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HomeMy WebLinkAbout21019_Homewood Banks Apartments_BAR_20180313= EN March 13, 2018 North Carolina Department of Environmental Quality Division of Waste Management, Brownfields Program 217 West Jones Street Raleigh, North Carolina 27605 Attention: Ms. Sarah Hardison Young Reference: Report of Additional Site Assessment Activities Homewood Banks Apartments Site 5510 Homewood Banks Drive Raleigh, Wake County, North Carolina NCDEQ, Brownfields Project No.: 2109-17-0092 S&ME Project No. 4335-16-102, Ph 03 Dear Ms. Hardison Young: S&ME, Inc. (S&ME), on behalf of our client, Dominion Realty Partners, LLC/Homewood DRP, LLC (DRP), submits this Report of Additional Site Assessment Activities that were recently conducted at the above referenced site. The assessment activities were conducted in accordance with the approved Work Plan for Additional Environmental Assessment (S&ME Project No. 4335-16-102, Ph 03) dated February 5, 2018 and approved in a February 8, 2018 email from Ms. Hardison Young of the North Carolina Department of Environmental Quality, Brownfields Program (NCDEQ, BF) to Mr. Smith of S&ME. This report presents the purpose for the sampling event, the methods used to collect soil and groundwater samples, the results of the laboratory analyses, and the conclusions based on the results of the analyses. Site Description The subject site property consists of two parcels which includes parcel number 0795491345 (2.77 acres) and parcel number 0795484971 (13.25 acres), totaling approximately 16 acres. According to the Wake County GIS Department's website, the parcels are owned by Dorothy R. Kerr RVCBLE Trust Wells Fargo Bank Trustee. The subject property contained a residence, a pond, wooded and open land but DRP is proposing to redevelop the site as a multi -family residential development. Appendix I contains a USGS Topographic Map indicating the site location (Figure 1) and a Site Aerial indicating the site parcels and approximate former UST and AST areas is provided as Figure 2. Project Background and Purpose On May 18, 2016, DRP provided S&ME with a Phase I Environmental Site Assessment (Phase I ESA) that was conducted by Soil & Environmental Consultants, PA (S&EC) for an approximate 16-acre tract, referenced as the Kerr Properties located at the intersection of Homewood Banks Drive and Blue Ridge Road in Raleigh, Wake County, North Carolina. Mr. Campbell requested that S&ME review the report and provide an opinion as to the potential for the site to be eligible to enter the NCDEQ, BF. According to the report, S&EC identified one S&ME, Inc. 19751 Southern Pine Boulevard I Charlotte, NC 28273 1 p 704.523.4726 1 www.smeinc.com =0 Report of Additional Site Assessment Activities Homewood Banks Apartments Site 5510 Homewood Banks Drive Raleigh, Wake County, North Carolina NCDEQ, Brownfields Project No.: 2109-17-092 S&ME Project No. 4335-16-102, Ph 03 Historical Recognized Environmental Condition (HREC) and a Recognized Environmental Condition (REC) on the subject property. Below is a summary of each: The HREC identified was a leaking underground storage tank (UST) previously existing at the site, which was reportedly removed and the impacted soils removed, and the NCDEQ (formerly North Carolina Department of Environment and Natural Resources) issued a letter of No Further Action (NFA) for the incident on October 3, 2014. The REC consisted of an existing aboveground petroleum storage tank (AST) that remained at the site. Although the AST did not appear to be in use, no information was available pertaining to potential environmental impacts (release) from former use. Former UST Area In order to further evaluate the former UST incident for potential remaining impacts that would appear to qualify the site as a potential Brownfields, S&ME reviewed historical files located at the NCDEQ office in Raleigh, North Carolina. The files included a 20-Day Report dated August, 2014, and an Initial Abatement Report (IAR) dated September, 2014 by Cohesion, Inc. (Cohesion). The 20-Day Report indicated that Cohesion removed an approximate 1,000-gallon heating oil UST (later determined to be a gasoline UST) and associated product piping and dispenser from the site. Following the removal, Cohesion collected one soil sample below the UST, three soil samples below the product piping and one sample below the dispenser. Based on the IAR, the analytical results detected total petroleum hydrocarbons (TPH) — diesel range organics (DRO) in product line sample B-3 (11 milligrams per kilogram or mg/kg) and in the dispenser sample B-5 (18.0 mg/kg) at concentrations greater than the NCDEQ action level of 10 mg/kg. TPH-DRO was also detected in sample B-4 (also collected below the former product line) at 6.6 mg/kg, which is less than the NCDEQ Action Level. Furthermore, TPH — gasoline range organics (GRO) was detected in soil sample B-5 (2.2 mg/kg) at a concentration less than the NCDEQ Action Level of 10 mg/kg. Based on the analytical results, Cohesion conducted initial abatement at the site, which included excavating 8.02 tons of impacted soils in the vicinity of soil samples B-3 and B-5. Following the excavation activities, Cohesion collected soil samples at the bottom of each excavation. The samples were analyzed for volatile organic compounds (VOCs), semi -volatile organic compounds (SVOCs), extractable petroleum hydrocarbons (EPH), and volatile petroleum hydrocarbons (VPH). The analytical results were less than the Soil -to -Groundwater and the Residential Maximum Soil Contamination Concentrations (MSCCs). However, C9-C12 Aliphatics, Chlorobenzene, and Naphthalene were detected. Based on the results of the IAR, NCDEQ issued a letter of No Further Action (NFA) for the incident on October 3, 2014. Although the NFA was granted for the UST incident, samples of remaining soils contained detectable concentrations of petroleum constituents: 6.6 mg/kg TPH-DRO at former sample location B-4 and C9-C12 Aliphatics, Chlorobenzene and Naphthalene at former sample location B-3. =0 Report of Additional Site Assessment Activities Homewood Banks Apartments Site 5510 Homewood Banks Drive Raleigh, Wake County, North Carolina NCDEQ, Brownfields Project No.: 2109-17-092 S&ME Project No. 4335-16-102, Ph 03 As indicated by a Cut/Fill site map provided by DRP on January 25, 2018, when the former sample locations were superimposed on the figure, the area of the soil samples collected by Cohesion appear to be located in an area that is projected to be cut (i.e., undercut) ranging from approximately 11 to 16 feet. Additionally, the former sample locations appear to be located within, or very near to the proposed footprint of one of the residential buildings. AST Area In order to assess the soils in the area of the AST, on June 19, 2016, S&ME collected one shallow soil sample from each end of the AST. The details regarding the collection of soil samples HA-1 and HA-2 were provided to DRP in S&ME's Limited Phase 11 Environmental Assessment of AST, dated July 7, 2016. Results of the analysis of sample HA-1 contained detectable concentrations of petroleum (TPH-GRO at 7.88 mg/kg and TPH-DRO at 7.97 mg/kg) less than the NCDEQ Action level of 10 mg/kg. Laboratory analysis of sample HA-2 contained TPH-DRO at 60.9 mg/kg, greater than the Action level, but TPH-GRO was not detected above the laboratory reporting limit. Risk - based analysis of sample HA-2 identified several SVOCs at concentration greater than their respective Residential MSCCs, with four additional compounds greater than their respective Soil -to -Groundwater MSCCs. Status of Soils at Former UST and AST Areas Since soils containing petroleum constituents from the former UST remained at former sample locations B-3 and B-4; soils at the AST area remain with detectable petroleum concentrations at former sample location HA-1; and petroleum soils greater than the MSCCs remain at former sample location HA-2, DRP elected to pursue a BFA from the NCDEQ, prior to site redevelopment. Therefore, on April 6, 2017, DRP submitted a Brownfields Property Application (BPA) to the NCDEQ, Brownfields for the site. After submittal of additionally requested information and conversations with NCDEQ, DRP received a Letter of Eligibility (LOE) from the NCDEQ, Brownfields for the site, dated December 1, 2017. Based on conversations with Ms. Hardison Young of the NCDEQ, Brownfields as referenced above, additional assessment and other environmental consulting activities associated with the Homewood Banks Brownfields site is required. Prior to the NCDEQ required Environmental Management Plan (EMP) and Brownfields Agreement for the site, as stated above, NCDEQ requested that additional assessment of the soils and groundwater at the former UST area and at the AST areas be conducted. Therefore, on February 5, 2018, S&ME on behalf of DRP submitted a Work Plan for Additional Assessment Activities (Work Plan) to further address the former UST and AST areas, as requested by the NCDEQ, BF. The Work Plan was approved by NCDEQ, BF in a February 6, 2018 email from Ms. Hardison Young to Mr. Smith of S&ME. The following sections presents the field methods of the assessment, the laboratory analytical results of collected samples, comparison of the analytical results to applicable standards and screening levels, and conclusions. After approval of the Work Plan, S&ME mobilized to the site on February 8 to conduct the approved additional assessment. The following sections presents the field methods of the assessment, the laboratory analytical results =0 Report of Additional Site Assessment Activities Homewood Banks Apartments Site 5510 Homewood Banks Drive Raleigh, Wake County, North Carolina NCDEQ, Brownfields Project No.: 2109-17-092 S&ME Project No. 4335-16-102, Ph 03 of collected samples, comparison of the analytical results to applicable standards and screening levels, and conclusions. A photographic log is included as Appendix III. In accordance with the NCDEQ, Brownfields request and the approved revised proposal, the scope of services conducted by S&ME generally included the following: ♦ Preparation of a Health and Safety Plan (HASP). ♦ Contacting NC One Call, the public utility locating service. ♦ Collection of a soil sample from the AST area if evidence of a release is noted. ♦ Collection of up to nine soil samples collected from six soil borings advanced at the former UST area. ♦ Installation of and sampling of groundwater from two (one at the former UST area and one at the AST area) temporary monitoring wells. The only deviation to the proposed Work Plan during sampling activities consisted of no groundwater sample was collected from a temporary monitoring well in the former UST area due to encountering refusal prior to reaching groundwater and, therefore no temporary monitoring well was installed. Methods Health and Safety Plan and Utility Clearance S&ME prepared a site -specific HASP in general accordance with 29 CFR 1910.120, which addressed the contaminants known or suspected to be present on -site, personal protective equipment, monitoring performed during the field activities, and response actions to be taken in the event monitoring thresholds are exceeded. Prior to beginning sampling activities, S&ME contacted NC One Call to mark the location of underground utilities at the site in order to mitigate the potential for damage to underground utilities. Additionally, S&ME contracted with Quantex, Inc. (Quantex) to use a North Carolina licensed driller to conduct the soil borings, as well as the installation and abandonment of temporary monitor wells. S&ME also contracted with Prism Laboratories, Inc. (Prism), a North Carolina certified laboratory, to conduct the analysis of the soil and groundwater samples collected from the site. Former UST Area Assessment On February 8 and 9, 2018, six soil borings were advanced at the former UST area at the locations shown on Figures 3 and 4 in Appendix I. A track mounted Geoprobe° unit was utilized to advance the soil borings, with the exception of soil boring UST-5. Due to the topographic slope of the soil boring area and the proximity of the site structure, soil boring UST-5 was advanced using a hand -auger. The soil borings conducted using the Geoprobe® ranged in depths from 12 feet below ground surface or ft-bgs (UST-6) to 30 ft-bgs (UST-1). During advancement, the following field activities conducted to evaluate the soils and sample collection, generally consisted of the following: =0 Report of Additional Site Assessment Activities Homewood Banks Apartments Site 5510 Homewood Banks Drive Raleigh, Wake County, North Carolina NCDEQ, Brownfields Project No.: 2109-17-092 S&ME Project No. 4335-16-102, Ph 03 Soil borings were conducted using a direct push (Geoprobe(g) type drilling rig by advancing a macro -core sampler equipped with a new/clean inner clear acetate liner for every 4 to 5 foot depth intervals. Soils were collected continuously from the ground surface to refusal. Upon retrieval of the macro -core sampler, the acetate liner will be removed and opened, and the depths and description of soils will be noted on a bore log. The soils were removed and field screened for evidence of apparent impacts such as indications of staining, odors, etc. and also be screened for organic vapors using a flame ionization detector (FID). Soils were screened for organic vapors in approximate 2.5-foot intervals with a FID during the advancement of the soil borings, with the exception of soil boring UST-5. The soil samples in soil boring UST-5 were screened in 1-foot intervals The macro -core sampling drill rods were then decontaminated between sampling by removing solids/soils from rods, rinsing with water, scrub the rods using a nylon brush and a mixture of alconox or liquinox and water, rinse with deionized water. The soil sample intervals selected for laboratory analysis from each boring was based on either: field screening findings, depth of potential source of concern (i.e., predetermined by NCDEQ, BF), refusal, or the depth just above the estimated seasonal high groundwater elevation. Generally the soil sample from each soil boring exhibiting the highest FID reading was selected for laboratory analysis. An additional soil sample was selected for laboratory analysis from soil borings UST-3 at 2.5-3 ft-bgs as that was the depth of the former excavations at those areas, and a sample from the 12 to 14 foot interval was also selected for laboratory analysis from soil boring UST-3 as that sample represents the approximate depth of the cut that will be done as part of the development of the site. As no FID readings were noted in the soil samples collected from soil boring UST-5, the soil sample collected from approximately three ft-bgs was selected for laboratory analysis. The boring logs for the six soil borings are included in Appendix IV. The soil samples were placed directly into the laboratory supplied containers, placed on ice in a cooler, and shipped under standard chain -of -custody procedure to Prism for analysis. The samples were analyzed for VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and RCRA Metals by EPA Methods 6010/7471. AST Area Assessment On February 8, 2018, S&ME observed and documented the advancement of one soil boring for the installation of one temporary monitoring well (AST-1/TW-1) in the vicinity of former sample location HA-2 at the AST area. The location of the boring/temporary monitoring well is shown on Figure 3in Appendix I. A track mounted Geoprobe° unit was utilized to conduct the boring with soils evaluated as stated above. The temporary monitoring well was installed to a depth of approximately eight feet deeper than the point where moist/wet soil was encountered. Once the total depth of the temporary monitoring well was identified, a two-inch diameter 10-foot long PVC 0.010" well screen was installed with PVC well casing from the top of the well screen up to approximately one foot above ground surface (stick-up). A sand pack was installed around the well screen up to approximately two feet above the well screen. A two foot bentonite seal was installed directly above the =0 Report of Additional Site Assessment Activities Homewood Banks Apartments Site 5510 Homewood Banks Drive Raleigh, Wake County, North Carolina NCDEQ, Brownfields Project No.: 2109-17-092 S&ME Project No. 4335-16-102, Ph 03 sand pack. As described above, soil samples were screened for apparent impacts in five-foot intervals with a flame -ionization device (FID) during the advancement of the soil boring for the temporary monitoring well installation. No measurable organic vapors were encountered during the installation of AST-1/TW-1. In addition, no evidence of a release was noted during the installation of the temporary monitoring well. As in accordance with the Work Plan, no soil samples were submitted for laboratory analysis from soil boring AST-1/TW-1 as no apparent impacts were noted. The boring log and well construction record for the temporary monitoring well are included in Appendix IV. S&ME personnel collected a groundwater sample from temporary monitoring well AST-1/TW-1 on February 9, 2018. Prior to sampling the well, the depth to groundwater was measured using a water level indicator. Due to the depth to water (approximately 30 ft-bgs) a disposal bailer was used to develop and purge the temporary monitoring well rather than using a peristaltic pump, by evacuating groundwater until approximately five well volumes were removed. During purging, field parameter readings were collected at approximate 0.5 gallon increments between 1 to 4 gallons of removed groundwater. The field readings collected consisted of pH, temperature, and Specific Conductivity. The temporary monitoring well was allowed to recharge and suspended sediments allowed to settle, prior to sampling. A copy of the completed field sampling form, including the field parameter readings is included in Appendix V. Following well purging, a groundwater sample was collected using the bailer by pouring directly into laboratory supplied containers. The collected sample was placed on ice in a cooler and shipped under standard chain -of - custody procedure to Prism. The samples were analyzed for VOCs and SVOCs by the previously stated methods. Upon completion of the sampling, S&ME utilized a GPS unit capable of sub -meter accuracy to record the horizontal location of the temporary monitoring well. Once completed, the temporary well was abandoned by a NC licensed driller with Quantex by removing the PVC screen and casing, and backfilling the boring with bentonite clay and hydrating. A copy of the well abandonment record for the temporary monitoring well is included in Appendix IV. Quality Assurance/Quality Control During the groundwater sampling, a duplicate groundwater sample was also collected and a trip blank sample were submitted for quality assurance/quality control (QA/QC) purposes. In addition, a duplicate soil sample was also collected from the UST-4 soil boring at the 7.5-10 ft-bgs interval. The duplicate samples were submitted for the same analyses as the record samples. The trip blank sample was submitted for analysis for VOCs by EPA Method 8260. Background Soil Samples In order to assess for natural metal concentrations in site soils, on February 9, 2018, S&ME also advanced a soil boring (Background) in a location outside of the areas of potential contamination as shown on Figure 3 in Appendix I. Two soil samples were collected from the 2.5-3 ft-bgs and 7.5-10 ft-bgs intervals and submitted for =0 Report of Additional Site Assessment Activities Homewood Banks Apartments Site 5510 Homewood Banks Drive Raleigh, Wake County, North Carolina NCDEQ, Brownfields Project No.: 2109-17-092 S&ME Project No. 4335-16-102, Ph 03 analysis for RCRA Metals by EPA Methods 6010/7471 as background samples for comparison with the record soil samples. The soils and sample intervals selected for the laboratory analysis were selected in order to be as consistent as possible with those soils submitted from the record samples, based on field observations (e.g., color, grain size, depths, etc.). Results AST Area Sampling Results Review of the laboratory analytical results for the groundwater sample collected from temporary monitoring well AST-1/TW-1 did not indicate any compounds present at concentrations greater than the laboratory method reporting limits. A copy of the laboratory analytical report and chain -of -custody form is in Appendix VI. Former UST Area Sampling Results The soil sampling results are summarized in Table 1, Appendix II. Review of the laboratory analytical results indicated concentrations of acetone in soil sample UST-4 (2.5-3), UST-6 (2.5-3), and UST-6 (7.5-10) greater than the laboratory method reporting limit, but less than the Protection of Groundwater and Residential Preliminary Site Remediation Goals (PSRG). 4-isopropyltoluene was also detected in soil sample UST-6 (7.5-10) greater than the laboratory method reporting limit; however, there are no established PSRGs for 4-isopropyltoluene. No SVOCs were detected at concentrations greater than the laboratory method reporting limits in any of the soil samples collected. Various metals were detected in each of the soil samples collected at concentrations greater than the laboratory method reporting limit; however, only the concentration of arsenic in UST-6 (2.5-3) at 4.3 milligrams per kilogram (mg/kg) was greater than its Residential PSRG and background concentrations, but the concentration was less than its Protection to Groundwater PSRG. A copy of the laboratory analytical results is included in Appendix VI. Quality Assurance/Quality Control Results The duplicate groundwater and soil samples collected were consistent with the associated record samples. No compounds were detected at concentration greater than the laboratory method reporting limit in the trip blank sample submitted. The analytical results of the duplicate soil sample are summarized on Table 1 in Appendix II. All metals detected in the record soil samples were consistent with naturally occurring metals levels, including the concentration of arsenic in soil sample UST-6 (2.5-3) even though it was greater than its Residential PSRG. The analytical results of the background soil samples are summarized on Table 1 in Appendix I. Report of Additional Site Assessment Activities Homewood Banks Apartments Site 5510 Homewood Banks Drive Raleigh, Wake County, North Carolina NCDEQ, Brownfields Project No.: 2109-17-092 S&ME Project No. 4335-16-102, Ph 03 Conclusions Based on the soil and groundwater sampling results, the following conclusions are presented: No compounds were detected at concentrations greater than the laboratory method reporting limits in the groundwater sample collected from temporary monitoring well AST-1/TW-1. In addition, no evidence of a release was noted during the soil boring advancement for the installation of temporary monitoring well AST-1/TW-1. No VOCs were detected at concentrations greater than their respective Protection to Groundwater or Residential PSRGs and no SVOCs were detected at concentrations greater than the laboratory method reporting limits in the soil samples collected from the former UST area. While one soil sample did contain a concentration of arsenic greater than the Residential PSRG and background concentrations, the concentration is estimated to be from natural occurring concentrations in site soils and an indication of a release or impacts to the site. If you have questions regarding this report or require ad( 523-4726. Sincerely, S& , Inc./ Scott YOU o g, P. / Prcjecx eolo st Attachments: Appendix I: Appendix II: Appendix III: Appendix IV: Appendix V: Appendix VI: Senior Geologist/Project Manager Figures Table Site Photographs Boring Log, Well Construction Record, and Well Abandonment Record Field Sampling Forms Laboratory Report ict us at (704) H-1 Attachments Attachment I — Figures OVsh: 7w, z ®r 1.3 , m Attachment II - Table TABLE 1 ISUMMARY OF SOIL SAMPLING RESULTS Homewood Banks Site 5510 Homewood Bansk Drive, Raleigh, North Carolina S&ME Project No.: 4335-16-102 Analysis >> VOCs by 8260B SVOCS by Total RCRA Metals by 6020B / 7471B v Sample FID o o Sample ID Date Depth Reading Collected (ft-BGS) (ppm) c U U U in .p Protection of Groundwater PSRG 25 NE Various 5.8 580 3.0 360,000 270 1.0 2.1 3.4 Residential PSRG 12,000 NE Various 0.68 3,100 14 23,000 NE 2.3 78 78 UST-1 02/08/18 17.5-20 4.6 < 0.061 < 0.0061 BRL < 0.82 82 < 0.14 1.5 3.4 < 0.023 0.72 < 0.14 UST-2 02/08/18 12.5-15 9.8 < 0.058 < 0.0058 BRL < 0.80 81 < 0.13 1.3 3.8 < 0.021 0.71 < 0.13 UST-3 02/08/18 7.5-10 13.0 < 0.056 < 0.0056 BRL < 0.85 57 < 0.14 1.0 4.9 < 0.024 0.82 < 0.14 02/09/18 2.5-3 6.9 0.077 < 0.0066 BRL < 0.092 61 < 0.15 1.4 8.3 < 0.026 < 0.61 < 0.15 UST-4 02/08/18 7.5-10 44.0 < 0.063 <0.0063 BRL 0.86 66 < 0.14 1.1 4.1 < 0.023 1.0 < 0.14 02/09/18 12-14 7.9 < 0.056 < 0.0056 BRL < 0.82 95 < 0.14 2.3 3.4 < 0.020 0.97 < 0.14 Dup-01 02/08/18 7.5-10 44.0 0.058 < 0.0058 BRL 0.85 77 < 0.14 1.2 4.6 < 0.024 1.2 < 0.14 UST-5 02/09/18 2.5-3 0.0 < 0.061 < 0.0061 BRL < 0.93 92 < 0.15 1.4 7.7 < 0.027 0.96 < 0.15 UST-6 02/09/18 2.5-3 8.9 0.13 0.0055 BRL 4.3 49 < 0.16 29 18 0.042 0.88 < 0.16 02/08/18 7.5-10 23.2 0.11 < 0.0058 BRL < 0.87 160 < 0.15 1.5 4.8 < 0.024 0.62 < 0.15 Background 02/09/18 2.5-3 0.0 NA NA NA 1.9 170 < 0.15 17 16 0.028 1.6 < 0.15 02/09/18 1 7.5-10 0.0 NA NA NA < 0.81 240 < 0.14 24 6.0 < 0.023 1.4 0.14 Notes: Results reported in milligrams per kilogram (mg/kg) PSRG: Preliminary Soil Remedaition Goals ft-BGS : feet below ground surface Value Concentration exceeds the Protection of Groundwater PSRG ppm : parts per million Value I Concentration exceeds the Residential PSRG NE: No standard established NA: Not analyzed for compound BRL: Below reporting limit FID : Flame Ionization Detector Attachment III — Site Photographs Homewood Banks Apartment Site Raleigh, NC Project #: 4335-16-102 Sheet 1 of 4 Photo 1 0 Ca 7 N d R d � i a � - •u? +5 0 O Ilk `l5 a Location 5510 Homewood Banks Drive, Raleigh, NC Remarks View of Former UST Area near end of carport. Photo 2 N cr UST' 3 �t V C >N m i Gl s a L O Y O s a Location 5510 Homewood Banks Drive, Raleigh, NC Remarks View of UST-1, UST-2, and UST-3 Sample Locations Homewood Banks Apartment Site Raleigh, NC Project #: 4335-16-102 I I Sheet 2 of 4 Photo 3 CO o �- U- .r N -i6 01 o Location 5510 Homewood Banks Drive, Raleigh, NC Remarks View of UST-4 Sample Location Photo 4 '9. 7 N ate+ R 0 N C >N 00 J L d M 0 o Location 5510 Homewood Banks Drive, Raleigh, NC Remarks View of UST-5 Sample Location (boring was conducted via hand auger) Homewood Banks Apartment Site Raleigh, NC Project #: 4335-16-102 Sheet 3 of 4 Photo 5 r o N N LL d L R u CO i GJ a "? L _ 0 K " O t a Location 5510 Homewood Banks Drive, Raleigh, NC Remarks View of UST-6 Sample Location Photo. s ;kj k iF"CO Cd I • S 4. • �tion5510 • ••• Banks Drive, Raleigh, Homewood Banks Apartment Site Raleigh, NC Project #: 4335-16-102 Sheet 4 of 4 Photo 7 0 N CO N 2 Gl 4. R ?4c a U C i M A a Location 5510 Homewood Banks Drive, Raleigh, NC Remarks View of AST-1/TW-1 Installation Photo 8 .,00 N -s, 0) S x L 0 4.• 0 s a Location 5510 Homewood Banks Drive, Raleigh, NC Remarks View of AST-1/TW-1 Sampling Attachment IV - Borings Logs, Well Construction Records, and Well Abandonment Records s LOG OF SOIL BORING AST-1 ; WITH MONITOR WELL CONSTRUCTION NOTES �II � PROJECT NAME: Homewoods Banks DATE DRILLED: 2/9/18 LOGGED BY: B. Wence DRILLING METHOD: Geoprobe/HSA DRILLER: Quantex, Inc. DEPTH TO WATER: 30.35 LATITUDE: 35.8352410 TOC ELEVATION: NM LONGITUDE:-78.6811730 ELEVATION (ft.) LIT HOLOGY Description FID Epp m ) Well Construction Well Description DEPTH (ft.) 0 0 Clayey SILT: Brownish Red; stiff, with some mica fragments, moist 0.0 -5 -5 — ... — . ---.. Sandy SILT: Orange; firm, with some mica fragments, dry f.. c o - - . 0.0 ,- Sandy SILT: Tannish Orange; soft, with some mica fragments, dry -10 -10 T.. T. Open Hole N to F+ oin o in P 00 0 00 0 0.0 Sch. 40 PVC Casing -15 -15 ... v1 F+ oin c in P 00 0 00 0 — .. 0.0 -20 -20 - - .- — — oin o in P 00 0 00 0 ....... 0.0 Bentonite -25 -25 — — --- - ON V1 V W Oin O YIP 00 O O O O — — Sandy SILT: Grayish Orange; soft, with some mica 0.0 ... _ fragments, wet ... #2 Filter Sand -30 -30 — Sandy SILT: Brownish Orange, firm, with seams of Sch. 40 0.010" Slotted PVC Screen CN to F+ oin o in P 00 0 0 0 mica fragments, wet 0.0 -35 -35 monitoring well was abandoned following Temporary groundwater sample NOTES: collection on 2/9/18 WELL CONSTRUCTION RECORD This form can be used for single or multiple wells For Internal Use ONLY: 1. Well Contractor Information: James D. Barker Well Contractor Name 3106A NC Well Contractor Certification Number Quantex, Inc. Company Name 2. Well Construction Permit #: NA List all applicable well construction permits (i.e. County, State, Variance, etc.) 3. Well Use (check well use): Water Supply Well: ❑Agricultural ❑Geothermal (Heating/Cooling Supply) ❑ Industrial/Commercial ❑ imgation Non -Water Supply Well: ❑Municipal/Public ❑Residential Water Supply (single) ❑Residential Water Supply (shared) Injection Well: ❑Aquifer Recharge ❑Groundwater Remediation ❑Aquifer Storage and Recovery ❑Salinity Barrier ❑Aquifer Test ❑Stormwater Drainage ❑Experimental Technology ❑Subsidence Control ❑Geothermal (Closed Loop) ❑Tracer ❑Geothermal (Heating/Cooling Return) ❑Other (explain under #21 Remarks) 4. Date Well(s) Completed: 2/8/1 8 Well ID# TW-1 5a. Well Location: 1-Inmoteinnrl Rnnlrc G\ifo KIA Facility/Owner Name Facility ID# (if applicable) 5510 Homewood Banks Dr., Raleigh NC 27612 Physical Address, City, and Zip Wake NA County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one ]at/long is sufficient) 35.835073 N 78.681291 W 6. is (are) the well(s): LiPermanent or ❑'Temporary 7. Is this a repair to an existing well: ❑Yes or ZNo If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: One For multiple injection or non -water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: 35' (ft.) For multiple wells list all depths if different (example- 3(a200' and 2L100') 10. Static water level below top of casing: -31' (ft.) Ifwater level is above casing, use "+" 11. Borehole diameter: (in.) 12. Well construction method: Auger (i.e. auger, rotary, cable, direct push, etc.) 14. WATER ZONES FROM TO DESCRIPTION 29 ft• 30 ft• Grey Cemented fine SANDS ft. ft. 15. OUTER CASING for multi -cased wells) OR LINER if ap icable FROM TO DIAMETER THICKNESS MATERIAL 0 ft• 20 ft- 2 in- Sch 40 PVC 16. INNER CASING OR TUBING eother al closed -loop) FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft. in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL 20 ft' 35 ft' 2 in. 0.010 Sch 40 PVC ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT 0 et. 16 ft. neat cement Pour - 220 lbs. neat cement 16 et. 18 ft. bentonite Pour - 30 lbs. 3/8" bentonite ft. ft. ND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD 18 ft• 35 ft. #2 sand Pour ft. ft. 20. DRILLING LOG attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) 0 rt. 8 t't. Dark Brown Clayey SILT 8 rt• 35 rt• Brown to Grey Silt to Cemented SANDS ft. ft. ft. ft. ft. ft. ft. ft. ft. ft. 21. REMARKS Well was temporary and was properly abandoned on 2/9/18 zi 22. CerUA on: 6 . � 2/27/18 Signature of[erutiied Well Contractor Date By signing this form, I hereby certify that the wells) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Iniection Wells: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Quality, Underground Injection Control Program, FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636 13a. Yield (gpm) Method of test: 24c. For Water Supply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of 13b. Disinfection type: Amount: completion of well construction to the county health department of the county where constructed. Form GW-1 North Carolina Department of Environment and Natural Resources - Division of Water Quality Revised Jan. 2013 WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: James D. Barker Well Contractor Name (or well owner personally abandoning well on his/her property) 3106-A NC Well Contractor Certification Number Quantex, Inc. Company Name 2. Well Construction Permit #: NA List all applicable wolf construction permits (i.e. County, State, Variance, etc.) tiknown 3. Well use (check well use): Water Supply Well: []Agricultural ❑Geothermal (Heating/Cooling Supply) ❑ hidustrial/Commercial ❑ Irrigation Non -Water Supply Well: ❑Municipal/Public ❑Residential Water Supply (single) ❑Residential Water Supply (shared) Injection well: ❑Aquifer Recharge ❑Groundwater Remediation ❑Aquifer Storage and Recovery ❑Salinity Barrier ❑Aquifer Test ❑Stormwater Drainage ❑Experimental Technology El Subsidence Control ❑Geothermal (Closed Loop) ❑Tracer ❑Geothermal (Heating/Cooling Return) ❑Other (explain under 7g) 4. Date well(s) abandoned: 2/9/18 For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: One For multiple injection or non -water supply welts ONL Y with the same construction/abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): NA (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: NA 7d. Amount of disinfectant used: NA 7e. Sealing materials used (check all that apply): hJ Neat Cement Grout 0 Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑ Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Bentonite Slurry ❑ Gravel ❑ Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: Approximately 55 lbs. 3/8 bentonite pellets Neat Cement 0'-5' Mixed and Poured 7g. Provide a brief description of the abandonment procedure: Bentonite pellets were poured at a rate 5 Ibs/min per mfr. recommendations. Bentonite was used to fill screen and casing (tamping and hydration) 5Q. Well location: Kt1cI of o IVCCa GCletClCu �., ..... . fIulIICllluJll ICIGC lu J 0LJ Homewood Banks Site NA Facility/Owner Name Facility ID# (if applicable) 8. e r f i cation : 5510 Homewood Banks Dr., Raleigh, NC 27612 f,,22J2/27/18 Physical Address, City, and Zip Signarfft afCer[ifted Well Contractor or Well Owner Date Wake NA By signing this form, l hereby certify that the well(s) was (were) abandoned in County Parcel Identification No. (PIN) accordance with 15A NCAC 02C .0100 or 2C .0200 Weft Construction Standards and that a copy of this record has been provided to the well owner. 