBmg/kg dry 0.0010Vinyl chloride BRL 8260D P9G014310.015 7/9/19 20:19 JLBmg/kg dry 0.0018Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 84-123108 %Dibromofluoromethane 76-12997 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-6 Prism Sample ID: 9070063-03 Prism Work Order: 9070063 Time Collected: 07/03/19 10:45 Time Submitted: 07/05/19 11:05 General Chemistry Parameters 81.1 SM2540 G P9G014110.100 7/10/19 9:20 KBS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.141,2,4-Trichlorobenzene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.131,2-Dichlorobenzene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.121,3-Dichlorobenzene BRL 8270E P9G012110.41 7/8/19 21:01 JMVmg/kg dry 0.131,4-Dichlorobenzene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.171-Methylnaphthalene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.172,4,5-Trichlorophenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.202,4,6-Trichlorophenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.162,4-Dichlorophenol BRL 8270E P9G012110.41 7/8/19 21:01 JMVmg/kg dry 0.172,4-Dimethylphenol BRL 8270E P9G012111.8 7/8/19 21:01 JMVmg/kg dry 0.482,4-Dinitrophenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.222,4-Dinitrotoluene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.212,6-Dinitrotoluene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.202-Chloronaphthalene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.162-Chlorophenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.162-Methylnaphthalene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.162-Methylphenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.142-Nitrophenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.163,3’-Dichlorobenzidine BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.183/4-Methylphenol BRL 8270E P9G012111.8 7/8/19 21:01 JMVmg/kg dry 0.454,6-Dinitro-2-methylphenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.194-Bromophenyl phenyl ether BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.164-Chloro-3-methylphenol BRL 8270E P9G012110.41 7/8/19 21:01 JMVmg/kg dry 0.0994-Chloroaniline BRL 8270E P9G012111.2 7/8/19 21:01 JMVmg/kg dry 0.254-Chlorophenyl phenyl ether BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.204-Nitrophenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.20Acenaphthene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.22Acenaphthylene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.22Anthracene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.17Azobenzene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.17Benzo(a)anthracene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.18Benzo(a)pyrene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.19Benzo(b)fluoranthene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.16Benzo(g,h,i)perylene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.18Benzo(k)fluoranthene BRL 8270E P9G012112.5 7/8/19 21:01 JMVmg/kg dry 0.68Benzoic Acid BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.15Benzyl alcohol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.16bis(2-Chloroethoxy)methane BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.13Bis(2-Chloroethyl)ether BRL 8270E P9G012110.41 7/8/19 21:01 JMVmg/kg dry 0.15Bis(2-chloroisopropyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-6 Prism Sample ID: 9070063-03 Prism Work Order: 9070063 Time Collected: 07/03/19 10:45 Time Submitted: 07/05/19 11:05 BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.18Bis(2-Ethylhexyl)phthalate BRL 8270E P9G012110.41 7/8/19 21:01 JMVmg/kg dry 0.14Butyl benzyl phthalate BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.18Chrysene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.23Dibenzo(a,h)anthracene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.22Dibenzofuran BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.21Diethyl phthalate BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.19Dimethyl phthalate BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.20Di-n-butyl phthalate BRL 8270E P9G012110.41 7/8/19 21:01 JMVmg/kg dry 0.21Di-n-octyl phthalate BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.20Fluoranthene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.24Fluorene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.18Hexachlorobenzene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.18Hexachlorobutadiene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.28Hexachlorocyclopentadiene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.13Hexachloroethane BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.15Indeno(1,2,3-cd)pyrene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.17Isophorone BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.16Naphthalene BRL 8270E P9G012110.41 7/8/19 21:01 JMVmg/kg dry 0.17Nitrobenzene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.19N-Nitroso-di-n-propylamine BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.22N-Nitrosodiphenylamine BRL 8270E P9G012111.2 7/8/19 21:01 JMVmg/kg dry 0.52Pentachlorophenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.21Phenanthrene BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.13Phenol BRL 8270E P9G012110.81 7/8/19 21:01 JMVmg/kg dry 0.19Pyrene BRL 8270E P9G012110.41 7/8/19 21:01 JMVmg/kg dry 0.078Pyridine Surrogate Recovery Control Limits 39-13290 %2,4,6-Tribromophenol 44-11582 %2-Fluorobiphenyl 35-11583 %2-Fluorophenol 37-12270 %Nitrobenzene-d5 34-12182 %Phenol-d5 54-12789 %Terphenyl-d14 Total Metals 0.81 7196A P9G012210.49 7/9/19 0:00 BMSmg/kg dry 0.12Hexavalent Chromium 0.045 7471B P9G013110.061 7/9/19 12:19 JABJmg/kg dry 0.021Mercury 7.6 6020B P9G0166101.2 7/12/19 0:39 JABmg/kg dry 0.41Arsenic 66 6020B P9G016610127/12/19 0:39 JABmg/kg dry 0.42Barium 1.8 6020B P9G0166100.62 7/12/19 0:39 JABmg/kg dry 0.12Cadmium 47 6020B P9G0166101.2 7/12/19 0:39 JABmg/kg dry 0.33Chromium 170 6020B P9G0166101.2 7/12/19 0:39 JABmg/kg dry 0.24Lead 1.0 6020B P9G0166101.2 7/12/19 0:39 JABJmg/kg dry 0.34Selenium BRL 6020B P9G0166100.62 7/12/19 0:39 JABmg/kg dry 0.15Silver This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-6 Prism Sample ID: 9070063-03 Prism Work Order: 9070063 Time Collected: 07/03/19 10:45 Time Submitted: 07/05/19 11:05 Volatile Organic Compounds by GC/MS BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00111,1,1,2-Tetrachloroethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00141,1,1-Trichloroethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.000681,1,2,2-Tetrachloroethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00101,1,2-Trichloroethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00171,1-Dichloroethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00171,1-Dichloroethylene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00141,1-Dichloropropylene BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.00131,2,3-Trichlorobenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00111,2,3-Trichloropropane BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.000901,2,4-Trichlorobenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00101,2,4-Trimethylbenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.000841,2-Dibromoethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00101,2-Dichlorobenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00111,2-Dichloroethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00141,2-Dichloropropane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00121,3,5-Trimethylbenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00121,3-Dichlorobenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.000791,3-Dichloropropane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00121,4-Dichlorobenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00122,2-Dichloropropane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00132-Chlorotoluene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00114-Chlorotoluene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00244-Isopropyltoluene 0.036 8260D P9G014310.038 7/9/19 20:49 JLBJmg/kg dry 0.0024Acetone BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0015Benzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0013Bromobenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0015Bromochloromethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00089Bromodichloromethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00073Bromoform BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.0046Bromomethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0018Carbon Tetrachloride BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0015Chlorobenzene BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.0018Chloroethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0012Chloroform BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.0029Chloromethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0015cis-1,2-Dichloroethylene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00093cis-1,3-Dichloropropylene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00063Dibromochloromethane BRL 8260D P9G014310.019 7/9/19 20:49 JLBCCVmg/kg dry 0.0027Dichlorodifluoromethane BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0014Ethylbenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0014Isopropyl Ether BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0011Isopropylbenzene (Cumene) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-6 Prism Sample ID: 9070063-03 Prism Work Order: 9070063 Time Collected: 07/03/19 10:45 Time Submitted: 07/05/19 11:05 BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.0024m,p-Xylenes BRL 8260D P9G014310.038 7/9/19 20:49 JLBmg/kg dry 0.00065Methyl Butyl Ketone (2-Hexanone) BRL 8260D P9G014310.038 7/9/19 20:49 JLBmg/kg dry 0.0022Methyl Ethyl Ketone (2-Butanone) BRL 8260D P9G014310.038 7/9/19 20:49 JLBmg/kg dry 0.00077Methyl Isobutyl Ketone BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0015Methylene Chloride BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0013Methyl-tert-Butyl Ether BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.00095Naphthalene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00088n-Butylbenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0014n-Propylbenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0010o-Xylene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0010sec-Butylbenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00091Styrene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0011tert-Butylbenzene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0017Tetrachloroethylene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0015Toluene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0018trans-1,2-Dichloroethylene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.00080trans-1,3-Dichloropropylene BRL 8260D P9G014310.0094 7/9/19 20:49 JLBmg/kg dry 0.0018Trichloroethylene BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.0025Trichlorofluoromethane BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.0010Vinyl acetate BRL 8260D P9G014310.019 7/9/19 20:49 JLBmg/kg dry 0.0019Vinyl chloride BRL 8260D P9G014310.028 7/9/19 20:49 JLBmg/kg dry 0.0034Xylenes, total Surrogate Recovery Control Limits 70-130102 %4-Bromofluorobenzene 84-123106 %Dibromofluoromethane 76-12996 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-9 Prism Sample ID: 9070063-04 Prism Work Order: 9070063 Time Collected: 07/03/19 11:10 Time Submitted: 07/05/19 11:05 General Chemistry Parameters 88.6 SM2540 G P9G014110.100 7/10/19 9:20 KBS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.131,2,4-Trichlorobenzene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.121,2-Dichlorobenzene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.111,3-Dichlorobenzene BRL 8270E P9G012110.37 7/8/19 22:10 JMVmg/kg dry 0.121,4-Dichlorobenzene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.161-Methylnaphthalene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.162,4,5-Trichlorophenol BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.182,4,6-Trichlorophenol BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.152,4-Dichlorophenol BRL 8270E P9G012110.37 7/8/19 22:10 JMVmg/kg dry 0.152,4-Dimethylphenol BRL 8270E P9G012111.7 7/8/19 22:10 JMVmg/kg dry 0.442,4-Dinitrophenol BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.202,4-Dinitrotoluene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.192,6-Dinitrotoluene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.182-Chloronaphthalene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.142-Chlorophenol BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.142-Methylnaphthalene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.142-Methylphenol BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.122-Nitrophenol BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.153,3’-Dichlorobenzidine BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.163/4-Methylphenol BRL 8270E P9G012111.7 7/8/19 22:10 JMVmg/kg dry 0.414,6-Dinitro-2-methylphenol BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.174-Bromophenyl phenyl ether BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.144-Chloro-3-methylphenol BRL 8270E P9G012110.37 7/8/19 22:10 JMVmg/kg dry 0.0904-Chloroaniline BRL 8270E P9G012111.1 7/8/19 22:10 JMVmg/kg dry 0.234-Chlorophenyl phenyl ether BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.184-Nitrophenol BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.18Acenaphthene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.20Acenaphthylene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.20Anthracene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.16Azobenzene 0.32 8270E P9G012110.74 7/8/19 22:10 JMVJmg/kg dry 0.16Benzo(a)anthracene 0.31 8270E P9G012110.74 7/8/19 22:10 JMVJmg/kg dry 0.17Benzo(a)pyrene 0.44 8270E P9G012110.74 7/8/19 22:10 JMVJmg/kg dry 0.17Benzo(b)fluoranthene 0.20 8270E P9G012110.74 7/8/19 22:10 JMVJmg/kg dry 0.14Benzo(g,h,i)perylene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.16Benzo(k)fluoranthene BRL 8270E P9G012112.3 7/8/19 22:10 JMVmg/kg dry 0.62Benzoic Acid BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.14Benzyl alcohol BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.14bis(2-Chloroethoxy)methane BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.12Bis(2-Chloroethyl)ether BRL 8270E P9G012110.37 7/8/19 22:10 JMVmg/kg dry 0.13Bis(2-chloroisopropyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-9 Prism Sample ID: 9070063-04 Prism Work Order: 9070063 Time Collected: 07/03/19 11:10 Time Submitted: 07/05/19 11:05 BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.17Bis(2-Ethylhexyl)phthalate BRL 8270E P9G012110.37 7/8/19 22:10 JMVmg/kg dry 0.13Butyl benzyl phthalate 0.31 8270E P9G012110.74 7/8/19 22:10 JMVJmg/kg dry 0.16Chrysene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.21Dibenzo(a,h)anthracene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.20Dibenzofuran BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.19Diethyl phthalate BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.18Dimethyl phthalate BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.18Di-n-butyl phthalate BRL 8270E P9G012110.37 7/8/19 22:10 JMVmg/kg dry 0.19Di-n-octyl phthalate 0.63 8270E P9G012110.74 7/8/19 22:10 JMVJmg/kg dry 0.19Fluoranthene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.22Fluorene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.16Hexachlorobenzene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.17Hexachlorobutadiene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.26Hexachlorocyclopentadiene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.12Hexachloroethane 0.22 8270E P9G012110.74 7/8/19 22:10 JMVJmg/kg dry 0.14Indeno(1,2,3-cd)pyrene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.16Isophorone BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.15Naphthalene BRL 8270E P9G012110.37 7/8/19 22:10 JMVmg/kg dry 0.16Nitrobenzene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.17N-Nitroso-di-n-propylamine BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.20N-Nitrosodiphenylamine BRL 8270E P9G012111.1 7/8/19 22:10 JMVmg/kg dry 0.47Pentachlorophenol 0.28 8270E P9G012110.74 7/8/19 22:10 JMVJmg/kg dry 0.19Phenanthrene BRL 8270E P9G012110.74 7/8/19 22:10 JMVmg/kg dry 0.12Phenol 0.53 8270E P9G012110.74 7/8/19 22:10 JMVJmg/kg dry 0.17Pyrene BRL 8270E P9G012110.37 7/8/19 22:10 JMVmg/kg dry 0.071Pyridine Surrogate Recovery Control Limits 39-13290 %2,4,6-Tribromophenol 44-11583 %2-Fluorobiphenyl 35-11579 %2-Fluorophenol 37-12266 %Nitrobenzene-d5 34-12176 %Phenol-d5 54-12779 %Terphenyl-d14 Total Metals 1.2 7196A P9G012210.45 7/9/19 0:00 BMSmg/kg dry 0.11Hexavalent Chromium 0.29 7471B P9G013110.059 7/9/19 12:24 JABmg/kg dry 0.021Mercury 2.7 6020B P9G0166101.1 7/12/19 0:45 JABmg/kg dry 0.36Arsenic 84 6020B P9G016610117/12/19 0:45 JABmg/kg dry 0.38Barium 0.18 6020B P9G0166100.56 7/12/19 0:45 JABJmg/kg dry 0.11Cadmium 33 6020B P9G0166101.1 7/12/19 0:45 JABmg/kg dry 0.29Chromium 210 6020B P9G0166101.1 7/12/19 0:45 JABmg/kg dry 0.21Lead 1.4 6020B P9G0166101.1 7/12/19 0:45 JABmg/kg dry 0.30Selenium This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-9 Prism Sample ID: 9070063-04 Prism Work Order: 9070063 Time Collected: 07/03/19 11:10 Time Submitted: 07/05/19 11:05 BRL 6020B P9G0166100.56 7/12/19 0:45 JABmg/kg dry 0.13Silver Volatile Organic Compounds by GC/MS BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00121,1,1,2-Tetrachloroethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00141,1,1-Trichloroethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.000691,1,2,2-Tetrachloroethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00101,1,2-Trichloroethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00171,1-Dichloroethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00171,1-Dichloroethylene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00151,1-Dichloropropylene BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.00141,2,3-Trichlorobenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00111,2,3-Trichloropropane BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.000911,2,4-Trichlorobenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00101,2,4-Trimethylbenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.000851,2-Dibromoethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00111,2-Dichlorobenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00111,2-Dichloroethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00141,2-Dichloropropane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00121,3,5-Trimethylbenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00121,3-Dichlorobenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.000791,3-Dichloropropane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00121,4-Dichlorobenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00122,2-Dichloropropane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00132-Chlorotoluene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00114-Chlorotoluene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00244-Isopropyltoluene 0.21 8260D P9G014310.038 7/9/19 21:19 JLBmg/kg dry 0.0024Acetone BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0015Benzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0013Bromobenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0016Bromochloromethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00090Bromodichloromethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00074Bromoform BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.0047Bromomethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0019Carbon Tetrachloride BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0015Chlorobenzene BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.0018Chloroethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0012Chloroform BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.0029Chloromethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0015cis-1,2-Dichloroethylene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00094cis-1,3-Dichloropropylene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00064Dibromochloromethane BRL 8260D P9G014310.019 7/9/19 21:19 JLBCCVmg/kg dry 0.0027Dichlorodifluoromethane BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0014Ethylbenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0014Isopropyl Ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-9 Prism Sample ID: 9070063-04 Prism Work Order: 9070063 Time Collected: 07/03/19 11:10 Time Submitted: 07/05/19 11:05 BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0011Isopropylbenzene (Cumene) BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.0024m,p-Xylenes BRL 8260D P9G014310.038 7/9/19 21:19 JLBmg/kg dry 0.00066Methyl Butyl Ketone (2-Hexanone) BRL 8260D P9G014310.038 7/9/19 21:19 JLBmg/kg dry 0.0022Methyl Ethyl Ketone (2-Butanone) BRL 8260D P9G014310.038 7/9/19 21:19 JLBmg/kg dry 0.00078Methyl Isobutyl Ketone BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0015Methylene Chloride BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0013Methyl-tert-Butyl Ether BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.00096Naphthalene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00089n-Butylbenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0014n-Propylbenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0010o-Xylene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0010sec-Butylbenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00092Styrene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0011tert-Butylbenzene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0017Tetrachloroethylene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0015Toluene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0018trans-1,2-Dichloroethylene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.00081trans-1,3-Dichloropropylene BRL 8260D P9G014310.0095 7/9/19 21:19 JLBmg/kg dry 0.0018Trichloroethylene BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.0026Trichlorofluoromethane BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.0010Vinyl acetate BRL 8260D P9G014310.019 7/9/19 21:19 JLBmg/kg dry 0.0019Vinyl chloride BRL 8260D P9G014310.029 7/9/19 21:19 JLBmg/kg dry 0.0034Xylenes, total Surrogate Recovery Control Limits 70-130102 %4-Bromofluorobenzene 84-123107 %Dibromofluoromethane 76-12995 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-9 Dup Prism Sample ID: 9070063-05 Prism Work Order: 9070063 Time Collected: 07/03/19 11:15 Time Submitted: 07/05/19 11:05 General Chemistry Parameters 83.8 SM2540 G P9G014110.100 7/10/19 9:20 KBS% by Weight 0.100% Solids Semivolatile Organic Compounds by GC/MS BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.141,2,4-Trichlorobenzene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.131,2-Dichlorobenzene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.121,3-Dichlorobenzene BRL 8270E P9G012110.39 7/8/19 22:33 JMVmg/kg dry 0.121,4-Dichlorobenzene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.171-Methylnaphthalene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.172,4,5-Trichlorophenol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.192,4,6-Trichlorophenol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.152,4-Dichlorophenol BRL 8270E P9G012110.39 7/8/19 22:33 JMVmg/kg dry 0.162,4-Dimethylphenol BRL 8270E P9G012111.8 7/8/19 22:33 JMVmg/kg dry 0.462,4-Dinitrophenol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.212,4-Dinitrotoluene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.202,6-Dinitrotoluene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.192-Chloronaphthalene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.152-Chlorophenol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.152-Methylnaphthalene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.152-Methylphenol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.132-Nitrophenol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.163,3’-Dichlorobenzidine BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.173/4-Methylphenol BRL 8270E P9G012111.8 7/8/19 22:33 JMVmg/kg dry 0.434,6-Dinitro-2-methylphenol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.184-Bromophenyl phenyl ether BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.154-Chloro-3-methylphenol BRL 8270E P9G012110.39 7/8/19 22:33 JMVmg/kg dry 0.0954-Chloroaniline BRL 8270E P9G012111.2 7/8/19 22:33 JMVmg/kg dry 0.244-Chlorophenyl phenyl ether BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.194-Nitrophenol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.19Acenaphthene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.21Acenaphthylene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.21Anthracene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.17Azobenzene 0.17 8270E P9G012110.79 7/8/19 22:33 JMVJmg/kg dry 0.17Benzo(a)anthracene 0.18 8270E P9G012110.79 7/8/19 22:33 JMVJmg/kg dry 0.18Benzo(a)pyrene 0.26 8270E P9G012110.79 7/8/19 22:33 JMVJmg/kg dry 0.18Benzo(b)fluoranthene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.15Benzo(g,h,i)perylene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.17Benzo(k)fluoranthene BRL 8270E P9G012112.4 7/8/19 22:33 JMVmg/kg dry 0.65Benzoic Acid BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.15Benzyl alcohol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.15bis(2-Chloroethoxy)methane BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.13Bis(2-Chloroethyl)ether BRL 8270E P9G012110.39 7/8/19 22:33 JMVmg/kg dry 0.14Bis(2-chloroisopropyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-9 Dup Prism Sample ID: 9070063-05 Prism Work Order: 9070063 Time Collected: 07/03/19 11:15 Time Submitted: 07/05/19 11:05 BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.18Bis(2-Ethylhexyl)phthalate BRL 8270E P9G012110.39 7/8/19 22:33 JMVmg/kg dry 0.14Butyl benzyl phthalate BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.17Chrysene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.23Dibenzo(a,h)anthracene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.21Dibenzofuran BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.20Diethyl phthalate BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.19Dimethyl phthalate BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.20Di-n-butyl phthalate BRL 8270E P9G012110.39 7/8/19 22:33 JMVmg/kg dry 0.20Di-n-octyl phthalate 0.24 8270E P9G012110.79 7/8/19 22:33 JMVJmg/kg dry 0.20Fluoranthene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.24Fluorene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.17Hexachlorobenzene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.18Hexachlorobutadiene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.27Hexachlorocyclopentadiene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.12Hexachloroethane BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.14Indeno(1,2,3-cd)pyrene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.17Isophorone BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.16Naphthalene BRL 8270E P9G012110.39 7/8/19 22:33 JMVmg/kg dry 0.17Nitrobenzene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.18N-Nitroso-di-n-propylamine BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.22N-Nitrosodiphenylamine BRL 8270E P9G012111.2 7/8/19 22:33 JMVmg/kg dry 0.50Pentachlorophenol BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.20Phenanthrene BRL 8270E P9G012110.79 7/8/19 22:33 JMVmg/kg dry 0.13Phenol 0.29 8270E P9G012110.79 7/8/19 22:33 JMVJmg/kg dry 0.18Pyrene BRL 8270E P9G012110.39 7/8/19 22:33 JMVmg/kg dry 0.075Pyridine Surrogate Recovery Control Limits 39-13277 %2,4,6-Tribromophenol 44-11569 %2-Fluorobiphenyl 35-11561 %2-Fluorophenol 37-12257 %Nitrobenzene-d5 34-12164 %Phenol-d5 54-12773 %Terphenyl-d14 Total Metals 0.55 7196A P9G012210.48 7/9/19 0:00 BMSmg/kg dry 0.12Hexavalent Chromium 0.045 7471B P9G013110.056 7/9/19 12:29 JABJmg/kg dry 0.019Mercury 3.1 6020B P9G0166101.2 7/12/19 0:52 JABmg/kg dry 0.38Arsenic 91 6020B P9G016610127/12/19 0:52 JABmg/kg dry 0.39Barium 0.29 6020B P9G0166100.58 7/12/19 0:52 JABJmg/kg dry 0.11Cadmium 49 6020B P9G0166101.2 7/12/19 0:52 JABmg/kg dry 0.30Chromium 82 6020B P9G0166101.2 7/12/19 0:52 JABmg/kg dry 0.22Lead 1.8 6020B P9G0166101.2 7/12/19 0:52 JABmg/kg dry 0.31Selenium This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-9 Dup Prism Sample ID: 9070063-05 Prism Work Order: 9070063 Time Collected: 07/03/19 11:15 Time Submitted: 07/05/19 11:05 BRL 6020B P9G0166100.58 7/12/19 0:52 JABmg/kg dry 0.14Silver Volatile Organic Compounds by GC/MS BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000611,1,1,2-Tetrachloroethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000741,1,1-Trichloroethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000371,1,2,2-Tetrachloroethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000541,1,2-Trichloroethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000911,1-Dichloroethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000921,1-Dichloroethylene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000781,1-Dichloropropylene BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.000721,2,3-Trichlorobenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000571,2,3-Trichloropropane BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.000481,2,4-Trichlorobenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000531,2,4-Trimethylbenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000451,2-Dibromoethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000561,2-Dichlorobenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000601,2-Dichloroethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000761,2-Dichloropropane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000631,3,5-Trimethylbenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000631,3-Dichlorobenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000421,3-Dichloropropane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000641,4-Dichlorobenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000632,2-Dichloropropane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000672-Chlorotoluene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.000574-Chlorotoluene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00134-Isopropyltoluene 0.031 8260D P9G014310.020 7/9/19 21:49 JLBmg/kg dry 0.0013Acetone BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00078Benzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00070Bromobenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00083Bromochloromethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00048Bromodichloromethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00039Bromoform BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.0025Bromomethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00099Carbon Tetrachloride BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00079Chlorobenzene BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.00096Chloroethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00062Chloroform BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.0015Chloromethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00079cis-1,2-Dichloroethylene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00050cis-1,3-Dichloropropylene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00034Dibromochloromethane BRL 8260D P9G014310.010 7/9/19 21:49 JLBCCVmg/kg dry 0.0014Dichlorodifluoromethane BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00076Ethylbenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00074Isopropyl Ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-9 Dup Prism Sample ID: 9070063-05 Prism Work Order: 9070063 Time Collected: 07/03/19 11:15 Time Submitted: 07/05/19 11:05 BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00059Isopropylbenzene (Cumene) BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.0013m,p-Xylenes BRL 8260D P9G014310.020 7/9/19 21:49 JLBmg/kg dry 0.00035Methyl Butyl Ketone (2-Hexanone) BRL 8260D P9G014310.020 7/9/19 21:49 JLBmg/kg dry 0.0012Methyl Ethyl Ketone (2-Butanone) BRL 8260D P9G014310.020 7/9/19 21:49 JLBmg/kg dry 0.00041Methyl Isobutyl Ketone BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00081Methylene Chloride BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00070Methyl-tert-Butyl Ether BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.00051Naphthalene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00047n-Butylbenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00073n-Propylbenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00054o-Xylene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00054sec-Butylbenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00049Styrene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00060tert-Butylbenzene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00091Tetrachloroethylene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00080Toluene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00096trans-1,2-Dichloroethylene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00043trans-1,3-Dichloropropylene BRL 8260D P9G014310.0050 7/9/19 21:49 JLBmg/kg dry 0.00098Trichloroethylene BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.0014Trichlorofluoromethane BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.00055Vinyl acetate BRL 8260D P9G014310.010 7/9/19 21:49 JLBmg/kg dry 0.00099Vinyl chloride BRL 8260D P9G014310.015 7/9/19 21:49 JLBmg/kg dry 0.0018Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 84-123110 %Dibromofluoromethane 76-12994 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Solid Client Sample ID: B-10 Prism Sample ID: 9070063-06 Prism Work Order: 9070063 Time Collected: 07/03/19 11:35 Time Submitted: 07/05/19 11:05 General Chemistry Parameters 95.9 SM2540 G P9G014110.100 7/10/19 9:20 KBS% by Weight 0.100% Solids Total Metals 0.29 7196A P9G012210.42 7/9/19 0:00 BMSJmg/kg dry 0.10Hexavalent Chromium 0.065 7471B P9G013110.053 7/9/19 12:33 JABmg/kg dry 0.018Mercury 4.5 6020B P9G0166101.1 7/12/19 0:58 JABmg/kg dry 0.34Arsenic 100 6020B P9G016610117/12/19 0:58 JABmg/kg dry 0.36Barium 1.1 6020B P9G0166100.53 7/12/19 0:58 JABmg/kg dry 0.10Cadmium 57 6020B P9G0166101.1 7/12/19 0:58 JABmg/kg dry 0.27Chromium 220 6020B P9G0166101.1 7/12/19 0:58 JABmg/kg dry 0.20Lead 2.0 6020B P9G0166101.1 7/12/19 0:58 JABmg/kg dry 0.28Selenium 0.18 6020B P9G0166100.53 7/12/19 0:58 JABJmg/kg dry 0.12Silver This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Water Client Sample ID: Field Blank Prism Sample ID: 9070063-07 Prism Work Order: 9070063 Time Collected: 07/03/19 10:00 Time Submitted: 07/05/19 11:05 Semivolatile Organic Compounds by GC/MS BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.61,2,4-Trichlorobenzene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 2.91,2-Dichlorobenzene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.71,3-Dichlorobenzene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 5.01,4-Dichlorobenzene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.31-Methylnaphthalene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 4.42,4,5-Trichlorophenol BRL 8270E P9G01121247/9/19 22:07 JMVug/L 5.42,4,6-Trichlorophenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.22,4-Dichlorophenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 5.92,4-Dimethylphenol BRL 8270E P9G01121607/9/19 22:07 JMVug/L 142,4-Dinitrophenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 5.02,4-Dinitrotoluene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 4.72,6-Dinitrotoluene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 5.62-Chloronaphthalene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.32-Chlorophenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 5.12-Methylnaphthalene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 2.92-Methylphenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.92-Nitroaniline BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.12-Nitrophenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.73,3’-Dichlorobenzidine BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.03/4-Methylphenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.53-Nitroaniline BRL 8270E P9G01121607/9/19 22:07 JMVug/L 144,6-Dinitro-2-methylphenol BRL 8270E P9G01121247/9/19 22:07 JMVug/L 5.34-Bromophenyl phenyl ether BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.54-Chloro-3-methylphenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.24-Chloroaniline BRL 8270E P9G01121247/9/19 22:07 JMVug/L 5.64-Chlorophenyl phenyl ether BRL 8270E P9G01121127/9/19 22:07 JMVug/L 5.04-Nitroaniline BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.14-Nitrophenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 5.1Acenaphthene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 5.3Acenaphthylene BRL 8270E P9G01121607/9/19 22:07 JMVug/L 14Aniline BRL 8270E P9G01121127/9/19 22:07 JMVug/L 5.5Anthracene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.9Azobenzene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.8Benzo(a)anthracene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.2Benzo(a)pyrene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.2Benzo(b)fluoranthene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.3Benzo(g,h,i)perylene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.2Benzo(k)fluoranthene BRL 8270E P9G011211207/9/19 22:07 JMVug/L 23Benzoic Acid BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.0Benzyl alcohol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.6bis(2-Chloroethoxy)methane BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.1Bis(2-Chloroethyl)ether This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Water Client Sample ID: Field Blank Prism Sample ID: 9070063-07 Prism Work Order: 9070063 Time Collected: 07/03/19 10:00 Time Submitted: 07/05/19 11:05 BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.3Bis(2-chloroisopropyl)ether BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.5Bis(2-Ethylhexyl)phthalate BRL 8270E P9G01121127/9/19 22:07 JMVug/LBromochloroacetonitrile BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.5Butyl benzyl phthalate BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.0Chrysene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 6.8Dibenzo(a,h)anthracene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 5.0Dibenzofuran BRL 8270E P9G01121247/9/19 22:07 JMVug/L 5.1Diethyl phthalate BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.9Dimethyl phthalate BRL 8270E P9G01121127/9/19 22:07 JMVug/L 5.2Di-n-butyl phthalate BRL 8270E P9G01121127/9/19 22:07 JMVug/L 5.4Di-n-octyl phthalate BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.9Fluoranthene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 6.0Fluorene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 4.7Hexachlorobenzene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 5.4Hexachlorobutadiene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 8.7Hexachlorocyclopentadiene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.5Hexachloroethane BRL 8270E P9G01121127/9/19 22:07 JMVug/L 3.2Indeno(1,2,3-cd)pyrene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.9Isophorone BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.9Naphthalene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.6Nitrobenzene BRL 8270E P9G01121247/9/19 22:07 JMVug/L 3.9N-Nitroso-di-n-propylamine BRL 8270E P9G01121247/9/19 22:07 JMVug/L 5.3N-Nitrosodiphenylamine BRL 8270E P9G01121607/9/19 22:07 JMVug/L 13Pentachlorophenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.7Phenanthrene BRL 8270E P9G01121127/9/19 22:07 JMVug/L 1.7Phenol BRL 8270E P9G01121127/9/19 22:07 JMVug/L 4.2Pyrene Surrogate Recovery Control Limits 43-140110 %2,4,6-Tribromophenol 44-119100 %2-Fluorobiphenyl 19-11971 %2-Fluorophenol 44-12091 %Nitrobenzene-d5 11-5249 %Phenol-d5 50-134120 %Terphenyl-d14 Total Metals BRL SM3500-Cr B P9G010910.010 7/5/19 15:45 BMSHTmg/L 0.0033Hexavalent Chromium BRL 7470A P9G016710.00050 7/11/19 12:39 JABmg/L 0.00016Mercury BRL 6020B P9G015011.0 7/11/19 21:01 JABug/L 0.34Arsenic BRL 6020B P9G01501107/11/19 21:01 JABug/L 3.2Barium BRL 6020B P9G015011.0 7/11/19 21:01 JABug/L 0.22Cadmium BRL 6020B P9G015013.0 7/11/19 21:01 JABug/L 0.90Chromium BRL 6020B P9G015011.0 7/11/19 21:01 JABug/L 0.44Lead BRL 6020B P9G015015.0 7/11/19 21:01 JABug/L 0.98Selenium This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Water Client Sample ID: Field Blank Prism Sample ID: 9070063-07 Prism Work Order: 9070063 Time Collected: 07/03/19 10:00 Time Submitted: 07/05/19 11:05 BRL 6020B P9G015011.0 7/11/19 