21002_Eagle Island_IRRPT_20170830

Geosyntec Consultants of NC, PC
2501 Blue Ridge Road, Suite 430
Raleigh, North Carolina 27607
PH 919.870.0576
www.geosyntec.com

GN6353\Eagle Island Interim Removal Report
30 August 2017

Mr. Samuel P. Watson, P.G.
Division of Waste Management – Brownfields
North Carolina Department of Environmental Quality
127 Cardinal Drive Ext.
Wilmington, NC 28405

Subject: Interim Removal Action Report
Subject Site: Parcel No. 0390000901, 03900008, and 03900011 located on Battle
Ship Road NE, Eagle Island, Leland, North Carolina
Brownfields Project Number: 21002-17-010

Dear Mr. Watson:

Geosyntec Consultants of NC, PC (Geosyntec) is pleased to submit this Interim Removal Action
Report (IRA Report) on behalf of our client, Burgess Group Consolidated, LLC (Burgess; the
Prospective Developer [PD] for the above-referenced Brownfields Site). Geosyntec is working on
behalf of Burgess to achieve a finalized Brownfields Agreement (BFA) for the multi-parcel
property located on Battleship Road, Leland, NC (Brunswick County Parcel numbers 0390000901,
03900008, and 0390000901) (“Site”). The North Carolina Department of Environmental Quality
(NCDEQ) approved Burgess’ 25 January 2017 Brownfields Property Application (BPA) in a 3
April 2017 Letter of Eligibility (LOE). On 17 May 2017, Geosyntec submitted a Phase II
Environmental Site Assessment (ESA) to NCDEQ summarizing the results of soil and
groundwater testing and excavation test pitting completed at the Site in 2017. On 26 May 2017,
Geosyntec submitted an Interim Removal Action Work Plan to the NCDEQ to detail a targeted
soil removal action plan for addressing impacted soils identified during the Phase II ESA. The
interim removal action was not required to satisfy the BPA requirements, although it was
completed to facilitate Site re-use and support future land development. This IRA Report details
the targeted soil removal work discussed in the Interim Removal Action Work Plan.

BACKGROUND

The Site consists of three contiguous parcels (Brunswick County Parcel No. 0390000901,
03900008, and 03900011) totaling approximately 23 acres located on Battle Ship Rd NE on Eagle
Island in Leland, North Carolina. Site Parcels 0390000901 and 03900011 are each divided into
two properties by Battle Ship Road NE; portions of each parcel are located east and west of the
road. The Site is largely surrounded by unoccupied or undeveloped land in a former primarily
commercial/industrial area, with the exception of an electrical substation located adjacent to the
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south of the Site. The Site location is shown on Figure 1. The Site layout with pertinent Site
features is provided on Figure 2.

In 2016, Geosyntec performed a Phase I Environmental Site Assessment (ESA) in support of
Burgess’ purchase of the Site; this work was summarized in a 3 January 2017 Phase I ESA Report
(“January 2017 Phase I ESA”) and submitted to the NCDEQ as part of Burgess’ 16 February 2017
BPA. Geosyntec was retained by Burgess to guide the environmental efforts to achieve a finalized
Brownfields Agreement for the Site. At the direction of NCDEQ, Geosyntec completed Phase II
ESA work at the Site largely to address the Recognized Environmental Conditions (RECs)1
identified in the January 2017 Phase I ESA and to establish Site-wide baseline soil and
groundwater conditions. The Phase II ESA work consisted of test pitting, soil sampling, and a
groundwater quality assessment.

On 17 May 2017, Geosyntec submitted a Phase II Environmental Site Assessment (Phase II ESA)
report to NCDEQ. As discussed in the Phase II ESA, a tar (or resin), stick-up pipe, and winch were
observed during test pitting in the southern portion of Finding A2, proximal to the Parcel
0390000901 shoreline. Several polynuclear aromatic hydrocarbons (PAHs) and metals in this area
were identified in soil above their respective NCDEQ Inactive Hazardous Sites Branch (IHSB)
Residential and Commercial / Industrial Preliminary Soil Remediation Goals (PSRGs) (Figure 3).
In anticipation of Site redevelopment and reuse, Geosyntec oversaw a targeted soil excavation in
this area (“the remedial area”), off-Site soil disposal, and confirmation soil sampling as an interim
soil remedy. This IRA Report outlines the methods implemented; sampling results and disposal
quantities; and overall conclusions, including the implications this IRA has on the overall Site risk
assessment.

INTERIM REMOVAL ACTION

Soil removal activities were conducted by Burgess Construction Group at the Site throughout July
and August 2017. In general, the work included the following activities:
• Site preparation and debris removal;
• soil removal and stockpiling;
• waste characterization soil sampling;

1 Recognized Environmental Conditions (RECs), as defined by the ASTM E1527 13 Standard.
2 “Finding A” refers to the findings as defined by Geosyntec in the January 2017 Phase I ESA.
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• confirmation soil sampling;
• soil disposal;
• backfill testing; and
• placement of backfill.
Multiple entities were involved in completing this project. The entities and their responsibilities
are described as follows:
• Geosyntec was the environmental consultant responsible for sample collection and
overseeing / managing the on-Site soil excavation and removal activities;
• TestAmerica Laboratories (Test America) performed the laboratory analysis and reporting
for the waste characterization and confirmation soil samples;
• SGS Accutest, Inc. (SGS) performed laboratory analysis and reporting for the backfill
samples;
• Burgess Construction Group (Burgess Construction) was the contractor responsible for:
Site clearing; soil excavation; and backfill grading and compaction in the excavation areas;
• Contaminant Control Inc. (CCI) was responsible for removing and disposing of debris
(non-soil);
• Capitol Environmental Services, Inc. (Capitol Environmental) was responsible for
coordinating waste (soil) transportation and disposal;
• ES&J Landfill was responsible for disposing petroleum / tar-impacted soils; and
• Sampson County Landfill (Roseboro, North Carolina) is responsible for the disposal of
excavated metals-contaminated soils.
Field activities were performed in Level D personal protective equipment (PPE). Prior to
mobilizing to the Site, Geosyntec notified NCDEQ and contacted North Carolina 811 to ensure
public underground utilities were marked.
Site Preparation and Debris Removal
Site access was largely clear of vegetation prior to performing the interim measure due to an on-
Site utility right-of-way (ROW); however, some light vegetative clearing was required for building
a heavy-vehicle temporary access road. Burgess Construction cleared vegetation for access and
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built a temporary stone and gravel driveway from Battleship Rd to the remedial area, generally
along the pre-existing utility ROW (shown in Figure 4). The Site wetlands were avoided during
clearing and access road construction.
Once proper ingress and egress were established, several structures and debris within the remedial
area were removed and transported off-Site, including a deteriorated winch and associated brake
pads, building debris, and portions of a concrete pad.
Soil Excavation
On 3 and 4 August 2017, Geosyntec oversaw soil excavation within the remedial area shown on
Figure 4. Soil removal was performed in two phases. First, the “tar/resin-impacted soil” was
excavated to the groundwater table (observed to be approximately 3 feet below ground surface) in
an approximate 10 feet by 10 feet area (“primary excavation”). The primary excavation was co-
located with the Phase II ESA test pit. Soil was removed to the approximate top of the water table
until no visible tar/resin was observed in the excavation.
A second, surficial excavation was performed along the top foot of soil surrounding the primary
excavation (“surficial excavation”). The surficial excavation included the surficial soil beneath
and proximal to the stick-up pipe and winch where metal and PAH impacts were detected above
NCDEQ PSRGs. The excavation area extended to the limits of the onsite wetlands on the southern
portion of the excavation; wetland areas were not disturbed or excavated.
The primary excavation and surficial excavation soils were stockpiled separately on visqueen and
covered while awaiting waste characterization and confirmation sampling results.
Waste Characterization and Confirmation Sampling
Composite waste characterization samples were collected from the soil excavation stockpiles to
evaluate hazardous versus non-hazardous waste disposal options. For each stockpile, three
aliquots were collected and composited for analysis (i.e., one composite sample from the primary
excavation stockpile and one composite sample from the surficial excavation stockpile). Waste
characterization samples were shipped to Test America for analysis of the 40 contaminants listed
in Table 1 of 40 CFR §261.24 using the Toxicity Characterization Leaching Procedure (TCLP).
The TCLP list includes select volatile organic compounds (VOCs), semi-volatile organic
compounds (SVOCs), pesticides, herbicides, and metals.
Following excavation and stockpiling, confirmation soil samples were collected at the locations as
shown on Figures 5a and 5b to confirm removal of impacted soils:
• Four sidewall samples collected at each of the four primary excavation sidewalls;
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• Three base samples collected below the surficial excavation area; and
• Three edge samples collected at the outer boundary of the surficial excavation area.
Sidewall samples were analyzed for SVOCs by EPA Method 8270D, and extractable petroleum
hydrocarbons (EPH) and volatile petroleum hydrocarbons (VPH) by the MADEP Method in
accordance with NCDEQ’s Guidelines for Site Checks, Tank Closures, and Initial Response.
SVOCs and metals were identified as Site COC categories during Phase II ESA activities; thus,
surficial excavation confirmations samples (i.e. base and edge samples) were analyzed for SVOCs
by EPA Method 8270D and metals by EPA Methods 6020B, 6010D, and 7471B. Laboratory
analytical reports are included in Attachment A. The results of the primary excavation and
surficial excavation confirmation samples are presented in Table 1a and Table 1b, respectively.
Results from the TCLP analyses for both the primary and surficial excavation stockpiles indicated
the soils were classified as non-hazardous waste. Surficial excavation confirmation results
identified select metals and SVOCs above commercial / industrial PSRGs for samples SURF-
EDGE-1 and SURF-BASE-3. In response, on 17 August 2017, Geosyntec and Burgess
Construction remobilized to the Site to over-excavate targeted regions of the surficial impact area
as shown on Figure 5b. These areas were excavated an additional 1-2 feet below the existing
grade; over-excavated soil was added to the existing surficial excavation stockpile. One edge
confirmation sample was collected following over-excavation as shown on Figure 5b. No
additional base samples were collected in the over excavated areas due to water infiltration.
Soil Disposal
Stockpiled soils remained covered on-Site until receipt of waste characterization and confirmation
sample results. Stockpiled soil was loaded directly onto trucks at the Site and transported to the
disposal location.

ES&J Enterprises disposed 42.09 tons of tar/resin-impacted soil that was excavated from the
primary excavation area. The dominant COCs in this soil were petroleum-related compounds;
thus, the material was disposed at a land farm. Transportation and disposal documentation is
presented in Attachment B.
Excavated soil from the surficial excavation area primarily contained metal-impacted soils and
was disposed off-Site at the Sampson County Landfill as non-hazardous contaminated soil. A
lined landfill is a more appropriate disposal option for the metal-impacted soils than the land
farming option implemented for petroleum-impacted soils. Disposal manifests for metals-
impacted soil are pending; Geosyntec estimates that approximately 60 to 90 tons of soil was
removed from the surficial excavation. The total weight of surficial soil removed from the Site for
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offsite disposal, including weigh tickets and disposal manifests, will be provided to NCDEQ under
separate cover, as an appendix to this report.
Backfilling
The soil excavations were backfilled for Site restoration and grading purposes. However, prior to
backfilling, a sample from the proposed soil backfill source (Sample ID: FILL-01) was collected
and analyzed for VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and the IHSB
Hazardous Substance List (HSL) metals by EPA Method 6010 or 6020. No VOCs or SVOCs were
detected and low-level metals were detected. The results of the backfill testing are summarized in
a 23 August 2017 Backfill Soil Authorization Memorandum. NCDEQ approved the backfill
source, the Sawmill Sand Mine, for use onsite in a 23 August 2017 email (Attachment C).
Upon receipt of the second-round confirmation sampling results, the primary excavation area was
backfilled with imported #57 gravel stone and the remaining surface excavation footprint was
filled to land surface with imported sand. Hauling tickets for imported backfill are pending and
will be provided to NCDEQ as an appendix to this report under separate cover.
CONCLUSIONS
An area of impacted soil identified during Geosyntec’s 2017 Phase II ESA activities was removed
and disposed off-Site as detailed in this document. Confirmation soil sampling results showed
Site metals and PAHs were largely removed within the excavation area to below PSRGs or Site
background levels. Geosyntec concludes that the 2017 Phase II ESA, in conjunction with this
IRA, satisfy the site assessment requirements of the Brownfields Agreement process.

Currently, Geosyntec is performing a Site risk assessment for remaining onsite soil that will be
submitted under separate cover. In accordance with this 2017 IRA, soil sample data from within
the excavation footprint will not be included in the risk assessment. This includes Phase II ESA
samples PS3, PS5, and SS-MW5, and IRA samples SURF-BASE-1, SURF-BASE-2, SURF-
BASE-3, SURF-EDGE-1, and EI-EXC-N1. We anticipate the results of the risk assessment will
show that unrestricted use at the Site will be permitted through the implementation of targeted
engineering controls. This may include placement of a clean backfill or cover (e.g., soil, asphalt
pavement, buildings, etc.) in select areas.

Following review of this IRA Report and Geosyntec’s forthcoming risk assessment, Geosyntec
requests NCDEQ’s concurrence that no additional assessment is required and that NCDEQ will
initiate drafting the Brownfields Agreement (BFA) for the Site. Upon agreement that the Site
assessment is complete, Geosyntec will submit an amended plat mat for NCDEQ approval.

