21041 Northend Square II BAR 2019.04.12

Wood Environment & Infrastructure Solutions, Inc.
2801 Yorkmont Road, Suite 100
Charlotte, North Carolina 28208
Licensures: NC Engineering F-1253, Geology C-247
T: 704-357-8600
www.woodplc.com
‘Wood’ is a trading name for John Wood Group PLC and its subsidiaries
April 12, 2019
Ms. Caroline Goodwin, Brownfields Project Manager
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Subject:Report of Soil-Gas Sampling and Analysis
North End Square II
813 Oaklawn Avenue
Charlotte, North Carolina
Brownfields Project Number 21041-17-060
Wood Project No: 6228-17-0442
Dear Ms.Goodwin:
Wood Environment & Infrastructure Solutions, Inc. (Wood) is pleased to submit this Report of
Soil-Gas Sampling and Analysis outlining work activities performed at the above-referenced site.
Included in this report is site information and history,description of the field assessment
activities,results, and conclusions and recommendations. This work was performed in
accordance with the Work Plan (dated March 14, 2019).Approval of the work plan was received
from the North Carolina Department of Environmental Quality (NCDEQ) Brownfields Program
(BFP)via email on March 19, 2019.
Site Information and History
The subject property encompasses approximately 7 acres at the intersection of Statesville and
Oaklawn Avenues in Charlotte, North Carolina (Figure 1). Wood completed a Brownfields
Assessment Report (dated February 4, 2019) and submitted the report to the NCDEQ,BFP for
review.Based on the results of the assessment, Wood concluded the following:
Report of Soil-Gas Sampling and Analysis April 12, 2019
North End Square II
Charlotte, North Carolina
Wood Project: 6228-17-0442
2
The source of the hexavalent chromium in the soil sample SS-5 is unknown.
Analysis of the groundwater sample collected from well MW-1 (near former drycleaners)
identified PCE.
Analysis of the groundwater sample collected from well MW-2 (vicinity of the former
auto filling station and hydraulically downgradient from the Rite Aid Property (also
known as NewCAMP and the Former Charlotte Army Missile Plant)did not identify
detectable concentrations of VOCs or SVOCs.
Analysis of the groundwater sample collected from well MW-3 (installed along Oaklawn
Avenue near the former filling station)identified several different petroleum and
chlorinated solvent constituents.
Analysis of the groundwater sample collected from well MW-4 (in the southern portion
of the boundary in the vicinity of the former paint shop)identified TCE.
Following review by BFP personnel, in a letter dated March 12, 2019, Ms. Caroline Goodwin
requested that soil-gas sampling and analysis be performed to address a data gap. The data gap
to be addressed is the potential for vapor intrusion into structures proposed to be built at the
property.
The assessment activities have been performed in general accordance with the most recent
Inactive Hazardous Sites Branch (IHSB) Program Guidelines for Assessment and Cleanup
(http://portal.ncdenr.org/web/wm/sf/ihs/ihsguide), dated October 2015 and the most recent
versions of the U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem
Support Division (SESD) Field Branches Quality System and Technical Procedures guidance.
Field Assessment Activities
On March 27, 2019, Wood’s subcontractor,Geologic Exploration Inc. (GEX),advanced one
boring to a depth of 5 feet bgs using a direct-push rig and due to equipment failure,six borings
to a depth of 5 feet bgs using a hand auger. GEX and Wood personnel installed soil-gas
sampling points in each of the borings to a depth of 5 bgs.The soil-gas sampling was
performed in general accordance with the NCDEQ, DWM Vapor Intrusion Guidance, dated
February 2018 (https://deq.nc.gov/about/divisions/waste-management/waste-management-
permit-guidance/dwm-vapor-intrusion-guidance).The locations of the seven soil-gas sampling
Report of Soil-Gas Sampling and Analysis April 12, 2019
North End Square II
Charlotte, North Carolina
Wood Project: 6228-17-0442
3
points are shown on Figure 2.For the seven locations, dedicated sampling points were placed in
each open borehole and connected to Teflon™ tubing extending to the ground surface and
attached to 6-liter Summa®canisters. A sand pack of approximately 8 to 10 inches thick was
placed around the sampling points. The remaining annulus of the boreholes was filled with
hydrated bentonite to the ground surface. Prior to sample collection, each sample train was
purged of stagnant air and a leak-check was performed.
The Summa®canisters and sample train were surrounded by a helium-shroud for leak-check
detection.The helium-shroud consisted of plastic bag placed over the Summa®canisters and
sample tubing and then filled with helium. A leak test was performed at each soil-gas point.
Wood personnel collected the leak test samples using Tedlar®bags. Each leak test sample was
screened in the field for helium using a MGD-2002 Multi-Gas leak (di-electric) detector. Wood
personnel also used the helium detector to monitor the concentration of helium inside the
shrouds. A leak was considered to have occurred when the helium concentration inside the
Tedlar®bag was greater than 10% of the helium concentration within the shroud.The vacuum
reading of each Summa®canister was recorded prior to and after sample collection and
sampling was considered complete when a residual vacuum of less than 5 inches of mercury was
present in the canister.
Following the leak-check, a soil-gas sample was collected into the Summa®canister at an
approximate flow rate of 200 mL/min (30-min sample time). Following collection of the soil-gas
samples, the Summa®canisters were shipped via courier to Con-Test®Analytical Laboratory for
analysis. The soil-gas samples were analyzed by Con-Test®for analysis of VOCs via EPA Method
TO-15. The soil-gas samples were maintained under chain-of-custody protocol. One field
duplicate QA/QC soil-gas sample (SG-Dup) was collected from the sample point SG-7 for
analysis by Method TO-15.Following the collection of the soil-gas samples, the soil-gas points
were removed and the boreholes were abandoned by filling with bentonite to grade.Field
worksheets for the soil-gas sampling are included as Attachment A.
Report of Soil-Gas Sampling and Analysis April 12, 2019
North End Square II
Charlotte, North Carolina
Wood Project: 6228-17-0442
Table
Constituent SG-1 SG-2 SG-3 SG-4 SG-5 SG-6 SG-7 SG-Dup
Date Collected 3/26/2019 3/26/2019 3/26/2019 3/26/2019 3/26/2019 3/26/2019 3/26/2019 3/26/2019
Acetone 13 J <19 <19 23 <19 <19 18 J 29 220,000
Benzene 2.4 1.8 2.3 2.8 2.3 2.1 2.5 3.6 120
2-Butanone (MEK)4.6 J <24 <24 3.1 J 1.7 J 1.5 J 5.2 J 4.7 J 35,000
Chloroform 3.2 <0.98 <0.98 <0.98 <0.98 <0.98 <0.98 <0.98 41
Cyclohexane <0.69 3.5 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 42,000
1,3-Dichlorobenzene 2.9 <1.2 2.7 2.3 3.4 1.8 2.5 2.0 NSL
Dichlorodifluoromethane (Freon 12)1.7 2.0 1.4 1.6 1.6 1.6 2.2 1.9 700
Ethylbenzene 1.6 2.0 2.3 1.1 1.4 1.1 2.2 2.6 370
4-Ethyltoluene 2.9 <0.98 <0.98 <0.98 <0.98 <0.98 2.8 1.9 NSL
Heptane 8.1 5.5 6.2 4.9 4.8 5.1 7.4 6.5 2,800
Hexane 5.0 J 11 J 11 J 7.6 J 10.0 J 7.1 J 10 J 9.4 J 4,900
Methylene Chloride 1.8 J 3.6 J 4.0 J 1.7 J 2.0 J 2.0 J 3.0 J 3.4 J 4,200
4-Methyl-2-pentanone (MIBK)<0.82 <0.82 <0.82 <0.82 <0.82 <0.82 4.1 3.2 21,000
Propene 9.9 J <14 <14 14 <14 <14 <14 <14 21,000
Tetrachloroethylene 130 170 190 100 130 110 150 170 280
Toluene 16 17 21 11 12 11 20 23 35,000
Trichlorofluoromethane (Freon 11)1.3 J 1.4 J <4.5 1.3 J 1.2 J 1.1 J 1.2 J 1.3 J NSL
1,2,4-Trimethylbenzene 2.1 <0.98 1.6 <0.98 <0.98 <0.98 <0.98 1.6 420
1,3,5-Trimethylbenzene 0.63 J <0.98 <0.98 <0.98 <0.98 <0.98 <0.98 <0.98 420
m&p-Xylene 3.6 6.5 7.3 3.3 3.5 2.8 5.9 7.6 720
o-Xylene 1.4 2.1 2.4 1.1 1.0 1.1 2.1 2.7 720
Notes:Prepared By/Date:MDF/4-2-19
1. Concentrations shown in micrograms per meter cubed (µg/m3)Checked By/Date:RPD/4-2-19
2. DWM Residential SGSLs = Division of Waste Management Residential Soil-Gas Screening Levels, dated February 2018
3. NSL = No screening level established
4. J = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
5. Samples analyzed for VOCs via EPA Method TO-15
6. Helium used as leak-check and was added to shroud surrounding the sample train prior to collection of the sample. Helium was analyzed in the field using a MGD-2002 Multi-Gas leak (di-electric) detector
7. Values shown as less than (<) reference the reporting limits (RLs)
8. SG-Dup collected from SG-7 location
Table 1: Soil-Gas Analytical Results
DWM Residential SGSLs
Wood Project: 6228-17-0442
Charlotte, North Carolina
North End Square II
Report of Soil-Gas Sampling and Analysis April 12, 2019
North End Square II
Charlotte, North Carolina
Wood Project: 6228-17-0442
Figures
Copyright:© 2013 National Geographic Society, i-cubed
PREPARED BY: LM DATE: 10/23/2018 DATE: 10/23/2018CHECKED BY: RF
Site Boundary
Document Path: F:\AMEC_Projects\2017\6228-17-0442 Drakeford\GIS\MXDs\Topo.mxd¯
PROJECT NO: 6228-17-0442 FIGURE NO: 1
SITE TOPONorth End Square II813 Oaklawn Avenue Charlotte, North Carolina
0 1,000 2,000500Feet
P
P
P
P
P
P
P
SG-3
SG-4
SG-2
SG-5
SG-1
SG-6
SG-7/SG-Dup
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/AirbusDS, USDA, USGS, AeroGRID, IGN, and the GIS User Community
¯
Soil-Gas, Groundwater and Soil Sample LocationsNorth End Square II813 Oaklawn AvenueCharlotte, North Carolina
0 125 25062.5 Feet
?