21:01 JABug/L 0.34Silver Volatile Organic Compounds by GC/MS BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0611,1,1-Trichloroethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0661,1,2-Trichloroethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0831,1-Dichloroethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMCCVug/L 0.0831,1-Dichloroethylene BRL 8260D P9G012410.50 7/8/19 19:19 KDMCCVug/L 0.0511,1-Dichloropropylene BRL 8260D P9G012412.0 7/8/19 19:19 KDMug/L 0.401,2,3-Trichlorobenzene BRL 8260D P9G012411.0 7/8/19 19:19 KDMug/L 0.141,2,3-Trichloropropane BRL 8260D P9G012411.0 7/8/19 19:19 KDMug/L 0.131,2,4-Trichlorobenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0541,2,4-Trimethylbenzene BRL 8260D P9G012412.0 7/8/19 19:19 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0511,2-Dibromoethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0761,2-Dichlorobenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0661,2-Dichloroethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.111,2-Dichloropropane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0761,3,5-Trimethylbenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0541,3-Dichlorobenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0431,3-Dichloropropane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0501,4-Dichlorobenzene BRL 8260D P9G012412.0 7/8/19 19:19 KDMug/L 0.112,2-Dichloropropane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0662-Chlorotoluene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0504-Chlorotoluene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.0894-Isopropyltoluene 14 8260D P9G012415.0 7/8/19 19:19 KDMug/L 0.31Acetone BRL 8260D P9G01241207/8/19 19:19 KDMug/L 0.20Acrolein BRL 8260D P9G01241207/8/19 19:19 KDMug/L 0.20Acrylonitrile BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.048Benzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.057Bromobenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.14Bromochloromethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.062Bromodichloromethane BRL 8260D P9G012411.0 7/8/19 19:19 KDMug/L 0.040Bromoform BRL 8260D P9G012411.0 7/8/19 19:19 KDMug/L 0.18Bromomethane BRL 8260D P9G012415.0 7/8/19 19:19 KDMug/L 0.075Carbon disulfide BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.11Carbon Tetrachloride BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.062Chlorobenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.22Chloroethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.076Chloroform BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.079Chloromethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.056cis-1,2-Dichloroethylene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.079cis-1,3-Dichloropropylene This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Water Client Sample ID: Field Blank Prism Sample ID: 9070063-07 Prism Work Order: 9070063 Time Collected: 07/03/19 10:00 Time Submitted: 07/05/19 11:05 BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.081Dibromochloromethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.065Dibromomethane BRL 8260D P9G012415.0 7/8/19 19:19 KDMug/L 0.11Dichlorodifluoromethane BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.061Ethylbenzene BRL 8260D P9G012412.0 7/8/19 19:19 KDMug/L 0.16Hexachlorobutadiene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.050Isopropyl Ether BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.054Isopropylbenzene (Cumene) BRL 8260D P9G012411.0 7/8/19 19:19 KDMug/L 0.12m,p-Xylenes BRL 8260D P9G012415.0 7/8/19 19:19 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL 8260D P9G012415.0 7/8/19 19:19 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL 8260D P9G012415.0 7/8/19 19:19 KDMug/L 0.078Methyl Isobutyl Ketone BRL 8260D P9G012411.0 7/8/19 19:19 KDMug/L 0.083Methylene Chloride BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.042Methyl-tert-Butyl Ether BRL 8260D P9G012411.0 7/8/19 19:19 KDMug/L 0.19Naphthalene BRL 8260D P9G012411.0 7/8/19 19:19 KDMug/L 0.076n-Butylbenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.087n-Propylbenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.044o-Xylene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.076sec-Butylbenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.047Styrene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.088tert-Butylbenzene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.098Tetrachloroethylene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.044Toluene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.094trans-1,2-Dichloroethylene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.070trans-1,3-Dichloropropylene BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.078Trichloroethylene BRL 8260D P9G012410.50 7/8/19 19:19 KDMCCVug/L 0.062Trichlorofluoromethane BRL 8260D P9G012412.0 7/8/19 19:19 KDMug/L 0.060Vinyl acetate BRL 8260D P9G012410.50 7/8/19 19:19 KDMug/L 0.097Vinyl chloride BRL 8260D P9G012411.5 7/8/19 19:19 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 80-124102 %4-Bromofluorobenzene 75-12993 %Dibromofluoromethane 77-12392 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Water Client Sample ID: Trip Blank Prism Sample ID: 9070063-08 Prism Work Order: 9070063 Time Collected: 07/03/19 00:00 Time Submitted: 07/05/19 11:05 Volatile Organic Compounds by GC/MS BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0611,1,1-Trichloroethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0661,1,2-Trichloroethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0831,1-Dichloroethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMCCVug/L 0.0831,1-Dichloroethylene BRL 8260D P9G012410.50 7/8/19 19:45 KDMCCVug/L 0.0511,1-Dichloropropylene BRL 8260D P9G012412.0 7/8/19 19:45 KDMug/L 0.401,2,3-Trichlorobenzene BRL 8260D P9G012411.0 7/8/19 19:45 KDMug/L 0.141,2,3-Trichloropropane BRL 8260D P9G012411.0 7/8/19 19:45 KDMug/L 0.131,2,4-Trichlorobenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0541,2,4-Trimethylbenzene BRL 8260D P9G012412.0 7/8/19 19:45 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0511,2-Dibromoethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0761,2-Dichlorobenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0661,2-Dichloroethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.111,2-Dichloropropane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0761,3,5-Trimethylbenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0541,3-Dichlorobenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0431,3-Dichloropropane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0501,4-Dichlorobenzene BRL 8260D P9G012412.0 7/8/19 19:45 KDMug/L 0.112,2-Dichloropropane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0662-Chlorotoluene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0504-Chlorotoluene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.0894-Isopropyltoluene 4.0 8260D P9G012415.0 7/8/19 19:45 KDMJug/L 0.31Acetone BRL 8260D P9G01241207/8/19 19:45 KDMug/L 0.20Acrolein BRL 8260D P9G01241207/8/19 19:45 KDMug/L 0.20Acrylonitrile BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.048Benzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.057Bromobenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.14Bromochloromethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.062Bromodichloromethane BRL 8260D P9G012411.0 7/8/19 19:45 KDMug/L 0.040Bromoform BRL 8260D P9G012411.0 7/8/19 19:45 KDMug/L 0.18Bromomethane BRL 8260D P9G012415.0 7/8/19 19:45 KDMug/L 0.075Carbon disulfide BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.11Carbon Tetrachloride BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.062Chlorobenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.22Chloroethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.076Chloroform BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.079Chloromethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.056cis-1,2-Dichloroethylene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.079cis-1,3-Dichloropropylene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.081Dibromochloromethane This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 of 64 Laboratory Report 07/15/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Sample Matrix: Water Client Sample ID: Trip Blank Prism Sample ID: 9070063-08 Prism Work Order: 9070063 Time Collected: 07/03/19 00:00 Time Submitted: 07/05/19 11:05 BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.065Dibromomethane BRL 8260D P9G012415.0 7/8/19 19:45 KDMug/L 0.11Dichlorodifluoromethane BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.061Ethylbenzene BRL 8260D P9G012412.0 7/8/19 19:45 KDMug/L 0.16Hexachlorobutadiene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.050Isopropyl Ether BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.054Isopropylbenzene (Cumene) BRL 8260D P9G012411.0 7/8/19 19:45 KDMug/L 0.12m,p-Xylenes BRL 8260D P9G012415.0 7/8/19 19:45 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL 8260D P9G012415.0 7/8/19 19:45 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL 8260D P9G012415.0 7/8/19 19:45 KDMug/L 0.078Methyl Isobutyl Ketone BRL 8260D P9G012411.0 7/8/19 19:45 KDMug/L 0.083Methylene Chloride BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.042Methyl-tert-Butyl Ether BRL 8260D P9G012411.0 7/8/19 19:45 KDMug/L 0.19Naphthalene BRL 8260D P9G012411.0 7/8/19 19:45 KDMug/L 0.076n-Butylbenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.087n-Propylbenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.044o-Xylene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.076sec-Butylbenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.047Styrene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.088tert-Butylbenzene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.098Tetrachloroethylene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.044Toluene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.094trans-1,2-Dichloroethylene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.070trans-1,3-Dichloropropylene BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.078Trichloroethylene BRL 8260D P9G012410.50 7/8/19 19:45 KDMCCVug/L 0.062Trichlorofluoromethane BRL 8260D P9G012412.0 7/8/19 19:45 KDMug/L 0.060Vinyl acetate BRL 8260D P9G012410.50 7/8/19 19:45 KDMug/L 0.097Vinyl chloride BRL 8260D P9G012411.5 7/8/19 19:45 KDMug/L 0.15Xylenes, total Surrogate Recovery Control Limits 80-124100 %4-Bromofluorobenzene 75-129100 %Dibromofluoromethane 77-12395 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0124 - 5030B Blank (P9G0124-BLK1)Prepared & Analyzed: 07/08/19 1,1,1,2-Tetrachloroethane ug/LBRL0.50 1,1,1-Trichloroethane ug/LBRL0.50 1,1,2,2-Tetrachloroethane ug/LBRL0.50 1,1,2-Trichloroethane ug/LBRL0.50 1,1-Dichloroethane ug/LBRL0.50 1,1-Dichloroethylene ug/LBRL0.50 1,1-Dichloropropylene ug/LBRL0.50 1,2,3-Trichlorobenzene ug/LBRL2.0 1,2,3-Trichloropropane ug/LBRL1.0 1,2,4-Trichlorobenzene ug/LBRL1.0 1,2,4-Trimethylbenzene ug/LBRL0.50 1,2-Dibromo-3-chloropropane ug/LBRL2.0 1,2-Dibromoethane ug/LBRL0.50 1,2-Dichlorobenzene ug/LBRL0.50 1,2-Dichloroethane ug/LBRL0.50 1,2-Dichloropropane ug/LBRL0.50 1,3,5-Trimethylbenzene ug/LBRL0.50 1,3-Dichlorobenzene ug/LBRL0.50 1,3-Dichloropropane ug/LBRL0.50 1,4-Dichlorobenzene ug/LBRL0.50 2,2-Dichloropropane ug/LBRL2.0 2-Chlorotoluene ug/LBRL0.50 4-Chlorotoluene ug/LBRL0.50 4-Isopropyltoluene ug/LBRL0.50 Acetone ug/LBRL5.0 Acrolein ug/LBRL20 Acrylonitrile ug/LBRL20 Benzene ug/LBRL0.50 Bromobenzene ug/LBRL0.50 Bromochloromethane ug/LBRL0.50 Bromodichloromethane ug/LBRL0.50 Bromoform ug/LBRL1.0 Bromomethane ug/LBRL1.0 Carbon disulfide ug/LBRL5.0 Carbon Tetrachloride ug/LBRL0.50 Chlorobenzene ug/LBRL0.50 Chloroethane ug/LBRL0.50 Chloroform ug/LBRL0.50 Chloromethane ug/LBRL0.50 cis-1,2-Dichloroethylene ug/LBRL0.50 cis-1,3-Dichloropropylene ug/LBRL0.50 Dibromochloromethane ug/LBRL0.50 Dibromomethane ug/LBRL0.50 Dichlorodifluoromethane ug/LBRL5.0 Ethylbenzene ug/LBRL0.50 Hexachlorobutadiene ug/LBRL2.0 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0124 - 5030B Blank (P9G0124-BLK1)Prepared & Analyzed: 07/08/19 Isopropyl Ether ug/LBRL0.50 Isopropylbenzene (Cumene)ug/LBRL0.50 m,p-Xylenes ug/LBRL1.0 Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0 Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0 Methyl Isobutyl Ketone ug/LBRL5.0 Methylene Chloride ug/LBRL1.0 Methyl-tert-Butyl Ether ug/LBRL0.50 Naphthalene ug/LBRL1.0 n-Butylbenzene ug/LBRL1.0 n-Propylbenzene ug/LBRL0.50 o-Xylene ug/LBRL0.50 sec-Butylbenzene ug/LBRL0.50 Styrene ug/LBRL0.50 tert-Butylbenzene ug/LBRL0.50 Tetrachloroethylene ug/LBRL0.50 Toluene ug/LBRL0.50 trans-1,2-Dichloroethylene ug/LBRL0.50 trans-1,3-Dichloropropylene ug/LBRL0.50 Trichloroethylene ug/LBRL0.50 Trichlorofluoromethane ug/LBRL0.50 Vinyl acetate ug/LBRL2.0 Vinyl chloride ug/LBRL0.50 Xylenes, total ug/LBRL1.5 Heptane ug/L0.00 ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10250.8 ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9748.6 ug/L 50.00 77-123Surrogate: Toluene-d8 9145.5 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 35 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0124 - 5030B LCS (P9G0124-BS1)Prepared & Analyzed: 07/08/19 1,1,1,2-Tetrachloroethane ug/L21.0 0.50 20.00 79-134105 1,1,1-Trichloroethane ug/L24.0 0.50 20.00 75-136120 1,1,2,2-Tetrachloroethane ug/L19.8 0.50 20.00 62-12799 1,1,2-Trichloroethane ug/L21.4 0.50 20.00 70-140107 1,1-Dichloroethane ug/L24.2 0.50 20.00 78-130121 1,1-Dichloroethylene ug/L23.8 0.50 20.00 70-154119 1,1-Dichloropropylene ug/L22.4 0.50 20.00 71-136112 1,2,3-Trichlorobenzene ug/L18.7 2.0 20.00 58-14494 1,2,3-Trichloropropane ug/L19.8 1.0 20.00 71-12799 1,2,4-Trichlorobenzene ug/L18.9 1.0 20.00 66-13995 1,2,4-Trimethylbenzene ug/L19.8 0.50 20.00 75-13399 1,2-Dibromo-3-chloropropane ug/L19.0 2.0 20.00 63-13495 1,2-Dibromoethane ug/L20.7 0.50 20.00 77-135103 1,2-Dichlorobenzene ug/L19.4 0.50 20.00 78-12897 1,2-Dichloroethane ug/L23.6 0.50 20.00 68-131118 1,2-Dichloropropane ug/L23.6 0.50 20.00 77-130118 1,3,5-Trimethylbenzene ug/L19.9 0.50 20.00 75-13199 1,3-Dichlorobenzene ug/L18.8 0.50 20.00 77-12594 1,3-Dichloropropane ug/L21.8 0.50 20.00 76-132109 1,4-Dichlorobenzene ug/L19.5 0.50 20.00 75-12698 2,2-Dichloropropane ug/L24.4 2.0 20.00 29-149122 2-Chlorotoluene ug/L19.2 0.50 20.00 74-12696 4-Chlorotoluene ug/L19.2 0.50 20.00 78-12996 4-Isopropyltoluene ug/L19.7 0.50 20.00 69-13299 Acetone ug/L48.1 5.0 40.00 40-166120 Acrolein ug/L39.7 20 40.00 70-13099 Acrylonitrile ug/L47.6 20 40.00 81-127119 Benzene ug/L23.6 0.50 20.00 77-128118 Bromobenzene ug/L20.3 0.50 20.00 78-129101 Bromochloromethane ug/L23.6 0.50 20.00 78-135118 Bromodichloromethane ug/L22.7 0.50 20.00 76-138114 Bromoform ug/L20.0 1.0 20.00 71-135100 Bromomethane ug/L18.5 1.0 20.00 41-16893 Carbon disulfide ug/L24.6 5.0 20.00 59-135123 Carbon Tetrachloride ug/L22.2 0.50 20.00 72-142111 Chlorobenzene ug/L20.8 0.50 20.00 78-119104 Chloroethane ug/L21.4 0.50 20.00 57-142107 Chloroform ug/L23.2 0.50 20.00 77-130116 Chloromethane ug/L16.8 0.50 20.00 47-14584 cis-1,2-Dichloroethylene ug/L23.2 0.50 20.00 76-141116 cis-1,3-Dichloropropylene ug/L23.3 0.50 20.00 65-140117 Dibromochloromethane ug/L19.9 0.50 20.00 75-13499 Dibromomethane ug/L22.4 0.50 20.00 76-138112 Dichlorodifluoromethane ug/L16.5 5.0 20.00 28-16383 Ethylbenzene ug/L21.7 0.50 20.00 80-127109 Hexachlorobutadiene ug/L18.2 2.0 20.00 61-13491 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 36 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0124 - 5030B LCS (P9G0124-BS1)Prepared & Analyzed: 07/08/19 Isopropyl Ether ug/L22.6 0.50 20.00 60-154113 Isopropylbenzene (Cumene)ug/L19.6 0.50 20.00 70-13098 m,p-Xylenes ug/L42.8 1.0 40.00 77-133107 Methyl Butyl Ketone (2-Hexanone)ug/L20.7 5.0 20.00 64-137103 Methyl Ethyl Ketone (2-Butanone)ug/L23.8 5.0 20.00 71-134119 Methyl Isobutyl Ketone ug/L22.1 5.0 20.00 69-134111 Methylene Chloride ug/L23.4 1.0 20.00 73-131117 Methyl-tert-Butyl Ether ug/L24.3 0.50 20.00 68-135122 Naphthalene ug/L17.8 1.0 20.00 64-13689 n-Butylbenzene ug/L20.2 1.0 20.00 68-134101 n-Propylbenzene ug/L20.0 0.50 20.00 72-132100 o-Xylene ug/L21.0 0.50 20.00 78-128105 sec-Butylbenzene ug/L20.3 0.50 20.00 71-131102 Styrene ug/L20.2 0.50 20.00 78-129101 tert-Butylbenzene ug/L20.0 0.50 20.00 70-132100 Tetrachloroethylene ug/L22.0 0.50 20.00 80-129110 Toluene ug/L23.6 0.50 20.00 76-131118 trans-1,2-Dichloroethylene ug/L24.2 0.50 20.00 76-135121 trans-1,3-Dichloropropylene ug/L23.5 0.50 20.00 67-140118 Trichloroethylene ug/L23.8 0.50 20.00 77-133119 Trichlorofluoromethane ug/L23.4 0.50 20.00 62-148117 Vinyl acetate ug/L23.2 2.0 20.00 34-167116 Vinyl chloride ug/L20.5 0.50 20.00 57-141102 Xylenes, total ug/L63.8 1.5 60.00 77-133106 ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10049.8 ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9849.0 ug/L 50.00 77-123Surrogate: Toluene-d8 9447.0 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0124 - 5030B LCS Dup (P9G0124-BSD1)Prepared & Analyzed: 07/08/19 1,1,1,2-Tetrachloroethane ug/L21.8 0.50 20.00 2079-134109 4 1,1,1-Trichloroethane ug/L23.2 0.50 20.00 2075-136116 3 1,1,2,2-Tetrachloroethane ug/L20.8 0.50 20.00 2062-127104 5 1,1,2-Trichloroethane ug/L21.4 0.50 20.00 2070-140107 0.2 1,1-Dichloroethane ug/L24.0 0.50 20.00 2078-130120 0.9 1,1-Dichloroethylene ug/L23.4 0.50 20.00 2070-154117 1 1,1-Dichloropropylene ug/L22.6 0.50 20.00 2071-136113 1 1,2,3-Trichlorobenzene ug/L19.2 2.0 20.00 2058-14496 3 1,2,3-Trichloropropane ug/L21.6 1.0 20.00 2071-127108 9 1,2,4-Trichlorobenzene ug/L19.6 1.0 20.00 2066-13998 4 1,2,4-Trimethylbenzene ug/L20.5 0.50 20.00 2075-133102 3 1,2-Dibromo-3-chloropropane ug/L18.9 2.0 20.00 2063-13494 0.4 1,2-Dibromoethane ug/L21.2 0.50 20.00 2077-135106 3 1,2-Dichlorobenzene ug/L20.4 0.50 20.00 2078-128102 5 1,2-Dichloroethane ug/L24.1 0.50 20.00 2068-131121 2 1,2-Dichloropropane ug/L23.3 0.50 20.00 2077-130117 1 1,3,5-Trimethylbenzene ug/L20.6 0.50 20.00 2075-131103 4 1,3-Dichlorobenzene ug/L20.3 0.50 20.00 2077-125102 8 1,3-Dichloropropane ug/L22.3 0.50 20.00 2076-132112 2 1,4-Dichlorobenzene ug/L20.4 0.50 20.00 2075-126102 4 2,2-Dichloropropane ug/L24.2 2.0 20.00 2029-149121 0.6 2-Chlorotoluene ug/L19.9 0.50 20.00 2074-12699 3 4-Chlorotoluene ug/L20.1 0.50 20.00 2078-129100 5 4-Isopropyltoluene ug/L20.7 0.50 20.00 2069-132104 5 Acetone ug/L49.8 5.0 40.00 2040-166124 4 Acrolein ug/L41.0 20 40.00 2070-130102 3 Acrylonitrile ug/L48.0 20 40.00 2081-127120 0.9 Benzene ug/L23.5 0.50 20.00 2077-128117 0.4 Bromobenzene ug/L21.4 0.50 20.00 2078-129107 6 Bromochloromethane ug/L23.2 0.50 20.00 2078-135116 2 Bromodichloromethane ug/L22.8 0.50 20.00 2076-138114 0.6 Bromoform ug/L20.4 1.0 20.00 2071-135102 2 Bromomethane ug/L19.8 1.0 20.00 2041-16899 7 Carbon disulfide ug/L24.2 5.0 20.00 2059-135121 2 Carbon Tetrachloride ug/L21.8 0.50 20.00 2072-142109 2 Chlorobenzene ug/L21.1 0.50 20.00 2078-119106 2 Chloroethane ug/L21.3 0.50 20.00 2057-142106 0.3 Chloroform ug/L23.4 0.50 20.00 2077-130117 0.8 Chloromethane ug/L16.2 0.50 20.00 2047-14581 3 cis-1,2-Dichloroethylene ug/L23.3 0.50 20.00 2076-141117 0.8 cis-1,3-Dichloropropylene ug/L23.6 0.50 20.00 2065-140118 1 Dibromochloromethane ug/L20.3 0.50 20.00 2075-134102 2 Dibromomethane ug/L23.0 0.50 20.00 2076-138115 3 Dichlorodifluoromethane ug/L16.4 5.0 20.00 2028-16382 1 Ethylbenzene ug/L21.4 0.50 20.00 2080-127107 1 Hexachlorobutadiene ug/L19.2 2.0 20.00 2061-13496 5 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0124 - 5030B LCS Dup (P9G0124-BSD1)Prepared & Analyzed: 07/08/19 Isopropyl Ether ug/L22.4 0.50 20.00 2060-154112 0.4 Isopropylbenzene (Cumene)ug/L20.3 0.50 20.00 2070-130102 4 m,p-Xylenes ug/L43.2 1.0 40.00 2077-133108 0.9 Methyl Butyl Ketone (2-Hexanone)ug/L21.2 5.0 20.00 2064-137106 3 Methyl Ethyl Ketone (2-Butanone)ug/L23.3 5.0 20.00 2071-134117 2 Methyl Isobutyl Ketone ug/L23.2 5.0 20.00 2069-134116 5 Methylene Chloride ug/L23.7 1.0 20.00 2073-131119 1 Methyl-tert-Butyl Ether ug/L24.6 0.50 20.00 2068-135123 1 Naphthalene ug/L18.8 1.0 20.00 2064-13694 6 n-Butylbenzene ug/L20.5 1.0 20.00 2068-134103 2 n-Propylbenzene ug/L20.9 0.50 20.00 2072-132104 5 o-Xylene ug/L21.5 0.50 20.00 2078-128108 2 sec-Butylbenzene ug/L21.1 0.50 20.00 2071-131105 3 Styrene ug/L20.6 0.50 20.00 2078-129103 2 tert-Butylbenzene ug/L20.4 0.50 20.00 2070-132102 2 Tetrachloroethylene ug/L22.8 