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (ifwell field, one lat/long is sufficient) 9. Site diagram or additional well details: 35.835073 78.681291 You may use the back of this page to provide additional well site details or well N W abandonment details. You may also attach additional pages if necessary. CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED SUBMITTAL INSTRUCTIONS Attach well construction records) if available. for multiple injection or non -water supply wells ONL Y with the same construction/abandonment, you can submit one form. 10a. F o r A I I W e I I s: Submit this form within 30 days of completion of well 6a. Well I D#: TW-1 abandonment to the following: 6b. Total well depth: 35' (ft.) n 6c. Borehole diameter: pvc (in.) 6d. Water level below ground surface: —29' (ft.) 6e. Outer casing length (if known): NA (ft.) 20 6f. Inner casing/tubing length (if known): (ft.) 6g. Screen length (if known): 15 (ft.) Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Infection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Infection Wells: hi addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. Form GW-30 North Carolina Department of Environment and Natural Resources — Division of Water Quality Revised March 2013 LOG OF SOIL BORING UST-1 PROJECT NAME: Homewood Banks LOGGED BY: B. Wence DATE DRILLED: 2/9/18 DRILLER: Quantex, Inc. DRILLING METHOD: Geoprobe/HSA LATITUDE: 35.8346830 ELEVATION: NM LONGITUDE: -78.6819810 ELEVATION Soil (ft.) LrrHOLOGY Soil Description Interval DEPTH (ft.) Sample 0 0 — Sandy SILT: Brownish Tan; soft, with some mica fragments, dry ......... ...... . .— Sandy SILT: Light Tan; very soft, with some mica fragments, dry 10 -10 - - . 15 -15 - - .- 20 -20 _ . 25 -25 - — . Auger refusal at 30' 30 -30 FID (ppm) 0.0 0.0 O !-n hitNii o co 0 0 0.0 10 o O O 0.0 F+ N N O Vf O V� O O O O 0.0 10 O O O 0.0 F+ F+ N N O V} O to 0.0110 O O O 0.0 1.A F+ O of O cn G C O O 0.0 O O O O 0.0 NOTES: LOG OF SOIL BORING UST-2 PROJECT NAME: Homewood Banks LOGGED BY: B. Wence DATE DRILLED: 2/9/18 DRILLER: Quantex, Inc. DRILLING METHOD: Geoprobe/HSA LATITUDE: 35.8346650 ELEVATION: NM LONGITUDE: -78.6819990 ELEVATION Soil ft' LITHOLOGY Soil Description Interval DEPTH (ft.) Sample 0 0 — Sandy SILT: Tannish Orange; soft, with some mica fragments, moist .- Sandy SILT: Brownish Tan; soft, with some mica fragments, dry 5 -5 Sandy SILT: Light Tan; soft, with some mica fragments, dry 10 -10 - - .- 15 -15 - _ . 20 -20 — — Auger refusal at 25' 25 -25 — — FID (ppm) 0.0 0.0 0 o w 4.6 0.0 w o w o w 2.4 9.8 w 0 0 1.7 4.9 o� w 1.2 NOTES: LOG OF SOIL BORING UST-3 PROJECT NAME: Homewood Banks LOGGED BY: B. Wence DATE DRILLED: 2/9/18 DRILLER: Quantex, Inc. DRILLING METHOD: Geoprobe/HSA LATITUDE: 35.8346430 ELEVATION: NM LONGITUDE:-78.6820220 ELEVATION Soil "t.) LITHOLOGY Soil Description Interval FID DEPTH (ft.) Sample (pPm) 0 0 — — Sandy SILT: Tannish Orange; soft, with some mica fragments, moist ... .... — 3.2 ■ Sandy SILT: Brownish Tan; soft, with some mica fragments, dry -...-. 5.700 6.8 0 ......... ......... ......... ......... ......... ......... ......... ......... ......... ......... ............ Sandy SILT: Light Tan; soft, with some mica fragments, dry ..—. - 10 -10 — ... 113:0 P PO ....... 8.9 c w; o wi ■ - — Auger refusal at 15' 6.7 15 -15 0 0 Ln 0 0 NOTES: LOG OF SOIL BORING UST-4 PROJECT NAME: Homewood Banks LOGGED BY: B. Wence DATE DRILLED: 2/9/18 DRILLER: Quantex, Inc. DRILLING METHOD: Geoprobe/HSA LATITUDE: 35.8346170 ELEVATION: NM LONGITUDE:-78.6820500 ELEVATION Soil "t.) LITHOLOGY Soil Description Interval FID DEPTH (ft.) Sample (pPm) 0 0 — — Sandy SILT: Brownish Red; soft, with some mica fragments, moist ... .... — 2.8 Sandy SILT: Brownish Tan; soft, with some mica fragments, dry 6.9 4 16.8 o o — _ ......... ......... ......... ......... ......... ......... ......... ......... ......... ............ Sandy SILT: Light Tan; with some mica fragments, dry 10 -10 r+ _...-. 14.8 c o+ 0 — Auger refusal at 14' 7.9 ..... NOTES: LOG OF SOIL BORING UST-5 PROJECT NAME: Homewood Banks DATE DRILLED: 2/9/18 DRILLING METHOD: Hand Auger ELEVATION: NM ELEVATION LITHOLOGY DEPTH (ft.) 0 0 Soil Description LOGGED BY: B. Wence DRILLER: Quantex, Inc. LATITUDE: 35.8345950 LONGITUDE:-78.682069' Soil Interval Sample — Sandy SILT: Brownish Red; soft, with some mica fragments, moist, dry at 1' Sandy SILT: Light Tan; soft, with some mica fragments, dry 0.0 0.0 0.0 FID (ppm) NOTES: LOG OF SOIL BORING UST-6 PROJECT NAME: Homewood Banks LOGGED BY: B. Wence DATE DRILLED: 2/9/18 DRILLER: Quantex, Inc. DRILLING METHOD: Geoprobe/HSA LATITUDE: 35.8345650 ELEVATION: NM LONGITUDE:-78.6821060 ELEVATION Soil "t.) LITHOLOGY Soil Description Interval FID DEPTH (ft.) Sample (pPm) 0 0 — — Sandy SILT: Brownish Red; soft, with some mica fragments, moist ... .... — ............ Sandy SILT: Brownish Tan; fragments, dry 2.8 soft, with some mica -...-. 8.9 — ... ......... ......... ......... ......... ......... ......... ......... ......... ......... ............ C w 11.7 o w K Sandy SILT: Light Tan; soft, with some mica fragments, dry -.—.-. 23.2 10 -10 Auger refusal at 12' 9_7 o wr'� 0 0 Ln 0 0 NOTES: LOG OF SOIL BORING BKG PROJECT NAME: Homewood Banks LOGGED BY: B. Wence DATE DRILLED: 2/9/18 DRILLER: Quantex, Inc. DRILLING METHOD: Geoprobe/HSA LATITUDE: 35.8347630 ELEVATION: NM LONGITUDE: -78.6817680 ELEVATION Soil (ft.) LITHOLOGY Soil Description Interval FID DEPTH (ft.) Sample (pPm) 0 0 Sandy SILT: Brownish Red; soft, with some mica fragments, moist 0.0 0.0 5 -5 Sandy SILT: Brownish Tan; soft, with some mica fragments, dry 0.0 Sandy SILT: Light Tan; soft, with some mica fragments, dry 0.0 10 -10 0 0 NOTES: Attachment V - Field Sampling Forms Project Name: Homewood Banks Site 5510 Homeood Banks Drive, Raleigh, NC g 4335-16-102 Purge Date: s I I February 9, 2018 Project Location: J Project Number: Source Well: TW-1 Purge Time (Min.): 35 Locked?: No Sample Date: February 9, 2018 Sampled By: B. Wence Sample Time: 14:45 Weather: Sunny Air Temp: ° F Equipment Calibration Information: Equipment Date Time Calibration Solution Calibration Check pH 4/9/18 14:00 4.00, 7.00, 10.00 4.0 7.0 10.0 Conductivity 4/9/18 14:00 1,413 pS/cm 1,409 pS/cm Level & Well Data Measuring Point: Top of Casing Depth to Water: 30.35 ft-TOC Total Well Depth: 35.00 ft-TOC Height of Water Column: 4.65 feet Screen Length: 10 ft-GRD Stickup Height: 0 ft-GRD Purging Well Volume Well Diameter 2 inch Well Volume 0.8 gal 3 * Well Volume 2.3 gal 5 * Well Volume 3.8 gal Purge Method: Bailer Purge Start Time: 14:05 j End Time: 1 14:40 Total Volume Purged: 4.0 gal Well Purged Dry?:1 No Field Parameters Cumulative Volume (Gal) Time pH (s.u.) Temp (°C) Cond PS/cm Turbidity (NTU) Comments 1.0 14:10 6.4 16.17 122 +++ No Odors 1.5 14:15 6.2 15.57 106 +++ No Odors 2.0 14:20 6.1 15.52 104 +++ No Odors 2.5 14:25 6.1 15.53 103 +++ No Odors 3.0 14:30 6.0 15.47 102 +++ No Odors 3.5 14:35 6.0 15.51 101 +++ No Odors 4.0 14:40 6.0 15.52 100 +++ No Odors Sample Method: 1 Bailer Sample Time: 14:45 lytical Data Method Qty Container Pres. Method Qty Container Pres. VOCs 8260 3 40mL VOAs HCl SVOCs 8270 2 1L A None Signature Bryan S. Wence 2/9/2018 Form Revision Date: 9/13/17 8:00 AM Attachment VI - Laboratory Report Case Narrative PRISM `,. LABORATORIES, INC. S&ME, Inc - Charlotte Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 NC Certification No. 402 Full -Service Analytical & NC Drinking Water Cert No. 37735 Environmental Solutions SC Certification No. 99012 Project: Homewood Banks Lab Submittal Date: 02/10/2018 Prism Work Order: 8020189 02/14/2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A. Jones President/Project Manager Data Qualifiers Key Reference: Reviewed By Robbi A. Jones President/Project Manager A CCV result is below range. Analyte is not detected in samples. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 25 /P R I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Sample Receipt Summary 02/14/2018 Prism Work Order: 8020189 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received TW-1 8020189-01 Water 02/09/18 02/10/18 GW-Dup-1 8020189-02 Water 02/09/18 02/10/18 Trip Blank 8020189-03 Water 02/09/18 02/10/18 Samples were received in good condition at 3.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 25 �P R I S M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Prism ID Client ID There were no detections reported. Parameter Summary of Detections Method Prism Work Order: Result Units This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 25 /PRISM Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 02/14/2018 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Water Client Sample ID: TW-1 Prism Sample ID: 8020189-01 Prism Work Order: 8020189 Time Collected: 02/09/18 14:45 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 11 1.9 1 8270D 2/12/18 16:05 JMV P8130204 1,2-Dichlorobenzene BRL ug/L 11 1.7 1 8270D 2/12/18 16:05 JMV P8130204 1,3-Dichlorobenzene BRL ug/L 11 2.0 1 8270D 2/12/18 16:05 JMV P8130204 1,4-Dichlorobenzene BRL ug/L 11 1.7 1 8270D 2/12/18 16:05 JMV P8130204 1-Methyl naphthalene BRL ug/L 11 2.7 1 8270D 2/12/18 16:05 JMV P8130204 2,4,5-Trichlorophenol BRL ug/L 11 1.7 1 8270D 2/12/18 16:05 JMV P8130204 2,4,6-Trichlorophenol BRL ug/L 11 1.9 1 8270D 2/12/18 16:05 JMV P8130204 2,4-Dichlorophenol BRL ug/L 11 2.7 1 8270D 2/12/18 16:05 JMV P8130204 2,4-Dimethylphenol BRL ug/L 11 3.6 1 8270D 2/12/18 16:05 JMV P8130204 2,4-Dinitrophenol BRL ug/L 11 2.8 1 8270D 2/12/18 16:05 JMV P8130204 2,4-Dinitrotoluene BRL A ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 2,6-Dinitrotoluene BRL ug/L 11 1.2 1 8270D 2/12/18 16:05 JMV P8130204 2-Chloronaphthalene BRL ug/L 11 2.9 1 8270D 2/12/18 16:05 JMV P8130204 2-Chlorophenol BRL ug/L 11 2.0 1 8270D 2/12/18 16:05 JMV P8130204 2-Methyl naphthalene BRL ug/L 11 2.5 1 8270D 2/12/18 16:05 JMV P8130204 2-Methylphenol BRL ug/L 11 1.9 1 8270D 2/12/18 16:05 JMV P8130204 2-Nitroaniline BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 2-Nitrophenol BRL ug/L 11 2.5 1 8270D 2/12/18 16:05 JMV P8130204 3,3'-Dichlorobenzidine BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 3/4-Methyl phenol BRL ug/L 11 1.6 1 8270D 2/12/18 16:05 JMV P8130204 3-Nitroaniline BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 4,6-Dinitro-2-methylphenol BRL ug/L 11 1.4 1 8270D 2/12/18 16:05 JMV P8130204 4-Bromophenyl phenyl ether BRL ug/L 11 1.3 1 8270D 2/12/18 16:05 JMV P8130204 4-Chloro-3-methylphenol BRL ug/L 11 2.5 1 8270D 2/12/18 16:05 JMV P8130204 4-Chloroaniline BRL ug/L 11 2.6 1 8270D 2/12/18 16:05 JMV P8130204 4-Chlorophenyl phenyl ether BRL ug/L 11 1.4 1 8270D 2/12/18 16:05 JMV P8130204 4-Nitroaniline BRL ug/L 11 0.98 1 8270D 2/12/18 16:05 JMV P8130204 4-Nitrophenol BRL ug/L 11 0.63 1 8270D 2/12/18 16:05 JMV P8130204 Acenaphthene BRL ug/L 11 1.9 1 8270D 2/12/18 16:05 JMV P8130204 Acenaphthylene BRL ug/L 11 2.1 1 8270D 2/12/18 16:05 JMV P8130204 Aniline BRL ug/L 11 2.5 1 8270D 2/12/18 16:05 JMV P8130204 Anthracene BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 Azobenzene BRL ug/L 11 1.9 1 8270D 2/12/18 16:05 JMV P8130204 Benzo(a)anthracene BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 Benzo(a)pyrene BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 Benzo(b)fluoranthene BRL ug/L 11 1.2 1 8270D 2/12/18 16:05 JMV P8130204 Benzo(g,h,i)perylene BRL ug/L 11 1.4 1 8270D 2/12/18 16:05 JMV P8130204 Benzo(k)fluoranthene BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 Benzoic Acid BRL ug/L 110 4.9 1 8270D 2/12/18 16:05 JMV P8130204 Benzyl alcohol BRL ug/L 11 2.2 1 8270D 2/12/18 16:05 JMV P8130204 bis(2-Chloroethoxy)methane BRL ug/L 11 2.7 1 8270D 2/12/18 16:05 JMV P8130204 Bis(2-Chloroethyl)ether BRL ug/L 11 2.4 1 8270D 2/12/18 16:05 JMV P8130204 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 25 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: TW-1 Attn: Roger Smith Prism Sample ID: 8020189-01 9751 Southern Pine Blvd. Prism Work Order: 8020189 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 02/09/18 14:45 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Bis(2-chloroisopropyl)ether BRL ug/L 11 2.1 1 8270D 2/12/18 16:05 JMV P8130204 Bis(2-Ethylhexyl)phthalate BRL ug/L 11 1.4 1 8270D 2/12/18 16:05 JMV P8130204 Butyl benzyl phthalate BRL ug/L 11 1.4 1 8270D 2/12/18 16:05 JMV P8130204 Chrysene BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 Dibenzo(a,h)anthracene BRL ug/L 11 1.3 1 8270D 2/12/18 16:05 JMV P8130204 Dibenzofuran BRL ug/L 11 1.8 1 8270D 2/12/18 16:05 JMV P8130204 Diethyl phthalate BRL ug/L 11 3.5 1 8270D 2/12/18 16:05 JMV P8130204 Dimethyl phthalate BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 Di-n-butyl phthalate BRL ug/L 11 1.8 1 8270D 2/12/18 16:05 JMV P8130204 Di-n-octyl phthalate BRL ug/L 11 1.4 1 8270D 2/12/18 16:05 JMV P8130204 Fluoranthene BRL ug/L 11 1.8 1 8270D 2/12/18 16:05 JMV P8130204 Fluorene BRL ug/L 11 1.8 1 8270D 2/12/18 16:05 JMV P8130204 Hexachlorobenzene BRL ug/L 11 1.4 1 8270D 2/12/18 16:05 JMV P8130204 Hexachlorobutadiene BRL ug/L 11 2.3 1 8270D 2/12/18 16:05 JMV P8130204 Hexachlorocyclopentadiene BRL ug/L 11 1.8 1 8270D 2/12/18 16:05 JMV P8130204 Hexachloroethane BRL ug/L 11 1.8 1 8270D 2/12/18 16:05 JMV P8130204 Indeno(1,2,3-cd)pyrene BRL ug/L 11 4.1 1 8270D 2/12/18 16:05 JMV P8130204 Isophorone BRL ug/L 11 2.6 1 8270D 2/12/18 16:05 JMV P8130204 Naphthalene BRL ug/L 11 2.7 1 8270D 2/12/18 16:05 JMV P8130204 Nitrobenzene BRL ug/L 11 2.7 1 8270D 2/12/18 16:05 JMV P8130204 N-Nitroso-di-n-propylamine BRL ug/L 11 2.3 1 8270D 2/12/18 16:05 JMV P8130204 N-Nitrosodiphenylamine BRL ug/L 11 1.4 1 8270D 2/12/18 16:05 JMV P8130204 Pentachlorophenol BRL ug/L 11 1.3 1 8270D 2/12/18 16:05 JMV P8130204 Phenanthrene BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 Phenol BRL ug/L 11 1.0 1 8270D 2/12/18 16:05 JMV P8130204 Pyrene BRL ug/L 11 1.5 1 8270D 2/12/18 16:05 JMV P8130204 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 71 % 43-140 2-Fluorobiphenyl 71 % 44-119 2-Fluorophenol 46 % 19-119 Nitrobenzene-d5 64 % 44-120 Phenol-d5 29 % 11-52 Terphenyl-d14 75 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260B 2/13/18 19:46 KDM P8130244 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260B 2/13/18 19:46 KDM P8130244 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 2/13/18 19:46 KDM P8130244 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 2/13/18 19:46 KDM P8130244 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260B 2/13/18 19:46 KDM P8130244 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 2/13/18 19:46 KDM P8130244 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260B 2/13/18 19:46 KDM P8130244 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260B 2/13/18 19:46 KDM P8130244 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260B 2/13/18 19:46 KDM P8130244 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 25 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Water Report 02/14/2018 Client Sample ID: TW-1 Prism Sample ID: 8020189-01 Prism Work Order: 8020189 Time Collected: 02/09/18 14:45 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260B 2/13/18 19:46 KDM P8130244 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260B 2/13/18 19:46 KDM P8130244 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 2/13/18 19:46 KDM P8130244 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260B 2/13/18 19:46 KDM P8130244 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 2/13/18 19:46 KDM P8130244 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260B 2/13/18 19:46 KDM P8130244 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 2/13/18 19:46 KDM P8130244 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260B 2/13/18 19:46 KDM P8130244 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 2/13/18 19:46 KDM P8130244 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 2/13/18 19:46 KDM P8130244 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 2/13/18 19:46 KDM P8130244 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 2/13/18 19:46 KDM P8130244 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 2/13/18 19:46 KDM P8130244 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 2/13/18 19:46 KDM P8130244 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 2/13/18 19:46 KDM P8130244 Acetone BRL ug/L 5.0 0.31 1 8260B 2/13/18 19:46 KDM P8130244 Acrolein BRL ug/L 20 0.20 1 8260B 2/13/18 19:46 KDM P8130244 Acrylonitrile BRL ug/L 20 0.20 1 8260B 2/13/18 19:46 KDM P8130244 Benzene BRL ug/L 0.50 0.048 1 8260B 2/13/18 19:46 KDM P8130244 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 2/13/18 19:46 KDM P8130244 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 2/13/18 19:46 KDM P8130244 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 2/13/18 19:46 KDM P8130244 Bromoform BRL ug/L 1.0 0.040 1 8260B 2/13/18 19:46 KDM P8130244 Bromomethane BRL ug/L 1.0 0.18 1 8260B 2/13/18 19:46 KDM P8130244 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 2/13/18 19:46 KDM P8130244 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 2/13/18 19:46 KDM P8130244 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 2/13/18 19:46 KDM P8130244 Chloroethane BRL ug/L 0.50 0.22 1 8260B 2/13/18 19:46 KDM P8130244 Chloroform BRL ug/L 0.50 0.076 1 8260B 2/13/18 19:46 KDM P8130244 Chloromethane BRL ug/L 0.50 0.079 1 8260B 2/13/18 19:46 KDM P8130244 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260B 2/13/18 19:46 KDM P8130244 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 2/13/18 19:46 KDM P8130244 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260B 2/13/18 19:46 KDM P8130244 Dibromomethane BRL ug/L 0.50 0.065 1 8260B 2/13/18 19:46 KDM P8130244 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 2/13/18 19:46 KDM P8130244 Ethylbenzene BRL ug/L 0.50 0.061 1 8260B 2/13/18 19:46 KDM P8130244 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260B 2/13/18 19:46 KDM P8130244 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 2/13/18 19:46 KDM P8130244 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260B 2/13/18 19:46 KDM P8130244 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 2/13/18 19:46 KDM P8130244 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 2/13/18 19:46 KDM P8130244 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 2/13/18 19:46 KDM P8130244 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 2/13/18 19:46 KDM P8130244 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 25 Report Full -Service Analytical & PRISMLaboratory LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: TW-1 Attn: Roger Smith Prism Sample ID: 8020189-01 9751 Southern Pine Blvd. Prism Work Order: 8020189 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 02/09/18 14:45 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260B 2/13/18 19:46 KDM P8130244 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260B 2/13/18 19:46 KDM P8130244 Naphthalene BRL ug/L 1.0 0.19 1 8260B 2/13/18 19:46 KDM P8130244 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260B 2/13/18 19:46 KDM P8130244 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260B 2/13/18 19:46 KDM P8130244 o-Xylene BRL ug/L 0.50 0.044 1 8260B 2/13/18 19:46 KDM P8130244 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260B 2/13/18 19:46 KDM P8130244 Styrene BRL ug/L 0.50 0.047 1 8260B 2/13/18 19:46 KDM P8130244 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260B 2/13/18 19:46 KDM P8130244 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260B 2/13/18 19:46 KDM P8130244 Toluene BRL ug/L 0.50 0.044 1 8260B 2/13/18 19:46 KDM P8130244 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260B 2/13/18 19:46 KDM P8130244 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260B 2/13/18 19:46 KDM P8130244 Trichloroethylene BRL ug/L 0.50 0.078 1 8260B 2/13/18 19:46 KDM P8130244 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260B 2/13/18 19:46 KDM P8130244 Vinyl acetate BRL ug/L 2.0 0.060 1 8260B 2/13/18 19:46 KDM P8130244 Vinyl chloride BRL ug/L 0.50 0.097 1 8260B 2/13/18 19:46 KDM P8130244 Surrogate Recovery Control Limits 4-Bromofluorobenzene 104 % 80-124 Dibromofluoromethane 99 % 75-129 Toluene-d8 100 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 25 /PRISM Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 02/14/2018 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Water Client Sample ID: GW-Dup-1 Prism Sample ID: 8020189-02 Prism Work Order: 8020189 Time Collected: 02/09/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 11 1.9 1 8270D 2/12/18 16:27 JMV P8130204 1,2-Dichlorobenzene BRL ug/L 11 1.7 1 8270D 2/12/18 16:27 JMV P8130204 1,3-Dichlorobenzene BRL ug/L 11 2.0 1 8270D 2/12/18 16:27 JMV P8130204 1,4-Dichlorobenzene BRL ug/L 11 1.7 1 8270D 2/12/18 16:27 JMV P8130204 1-Methyl naphthalene BRL ug/L 11 2.7 1 8270D 2/12/18 16:27 JMV P8130204 2,4,5-Trichlorophenol BRL ug/L 11 1.7 1 8270D 2/12/18 16:27 JMV P8130204 2,4,6-Trichlorophenol BRL ug/L 11 1.9 1 8270D 2/12/18 16:27 JMV P8130204 2,4-Dichlorophenol BRL ug/L 11 2.7 1 8270D 2/12/18 16:27 JMV P8130204 2,4-Dimethylphenol BRL ug/L 11 3.6 1 8270D 2/12/18 16:27 JMV P8130204 2,4-Dinitrophenol BRL ug/L 11 2.8 1 8270D 2/12/18 16:27 JMV P8130204 2,4-Dinitrotoluene BRL A ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 2,6-Dinitrotoluene BRL ug/L 11 1.2 1 8270D 2/12/18 16:27 JMV P8130204 2-Chloronaphthalene BRL ug/L 11 2.9 1 8270D 2/12/18 16:27 JMV P8130204 2-Chlorophenol BRL ug/L 11 2.0 1 8270D 2/12/18 16:27 JMV P8130204 2-Methyl naphthalene BRL ug/L 11 2.5 1 8270D 2/12/18 16:27 JMV P8130204 2-Methylphenol BRL ug/L 11 1.9 1 8270D 2/12/18 16:27 JMV P8130204 2-Nitroaniline BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 2-Nitrophenol BRL ug/L 11 2.5 1 8270D 2/12/18 16:27 JMV P8130204 3,3'-Dichlorobenzidine BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 3/4-Methyl phenol BRL ug/L 11 1.6 1 8270D 2/12/18 16:27 JMV P8130204 3-Nitroaniline BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 4,6-Dinitro-2-methylphenol BRL ug/L 11 1.4 1 8270D 2/12/18 16:27 JMV P8130204 4-Bromophenyl phenyl ether BRL ug/L 11 1.3 1 8270D 2/12/18 16:27 JMV P8130204 4-Chloro-3-methylphenol BRL ug/L 11 2.5 1 8270D 2/12/18 16:27 JMV P8130204 4-Chloroaniline BRL ug/L 11 2.6 1 8270D 2/12/18 16:27 JMV P8130204 4-Chlorophenyl phenyl ether BRL ug/L 11 1.4 1 8270D 2/12/18 16:27 JMV P8130204 4-Nitroaniline BRL ug/L 11 0.98 1 8270D 2/12/18 16:27 JMV P8130204 4-Nitrophenol BRL ug/L 11 0.63 1 8270D 2/12/18 16:27 JMV P8130204 Acenaphthene BRL ug/L 11 1.9 1 8270D 2/12/18 16:27 JMV P8130204 Acenaphthylene BRL ug/L 11 2.1 1 8270D 2/12/18 16:27 JMV P8130204 Aniline BRL ug/L 11 2.5 1 8270D 2/12/18 16:27 JMV P8130204 Anthracene BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 Azobenzene BRL ug/L 11 1.9 1 8270D 2/12/18 16:27 JMV P8130204 Benzo(a)anthracene BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 Benzo(a)pyrene BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 Benzo(b)fluoranthene BRL ug/L 11 1.2 1 8270D 2/12/18 16:27 JMV P8130204 Benzo(g,h,i)perylene BRL ug/L 11 1.4 1 8270D 2/12/18 16:27 JMV P8130204 Benzo(k)fluoranthene BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 Benzoic Acid BRL ug/L 110 4.9 1 8270D 2/12/18 16:27 JMV P8130204 Benzyl alcohol BRL ug/L 11 2.2 1 8270D 2/12/18 16:27 JMV P8130204 bis(2-Chloroethoxy)methane BRL ug/L 11 2.7 1 8270D 2/12/18 16:27 JMV P8130204 Bis(2-Chloroethyl)ether BRL ug/L 11 2.4 1 8270D 2/12/18 16:27 JMV P8130204 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 25 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: GW-Dup-1 Attn: Roger Smith Prism Sample ID: 8020189-02 9751 Southern Pine Blvd. Prism Work Order: 8020189 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 02/09/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Bis(2-chloroisopropyl)ether BRL ug/L 11 2.1 1 8270D 2/12/18 16:27 JMV P8130204 Bis(2-Ethylhexyl)phthalate BRL ug/L 11 1.4 1 8270D 2/12/18 16:27 JMV P8130204 Butyl benzyl phthalate BRL ug/L 11 1.4 1 8270D 2/12/18 16:27 JMV P8130204 Chrysene BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 Dibenzo(a,h)anthracene BRL ug/L 11 1.3 1 8270D 2/12/18 16:27 JMV P8130204 Dibenzofuran BRL ug/L 11 1.8 1 8270D 2/12/18 16:27 JMV P8130204 Diethyl phthalate BRL ug/L 11 3.5 1 8270D 2/12/18 16:27 JMV P8130204 Dimethyl phthalate BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 Di-n-butyl phthalate BRL ug/L 11 1.8 1 8270D 2/12/18 16:27 JMV P8130204 Di-n-octyl phthalate BRL ug/L 11 1.4 1 8270D 2/12/18 16:27 JMV P8130204 Fluoranthene BRL ug/L 11 1.8 1 8270D 2/12/18 16:27 JMV P8130204 Fluorene BRL ug/L 11 1.8 1 8270D 2/12/18 16:27 JMV P8130204 Hexachlorobenzene BRL ug/L 11 1.4 1 8270D 2/12/18 16:27 JMV P8130204 Hexachlorobutadiene BRL ug/L 11 2.3 1 8270D 2/12/18 16:27 JMV P8130204 Hexachlorocyclopentadiene BRL ug/L 11 1.8 1 8270D 2/12/18 16:27 JMV P8130204 Hexachloroethane BRL ug/L 11 1.8 1 8270D 2/12/18 16:27 JMV P8130204 Indeno(1,2,3-cd)pyrene BRL ug/L 11 4.1 1 8270D 2/12/18 16:27 JMV P8130204 Isophorone BRL ug/L 11 2.6 1 8270D 2/12/18 16:27 JMV P8130204 Naphthalene BRL ug/L 11 2.7 1 8270D 2/12/18 16:27 JMV P8130204 Nitrobenzene BRL ug/L 11 2.7 1 8270D 2/12/18 16:27 JMV P8130204 N-Nitroso-di-n-propylamine BRL ug/L 11 2.3 1 8270D 2/12/18 16:27 JMV P8130204 N-Nitrosodiphenylamine BRL ug/L 11 1.4 1 8270D 2/12/18 16:27 JMV P8130204 Pentachlorophenol BRL ug/L 11 1.3 1 8270D 2/12/18 16:27 JMV P8130204 Phenanthrene BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 Phenol BRL ug/L 11 1.0 1 8270D 2/12/18 16:27 JMV P8130204 Pyrene BRL ug/L 11 1.5 1 8270D 2/12/18 16:27 JMV P8130204 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 74 % 43-140 2-Fluorobiphenyl 72 % 44-119 2-Fluorophenol 47 % 19-119 Nitrobenzene-d5 66 % 44-120 Phenol-d5 30 % 11-52 Terphenyl-d14 79 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260B 2/13/18 20:12 KDM P8130244 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260B 2/13/18 20:12 KDM P8130244 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 2/13/18 20:12 KDM P8130244 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 2/13/18 20:12 KDM P8130244 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260B 2/13/18 20:12 KDM P8130244 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 2/13/18 20:12 KDM P8130244 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260B 2/13/18 20:12 KDM P8130244 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260B 2/13/18 20:12 KDM P8130244 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260B 2/13/18 20:12 KDM P8130244 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 25 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Water Report 02/14/2018 Client Sample ID: GW-Dup-1 Prism Sample ID: 8020189-02 Prism Work Order: 8020189 Time Collected: 02/09/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260B 2/13/18 20:12 KDM P8130244 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260B 2/13/18 20:12 KDM P8130244 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 2/13/18 20:12 KDM P8130244 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260B 2/13/18 20:12 KDM P8130244 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 2/13/18 20:12 KDM P8130244 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260B 2/13/18 20:12 KDM P8130244 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 2/13/18 20:12 KDM P8130244 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260B 2/13/18 20:12 KDM P8130244 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 2/13/18 20:12 KDM P8130244 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 2/13/18 20:12 KDM P8130244 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 2/13/18 20:12 KDM P8130244 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 2/13/18 20:12 KDM P8130244 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 2/13/18 20:12 KDM P8130244 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 2/13/18 20:12 KDM P8130244 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 2/13/18 20:12 KDM P8130244 Acetone BRL ug/L 5.0 0.31 1 8260B 2/13/18 20:12 KDM P8130244 Acrolein BRL ug/L 20 0.20 1 8260B 2/13/18 20:12 KDM P8130244 Acrylonitrile BRL ug/L 20 0.20 1 8260B 2/13/18 20:12 KDM P8130244 Benzene BRL ug/L 0.50 0.048 1 8260B 2/13/18 20:12 KDM P8130244 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 2/13/18 20:12 KDM P8130244 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 2/13/18 20:12 KDM P8130244 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 2/13/18 20:12 KDM P8130244 Bromoform BRL ug/L 1.0 0.040 1 8260B 2/13/18 20:12 KDM P8130244 Bromomethane BRL ug/L 1.0 0.18 1 8260B 2/13/18 20:12 KDM P8130244 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 2/13/18 20:12 KDM P8130244 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 2/13/18 20:12 KDM P8130244 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 2/13/18 20:12 KDM P8130244 Chloroethane BRL ug/L 0.50 0.22 1 8260B 2/13/18 20:12 KDM P8130244 Chloroform BRL ug/L 0.50 0.076 1 8260B 2/13/18 20:12 KDM P8130244 Chloromethane BRL ug/L 0.50 0.079 1 8260B 2/13/18 20:12 KDM P8130244 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260B 2/13/18 20:12 KDM P8130244 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 2/13/18 20:12 KDM P8130244 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260B 2/13/18 20:12 KDM P8130244 Dibromomethane BRL ug/L 0.50 0.065 1 8260B 2/13/18 20:12 KDM P8130244 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 2/13/18 20:12 KDM P8130244 Ethylbenzene BRL ug/L 0.50 0.061 1 8260B 2/13/18 20:12 KDM P8130244 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260B 2/13/18 20:12 KDM P8130244 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 2/13/18 20:12 KDM P8130244 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260B 2/13/18 20:12 KDM P8130244 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 2/13/18 20:12 KDM P8130244 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 2/13/18 20:12 KDM P8130244 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 2/13/18 20:12 KDM P8130244 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 2/13/18 20:12 KDM P8130244 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 25 Report Full -Service Analytical & PRISMLaboratory LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: GW-Dup-1 Attn: Roger Smith Prism Sample ID: 8020189-02 9751 Southern Pine Blvd. Prism Work Order: 8020189 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 02/09/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260B 2/13/18 20:12 KDM P8130244 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260B 2/13/18 20:12 KDM P8130244 Naphthalene BRL ug/L 1.0 0.19 1 8260B 2/13/18 20:12 KDM P8130244 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260B 2/13/18 20:12 KDM P8130244 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260B 2/13/18 20:12 KDM P8130244 o-Xylene BRL ug/L 0.50 0.044 1 8260B 2/13/18 20:12 KDM P8130244 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260B 2/13/18 20:12 KDM P8130244 Styrene BRL ug/L 0.50 0.047 1 8260B 2/13/18 20:12 KDM P8130244 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260B 2/13/18 20:12 KDM P8130244 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260B 2/13/18 20:12 KDM P8130244 Toluene BRL ug/L 0.50 0.044 1 8260B 2/13/18 20:12 KDM P8130244 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260B 2/13/18 20:12 KDM P8130244 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260B 2/13/18 20:12 KDM P8130244 Trichloroethylene BRL ug/L 0.50 0.078 1 8260B 2/13/18 20:12 KDM P8130244 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260B 2/13/18 20:12 KDM P8130244 Vinyl acetate BRL ug/L 2.0 0.060 1 8260B 2/13/18 20:12 KDM P8130244 Vinyl chloride BRL ug/L 0.50 0.097 1 8260B 2/13/18 20:12 KDM P8130244 Surrogate Recovery Control Limits 4-Bromofluorobenzene 104 % 80-124 Dibromofluoromethane 102 % 75-129 Toluene-d8 99 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 25 /PRISM Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 02/14/2018 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Water Client Sample ID: Trip Blank Prism Sample ID: 8020189-03 Prism Work Order: 8020189 Time Collected: 02/09/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260B 2/13/18 14:37 KDM P8130244 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260B 2/13/18 14:37 KDM P8130244 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 2/13/18 14:37 KDM P8130244 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 2/13/18 14:37 KDM P8130244 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260B 2/13/18 14:37 KDM P8130244 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 2/13/18 14:37 KDM P8130244 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260B 2/13/18 14:37 KDM P8130244 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260B 2/13/18 14:37 KDM P8130244 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260B 2/13/18 14:37 KDM P8130244 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260B 2/13/18 14:37 KDM P8130244 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260B 2/13/18 14:37 KDM P8130244 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 2/13/18 14:37 KDM P8130244 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260B 2/13/18 14:37 KDM P8130244 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 2/13/18 14:37 KDM P8130244 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260B 2/13/18 14:37 KDM P8130244 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 2/13/18 14:37 KDM P8130244 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260B 2/13/18 14:37 KDM P8130244 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 2/13/18 14:37 KDM P8130244 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 2/13/18 14:37 KDM P8130244 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 2/13/18 14:37 KDM P8130244 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 2/13/18 14:37 KDM P8130244 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 2/13/18 14:37 KDM P8130244 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 2/13/18 14:37 KDM P8130244 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 2/13/18 14:37 KDM P8130244 Acetone BRL ug/L 5.0 0.31 1 8260B 2/13/18 14:37 KDM P8130244 Acrolein BRL ug/L 20 0.20 1 8260B 2/13/18 14:37 KDM P8130244 Acrylonitrile BRL ug/L 20 0.20 1 8260B 2/13/18 14:37 KDM P8130244 Benzene BRL ug/L 0.50 0.048 1 8260B 2/13/18 14:37 KDM P8130244 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 2/13/18 14:37 KDM P8130244 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 2/13/18 14:37 KDM P8130244 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 2/13/18 14:37 KDM P8130244 Bromoform BRL ug/L 1.0 0.040 1 8260B 2/13/18 14:37 KDM P8130244 Bromomethane BRL ug/L 1.0 0.18 1 8260B 2/13/18 14:37 KDM P8130244 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 2/13/18 14:37 KDM P8130244 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 2/13/18 14:37 KDM P8130244 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 2/13/18 14:37 KDM P8130244 Chloroethane BRL ug/L 0.50 0.22 1 8260B 2/13/18 14:37 KDM P8130244 Chloroform BRL ug/L 0.50 0.076 1 8260B 2/13/18 14:37 KDM P8130244 Chloromethane BRL ug/L 0.50 0.079 1 8260B 2/13/18 14:37 KDM P8130244 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260B 2/13/18 14:37 KDM P8130244 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 2/13/18 14:37 KDM P8130244 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260B 2/13/18 14:37 KDM P8130244 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 0f 25 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: Trip Blank Attn: Roger Smith Prism Sample ID: 8020189-03 9751 Southern Pine Blvd. Prism Work Order: 8020189 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 02/09/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromomethane BRL ug/L 0.50 0.065 1 8260B 2/13/18 14:37 KDM P8130244 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 2/13/18 14:37 KDM P8130244 Ethylbenzene BRL ug/L 0.50 0.061 1 8260B 2/13/18 14:37 KDM P8130244 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260B 2/13/18 14:37 KDM P8130244 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 2/13/18 14:37 KDM P8130244 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260B 2/13/18 14:37 KDM P8130244 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 2/13/18 14:37 KDM P8130244 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 2/13/18 14:37 KDM P8130244 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 2/13/18 14:37 KDM P8130244 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 2/13/18 14:37 KDM P8130244 Methylene Chloride BRL ug/L 1.0 0.083 1 8260B 2/13/18 14:37 KDM P8130244 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260B 2/13/18 14:37 KDM P8130244 Naphthalene BRL ug/L 1.0 0.19 1 8260B 2/13/18 14:37 KDM P8130244 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260B 2/13/18 14:37 KDM P8130244 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260B 2/13/18 14:37 KDM P8130244 o-Xylene BRL ug/L 0.50 0.044 1 8260B 2/13/18 14:37 KDM P8130244 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260B 2/13/18 14:37 KDM P8130244 Styrene BRL ug/L 0.50 0.047 1 8260B 2/13/18 14:37 KDM P8130244 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260B 2/13/18 14:37 KDM P8130244 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260B 2/13/18 14:37 KDM P8130244 Toluene BRL ug/L 0.50 0.044 1 8260B 2/13/18 14:37 KDM P8130244 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260B 2/13/18 14:37 KDM P8130244 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260B 2/13/18 14:37 KDM P8130244 Trichloroethylene BRL ug/L 0.50 0.078 1 8260B 2/13/18 14:37 KDM P8130244 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260B 2/13/18 14:37 KDM P8130244 Vinyl acetate BRL ug/L 2.0 0.060 1 8260B 2/13/18 14:37 KDM P8130244 Vinyl chloride BRL ug/L 0.50 0.097 1 8260B 2/13/18 14:37 KDM P8130244 Surrogate Recovery Control Limits 4-Bromofluorobenzene 103 % 80-124 Dibromofluoromethane 99 % 75-129 Toluene-d8 99 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 25 P R I IS M Full -Service Analytical Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Project: Homewood Banks Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 8020189 Time Submitted: 2/10/2018 9:55:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P860244 - 5030B Blank (P8B0244-BLK1) Prepared &Analyzed: 02/13/18 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 1,1,1-Trichloroethane BRL 0.50 ug/L 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 1,1,2-Trichloroethane BRL 0.50 ug/L 1,1-Dichloroethane BRL 0.50 ug/L 1,1-Dichloroethylene BRL 0.50 ug/L 1,1-Dichloropropylene BRL 0.50 ug/L 1,2,3-Trichlorobenzene BRL 2.0 ug/L 1,2,3-Trichloropropane BRL 1.0 ug/L 1,2,4-Trichlorobenzene BRL 1.0 ug/L 1,2,4-Trimethyl benzene BRL 0.50 ug/L 1,2-Dibromo-3-chloropropane BRL 2.0 ug/L 1,2-Dibromoethane BRL 0.50 ug/L 1,2-Dichlorobenzene BRL 0.50 ug/L 1,2-Dichloroethane BRL 0.50 ug/L 1,2-Dichloropropane BRL 0.50 ug/L 1,3,5-Trimethyl benzene BRL 0.50 ug/L 1,3-Dichlorobenzene BRL 0.50 ug/L 1,3-Dichloropropane BRL 0.50 ug/L 1,4-Dichlorobenzene BRL 0.50 ug/L 2,2-Dichloropropane BRL 2.0 ug/L 2-Chlorotoluene BRL 0.50 ug/L 4-Chlorotoluene BRL 0.50 ug/L 4-Isopropyltoluene BRL 0.50 ug/L Acetone BRL 5.0 ug/L Acrolein BRL 20 ug/L Acrylonitrile BRL 20 ug/L Benzene BRL 0.50 ug/L Bromobenzene BRL 0.50 ug/L Bromochloromethane BRL 0.50 ug/L Bromodichloromethane BRL 0.50 ug/L Bromoform BRL 1.0 ug/L Bromomethane BRL 1.0 ug/L Carbon disulfide BRL 5.0 ug/L Carbon Tetrachloride BRL 0.50 ug/L Chlorobenzene BRL 0.50 ug/L Chloroethane BRL 0.50 ug/L Chloroform BRL 0.50 ug/L Chloromethane BRL 0.50 ug/L cis-1,2-Dichloroethylene BRL 0.50 ug/L cis-1,3-Dichloropropylene BRL 0.50 ug/L Dibromochloromethane BRL 0.50 ug/L Dibromomethane BRL 0.50 ug/L Dichlorodifluoromethane BRL 1.0 ug/L Ethylbenzene BRL 0.50 ug/L Hexachlorobutadiene BRL 2.0 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 25 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Project: Homewood Banks Prism Work Order: 8020189 Attn: Roger Smith Time Submitted: 2/10/2018 9:55:OOAM 9751 Southern Pine Blvd. Charlotte, NC 28273 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81130244 - 5030B Blank (1138130244-BLK1) Prepared &Analyzed: 02/13/18 Isopropyl Ether BRL 0.50 ug/L Isopropylbenzene (Cumene) BRL 0.50 ug/L m,p-Xylenes BRL 1.0 ug/L Methyl Butyl Ketone (2-Hexanone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 1.0 ug/L Methyl-tert-Butyl Ether BRL 0.50 ug/L Naphthalene BRL 1.0 ug/L n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 0.50 ug/L o-Xylene BRL 0.50 ug/L sec-Butylbenzene BRL 0.50 ug/L Styrene BRL 0.50 ug/L tert-Butyl benzene BRL 0.50 ug/L Tetrachloroethylene BRL 0.50 ug/L Toluene BRL 0.50 ug/L trans- 1,2-Dichloroethylene BRL 0.50 ug/L trans- 1,3-Dichloropropylene BRL 0.50 ug/L Trichloroethylene BRL 0.50 ug/L Trichlorofluoromethane BRL 0.50 ug/L Vinyl acetate BRL 2.0 ug/L Vinyl chloride BRL 0.50 ug/L Surrogate:4-Bromofluorobenzene 51.3 ug/L 50.00 103 80-124 Surrogate: Dibromofluoromethane 49.5 ug/L 50.00 99 75-129 Surrogate: Toluene-d8 49.4 ug/L 50.00 99 77-123 LCS (13811130244-13SI) Prepared &Analyzed: 02/13/18 1,1,1,2-Tetrachloroethane 23.7 0.50 ug/L 20.00 118 79-134 1,1,1-Trichloroethane 21.9 0.50 ug/L 20.00 109 75-136 1,1,2,2-Tetrachloroethane 23.0 0.50 ug/L 20.00 115 62-127 1,1,2-Trichloroethane 23.1 0.50 ug/L 20.00 116 70-140 1,1-Dichloroethane 23.7 0.50 ug/L 20.00 119 78-130 1,1-Dichloroethylene 22.0 0.50 ug/L 20.00 110 70-154 1, 1 -Dichloropropylene 25.4 0.50 ug/L 20.00 127 71-136 1,2,3-Trichlorobenzene 21.0 2.0 ug/L 20.00 105 58-144 1,2,3-Trichloropropane 22.8 1.0 ug/L 20.00 114 71-127 1,2,4-Trichlorobenzene 22.5 1.0 ug/L 20.00 112 66-139 1,2,4-Trimethylbenzene 23.9 0.50 ug/L 20.00 120 75-133 1,2-Dibromo-3-chloropropane 20.6 2.0 ug/L 20.00 103 63-134 1,2-Dibromoethane 23.1 0.50 ug/L 20.00 116 77-135 1,2-Dichlorobenzene 23.3 0.50 ug/L 20.00 116 78-128 1,2-Dichloroethane 23.0 0.50 ug/L 20.00 115 68-131 1,2-Dichloropropane 24.4 0.50 ug/L 20.00 122 77-130 1,3,5-Trimethylbenzene 24.0 0.50 ug/L 20.00 120 75-131 1,3-Dichlorobenzene 23.0 0.50 ug/L 20.00 115 77-125 1,3-Dichloropropane 24.2 0.50 ug/L 20.00 121 76-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 0f 25 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Project: Homewood Banks Prism Work Order: 8020189 Attn: Roger Smith Time Submitted: 2/10/2018 9:55:OOAM 9751 Southern Pine Blvd. Charlotte, NC 28273 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81130244 - 5030B LCS (P8B0244-BS1) Prepared &Analyzed: 02/13/18 1,4-Dichlorobenzene 23.1 0.50 ug/L 20.00 115 75-126 2,2-Dichloropropane 23.8 2.0 ug/L 20.00 119 29-149 2-Chlorotoluene 23.5 0.50 ug/L 20.00 117 74-126 4-Chlorotoluene 23.7 0.50 ug/L 20.00 118 78-129 4-Isopropyltoluene 22.6 0.50 ug/L 20.00 113 69-132 Acetone 42.7 5.0 ug/L 40.00 107 40-166 Acrolein 42.3 20 ug/L 40.00 106 70-130 Acrylonitrile 45.0 20 ug/L 40.00 113 81-127 Benzene 24.0 0.50 ug/L 20.00 120 77-128 Bromobenzene 23.4 0.50 ug/L 20.00 117 78-129 Bromochloromethane 23.8 0.50 ug/L 20.00 119 78-135 Bromodichloromethane 24.2 0.50 ug/L 20.00 121 76-138 Bromoform 18.7 1.0 ug/L 20.00 93 71-135 Bromomethane 20.3 1.0 ug/L 20.00 101 41-168 Carbon disulfide 25.0 5.0 ug/L 20.00 125 59-135 Carbon Tetrachloride 22.4 0.50 ug/L 20.00 112 72-142 Chlorobenzene 23.8 0.50 ug/L 20.00 119 78-119 Chloroethane 24.5 0.50 ug/L 20.00 122 57-142 Chloroform 22.7 0.50 ug/L 20.00 114 77-130 Chloromethane 18.3 0.50 ug/L 20.00 92 47-145 cis-1,2-Dichloroethylene 24.2 0.50 ug/L 20.00 121 76-141 cis-1,3-Dichloropropylene 22.6 0.50 ug/L 20.00 113 65-140 Dibromochloromethane 21.2 0.50 ug/L 20.00 106 75-134 Dibromomethane 23.6 0.50 ug/L 20.00 118 76-138 Dichlorodifluoromethane 19.1 1.0 ug/L 20.00 96 28-163 Ethylbenzene 23.8 0.50 ug/L 20.00 119 80-127 Hexachlorobutadiene 23.4 2.0 ug/L 20.00 117 61-134 Isopropyl Ether 23.1 0.50 ug/L 20.00 115 60-154 Isopropylbenzene (Cumene) 24.2 0.50 ug/L 20.00 121 70-130 m,p-Xylenes 49.3 1.0 ug/L 40.00 123 77-133 Methyl Butyl Ketone (2-Hexanone) 22.3 5.0 ug/L 20.00 111 64-137 Methyl Ethyl Ketone (2-Butanone) 22.6 5.0 ug/L 20.00 113 71-134 Methyl Isobutyl Ketone 23.2 5.0 ug/L 20.00 116 69-134 Methylene Chloride 22.6 1.0 ug/L 20.00 113 73-131 Methyl-tert-Butyl Ether 23.5 0.50 ug/L 20.00 118 68-135 Naphthalene 21.1 1.0 ug/L 20.00 105 64-136 n-Butylbenzene 23.3 1.0 ug/L 20.00 117 68-134 n-Propylbenzene 24.6 0.50 ug/L 20.00 123 72-132 o-Xylene 23.4 0.50 ug/L 20.00 117 78-128 sec-Butylbenzene 24.0 0.50 ug/L 20.00 120 71-131 Styrene 21.6 0.50 ug/L 20.00 108 78-129 tert-Butyl benzene 23.4 0.50 ug/L 20.00 117 70-132 Tetrachloroethylene 23.5 0.50 ug/L 20.00 117 80-129 Toluene 24.0 0.50 ug/L 20.00 120 76-131 trans- 1,2-Dichloroethylene 22.6 0.50 ug/L 20.00 113 76-135 trans- 1,3-Dichloropropylene 22.0 0.50 ug/L 20.00 110 67-140 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 0f 25 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130244 - 5030B Reporting Result Limit Units Prism Work Order: 8020189 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P8B0244-BS1) Prepared &Analyzed: 02/13/18 Trichloroethylene 24.2 0.50 ug/L 20.00 121 77-133 Trichlorofluoromethane 26.2 0.50 ug/L 20.00 131 62-148 Vinyl acetate 25.0 2.0 ug/L 20.00 125 34-167 Vinyl chloride 21.2 0.50 ug/L 20.00 106 57-141 Surrogate:4-Bromofluorobenzene 51.7 ug/L 50.00 103 80-124 Surrogate: Dibromofluoromethane 49.3 ug/L 50.00 99 75-129 Surrogate: Toluene-d8 49.5 ug/L 50.00 99 77-123 LCS Dup (P8130244-Ill Prepared & Analyzed: 02/13/18 1,1,1,2-Tetrachloroethane 23.2 0.50 ug/L 20.00 116 79-134 2 20 1,1,1-Trichloroethane 21.5 0.50 ug/L 20.00 107 75-136 2 20 1,1,2,2-Tetrachloroethane 22.8 0.50 ug/L 20.00 114 62-127 0.7 20 1,1,2-Trichloroethane 23.1 0.50 ug/L 20.00 116 70-140 0.04 20 1,1-Dichloroethane 22.8 0.50 ug/L 20.00 114 78-130 4 20 1,1-Dichloroethylene 21.2 0.50 ug/L 20.00 106 70-154 4 20 1, 1 -Dichloropropylene 25.0 0.50 ug/L 20.00 125 71-136 2 20 1,2,3-Trichlorobenzene 21.5 2.0 ug/L 20.00 107 58-144 2 20 1,2,3-Trichloropropane 23.4 1.0 ug/L 20.00 117 71-127 2 20 1,2,4-Trichlorobenzene 22.1 1.0 ug/L 20.00 110 66-139 2 20 1,2,4-Trimethylbenzene 23.2 0.50 ug/L 20.00 116 75-133 3 20 1,2-Dibromo-3-chloropropane 21.6 2.0 ug/L 20.00 108 63-134 5 20 1,2-Dibromoethane 23.4 0.50 ug/L 20.00 117 77-135 1 20 1,2-Dichlorobenzene 22.7 0.50 ug/L 20.00 114 78-128 3 20 1,2-Dichloroethane 23.0 0.50 ug/L 20.00 115 68-131 0.09 20 1,2-Dichloropropane 23.7 0.50 ug/L 20.00 119 77-130 3 20 1,3,5-Trimethylbenzene 23.1 0.50 ug/L 20.00 116 75-131 4 20 1,3-Dichlorobenzene 23.0 0.50 ug/L 20.00 115 77-125 0.1 20 1,3-Dichloropropane 24.0 0.50 ug/L 20.00 120 76-132 0.7 20 1,4-Dichlorobenzene 22.2 0.50 ug/L 20.00 ill 75-126 4 20 2,2-Dichloropropane 23.2 2.0 ug/L 20.00 116 29-149 2 20 2-Chlorotoluene 22.9 0.50 ug/L 20.00 114 74-126 3 20 4-Chlorotoluene 23.0 0.50 ug/L 20.00 115 78-129 3 20 4-Isopropyltoluene 22.1 0.50 ug/L 20.00 110 69-132 3 20 Acetone 45.8 5.0 ug/L 40.00 114 40-166 7 20 Acrolein 45.7 20 ug/L 40.00 114 70-130 8 20 Acrylonitrile 47.4 20 ug/L 40.00 118 81-127 5 20 Benzene 23.7 0.50 ug/L 20.00 118 77-128 1 20 Bromobenzene 22.4 0.50 ug/L 20.00 112 78-129 4 20 Bromochloromethane 23.5 0.50 ug/L 20.00 118 78-135 1 20 Bromodichloromethane 23.7 0.50 ug/L 20.00 118 76-138 2 20 Bromoform 19.0 1.0 ug/L 20.00 95 71-135 2 20 Bromomethane 18.5 1.0 ug/L 20.00 92 41-168 9 20 Carbon disulfide 24.1 5.0 ug/L 20.00 120 59-135 4 20 Carbon Tetrachloride 21.8 0.50 ug/L 20.00 109 72-142 3 20 Chlorobenzene 23.2 0.50 ug/L 20.00 116 78-119 3 20 Chloroethane 21.2 0.50 ug/L 20.00 106 57-142 14 20 Chloroform 22.2 0.50 ug/L 20.00 ill 77-130 3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 0f 25 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Project: Homewood Banks Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 8020189 Time Submitted: 2/10/2018 9:55:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81130244 - 5030B LCS Dup (P8B0244-BSD1) Prepared & Analyzed: 02/13/18 Chloromethane 17.1 0.50 ug/L 20.00 85 47-145 7 20 cis-1,2-Dichloroethylene 23.6 0.50 ug/L 20.00 118 76-141 3 20 cis-1,3-Dichloropropylene 22.0 0.50 ug/L 20.00 110 65-140 3 20 Dibromochloromethane 21.0 0.50 ug/L 20.00 105 75-134 1 20 Dibromomethane 23.6 0.50 ug/L 20.00 118 76-138 0.08 20 Dichlorodifluoromethane 18.7 1.0 ug/L 20.00 93 28-163 2 20 Ethylbenzene 23.6 0.50 ug/L 20.00 118 80-127 0.9 20 Hexachlorobutadiene 22.5 2.0 ug/L 20.00 112 61-134 4 20 Isopropyl Ether 22.7 0.50 ug/L 20.00 113 60-154 2 20 Isopropylbenzene (Cumene) 23.4 0.50 ug/L 20.00 117 70-130 3 20 m,p-Xylenes 48.5 1.0 ug/L 40.00 121 77-133 2 20 Methyl Butyl Ketone (2-Hexanone) 23.2 5.0 ug/L 20.00 116 64-137 4 20 Methyl Ethyl Ketone (2-Butanone) 23.4 5.0 ug/L 20.00 117 71-134 3 20 Methyl Isobutyl Ketone 23.8 5.0 ug/L 20.00 119 69-134 2 20 Methylene Chloride 21.9 1.0 ug/L 20.00 110 73-131 3 20 Methyl-tert-Butyl Ether 23.3 0.50 ug/L 20.00 117 68-135 0.7 20 Naphthalene 21.9 1.0 ug/L 20.00 110 64-136 4 20 n-Butylbenzene 22.4 1.0 ug/L 20.00 112 68-134 4 20 n-Propylbenzene 23.9 0.50 ug/L 20.00 120 72-132 3 20 o-Xylene 23.0 0.50 ug/L 20.00 115 78-128 2 20 sec-Butylbenzene 23.3 0.50 ug/L 20.00 117 71-131 3 20 Styrene 21.3 0.50 ug/L 20.00 106 78-129 1 20 tert-Butylbenzene 22.4 0.50 ug/L 20.00 112 70-132 4 20 Tetrachloroethylene 22.9 0.50 ug/L 20.00 114 80-129 3 20 Toluene 23.5 0.50 ug/L 20.00 118 76-131 2 20 trans-1,2-Dichloroethylene 22.2 0.50 ug/L 20.00 ill 76-135 2 20 trans-1,3-Dichloropropylene 21.8 0.50 ug/L 20.00 109 67-140 1 20 Trichloroethylene 23.4 0.50 ug/L 20.00 117 77-133 3 20 Trichlorofluoromethane 23.6 0.50 ug/L 20.00 118 62-148 10 20 Vinyl acetate 25.3 2.0 ug/L 20.00 127 34-167 1 20 Vinyl chloride 20.7 0.50 ug/L 20.00 104 57-141 2 20 Surrogate:4-Bromofluorobenzene 51.2 ug/L 50.00 102 80-124 Surrogate: Dibromofluoromethane 50.1 ug/L 50.00 100 75-129 Surrogate: Toluene-d8 50.3 ug/L 50.00 101 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 25 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130204 - 3510C MS Reporting Result Limit Units Prism Work Order: 8020189 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P8B0204-BLK1) Prepared: 02/10/18 Analyzed: 02/12/18 1,2,4-Trichlorobenzene BRL 10 ug/L 1,2-Dichlorobenzene BRL 10 ug/L 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug/L 1-Methyl naphthalene BRL 10 ug/L 2,4,5-Trichlorophenol BRL 10 ug/L 2,4,6-Trichlorophenol BRL 10 ug/L 2,4-Dichlorophenol BRL 10 ug/L 2,4-Dimethylphenol BRL 10 ug/L 2,4-Dinitrophenol BRL 10 ug/L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinitrotoluene BRL 10 ug/L 2-Chloronaphthalene BRL 10 ug/L 2-Chlorophenol BRL 10 ug/L 2-Methyl naphthalene BRL 10 ug/L 2-Methylphenol BRL 10 ug/L 2-Nitroaniline BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3'-Dichlorobenzidine BRL 10 ug/L 3/4-Methyl phenol BRL 10 ug/L 3-Nitroaniline BRL 10 ug/L 4,6-Dinitro-2-methylphenol BRL 10 ug/L 4-Bromophenyl phenyl ether BRL 10 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chloroaniline BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 10 ug/L 4-Nitroaniline BRL 10 ug/L 4-Nitrophenol BRL 10 ug/L Acenaphthene BRL 10 ug/L Acenaphthylene BRL 10 ug/L Aniline BRL 10 ug/L Anthracene BRL 10 ug/L Azobenzene BRL 10 ug/L Benzo(a)anthracene BRL 10 ug/L Benzo(a)pyrene BRL 10 ug/L Benzo(b)fluoranthene BRL 10 ug/L Benzo(g,h,i)perylene BRL 10 ug/L Benzo(k)fluoranthene BRL 10 ug/L Benzoic Acid BRL 100 ug/L Benzyl alcohol BRL 10 ug/L bis(2-Chloroethoxy)methane BRL 10 ug/L Bis(2-Chloroethyl)ether BRL 10 ug/L Bis(2-chloroisopropyl)ether BRL 10 ug/L Bis(2-Ethylhexyl)phthalate BRL 10 ug/L Butyl benzyl phthalate BRL 10 ug/L Chrysene BRL 10 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 25 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Project: Homewood Banks Prism Work Order: 8020189 Attn: Roger Smith Time Submitted: 2/10/2018 9:55:OOAM 9751 Southern Pine Blvd. Charlotte, NC 28273 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81130204 - 3510C MS Blank (P8B0204-BLK1) Prepared: 02/10/18 Analyzed: 02/12/18 Dibenzo(a,h)anthracene BRL 10 ug/L Dibenzofuran BRL 10 ug/L Diethyl phthalate BRL 10 ug/L Dimethyl phthalate BRL 10 ug/L Di-n-butyl phthalate BRL 10 ug/L Di-n-octyl phthalate BRL 10 ug/L Fluoranthene BRL 10 ug/L Fluorene BRL 10 ug/L Hexachlorobenzene BRL 10 ug/L Hexachlorobutadiene BRL 10 ug/L Hexachlorocyclopentadiene BRL 10 ug/L Hexachloroethane BRL 10 ug/L Indeno(1,2,3-cd)pyrene BRL 10 ug/L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug/L N-Nitroso-di-n-propylamine BRL 10 ug/L N-Nitrosodiphenylamine BRL 10 ug/L Pentachlorophenol BRL 10 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 ug/L Surrogate: 2,4,6-Tribromophenol 79.2 ug/L 100.0 79 43-140 Surrogate:2-Fluorobiphenyl 36.7 ug/L 50.00 73 44-119 Surrogate:2-Fluorophenol 49.4 ug/L 100.0 49 19-119 Surrogate: Nitrobenzene-d5 34.9 ug/L 50.00 70 44-120 Surrogate: Phenol-d5 30.1 ug/L 100.0 30 11-52 Surrogate: Terphenyl-d14 44.2 ug/L 50.00 88 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 25 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130204 - 3510C MS Reporting Result Limit Units Prism Work Order: 8020189 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P8B0204-BS1) Prepared: 02/10/18 Analyzed: 02/12/18 1,2,4-Trichlorobenzene 26.4 10 ug/L 50.00 53 29-126 1,2-Dichlorobenzene 25.8 10 ug/L 50.00 52 32-111 1,3-Dichlorobenzene 24.6 10 ug/L 50.00 49 28-110 1,4-Dichlorobenzene 24.5 10 ug/L 50.00 49 29-112 1-Methyl naphthalene 32.2 10 ug/L 50.00 64 41-119 2,4,5-Trichlorophenol 36.1 10 ug/L 50.00 72 53-123 2,4,6-Trichlorophenol 35.4 10 ug/L 50.00 71 50-125 2,4-Dichlorophenol 34.6 10 ug/L 50.00 69 47-121 2,4-Dimethylphenol 34.6 10 ug/L 50.00 69 31-124 2,4-Dinitrophenol 35.0 10 ug/L 50.00 70 23-143 2,4-Dinitrotoluene 34.5 10 ug/L 50.00 69 57-128 2,6-Dinitrotoluene 36.2 10 ug/L 50.00 72 57-124 2-Chloronaphthalene 31.7 10 ug/L 50.00 63 40-116 2-Chlorophenol 32.7 10 ug/L 50.00 65 38-117 2-Methyl naphthalene 30.0 10 ug/L 50.00 60 40-121 2-Methylphenol 31.3 10 ug/L 50.00 63 30-117 2-Nitroaniline 33.1 10 ug/L 50.00 66 55-127 2-Nitrophenol 34.1 10 ug/L 50.00 68 47-123 3,3'-Dichlorobenzidine 43.5 10 ug/L 50.00 87 27-129 3/4-Methyl phenol 25.1 10 ug/L 50.00 50 29-110 3-Nitroaniline 34.3 10 ug/L 50.00 69 41-128 4,6-Dinitro-2-methylphenol 34.5 10 ug/L 50.00 69 44-137 4-Bromophenyl phenyl ether 34.9 10 ug/L 50.00 70 55-124 4-Chloro-3-methylphenol 33.8 10 ug/L 50.00 68 52-119 4-Chloroaniline 37.6 10 ug/L 50.00 75 33-117 4-Chlorophenyl phenyl ether 33.4 10 ug/L 50.00 67 53-121 4-Nitroaniline 31.8 10 ug/L 50.00 64 45-135 4-Nitrophenol 13.9 10 ug/L 50.00 28 10-77 Acenaphthene 33.7 10 ug/L 50.00 67 47-122 Acenaphthylene 35.8 10 ug/L 50.00 72 41-130 Aniline 58.3 10 ug/L 50.00 117 12-197 Anthracene 38.9 10 ug/L 50.00 78 57-123 Azobenzene 33.8 10 ug/L 50.00 68 61-116 Benzo(a)anthracene 38.8 10 ug/L 50.00 78 58-125 Benzo(a)pyrene 37.8 10 ug/L 50.00 76 54-128 Benzo(b)fluoranthene 38.6 10 ug/L 50.00 77 53-131 Benzo(g,hJ)perylene 37.2 10 ug/L 50.00 74 50-134 Benzo(k)fluoranthene 40.6 10 ug/L 50.00 81 57-129 Benzoic Acid 7.16 100 ug/L 50.00 14 10-125 J Benzyl alcohol 27.0 10 ug/L 50.00 54 31-112 bis(2-Chloroethoxy)methane 33.9 10 ug/L 50.00 68 48-120 Bis(2-Chloroethyl)ether 32.2 10 ug/L 50.00 64 43-118 Bis(2-chloroisopropyl)ether 28.3 10 ug/L 50.00 57 37-130 Bis(2-Ethylhexyl)phthalate 37.9 10 ug/L 50.00 76 55-135 Butyl benzyl phthalate 34.8 10 ug/L 50.00 70 53-134 Chrysene 37.5 10 ug/L 50.00 75 59-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 0f 25 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Project: Homewood Banks Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130204 - 3510C MS Reporting Result Limit Units Prism Work Order: 8020189 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P8B0204-BSI) Prepared: 02/10/18 Analyzed: 02/12/18 Dibenzo(a,h)anthracene 20.2 10 ug/L 50.00 40 51-134 L Dibenzofuran 32.9 10 ug/L 50.00 66 53-118 Diethyl phthalate 34.9 10 ug/L 50.00 70 56-125 Dimethyl phthalate 34.7 10 ug/L 50.00 69 45-127 Di-n-butyl phthalate 36.9 10 ug/L 50.00 74 59-127 Di-n-octyl phthalate 37.3 10 ug/L 50.00 75 51-140 Fluoranthene 38.3 10 ug/L 50.00 77 57-128 Fluorene 34.2 10 ug/L 50.00 68 52-124 Hexachlorobenzene 36.0 10 ug/L 50.00 72 53-125 Hexachlorobutadiene 23.6 10 ug/L 50.00 47 22-124 Hexachlorocyclopentadiene 26.9 10 ug/L 50.00 54 32-117 Hexachloroethane 21.8 10 ug/L 50.00 44 21-115 Indeno(1,2,3-cd)pyrene 41.4 10 ug/L 50.00 83 52-134 Isophorone 33.0 10 ug/L 50.00 66 42-124 Naphthalene 30.5 10 ug/L 50.00 61 40-121 Nitrobenzene 27.8 10 ug/L 50.00 56 45-121 N-Nitroso-di-n-propylamine 30.1 10 ug/L 50.00 60 49-119 N-Nitrosodiphenylamine 44.0 10 ug/L 50.00 88 51-123 Pentachlorophenol 44.2 10 ug/L 50.00 88 35-138 Phenanthrene 38.3 10 ug/L 50.00 77 59-120 Phenol 16.8 10 ug/L 50.00 34 12-58 Pyrene 39.7 10 ug/L 50.00 79 57-126 Surrogate: 2,4,6-Tribromophenol 80.9 ug/L 100.0 81 43-140 Surrogate:2-Fluorobiphenyl 34.8 ug/L 50.00 70 44-119 Surrogate:2-Fluorophenol 47.3 ug/L 100.0 47 19-119 Surrogate: Nitrobenzene-d5 31.7 ug/L 50.00 63 44-120 Surrogate: Phenol-d5 29.5 ug/L 100.0 29 11-52 Surrogate: Terphenyl-d14 40.3 ug/L 50.00 81 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 25 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130204 - 3510C MS Reporting Result Limit Units Prism Work Order: 8020189 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P8B0204-BSD1) Prepared: 02/10/18 Analyzed: 02/12/18 1,2,4-Trichlorobenzene 26.5 10 ug/L 50.00 53 29-126 0.3 20 1,2-Dichlorobenzene 25.3 10 ug/L 50.00 51 32-111 2 20 1,3-Dichlorobenzene 24.2 10 ug/L 50.00 48 28-110 1 20 1,4-Dichlorobenzene 24.3 10 ug/L 50.00 49 29-112 0.6 20 1-Methyl naphthalene 31.9 10 ug/L 50.00 64 41-119 0.9 20 2,4,5-Trichlorophenol 36.5 10 ug/L 50.00 73 53-123 1 20 2,4,6-Trichlorophenol 34.6 10 ug/L 50.00 69 50-125 2 20 2,4-Dichlorophenol 35.8 10 ug/L 50.00 72 47-121 3 20 2,4-Dimethylphenol 37.2 10 ug/L 50.00 74 31-124 7 20 2,4-Dinitrophenol 33.1 10 ug/L 50.00 66 23-143 5 20 2,4-Dinitrotoluene 33.9 10 ug/L 50.00 68 57-128 2 20 2,6-Dinitrotoluene 35.8 10 ug/L 50.00 72 57-124 1 20 2-Chloronaphthalene 30.6 10 ug/L 50.00 61 40-116 4 20 2-Chlorophenol 34.1 10 ug/L 50.00 68 38-117 4 20 2-Methyl naphthalene 30.1 10 ug/L 50.00 60 40-121 0.2 20 2-Methylphenol 32.3 10 ug/L 50.00 65 30-117 3 20 2-Nitroaniline 32.6 10 ug/L 50.00 65 55-127 2 20 2-Nitrophenol 35.4 10 ug/L 50.00 71 47-123 4 20 3,3'-Dichlorobenzidine 43.8 10 ug/L 50.00 88 27-129 0.7 20 3/4-Methyl phenol 25.5 10 ug/L 50.00 51 29-110 1 20 3-Nitroaniline 33.1 10 ug/L 50.00 66 41-128 4 20 4,6-Dinitro-2-methylphenol 34.1 10 ug/L 50.00 68 44-137 1 20 4-Bromophenyl phenyl ether 33.8 10 ug/L 50.00 68 55-124 3 20 4-Chloro-3-methylphenol 34.4 10 ug/L 50.00 69 52-119 2 20 4-Chloroaniline 38.4 10 ug/L 50.00 77 33-117 2 20 4-Chlorophenyl phenyl ether 32.2 10 ug/L 50.00 64 53-121 4 20 4-Nitroaniline 31.4 10 ug/L 50.00 63 45-135 1 20 4-Nitrophenol 13.7 10 ug/L 50.00 27 10-77 2 20 Acenaphthene 33.2 10 ug/L 50.00 66 47-122 2 20 Acenaphthylene 34.3 10 ug/L 50.00 69 41-130 4 20 Aniline 63.1 10 ug/L 50.00 126 12-197 8 20 Anthracene 38.2 10 ug/L 50.00 76 57-123 2 20 Azobenzene 33.4 10 ug/L 50.00 67 61-116 1 20 Benzo(a)anthracene 38.3 10 ug/L 50.00 77 58-125 1 20 Benzo(a)pyrene 37.0 10 ug/L 50.00 74 54-128 2 20 Benzo(b)fluoranthene 37.2 10 ug/L 50.00 74 53-131 4 20 Benzo(g,hJ)perylene 36.3 10 ug/L 50.00 73 50-134 2 20 Benzo(k)fluoranthene 39.1 10 ug/L 50.00 78 57-129 4 20 Benzoic Acid 7.66 100 ug/L 50.00 15 10-125 7 20 J Benzyl alcohol 27.7 10 ug/L 50.00 55 31-112 2 20 bis(2-Chloroethoxy)methane 34.9 10 ug/L 50.00 70 48-120 3 20 Bis(2-Chloroethyl)ether 33.1 10 ug/L 50.00 66 43-118 3 20 Bis(2-chloroisopropyl)ether 29.0 10 ug/L 50.00 58 37-130 2 20 Bis(2-Ethylhexyl)phthalate 37.6 10 ug/L 50.00 75 55-135 0.9 20 Butyl benzyl phthalate 34.4 10 ug/L 50.00 69 53-134 1 20 Chrysene 36.8 10 ug/L 50.00 74 59-123 2 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 0f 25 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Project: Homewood Banks Prism Work Order: 8020189 Attn: Roger Smith Time Submitted: 2/10/2018 9:55:OOAM 9751 Southern Pine Blvd. Charlotte, NC 28273 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81130204 - 3510C MS LCS Dup (P8130204-13SD1) Prepared: 02/10/18 Analyzed: 02/12/18 Dibenzo(a,h)anthracene 19.7 10 ug/L 50.00 39 51-134 2 20 L Dibenzofuran 32.5 10 ug/L 50.00 65 53-118 1 20 Diethyl phthalate 32.9 10 ug/L 50.00 66 56-125 6 20 Dimethyl phthalate 33.6 10 ug/L 50.00 67 45-127 3 20 Di-n-butyl phthalate 35.8 10 ug/L 50.00 72 59-127 3 20 Di-n-octyl phthalate 36.5 10 ug/L 50.00 73 51-140 2 20 Fluoranthene 37.0 10 ug/L 50.00 74 57-128 4 20 Fluorene 33.2 10 ug/L 50.00 66 52-124 3 20 Hexachlorobenzene 35.2 10 ug/L 50.00 70 53-125 2 20 Hexachlorobutadiene 23.8 10 ug/L 50.00 48 22-124 1 20 Hexachlorocyclopentadiene 26.0 10 ug/L 50.00 52 32-117 3 20 Hexachloroethane 21.3 10 ug/L 50.00 43 21-115 3 20 Indeno(1,2,3-cd)pyrene 40.6 10 ug/L 50.00 81 52-134 2 20 Isophorone 33.8 10 ug/L 50.00 68 42-124 2 20 Naphthalene 31.1 10 ug/L 50.00 62 40-121 2 20 Nitrobenzene 29.2 10 ug/L 50.00 58 45-121 5 20 N-Nitroso-di-n-propylamine 30.9 10 ug/L 50.00 62 49-119 3 20 N-Nitrosodiphenylamine 43.0 10 ug/L 50.00 86 51-123 3 20 Pentachlorophenol 43.3 10 ug/L 50.00 87 35-138 2 20 Phenanthrene 37.6 10 ug/L 50.00 75 59-120 2 20 Phenol 17.2 10 ug/L 50.00 34 12-58 3 20 Pyrene 39.2 10 ug/L 50.00 78 57-126 1 20 Surrogate: 2,4,6-Tribromophenol 78.2 ug/L 100.0 78 43-140 Surrogate:2-Fluorobiphenyl 36.2 ug/L 50.00 72 44-119 Surrogate:2-Fluorophenol 51.2 ug/L 100.0 51 19-119 Surrogate: Nitrobenzene-d5 33.9 ug/L 50.00 68 44-120 Surrogate: Phenol-d5 30.8 ug/L 100.0 31 11-52 Surrogate: Terphenyl-d14 39.7 ug/L 50.00 79 50-134 Sample Extraction Data Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 8020189-01 P860204 950 mL 1 mL 02/10/18 10:45 8020189-02 P8130204 950 mL 1 mL 02/10/18 10:45 Prep Method: 5030E Lab Number Batch Initial Final Date/Time 8020189-01 P8130244 10 mL 10 mL 02/13/18 10:39 8020189-02 P860244 10 mL 10 mL 02/13/18 10:39 8020189-03 P8130244 10 mL 10 mL 02/13/18 10:39 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 25 LU 0 m LU z 0 1 5 LU S xl m � T y � u] ` O .O ❑ OQ C W O Q5 d ❑ ® Ti 0 a O C Hpo M p O X 0� C✓ ❑ ul a N�®� 98 ® 10 L zo N Cl ® N -9 C IOU vs 1 Cl ® m � � ® ® a6 o o r �a �S2 ® ® ❑ N Q2 a cu®o A �NLU 0- S E ® N a LU y g aN o Um, UU2 M a ® E c � � cc Q W Z,� b { E Z ,,g, z a LL, LU 0 z ® z. 4 uu LU x ®aa� . - w NE �3 cl LU E M� MOM im a® 0E ®� 5 'N z E zL) �� 5 •� �® u a� co �� 1 Case Narrative PRISM `,. LABORATORIES, INC. S&ME, Inc - Charlotte Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 NC Certification No. 402 Full -Service Analytical & NC Drinking Water Cert No. 37735 Environmental Solutions SC Certification No. 99012 Project: Homewood Banks Lab Submittal Date: 02/10/2018 Prism Work Order: 8020190 02/14/2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A. Jones President/Project Manager Data Qualifiers Key Reference: D RPD value outside of the control limits. M Matrix spike outside of the control limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Reviewed By Robbi A. Jones President/Project Manager * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 67 /P R I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Sample Receipt Summary 02/14/2018 Prism Work Order: 8020190 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received UST-1 (17.5-20) 8020190-01 Solid 02/08/18 02/10/18 UST-2 (12.5-15) 8020190-02 Solid 02/08/18 02/10/18 UST-3 (7.5-10) 8020190-03 Solid 02/08/18 02/10/18 UST-4 (2.5-3) 8020190-04 Solid 02/09/18 02/10/18 UST-4 (7.5-10) 8020190-05 Solid 02/08/18 02/10/18 UST-4 (12-14) 8020190-06 Solid 02/09/18 02/10/18 UST-5 (2.5-3) 8020190-07 Solid 02/09/18 02/10/18 UST-6 (2.5-3) 8020190-08 Solid 02/09/18 02/10/18 UST-6 (7.5-10) 8020190-09 Solid 02/08/18 02/10/18 Background (2.5-3) 8020190-10 Solid 02/09/18 02/10/18 Background (7.5-10) 8020190-11 Solid 02/09/18 02/10/18 Soil-Dup-1 8020190-12 Solid 02/08/18 02/10/18 Samples were received in good condition at 3.