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CLOSING

We look forward to NCDEQ’s review and approval of this Interim Removal Action Report. Please
feel free to contact the undersigned with any questions or comments.
Sincerely,

Matthew Jenny, E.I. Kaitlyn S. Rhonehouse, P.E.
Senior Staff Engineer Senior Engineer

FIGURES
Site Location Map
Figure
1
Raleigh, NC April 2017
Legend
Subject Site Boundary
³
Notes:
1. 2013 topographic map obtained from USGS The National
Boundaries Dataset.
2. Site is within the Wilmington Quadrangle.
3. Site Boundary was estimated based on information provided by
Brunswick County, North Carolina GIS Website.
0 1,000 2,000
Feet
0390000901
03900011
03900008
Subject Site: Parcel No. 0390000901, 03900011,
and 03900008
Battle Ship Road NE
Eagle Island, North Carolina
N:\GN6146 Burgess Eagle Island\GIS\MXD\Phase I ESA\Figure 1.mxd
Muddy Waters (Former Marine Railway)Cape FearRiverCape Fear Memorial BridgeBattleship RoadSubstationMetal Buildingwith Tank B WinchBoatWinchWood Shed D Metal DockAreaConcrete Slab and Concrete BlockBuilding A Remnants of Metal/Wood Building/Roof C Concrete I-BeamsConcrete BarricadesConcrete Foundation, Metal Mounting Structures, Electrical Box, and Stick Up PipesSubject Site: Parcel No. 0390000901, 03900011, and 03900008 Battle Ship Road NEEagle Island, North CarolinaRaleigh, NCAugust 2017Figure20 140 280FeetConcrete I-Beam on55 Gallon DrumsElectrical Box Owned by Adjacent Substation Present on Subject PropertyCarolina Christian Radio N:\GN6146 Burgess Eagle Island\GIS\MXD\Phase I ESA\Figure 2.mxd³Notes:1. Site Boundary was provided by Brunswick County Property Apprasier.2. 2013 Aerial Map was provided by ESRI Online Database.3. Refer to Geosyntec's 13 January 2017 Phase I ESA Report for A B C D description and Findings descriptions.LegendSubject Site BoundaryStick Up PipeSite Layout MapSite Features Removed as Part of Interim Removal Action
LegendNamePhase II ESA Grab DPT Soil SamplePhase II ESA Grab Hand Auger Soil SamplePhase II ESA Composite Soil Sample Zone BoundarySubject Site BoundaryApproximate Wetlands³Phase II ESA Soil Sampling Results forTest Pit AreaFigure3Raleigh, North CarolinaAugust 20170 40 80FeetNotes:1. Site Boundary was provided by Brunswick County Property Appraiser.2. 2013 Aerial Map was provided by ESRI Online Database.3. Discrete hand auger soil samples were collected by hand augering from approximately 0-1 foot below ground surface.4. SS-MW5 was collected from 1-2 feet below land surface. 5. All results are in milligrams per kilogram (mg/kg).6. PSRG indicates preliminary soil remediation goal7. PSRG values provided by the North Carolina Department of Environmental Quality, amended October 20168. Detections are identified in bold.9. Results with method detection limits exceeding PSRGs are identified in bold italics.10. DPT indicates direct push technology.11. J indicates estimated value.12. < indicates analyte was not detected above method detection limit.13. Highlighting corresponds to the following: yellow = exceedance of Residential PSRG, orange = exceedance of Commercial / Industrial PSRG.14. Only analytes exceeding one or more PSRG in one or more discrete or composite soil samples are displayed on figure.15. Wetland delineation based on survey completed by Southern Environmental Group, Inc. in March 2017.16. SVOC indicates semi-volatile organic compound.Arsenic9.33Copper1240Lead1660Manganese202Mercury7.40Thallium<0.265Benzo[a]anthracene<0.201Benzo[a]pyrene<0.181Benzo[b]fluoranthene<0.187Dibenz(a,h)anthracene<0.214Indeno[1,2,3-cd]pyrene<0.194Sampled on 3/8/17MetalsPS5SVOCsArsenic3.47Copper42.6Lead3,390Manganese53.9Mercury2.30Thallium <0.0524Benzo[a]anthracene0.131Benzo[a]pyrene0.148Benzo[b]fluoranthene0.175Dibenz(a,h)anthracene<0.0393Indeno[1,2,3-cd]pyrene0.0791 JMetalsSS-MW5Sampled on 3/23/17SVOCsConstituentResidential PSRG (mg/kg)Industrial / Commercial PSRG (mg/kg)Arsenic 0.680 3.00Copper 620 9400Lead 400 800Manganese 360 5200Mercury 2.20 3.13Thallium 0.156 2.40Benzo[a]anthracene 0.160 2.90Benzo[a]pyrene 0.0160 0.290Benzo[b]fluoranthene 0.160 2.90Dibenz(a,h)anthracene 0.0160 0.290Indeno[1,2,3-cd]pyrene 0.160 2.90N:\GN6353 Eagle Island Interim Measure\GIS\MXD\Figure 3.mxdSubject Site: Parcel No. 0390000901, 03900011, and 03900008 Battle Ship Road NEEagle Island, North CarolinaArsenic21.1Copper993Lead2860Manganese417Mercury7.55Thallium<0.291Benzo[a]anthracene0.259Benzo[a]pyrene0.317Benzo[b]fluoranthene0.399Dibenz(a,h)anthracene0.0788 JIndeno[1,2,3-cd]pyrene0.369SVOCsSampled on 3/8/17MetalsPS3WinchStick Up PipeTest Pit LocationBattleship RoadUtility Right-of-Way
³
Legend
Primary Excavation
Surficial Excavation
Access Route
Subject Site Boundary
Approximate Wetlands
15 ft
135 ft
280 ft
N:\GN6353 Eagle Island Interim Measure\GIS\MXD\Figure 4.mxd0 30 60Feet
Subject Site: Parcel No. 0390000901, 03900011,
and 03900008
Battle Ship Road NE, Eagle Island, North Carolina
Excavation Access Route and
Approximate Excavation Footprint
Figure
4August 2017Raleigh, NC
Notes:
1. Site Boundary was provided by Brunswick
County Property Appraiser.
2. 2013 Aerial Map was provided by ESRI Online
Database.
3. ft. BLS indicates feet below land surface.
4. Wetland delineation based on March 2017
survey completed by Southern Environmental Group,
Inc.Utility Right-of-Way