!?
P
P
!
!
MW-3
BG
MW-1
SS-2/MW-2
SS-4/MW-4
SS-3
SS-6
SS-5
SS-7
!SS-1
!
SS-8
Monitoring Well Location!
!
P
?
!?
Shallow Soil Sample Location (VOCs, SVOCs, Total Metals) and Monitoring Well LocationShallow Soil Sample Location (VOCs, SVOCs, Total Metals and Hexavalent Chromium) and Monitoring Well Location
Shallow Soil Sample Location (VOCs, SVOCs, Total Metals and Hexavalent Chromium) "background" shallow soil sampling for metals
Shallow Soil Sample Location (VOCs, SVOCs and Total Metals)
P Soil-Gas Sample Location
PROJECT NO: 6228-17-0442 FIGURE NO: 2PREPARED BY: LM DATE: 3/27/2019 CHECKED BY: MF DATE: 3/27/2019
Report of Soil-Gas Sampling and Analysis April 12, 2019
North End Square II
Charlotte, North Carolina
Wood Project: 6228-17-0442
Attachment A
Field Worksheets
Report of Soil-Gas Sampling and Analysis April 12, 2019
North End Square II
Charlotte, North Carolina
Wood Project: 6228-17-0442
Attachment B
Laboratory Analytical Report and Chain-of-Custody Forms
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 2, 2019
Rob Foster
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: Charlotte, NC
Client Job Number:
Project Number: 6228170442
Laboratory Work Order Number: 19C1502
Enclosed are results of analyses for samples received by the laboratory on March 26, 2019. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/2/2019Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228170442
19C1502
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
SG-1 19C1502-01 Soil Gas EPA TO-15
SG-2 19C1502-02 Soil Gas EPA TO-15
SG-3 19C1502-03 Soil Gas EPA TO-15
SG-4 19C1502-04 Soil Gas EPA TO-15
SG-5 19C1502-05 Soil Gas EPA TO-15
SG-6 19C1502-06 Soil Gas EPA TO-15
SG-7 19C1502-07 Soil Gas EPA TO-15
SG-DUP 19C1502-08 Soil Gas EPA TO-15
Page 2 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be
biased on the low side.
Analyte & Samples(s) Qualified:
1,1,1-Trichloroethane, Benzene, Tetrahydrofuran
19C1502-01[SG-1], 19C1502-02[SG-2], 19C1502-03[SG-3], 19C1502-04[SG-4], 19C1502-05[SG-5], 19C1502-06[SG-6], 19C1502-07[SG-7], 19C1502-08[SG-DUP],
B227059-BS1
Duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result.
Analyte & Samples(s) Qualified:
Benzene
B227059-DUP1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
Benzene, Carbon Tetrachloride
S034124-CCV1, 19C1502-01[SG-1], 19C1502-02[SG-2], 19C1502-03[SG-3], 19C1502-04[SG-4], 19C1502-05[SG-5], 19C1502-06[SG-6], 19C1502-07[SG-7],
19C1502-08[SG-DUP]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 3 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-1
Sample ID: 19C1502-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.1
Sampled: 3/26/2019 15:05
Canister ID: 2044
Flow Controller ID: 4201
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 5.4 8.0 3/30/19 21:30 BRFJ13 4192.8 6.6
Benzene 0.74 0.20 3/30/19 21:30 BRFL-03 2.4 40.640.082 0.26
Benzyl chloride ND 0.20 3/30/19 21:30 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/30/19 21:30 BRFND41.30.074 0.49
Bromoform ND 0.20 3/30/19 21:30 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/30/19 21:30 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 3/30/19 21:30 BRFND40.440.13 0.28
2-Butanone (MEK)1.6 8.0 3/30/19 21:30 BRFJ4.6 4240.31 0.92
Carbon Disulfide ND 2.0 3/30/19 21:30 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/30/19 21:30 BRFV-05 ND 41.30.065 0.41
Chlorobenzene ND 0.20 3/30/19 21:30 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/30/19 21:30 BRFND40.530.12 0.32
Chloroform 0.65 0.20 3/30/19 21:30 BRF3.2 40.980.074 0.36
Chloromethane ND 0.40 3/30/19 21:30 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/30/19 21:30 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/30/19 21:30 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/30/19 21:30 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/30/19 21:30 BRFND41.20.096 0.58
1,3-Dichlorobenzene 0.48 0.20 3/30/19 21:30 BRF2.9 41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/30/19 21:30 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.34 0.20 3/30/19 21:30 BRF1.7 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/30/19 21:30 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/30/19 21:30 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/30/19 21:30 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/30/19 21:30 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/30/19 21:30 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/30/19 21:30 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/30/19 21:30 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/30/19 21:30 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/30/19 21:30 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 3/30/19 21:30 BRFND47.21.3 4.6
Ethanol ND 8.0 3/30/19 21:30 BRFND4153.6 6.7
Ethyl Acetate ND 0.20 3/30/19 21:30 BRFND40.720.15 0.54
Ethylbenzene 0.36 0.20 3/30/19 21:30 BRF1.6 40.870.12 0.50
4-Ethyltoluene 0.58 0.20 3/30/19 21:30 BRF2.9 40.980.12 0.60
Heptane 2.0 0.20 3/30/19 21:30 BRF8.1 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/30/19 21:30 BRFND42.10.092 0.98
Hexane 1.4 8.0 3/30/19 21:30 BRFJ5.0 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/30/19 21:30 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/30/19 21:30 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/30/19 21:30 BRFND40.720.10 0.36
Methylene Chloride 0.52 2.0 3/30/19 21:30 BRFJ1.8 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/30/19 21:30 BRFND40.820.096 0.39
Naphthalene ND 0.20 3/30/19 21:30 BRFND41.00.15 0.80
Propene 5.8 8.0 3/30/19 21:30 BRFJ9.9 4140.20 0.34
Styrene ND 0.20 3/30/19 21:30 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/30/19 21:30 BRFND41.40.089 0.61
Page 4 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-1
Sample ID: 19C1502-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.1
Sampled: 3/26/2019 15:05
Canister ID: 2044
Flow Controller ID: 4201
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 19 0.20 3/30/19 21:30 BRF130 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/30/19 21:30 BRFL-03 ND 40.590.13 0.39
Toluene 4.4 0.20 3/30/19 21:30 BRF16 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/30/19 21:30 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/30/19 21:30 BRFL-03 ND 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/30/19 21:30 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/30/19 21:30 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.23 0.80 3/30/19 21:30 BRFJ1.3 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/30/19 21:30 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 0.44 0.20 3/30/19 21:30 BRF2.1 40.980.13 0.63
1,3,5-Trimethylbenzene 0.13 0.20 3/30/19 21:30 BRFJ0.63 40.980.13 0.62
Vinyl Acetate ND 4.0 3/30/19 21:30 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/30/19 21:30 BRFND40.510.13 0.32
m&p-Xylene 0.84 0.40 3/30/19 21:30 BRF3.6 41.70.23 1.00
o-Xylene 0.33 0.20 3/30/19 21:30 BRF1.4 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 3/30/19 21:3070-130
Page 5 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-2
Sample ID: 19C1502-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.8
Sampled: 3/26/2019 11:10
Canister ID: 1735
Flow Controller ID: 4288
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 3/30/19 22:12 BRFND4192.8 6.6
Benzene 0.55 0.20 3/30/19 22:12 BRFL-03 1.8 40.640.082 0.26
Benzyl chloride ND 0.20 3/30/19 22:12 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/30/19 22:12 BRFND41.30.074 0.49
Bromoform ND 0.20 3/30/19 22:12 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/30/19 22:12 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 3/30/19 22:12 BRFND40.440.13 0.28
2-Butanone (MEK)ND 8.0 3/30/19 22:12 BRFND4240.31 0.92