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 67 P R I S M Full Service Analytical & Environmental Solutions LABORATORIES, INC. Summary of Detections 02/14/2018 Prism Work Order: 8020190 Prism ID Client ID Parameter Method Result Units 8020190-01 UST-1 (17.5-20) Barium '6020B 82 mg/kg dry 8020190-01 UST-1 (17.5-20) Chromium *6020B 1.5 mg/kg dry 8020190-01 UST-1 (17.5-20) Lead *6020B 3.4 mg/kg dry 8020190-01 UST-1 (17.5-20) Selenium `6020B 0.72 mg/kg dry 8020190-02 UST-2 (12.5-15) Barium '6020B 81 mg/kg dry 8020190-02 UST-2 (12.5-15) Chromium *6020B 1.3 mg/kg dry 8020190-02 UST-2 (12.5-15) Lead *6020B 3.8 mg/kg dry 8020190-02 UST-2 (12.5-15) Selenium '6020B 0.71 mg/kg dry 8020190-03 UST-3 (7.5-10) Barium "6020B 57 mg/kg dry 8020190-03 UST-3 (7.5-10) Chromium *6020B 1.0 mg/kg dry 8020190-03 UST-3 (7.5-10) Lead `6020B 4.9 mg/kg dry 8020190-03 UST-3 (7.5-10) Selenium '6020B 0.82 mg/kg dry 8020190-04 UST-4 (2.5-3) Barium "6020B 61 mg/kg dry 8020190-04 UST-4 (2.5-3) Chromium `602013 1.4 mg/kg dry 8020190-04 UST-4 (2.5-3) Lead '6020B 8.3 mg/kg dry 8020190-04 UST-4 (2.5-3) Acetone *8260B 0.077 mg/kg dry 8020190-05 UST-4 (7.5-10) Arsenic '6020B 0.86 mg/kg dry 8020190-05 UST-4 (7.5-10) Barium '6020B 66 mg/kg dry 8020190-05 UST-4 (7.5-10) Chromium *6020B 1.1 mg/kg dry 8020190-05 UST-4 (7.5-10) Lead "6020B 4.1 mg/kg dry 8020190-05 UST-4 (7.5-10) Selenium `6020B 1.0 mg/kg dry 8020190-06 UST-4 (12-14) Barium '6020B 95 mg/kg dry 8020190-06 UST-4 (12-14) Chromium "6020B 2.3 mg/kg dry 8020190-06 UST-4 (12-14) Lead `6020B 3.4 mg/kg dry 8020190-06 UST-4 (12-14) Selenium '6020B 0.97 mg/kg dry 8020190-07 UST-5 (2.5-3) Barium *6020B 92 mg/kg dry 8020190-07 UST-5 (2.5-3) Chromium "6020B 1.4 mg/kg dry 8020190-07 UST-5 (2.5-3) Lead `6020B 7.7 mg/kg dry 8020190-07 UST-5 (2.5-3) Selenium '6020B 0.96 mg/kg dry 8020190-08 UST-6 (2.5-3) Mercury *7471 B 0.042 mg/kg dry 8020190-08 UST-6 (2.5-3) Arsenic `6020B 4.3 mg/kg dry 8020190-08 UST-6 (2.5-3) Barium '6020B 49 mg/kg dry 8020190-08 UST-6 (2.5-3) Chromium *6020B 29 mg/kg dry 8020190-08 UST-6 (2.5-3) Lead "6020B 18 mg/kg dry 8020190-08 UST-6 (2.5-3) Selenium `6020B 0.88 mg/kg dry 8020190-08 UST-6 (2.5-3) 4-Isopropyltoluene '8260B 0.0055 mg/kg dry 8020190-08 UST-6 (2.5-3) Acetone "8260B 0.13 mg/kg dry 8020190-09 UST-6 (7.5-10) Barium `602013 160 mg/kg dry 8020190-09 UST-6 (7.5-10) Chromium '6020B 1.5 mg/kg dry 8020190-09 UST-6 (7.5-10) Lead "6020B 4.8 mg/kg dry 8020190-09 UST-6 (7.5-10) Selenium '6020B 0.62 mg/kg dry 8020190-09 UST-6 (7.5-10) Acetone `8260B 0.11 mg/kg dry 8020190-10 Background(2.5-3) Mercury *7471B 0.028 mg/kg dry 8020190-10 Background (2.5-3) Arsenic "6020B 1.9 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 67 /,GA1P-R I S M Full -Service Analytical Environmental Solutions LABORATORIES, ING Summary of Detections 02/14/2018 Prism Work Order: 8020190 Prism ID Client ID Parameter Method Result Units 8020190-10 Background (2.5-3) Barium "6020B 170 mg/kg dry 8020190-10 Background (2.5-3) Chromium *6020B 17 mg/kg dry 8020190-10 Background (2.5-3) Lead `6020B 16 mg/kg dry 8020190-10 Background (2.5-3) Selenium '6020B 1.6 mg/kg dry 8020190-11 Background (7.5-10) Barium *6020B 240 mg/kg dry 8020190-11 Background (7.5-10) Chromium *602013 24 mg/kg dry 8020190-11 Background (7.5-10) Lead '6020B 6.0 mg/kg dry 8020190-11 Background (7.5-10) Selenium "6020B 1.4 mg/kg dry 8020190-11 Background (7.5-10) Silver *6020B 0.14 mg/kg dry 8020190-12 Soil-Dup-1 Arsenic '6020B 0.85 mg/kg dry 8020190-12 Soil-Dup-1 Barium *6020B 77 mg/kg dry 8020190-12 Soil-Dup-1 Chromium *6020B 1.2 mg/kg dry 8020190-12 Soil-Dup-1 Lead `6020B 4.6 mg/kg dry 8020190-12 Soil-Dup-1 Selenium '6020B 1.2 mg/kg dry 8020190-12 Soil-Dup-1 Acetone *8260B 0.058 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-1 (17.5-20) Attn: Roger Smith Prism Sample ID: 8020190-01 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 13:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 91.6 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.36 0.056 1 *8270D 2/13/18 17:39 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 17:39 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 17:39 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 17:39 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.36 0.069 1 *8270D 2/13/18 17:39 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.36 0.067 1 *8270D 2/13/18 17:39 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.36 0.070 1 *8270D 2/13/18 17:39 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 17:39 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 17:39 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 17:39 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 17:39 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 17:39 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 17:39 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.36 0.058 1 *8270D 2/13/18 17:39 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.36 0.046 1 *8270D 2/13/18 17:39 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.36 0.065 1 *8270D 2/13/18 17:39 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.36 0.071 1 *8270D 2/13/18 17:39 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 17:39 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.36 0.054 1 *8270D 2/13/18 17:39 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.36 0.062 1 *8270D 2/13/18 17:39 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 17:39 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.36 0.043 1 *8270D 2/13/18 17:39 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 17:39 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 17:39 JMV P8130242 Acenaphthene BRL mg/kg dry 0.36 0.049 1 *8270D 2/13/18 17:39 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 17:39 JMV P8130242 Anthracene BRL mg/kg dry 0.36 0.058 1 *8270D 2/13/18 17:39 JMV P8130242 Azobenzene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 17:39 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 17:39 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.36 0.039 1 *8270D 2/13/18 17:39 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.36 0.042 1 *8270D 2/13/18 17:39 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.36 0.039 1 *8270D 2/13/18 17:39 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 17:39 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.36 0.030 1 *8270D 2/13/18 17:39 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 17:39 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.36 0.062 1 *8270D 2/13/18 17:39 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 17:39 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.36 0.061 1 *8270D 2/13/18 17:39 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 17:39 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-1 (17.5-20) Attn: Roger Smith Prism Sample ID: 8020190-01 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 13:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 17:39 JMV P8130242 Chrysene BRL mg/kg dry 0.36 0.045 1 *8270D 2/13/18 17:39 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 17:39 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 17:39 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 17:39 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 17:39 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 17:39 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 17:39 JMV P8130242 Fluoranthene BRL mg/kg dry 0.36 0.046 1 *8270D 2/13/18 17:39 JMV P8130242 Fluorene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 17:39 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.36 0.057 1 *8270D 2/13/18 17:39 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.36 0.065 1 *8270D 2/13/18 17:39 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.36 0.064 1 *8270D 2/13/18 17:39 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.36 0.060 1 *8270D 2/13/18 17:39 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.36 0.041 1 *8270D 2/13/18 17:39 JMV P8130242 Isophorone BRL mg/kg dry 0.36 0.049 1 *8270D 2/13/18 17:39 JMV P8130242 Naphthalene BRL mg/kg dry 0.36 0.058 1 *8270D 2/13/18 17:39 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 17:39 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.36 0.057 1 *8270D 2/13/18 17:39 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 17:39 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.36 0.043 1 *8270D 2/13/18 17:39 JMV P8130242 Phenanthrene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 17:39 JMV P8130242 Phenol BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 17:39 JMV P8130242 Pyrene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 17:39 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 82 % 39-132 2-Fluorobiphenyl 87 % 44-115 2-Fluorophenol 78 % 35-115 Nitrobenzene-d5 79 % 37-122 Phenol-d5 79 % 34-121 Terphenyl-d14 84 % 54-127 Total Metals Mercury BRL mg/kg dry 0.023 0.0022 1 *7471 B 2/13/18 13:44 JAB P8130233 Arsenic BRL mg/kg dry 0.82 0.075 5 *6020B 2/13/18 22:04 EGC P8130232 Barium 82 mg/kg dry 5.5 0.033 5 *6020B 2/13/18 22:04 EGC P8130232 Cadmium BRL mg/kg dry 0.14 0.010 5 *6020B 2/13/18 22:04 EGC P8130232 Chromium 1.5 mg/kg dry 0.27 0.015 5 *6020B 2/13/18 22:04 EGC 1128130232 Lead 3.4 mg/kg dry 0.14 0.031 5 *6020B 2/13/18 22:04 EGC 1128130232 Selenium 0.72 mg/kg dry 0.55 0.11 5 *6020B 2/13/18 22:04 EGC P8130232 Silver BRL mg/kg dry 0.14 0.010 5 *6020B 2/13/18 22:04 EGC P8130232 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0061 0.00050 1 *8260B 2/12/18 12:55 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: UST-1 (17.5-20) Prism Sample ID: 8020190-01 Prism Work Order: 8020190 Time Collected: 02/08/18 13:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1-Trichloroethane BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 12:55 ANG P8130215 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0061 0.00041 1 *8260B 2/12/18 12:55 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0061 0.00054 1 *8260B 2/12/18 12:55 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0061 0.00017 1 *8260B 2/12/18 12:55 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0061 0.00027 1 *8260B 2/12/18 12:55 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0061 0.00033 1 *8260B 2/12/18 12:55 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0061 0.00035 1 *8260B 2/12/18 12:55 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0061 0.00078 1 *8260B 2/12/18 12:55 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0061 0.00045 1 *8260B 2/12/18 12:55 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0061 0.00046 1 *8260B 2/12/18 12:55 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0061 0.00024 1 *8260B 2/12/18 12:55 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 12:55 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 12:55 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0061 0.00038 1 *8260B 2/12/18 12:55 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0061 0.00046 1 *8260B 2/12/18 12:55 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0061 0.00040 1 *8260B 2/12/18 12:55 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0061 0.00031 1 *8260B 2/12/18 12:55 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0061 0.00024 1 *8260B 2/12/18 12:55 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 12:55 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0061 0.00031 1 *8260B 2/12/18 12:55 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 12:55 ANG P8130215 4-Isopropyltoluene BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 12:55 ANG P8130215 Acetone BRL mg/kg dry 0.061 0.0015 1 *8260B 2/12/18 12:55 ANG P8130215 Benzene BRL mg/kg dry 0.0036 0.00035 1 *8260B 2/12/18 12:55 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0061 0.00051 1 *8260B 2/12/18 12:55 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0061 0.00033 1 *8260B 2/12/18 12:55 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0061 0.00034 1 *8260B 2/12/18 12:55 ANG P8130215 Bromoform BRL mg/kg dry 0.0061 0.00069 1 *8260B 2/12/18 12:55 ANG P8130215 Bromomethane BRL mg/kg dry 0.012 0.00075 1 *8260B 2/12/18 12:55 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0061 0.00030 1 *8260B 2/12/18 12:55 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0061 0.00032 1 *8260B 2/12/18 12:55 ANG P8130215 Chloroethane BRL mg/kg dry 0.012 0.00051 1 *8260B 2/12/18 12:55 ANG P8130215 Chloroform BRL mg/kg dry 0.0061 0.00044 1 *8260B 2/12/18 12:55 ANG P8130215 Chloromethane BRL mg/kg dry 0.0061 0.00041 1 *8260B 2/12/18 12:55 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0061 0.00026 1 *8260B 2/12/18 12:55 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0061 0.00020 1 *8260B 2/12/18 12:55 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0061 0.00025 1 *8260B 2/12/18 12:55 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0061 0.00028 1 *8260B 2/12/18 12:55 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0061 0.00023 1 *8260B 2/12/18 12:55 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0061 0.00025 1 *8260B 2/12/18 12:55 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 12:55 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.012 0.00056 1 *8260B 2/12/18 12:55 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.061 0.00055 1 *8260B 2/12/18 12:55 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-1 (17.5-20) Attn: Roger Smith Prism Sample ID: 8020190-01 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 13:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.12 0.00055 1 *8260B 2/12/18 12:55 ANG P8130215 Methyl Isobutyl Ketone BRL mg/kg dry 0.061 0.00052 1 *8260B 2/12/18 12:55 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.012 0.00034 1 *8260B 2/12/18 12:55 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.012 0.00019 1 *8260B 2/12/18 12:55 ANG P8130215 Naphthalene BRL mg/kg dry 0.012 0.00019 1 *8260B 2/12/18 12:55 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0061 0.00031 1 *8260B 2/12/18 12:55 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 12:55 ANG P8130215 o-Xylene BRL mg/kg dry 0.0061 0.00025 1 *8260B 2/12/18 12:55 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 12:55 ANG P8130215 Styrene BRL mg/kg dry 0.0061 0.00037 1 *8260B 2/12/18 12:55 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0061 0.00021 1 *8260B 2/12/18 12:55 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 12:55 ANG P8130215 Toluene BRL mg/kg dry 0.0061 0.00035 1 *8260B 2/12/18 12:55 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 12:55 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0061 0.00032 1 *8260B 2/12/18 12:55 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0061 0.00039 1 *8260B 2/12/18 12:55 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0061 0.00039 1 *8260B 2/12/18 12:55 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.030 0.00083 1 *8260B 2/12/18 12:55 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 12:55 ANG P8130215 Xylenes, total BRL mg/kg dry 0.018 0.0011 1 *8260B 2/12/18 12:55 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 103 % 70-130 Dibromofluoromethane 100 % 84-123 Toluene-d8 93 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-2 (12.5-15) Attn: Roger Smith Prism Sample ID: 8020190-02 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 14:15 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 91.8 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.36 0.056 1 *8270D 2/13/18 18:01 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.36 0.054 1 *8270D 2/13/18 18:01 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:01 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 18:01 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.36 0.069 1 *8270D 2/13/18 18:01 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.36 0.067 1 *8270D 2/13/18 18:01 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.36 0.069 1 *8270D 2/13/18 18:01 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 18:01 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 18:01 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 18:01 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 18:01 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 18:01 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:01 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.36 0.057 1 *8270D 2/13/18 18:01 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.36 0.046 1 *8270D 2/13/18 18:01 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.36 0.065 1 *8270D 2/13/18 18:01 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.36 0.071 1 *8270D 2/13/18 18:01 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 18:01 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.36 0.054 1 *8270D 2/13/18 18:01 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.36 0.062 1 *8270D 2/13/18 18:01 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 18:01 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.36 0.043 1 *8270D 2/13/18 18:01 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:01 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 18:01 JMV P8130242 Acenaphthene BRL mg/kg dry 0.36 0.049 1 *8270D 2/13/18 18:01 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 18:01 JMV P8130242 Anthracene BRL mg/kg dry 0.36 0.058 1 *8270D 2/13/18 18:01 JMV P8130242 Azobenzene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:01 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:01 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.36 0.039 1 *8270D 2/13/18 18:01 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.36 0.042 1 *8270D 2/13/18 18:01 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.36 0.039 1 *8270D 2/13/18 18:01 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:01 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.36 0.030 1 *8270D 2/13/18 18:01 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:01 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.36 0.062 1 *8270D 2/13/18 18:01 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:01 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.36 0.061 1 *8270D 2/13/18 18:01 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 18:01 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-2 (12.5-15) Attn: Roger Smith Prism Sample ID: 8020190-02 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 14:15 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:01 JMV P8130242 Chrysene BRL mg/kg dry 0.36 0.045 1 *8270D 2/13/18 18:01 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 18:01 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 18:01 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.36 0.049 1 *8270D 2/13/18 18:01 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:01 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:01 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 18:01 JMV P8130242 Fluoranthene BRL mg/kg dry 0.36 0.046 1 *8270D 2/13/18 18:01 JMV P8130242 Fluorene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 18:01 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.36 0.057 1 *8270D 2/13/18 18:01 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.36 0.064 1 *8270D 2/13/18 18:01 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.36 0.064 1 *8270D 2/13/18 18:01 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.36 0.060 1 *8270D 2/13/18 18:01 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.36 0.041 1 *8270D 2/13/18 18:01 JMV P8130242 Isophorone BRL mg/kg dry 0.36 0.049 1 *8270D 2/13/18 18:01 JMV P8130242 Naphthalene BRL mg/kg dry 0.36 0.058 1 *8270D 2/13/18 18:01 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:01 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.36 0.057 1 *8270D 2/13/18 18:01 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 18:01 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.36 0.042 1 *8270D 2/13/18 18:01 JMV P8130242 Phenanthrene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:01 JMV P8130242 Phenol BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 18:01 JMV P8130242 Pyrene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 18:01 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 80 % 39-132 2-Fluorobiphenyl 86 % 44-115 2-Fluorophenol 77 % 35-115 Nitrobenzene-d5 77 % 37-122 Phenol-d5 78 % 34-121 Terphenyl-d14 84 % 54-127 Total Metals Mercury BRL mg/kg dry 0.021 0.0020 1 *7471 B 2/13/18 13:49 JAB P8130233 Arsenic BRL mg/kg dry 0.80 0.073 5 *6020B 2/13/18 22:28 EGC P8130232 Barium 81 mg/kg dry 5.3 0.033 5 *6020B 2/13/18 22:28 EGC P8130232 Cadmium BRL mg/kg dry 0.13 0.010 5 *6020B 2/13/18 22:28 EGC P8130232 Chromium 1.3 mg/kg dry 0.27 0.015 5 *6020B 2/13/18 22:28 EGC 1128130232 Lead 3.8 mg/kg dry 0.13 0.030 5 *6020B 2/13/18 22:28 EGC 1128130232 Selenium 0.71 mg/kg dry 0.53 0.11 5 *6020B 2/13/18 22:28 EGC P8130232 Silver BRL mg/kg dry 0.13 0.010 5 *6020B 2/13/18 22:28 EGC P8130232 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0058 0.00048 1 *8260B 2/12/18 13:23 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: UST-2 (12.5-15) Prism Sample ID: 8020190-02 Prism Work Order: 8020190 Time Collected: 02/08/18 14:15 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1-Trichloroethane BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 13:23 ANG P8130215 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0058 0.00040 1 *8260B 2/12/18 13:23 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0058 0.00052 1 *8260B 2/12/18 13:23 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0058 0.00016 1 *8260B 2/12/18 13:23 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0058 0.00026 1 *8260B 2/12/18 13:23 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0058 0.00032 1 *8260B 2/12/18 13:23 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0058 0.00033 1 *8260B 2/12/18 13:23 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0058 0.00075 1 *8260B 2/12/18 13:23 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0058 0.00044 1 *8260B 2/12/18 13:23 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0058 0.00045 1 *8260B 2/12/18 13:23 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 13:23 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0058 0.00027 1 *8260B 2/12/18 13:23 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 13:23 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0058 0.00036 1 *8260B 2/12/18 13:23 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0058 0.00044 1 *8260B 2/12/18 13:23 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0058 0.00039 1 *8260B 2/12/18 13:23 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0058 0.00029 1 *8260B 2/12/18 13:23 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0058 0.00023 1 *8260B 2/12/18 13:23 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 13:23 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0058 0.00030 1 *8260B 2/12/18 13:23 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 13:23 ANG P8130215 4-Isopropyltoluene BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 13:23 ANG P8130215 Acetone BRL mg/kg dry 0.058 0.0014 1 *8260B 2/12/18 13:23 ANG P8130215 Benzene BRL mg/kg dry 0.0035 0.00034 1 *8260B 2/12/18 13:23 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0058 0.00049 1 *8260B 2/12/18 13:23 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0058 0.00032 1 *8260B 2/12/18 13:23 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0058 0.00033 1 *8260B 2/12/18 13:23 ANG P8130215 Bromoform BRL mg/kg dry 0.0058 0.00066 1 *8260B 2/12/18 13:23 ANG P8130215 Bromomethane BRL mg/kg dry 0.012 0.00072 1 *8260B 2/12/18 13:23 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0058 0.00029 1 *8260B 2/12/18 13:23 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0058 0.00031 1 *8260B 2/12/18 13:23 ANG P8130215 Chloroethane BRL mg/kg dry 0.012 0.00049 1 *8260B 2/12/18 13:23 ANG P8130215 Chloroform BRL mg/kg dry 0.0058 0.00042 1 *8260B 2/12/18 13:23 ANG P8130215 Chloromethane BRL mg/kg dry 0.0058 0.00039 1 *8260B 2/12/18 13:23 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0058 0.00025 1 *8260B 2/12/18 13:23 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0058 0.00020 1 *8260B 2/12/18 13:23 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 13:23 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0058 0.00027 1 *8260B 2/12/18 13:23 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0058 0.00022 1 *8260B 2/12/18 13:23 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 13:23 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 13:23 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.012 0.00054 1 *8260B 2/12/18 13:23 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.058 0.00053 1 *8260B 2/12/18 13:23 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-2 (12.5-15) Attn: Roger Smith Prism Sample ID: 8020190-02 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 14:15 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.12 0.00053 1 *8260B 2/12/18 13:23 ANG P8130215 Methyl Isobutyl Ketone BRL mg/kg dry 0.058 0.00050 1 *8260B 2/12/18 13:23 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.012 0.00033 1 *8260B 2/12/18 13:23 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.012 0.00019 1 *8260B 2/12/18 13:23 ANG P8130215 Naphthalene BRL mg/kg dry 0.012 0.00018 1 *8260B 2/12/18 13:23 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0058 0.00030 1 *8260B 2/12/18 13:23 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 13:23 ANG P8130215 o-Xylene BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 13:23 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 13:23 ANG P8130215 Styrene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 13:23 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0058 0.00020 1 *8260B 2/12/18 13:23 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 13:23 ANG P8130215 Toluene BRL mg/kg dry 0.0058 0.00034 1 *8260B 2/12/18 13:23 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 13:23 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0058 0.00031 1 *8260B 2/12/18 13:23 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0058 0.00038 1 *8260B 2/12/18 13:23 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0058 0.00038 1 *8260B 2/12/18 13:23 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.029 0.00080 1 *8260B 2/12/18 13:23 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 13:23 ANG P8130215 Xylenes, total BRL mg/kg dry 0.018 0.0011 1 *8260B 2/12/18 13:23 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 100 % 70-130 Dibromofluoromethane 104 % 84-123 Toluene-d8 94 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-3 (7.5-10) Attn: Roger Smith Prism Sample ID: 8020190-03 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 14:45 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 90.4 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.36 0.057 1 *8270D 2/13/18 18:23 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 18:23 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:23 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 18:23 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.36 0.070 1 *8270D 2/13/18 18:23 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.36 0.068 1 *8270D 2/13/18 18:23 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.36 0.071 1 *8270D 2/13/18 18:23 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.36 0.056 1 *8270D 2/13/18 18:23 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:23 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 18:23 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.36 0.049 1 *8270D 2/13/18 18:23 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 18:23 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 18:23 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.36 0.058 1 *8270D 2/13/18 18:23 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:23 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.36 0.066 1 *8270D 2/13/18 18:23 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.36 0.072 1 *8270D 2/13/18 18:23 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.36 0.045 1 *8270D 2/13/18 18:23 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 18:23 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.36 0.063 1 *8270D 2/13/18 18:23 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:23 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 18:23 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:23 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.36 0.056 1 *8270D 2/13/18 18:23 JMV P8130242 Acenaphthene BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 18:23 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 18:23 JMV P8130242 Anthracene BRL mg/kg dry 0.36 0.059 1 *8270D 2/13/18 18:23 JMV P8130242 Azobenzene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 18:23 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 18:23 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.36 0.039 1 *8270D 2/13/18 18:23 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.36 0.042 1 *8270D 2/13/18 18:23 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.36 0.040 1 *8270D 2/13/18 18:23 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 18:23 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.36 0.031 1 *8270D 2/13/18 18:23 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 18:23 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.36 0.063 1 *8270D 2/13/18 18:23 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 18:23 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.36 0.062 1 *8270D 2/13/18 18:23 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.36 0.054 1 *8270D 2/13/18 18:23 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 0f 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-3 (7.5-10) Attn: Roger Smith Prism Sample ID: 8020190-03 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 14:45 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 18:23 JMV P8130242 Chrysene BRL mg/kg dry 0.36 0.046 1 *8270D 2/13/18 18:23 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 18:23 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 18:23 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 18:23 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 18:23 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 18:23 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.36 0.045 1 *8270D 2/13/18 18:23 JMV P8130242 Fluoranthene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:23 JMV P8130242 Fluorene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 18:23 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.36 0.058 1 *8270D 2/13/18 18:23 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.36 0.066 1 *8270D 2/13/18 18:23 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.36 0.065 1 *8270D 2/13/18 18:23 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.36 0.061 1 *8270D 2/13/18 18:23 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.36 0.042 1 *8270D 2/13/18 18:23 JMV P8130242 Isophorone BRL mg/kg dry 0.36 0.049 1 *8270D 2/13/18 18:23 JMV P8130242 Naphthalene BRL mg/kg dry 0.36 0.059 1 *8270D 2/13/18 18:23 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 18:23 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.36 0.057 1 *8270D 2/13/18 18:23 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 18:23 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.36 0.043 1 *8270D 2/13/18 18:23 JMV P8130242 Phenanthrene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 18:23 JMV P8130242 Phenol BRL mg/kg dry 0.36 0.054 1 *8270D 2/13/18 18:23 JMV P8130242 Pyrene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 18:23 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 80 % 39-132 2-Fluorobiphenyl 86 % 44-115 2-Fluorophenol 77 % 35-115 Nitrobenzene-d5 76 % 37-122 Phenol-d5 78 % 34-121 Terphenyl-d14 82 % 54-127 Total Metals Mercury BRL mg/kg dry 0.024 0.0023 1 *7471 B 2/13/18 14:21 JAB P8130234 Arsenic BRL mg/kg dry 0.85 0.077 5 *6020B 2/13/18 22:36 EGC P8130232 Barium 57 mg/kg dry 5.6 0.034 5 *6020B 2/13/18 22:36 EGC P8130232 Cadmium BRL mg/kg dry 0.14 0.011 5 *6020B 2/13/18 22:36 EGC P8130232 Chromium 1.0 mg/kg dry 0.28 0.016 5 *6020B 2/13/18 22:36 EGC 1128130232 Lead 4.9 mg/kg dry 0.14 0.032 5 *6020B 2/13/18 22:36 EGC 1128130232 Selenium 0.82 mg/kg dry 0.56 0.12 5 *6020B 2/13/18 22:36 EGC P8130232 Silver BRL mg/kg dry 0.14 0.011 5 *6020B 2/13/18 22:36 EGC P8130232 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0056 0.00046 1 *8260B 2/12/18 13:51 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 0f 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: UST-3 (7.5-10) Prism Sample ID: 8020190-03 Prism Work Order: 8020190 Time Collected: 02/08/18 14:45 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1-Trichloroethane BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 13:51 ANG P8130215 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0056 0.00038 1 *8260B 2/12/18 13:51 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0056 0.00049 1 *8260B 2/12/18 13:51 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0056 0.00016 1 *8260B 2/12/18 13:51 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0056 0.00025 1 *8260B 2/12/18 13:51 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0056 0.00031 1 *8260B 2/12/18 13:51 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0056 0.00032 1 *8260B 2/12/18 13:51 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0056 0.00071 1 *8260B 2/12/18 13:51 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0056 0.00041 1 *8260B 2/12/18 13:51 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0056 0.00043 1 *8260B 2/12/18 13:51 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0056 0.00022 1 *8260B 2/12/18 13:51 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0056 0.00026 1 *8260B 2/12/18 13:51 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 13:51 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0056 0.00035 1 *8260B 2/12/18 13:51 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0056 0.00042 1 *8260B 2/12/18 13:51 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0056 0.00037 1 *8260B 2/12/18 13:51 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0056 0.00028 1 *8260B 2/12/18 13:51 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0056 