0.50 20.00 2080-129114 4 Toluene ug/L23.4 0.50 20.00 2076-131117 0.8 trans-1,2-Dichloroethylene ug/L24.1 0.50 20.00 2076-135121 0.2 trans-1,3-Dichloropropylene ug/L24.2 0.50 20.00 2067-140121 3 Trichloroethylene ug/L23.7 0.50 20.00 2077-133118 0.4 Trichlorofluoromethane ug/L22.9 0.50 20.00 2062-148114 2 Vinyl acetate ug/L23.5 2.0 20.00 2034-167118 1 Vinyl chloride ug/L20.5 0.50 20.00 2057-141102 0.05 Xylenes, total ug/L64.6 1.5 60.00 2077-133108 1 ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9748.5 ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9547.4 ug/L 50.00 77-123Surrogate: Toluene-d8 9346.7 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 39 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0143 - 5035 Blank (P9G0143-BLK1)Prepared & Analyzed: 07/09/19 1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050 1,1,1-Trichloroethane mg/kg wetBRL0.0050 1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050 1,1,2-Trichloroethane mg/kg wetBRL0.0050 1,1-Dichloroethane mg/kg wetBRL0.0050 1,1-Dichloroethylene mg/kg wetBRL0.0050 1,1-Dichloropropylene mg/kg wetBRL0.0050 1,2,3-Trichlorobenzene mg/kg wetBRL0.010 1,2,3-Trichloropropane mg/kg wetBRL0.0050 1,2,4-Trichlorobenzene mg/kg wetBRL0.010 1,2,4-Trimethylbenzene mg/kg wetBRL0.0050 1,2-Dibromoethane mg/kg wetBRL0.0050 1,2-Dichlorobenzene mg/kg wetBRL0.0050 1,2-Dichloroethane mg/kg wetBRL0.0050 1,2-Dichloropropane mg/kg wetBRL0.0050 1,3,5-Trimethylbenzene mg/kg wetBRL0.0050 1,3-Dichlorobenzene mg/kg wetBRL0.0050 1,3-Dichloropropane mg/kg wetBRL0.0050 1,4-Dichlorobenzene mg/kg wetBRL0.0050 2,2-Dichloropropane mg/kg wetBRL0.0050 2-Chlorotoluene mg/kg wetBRL0.0050 4-Chlorotoluene mg/kg wetBRL0.0050 4-Isopropyltoluene mg/kg wetBRL0.0050 Acetone mg/kg wetBRL0.020 Benzene mg/kg wetBRL0.0050 Bromobenzene mg/kg wetBRL0.0050 Bromochloromethane mg/kg wetBRL0.0050 Bromodichloromethane mg/kg wetBRL0.0050 Bromoform mg/kg wetBRL0.0050 Bromomethane mg/kg wetBRL0.010 Carbon Tetrachloride mg/kg wetBRL0.0050 Chlorobenzene mg/kg wetBRL0.0050 Chloroethane mg/kg wetBRL0.010 Chloroform mg/kg wetBRL0.0050 Chloromethane mg/kg wetBRL0.010 cis-1,2-Dichloroethylene mg/kg wetBRL0.0050 cis-1,3-Dichloropropylene mg/kg wetBRL0.0050 Dibromochloromethane mg/kg wetBRL0.0050 Dichlorodifluoromethane mg/kg wetBRL0.010 Ethylbenzene mg/kg wetBRL0.0050 Isopropyl Ether mg/kg wetBRL0.0050 Isopropylbenzene (Cumene)mg/kg wetBRL0.0050 m,p-Xylenes mg/kg wetBRL0.010 Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.020 Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.020 Methyl Isobutyl Ketone mg/kg wetBRL0.020 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0143 - 5035 Blank (P9G0143-BLK1)Prepared & Analyzed: 07/09/19 Methylene Chloride mg/kg wetBRL0.0050 Methyl-tert-Butyl Ether mg/kg wetBRL0.0050 Naphthalene mg/kg wetBRL0.010 n-Butylbenzene mg/kg wetBRL0.0050 n-Propylbenzene mg/kg wetBRL0.0050 o-Xylene mg/kg wetBRL0.0050 sec-Butylbenzene mg/kg wetBRL0.0050 Styrene mg/kg wetBRL0.0050 tert-Butylbenzene mg/kg wetBRL0.0050 Tetrachloroethylene mg/kg wetBRL0.0050 Toluene mg/kg wetBRL0.0050 trans-1,2-Dichloroethylene mg/kg wetBRL0.0050 trans-1,3-Dichloropropylene mg/kg wetBRL0.0050 Trichloroethylene mg/kg wetBRL0.0050 Trichlorofluoromethane mg/kg wetBRL0.010 Vinyl acetate mg/kg wetBRL0.010 Vinyl chloride mg/kg wetBRL0.010 Xylenes, total mg/kg wetBRL0.015 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.4 ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10351.3 ug/L 50.00 76-129Surrogate: Toluene-d8 9648.1 LCS (P9G0143-BS1)Prepared & Analyzed: 07/09/19 1,1,1,2-Tetrachloroethane mg/kg wet0.0476 0.0050 0.05000 72-11595 1,1,1-Trichloroethane mg/kg wet0.0456 0.0050 0.05000 67-13191 1,1,2,2-Tetrachloroethane mg/kg wet0.0437 0.0050 0.05000 56-12687 1,1,2-Trichloroethane mg/kg wet0.0455 0.0050 0.05000 70-13391 1,1-Dichloroethane mg/kg wet0.0445 0.0050 0.05000 74-12789 1,1-Dichloroethylene mg/kg wet0.0442 0.0050 0.05000 67-14988 1,1-Dichloropropylene mg/kg wet0.0476 0.0050 0.05000 71-13095 1,2,3-Trichlorobenzene mg/kg wet0.0410 0.010 0.05000 68-13082 1,2,3-Trichloropropane mg/kg wet0.0460 0.0050 0.05000 60-13792 1,2,4-Trichlorobenzene mg/kg wet0.0419 0.010 0.05000 66-12584 1,2,4-Trimethylbenzene mg/kg wet0.0434 0.0050 0.05000 69-12987 1,2-Dibromoethane mg/kg wet0.0441 0.0050 0.05000 70-13288 1,2-Dichlorobenzene mg/kg wet0.0417 0.0050 0.05000 72-12383 1,2-Dichloroethane mg/kg wet0.0448 0.0050 0.05000 68-12890 1,2-Dichloropropane mg/kg wet0.0458 0.0050 0.05000 73-13092 1,3,5-Trimethylbenzene mg/kg wet0.0434 0.0050 0.05000 69-12887 1,3-Dichlorobenzene mg/kg wet0.0414 0.0050 0.05000 71-12083 1,3-Dichloropropane mg/kg wet0.0455 0.0050 0.05000 75-12491 1,4-Dichlorobenzene mg/kg wet0.0415 0.0050 0.05000 71-12383 2,2-Dichloropropane mg/kg wet0.0469 0.0050 0.05000 50-14294 2-Chlorotoluene mg/kg wet0.0422 0.0050 0.05000 67-12484 4-Chlorotoluene mg/kg wet0.0422 0.0050 0.05000 71-12684 4-Isopropyltoluene mg/kg wet0.0437 0.0050 0.05000 68-12987 Acetone mg/kg wet0.100 0.020 0.1000 29-198100 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 41 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0143 - 5035 LCS (P9G0143-BS1)Prepared & Analyzed: 07/09/19 Benzene mg/kg wet0.0448 0.0050 0.05000 74-12790 Bromobenzene mg/kg wet0.0422 0.0050 0.05000 73-12584 Bromochloromethane mg/kg wet0.0450 0.0050 0.05000 72-13490 Bromodichloromethane mg/kg wet0.0448 0.0050 0.05000 75-12290 Bromoform mg/kg wet0.0452 0.0050 0.05000 66-13590 Bromomethane mg/kg wet0.0530 0.010 0.05000 20-180106 Carbon Tetrachloride mg/kg wet0.0470 0.0050 0.05000 64-14394 Chlorobenzene mg/kg wet0.0433 0.0050 0.05000 74-11887 Chloroethane mg/kg wet0.0460 0.010 0.05000 33-14992 Chloroform mg/kg wet0.0450 0.0050 0.05000 73-12790 Chloromethane mg/kg wet0.0476 0.010 0.05000 45-14395 cis-1,2-Dichloroethylene mg/kg wet0.0450 0.0050 0.05000 76-13490 cis-1,3-Dichloropropylene mg/kg wet0.0466 0.0050 0.05000 71-12593 Dibromochloromethane mg/kg wet0.0449 0.0050 0.05000 73-12290 Dichlorodifluoromethane mg/kg wet0.0711 0.010 0.05000 26-146142 Ethylbenzene mg/kg wet0.0456 0.0050 0.05000 74-12891 Isopropyl Ether mg/kg wet0.0426 0.0050 0.05000 59-15985 Isopropylbenzene (Cumene)mg/kg wet0.0447 0.0050 0.05000 68-12689 m,p-Xylenes mg/kg wet0.0919 0.010 0.1000 75-12492 Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0481 0.020 0.05000 61-15796 Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0473 0.020 0.05000 63-14995 Methyl Isobutyl Ketone mg/kg wet0.0459 0.020 0.05000 57-16292 Methylene Chloride mg/kg wet0.0436 0.0050 0.05000 74-12987 Methyl-tert-Butyl Ether mg/kg wet0.0463 0.0050 0.05000 70-13093 Naphthalene mg/kg wet0.0432 0.010 0.05000 57-15786 n-Butylbenzene mg/kg wet0.0443 0.0050 0.05000 65-13589 n-Propylbenzene mg/kg wet0.0430 0.0050 0.05000 67-13086 o-Xylene mg/kg wet0.0452 0.0050 0.05000 74-12690 sec-Butylbenzene mg/kg wet0.0440 0.0050 0.05000 66-13188 Styrene mg/kg wet0.0456 0.0050 0.05000 77-12191 tert-Butylbenzene mg/kg wet0.0436 0.0050 0.05000 67-13287 Tetrachloroethylene mg/kg wet0.0463 0.0050 0.05000 68-13093 Toluene mg/kg wet0.0455 0.0050 0.05000 71-12991 trans-1,2-Dichloroethylene mg/kg wet0.0441 0.0050 0.05000 73-13288 trans-1,3-Dichloropropylene mg/kg wet0.0475 0.0050 0.05000 68-12395 Trichloroethylene mg/kg wet0.0445 0.0050 0.05000 75-13389 Trichlorofluoromethane mg/kg wet0.0513 0.010 0.05000 44-146103 Vinyl acetate mg/kg wet0.0511 0.010 0.05000 85-161102 Vinyl chloride mg/kg wet0.0540 0.010 0.05000 48-147108 Xylenes, total mg/kg wet0.137 0.015 0.1500 74-12691 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.8 ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9848.8 ug/L 50.00 76-129Surrogate: Toluene-d8 9848.8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 42 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0143 - 5035 LCS Dup (P9G0143-BSD1)Prepared & Analyzed: 07/09/19 1,1,1,2-Tetrachloroethane mg/kg wet0.0401 0.0050 0.05000 2072-11580 17 1,1,1-Trichloroethane mg/kg wet0.0387 0.0050 0.05000 2067-13177 16 1,1,2,2-Tetrachloroethane mg/kg wet0.0388 0.0050 0.05000 2056-12678 12 1,1,2-Trichloroethane mg/kg wet0.0399 0.0050 0.05000 2070-13380 13 1,1-Dichloroethane mg/kg wet0.0389 0.0050 0.05000 2074-12778 13 1,1-Dichloroethylene mg/kg wet0.0375 0.0050 0.05000 2067-14975 16 1,1-Dichloropropylene mg/kg wet0.0406 0.0050 0.05000 2071-13081 16 1,2,3-Trichlorobenzene mg/kg wet0.0360 0.010 0.05000 2068-13072 13 1,2,3-Trichloropropane mg/kg wet0.0403 0.0050 0.05000 2060-13781 13 1,2,4-Trichlorobenzene mg/kg wet0.0356 0.010 0.05000 2066-12571 16 1,2,4-Trimethylbenzene mg/kg wet0.0366 0.0050 0.05000 2069-12973 17 1,2-Dibromoethane mg/kg wet0.0391 0.0050 0.05000 2070-13278 12 1,2-Dichlorobenzene mg/kg wet0.0360 0.0050 0.05000 2072-12372 15 1,2-Dichloroethane mg/kg wet0.0398 0.0050 0.05000 2068-12880 12 1,2-Dichloropropane mg/kg wet0.0403 0.0050 0.05000 2073-13081 13 1,3,5-Trimethylbenzene mg/kg wet0.0367 0.0050 0.05000 2069-12873 17 1,3-Dichlorobenzene mg/kg wet0.0351 0.0050 0.05000 20 L271-12070 17 1,3-Dichloropropane mg/kg wet0.0399 0.0050 0.05000 2075-12480 13 1,4-Dichlorobenzene mg/kg wet0.0357 0.0050 0.05000 2071-12371 15 2,2-Dichloropropane mg/kg wet0.0398 0.0050 0.05000 2050-14280 16 2-Chlorotoluene mg/kg wet0.0355 0.0050 0.05000 2067-12471 17 4-Chlorotoluene mg/kg wet0.0356 0.0050 0.05000 2071-12671 17 4-Isopropyltoluene mg/kg wet0.0368 0.0050 0.05000 2068-12974 17 Acetone mg/kg wet0.0844 0.020 0.1000 2029-19884 17 Benzene mg/kg wet0.0390 0.0050 0.05000 2074-12778 14 Bromobenzene mg/kg wet0.0360 0.0050 0.05000 20 L273-12572 16 Bromochloromethane mg/kg wet0.0398 0.0050 0.05000 2072-13480 12 Bromodichloromethane mg/kg wet0.0392 0.0050 0.05000 2075-12278 13 Bromoform mg/kg wet0.0398 0.0050 0.05000 2066-13580 13 Bromomethane mg/kg wet0.0479 0.010 0.05000 2020-18096 10 Carbon Tetrachloride mg/kg wet0.0394 0.0050 0.05000 2064-14379 17 Chlorobenzene mg/kg wet0.0373 0.0050 0.05000 2074-11875 15 Chloroethane mg/kg wet0.0386 0.010 0.05000 2033-14977 18 Chloroform mg/kg wet0.0393 0.0050 0.05000 2073-12779 13 Chloromethane mg/kg wet0.0441 0.010 0.05000 2045-14388 8 cis-1,2-Dichloroethylene mg/kg wet0.0394 0.0050 0.05000 2076-13479 13 cis-1,3-Dichloropropylene mg/kg wet0.0421 0.0050 0.05000 2071-12584 10 Dibromochloromethane mg/kg wet0.0388 0.0050 0.05000 2073-12278 15 Dichlorodifluoromethane mg/kg wet0.0596 0.010 0.05000 2026-146119 18 Ethylbenzene mg/kg wet0.0381 0.0050 0.05000 2074-12876 18 Isopropyl Ether mg/kg wet0.0376 0.0050 0.05000 2059-15975 13 Isopropylbenzene (Cumene)mg/kg wet0.0371 0.0050 0.05000 2068-12674 19 m,p-Xylenes mg/kg wet0.0775 0.010 0.1000 2075-12477 17 Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0439 0.020 0.05000 2061-15788 9 Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0436 0.020 0.05000 2063-14987 8 Methyl Isobutyl Ketone mg/kg wet0.0427 0.020 0.05000 2057-16285 7 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 43 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9G0143 - 5035 LCS Dup (P9G0143-BSD1)Prepared & Analyzed: 07/09/19 Methylene Chloride mg/kg wet0.0380 0.0050 0.05000 2074-12976 14 Methyl-tert-Butyl Ether mg/kg wet0.0393 0.0050 0.05000 2070-13079 16 Naphthalene mg/kg wet0.0384 0.010 0.05000 2057-15777 12 n-Butylbenzene mg/kg wet0.0367 0.0050 0.05000 2065-13573 19 n-Propylbenzene mg/kg wet0.0359 0.0050 0.05000 2067-13072 18 o-Xylene mg/kg wet0.0382 0.0050 0.05000 2074-12676 17 sec-Butylbenzene mg/kg wet0.0369 0.0050 0.05000 2066-13174 18 Styrene mg/kg wet0.0390 0.0050 0.05000 2077-12178 16 tert-Butylbenzene mg/kg wet0.0368 0.0050 0.05000 2067-13274 17 Tetrachloroethylene mg/kg wet0.0394 0.0050 0.05000 2068-13079 16 Toluene mg/kg wet0.0391 0.0050 0.05000 2071-12978 15 trans-1,2-Dichloroethylene mg/kg wet0.0385 0.0050 0.05000 2073-13277 14 trans-1,3-Dichloropropylene mg/kg wet0.0421 0.0050 0.05000 2068-12384 12 Trichloroethylene mg/kg wet0.0384 0.0050 0.05000 2075-13377 15 Trichlorofluoromethane mg/kg wet0.0433 0.010 0.05000 2044-14687 17 Vinyl acetate mg/kg wet0.0476 0.010 0.05000 2085-16195 7 Vinyl chloride mg/kg wet0.0467 0.010 0.05000 2048-14793 15 Xylenes, total mg/kg wet0.116 0.015 0.1500 2074-12677 17 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9848.8 ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.3 ug/L 50.00 76-129Surrogate: Toluene-d8 9648.1 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 44 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0112 - 3510C MS Blank (P9G0112-BLK1)Prepared & Analyzed: 07/08/19 1,2,4-Trichlorobenzene ug/LBRL10 1,2-Dichlorobenzene ug/LBRL10 1,3-Dichlorobenzene ug/LBRL10 1,4-Dichlorobenzene ug/LBRL10 1-Methylnaphthalene ug/LBRL10 2,4,5-Trichlorophenol ug/LBRL20 2,4,6-Trichlorophenol ug/LBRL20 2,4-Dichlorophenol ug/LBRL10 2,4-Dimethylphenol ug/LBRL10 2,4-Dinitrophenol ug/LBRL50 2,4-Dinitrotoluene ug/LBRL10 2,6-Dinitrotoluene ug/LBRL20 2-Chloronaphthalene ug/LBRL20 2-Chlorophenol ug/LBRL10 2-Methylnaphthalene ug/LBRL10 2-Methylphenol ug/LBRL10 2-Nitroaniline ug/LBRL10 2-Nitrophenol ug/LBRL10 3,3’-Dichlorobenzidine ug/LBRL10 3/4-Methylphenol ug/LBRL10 3-Nitroaniline ug/LBRL10 4,6-Dinitro-2-methylphenol ug/LBRL50 4-Bromophenyl phenyl ether ug/LBRL20 4-Chloro-3-methylphenol ug/LBRL10 4-Chloroaniline ug/LBRL10 4-Chlorophenyl phenyl ether ug/LBRL20 4-Nitroaniline ug/LBRL10 4-Nitrophenol ug/LBRL10 Acenaphthene ug/LBRL10 Acenaphthylene ug/LBRL20 Aniline ug/LBRL50 Anthracene ug/LBRL10 Azobenzene ug/LBRL10 Benzo(a)anthracene ug/LBRL10 Benzo(a)pyrene ug/LBRL10 Benzo(b)fluoranthene ug/LBRL10 Benzo(g,h,i)perylene ug/LBRL10 Benzo(k)fluoranthene ug/LBRL10 Benzoic Acid ug/LBRL100 Benzyl alcohol ug/LBRL10 bis(2-Chloroethoxy)methane ug/LBRL10 Bis(2-Chloroethyl)ether ug/LBRL10 Bis(2-chloroisopropyl)ether ug/LBRL10 Bis(2-Ethylhexyl)phthalate ug/LBRL10 Bromochloroacetonitrile ug/LBRL10 Butyl benzyl phthalate ug/LBRL10 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 45 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0112 - 3510C MS Blank (P9G0112-BLK1)Prepared & Analyzed: 07/08/19 Chrysene ug/LBRL10 Dibenzo(a,h)anthracene ug/LBRL20 Dibenzofuran ug/LBRL20 Diethyl phthalate ug/LBRL20 Dimethyl phthalate ug/LBRL10 Di-n-butyl phthalate ug/LBRL10 Di-n-octyl phthalate ug/LBRL10 Fluoranthene ug/LBRL10 Fluorene ug/LBRL10 Hexachlorobenzene ug/LBRL20 Hexachlorobutadiene ug/LBRL20 Hexachlorocyclopentadiene ug/LBRL20 Hexachloroethane ug/LBRL10 Indeno(1,2,3-cd)pyrene ug/LBRL10 Isophorone ug/LBRL10 Naphthalene ug/LBRL10 Nitrobenzene ug/LBRL10 N-Nitroso-di-n-propylamine ug/LBRL20 N-Nitrosodiphenylamine ug/LBRL20 Pentachlorophenol ug/LBRL50 Phenanthrene ug/LBRL10 Phenol ug/LBRL10 Pyrene ug/LBRL10 ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 132132 ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 11758.6 ug/L 100.0 19-119Surrogate: 2-Fluorophenol 7777.0 ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 10552.3 ug/L 100.0 11-52Surrogate: Phenol-d5 5151.0 ug/L 50.00 50-134Surrogate: Terphenyl-d14 11858.9 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 46 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0112 - 3510C MS Blank (P9G0112-BLK2)Prepared & Analyzed: 07/08/19 1,2,4-Trichlorobenzene ug/LBRL10 1,2-Dichlorobenzene ug/LBRL10 1,3-Dichlorobenzene ug/LBRL10 1,4-Dichlorobenzene ug/LBRL10 1-Methylnaphthalene ug/LBRL10 2,4,5-Trichlorophenol ug/LBRL20 2,4,6-Trichlorophenol ug/LBRL20 2,4-Dichlorophenol ug/LBRL10 2,4-Dimethylphenol ug/LBRL10 2,4-Dinitrophenol ug/LBRL50 2,4-Dinitrotoluene ug/LBRL10 2,6-Dinitrotoluene ug/LBRL20 2-Chloronaphthalene ug/LBRL20 2-Chlorophenol ug/LBRL10 2-Methylnaphthalene ug/LBRL10 2-Methylphenol ug/LBRL10 2-Nitroaniline ug/LBRL10 2-Nitrophenol ug/LBRL10 3,3’-Dichlorobenzidine ug/LBRL10 3/4-Methylphenol ug/LBRL10 3-Nitroaniline ug/LBRL10 4,6-Dinitro-2-methylphenol ug/LBRL50 4-Bromophenyl phenyl ether ug/LBRL20 4-Chloro-3-methylphenol ug/LBRL10 4-Chloroaniline ug/LBRL10 4-Chlorophenyl phenyl ether ug/LBRL20 4-Nitroaniline ug/LBRL10 4-Nitrophenol ug/LBRL10 Acenaphthene ug/LBRL10 Acenaphthylene ug/LBRL20 Aniline ug/LBRL50 Anthracene ug/LBRL10 Azobenzene ug/LBRL10 Benzo(a)anthracene ug/LBRL10 Benzo(a)pyrene ug/LBRL10 Benzo(b)fluoranthene ug/LBRL10 Benzo(g,h,i)perylene ug/LBRL10 Benzo(k)fluoranthene ug/LBRL10 Benzoic Acid ug/LBRL100 Benzyl alcohol ug/LBRL10 bis(2-Chloroethoxy)methane ug/LBRL10 Bis(2-Chloroethyl)ether ug/LBRL10 Bis(2-chloroisopropyl)ether ug/LBRL10 Bis(2-Ethylhexyl)phthalate ug/LBRL10 Bromochloroacetonitrile ug/LBRL10 Butyl benzyl phthalate ug/LBRL10 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 47 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0112 - 3510C MS Blank (P9G0112-BLK2)Prepared & Analyzed: 07/08/19 Chrysene ug/LBRL10 Dibenzo(a,h)anthracene ug/LBRL20 Dibenzofuran ug/LBRL20 Diethyl phthalate ug/LBRL20 Dimethyl phthalate ug/LBRL10 Di-n-butyl phthalate ug/LBRL10 Di-n-octyl phthalate ug/LBRL10 Fluoranthene ug/LBRL10 Fluorene ug/LBRL10 Hexachlorobenzene ug/LBRL20 Hexachlorobutadiene ug/LBRL20 Hexachlorocyclopentadiene ug/LBRL20 Hexachloroethane ug/LBRL10 Indeno(1,2,3-cd)pyrene ug/LBRL10 Isophorone ug/LBRL10 Naphthalene ug/LBRL10 Nitrobenzene ug/LBRL10 N-Nitroso-di-n-propylamine ug/LBRL20 N-Nitrosodiphenylamine ug/LBRL20 Pentachlorophenol ug/LBRL50 Phenanthrene ug/LBRL10 Phenol ug/LBRL10 Pyrene ug/LBRL10 ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 128128 ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 11055.0 ug/L 100.0 19-119Surrogate: 2-Fluorophenol 6565.4 ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 8542.3 ug/L 100.0 11-52Surrogate: Phenol-d5 4544.5 ug/L 50.00 50-134Surrogate: Terphenyl-d14 11557.7 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 48 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0112 - 3510C MS LCS (P9G0112-BS1)Prepared & Analyzed: 07/08/19 1,2,4-Trichlorobenzene ug/L43.4 10 50.00 29-12687 1,2-Dichlorobenzene ug/L39.8 10 50.00 32-11180 1,3-Dichlorobenzene ug/L37.8 10 50.00 28-11076 1,4-Dichlorobenzene ug/L39.2 10 50.00 29-11278 1-Methylnaphthalene ug/L46.5 10 50.00 41-11993 2,4,5-Trichlorophenol ug/L53.0 20 50.00 53-123106 2,4,6-Trichlorophenol ug/L55.5 20 50.00 50-125111 2,4-Dichlorophenol ug/L48.5 10 50.00 47-12197 2,4-Dimethylphenol ug/L60.2 10 50.00 31-124120 2,4-Dinitrophenol ug/L33.9 50 50.00 J23-14368 2,4-Dinitrotoluene ug/L53.8 10 50.00 57-128108 2,6-Dinitrotoluene ug/L56.2 20 50.00 57-124112 2-Chloronaphthalene ug/L52.1 20 50.00 40-116104 2-Chlorophenol ug/L49.6 10 50.00 38-11799 2-Methylnaphthalene ug/L45.3 10 50.00 40-12191 2-Methylphenol ug/L46.6 10 50.00 30-11793 2-Nitroaniline ug/L53.1 10 50.00 55-127106 2-Nitrophenol ug/L47.7 10 50.00 47-12395 3,3’-Dichlorobenzidine ug/L71.0 10 50.00 LH27-129142 3/4-Methylphenol ug/L37.5 10 50.00 29-11075 3-Nitroaniline ug/L55.0 10 50.00 41-128110 4,6-Dinitro-2-methylphenol ug/L41.9 50 50.00 J44-13784 4-Bromophenyl phenyl ether ug/L55.6 20 50.00 55-124111 4-Chloro-3-methylphenol ug/L48.2 10 50.00 52-11996 4-Chloroaniline ug/L52.8 10 50.00 33-117106 4-Chlorophenyl phenyl ether ug/L57.6 20 50.00 53-121115 4-Nitroaniline ug/L57.0 10 50.00 45-135114 4-Nitrophenol ug/L19.4 10 50.00 10-7739 Acenaphthene ug/L56.7 10 50.00 47-122113 Acenaphthylene ug/L51.4 20 50.00 41-130103 Aniline ug/L54.5 50 50.00 12-197109 Anthracene ug/L58.1 10 50.00 57-123116 Azobenzene ug/L53.2 10 50.00 61-116106 Benzo(a)anthracene ug/L55.4 10 50.00 58-125111 Benzo(a)pyrene ug/L55.7 10 50.00 54-128111 Benzo(b)fluoranthene ug/L64.6 10 50.00 53-131129 Benzo(g,h,i)perylene ug/L70.7 10 50.00 L150-134141 Benzo(k)fluoranthene ug/L69.8 10 50.00 L157-129140 Benzoic Acid ug/LBRL100 50.00 L10-125 Benzyl alcohol ug/L41.7 10 50.00 31-11283 bis(2-Chloroethoxy)methane ug/L50.2 10 50.00 48-120100 Bis(2-Chloroethyl)ether ug/L51.3 10 50.00 43-118103 Bis(2-chloroisopropyl)ether ug/L48.8 10 50.00 37-13098 Bis(2-Ethylhexyl)phthalate ug/L64.3 10 50.00 55-135129 Bromochloroacetonitrile ug/LBRL10 70-130 Butyl benzyl phthalate ug/L55.0 10 50.00 53-134110 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 49 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0112 - 3510C MS LCS (P9G0112-BS1)Prepared & Analyzed: 07/08/19 Chrysene ug/L55.7 10 50.00 59-123111 Dibenzo(a,h)anthracene ug/L39.6 20 50.00 51-13479 Dibenzofuran ug/L54.0 20 50.00 53-118108 Diethyl phthalate ug/L57.8 20 50.00 56-125116 Dimethyl phthalate ug/L55.2 10 50.00 45-127110 Di-n-butyl phthalate ug/L59.8 10 50.00 59-127120 Di-n-octyl phthalate ug/L68.3 10 50.00 51-140137 Fluoranthene ug/L57.0 10 50.00 57-128114 Fluorene ug/L59.4 10 50.00 52-124119 Hexachlorobenzene ug/L54.8 20 50.00 53-125110 