TABLES
Table 1a
Primary Excavation Soil Analytical Results
Parcels 0390000901, 03900011, and 03900008
Battle Ship Rd NE, Leland, NC
Sample ID EI-EXC-E1 EI-EXC-N1***EI-EXC-S1 EI-EXC-W1
Sample Date 8/4/2017 8/3/2017 8/3/2017 8/3/2017
Sample Type Grab Grab Grab Grab
Sample Depth (ft bgs)2 2 2 2
Units
1,2,4-Trichlorobenzene 11.6 52 NA NA mg/kg <0.224 <0.272 <0.214 <0.236
1,2-Dichlorobenzene 360 376 NA NA mg/kg <0.235 <0.285 <0.225 <0.248
1,3-Dichlorobenzene NA NA NA NA mg/kg <0.235 <0.285 <0.225 <0.248
1,4-Dichlorobenzene 2.6 11 NA NA mg/kg <0.243 <0.294 <0.232 <0.256
1-Methylnaphthalene 18 73 NA NA mg/kg <0.0347 <0.0420 <0.0331 <0.0365
2,4,5-Trichlorophenol 1,260 16,400 NA NA mg/kg <0.270 <0.327 <0.258 <0.284
2,4,6-Trichlorophenol 12.6 164 NA NA mg/kg <0.238 <0.288 <0.227 <0.251
2,4-Dichlorophenol 38 500 NA NA mg/kg <0.217 <0.263 <0.207 <0.228
2,4-Dimethylphenol 260 3,200 NA NA mg/kg <0.415 <0.503 <0.396 <0.437
2,4-Dinitrophenol 26 320 NA NA mg/kg <0.311 <0.377 <0.297 <0.328
2,4-Dinitrotoluene 1.7 7.4 NA NA mg/kg <0.258 <0.312 <0.246 <0.271
2,6-Dinitrotoluene 0.36 1.5 NA NA mg/kg <0.276 <0.335 <0.264 <0.291
2-Chloronaphthalene 960 12,000 NA NA mg/kg <0.259 <0.314 <0.247 <0.273
2-Chlorophenol 78 1,160 NA NA mg/kg <0.237 <0.287 <0.226 <0.249
2-Methylnaphthalene 48 600 NA NA mg/kg <0.0322 <0.0390 <0.0308 <0.0339
2-Methylphenol 640 8,200 NA NA mg/kg <0.268 <0.324 <0.255 <0.282
2-Nitroaniline 126 1,600 NA NA mg/kg <0.256 <0.311 <0.245 <0.270
2-Nitrophenol NA NA NA NA mg/kg <0.301 <0.365 <0.287 <0.317
3 & 4 Methylphenol NA NA NA NA mg/kg <0.251 <0.305 <0.240 <0.265
3,3'-Dichlorobenzidine 1.2 5.1 NA NA mg/kg <0.253 <0.306 <0.241 <0.266
3-Nitroaniline NA NA NA NA mg/kg <0.285 <0.345 <0.272 <0.300
4,6-Dinitro-2-methylphenol 1.02 13.2 NA NA mg/kg <0.284 <0.344 <0.271 <0.299
4-Bromophenyl phenyl ether NA NA NA NA mg/kg <0.254 <0.308 <0.242 <0.268
4-Chloro-3-methylphenol 1,260 16,400 NA NA mg/kg <0.208 <0.252 <0.199 <0.219
4-Chloroaniline 2,700 11 NA NA mg/kg <0.281 <0.341 <0.268 <0.296
4-Chlorophenyl phenyl ether NA NA NA NA mg/kg <0.249 <0.302 <0.238 <0.262
4-Nitroaniline 27 110 NA NA mg/kg <0.295 <0.357 <0.281 <0.311
4-Nitrophenol NA NA NA NA mg/kg <0.473 <0.573 <0.452 <0.498
Acenaphthene 720 9,000 NA NA mg/kg <0.0396 <0.0480 <0.0378 <0.0418
Acenaphthylene NA NA NA NA mg/kg <0.0359 <0.0435 <0.0343 <0.0378
Anthracene 3,600 46,000 NA NA mg/kg <0.0359 <0.0435 <0.0343 <0.0378
Benzo[a]anthracene 0.16 2.9 NA NA mg/kg <0.0372 <0.0450 0.319 <0.0391
Benzo[a]pyrene 0.016 0.29 NA NA mg/kg 0.0683 J 0.0674 J 0.311 0.0518 J
Benzo[b]fluoranthene 0.16 2.9 NA NA mg/kg 0.0478 J <0.0420 0.416 <0.0365
Benzo[g,h,i]perylene NA NA NA NA mg/kg <0.0409 <0.0495 0.238 <0.0431
Benzo[k]fluoranthene 1.6 29 NA NA mg/kg <0.0334 <0.0405 0.220 <0.0352
bis (2-chloroisopropyl) ether 620 1,020 NA NA mg/kg <0.245 <0.297 <0.234 <0.258
Bis(2-chloroethoxy)methane 38 500 NA NA mg/kg <0.248 <0.300 <0.237 <0.261
Semi-Volatile Organic Compounds (SVOCs) by EPA Method 8270 D
Analyte Residential PSRG
(mg/kg)
Commercial /
Industrial PSRG
(mg/kg)
Total Petroleum
Hydrocarbons
Gasoline Range
Organics (mg/kg)
Total Petroleum
Hydrocarbons
Diesel Range
Organics (mg/kg)
Page 1 of 3
Table 1a
Primary Excavation Soil Analytical Results
Parcels 0390000901, 03900011, and 03900008
Battle Ship Rd NE, Leland, NC
Sample ID EI-EXC-E1 EI-EXC-N1***EI-EXC-S1 EI-EXC-W1
Sample Date 8/4/2017 8/3/2017 8/3/2017 8/3/2017
Sample Type Grab Grab Grab Grab
Sample Depth (ft bgs)2 2 2 2
Units
Analyte Residential PSRG
(mg/kg)
Commercial /
Industrial PSRG
(mg/kg)
Total Petroleum
Hydrocarbons
Gasoline Range
Organics (mg/kg)
Total Petroleum
Hydrocarbons
Diesel Range
Organics (mg/kg)
Bis(2-chloroethyl)ether 0.23 1 NA NA mg/kg <0.264 <0.320 <0.252 <0.278
Bis(2-ethylhexyl) phthalate 39 160 NA NA mg/kg <0.256 <0.311 <0.245 <0.270
Butyl benzyl phthalate 290 1,200 NA NA mg/kg <0.266 <0.323 <0.254 <0.281
Carbazole NA NA NA NA mg/kg <0.256 <0.311 <0.245 <0.270
Chrysene 16 290 NA NA mg/kg <0.0458 <0.0555 0.321 <0.0483
Cresols 1,260 16,400 NA NA mg/kg <0.140 <0.170 <0.134 <0.147
Dibenz(a,h)anthracene 0.016 0.29 NA NA mg/kg <0.0396 <0.0480 0.0540 J <0.0418
Dibenzofuran 14.6 200 NA NA mg/kg <0.260 <0.315 <0.248 <0.274
Diethyl phthalate 10,200 100,000 NA NA mg/kg <0.263 <0.318 <0.251 <0.277
Dimethyl phthalate NA NA NA NA mg/kg <0.256 <0.311 <0.245 <0.270
Di-n-butyl phthalate 1260 16,400 NA NA mg/kg <0.261 <0.317 <0.250 <0.275
Di-n-octyl phthalate 126 1,640 NA NA mg/kg <0.220 <0.267 <0.211 <0.232
Fluoranthene 480 6,000 NA NA mg/kg 0.0449 J <0.0510 0.399 <0.0444
Fluorene 480 6,000 NA NA mg/kg <0.0359 <0.0435 <0.0343 <0.0378
Hexachlorobenzene 0.21 0.96 NA NA mg/kg <0.310 <0.375 <0.296 <0.326
Hexachlorobutadiene 1.2 5.3 NA NA mg/kg <0.207 <0.251 <0.198 <0.218
Hexachlorocyclopentadiene 0.36 1.5 NA NA mg/kg <0.186 *<0.225 *<0.177 *<0.196 *
Hexachloroethane 1.8 8 NA NA mg/kg <0.224 <0.272 <0.214 <0.236
Indeno[1,2,3-cd]pyrene 0.16 2.9 NA NA mg/kg <0.0359 <0.0435 0.176 <0.0378
Isophorone 570 2,400 NA NA mg/kg <0.233 <0.282 <0.222 <0.245
Naphthalene 3.8 17 NA NA mg/kg <0.0359 <0.0435 <0.0343 <0.0378
Nitrobenzene 5.1 22 NA NA mg/kg <0.249 <0.302 <0.238 <0.262
N-Nitrosodi-n-propylamine 0.078 0.33 NA NA mg/kg <0.240 <0.291 <0.229 <0.253
n-Nitrosodiphenylamine(as diphenylamine)110 470 NA NA mg/kg <0.0656 <0.0795 <0.0627 <0.0692
Pentachlorophenol 1 4 NA NA mg/kg <0.329 <0.399 <0.315 <0.347
Phenanthrene NA NA NA NA mg/kg <0.0421 <0.0510 0.0596 J <0.0444
Phenol 3,800 50,000 NA NA mg/kg <0.251 <0.305 <0.240 <0.265
Pyrene 360 4,600 NA NA mg/kg 0.0444 J <0.0510 0.402 <0.0444
C5-C8 Aliphatics NA NA mg/kg <3.74 <5.26 <3.42 <4.06
C9-C10 Aromatics NA NA mg/kg <4.32 <6.07 <3.94 <4.69
C9-C12 Aliphatics NA NA mg/kg 6.68 J 8.67 J 5.70 J 6.63 J
C9-C12 Aliphatics (North Carolina)NA NA mg/kg 6.68 8.67 5.70 J 6.63
Total VPH NA NA mg/kg 10.71 14.34 9.38 11.01
Volatile Petroleum Hydrocarbons (VPH) by the MADEP Method
50 (Total)NA
Page 2 of 3
Table 1a
Primary Excavation Soil Analytical Results
Parcels 0390000901, 03900011, and 03900008
Battle Ship Rd NE, Leland, NC
Sample ID EI-EXC-E1 EI-EXC-N1***EI-EXC-S1 EI-EXC-W1
Sample Date 8/4/2017 8/3/2017 8/3/2017 8/3/2017
Sample Type Grab Grab Grab Grab
Sample Depth (ft bgs)2 2 2 2
Units
Analyte Residential PSRG
(mg/kg)
Commercial /
Industrial PSRG
(mg/kg)
Total Petroleum
Hydrocarbons
Gasoline Range
Organics (mg/kg)
Total Petroleum
Hydrocarbons
Diesel Range
Organics (mg/kg)
C11-C22 Aromatics NA NA mg/kg 8.10 J 11.3 J <5.46 24.8
C19-C36 Aliphatics NA NA mg/kg <6.27 <7.48 10.7 J <6.45
C9-C18 Aliphatics NA NA mg/kg <3.01 <3.59 <2.67 <3.09
Total EPH NA NA mg/kg 12.74 16.835 14.77 29.57
Notes:
(1) < indicates analyte was not detected above method detection limits
(2) J indicates an estimated value
(3) * indicates laboratory control samples or laboratory control sample duplicates is outside acceptance limits
(4) mg/kg indicates milligrams per kilogram
(5) NA indicates analyte standard not available
(6) Analyte detections (e.g., 6.68) are identified in bold
(7) PSRG indicates North Carolina Department of Environmental Quality (NCDEQ) Inactive Hazardous Sites Preliminary Remediation Goal, amended October 2016
(8) All analyzed constituents are included in this table
(9) If multiple screening criteria are exceeded, the highlight corresponds to the highest value screening criteria exceedance
(10) Analytes that were not detected (i.e. concentrations that were below the laboratory Method Detection Limit [MDL]), but exceeded a PSRG standard are identified in italics and in bold
(11) TPH GRO and TPH DRO standards taken from NCDEQ 26 July 2016 Guidelines for North Carolina Action Limits for Total Petroleum Hydrocarbons (TPH)
Residential PSRG Commercial /
Industrial PSRG
Total Petroleum
Hydrocarbons
Gasoline Range
Organics
Total Petroleum
Hydrocarbons Diesel
Range Organics
(14) ft bgs indicates feet below ground surface
(15) For total VPH and EPH calculations, half of the method detection limit was used for non-detected analytes
(16) MADEP indicates Massachusetts Department of Environmental Protection
(12) Concentrations exceeding PSRGs are highlighted in
bold as shown:
(13) *** indicates that the area where this sample was collected was overexcavated and disposed of off-Site following analysis of sample results. Constituent concentrations for these samples are also
highlighted in gray.
100 (Total)
Extractable Petroleum Hydrocarbons (EPH) by the MADEP Method
NA
Page 3 of 3
Table 1b
Surficial Excavation Soil Analytical Results
Parcels 0390000901, 03900011, and 03900008
Battle Ship Rd NE, Leland, NC
Sample ID SURF-EDGE-1***SURF-EDGE-2 SURF-EDGE-3 SURF-EDGE-4 SURF-BASE-1***SURF-BASE-2***SURF-BASE-3***
Sample Date 8/4/2017 8/4/2017 8/4/2017 8/17/2017 8/4/2017 8/4/2017 8/4/2017
Sample Type Grab Grab Grab Grab Grab Grab Grab
Sample Depth (ft bgs)0-2 0-2 0-2 0-2 0-2 0-2 0-2
Units
1,2,4-Trichlorobenzene 11.6 52 mg/kg <1.18 <0.212 <0.212 <0.202 <0.287 <1.20 <0.243