Carbon Disulfide ND 2.0 3/30/19 22:12 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/30/19 22:12 BRFV-05 ND 41.30.065 0.41
Chlorobenzene ND 0.20 3/30/19 22:12 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/30/19 22:12 BRFND40.530.12 0.32
Chloroform ND 0.20 3/30/19 22:12 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/30/19 22:12 BRFND40.830.14 0.28
Cyclohexane 1.0 0.20 3/30/19 22:12 BRF3.5 40.690.14 0.49
Dibromochloromethane ND 0.20 3/30/19 22:12 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/30/19 22:12 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/30/19 22:12 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/30/19 22:12 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/30/19 22:12 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.41 0.20 3/30/19 22:12 BRF2.0 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/30/19 22:12 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/30/19 22:12 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/30/19 22:12 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/30/19 22:12 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/30/19 22:12 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/30/19 22:12 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/30/19 22:12 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/30/19 22:12 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/30/19 22:12 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 3/30/19 22:12 BRFND47.21.3 4.6
Ethanol ND 8.0 3/30/19 22:12 BRFND4153.6 6.7
Ethyl Acetate ND 0.20 3/30/19 22:12 BRFND40.720.15 0.54
Ethylbenzene 0.47 0.20 3/30/19 22:12 BRF2.0 40.870.12 0.50
4-Ethyltoluene ND 0.20 3/30/19 22:12 BRFND40.980.12 0.60
Heptane 1.3 0.20 3/30/19 22:12 BRF5.5 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/30/19 22:12 BRFND42.10.092 0.98
Hexane 3.0 8.0 3/30/19 22:12 BRFJ11 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/30/19 22:12 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/30/19 22:12 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/30/19 22:12 BRFND40.720.10 0.36
Methylene Chloride 1.0 2.0 3/30/19 22:12 BRFJ3.6 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/30/19 22:12 BRFND40.820.096 0.39
Naphthalene ND 0.20 3/30/19 22:12 BRFND41.00.15 0.80
Propene ND 8.0 3/30/19 22:12 BRFND4140.20 0.34
Styrene ND 0.20 3/30/19 22:12 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/30/19 22:12 BRFND41.40.089 0.61
Page 6 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-2
Sample ID: 19C1502-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.8
Sampled: 3/26/2019 11:10
Canister ID: 1735
Flow Controller ID: 4288
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 25 0.20 3/30/19 22:12 BRF170 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/30/19 22:12 BRFL-03 ND 40.590.13 0.39
Toluene 4.4 0.20 3/30/19 22:12 BRF17 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/30/19 22:12 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/30/19 22:12 BRFL-03 ND 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/30/19 22:12 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/30/19 22:12 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.24 0.80 3/30/19 22:12 BRFJ1.4 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/30/19 22:12 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 3/30/19 22:12 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/30/19 22:12 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/30/19 22:12 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/30/19 22:12 BRFND40.510.13 0.32
m&p-Xylene 1.5 0.40 3/30/19 22:12 BRF6.5 41.70.23 1.00
o-Xylene 0.48 0.20 3/30/19 22:12 BRF2.1 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 3/30/19 22:1270-130
Page 7 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-3
Sample ID: 19C1502-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.2
Sampled: 3/26/2019 11:56
Canister ID: 1841
Flow Controller ID: 4292
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 3/31/19 7:44 BRFND4192.8 6.6
Benzene 0.72 0.20 3/31/19 7:44 BRFL-03 2.3 40.640.082 0.26
Benzyl chloride ND 0.20 3/31/19 7:44 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/31/19 7:44 BRFND41.30.074 0.49
Bromoform ND 0.20 3/31/19 7:44 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/31/19 7:44 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 3/31/19 7:44 BRFND40.440.13 0.28
2-Butanone (MEK)ND 8.0 3/31/19 7:44 BRFND4240.31 0.92
Carbon Disulfide ND 2.0 3/31/19 7:44 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/31/19 7:44 BRFV-05 ND 41.30.065 0.41
Chlorobenzene ND 0.20 3/31/19 7:44 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/31/19 7:44 BRFND40.530.12 0.32
Chloroform ND 0.20 3/31/19 7:44 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/31/19 7:44 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/31/19 7:44 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/31/19 7:44 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/31/19 7:44 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/31/19 7:44 BRFND41.20.096 0.58
1,3-Dichlorobenzene 0.44 0.20 3/31/19 7:44 BRF2.7 41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/31/19 7:44 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.28 0.20 3/31/19 7:44 BRF1.4 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/31/19 7:44 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/31/19 7:44 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/31/19 7:44 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/31/19 7:44 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/31/19 7:44 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/31/19 7:44 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/31/19 7:44 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/31/19 7:44 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/31/19 7:44 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 3/31/19 7:44 BRFND47.21.3 4.6
Ethanol ND 8.0 3/31/19 7:44 BRFND4153.6 6.7
Ethyl Acetate ND 0.20 3/31/19 7:44 BRFND40.720.15 0.54
Ethylbenzene 0.52 0.20 3/31/19 7:44 BRF2.3 40.870.12 0.50
4-Ethyltoluene ND 0.20 3/31/19 7:44 BRFND40.980.12 0.60
Heptane 1.5 0.20 3/31/19 7:44 BRF6.2 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/31/19 7:44 BRFND42.10.092 0.98
Hexane 3.2 8.0 3/31/19 7:44 BRFJ11 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/31/19 7:44 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/31/19 7:44 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/31/19 7:44 BRFND40.720.10 0.36
Methylene Chloride 1.2 2.0 3/31/19 7:44 BRFJ4.0 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/31/19 7:44 BRFND40.820.096 0.39
Naphthalene ND 0.20 3/31/19 7:44 BRFND41.00.15 0.80
Propene ND 8.0 3/31/19 7:44 BRFND4140.20 0.34
Styrene ND 0.20 3/31/19 7:44 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/31/19 7:44 BRFND41.40.089 0.61
Page 8 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-3
Sample ID: 19C1502-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.2
Sampled: 3/26/2019 11:56
Canister ID: 1841
Flow Controller ID: 4292
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 28 0.20 3/31/19 7:44 BRF190 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/31/19 7:44 BRFL-03 ND 40.590.13 0.39
Toluene 5.5 0.20 3/31/19 7:44 BRF21 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/31/19 7:44 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/31/19 7:44 BRFL-03 ND 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/31/19 7:44 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/31/19 7:44 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)ND 0.80 3/31/19 7:44 BRFND44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/31/19 7:44 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 0.32 0.20 3/31/19 7:44 BRF1.6 40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/31/19 7:44 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/31/19 7:44 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/31/19 7:44 BRFND40.510.13 0.32