Hexachlorobutadiene ug/L44.0 20 50.00 22-12488 Hexachlorocyclopentadiene ug/L35.0 20 50.00 32-11770 Hexachloroethane ug/L35.4 10 50.00 21-11571 Indeno(1,2,3-cd)pyrene ug/L54.6 10 50.00 52-134109 Isophorone ug/L48.8 10 50.00 42-12498 Naphthalene ug/L46.9 10 50.00 40-12194 Nitrobenzene ug/L49.1 10 50.00 45-12198 N-Nitroso-di-n-propylamine ug/L44.6 20 50.00 49-11989 N-Nitrosodiphenylamine ug/L65.5 20 50.00 L151-123131 Pentachlorophenol ug/L61.3 50 50.00 35-138123 Phenanthrene ug/L56.7 10 50.00 59-120113 Phenol ug/L24.5 10 50.00 12-5849 Pyrene ug/L54.4 10 50.00 57-126109 ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 117117 ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 10251.2 ug/L 100.0 19-119Surrogate: 2-Fluorophenol 6565.3 ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 9246.2 ug/L 100.0 11-52Surrogate: Phenol-d5 4343.4 ug/L 50.00 50-134Surrogate: Terphenyl-d14 10351.5 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 50 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0112 - 3510C MS LCS Dup (P9G0112-BSD1)Prepared & Analyzed: 07/08/19 1,2,4-Trichlorobenzene ug/L35.7 10 50.00 2029-12671 19 1,2-Dichlorobenzene ug/L33.6 10 50.00 2032-11167 17 1,3-Dichlorobenzene ug/L33.0 10 50.00 2028-11066 14 1,4-Dichlorobenzene ug/L33.3 10 50.00 2029-11267 16 1-Methylnaphthalene ug/L40.8 10 50.00 2041-11982 13 2,4,5-Trichlorophenol ug/L47.3 20 50.00 2053-12395 11 2,4,6-Trichlorophenol ug/L47.7 20 50.00 2050-12595 15 2,4-Dichlorophenol ug/L41.5 10 50.00 2047-12183 16 2,4-Dimethylphenol ug/L49.8 10 50.00 2031-124100 19 2,4-Dinitrophenol ug/L30.5 50 50.00 20 J23-14361 11 2,4-Dinitrotoluene ug/L49.0 10 50.00 2057-12898 9 2,6-Dinitrotoluene ug/L50.4 20 50.00 2057-124101 11 2-Chloronaphthalene ug/L43.8 20 50.00 2040-11688 17 2-Chlorophenol ug/L41.8 10 50.00 2038-11784 17 2-Methylnaphthalene ug/L38.6 10 50.00 2040-12177 16 2-Methylphenol ug/L41.1 10 50.00 2030-11782 13 2-Nitroaniline ug/L48.0 10 50.00 2055-12796 10 2-Nitrophenol ug/L39.2 10 50.00 2047-12378 20 3,3’-Dichlorobenzidine ug/L65.9 10 50.00 20 LH27-129132 7 3/4-Methylphenol ug/L33.7 10 50.00 2029-11067 11 3-Nitroaniline ug/L49.6 10 50.00 2041-12899 10 4,6-Dinitro-2-methylphenol ug/L39.3 50 50.00 20 J44-13779 6 4-Bromophenyl phenyl ether ug/L49.6 20 50.00 2055-12499 11 4-Chloro-3-methylphenol ug/L45.2 10 50.00 2052-11990 6 4-Chloroaniline ug/L44.6 10 50.00 2033-11789 17 4-Chlorophenyl phenyl ether ug/L49.8 20 50.00 2053-121100 15 4-Nitroaniline ug/L52.8 10 50.00 2045-135106 8 4-Nitrophenol ug/L18.4 10 50.00 2010-7737 5 Acenaphthene ug/L48.6 10 50.00 2047-12297 15 Acenaphthylene ug/L45.0 20 50.00 2041-13090 13 Aniline ug/L46.0 50 50.00 20 J12-19792 17 Anthracene ug/L54.6 10 50.00 2057-123109 6 Azobenzene ug/L49.7 10 50.00 2061-11699 7 Benzo(a)anthracene ug/L51.1 10 50.00 2058-125102 8 Benzo(a)pyrene ug/L50.6 10 50.00 2054-128101 10 Benzo(b)fluoranthene ug/L52.8 10 50.00 20 D53-131106 20 Benzo(g,h,i)perylene ug/L52.7 10 50.00 20 D50-134105 29 Benzo(k)fluoranthene ug/L56.7 10 50.00 20 D57-129113 21 Benzoic Acid ug/LBRL100 50.00 20 L10-125 Benzyl alcohol ug/L36.1 10 50.00 2031-11272 14 bis(2-Chloroethoxy)methane ug/L41.8 10 50.00 2048-12084 18 Bis(2-Chloroethyl)ether ug/L42.6 10 50.00 2043-11885 19 Bis(2-chloroisopropyl)ether ug/L41.7 10 50.00 2037-13083 16 Bis(2-Ethylhexyl)phthalate ug/L57.0 10 50.00 2055-135114 12 Bromochloroacetonitrile ug/LBRL10 2070-130 Butyl benzyl phthalate ug/L52.4 10 50.00 2053-134105 5 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 51 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0112 - 3510C MS LCS Dup (P9G0112-BSD1)Prepared & Analyzed: 07/08/19 Chrysene ug/L51.5 10 50.00 2059-123103 8 Dibenzo(a,h)anthracene ug/L36.5 20 50.00 2051-13473 8 Dibenzofuran ug/L48.0 20 50.00 2053-11896 12 Diethyl phthalate ug/L52.0 20 50.00 2056-125104 11 Dimethyl phthalate ug/L50.0 10 50.00 2045-127100 10 Di-n-butyl phthalate ug/L55.6 10 50.00 2059-127111 7 Di-n-octyl phthalate ug/L54.8 10 50.00 20 D51-140110 22 Fluoranthene ug/L53.3 10 50.00 2057-128107 7 Fluorene ug/L51.5 10 50.00 2052-124103 14 Hexachlorobenzene ug/L48.5 20 50.00 2053-12597 12 Hexachlorobutadiene ug/L36.4 20 50.00 2022-12473 19 Hexachlorocyclopentadiene ug/L29.6 20 50.00 2032-11759 17 Hexachloroethane ug/L30.4 10 50.00 2021-11561 15 Indeno(1,2,3-cd)pyrene ug/L51.5 10 50.00 2052-134103 6 Isophorone ug/L41.2 10 50.00 2042-12482 17 Naphthalene ug/L38.6 10 50.00 2040-12177 19 Nitrobenzene ug/L39.5 10 50.00 20 D45-12179 22 N-Nitroso-di-n-propylamine ug/L38.0 20 50.00 2049-11976 16 N-Nitrosodiphenylamine ug/L61.6 20 50.00 2051-123123 6 Pentachlorophenol ug/L57.1 50 50.00 2035-138114 7 Phenanthrene ug/L52.6 10 50.00 2059-120105 7 Phenol ug/L20.7 10 50.00 2012-5841 17 Pyrene ug/L51.4 10 50.00 2057-126103 6 ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 103103 ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 8743.6 ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5655.7 ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7336.5 ug/L 100.0 11-52Surrogate: Phenol-d5 3636.4 ug/L 50.00 50-134Surrogate: Terphenyl-d14 9748.4 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 52 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0121 - 3546 Blank (P9G0121-BLK1)Prepared & Analyzed: 07/08/19 1,2,4-Trichlorobenzene mg/kg wetBRL0.66 1,2-Dichlorobenzene mg/kg wetBRL0.66 1,3-Dichlorobenzene mg/kg wetBRL0.66 1,4-Dichlorobenzene mg/kg wetBRL0.33 1-Methylnaphthalene mg/kg wetBRL0.66 2,4,5-Trichlorophenol mg/kg wetBRL0.66 2,4,6-Trichlorophenol mg/kg wetBRL0.66 2,4-Dichlorophenol mg/kg wetBRL0.66 2,4-Dimethylphenol mg/kg wetBRL0.33 2,4-Dinitrophenol mg/kg wetBRL1.5 2,4-Dinitrotoluene mg/kg wetBRL0.66 2,6-Dinitrotoluene mg/kg wetBRL0.66 2-Chloronaphthalene mg/kg wetBRL0.66 2-Chlorophenol mg/kg wetBRL0.66 2-Methylnaphthalene mg/kg wetBRL0.66 2-Methylphenol mg/kg wetBRL0.66 2-Nitrophenol mg/kg wetBRL0.66 3,3’-Dichlorobenzidine mg/kg wetBRL0.66 3/4-Methylphenol mg/kg wetBRL0.66 4,6-Dinitro-2-methylphenol mg/kg wetBRL1.5 4-Bromophenyl phenyl ether mg/kg wetBRL0.66 4-Chloro-3-methylphenol mg/kg wetBRL0.66 4-Chloroaniline mg/kg wetBRL0.33 4-Chlorophenyl phenyl ether mg/kg wetBRL1.0 4-Nitrophenol mg/kg wetBRL0.66 Acenaphthene mg/kg wetBRL0.66 Acenaphthylene mg/kg wetBRL0.66 Anthracene mg/kg wetBRL0.66 Azobenzene mg/kg wetBRL0.66 Benzo(a)anthracene mg/kg wetBRL0.66 Benzo(a)pyrene mg/kg wetBRL0.66 Benzo(b)fluoranthene mg/kg wetBRL0.66 Benzo(g,h,i)perylene mg/kg wetBRL0.66 Benzo(k)fluoranthene mg/kg wetBRL0.66 Benzoic Acid mg/kg wetBRL2.0 Benzyl alcohol mg/kg wetBRL0.66 bis(2-Chloroethoxy)methane mg/kg wetBRL0.66 Bis(2-Chloroethyl)ether mg/kg wetBRL0.66 Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33 Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.66 Butyl benzyl phthalate mg/kg wetBRL0.33 Chrysene mg/kg wetBRL0.66 Dibenzo(a,h)anthracene mg/kg wetBRL0.66 Dibenzofuran mg/kg wetBRL0.66 Diethyl phthalate mg/kg wetBRL0.66 Dimethyl phthalate mg/kg wetBRL0.66 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 53 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0121 - 3546 Blank (P9G0121-BLK1)Prepared & Analyzed: 07/08/19 Di-n-butyl phthalate mg/kg wetBRL0.66 Di-n-octyl phthalate mg/kg wetBRL0.33 Fluoranthene mg/kg wetBRL0.66 Fluorene mg/kg wetBRL0.66 Hexachlorobenzene mg/kg wetBRL0.66 Hexachlorobutadiene mg/kg wetBRL0.66 Hexachlorocyclopentadiene mg/kg wetBRL0.66 Hexachloroethane mg/kg wetBRL0.66 Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.66 Isophorone mg/kg wetBRL0.66 Naphthalene mg/kg wetBRL0.66 Nitrobenzene mg/kg wetBRL0.33 N-Nitroso-di-n-propylamine mg/kg wetBRL0.66 N-Nitrosodiphenylamine mg/kg wetBRL0.66 Pentachlorophenol mg/kg wetBRL1.0 Phenanthrene mg/kg wetBRL0.66 Phenol mg/kg wetBRL0.66 Pyrene mg/kg wetBRL0.66 Pyridine mg/kg wetBRL0.33 mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 802.66 mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 771.29 mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 782.59 mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 651.08 mg/kg wet 3.333 34-121Surrogate: Phenol-d5 762.53 mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 741.23 LCS (P9G0121-BS1)Prepared & Analyzed: 07/08/19 1,2,4-Trichlorobenzene mg/kg wet1.21 0.66 1.667 34-11873 1,2-Dichlorobenzene mg/kg wet1.13 0.66 1.667 33-11768 1,3-Dichlorobenzene mg/kg wet1.08 0.66 1.667 30-11565 1,4-Dichlorobenzene mg/kg wet1.07 0.33 1.667 31-11564 1-Methylnaphthalene mg/kg wet1.36 0.66 1.667 40-11982 2,4,5-Trichlorophenol mg/kg wet1.48 0.66 1.667 62-12489 2,4,6-Trichlorophenol mg/kg wet1.49 0.66 1.667 39-12689 2,4-Dichlorophenol mg/kg wet1.35 0.66 1.667 40-12281 2,4-Dimethylphenol mg/kg wet1.85 0.33 1.667 30-127111 2,4-Dinitrophenol mg/kg wet0.735 1.5 1.667 J27-12944 2,4-Dinitrotoluene mg/kg wet1.48 0.66 1.667 48-12689 2,6-Dinitrotoluene mg/kg wet1.49 0.66 1.667 46-12489 2-Chloronaphthalene mg/kg wet1.45 0.66 1.667 41-11487 2-Chlorophenol mg/kg wet1.37 0.66 1.667 34-12182 2-Methylnaphthalene mg/kg wet1.31 0.66 1.667 38-12278 2-Methylphenol mg/kg wet1.46 0.66 1.667 32-12288 2-Nitrophenol mg/kg wet1.20 0.66 1.667 36-12372 3,3’-Dichlorobenzidine mg/kg wet1.92 0.66 1.667 22-121115 3/4-Methylphenol mg/kg wet1.30 0.66 1.667 34-11978 4,6-Dinitro-2-methylphenol mg/kg wet1.08 1.5 1.667 J29-13265 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 54 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0121 - 3546 LCS (P9G0121-BS1)Prepared & Analyzed: 07/08/19 4-Bromophenyl phenyl ether mg/kg wet1.49 0.66 1.667 46-12489 4-Chloro-3-methylphenol mg/kg wet1.43 0.66 1.667 45-12286 4-Chloroaniline mg/kg wet1.40 0.33 1.667 17-10684 4-Chlorophenyl phenyl ether mg/kg wet1.56 1.0 1.667 45-12194 4-Nitrophenol mg/kg wet1.20 0.66 1.667 30-13272 Acenaphthene mg/kg wet1.54 0.66 1.667 40-12392 Acenaphthylene mg/kg wet1.50 0.66 1.667 32-13290 Anthracene mg/kg wet1.60 0.66 1.667 47-12396 Azobenzene mg/kg wet1.51 0.66 1.667 39-12591 Benzo(a)anthracene mg/kg wet1.53 0.66 1.667 49-12692 Benzo(a)pyrene mg/kg wet1.49 0.66 1.667 45-12989 Benzo(b)fluoranthene mg/kg wet1.57 0.66 1.667 45-13294 Benzo(g,h,i)perylene mg/kg wet1.46 0.66 1.667 43-13487 Benzo(k)fluoranthene mg/kg wet1.65 0.66 1.667 47-13299 Benzoic Acid mg/kg wet0.911 2.0 1.667 J10-8355 Benzyl alcohol mg/kg wet1.19 0.66 1.667 29-12271 bis(2-Chloroethoxy)methane mg/kg wet1.28 0.66 1.667 36-12177 Bis(2-Chloroethyl)ether mg/kg wet1.18 0.66 1.667 31-12071 Bis(2-chloroisopropyl)ether mg/kg wet1.25 0.33 1.667 33-13175 Bis(2-Ethylhexyl)phthalate mg/kg wet1.63 0.66 1.667 51-13398 Butyl benzyl phthalate mg/kg wet1.57 0.33 1.667 48-13294 Chrysene mg/kg wet1.53 0.66 1.667 50-12492 Dibenzo(a,h)anthracene mg/kg wet1.19 0.66 1.667 45-13471 Dibenzofuran mg/kg wet1.51 0.66 1.667 44-12091 Diethyl phthalate mg/kg wet1.57 0.66 1.667 50-12494 Dimethyl phthalate mg/kg wet1.53 0.66 1.667 48-12492 Di-n-butyl phthalate mg/kg wet1.61 0.66 1.667 51-12896 Di-n-octyl phthalate mg/kg wet1.60 0.33 1.667 45-14096 Fluoranthene mg/kg wet1.55 0.66 1.667 50-12793 Fluorene mg/kg wet1.62 0.66 1.667 43-12597 Hexachlorobenzene mg/kg wet1.43 0.66 1.667 45-12286 Hexachlorobutadiene mg/kg wet1.30 0.66 1.667 32-12378 Hexachlorocyclopentadiene mg/kg wet1.03 0.66 1.667 32-11762 Hexachloroethane mg/kg wet1.04 0.66 1.667 28-11763 Indeno(1,2,3-cd)pyrene mg/kg wet1.38 0.66 1.667 45-13383 Isophorone mg/kg wet1.28 0.66 1.667 30-12277 Naphthalene mg/kg wet1.28 0.66 1.667 35-12377 Nitrobenzene mg/kg wet1.18 0.33 1.667 34-12271 N-Nitroso-di-n-propylamine mg/kg wet1.18 0.66 1.667 36-12071 N-Nitrosodiphenylamine mg/kg wet1.80 0.66 1.667 38-127108 Pentachlorophenol mg/kg wet1.63 1.0 1.667 25-13398 Phenanthrene mg/kg wet1.56 0.66 1.667 50-12193 Phenol mg/kg wet1.35 0.66 1.667 34-12181 Pyrene mg/kg wet1.52 0.66 1.667 47-12791 Pyridine mg/kg wet0.741 0.33 1.667 10-6044 mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 963.20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 55 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0121 - 3546 LCS (P9G0121-BS1)Prepared & Analyzed: 07/08/19 mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 871.46 mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 822.73 mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 691.15 mg/kg wet 3.333 34-121Surrogate: Phenol-d5 832.75 mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 891.49 LCS Dup (P9G0121-BSD1)Prepared & Analyzed: 07/08/19 1,2,4-Trichlorobenzene mg/kg wet1.25 0.66 1.667 2034-11875 3 1,2-Dichlorobenzene mg/kg wet1.18 0.66 1.667 2033-11771 4 1,3-Dichlorobenzene mg/kg wet1.13 0.66 1.667 2030-11568 4 1,4-Dichlorobenzene mg/kg wet1.14 0.33 1.667 2031-11569 6 1-Methylnaphthalene mg/kg wet1.40 0.66 1.667 2040-11984 3 2,4,5-Trichlorophenol mg/kg wet1.43 0.66 1.667 2062-12486 3 2,4,6-Trichlorophenol mg/kg wet1.50 0.66 1.667 2039-12690 0.4 2,4-Dichlorophenol mg/kg wet1.40 0.66 1.667 2040-12284 4 2,4-Dimethylphenol mg/kg wet1.87 0.33 1.667 2030-127112 1 2,4-Dinitrophenol mg/kg wet0.775 1.5 1.667 20 J27-12946 5 2,4-Dinitrotoluene mg/kg wet1.45 0.66 1.667 2048-12687 2 2,6-Dinitrotoluene mg/kg wet1.50 0.66 1.667 2046-12490 0.6 2-Chloronaphthalene mg/kg wet1.42 0.66 1.667 2041-11485 2 2-Chlorophenol mg/kg wet1.42 0.66 1.667 2034-12185 3 2-Methylnaphthalene mg/kg wet1.33 0.66 1.667 2038-12280 2 2-Methylphenol mg/kg wet1.55 0.66 1.667 2032-12293 6 2-Nitrophenol mg/kg wet1.25 0.66 1.667 2036-12375 4 3,3’-Dichlorobenzidine mg/kg wet1.87 0.66 1.667 2022-121112 3 3/4-Methylphenol mg/kg wet1.42 0.66 1.667 2034-11985 9 4,6-Dinitro-2-methylphenol mg/kg wet1.10 1.5 1.667 20 J29-13266 2 4-Bromophenyl phenyl ether mg/kg wet1.51 0.66 1.667 2046-12491 2 4-Chloro-3-methylphenol mg/kg wet1.49 0.66 1.667 2045-12290 4 4-Chloroaniline mg/kg wet1.43 0.33 1.667 2017-10686 3 4-Chlorophenyl phenyl ether mg/kg wet1.56 1.0 1.667 2045-12194 0.2 4-Nitrophenol mg/kg wet1.13 0.66 1.667 2030-13268 5 Acenaphthene mg/kg wet1.51 0.66 1.667 2040-12390 2 Acenaphthylene mg/kg wet1.46 0.66 1.667 2032-13288 3 Anthracene mg/kg wet1.62 0.66 1.667 2047-12397 0.9 Azobenzene mg/kg wet1.49 0.66 1.667 2039-12589 2 Benzo(a)anthracene mg/kg wet1.48 0.66 1.667 2049-12688 3 Benzo(a)pyrene mg/kg wet1.50 0.66 1.667 2045-12990 0.6 Benzo(b)fluoranthene mg/kg wet1.52 0.66 1.667 2045-13291 3 Benzo(g,h,i)perylene mg/kg wet1.54 0.66 1.667 2043-13492 5 Benzo(k)fluoranthene mg/kg wet1.64 0.66 1.667 2047-13299 0.1 Benzoic Acid mg/kg wet0.893 2.0 1.667 20 J10-8354 2 Benzyl alcohol mg/kg wet1.25 0.66 1.667 2029-12275 5 bis(2-Chloroethoxy)methane mg/kg wet1.31 0.66 1.667 2036-12179 2 Bis(2-Chloroethyl)ether mg/kg wet1.19 0.66 1.667 2031-12071 1 Bis(2-chloroisopropyl)ether mg/kg wet1.28 0.33 1.667 2033-13177 3 Bis(2-Ethylhexyl)phthalate mg/kg wet1.62 0.66 1.667 2051-13397 0.5 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 56 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Semivolatile Organic Compounds by GC/MS - Quality Control Batch P9G0121 - 3546 LCS Dup (P9G0121-BSD1)Prepared & Analyzed: 07/08/19 Butyl benzyl phthalate mg/kg wet1.49 0.33 1.667 2048-13289 6 Chrysene mg/kg wet1.51 0.66 1.667 2050-12490 1 Dibenzo(a,h)anthracene mg/kg wet1.04 0.66 1.667 2045-13463 13 Dibenzofuran mg/kg wet1.47 0.66 1.667 2044-12088 3 Diethyl phthalate mg/kg wet1.53 0.66 1.667 2050-12492 3 Dimethyl phthalate mg/kg wet1.50 0.66 1.667 2048-12490 2 Di-n-butyl phthalate mg/kg wet1.61 0.66 1.667 2051-12896 0 Di-n-octyl phthalate mg/kg wet1.60 0.33 1.667 2045-14096 0.06 Fluoranthene mg/kg wet1.57 0.66 1.667 2050-12794 1 Fluorene mg/kg wet1.59 0.66 1.667 2043-12596 2 Hexachlorobenzene mg/kg wet1.45 0.66 1.667 2045-12287 1 Hexachlorobutadiene mg/kg wet1.34 0.66 1.667 2032-12381 3 Hexachlorocyclopentadiene mg/kg wet0.917 0.66 1.667 2032-11755 12 Hexachloroethane mg/kg wet1.06 0.66 1.667 2028-11764 2 Indeno(1,2,3-cd)pyrene mg/kg wet1.40 0.66 1.667 2045-13384 1 Isophorone mg/kg wet1.29 0.66 1.667 2030-12278 0.9 Naphthalene mg/kg wet1.32 0.66 1.667 2035-12379 3 Nitrobenzene mg/kg wet1.21 0.33 1.667 2034-12273 2 N-Nitroso-di-n-propylamine mg/kg wet1.26 0.66 1.667 2036-12075 7 N-Nitrosodiphenylamine mg/kg wet1.81 0.66 1.667 2038-127109 0.5 Pentachlorophenol mg/kg wet1.66 1.0 1.667 2025-133100 2 Phenanthrene mg/kg wet1.57 0.66 1.667 2050-12194 0.5 Phenol mg/kg wet1.41 0.66 1.667 2034-12184 4 Pyrene mg/kg wet1.44 0.66 1.667 2047-12787 5 Pyridine mg/kg wet0.855 0.33 1.667 2010-6051 14 mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 923.07 mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 811.35 mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 852.83 mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 681.14 mg/kg wet 3.333 34-121Surrogate: Phenol-d5 842.81 mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 811.35 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 57 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P9G0109 - NO PREP Blank (P9G0109-BLK1)Prepared & Analyzed: 07/05/19 Hexavalent Chromium mg/LBRL0.010 LCS (P9G0109-BS1)Prepared & Analyzed: 07/05/19 Hexavalent Chromium mg/L0.404 0.010 0.4000 90-110101 Batch P9G0122 - 3060A Blank (P9G0122-BLK1)Prepared: 07/08/19 Analyzed: 07/09/19 Hexavalent Chromium mg/kg wetBRL0.40 LCS (P9G0122-BS1)Prepared: 07/08/19 Analyzed: 07/09/19 Hexavalent Chromium mg/kg wet16.3 0.40 16.00 80-120102 Matrix Spike (P9G0122-MS1)Prepared: 07/08/19 Analyzed: 07/09/19 Source: 9070063-01 Hexavalent Chromium mg/kg dry18.8 0.49 19.80 0.204 60-11994 Matrix Spike Dup (P9G0122-MSD1)Prepared: 07/08/19 Analyzed: 07/09/19 Source: 9070063-01 Hexavalent Chromium mg/kg dry18.7 0.49 19.80 0.204 2060-11994 0.6 Post Spike (P9G0122-PS1)Prepared: 07/08/19 Analyzed: 07/09/19 Source: 9070063-01 Hexavalent Chromium mg/kg0.365 0.4000 0.00412 85-11590 Batch P9G0131 - 7471B Blank (P9G0131-BLK1)Prepared & Analyzed: 07/09/19 Mercury mg/kg wetBRL0.050 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 58 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P9G0131 - 7471B LCS (P9G0131-BS1)Prepared & Analyzed: 07/09/19 Mercury mg/kg wet0.408 0.050 0.4167 80-12098 Batch P9G0150 - 3005A Blank (P9G0150-BLK1)Prepared: 07/10/19 Analyzed: 07/11/19 Arsenic ug/LBRL1.0 Barium ug/LBRL10 Cadmium ug/LBRL1.0 Chromium ug/LBRL3.0 Lead ug/LBRL1.0 Selenium ug/LBRL5.0 Silver ug/LBRL1.0 LCS (P9G0150-BS1)Prepared: 07/10/19 Analyzed: 07/11/19 Arsenic ug/L1001.0 100.0 80-120100 Barium ug/L96.5 10 100.0 80-12097 Cadmium ug/L98.5 1.0 100.0 80-12099 Chromium ug/L1063.0 100.0 80-120106 Lead ug/L1021.0 100.0 80-120102 Selenium ug/L1025.0 100.0 80-120102 Silver ug/L1021.0 100.0 80-120102 Matrix Spike (P9G0150-MS1)Prepared: 07/10/19 Analyzed: 07/11/19 Source: 9070063-07 Arsenic ug/L98.3 1.0 100.0 BRL 75-12598 Barium ug/L95.0 10 100.0 BRL 75-12595 Cadmium ug/L98.0 1.0 100.0 BRL 75-12598 Chromium ug/L1053.0 100.0 BRL 75-125105 Lead ug/L1011.0 100.0 BRL 75-125101 Selenium ug/L96.1 5.0 100.0 BRL 75-12596 Silver ug/L1001.0 100.0 BRL 75-125100 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 59 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P9G0150 - 3005A Matrix Spike Dup (P9G0150-MSD1)Prepared: 07/10/19 Analyzed: 07/11/19 Source: 9070063-07 Arsenic ug/L98.7 1.0 100.0 BRL 2075-12599 0.5 Barium ug/L95.5 10 100.0 BRL 2075-12595 0.5 Cadmium ug/L98.3 1.0 100.0 BRL 2075-12598 0.3 Chromium ug/L1053.0 100.0 BRL 2075-125105 0.05 Lead ug/L1021.0 100.0 BRL 2075-125102 1 Selenium ug/L95.3 5.0 100.0 BRL 2075-12595 0.8 Silver ug/L1011.0 100.0 BRL 2075-125101 0.5 Batch P9G0166 - 3050B Blank (P9G0166-BLK1)Prepared & Analyzed: 07/11/19 Arsenic mg/kg wetBRL1.0 Barium mg/kg wetBRL10 Cadmium mg/kg wetBRL0.50 Chromium mg/kg wetBRL1.0 Lead mg/kg wetBRL1.0 Selenium mg/kg wetBRL1.0 Silver mg/kg wetBRL0.50 LCS (P9G0166-BS1)Prepared: 07/11/19 Analyzed: 07/12/19 Arsenic mg/kg wet12.5 1.0 12.50 80-120100 Barium mg/kg wet12.5 10 12.50 80-120100 Cadmium mg/kg wet12.3 0.50 12.50 80-12098 Chromium mg/kg wet13.2 1.0 12.50 80-120106 Lead mg/kg wet13.0 1.0 12.50 80-120104 Selenium mg/kg wet11.9 1.0 12.50 80-12095 Silver mg/kg wet5.06 0.50 5.000 80-120101 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 60 of 64 7/15/19 Level II QC Report 3300 International Airport Dr., Suite 600 Project: Barringer HomesFroehling & Robertson, Inc. (Charlotte) Charlotte, NC 28208 Attn: Brian Olin Prism Work Order: 9070063 Time Submitted: 7/5/2019 11:05:00AM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Total Metals - Quality Control Batch P9G0167 - 7470A Blank (P9G0167-BLK1)Prepared & Analyzed: 07/11/19 Mercury mg/LBRL0.00050 LCS (P9G0167-BS1)Prepared & Analyzed: 07/11/19 Mercury mg/L0.00925 0.00050 0.009375 80-12099 Matrix Spike (P9G0167-MS1)Prepared & Analyzed: 07/11/19 Source: 9070063-07 Mercury mg/L0.00930 0.00050 0.009375 BRL 80-12099 Matrix Spike Dup (P9G0167-MSD1)Prepared & Analyzed: 07/11/19 Source: 9070063-07 Mercury mg/L0.00947 0.00050 0.009375 BRL 2080-120101 2 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 61 of 64 Sample Extraction Data Prep Method: 3510C MS Lab Number Batch Date/TimeInitialFinal P9G01129070063-07 07/08/19 12:358301mL mL Prep Method: 3546 Lab Number Batch Date/TimeInitialFinal P9G01219070063-01 07/08/19 11:0030.03 1g mL P9G01219070063-02 07/08/19 11:0030.07 1g mL P9G01219070063-03 07/08/19 11:0030.02 1g mL P9G01219070063-04 07/08/19 11:0030.09 1g mL P9G01219070063-05 07/08/19 11:0030.02 1g mL Prep Method: 3005A Lab Number Batch Date/TimeInitialFinal P9G01509070063-07 07/10/19 8:2550 50mL mL Prep Method: 3050B Lab Number Batch Date/TimeInitialFinal P9G01669070063-01 07/11/19 8:551.96 50g mL P9G01669070063-02 07/11/19 8:551.96 50g mL P9G01669070063-03 07/11/19 8:551.98 50g mL P9G01669070063-04 07/11/19 8:552.03 50g mL P9G01669070063-05 07/11/19 8:552.05 50g mL P9G01669070063-06 07/11/19 8:551.98 50g mL Prep Method: 3060A Lab Number Batch Date/TimeInitialFinal P9G01229070063-01 07/08/19 14:302.5 100g mL P9G01229070063-02 07/08/19 14:302.5 100g mL P9G01229070063-03 07/08/19 14:302.5 100g mL P9G01229070063-04 07/08/19 14:302.5 100g mL P9G01229070063-05 07/08/19 14:302.5 100g mL P9G01229070063-06 07/08/19 14:302.5 100g mL Prep Method: 7470A Lab Number Batch Date/TimeInitialFinal P9G01679070063-07 07/11/19 9:1520 30mL mL Prep Method: 7471B Lab Number Batch Date/TimeInitialFinal P9G01319070063-01 07/09/19 8:550.62 50g mL P9G01319070063-02 07/09/19 8:550.64 50g mL P9G01319070063-03 07/09/19 8:550.61 50g mL P9G01319070063-04 07/09/19 8:550.57 50g mL P9G01319070063-05 07/09/19 8:550.64 50g mL P9G01319070063-06 07/09/19 8:550.59 50g mL Prep Method: 5030B Lab Number Batch Date/TimeInitialFinal P9G01249070063-07 07/08/19 14:2710 10mL mL P9G01249070063-08 07/08/19 14:2710 10mL mL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 62 of 64 Sample Extraction Data Prep Method: 5035 Lab Number Batch Date/TimeInitialFinal P9G01439070063-01 07/09/19 8:265.28 5g mL P9G01439070063-02 07/09/19 8:266.02 5g mL P9G01439070063-03 07/09/19 8:263.28 5g mL P9G01439070063-04 07/09/19 8:262.97 5g mL P9G01439070063-05 07/09/19 8:265.93 5g mL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 63 of 64 Page 64 of 64                   Groundwater      Page 1 of 67 Page 2 of 67 Page 3 of 67 Page 4 of 67 Page 5 of 67 Page 6 of 67 Page 7 of 67 Page 8 of 67 Page 9 of 67 Page 10 of 67 Page 11 of 67 Page 12 of 67 Page 13 of 67 Page 14 of 67 Page 15 of 67 Page 16 of 67 Page 17 of 67 Page 18 of 67 Page 19 of 67 Page 20 of 67 Page 21 of 67 Page 22 of 67 Page 23 of 67 Page 24 of 67 Page 25 of 67 Page 26 of 67 Page 27 of 67 Page 28 of 67 Page 29 of 67 Page 30 of 67 Page 31 of 67 Page 32 of 67 Page 33 of 67 Page 34 of 67 Page 35 of 67 Page 36 of 67 Page 37 of 67 Page 38 of 67 Page 39 of 67 Page 40 of 67 Page 41 of 67 Page 42 of 67 Page 43 of 67 Page 44 of 67 Page 45 of 67 Page 46 of 67 Page 47 of 67 Page 48 of 67 Page 49 of 67 Page 50 of 67 Page 51 of 67 Page 52 of 67 Page 53 of 67 Page 54 of 67 Page 55 of 67 Page 56 of 67 Page 57 of 67 Page 58 of 67 Page 59 of 67 Page 60 of 67 Page 61 of 67 Page 62 of 67 Page 63 of 67 Page 64 of 67 Page 65 of 67 Page 66 of 67 Page 67 of 67                   Soil‐Gas     39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 July 17, 2019 Brian Olin Froehling & Robertson 3300 International Airport Drive, Suite 600 Charlotte, NC 28208 Project Location: 510 W. Tremont Ave, Charlotte, NC Client Job Number: Project Number: 63X0084-00004 Laboratory Work Order Number: 19G0281 Enclosed are results of analyses for samples received by the laboratory on July 5, 2019. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL SUMMARY 7/17/2019Froehling & Robertson 3300 International Airport Drive, Suite 600 Charlotte, NC 28208 ATTN: Brian Olin 63X0084-00004 19G0281 The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report. PROJECT LOCATION: PURCHASE ORDER NUMBER: PROJECT NUMBER: REPORT DATE: WORK ORDER NUMBER: FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB 510 W. Tremont Ave, Charlotte, NC 63X0084-00004 B-2 19G0281-01 Sub Slab - EPA TO-15 B-2 DUP 19G0281-02 Sub Slab EPA TO-15 B-4 19G0281-03 Sub Slab - EPA TO-15 B-7 19G0281-04 Sub Slab - EPA TO-15 Page 2 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. Page 3 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 EPA TO-15 Qualifications: Laboratory fortified blank /laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. Analyte & Samples(s) Qualified: Vinyl Acetate B235636-BS1 Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the low side. Analyte & Samples(s) Qualified: Chloromethane 19G0281-03[B-4], 19G0281-04[B-7], B235636-BLK1, B235636-BS1 Elevated reporting limit due to high concentration of target compounds. Analyte & Samples(s) Qualified: 19G0281-01[B-2] Elevated reporting limit due to matrix interference. Analyte & Samples(s) Qualified: 19G0281-02[B-2 DUP], 19G0281-03[B-4], 19G0281-04[B-7] Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound. Analyte & Samples(s) Qualified: Chloromethane, Propene 19G0281-03[B-4], 19G0281-04[B-7], B235636-BLK1, B235636-BS1, S038157-CCV1 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: Vinyl Acetate S038157-CCV1 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: Vinyl Acetate B235636-BS1, S038157-CCV1 Calibrations RSD for this compound is >30% but <40%. Analyte & Samples(s) Qualified: 1,2,4-Trichlorobenzene, Naphthalene 19G0281-01[B-2], 19G0281-02[B-2 DUP], B235607-BLK1, B235607-BS1, S038140-CCV1 Page 4 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in house limits of 50-150%. Analyte & Samples(s) Qualified: Propene 19G0281-03[B-4], 19G0281-04[B-7], B235636-BLK1, B235636-BS1 The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Technical Representative Page 5 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 510 W. Tremont Ave, Charlotte, N Date Received: 7/5/2019 Work Order: 19G0281Sample Description/Location: Field Sample #: B-2 Sample ID: 19G0281-01 Sample Matrix: Sub Slab Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -2 Receipt Vacuum(in Hg): -5.1 Sampled: 7/3/2019 12:02 Canister ID: 2323 Flow Controller ID: 4207 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 5 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 Sample Flags: RL-11 MDL MDL Acetone 150 20 7/16/19 9:13 BRF370 10486.9 16 Benzene 8.6 0.50 7/16/19 9:13 BRF28 101.60.21 0.66 Benzyl chloride ND 0.50 7/16/19 9:13 BRFU ND 102.60.11 0.57 Bromodichloromethane ND 0.50 7/16/19 9:13 BRFU ND 103.40.18 1.2 Bromoform ND 0.50 7/16/19 9:13 BRFU ND 105.20.22 2.3 Bromomethane ND 0.50 7/16/19 9:13 BRFU ND 101.90.34 1.3 1,3-Butadiene 72 0.50 7/16/19 9:13 BRF160 101.10.32 0.70 2-Butanone (MEK)17 20 7/16/19 9:13 BRFJ50 10590.78 2.3 Carbon Disulfide 35 5.0 7/16/19 9:13 BRF110 10160.34 1.1 Carbon Tetrachloride ND 0.50 7/16/19 9:13 BRFU ND 103.10.16 1.0 Chlorobenzene ND 0.50 7/16/19 9:13 BRFU ND 102.30.24 1.1 Chloroethane ND 0.50 7/16/19 9:13 BRFU ND 101.30.30 0.80 Chloroform ND 0.50 7/16/19 9:13 BRFU ND 102.40.19 0.91 Chloromethane ND 1.0 7/16/19 9:13 BRFU ND 102.10.34 0.70 Cyclohexane ND 0.50 7/16/19 9:13 BRFU ND 101.70.36 1.2 Dibromochloromethane ND 0.50 7/16/19 9:13 BRFU ND 104.30.17 1.4 1,2-Dibromoethane (EDB)ND 0.50 7/16/19 9:13 BRFU ND 103.80.20 1.5 1,2-Dichlorobenzene ND 0.50 7/16/19 9:13 BRFU ND 103.00.24 1.4 1,3-Dichlorobenzene ND 0.50 7/16/19 9:13 BRFU ND 103.00.26 1.6 1,4-Dichlorobenzene ND 0.50 7/16/19 9:13 BRFU ND 103.00.30 1.8 Dichlorodifluoromethane (Freon 12)ND 0.50 7/16/19 9:13 BRFU ND 102.50.22 1.1 1,1-Dichloroethane ND 0.50 7/16/19 9:13 BRFU ND 102.00.15 0.62 1,2-Dichloroethane ND 0.50 7/16/19 9:13 BRFU ND 102.00.19 0.77 1,1-Dichloroethylene ND 0.50 7/16/19 9:13 BRFU ND 102.00.20 0.80 cis-1,2-Dichloroethylene ND 0.50 7/16/19 9:13 BRFU ND 102.00.20 0.81 trans-1,2-Dichloroethylene ND 0.50 7/16/19 9:13 BRFU ND 102.00.20 0.80 1,2-Dichloropropane ND 0.50 7/16/19 9:13 BRFU ND 102.30.18 0.82 cis-1,3-Dichloropropene ND 0.50 7/16/19 9:13 BRFU ND 102.30.18 0.79 trans-1,3-Dichloropropene ND 0.50 7/16/19 9:13 BRFU ND 102.30.18 0.83 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.50 7/16/19 9:13 BRFU ND 103.50.25 1.7 1,4-Dioxane ND 5.0 7/16/19 9:13 BRFU ND 10183.2 12 Ethanol 23 20 7/16/19 9:13 BRF44 10388.9 17 Ethyl Acetate 37 2.0 7/16/19 9:13 BRF130 107.20.37 1.3 Ethylbenzene 3.6 0.50 7/16/19 9:13 BRF16 102.20.29 1.3 4-Ethyltoluene 6.8 0.50 7/16/19 9:13 BRF34 102.50.30 1.5 Heptane 13 0.50 7/16/19 9:13 BRF53 102.00.29 1.2 Hexachlorobutadiene ND 0.50 7/16/19 9:13 BRFU ND 105.30.23 2.5 Hexane ND 20 7/16/19 9:13 BRFU ND 10700.88 3.1 2-Hexanone (MBK)ND 0.50 7/16/19 9:13 BRFU ND 102.00.30 1.2 Isopropanol ND 20 7/16/19 9:13 BRFU ND 10490.61 1.5 Methyl tert-Butyl Ether (MTBE)10 0.50 7/16/19 9:13 BRF37 101.80.25 0.90 Methylene Chloride 1.5 5.0 7/16/19 9:13 BRFJ5.3 10170.61 2.1 4-Methyl-2-pentanone (MIBK)ND 0.50 7/16/19 9:13 BRFU ND 102.00.24 0.99 Naphthalene ND 0.50 7/16/19 9:13 BRFZ-01, U ND 102.60.38 2.0 Propene 2600 600 7/16/19 10:12 BRF4500 30010001526 Styrene ND 0.50 7/16/19 9:13 BRFU ND 102.10.31 1.3 1,1,2,2-Tetrachloroethane ND 0.50 7/16/19 9:13 BRFU ND 103.40.22 1.5 Page 6 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 510 W. Tremont Ave, Charlotte, N Date Received: 7/5/2019 Work Order: 19G0281Sample Description/Location: Field Sample #: B-2 Sample ID: 19G0281-01 Sample Matrix: Sub Slab Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -2 Receipt Vacuum(in Hg): -5.1 Sampled: 7/3/2019 12:02 Canister ID: 2323 Flow Controller ID: 4207 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 5 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 Sample Flags: RL-11 MDL MDL Tetrachloroethylene ND 0.50 7/16/19 9:13 BRFU ND 103.40.28 1.9 Tetrahydrofuran ND 0.50 7/16/19 9:13 BRFU ND 101.50.33 0.98 Toluene 11 0.50 7/16/19 9:13 BRF42 101.90.26 0.97 1,2,4-Trichlorobenzene ND 1.0 7/16/19 9:13 BRFZ-01, U ND 107.40.34 2.6 1,1,1-Trichloroethane ND 0.50 7/16/19 9:13 BRFU ND 102.70.19 1.0 1,1,2-Trichloroethane ND 0.50 7/16/19 9:13 BRFU ND 102.70.21 1.1 Trichloroethylene ND 0.50 7/16/19 9:13 BRFU ND 102.70.20 1.1 Trichlorofluoromethane (Freon 11)ND 2.0 7/16/19 9:13 BRFU ND 10110.29 1.6 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 2.0 7/16/19 9:13 BRFU ND 10150.30 2.3 1,2,4-Trimethylbenzene 15 0.50 7/16/19 9:13 BRF72 102.50.32 1.6 1,3,5-Trimethylbenzene 4.7 0.50 7/16/19 9:13 BRF23 102.50.31 1.5 Vinyl Acetate ND 10 7/16/19 9:13 BRFU ND 10350.24 0.84 Vinyl Chloride ND 0.50 7/16/19 9:13 BRFU ND 101.30.32 0.81 m&p-Xylene 8.0 1.0 7/16/19 9:13 BRF35 104.30.58 2.5 o-Xylene 3.6 0.50 7/16/19 9:13 BRF16 102.20.31 1.4 Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1)102 7/16/19 10:1270-130 4-Bromofluorobenzene (1)109 7/16/19 9:1370-130 Page 7 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 510 W. Tremont Ave, Charlotte, N Date Received: 7/5/2019 Work Order: 19G0281Sample Description/Location: Field Sample #: B-2 DUP Sample ID: 19G0281-02 Sample Matrix: Sub Slab Initial Vacuum(in Hg): -27 Final Vacuum(in Hg): -3 Receipt Vacuum(in Hg): -6.7 Sampled: 7/3/2019 12:07 Canister ID: 2311 Flow Controller ID: 429 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 5 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 Sample Flags: RL-12 MDL MDL Acetone 98 20 7/16/19 10:39 BRF230 10486.9 16 Benzene 4.4 0.50 7/16/19 10:39 BRF14 101.60.21 0.66 Benzyl chloride ND 0.50 7/16/19 10:39 BRFU ND 102.60.11 0.57 Bromodichloromethane ND 0.50 7/16/19 10:39 BRFU ND 103.40.18 1.2 Bromoform ND 0.50 7/16/19 10:39 BRFU ND 105.20.22 2.3 Bromomethane ND 0.50 7/16/19 10:39 BRFU ND 101.90.34 1.3 1,3-Butadiene 33 0.50 7/16/19 10:39 BRF72 101.10.32 0.70 2-Butanone (MEK)15 20 7/16/19 10:39 BRFJ43 10590.78 2.3 Carbon Disulfide 24 5.0 7/16/19 10:39 BRF74 10160.34 1.1 Carbon Tetrachloride ND 0.50 7/16/19 10:39 BRFU ND 103.10.16 1.0 Chlorobenzene ND 0.50 7/16/19 10:39 BRFU ND 102.30.24 1.1 Chloroethane ND 0.50 7/16/19 10:39 BRFU ND 101.30.30 0.80 Chloroform ND 0.50 7/16/19 10:39 BRFU ND 102.40.19 0.91 Chloromethane ND 1.0 7/16/19 10:39 BRFU ND 102.10.34 0.70 Cyclohexane ND 0.50 7/16/19 10:39 BRFU ND 101.70.36 1.2 Dibromochloromethane ND 0.50 7/16/19 10:39 BRFU ND 104.30.17 1.4 1,2-Dibromoethane (EDB)ND 0.50 7/16/19 10:39 BRFU ND 103.80.20 1.5 1,2-Dichlorobenzene ND 0.50 7/16/19 10:39 BRFU ND 103.00.24 1.4 1,3-Dichlorobenzene ND 0.50 7/16/19 10:39 BRFU ND 103.00.26 1.6 1,4-Dichlorobenzene ND 0.50 7/16/19 10:39 BRFU ND 103.00.30 1.8 Dichlorodifluoromethane (Freon 12)ND 0.50 7/16/19 10:39 BRFU ND 102.50.22 1.1 1,1-Dichloroethane ND 0.50 7/16/19 10:39 BRFU ND 102.00.15 0.62 1,2-Dichloroethane ND 0.50 7/16/19 10:39 BRFU ND 102.00.19 0.77 1,1-Dichloroethylene ND 0.50 7/16/19 10:39 BRFU ND 102.00.20 0.80 cis-1,2-Dichloroethylene ND 0.50 7/16/19 10:39 BRFU ND 102.00.20 0.81 trans-1,2-Dichloroethylene ND 0.50 7/16/19 10:39 BRFU ND 102.00.20 0.80 1,2-Dichloropropane ND 0.50 7/16/19 10:39 BRFU ND 102.30.18 0.82 cis-1,3-Dichloropropene ND 0.50 7/16/19 10:39 BRFU ND 102.30.18 0.79 trans-1,3-Dichloropropene ND 0.50 7/16/19 10:39 BRFU ND 102.30.18 0.83 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.50 7/16/19 10:39 BRFU ND 103.50.25 1.7 1,4-Dioxane ND 5.0 7/16/19 10:39 BRFU ND 10183.2 12 Ethanol 16 20 7/16/19 10:39 BRFJ30 10388.9 17 Ethyl Acetate 18 2.0 7/16/19 10:39 BRF66 107.20.37 1.3 Ethylbenzene 2.5 0.50 7/16/19 10:39 BRF11 102.20.29 1.3 4-Ethyltoluene 6.0 0.50 7/16/19 10:39 BRF30 102.50.30 1.5 Heptane 4.3 0.50 7/16/19 10:39 BRF18 102.00.29 1.2 Hexachlorobutadiene ND 0.50 7/16/19 10:39 BRFU ND 105.30.23 2.5 Hexane ND 20 7/16/19 10:39 BRFU ND 10700.88 3.1 2-Hexanone (MBK)ND 0.50 7/16/19 10:39 BRFU ND 102.00.30 1.2 Isopropanol ND 20 7/16/19 10:39 BRFU ND 10490.61 1.5 Methyl tert-Butyl Ether (MTBE)7.7 0.50 7/16/19 10:39 BRF28 101.80.25 0.90 Methylene Chloride ND 5.0 7/16/19 10:39 BRFU ND 10170.61 2.1 4-Methyl-2-pentanone (MIBK)ND 0.50 7/16/19 10:39 BRFU ND 102.00.24 0.99 Naphthalene ND 0.50 7/16/19 10:39 BRFZ-01, U ND 102.60.38 2.0 Propene 1200 80 7/15/19 15:36 BRF2000 401402.0 3.4 Styrene ND 0.50 7/16/19 10:39 BRFU ND 102.10.31 1.3 1,1,2,2-Tetrachloroethane ND 0.50 7/16/19 10:39 BRFU ND 103.40.22 1.5 Page 8 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 510 W. Tremont Ave, Charlotte, N Date Received: 7/5/2019 Work Order: 19G0281Sample Description/Location: Field Sample #: B-2 DUP Sample ID: 19G0281-02 Sample Matrix: Sub Slab Initial Vacuum(in Hg): -27 Final Vacuum(in Hg): -3 Receipt Vacuum(in Hg): -6.7 Sampled: 7/3/2019 12:07 Canister ID: 2311 Flow Controller ID: 429 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 5 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 Sample Flags: RL-12 MDL MDL Tetrachloroethylene ND 0.50 7/16/19 10:39 BRFU ND 103.40.28 1.9 Tetrahydrofuran ND 0.50 7/16/19 10:39 BRFU ND 101.50.33 0.98 Toluene 5.7 0.50 7/16/19 10:39 BRF21 101.90.26 0.97 1,2,4-Trichlorobenzene ND 1.0 7/16/19 10:39 BRFZ-01, U ND 107.40.34 2.6 1,1,1-Trichloroethane ND 0.50 7/16/19 10:39 BRFU ND 102.70.19 1.0 1,1,2-Trichloroethane ND 0.50 7/16/19 10:39 BRFU ND 102.70.21 1.1 Trichloroethylene ND 0.50 7/16/19 10:39 BRFU ND 102.70.20 1.1 Trichlorofluoromethane (Freon 11)ND 2.0 7/16/19 10:39 BRFU ND 10110.29 1.6 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 2.0 7/16/19 10:39 BRFU ND 10150.30 2.3 1,2,4-Trimethylbenzene 17 0.50 7/16/19 10:39 BRF85 102.50.32 1.6 1,3,5-Trimethylbenzene 4.6 0.50 7/16/19 10:39 BRF22 102.50.31 1.5 Vinyl Acetate ND 10 7/16/19 10:39 BRFU ND 10350.24 0.84 Vinyl Chloride ND 0.50 7/16/19 10:39 BRFU ND 101.30.32 0.81 m&p-Xylene 7.4 1.0 7/16/19 10:39 BRF32 104.30.58 2.5 o-Xylene 3.4 0.50 7/16/19 10:39 BRF15 102.20.31 1.4 Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1)104 7/15/19 15:3670-130 4-Bromofluorobenzene (1)107 7/16/19 10:3970-130 Page 9 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 510 W. Tremont Ave, Charlotte, N Date Received: 7/5/2019 Work Order: 19G0281Sample Description/Location: Field Sample #: B-4 Sample ID: 19G0281-03 Sample Matrix: Sub Slab Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -3 Receipt Vacuum(in Hg): -4.7 Sampled: 7/3/2019 12:27 Canister ID: 2234 Flow Controller ID: 4370 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 5 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 Sample Flags: RL-12 MDL MDL Acetone ND 40 7/16/19 15:13 BRFU ND 20951433 Benzene 2.9 1.0 7/16/19 15:13 BRF9.1 203.20.41 1.3 Benzyl chloride ND 1.0 7/16/19 15:13 BRFU ND 205.20.22 1.1 Bromodichloromethane ND 1.0 7/16/19 15:13 BRFU ND 206.70.37 2.5 Bromoform ND 1.0 7/16/19 15:13 BRFU ND 20100.45 4.7 Bromomethane ND 1.0 7/16/19 15:13 BRFU ND 203.90.69 2.7 1,3-Butadiene ND 1.0 7/16/19 15:13 BRFU ND 202.20.63 1.4 2-Butanone (MEK)7.4 40 7/16/19 15:13 BRFJ22 201201.6 4.6 Carbon Disulfide 24 10 7/16/19 15:13 BRF75 20310.69 2.1 Carbon Tetrachloride ND 1.0 7/16/19 15:13 BRFU ND 206.30.33 2.1 Chlorobenzene ND 1.0 7/16/19 15:13 BRFU ND 204.60.49 2.3 Chloroethane ND 1.0 7/16/19 15:13 BRFU ND 202.60.61 1.6 Chloroform ND 1.0 7/16/19 15:13 BRFU ND 204.90.37 1.8 Chloromethane ND 2.0 7/16/19 15:13 BRFL-03, V-05, U ND 204.10.68 1.4 Cyclohexane ND 1.0 7/16/19 15:13 BRFU ND 203.40.71 2.4 Dibromochloromethane ND 1.0 7/16/19 15:13 BRFU ND 208.50.33 2.8 1,2-Dibromoethane (EDB)ND 1.0 7/16/19 15:13 BRFU ND 207.70.39 3.0 1,2-Dichlorobenzene ND 1.0 7/16/19 15:13 BRFU ND 206.00.48 2.9 1,3-Dichlorobenzene ND 1.0 7/16/19 15:13 BRFU ND 206.00.52 3.1 1,4-Dichlorobenzene ND 1.0 7/16/19 15:13 BRFU ND 206.00.61 3.7 Dichlorodifluoromethane (Freon 12)ND 1.0 7/16/19 15:13 BRFU ND 204.90.43 2.1 1,1-Dichloroethane ND 1.0 7/16/19 15:13 BRFU ND 204.00.30 1.2 1,2-Dichloroethane ND 1.0 7/16/19 15:13 BRFU ND 204.00.38 1.5 1,1-Dichloroethylene ND 1.0 7/16/19 15:13 BRFU ND 204.00.41 1.6 cis-1,2-Dichloroethylene ND 1.0 7/16/19 15:13 BRFU ND 204.00.41 1.6 trans-1,2-Dichloroethylene ND 1.0 7/16/19 15:13 BRFU ND 204.00.41 1.6 1,2-Dichloropropane ND 1.0 7/16/19 15:13 BRFU ND 204.60.35 1.6 cis-1,3-Dichloropropene ND 1.0 7/16/19 15:13 BRFU ND 204.50.35 1.6 trans-1,3-Dichloropropene ND 1.0 7/16/19 15:13 BRFU ND 204.50.36 1.7 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 1.0 7/16/19 15:13 BRFU ND 207.00.50 3.5 1,4-Dioxane ND 10 7/16/19 15:13 BRFU ND 20366.4 23 Ethanol 93 40 7/16/19 15:13 BRF170 20751834 Ethyl Acetate 14 1.0 7/16/19 15:13 BRF50 203.60.75 2.7 Ethylbenzene 59 1.0 7/16/19 15:13 BRF260 204.30.58 2.5 4-Ethyltoluene ND 1.0 7/16/19 15:13 BRFU ND 204.90.61 3.0 Heptane 6.2 1.0 7/16/19 15:13 BRF25 204.10.59 2.4 Hexachlorobutadiene ND 1.0 7/16/19 15:13 BRFU ND 20110.46 4.9 Hexane 23 40 7/16/19 15:13 BRFJ80 201401.8 6.2 2-Hexanone (MBK)ND 1.0 7/16/19 15:13 BRFU ND 204.10.59 2.4 Isopropanol ND 40 7/16/19 15:13 BRFU ND 20981.2 3.0 Methyl tert-Butyl Ether (MTBE)20 1.0 7/16/19 15:13 BRF72 203.60.50 1.8 Methylene Chloride ND 10 7/16/19 15:13 BRFU ND 20351.2 4.2 4-Methyl-2-pentanone (MIBK)ND 1.0 7/16/19 15:13 BRFU ND 204.10.48 2.0 Naphthalene ND 1.0 7/16/19 15:13 BRFU ND 205.20.77 4.0 Propene ND 40 7/16/19 15:13 BRFV-05, Z-01a, U ND 20690.99 1.7 Page 10 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 510 W. Tremont Ave, Charlotte, N Date Received: 7/5/2019 Work Order: 19G0281Sample Description/Location: Field Sample #: B-4 Sample ID: 19G0281-03 Sample Matrix: Sub Slab Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -3 Receipt Vacuum(in Hg): -4.7 Sampled: 7/3/2019 12:27 Canister ID: 2234 Flow Controller ID: 4370 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 5 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 Sample Flags: RL-12 MDL MDL Styrene ND 1.0 7/16/19 15:13 BRFU ND 204.30.62 2.6 1,1,2,2-Tetrachloroethane ND 1.0 7/16/19 15:13 BRFU ND 206.90.44 3.0 Tetrachloroethylene ND 1.0 7/16/19 15:13 BRFU ND 206.80.56 3.8 Tetrahydrofuran ND 1.0 7/16/19 15:13 BRFU ND 202.90.66 2.0 Toluene 7.2 1.0 7/16/19 15:13 BRF27 203.80.52 1.9 1,2,4-Trichlorobenzene ND 1.0 7/16/19 15:13 BRFU ND 207.40.69 5.1 1,1,1-Trichloroethane ND 1.0 7/16/19 15:13 BRFU ND 205.50.37 2.0 1,1,2-Trichloroethane ND 1.0 7/16/19 15:13 BRFU ND 205.50.41 2.2 Trichloroethylene ND 1.0 7/16/19 15:13 BRFU ND 205.40.40 2.2 Trichlorofluoromethane (Freon 11)ND 4.0 7/16/19 15:13 BRFU ND 20220.58 3.3 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 4.0 7/16/19 15:13 BRFU ND 20310.60 4.6 1,2,4-Trimethylbenzene ND 1.0 7/16/19 15:13 BRFU ND 204.90.64 3.1 