1,2-Dichlorobenzene 360 376 mg/kg <1.24 <0.222 <0.222 <0.213 <0.301 <1.26 <0.255
1,3-Dichlorobenzene NA NA mg/kg <1.24 <0.222 <0.222 <0.213 <0.301 <1.26 <0.255
1,4-Dichlorobenzene 2.6 11 mg/kg <1.28 <0.229 <0.229 <0.219 <0.311 <1.30 <0.263
1-Methylnaphthalene 18 73 mg/kg <0.182 <0.0328 <0.0327 <0.0313 <0.0444 <0.185 <0.0376
2,4,5-Trichlorophenol 1,260 16,400 mg/kg <1.42 <0.255 <0.255 <0.244 <0.346 <1.44 <0.293
2,4,6-Trichlorophenol 12.6 164 mg/kg <1.25 <0.225 <0.225 <0.215 <0.304 <1.27 <0.258
2,4-Dichlorophenol 38 500 mg/kg <1.14 <0.205 <0.205 <0.196 <0.277 <1.16 <0.235
2,4-Dimethylphenol 260 3,200 mg/kg <2.18 <0.392 <0.392 <0.375 <0.531 <2.22 <0.450
2,4-Dinitrophenol 26 320 mg/kg <1.63 <0.294 <0.294 <0.281 <0.398 <1.66 <0.337
2,4-Dinitrotoluene 1.7 7.4 mg/kg <1.35 <0.243 <0.243 <0.233 <0.330 <1.38 <0.279
2,6-Dinitrotoluene 0.36 1.5 mg/kg <1.45 <0.261 <0.261 <0.249 <0.354 <1.48 <0.300
2-Chloronaphthalene 960 12,000 mg/kg <1.36 <0.244 <0.244 <0.234 <0.331 <1.38 <0.281
2-Chlorophenol 78 1,160 mg/kg <1.24 <0.223 <0.223 <0.214 <0.303 <1.27 <0.257
2-Methylnaphthalene 48 600 mg/kg <0.169 <0.0304 <0.0304 <0.0291 <0.0412 <0.172 <0.0349
2-Methylphenol 640 8,200 mg/kg <1.41 <0.253 <0.253 <0.242 <0.342 <1.43 <0.290
2-Nitroaniline 126 1,600 mg/kg <1.35 <0.242 <0.242 <0.232 <0.328 <1.37 <0.278
2-Nitrophenol NA NA mg/kg <1.58 <0.284 <0.284 <0.272 <0.385 <1.61 <0.326
3 & 4 Methylphenol NA NA mg/kg <1.32 <0.237 <0.237 <0.227 <0.322 <1.34 <0.273
3,3'-Dichlorobenzidine 1.2 5.1 mg/kg <1.33 <0.239 <0.239 <0.228 <0.323 <1.35 <0.274
3-Nitroaniline NA NA mg/kg <1.50 <0.269 <0.269 <0.257 <0.365 <1.52 <0.309
4,6-Dinitro-2-methylphenol 1.02 13.2 mg/kg <1.49 <0.268 <0.268 <0.256 <0.363 <1.52 <0.308
4-Bromophenyl phenyl ether NA NA mg/kg <1.34 <0.240 <0.240 <0.229 <0.325 <1.36 <0.275
4-Chloro-3-methylphenol 1,260 16,400 mg/kg <1.09 <0.197 <0.196 <0.188 <0.266 <1.11 <0.226
4-Chloroaniline 2,700 11 mg/kg <1.48 <0.266 <0.265 <0.254 <0.360 <1.50 <0.305
4-Chlorophenyl phenyl ether NA NA mg/kg <1.31 <0.235 <0.235 <0.225 <0.319 <1.33 <0.270
4-Nitroaniline 27 110 mg/kg <1.55 <0.278 <0.278 <0.266 <0.377 <1.58 <0.320
4-Nitrophenol NA NA mg/kg <2.49 <0.447 <0.447 <0.427 <0.606 <2.53 <0.513
Acenaphthene 720 9,000 mg/kg 0.671 <0.0374 <0.0374 <0.0358 <0.0507 <0.212 <0.0430
Acenaphthylene NA NA mg/kg <0.189 <0.0339 <0.0339 <0.0324 <0.0460 <0.192 <0.0390
Anthracene 3,600 46,000 mg/kg 1.34 <0.0339 <0.0339 <0.0324 <0.0460 <0.192 0.0922
Benzo[a]anthracene 0.16 2.9 mg/kg 4.87 0.0554 J <0.0351 <0.0336 <0.0476 <0.199 0.273
Benzo[a]pyrene 0.016 0.29 mg/kg 3.98 0.0915 0.0543 J <0.0302 0.0573 J <0.179 0.265
Benzo[b]fluoranthene 0.16 2.9 mg/kg 5.32 0.0877 0.0348 J <0.0313 <0.0444 <0.185 0.280
Benzo[g,h,i]perylene NA NA mg/kg 2.47 0.0586 J <0.0386 <0.0369 <0.0523 <0.219 0.199
Benzo[k]fluoranthene 1.6 29 mg/kg 2.95 0.0437 J <0.0316 <0.0302 <0.0428 <0.179 0.173
bis (2-chloroisopropyl) ether 620 1,020 mg/kg <1.29 <0.232 <0.232 <0.221 <0.314 <1.31 <0.266
Bis(2-chloroethoxy)methane 38 500 mg/kg <1.30 <0.234 <0.234 <0.224 <0.317 <1.32 <0.269
Bis(2-chloroethyl)ether 0.23 1 mg/kg <1.39 <0.249 <0.249 <0.238 <0.338 <1.41 <0.286
Bis(2-ethylhexyl) phthalate 39 160 mg/kg <1.35 <0.242 <0.242 <0.232 <0.328 <1.37 <0.278
Butyl benzyl phthalate 290 1,200 mg/kg <1.40 <0.252 <0.251 <0.240 <0.341 <1.42 <0.289
Carbazole NA NA mg/kg <1.35 <0.242 <0.242 <0.232 <0.328 <1.37 <0.278
Chrysene 16 290 mg/kg 5.01 0.0538 J <0.0433 <0.0414 <0.0587 <0.245 0.249
Cresols 1,260 16,400 mg/kg <0.736 <0.132 <0.132 <0.126 <0.179 <0.749 <0.152
Dibenz(a,h)anthracene 0.016 0.29 mg/kg 0.721 <0.0374 <0.0374 <0.0358 <0.0507 <0.212 <0.0430
Dibenzofuran 14.6 200 mg/kg <1.37 <0.246 <0.246 <0.235 <0.333 <1.39 <0.282
Diethyl phthalate 10,200 100,000 mg/kg <1.38 <0.248 <0.248 <0.237 <0.336 <1.40 <0.285
Semi-Volatile Organic Compounds (SVOCs) by EPA Method 8270 D
Analyte Residential PSRG
(mg/kg)
Commercial /
Industrial PSRG
(mg/kg)
Page 1 of 3
Table 1b
Surficial Excavation Soil Analytical Results
Parcels 0390000901, 03900011, and 03900008
Battle Ship Rd NE, Leland, NC
Sample ID SURF-EDGE-1***SURF-EDGE-2 SURF-EDGE-3 SURF-EDGE-4 SURF-BASE-1***SURF-BASE-2***SURF-BASE-3***
Sample Date 8/4/2017 8/4/2017 8/4/2017 8/17/2017 8/4/2017 8/4/2017 8/4/2017
Sample Type Grab Grab Grab Grab Grab Grab Grab
Sample Depth (ft bgs)0-2 0-2 0-2 0-2 0-2 0-2 0-2
Units
Analyte Residential PSRG
(mg/kg)
Commercial /
Industrial PSRG
(mg/kg)
Dimethyl phthalate NA NA mg/kg <1.35 <0.242 <0.242 <0.232 <0.328 <1.37 <0.278
Di-n-butyl phthalate 1260 16,400 mg/kg <1.37 <0.247 <0.247 <0.236 <0.335 <1.40 <0.283
Di-n-octyl phthalate 126 1,640 mg/kg <1.16 <0.208 <0.208 <0.199 <0.282 <1.18 <0.239
Fluoranthene 480 6,000 mg/kg 10.6 0.0798 <0.0398 <0.0380 <0.0539 <0.225 0.497
Fluorene 480 6,000 mg/kg 0.494 <0.0339 <0.0339 <0.0324 <0.0460 <0.192 <0.0390
Hexachlorobenzene 0.21 0.96 mg/kg <1.63 <0.292 <0.292 <0.280 <0.396 <1.66 <0.336
Hexachlorobutadiene 1.2 5.3 mg/kg <1.09 <0.195 <0.195 <0.187 <0.265 <1.11 <0.224
Hexachlorocyclopentadiene 0.36 1.5 mg/kg <0.977 *<0.175 *<0.175 *<0.168 *<0.238 *<0.994 *<0.202 *
Hexachloroethane 1.8 8 mg/kg <1.18 <0.212 <0.212 <0.202 <0.287 <1.20 <0.243
Indeno[1,2,3-cd]pyrene 0.16 2.9 mg/kg 2.16 0.0522 J <0.0339 <0.0324 <0.0460 <0.192 0.161
Isophorone 570 2,400 mg/kg <1.22 <0.220 <0.220 <0.210 <0.298 <1.25 <0.253
Naphthalene 3.8 17 mg/kg <0.189 <0.0339 <0.0339 <0.0324 <0.0460 <0.192 <0.0390
Nitrobenzene 5.1 22 mg/kg <1.31 <0.235 <0.235 <0.225 <0.319 <1.33 <0.270
N-Nitrosodi-n-propylamine 0.078 0.33 mg/kg <1.26 <0.227 <0.227 <0.217 <0.308 <1.29 <0.261
n-Nitrosodiphenylamine(as diphenylamine)110 470 mg/kg <0.345 <0.0620 <0.0620 <0.0593 <0.0840 <0.351 <0.0712
Pentachlorophenol 1 4 mg/kg <1.73 <0.311 <0.311 <0.298 <0.422 <1.76 <0.357
Phenanthrene NA NA mg/kg 7.01 <0.0398 <0.0398 <0.0380 <0.0539 <0.225 0.258
Phenol 3,800 50,000 mg/kg <1.32 <0.237 <0.237 <0.227 <0.322 <1.34 <0.273
Pyrene 360 4,600 mg/kg 8.83 0.0759 J <0.0398 <0.0380 <0.0539 <0.225 0.493
Page 2 of 3
Table 1b
Surficial Excavation Soil Analytical Results
Parcels 0390000901, 03900011, and 03900008
Battle Ship Rd NE, Leland, NC
Sample ID SURF-EDGE-1***SURF-EDGE-2 SURF-EDGE-3 SURF-EDGE-4 SURF-BASE-1***SURF-BASE-2***SURF-BASE-3***
Sample Date 8/4/2017 8/4/2017 8/4/2017 8/17/2017 8/4/2017 8/4/2017 8/4/2017
Sample Type Grab Grab Grab Grab Grab Grab Grab
Sample Depth (ft bgs)0-2 0-2 0-2 0-2 0-2 0-2 0-2
Units
Analyte Residential PSRG
(mg/kg)
Commercial /
Industrial PSRG
(mg/kg)
Antimony 6.2 94 mg/kg 0.510 J 0.557 J 0.240 J <1.09 ^1.75 0.367 J 1.07
Arsenic 0.68 3 mg/kg 5.66 5.10 2.03 <1.31 10.4 5.26 9.21
Beryllium 32 460 mg/kg <0.261 0.355 J <0.230 <0.218 1.49 J 0.618 J <0.274
Cadmium 14.2 196 mg/kg 0.313 J <0.118 <0.115 <0.109 <0.159 <0.129 2.63
Chromium 24,000 100,000 mg/kg 9.60 11.3 3.45 <0.983 25.0 B 14.3 3.97
Copper 620 9,400 mg/kg 335 23.000 34.2 <1.20 1070 57.8 174
Lead 400 800 mg/kg 142 72.1 76.5 <0.546 644 86.6 1240
Manganese 360 5,200 mg/kg 193 185 94.5 3.69 486 118 204
Mercury 2.2 3.13 mg/kg 222 F2 0.351 0.324 <0.0336 0.432 0.264 0.483
Nickel 300 4,400 mg/kg 3.23 2.79 1.50 J <0.655 6.67 4.38 2.52 J
Selenium 78 1,160 mg/kg <1.43 <1.30 <1.27 <1.20 <1.75 <1.42 <1.51
Thallium 0.156 2.4 mg/kg <0.249 <0.229 <0.224 <0.437 <0.310 <0.255 <0.272
Silver 78 1,160 mg/kg <0.522 0.615 J <0.460 <0.655 2.70 0.644 J 0.575 J
Zinc 4,600 70,000 mg/kg 228 55.3 58.7 <5.46 131 92.1 750
Notes:
(1) < indicates analyte was not detected above method detection limits
(2) J indicates an estimated value
(3) B indicates analyte was detected in method blank
(4) F2 indicates MS/MSD relative percent difference exceeds control limits
(5) * indicates laboratory control sample or laboratory control sample duplicate is outside acceptance limits
(6) mg/kg indicates milligrams per kilogram
(7) NA indicates analyte standard not available
(8) Analyte detections (e.g., 6.68) are identified in bold
(9) PSRG indicates North Carolina Department of Environmental Quality (NCDEQ) Inactive Hazardous Sites Preliminary Remediation Goal, amended October 2016
(10) All analyzed constituents are included in this table
(11) If multiple screening criteria are exceeded, the highlight corresponds to the highest value screening criteria exceedance
(12) Analytes that were not detected (i.e. concentrations that were below the laboratory Method Detection Limit [MDL]), but exceeded a PSRG standard are identified in italics and in bold
(13) Concentrations exceeding PSRGs are highlighted in bold as shown:
Residential PSRG Commercial /
Industrial PSRG
(14) *** indicates that the area where this sample was collected was overexcavated and disposed off-Site following analysis of sample results. Constituent concentrations for these samples are also highlighted in gray.
(15) ft bgs indicates feet below ground surface
(16) ^ indicates instrument related QC is outside acceptance limits
Metals by EPA Methods 6020B, 6010D, and 7471B
Page 3 of 3

