HomeMy WebLinkAbout22018_2019-5-03 Indoor Air Quality Assessment ReportINDOOR AIR QUALITY MONITORING REPORT
PARKER LINCOLN PROPERTY
2728 CAPITAL BOULEVARD
RALEIGH, WAKE COUNTY, NORTH CAROLINA
Prepared For:
SharpVue Capital
700 Spring Forest Road, Suite 105
Raleigh, North Carolina 27609
Prepared By:
Mid -Atlantic Associates, Inc.
409 Rogers View Court
Raleigh, North Carolina 27610
Mid -Atlantic Job No. OOOR2980.05
May 3, 2019
Atlantic.,.
0
Mid Atlantic
Engineering & Environmental Solutions
409 Rogers View Court
Raleigh, NC 271610
office 919.250 9918
fav smile 919,250 9950
MAAONLINE COM
INDOOR AIR QUALITY MONITORING REPORT
PARKER LINCOLN PROPERTY
2728 CAPITAL BOULEVARD
RALEIGH, WAKE COUNTY, NORTH CAROLINA
May 3, 2019
Mid -Atlantic Job No. OOOR2980.05
Prepared For:
SharpVue Capital
Attn: Frederic F. Faizon
700 Spring Forest Road, Suite 105
Raleigh, North Carolina 27608
Prepared By:
MID -ATLANTIC ASSOCIATES, INC.
Darin M. McClure, PE
Principal Eng
l�
Mid Atlantic
TABLE OF CONTENTS
1.0 GENERAL INFORMATION AND BACKGROUND................................................1
2.0 SUMMARY OF FIELD ACTIVITIES.......................................................................1
2.1 Preliminary Site Reconnaissance................................................................. 1
2.2 Initial and Follow Up Air Sample Collection .................................................. 2
2.2.1 Radiello® Seven -Day Air Sample Collection ................................................ 2
2.2.2 Summa Canister Eight -Hour Air Sample Collection ...................................... 3
3.0 LABORATORY ANALYTICAL RESULTS............................................................. 3
3.1 Risk Evaluation Methodology....................................................................... 3
3.2 Indoor Air Screening Levels (Tier 1)............................................................. 4
3.3 Indoor Air Risk Calculations (Tier 2)............................................................. 4
4.0 REMEDIAL ACTIONS AND FOLLOW UP TESTING............................................5
4.1 GEM Indoor Air Screening Levels (Tier 1).................................................... 6
4.2 GEM Indoor Air Risk Calculations (Tier 2).................................................... 6
5.0 SUMMARY AND CONCLUSIONS......................................................................... 6
DRAWINGS
Drawing 1.1
Topographic Site Map
Drawing 1.2
Site Map
Drawing 2.1
Air Sample Location Map
TABLES
Table 2.1
Air Sample Locations and Tenant Space Occupants
Table 3.1
Summary of Chemical Constituents Detected in Indoor Air and Risk
Calculations February 2019
Table 3.2
Summary of Chemical Constituents Detected in Indoor Air and Risk
Calculations March 2019
APPENDICES
Appendix A
Indoor Air Building Survey and Sampling Form & Observation Form
Appendix B
February 2019 Laboratory Analytical Report and Chain of Custody
Appendix C
March 2019 Laboratory Analytical Reports and Chains of Custody
Appendix D
Indoor Air DEQ Risk Calculator Summary Sheets
�� Atlantic
1.0 GENERAL INFORMATION AND BACKGROUND
The subject site consists of one parcel totaling approximately 32.33 acres located along
Capital Boulevard and Westinghouse Boulevard in Raleigh, Wake County, North Carolina
(Drawing 1.1 and Drawing 1.2). The subject site is currently occupied by one 546,791-
square foot structure and associated parking lots. The structure is occupied by six tenants,
with some of the spaces being unoccupied at the time of these activities. The current
tenants include the North Carolina Education Lottery (Lottery), Inventory Management
Incorporated (IMI), Reico Kitchen and Bath (Reico), Web -Don, Inc., Habitat for Humanity of
Wake County (Habitat), and Great Escape Millwork, Inc. (GEM).
During performance of several investigations at the site, it was determined that past
operations have had an adverse environmental impact on the site. More specifically, it was
determined that a vapor intrusion condition appears to exist at the site. SVC 2728 Capital
Partners, LLC (SVC) submitted an application to the North Carolina Brownfields Program
(NCBP) on April 3, 2018 and received their Letter of Eligibility on June 1, 2018. The project
is currently working its way through the brownfield process.
Since vapor intrusion conditions are known to exist at the site, an Indoor Air Quality
Monitoring Work Plan (Work Plan) dated October 4, 2018 was developed by Mid -Atlantic
and the NCBP. At your request, Mid -Atlantic has conducted indoor air quality monitoring
services in general accordance with the referenced Work Plan and our proposal to you
dated August 28, 2018. One significant change to this Work Plan was implemented and
that change was to increase the sampling frequency from semi-annually to quarterly.
2.0 SUMMARY OF FIELD ACTIVITIES
2.1 Preliminary Site Reconnaissance
On February 19, 2019, Mid -Atlantic personnel conducted a reconnaissance visit to the
site to inspect sampling locations and place Radiello® samplers. Mid -Atlantic personnel
were accompanied by the site property manager, Lowell Lovell and Marian Kozek
(facilities manager for the Lottery space). During this visit, Mid -Atlantic personnel
completed the Indoor Air Building Survey and Sampling Form as presented in the North
Carolina Department of Environmental Quality (NCDEQ) Division of Waste
Management's (DWM) Vapor Intrusion Guidance Document (March 2018). A copy of
this form is included in Appendix A. The sample locations are identified on Drawing 2.1
and Table 2.1 presents the tenant space occupants for each of the indoor air samples.
Additionally, as per the activities outlined in the referenced Work Plan, during the site
reconnaissance Mid -Atlantic observed the floor slab of the warehouse spaces for
indications that it had been breached. These observations were recorded on February
19, 2019 and are included in Appendix A. No breaches were identified.
Mid Atlantic
Indoor Air Quality Monitoring Report
Parker Lincoln Property
Raleigh, North Carolina
May 3, 2019
Page 2
Mid -Atlantic's reconnaissance included an inspection of the HVAC fresh air system for
the southeast corner space (Web -Don). The inspection confirmed the air handing units
(AHU) controls were in the same location as previously set (estimated to be 30% fresh
air make up). The controls for these units are located above the ceiling and are labelled
with instructions prohibiting the disturbance of the controls.
2.2 Initial and Follow Up Air Sample Collection
Initial air sampling (February 19-26, 2019) was accomplished using Radiello® samples.
The indoor Radiello® air samplers were placed in locations throughout the building
including areas where previous assessment findings identified elevated contaminants in
sub -slab soil gas. All Radiello® samplers were exposed for approximately seven days.
The samplers were placed in the breathing zone (3 to 6 feet above the floor) for seated
and standing building occupants. The air sample locations are illustrated on Drawing 2.1
and the respective spaces are detailed in Table 2.1.
2.2.1 Radiello® Seven -Day Air Sample Collection
On February 19, 2019, a total of 11 Radiello® air samplers were placed at the subject
site; 10 were placed to collect indoor air samples (IA-103R, IA-106R, IA-107R, IA-11OR,
and IA-113R through IA-118R) and one was placed to collect an air sample outside the
building (OA-102R). The Radiello® air sampler (OA-102R) was placed outside the south
side of the building near the southeast corner (between the Habitat and Web -Don
spaces). The outdoor air sample was collected to provide a comparison with the indoor
air quality results.
The Radiello® diffusive air samplers were deployed in accordance with the
manufacturer instructions and the NCDEQ DWM Vapor Intrusion Guidance Document
(March 2018). The sampling cartridge was removed from its plastic sleeve and placed
into the diffuser, the end of the cartridge was positioned in the seat, and the diffuser was
then screwed into the supporting plate. The cartridges were collected seven days later
on February 26, 2019. The diffusers were unscrewed from the plates, the sampling
cartridges replaced into their original tubes, the tubes properly labeled, and placed back
into their corresponding plastic bags.
After collection, the Radiello® air samplers were shipped to Con -test Analytical
Laboratory in East Longmeadow, Massachusetts under proper chain of custody for
analysis. The cartridges were analyzed for tetrachloroethene (PCE), trichloroethene
(TCE), 1,1-dichloroethene, trans- 1,2-dichloroethene, cis-1,2-dichloroethene and vinyl
chloride in accordance with EPA Method Rad 130.
Mid Atlantic
Indoor Air Quality Monitoring Report
Parker Lincoln Property
Raleigh, North Carolina
May 3, 2019
Page 3
Based on the results of the initial sampling (February 19-26, 2019), follow up sampling
using Radiellos® and Summa canisters was conducted in the GEM space (see Section
4.0 for details). Three additional indoor air (IA-107RR, IA-119RR and IA-120RR)
samples and one outdoor sample (OA-103RR) were collected over the period of March
15 to March 22, 2019. These Radiello® cartridges were also analyzed for
tetrachloroethene (PCE), tichloroethene (TCE), 1, 1 -dichloroethene, trans-1,2-
dichloroethene, cis-1,2-dichloroethene and vinyl chloride in accordance with EPA
Method Rad 130.
2.2.2 Summa Canister Eight -Hour Air Sample Collection
Follow up sampling (March 15 to 22, 2019) was also conducted using Summa canisters
at three indoor air sample locations (IA-107SR, IA-119SR, and IA-120SR) in the GEM
space. These samples were collected, along with outdoor air sample OA-103SR,
concurrently with the follow up Radiello® samples. These 8-hour samples were
collected in order to provide indoor air quality data rapidly and to provide a comparison
between the different sampling methodologies. They were deployed in the morning of
March 15, 2019 and were collected approximately eight hours later. These sample
locations are also illustrated on Drawing 2.1.
After collection, the air samples were shipped to Con -test Analytical Laboratory in East
Longmeadow, Massachusetts under proper chain of custody for analysis. The air
samples were analyzed for VOCs in accordance with EPA Method TO-15.
3.0 LABORATORY ANALYTICAL RESULTS
The laboratory analytical reports and chain -of -custody records for the Radiello® air
samples collected from February 19 to February 26, 2019 (initial sampling) are provided in
Appendix B and summarized in Table 3.1. The results of the Radiello® and Summa
canister collected samples collected from March 15 to March 22, 2019 (follow up sampling)
from the GEM space are summarized in Table 3.2 and included in Appendix C. Both the
initial and follow up sampling indoor air analytical results were compared to the DWM Non -
Residential Indoor Air Screening Levels (IASLs) February 2018 Table.