m&p-Xylene 1.7 0.40 3/31/19 7:44 BRF7.3 41.70.23 1.00
o-Xylene 0.55 0.20 3/31/19 7:44 BRF2.4 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 3/31/19 7:4470-130
Page 9 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-4
Sample ID: 19C1502-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.4
Sampled: 3/26/2019 12:31
Canister ID: 1027
Flow Controller ID: 4300
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 9.5 8.0 3/30/19 23:34 BRF23 4192.8 6.6
Benzene 0.89 0.20 3/30/19 23:34 BRFL-03 2.8 40.640.082 0.26
Benzyl chloride ND 0.20 3/30/19 23:34 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/30/19 23:34 BRFND41.30.074 0.49
Bromoform ND 0.20 3/30/19 23:34 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/30/19 23:34 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 3/30/19 23:34 BRFND40.440.13 0.28
2-Butanone (MEK)1.0 8.0 3/30/19 23:34 BRFJ3.1 4240.31 0.92
Carbon Disulfide ND 2.0 3/30/19 23:34 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/30/19 23:34 BRFV-05 ND 41.30.065 0.41
Chlorobenzene ND 0.20 3/30/19 23:34 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/30/19 23:34 BRFND40.530.12 0.32
Chloroform ND 0.20 3/30/19 23:34 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/30/19 23:34 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/30/19 23:34 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/30/19 23:34 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/30/19 23:34 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/30/19 23:34 BRFND41.20.096 0.58
1,3-Dichlorobenzene 0.38 0.20 3/30/19 23:34 BRF2.3 41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/30/19 23:34 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.32 0.20 3/30/19 23:34 BRF1.6 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/30/19 23:34 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/30/19 23:34 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/30/19 23:34 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/30/19 23:34 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/30/19 23:34 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/30/19 23:34 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/30/19 23:34 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/30/19 23:34 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/30/19 23:34 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 3/30/19 23:34 BRFND47.21.3 4.6
Ethanol ND 8.0 3/30/19 23:34 BRFND4153.6 6.7
Ethyl Acetate ND 0.20 3/30/19 23:34 BRFND40.720.15 0.54
Ethylbenzene 0.24 0.20 3/30/19 23:34 BRF1.1 40.870.12 0.50
4-Ethyltoluene ND 0.20 3/30/19 23:34 BRFND40.980.12 0.60
Heptane 1.2 0.20 3/30/19 23:34 BRF4.9 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/30/19 23:34 BRFND42.10.092 0.98
Hexane 2.2 8.0 3/30/19 23:34 BRFJ7.6 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/30/19 23:34 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/30/19 23:34 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/30/19 23:34 BRFND40.720.10 0.36
Methylene Chloride 0.48 2.0 3/30/19 23:34 BRFJ1.7 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/30/19 23:34 BRFND40.820.096 0.39
Naphthalene ND 0.20 3/30/19 23:34 BRFND41.00.15 0.80
Propene 8.1 8.0 3/30/19 23:34 BRF14 4140.20 0.34
Styrene ND 0.20 3/30/19 23:34 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/30/19 23:34 BRFND41.40.089 0.61
Page 10 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-4
Sample ID: 19C1502-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.4
Sampled: 3/26/2019 12:31
Canister ID: 1027
Flow Controller ID: 4300
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 15 0.20 3/30/19 23:34 BRF100 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/30/19 23:34 BRFL-03 ND 40.590.13 0.39
Toluene 2.8 0.20 3/30/19 23:34 BRF11 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/30/19 23:34 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/30/19 23:34 BRFL-03 ND 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/30/19 23:34 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/30/19 23:34 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.24 0.80 3/30/19 23:34 BRFJ1.3 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/30/19 23:34 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 3/30/19 23:34 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/30/19 23:34 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/30/19 23:34 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/30/19 23:34 BRFND40.510.13 0.32
m&p-Xylene 0.76 0.40 3/30/19 23:34 BRF3.3 41.70.23 1.00
o-Xylene 0.26 0.20 3/30/19 23:34 BRF1.1 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 3/30/19 23:3470-130
Page 11 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-5
Sample ID: 19C1502-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.5
Sampled: 3/26/2019 13:00
Canister ID: 1075
Flow Controller ID: 4293
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 3/31/19 9:10 BRFND4192.8 6.6
Benzene 0.72 0.20 3/31/19 9:10 BRFL-03 2.3 40.640.082 0.26
Benzyl chloride ND 0.20 3/31/19 9:10 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/31/19 9:10 BRFND41.30.074 0.49
Bromoform ND 0.20 3/31/19 9:10 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/31/19 9:10 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 3/31/19 9:10 BRFND40.440.13 0.28
2-Butanone (MEK)0.59 8.0 3/31/19 9:10 BRFJ1.7 4240.31 0.92
Carbon Disulfide ND 2.0 3/31/19 9:10 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/31/19 9:10 BRFV-05 ND 41.30.065 0.41
Chlorobenzene ND 0.20 3/31/19 9:10 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/31/19 9:10 BRFND40.530.12 0.32
Chloroform ND 0.20 3/31/19 9:10 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/31/19 9:10 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/31/19 9:10 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/31/19 9:10 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/31/19 9:10 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/31/19 9:10 BRFND41.20.096 0.58
1,3-Dichlorobenzene 0.56 0.20 3/31/19 9:10 BRF3.4 41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/31/19 9:10 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.33 0.20 3/31/19 9:10 BRF1.6 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/31/19 9:10 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/31/19 9:10 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/31/19 9:10 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/31/19 9:10 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/31/19 9:10 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/31/19 9:10 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/31/19 9:10 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/31/19 9:10 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/31/19 9:10 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 3/31/19 9:10 BRFND47.21.3 4.6
Ethanol ND 8.0 3/31/19 9:10 BRFND4153.6 6.7
Ethyl Acetate ND 0.20 3/31/19 9:10 BRFND40.720.15 0.54
Ethylbenzene 0.32 0.20 3/31/19 9:10 BRF1.4 40.870.12 0.50
4-Ethyltoluene ND 0.20 3/31/19 9:10 BRFND40.980.12 0.60
Heptane 1.2 0.20 3/31/19 9:10 BRF4.8 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/31/19 9:10 BRFND42.10.092 0.98
Hexane 2.8 8.0 3/31/19 9:10 BRFJ10.0 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/31/19 9:10 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/31/19 9:10 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/31/19 9:10 BRFND40.720.10 0.36