ATTACHMENTS
ATTACHMENT A
LABORATORY ANALYTICAL REPORTS
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-133167-1
Client Project/Site: Eagle Island
For:
Geosyntec Consultants, Inc.
2501 Blue Ridge Rd.
Suite 430
Raleigh, North Carolina 27607
Attn: Ms. Kaitlyn S Rhonehouse
Authorized for release by:
7/27/2017 2:05:04 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
TestAmerica Job ID: 490-133167-1
Page 2 of 29 TestAmerica Nashville7/27/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
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Sample Summary
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-133167-1 SURFACE-TCLP-170719 Solid 07/19/17 10:45 07/20/17 09:05
490-133167-2 EXCAVATION-TCLP-170719 Solid 07/19/17 11:20 07/20/17 09:05
TestAmerica Nashville
Page 3 of 29 7/27/2017
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Case Narrative
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-133167-1
Project/Site: Eagle Island
Job ID: 490-133167-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-133167-1
Comments
No additional comments.
Receipt
The samples were received on 7/20/2017 9:05 AM; the samples arrived in good condition, properly preserved. Samples were received
above the recommended temperature of 6.0°C. The temperature of the cooler at receipt was 15.7º C.
Receipt Exceptions
The following samples were received at the laboratory outside the required temperature criteria: SURFACE-TCLP-170719 (490-133167-1)
and EXCAVATION-TCLP-170719 (490-133167-2). There was no cooling media present in the cooler. The client was contacted regarding
this issue, and the laboratory was instructed to proceed with analysis.
GC/MS VOA
Method 8260B: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical batch
490-447438 recovered outside control limits for the following analytes: Trichloroethene, Vinyl chloride, 1,2-Dichloroethane, 2-Butanone
(MEK), Benzene, Carbon tetrachloride, Chlorobenzene, Chloroform and Tetrachloroethene.
Method 8260B: The TCLP leachate blank for batch 490-446966 contained a target analyte above the reporting limit (RL). None of the
samples associated with this leachate blank contained this target analyte; therefore, re-extraction of the samples was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-447040 and analytical batch 490-447145.
Method 8270D: The continuing calibration verification (CCV) associated with batch 490-447299 recovered above the upper control limit for
Nitrobenzene-d5, Pyridine, 2-Fluorophenol (Surr), Phenol-d5 (Surr) and Nitrobenzene. The samples associated with this CCV were
non-detect for analytes associated with this surrogate; therefore, the data has been reported. The following sample is impacted: (CCVIS
490-447299/3).
Method 8270D: The continuing calibration verification (CCVIS) associated with batch 490-447464 recovered above the upper control limit
for Nitrobenzene and Pyridine. The samples associated with this CCVIS were non-detect for the affected analytes; therefore, the data has
been reported. The following sample is impacted: (CCVIS 490-447464/3).
Method 8270D: Surrogate recovery for the following sample was outside the upper control limit: EXCAVATION-TCLP-170719
(490-133167-2). This sample did not contain any target analytes; therefore, re-extraction was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
Method 8081B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-447043 and analytical batch 490-447169.
Method 8081B: The closing continuing calibration verification (CCVC) associated with batch 490-447169 recovered above the upper
control limit for Toxaphene. The samples associated with this CCV were non-detects for the affected analyte; therefore, the data has been
reported.
Method 8151A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-447044 and analytical batch 490-447172.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica NashvillePage 4 of 29 7/27/2017
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Case Narrative
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-133167-1
Project/Site: Eagle Island
Job ID: 490-133167-1 (Continued)
Laboratory: TestAmerica Nashville (Continued)
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Qualifiers
GC/MS VOA
Qualifier Description
*RPD of the LCS and LCSD exceeds the control limits
Qualifier
GC/MS Semi VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-133167-1Client Sample ID: SURFACE-TCLP-170719
Matrix: SolidDate Collected: 07/19/17 10:45
Date Received: 07/20/17 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS) - TCLP
RL MDL
1,1-Dichloroethene <0.00250 0.0100 0.00250 mg/L 07/25/17 14:49 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00200 mg/L 07/25/17 14:49 101,2-Dichloroethane <0.00200
0.500 0.0260 mg/L 07/25/17 14:49 102-Butanone (MEK)<0.0260
0.0100 0.00200 mg/L 07/25/17 14:49 10Benzene<0.00200
0.0100 0.00180 mg/L 07/25/17 14:49 10Carbon tetrachloride <0.00180
0.0100 0.00180 mg/L 07/25/17 14:49 10Chlorobenzene<0.00180
0.0100 0.00250 mg/L 07/25/17 14:49 10Tetrachloroethene<0.00250
0.0100 0.00200 mg/L 07/25/17 14:49 10Trichloroethene<0.00200
0.0100 0.00240 mg/L 07/25/17 14:49 10Vinyl chloride <0.00240
0.0100 0.00230 mg/L 07/25/17 14:49 10Chloroform<0.00230
1,2-Dichloroethane-d4 (Surr)85 70-130 07/25/17 14:49 10
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)101 07/25/17 14:49 1070-130
Dibromofluoromethane (Surr)97 07/25/17 14:49 1070-130
Toluene-d8 (Surr)102 07/25/17 14:49 1070-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS) - TCLP
RL MDL
1,4-Dichlorobenzene <0.00620 0.0200 0.00620 mg/L 07/24/17 13:14 07/24/17 21:16 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0600 0.00380 mg/L 07/24/17 13:14 07/24/17 21:16 22,4,5-Trichlorophenol <0.00380
0.0200 0.00320 mg/L 07/24/17 13:14 07/24/17 21:16 22,4,6-Trichlorophenol <0.00320
0.0200 0.00380 mg/L 07/24/17 13:14 07/24/17 21:16 22,4-Dinitrotoluene <0.00380
0.0400 0.0280 mg/L 07/24/17 13:14 07/24/17 21:16 2Cresols<0.0280
0.0200 0.00360 mg/L 07/24/17 13:14 07/24/17 21:16 2Hexachlorobenzene<0.00360
0.0200 0.00600 mg/L 07/24/17 13:14 07/24/17 21:16 2Hexachlorobutadiene<0.00600
0.0200 0.00640 mg/L 07/24/17 13:14 07/24/17 21:16 2Hexachloroethane<0.00640
0.0200 0.00380 mg/L 07/24/17 13:14 07/24/17 21:16 2Nitrobenzene<0.00380
0.0200 0.00360 mg/L 07/24/17 13:14 07/24/17 21:16 2Pyridine<0.00360
0.0600 0.00700 mg/L 07/24/17 13:14 07/24/17 21:16 2Pentachlorophenol<0.00700
2,4,6-Tribromophenol (Surr)76 10-120 07/24/17 13:14 07/24/17 21:16 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)68 07/24/17 13:14 07/24/17 21:16 229-120
2-Fluorophenol (Surr)95 07/24/17 13:14 07/24/17 21:16 210-120
Nitrobenzene-d5 (Surr)86 07/24/17 13:14 07/24/17 21:16 227-120
Phenol-d5 (Surr)82 07/24/17 13:14 07/24/17 21:16 210-120
Terphenyl-d14 (Surr)85 07/24/17 13:14 07/24/17 21:16 213-120
Method: 8081B - Organochlorine Pesticides (GC) - TCLP
RL MDL
gamma-BHC (Lindane)<0.000100 0.00100 0.000100 mg/L 07/24/17 13:39 07/24/17 18:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00100 0.000700 mg/L 07/24/17 13:39 07/24/17 18:31 1Chlordane (technical)<0.000700
0.00100 0.000100 mg/L 07/24/17 13:39 07/24/17 18:31 1Endrin<0.000100
0.00100 0.000100 mg/L 07/24/17 13:39 07/24/17 18:31 1Heptachlor<0.000100
0.00100 0.000700 mg/L 07/24/17 13:39 07/24/17 18:31 1Heptachlor epoxide <0.000700
0.00100 0.000100 mg/L 07/24/17 13:39 07/24/17 18:31 1Methoxychlor<0.000100
0.0500 0.0350 mg/L 07/24/17 13:39 07/24/17 18:31 1Toxaphene<0.0350
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Client Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-133167-1Client Sample ID: SURFACE-TCLP-170719
Matrix: SolidDate Collected: 07/19/17 10:45
Date Received: 07/20/17 09:05
Tetrachloro-m-xylene 76 27-129 07/24/17 13:39 07/24/17 18:31 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr)81 07/24/17 13:39 07/24/17 18:31 124-132
Method: 8151A - Herbicides (GC) - TCLP
RL MDL
Silvex (2,4,5-TP)<0.0500 0.100 0.0500 mg/L 07/23/17 23:05 07/24/17 13:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.100 0.0500 mg/L 07/23/17 23:05 07/24/17 13:57 12,4-D <0.0500
Dichloroacetic acid(Surr)55 10-150 07/23/17 23:05 07/24/17 13:57 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP) - TCLP
RL MDL
Silver <0.0300 0.500 0.0300 mg/L 07/24/17 11:00 07/25/17 12:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 0.0860 mg/L 07/24/17 11:00 07/25/17 12:27 1Arsenic<0.0860
10.0 0.0500 mg/L 07/24/17 11:00 07/25/17 12:27 1Barium0.235 J
0.100 0.00500 mg/L 07/24/17 11:00 07/25/17 12:27 1Cadmium<0.00500
0.500 0.0300 mg/L 07/24/17 11:00 07/25/17 12:27 1Chromium<0.0300
0.500 0.0200 mg/L 07/24/17 11:00 07/25/17 12:27 1Lead0.242 J
0.100 0.0500 mg/L 07/24/17 11:00 07/25/17 12:27 1Selenium<0.0500
Method: 7470A - Mercury (CVAA) - TCLP
RL MDL
Mercury <0.00100 0.00200 0.00100 mg/L 07/24/17 12:05 07/24/17 15:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-133167-2Client Sample ID: EXCAVATION-TCLP-170719
Matrix: SolidDate Collected: 07/19/17 11:20
Date Received: 07/20/17 09:05
Method: 8260B - Volatile Organic Compounds (GC/MS) - TCLP
RL MDL
1,1-Dichloroethene <0.00250 0.0100 0.00250 mg/L 07/25/17 14:19 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00200 mg/L 07/25/17 14:19 101,2-Dichloroethane <0.00200
0.500 0.0260 mg/L 07/25/17 14:19 102-Butanone (MEK)<0.0260
0.0100 0.00200 mg/L 07/25/17 14:19 10Benzene<0.00200
0.0100 0.00180 mg/L 07/25/17 14:19 10Carbon tetrachloride <0.00180
0.0100 0.00180 mg/L 07/25/17 14:19 10Chlorobenzene<0.00180
0.0100 0.00250 mg/L 07/25/17 14:19 10Tetrachloroethene<0.00250
0.0100 0.00200 mg/L 07/25/17 14:19 10Trichloroethene<0.00200
0.0100 0.00240 mg/L 07/25/17 14:19 10Vinyl chloride <0.00240
0.0100 0.00230 mg/L 07/25/17 14:19 10Chloroform<0.00230
1,2-Dichloroethane-d4 (Surr)86 70-130 07/25/17 14:19 10
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 07/25/17 14:19 1070-130
Dibromofluoromethane (Surr)97 07/25/17 14:19 1070-130
Toluene-d8 (Surr)100 07/25/17 14:19 1070-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS) - TCLP
RL MDL
1,4-Dichlorobenzene <0.00620 0.0200 0.00620 mg/L 07/24/17 17:24 07/25/17 19:37 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0600 0.00380 mg/L 07/24/17 17:24 07/25/17 19:37 22,4,5-Trichlorophenol <0.00380
0.0200 0.00320 mg/L 07/24/17 17:24 07/25/17 19:37 22,4,6-Trichlorophenol <0.00320
0.0200 0.00380 mg/L 07/24/17 17:24 07/25/17 19:37 22,4-Dinitrotoluene <0.00380
0.0400 0.0280 mg/L 07/24/17 17:24 07/25/17 19:37 2Cresols<0.0280
0.0200 0.00360 mg/L 07/24/17 17:24 07/25/17 19:37 2Hexachlorobenzene<0.00360
0.0200 0.00600 mg/L 07/24/17 17:24 07/25/17 19:37 2Hexachlorobutadiene<0.00600
0.0200 0.00640 mg/L 07/24/17 17:24 07/25/17 19:37 2Hexachloroethane<0.00640
0.0200 0.00380 mg/L 07/24/17 17:24 07/25/17 19:37 2Nitrobenzene<0.00380
0.0200 0.00360 mg/L 07/24/17 17:24 07/25/17 19:37 2Pyridine<0.00360
0.0600 0.00700 mg/L 07/24/17 17:24 07/25/17 19:37 2Pentachlorophenol<0.00700
2,4,6-Tribromophenol (Surr)151 X 10-120 07/24/17 17:24 07/25/17 19:37 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)74 07/24/17 17:24 07/25/17 19:37 229-120
2-Fluorophenol (Surr)101 07/24/17 17:24 07/25/17 19:37 210-120
Nitrobenzene-d5 (Surr)96 07/24/17 17:24 07/25/17 19:37 227-120
Phenol-d5 (Surr)91 07/24/17 17:24 07/25/17 19:37 210-120
Terphenyl-d14 (Surr)93 07/24/17 17:24 07/25/17 19:37 213-120
Method: 8081B - Organochlorine Pesticides (GC) - TCLP
RL MDL
gamma-BHC (Lindane)<0.000100 0.00100 0.000100 mg/L 07/24/17 17:25 07/25/17 11:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00100 0.000700 mg/L 07/24/17 17:25 07/25/17 11:51 1Chlordane (technical)<0.000700
0.00100 0.000100 mg/L 07/24/17 17:25 07/25/17 11:51 1Endrin<0.000100
0.00100 0.000100 mg/L 07/24/17 17:25 07/25/17 11:51 1Heptachlor<0.000100
0.00100 0.000700 mg/L 07/24/17 17:25 07/25/17 11:51 1Heptachlor epoxide <0.000700
0.00100 0.000100 mg/L 07/24/17 17:25 07/25/17 11:51 1Methoxychlor<0.000100
0.0500 0.0350 mg/L 07/24/17 17:25 07/25/17 11:51 1Toxaphene<0.0350
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Client Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-133167-2Client Sample ID: EXCAVATION-TCLP-170719
Matrix: SolidDate Collected: 07/19/17 11:20
Date Received: 07/20/17 09:05
Tetrachloro-m-xylene 61 27-129 07/24/17 17:25 07/25/17 11:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr)70 07/24/17 17:25 07/25/17 11:51 124-132
Method: 8151A - Herbicides (GC) - TCLP
RL MDL
Silvex (2,4,5-TP)<0.0500 0.100 0.0500 mg/L 07/23/17 23:05 07/24/17 14:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.100 0.0500 mg/L 07/23/17 23:05 07/24/17 14:12 12,4-D <0.0500
Dichloroacetic acid(Surr)98 10-150 07/23/17 23:05 07/24/17 14:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP) - TCLP
RL MDL
Silver <0.0300 0.500 0.0300 mg/L 07/24/17 11:00 07/25/17 12:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.500 0.0860 mg/L 07/24/17 11:00 07/25/17 12:21 1Arsenic<0.0860
10.0 0.0500 mg/L 07/24/17 11:00 07/25/17 12:21 1Barium0.432 J
0.100 0.00500 mg/L 07/24/17 11:00 07/25/17 12:21 1Cadmium0.0260 J
0.500 0.0300 mg/L 07/24/17 11:00 07/25/17 12:21 1Chromium<0.0300
0.500 0.0200 mg/L 07/24/17 11:00 07/25/17 12:21 1Lead3.83
0.100 0.0500 mg/L 07/24/17 11:00 07/25/17 12:21 1Selenium<0.0500
Method: 7470A - Mercury (CVAA) - TCLP
RL MDL
Mercury <0.00100 0.00200 0.00100 mg/L 07/24/17 12:05 07/24/17 15:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-447438/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447438
RL MDL
1,1-Dichloroethene <0.000250 0.00100 0.000250 mg/L 07/25/17 12:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000200 0.0002000.00100 mg/L 07/25/17 12:21 11,2-Dichloroethane