3.1 Risk Evaluation Methodology
The NCDEQ has developed a tier -based Technical Guidance Document for Risk -Based
Environmental Remediation of Sites (March 2017). Tier 1, the first step in establishing risk
assessment, is to compare the individual contaminant concentrations detected at the site to
the vapor intrusion and indoor air screening levels established by the DWM. The DWM
establishes screening levels for individual compounds for Non -Residential
(industrial/commercial) exposure scenarios.
Mid Atlantic
Indoor Air Quality Monitoring Report
Parker Lincoln Property
Raleigh, North Carolina
May 3, 2019
Page 4
When the concentrations of contaminants detected at the site exceed the screening levels
for all pathways established by the DWM, the Tier 2 evaluation is required. For a Tier 2
evaluation, the cumulative risk is calculated by entering the maximum concentrations of all
contaminants detected at each established exposure unit (EU) into the DEQ Risk
Calculator (October 2017). An EU is a defined area of a site represented by a specific set
of land use(s), receptors, contaminant concentrations, and exposure pathways. Due to the
size of the onsite structure, the distance between sample locations and the potential for the
future use of the building areas to change, exposure units were not used during this
assessment and risk calculations were performed on concentrations detected at each
sample location.
The DEQ Risk Calculator determines the cancer risk sum for all carcinogens and the
cumulative hazard index for all non -carcinogens. The DWM allows a maximum cancer risk
sum for all carcinogens of 1.0E-04 and a maximum cumulative hazard index (HI) of 1.0 for
all non -carcinogens in each exposure pathway. The HI is the sum of the hazard quotient
(HQs) calculated for each compound detected above the reporting limit. The NCDEQ risk
calculations for the subject site are included in Appendix D. The results of the Tier 1 and
Tier 2 evaluations for indoor air exposure pathway is summarized in Table 3.1 and Table
4.1, and are discussed below.
3.2 Indoor Air Screening Levels (Tier 1)
As summarized in Table 3.1, trichloroethene was detected above the laboratory MDL in 7
of the 10 indoor air Radiello® samples; the exceptions were IA-103R, IA-117R, and IA-
118R. TCE was not detected above the laboratory MDL in OA-102R. Seven of the indoor
air samples exhibited levels in excess of the NCDEQ Non -Residential Indoor Air Screening
Levels (IASLs). These included IA-106R, IA-107R, IA-110R, IA-113R, IA-114R, IA-115R,
and IA-116R.
Tetrachloroethene was detected above the laboratory MDL in 8 of the 10 indoor air
Radiello® samples; the exceptions were IA-117R and IA-118R. PCE was not detected
above the laboratory MDL in OA-102R. None of the indoor air samples exhibited levels in
excess of the NCDEQ IASLs.
3.3 Indoor Air Risk Calculations (Tier 2)
As summarized in Table 3.1, the Non -Residential cancer risk sum calculated for the air
samples collected at the site did not exceed the target cancer risk sum of 1.0E-04 for any
of the samples. However, the Non -Residential cumulative non -carcinogenic hazard index
calculated for the air samples collected at the site showed one sample (IA-107R in the
GEM space) exceeding the target non -cancer hazard index of 1.0E+00 (1.7E+0.0). In
Mid Atlantic
Indoor Air Quality Monitoring Report
Parker Lincoln Property
Raleigh, North Carolina
May 3, 2019
Page 5
addition, this sample exceeded the TCE sensitive population short term exposure limit of 9
ug/m3.
4.0 REMEDIAL ACTIONS AND FOLLOW UP TESTING
North Carolina Department of Environmental Quality considers TCE a `short term'
exposure contaminant of concern due to its potential for adverse health effects to
pregnant women in their first trimester. Under NCDEQ guidance, women between the
ages of 15 and 50 are considered a population sensitive to the exposure to TCE.
Trichloroethene was detected at 14 ug/m3° which is above the short term exposure limit
of 9 ug/ m3 in the sample collected from the GEM space.
On March 8, 2019, upon determining the sample collected from GEM space exceeded
the target non -cancer hazard index of 1.0E+00 and the TCE sensitive population short
term exposure limit of 9 ug/m3, the following activities were conducted:
• March 8, 2019 GEM was notified of the issue and overhead doors opened to
temporarily increase ventilation in the space. GEM personnel also indicated that
their space is not regularly occupied by individuals meeting the criteria of the
sensitive population. It was later determined that one part time employee working as
a bookkeeper met the definition of sensitive population.
• March 12, 2019 NCDEQ was notified of the TCE detection above acceptable levels
and of the actions taken to increase ventilation in the GEM space.
• March 12, 2019 permanent modifications to the ventilation system were installed.
These included the activation of an intake fan and the installation of two exhaust
vents. The operation of permanent ventilation in the GEM space is access
controlled.
• March 15, 2019 follow up 8-hour Summa air samples were collected and Radiellos®
deployed at the same three locations in the GEM space to assess indoor air quality
after the ventilation modifications were implemented. These samples were collected
with the overhead door closed (except when necessary to move materials into and
out of the GEM space). One outdoor air sample was also collected.
• March 21, 2019 a NCDEQ toxicologist and the GEM bookkeeper discussed the
potential health risks associated with TCE.
Mid Atlantic
Indoor Air Quality Monitoring Report May 3, 2019
Parker Lincoln Property Page 6
Raleigh, North Carolina
4.1 GEM Indoor Air Screening Levels (Tier 1)1
As summarized in Table 4.1, after the ventilation system improvements were implemented,
but the overhead door remained closed, trichloroethene was detected above the laboratory
MDL in one Radiello® sample collected in the GEM space. Trichlorethene was not
detected in any of the Summa-collected samples. The TCE concentration detected in the
Radiello® sample is above the NCDEQ Non -Residential IASL. Tetrachloethene was
detected in each sample (Radiello® and Summa) but at concentrations below NCDEQ
Non -Residential IASLs. Low concentrations of three other chlorinated compounds were
also detected.
4.2 GEM Indoor Air Risk Calculations (Tier 2)2
As summarized in Table 4.1, the Non -Residential cancer risk sum calculated for the air
samples collected at the site after implementation of the ventilation system improvements
did not exceed the target cancer risk sum of 1.0E-04 for either the Radiello® samples or
the 8-hour Summa canister samples. The Non -Residential cumulative non -carcinogenic
hazard index calculated for the air samples collected at the site did not exceed the target
non -cancer hazard index of 1.0E+00 at the sampling locations for either the Radiello®
samples or the 8-hour Summa canister samples.
5.0 SUMMARY AND CONCLUSIONS
During the February 2019 indoor air quality monitoring activities, a total of 10 indoor air
samples were collected from the interior of the building on the subject site. In addition,
one Radiello® outdoor air sample was collected in the vicinity of the southeast corner of
the building. Due to an exceedance of the target Hazard Index in one sample collected
from the GEM space, ventilation system improvements were implemented and follow up
sampling was conducted. Based on the actions taken and the data collected during this
investigation, we offer the following observations for the Non -Residential scenario.
The GEM space is used for cabinet construction. For these activities petroleum -based adhesives,
solvents, paints and stains are extensively used. Petroleum products are not present in the groundwater
at the site. Chlorinated solvents are present in the groundwater. Therefore, the Tier 1 analysis was
conducted for chlorinated compounds only. Petroleum compounds were not included in the analysis.
2 The GEM space is used for cabinet construction. For these activities petroleum -based adhesives,
solvents, paints and stains are extensively used. Petroleum products are not present in the groundwater
at the site. Chlorinated solvents are present in the groundwater. Therefore, Tier 2 analysis was conducted
for chlorinated compounds only. Petroleum compounds were not included in the analysis.
I% Mid Atlantic
Indoor Air Quality Monitoring Report
Parker Lincoln Property
Raleigh, North Carolina
Summary
May 3, 2019
Page 7
• No breaches in the floor slab in the warehouse were observed.
• The AHUs in the Web -Don office area were unchanged and set at 30% fresh air
prior to the sampling activities occurring.
• The indoor samples collected from the Lottery Office space were non -detect for
PCE and TCE.
• All of the indoor air samples collected in the `warehouse' portion of the building
contained detectable concentrations of PCE and TCE.
• The outdoor air sample did not contain detectable concentrations of PCE or TCE.
• The PCE concentrations in the indoor air samples did not exceed the Non -
Residential IASL.
• Seven indoor air samples exhibited TCE in concentrations exceeding the Non -
Residential IASL.
• None of the indoor air samples exceeded the Non -Residential target cancer risk
sum of 1.0E-04.
• One of the initial indoor air samples, collected from the GEM space, exceeded
the Non -Residential cumulative risk HI of 1.0.
• North Carolina Department of Environmental Quality considers TCE a `short
term' exposure contaminant of concern due to its potential for adverse health
effects to pregnant women in their first trimester. Trichloroethene was detected in
one sample collected in the warehouse area (GEM space) at a concentration
exceeding the Non -Residential `short term limit' of 9 ug/m3 (the concentration
where NCDEQ requires immediate actions) which equates to the Non -Residential
cumulative HI of 1.0 for TCE alone.
• GEM and NCDEQ personnel were notified of the exceedance and the one part-
time occupant of the GEM space meeting the sensitive population criterion was
informed of the health risks associated with TCE.
• Immediate actions were taken to ventilate the GEM space and permanent
improvements to the ventilation system were implemented within four days of
identifying the issue.
• Both short term (Summa) and longer term (Radiello®) samples were collected
immediately following the ventilation system upgrades. These data show indoor
air quality in the GEM space meets acceptable risk criteria (HI<1).
Conclusions
The data collected during this assessment indicate that vapor intrusion is occurring at the
subject site, but not at a rate that results in an unacceptable risk under the Non -Residential
use scenario. However, to achieve this condition supplemental ventilation is required in the
Web -Don and GEM spaces.
Mid Atlantic
Indoor Air Quality Monitoring Report
Parker Lincoln Property
Raleigh, North Carolina
May 3, 2019
Page 8
Comparison of the data collected during in February 2019 described in this report to
previous indoor air quality data collected at the subject site in November 2018 shows that,
with the exception of the GEM space, the results are consistent. The GEM space is
equipped with a large overhead door that was often open during the warmer November
2018 sample event. During the cooler weather of February 2019 the overhead door was
closed much more often. The follow up (March 15-22, 2019) indoor testing was conducted
with the overhead door closed and the new ventilation system operational. The data
indicates the ventilation system has abated the problem.
The data collected from the two sample locations in the Lottery offices show no detections
of PCE or TCE. These data are similar to historical data from the Lottery office area. These
data suggest that continued monitoring in the Lottery office may not be warranted.