0.00022 1 *8260B 2/12/18 13:51 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 13:51 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0056 0.00029 1 *8260B 2/12/18 13:51 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 13:51 ANG P8130215 4-Isopropyltoluene BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 13:51 ANG P8130215 Acetone BRL mg/kg dry 0.056 0.0014 1 *8260B 2/12/18 13:51 ANG P8130215 Benzene BRL mg/kg dry 0.0033 0.00032 1 *8260B 2/12/18 13:51 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0056 0.00047 1 *8260B 2/12/18 13:51 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0056 0.00031 1 *8260B 2/12/18 13:51 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0056 0.00031 1 *8260B 2/12/18 13:51 ANG P8130215 Bromoform BRL mg/kg dry 0.0056 0.00063 1 *8260B 2/12/18 13:51 ANG P8130215 Bromomethane BRL mg/kg dry 0.011 0.00069 1 *8260B 2/12/18 13:51 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0056 0.00028 1 *8260B 2/12/18 13:51 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0056 0.00030 1 *8260B 2/12/18 13:51 ANG P8130215 Chloroethane BRL mg/kg dry 0.011 0.00047 1 *8260B 2/12/18 13:51 ANG P8130215 Chloroform BRL mg/kg dry 0.0056 0.00040 1 *8260B 2/12/18 13:51 ANG P8130215 Chloromethane BRL mg/kg dry 0.0056 0.00037 1 *8260B 2/12/18 13:51 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0056 0.00024 1 *8260B 2/12/18 13:51 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0056 0.00019 1 *8260B 2/12/18 13:51 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0056 0.00023 1 *8260B 2/12/18 13:51 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0056 0.00025 1 *8260B 2/12/18 13:51 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0056 0.00021 1 *8260B 2/12/18 13:51 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0056 0.00023 1 *8260B 2/12/18 13:51 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 13:51 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.011 0.00051 1 *8260B 2/12/18 13:51 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.056 0.00050 1 *8260B 2/12/18 13:51 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 0f 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-3 (7.5-10) Attn: Roger Smith Prism Sample ID: 8020190-03 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 14:45 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.11 0.00050 1 *8260B 2/12/18 13:51 ANG P8130215 Methyl Isobutyl Ketone BRL mg/kg dry 0.056 0.00048 1 *8260B 2/12/18 13:51 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.011 0.00031 1 *8260B 2/12/18 13:51 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.011 0.00018 1 *8260B 2/12/18 13:51 ANG P8130215 Naphthalene BRL mg/kg dry 0.011 0.00018 1 *8260B 2/12/18 13:51 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0056 0.00028 1 *8260B 2/12/18 13:51 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 13:51 ANG P8130215 o-Xylene BRL mg/kg dry 0.0056 0.00023 1 *8260B 2/12/18 13:51 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 13:51 ANG P8130215 Styrene BRL mg/kg dry 0.0056 0.00034 1 *8260B 2/12/18 13:51 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0056 0.00019 1 *8260B 2/12/18 13:51 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 13:51 ANG P8130215 Toluene BRL mg/kg dry 0.0056 0.00032 1 *8260B 2/12/18 13:51 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 13:51 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0056 0.00029 1 *8260B 2/12/18 13:51 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0056 0.00036 1 *8260B 2/12/18 13:51 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0056 0.00036 1 *8260B 2/12/18 13:51 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.028 0.00076 1 *8260B 2/12/18 13:51 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 13:51 ANG P8130215 Xylenes, total BRL mg/kg dry 0.017 0.0010 1 *8260B 2/12/18 13:51 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 70-130 Dibromofluoromethane 105 % 84-123 Toluene-d8 94 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-4 (2.5-3) Attn: Roger Smith Prism Sample ID: 8020190-04 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 13:10 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 82.6 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.40 0.062 1 *8270D 2/13/18 18:45 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.40 0.061 1 *8270D 2/13/18 18:45 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.40 0.056 1 *8270D 2/13/18 18:45 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.40 0.058 1 *8270D 2/13/18 18:45 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.40 0.077 1 *8270D 2/13/18 18:45 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.40 0.075 1 *8270D 2/13/18 18:45 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.40 0.077 1 *8270D 2/13/18 18:45 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.40 0.061 1 *8270D 2/13/18 18:45 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.40 0.056 1 *8270D 2/13/18 18:45 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.40 0.049 1 *8270D 2/13/18 18:45 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.40 0.053 1 *8270D 2/13/18 18:45 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.40 0.058 1 *8270D 2/13/18 18:45 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.40 0.057 1 *8270D 2/13/18 18:45 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.40 0.064 1 *8270D 2/13/18 18:45 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.40 0.051 1 *8270D 2/13/18 18:45 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.40 0.073 1 *8270D 2/13/18 18:45 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.40 0.079 1 *8270D 2/13/18 18:45 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.40 0.049 1 *8270D 2/13/18 18:45 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.40 0.060 1 *8270D 2/13/18 18:45 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.40 0.069 1 *8270D 2/13/18 18:45 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.40 0.056 1 *8270D 2/13/18 18:45 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.40 0.048 1 *8270D 2/13/18 18:45 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.40 0.052 1 *8270D 2/13/18 18:45 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.40 0.062 1 *8270D 2/13/18 18:45 JMV P8130242 Acenaphthene BRL mg/kg dry 0.40 0.054 1 *8270D 2/13/18 18:45 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.40 0.058 1 *8270D 2/13/18 18:45 JMV P8130242 Anthracene BRL mg/kg dry 0.40 0.064 1 *8270D 2/13/18 18:45 JMV P8130242 Azobenzene BRL mg/kg dry 0.40 0.053 1 *8270D 2/13/18 18:45 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.40 0.052 1 *8270D 2/13/18 18:45 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.40 0.043 1 *8270D 2/13/18 18:45 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.40 0.046 1 *8270D 2/13/18 18:45 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.40 0.044 1 *8270D 2/13/18 18:45 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.40 0.052 1 *8270D 2/13/18 18:45 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.40 0.034 1 *8270D 2/13/18 18:45 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.40 0.053 1 *8270D 2/13/18 18:45 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.40 0.069 1 *8270D 2/13/18 18:45 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.40 0.056 1 *8270D 2/13/18 18:45 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.40 0.068 1 *8270D 2/13/18 18:45 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.40 0.059 1 *8270D 2/13/18 18:45 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 0f 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-4 (2.5-3) Attn: Roger Smith Prism Sample ID: 8020190-04 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 13:10 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.40 0.057 1 *8270D 2/13/18 18:45 JMV P8130242 Chrysene BRL mg/kg dry 0.40 0.050 1 *8270D 2/13/18 18:45 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.40 0.049 1 *8270D 2/13/18 18:45 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.40 0.061 1 *8270D 2/13/18 18:45 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.40 0.055 1 *8270D 2/13/18 18:45 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.40 0.053 1 *8270D 2/13/18 18:45 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.40 0.057 1 *8270D 2/13/18 18:45 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.40 0.049 1 *8270D 2/13/18 18:45 JMV P8130242 Fluoranthene BRL mg/kg dry 0.40 0.051 1 *8270D 2/13/18 18:45 JMV P8130242 Fluorene BRL mg/kg dry 0.40 0.057 1 *8270D 2/13/18 18:45 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.40 0.063 1 *8270D 2/13/18 18:45 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.40 0.072 1 *8270D 2/13/18 18:45 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.40 0.071 1 *8270D 2/13/18 18:45 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.40 0.067 1 *8270D 2/13/18 18:45 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.40 0.046 1 *8270D 2/13/18 18:45 JMV P8130242 Isophorone BRL mg/kg dry 0.40 0.054 1 *8270D 2/13/18 18:45 JMV P8130242 Naphthalene BRL mg/kg dry 0.40 0.064 1 *8270D 2/13/18 18:45 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.40 0.057 1 *8270D 2/13/18 18:45 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.40 0.063 1 *8270D 2/13/18 18:45 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.40 0.061 1 *8270D 2/13/18 18:45 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.40 0.047 1 *8270D 2/13/18 18:45 JMV P8130242 Phenanthrene BRL mg/kg dry 0.40 0.052 1 *8270D 2/13/18 18:45 JMV P8130242 Phenol BRL mg/kg dry 0.40 0.059 1 *8270D 2/13/18 18:45 JMV P8130242 Pyrene BRL mg/kg dry 0.40 0.053 1 *8270D 2/13/18 18:45 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 83 % 39-132 2-Fluorobiphenyl 84 % 44-115 2-Fluorophenol 77 % 35-115 Nitrobenzene-d5 75 % 37-122 Phenol-d5 77 % 34-121 Terphenyl-d14 81 % 54-127 Total Metals Mercury BRL mg/kg dry 0.026 0.0025 1 *7471 B 2/13/18 14:34 JAB P8130234 Arsenic BRL mg/kg dry 0.92 0.083 5 *6020B 2/13/18 22:43 EGC P8130232 Barium 61 mg/kg dry 6.1 0.037 5 *6020B 2/13/18 22:43 EGC P8130232 Cadmium BRL mg/kg dry 0.15 0.012 5 *6020B 2/13/18 22:43 EGC P8130232 Chromium 1.4 mg/kg dry 0.31 0.017 5 *6020B 2/13/18 22:43 EGC 1128130232 Lead 8.3 mg/kg dry 0.15 0.035 5 *6020B 2/13/18 22:43 EGC 1128130232 Selenium BRL mg/kg dry 0.61 0.13 5 *6020B 2/13/18 22:43 EGC P8130232 Silver BRL mg/kg dry 0.15 0.012 5 *6020B 2/13/18 22:43 EGC P8130232 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0066 0.00054 1 *8260B 2/12/18 14:18 ANG P8130215 1,1,1-Trichloroethane BRL mg/kg dry 0.0066 0.00032 1 *8260B 2/12/18 14:18 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 0f 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: UST-4 (2.5-3) Prism Sample ID: 8020190-04 Prism Work Order: 8020190 Time Collected: 02/09/18 13:10 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0066 0.00044 1 *8260B 2/12/18 14:18 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0066 0.00058 1 *8260B 2/12/18 14:18 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0066 0.00018 1 *8260B 2/12/18 14:18 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0066 0.00029 1 *8260B 2/12/18 14:18 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0066 0.00036 1 *8260B 2/12/18 14:18 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0066 0.00037 1 *8260B 2/12/18 14:18 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0066 0.00084 1 *8260B 2/12/18 14:18 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0066 0.00049 1 *8260B 2/12/18 14:18 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0066 0.00050 1 *8260B 2/12/18 14:18 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0066 0.00026 1 *8260B 2/12/18 14:18 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0066 0.00031 1 *8260B 2/12/18 14:18 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0066 0.00039 1 *8260B 2/12/18 14:18 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0066 0.00041 1 *8260B 2/12/18 14:18 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0066 0.00050 1 *8260B 2/12/18 14:18 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0066 0.00043 1 *8260B 2/12/18 14:18 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0066 0.00033 1 *8260B 2/12/18 14:18 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0066 0.00026 1 *8260B 2/12/18 14:18 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0066 0.00031 1 *8260B 2/12/18 14:18 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0066 0.00034 1 *8260B 2/12/18 14:18 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0066 0.00039 1 *8260B 2/12/18 14:18 ANG P8130215 4-Isopropyltoluene BRL mg/kg dry 0.0066 0.00032 1 *8260B 2/12/18 14:18 ANG P8130215 Acetone 0.077 mg/kg dry 0.066 0.0016 1 *8260B 2/12/18 14:18 ANG P8130215 Benzene BRL mg/kg dry 0.0039 0.00038 1 *8260B 2/12/18 14:18 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0066 0.00055 1 *8260B 2/12/18 14:18 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0066 0.00036 1 *8260B 2/12/18 14:18 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0066 0.00037 1 *8260B 2/12/18 14:18 ANG P8130215 Bromoform BRL mg/kg dry 0.0066 0.00074 1 *8260B 2/12/18 14:18 ANG P8130215 Bromomethane BRL mg/kg dry 0.013 0.00081 1 *8260B 2/12/18 14:18 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0066 0.00033 1 *8260B 2/12/18 14:18 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0066 0.00035 1 *8260B 2/12/18 14:18 ANG P8130215 Chloroethane BRL mg/kg dry 0.013 0.00055 1 *8260B 2/12/18 14:18 ANG P8130215 Chloroform BRL mg/kg dry 0.0066 0.00047 1 *8260B 2/12/18 14:18 ANG P8130215 Chloromethane BRL mg/kg dry 0.0066 0.00044 1 *8260B 2/12/18 14:18 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0066 0.00028 1 *8260B 2/12/18 14:18 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0066 0.00022 1 *8260B 2/12/18 14:18 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0066 0.00027 1 *8260B 2/12/18 14:18 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0066 0.00030 1 *8260B 2/12/18 14:18 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0066 0.00025 1 *8260B 2/12/18 14:18 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0066 0.00027 1 *8260B 2/12/18 14:18 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0066 0.00039 1 *8260B 2/12/18 14:18 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.013 0.00060 1 *8260B 2/12/18 14:18 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.066 0.00059 1 *8260B 2/12/18 14:18 ANG P8130215 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.13 0.00059 1 *8260B 2/12/18 14:18 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-4 (2.5-3) Attn: Roger Smith Prism Sample ID: 8020190-04 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 13:10 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Methyl Isobutyl Ketone BRL mg/kg dry 0.066 0.00056 1 *8260B 2/12/18 14:18 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.013 0.00037 1 *8260B 2/12/18 14:18 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.013 0.00021 1 *8260B 2/12/18 14:18 ANG P8130215 Naphthalene BRL mg/kg dry 0.013 0.00021 1 *8260B 2/12/18 14:18 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0066 0.00033 1 *8260B 2/12/18 14:18 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0066 0.00039 1 *8260B 2/12/18 14:18 ANG P8130215 o-Xylene BRL mg/kg dry 0.0066 0.00027 1 *8260B 2/12/18 14:18 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0066 0.00032 1 *8260B 2/12/18 14:18 ANG P8130215 Styrene BRL mg/kg dry 0.0066 0.00039 1 *8260B 2/12/18 14:18 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0066 0.00022 1 *8260B 2/12/18 14:18 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0066 0.00031 1 *8260B 2/12/18 14:18 ANG P8130215 Toluene BRL mg/kg dry 0.0066 0.00038 1 *8260B 2/12/18 14:18 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0066 0.00039 1 *8260B 2/12/18 14:18 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0066 0.00034 1 *8260B 2/12/18 14:18 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0066 0.00042 1 *8260B 2/12/18 14:18 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0066 0.00042 1 *8260B 2/12/18 14:18 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.033 0.00090 1 *8260B 2/12/18 14:18 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0066 0.00032 1 *8260B 2/12/18 14:18 ANG P8130215 Xylenes, total BRL mg/kg dry 0.020 0.0012 1 *8260B 2/12/18 14:18 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 102 % 84-123 Toluene-d8 92 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-4 (7.5-10) Attn: Roger Smith Prism Sample ID: 8020190-05 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 15:10 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 87.7 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.38 0.059 1 *8270D 2/13/18 19:07 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.38 0.057 1 *8270D 2/13/18 19:07 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 19:07 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.38 0.055 1 *8270D 2/13/18 19:07 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.38 0.072 1 *8270D 2/13/18 19:07 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.38 0.070 1 *8270D 2/13/18 19:07 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.38 0.073 1 *8270D 2/13/18 19:07 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.38 0.058 1 *8270D 2/13/18 19:07 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.38 0.052 1 *8270D 2/13/18 19:07 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.38 0.046 1 *8270D 2/13/18 19:07 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 19:07 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.38 0.054 1 *8270D 2/13/18 19:07 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 19:07 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.38 0.060 1 *8270D 2/13/18 19:07 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.38 0.048 1 *8270D 2/13/18 19:07 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.38 0.068 1 *8270D 2/13/18 19:07 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.38 0.074 1 *8270D 2/13/18 19:07 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.38 0.046 1 *8270D 2/13/18 19:07 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.38 0.056 1 *8270D 2/13/18 19:07 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.38 0.065 1 *8270D 2/13/18 19:07 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 19:07 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.38 0.045 1 *8270D 2/13/18 19:07 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.38 0.049 1 *8270D 2/13/18 19:07 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.38 0.058 1 *8270D 2/13/18 19:07 JMV P8130242 Acenaphthene BRL mg/kg dry 0.38 0.051 1 *8270D 2/13/18 19:07 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.38 0.054 1 *8270D 2/13/18 19:07 JMV P8130242 Anthracene BRL mg/kg dry 0.38 0.061 1 *8270D 2/13/18 19:07 JMV P8130242 Azobenzene BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 19:07 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.38 0.049 1 *8270D 2/13/18 19:07 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.38 0.041 1 *8270D 2/13/18 19:07 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.38 0.044 1 *8270D 2/13/18 19:07 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.38 0.041 1 *8270D 2/13/18 19:07 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.38 0.049 1 *8270D 2/13/18 19:07 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.38 0.032 1 *8270D 2/13/18 19:07 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 19:07 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.38 0.065 1 *8270D 2/13/18 19:07 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 19:07 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.38 0.064 1 *8270D 2/13/18 19:07 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.38 0.056 1 *8270D 2/13/18 19:07 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 0f 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-4 (7.5-10) Attn: Roger Smith Prism Sample ID: 8020190-05 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 15:10 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 19:07 JMV P8130242 Chrysene BRL mg/kg dry 0.38 0.047 1 *8270D 2/13/18 19:07 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.38 0.046 1 *8270D 2/13/18 19:07 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.38 0.057 1 *8270D 2/13/18 19:07 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.38 0.052 1 *8270D 2/13/18 19:07 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 19:07 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 19:07 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.38 0.046 1 *8270D 2/13/18 19:07 JMV P8130242 Fluoranthene BRL mg/kg dry 0.38 0.048 1 *8270D 2/13/18 19:07 JMV P8130242 Fluorene BRL mg/kg dry 0.38 0.054 1 *8270D 2/13/18 19:07 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.38 0.060 1 *8270D 2/13/18 19:07 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.38 0.067 1 *8270D 2/13/18 19:07 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.38 0.067 1 *8270D 2/13/18 19:07 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.38 0.063 1 *8270D 2/13/18 19:07 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.38 0.043 1 *8270D 2/13/18 19:07 JMV P8130242 Isophorone BRL mg/kg dry 0.38 0.051 1 *8270D 2/13/18 19:07 JMV P8130242 Naphthalene BRL mg/kg dry 0.38 0.060 1 *8270D 2/13/18 19:07 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 19:07 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.38 0.059 1 *8270D 2/13/18 19:07 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.38 0.057 1 *8270D 2/13/18 19:07 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.38 0.044 1 *8270D 2/13/18 19:07 JMV P8130242 Phenanthrene BRL mg/kg dry 0.38 0.049 1 *8270D 2/13/18 19:07 JMV P8130242 Phenol BRL mg/kg dry 0.38 0.055 1 *8270D 2/13/18 19:07 JMV P8130242 Pyrene BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 19:07 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 77 % 39-132 2-Fluorobiphenyl 81 % 44-115 2-Fluorophenol 71 % 35-115 Nitrobenzene-d5 71 % 37-122 Phenol-d5 72 % 34-121 Terphenyl-d14 82 % 54-127 Total Metals Mercury BRL mg/kg dry 0.023 0.0022 1 *7471B 2/13/18 14:39 JAB P8130234 Arsenic 0.86 mg/kg dry 0.86 0.078 5 *6020B 2/13/18 22:51 EGC P8B0232 Barium 66 mg/kg dry 5.7 0.035 5 *6020B 2/13/18 22:51 EGC P8130232 Cadmium BRL mg/kg dry 0.14 0.011 5 *6020B 2/13/18 22:51 EGC P8130232 Chromium 1.1 mg/kg dry 0.29 0.016 5 *6020B 2/13/18 22:51 EGC 1138130232 Lead 4.1 mg/kg dry 0.14 0.033 5 *6020B 2/13/18 22:51 EGC P8130232 Selenium 1.0 mg/kg dry 0.57 0.12 5 *6020B 2/13/18 22:51 EGC P8130232 Silver BRL mg/kg dry 0.14 0.011 5 *6020B 2/13/18 22:51 EGC P8130232 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0063 0.00052 1 *8260B 2/12/18 14:46 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 0f 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: UST-4 (7.5-10) Prism Sample ID: 8020190-05 Prism Work Order: 8020190 Time Collected: 02/08/18 15:10 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1-Trichloroethane BRL mg/kg dry 0.0063 0.00030 1 *8260B 2/12/18 14:46 ANG P8130215 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0063 0.00042 1 *8260B 2/12/18 14:46 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0063 0.00056 1 *8260B 2/12/18 14:46 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0063 0.00017 1 *8260B 2/12/18 14:46 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0063 0.00028 1 *8260B 2/12/18 14:46 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0063 0.00034 1 *8260B 2/12/18 14:46 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0063 0.00036 1 *8260B 2/12/18 14:46 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0063 0.00080 1 *8260B 2/12/18 14:46 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0063 0.00047 1 *8260B 2/12/18 14:46 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0063 0.00048 1 *8260B 2/12/18 14:46 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0063 0.00025 1 *8260B 2/12/18 14:46 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0063 0.00030 1 *8260B 2/12/18 14:46 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0063 0.00037 1 *8260B 2/12/18 14:46 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0063 0.00039 1 *8260B 2/12/18 14:46 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0063 0.00047 1 *8260B 2/12/18 14:46 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0063 0.00042 1 *8260B 2/12/18 14:46 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0063 0.00032 1 *8260B 2/12/18 14:46 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0063 0.00025 1 *8260B 2/12/18 14:46 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0063 0.00030 1 *8260B 2/12/18 14:46 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0063 0.00032 1 *8260B 2/12/18 14:46 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0063 0.00037 1 *8260B 2/12/18 14:46 ANG P8130215 4-Isopropyltoluene BRL mg/kg dry 0.0063 0.00030 1 *8260B 2/12/18 14:46 ANG P8130215 Acetone BRL mg/kg dry 0.063 0.0015 1 *8260B 2/12/18 14:46 ANG P8130215 Benzene BRL mg/kg dry 0.0038 0.00037 1 *8260B 2/12/18 14:46 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0063 0.00052 1 *8260B 2/12/18 14:46 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0063 0.00035 1 *8260B 2/12/18 14:46 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0063 0.00035 1 *8260B 2/12/18 14:46 ANG P8130215 Bromoform BRL mg/kg dry 0.0063 0.00071 1 *8260B 2/12/18 14:46 ANG P8130215 Bromomethane BRL mg/kg dry 0.013 0.00077 1 *8260B 2/12/18 14:46 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0063 0.00031 1 *8260B 2/12/18 14:46 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0063 0.00033 1 *8260B 2/12/18 14:46 ANG P8130215 Chloroethane BRL mg/kg dry 0.013 0.00052 1 *8260B 2/12/18 14:46 ANG P8130215 Chloroform BRL mg/kg dry 0.0063 0.00045 1 *8260B 2/12/18 14:46 ANG P8130215 Chloromethane BRL mg/kg dry 0.0063 0.00042 1 *8260B 2/12/18 14:46 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0063 0.00027 1 *8260B 2/12/18 14:46 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0063 0.00021 1 *8260B 2/12/18 14:46 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0063 0.00026 1 *8260B 2/12/18 14:46 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0063 0.00028 1 *8260B 2/12/18 14:46 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0063 0.00024 1 *8260B 2/12/18 14:46 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0063 0.00026 1 *8260B 2/12/18 14:46 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0063 0.00037 1 *8260B 2/12/18 14:46 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.013 0.00058 1 *8260B 2/12/18 14:46 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.063 0.00057 1 *8260B 2/12/18 14:46 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 0f 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-4 (7.5-10) Attn: Roger Smith Prism Sample ID: 8020190-05 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 15:10 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.13 0.00057 1 *8260B 2/12/18 14:46 ANG P8130215 Methyl Isobutyl Ketone BRL mg/kg dry 0.063 0.00053 1 *8260B 2/12/18 14:46 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.013 0.00035 1 *8260B 2/12/18 14:46 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.013 0.00020 1 *8260B 2/12/18 14:46 ANG P8130215 Naphthalene BRL mg/kg dry 0.013 0.00020 1 *8260B 2/12/18 14:46 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0063 0.00032 1 *8260B 2/12/18 14:46 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0063 0.00037 1 *8260B 2/12/18 14:46 ANG P8130215 o-Xylene BRL mg/kg dry 0.0063 0.00026 1 *8260B 2/12/18 14:46 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0063 0.00030 1 *8260B 2/12/18 14:46 ANG P8130215 Styrene BRL mg/kg dry 0.0063 0.00038 1 *8260B 2/12/18 14:46 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0063 0.00021 1 *8260B 2/12/18 14:46 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0063 0.00030 1 *8260B 2/12/18 14:46 ANG P8130215 Toluene BRL mg/kg dry 0.0063 0.00036 1 *8260B 2/12/18 14:46 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0063 0.00038 1 *8260B 2/12/18 14:46 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0063 0.00033 1 *8260B 2/12/18 14:46 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0063 0.00041 1 *8260B 2/12/18 14:46 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0063 0.00041 1 *8260B 2/12/18 14:46 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.031 0.00086 1 *8260B 2/12/18 14:46 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0063 0.00030 1 *8260B 2/12/18 14:46 ANG P8130215 Xylenes, total BRL mg/kg dry 0.019 0.0012 1 *8260B 2/12/18 14:46 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 101 % 84-123 Toluene-d8 95 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-4 (12-14) Attn: Roger Smith Prism Sample ID: 8020190-06 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 12:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 92.0 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.36 0.056 1 *8270D 2/13/18 19:29 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.36 0.054 1 *8270D 2/13/18 19:29 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 19:29 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 19:29 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.36 0.069 1 *8270D 2/13/18 19:29 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.36 0.067 1 *8270D 2/13/18 19:29 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.36 0.069 1 *8270D 2/13/18 19:29 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 19:29 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 19:29 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.36 0.043 1 *8270D 2/13/18 19:29 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 19:29 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 19:29 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 19:29 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.36 0.057 1 *8270D 2/13/18 19:29 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.36 0.046 1 *8270D 2/13/18 19:29 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.36 0.065 1 *8270D 2/13/18 19:29 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.36 0.071 1 *8270D 2/13/18 19:29 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 19:29 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.36 0.054 1 *8270D 2/13/18 19:29 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.36 0.061 1 *8270D 2/13/18 19:29 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.36 0.050 1 *8270D 2/13/18 19:29 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.36 0.043 1 *8270D 2/13/18 19:29 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 19:29 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.36 0.055 1 *8270D 2/13/18 19:29 JMV P8130242 Acenaphthene BRL mg/kg dry 0.36 0.049 1 *8270D 2/13/18 19:29 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.36 0.052 1 *8270D 2/13/18 19:29 JMV P8130242 Anthracene BRL mg/kg dry 0.36 0.058 1 *8270D 2/13/18 19:29 JMV P8130242 Azobenzene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 19:29 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 19:29 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.36 0.039 1 *8270D 2/13/18 19:29 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.36 0.042 1 *8270D 2/13/18 19:29 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.36 0.039 1 *8270D 2/13/18 19:29 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 19:29 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.36 0.030 1 *8270D 2/13/18 19:29 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 19:29 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.36 0.062 1 *8270D 2/13/18 19:29 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 19:29 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.36 0.061 1 *8270D 2/13/18 19:29 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 19:29 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 0f 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-4 (12-14) Attn: Roger Smith Prism Sample ID: 8020190-06 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 12:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 19:29 JMV P8130242 Chrysene BRL mg/kg dry 0.36 0.045 1 *8270D 2/13/18 19:29 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 19:29 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.36 0.054 1 *8270D 2/13/18 19:29 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.36 0.049 1 *8270D 2/13/18 19:29 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 19:29 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 19:29 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.36 0.044 1 *8270D 2/13/18 19:29 JMV P8130242 Fluoranthene BRL mg/kg dry 0.36 0.046 1 *8270D 2/13/18 19:29 JMV P8130242 Fluorene BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 19:29 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.36 0.057 1 *8270D 2/13/18 19:29 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.36 0.064 1 *8270D 2/13/18 19:29 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.36 0.064 1 *8270D 2/13/18 19:29 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.36 