<0.00260 0.002600.0500 mg/L 07/25/17 12:21 12-Butanone (MEK)
<0.000200 0.0002000.00100 mg/L 07/25/17 12:21 1Benzene
<0.000180 0.0001800.00100 mg/L 07/25/17 12:21 1Carbon tetrachloride
<0.000180 0.0001800.00100 mg/L 07/25/17 12:21 1Chlorobenzene
<0.000250 0.0002500.00100 mg/L 07/25/17 12:21 1Tetrachloroethene
<0.000200 0.0002000.00100 mg/L 07/25/17 12:21 1Trichloroethene
<0.000240 0.0002400.00100 mg/L 07/25/17 12:21 1Vinyl chloride
<0.000230 0.0002300.00100 mg/L 07/25/17 12:21 1Chloroform
1,2-Dichloroethane-d4 (Surr)88 70-130 07/25/17 12:21 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 07/25/17 12:21 14-Bromofluorobenzene (Surr)70-130
99 07/25/17 12:21 1Dibromofluoromethane (Surr)70-130
101 07/25/17 12:21 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-447438/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447438
1,1-Dichloroethene 0.0200 0.01761 mg/L 88 70-132
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane 0.0200 0.01678 mg/L 84 70-130
2-Butanone (MEK)0.100 0.09691 mg/L 97 55-143
Benzene 0.0200 0.01782 mg/L 89 70-130
Carbon tetrachloride 0.0200 0.01533 mg/L 77 70-147
Chlorobenzene 0.0200 0.01780 mg/L 89 70-130
Tetrachloroethene 0.0200 0.01665 mg/L 83 70-130
Trichloroethene 0.0200 0.01758 mg/L 88 70-130
Vinyl chloride 0.0200 0.01943 mg/L 97 57-137
Chloroform 0.0200 0.01694 mg/L 85 70-130
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
994-Bromofluorobenzene (Surr)70 -130
96Dibromofluoromethane (Surr)70 -130
106Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-447438/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447438
1,1-Dichloroethene 0.0200 0.02147 mg/L 107 70-132 20 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,2-Dichloroethane 0.0200 0.02085 *mg/L 104 70-130 22 13
2-Butanone (MEK)0.100 0.1215 *mg/L 122 55-143 23 19
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-447438/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447438
Benzene 0.0200 0.02287 *mg/L 114 70-130 25 12
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Carbon tetrachloride 0.0200 0.01943 *mg/L 97 70-147 24 16
Chlorobenzene 0.0200 0.02162 *mg/L 108 70-130 19 12
Tetrachloroethene 0.0200 0.02033 *mg/L 102 70-130 20 17
Trichloroethene 0.0200 0.02133 *mg/L 107 70-130 19 14
Vinyl chloride 0.0200 0.02426 *mg/L 121 57-137 22 15
Chloroform 0.0200 0.02057 *mg/L 103 70-130 19 14
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
96
LCSD LCSD
Qualifier Limits%Recovery
984-Bromofluorobenzene (Surr)70 -130
98Dibromofluoromethane (Surr)70 -130
98Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: LB 490-446966/1-A
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447438
RL MDL
1,1-Dichloroethene <0.000250 0.00100 0.000250 mg/L 07/25/17 12:51 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000200 0.0002000.00100 mg/L 07/25/17 12:51 11,2-Dichloroethane
<0.00260 0.002600.0500 mg/L 07/25/17 12:51 12-Butanone (MEK)
<0.000200 0.0002000.00100 mg/L 07/25/17 12:51 1Benzene
<0.000180 0.0001800.00100 mg/L 07/25/17 12:51 1Carbon tetrachloride
<0.000180 0.0001800.00100 mg/L 07/25/17 12:51 1Chlorobenzene
<0.000250 0.0002500.00100 mg/L 07/25/17 12:51 1Tetrachloroethene
<0.000200 0.0002000.00100 mg/L 07/25/17 12:51 1Trichloroethene
<0.000240 0.0002400.00100 mg/L 07/25/17 12:51 1Vinyl chloride
0.006855 0.0002300.00100 mg/L 07/25/17 12:51 1Chloroform
1,2-Dichloroethane-d4 (Surr)87 70-130 07/25/17 12:51 1
LB LB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 07/25/17 12:51 14-Bromofluorobenzene (Surr)70-130
96 07/25/17 12:51 1Dibromofluoromethane (Surr)70-130
98 07/25/17 12:51 1Toluene-d8 (Surr)70-130
Client Sample ID: Matrix SpikeLab Sample ID: 490-133228-A-1-C MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447438
1,1-Dichloroethene <0.00250 0.500 0.4662 mg/L 93 54-150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dichloroethane <0.00200 0.500 0.4328 mg/L 87 64-136
2-Butanone (MEK)<0.0260 2.50 2.334 mg/L 93 50-143
Benzene <0.00200 0.500 0.4794 mg/L 96 55-147
Carbon tetrachloride <0.00180 0.500 0.4184 mg/L 84 56-150
Chlorobenzene <0.00180 0.500 0.4615 mg/L 92 70-130
Tetrachloroethene <0.00250 0.500 0.4412 mg/L 88 57-138
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-133228-A-1-C MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447438
Trichloroethene <0.00200 0.500 0.4582 mg/L 92 63-135
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Vinyl chloride <0.00240 0.500 0.5175 mg/L 104 57-150
Chloroform <0.00230 0.500 0.4648 mg/L 93 66-138
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
89
MS MS
Qualifier Limits%Recovery
974-Bromofluorobenzene (Surr)70 -130
100Dibromofluoromethane (Surr)70 -130
99Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-133228-A-1-C MSD
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447438
1,1-Dichloroethene <0.00250 0.500 0.4567 mg/L 91 54-150 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2-Dichloroethane <0.00200 0.500 0.4290 mg/L 86 64-136 1 17
2-Butanone (MEK)<0.0260 2.50 2.401 mg/L 96 50-143 3 19
Benzene <0.00200 0.500 0.4646 mg/L 93 55-147 3 50
Carbon tetrachloride <0.00180 0.500 0.4066 mg/L 81 56-150 3 19
Chlorobenzene <0.00180 0.500 0.4569 mg/L 91 70-130 1 14
Tetrachloroethene <0.00250 0.500 0.4340 mg/L 87 57-138 2 17
Trichloroethene <0.00200 0.500 0.4523 mg/L 90 63-135 1 17
Vinyl chloride <0.00240 0.500 0.5037 mg/L 101 57-150 3 17
Chloroform <0.00230 0.500 0.4588 mg/L 92 66-138 1 18
1,2-Dichloroethane-d4 (Surr)70 -130
Surrogate
89
MSD MSD
Qualifier Limits%Recovery
1004-Bromofluorobenzene (Surr)70 -130
100Dibromofluoromethane (Surr)70 -130
98Toluene-d8 (Surr)70 -130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-447040/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447145 Prep Batch: 447040
1,4-Dichlorobenzene 0.200 0.1403 mg/L 70 24-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
2,4,5-Trichlorophenol 0.200 0.1842 mg/L 92 10-150
2,4,6-Trichlorophenol 0.200 0.1851 mg/L 93 10-150
2,4-Dinitrotoluene 0.200 0.1841 mg/L 92 36-138
Cresols 0.400 0.3001 mg/L 75 10-132
Hexachlorobenzene 0.200 0.1890 mg/L 94 36-140
Hexachlorobutadiene 0.200 0.1663 mg/L 83 18-136
Hexachloroethane 0.200 0.1337 mg/L 67 23-120
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-447040/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447145 Prep Batch: 447040
Nitrobenzene 0.200 0.1433 mg/L 72 10-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Pyridine 0.200 0.09009 mg/L 45 10-110
Pentachlorophenol 0.400 0.3399 mg/L 85 10-150
2,4,6-Tribromophenol (Surr)10 -120
Surrogate
91
LCS LCS
Qualifier Limits%Recovery
832-Fluorobiphenyl (Surr)29 -120
732-Fluorophenol (Surr)10 -120
82Nitrobenzene-d5 (Surr)27 -120
69Phenol-d5 (Surr)10 -120
95Terphenyl-d14 (Surr)13 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-447040/6-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447145 Prep Batch: 447040
1,4-Dichlorobenzene 0.200 0.1378 mg/L 69 24-120 2 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2,4,5-Trichlorophenol 0.200 0.1730 mg/L 87 10-150 6 50
2,4,6-Trichlorophenol 0.200 0.1776 mg/L 89 10-150 4 50
2,4-Dinitrotoluene 0.200 0.1796 mg/L 90 36-138 2 50
Cresols 0.400 0.2965 mg/L 74 10-132 1 50
Hexachlorobenzene 0.200 0.1803 mg/L 90 36-140 5 50
Hexachlorobutadiene 0.200 0.1590 mg/L 80 18-136 4 50
Hexachloroethane 0.200 0.1307 mg/L 65 23-120 2 50
Nitrobenzene 0.200 0.1364 mg/L 68 10-150 5 50
Pyridine 0.200 0.09052 mg/L 45 10-110 0 50
Pentachlorophenol 0.400 0.3296 mg/L 82 10-150 3 50
2,4,6-Tribromophenol (Surr)10 -120
Surrogate
90
LCSD LCSD
Qualifier Limits%Recovery
792-Fluorobiphenyl (Surr)29 -120
722-Fluorophenol (Surr)10 -120
78Nitrobenzene-d5 (Surr)27 -120
68Phenol-d5 (Surr)10 -120
91Terphenyl-d14 (Surr)13 -120
Client Sample ID: Method BlankLab Sample ID: LB 490-446989/1-B
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447145 Prep Batch: 447040
RL MDL
1,4-Dichlorobenzene <0.00620 0.0200 0.00620 mg/L 07/23/17 16:21 07/24/17 14:45 2
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00380 0.003800.0600 mg/L 07/23/17 16:21 07/24/17 14:45 22,4,5-Trichlorophenol
<0.00320 0.003200.0200 mg/L 07/23/17 16:21 07/24/17 14:45 22,4,6-Trichlorophenol
<0.00380 0.003800.0200 mg/L 07/23/17 16:21 07/24/17 14:45 22,4-Dinitrotoluene
<0.0280 0.02800.0400 mg/L 07/23/17 16:21 07/24/17 14:45 2Cresols
<0.00360 0.003600.0200 mg/L 07/23/17 16:21 07/24/17 14:45 2Hexachlorobenzene
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 490-446989/1-B
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447145 Prep Batch: 447040
RL MDL
Hexachlorobutadiene <0.00600 0.0200 0.00600 mg/L 07/23/17 16:21 07/24/17 14:45 2
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00640 0.006400.0200 mg/L 07/23/17 16:21 07/24/17 14:45 2Hexachloroethane
<0.00380 0.003800.0200 mg/L 07/23/17 16:21 07/24/17 14:45 2Nitrobenzene
<0.00360 0.003600.0200 mg/L 07/23/17 16:21 07/24/17 14:45 2Pyridine
<0.00700 0.007000.0600 mg/L 07/23/17 16:21 07/24/17 14:45 2Pentachlorophenol
2,4,6-Tribromophenol (Surr)81 10-120 07/24/17 14:45 2
LB LB
Surrogate
07/23/17 16:21
Dil FacPreparedAnalyzedQualifierLimits%Recovery
76 07/23/17 16:21 07/24/17 14:45 22-Fluorobiphenyl (Surr)29-120
64 07/23/17 16:21 07/24/17 14:45 22-Fluorophenol (Surr)10-120
77 07/23/17 16:21 07/24/17 14:45 2Nitrobenzene-d5 (Surr)27-120
58 07/23/17 16:21 07/24/17 14:45 2Phenol-d5 (Surr)10-120
87 07/23/17 16:21 07/24/17 14:45 2Terphenyl-d14 (Surr)13-120
Client Sample ID: Method BlankLab Sample ID: MB 490-446989/9-B
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447145 Prep Batch: 447040
RL MDL
1,4-Dichlorobenzene <0.00620 0.0200 0.00620 mg/L 07/23/17 16:21 07/24/17 15:04 2
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00380 0.003800.0600 mg/L 07/23/17 16:21 07/24/17 15:04 22,4,5-Trichlorophenol
<0.00320 0.003200.0200 mg/L 07/23/17 16:21 07/24/17 15:04 22,4,6-Trichlorophenol
<0.00380 0.003800.0200 mg/L 07/23/17 16:21 07/24/17 15:04 22,4-Dinitrotoluene
<0.0280 0.02800.0400 mg/L 07/23/17 16:21 07/24/17 15:04 2Cresols
<0.00360 0.003600.0200 mg/L 07/23/17 16:21 07/24/17 15:04 2Hexachlorobenzene
<0.00600 0.006000.0200 mg/L 07/23/17 16:21 07/24/17 15:04 2Hexachlorobutadiene
<0.00640 0.006400.0200 mg/L 07/23/17 16:21 07/24/17 15:04 2Hexachloroethane
<0.00380 0.003800.0200 mg/L 07/23/17 16:21 07/24/17 15:04 2Nitrobenzene
<0.00360 0.003600.0200 mg/L 07/23/17 16:21 07/24/17 15:04 2Pyridine
<0.00700 0.007000.0600 mg/L 07/23/17 16:21 07/24/17 15:04 2Pentachlorophenol
2,4,6-Tribromophenol (Surr)77 10-120 07/24/17 15:04 2
MB MB
Surrogate
07/23/17 16:21
Dil FacPreparedAnalyzedQualifierLimits%Recovery
73 07/23/17 16:21 07/24/17 15:04 22-Fluorobiphenyl (Surr)29-120
56 07/23/17 16:21 07/24/17 15:04 22-Fluorophenol (Surr)10-120
74 07/23/17 16:21 07/24/17 15:04 2Nitrobenzene-d5 (Surr)27-120
54 07/23/17 16:21 07/24/17 15:04 2Phenol-d5 (Surr)10-120
96 07/23/17 16:21 07/24/17 15:04 2Terphenyl-d14 (Surr)13-120
Method: 8081B - Organochlorine Pesticides (GC)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-447043/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447169 Prep Batch: 447043
gamma-BHC (Lindane)0.0100 0.009857 mg/L 99 32-135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-447043/5-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447169 Prep Batch: 447043
Endrin 0.0100 0.01029 mg/L 103 32-142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Heptachlor 0.0100 0.009444 mg/L 94 30-148
Heptachlor epoxide 0.0100 0.01043 mg/L 104 36-133
Methoxychlor 0.0100 0.008958 mg/L 90 10-150
Tetrachloro-m-xylene 27 -129
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
87DCB Decachlorobiphenyl (Surr)24 -132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-447043/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447169 Prep Batch: 447043
Chlordane (technical)0.0500 0.04850 mg/L 97 30-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Toxaphene 0.100 0.07445 mg/L 74 32-130
Tetrachloro-m-xylene 27 -129
Surrogate
81
LCS LCS
Qualifier Limits%Recovery
100DCB Decachlorobiphenyl (Surr)24 -132
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-447043/6-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447169 Prep Batch: 447043
gamma-BHC (Lindane)0.0100 0.009101 mg/L 91 32-135 8 35
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Endrin 0.0100 0.009525 mg/L 95 32-142 8 35
Heptachlor 0.0100 0.008748 mg/L 87 30-148 8 35
Heptachlor epoxide 0.0100 0.009630 mg/L 96 36-133 8 35
Methoxychlor 0.0100 0.009809 mg/L 98 10-150 9 35
Tetrachloro-m-xylene 27 -129
Surrogate
89
LCSD LCSD
Qualifier Limits%Recovery
76DCB Decachlorobiphenyl (Surr)24 -132
Client Sample ID: Method BlankLab Sample ID: LB 490-446989/1-C
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447169 Prep Batch: 447043
RL MDL
gamma-BHC (Lindane)<0.000100 0.00100 0.000100 mg/L 07/23/17 21:49 07/24/17 15:59 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000700 0.0007000.00100 mg/L 07/23/17 21:49 07/24/17 15:59 1Chlordane (technical)
<0.000100 0.0001000.00100 mg/L 07/23/17 21:49 07/24/17 15:59 1Endrin
<0.000100 0.0001000.00100 mg/L 07/23/17 21:49 07/24/17 15:59 1Heptachlor
<0.000700 0.0007000.00100 mg/L 07/23/17 21:49 07/24/17 15:59 1Heptachlor epoxide
<0.000100 0.0001000.00100 mg/L 07/23/17 21:49 07/24/17 15:59 1Methoxychlor
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 490-446989/1-C
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447169 Prep Batch: 447043
RL MDL
Toxaphene <0.0350 0.0500 0.0350 mg/L 07/23/17 21:49 07/24/17 15:59 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Tetrachloro-m-xylene 62 27-129 07/24/17 15:59 1
LB LB
Surrogate
07/23/17 21:49
Dil FacPreparedAnalyzedQualifierLimits%Recovery
82 07/23/17 21:49 07/24/17 15:59 1DCB Decachlorobiphenyl (Surr)24-132