The data collected from the warehouse portions of the building (south of the Lottery offices)
suggests that periodic indoor air quality monitoring is warranted and ventilation is required
in the Web -Don and GEM spaces.
The results for the three samples collected concurrently using Radiellos® and Summa
canisters during the follow up sampling in the GEM space show comparable results with
the Radiellos® typically slightly higher concentrations than the Summa collected samples.
The only TCE detection during this sampling was identified in a Radiello® sample. This
subjective evaluation suggests that either sample collection method is satisfactory. Similar
results were observed during previous assessments conducted at the subject site. It
appears that the sample collection method to use at this site can be determined based on
factors other than representativeness of the samples collected.
Recommendation
Mid -Atlantic recommends that the indoor air monitoring continue on a quarterly schedule.
Mid Atlantic
DRAWINGS
IS Mid Atlantic
a
1. RALEIGH EAST, NC DIGITAL RASTER GRAPHICS,
USGS. SCANNED FROM1:24,000-SCALE RALEIGH EAST, NC
TOPOGRAPHIC MAPS, PUBLISHED 2013, USGS.
2. INSET MAP DIGITAL DATA FROM 2002 NATIONAL TRANSPORTATION ATLAS,
BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, D.C.
3. PROPERTY BOUNDARY DATA FROM WAKE COUNTY GIS.
TOPOGRAPHIC SITE MAP
Mid Atlantic PARKER LINCOLN PROPERTY
2728 CAPITALPITAL BOULEVARD
Enginrrring & Enr4ronmrnral5ai�clnns RALEIGH, NORTH CAROLINA
SCALE: 1:12,000
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BY: DRAWING NO.: 1.2
REFERENCE: DATA AND 2016 AERIAL PHOTOGRAPH FROM WAKE COUNTY COUNTY GIS. MID -ATLANTIC FIELD NOTES.
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80 160 240
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Mid Atlantic
Engineering & Environmental Solutions
SAMPLE LOCATION MAP
PARKER LINCOLN BUILDING
2728 CAPITAL BOULEVARD
RALEIGH, NORTH CAROLINA
DRAWN BY: RDC
DRAFT CHECK
BY:
ENGINEER CHECK
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APPROVED
BY:
LEGEND
SAMPLE LOCATIONS
® AMBIENT RADIELLO SAMPLE
® RADIELLO SAMPLE
L SUMMACANNISTER SAMPLE
SUBJECT SITE
DATE: APRIL 2019
JOB NO.: 00OR2980.05
GIS NO.: 6G-R2980.05-6
DRAWING NO.: 2.1
I REFERENCE: DATA AND 2016 AERIAL PHOTOGRAPH FROM WAKE COUNTY COUNTY GIS. MID -ATLANTIC FIELD NOTES. I
TABLES
I M i d Atlanti c
TABLE 2.1
AIR SAMPLE LOCATIONS AND TENANT SPACE OCCUPANTS
PARKER LINCOLN PROPERTY
RALEIGH, NORTH CAROLINA
MID -ATLANTIC JOB NO. OOOR2980.05
SAMPLE LOCATION ID
TENANT SPACE OCCUPANT
IA-115, IA-117, IA-118
NC Lottery
IA-110
Reico Kitchen and Bath
IA-113, IA-114
Inventory Management, Inc.
IA-107, IA-119, IA-120
Great Escape Millworks
IA-106, IA-116
Habitat for Humanity
IA-103
Web -Don, Inc.
OA-102
Outside between Web -Don & Habitat
OA-103
Outside Great Escape Millworks
Notes:
IA = Indoor Air
OA = Outdoor Air
TABLE 3.1
SUMMARY OF CHEMICAL CONSTITUENTS DETECTED IN INDOOR
AIR
AND RISK CALCULATIONS FEBRUARY 2019
PARKER LINCOLN PROPERTY
RALEIGH, NORTH CAROLINA
MID -ATLANTIC JOB NO. OOOR2980.05
Sample ID
IA-103R
IA-106R
IA-107R
IA-110R
IA-113R
IA-114R
IA-115R
IA-116R
IA-117R
IA-118R
OA-102R
NCDEQ DWM Non -Residential Indoor Air
Screening Levels
February 2018 (ug/m3)
Sampling Date
2/26/2019
2/26/2019
2/26/2019
2/26/2019
2/26/2019
2/26/2019
2/26/2019
2/26/2019
2/26/2019
2/26/2019
2/26/2019
Tetrachloroethene
16
6.1
12
6
2.4
4.6
8.2
7.7
<0.34
<0.34
<0.34
35
Trichloroethene
0.69
5.9
14
3.3
3.4
2.4
3.8
5.1
<0.29
<0.29
<0.29
1.8
Non -Residential Acceptable Carcinogenic
NON-RESIDENTIAL RISK CALCULATIONS SUMMARY
Sum Risk Range and Maximum Non -Cancer Hazard
Index
Calculated Sample Sum Cancer Risk
5.7E-07
2.1 E-06
4.9E-06
1.2E-06
1.2E-06
9.0E-07
1.4E-06
1.9E-06
NC
NC
NC
1.0 E-04
Calculated Sample Non -Carcinogenic Hazard
1.7E-01
7.1 E-01
1.7E+00
4.1 E-01
4.0E-01
3.0E-01
4.8E-01
6.3E-01
NC
NC
NC
HI=1
Index
Notes:
Concentration units; ug/m3
J = Estimated Concentration
NC = Not Calculated
R suffix on Sample ID = Sample collected with Radiello
<0.34 = Not detected above the laboratory method detection limit
Bold = Concentration detected above the NCDEQ DWM Non -Residential Indoor Air Screening
Levels
Highlight = Hazard Index 1.0 exceeded
TABLE 4.1
SUMMARY
OF
CHEMICAL CONSTITUENTS DETECTED IN INDOOR
AIR
AND RISK CALCULATIONS MARCH 2O19
GREAT ESCAPE MILLWORK RESAMPLING
PARKER LINCOLN PROPERTY
RALEIGH, NORTH CAROLINA
MID -ATLANTIC JOB NO. OOOR2980.05
Sample ID
IA-107SR
IA-107RR
IA-119SR
IA-119RR
IA-120SR
IA-120RR
OA-103SR
OA-103RR
NCDEQ DWM Non -Residential Indoor Air
Screening Levels
February 2018 (ug/m3)
Sampling Date
3/15/2019
3/22/2019
3/15/2019
3/22/2019
3/15/2019
3/22/2019
3/15/2019
3/22/2019
Carbon Tetrachloride
0.37
NT
<0.072
NT
0.4
NT
<0.44
NT
88
1, 2 trans-Dichloroethylene
<0.056
NT
<0.98
NT
1.7
NT
<0.048
NT
NE
Methylene Chloride
<0.15
NT
<0.15
NT
2.3
NT
<0.39
NT
530
Tetrachloroethene
8.6
15
9.1
15
1.3
5.4
<0.11
<0.34
35
Trichloroethene
<0.076
2.2
<0.076
<0.29
<0.076
<0.29
<0.065
<0.29
1.8
Non -Residential Acceptable Carcinogenic
NON-RESIDENTIAL RISK CALCULATIONS
SUMMARY
Sum Risk Range and Maximum Non -Cancer Hazard
Index
Calculated Sample Sum Cancer Risk
3.6E-07
6.9E-07
1.9E-07
2.0E-07
2.3E-07
6.80E-08
NC
NC
1.0 E-04
Calculated Sample Non -Carcinogenic Hazard
5.0E-02
2.2E-01
5.2E-02
5.3E-02
9.2E-03
1.80E-02
NC
NC
HI=1
Index
Notes:
Concentration units; ug/m3
SR suffix on Sample ID = Repeat sample collected with Summa canister
RR suffix on Sample ID = Repeat sample collected with Radiello
NT = Not Tested for this compound
NE = Not Established
J = Estimated Concentration
NC = Not Calculated
<0.34 = Not detected above the laboratory method detection limit
Bold = Concentration detected above the NCDEQ DWM Non -Residential Indoor Air Screening
Levels
Highlight = Hazard Index 1.0 exceeded
APPENDIX A
INDOOR AIR BUILDING SURVEY AND SAMPLING FORM
OBSERVATION FORM
IS Mid Atlantic
INDOOR AIR BUILDING SURVEY
and SAMPLING FORM
Site Name: Parker Lincoln Property
Preparer's name: Mid -Atlantic Associates/Sandy Miller
Preparer's affiliation: Consultant to Owner
Part I - Occupants
ID#: E�, e kk Z. (.Ka u,, Lt)
Date: 2. - rD_t,) ® al' ` to
Phone #: 919-250-9918
Building Address: 2728 Capital Boulevard, Raleigh, NC 27604
Property Contact: Mr. Lowell Lovell
Owner / Renter / other Property Manager
Contact's Phone: home ( ) work (919) 866-4263 cell (919) 412-1295
# of Building occupants: Children under age 13 Children age 13-18 Adults —300
Part 11— Building Characteristics
Building type: residential / multi -family residential <office / strip mall /commercial industrial
Describe building: Large (547,000 sq. ft.) office /warehouse Year constructed: 1953
Sensitive population: day care / nursing home / hospital / school / other (specify): None
Number of floors below grade: 0 (full basement / crawl space /slab on grade
Number of floors at or above grade: 1
Depth of basement below grade surface: N/A ft. Basement size: N/A ft2
Basement floor construction: concrete / dirt / floating / stone / other (specify): N/A
Foundation walls: poured concrete ! cinder blocks / stone / other (specify) N/A
Basement sump present? Yes / No Sump pump? Yes No Water in sump? Yes / No
Type of heating circle all that
hot air circulation hot air radiation wood steam radiation
heat pump hot wa r ra cation kerosene heater electric baseboard
other (specify):
Type of ventilation suit m circle all that apply):
central air conditioning mechanica— 1 fang atliroom ventilation f na
indivi ua air con itioning units kitchen range hood fan outside air inta e
other (specify):
Type of fuel utilized (circle all that apply):
Natura gas / e ectnc / fuel oil / wood / coal / solar / kerosene
Are the basement walls or floor sealed with waterproof paint or epoxy coatings? N/A Yes / No
Is there a whole house fan?
Septic system?
Yes / No
Yes / Yes (but not used) / No
Irrigation/private well? Yes /Yes (but not used / No
Type of ground cover outside of building: grass / concrete / aspha t / other (specify)
Existing subsurface depressurization (radon) system in place? Yes / No active /passive
Sub -slab vapor/moisture barrier in place?