1,3,5-Trimethylbenzene ND 1.0 7/16/19 15:13 BRFU ND 204.90.63 3.1 Vinyl Acetate ND 20 7/16/19 15:13 BRFU ND 20700.48 1.7 Vinyl Chloride ND 1.0 7/16/19 15:13 BRFU ND 202.60.63 1.6 m&p-Xylene 320 2.0 7/16/19 15:13 BRF1400 208.71.2 5.0 o-Xylene 120 1.0 7/16/19 15:13 BRF530 204.30.62 2.7 Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1)95.7 7/16/19 15:1370-130 Page 11 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 510 W. Tremont Ave, Charlotte, N Date Received: 7/5/2019 Work Order: 19G0281Sample Description/Location: Field Sample #: B-7 Sample ID: 19G0281-04 Sample Matrix: Sub Slab Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -2 Receipt Vacuum(in Hg): -4.4 Sampled: 7/3/2019 13:12 Canister ID: 2329 Flow Controller ID: 4369 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 5 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 Sample Flags: RL-12 MDL MDL Acetone ND 40 7/16/19 15:48 BRFU ND 20951433 Benzene 2.7 1.0 7/16/19 15:48 BRF8.6 203.20.41 1.3 Benzyl chloride ND 1.0 7/16/19 15:48 BRFU ND 205.20.22 1.1 Bromodichloromethane ND 1.0 7/16/19 15:48 BRFU ND 206.70.37 2.5 Bromoform ND 1.0 7/16/19 15:48 BRFU ND 20100.45 4.7 Bromomethane ND 1.0 7/16/19 15:48 BRFU ND 203.90.69 2.7 1,3-Butadiene ND 1.0 7/16/19 15:48 BRFU ND 202.20.63 1.4 2-Butanone (MEK)10 40 7/16/19 15:48 BRFJ30 201201.6 4.6 Carbon Disulfide 34 10 7/16/19 15:48 BRF110 20310.69 2.1 Carbon Tetrachloride ND 1.0 7/16/19 15:48 BRFU ND 206.30.33 2.1 Chlorobenzene ND 1.0 7/16/19 15:48 BRFU ND 204.60.49 2.3 Chloroethane ND 1.0 7/16/19 15:48 BRFU ND 202.60.61 1.6 Chloroform ND 1.0 7/16/19 15:48 BRFU ND 204.90.37 1.8 Chloromethane ND 2.0 7/16/19 15:48 BRFL-03, V-05, U ND 204.10.68 1.4 Cyclohexane 14 1.0 7/16/19 15:48 BRF49 203.40.71 2.4 Dibromochloromethane ND 1.0 7/16/19 15:48 BRFU ND 208.50.33 2.8 1,2-Dibromoethane (EDB)ND 1.0 7/16/19 15:48 BRFU ND 207.70.39 3.0 1,2-Dichlorobenzene ND 1.0 7/16/19 15:48 BRFU ND 206.00.48 2.9 1,3-Dichlorobenzene ND 1.0 7/16/19 15:48 BRFU ND 206.00.52 3.1 1,4-Dichlorobenzene ND 1.0 7/16/19 15:48 BRFU ND 206.00.61 3.7 Dichlorodifluoromethane (Freon 12)ND 1.0 7/16/19 15:48 BRFU ND 204.90.43 2.1 1,1-Dichloroethane ND 1.0 7/16/19 15:48 BRFU ND 204.00.30 1.2 1,2-Dichloroethane ND 1.0 7/16/19 15:48 BRFU ND 204.00.38 1.5 1,1-Dichloroethylene ND 1.0 7/16/19 15:48 BRFU ND 204.00.41 1.6 cis-1,2-Dichloroethylene ND 1.0 7/16/19 15:48 BRFU ND 204.00.41 1.6 trans-1,2-Dichloroethylene ND 1.0 7/16/19 15:48 BRFU ND 204.00.41 1.6 1,2-Dichloropropane ND 1.0 7/16/19 15:48 BRFU ND 204.60.35 1.6 cis-1,3-Dichloropropene ND 1.0 7/16/19 15:48 BRFU ND 204.50.35 1.6 trans-1,3-Dichloropropene ND 1.0 7/16/19 15:48 BRFU ND 204.50.36 1.7 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 1.0 7/16/19 15:48 BRFU ND 207.00.50 3.5 1,4-Dioxane ND 10 7/16/19 15:48 BRFU ND 20366.4 23 Ethanol ND 40 7/16/19 15:48 BRFU ND 20751834 Ethyl Acetate 7.0 1.0 7/16/19 15:48 BRF25 203.60.75 2.7 Ethylbenzene 16 1.0 7/16/19 15:48 BRF68 204.30.58 2.5 4-Ethyltoluene ND 1.0 7/16/19 15:48 BRFU ND 204.90.61 3.0 Heptane 23 1.0 7/16/19 15:48 BRF96 204.10.59 2.4 Hexachlorobutadiene ND 1.0 7/16/19 15:48 BRFU ND 20110.46 4.9 Hexane 220 40 7/16/19 15:48 BRF760 201401.8 6.2 2-Hexanone (MBK)ND 1.0 7/16/19 15:48 BRFU ND 204.10.59 2.4 Isopropanol 5.6 40 7/16/19 15:48 BRFJ14 20981.2 3.0 Methyl tert-Butyl Ether (MTBE)ND 1.0 7/16/19 15:48 BRFU ND 203.60.50 1.8 Methylene Chloride ND 10 7/16/19 15:48 BRFU ND 20351.2 4.2 4-Methyl-2-pentanone (MIBK)ND 1.0 7/16/19 15:48 BRFU ND 204.10.48 2.0 Naphthalene ND 1.0 7/16/19 15:48 BRFU ND 205.20.77 4.0 Propene ND 40 7/16/19 15:48 BRFV-05, Z-01a, U ND 20690.99 1.7 Page 12 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 510 W. Tremont Ave, Charlotte, N Date Received: 7/5/2019 Work Order: 19G0281Sample Description/Location: Field Sample #: B-7 Sample ID: 19G0281-04 Sample Matrix: Sub Slab Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -2 Receipt Vacuum(in Hg): -4.4 Sampled: 7/3/2019 13:12 Canister ID: 2329 Flow Controller ID: 4369 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 5 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 Sample Flags: RL-12 MDL MDL Styrene ND 1.0 7/16/19 15:48 BRFU ND 204.30.62 2.6 1,1,2,2-Tetrachloroethane ND 1.0 7/16/19 15:48 BRFU ND 206.90.44 3.0 Tetrachloroethylene ND 1.0 7/16/19 15:48 BRFU ND 206.80.56 3.8 Tetrahydrofuran ND 1.0 7/16/19 15:48 BRFU ND 202.90.66 2.0 Toluene 3.2 1.0 7/16/19 15:48 BRF12 203.80.52 1.9 1,2,4-Trichlorobenzene ND 1.0 7/16/19 15:48 BRFU ND 207.40.69 5.1 1,1,1-Trichloroethane ND 1.0 7/16/19 15:48 BRFU ND 205.50.37 2.0 1,1,2-Trichloroethane ND 1.0 7/16/19 15:48 BRFU ND 205.50.41 2.2 Trichloroethylene ND 1.0 7/16/19 15:48 BRFU ND 205.40.40 2.2 Trichlorofluoromethane (Freon 11)ND 4.0 7/16/19 15:48 BRFU ND 20220.58 3.3 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 4.0 7/16/19 15:48 BRFU ND 20310.60 4.6 1,2,4-Trimethylbenzene ND 1.0 7/16/19 15:48 BRFU ND 204.90.64 3.1 1,3,5-Trimethylbenzene ND 1.0 7/16/19 15:48 BRFU ND 204.90.63 3.1 Vinyl Acetate ND 20 7/16/19 15:48 BRFU ND 20700.48 1.7 Vinyl Chloride ND 1.0 7/16/19 15:48 BRFU ND 202.60.63 1.6 m&p-Xylene 84 2.0 7/16/19 15:48 BRF360 208.71.2 5.0 o-Xylene 28 1.0 7/16/19 15:48 BRF120 204.30.62 2.7 Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1)87.4 7/16/19 15:4870-130 Page 13 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep-EPA TO-15 Lab Number [Field ID]Batch Date Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL 19G0281-01 [B-2]B235607 1.5 1 N/A 1000 400 60 07/15/19 19G0281-01RE1 [B-2]B235607 1.5 200 5 1000 400 400 07/15/19 19G0281-02 [B-2 DUP]B235607 1.5 1 N/A 1000 400 60 07/15/19 19G0281-02RE1 [B-2 DUP]B235607 1.5 1 N/A 1000 400 15 07/15/19 Prep Method: TO-15 Prep-EPA TO-15 Lab Number [Field ID]Batch Date Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL 19G0281-03 [B-4]B235636 1.5 1 N/A 1000 400 30 07/16/19 19G0281-04 [B-7]B235636 1.5 1 N/A 1000 400 30 07/16/19 Page 14 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B235607 - TO-15 Prep Blank (B235607-BLK1)Prepared & Analyzed: 07/15/19 1.4 UNDAcetone 0.035 UNDBenzene 0.035 UNDBenzyl chloride 0.035 UNDBromodichloromethane 0.035 UNDBromoform 0.035 UNDBromomethane 0.035 UND1,3-Butadiene 1.4 UND2-Butanone (MEK) 0.35 UNDCarbon Disulfide 0.035 UNDCarbon Tetrachloride 0.035 UNDChlorobenzene 0.035 UNDChloroethane 0.035 UNDChloroform 0.070 UNDChloromethane 0.035 UNDCyclohexane 0.035 UNDDibromochloromethane 0.035 UND1,2-Dibromoethane (EDB) 0.035 UND1,2-Dichlorobenzene 0.035 UND1,3-Dichlorobenzene 0.035 UND1,4-Dichlorobenzene 0.035 UNDDichlorodifluoromethane (Freon 12) 0.035 UND1,1-Dichloroethane 0.035 UND1,2-Dichloroethane 0.035 UND1,1-Dichloroethylene 0.035 UNDcis-1,2-Dichloroethylene 0.035 UNDtrans-1,2-Dichloroethylene 0.035 UND1,2-Dichloropropane 0.035 UNDcis-1,3-Dichloropropene 0.035 UNDtrans-1,3-Dichloropropene 0.035 UND1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 0.35 UND1,4-Dioxane 1.4 UNDEthanol 0.14 UNDEthyl Acetate 0.035 UNDEthylbenzene 0.035 UND4-Ethyltoluene 0.035 UNDHeptane 0.035 UNDHexachlorobutadiene 1.4 UNDHexane 0.035 UND2-Hexanone (MBK) 1.4 UNDIsopropanol 0.035 UNDMethyl tert-Butyl Ether (MTBE) 0.35 UNDMethylene Chloride 0.035 UND4-Methyl-2-pentanone (MIBK) 0.035 Z-01, UNDNaphthalene 1.4 UNDPropene 0.035 UNDStyrene Page 15 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B235607 - TO-15 Prep Blank (B235607-BLK1)Prepared & Analyzed: 07/15/19 0.035 UND1,1,2,2-Tetrachloroethane 0.035 UNDTetrachloroethylene 0.035 UNDTetrahydrofuran 0.035 UNDToluene 0.035 Z-01, UND1,2,4-Trichlorobenzene 0.035 UND1,1,1-Trichloroethane 0.035 UND1,1,2-Trichloroethane 0.035 UNDTrichloroethylene 0.14 UNDTrichlorofluoromethane (Freon 11) 0.14 UND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.035 UND1,2,4-Trimethylbenzene 0.035 UND1,3,5-Trimethylbenzene 0.70 UNDVinyl Acetate 0.035 UNDVinyl Chloride 0.070 UNDm&p-Xylene 0.035 UNDo-Xylene 8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1018.06 LCS (B235607-BS1)Prepared & Analyzed: 07/15/19 5.00 70-13093.34.66Acetone 5.00 70-13092.84.64Benzene 5.00 70-13091.54.58Benzyl chloride 5.00 70-13090.54.53Bromodichloromethane 5.00 70-1301025.11Bromoform 5.00 70-13090.84.54Bromomethane 5.00 70-13090.44.521,3-Butadiene 5.00 70-13097.14.862-Butanone (MEK) 5.00 70-13090.84.54Carbon Disulfide 5.00 70-13091.44.57Carbon Tetrachloride 5.00 70-13090.94.54Chlorobenzene 5.00 70-1301005.02Chloroethane 5.00 70-13092.94.65Chloroform 5.00 70-13097.04.85Chloromethane 5.00 70-13096.84.84Cyclohexane 5.00 70-13094.14.71Dibromochloromethane 5.00 70-13096.34.821,2-Dibromoethane (EDB) 5.00 70-13092.34.621,2-Dichlorobenzene 5.00 70-13090.94.551,3-Dichlorobenzene 5.00 70-13089.74.481,4-Dichlorobenzene 5.00 70-13089.04.45Dichlorodifluoromethane (Freon 12) 5.00 70-13093.74.691,1-Dichloroethane 5.00 70-13099.04.951,2-Dichloroethane 5.00 70-13091.94.591,1-Dichloroethylene 5.00 70-13095.64.78cis-1,2-Dichloroethylene 5.00 70-13095.84.79trans-1,2-Dichloroethylene 5.00 70-13096.04.801,2-Dichloropropane Page 16 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B235607 - TO-15 Prep LCS (B235607-BS1)Prepared & Analyzed: 07/15/19 5.00 70-13095.24.76cis-1,3-Dichloropropene 5.00 70-1301025.08trans-1,3-Dichloropropene 5.00 70-13083.84.191,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 5.00 70-1301145.681,4-Dioxane 5.00 70-1301045.18Ethanol 5.00 70-13097.64.88Ethyl Acetate 5.00 70-13093.64.68Ethylbenzene 5.00 70-13094.44.724-Ethyltoluene 5.00 70-13094.34.71Heptane 5.00 70-13089.14.46Hexachlorobutadiene 5.00 70-13098.94.94Hexane 5.00 70-1301025.122-Hexanone (MBK) 5.00 70-13099.54.98Isopropanol 5.00 70-13099.74.99Methyl tert-Butyl Ether (MTBE) 5.00 70-13090.14.51Methylene Chloride 5.00 70-13096.84.844-Methyl-2-pentanone (MIBK) 5.00 Z-0170-13080.74.04Naphthalene 5.00 70-13080.94.05Propene 5.00 70-1301025.11Styrene 5.00 70-13088.94.441,1,2,2-Tetrachloroethane 5.00 70-13090.04.50Tetrachloroethylene 5.00 70-1301175.83Tetrahydrofuran 5.00 70-13097.04.85Toluene 5.00 Z-0170-13092.14.601,2,4-Trichlorobenzene 5.00 70-13089.04.451,1,1-Trichloroethane 5.00 70-13098.14.901,1,2-Trichloroethane 5.00 70-13094.34.71Trichloroethylene 5.00 70-13097.24.86Trichlorofluoromethane (Freon 11) 5.00 70-13085.94.301,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 5.00 70-13093.14.651,2,4-Trimethylbenzene 5.00 70-13091.24.561,3,5-Trimethylbenzene 5.00 70-13095.94.79Vinyl Acetate 5.00 70-13090.14.51Vinyl Chloride 10.0 70-13092.09.20m&p-Xylene 5.00 70-13094.24.71o-Xylene 8.00 70-130Surrogate: 4-Bromofluorobenzene (1)99.97.99 Page 17 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B235636 - TO-15 Prep Blank (B235636-BLK1)Prepared & Analyzed: 07/16/19 1.4 UNDAcetone 0.035 UNDBenzene 0.035 UNDBenzyl chloride 0.035 UNDBromodichloromethane 0.035 UNDBromoform 0.035 UNDBromomethane 0.035 UND1,3-Butadiene 1.4 UND2-Butanone (MEK) 0.35 UNDCarbon Disulfide 0.035 UNDCarbon Tetrachloride 0.035 UNDChlorobenzene 0.035 UNDChloroethane 0.035 UNDChloroform 0.070 L-03, V-05, U NDChloromethane 0.035 UNDCyclohexane 0.035 UNDDibromochloromethane 0.035 UND1,2-Dibromoethane (EDB) 0.035 UND1,2-Dichlorobenzene 0.035 UND1,3-Dichlorobenzene 0.035 UND1,4-Dichlorobenzene 0.035 UNDDichlorodifluoromethane (Freon 12) 0.035 UND1,1-Dichloroethane 0.035 UND1,2-Dichloroethane 0.035 UND1,1-Dichloroethylene 0.035 UNDcis-1,2-Dichloroethylene 0.035 UNDtrans-1,2-Dichloroethylene 0.035 UND1,2-Dichloropropane 0.035 UNDcis-1,3-Dichloropropene 0.035 UNDtrans-1,3-Dichloropropene 0.035 UND1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 0.35 UND1,4-Dioxane 1.4 UNDEthanol 0.035 UNDEthyl Acetate 0.035 UNDEthylbenzene 0.035 UND4-Ethyltoluene 0.035 UNDHeptane 0.035 UNDHexachlorobutadiene 1.4 UNDHexane 0.035 UND2-Hexanone (MBK) 1.4 UNDIsopropanol 0.035 UNDMethyl tert-Butyl Ether (MTBE) 0.35 UNDMethylene Chloride 0.035 UND4-Methyl-2-pentanone (MIBK) 0.035 UNDNaphthalene Page 18 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B235636 - TO-15 Prep Blank (B235636-BLK1)Prepared & Analyzed: 07/16/19 1.4 V-05, Z-01a, U NDPropene 0.035 UNDStyrene 0.035 UND1,1,2,2-Tetrachloroethane 0.035 UNDTetrachloroethylene 0.035 UNDTetrahydrofuran 0.035 UNDToluene 0.035 UND1,2,4-Trichlorobenzene 0.035 UND1,1,1-Trichloroethane 0.035 UND1,1,2-Trichloroethane 0.035 UNDTrichloroethylene 0.14 UNDTrichlorofluoromethane (Freon 11) 0.14 UND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.035 UND1,2,4-Trimethylbenzene 0.035 UND1,3,5-Trimethylbenzene 0.70 UNDVinyl Acetate 0.035 UNDVinyl Chloride 0.070 UNDm&p-Xylene 0.035 UNDo-Xylene 8.00 70-130Surrogate: 4-Bromofluorobenzene (1)90.37.23 LCS (B235636-BS1)Prepared & Analyzed: 07/16/19 5.00 70-13083.94.20Acetone 5.00 70-13084.74.23Benzene 5.00 70-1301145.72Benzyl chloride 5.00 70-13091.54.57Bromodichloromethane 5.00 70-13091.94.60Bromoform 5.00 70-1301105.50Bromomethane 5.00 70-13091.84.591,3-Butadiene 5.00 70-13090.34.512-Butanone (MEK) 5.00 70-1301296.47Carbon Disulfide 5.00 70-13090.34.52Carbon Tetrachloride 5.00 70-13091.34.56Chlorobenzene 5.00 70-13092.34.62Chloroethane 5.00 70-1301226.08Chloroform 5.00 V-05, L-0370-13068.83.44Chloromethane * 5.00 70-13084.14.21Cyclohexane 5.00 70-13087.14.36Dibromochloromethane 5.00 70-13094.94.741,2-Dibromoethane (EDB) 5.00 70-13095.94.801,2-Dichlorobenzene 5.00 70-13097.94.901,3-Dichlorobenzene 5.00 70-13096.44.821,4-Dichlorobenzene 5.00 70-1301015.04Dichlorodifluoromethane (Freon 12) 5.00 70-1301035.151,1-Dichloroethane 5.00 70-1301246.221,2-Dichloroethane 5.00 70-1301035.171,1-Dichloroethylene Page 19 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B235636 - TO-15 Prep LCS (B235636-BS1)Prepared & Analyzed: 07/16/19 5.00 70-13098.74.94cis-1,2-Dichloroethylene 5.00 70-1301055.25trans-1,2-Dichloroethylene 5.00 70-13072.23.611,2-Dichloropropane 5.00 70-13085.64.28cis-1,3-Dichloropropene 5.00 70-13093.34.66trans-1,3-Dichloropropene 5.00 70-13093.44.671,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 5.00 70-1301035.171,4-Dioxane 5.00 70-1301045.20Ethanol 5.00 70-13074.43.72Ethyl Acetate 5.00 70-13090.44.52Ethylbenzene 5.00 70-13098.44.924-Ethyltoluene 5.00 70-13071.33.56Heptane 5.00 70-13078.03.90Hexachlorobutadiene 5.00 70-1301015.06Hexane 5.00 70-13072.63.632-Hexanone (MBK) 5.00 70-13082.94.14Isopropanol 5.00 70-1301195.96Methyl tert-Butyl Ether (MTBE) 5.00 70-13092.54.62Methylene Chloride 5.00 70-13072.43.624-Methyl-2-pentanone (MIBK) 5.00 70-1301045.22Naphthalene 5.00 V-05, Z-01a 70-13057.72.88Propene * 5.00 70-1301075.37Styrene 5.00 70-13092.44.621,1,2,2-Tetrachloroethane 5.00 70-13084.44.22Tetrachloroethylene 5.00 70-13095.44.77Tetrahydrofuran 5.00 70-13090.84.54Toluene 5.00 70-13090.34.521,2,4-Trichlorobenzene 5.00 70-13087.34.361,1,1-Trichloroethane 5.00 70-13093.74.691,1,2-Trichloroethane 5.00 70-13085.94.29Trichloroethylene 5.00 70-1301216.07Trichlorofluoromethane (Freon 11) 5.00 70-1301216.071,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 5.00 70-13097.54.881,2,4-Trimethylbenzene 5.00 70-1301015.031,3,5-Trimethylbenzene 5.00 L-01, V-3670-1301798.96Vinyl Acetate * 5.00 70-13084.34.22Vinyl Chloride 10.0 70-13099.19.91m&p-Xylene 5.00 70-13095.64.78o-Xylene 8.00 70-130Surrogate: 4-Bromofluorobenzene (1)91.87.35 Page 20 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY *QC result is outside of established limits. Wide recovery limits established for difficult compound. Wide RPD limits established for difficult compound. #Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency Percent Recovery% REC ND Not Detected Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. Not ApplicableN/A DL Detection Limit Not CalculatedNC LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation-Reduction Potential Not dry weight correctedwet Percent weight% wt KilogramKg Gramg Milligrammg Microgramg Nanogramng LiterL MillilitermL Microliter L Cubic Meterm3 Extractable Petroleum HydrocarbonsEPH Volatile Petroleum HydrocarbonsVPH Air Petroleum HydrocarbonsAPH Flame Ionization DetectorFID Photo Ionization DetectorPID Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). J Laboratory fortified blank /laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. L-01 Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the low side. L-03 Elevated reporting limit due to high concentration of target compounds.RL-11 Elevated reporting limit due to matrix interference.RL-12 Analyte included in the analysis, but not detectedU Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound. V-05 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. V-20 Page 21 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. V-36 Calibrations RSD for this compound is >30% but <40%.Z-01 Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in house limits of 50-150%. Z-01a ANALYST Thomas P. HniteckiTPH Raisa A. PetraitisRAP PDF Management StationSTATION Paula E. BlakeboroughPEB Kerry K. McGeeKKM Brittany R. FiskBRF Page 22 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 RTResponseInternal Standard Area %RT DiffResponse Reference RT Reference Area % Limits RT Diff Limit Q Initial Cal Check (S035866-ICV1 )Lab File ID: F1913421.D Analyzed: 05/15/19 07:19 Bromochloromethane (1)220675 8.627 224825 8.624 60 - 14098 0.0030 +/-0.50 1,4-Difluorobenzene (1)904687 10.392 914686 10.389 60 - 14099 0.0030 +/-0.50 Chlorobenzene-d5 (1)842982 14.756 837686 14.755 60 - 140101 0.0010 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 RTResponseInternal Standard Area %RT DiffResponse Reference RT Reference Area % Limits RT Diff Limit Q Initial Cal Check (S038098-ICV1 )Lab File ID: B1919519.D Analyzed: 07/14/19 22:24 Bromochloromethane (1)98205 5.067 101126 5.055 60 - 14097 0.0120 +/-0.50 1,4-Difluorobenzene (1)153800 6.275 151139 6.269 60 - 140102 0.0060 +/-0.50 Chlorobenzene-d5 (1)139472 9.862 138002 9.862 60 - 140101 0.0000 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 RTResponseInternal Standard Area %RT DiffResponse Reference RT Reference Area % Limits RT Diff Limit Q Calibration Check (S038140-CCV1 )Lab File ID: B1919604.D Analyzed: 07/15/19 12:11 Bromochloromethane (1)103304 5.057 101126 5.055 60 - 140102 0.0020 +/-0.50 1,4-Difluorobenzene (1)159830 6.271 151139 6.269 60 - 140106 0.0020 +/-0.50 Chlorobenzene-d5 (1)145432 9.864 138002 9.862 60 - 140105 0.0020 +/-0.50 LCS (B235607-BS1 )Lab File ID: B1919606.D Analyzed: 07/15/19 13:07 Bromochloromethane (1)101622 5.054 103304 5.057 60 - 14098 -0.0030 +/-0.50 1,4-Difluorobenzene (1)155433 6.274 159830 6.271 60 - 14097 0.0030 +/-0.50 Chlorobenzene-d5 (1)142473 9.861 145432 9.864 60 - 14098 -0.0030 +/-0.50 Blank (B235607-BLK1 )Lab File ID: B1919609.D Analyzed: 07/15/19 14:40 Bromochloromethane (1)95665 5.047 103304 5.057 60 - 14093 -0.0100 +/-0.50 1,4-Difluorobenzene (1)147743 6.267 159830 6.271 60 - 14092 -0.0040 +/-0.50 Chlorobenzene-d5 (1)129506 9.86 145432 9.864 60 - 14089 -0.0040 +/-0.50 B-2 DUP (19G0281-02RE1 )Lab File ID: B1919611.D Analyzed: 07/15/19 15:36 Bromochloromethane (1)96795 5.053 103304 5.057 60 - 14094 -0.0040 +/-0.50 1,4-Difluorobenzene (1)149264 6.273 159830 6.271 60 - 14093 0.0020 +/-0.50 Chlorobenzene-d5 (1)131968 9.86 145432 9.864 60 - 14091 -0.0040 +/-0.50 B-2 (19G0281-01 )Lab File ID: B1919638.D Analyzed: 07/16/19 09:13 Bromochloromethane (1)113027 5.049 103304 5.057 60 - 140109 -0.0080 +/-0.50 1,4-Difluorobenzene (1)180612 6.269 159830 6.271 60 - 140113 -0.0020 +/-0.50 Chlorobenzene-d5 (1)169062 9.856 145432 9.864 60 - 140116 -0.0080 +/-0.50 Page 23 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 RTResponseInternal Standard Area %RT DiffResponse Reference RT Reference Area % Limits RT Diff Limit Q B-2 (19G0281-01RE1 )Lab File ID: B1919640.D Analyzed: 07/16/19 10:12 Bromochloromethane (1)97472 5.048 103304 5.057 60 - 14094 -0.0090 +/-0.50 1,4-Difluorobenzene (1)164698 6.268 159830 6.271 60 - 140103 -0.0030 +/-0.50 Chlorobenzene-d5 (1)145490 9.856 145432 9.864 60 - 140100 -0.0080 +/-0.50 B-2 DUP (19G0281-02 )Lab File ID: B1919641.D Analyzed: 07/16/19 10:39 Bromochloromethane (1)102093 5.06 103304 5.057 60 - 14099 0.0030 +/-0.50 1,4-Difluorobenzene (1)167218 6.274 159830 6.271 60 - 140105 0.0030 +/-0.50 Chlorobenzene-d5 (1)152585 9.861 145432 9.864 60 - 140105 -0.0030 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 RTResponseInternal Standard Area %RT DiffResponse Reference RT Reference Area % Limits RT Diff Limit Q Calibration Check (S038157-CCV1 )Lab File ID: F1919704.D Analyzed: 07/16/19 11:03 Bromochloromethane (1)165643 8.627 224825 8.624 60 - 14074 0.0030 +/-0.50 1,4-Difluorobenzene (1)883956 10.396 914686 10.389 60 - 14097 0.0070 +/-0.50 Chlorobenzene-d5 (1)788396 14.752 837686 14.755 60 - 14094 -0.0030 +/-0.50 LCS (B235636-BS1 )Lab File ID: F1919707.D Analyzed: 07/16/19 13:03 Bromochloromethane (1)150987 8.621 165643 8.627 60 - 14091 -0.0060 +/-0.50 1,4-Difluorobenzene (1)828313 10.389 883956 10.396 60 - 14094 -0.0070 +/-0.50 Chlorobenzene-d5 (1)756055 14.752 788396 14.752 60 - 14096 0.0000 +/-0.50 Blank (B235636-BLK1 )Lab File ID: F1919709.D Analyzed: 07/16/19 14:27 Bromochloromethane (1)153525 8.627 165643 8.627 60 - 14093 0.0000 +/-0.50 1,4-Difluorobenzene (1)799471 10.389 883956 10.396 60 - 14090 -0.0070 +/-0.50 Chlorobenzene-d5 (1)712905 14.749 788396 14.752 60 - 14090 -0.0030 +/-0.50 B-4 (19G0281-03 )Lab File ID: F1919710.D Analyzed: 07/16/19 15:13 Bromochloromethane (1)146941 8.624 165643 8.627 60 - 14089 -0.0030 +/-0.50 1,4-Difluorobenzene (1)792518 10.386 883956 10.396 60 - 14090 -0.0100 +/-0.50 Chlorobenzene-d5 (1)712950 14.752 788396 14.752 60 - 14090 0.0000 +/-0.50 B-7 (19G0281-04 )Lab File ID: F1919711.D Analyzed: 07/16/19 15:48 Bromochloromethane (1)162268 8.624 165643 8.627 60 - 14098 -0.0030 +/-0.50 1,4-Difluorobenzene (1)870641 10.389 883956 10.396 60 - 14098 -0.0070 +/-0.50 Chlorobenzene-d5 (1)746873 14.749 788396 14.752 60 - 14095 -0.0030 +/-0.50 Page 24 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S038140-CCV1 COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR STD 0.9523581A -4.6 304.77 0.99831585.00Acetone 0.9076544A -1.7 304.92 0.92338115.00Benzene 0.8019693A 5.0 305.25 0.76363885.00Benzyl chloride 0.6376275A -3.9 304.81 0.66333885.00Bromodichloromethane 0.4765829A 14.5 305.72 0.41630945.00Bromoform 0.6722218A -3.3 304.83 0.69535125.00Bromomethane 0.5467513A -0.3 304.98 0.54861855.001,3-Butadiene 1.303198A 1.2 305.06 1.2883785.002-Butanone (MEK) 1.584821A -12.0 304.40 1.8012625.00Carbon Disulfide 0.4796897A -1.7 304.92 0.48799245.00Carbon Tetrachloride 0.7001485A -1.7 304.92 0.71212895.00Chlorobenzene 0.4509719A 2.4 305.12 0.44027075.00Chloroethane 0.93069A -2.1 304.90 0.95016935.00Chloroform 0.6453032A 5.5 305.27 0.61181075.00Chloromethane 0.3931377A 1.4 305.07 0.38765155.00Cyclohexane 0.5629353A 3.2 305.16 0.54564225.00Dibromochloromethane 0.4896419A 4.1 305.21 0.47017375.001,2-Dibromoethane (EDB) 0.4622476A 1.0 305.05 0.45772785.001,2-Dichlorobenzene 0.5113593A 0.09 305.00 0.5109155.001,3-Dichlorobenzene 0.5214148A 1.5 305.08 0.51367775.001,4-Dichlorobenzene 1.233083A -5.3 304.74 1.301815.00Dichlorodifluoromethane (Freon 12) 0.9222179A -2.9 304.86 0.94970575.001,1-Dichloroethane 0.6650972A 4.0 305.20 0.63970315.001,2-Dichloroethane 1.045768A -7.7 304.62 1.1331135.001,1-Dichloroethylene 0.6969411A 2.0 305.10 0.68320495.00cis-1,2-Dichloroethylene 0.7397042A 0.2 305.01 0.73837235.00trans-1,2-Dichloroethylene 0.3558181A 1.4 305.07 0.35087115.001,2-Dichloropropane 0.5767828A 7.1 305.36 0.53846395.00cis-1,3-Dichloropropene 0.5197322A 7.9 305.40 0.48152295.00trans-1,3-Dichloropropene 1.258468A -7.5 304.62 1.3611965.