Client Sample ID: Method BlankLab Sample ID: MB 490-446989/9-C
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447169 Prep Batch: 447043
RL MDL
gamma-BHC (Lindane)<0.000100 0.00100 0.000100 mg/L 07/23/17 21:49 07/24/17 16:12 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.000700 0.0007000.00100 mg/L 07/23/17 21:49 07/24/17 16:12 1Chlordane (technical)
<0.000100 0.0001000.00100 mg/L 07/23/17 21:49 07/24/17 16:12 1Endrin
<0.000100 0.0001000.00100 mg/L 07/23/17 21:49 07/24/17 16:12 1Heptachlor
<0.000700 0.0007000.00100 mg/L 07/23/17 21:49 07/24/17 16:12 1Heptachlor epoxide
<0.000100 0.0001000.00100 mg/L 07/23/17 21:49 07/24/17 16:12 1Methoxychlor
<0.0350 0.03500.0500 mg/L 07/23/17 21:49 07/24/17 16:12 1Toxaphene
Tetrachloro-m-xylene 87 27-129 07/24/17 16:12 1
MB MB
Surrogate
07/23/17 21:49
Dil FacPreparedAnalyzedQualifierLimits%Recovery
76 07/23/17 21:49 07/24/17 16:12 1DCB Decachlorobiphenyl (Surr)24-132
Method: 8151A - Herbicides (GC)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-447044/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447172 Prep Batch: 447044
Silvex (2,4,5-TP)0.0500 0.02985 mg/L 60 10-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
2,4-D 0.0500 0.03475 mg/L 69 10-150
Dichloroacetic acid(Surr)10 -150
Surrogate
67
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-447044/4-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447172 Prep Batch: 447044
Silvex (2,4,5-TP)0.0500 0.03396 mg/L 68 10-150 13 35
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2,4-D 0.0500 0.03924 mg/L 78 10-150 12 35
Dichloroacetic acid(Surr)10 -150
Surrogate
61
LCSD LCSD
Qualifier Limits%Recovery
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8151A - Herbicides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 490-446989/1-D
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447172 Prep Batch: 447044
RL MDL
Silvex (2,4,5-TP)<0.0100 0.0200 0.0100 mg/L 07/23/17 23:05 07/24/17 12:56 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.0100 0.01000.0200 mg/L 07/23/17 23:05 07/24/17 12:56 12,4-D
Dichloroacetic acid(Surr)32 10-150 07/24/17 12:56 1
LB LB
Surrogate
07/23/17 23:05
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-447195/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447581 Prep Batch: 447195
RL MDL
Silver <0.00300 0.0500 0.00300 mg/L 07/24/17 11:00 07/25/17 11:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00860 0.008600.0500 mg/L 07/24/17 11:00 07/25/17 11:24 1Arsenic
<0.00500 0.005001.00 mg/L 07/24/17 11:00 07/25/17 11:24 1Barium
<0.000500 0.0005000.0100 mg/L 07/24/17 11:00 07/25/17 11:24 1Cadmium
<0.00300 0.003000.0500 mg/L 07/24/17 11:00 07/25/17 11:24 1Chromium
<0.00200 0.002000.0500 mg/L 07/24/17 11:00 07/25/17 11:24 1Lead
<0.00500 0.005000.0100 mg/L 07/24/17 11:00 07/25/17 11:24 1Selenium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-447195/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447581 Prep Batch: 447195
Silver 0.200 0.1922 mg/L 96 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 0.200 0.2078 mg/L 104 80-120
Barium 2.00 1.986 mg/L 99 80-120
Cadmium 0.200 0.1991 mg/L 100 80-120
Chromium 1.00 0.9813 mg/L 98 80-120
Lead 1.00 1.008 mg/L 101 80-120
Selenium 0.200 0.1988 mg/L 99 80-120
Client Sample ID: Method BlankLab Sample ID: LB 490-446989/1-E
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447581 Prep Batch: 447195
RL MDL
Silver <0.0300 0.500 0.0300 mg/L 07/24/17 11:00 07/25/17 11:34 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.0860 0.08600.500 mg/L 07/24/17 11:00 07/25/17 11:34 1Arsenic
<0.0500 0.050010.0 mg/L 07/24/17 11:00 07/25/17 11:34 1Barium
<0.00500 0.005000.100 mg/L 07/24/17 11:00 07/25/17 11:34 1Cadmium
<0.0300 0.03000.500 mg/L 07/24/17 11:00 07/25/17 11:34 1Chromium
<0.0200 0.02000.500 mg/L 07/24/17 11:00 07/25/17 11:34 1Lead
<0.0500 0.05000.100 mg/L 07/24/17 11:00 07/25/17 11:34 1Selenium
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-133141-C-2-E MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447581 Prep Batch: 447195
Silver <0.0300 2.00 1.906 mg/L 95 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic <0.0860 2.00 2.125 mg/L 106 75-125
Barium 1.19 J 20.0 20.46 mg/L 96 75-125
Cadmium <0.00500 2.00 1.991 mg/L 100 75-125
Chromium <0.0300 10.0 9.650 mg/L 97 75-125
Lead 0.0570 J 10.0 9.588 mg/L 95 75-125
Selenium <0.0500 2.00 2.130 mg/L 107 75-125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-133141-C-2-F MSD
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447581 Prep Batch: 447195
Silver <0.0300 2.00 1.884 mg/L 94 75-125 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic <0.0860 2.00 2.129 mg/L 106 75-125 0 20
Barium 1.19 J 20.0 20.32 mg/L 96 75-125 1 20
Cadmium <0.00500 2.00 1.967 mg/L 98 75-125 1 20
Chromium <0.0300 10.0 9.531 mg/L 95 75-125 1 20
Lead 0.0570 J 10.0 9.375 mg/L 93 75-125 2 20
Selenium <0.0500 2.00 2.055 mg/L 103 75-125 4 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-447221/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447330 Prep Batch: 447221
RL MDL
Mercury <0.000100 0.000200 0.000100 mg/L 07/24/17 12:05 07/24/17 15:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-447221/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 447330 Prep Batch: 447221
Mercury 0.00200 0.002001 mg/L 100 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: LB 490-446989/1-F
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447330 Prep Batch: 447221
RL MDL
Mercury <0.00100 0.00200 0.00100 mg/L 07/24/17 12:05 07/24/17 15:16 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-133141-C-2-H MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447330 Prep Batch: 447221
Mercury <0.00100 0.0200 0.02011 mg/L 101 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-133141-C-2-I MSD
Matrix: Solid Prep Type: TCLP
Analysis Batch: 447330 Prep Batch: 447221
Mercury <0.00100 0.0200 0.01837 mg/L 92 75-125 9 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
GC/MS VOA
Leach Batch: 446966
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 1311490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 1311LB 490-446966/1-A Method Blank TCLP
Solid 1311490-133228-A-1-C MS Matrix Spike TCLP
Solid 1311490-133228-A-1-C MSD Matrix Spike Duplicate TCLP
Analysis Batch: 447438
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 446966490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 8260B 446966490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 8260B 446966LB 490-446966/1-A Method Blank TCLP
Solid 8260BMB 490-447438/6 Method Blank Total/NA
Solid 8260BLCS 490-447438/3 Lab Control Sample Total/NA
Solid 8260BLCSD 490-447438/4 Lab Control Sample Dup Total/NA
Solid 8260B 446966490-133228-A-1-C MS Matrix Spike TCLP
Solid 8260B 446966490-133228-A-1-C MSD Matrix Spike Duplicate TCLP
GC/MS Semi VOA
Leach Batch: 446989
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 1311490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 1311LB 490-446989/1-B Method Blank TCLP
Solid 1311MB 490-446989/9-B Method Blank TCLP
Prep Batch: 447040
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3510C 446989490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 3510C 446989490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 3510C 446989LB 490-446989/1-B Method Blank TCLP
Solid 3510C 446989MB 490-446989/9-B Method Blank TCLP
Solid 3510CLCS 490-447040/5-A Lab Control Sample Total/NA
Solid 3510CLCSD 490-447040/6-A Lab Control Sample Dup Total/NA
Analysis Batch: 447145
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 447040LB 490-446989/1-B Method Blank TCLP
Solid 8270D 447040MB 490-446989/9-B Method Blank TCLP
Solid 8270D 447040LCS 490-447040/5-A Lab Control Sample Total/NA
Solid 8270D 447040LCSD 490-447040/6-A Lab Control Sample Dup Total/NA
Analysis Batch: 447299
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 447040490-133167-1 SURFACE-TCLP-170719 TCLP
Analysis Batch: 447464
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 447040490-133167-2 EXCAVATION-TCLP-170719 TCLP
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QC Association Summary
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
GC Semi VOA
Leach Batch: 446989
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 1311490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 1311LB 490-446989/1-C Method Blank TCLP
Solid 1311LB 490-446989/1-D Method Blank TCLP
Solid 1311MB 490-446989/9-C Method Blank TCLP
Prep Batch: 447043
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3510C 446989490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 3510C 446989490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 3510C 446989LB 490-446989/1-C Method Blank TCLP
Solid 3510C 446989MB 490-446989/9-C Method Blank TCLP
Solid 3510CLCS 490-447043/5-A Lab Control Sample Total/NA
Solid 3510CLCS 490-447043/7-A Lab Control Sample Total/NA
Solid 3510CLCSD 490-447043/6-A Lab Control Sample Dup Total/NA
Prep Batch: 447044
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8151A 446989490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 8151A 446989490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 8151A 446989LB 490-446989/1-D Method Blank TCLP
Solid 8151ALCS 490-447044/3-A Lab Control Sample Total/NA
Solid 8151ALCSD 490-447044/4-A Lab Control Sample Dup Total/NA
Analysis Batch: 447169
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8081B 447043490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 8081B 447043LB 490-446989/1-C Method Blank TCLP
Solid 8081B 447043MB 490-446989/9-C Method Blank TCLP
Solid 8081B 447043LCS 490-447043/5-A Lab Control Sample Total/NA
Solid 8081B 447043LCS 490-447043/7-A Lab Control Sample Total/NA
Solid 8081B 447043LCSD 490-447043/6-A Lab Control Sample Dup Total/NA
Analysis Batch: 447172
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8151A 447044490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 8151A 447044490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 8151A 447044LB 490-446989/1-D Method Blank TCLP
Solid 8151A 447044LCS 490-447044/3-A Lab Control Sample Total/NA
Solid 8151A 447044LCSD 490-447044/4-A Lab Control Sample Dup Total/NA
Analysis Batch: 447486
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8081B 447043490-133167-2 EXCAVATION-TCLP-170719 TCLP
Metals
Leach Batch: 446989
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311490-133167-1 SURFACE-TCLP-170719 TCLP
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QC Association Summary
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Metals (Continued)
Leach Batch: 446989 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 1311LB 490-446989/1-E Method Blank TCLP
Solid 1311LB 490-446989/1-F Method Blank TCLP
Solid 1311490-133141-C-2-E MS Matrix Spike TCLP
Solid 1311490-133141-C-2-F MSD Matrix Spike Duplicate TCLP
Solid 1311490-133141-C-2-H MS Matrix Spike TCLP
Solid 1311490-133141-C-2-I MSD Matrix Spike Duplicate TCLP
Prep Batch: 447195
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3010A 446989490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 3010A 446989490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 3010A 446989LB 490-446989/1-E Method Blank TCLP
Solid 3010AMB 490-447195/1-A Method Blank Total/NA
Solid 3010ALCS 490-447195/2-A Lab Control Sample Total/NA
Solid 3010A 446989490-133141-C-2-E MS Matrix Spike TCLP
Solid 3010A 446989490-133141-C-2-F MSD Matrix Spike Duplicate TCLP
Prep Batch: 447221
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 446989490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 7470A 446989490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 7470A 446989LB 490-446989/1-F Method Blank TCLP
Solid 7470AMB 490-447221/1-A Method Blank Total/NA
Solid 7470ALCS 490-447221/2-A Lab Control Sample Total/NA
Solid 7470A 446989490-133141-C-2-H MS Matrix Spike TCLP
Solid 7470A 446989490-133141-C-2-I MSD Matrix Spike Duplicate TCLP
Analysis Batch: 447330
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 447221490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 7470A 447221490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 7470A 447221LB 490-446989/1-F Method Blank TCLP
Solid 7470A 447221MB 490-447221/1-A Method Blank Total/NA
Solid 7470A 447221LCS 490-447221/2-A Lab Control Sample Total/NA
Solid 7470A 447221490-133141-C-2-H MS Matrix Spike TCLP
Solid 7470A 447221490-133141-C-2-I MSD Matrix Spike Duplicate TCLP
Analysis Batch: 447581
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010D 447195490-133167-1 SURFACE-TCLP-170719 TCLP
Solid 6010D 447195490-133167-2 EXCAVATION-TCLP-170719 TCLP
Solid 6010D 447195LB 490-446989/1-E Method Blank TCLP
Solid 6010D 447195MB 490-447195/1-A Method Blank Total/NA
Solid 6010D 447195LCS 490-447195/2-A Lab Control Sample Total/NA
Solid 6010D 447195490-133141-C-2-E MS Matrix Spike TCLP
Solid 6010D 447195490-133141-C-2-F MSD Matrix Spike Duplicate TCLP
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Lab Chronicle
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-133167-1
Project/Site: Eagle Island
Client Sample ID: SURFACE-TCLP-170719 Lab Sample ID: 490-133167-1
Matrix: SolidDate Collected: 07/19/17 10:45
Date Received: 07/20/17 09:05
Leach 1311 SCR07/22/17 15:14 TAL NSH446966
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
TCLP 1.0 g 1.0 mL
Analysis 8260B 10 447438 07/25/17 14:49 P1B TAL NSHTCLP10 mL 10 mL
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 3510C 447040 07/24/17 13:14 DHC TAL NSHTCLP500 mL 1.0 mL
Analysis 8270D 2 447299 07/24/17 21:16 T1C TAL NSHTCLP
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 3510C 447043 07/24/17 13:39 DHC TAL NSHTCLP100 mL 10 mL
Analysis 8081B 1 447169 07/24/17 18:31 JML TAL NSHTCLP