0.060 1 *8270D 2/13/18 19:29 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.36 0.041 1 *8270D 2/13/18 19:29 JMV P8130242 Isophorone BRL mg/kg dry 0.36 0.048 1 *8270D 2/13/18 19:29 JMV P8130242 Naphthalene BRL mg/kg dry 0.36 0.058 1 *8270D 2/13/18 19:29 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.36 0.051 1 *8270D 2/13/18 19:29 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.36 0.056 1 *8270D 2/13/18 19:29 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.36 0.054 1 *8270D 2/13/18 19:29 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.36 0.042 1 *8270D 2/13/18 19:29 JMV P8130242 Phenanthrene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 19:29 JMV P8130242 Phenol BRL mg/kg dry 0.36 0.053 1 *8270D 2/13/18 19:29 JMV P8130242 Pyrene BRL mg/kg dry 0.36 0.047 1 *8270D 2/13/18 19:29 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 77 % 39-132 2-Fluorobiphenyl 78 % 44-115 2-Fluorophenol 72 % 35-115 Nitrobenzene-d5 65 % 37-122 Phenol-d5 72 % 34-121 Terphenyl-d14 78 % 54-127 Total Metals Mercury BRL mg/kg dry 0.020 0.0019 1 *7471 B 2/13/18 14:43 JAB P8130234 Arsenic BRL mg/kg dry 0.82 0.075 5 *6020B 2/13/18 22:59 EGC P8130232 Barium 95 mg/kg dry 5.5 0.033 5 *6020B 2/13/18 22:59 EGC P8130232 Cadmium BRL mg/kg dry 0.14 0.010 5 *6020B 2/13/18 22:59 EGC P8130232 Chromium 2.3 mg/kg dry 0.27 0.015 5 *6020B 2/13/18 22:59 EGC 1128130232 Lead 3.4 mg/kg dry 0.14 0.031 5 *6020B 2/13/18 22:59 EGC 1128130232 Selenium 0.97 mg/kg dry 0.55 0.11 5 *6020B 2/13/18 22:59 EGC P8130232 Silver BRL mg/kg dry 0.14 0.010 5 *6020B 2/13/18 22:59 EGC P8130232 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0056 0.00046 1 *8260B 2/12/18 15:14 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 0f 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: UST-4 (12-14) Prism Sample ID: 8020190-06 Prism Work Order: 8020190 Time Collected: 02/09/18 12:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1-Trichloroethane BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 15:14 ANG P8130215 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0056 0.00038 1 *8260B 2/12/18 15:14 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0056 0.00049 1 *8260B 2/12/18 15:14 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0056 0.00015 1 *8260B 2/12/18 15:14 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0056 0.00025 1 *8260B 2/12/18 15:14 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0056 0.00030 1 *8260B 2/12/18 15:14 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0056 0.00032 1 *8260B 2/12/18 15:14 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0056 0.00071 1 *8260B 2/12/18 15:14 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0056 0.00041 1 *8260B 2/12/18 15:14 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0056 0.00042 1 *8260B 2/12/18 15:14 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0056 0.00022 1 *8260B 2/12/18 15:14 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0056 0.00026 1 *8260B 2/12/18 15:14 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 15:14 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0056 0.00034 1 *8260B 2/12/18 15:14 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0056 0.00042 1 *8260B 2/12/18 15:14 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0056 0.00037 1 *8260B 2/12/18 15:14 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0056 0.00028 1 *8260B 2/12/18 15:14 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0056 0.00022 1 *8260B 2/12/18 15:14 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0056 0.00026 1 *8260B 2/12/18 15:14 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0056 0.00029 1 *8260B 2/12/18 15:14 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 15:14 ANG P8130215 4-Isopropyltoluene BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 15:14 ANG P8130215 Acetone BRL mg/kg dry 0.056 0.0014 1 *8260B 2/12/18 15:14 ANG P8130215 Benzene BRL mg/kg dry 0.0033 0.00032 1 *8260B 2/12/18 15:14 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0056 0.00046 1 *8260B 2/12/18 15:14 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0056 0.00031 1 *8260B 2/12/18 15:14 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0056 0.00031 1 *8260B 2/12/18 15:14 ANG P8130215 Bromoform BRL mg/kg dry 0.0056 0.00063 1 *8260B 2/12/18 15:14 ANG P8130215 Bromomethane BRL mg/kg dry 0.011 0.00069 1 *8260B 2/12/18 15:14 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0056 0.00028 1 *8260B 2/12/18 15:14 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0056 0.00029 1 *8260B 2/12/18 15:14 ANG P8130215 Chloroethane BRL mg/kg dry 0.011 0.00046 1 *8260B 2/12/18 15:14 ANG P8130215 Chloroform BRL mg/kg dry 0.0056 0.00040 1 *8260B 2/12/18 15:14 ANG P8130215 Chloromethane BRL mg/kg dry 0.0056 0.00037 1 *8260B 2/12/18 15:14 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0056 0.00024 1 *8260B 2/12/18 15:14 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0056 0.00019 1 *8260B 2/12/18 15:14 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0056 0.00023 1 *8260B 2/12/18 15:14 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0056 0.00025 1 *8260B 2/12/18 15:14 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0056 0.00021 1 *8260B 2/12/18 15:14 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0056 0.00023 1 *8260B 2/12/18 15:14 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 15:14 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.011 0.00051 1 *8260B 2/12/18 15:14 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.056 0.00050 1 *8260B 2/12/18 15:14 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 0f 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-4 (12-14) Attn: Roger Smith Prism Sample ID: 8020190-06 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 12:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.11 0.00050 1 *8260B 2/12/18 15:14 ANG P8130215 Methyl Isobutyl Ketone BRL mg/kg dry 0.056 0.00047 1 *8260B 2/12/18 15:14 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.011 0.00031 1 *8260B 2/12/18 15:14 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.011 0.00018 1 *8260B 2/12/18 15:14 ANG P8130215 Naphthalene BRL mg/kg dry 0.011 0.00018 1 *8260B 2/12/18 15:14 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0056 0.00028 1 *8260B 2/12/18 15:14 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 15:14 ANG P8130215 o-Xylene BRL mg/kg dry 0.0056 0.00023 1 *8260B 2/12/18 15:14 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 15:14 ANG P8130215 Styrene BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 15:14 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0056 0.00019 1 *8260B 2/12/18 15:14 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0056 0.00026 1 *8260B 2/12/18 15:14 ANG P8130215 Toluene BRL mg/kg dry 0.0056 0.00032 1 *8260B 2/12/18 15:14 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0056 0.00033 1 *8260B 2/12/18 15:14 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0056 0.00029 1 *8260B 2/12/18 15:14 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0056 0.00036 1 *8260B 2/12/18 15:14 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0056 0.00036 1 *8260B 2/12/18 15:14 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.028 0.00076 1 *8260B 2/12/18 15:14 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0056 0.00027 1 *8260B 2/12/18 15:14 ANG P8130215 Xylenes, total BRL mg/kg dry 0.017 0.0010 1 *8260B 2/12/18 15:14 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 70-130 Dibromofluoromethane 101 % 84-123 Toluene-d8 94 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-5 (2.5-3) Attn: Roger Smith Prism Sample ID: 8020190-07 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 11:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 79.8 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.41 0.065 1 *8270D 2/13/18 19:51 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.41 0.063 1 *8270D 2/13/18 19:51 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 19:51 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.41 0.061 1 *8270D 2/13/18 19:51 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.41 0.080 1 *8270D 2/13/18 19:51 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.41 0.078 1 *8270D 2/13/18 19:51 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.41 0.080 1 *8270D 2/13/18 19:51 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.41 0.063 1 *8270D 2/13/18 19:51 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 19:51 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.41 0.050 1 *8270D 2/13/18 19:51 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.41 0.055 1 *8270D 2/13/18 19:51 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.41 0.060 1 *8270D 2/13/18 19:51 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.41 0.059 1 *8270D 2/13/18 19:51 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.41 0.066 1 *8270D 2/13/18 19:51 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.41 0.053 1 *8270D 2/13/18 19:51 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.41 0.075 1 *8270D 2/13/18 19:51 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.41 0.082 1 *8270D 2/13/18 19:51 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.41 0.051 1 *8270D 2/13/18 19:51 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.41 0.062 1 *8270D 2/13/18 19:51 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.41 0.071 1 *8270D 2/13/18 19:51 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 19:51 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.41 0.050 1 *8270D 2/13/18 19:51 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 19:51 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.41 0.064 1 *8270D 2/13/18 19:51 JMV P8130242 Acenaphthene BRL mg/kg dry 0.41 0.056 1 *8270D 2/13/18 19:51 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.41 0.060 1 *8270D 2/13/18 19:51 JMV P8130242 Anthracene BRL mg/kg dry 0.41 0.067 1 *8270D 2/13/18 19:51 JMV P8130242 Azobenzene BRL mg/kg dry 0.41 0.055 1 *8270D 2/13/18 19:51 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 19:51 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.41 0.045 1 *8270D 2/13/18 19:51 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.41 0.048 1 *8270D 2/13/18 19:51 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.41 0.045 1 *8270D 2/13/18 19:51 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 19:51 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.41 0.035 1 *8270D 2/13/18 19:51 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.41 0.055 1 *8270D 2/13/18 19:51 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.41 0.072 1 *8270D 2/13/18 19:51 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 19:51 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.41 0.071 1 *8270D 2/13/18 19:51 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.41 0.061 1 *8270D 2/13/18 19:51 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 0f 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-5 (2.5-3) Attn: Roger Smith Prism Sample ID: 8020190-07 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 11:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.41 0.059 1 *8270D 2/13/18 19:51 JMV P8130242 Chrysene BRL mg/kg dry 0.41 0.052 1 *8270D 2/13/18 19:51 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.41 0.050 1 *8270D 2/13/18 19:51 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.41 0.063 1 *8270D 2/13/18 19:51 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.41 0.057 1 *8270D 2/13/18 19:51 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.41 0.055 1 *8270D 2/13/18 19:51 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.41 0.059 1 *8270D 2/13/18 19:51 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.41 0.051 1 *8270D 2/13/18 19:51 JMV P8130242 Fluoranthene BRL mg/kg dry 0.41 0.053 1 *8270D 2/13/18 19:51 JMV P8130242 Fluorene BRL mg/kg dry 0.41 0.059 1 *8270D 2/13/18 19:51 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.41 0.066 1 *8270D 2/13/18 19:51 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.41 0.074 1 *8270D 2/13/18 19:51 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.41 0.074 1 *8270D 2/13/18 19:51 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.41 0.069 1 *8270D 2/13/18 19:51 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.41 0.047 1 *8270D 2/13/18 19:51 JMV P8130242 Isophorone BRL mg/kg dry 0.41 0.056 1 *8270D 2/13/18 19:51 JMV P8130242 Naphthalene BRL mg/kg dry 0.41 0.067 1 *8270D 2/13/18 19:51 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.41 0.059 1 *8270D 2/13/18 19:51 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.41 0.065 1 *8270D 2/13/18 19:51 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.41 0.063 1 *8270D 2/13/18 19:51 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.41 0.049 1 *8270D 2/13/18 19:51 JMV P8130242 Phenanthrene BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 19:51 JMV P8130242 Phenol BRL mg/kg dry 0.41 0.061 1 *8270D 2/13/18 19:51 JMV P8130242 Pyrene BRL mg/kg dry 0.41 0.055 1 *8270D 2/13/18 19:51 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 81 % 39-132 2-Fluorobiphenyl 79 % 44-115 2-Fluorophenol 71 % 35-115 Nitrobenzene-d5 68 % 37-122 Phenol-d5 71 % 34-121 Terphenyl-d14 80 % 54-127 Total Metals Mercury BRL mg/kg dry 0.027 0.0026 1 *7471 B 2/13/18 14:48 JAB P8130234 Arsenic BRL mg/kg dry 0.93 0.084 5 *6020B 2/13/18 23:22 EGC P8130232 Barium 92 mg/kg dry 6.2 0.038 5 *6020B 2/13/18 23:22 EGC P8130232 Cadmium BRL mg/kg dry 0.15 0.012 5 *6020B 2/13/18 23:22 EGC P8130232 Chromium 1.4 mg/kg dry 0.31 0.017 5 *6020B 2/13/18 23:22 EGC 1128130232 Lead 7.7 mg/kg dry 0.15 0.035 5 *6020B 2/13/18 23:22 EGC 1128130232 Selenium 0.96 mg/kg dry 0.62 0.13 5 *6020B 2/13/18 23:22 EGC P8130232 Silver BRL mg/kg dry 0.15 0.012 5 *6020B 2/13/18 23:22 EGC P8130232 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0061 0.00050 1 *8260B 2/12/18 15:42 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 0f 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: UST-5 (2.5-3) Prism Sample ID: 8020190-07 Prism Work Order: 8020190 Time Collected: 02/09/18 11:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1-Trichloroethane BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 15:42 ANG P8130215 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0061 0.00041 1 *8260B 2/12/18 15:42 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0061 0.00054 1 *8260B 2/12/18 15:42 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0061 0.00017 1 *8260B 2/12/18 15:42 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0061 0.00027 1 *8260B 2/12/18 15:42 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0061 0.00033 1 *8260B 2/12/18 15:42 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0061 0.00034 1 *8260B 2/12/18 15:42 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0061 0.00077 1 *8260B 2/12/18 15:42 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0061 0.00045 1 *8260B 2/12/18 15:42 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0061 0.00046 1 *8260B 2/12/18 15:42 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0061 0.00024 1 *8260B 2/12/18 15:42 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 15:42 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 15:42 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0061 0.00038 1 *8260B 2/12/18 15:42 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0061 0.00046 1 *8260B 2/12/18 15:42 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0061 0.00040 1 *8260B 2/12/18 15:42 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0061 0.00030 1 *8260B 2/12/18 15:42 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0061 0.00024 1 *8260B 2/12/18 15:42 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 15:42 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0061 0.00031 1 *8260B 2/12/18 15:42 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 15:42 ANG P8130215 4-Isopropyltoluene BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 15:42 ANG P8130215 Acetone BRL mg/kg dry 0.061 0.0015 1 *8260B 2/12/18 15:42 ANG P8130215 Benzene BRL mg/kg dry 0.0036 0.00035 1 *8260B 2/12/18 15:42 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0061 0.00051 1 *8260B 2/12/18 15:42 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0061 0.00033 1 *8260B 2/12/18 15:42 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0061 0.00034 1 *8260B 2/12/18 15:42 ANG P8130215 Bromoform BRL mg/kg dry 0.0061 0.00069 1 *8260B 2/12/18 15:42 ANG P8130215 Bromomethane BRL mg/kg dry 0.012 0.00075 1 *8260B 2/12/18 15:42 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0061 0.00030 1 *8260B 2/12/18 15:42 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0061 0.00032 1 *8260B 2/12/18 15:42 ANG P8130215 Chloroethane BRL mg/kg dry 0.012 0.00051 1 *8260B 2/12/18 15:42 ANG P8130215 Chloroform BRL mg/kg dry 0.0061 0.00044 1 *8260B 2/12/18 15:42 ANG P8130215 Chloromethane BRL mg/kg dry 0.0061 0.00041 1 *8260B 2/12/18 15:42 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0061 0.00026 1 *8260B 2/12/18 15:42 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0061 0.00020 1 *8260B 2/12/18 15:42 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0061 0.00025 1 *8260B 2/12/18 15:42 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0061 0.00028 1 *8260B 2/12/18 15:42 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0061 0.00023 1 *8260B 2/12/18 15:42 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0061 0.00025 1 *8260B 2/12/18 15:42 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 15:42 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.012 0.00056 1 *8260B 2/12/18 15:42 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.061 0.00055 1 *8260B 2/12/18 15:42 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 0f 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-5 (2.5-3) Attn: Roger Smith Prism Sample ID: 8020190-07 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 11:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.12 0.00055 1 *8260B 2/12/18 15:42 ANG P8130215 Methyl Isobutyl Ketone BRL mg/kg dry 0.061 0.00052 1 *8260B 2/12/18 15:42 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.012 0.00034 1 *8260B 2/12/18 15:42 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.012 0.00019 1 *8260B 2/12/18 15:42 ANG P8130215 Naphthalene BRL mg/kg dry 0.012 0.00019 1 *8260B 2/12/18 15:42 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0061 0.00031 1 *8260B 2/12/18 15:42 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 15:42 ANG P8130215 o-Xylene BRL mg/kg dry 0.0061 0.00025 1 *8260B 2/12/18 15:42 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 15:42 ANG P8130215 Styrene BRL mg/kg dry 0.0061 0.00037 1 *8260B 2/12/18 15:42 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0061 0.00021 1 *8260B 2/12/18 15:42 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 15:42 ANG P8130215 Toluene BRL mg/kg dry 0.0061 0.00035 1 *8260B 2/12/18 15:42 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0061 0.00036 1 *8260B 2/12/18 15:42 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0061 0.00032 1 *8260B 2/12/18 15:42 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0061 0.00039 1 *8260B 2/12/18 15:42 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0061 0.00039 1 *8260B 2/12/18 15:42 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.030 0.00083 1 *8260B 2/12/18 15:42 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0061 0.00029 1 *8260B 2/12/18 15:42 ANG P8130215 Xylenes, total BRL mg/kg dry 0.018 0.0011 1 *8260B 2/12/18 15:42 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 70-130 Dibromofluoromethane 97 % 84-123 Toluene-d8 92 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-6 (2.5-3) Attn: Roger Smith Prism Sample ID: 8020190-08 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 13:20 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 80.5 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.41 0.064 1 *8270D 2/13/18 21:40 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.41 0.062 1 *8270D 2/13/18 21:40 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 21:40 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.41 0.060 1 *8270D 2/13/18 21:40 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.41 0.079 1 *8270D 2/13/18 21:40 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.41 0.077 1 *8270D 2/13/18 21:40 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.41 0.079 1 *8270D 2/13/18 21:40 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.41 0.063 1 *8270D 2/13/18 21:40 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.41 0.057 1 *8270D 2/13/18 21:40 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.41 0.050 1 *8270D 2/13/18 21:40 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 21:40 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.41 0.059 1 *8270D 2/13/18 21:40 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 21:40 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.41 0.066 1 *8270D 2/13/18 21:40 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.41 0.052 1 *8270D 2/13/18 21:40 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.41 0.075 1 *8270D 2/13/18 21:40 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.41 0.081 1 *8270D 2/13/18 21:40 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.41 0.050 1 *8270D 2/13/18 21:40 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.41 0.062 1 *8270D 2/13/18 21:40 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.41 0.070 1 *8270D 2/13/18 21:40 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.41 0.057 1 *8270D 2/13/18 21:40 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.41 0.049 1 *8270D 2/13/18 21:40 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.41 0.053 1 *8270D 2/13/18 21:40 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.41 0.063 1 *8270D 2/13/18 21:40 JMV P8130242 Acenaphthene BRL mg/kg dry 0.41 0.056 1 *8270D 2/13/18 21:40 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.41 0.059 1 *8270D 2/13/18 21:40 JMV P8130242 Anthracene BRL mg/kg dry 0.41 0.066 1 *8270D 2/13/18 21:40 JMV P8130242 Azobenzene BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 21:40 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 21:40 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.41 0.044 1 *8270D 2/13/18 21:40 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.41 0.048 1 *8270D 2/13/18 21:40 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.41 0.045 1 *8270D 2/13/18 21:40 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 21:40 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.41 0.034 1 *8270D 2/13/18 21:40 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 21:40 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.41 0.071 1 *8270D 2/13/18 21:40 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 21:40 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.41 0.070 1 *8270D 2/13/18 21:40 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.41 0.061 1 *8270D 2/13/18 21:40 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 0f 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-6 (2.5-3) Attn: Roger Smith Prism Sample ID: 8020190-08 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 13:20 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 21:40 JMV P8130242 Chrysene BRL mg/kg dry 0.41 0.052 1 *8270D 2/13/18 21:40 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.41 0.050 1 *8270D 2/13/18 21:40 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.41 0.062 1 *8270D 2/13/18 21:40 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.41 0.056 1 *8270D 2/13/18 21:40 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 21:40 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 21:40 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.41 0.050 1 *8270D 2/13/18 21:40 JMV P8130242 Fluoranthene BRL mg/kg dry 0.41 0.052 1 *8270D 2/13/18 21:40 JMV P8130242 Fluorene BRL mg/kg dry 0.41 0.059 1 *8270D 2/13/18 21:40 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.41 0.065 1 *8270D 2/13/18 21:40 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.41 0.074 1 *8270D 2/13/18 21:40 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.41 0.073 1 *8270D 2/13/18 21:40 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.41 0.069 1 *8270D 2/13/18 21:40 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.41 0.047 1 *8270D 2/13/18 21:40 JMV P8130242 Isophorone BRL mg/kg dry 0.41 0.055 1 *8270D 2/13/18 21:40 JMV P8130242 Naphthalene BRL mg/kg dry 0.41 0.066 1 *8270D 2/13/18 21:40 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.41 0.058 1 *8270D 2/13/18 21:40 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.41 0.065 1 *8270D 2/13/18 21:40 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.41 0.062 1 *8270D 2/13/18 21:40 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.41 0.048 1 *8270D 2/13/18 21:40 JMV P8130242 Phenanthrene BRL mg/kg dry 0.41 0.053 1 *8270D 2/13/18 21:40 JMV P8130242 Phenol BRL mg/kg dry 0.41 0.060 1 *8270D 2/13/18 21:40 JMV P8130242 Pyrene BRL mg/kg dry 0.41 0.054 1 *8270D 2/13/18 21:40 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 78 % 39-132 2-Fluorobiphenyl 82 % 44-115 2-Fluorophenol 77 % 35-115 Nitrobenzene-d5 74 % 37-122 Phenol-d5 77 % 34-121 Terphenyl-d14 81 % 54-127 Total Metals Mercury 0.042 mg/kg dry 0.025 0.0024 1 *7471B 2/13/18 14:52 JAB P8130234 Arsenic 4.3 mg/kg dry 0.95 0.086 5 *6020B 2/13/18 23:30 EGC 1128130232 Barium 49 mg/kg dry 6.3 0.038 5 *6020B 2113/18 23:30 EGC P8130232 Cadmium BRL mg/kg dry 0.16 0.012 5 *6020B 2/13/18 23:30 EGC P8130232 Chromium 29 mg/kg dry 0.32 0.018 5 *6020B 2113/18 23:30 EGC P8130232 Lead 18 mg/kg dry 0.16 0.036 5 *6020B 2/13/18 23:30 EGC P8B0232 Selenium 0.88 mg/kg dry 0.63 0.13 5 *6020B 2/13/18 23:30 EGC 1128130232 Silver BRL mg/kg dry 0.16 0.012 5 *6020B 2/13/18 23:30 EGC P8130232 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0053 0.00043 1 *8260B 2/12/18 16:09 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 0f 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: UST-6 (2.5-3) Prism Sample ID: 8020190-08 Prism Work Order: 8020190 Time Collected: 02/09/18 13:20 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1-Trichloroethane BRL mg/kg dry 0.0053 0.00025 1 *8260B 2/12/18 16:09 ANG P8130215 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0053 0.00036 1 *8260B 2/12/18 16:09 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0053 0.00047 1 *8260B 2/12/18 16:09 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0053 0.00015 1 *8260B 2/12/18 16:09 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0053 0.00023 1 *8260B 2/12/18 16:09 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0053 0.00029 1 *8260B 2/12/18 16:09 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0053 0.00030 1 *8260B 2/12/18 16:09 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0053 0.00067 1 *8260B 2/12/18 16:09 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0053 0.00039 1 *8260B 2/12/18 16:09 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0053 0.00040 1 *8260B 2/12/18 16:09 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0053 0.00021 1 *8260B 2/12/18 16:09 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0053 0.00025 1 *8260B 2/12/18 16:09 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0053 0.00031 1 *8260B 2/12/18 16:09 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0053 0.00033 1 *8260B 2/12/18 16:09 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0053 0.00040 1 *8260B 2/12/18 16:09 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0053 0.00035 1 *8260B 2/12/18 16:09 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0053 0.00026 1 *8260B 2/12/18 16:09 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0053 0.00021 1 *8260B 2/12/18 16:09 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0053 0.00025 1 *8260B 2/12/18 16:09 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0053 0.00027 1 *8260B 2/12/18 16:09 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0053 0.00031 1 *8260B 2/12/18 16:09 ANG P8130215 4-Isopropyltoluene 0.0055 mg/kg dry 0.0053 0.00025 1 *8260B 2/12/18 16:09 ANG P8130215 Acetone 0.13 mg/kg dry 0.053 0.0013 1 *8260B 2/12/18 16:09 ANG P8130215 Benzene BRL mg/kg dry 0.0032 0.00031 1 *8260B 2/12/18 16:09 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0053 0.00044 1 *8260B 2/12/18 16:09 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0053 0.00029 1 *8260B 2/12/18 16:09 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0053 0.00029 1 *8260B 2/12/18 16:09 ANG P8130215 Bromoform BRL mg/kg dry 0.0053 0.00060 1 *8260B 2/12/18 16:09 ANG P8130215 Bromomethane BRL mg/kg dry 0.011 0.00065 1 *8260B 2/12/18 16:09 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0053 0.00026 1 *8260B 2/12/18 16:09 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0053 0.00028 1 *8260B 2/12/18 16:09 ANG P8130215 Chloroethane BRL mg/kg dry 0.011 0.00044 1 *8260B 2/12/18 16:09 ANG P8130215 Chloroform BRL mg/kg dry 0.0053 0.00038 1 *8260B 2/12/18 16:09 ANG P8130215 Chloromethane BRL mg/kg dry 0.0053 0.00035 1 *8260B 2/12/18 16:09 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0053 0.00022 1 *8260B 2/12/18 16:09 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0053 0.00018 1 *8260B 2/12/18 16:09 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0053 0.00022 1 *8260B 2/12/18 16:09 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0053 0.00024 1 *8260B 2/12/18 16:09 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0053 0.00020 1 *8260B 2/12/18 16:09 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0053 0.00021 1 *8260B 2/12/18 16:09 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0053 0.00031 1 *8260B 2/12/18 16:09 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.011 0.00048 1 *8260B 2/12/18 16:09 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.053 0.00047 1 *8260B 2/12/18 16:09 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 35 0f 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-6 (2.5-3) Attn: Roger Smith Prism Sample ID: 8020190-08 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/09/18 13:20 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.11 0.00047 1 *8260B 2/12/18 16:09 ANG P8130215 Methyl Isobutyl Ketone BRL mg/kg dry 0.053 0.00045 1 *8260B 2/12/18 16:09 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.011 0.00030 1 *8260B 2/12/18 16:09 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.011 0.00017 1 *8260B 2/12/18 16:09 ANG P8130215 Naphthalene BRL mg/kg dry 0.011 0.00017 1 *8260B 2/12/18 16:09 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0053 0.00027 1 *8260B 2/12/18 16:09 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0053 0.00031 1 *8260B 2/12/18 16:09 ANG P8130215 o-Xylene BRL mg/kg dry 0.0053 0.00022 1 *8260B 2/12/18 16:09 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0053 0.00025 1 *8260B 2/12/18 16:09 ANG P8130215 Styrene BRL mg/kg dry 0.0053 0.00032 1 *8260B 2/12/18 16:09 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0053 0.00018 1 *8260B 2/12/18 16:09 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0053 0.00025 1 *8260B 2/12/18 16:09 ANG P8130215 Toluene BRL mg/kg dry 0.0053 0.00030 1 *8260B 2/12/18 16:09 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0053 0.00031 1 *8260B 2/12/18 16:09 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0053 0.00028 1 *8260B 2/12/18 16:09 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0053 0.00034 1 *8260B 2/12/18 16:09 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0053 0.00034 1 *8260B 2/12/18 16:09 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.026 0.00072 1 *8260B 2/12/18 16:09 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0053 0.00025 1 *8260B 2/12/18 16:09 ANG P8130215 Xylenes, total BRL mg/kg dry 0.016 0.00098 1 *8260B 2/12/18 16:09 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 103 % 70-130 Dibromofluoromethane 103 % 84-123 Toluene-d8 94 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 36 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-6 (7.5-10) Attn: Roger Smith Prism Sample ID: 8020190-09 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 15:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 87.0 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.38 0.059 1 *8270D 2/13/18 20:12 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.38 0.058 1 *8270D 2/13/18 20:12 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 20:12 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.38 0.055 1 *8270D 2/13/18 20:12 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.38 0.073 1 *8270D 2/13/18 20:12 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.38 0.071 1 *8270D 2/13/18 20:12 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.38 0.073 1 *8270D 2/13/18 20:12 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.38 0.058 1 *8270D 2/13/18 20:12 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 20:12 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.38 0.046 1 *8270D 2/13/18 20:12 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 