Methylene Chloride 0.57 2.0 3/31/19 9:10 BRFJ2.0 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/31/19 9:10 BRFND40.820.096 0.39
Naphthalene ND 0.20 3/31/19 9:10 BRFND41.00.15 0.80
Propene ND 8.0 3/31/19 9:10 BRFND4140.20 0.34
Styrene ND 0.20 3/31/19 9:10 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/31/19 9:10 BRFND41.40.089 0.61
Page 12 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-5
Sample ID: 19C1502-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.5
Sampled: 3/26/2019 13:00
Canister ID: 1075
Flow Controller ID: 4293
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 20 0.20 3/31/19 9:10 BRF130 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/31/19 9:10 BRFL-03 ND 40.590.13 0.39
Toluene 3.3 0.20 3/31/19 9:10 BRF12 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/31/19 9:10 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/31/19 9:10 BRFL-03 ND 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/31/19 9:10 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/31/19 9:10 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.22 0.80 3/31/19 9:10 BRFJ1.2 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/31/19 9:10 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 3/31/19 9:10 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/31/19 9:10 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/31/19 9:10 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/31/19 9:10 BRFND40.510.13 0.32
m&p-Xylene 0.82 0.40 3/31/19 9:10 BRF3.5 41.70.23 1.00
o-Xylene 0.24 0.20 3/31/19 9:10 BRF1.0 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 3/31/19 9:1070-130
Page 13 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-6
Sample ID: 19C1502-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7
Sampled: 3/26/2019 13:51
Canister ID: 1756
Flow Controller ID: 4312
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone ND 8.0 3/31/19 9:51 BRFND4192.8 6.6
Benzene 0.65 0.20 3/31/19 9:51 BRFL-03 2.1 40.640.082 0.26
Benzyl chloride ND 0.20 3/31/19 9:51 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/31/19 9:51 BRFND41.30.074 0.49
Bromoform ND 0.20 3/31/19 9:51 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/31/19 9:51 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 3/31/19 9:51 BRFND40.440.13 0.28
2-Butanone (MEK)0.51 8.0 3/31/19 9:51 BRFJ1.5 4240.31 0.92
Carbon Disulfide ND 2.0 3/31/19 9:51 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/31/19 9:51 BRFV-05 ND 41.30.065 0.41
Chlorobenzene ND 0.20 3/31/19 9:51 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/31/19 9:51 BRFND40.530.12 0.32
Chloroform ND 0.20 3/31/19 9:51 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/31/19 9:51 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/31/19 9:51 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/31/19 9:51 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/31/19 9:51 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/31/19 9:51 BRFND41.20.096 0.58
1,3-Dichlorobenzene 0.30 0.20 3/31/19 9:51 BRF1.8 41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/31/19 9:51 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.33 0.20 3/31/19 9:51 BRF1.6 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/31/19 9:51 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/31/19 9:51 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/31/19 9:51 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/31/19 9:51 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/31/19 9:51 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/31/19 9:51 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/31/19 9:51 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/31/19 9:51 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/31/19 9:51 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 3/31/19 9:51 BRFND47.21.3 4.6
Ethanol ND 8.0 3/31/19 9:51 BRFND4153.6 6.7
Ethyl Acetate ND 0.20 3/31/19 9:51 BRFND40.720.15 0.54
Ethylbenzene 0.26 0.20 3/31/19 9:51 BRF1.1 40.870.12 0.50
4-Ethyltoluene ND 0.20 3/31/19 9:51 BRFND40.980.12 0.60
Heptane 1.2 0.20 3/31/19 9:51 BRF5.1 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/31/19 9:51 BRFND42.10.092 0.98
Hexane 2.0 8.0 3/31/19 9:51 BRFJ7.1 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/31/19 9:51 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/31/19 9:51 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/31/19 9:51 BRFND40.720.10 0.36
Methylene Chloride 0.57 2.0 3/31/19 9:51 BRFJ2.0 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/31/19 9:51 BRFND40.820.096 0.39
Naphthalene ND 0.20 3/31/19 9:51 BRFND41.00.15 0.80
Propene ND 8.0 3/31/19 9:51 BRFND4140.20 0.34
Styrene ND 0.20 3/31/19 9:51 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/31/19 9:51 BRFND41.40.089 0.61
Page 14 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-6
Sample ID: 19C1502-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7
Sampled: 3/26/2019 13:51
Canister ID: 1756
Flow Controller ID: 4312
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 17 0.20 3/31/19 9:51 BRF110 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/31/19 9:51 BRFL-03 ND 40.590.13 0.39
Toluene 2.9 0.20 3/31/19 9:51 BRF11 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/31/19 9:51 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/31/19 9:51 BRFL-03 ND 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/31/19 9:51 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/31/19 9:51 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.20 0.80 3/31/19 9:51 BRFJ1.1 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/31/19 9:51 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 3/31/19 9:51 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/31/19 9:51 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/31/19 9:51 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/31/19 9:51 BRFND40.510.13 0.32
m&p-Xylene 0.64 0.40 3/31/19 9:51 BRF2.8 41.70.23 1.00
o-Xylene 0.26 0.20 3/31/19 9:51 BRF1.1 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 3/31/19 9:5170-130
Page 15 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-7
Sample ID: 19C1502-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6
Sampled: 3/26/2019 14:16
Canister ID: 1909
Flow Controller ID: 4313
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 7.6 8.0 3/31/19 1:42 BRFJ18 4192.8 6.6
Benzene 0.78 0.20 3/31/19 1:42 BRFL-03 2.5 40.640.082 0.26
Benzyl chloride ND 0.20 3/31/19 1:42 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/31/19 1:42 BRFND41.30.074 0.49
Bromoform ND 0.20 3/31/19 1:42 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/31/19 1:42 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 3/31/19 1:42 BRFND40.440.13 0.28
2-Butanone (MEK)1.8 8.0 3/31/19 1:42 BRFJ5.2 4240.31 0.92
Carbon Disulfide ND 2.0 3/31/19 1:42 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/31/19 1:42 BRFV-05 ND 41.30.065 0.41
Chlorobenzene ND 0.20 3/31/19 1:42 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/31/19 1:42 BRFND40.530.12 0.32
Chloroform ND 0.20 3/31/19 1:42 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/31/19 1:42 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/31/19 1:42 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/31/19 1:42 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/31/19 1:42 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/31/19 1:42 BRFND41.20.096 0.58