Type of barrier:
Part III - Outside Contaminant Sources
Yes / No nknown
Other stationary sources nearby (gas stations, emission stacks, etc.): Yes; gas station
Heavy vehicular traffic nearby (or other mobile sources): Yes; Capital Boulevard
Part IV — Indoor Contaminant Sources
Identify all potential indoor sources found in the building (including attached garages) and crawlspace (if
present), the location of the source (floor and room), and whether the item was removed from the building
48 hours prior to indoor air sampling event. Any ventilation implemented after removal of the items
should be completed at least 24 hours prior to the commencement of the indoor air sampling event.
Potential Sources
Location(s)
Removed
(Yes / No / NA)
Gasoline storage cans
Gas -powered equipment
Kerosene storage cans
Paints / thinners / strippers
Cleaning solvents
Oven cleaners
Carpet / upholstery cleaners
Other house cleaning products
Moth balls
Polishes / waxes
Insecticides
Furniture / floor polish
Nail polish / polish remover
Hairspray
Cologne / perfume
Air fresheners
Fuel tank (inside building)
NA
Wood stove or fireplace
NA
New furniture / upholstery
New carpeting / flooring
NA
Hobbies - glues, paints, etc.
Provide Drawing of Sample Location(s) in Building
See attached map
Part VII - Meteorological Conditions
Was there significant precipitation within 12 hours prior to (or during) the sampling event? Yes / No
Describe the general weather conditions: _ Et�o i s 14kAr,.- F-a) `z L, 12:� h
G ,1a5 64 c(-V--7" a S
✓l. Gt t C{ }� r bct `� f 3 1 `t Ck Ct.'\
Part VIII — General Observations la
Provide any information that may be pertinent to the sampling event and may assist in the data
interpretation process (e.g., observed that drycleaner operated with door or windows propped open for
ventilation).
(Adapted from the NJDEP Vapor Intrusion Guidance, October 2005)
Part V — Miscellaneous Items
Do any occupants of the building smoke? Yes / No
Last time someone smoked in the building? N/A
How often? N/A
hours / days ago
Does the building have an attached garage directly connected to living space? Yes / No
If so, is a car usually parked in the garage? Yes / No /A
Are gas -powered equipment or cans of gasoline/fuels stored in the garage? Yes / No
Do the occupants of the building have their clothes dry cleaned? Yes / No ossibl
If yes, how often? weekly / monthly / 3-4 times a year nknown
Do any of the occupants use solvents in work? Yes / No
If yes, what types of solvents are used?
If yes, are their clothes washed at work? Yes / No
Have any pesticides/herbicides been applied around the building or in the yard? Yes / No inor, if an
If so, when and which chemicals? Unknown
Has there ever been a fire in the building? Yes / No Unknown If yes, when?
Has painting or staining been done in the building in the last 6 months? Yes / No Unknow
If yes, when and where?
Part VI — Sampling Information
Sample Technician: Sandy Miller Phone number: ( 919) 250-9918
Sample Source: Qndoor Air / Crawlspace Air / Sub -Slab / Near Slab Soil Gas / Exterior Soil Gas
Sampler Type: Tedlar bag / Sorbent / Stainless Steel Canister / Other (specify):
Analytical Method: TO-15 / TO-17 / other: Radiello s 150 Cert. Laboratory: Con -test
Sample locations (floor, room):
Field ID # - See attached map Field ID # -
Field ID # -
Field ID # -
11-1111
Were "Instructions for Occupants" followed? (Yes/No
If not, describe modifications:
INDOOR AIR BUILDING SURVEY
and SAMPLING FORM
Site Name: Parker Lincoln Property
Preparer's name: Mid -Atlantic Associates/Sandy Miller
Preparer's affiliation: Consultant to Owner
ID#: R 2, q u• 05
Date: r-I &A Gk 15 Z L7 k Q 5 tAw��v�Cc 5
L-f5
Phone #: 919-250-9918
,,ait.i alas a 314s
Part I - Occupants
Building Address: 2728 Capital Boulevard, Raleigh, NC 27604 - -
Property Contact: Mr. Lowell Lovell Owner 1 Renter 1 othe Property Manager
Contact's Phone: home ( } work (919)866-4263 cell (419).412-1295
# of Building occupants: Children under age 13 Children age 13-18 Adults —300
Part II — Building Characteristics
Building type: residential 1 multi -family residential <aie>strip mall 1 commercial industrial
Describe building: Large (547,000 sq. ft.) office /warehouse Year constructed: 1953
Sensitive population: day care 1 nursing home 1 hospital 1 school 1 other (specify): None
Number of floors below grade: 0 (full basement 1 crawl space 1 slab on grade.
Number of floors at or above grade: 1
Depth of basement below grade surface: NIA ft. Basement size: NIA ft'
Basement floor construction: concrete 1 dirt 1 floating 1 stone 1 other (specify): NIA _
Foundation walls: poured concrete 1 cinder blocks 1 stone 1 other (specify) NIA
Basement sump present? Yes I Na Sump pump? Yes No Water in sump? Yes I No
Type ofheat circle all that
of air circulation of air radiation wood steam radiation
heat pump haw cation kerosene heater electric baseboard
other (specify):
Type of ventilate�con
that apply}:
central echanical fans at om ventilation ans
endive units kitchen range hood fan utsi a air rota e
other (specify):
Type of fuel utilized (circle all that apply):
Naturai gas 1 Oe ectrtc 1 fuel oil 1 wood 1 coal 1 solar 1 kerosene
Are the basement walls or floor sealed with waterproof paint or epoxy coatings? N/ Yes 1 No
Is there a whole house fan? Yes I No
Septic system? Yes I Yes (but not used) 19
Irrigation/private well? Yes I es {but not use I No
Type of ground cover outside of building: grass 1 concret 1 aspha 1 other (specify)
Existing subsurface depressurization (radon) system in place? Yes 1 No active 1 passive
Sub -slab vapor/moisture barrier in place? Yes I No nknown
Type of barrier:
Part III - Outside Contaminant Sources
Other stationary sources nearby (gas stations, emission stacks, etc.): Yes; gas station
Heavy vehicular traffic nearby (or other mobile sources): Yes-, Capital Boulevard
Part fV — Indoor Contaminant Sources
Identify all potential indoor sources found in the building (including attached garages) and crawlspace (if
present), the location of the source (floor and room), and whether the item was removed from the building
48 hours prior to indoor air sampling event. Any ventilation implemented after removal of the items
should be completed at least 24 hours prior to the commencement of the indoor air sampling event.
Potential Sources
Location(s)
Removed
(Yes 1 No 1 NA)
Gasoline storage cans
�} W
Gas -powered equipment
Kerosene storage cans
Paints 1 thinners 1 strippers
V/ Us, C Ck VN ' _ , r V A i
til o
Cleaning solvents
l pra�ic�
Oven cleaners
Carpet 1 upholstery cleaners
Other house cleaning products
Moth balls
Polishes 1 waxes
Insecticides
Furniture 1 floor polish
Nail polish 1 polish remover
Hairspray
Cologne 1 perfume
Air fresheners
Fuel tank (inside building)
NA
Wood stove or fireplace
NA
New furniture 1 upholstery
New carpeting 1 flooring
NA
llehbiea- glues, paints, etc.
5 9 a LL- rp V a
0
Part V — Miscellaneous Items
Do any occupants of the building smoke? Yes I No How often? NIA
Last time someone smoked in the building? N/A hours I days ago
Does the building have an attached garage directly connected to living space? Yes I No
If so, is a car usually parked in the garage? Yes I No
Are gas -powered equipment or cans of gasoline/fuels stored in the garage? Yes 1 No
Do the occupants of the building have their clothes dry cleaned? Yes I No o55ih1
If yes, how often? weekly 1 monthly 13-4 times a year nkno
Do any of the occupants use solvents in work? Yes I No
If yes, what types of solvents are used?
If yes, are their clothes washed at work? Yes I No
Have any pesticides/herbicides been applied around the building or in the yard? Yes 1 No inor, if an
If so, when and which chemicals? Unknown
Has there ever been a fire in the building? Yes I No nknown If yes, when?
Has painting or staining been done in the building in the last G months? Yes I No nkno
If yes, when and where?
Part VI — Sampling Information
Sample Technician: Sandy Miller Phone number: ( 919 } 250-9918
Sample Source: Qndoor Air 1 Crawl space Air 1 Sub -Slab 1 Near Slab Soil Gas 1 Exterior Soil Gas
Sampler Type: Tedlar bag 1 orbent 1 tainless Steel Canist Other (specify):
Analytical Method: O-1S 1 TO-17 1 other: Radiello - tAo Cert. Laboratory: Con -test
Sample locations (floor, room):
Field ID # - See attached map Field ID # -
Field ID # -
Field ID # -
Were "Instructions for Occupants" followed? Yes I No
If not, describe modifications:
Provide Drawing of Sample Location(s) in Building
See attached map
Part VII - Meteorological Conditions
Was there significant precipitation within 12 hours prior to (or during) the sampling event? Yes No
Describe the general weather conditions: I7I ❑ - Le5 ° C et5t tji F t cL
Part VIII — General Observations
Provide any information that may be pertinent to the sampling event and may assist in the data
interpretation process (e.g., observed that drycleaner operated with door or windows propped open for
ventilation).
ern sib Q�.c�
sP6t-a-
u
{Adapted from the N]DEP Vapor Intrusion Guidance, October 2005)
I
QUARTERLY INSPECTION CHECKLIST
PARKER LINCOLN PROPERTY
2728 CAPITAL BOULEVARD
RALEIGH, NORTH CAROLINA
MID -ATLANTIC JOB NO. R2980.05
NCBP PROJECT NO. 22018-18-092
INSPECTION DATE: 02/19/2019
CHANGES IN
CHANGES
CHANGES IN
CHANGES TO
SECTION
FLOOR SLAB:
TO HVAC
TENANTS/
SAMPLING
DISCUSSIONS WITH
OBSERVATIONS
COMMENTS
Y I N - TYPE
SYSTEM:
OPERATIONS:
REQUIRED:
PROPERTY MANAGER
YIN
YIN - TYPE
Y/N - WHY
�l d,
Section I
{
7.1 C�tQ,
a;�
vu-E du d
_ aki co i u�re �� t��
c r, e. C u i r C
Western quadrant -
�`0 �� orR d
dID "` -(' `�
# erg ,
aw� Gi
441*_1 a� p {i1 '
REICO Kitchen & Bath
r► o r v �l S
IA410
CAj
(,kv i#Vk,
tt
pact large ccfvtiau.�t
Section 11
1^ `}Lvs
A i��-+ t-+ �� �P
M i nv-e•��-un ],-- �`�t n�
Central -west quadrant
�l
;�Cce'1
17r� or �v4t5s
jai �f u� � •
5�f3u ,�°C9'
r+ '
Inventory
���
Management, Inc.