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 0.1473766A 8.0 305.40 0.13652265.001,4-Dioxane 0.2210331A 3.5 305.18 0.21357515.00Ethanol 0.2274762A 8.2 305.41 0.21016475.00Ethyl Acetate 1.219011A 1.6 305.08 1.1995225.00Ethylbenzene 1.085153A 3.1 305.15 1.0527155.004-Ethyltoluene 0.3245548A 0.7 305.04 0.32223955.00Heptane 0.2973321A 16.8 305.84 0.25448885.00Hexachlorobutadiene 0.4153953L 3.3 305.16 0.42550445.00Hexane Page 25 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S038140-CCV1 COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR STD 0.9736839A 7.9 305.40 0.90238725.002-Hexanone (MBK) 0.9479284A 3.5 305.17 0.91599175.00Isopropanol 1.356137A 5.3 305.27 1.2876815.00Methyl tert-Butyl Ether (MTBE) 0.7066677A -5.6 304.72 0.7489545.00Methylene Chloride 1.029744A 2.2 305.11 1.0071165.004-Methyl-2-pentanone (MIBK) 0.7457726A 8.7 305.44 0.68581415.00Naphthalene 0.5818942A -9.2 304.54 0.64069955.00Propene 0.6686066A 12.2 305.61 0.59591755.00Styrene 0.8087574A -2.5 304.88 0.82935315.001,1,2,2-Tetrachloroethane 0.3431212A -2.5 304.87 0.35201115.00Tetrachloroethylene 0.7996747A 15.5 305.78 0.69223985.00Tetrahydrofuran 0.8959679A 2.6 305.13 0.87349125.00Toluene 0.3193795A 24.0 306.20 0.25755335.001,2,4-Trichlorobenzene 0.4782381A 0.6 305.03 0.47552485.001,1,1-Trichloroethane 0.3139667A 5.1 305.26 0.29865775.001,1,2-Trichloroethane 0.2927911A -0.8 304.96 0.29518325.00Trichloroethylene 1.435189A 4.8 305.24 1.3692265.00Trichlorofluoromethane (Freon 11) 0.8398668A -13.2 304.34 0.96803485.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.8410804A 5.0 305.25 0.80123525.001,2,4-Trimethylbenzene 0.8735354A 4.0 305.20 0.84013145.001,3,5-Trimethylbenzene 1.751336A 3.9 305.20 1.6854815.00Vinyl Acetate 0.6747928A -0.9 304.96 0.68084435.00Vinyl Chloride 0.9317454A -0.5 309.95 0.936281710.0m&p-Xylene 0.8720392A 2.8 305.14 0.84797845.00o-Xylene * Values outside of QC limits # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk Page 26 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S038157-CCV1 COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR STD 0.9358826A -17.5 304.12 1.1342935.00Acetone 0.5073393A -10.8 304.46 0.56882175.00Benzene 0.8994546A 21.5 306.07 0.74047935.00Benzyl chloride 0.4318459A -2.8 304.86 0.44444915.00Bromodichloromethane 0.4953896A -2.7 304.86 0.50911555.00Bromoform 1.078763A 8.3 305.42 0.99588145.00Bromomethane 0.5937299A -8.9 304.56 0.65156525.001,3-Butadiene 1.069925A -7.9 304.61 1.1615115.002-Butanone (MEK) 2.474411A 24.9 306.24 1.9813125.00Carbon Disulfide 0.4355764A -4.6 304.77 0.45665715.00Carbon Tetrachloride 0.7144389A -1.5 304.92 0.72559235.00Chlorobenzene 0.4061168A -6.6 304.67 0.43470765.00Chloroethane 2.054848A 23.6 306.18 1.6622165.00Chloroform 0.7475354A -31.6 *303.42 1.0930385.00Chloromethane 0.2231134A -13.2 304.34 0.25715745.00Cyclohexane 0.5499409A -5.5 304.73 0.58179985.00Dibromochloromethane 0.4667502A 1.3 305.07 0.46054095.001,2-Dibromoethane (EDB) 0.6477415A -0.5 304.98 0.65087035.001,2-Dichlorobenzene 0.7151432A 3.1 305.16 0.69334585.001,3-Dichlorobenzene 0.7135399A 1.8 305.09 0.70074965.001,4-Dichlorobenzene 2.768624A -2.1 304.89 2.8286685.00Dichlorodifluoromethane (Freon 12) 1.347293A 3.8 305.19 1.2978485.001,1-Dichloroethane 1.128634A 23.8 306.19 0.91199525.001,2-Dichloroethane 1.167813A 6.0 305.30 1.1015455.001,1-Dichloroethylene 0.9436101A 4.2 305.21 0.90518535.00cis-1,2-Dichloroethylene 0.9926311A 8.9 305.45 0.9111535.00trans-1,2-Dichloroethylene 0.1536384A -25.2 303.74 0.205365.001,2-Dichloropropane 0.3031753A -4.3 304.79 0.31675885.00cis-1,3-Dichloropropene 0.2653055A -2.7 304.86 0.27269745.00trans-1,3-Dichloropropene 2.947544A -0.8 304.96 2.9708225.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 0.1098933A -5.9 304.70 0.11680365.001,4-Dioxane 0.1375392A -11.9 304.40 0.15616835.00Ethanol 0.1855653A -20.3 303.98 0.23286445.00Ethyl Acetate 0.9856712A -2.4 304.88 1.0098235.00Ethylbenzene 1.187101A 7.3 305.36 1.1064535.004-Ethyltoluene 0.1155008A -21.2 303.94 0.14666155.00Heptane 0.3601053A -14.1 304.30 0.41914395.00Hexachlorobutadiene 0.639631L 1.2 305.06 0.67336385.00Hexane Page 27 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S038157-CCV1 COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR STD 0.2497141A -24.0 303.80 0.32842495.002-Hexanone (MBK) 0.9403355A -17.9 304.10 1.1452925.00Isopropanol 2.294969A 19.7 305.98 1.9174845.00Methyl tert-Butyl Ether (MTBE) 0.6947761A -8.3 304.58 0.75794435.00Methylene Chloride 0.1129758A -24.7 303.76 0.15008715.004-Methyl-2-pentanone (MIBK) 1.217782A 12.6 305.63 1.0816855.00Naphthalene 0.7123947A -42.1 *302.90 1.2302855.00Propene 0.6821019A 17.6 305.88 0.57988175.00Styrene 0.5875869A -2.2 304.89 0.60050275.001,1,2,2-Tetrachloroethane 0.3767751A -11.6 304.42 0.42617085.00Tetrachloroethylene 0.5288772A -5.7 304.72 0.56089265.00Tetrahydrofuran 0.7638882A -2.5 304.88 0.78317865.00Toluene 0.486316A -1.8 304.91 0.49501185.001,2,4-Trichlorobenzene 0.4209024A -0.2 304.99 0.42183665.001,1,1-Trichloroethane 0.287417A -0.6 304.97 0.28915135.001,1,2-Trichloroethane 0.2623407A -8.9 304.56 0.28798835.00Trichloroethylene 2.605729A 20.7 306.04 2.1587395.00Trichlorofluoromethane (Freon 11) 2.203756A 22.3 306.12 1.8017425.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1.007518A 7.3 305.37 0.93880775.001,2,4-Trimethylbenzene 1.011167A 8.1 305.41 0.93512725.001,3,5-Trimethylbenzene 1.749266A 87.1 *309.36 0.93478025.00Vinyl Acetate 0.9039875A -14.7 304.26 1.060395.00Vinyl Chloride 0.7846321A -0.6 309.94 0.78923210.0m&p-Xylene 0.8096824A 1.6 305.08 0.79667485.00o-Xylene * Values outside of QC limits # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk Page 28 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA TO-15 in Air AIHA,NY,ME,NHAcetone AIHA,FL,NJ,NY,ME,NH,VABenzene AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride AIHA,NJ,NY,ME,NH,VABromodichloromethane AIHA,NJ,NY,ME,NH,VABromoform AIHA,FL,NJ,NY,ME,NHBromomethane AIHA,NJ,NY,ME,NH,VA1,3-Butadiene AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK) AIHA,NJ,NY,ME,NH,VACarbon Disulfide AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene AIHA,FL,NJ,NY,ME,NH,VAChloroethane AIHA,FL,NJ,NY,ME,NH,VAChloroform AIHA,FL,NJ,NY,ME,NH,VAChloromethane AIHA,NJ,NY,ME,NH,VACyclohexane AIHA,NY,ME,NHDibromochloromethane AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB) AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12) AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene AIHA,NY,ME,NHtrans-1,3-Dichloropropene AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) AIHA,NJ,NY,ME,NH,VA1,4-Dioxane AIHAEthanol AIHAEthyl Acetate AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene AIHA,NJ4-Ethyltoluene AIHA,NJ,NY,ME,NH,VAHeptane AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene AIHA,FL,NJ,NY,ME,NH,VAHexane AIHA2-Hexanone (MBK) AIHA,NY,ME,NHIsopropanol AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE) AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK) NY,ME,NHNaphthalene AIHAPropene AIHA,FL,NJ,NY,ME,NH,VAStyrene AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane Page 29 of 33 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA TO-15 in Air AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene AIHATetrahydrofuran AIHA,FL,NJ,NY,ME,NH,VAToluene AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11) AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene AIHA,FL,NJ,NY,ME,NH,VAo-Xylene The CON-TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires 100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020 M-MA100Massachusetts DEPMA 06/30/2020 PH-0567Connecticut Department of Publilc HealthCT 09/30/2019 10899 NELAPNew York State Department of HealthNY 04/1/2020 2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020 LAO00112Rhode Island Department of HealthRI 12/30/2019 652North Carolina Div. of Water QualityNC 12/31/2019 MA007 NELAPNew Jersey DEPNJ 06/30/2020 E871027 NELAPFlorida Department of HealthFL 06/30/2020 LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020 2011028State of MaineME 06/9/2021 460217Commonwealth of VirginiaVA 12/14/2019 2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2019 VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020 25703North Carolina Department of HealthNC-DW 07/31/2019 68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020 Page 30 of 33 Page 31 of 33 Page 32 of 33 Page 33 of 33                         Appendix D  Monitoring Well Records     Stefan Smith 3576A SAEDACCO Inc X 7-5-2019 MW-2R Barringer Homes 510 W. Tremont Avenue, Charlotte, NC, 28203 Mecklenburg 35.211737 80.868786 X X 1 30 8" HSA 0 20'2"SCH-40 PVC 20'30'2".010 SCH-40 PVC 0 16'Aquaguard Tremie 18'30'Sand #2 0 8'Brown silt (fill) 8'13'Brown sandy silt (fill) 13'30'Black damp...silt with organtics 2 foot bentonite seal from 16 to 18 feet 7/9/2019 Stefan Smith 3576A SAEDACCO Inc X 7-5-2019 MW-3R Barringer Homes 510 W. Tremont Avenue, Charlotte, NC, 28203 Mecklenburg 35.211860 80.868481 X X 1 35' 8" HSA 0 25'2"SCH-40 PVC 25'35'2".010 SCH-40 PVC 0 21'Aquaguard Tremie 23'35'Sand #2 0 8'Brown silt (fill) 8'13'Brown sandy silt (fill) 13'35'Black damp...silt with organtics 2 foot bentonite seal from 21 to 23 feet 7/9/2019 Stefan Smith 3576A SAEDACCO Inc X 7-5-2019 MW-4R Barringer Homes 510 W. Tremont Avenue, Charlotte, NC, 28203 Mecklenburg 35.211443 80.868704 X X 1 35 8" HSA 0 25'2"SCH-40 PVC 25'35'2".010 SCH-40 PVC 0 21'Aquaguard Tremie 23'35'Sand #2 0 8'Brown silt (fill) 8'13'Brown sandy silt (fill) 13'35'Black damp...silt with organtics 2 foot bentonite seal from 21 to 23 feet 7/9/2019                         Appendix E  Brownfield Receptor Survey    North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Rev. 09/2015 Page 1 of 3 BROWNFIELDS PROPERTY RECEPTOR SURVEY This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information requested below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ Brownfield’s Project Manager (PM). Site: 510 West Tremont/ Barringer Homes Address: 510 West Tremont Avenue City: Charlotte County: Mecklenburg Brownfields Project Number: 21033-17-060 Date: 4 June 2019 Property and Building Characteristics Surface Conditions Current Usage Proposed Usage Size of Property (acres) 1.9 NA % of property that is wooded/brush 10% 0% % of property that is grassed areas 90% 10% % of property that is agricultural crops 0% 0% % of property that is paved 0% 5% % of property that is covered by buildings 0% 80% If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may be needed. a. Provide occupancy and use information. N/A No buildings are on-site b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings (e.g. windows, bay doors), and height (number of stories). N/A c. Describe the foundation construction. Include details on type, floor construction, and depth below grade. N/A d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design considerations (e.g. positive pressure?). N/A e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details. N/A North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Rev. 09/2015 Page 2 of 3 Surrounding Property Land Use Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If specific receptors are present, please provide addresses of the facilities. Zoning/Land Use Current Use/Occupant Proposed Usage North Undeveloped Residential townhomes South Tremont Ave Tremont Ave East Residential townhomes Residential townhomes West vacant unknown Specific Land Uses of Interest Y/N * Distance (ft) Direction Address Is a school or daycare center within 1,000 ft of the N n/a n/a n/a Is there a residence within 1,000 ft of the Property? Y 300 ft. N Multiple Is there a basement within 1,000 ft of the Property N n/a n/a n/a * If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses. Utilities For the subject property, please provide a map of known buried utilities. If available, include depth to top, construction material, and diameter of the utilities. In addition, please provide the following information on utility providers. If additional assessment is required, the public utility locators should be contacted. This information can then be added to a site map. Is there a septic system on-site? (Y or N) N Please provide the utility providers for the subject property a. Natural Gas Duke/ Piedmont b. Sewer Charlotte Water c. Electricity Duke Energy d. Other n/a For surrounding properties, please complete the following table with available information. Utility/Potential Receptor Y/N * Distance (ft) Direction Is a storm water pipe within 100 ft of the Property boundary? N n/a n/a Is a sanitary sewer within 100 ft of the Property boundary? Y 50 S Is a septic system leach field within 500 ft of the Property boundary? N n/a n/a Is a water line main within 100 ft of Property boundary? Y 10 S Is a natural gas line main within 100 ft of the Property boundary? Y 20 S Is a buried telephone/ cable main within 100 ft of the Property boundary? N n/a n/a Is a buried electrical cable main within 100 ft of Property boundary? N n/a n/a * If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject property. North Carolina Department of Environmental Quality Division of Waste Management Brownfields Program Rev. 09/2015 Page 3 of 3 Water Supply The purpose of this section is to provide information on the water supply for the site and surrounding areas. What is the potable water supply for the property? Public Charlotte Water Private If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the water providers name. n/a Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation wells may be present. Information from applicable databases can and should be utilized; however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested radius, please provide a map of the well locations. If needed, please attach a separate table to list all wells. Please note, the PM may opt for a more extensive water supply well survey if needed. Water Supply Wells Y/N Distance (ft) Direction Address Is a public water supply well within 1 mile of the Property boundary? N n/a n/a n/a Is a private water supply well within 1,500 ft of the Property N n/a n/a n/a Is an irrigation well within 1,500 ft of the Property boundary? N n/a n/a n/a Surface Water & Wetlands The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the Property. Provide Information regarding Surface Water and Wetlands Response/Comments Are there surface water features on the property? (If yes, please complete a. to d.) No a. Is the water body naturally developed or man-made? n/a b. List the uses of the water body. n/a c. What is the source of the water for the water body? n/a d. What is the nature of the bottom of the water body (e.g., rocky or concrete bottom, drainage ways or impoundments) n/a If no on-site surface water features, what is the nearest surface water body? Irwin Creek approx. 2,000 ft west of the property Are there any wetlands present on the property? If no wetlands on-site, are wetlands suspected on adjoining properties? No Drawn: BTO  Scale: As Shown  Project No.: 63X‐0084 Checked: BTO Date: 6/10/2019  Drawing No.: 1 Site Location Map Adams Property Brownfields Project No.: 21022‐17‐060 N Wendys BP Gasoline,  McDonald's Approximate  Brownfields Limit FROEHLING & ROBERTSON, INC. Engineering Stability Since 1881 3300 International Airport Drive, Suite 600 Charlotte, North Carolina  28208 T 704.596.2889 I F 704.596.3784 Drawn: KNW  Scale: NTS  Project No.: 63X0084 Checked: BTO Date: 6/4/2019  Drawing No.: 2 Receptor Features & Buffers Map Barringer Homes Brownfields Project No.: 21022‐17‐060 Wendys BP Gasoline,  McDonald's FROEHLING & ROBERTSON, INC. Engineering Stability Since 1881 2505 Hutchison‐McDonald Road Charlotte, North Carolina  28269 T 704.596.2889 I F 704.596.3784 N 500 ft. buffer 1,000 ft. buffer Approximate  location of  utilities (Water,  Gas,  and  Sanitary Sewer) 200ft200ft200ft200ft200ft + – 1,444,683.198 537,986.915 Feet Find Address, Street, or PID Well Information System 4.0 Mecklenburg County Health Dept. / LUESA-GIS GWS Home Page Layer List Active Inactive Permanent Abandoned Temporary Abandoned Unknown Community Non-Transient Transient Active Inactive Permanent Abandoned Temporary Abandoned GWMPL LF MPL Groundwater/Wastewater Ambient_Wells Private_Wells Public_Wells Monitoring_Wells SIPs Issued MPL_SITES Countywide NC Public Water Supply Map Esri, HERE, Garmin, (c) OpenStreetMap contributors, and the GIS user community 6/4/2019, 10:10:41 AM 0 0.15 0.30.07 mi 0 0.25 0.50.13 km 1:9,028 NC Public Water SupplyCity of Charlotte, State of North Carolina DOT, Esri, HERE, Garmin, INCREMENT P, NGA, USGS | City of Charlotte, State of North Carolina DOT, Esri, HERE | 00000 300300300300300 600ft600ft600ft600ft600ft + – Find address or place Legend Surface Water Sources Surface Water Community Surface Water Non-Transient Non-Community Ground Water Community Ground Water Non-Transient Non-Community Ground Water Transient Non-Community Ground Water Adjacent Ground Water Sources Groundwater_Sources_2015 Ground Water Community Ground Water Non-Transient Non-Community Ground Water Transient Non-Community Ground Water Adjacent All PWS Sources All PWS Sources 2015 Surface Water Community Surface Water Non-Transient Non-Community Ground Water Community Ground Water Non-Transient Non-Community Ground Water Transient Non-Community Ground Water Adjacent SWAPInfo 2.0 Get SWAP Reports SWAP Data Info Tool Instructions Contacts