1,3-Dichlorobenzene 0.42 0.20 3/31/19 1:42 BRF2.5 41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/31/19 1:42 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.44 0.20 3/31/19 1:42 BRF2.2 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/31/19 1:42 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/31/19 1:42 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/31/19 1:42 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/31/19 1:42 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/31/19 1:42 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/31/19 1:42 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/31/19 1:42 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/31/19 1:42 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/31/19 1:42 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 3/31/19 1:42 BRFND47.21.3 4.6
Ethanol ND 8.0 3/31/19 1:42 BRFND4153.6 6.7
Ethyl Acetate ND 0.20 3/31/19 1:42 BRFND40.720.15 0.54
Ethylbenzene 0.50 0.20 3/31/19 1:42 BRF2.2 40.870.12 0.50
4-Ethyltoluene 0.57 0.20 3/31/19 1:42 BRF2.8 40.980.12 0.60
Heptane 1.8 0.20 3/31/19 1:42 BRF7.4 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/31/19 1:42 BRFND42.10.092 0.98
Hexane 2.9 8.0 3/31/19 1:42 BRFJ10 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/31/19 1:42 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/31/19 1:42 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/31/19 1:42 BRFND40.720.10 0.36
Methylene Chloride 0.87 2.0 3/31/19 1:42 BRFJ3.0 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)1.0 0.20 3/31/19 1:42 BRF4.1 40.820.096 0.39
Naphthalene ND 0.20 3/31/19 1:42 BRFND41.00.15 0.80
Propene ND 8.0 3/31/19 1:42 BRFND4140.20 0.34
Styrene ND 0.20 3/31/19 1:42 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/31/19 1:42 BRFND41.40.089 0.61
Page 16 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-7
Sample ID: 19C1502-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6
Sampled: 3/26/2019 14:16
Canister ID: 1909
Flow Controller ID: 4313
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 22 0.20 3/31/19 1:42 BRF150 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/31/19 1:42 BRFL-03 ND 40.590.13 0.39
Toluene 5.3 0.20 3/31/19 1:42 BRF20 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/31/19 1:42 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/31/19 1:42 BRFL-03 ND 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/31/19 1:42 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/31/19 1:42 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.22 0.80 3/31/19 1:42 BRFJ1.2 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/31/19 1:42 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 3/31/19 1:42 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/31/19 1:42 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/31/19 1:42 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/31/19 1:42 BRFND40.510.13 0.32
m&p-Xylene 1.4 0.40 3/31/19 1:42 BRF5.9 41.70.23 1.00
o-Xylene 0.49 0.20 3/31/19 1:42 BRF2.1 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)103 3/31/19 1:4270-130
Page 17 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-DUP
Sample ID: 19C1502-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.1
Sampled: 3/26/2019 14:48
Canister ID: 2176
Flow Controller ID: 4069
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 12 8.0 3/31/19 2:23 BRF29 4192.8 6.6
Benzene 1.1 0.20 3/31/19 2:23 BRFL-03 3.6 40.640.082 0.26
Benzyl chloride ND 0.20 3/31/19 2:23 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/31/19 2:23 BRFND41.30.074 0.49
Bromoform ND 0.20 3/31/19 2:23 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/31/19 2:23 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 3/31/19 2:23 BRFND40.440.13 0.28
2-Butanone (MEK)1.6 8.0 3/31/19 2:23 BRFJ4.7 4240.31 0.92
Carbon Disulfide ND 2.0 3/31/19 2:23 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/31/19 2:23 BRFV-05 ND 41.30.065 0.41
Chlorobenzene ND 0.20 3/31/19 2:23 BRFND40.920.098 0.45
Chloroethane ND 0.20 3/31/19 2:23 BRFND40.530.12 0.32
Chloroform ND 0.20 3/31/19 2:23 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/31/19 2:23 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/31/19 2:23 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/31/19 2:23 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/31/19 2:23 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/31/19 2:23 BRFND41.20.096 0.58
1,3-Dichlorobenzene 0.34 0.20 3/31/19 2:23 BRF2.0 41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/31/19 2:23 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.39 0.20 3/31/19 2:23 BRF1.9 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/31/19 2:23 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/31/19 2:23 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/31/19 2:23 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/31/19 2:23 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/31/19 2:23 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/31/19 2:23 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/31/19 2:23 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/31/19 2:23 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/31/19 2:23 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 3/31/19 2:23 BRFND47.21.3 4.6
Ethanol ND 8.0 3/31/19 2:23 BRFND4153.6 6.7
Ethyl Acetate ND 0.20 3/31/19 2:23 BRFND40.720.15 0.54
Ethylbenzene 0.59 0.20 3/31/19 2:23 BRF2.6 40.870.12 0.50
4-Ethyltoluene 0.38 0.20 3/31/19 2:23 BRF1.9 40.980.12 0.60
Heptane 1.6 0.20 3/31/19 2:23 BRF6.5 40.820.12 0.48
Hexachlorobutadiene ND 0.20 3/31/19 2:23 BRFND42.10.092 0.98
Hexane 2.7 8.0 3/31/19 2:23 BRFJ9.4 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/31/19 2:23 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/31/19 2:23 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/31/19 2:23 BRFND40.720.10 0.36
Methylene Chloride 0.98 2.0 3/31/19 2:23 BRFJ3.4 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)0.78 0.20 3/31/19 2:23 BRF3.2 40.820.096 0.39
Naphthalene ND 0.20 3/31/19 2:23 BRFND41.00.15 0.80
Propene ND 8.0 3/31/19 2:23 BRFND4140.20 0.34
Styrene ND 0.20 3/31/19 2:23 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/31/19 2:23 BRFND41.40.089 0.61
Page 18 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/26/2019
Work Order: 19C1502Sample Description/Location:
Field Sample #: SG-DUP
Sample ID: 19C1502-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.1
Sampled: 3/26/2019 14:48
Canister ID: 2176
Flow Controller ID: 4069
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 25 0.20 3/31/19 2:23 BRF170 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/31/19 2:23 BRFL-03 ND 40.590.13 0.39
Toluene 6.1 0.20 3/31/19 2:23 BRF23 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 3/31/19 2:23 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 3/31/19 2:23 BRFL-03 ND 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/31/19 2:23 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/31/19 2:23 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.22 0.80 3/31/19 2:23 BRFJ1.3 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/31/19 2:23 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 0.32 0.20 3/31/19 2:23 BRF1.6 40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/31/19 2:23 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/31/19 2:23 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/31/19 2:23 BRFND40.510.13 0.32
m&p-Xylene 1.8 0.40 3/31/19 2:23 BRF7.6 41.70.23 1.00
o-Xylene 0.62 0.20 3/31/19 2:23 BRF2.7 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)103 3/31/19 2:2370-130
Page 19 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
19C1502-01 [SG-1]B227059 1.5 1 N/A 1000 400 150 03/30/19
19C1502-02 [SG-2]B227059 1.5 1 N/A 1000 400 150 03/30/19
19C1502-03 [SG-3]B227059 1.5 1 N/A 1000 400 150 03/30/19
19C1502-04 [SG-4]B227059 1.5 1 N/A 1000 400 150 03/30/19
19C1502-05 [SG-5]B227059 1.5 1 N/A 1000 400 150 03/30/19
19C1502-06 [SG-6]B227059 1.5 1 N/A 1000 400 150 03/30/19
19C1502-07 [SG-7]B227059 1.5 1 N/A 1000 400 150 03/30/19
19C1502-08 [SG-DUP]B227059 1.5 1 N/A 1000 400 150 03/30/19