"'Jetl 51
Q ca C`
IA-#13, #14
yMoLncz e r
CLVi C}.tiv► a ��w t j
wale �-
Section Ill
Northeast quadrant -
4�Iw�
1 C� Q
� �
�r' Ur 5
�1 a� r'1 e��'I�
� 5 4 � 5 CAY et
ire cL v�-'� ►r'"U4\
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b v-e �
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+]
warehouse/vacant
IA415
NOTE: CONFIRM
30%MAKE-UP
ti\4t `E
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�v� .U¢5 r13 5 In W(k�IADU
� � �• i3�1 Q i_+n
Section IV
Southeast quadrant -
q
� arr�
AIR
An [.
j.1oL `l
���
�tr.[ti�t-s
r M P. �t� y r
l&MIDl.i P-0 wit{
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u►" {ou � CLir
Great Escape
acerb
trtrn(SJ {.c_-"o-AS
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kaei a;I,' ;,"
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"n
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HabitatlWVeb-Dan
#-A w r
+��
Cc � e r
5
vv. Cc D'i:c • s t
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{'� SNw��+�sv�
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tiC�v� ��.L•� � t �. ;`l-�. , r��rt
yxp�,dU.�
rev► CVR�4s A
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#6, #7, #16
;,nst-ruc#io f%5
na+#cai+rr
�rswypl�te$.
rrd�«�1eL��
FEBRUARY 2019 LABORATORY ANALYTICAL REPORT AND CHAIN
OF CUSTODY
IS Mid Atlantic
cones ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
March 4, 2019
Dan Nielsen
Mid -Atlantic Associates, Inc. - Raleigh, NC
409 Rogers View Court
Raleigh, NC 27610
Project Location: 2728 Capital Blvd.
Client Job Number:
Project Number: R2980.05
Laboratory Work Order Number: 19B 1174
Enclosed are results of analyses for samples received by the laboratory on February 26, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
I,&, �. A��
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 24
cones ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
Mid -Atlantic Associates, Inc. - Raleigh, NC REPORT DATE: 3/4/2019
409 Rogers View Court
Raleigh, NC 27610 PURCHASE ORDER NUMBER:
ATTN: Dan Nielsen
PROJECT NUMBER: R2980.05
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 19B 1174
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: 2728 Capital Blvd.
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
IA-117R
19B 1174-01
Indoor air
RAD 130
IA-118R
19B 1174-02
Indoor air
RAD 130
IA-115R
19B 1174-03
Indoor air
RAD 130
IA-110R
19B 1174-04
Indoor air
RAD 130
IA- 114R
19B 1174-05
Indoor air
RAD 130
IA-113R
19B 1174-06
Indoor air
RAD 130
IA-107R
19B 1174-07
Indoor air
RAD 130
IA- 116R
19B 1174-08
Indoor air
RAD 130
IA-106R
19B 1174-09
Indoor air
RAD 130
OA-102R
19B1174-10
Air
RAD 130
IA-103R
19B1174-11
Indoor air
RAD 130
Page 2 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method Radiello RAD-130 - The sampling rates for trichloroethene and tetrachloroethene are as follows: trichloroethene = 69 mL/min,
tetrachloroethene = 59 tuUmin. The theoretical sampling rates for vinyl chloride, 1, 1 -dichloroethene, trans-1,2-dichloroethene, and
cis-1,2-dichloroethene are estimated using Graham's Law and are as follows: vinyl chloride = 103 mL/min, 1, 1 -dichloroethene = 83 mL/min,
trans-1,2-dichloroethene = 83 mUmin, cis-1,2-dichloroethene = 83 mL/min. The results for these 4 compounds are estimated values.
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 3 of 24
cane ,G)
ANALYTICAL LABORATORY
Project Location: 2728 Capital Blvd.
Date Received: 2/26/2019
Field Sample #: IA-117R
Sample ID: 19B1174-01
Sample Matrix: Indoor air
Sampled:2/26/2019 08:08
Analyte
Vinyl Chloride
1, 1 -Dichloroethene
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
Tichloroethene
Tetrachloroethene
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Sample Description/Location:
Sub Description/Location:
Flow Controller ID:
Sample Type:
Air Volume L: 10041
RAD 130
Work Order: 19BIt74
Total µg
ug/m3
Date/Time
Results
RL MDL
Flag/Qual Results
RL
MDL Dilution
Analyzed
Analyst
ND
0.16
ND
0.15
1
3/1/19 14:58
IMR
ND
1.0
ND
1.2
1
3/1/19 14:58
IMR
ND
1.0
ND
1.2
1
3/1/19 14:58
IMR
ND
0.20
ND
0.24
1
3/1/19 14:58
IMR
ND
0.20
ND
0.29
1
3/1/19 14:58
IMR
ND
0.20
ND
0.34
1
3/1/19 14:58
IMR
Page 4 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: IA-118R
Sample ID: 19131174-02
Sample Matrix: Indoor air
Flow Controller ID:
Sampled: 2/26/2019 08:14
Sample Type:
Air Volume L: 10041
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.15
1
3/1/19 15:21
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 15:21
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 15:21
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 15:21
IMR
Tichloroethene
ND
0.20
ND
0.29
1
3/1/19 15:21
IMR
Tetrachloroethene
ND
0.20
ND
0.34
1
3/1/19 15:21
IMR
Page 5 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: IA-115R
Sample ID: 19131174-03
Sample Matrix: Indoor air
Flow Controller ID:
Sampled: 2/26/2019 08:23
Sample Type:
Air Volume L: 10043
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.15
1
3/1/19 15:45
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 15:45
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 15:45
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 15:45
IMR
Tichloroethene
2.6
0.20
3.8
0.29
1
3/1/19 15:45
IMR
Tetrachloroethene
4.9
0.20
8.2
0.34
1
3/1/19 15:45
IMR
Page 6 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: IA-11OR
Sample ID: 19131174-04
Sample Matrix: Indoor air
Flow Controller ID:
Sampled: 2/26/2019 08:48
Sample Type:
Air Volume L: 10051
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.15
1
3/1/19 16:09
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 16:09
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 16:09
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 16:09
IMR
Tichloroethene
2.3
0.20
3.3
0.29
1
3/1/19 16:09
IMR
Tetrachloroethene
3.5
0.20
6.0
0.34
1
3/1/19 16:09
IMR
Page 7 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: IA-114R
Sample ID: 19131174-05
Sample Matrix: Indoor air
Flow Controller ID:
Sampled: 2/26/2019 08:58
Sample Type:
Air Volume L: 10031
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.15
1
3/1/19 16:32
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 16:32
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 16:32
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 16:32
IMR
Tichloroethene
1.6
0.20
2.4
0.29
1
3/1/19 16:32
IMR
Tetrachloroethene
2.7
0.20
4.6
0.34
1
3/1/19 16:32
IMR
Page 8 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: IA-113R
Sample ID: 19131174-06
Sample Matrix: Indoor air
Flow Controller ID:
Sampled: 2/26/2019 09:05
Sample Type:
Air Volume L: 10028
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.15
1
3/1/19 16:55
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 16:55
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 16:55
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 16:55
IMR
Tichloroethene
2.4
0.20
3.4
0.29
1
3/1/19 16:55
IMR
Tetrachloroethene
1.4
0.20
2.4
0.34
1
3/1/19 16:55
IMR
Page 9 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: IA-107R
Sample ID: 19131174-07
Sample Matrix: Indoor air
Flow Controller ID:
Sampled: 2/26/2019 09:16
Sample Type:
Air Volume L: 10018
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.16
1
3/1/19 17:18
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 17:18
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 17:18
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 17:18
IMR
Tichloroethene
9.5
0.20
14
0.29
1
3/1/19 17:18
IMR
Tetrachloroethene
7.2
0.20
12
0.34
1
3/1/19 17:18
IMR
Page 10 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: IA-116R
Sample ID: 19131174-08
Sample Matrix: Indoor air
Flow Controller ID:
Sampled: 2/26/2019 09:22
Sample Type:
Air Volume L: 10020
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.16
1
3/1/19 17:42
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 17:42
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 17:42
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 17:42
IMR
Tichloroethene
3.5
0.20
5.1
0.29
1
3/1/19 17:42
IMR
Tetrachloroethene
4.6
0.20
7.7
0.34
1
3/1/19 17:42
IMR
Page 11 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: IA-106R
Sample ID: 19131174-09
Sample Matrix: Indoor air
Flow Controller ID:
Sampled: 2/26/2019 09:26
Sample Type:
Air Volume L: 10026
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.15
1
3/1/19 18:05
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 18:05
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 18:05
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 18:05
IMR
Tichloroethene
4.1
0.20
5.9
0.29
1
3/1/19 18:05
IMR
Tetrachloroethene
3.6
0.20
6.1
0.34
1
3/1/19 18:05
IMR
Page 12 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: OA-102R
Sample ID: 19131174-10
Sample Matrix: Air
Flow Controller ID:
Sampled: 2/26/2019 09:34
Sample Type:
Air Volume L: 10031
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.15
1
3/1/19 18:29
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 18:29
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 18:29
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 18:29
IMR
Tichloroethene
ND
0.20
ND
0.29
1
3/1/19 18:29
IMR