20:12 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.38 0.055 1 *8270D 2/13/18 20:12 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.38 0.054 1 *8270D 2/13/18 20:12 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.38 0.061 1 *8270D 2/13/18 20:12 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.38 0.049 1 *8270D 2/13/18 20:12 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.38 0.069 1 *8270D 2/13/18 20:12 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.38 0.075 1 *8270D 2/13/18 20:12 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.38 0.047 1 *8270D 2/13/18 20:12 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.38 0.057 1 *8270D 2/13/18 20:12 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.38 0.065 1 *8270D 2/13/18 20:12 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.38 0.053 1 *8270D 2/13/18 20:12 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.38 0.046 1 *8270D 2/13/18 20:12 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.38 0.049 1 *8270D 2/13/18 20:12 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.38 0.058 1 *8270D 2/13/18 20:12 JMV P8130242 Acenaphthene BRL mg/kg dry 0.38 0.052 1 *8270D 2/13/18 20:12 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.38 0.055 1 *8270D 2/13/18 20:12 JMV P8130242 Anthracene BRL mg/kg dry 0.38 0.061 1 *8270D 2/13/18 20:12 JMV P8130242 Azobenzene BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 20:12 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 20:12 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.38 0.041 1 *8270D 2/13/18 20:12 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.38 0.044 1 *8270D 2/13/18 20:12 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.38 0.042 1 *8270D 2/13/18 20:12 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 20:12 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.38 0.032 1 *8270D 2/13/18 20:12 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 20:12 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.38 0.066 1 *8270D 2/13/18 20:12 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.38 0.054 1 *8270D 2/13/18 20:12 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.38 0.065 1 *8270D 2/13/18 20:12 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.38 0.056 1 *8270D 2/13/18 20:12 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 0f 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-6 (7.5-10) Attn: Roger Smith Prism Sample ID: 8020190-09 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 15:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.38 0.054 1 *8270D 2/13/18 20:12 JMV P8130242 Chrysene BRL mg/kg dry 0.38 0.048 1 *8270D 2/13/18 20:12 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.38 0.046 1 *8270D 2/13/18 20:12 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.38 0.058 1 *8270D 2/13/18 20:12 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.38 0.052 1 *8270D 2/13/18 20:12 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 20:12 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.38 0.054 1 *8270D 2/13/18 20:12 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.38 0.047 1 *8270D 2/13/18 20:12 JMV P8130242 Fluoranthene BRL mg/kg dry 0.38 0.048 1 *8270D 2/13/18 20:12 JMV P8130242 Fluorene BRL mg/kg dry 0.38 0.054 1 *8270D 2/13/18 20:12 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.38 0.060 1 *8270D 2/13/18 20:12 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.38 0.068 1 *8270D 2/13/18 20:12 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.38 0.068 1 *8270D 2/13/18 20:12 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.38 0.064 1 *8270D 2/13/18 20:12 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.38 0.044 1 *8270D 2/13/18 20:12 JMV P8130242 Isophorone BRL mg/kg dry 0.38 0.051 1 *8270D 2/13/18 20:12 JMV P8130242 Naphthalene BRL mg/kg dry 0.38 0.061 1 *8270D 2/13/18 20:12 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.38 0.054 1 *8270D 2/13/18 20:12 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.38 0.060 1 *8270D 2/13/18 20:12 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.38 0.058 1 *8270D 2/13/18 20:12 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.38 0.045 1 *8270D 2/13/18 20:12 JMV P8130242 Phenanthrene BRL mg/kg dry 0.38 0.049 1 *8270D 2/13/18 20:12 JMV P8130242 Phenol BRL mg/kg dry 0.38 0.056 1 *8270D 2/13/18 20:12 JMV P8130242 Pyrene BRL mg/kg dry 0.38 0.050 1 *8270D 2/13/18 20:12 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 89 % 39-132 2-Fluorobiphenyl 90 % 44-115 2-Fluorophenol 83 % 35-115 Nitrobenzene-d5 81 % 37-122 Phenol-d5 83 % 34-121 Terphenyl-d14 90 % 54-127 Total Metals Mercury BRL mg/kg dry 0.024 0.0023 1 *7471 B 2/13/18 14:57 JAB P8130234 Arsenic BRL mg/kg dry 0.87 0.079 5 *6020B 2/13/18 23:38 EGC P8130232 Barium 160 mg/kg dry 5.8 0.035 5 *6020B 2/13/18 23:38 EGC P8130232 Cadmium BRL mg/kg dry 0.15 0.011 5 *6020B 2/13/18 23:38 EGC P8130232 Chromium 1.5 mg/kg dry 0.29 0.016 5 *6020B 2/13/18 23:38 EGC 1128130232 Lead 4.8 mg/kg dry 0.15 0.033 5 *6020B 2/13/18 23:38 EGC 1128130232 Selenium 0.62 mg/kg dry 0.58 0.12 5 *6020B 2/13/18 23:38 EGC P8130232 Silver BRL mg/kg dry 0.15 0.011 5 *6020B 2/13/18 23:38 EGC P8130232 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0058 0.00048 1 *8260B 2/12/18 16:37 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 0f 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: UST-6 (7.5-10) Prism Sample ID: 8020190-09 Prism Work Order: 8020190 Time Collected: 02/08/18 15:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1-Trichloroethane BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 16:37 ANG P8130215 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0058 0.00039 1 *8260B 2/12/18 16:37 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0058 0.00052 1 *8260B 2/12/18 16:37 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0058 0.00016 1 *8260B 2/12/18 16:37 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0058 0.00026 1 *8260B 2/12/18 16:37 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0058 0.00032 1 *8260B 2/12/18 16:37 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0058 0.00033 1 *8260B 2/12/18 16:37 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0058 0.00074 1 *8260B 2/12/18 16:37 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0058 0.00043 1 *8260B 2/12/18 16:37 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0058 0.00045 1 *8260B 2/12/18 16:37 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0058 0.00023 1 *8260B 2/12/18 16:37 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0058 0.00027 1 *8260B 2/12/18 16:37 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 16:37 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0058 0.00036 1 *8260B 2/12/18 16:37 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0058 0.00044 1 *8260B 2/12/18 16:37 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0058 0.00039 1 *8260B 2/12/18 16:37 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0058 0.00029 1 *8260B 2/12/18 16:37 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0058 0.00023 1 *8260B 2/12/18 16:37 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 16:37 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0058 0.00030 1 *8260B 2/12/18 16:37 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 16:37 ANG P8130215 4-Isopropyltoluene BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 16:37 ANG P8130215 Acetone 0.11 mg/kg dry 0.058 0.0014 1 *8260B 2/12/18 16:37 ANG P8130215 Benzene BRL mg/kg dry 0.0035 0.00034 1 *8260B 2/12/18 16:37 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0058 0.00049 1 *8260B 2/12/18 16:37 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0058 0.00032 1 *8260B 2/12/18 16:37 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0058 0.00033 1 *8260B 2/12/18 16:37 ANG P8130215 Bromoform BRL mg/kg dry 0.0058 0.00066 1 *8260B 2/12/18 16:37 ANG P8130215 Bromomethane BRL mg/kg dry 0.012 0.00072 1 *8260B 2/12/18 16:37 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0058 0.00029 1 *8260B 2/12/18 16:37 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0058 0.00031 1 *8260B 2/12/18 16:37 ANG P8130215 Chloroethane BRL mg/kg dry 0.012 0.00049 1 *8260B 2/12/18 16:37 ANG P8130215 Chloroform BRL mg/kg dry 0.0058 0.00042 1 *8260B 2/12/18 16:37 ANG P8130215 Chloromethane BRL mg/kg dry 0.0058 0.00039 1 *8260B 2/12/18 16:37 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0058 0.00025 1 *8260B 2/12/18 16:37 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0058 0.00020 1 *8260B 2/12/18 16:37 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 16:37 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0058 0.00026 1 *8260B 2/12/18 16:37 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0058 0.00022 1 *8260B 2/12/18 16:37 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 16:37 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0058 0.00034 1 *8260B 2/12/18 16:37 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.012 0.00054 1 *8260B 2/12/18 16:37 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.058 0.00053 1 *8260B 2/12/18 16:37 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 39 0f 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: UST-6 (7.5-10) Attn: Roger Smith Prism Sample ID: 8020190-09 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 15:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.12 0.00053 1 *8260B 2/12/18 16:37 ANG P8130215 Methyl Isobutyl Ketone BRL mg/kg dry 0.058 0.00050 1 *8260B 2/12/18 16:37 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.012 0.00033 1 *8260B 2/12/18 16:37 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.012 0.00019 1 *8260B 2/12/18 16:37 ANG P8130215 Naphthalene BRL mg/kg dry 0.012 0.00018 1 *8260B 2/12/18 16:37 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0058 0.00030 1 *8260B 2/12/18 16:37 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 16:37 ANG P8130215 o-Xylene BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 16:37 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 16:37 ANG P8130215 Styrene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 16:37 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0058 0.00020 1 *8260B 2/12/18 16:37 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 16:37 ANG P8130215 Toluene BRL mg/kg dry 0.0058 0.00033 1 *8260B 2/12/18 16:37 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 16:37 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0058 0.00031 1 *8260B 2/12/18 16:37 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0058 0.00038 1 *8260B 2/12/18 16:37 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0058 0.00038 1 *8260B 2/12/18 16:37 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.029 0.00080 1 *8260B 2/12/18 16:37 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 16:37 ANG P8130215 Xylenes, total BRL mg/kg dry 0.017 0.0011 1 *8260B 2/12/18 16:37 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 105 % 84-123 Toluene-d8 94 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 of 67 /PRISM Full -Service Analytical Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Laboratory Report 02/14/2018 Client Sample ID: Background (2.5-3) Prism Sample ID: 8020190-10 Prism Work Order: 8020190 Time Collected: 02/09/18 12:30 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 81.3 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Total Metals Mercury 0.028 mg/kg dry 0.023 0.0022 1 *7471B 2/13/18 15:01 JAB P8130234 Arsenic 1.9 mg/kg dry 0.90 0.082 5 *6020B 2/13/18 23:46 EGC 138130232 Barium 170 mg/kg dry 6.0 0.037 5 *6020B 2/13/18 23:46 EGC 128130232 Cadmium BRL mg/kg dry 0.15 0.011 5 *6020B 2/13/18 23:46 EGC P8130232 Chromium 17 mg/kg dry 0.30 0.017 5 *6020B 2/13/18 23:46 EGC P8130232 Lead 16 mg/kg dry 0.15 0.034 5 *6020B 2113/18 23:46 EGC P8130232 Selenium 1.6 mg/kg dry 0.60 0.12 5 *6020B 2/13/18 23:46 EGC P8130232 Silver BRL mg/kg dry 0.15 0.011 5 *6020B 2/13/18 23:46 EGC P8130232 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 41 of 67 /PRISM Full -Service Analytical Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Laboratory Report 02/14/2018 Client Sample ID: Background (7.5-10) Prism Sample ID: 8020190-11 Prism Work Order: 8020190 Time Collected: 02/09/18 12:45 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 91.3 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Total Metals Mercury BRL mg/kg dry 0.023 0.0022 1 *7471 B 2/13/18 15:06 JAB P8130234 Arsenic BRL mg/kg dry 0.81 0.074 5 *6020B 2/13/18 23:54 EGC P8130232 Barium 240 mg/kg dry 5.4 0.033 5 *6020B 2/13/18 23:54 EGC P8130232 Cadmium BRL mg/kg dry 0.14 0.010 5 *6020B 2/13/18 23:54 EGC P8130232 Chromium 24 mg/kg dry 0.27 0.015 5 *6020B 2/13/18 23:54 EGC P8B0232 Lead 6.0 mg/kg dry 0.14 0.031 5 *6020B 2/13/18 23:54 EGC 138130232 Selenium 1.4 mg/kg dry 0.54 0.11 5 *6020B 2/13/18 23:54 EGC 128130232 Silver 0.14 mg/kg dry 0.14 0.010 5 *6020B 2/13/18 23:54 EGC P8130232 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 42 of 67 Report Full -Service PRISMLaboratory Analytical & Environmental Solutions LABORATORIES INC. 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: Soil-Dup-1 Attn: Roger Smith Prism Sample ID: 8020190-12 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 88.9 % by 0.100 0.100 1 *SM2540 G 2113/18 15:11 BJC P8B0256 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.37 0.058 1 *8270D 2/13/18 20:34 JMV P8130242 1,2-Dichlorobenzene BRL mg/kg dry 0.37 0.056 1 *8270D 2/13/18 20:34 JMV P8130242 1,3-Dichlorobenzene BRL mg/kg dry 0.37 0.052 1 *8270D 2/13/18 20:34 JMV P8130242 1,4-Dichlorobenzene BRL mg/kg dry 0.37 0.054 1 *8270D 2/13/18 20:34 JMV P8130242 1-Methyl naphthalene BRL mg/kg dry 0.37 0.071 1 *8270D 2/13/18 20:34 JMV P8130242 2,4,6-Trichlorophenol BRL mg/kg dry 0.37 0.069 1 *8270D 2/13/18 20:34 JMV P8130242 2,4-Dichlorophenol BRL mg/kg dry 0.37 0.072 1 *8270D 2/13/18 20:34 JMV P8130242 2,4-Dimethylphenol BRL mg/kg dry 0.37 0.057 1 *8270D 2/13/18 20:34 JMV P8130242 2,4-Dinitrophenol BRL mg/kg dry 0.37 0.052 1 *8270D 2/13/18 20:34 JMV P8130242 2,4-Dinitrotoluene BRL mg/kg dry 0.37 0.045 1 *8270D 2/13/18 20:34 JMV P8130242 2,6-Dinitrotoluene BRL mg/kg dry 0.37 0.049 1 *8270D 2/13/18 20:34 JMV P8130242 2-Chloronaphthalene BRL mg/kg dry 0.37 0.054 1 *8270D 2/13/18 20:34 JMV P8130242 2-Chlorophenol BRL mg/kg dry 0.37 0.052 1 *8270D 2/13/18 20:34 JMV P8130242 2-Methyl naphthalene BRL mg/kg dry 0.37 0.059 1 *8270D 2/13/18 20:34 JMV P8130242 2-Methylphenol BRL mg/kg dry 0.37 0.047 1 *8270D 2/13/18 20:34 JMV P8130242 2-Nitrophenol BRL mg/kg dry 0.37 0.067 1 *8270D 2/13/18 20:34 JMV P8130242 3,3'-Dichlorobenzidine BRL mg/kg dry 0.37 0.073 1 *8270D 2/13/18 20:34 JMV P8130242 3/4-Methyl phenol BRL mg/kg dry 0.37 0.046 1 *8270D 2/13/18 20:34 JMV P8130242 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.37 0.056 1 *8270D 2/13/18 20:34 JMV P8130242 4-Bromophenyl phenyl ether BRL mg/kg dry 0.37 0.064 1 *8270D 2/13/18 20:34 JMV P8130242 4-Chloro-3-methylphenol BRL mg/kg dry 0.37 0.052 1 *8270D 2/13/18 20:34 JMV P8130242 4-Chloroaniline BRL mg/kg dry 0.37 0.045 1 *8270D 2/13/18 20:34 JMV P8130242 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.37 0.048 1 *8270D 2/13/18 20:34 JMV P8130242 4-Nitrophenol BRL mg/kg dry 0.37 0.057 1 *8270D 2/13/18 20:34 JMV P8130242 Acenaphthene BRL mg/kg dry 0.37 0.050 1 *8270D 2/13/18 20:34 JMV P8130242 Acenaphthylene BRL mg/kg dry 0.37 0.054 1 *8270D 2/13/18 20:34 JMV P8130242 Anthracene BRL mg/kg dry 0.37 0.060 1 *8270D 2/13/18 20:34 JMV P8130242 Azobenzene BRL mg/kg dry 0.37 0.049 1 *8270D 2/13/18 20:34 JMV P8130242 Benzo(a)anthracene BRL mg/kg dry 0.37 0.048 1 *8270D 2/13/18 20:34 JMV P8130242 Benzo(a)pyrene BRL mg/kg dry 0.37 0.040 1 *8270D 2/13/18 20:34 JMV P8130242 Benzo(b)fluoranthene BRL mg/kg dry 0.37 0.043 1 *8270D 2/13/18 20:34 JMV P8130242 Benzo(g,hJ)perylene BRL mg/kg dry 0.37 0.041 1 *8270D 2/13/18 20:34 JMV P8130242 Benzo(k)fluoranthene BRL mg/kg dry 0.37 0.049 1 *8270D 2/13/18 20:34 JMV P8130242 Benzoic Acid BRL mg/kg dry 0.37 0.031 1 *8270D 2/13/18 20:34 JMV P8130242 Benzyl alcohol BRL mg/kg dry 0.37 0.049 1 *8270D 2/13/18 20:34 JMV P8130242 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.37 0.064 1 *8270D 2/13/18 20:34 JMV P8130242 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.37 0.052 1 *8270D 2/13/18 20:34 JMV P8130242 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.37 0.063 1 *8270D 2/13/18 20:34 JMV P8130242 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.37 0.055 1 *8270D 2/13/18 20:34 JMV P8130242 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 43 0f 67 Report PRISMLaboratory Full -Service Analytical & LABORATORIES INC. Environmental Solutions 02/14/2018 S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: Soil-Dup-1 Attn: Roger Smith Prism Sample ID: 8020190-12 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.37 0.053 1 *8270D 2/13/18 20:34 JMV P8130242 Chrysene BRL mg/kg dry 0.37 0.047 1 *8270D 2/13/18 20:34 JMV P8130242 Dibenzo(a,h)anthracene BRL mg/kg dry 0.37 0.045 1 *8270D 2/13/18 20:34 JMV P8130242 Dibenzofuran BRL mg/kg dry 0.37 0.056 1 *8270D 2/13/18 20:34 JMV P8130242 Diethyl phthalate BRL mg/kg dry 0.37 0.051 1 *8270D 2/13/18 20:34 JMV P8130242 Dimethyl phthalate BRL mg/kg dry 0.37 0.049 1 *8270D 2/13/18 20:34 JMV P8130242 Di-n-butyl phthalate BRL mg/kg dry 0.37 0.053 1 *8270D 2/13/18 20:34 JMV P8130242 Di-n-octyl phthalate BRL mg/kg dry 0.37 0.046 1 *8270D 2/13/18 20:34 JMV P8130242 Fluoranthene BRL mg/kg dry 0.37 0.047 1 *8270D 2/13/18 20:34 JMV P8130242 Fluorene BRL mg/kg dry 0.37 0.053 1 *8270D 2/13/18 20:34 JMV P8130242 Hexachlorobenzene BRL mg/kg dry 0.37 0.059 1 *8270D 2/13/18 20:34 JMV P8130242 Hexachlorobutadiene BRL mg/kg dry 0.37 0.067 1 *8270D 2/13/18 20:34 JMV P8130242 Hexachlorocyclopentadiene BRL mg/kg dry 0.37 0.066 1 *8270D 2/13/18 20:34 JMV P8130242 Hexachloroethane BRL mg/kg dry 0.37 0.062 1 *8270D 2/13/18 20:34 JMV P8130242 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.37 0.043 1 *8270D 2/13/18 20:34 JMV P8130242 Isophorone BRL mg/kg dry 0.37 0.050 1 *8270D 2/13/18 20:34 JMV P8130242 Naphthalene BRL mg/kg dry 0.37 0.060 1 *8270D 2/13/18 20:34 JMV P8130242 Nitrobenzene BRL mg/kg dry 0.37 0.053 1 *8270D 2/13/18 20:34 JMV P8130242 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.37 0.058 1 *8270D 2/13/18 20:34 JMV P8130242 N-Nitrosodiphenylamine BRL mg/kg dry 0.37 0.056 1 *8270D 2/13/18 20:34 JMV P8130242 Pentachlorophenol BRL mg/kg dry 0.37 0.044 1 *8270D 2/13/18 20:34 JMV P8130242 Phenanthrene BRL mg/kg dry 0.37 0.048 1 *8270D 2/13/18 20:34 JMV P8130242 Phenol BRL mg/kg dry 0.37 0.055 1 *8270D 2/13/18 20:34 JMV P8130242 Pyrene BRL mg/kg dry 0.37 0.049 1 *8270D 2/13/18 20:34 JMV P8130242 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 79 % 39-132 2-Fluorobiphenyl 80 % 44-115 2-Fluorophenol 75 % 35-115 Nitrobenzene-d5 74 % 37-122 Phenol-d5 73 % 34-121 Terphenyl-d14 80 % 54-127 Total Metals Mercury BRL mg/kg dry 0.024 0.0022 1 *7471B 2/13/18 15:10 JAB P8130234 Arsenic 0.85 mg/kg dry 0.85 0.077 5 *6020B 2/14/18 0:02 EGC P8B0232 Barium 77 mg/kg dry 5.7 0.035 5 *6020B 2/14/18 0:02 EGC P8130232 Cadmium BRL mg/kg dry 0.14 0.011 5 *6020B 2/14/18 0:02 EGC P8130232 Chromium 1.2 mg/kg dry 0.28 0.016 5 *6020B 2/14/18 0:02 EGC 1138130232 Lead 4.6 mg/kg dry 0.14 0.032 5 *6020B 2/14/18 0:02 EGC P8130232 Selenium 1.2 mg/kg dry 0.57 0.12 5 *6020B 2/14/18 0:02 EGC P8130232 Silver BRL mg/kg dry 0.14 0.011 5 *6020B 2/14/18 0:02 EGC P8130232 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0058 0.00048 1 *8260B 2/12/18 17:05 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 44 0f 67 Full -Service Analytical & PRISMLaboratory Environmental Solutions LABORATORIES INC. S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Sample Matrix: Solid Report 02/14/2018 Client Sample ID: Soil-Dup-1 Prism Sample ID: 8020190-12 Prism Work Order: 8020190 Time Collected: 02/08/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1-Trichloroethane BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 17:05 ANG P8130215 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0058 0.00039 1 *8260B 2/12/18 17:05 ANG P8130215 1,1,2-Trichloroethane BRL mg/kg dry 0.0058 0.00051 1 *8260B 2/12/18 17:05 ANG P8130215 1,1-Dichloroethane BRL mg/kg dry 0.0058 0.00016 1 *8260B 2/12/18 17:05 ANG P8130215 1,1-Dichloroethylene BRL mg/kg dry 0.0058 0.00026 1 *8260B 2/12/18 17:05 ANG P8130215 1,1-Dichloropropylene BRL mg/kg dry 0.0058 0.00032 1 *8260B 2/12/18 17:05 ANG P8130215 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0058 0.00033 1 *8260B 2/12/18 17:05 ANG P8130215 1,2,3-Trichloropropane BRL mg/kg dry 0.0058 0.00074 1 *8260B 2/12/18 17:05 ANG P8130215 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0058 0.00043 1 *8260B 2/12/18 17:05 ANG P8130215 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0058 0.00044 1 *8260B 2/12/18 17:05 ANG P8130215 1,2-Dibromoethane BRL mg/kg dry 0.0058 0.00023 1 *8260B 2/12/18 17:05 ANG P8130215 1,2-Dichlorobenzene BRL mg/kg dry 0.0058 0.00027 1 *8260B 2/12/18 17:05 ANG P8130215 1,2-Dichloroethane BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 17:05 ANG P8130215 1,2-Dichloropropane BRL mg/kg dry 0.0058 0.00036 1 *8260B 2/12/18 17:05 ANG P8130215 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0058 0.00044 1 *8260B 2/12/18 17:05 ANG P8130215 1,3-Dichlorobenzene BRL mg/kg dry 0.0058 0.00038 1 *8260B 2/12/18 17:05 ANG P8130215 1,3-Dichloropropane BRL mg/kg dry 0.0058 0.00029 1 *8260B 2/12/18 17:05 ANG P8130215 1,4-Dichlorobenzene BRL mg/kg dry 0.0058 0.00023 1 *8260B 2/12/18 17:05 ANG P8130215 2,2-Dichloropropane BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 17:05 ANG P8130215 2-Chlorotoluene BRL mg/kg dry 0.0058 0.00030 1 *8260B 2/12/18 17:05 ANG P8130215 4-Chlorotoluene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 17:05 ANG P8130215 4-Isopropyltoluene BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 17:05 ANG P8130215 Acetone 0.058 mg/kg dry 0.058 0.0014 1 *8260B 2/12/18 17:05 ANG P8130215 Benzene BRL mg/kg dry 0.0035 0.00034 1 *8260B 2/12/18 17:05 ANG P8130215 Bromobenzene BRL mg/kg dry 0.0058 0.00048 1 *8260B 2/12/18 17:05 ANG P8130215 Bromochloromethane BRL mg/kg dry 0.0058 0.00032 1 *8260B 2/12/18 17:05 ANG P8130215 Bromodichloromethane BRL mg/kg dry 0.0058 0.00032 1 *8260B 2/12/18 17:05 ANG P8130215 Bromoform BRL mg/kg dry 0.0058 0.00066 1 *8260B 2/12/18 17:05 ANG P8130215 Bromomethane BRL mg/kg dry 0.012 0.00072 1 *8260B 2/12/18 17:05 ANG P8130215 Carbon Tetrachloride BRL mg/kg dry 0.0058 0.00029 1 *8260B 2/12/18 17:05 ANG P8130215 Chlorobenzene BRL mg/kg dry 0.0058 0.00031 1 *8260B 2/12/18 17:05 ANG P8130215 Chloroethane BRL mg/kg dry 0.012 0.00048 1 *8260B 2/12/18 17:05 ANG P8130215 Chloroform BRL mg/kg dry 0.0058 0.00042 1 *8260B 2/12/18 17:05 ANG P8130215 Chloromethane BRL mg/kg dry 0.0058 0.00039 1 *8260B 2/12/18 17:05 ANG P8130215 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0058 0.00025 1 *8260B 2/12/18 17:05 ANG P8130215 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0058 0.00019 1 *8260B 2/12/18 17:05 ANG P8130215 Dibromochloromethane BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 17:05 ANG P8130215 Dichlorodifluoromethane BRL mg/kg dry 0.0058 0.00026 1 *8260B 2/12/18 17:05 ANG P8130215 Ethylbenzene BRL mg/kg dry 0.0058 0.00022 1 *8260B 2/12/18 17:05 ANG P8130215 Isopropyl Ether BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 17:05 ANG P8130215 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0058 0.00034 1 *8260B 2/12/18 17:05 ANG P8130215 m,p-Xylenes BRL mg/kg dry 0.012 0.00053 1 *8260B 2/12/18 17:05 ANG P8130215 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.058 0.00052 1 *8260B 2/12/18 17:05 ANG P8130215 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 45 0f 67 PRISMLaboratory Report Full -Service Analytical & Environmental Solutions 02/14/2018 LABORATORIES INC. S&ME, Inc - Charlotte Project: Homewood Banks Client Sample ID: Soil-Dup-1 Attn: Roger Smith Prism Sample ID: 8020190-12 9751 Southern Pine Blvd. Prism Work Order: 8020190 Charlotte, NC 28273 Sample Matrix: Solid Time Collected: 02/08/18 00:00 Time Submitted: 02/10/18 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.12 0.00052 1 *8260B 2/12/18 17:05 ANG P8130215 Methyl Isobutyl Ketone BRL mg/kg dry 0.058 0.00049 1 *8260B 2/12/18 17:05 ANG P8130215 Methylene Chloride BRL mg/kg dry 0.012 0.00033 1 *8260B 2/12/18 17:05 ANG P8130215 Methyl-tert-Butyl Ether BRL mg/kg dry 0.012 0.00019 1 *8260B 2/12/18 17:05 ANG P8130215 Naphthalene BRL mg/kg dry 0.012 0.00018 1 *8260B 2/12/18 17:05 ANG P8130215 n-Butylbenzene BRL mg/kg dry 0.0058 0.00030 1 *8260B 2/12/18 17:05 ANG P8130215 n-Propylbenzene BRL mg/kg dry 0.0058 0.00034 1 *8260B 2/12/18 17:05 ANG P8130215 o-Xylene BRL mg/kg dry 0.0058 0.00024 1 *8260B 2/12/18 17:05 ANG P8130215 sec-Butylbenzene BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 17:05 ANG P8130215 Styrene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 17:05 ANG P8130215 tert-Butylbenzene BRL mg/kg dry 0.0058 0.00020 1 *8260B 2/12/18 17:05 ANG P8130215 Tetrachloroethylene BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 17:05 ANG P8130215 Toluene BRL mg/kg dry 0.0058 0.00033 1 *8260B 2/12/18 17:05 ANG P8130215 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0058 0.00035 1 *8260B 2/12/18 17:05 ANG P8130215 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0058 0.00030 1 *8260B 2/12/18 17:05 ANG P8130215 Trichloroethylene BRL mg/kg dry 0.0058 0.00038 1 *8260B 2/12/18 17:05 ANG P8130215 Trichlorofluoromethane BRL mg/kg dry 0.0058 0.00037 1 *8260B 2/12/18 17:05 ANG P8130215 Vinyl acetate BRL mg/kg dry 0.029 0.00079 1 *8260B 2/12/18 17:05 ANG P8130215 Vinyl chloride BRL mg/kg dry 0.0058 0.00028 1 *8260B 2/12/18 17:05 ANG P8130215 Xylenes, total BRL mg/kg dry 0.017 0.0011 1 *8260B 2/12/18 17:05 ANG P8130215 Surrogate Recovery Control Limits 4-Bromofluorobenzene 98 % 70-130 Dibromofluoromethane 106 % 84-123 Toluene-d8 92 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 46 of 67 P R I IS M EService Analytical Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Project: Homewood Banks Prism Work Order: 8020190 Attn: Roger Smith Time Submitted: 2/10/2018 9:55:OOAM 9751 Southern Pine Blvd. Charlotte, NC 28273 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P860215 - 5035 Blank (M0215-131-K1) Prepared &Analyzed: 02/12/18 1,1,1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Trimethyl benzene BRL 0.0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethyl benzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.0050 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 47 0f 67 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130215 - 5035 Reporting Result Limit Units Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P8130215-BLK1) Prepared &Analyzed: 02/12/18 Methylene Chloride BRL 0.010 mg/kg wet Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butyl benzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans- 1,2-Dichloroethylene BRL 0.0050 mg/kg wet trans- 1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0.0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0.0050 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate:4-Bromofluorobenzene 52.4 ug/L 50.00 105 70-130 Surrogate: Dibromofluoromethane 49.0 ug/L 50.00 98 84-123 Surrogate: Toluene-d8 47.0 ug/L 50.00 94 76-129 LCS (P860215-BS1) Prepared &Analyzed: 02/12/18 1,1,1,2-Tetrachloroethane 0.0515 0.0050 mg/kg wet 0.05000 103 72-115 1,1,1-Trichloroethane 0.0502 0.0050 mg/kg wet 0.05000 100 67-131 1,1,2,2-Tetrachloroethane 0.0445 0.0050 mg/kg wet 0.05000 89 56-126 1,1,2-Trichloroethane 0.0489 0.0050 mg/kg wet 0.05000 98 70-133 1,1-Dichloroethane 0.0507 0.0050 mg/kg wet 0.05000 101 74-127 1,1-Dichloroethylene 0.0554 0.0050 mg/kg wet 0.05000 ill 67-149 1, 1 -Dichloropropylene 0.0552 0.0050 mg/kg wet 0.05000 110 71-130 1,2,3-Trichlorobenzene 0.0453 0.0050 mg/kg wet 0.05000 91 68-130 1,2,3-Trichloropropane 0.0450 0.0050 mg/kg wet 0.05000 90 60-137 1,2,4-Trichlorobenzene 0.0470 0.0050 mg/kg wet 0.05000 94 66-125 1,2,4-Trimethylbenzene 0.0471 0.0050 mg/kg wet 0.05000 94 69-129 1,2-Dibromoethane 0.0477 0.0050 mg/kg wet 0.05000 95 70-132 1,2-Dichlorobenzene 0.0463 0.0050 mg/kg wet 0.05000 93 72-123 1,2-Dichloroethane 0.0507 0.0050 mg/kg wet 0.05000 101 68-128 1,2-Dichloropropane 0.0529 0.0050 mg/kg wet 0.05000 106 73-130 1,3,5-Trimethylbenzene 0.0465 0.0050 mg/kg wet 0.05000 93 69-128 1,3-Dichlorobenzene 0.0453 0.0050 mg/kg wet 0.05000 91 71-120 1,3-Dichloropropane 0.0489 0.0050 mg/kg wet 0.05000 98 75-124 1,4-Dichlorobenzene 0.0464 0.0050 mg/kg wet 0.05000 93 71-123 2,2-Dichloropropane 0.0523 0.0050 mg/kg wet 0.05000 105 50-142 2-Chlorotoluene 0.0471 0.0050 mg/kg wet 0.05000 94 67-124 4-Chlorotoluene 0.0467 0.0050 mg/kg wet 0.05000 93 71-126 4-Isopropyltoluene 0.0456 0.0050 mg/kg wet 0.05000 91 68-129 Acetone 0.106 0.050 mg/kg wet 0.1000 106 29-198 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 48 0f 67 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P8130215 - 5035 Reporting Result Limit Units Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P8B0215-BS1) Prepared &Analyzed: 02/12/18 Benzene 0.0514 0.0030 mg/kg wet 0.05000 103 74-127 Bromobenzene 0.0453 0.0050 mg/kg wet 0.05000 91 73-125 Bromochloromethane 0.0508 0.0050 mg/kg wet 0.05000 102 72-134 Bromodichloromethane 0.0518 0.0050 mg/kg wet 0.05000 104 75-122 Bromoform 0.0494 0.0050 mg/kg wet 0.05000 99 66-135 Bromomethane 0.0512 0.010 mg/kg wet 0.05000 102 20-180 Carbon Tetrachloride 0.0523 0.0050 mg/kg wet 0.05000 105 64-143 Chlorobenzene 0.0490 0.0050 mg/kg wet 0.05000 98 74-118 Chloroethane 0.0446 0.010 mg/kg wet 0.05000 89 33-149 Chloroform 0.0550 0.0050 mg/kg wet 0.05000 110 73-127 Chloromethane 0.0507 0.0050 mg/kg wet 0.05000 101 45-143 cis-1,2-Dichloroethylene 0.0526 0.0050 mg/kg wet 0.05000 105 76-134 cis-1,3-Dichloropropylene 0.0545 0.0050 mg/kg wet 0.05000 109 71-125 Dibromochloromethane 0.0492 0.0050 mg/kg wet 0.05000 98 73-122 Dichlorodifluoromethane 0.0397 0.0050 mg/kg wet 0.05000 79 26-146 Ethylbenzene 0.0508 0.0050 mg/kg wet 0.05000 102 74-128 Isopropyl Ether 0.0509 0.0050 mg/kg wet 0.05000 102 59-159 Isopropylbenzene (Cumene) 0.0474 0.0050 mg/kg wet 0.05000 95 68-126 m,p-Xylenes 0.102 0.010 mg/kg wet 0.1000 102 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0482 0.050 mg/kg wet 0.05000 96 61-157 Methyl Ethyl Ketone (2-Butanone) 0.0519 0.10 mg/kg wet 0.05000 104 63-149 Methyl Isobutyl Ketone 0.0522 0.050 mg/kg wet 0.05000 104 57-162 Methylene Chloride 0.0527 0.010 mg/kg wet 0.05000 105 74-129 Methyl-tert-Butyl Ether 0.0529 0.010 mg/kg wet 0.05000 106 70-130 Naphthalene 0.0445 0.010 mg/kg wet 0.05000 89 57-157 n-Butylbenzene 0.0473 0.0050 mg/kg wet 0.05000 95 65-135 n-Propylbenzene 0.0474 0.0050 mg/kg wet 0.05000 95 67-130 o-Xylene 0.0503 0.0050 mg/kg wet 0.05000 101 74-126 sec-Butylbenzene 0.0470 0.0050 mg/kg wet 0.05000 94 66-131 Styrene 0.0514 0.0050 mg/kg wet 0.05000 103 77-121 tert-Butyl benzene 0.0463 0.0050 mg/kg wet 0.05000 93 67-132 Tetrachloroethylene 0.0517 0.0050 mg/kg wet 0.05000 103 68-130 Toluene 0.0519 0.0050 mg/kg wet 0.05000 104 71-129 trans- 1,2-Dichloroethylene 0.0522 0.0050 mg/kg wet 0.05000 104 73-132 trans- 1,3-Dichloropropylene 0.0534 0.0050 mg/kg wet 0.05000 107 68-123 Trichloroethylene 0.0525 0.0050 mg/kg wet 0.05000 105 75-133 Trichlorofluoromethane 0.0598 0.0050 mg/kg wet 0.05000 120 44-146 Vinyl acetate 0.0591 0.025 mg/kg wet 0.05000 118 85-161 Vinyl chloride 0.0502 0.0050 mg/kg wet 0.05000 100 48-147 Xylenes, total 0.152 0.015 mg/kg wet 0.1500 102 74-126 Surrogate:4-Bromofluorobenzene 48.8 ug/L 50.00 98 70-130 Surrogate: Dibromofluoromethane 47.6 ug/L 50.00 95 84-123 Surrogate: Toluene-d8 46.8 ug/L 50.00 94 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 49 0f 67 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8130215 - 5035 LCS Dup (P8B0215-BSD1) Prepared &Analyzed: 02/12/18 1,1,1,2-Tetrachloroethane 0.0508 0.0050 mg/kg wet 0.05000 102 72-115 2 20 1,1,1-Trichloroethane 0.0483 0.0050 mg/kg wet 0.05000 97 67-131 4 20 1,1,2,2-Tetrachloroethane 0.0463 0.0050 mg/kg wet 0.05000 93 56-126 4 20 1,1,2-Trichloroethane 0.0494 0.0050 mg/kg wet 0.05000 99 70-133 1 20 1,1-Dichloroethane 0.0492 0.0050 mg/kg wet 0.05000 98 74-127 3 20 1,1-Dichloroethylene 0.0560 0.0050 mg/kg wet 0.05000 112 67-149 1 20 1, 1 -Dichloropropylene 0.0530 0.0050 mg/kg wet 0.05000 106 71-130 4 20 1,2,3-Trichlorobenzene 0.0466 0.0050 mg/kg wet 0.05000 93 68-130 3 20 1,2,3-Trichloropropane 0.0454 0.0050 mg/kg wet 0.05000 91 60-137 0.9 20 1,2,4-Trichlorobenzene 0.0468 0.0050 mg/kg wet 0.05000 94 66-125 0.4 20 1,2,4-Trimethylbenzene 0.0467 0.0050 mg/kg wet 0.05000 93 69-129 0.9 20 1,2-Dibromoethane 0.0494 0.0050 mg/kg wet 0.05000 99 70-132 3 20 1,2-Dichlorobenzene 0.0465 0.0050 mg/kg wet 0.05000 93 72-123 0.3 20 1,2-Dichloroethane 0.0511 0.0050 mg/kg wet 0.05000 102 68-128 0.8 20 1,2-Dichloropropane 0.0528 0.0050 mg/kg wet 0.05000 106 73-130 0.2 20 1,3,5-Trimethylbenzene 0.0461 0.0050 mg/kg wet 0.05000 92 69-128 0.9 20 1,3-Dichlorobenzene 0.0458 0.0050 mg/kg wet 0.05000 92 71-120 1 20 1,3-Dichloropropane 0.0496 0.0050 