Page 20 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B227059 - TO-15 Prep
Blank (B227059-BLK1)Prepared & Analyzed: 03/30/19
1.4NDAcetone
0.035NDBenzene
0.035NDBenzyl chloride
0.035NDBromodichloromethane
0.035NDBromoform
0.035NDBromomethane
0.035ND1,3-Butadiene
1.4ND2-Butanone (MEK)
0.35NDCarbon Disulfide
0.035NDCarbon Tetrachloride
0.035NDChlorobenzene
0.035NDChloroethane
0.035NDChloroform
0.070NDChloromethane
0.035NDCyclohexane
0.035NDDibromochloromethane
0.035ND1,2-Dibromoethane (EDB)
0.035ND1,2-Dichlorobenzene
0.035ND1,3-Dichlorobenzene
0.035ND1,4-Dichlorobenzene
0.035NDDichlorodifluoromethane (Freon 12)
0.035ND1,1-Dichloroethane
0.035ND1,2-Dichloroethane
0.035ND1,1-Dichloroethylene
0.035NDcis-1,2-Dichloroethylene
0.035NDtrans-1,2-Dichloroethylene
0.035ND1,2-Dichloropropane
0.035NDcis-1,3-Dichloropropene
0.035NDtrans-1,3-Dichloropropene
0.035ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.35ND1,4-Dioxane
1.4NDEthanol
0.035NDEthyl Acetate
0.035NDEthylbenzene
0.035ND4-Ethyltoluene
0.035NDHeptane
0.035NDHexachlorobutadiene
1.4NDHexane
0.035ND2-Hexanone (MBK)
1.4NDIsopropanol
0.035NDMethyl tert-Butyl Ether (MTBE)
0.35NDMethylene Chloride
0.035ND4-Methyl-2-pentanone (MIBK)
0.035NDNaphthalene
1.4NDPropene
0.035NDStyrene
Page 21 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B227059 - TO-15 Prep
Blank (B227059-BLK1)Prepared & Analyzed: 03/30/19
0.035ND1,1,2,2-Tetrachloroethane
0.035NDTetrachloroethylene
0.035NDTetrahydrofuran
0.035NDToluene
0.035ND1,2,4-Trichlorobenzene
0.035ND1,1,1-Trichloroethane
0.035ND1,1,2-Trichloroethane
0.035NDTrichloroethylene
0.14NDTrichlorofluoromethane (Freon 11)
0.14ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.035ND1,2,4-Trimethylbenzene
0.035ND1,3,5-Trimethylbenzene
0.70NDVinyl Acetate
0.035NDVinyl Chloride
0.070NDm&p-Xylene
0.035NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1068.51
LCS (B227059-BS1)Prepared & Analyzed: 03/30/19
5.00 70-13083.84.19Acetone
5.00 L-0370-13053.92.69Benzene *
5.00 70-1301025.09Benzyl chloride
5.00 70-13079.73.98Bromodichloromethane
5.00 70-1301045.21Bromoform
5.00 70-1301055.23Bromomethane
5.00 70-1301015.051,3-Butadiene
5.00 70-13081.34.062-Butanone (MEK)
5.00 70-1301195.96Carbon Disulfide
5.00 70-13087.24.36Carbon Tetrachloride
5.00 70-13089.94.50Chlorobenzene
5.00 70-1301085.40Chloroethane
5.00 70-1301005.00Chloroform
5.00 70-13093.84.69Chloromethane
5.00 70-13078.63.93Cyclohexane
5.00 70-13090.74.54Dibromochloromethane
5.00 70-13088.24.411,2-Dibromoethane (EDB)
5.00 70-13094.24.711,2-Dichlorobenzene
5.00 70-13099.64.981,3-Dichlorobenzene
5.00 70-13098.24.911,4-Dichlorobenzene
5.00 70-13099.14.95Dichlorodifluoromethane (Freon 12)
5.00 70-13097.44.871,1-Dichloroethane
5.00 70-13092.64.631,2-Dichloroethane
5.00 70-13096.04.801,1-Dichloroethylene
5.00 70-13092.14.61cis-1,2-Dichloroethylene
5.00 70-1301045.22trans-1,2-Dichloroethylene
5.00 70-13074.93.751,2-Dichloropropane
Page 22 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B227059 - TO-15 Prep
LCS (B227059-BS1)Prepared & Analyzed: 03/30/19
5.00 70-13076.33.82cis-1,3-Dichloropropene
5.00 70-13080.04.00trans-1,3-Dichloropropene
5.00 70-13098.04.901,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 70-13087.24.361,4-Dioxane
5.00 70-1301085.41Ethanol
5.00 70-13076.03.80Ethyl Acetate
5.00 70-13079.03.95Ethylbenzene
5.00 70-13083.64.184-Ethyltoluene
5.00 70-13071.03.55Heptane
5.00 70-13079.83.99Hexachlorobutadiene
5.00 70-13078.63.93Hexane
5.00 70-13076.63.832-Hexanone (MBK)
5.00 70-13077.93.89Isopropanol
5.00 70-13093.14.66Methyl tert-Butyl Ether (MTBE)
5.00 70-13087.44.37Methylene Chloride
5.00 70-13076.13.804-Methyl-2-pentanone (MIBK)
5.00 70-13092.24.61Naphthalene
5.00 70-13075.93.80Propene
5.00 70-13084.34.21Styrene
5.00 70-13090.54.521,1,2,2-Tetrachloroethane
5.00 70-13089.24.46Tetrachloroethylene
5.00 L-0370-13069.63.48Tetrahydrofuran *
5.00 70-13082.54.12Toluene
5.00 70-13088.94.441,2,4-Trichlorobenzene
5.00 L-0370-13068.23.411,1,1-Trichloroethane *
5.00 70-13086.94.341,1,2-Trichloroethane
5.00 70-13079.03.95Trichloroethylene
5.00 70-13095.54.77Trichlorofluoromethane (Freon 11)
5.00 70-1301035.141,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-13084.44.221,2,4-Trimethylbenzene
5.00 70-13084.94.241,3,5-Trimethylbenzene
5.00 70-1301226.11Vinyl Acetate
5.00 70-13098.74.93Vinyl Chloride
10.0 70-13082.68.26m&p-Xylene
5.00 70-13084.34.21o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1068.45
Page 23 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B227059 - TO-15 Prep
Duplicate (B227059-DUP1)Prepared: 03/30/19 Analyzed: 03/31/19 Source: 19C1502-03
8.0 ND 25NDAcetone19ND
0.20 0.72 25 R-0134.61.0Benzene 0.643.2
0.20 ND 25NDBenzyl chloride 1.0ND
0.20 ND 25NDBromodichloromethane1.3ND
0.20 ND 25NDBromoform2.1ND
0.20 ND 25NDBromomethane0.78ND
0.20 ND 25ND1,3-Butadiene 0.44ND
8.0 ND 25ND2-Butanone (MEK)24ND
2.0 ND 25NDCarbon Disulfide 6.2ND
0.20 ND 25NDCarbon Tetrachloride 1.3ND
0.20 ND 25NDChlorobenzene0.92ND
0.20 ND 25NDChloroethane0.53ND
0.20 ND 25NDChloroform0.98ND
0.40 ND 25NDChloromethane0.83ND
0.20 ND 25NDCyclohexane0.69ND
0.20 ND 25NDDibromochloromethane1.7ND
0.20 ND 25ND1,2-Dibromoethane (EDB)1.5ND
0.20 ND 25ND1,2-Dichlorobenzene 1.2ND
0.20 0.44 253.540.461,3-Dichlorobenzene 1.22.8
0.20 ND 25ND1,4-Dichlorobenzene 1.2ND
0.20 0.28 2516.00.32Dichlorodifluoromethane (Freon 12)0.991.6
0.20 ND 25ND1,1-Dichloroethane 0.81ND
0.20 ND 25ND1,2-Dichloroethane 0.81ND
0.20 ND 25ND1,1-Dichloroethylene 0.79ND
0.20 ND 25NDcis-1,2-Dichloroethylene 0.79ND
0.20 ND 25NDtrans-1,2-Dichloroethylene 0.79ND
0.20 ND 25ND1,2-Dichloropropane 0.92ND
0.20 ND 25NDcis-1,3-Dichloropropene 0.91ND
0.20 ND 25NDtrans-1,3-Dichloropropene 0.91ND
0.20 ND 25ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
1.4ND
2.0 ND 25ND1,4-Dioxane 7.2ND
8.0 ND 25NDEthanol15ND
0.20 ND 25NDEthyl Acetate 0.72ND
0.20 0.52 256.640.56Ethylbenzene 0.872.4
0.20 ND 25ND4-Ethyltoluene 0.98ND
0.20 1.5 251.871.5Heptane 0.826.1
0.20 ND 25NDHexachlorobutadiene2.1ND
8.0 3.2 25 J8.383.0Hexane 2810
0.20 ND 25ND2-Hexanone (MBK)0.82ND
8.0 ND 25NDIsopropanol20ND
0.20 ND 25NDMethyl tert-Butyl Ether (MTBE)0.72ND
2.0 1.2 25 J13.71.0Methylene Chloride 6.93.5
0.20 ND 25ND4-Methyl-2-pentanone (MIBK)0.82ND
0.20 ND 25NDNaphthalene1.0ND
8.0 ND 25NDPropene14ND
0.20 ND 25NDStyrene0.85ND
Page 24 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B227059 - TO-15 Prep
Duplicate (B227059-DUP1)Prepared: 03/30/19 Analyzed: 03/31/19 Source: 19C1502-03
0.20 ND 25ND1,1,2,2-Tetrachloroethane 1.4ND
0.20 28 254.2829Tetrachloroethylene1.4200
0.20 ND 25NDTetrahydrofuran0.59ND
0.20 5.5 252.645.7Toluene 0.7521
0.20 ND 25ND1,2,4-Trichlorobenzene 1.5ND
0.20 ND 25ND1,1,1-Trichloroethane 1.1ND
0.20 ND 25ND1,1,2-Trichloroethane 1.1ND
0.20 ND 25NDTrichloroethylene1.1ND
0.80 ND 25NDTrichlorofluoromethane (Freon 11)4.5ND
0.80 ND 25ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
6.1ND
0.20 0.32 257.320.341,2,4-Trimethylbenzene 0.981.7
0.20 ND 25ND1,3,5-Trimethylbenzene 0.98ND
4.0 ND 25NDVinyl Acetate 14ND
0.20 ND 25NDVinyl Chloride 0.51ND
0.40 1.7 256.881.8m&p-Xylene 1.77.8
0.20 0.55 257.670.60o-Xylene 0.872.6
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1028.15
Page 25 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this
compound is likely to be biased on the low side.
L-03
Duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result.R-01
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Page 26 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYST
Rebecca FaustRLF
PDF Management StationSTATION
Paula E. BlakeboroughPEB
Kerry K. McGeeKKM
Brittany R. FiskBRF
Page 27 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S033211-ICV1 )Lab File ID: F030617.D Analyzed: 03/06/19 20:40