Tetrachloroethene
ND
0.20
ND
0.34
1
3/1/19 18:29
IMR
Page 13 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19B1174
Date Received: 2/26/2019
Sub Description/Location:
Field Sample #: IA-103R
Sample ID: 19B1174-11
Sample Matrix: Indoor air
Flow Controller ID:
Sampled: 2/26/2019 09:40
Sample Type:
Air Volume L: 10035
RAD 130
Total µg
ug/m3
Date/Time
Analyte
Results
RL MDL Flag/Qual
Results
RL MDL
Dilution
Analyzed
Analyst
Vinyl Chloride
ND
0.16
ND
0.15
1
3/1/19 18:53
IMR
1,1-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 18:53
IMR
trans-1,2-Dichloroethene
ND
1.0
ND
1.2
1
3/1/19 18:53
IMR
cis-1,2-Dichloroethene
ND
0.20
ND
0.24
1
3/1/19 18:53
IMR
Tichloroethene
0.48
0.20
0.69
0.29
1
3/1/19 18:53
IMR
Tetrachloroethene
9.3
0.20
16
0.34
1
3/1/19 18:53
IMR
Page 14 of 24
cones ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
Sample Extraction Data
Prep Method: Radiello-RAD 130
Lab Number [Field ID] Batch Initial [Cartridge Final [mL] Date
19B1174-01[IA-117R]
B224772
1.00
2.00
03/01/19
19B1174-02 [IA-118R]
B224772
1.00
2.00
03/01/19
19B1174-03 [IA-115R]
B224772
1.00
2.00
03/01/19
19B1174-04 [IA-11OR]
B224772
1.00
2.00
03/01/19
19B1174-05 [IA-114R]
B224772
1.00
2.00
03/01/19
19B1174-06[IA-113R]
B224772
1.00
2.00
03/01/19
19B1174-07 [IA-107R]
B224772
1.00
2.00
03/01/19
19B1174-08 [IA-116R]
B224772
1.00
2.00
03/01/19
19B1174-09 [IA-106R]
B224772
1.00
2.00
03/01/19
19B1174-10 [OA-102R]
B224772
1.00
2.00
03/01/19
19B1174-11[IA-103R]
B224772
1.00
2.00
03/01/19
Page 15 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
QUALITY CONTROL
Miscellaneous Air Analyses - Quality Control
Total µg ug/m3 Spike Level Source %REC RPD
nalyte Results RL Results RL Total µg Result %REC Limits RPD Limit Flag/Qua
Batch B224772 - Radiello
Blank (B224772-BLK1)
Prepared & Analyzed: 03/01/19
Vinyl Chloride
ND
0.16
1,1-Dichloroethene
ND
1.0
trans-1,2-Dichloroethene
ND
1.0
cis-1,2-Dichloroethene
ND
0.20
Trichloroethene
ND
0.20
Tetrachloroethene
ND
0.20
LCS (B224772-BS1)
Prepared & Analyzed: 03/01/19
Vinyl Chloride
7.58
0.16
0.41 10.0 75.8
40-140
1, 1 -Dichloroethene
7.72
1.0
10.0 77.2
40-140
trans-1,2-Dichloroethene
7.72
1.0
10.0 77.2
40-140
cis-1,2-Dichloroethene
8.31
0.20
10.0 83.1
40-140
Trichloroethene
7.59
0.20
10.0 75.9
40-140
Tetrachloroethene
7.39
0.20
10.0 73.9
40-140
LCS Dup (B224772-BSD1) Prepared & Analyzed: 03/01/19
Vinyl Chloride
9.24
0.16
0.41 10.0
92.4
1,1-Dichloroethene
9.14
1.0
10.0
91.4
trans-1,2-Dichloroethene
9.43
1.0
10.0
94.3
cis-1,2-Dichloroethene
9.85
0.20
10.0
98.5
Trichloroethene
9.13
0.20
10.0
91.3
Tetrachloroethene
8.79
0.20
10.0
87.9
40-140
19.8 30
40-140
16.9 30
40-140
20.0 30
40-140
16.9 30
40-140
18.5 30
40-140
17.4 30
Page 16 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 * FAX 413/525-6405 " TEL. 413/525-2332
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
t
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
RL
Reporting Limit
MDL
Method Detection Limit
RPD
Relative Percent Difference
LCS
Laboratory Control Sample
LCS Dup
Duplicate Laboratory Control Sample
MS
Matrix Spike Sample
MS Dup
Duplicate Matrix Spike Sample
REC
Recovery
QC
Quality Control
ppbv
Parts per billion volume
EPA
United States Environmental Protection Agency
% REC Percent Recovery
ND Not Detected
N/A Not Applicable
DL Detection Limit
NC Not Calculated
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation -Reduction Potential
wet Not dry weight corrected
% wt Percent weight
Kg Kilogram
g Gram
mg Milligram
µg Microgram
ng Nanogram
L Liter
mL Milliliter
µL Microliter
m3 Cubic Meter
EPH Extractable Petroleum Hydrocarbons
VPH Volatile Petroleum Hydrocarbons
APH Air Petroleum Hydrocarbons
FID Flame Ionization Detector
PID Photo Ionization Detector
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
ANALYST
RLF
Rebecca Faust
RAP
Raisa A. Petraitis
STATION PDF Management Station
KKM
Kerry K. McGee
IMR
Irina Raducan
Page 17 of 24
cones ,G)
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
INTERNAL STANDARD AREAAND RT SUMMARY
RAD 130
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area %
Limits
RT Diff
RT Diff
Limit
Q
LCS (B224772-BS1 Lab File ID: B0301002.1) Analyzed: 03/01/19 13:48
2-Fluorotoluene
7070325
13.447
6660202
13.448
106
50-200
-0.0010
+/-0.50
LCS Dup (B224772-BSD1) Lab File ID: B0301003.D Analyzed: 03/01/19 14:12
2-Fluorotoluene
6342756
13.444
6660202
13.448
95
50 - 200
-0.0040
+/-0.50
Blank (B224772-BLK1 Lab File ID: B0301004.D Analyzed: 03/01/19 14:35
2-Fluorotoluene
6482884
13.44
6660202
13.448
97
50-200
-0.0080
FTO.50
IA-117R (19B1174-01 ) Lab File ID: B0301005.D Analyzed: 03/01/19 14:58
2-Fluorotoluene
6854190
13.437
6660202
13.448
103
50-200
-0.0110
+/-0.50
IA-118R (19111174-02 ) Lab File ID: B0301006.13 Analyzed: 03/01/19 15:21
2-Fluorotoluene
6947314
13.432
6660202
13.448
104
50-200
-0.0160
+/-0.50
IA-115R (19B1174-03 ) Lab File ID: B0301007.D Analyzed: 03/01/19 15:45
2-Fluorotoluene
7248073
13.438
6660202
13.448
109
50-200
-0.0100
+/-0.50
IA-110R (19B1174-04) Lab File ID: B0301008.D Analyzed: 03/01/19 16:09
2-Fluorotoluene
6673946
13.437
6660202
13.448
100
50-200
-0.0110
+/-0.50
IA-114R (19111174-05) Lab File ID: B0301009.13 Analyzed: 03/01/19 16:32
2-Fluorotoluene
7165271
13.436
6660202
13.448
108
50 - 200
-0.0120
+/-0.50
IA-113R (19B1174-06) Lab File ID: B0301010.D Analyzed: 03/01/19 16:55
2-Fluorotoluene
7300717
13.433
6660202
13.448
110
50-200
-0.0150
+/-0.50
IA-107R (19B1174-07) Lab File ID: B0301011.13 Analyzed: 03/01/19 17:18
2-Fluorotoluene
7377110
13.434
6660202
13.448
111
50-200
-0.0140
+/-0.50
IA-116R (19B1174-08) Lab File ID: B0301012.D Analyzed: 03/01/19 17:42
2-Fluorotoluene
6320409
13.436
6660202
13.448
95
50 - 200
-0.0120
+/-0.50
IA-106R (19111174-09) Lab File ID: B0301013.13 Analyzed: 03/01/19 18:05
2-Fluorotoluene
6859935
13.442
6660202
13.448
103
50 - 200
-0.0060
+/-0.50
OA-102R (19B1174-10) Lab File ID: B0301014.D Analyzed: 03/01/19 18:29
2-Fluorotoluene
7113003
13.442
6660202
13.448
107
50-200
-0.0060
+/-0.50
IA-103R (19B1174-11) Lab File ID: B0301015.13 Analyzed: 03/01/19 18:53
2-Fluorotoluene
6746431
13.439
6660202
13.448
101
50-200
-0.0090
+/-0.50
Page 18 of 24
cane ,G)
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332
CONTINUING CALIBRATION CHECK
COMPOUND
TYPE
RESPONSE FACTOR
% DIFF / DRIFT
STD
CCV
ICAL
CCV
MIN (#)
CCV
LIMIT (#)
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
* Values outside of QC limits
Page 19 of 24
cones o
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
No certified Analyses included in this Report
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2005
100033
03/l/2020
MA
Massachusetts DEP
M-MA100
06/30/2019
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY
New York State Department of Health
10899 NELAP
04/1/2019
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2020
RI
Rhode Island Department of Health
LA000112
12/30/2019
NC
North Carolina Div. of Water Quality
652
12/31/2019
NJ
New Jersey DEP
MA007 NELAP
06/30/2019
FL
Florida Department of Health
E871027 NELAP
06/30/2019
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2019
ME
State of Maine
2011028
06/9/2019
VA
Commonwealth of Virginia
460217
12/14/2019
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2019
NC-DW
North Carolina Department of Health
25703
07/31/2019
Page 20 of 24
A
0
m
a
m
m
m
U
Q.
N
Cli
M
Page 21 of 24
2/27/2019 Track your package or shipment with FedEx Tracking
774567966632
Del ivered
Wednesday 2/27/2019 at 9.25 am
DELIVERED
Signed for by: B.BECCA
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
FROM
Raleigh, NC US
TO
EAST LONGMF-ADCW, MA US
Multiple -piece Shipment
3 Piece shipment
TRACKING NUMBER
SHIPPER CITY,
STATE:`.
SHIP BATE STATUS
' <r
BELiVERY BATE
DESTINATION/RECIPIENT.
CITY,':STATI" s
774567966632
RALEIGH, NC
2/26/2019 =-
2./27/2019
FAST LONGMEADOW, MA
774567966106
RALFIGH, NC
2/26/2019
2/27/2019
FAST LONGMEADOW, MA
774567966827
RALEIGH, NC
2/2b/2019
2/27/2019
FAST LONGMEADOW, MA
Shipment Facts
TRACKING NUMBER
774567966632
WEIGHT
15 Ihs / 6 8 kgs
TOTAL PIECES
3
SHIPPER REFERENCE
80
SERVICE
FedEx Priority Overnight
DIMENSIONS
24x14x14 in.
TOTAL SHIPMENT WEIGHT
45 Ibs / 20.41 kgs
PACKAGING
Your Packaging
MASTER TRACKING NUMBER
774667966622
DELIVERED TO
Shipping/Receiving
TERMS
Third Party
SPECIAL HANDLING SECTION
Deliver Weekday, Additional Handling
Surcharge
https://www.fedex.com/apps/fedextracklindex.htmt?action=track&tracknumbers=774567966632&locale=en_US&cr)try_code=en Page 23 of 24
I Have Not Confirmed Sample Container
Numbers With Lab Staff Before Coo n MW be st
Relinquishing Over j0XN^-V-r11CAL-
Samples
. Doc 27t3 Rear .6 017: .
Air Media Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client��
Received By 1= Date 2 2 , CA Time � 5"
How were the samples In Cooler - On Ice No Ice
received? In Box Ambient Melted Ice
Were samples within Temperature By Gun # `3 Actual Temp - S� 5
Compliance? 2-6°C By Blank #
Was Custody Seal Intact? /1/I
Was COC Relinquished ?
Are there any loose caps/valves on any samples?
Is COC in ink/ Legible? -T
Actual Temp -
Were Samples Tampered with? AA -
Does Chain Agree With Samples?