mg/kg wet 0.05000 99 75-124 1 20 1,4-Dichlorobenzene 0.0463 0.0050 mg/kg wet 0.05000 93 71-123 0.2 20 2,2-Dichloropropane 0.0501 0.0050 mg/kg wet 0.05000 100 50-142 4 20 2-Chlorotoluene 0.0462 0.0050 mg/kg wet 0.05000 92 67-124 2 20 4-Chlorotoluene 0.0463 0.0050 mg/kg wet 0.05000 93 71-126 0.8 20 4-Isopropyltoluene 0.0442 0.0050 mg/kg wet 0.05000 88 68-129 3 20 Acetone 0.110 0.050 mg/kg wet 0.1000 110 29-198 4 20 Benzene 0.0505 0.0030 mg/kg wet 0.05000 101 74-127 2 20 Bromobenzene 0.0456 0.0050 mg/kg wet 0.05000 91 73-125 0.7 20 Bromochloromethane 0.0504 0.0050 mg/kg wet 0.05000 101 72-134 0.7 20 Bromodichloromethane 0.0526 0.0050 mg/kg wet 0.05000 105 75-122 1 20 Bromoform 0.0500 0.0050 mg/kg wet 0.05000 100 66-135 1 20 Bromomethane 0.0534 0.010 mg/kg wet 0.05000 107 20-180 4 20 Carbon Tetrachloride 0.0518 0.0050 mg/kg wet 0.05000 104 64-143 1 20 Chlorobenzene 0.0484 0.0050 mg/kg wet 0.05000 97 74-118 1 20 Chloroethane 0.0426 0.010 mg/kg wet 0.05000 85 33-149 5 20 Chloroform 0.0533 0.0050 mg/kg wet 0.05000 107 73-127 3 20 Chloromethane 0.0500 0.0050 mg/kg wet 0.05000 100 45-143 1 20 cis-1,2-Dichloroethylene 0.0518 0.0050 mg/kg wet 0.05000 104 76-134 1 20 cis-1,3-Dichloropropylene 0.0546 0.0050 mg/kg wet 0.05000 109 71-125 0.07 20 Dibromochloromethane 0.0496 0.0050 mg/kg wet 0.05000 99 73-122 0.9 20 Dichlorodifluoromethane 0.0380 0.0050 mg/kg wet 0.05000 76 26-146 4 20 Ethylbenzene 0.0492 0.0050 mg/kg wet 0.05000 98 74-128 3 20 Isopropyl Ether 0.0520 0.0050 mg/kg wet 0.05000 104 59-159 2 20 Isopropylbenzene (Cumene) 0.0462 0.0050 mg/kg wet 0.05000 92 68-126 2 20 m,p-Xylenes 0.0991 0.010 mg/kg wet 0.1000 99 75-124 3 20 Methyl Butyl Ketone (2-Hexanone) 0.0502 0.050 mg/kg wet 0.05000 100 61-157 4 20 Methyl Ethyl Ketone (2-Butanone) 0.0533 0.10 mg/kg wet 0.05000 107 63-149 3 20 Methyl Isobutyl Ketone 0.0547 0.050 mg/kg wet 0.05000 109 57-162 5 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 50 0f 67 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81130215 - 5035 LCS Dup (P8B0215-BSD1) Prepared &Analyzed: 02/12/18 Methylene Chloride 0.0525 0.010 mg/kg wet 0.05000 105 74-129 0.4 20 Methyl-tert-Butyl Ether 0.0509 0.010 mg/kg wet 0.05000 102 70-130 4 20 Naphthalene 0.0467 0.010 mg/kg wet 0.05000 93 57-157 5 20 n-Butylbenzene 0.0467 0.0050 mg/kg wet 0.05000 93 65-135 1 20 n-Propylbenzene 0.0466 0.0050 mg/kg wet 0.05000 93 67-130 2 20 o-Xylene 0.0488 0.0050 mg/kg wet 0.05000 98 74-126 3 20 sec-Butylbenzene 0.0462 0.0050 mg/kg wet 0.05000 92 66-131 2 20 Styrene 0.0501 0.0050 mg/kg wet 0.05000 100 77-121 3 20 tert-Butyl benzene 0.0460 0.0050 mg/kg wet 0.05000 92 67-132 0.8 20 Tetrachloroethylene 0.0514 0.0050 mg/kg wet 0.05000 103 68-130 0.6 20 Toluene 0.0507 0.0050 mg/kg wet 0.05000 101 71-129 2 20 trans- 1,2-Dichloroethylene 0.0504 0.0050 mg/kg wet 0.05000 101 73-132 3 20 trans- 1,3-Dichloropropylene 0.0537 0.0050 mg/kg wet 0.05000 107 68-123 0.5 20 Trichloroethylene 0.0511 0.0050 mg/kg wet 0.05000 102 75-133 3 20 Trichlorofluoromethane 0.0572 0.0050 mg/kg wet 0.05000 114 44-146 4 20 Vinyl acetate 0.0578 0.025 mg/kg wet 0.05000 116 85-161 2 20 Vinyl chloride 0.0487 0.0050 mg/kg wet 0.05000 97 48-147 3 20 Xylenes, total 0.148 0.015 mg/kg wet 0.1500 99 74-126 3 20 Surrogate:4-Bromofluorobenzene 49.2 ug/L 50.00 98 70-130 Surrogate: Dibromofluoromethane 49.6 ug/L 50.00 99 84-123 Surrogate: Toluene-d8 46.0 ug/L 50.00 92 76-129 Matrix Spike (P8B0215-MS1) Source: 8020190-01 Prepared &Analyzed: 02/12/18 1,1,1,2-Tetrachloroethane 0.0368 0.0056 mg/kg dry 0.05558 BRL 66 60-120 1,1,1-Trichloroethane 0.0413 0.0056 mg/kg dry 0.05558 BRL 74 52-139 1,1,2,2-Tetrachloroethane 0.0288 0.0056 mg/kg dry 0.05558 BRL 52 39-135 1,1,2-Trichloroethane 0.0334 0.0056 mg/kg dry 0.05558 BRL 60 44-140 1,1-Dichloroethane 0.0404 0.0056 mg/kg dry 0.05558 BRL 73 59-137 1,1-Dichloroethylene 0.0483 0.0056 mg/kg dry 0.05558 BRL 87 54-162 1, 1 -Dichloropropylene 0.0453 0.0056 mg/kg dry 0.05558 BRL 82 55-137 1,2,3-Trichlorobenzene 0.0302 0.0056 mg/kg dry 0.05558 BRL 54 34-120 1,2,3-Trichloropropane 0.0290 0.0056 mg/kg dry 0.05558 BRL 52 45-139 1,2,4-Trichlorobenzene 0.0310 0.0056 mg/kg dry 0.05558 BRL 56 35-116 1,2,4-Trimethylbenzene 0.0334 0.0056 mg/kg dry 0.05558 BRL 60 38-142 1,2-Dibromoethane 0.0324 0.0056 mg/kg dry 0.05558 BRL 58 49-132 1,2-Dichlorobenzene 0.0324 0.0056 mg/kg dry 0.05558 BRL 58 42-130 1,2-Dichloroethane 0.0368 0.0056 mg/kg dry 0.05558 BRL 66 51-131 1,2-Dichloropropane 0.0397 0.0056 mg/kg dry 0.05558 BRL 71 55-138 1,3,5-Trimethylbenzene 0.0338 0.0056 mg/kg dry 0.05558 BRL 61 44-140 1,3-Dichlorobenzene 0.0321 0.0056 mg/kg dry 0.05558 BRL 58 41-129 1,3-Dichloropropane 0.0342 0.0056 mg/kg dry 0.05558 BRL 62 53-129 1,4-Dichlorobenzene 0.0329 0.0056 mg/kg dry 0.05558 BRL 59 44-134 2,2-Dichloropropane 0.0411 0.0056 mg/kg dry 0.05558 BRL 74 30-147 2-Chlorotoluene 0.0336 0.0056 mg/kg dry 0.05558 BRL 61 46-132 4-Chlorotoluene 0.0336 0.0056 mg/kg dry 0.05558 BRL 60 44-135 4-Isopropyltoluene 0.0334 0.0056 mg/kg dry 0.05558 BRL 60 32-144 Acetone 0.0956 0.056 mg/kg dry 0.1112 0.00870 78 34-143 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 51 0f 67 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P8130215 - 5035 Reporting Result Limit Units Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike (P8B0215-MS1) Source: 8020190-01 Prepared &Analyzed: 02/12/18 Benzene 0.0409 0.0033 mg/kg dry 0.05558 BRL 74 60-135 Bromobenzene 0.0313 0.0056 mg/kg dry 0.05558 BRL 56 45-135 Bromochloromethane 0.0393 0.0056 mg/kg dry 0.05558 BRL 71 55-136 Bromodichloromethane 0.0388 0.0056 mg/kg dry 0.05558 BRL 70 55-127 Bromoform 0.0340 0.0056 mg/kg dry 0.05558 BRL 61 40-136 Bromomethane 0.0474 0.011 mg/kg dry 0.05558 BRL 85 30-137 Carbon Tetrachloride 0.0446 0.0056 mg/kg dry 0.05558 BRL 80 48-153 Chlorobenzene 0.0362 0.0056 mg/kg dry 0.05558 BRL 65 57-125 Chloroethane 0.0475 0.011 mg/kg dry 0.05558 BRL 85 16-177 Chloroform 0.0428 0.0056 mg/kg dry 0.05558 BRL 77 56-137 Chloromethane 0.0476 0.0056 mg/kg dry 0.05558 BRL 86 40-145 cis-1,2-Dichloroethylene 0.0410 0.0056 mg/kg dry 0.05558 BRL 74 58-140 cis-1,3-Dichloropropylene 0.0396 0.0056 mg/kg dry 0.05558 BRL 71 42-135 Dibromochloromethane 0.0344 0.0056 mg/kg dry 0.05558 BRL 62 49-127 Dichlorodifluoromethane 0.0509 0.0056 mg/kg dry 0.05558 BRL 92 25-151 Ethylbenzene 0.0375 0.0056 mg/kg dry 0.05558 BRL 68 44-144 Isopropyl Ether 0.0369 0.0056 mg/kg dry 0.05558 BRL 66 51-155 Isopropylbenzene (Cumene) 0.0354 0.0056 mg/kg dry 0.05558 BRL 64 41-140 m,p-Xylenes 0.0747 0.011 mg/kg dry 0.1112 BRL 67 36-148 Methyl Butyl Ketone (2-Hexanone) 0.0289 0.056 mg/kg dry 0.05558 BRL 52 30-147 Methyl Ethyl Ketone (2-Butanone) 0.0330 0.11 mg/kg dry 0.05558 BRL 59 24-160 Methyl Isobutyl Ketone 0.0328 0.056 mg/kg dry 0.05558 BRL 59 25-163 Methylene Chloride 0.0421 0.011 mg/kg dry 0.05558 BRL 76 53-144 Methyl-tert-Butyl Ether 0.0390 0.011 mg/kg dry 0.05558 BRL 70 49-135 Naphthalene 0.0289 0.011 mg/kg dry 0.05558 BRL 52 32-127 n-Butylbenzene 0.0344 0.0056 mg/kg dry 0.05558 BRL 62 23-148 n-Propylbenzene 0.0344 0.0056 mg/kg dry 0.05558 BRL 62 35-144 o-Xylene 0.0367 0.0056 mg/kg dry 0.05558 BRL 66 43-143 sec-Butylbenzene 0.0354 0.0056 mg/kg dry 0.05558 BRL 64 34-144 Styrene 0.0370 0.0056 mg/kg dry 0.05558 BRL 67 42-132 tert-Butyl benzene 0.0344 0.0056 mg/kg dry 0.05558 BRL 62 36-150 Tetrachloroethylene 0.0402 0.0056 mg/kg dry 0.05558 BRL 72 47-142 Toluene 0.0408 0.0056 mg/kg dry 0.05558 BRL 73 57-135 trans- 1,2-Dichloroethylene 0.0422 0.0056 mg/kg dry 0.05558 BRL 76 58-141 trans- 1,3-Dichloropropylene 0.0376 0.0056 mg/kg dry 0.05558 BRL 68 41-124 Trichloroethylene 0.0417 0.0056 mg/kg dry 0.05558 BRL 75 38-164 Trichlorofluoromethane 0.0496 0.0056 mg/kg dry 0.05558 BRL 89 30-157 Vinyl acetate 0.0398 0.028 mg/kg dry 0.05558 BRL 72 61-154 Vinyl chloride 0.0488 0.0056 mg/kg dry 0.05558 BRL 88 40-156 Xylenes, total 0.111 0.017 mg/kg dry 0.1667 BRL 67 36-148 Surrogate:4-Bromofluorobenzene 48.8 ug/L 50.00 98 70-130 Surrogate: Dibromofluoromethane 48.4 ug/L 50.00 97 84-123 Surrogate: Toluene-d8 45.4 ug/L 50.00 91 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 52 0f 67 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Volatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P8130215 - 5035 Matrix Spike Dup (P8B0215-MSD1) Source: 8020190-01 Prepared &Analyzed: 02/12/18 1,1,1,2-Tetrachloroethane 0.0265 0.0056 mg/kg dry 0.05604 BRL 47 60-120 33 15 D, M 1,1,1-Trichloroethane 0.0221 0.0056 mg/kg dry 0.05604 BRL 39 52-139 61 21 D, M 1,1,2,2-Tetrachloroethane 0.0332 0.0056 mg/kg dry 0.05604 BRL 59 39-135 14 22 1,1,2-Trichloroethane 0.0310 0.0056 mg/kg dry 0.05604 BRL 55 44-140 7 21 1,1-Dichloroethane 0.0242 0.0056 mg/kg dry 0.05604 BRL 43 59-137 50 21 D, M 1,1-Dichloroethylene 0.0160 0.0056 mg/kg dry 0.05604 BRL 29 54-162 100 22 D, M 1, 1 -Dichloropropylene 0.0238 0.0056 mg/kg dry 0.05604 BRL 43 55-137 62 19 D, M 1,2,3-Trichlorobenzene 0.0258 0.0056 mg/kg dry 0.05604 BRL 46 34-120 16 41 1,2,3-Trichloropropane 0.0338 0.0056 mg/kg dry 0.05604 BRL 60 45-139 15 25 1,2,4-Trichlorobenzene 0.0239 0.0056 mg/kg dry 0.05604 BRL 43 35-116 26 62 1,2,4-Trimethylbenzene 0.0217 0.0056 mg/kg dry 0.05604 BRL 39 38-142 43 24 D 1,2-Dibromoethane 0.0329 0.0056 mg/kg dry 0.05604 BRL 59 49-132 2 15 1,2-Dichlorobenzene 0.0252 0.0056 mg/kg dry 0.05604 BRL 45 42-130 25 21 D 1,2-Dichloroethane 0.0332 0.0056 mg/kg dry 0.05604 BRL 59 51-131 10 13 1,2-Dichloropropane 0.0281 0.0056 mg/kg dry 0.05604 BRL 50 55-138 34 16 D, M 1,3,5-Trimethylbenzene 0.0199 0.0056 mg/kg dry 0.05604 BRL 36 44-140 52 29 D, M 1,3-Dichlorobenzene 0.0228 0.0056 mg/kg dry 0.05604 BRL 41 41-129 34 24 D 1,3-Dichloropropane 0.0315 0.0056 mg/kg dry 0.05604 BRL 56 53-129 8 15 1,4-Dichlorobenzene 0.0234 0.0056 mg/kg dry 0.05604 BRL 42 44-134 34 21 D, M 2,2-Dichloropropane 0.0223 0.0056 mg/kg dry 0.05604 BRL 40 30-147 59 20 D 2-Chlorotoluene 0.0209 0.0056 mg/kg dry 0.05604 BRL 37 46-132 47 29 D, M 4-Chlorotoluene 0.0217 0.0056 mg/kg dry 0.05604 BRL 39 44-135 43 23 D, M 4-Isopropyltoluene 0.0190 0.0056 mg/kg dry 0.05604 BRL 34 32-144 55 22 D Acetone 0.146 0.056 mg/kg dry 0.1121 0.00870 122 34-143 42 49 Benzene 0.0240 0.0034 mg/kg dry 0.05604 BRL 43 60-135 52 20 D, M Bromobenzene 0.0231 0.0056 mg/kg dry 0.05604 BRL 41 45-135 30 25 D, M Bromochloromethane 0.0311 0.0056 mg/kg dry 0.05604 BRL 56 55-136 23 18 D Bromodichloromethane 0.0294 0.0056 mg/kg dry 0.05604 BRL 52 55-127 28 17 D, M Bromoform 0.0347 0.0056 mg/kg dry 0.05604 BRL 62 40-136 2 35 Bromomethane 0.0304 0.011 mg/kg dry 0.05604 BRL 54 30-137 44 30 D Carbon Tetrachloride 0.0240 0.0056 mg/kg dry 0.05604 BRL 43 48-153 60 23 D, M Chlorobenzene 0.0244 0.0056 mg/kg dry 0.05604 BRL 43 57-125 39 14 D, M Chloroethane 0.0255 0.011 mg/kg dry 0.05604 BRL 45 16-177 60 47 D Chloroform 0.0270 0.0056 mg/kg dry 0.05604 BRL 48 56-137 45 18 D, M Chloromethane 0.0298 0.0056 mg/kg dry 0.05604 BRL 53 40-145 46 26 D cis-1,2-Dichloroethylene 0.0263 0.0056 mg/kg dry 0.05604 BRL 47 58-140 44 28 D, M cis-1,3-Dichloropropylene 0.0302 0.0056 mg/kg dry 0.05604 BRL 54 42-135 27 32 Dibromochloromethane 0.0300 0.0056 mg/kg dry 0.05604 BRL 54 49-127 14 24 Dichlorodifluoromethane 0.0247 0.0056 mg/kg dry 0.05604 BRL 44 25-151 69 37 D Ethylbenzene 0.0218 0.0056 mg/kg dry 0.05604 BRL 39 44-144 53 19 D, M Isopropyl Ether 0.0282 0.0056 mg/kg dry 0.05604 BRL 50 51-155 27 13 D, M Isopropylbenzene (Cumene) 0.0200 0.0056 mg/kg dry 0.05604 BRL 36 41-140 55 27 D, M m,p-Xylenes 0.0446 0.011 mg/kg dry 0.1121 BRL 40 36-148 50 20 D Methyl Butyl Ketone (2-Hexanone) 0.0448 0.056 mg/kg dry 0.05604 BRL 80 30-147 43 42 Methyl Ethyl Ketone (2-Butanone) 0.0518 0.11 mg/kg dry 0.05604 BRL 92 24-160 44 42 D Methyl Isobutyl Ketone 0.0469 0.056 mg/kg dry 0.05604 BRL 84 25-163 35 44 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 53 0f 67 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130215 - 5035 Reporting Result Limit Units Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike Dup (P8B0215-MSD1) Source: 8020190-01 Prepared & Analyzed: 02/12/18 Methylene Chloride 0.0275 0.011 mg/kg dry 0.05604 BRL 49 53-144 42 14 D, M Methyl-tert-Butyl Ether 0.0323 0.011 mg/kg dry 0.05604 BRL 58 49-135 19 22 Naphthalene 0.0333 0.011 mg/kg dry 0.05604 BRL 59 32-127 14 44 n-Butylbenzene 0.0193 0.0056 mg/kg dry 0.05604 BRL 34 23-148 56 39 D n-Propylbenzene 0.0195 0.0056 mg/kg dry 0.05604 BRL 35 35-144 55 27 D o-Xylene 0.0234 0.0056 mg/kg dry 0.05604 BRL 42 43-143 44 17 D, M sec-Butylbenzene 0.0198 0.0056 mg/kg dry 0.05604 BRL 35 34-144 56 28 D Styrene 0.0247 0.0056 mg/kg dry 0.05604 BRL 44 42-132 40 28 D tert-Butylbenzene 0.0202 0.0056 mg/kg dry 0.05604 BRL 36 36-150 52 29 D Tetrachloroethylene 0.0218 0.0056 mg/kg dry 0.05604 BRL 39 47-142 59 26 D, M Toluene 0.0243 0.0056 mg/kg dry 0.05604 BRL 43 57-135 51 22 D, M trans-1,2-Dichloroethylene 0.0236 0.0056 mg/kg dry 0.05604 BRL 42 58-141 57 18 D, M trans- 1,3-Dichloropropylene 0.0319 0.0056 mg/kg dry 0.05604 BRL 57 41-124 17 20 Trichloroethylene 0.0230 0.0056 mg/kg dry 0.05604 BRL 41 38-164 58 18 D Trichlorofluoromethane 0.0258 0.0056 mg/kg dry 0.05604 BRL 46 30-157 63 27 D Vinyl acetate 0.0435 0.028 mg/kg dry 0.05604 BRL 78 61-154 9 35 Vinyl chloride 0.0234 0.0056 mg/kg dry 0.05604 BRL 42 40-156 70 35 D Xylenes, total 0.0680 0.017 mg/kg dry 0.1681 BRL 40 36-148 48 20 D Surrogate:4-Bromofluorobenzene 49.7 ug/L 50.00 99 70-130 Surrogate: Dibromofluoromethane 50.4 ug/L 50.00 101 84-123 Surrogate: Toluene-d8 45.2 ug/L 50.00 90 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 54 0f 67 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Project: Homewood Banks Prism Work Order: 8020190 Attn: Roger Smith Time Submitted: 2/10/2018 9:55:OOAM 9751 Southern Pine Blvd. Charlotte, NC 28273 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81130242 - 3546 Blank (P8B0242-BLK1) Prepared & Analyzed: 02/13/18 1,2,4-Trichlorobenzene BRL 0.33 mg/kg wet 1,2-Dichlorobenzene BRL 0.33 mg/kg wet 1,3-Dichlorobenzene BRL 0.33 mg/kg wet 1,4-Dichlorobenzene BRL 0.33 mg/kg wet 1-Methyl naphthalene BRL 0.33 mg/kg wet 2,4,6-Trichlorophenol BRL 0.33 mg/kg wet 2,4-Dichlorophenol BRL 0.33 mg/kg wet 2,4-Dimethylphenol BRL 0.33 mg/kg wet 2,4-Dinitrophenol BRL 0.33 mg/kg wet 2,4-Dinitrotoluene BRL 0.33 mg/kg wet 2,6-Dinitrotoluene BRL 0.33 mg/kg wet 2-Chloronaphthalene BRL 0.33 mg/kg wet 2-Chlorophenol BRL 0.33 mg/kg wet 2-Methyl naphthalene BRL 0.33 mg/kg wet 2-Methylphenol BRL 0.33 mg/kg wet 2-Nitrophenol BRL 0.33 mg/kg wet 3,3'-Dichlorobenzidine BRL 0.33 mg/kg wet 3/4-Methyl phenol BRL 0.33 mg/kg wet 4,6-Dinitro-2-methylphenol BRL 0.33 mg/kg wet 4-Bromophenyl phenyl ether BRL 0.33 mg/kg wet 4-Chloro-3-methylphenol BRL 0.33 mg/kg wet 4-Chloroaniline BRL 0.33 mg/kg wet 4-Chlorophenyl phenyl ether BRL 0.33 mg/kg wet 4-Nitrophenol BRL 0.33 mg/kg wet Acenaphthene BRL 0.33 mg/kg wet Acenaphthylene BRL 0.33 mg/kg wet Anthracene BRL 0.33 mg/kg wet Azobenzene BRL 0.33 mg/kg wet Benzo(a)anthracene BRL 0.33 mg/kg wet Benzo(a)pyrene BRL 0.33 mg/kg wet Benzo(b)fluoranthene BRL 0.33 mg/kg wet Benzo(g,h,i)perylene BRL 0.33 mg/kg wet Benzo(k)fluoranthene BRL 0.33 mg/kg wet Benzoic Acid BRL 0.33 mg/kg wet Benzyl alcohol BRL 0.33 mg/kg wet bis(2-Chloroethoxy)methane BRL 0.33 mg/kg wet Bis(2-Chloroethyl)ether BRL 0.33 mg/kg wet Bis(2-chloroisopropyl)ether BRL 0.33 mg/kg wet Bis(2-Ethylhexyl)phthalate BRL 0.33 mg/kg wet Butyl benzyl phthalate BRL 0.33 mg/kg wet Chrysene BRL 0.33 mg/kg wet Dibenzo(a,h)anthracene BRL 0.33 mg/kg wet Dibenzofuran BRL 0.33 mg/kg wet Diethyl phthalate BRL 0.33 mg/kg wet Dimethyl phthalate BRL 0.33 mg/kg wet Di-n-butyl phthalate BRL 0.33 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 55 0f 67 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130242 - 3546 Reporting Result Limit Units Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P8B0242-BLK1) Prepared & Analyzed: 02/13/18 Di-n-octyl phthalate BRL 0.33 mg/kg wet Fluoranthene BRL 0.33 mg/kg wet Fluorene BRL 0.33 mg/kg wet Hexachlorobenzene BRL 0.33 mg/kg wet Hexachlorobutadiene BRL 0.33 mg/kg wet Hexachlorocyclopentadiene BRL 0.33 mg/kg wet Hexachloroethane BRL 0.33 mg/kg wet Indeno(1,2,3-cd)pyrene BRL 0.33 mg/kg wet Isophorone BRL 0.33 mg/kg wet Naphthalene BRL 0.33 mg/kg wet Nitrobenzene BRL 0.33 mg/kg wet N-Nitroso-di-n-propylamine BRL 0.33 mg/kg wet N-Nitrosodiphenylamine BRL 0.33 mg/kg wet Pentachlorophenol BRL 0.33 mg/kg wet Phenanthrene BRL 0.33 mg/kg wet Phenol BRL 0.33 mg/kg wet Pyrene BRL 0.33 mg/kg wet Surrogate: 2,4,6-Tribromophenol 2.89 mg/kg wet 3.333 87 39-132 Surrogate: 2-Fluorobiphenyl 1.52 mg/kg wet 1.667 91 44-115 Surrogate: 2-Fluorophenol 2.75 mg/kg wet 3.333 83 35-115 Surrogate: Nitrobenzene-d5 1.38 mg/kg wet 1.667 83 37-122 Surrogate: Phenol-d5 2.75 mg/kg wet 3.333 83 34-121 Surrogate: Terphenyl-d14 1.45 mg/kg wet 1.667 87 54-127 LCS (P8B0242-BSI) Prepared &Analyzed: 02/13/18 1,2,4-Trichlorobenzene 0.968 0.33 mg/kg wet 1.667 58 34-118 1,2-Dichlorobenzene 0.989 0.33 mg/kg wet 1.667 59 33-117 1,3-Dichlorobenzene 0.969 0.33 mg/kg wet 1.667 58 30-115 1,4-Dichlorobenzene 0.964 0.33 mg/kg wet 1.667 58 31-115 1-Methyl naphthalene 1.12 0.33 mg/kg wet 1.667 67 40-119 2,4,6-Trichlorophenol 1.21 0.33 mg/kg wet 1.667 73 39-126 2,4-Dichlorophenol 1.09 0.33 mg/kg wet 1.667 65 40-122 2,4-Dimethylphenol 1.27 0.33 mg/kg wet 1.667 76 30-127 2,4-Dinitrophenol 1.24 0.33 mg/kg wet 1.667 74 27-129 2,4-Dinitrotoluene 0.950 0.33 mg/kg wet 1.667 57 48-126 2,6-Dinitrotoluene 1.27 0.33 mg/kg wet 1.667 76 46-124 2-Chloronaphthalene 1.15 0.33 mg/kg wet 1.667 69 41-114 2-Chlorophenol 1.15 0.33 mg/kg wet 1.667 69 34-121 2-Methyl naphthalene 1.07 0.33 mg/kg wet 1.667 64 38-122 2-Methylphenol 1.20 0.33 mg/kg wet 1.667 72 32-122 2-Nitrophenol 1.01 0.33 mg/kg wet 1.667 61 36-123 3,3'-Dichlorobenzidine 1.19 0.33 mg/kg wet 1.667 71 22-121 3/4-Methyl phenol 1.16 0.33 mg/kg wet 1.667 69 34-119 4,6-Dinitro-2-methylphenol 1.21 0.33 mg/kg wet 1.667 73 29-132 4-Bromophenyl phenyl ether 1.15 0.33 mg/kg wet 1.667 69 46-124 4-Chloro-3-methylphenol 1.14 0.33 mg/kg wet 1.667 69 45-122 4-Chloroaniline 1.02 0.33 mg/kg wet 1.667 61 17-106 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 56 0f 67 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130242 - 3546 Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS (P8B0242-BSI) Prepared &Analyzed: 02/13/18 4-Chlorophenyl phenyl ether 1.21 0.33 mg/kg wet 1.667 73 45-121 4-Nitrophenol 1.32 0.33 mg/kg wet 1.667 79 30-132 Acenaphthene 1.22 0.33 mg/kg wet 1.667 73 40-123 Acenaphthylene 1.31 0.33 mg/kg wet 1.667 78 32-132 Anthracene 1.34 0.33 mg/kg wet 1.667 80 47-123 Azobenzene 1.27 0.33 mg/kg wet 1.667 76 39-125 Benzo(a)anthracene 1.30 0.33 mg/kg wet 1.667 78 49-126 Benzo(a)pyrene 1.29 0.33 mg/kg wet 1.667 77 45-129 Benzo(b)fluoranthene 1.29 0.33 mg/kg wet 1.667 78 45-132 Benzo(g,h,i)perylene 1.22 0.33 mg/kg wet 1.667 73 43-134 Benzo(k)fluoranthene 1.25 0.33 mg/kg wet 1.667 75 47-132 Benzoic Acid 0.807 0.33 mg/kg wet 1.667 48 10-83 Benzyl alcohol 1.02 0.33 mg/kg wet 1.667 61 29-122 bis(2-Chloroethoxy)methane 1.04 0.33 mg/kg wet 1.667 62 36-121 Bis(2-Chloroethyl)ether 0.996 0.33 mg/kg wet 1.667 60 31-120 Bis(2-chloroisopropyl)ether 0.981 0.33 mg/kg wet 1.667 59 33-131 Bis(2-Ethylhexyl)phthalate 1.35 0.33 mg/kg wet 1.667 81 51-133 Butyl benzyl phthalate 1.28 0.33 mg/kg wet 1.667 77 48-132 Chrysene 1.22 0.33 mg/kg wet 1.667 73 50-124 Dibenzo(a,h)anthracene 0.768 0.33 mg/kg wet 1.667 46 45-134 Dibenzofuran 1.20 0.33 mg/kg wet 1.667 72 44-120 Diethyl phthalate 1.22 0.33 mg/kg wet 1.667 73 50-124 Dimethyl phthalate 1.19 0.33 mg/kg wet 1.667 71 48-124 Di-n-butyl phthalate 1.33 0.33 mg/kg wet 1.667 80 51-128 Di-n-octyl phthalate 1.40 0.33 mg/kg wet 1.667 84 45-140 Fluoranthene 1.36 0.33 mg/kg wet 1.667 82 50-127 Fluorene 1.26 0.33 mg/kg wet 1.667 76 43-125 Hexachlorobenzene 1.17 0.33 mg/kg wet 1.667 70 45-122 Hexachlorobutadiene 0.979 0.33 mg/kg wet 1.667 59 32-123 Hexachlorocyclopentadiene 1.13 0.33 mg/kg wet 1.667 68 32-117 Hexachloroethane 0.961 0.33 mg/kg wet 1.667 58 28-117 Indeno(1,2,3-cd)pyrene 1.41 0.33 mg/kg wet 1.667 85 45-133 Isophorone 1.04 0.33 mg/kg wet 1.667 63 30-122 Naphthalene 1.04 0.33 mg/kg wet 1.667 62 35-123 Nitrobenzene 0.915 0.33 mg/kg wet 1.667 55 34-122 N-Nitroso-di-n-propylamine 1.20 0.33 mg/kg wet 1.667 72 36-120 N-Nitrosodiphenylamine 1.50 0.33 mg/kg wet 1.667 90 38-127 Pentachlorophenol 1.50 0.33 mg/kg wet 1.667 90 25-133 Phenanthrene 1.32 0.33 mg/kg wet 1.667 79 50-121 Phenol 1.18 0.33 mg/kg wet 1.667 71 34-121 Pyrene 1.31 0.33 mg/kg wet 1.667 79 47-127 Surrogate: 2,4,6-Tribromophenol 2.55 mg/kg wet 3.333 77 39-132 Surrogate: 2-Fluorobiphenyl 1.31 mg/kg wet 1.667 78 44-115 Surrogate: 2-Fluorophenol 2.40 mg/kg wet 3.333 72 35-115 Surrogate: Nitrobenzene-d5 1.08 mg/kg wet 1.667 65 37-122 Surrogate: Phenol-d5 2.44 mg/kg wet 3.333 73 34-121 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 57 0f 67 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc - Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Project: Homewood Banks Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P81130242 - 3546 Reporting Result Limit Units Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P8B0242-BS1) Prepared &Analyzed: 02/13/18 Surrogate: Terphenyl-d14 1.31 mg/kg wet 1.667 78 54-127 LCS Dup (P8B0242-BSD1) Prepared &Analyzed: 02/13/18 1,2,4-Trichlorobenzene 1.09 0.33 mg/kg wet 1.667 65 34-118 12 20 1,2-Dichlorobenzene 1.15 0.33 mg/kg wet 1.667 69 33-117 15 20 1,3-Dichlorobenzene 1.11 0.33 mg/kg wet 1.667 67 30-115 14 20 1,4-Dichlorobenzene 1.12 0.33 mg/kg wet 1.667 67 31-115 15 20 1-Methyl naphthalene 1.27 0.33 mg/kg wet 1.667 76 40-119 13 20 2,4,6-Trichlorophenol 1.38 0.33 mg/kg wet 1.667 83 39-126 13 20 2,4-Dichlorophenol 1.24 0.33 mg/kg wet 1.667 74 40-122 13 20 2,4-Dimethylphenol 1.44 0.33 mg/kg wet 1.667 86 30-127 13 20 2,4-Dinitrophenol 1.36 0.33 mg/kg wet 1.667 82 27-129 9 20 2,4-Dinitrotoluene 1.06 0.33 mg/kg wet 1.667 64 48-126 11 20 2,6-Dinitrotoluene 1.42 0.33 mg/kg wet 1.667 85 46-124 11 20 2-Chloronaphthalene 1.32 0.33 mg/kg wet 1.667 79 41-114 13 20 2-Chlorophenol 1.33 0.33 mg/kg wet 1.667 80 34-121 15 20 2-Methyl naphthalene 1.22 0.33 mg/kg wet 1.667 73 38-122 13 20 2-Methylphenol 1.42 0.33 mg/kg wet 1.667 85 32-122 16 20 2-Nitrophenol 1.18 0.33 mg/kg wet 1.667 71 36-123 15 20 3,3'-Dichlorobenzidine 1.35 0.33 mg/kg wet 1.667 81 22-121 13 20 3/4-Methyl phenol 1.33 0.33 mg/kg wet 1.667 80 34-119 14 20 4,6-Dinitro-2-methylphenol 1.34 0.33 mg/kg wet 1.667 80 29-132 10 20 4-Bromophenyl phenyl ether 1.30 0.33 mg/kg wet 1.667 78 46-124 12 20 4-Chloro-3-methylphenol 1.28 0.33 mg/kg wet 1.667 77 45-122 12 20 4-Chloroaniline 1.17 0.33 mg/kg wet 1.667 70 17-106 14 20 4-Chlorophenyl phenyl ether 1.35 0.33 mg/kg wet 1.667 81 45-121 11 20 4-Nitrophenol 1.48 0.33 mg/kg wet 1.667 89 30-132 11 20 Acenaphthene 1.38 0.33 mg/kg wet 1.667 83 40-123 13 20 Acenaphthylene 1.47 0.33 mg/kg wet 1.667 88 32-132 12 20 Anthracene 1.52 0.33 mg/kg wet 1.667 91 47-123 12 20 Azobenzene 1.44 0.33 mg/kg wet 1.667 86 39-125 13 20 Benzo(a)anthracene 1.45 0.33 mg/kg wet 1.667 87 49-126 11 20 Benzo(a)pyrene 1.44 0.33 mg/kg wet 1.667 87 45-129 11 20 Benzo(b)fluoranthene 1.48 0.33 mg/kg wet 1.667 89 45-132 13 20 Benzo(g,h,i)perylene 1.38 0.33 mg/kg wet 1.667 83 43-134 12 20 Benzo(k)fluoranthene 1.37 0.33 mg/kg wet 1.667 82 47-132 9 20 Benzoic Acid 0.995 0.33 mg/kg wet 1.667 60 10-83 21 20 D Benzyl alcohol 1.21 0.33 mg/kg wet 1.667 72 29-122 16 20 bis(2-Chloroethoxy)methane 1.18 0.33 mg/kg wet 1.667 71 36-121 13 20 Bis(2-Chloroethyl)ether 1.15 0.33 mg/kg wet 1.667 69 31-120 14 20 Bis(2-chloroisopropyl)ether 1.14 0.33 mg/kg wet 1.667 68 33-131 15 20 Bis(2-Ethylhexyl)phthalate 1.49 0.33 mg/kg wet 1.667 90 51-133 10 20 Butyl benzyl phthalate 1.41 0.33 mg/kg wet 1.667 85 48-132 9 20 Chrysene 1.36 0.33 mg/kg wet 1.667 82 50-124 11 20 Dibenzo(a,h)anthracene 0.837 0.33 mg/kg wet 1.667 50 45-134 9 20 Dibenzofuran 1.35 0.33 mg/kg wet 1.667 81 44-120 12 20 Diethyl phthalate 1.38 0.33 mg/kg wet 1.667 83 50-124 12 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 58 0f 67 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Project: Homewood Banks Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Analyte Result Limit Units Batch P81130242 - 3546 Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P8B0242-BSD1) Prepared & Analyzed: 02/13/18 Dimethyl phthalate 1.33 0.33 mg/kg wet 1.667 80 48-124 11 20 Di-n-butyl phthalate 1.50 0.33 mg/kg wet 1.667 90 51-128 12 20 Di-n-octyl phthalate 1.58 0.33 mg/kg wet 1.667 95 45-140 12 20 Fluoranthene 1.52 0.33 mg/kg wet 1.667 91 50-127 11 20 Fluorene 1.43 0.33 mg/kg wet 1.667 86 43-125 13 20 Hexachlorobenzene 1.32 0.33 mg/kg wet 1.667 79 45-122 12 20 Hexachlorobutadiene 1.13 0.33 mg/kg wet 1.667 68 32-123 14 20 Hexachlorocyclopentadiene 1.29 0.33 mg/kg wet 1.667 78 32-117 13 20 Hexachloroethane 1.09 0.33 mg/kg wet 1.667 66 28-117 13 20 Indeno(1,2,3-cd)pyrene 1.58 0.33 mg/kg wet 1.667 95 45-133 12 20 Isophorone 1.19 0.33 mg/kg wet 1.667 71 30-122 13 20 Naphthalene 1.19 0.33 mg/kg wet 1.667 71 35-123 13 20 Nitrobenzene 1.03 0.33 mg/kg wet 1.667 62 34-122 12 20 N-Nitroso-di-n-propylamine 1.35 0.33 mg/kg wet 1.667 81 36-120 12 20 N-Nitrosodiphenylamine 1.69 0.33 mg/kg wet 1.667 101 38-127 12 20 Pentachlorophenol 1.62 0.33 mg/kg wet 1.667 97 25-133 7 20 Phenanthrene 1.49 0.33 mg/kg wet 1.667 89 50-121 12 20 Phenol 1.37 0.33 mg/kg wet 1.667 82 34-121 15 20 Pyrene 1.44 0.33 mg/kg wet 1.667 86 47-127 9 20 Surrogate: 2,4,6-Tribromophenol 2.78 mg/kg wet 3.333 83 39-132 Surrogate: 2-Fluorobiphenyl 1.43 mg/kg wet 1.667 86 44-115 Surrogate: 2-Fluorophenol 2.67 mg/kg wet 3.333 80 35-115 Surrogate: Nitrobenzene-d5 1.16 mg/kg wet 1.667 70 37-122 Surrogate: Phenol-d5 2.68 mg/kg wet 3.333 80 34-121 Surrogate: Terphenyl-d14 1.39 mg/kg wet 1.667 83 54-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 59 of 67 Level II QC Report P R I IS M Full -Service Analytical 2/14/18 Environmental Solutions LABORATORIES, INC. S&ME, Inc - Charlotte Project: Homewood Banks Prism Work Order: 8020190 Attn: Roger Smith Time Submitted: 2/10/2018 9:55:OOAM 9751 Southern Pine Blvd. Charlotte, NC 28273 Total Metals - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8130232 - 3050B Blank (128130232-BLK1) Prepared &Analyzed: 02/13/18 Arsenic BRL 0.75 mg/kg wet Barium BRL 5.0 mg/kg wet Cadmium BRL 0.12 mg/kg wet Chromium BRL 0.25 mg/kg wet Lead BRL 0.12 mg/kg wet Selenium BRL 0.50 mg/kg wet Silver BRL 0.12 mg/kg wet LCS (P8B0232-BS1) Prepared &Analyzed: 02/13/18 Arsenic 12.5 0.75 mg/kg wet 12.50 100 80-120 Barium 12.4 5.0 mg/kg wet 12.50 99 80-120 Cadmium 11.9 0.12 mg/kg wet 12.50 95 80-120 Chromium 12.9 0.25 mg/kg wet 12.50 103 80-120 Lead 13.3 0.12 mg/kg wet 12.50 106 80-120 Selenium 11.7 0.50 mg/kg wet 12.50 94 80-120 Silver 5.03 0.12 mg/kg wet 5.000 101 80-120 Matrix Spike (P8B0232-MS1) Source: 8020190-01 Prepared &Analyzed: 02/13/18 Arsenic 13.5 0.83 mg/kg dry 13.79 0.552 94 75-125 Barium 96.9 5.5 mg/kg dry 13.78 82.2 107 75-125 Cadmium 13.1 0.14 mg/kg dry 13.78 0.0505 94 75-125 Chromium 15.1 0.28 mg/kg dry 13.79 1.48 99 75-125 Lead 17.7 0.14 mg/kg dry 13.79 3.43 104 75-125 Selenium 13.2 0.55 mg/kg dry 13.78 0.724 91 75-125 Silver 5.49 0.14 mg/kg dry 5.513 0.0583 98 75-125 Matrix Spike Dup (P8B0232-MSD1) Source: 8020190-01 Prepared &Analyzed: 02/13/18 Arsenic 13.8 0.82 mg/kg dry 13.72 0.552 96 75-125 2 20 Barium 97.0 5.5 mg/kg dry 13.71 82.2 108 75-125 0.1 20 Cadmium 13.2 0.14 mg/kg dry 13.71 0.0505 96 75-125 1 20 Chromium 15.2 0.27 mg/kg dry 13.72 1.48 100 75-125 0.5 20 Lead 18.0 0.14 mg/kg dry 13.72 3.43 106 75-125 1 20 Selenium 13.3 0.55 mg/kg dry 13.71 0.724 92 75-125 0.9 20 Silver 5.55 0.14 mg/kg dry 5.485 0.0583 100 75-125 1 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 60 0f 67 Level II QC Report PRISMFull -Service Analytical s 2/14/18 Environmental Solutions �- LABORATORIES, INC. S&ME, Inc -Charlotte Project: Homewood Banks Prism Work Order: 8020190 Attn: Roger Smith Time Submitted: 2/10/2018 9:55:OOAM 9751 Southern Pine Blvd. Charlotte, NC 28273 Total Metals - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81130232 - 3050B Post Spike (P8B0232-PS1) Source: 8020190-01 Prepared: 02/13/18 Analyzed: 02/14/18 Arsenic 101 ug/L 100.0 2.02 99 80-120 Barium 704 ug/L 100.0 301 403 80-120 M Cadmium 95.6 ug/L 100.0 0.185 95 80-120 Chromium 108 ug/L 100.0 5.41 103 80-120 Lead 126 ug/L 100.0 12.6 114 80-120 Selenium 96.7 ug/L 100.0 2.65 94 80-120 Silver 102 ug/L 100.0 0.214 101 80-120 Batch P860233 - 7471 B Blank (P8B0233-BLK1) Prepared & Analyzed: 02/13/18 Mercury BRL 0.020 mg/kg wet LCS (P8B0233-BS1) Prepared &Analyzed: 02/13/18 Mercury 0.432 0.020 mg/kg wet 0.4167 104 80-120 Batch P860234 - 7471 B Blank (P8130234-BLK1) Prepared & Analyzed: 02/13/18 Mercury BRL 0.020 mg/kg wet LCS (P8B0234-BSI) Prepared &Analyzed: 02/13/18 Mercury 0.453 0.020 mg/kg wet 0.4167 109 80-120 Matrix Spike (P8B0234-MS1) Source: 8020190-03 Prepared & Analyzed: 02/13/18 Mercury 0.559 0.024 mg/kg dry 0.5030 BRL 111 80-120 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 61 of 67 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. S&ME, Inc -Charlotte Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 Total Metals - Quality Control Analyte Batch P81130234 - 7471 B Project: Homewood Banks Level II QC Report 2/14/18 Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Matrix Spike Dup (P8B0234-MSD1) Source: 8020190-03 Prepared & Analyzed: 02/13/18 Mercury 0.549 0.023 mg/kg dry 0.4770 BRL 115 80-120 2 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 62 of 67 �P R I S Full -Service Analytical s Environmental Solutions �- LABORATORIES, INC. Level II QC Report 2/14/18 S&ME, Inc -Charlotte Project: Homewood Banks Attn: Roger Smith 9751 Southern Pine Blvd. Charlotte, NC 28273 General Chemistry Parameters - Quality Control Prism Work Order: 8020190 Time Submitted: 2/10/2018 9:55:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P81130256 - Solids, Dry Weight Duplicate (P8B0256-DUP2) Source: 8020190-01 Prepared & Analyzed: 02/13/18 % Solids 91.5 0.100 % by Weight 91.6 0.1 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 63 of 67 Sample Extraction Data Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 8020190-01 P8130256 30 g 30 g 02/13/18 15:11 8020190-02 P860256 30 g 30 g 02/13/18 15:11 8020190-03 P860256 30 g 30 g 02/13/18 15:11 8020190-04 P860256 30 g 30 g 02/13/18 15:11 8020190-05 P8130256 30 g 30 g 02/13/18 15:11 8020190-06 P8130256 30 g 30 g 02/13/18 15:11 8020190-07 P8130256 30 g 30 g 02/13/18 15:11 8020190-08 P8130256 30 g 30 g 02/13/18 15:11 8020190-09 P860256 30 g 30 g 02/13/18 15:11 8020190-10 P860256 30 g 30 g 02/13/18 15:11 8020190-11 P860256 30 g 30 g 02/13/18 15:11 8020190-12 P860256 30 g 30 g 02/13/18 15:11 Prep Method: 3546 Lab Number Batch Initial Final Date/Time 8020190-01 P860242 30.05 g 1 mL 02/13/18 14:05 8020190-02 P860242 30.08 g 1 mL 02/13/18 14:05 8020190-03 P860242 30.04 g 1 mL 02/13/18 14:05 8020190-04 P860242 30.01 g 1 mL 02/13/18 14:05 8020190-05 P8130242 30.05 g 1 mL 02/13/18 14:05 8020190-06 P8130242 30.08 g 1 mL 02/13/18 14:05 8020190-07 P8130242 30.01 g 1 mL 02/13/18 14:05 8020190-08 P8B0242 30.03 g 1 mL 02/13/18 14:05 8020190-09 P860242 30.01 g 1 mL 02/13/18 14:05 8020190-12 P860242 30.09 g 1 mL 02/13/18 14:05 Prep Method: 3050B Lab Number Batch Initial Final Date/Time 8020190-01 P8130232 1.99 g 50 mL 02/13/18 8:50 8020190-02 P8130232 2.04 g 50 mL 02/13/18 8:50 8020190-03 P860232 1.96 g 50 mL 02/13/18 8:50 8020190-04 P860232 1.98 g 50 mL 02/13/18 8:50 8020190-05 P860232 1.99 g 50 mL 02/13/18 8:50 8020190-06 P860232 1.98 g 50 mL 02/13/18 8:50 8020190-07 P8130232 2.03 g 50 mL 02/13/18 8:50 8020190-08 P8130232 1.97 g 50 mL 02/13/18 8:50 8020190-09 P8130232 1.98 g 50 mL 02/13/18 8:50 8020190-10 P8130232 2.05 g 50 mL 02/13/18 8:50 8020190-11 P8B0232 2.02 g 50 mL 02/13/18 8:50 8020190-12 P860232 1.98 g 50 mL 02/13/18 8:50 Prep Method: 7471B Lab Number Batch Initial Final Date/Time 8020190-01 P8130233 0.57 g 50 mL 02/13/18 10:00 8020190-02 P8130233 0.63 g 50 mL 02/13/18 10:00 8020190-03 P860234 0.56 g 50 mL 02/13/18 10:00 8020190-04 P860234 0.56 g 50 mL 02/13/18 10:00 8020190-05 P860234 0.59 g 50 mL 02/13/18 10:00 8020190-06 P860234 0.64 g 50 mL 02/13/18 10:00 8020190-07 P8130234 0.55 g 50 mL 02/13/18 10:00 8020190-08 P8130234 0.6 g 50 mL 02/13/18 10:00 8020190-09 P8130234 0.57 g 50 mL 02/13/18 10:00 8020190-10 P8130234 0.65 g 50 mL 02/13/18 10:00 8020190-11 P860234 0.56 g 50 mL 02/13/18 10:00 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 64 0f 67 Sample Extraction Data Prep Method: 7471E Lab Number Batch Initial Final Date/Time 8020190-12 P8130234 0.57 g 50 mL 02/13/18 10:00 Prep Method: 5035 Lab Number Batch Initial Final Date/Time 8020190-01 P8130215 4.49 g 5 mL 02/12/18 10:02 8020190-02 P8130215 4.66 g 5 mL 02/12/18 10:02 8020190-03 P860215 4.96 g 5 mL 02/12/18 10:02 8020190-04 P8130215 4.62 g 5 mL 02/12/18 10:02 8020190-05 P8130215 4.54 g 5 mL 02/12/18 10:02 8020190-06 P8130215 4.89 g 5 mL 02/12/18 10:02 8020190-07 P8130215 5.16 g 5 mL 02/12/18 10:02 8020190-08 P8130215 5.91 g 5 mL 02/12/18 10:02 8020190-09 P8130215 4.93 g 5 mL 02/12/18 10:02 8020190-12 P860215 4.85 g 5 mL 02/12/18 10:02 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. 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