Bromochloromethane (1)200323 8.624 194605 8.624 60 - 140103 0.0000 +/-0.50
1,4-Difluorobenzene (1)600461 10.389 580681 10.389 60 - 140103 0.0000 +/-0.50
Chlorobenzene-d5 (1)566414 14.756 545525 14.756 60 - 140104 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S034124-CCV1 )Lab File ID: F033005.D Analyzed: 03/30/19 15:57
Bromochloromethane (1)141678 8.624 194605 8.624 60 - 14073 0.0000 +/-0.50
1,4-Difluorobenzene (1)500821 10.382 580681 10.389 60 - 14086 -0.0070 +/-0.50
Chlorobenzene-d5 (1)429910 14.752 545525 14.756 60 - 14079 -0.0040 +/-0.50
LCS (B227059-BS1 )Lab File ID: F033007.D Analyzed: 03/30/19 17:17
Bromochloromethane (1)139957 8.627 141678 8.624 60 - 14099 0.0030 +/-0.50
1,4-Difluorobenzene (1)493584 10.383 500821 10.382 60 - 14099 0.0010 +/-0.50
Chlorobenzene-d5 (1)429265 14.752 429910 14.752 60 - 140100 0.0000 +/-0.50
Blank (B227059-BLK1 )Lab File ID: F033009.D Analyzed: 03/30/19 18:41
Bromochloromethane (1)126514 8.624 141678 8.624 60 - 14089 0.0000 +/-0.50
1,4-Difluorobenzene (1)431327 10.389 500821 10.382 60 - 14086 0.0070 +/-0.50
Chlorobenzene-d5 (1)397058 14.752 429910 14.752 60 - 14092 0.0000 +/-0.50
SG-1 (19C1502-01 )Lab File ID: F033013.D Analyzed: 03/30/19 21:30
Bromochloromethane (1)136312 8.63 141678 8.624 60 - 14096 0.0060 +/-0.50
1,4-Difluorobenzene (1)404510 10.379 500821 10.382 60 - 14081 -0.0030 +/-0.50
Chlorobenzene-d5 (1)418023 14.749 429910 14.752 60 - 14097 -0.0030 +/-0.50
SG-2 (19C1502-02 )Lab File ID: F033014.D Analyzed: 03/30/19 22:12
Bromochloromethane (1)136490 8.63 141678 8.624 60 - 14096 0.0060 +/-0.50
1,4-Difluorobenzene (1)500648 10.383 500821 10.382 60 - 140100 0.0010 +/-0.50
Chlorobenzene-d5 (1)431515 14.749 429910 14.752 60 - 140100 -0.0030 +/-0.50
SG-4 (19C1502-04 )Lab File ID: F033016.D Analyzed: 03/30/19 23:34
Bromochloromethane (1)134664 8.627 141678 8.624 60 - 14095 0.0030 +/-0.50
1,4-Difluorobenzene (1)461769 10.389 500821 10.382 60 - 14092 0.0070 +/-0.50
Chlorobenzene-d5 (1)424628 14.752 429910 14.752 60 - 14099 0.0000 +/-0.50
SG-7 (19C1502-07 )Lab File ID: F033019.D Analyzed: 03/31/19 01:42
Bromochloromethane (1)134239 8.63 141678 8.624 60 - 14095 0.0060 +/-0.50
1,4-Difluorobenzene (1)410896 10.38 500821 10.382 60 - 14082 -0.0020 +/-0.50
Chlorobenzene-d5 (1)421565 14.752 429910 14.752 60 - 14098 0.0000 +/-0.50
Page 28 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SG-DUP (19C1502-08 )Lab File ID: F033020.D Analyzed: 03/31/19 02:23
Bromochloromethane (1)129790 8.624 141678 8.624 60 - 14092 0.0000 +/-0.50
1,4-Difluorobenzene (1)455197 10.389 500821 10.382 60 - 14091 0.0070 +/-0.50
Chlorobenzene-d5 (1)427368 14.752 429910 14.752 60 - 14099 0.0000 +/-0.50
SG-3 (19C1502-03 )Lab File ID: F033021.D Analyzed: 03/31/19 07:44
Bromochloromethane (1)163313 8.627 141678 8.624 60 - 140115 0.0030 +/-0.50
1,4-Difluorobenzene (1)547808 10.38 500821 10.382 60 - 140109 -0.0020 +/-0.50
Chlorobenzene-d5 (1)457141 14.752 429910 14.752 60 - 140106 0.0000 +/-0.50
Duplicate (B227059-DUP1 )Lab File ID: F033022.D Analyzed: 03/31/19 08:26
Bromochloromethane (1)136155 8.624 141678 8.624 60 - 14096 0.0000 +/-0.50
1,4-Difluorobenzene (1)470224 10.389 500821 10.382 60 - 14094 0.0070 +/-0.50
Chlorobenzene-d5 (1)431254 14.752 429910 14.752 60 - 140100 0.0000 +/-0.50
SG-5 (19C1502-05 )Lab File ID: F033023.D Analyzed: 03/31/19 09:10
Bromochloromethane (1)134359 8.627 141678 8.624 60 - 14095 0.0030 +/-0.50
1,4-Difluorobenzene (1)466155 10.389 500821 10.382 60 - 14093 0.0070 +/-0.50
Chlorobenzene-d5 (1)426964 14.755 429910 14.752 60 - 14099 0.0030 +/-0.50
SG-6 (19C1502-06 )Lab File ID: F033024.D Analyzed: 03/31/19 09:51
Bromochloromethane (1)131865 8.627 141678 8.624 60 - 14093 0.0030 +/-0.50
1,4-Difluorobenzene (1)458653 10.389 500821 10.382 60 - 14092 0.0070 +/-0.50
Chlorobenzene-d5 (1)424253 14.752 429910 14.752 60 - 14099 0.0000 +/-0.50
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S034124-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.9079405A -18.5 304.08 1.1140045.00Acetone
0.3908686A -49.6 *302.52 0.77603365.00Benzene
0.9701305A 7.8 305.39 0.90016475.00Benzyl chloride
0.4757245A -15.3 304.24 0.56171285.00Bromodichloromethane
0.6832165A 11.7 305.58 0.61183795.00Bromoform
0.7356061A 0.6 305.03 0.73111045.00Bromomethane
0.537094A -5.5 304.73 0.56805775.001,3-Butadiene
1.247053A -20.0 304.00 1.5583765.002-Butanone (MEK)
1.900625A 5.6 305.28 1.7996495.00Carbon Disulfide
0.3705851A -31.0 *303.45 0.53701265.00Carbon Tetrachloride
0.7769812A -5.2 304.74 0.81983995.00Chlorobenzene
0.3575545A 5.6 305.28 0.33854255.00Chloroethane
1.558938A 2.0 305.10 1.5285835.00Chloroform
0.7457474A -6.7 304.66 0.79963215.00Chloromethane
0.267746A -21.5 303.93 0.34086745.00Cyclohexane
0.627242A -3.1 304.84 0.64737415.00Dibromochloromethane
0.4995092A -6.9 304.65 0.53676025.001,2-Dibromoethane (EDB)
0.7777888A -1.7 304.92 0.79128165.001,2-Dichlorobenzene
0.8626959A 4.0 305.20 0.82955115.001,3-Dichlorobenzene
0.8662985A 3.7 305.19 0.83530475.001,4-Dichlorobenzene
1.942557A -3.6 304.82 2.0157985.00Dichlorodifluoromethane (Freon 12)
1.322955A -1.0 304.95 1.3358985.001,1-Dichloroethane
0.8885275A -4.9 304.75 0.9344785.001,2-Dichloroethane
1.124273A -3.0 304.85 1.1595975.001,1-Dichloroethylene
0.9564336A -2.3 304.89 0.97883875.00cis-1,2-Dichloroethylene
0.9442369A -0.6 304.97 0.95005685.00trans-1,2-Dichloroethylene
0.2461814A -20.1 304.00 0.30800595.001,2-Dichloropropane
0.3574451A -19.1 304.04 0.44196765.00cis-1,3-Dichloropropene
0.3016998A -19.0 304.05 0.37253715.00trans-1,3-Dichloropropene
2.09881A 0.6 305.03 2.0865145.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.13932A -7.2 304.64 0.15016425.001,4-Dioxane
0.1338133A -21.6 303.92 0.17068915.00Ethanol
0.2622171A -0.4 304.98 0.26317965.00Ethyl Acetate
1.083799A -16.5 304.18 1.2978195.00Ethylbenzene
1.272743A -10.0 304.50 1.4140815.004-Ethyltoluene
0.1836281A -25.1 303.74 0.24513185.00Heptane
0.4791998A -9.8 304.51 0.53099725.00Hexachlorobutadiene
0.7260182A -20.6 303.97 0.91416555.00Hexane
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S034124-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.4850243A -17.5 304.12 0.58807285.002-Hexanone (MBK)
1.036062A -18.8 304.06 1.2752015.00Isopropanol
1.861641A -6.5 304.67 1.9918665.00Methyl tert-Butyl Ether (MTBE)
0.7901975A -11.7 304.41 0.89502675.00Methylene Chloride
0.178705A -19.6 304.02 0.22228915.004-Methyl-2-pentanone (MIBK)
1.343917A 2.5 305.12 1.3116095.00Naphthalene
0.709722A -24.8 303.76 0.94411315.00Propene
0.6928594A -10.2 304.49 0.77164665.00Styrene
0.7165407A -2.8 304.86 0.73744245.001,1,2,2-Tetrachloroethane
0.4744435A -5.8 304.71 0.50370195.00Tetrachloroethylene
0.5785175A -29.3 303.54 0.81789995.00Tetrahydrofuran
0.8648136A -14.5 304.27 1.0119085.00Toluene
0.6392817A 5.7 305.28 0.60507745.001,2,4-Trichlorobenzene
0.3906354A -23.4 303.83 0.51004875.001,1,1-Trichloroethane
0.3148975A -9.3 304.53 0.34736195.001,1,2-Trichloroethane
0.3010225A -15.7 304.22 0.35704165.00Trichloroethylene
1.628798A -5.9 304.71 1.7304695.00Trichlorofluoromethane (Freon 11)
1.640588A 5.6 305.28 1.5530595.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
1.047937A -10.8 304.46 1.1744775.001,2,4-Trimethylbenzene
1.084257A -9.8 304.51 1.2027255.001,3,5-Trimethylbenzene
0.8889115A -28.6 303.57 1.2452215.00Vinyl Acetate
0.7955166A -2.6 304.87 0.81657065.00Vinyl Chloride
0.8823782A -12.3 308.77 1.00586710.0m&p-Xylene
0.9056184A -11.5 304.42 1.0233645.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 32 of 36
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2019
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2019
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2019
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2019
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