Did COC Include all Client _f-- Analysis T Sampler Name 'I -
Pertinent Information? Project ID's T Collection Dates/Times -i
Are Sample Labels filled out and legible?
Are there Rushes? �T Who was notified?
Samples are received within holding time? T
Proper Media Used? T Individually Certified Cans?
Are there Trip Blanks? F Is there enough Volume? Z
1.
Summa Cans
Nut/Ferrule
IC Train
Tedlar Baqs
Tubing
TO-17 Tubes
T-Connector
Radiello
i i
Syringe
Pufs/TO-11 s
Tedlar
APPENDIX C
MARCH 2O19 LABORATORY ANALYTICAL REPORTS AND
CHAINS OF CUSTODY
IS Mid Atlantic
corl'u ,G)
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332
March 21, 2019
Dan Nielsen
Mid -Atlantic Associates, Inc. - Raleigh, NC
409 Rogers View Court
Raleigh, NC 27610
Project Location: 2728 Capital Blvd.
Client Job Number:
Project Number: R2980
Laboratory Work Order Number: 19CO786
Enclosed are results of analyses for samples received by the laboratory on March 18, 2019. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
I,&, �. A��
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 29
corl'u ,G)
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332
Mid -Atlantic Associates, Inc. - Raleigh, NC REPORT DATE: 3/21/2019
409 Rogers View Court
Raleigh, NC 27610 PURCHASE ORDER NUMBER:
ATTN: Dan Nielsen
PROJECT NUMBER: R2980
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 19C0786
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: 2728 Capital Blvd.
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
IA-107SR
19C0786-01
Indoor air
EPA TO-15
IA-119SR
19C0786-02
Indoor air
EPA TO-15
IA-120SR
19C0786-03
Indoor air
EPA TO-15
OA-103SR
19C0786-04
Air
EPA TO-15
Page 2 of 29
corl'u ,G)
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be
biased on the low side.
Analyte & Samples(s) Qualified:
2-Hexanone (MBK)
19C0786-01[IA-107SR], 19C0786-02[IA-119SR], 19C0786-03[IA-120SR], 19C0786-04[OA-103SR], B226068-BSI
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be
biased on the high side.
Analyte & Samples(s) Qualified:
Toluene
19C0786-02RE2[IA-119SR], B226163-BS 1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
2-Hexanone (MBK), 4-Methyl-2-pentanone (MIBK)
19C0786-01[IA-107SR], 19C0786-02[IA-119SR], 19C0786-03[IA-120SR], 19C0786-04[OA-103SR], 5033632-CCVI
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in
house limits of 50-150%.
Analyte & Samples(s) Qualified:
Ethanol
B226163-BS1
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 3 of 29
corl'u ,G)
ANALYTICAL LABORATORY
Project Location: 2728 Capital Blvd.
Date Received: 3/18/2019
Field Sample #: IA-107SR
Sample ID: 19CO786-01
Sample Matrix: Indoor air
Sampled: 3/15/2019 16:48
39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332
ANALYTICAL RESULTS
Sample Description/Location: Work Order: 19CO786
Sub Description/Location: Initial Vacuum(in Hg): -30
Canister ID: 2187 Final Vacuum(in Hg): -8
Canister Size: 6 liter Receipt Vacuum(in Hg): -7.8
Flow Controller ID: 3094 Flow Controller Type: Fixed -Orifice
Sample Type: 8 hr Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv
ug/m3
Date/Time
Analyte
Results
RL
MDL Flag/Qual
Results
RI
MDL
Dilution
Analyzed
Analyst
Acetone
3000
600
210
7200
1400
490
300
3/19/19 20:12
BRF
Benzene
1.0
0.035
0.014
3.2
0.11
0.046
0.702
3/19/19
1:40
BRF
Benzyl chloride
ND
0.035
0.0077
ND
0.18
0.040
0.702
3/19/19
1:40
BRF
Bromodichloromethane
ND
0.035
0.013
ND
0.24
0.087
0.702
3/19/19
1:40
BRF
Bromoform
ND
0.035
0.016
ND
0.36
0.16
0.702
3/19/19
1:40
BRF
Bromomethane
ND
0.035
0.024
ND
0.14
0.094
0.702
3/19/19
1:40
BRF
1,3-Butadiene
ND
0.035
0.022
ND
0.078
0.049
0.702
3/19/19
1:40
BRF
2-Butanone (MEK)
ND
1.4
0.055
ND
4.1
0.16
0.702
3/19/19
1:40
BRF
Carbon Disulfide
ND
0.35
0.024
ND
1.1
0.075
0.702
3/19/19
1:40
BRF
Carbon Tetrachloride
0.059
0.035
0.011
0.37
0.22
0.072
0.702
3/19/19
1:40
BRF
Chlorobenzene
ND
0.035
0.017
ND
0.16
0.079
0.702
3/19/19
1:40
BRF
Chloroethane
ND
0.035
0.021
ND
0.093
0.056
0.702
3/19/19
1:40
BRF
Chloroform
ND
0.035
0.013
ND
0.17
0.064
0.702
3/19/19
1:40
BRF
Chloromethane
ND
0.070
0.024
ND
0.14
0.049
0.702
3/19/19
1:40
BRF
Cyclohexane
1100
2.0
1.4
3800
6.9
4.9
40
3/19/19
9:21
BRF
Dibromochloromethane
ND
0.035
0.012
ND
0.30
0.099
0.702
3/19/19
1:40
BRF
1,2-Dibromoethane (EDB)
ND
0.035
0.014
ND
0.27
0.11
0.702
3/19/19
1:40
BRF
1,2-Dichlorobenzene
ND
0.035
0.017
ND
0.21
0.10
0.702
3/19/19
1:40
BRF
1,3-Dichlorobenzene
ND
0.035
0.018
ND
0.21
0.11
0.702
3/19/19
1:40
BRF
1,4-Dichlorobenzene
ND
0.035
0.021
ND
0.21
0.13
0.702
3/19/19
1:40
BRF
Dichlorodifluoromethane (Freon 12)
0.46
0.035
0.015
2.3
0.17
0.075
0.702
3/19/19
1:40
BRF
1, 1 -Dichloroethane
ND
0.035
0.011
ND
0.14
0.043
0.702
3/19/19
1:40
BRF
1,2-Dichloroethane
ND
0.035
0.013
ND
0.14
0.054
0.702
3/19/19
1:40
BRF
1, 1 -Dichloroethylene
ND
0.035
0.014
ND
0.14
0.056
0.702
3/19/19
1:40
BRF
cis-1,2-Dichloroethylene
ND
0.035
0.014
ND
0.14
0.057
0.702
3/19/19
1:40
BRF
trans-1,2-Dichloroethylene
ND
0.035
0.014
ND
0.14
0.056
0.702
3/19/19
1:40
BRF
1,2-Dichloropropane
ND
0.035
0.012
ND
0.16
0.057
0.702
3/19/19
1:40
BRF
cis- 1,3 -Dichloropropene
ND
0.035
0.012
ND
0.16
0.056
0.702
3/19/19
1:40
BRF
trans- 1, 3 -Dichloropropene
ND
0.035
0.013
ND
0.16
0.058
0.702
3/19/19
1:40
BRF
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND
0.035
0.017
ND
0.25
0.12
0.702
3/19/19
1:40
BRF
1,4-Dioxane
ND
0.35
0.23
ND
1.3
0.82
0.702
3/19/19
1:40
BRF
Ethanol
68
40
36
130
75
67
40
3/19/19
9:21
BRF
Ethyl Acetate
ND
0.035
0.026
ND
0.13
0.094
0.702
3/19/19
1:40
BRF
Ethylbenzene
2.2
0.035
0.020
9.6
0.15
0.088
0.702
3/19/19
1:40
BRF
4-Ethyltoluene
0.51
0.035
0.021
2.5
0.17
0.11
0.702
3/19/19
1:40
BRF
Heptane
16
0.035
0.021
66
0.14
0.085
0.702
3/19/19
1:40
BRF
Hexachlorobutadiene
ND
0.035
0.016
ND
0.37
0.17
0.702
3/19/19
1:40
BRF
Hexane
38
36
3.5
130
130
12
40
3/19/19
9:21
BRF
2-Hexanone (MBK)
ND
0.035
0.021 V-05, L-03
ND
0.14
0.085
0.702
3/19/19
1:40
BRF
Isopropanol
ND
1.4
0.043
ND
3.4
0.11
0.702
3/19/19
1:40
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.035
0.018
ND
0.13
0.063
0.702
3/19/19
1:40
BRF
Methylene Chloride
ND
0.35
0.043
ND
1.2
0.15
0.702
3/19/19
1:40
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.035
0.017 V-05
ND
0.14
0.069
0.702
3/19/19
1:40
BRF
Naphthalene
4.3
0.035
0.027
23
0.18
0.14
0.702
3/19/19
1:40
BRF
Propene
ND
1.4
0.035
ND
2.4
0.060
0.702
3/19/19
1:40
BRF
Styrene
ND
0.035
0.022
ND
0.15
0.092
0.702
3/19/19
1:40
BRF
1,1,2,2-Tetrachloroethane
ND
0.035
0.016
ND
0.24
0.11
0.702
3/19/19
1:40
BRF
Page 4 of 29
corl'u ,G)
ANALYTICAL LABORATORY
Project Location: 2728 Capital Blvd.
Date Received: 3/18/2019
Field Sample #: IA-107SR
Sample ID: 19CO786-01
Sample Matrix: Indoor air
Sampled: 3/ 15/2019 16:48
39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332
ANALYTICAL RESULTS
Sample Description/Location:
Sub Description/Location:
Canister ID: 2187
Canister Size: 6 liter
Flow Controller ID: 3094
Sample Type: 8 hr
Work Order: 19CO786
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -8
Receipt Vacuum(in Hg): -7.8
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv ug/m3 Date/Time
Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst
Tetrachloroethylene
1.3
0.035
0.020
8.6
0.24
0.13
0.702
3/19/19
1:40
BRF
Tetrahydrofuran
ND
0.035
0.023
ND
0.10
0.069
0.702
3/19/19
1:40
BRF
Toluene
1700
2.0
1.0
6500
7.5
3.9
40
3/19/19
9:21
BRF
1,2,4-Trichlorobenzene
ND
0.035
0.024
ND
0.26
0.18
0.702
3/19/19
1:40
BRF
1, 1, 1 -Trichloroethane
ND
0.035
0.013
ND
0.19
0.072
0.702
3/19/19
1:40
BRF
1,1,2-Trichloroethane
ND
0.035
0.014
ND
0.19
0.079
0.702
3/19/19
1:40
BRF
Trichloroethylene
ND
0.035
0.014
ND
0.19
0.076
0.702
3/19/19
1:40
BRF
Trichlorofluoromethane (Freon 11)
ND
0.14
0.020
ND
0.79
0.11
0.702
3/19/19
1:40
BRF
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113)
ND
0.14
0.021
ND
1.1
0.16
0.702
3/19/19
1:40
BRF
1,2,4-Trimethylbenzene
0.55
0.035
0.022
2.7
0.17
0.11
0.702
3/19/19
1:40
BRF
1,3,5-Trimethylbenzene
0.16
0.035
0.022
0.79
0.17
0.11
0.702
3/19/19
1:40
BRF
Vinyl Acetate
ND
0.70
0.017
ND
2.5
0.059
0.702
3/19/19
1:40
BRF
Vinyl Chloride
ND
0.035
0.022
ND
0.090
0.057
0.702
3/19/19
1:40
BRF
m&p-Xylene
8.0
0.070
0.040
35
0.30
0.18
0.702
3/19/19
1:40
BRF
o-Xylene
2.4
0.035
0.022
10
0.15
0.095
0.702
3/19/19
1:40
BRF
Surrogates
% Recovery
% REC Limits
4-Bromofluorobenzene (1) 107 70-130
4-Bromofluorobenzene (1) 92.1 70-130
4-Bromofluorobenzene (1) 120 70-130
3/19/19 9:21
3/19/19 20:12
3/19/19 1:40
Page 5 of 29
corl'u ,G)
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332
ANALYTICAL RESULTS
Project Location: 2728 Capital Blvd.
Sample Description/Location:
Work Order: 19CO786
Date Received: 3/18/2019
Sub Description/Location:
Initial Vacuum(in Hg): -30
Field Sample #: IA-119SR
Canister ID: 1014
Final Vacuum(in Hg): -7
Sample ID: 19CO786-02
Canister Size: 6 liter
Receipt Vacuum(in Hg): -8.3
Sample Matrix: Indoor air
Flow Controller ID: 3271
Flow Controller Type: Fixed -Orifice
Sampled: 3/15/2019 16:42
Sample Type: 8 hr
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual
Results
ug/m3
RL
MDL
Dilution
Date/Time
Analyzed
Analyst
Acetone
6200
600
210
15000
1400
490
300
3/19/19 20:51
BRF
Benzene
1.1
0.035
0.014
3.5
0.11
0.046
0.702
3/19/19 2:16
BRF
Benzyl chloride
ND
0.035
0.0077
ND
0.18
0.040
0.702
3/19/19 2:16
BRF
Bromodichloromethane
ND
0.035
0.013
ND
0.24
0.087
0.702
3/19/19 2:16
BRF
Bromoform
ND
0.035
0.016
ND
0.36
0.16
0.702
3/19/19 2:16
BRF
Bromomethane
ND
0.035
0.024
ND
0.14
0.094
0.702
3/19/19 2:16
BRF
1,3-Butadiene
ND
0.035
0.022
ND
0.078
0.049
0.702
3/19/19 2:16
BRF
2-Butanone (MEK)
ND
1.4
0.055
ND
4.1
0.16
0.702
3/19/19 2:16
BRF
Carbon Disulfide
ND
0.35
0.024
ND
1.1
0.075
0.702
3/19/19 2:16
BRF
Carbon Tetrachloride
ND
0.035
0.011
ND
0.22
0.072
0.702
3/19/19 2:16
BRF
Chlorobenzene
ND
0.035
0.017
ND
0.16
0.079
0.702
3/19/19 2:16
BRF
Chloroethane
ND
0.035
0.021
ND
0.093
0.056
0.702
3/19/19 2:16
BRF
Chloroform
ND
0.035
0.013
ND
0.17
0.064
0.702
3/19/19 2:16
BRF
Chloromethane
ND
0.070
0.024
ND
0.14
0.049
0.702
3/19/19 2:16
BRF
Cyclohexane
1700
15
11
5700
52
37
300
3/19/19 20:51
BRF
Dibromochloromethane
ND
0.035
0.012
ND
0.30
0.099
0.702
3/19/19 2:16
BRF
1,2-Dibromoethane (EDB)
ND
0.035
0.014
ND
0.27
0.11
0.702
3/19/19 2:16
BRF
1,2-Dichlorobenzene
ND
0.035
0.017
ND
0.21
0.10
0.702
3/19/19 2:16
BRF
1,3-Dichlorobenzene
ND
0.035
0.018
ND
0.21
0.11
0.702
3/19/19 2:16
BRF
1,4-Dichlorobenzene
ND
0.035
0.021
ND
0.21
0.13
0.702
3/19/19 2:16
BRF
Dichlorodifluoromethane (Freon 12)
0.53
0.035
0.015
2.6
0.17
0.075
0.702
3/19/19 2:16
BRF
1,1-Dichloroethane
ND
0.035
0.011
ND
0.14
0.043
0.702
3/19/19 2:16
BRF
1,2-Dichloroethane
ND
0.035
0.013
ND
0.14
0.054
0.702
3/19/19 2:16
BRF
1,1-Dichloroethylene
ND
0.035
0.014
ND
0.14
0.056
0.702
3/19/19 2:16
BRF
cis-1,2-Dichloroethylene
ND
0.035
0.014
ND
0.14
0.057
0.702
3/19/19 2:16
BRF
trans-1,2-Dichloroethylene
0.25
0.035
0.014
0.98
0.14
0.056
0.702
3/19/19 2:16
BRF
1,2-Dichloropropene
ND
0.035
0.012
ND
0.16
0.057
0.702
3/19/19 2:16
BRF
cis- 1,3 -Dichloropropene
ND
0.035
0.012
ND
0.16
0.056
0.702
3/19/19 2:16
BRF
trans- 1, 3 -Dichloropropene
ND
0.035
0.013
ND
0.16
0.058
0.702
3/19/19 2:16
BRF
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
ND
0.035
0.017
ND
0.25
0.12
0.702
3/19/19 2:16
BRF
1,4-Dioxane
ND
0.35
0.23
ND
1.3
0.82
0.702
3/19/19 2:16
BRF
Ethanol
70
40
36
130
75
67
40
3/19/19 9:48
BRF
Ethyl Acetate
ND
0.035
0.026
ND
0.13
0.094
0.702
3/19/19 2:16
BRF
Ethylbenzene
4.3
0.035
0.020
19
0.15
0.088
0.702
3/19/19 2:16
BRF
4-Ethyltoluene
0.56
0.035
0.021
2.8
0.17
0.11
0.702
3/19/19 2:16
BRF
Heptane
27
0.035
0.021
110
0.14
0.085
0.702
3/19/19 2:16
BRF
Hexachlorobutadiene
ND
0.035
0.016
ND
0.37
0.17
0.702
3/19/19 2:16
BRF
Hexane
79
40
3.5
280
140
12
40
3/19/19 9:48
BRF
2-Hexanone (MBK)
ND
0.035
0.021
L-03, V-05
ND
0.14
0.085
0.702
3/19/19 2:16
BRF
Isopropanol
ND
1.4
0.043
ND
3.4
0.11
0.702
3/19/19 2:16
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.035
0.018
ND
0.13
0.063
0.702
3/19/19 2:16
BRF
Methylene Chloride
ND
0.35
0.043
ND
1.2
0.15
0.702
3/19/19 2:16
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.035
0.017
V-05
ND
0.14
0.069
0.702
3/19/19 2:16
BRF
Naphthalene
3.1
0.035
0.027
16
0.18
0.14
0.702
3/19/19 2:16
BRF
Propene
ND
1.4
0.035
ND
2.4
0.060
0.702
3/19/19 2:16
BRF
Styrene
ND
0.035
0.022
ND
0.15
0.092
0.702
3/19/19 2:16
BRF
1,1,2,2-Tetrachloroethane
ND
0.035
0.016
ND
0.24
0.11
0.702
3/19/19 2:16
BRF
Page 6 of 29
corl'u ,G)
ANALYTICAL LABORATORY
Project Location: 2728 Capital Blvd.
Date Received: 3/18/2019
Field Sample #: IA-119SR
Sample ID: 19CO786-02
Sample Matrix: Indoor air
Sampled: 3/ 15/2019 16:42
39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332
ANALYTICAL RESULTS
Sample Description/Location:
Sub Description/Location:
Canister ID: 1014
Canister Size: 6 liter
Flow Controller ID: 3271
Sample Type: 8 hr
Work Order: 19CO786
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -7
Receipt Vacuum(in Hg): -8.3
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv ug/m3 Date/Time
Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst
Tetrachloroethylene
1.3
0.035
0.020
9.1
0.24
0.13
0.702
3/19/19 2:16
BRF
Tetrahydrofuran
ND
0.035
0.023
ND
0.10
0.069
0.702
3/19/19 2:16
BRF
Toluene
3700
15
7.7
L-05 14000
57
29
300
3/19/19 20:51
BRF
1,2,4-Trichlorobenzene
ND
0.035
0.024
ND
0.26
0.18
0.702
3/19/19 2:16
BRF
1, 1, 1 -Trichloroethane
ND
0.035
0.013
ND
0.19
0.072
0.702
3/19/19 2:16
BRF
1,1,2-Trichloroethane
ND
0.035
0.014
ND
0.19
0.079
0.702
3/19/19 2:16
BRF
Trichloroethylene
ND
0.035
0.014
ND
0.19
0.076
0.702
3/19/19 2:16
BRF
Trichlorofluoromethane (Freon 11)
ND
0.14
0.020
ND
0.79
0.11
0.702
3/19/19 2:16
BRF
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113)
ND
0.14
0.021
ND
1.1
0.16
0.702
3/19/19 2:16
BRF
1,2,4-Trimethylbenzene
0.60
0.035
0.022
2.9
0.17
0.11
0.702
3/19/19 2:16
BRF
1,3,5-Trimethylbenzene
0.16
0.035
0.022
0.81
0.17
0.11
0.702
3/19/19 2:16
BRF
Vinyl Acetate
ND
0.70
0.017
ND
2.5
0.059
0.702
3/19/19 2:16
BRF
Vinyl Chloride
ND
0.035
0.022
ND
0.090
0.057
0.702
3/19/19 2:16
BRF
m&p-Xylene
15
0.070
0.040
67
0.30
0.18
0.702
3/19/19 2:16
BRF
o-Xylene
4.6
0.035
0.022
20
0.15
0.095
0.702
3/19/19 2:16
BRF
Surrogates
% Recovery
% REC Limits
4-Bromofluorobenzene (1) 105 70-130
4-Bromofluorobenzene (1) 88.3 70-130
4-Bromofluorobenzene (1) 119 70-130
3/19/19 9:48
3/19/19 20:51
3/19/19 2:16
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