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 8151A 447044 07/23/17 23:05 DHC TAL NSHTCLP10 mL 10 mL
Analysis 8151A 1 447172 07/24/17 13:57 JML TAL NSHTCLP
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 3010A 447195 07/24/17 11:00 BVH TAL NSHTCLP5 mL 50 mL
Analysis 6010D 1 447581 07/25/17 12:27 LCS TAL NSHTCLP
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 7470A 447221 07/24/17 12:05 RDF TAL NSHTCLP3 mL 30 mL
Analysis 7470A 1 447330 07/24/17 15:27 RDF TAL NSHTCLP
Client Sample ID: EXCAVATION-TCLP-170719 Lab Sample ID: 490-133167-2
Matrix: SolidDate Collected: 07/19/17 11:20
Date Received: 07/20/17 09:05
Leach 1311 SCR07/22/17 15:14 TAL NSH446966
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
TCLP 1.0 g 1.0 mL
Analysis 8260B 10 447438 07/25/17 14:19 P1B TAL NSHTCLP10 mL 10 mL
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 3510C 447040 07/24/17 17:24 DHC TAL NSHTCLP500 mL 1.0 mL
Analysis 8270D 2 447464 07/25/17 19:37 RP TAL NSHTCLP
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 3510C 447043 07/24/17 17:25 DHC TAL NSHTCLP100 mL 10 mL
Analysis 8081B 1 447486 07/25/17 11:51 JML TAL NSHTCLP
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 8151A 447044 07/23/17 23:05 DHC TAL NSHTCLP10 mL 10 mL
Analysis 8151A 1 447172 07/24/17 14:12 JML TAL NSHTCLP
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 3010A 447195 07/24/17 11:00 BVH TAL NSHTCLP5 mL 50 mL
Analysis 6010D 1 447581 07/25/17 12:21 LCS TAL NSHTCLP
Leach 1311 446989 07/22/17 17:13 AJK TAL NSHTCLP1.0 g 1.0 mL
Prep 7470A 447221 07/24/17 12:05 RDF TAL NSHTCLP3 mL 30 mL
Analysis 7470A 1 447330 07/24/17 15:30 RDF TAL NSHTCLP
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-133167-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8468081BOrganochlorine Pesticides (GC)TAL NSH
SW8468151AHerbicides (GC)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Accreditation/Certification Summary
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-133167-1
Project/Site: Eagle Island
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3874State Program 12-31-17
Analysis Method Prep Method Matrix Analyte
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Geosyntec Consultants, Inc.Job Number: 490-133167-1
SDG Number:
Login Number: 133167
Question Answer Comment
Creator: Abernathy, Eric
List Source: TestAmerica Nashville
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
FalseSamples were received on ice.
FalseCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-134160-1
Client Project/Site: Eagle Island
For:
Geosyntec Consultants, Inc.
2501 Blue Ridge Rd.
Suite 430
Raleigh, North Carolina 27607
Attn: Ms. Kaitlyn S Rhonehouse
Authorized for release by:
8/15/2017 3:33:35 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
TestAmerica Job ID: 490-134160-1
Page 2 of 53 TestAmerica Nashville8/15/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .45
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .49
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53
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Sample Summary
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-134160-1 EI-EXC-E1 Solid 08/04/17 11:15 08/05/17 10:00
490-134160-2 SURF-EDGE-1 Solid 08/04/17 10:05 08/05/17 10:00
490-134160-3 SURF-EDGE-2 Solid 08/04/17 10:20 08/05/17 10:00
490-134160-4 SURF-EDGE-3 Solid 08/04/17 10:50 08/05/17 10:00
490-134160-5 SURF-BASE-1 Solid 08/04/17 11:30 08/05/17 10:00
490-134160-6 SURF-BASE-2 Solid 08/04/17 11:45 08/05/17 10:00
490-134160-7 SURF-BASE-3 Solid 08/04/17 12:05 08/05/17 10:00
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Case Narrative
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134160-1
Project/Site: Eagle Island
Job ID: 490-134160-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-134160-1
Comments
No additional comments.
Receipt
The samples were received on 8/5/2017 10:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 2.5º C.
GC/MS Semi VOA
Method 8270D: The continuing calibration verification (CCVIS) associated with batch 490-451551 recovered above the upper control limit
for 2,4-Dinitrophenol, 2,6-Dinitrotoluene and 2-Nitrophenol. The samples associated with this CCVIS were non-detect for the affected
analytes; therefore, the data has been reported. The following sample is impacted: (CCVIS 490-451551/3).
Method 8270D: The continuing calibration verification (CCVIS) analyzed in batch 490-451551 was outside the method criteria for
2,2'oxybis[1-chloropropane]. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is
considered estimated.
Method 8270D: The laboratory control sample (LCS) for preparation batch 490-450963 and analytical batch 490-451551 recovered outside
control limits for Hexachlorocyclopentadiene. This target analyte has been identified as poor performing when analyzed using this
method; therefore, re-extraction/re-analysis was not performed. These results have been reported and qualified.
Method 8270D: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 490-450963 and
analytical batch 490-451551 were outside control limits.
Method 8270D: The following samples were diluted due to the nature of the sample matrix: SURF-EDGE-1 (490-134160-2) and
SURF-BASE-2 (490-134160-6). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
Method MA-EPH: There was zero percent breakthroughs of the aromatic analytes Naphthalene and 2-Methylnaphthalene associated with
the following aliphatic laboratory control sample (LCS) and laboratory control sample duplicate (LCSD):
(LCS 490-450969/2-B) and (LCSD 490-450969/3-B)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 7471B: The following samples were diluted to bring the concentration of target analytes within the calibration range:
SURF-EDGE-1 (490-134160-2), (490-134160-B-2-B MS) and (490-134160-B-2-C MSD). Elevated reporting limits (RLs) are provided.
Method 7471B: Due to the high concentration of Mercury, the matrix spike / matrix spike duplicate (MS/MSD) for preparation batch
490-451077 and analytical batch 490-451811 could not be evaluated for accuracy and precision. The associated laboratory control
sample (LCS) met acceptance criteria.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Case Narrative
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134160-1
Project/Site: Eagle Island
Job ID: 490-134160-1 (Continued)
Laboratory: TestAmerica Nashville (Continued)
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Qualifiers
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
*LCS or LCSD is outside acceptance limits.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
B Compound was found in the blank and sample.
F1 MS and/or MSD Recovery is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-1Client Sample ID: EI-EXC-E1
Matrix: SolidDate Collected: 08/04/17 11:15
Percent Solids: 78.5Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0396 0.0830 0.0396 mg/Kg ☼08/08/17 10:12 08/10/17 12:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0830 0.0359 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Acenaphthylene <0.0359
0.0830 0.0359 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Anthracene <0.0359
0.0830 0.0372 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Benzo[a]anthracene <0.0372
0.0830 0.0334 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Benzo[a]pyrene 0.0683 J
0.0830 0.0347 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Benzo[b]fluoranthene 0.0478 J
0.0830 0.0409 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Benzo[g,h,i]perylene <0.0409
0.0830 0.0334 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Benzo[k]fluoranthene <0.0334
0.412 0.248 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Bis(2-chloroethoxy)methane <0.248
0.412 0.264 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Bis(2-chloroethyl)ether <0.264
0.412 0.245 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼bis (2-chloroisopropyl) ether <0.245
0.412 0.256 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Bis(2-ethylhexyl) phthalate <0.256
0.412 0.254 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼4-Bromophenyl phenyl ether <0.254
0.412 0.266 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Butyl benzyl phthalate <0.266
0.412 0.256 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Carbazole <0.256
0.412 0.281 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼4-Chloroaniline <0.281
0.412 0.208 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼4-Chloro-3-methylphenol <0.208
0.412 0.259 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2-Chloronaphthalene <0.259
0.412 0.237 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2-Chlorophenol <0.237
0.412 0.249 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼4-Chlorophenyl phenyl ether <0.249
0.0830 0.0458 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Chrysene <0.0458
0.825 0.140 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Cresols <0.140
0.0830 0.0396 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Dibenz(a,h)anthracene <0.0396
0.412 0.260 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Dibenzofuran <0.260
0.412 0.235 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼1,2-Dichlorobenzene <0.235
0.412 0.235 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼1,3-Dichlorobenzene <0.235
0.412 0.243 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼1,4-Dichlorobenzene <0.243
0.830 0.253 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼3,3'-Dichlorobenzidine <0.253
0.412 0.217 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2,4-Dichlorophenol <0.217
0.412 0.263 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Diethyl phthalate <0.263
0.830 0.415 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2,4-Dimethylphenol <0.415
0.412 0.256 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Dimethyl phthalate <0.256
0.412 0.261 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Di-n-butyl phthalate <0.261
0.412 0.284 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼4,6-Dinitro-2-methylphenol <0.284
0.412 0.311 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2,4-Dinitrophenol <0.311
0.412 0.258 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2,4-Dinitrotoluene <0.258
0.412 0.276 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2,6-Dinitrotoluene <0.276
0.412 0.220 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Di-n-octyl phthalate <0.220
0.0830 0.0421 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Fluoranthene 0.0449 J
0.0830 0.0359 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Fluorene <0.0359
0.412 0.310 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Hexachlorobenzene <0.310
0.412 0.207 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Hexachlorobutadiene <0.207
0.412 0.186 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Hexachlorocyclopentadiene <0.186 *
0.412 0.224 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Hexachloroethane <0.224
0.0830 0.0359 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Indeno[1,2,3-cd]pyrene <0.0359
0.412 0.233 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Isophorone <0.233
0.0830 0.0347 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼1-Methylnaphthalene <0.0347
0.0830 0.0322 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2-Methylnaphthalene <0.0322
0.412 0.268 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2-Methylphenol <0.268
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-1Client Sample ID: EI-EXC-E1
Matrix: SolidDate Collected: 08/04/17 11:15
Percent Solids: 78.5Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <0.251 0.412 0.251 mg/Kg ☼08/08/17 10:12 08/10/17 12:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0830 0.0359 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Naphthalene <0.0359
0.412 0.256 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2-Nitroaniline <0.256
0.830 0.285 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼3-Nitroaniline <0.285
0.830 0.295 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼4-Nitroaniline <0.295
0.412 0.249 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Nitrobenzene <0.249
0.412 0.301 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2-Nitrophenol <0.301
0.830 0.473 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼4-Nitrophenol <0.473
0.412 0.240 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼N-Nitrosodi-n-propylamine <0.240
0.412 0.0656 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0656
0.830 0.329 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Pentachlorophenol <0.329
0.0830 0.0421 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Phenanthrene <0.0421
0.412 0.251 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Phenol <0.251
0.0830 0.0421 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼Pyrene 0.0444 J
0.412 0.224 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼1,2,4-Trichlorobenzene <0.224
0.412 0.270 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2,4,5-Trichlorophenol <0.270
0.412 0.238 mg/Kg 08/08/17 10:12 08/10/17 12:23 1☼2,4,6-Trichlorophenol <0.238
2-Fluorobiphenyl (Surr)68 29-120 08/08/17 10:12 08/10/17 12:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)60 08/08/17 10:12 08/10/17 12:23 110-120
Nitrobenzene-d5 (Surr)64 08/08/17 10:12 08/10/17 12:23 127-120
Phenol-d5 (Surr)64 08/08/17 10:12 08/10/17 12:23 110-120
Terphenyl-d14 (Surr)84 08/08/17 10:12 08/10/17 12:23 113-120
2,4,6-Tribromophenol (Surr)87 08/08/17 10:12 08/10/17 12:23 110-120
Method: MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C9-C12 Aliphatics (North Carolina)6.68 6.37 3.18 mg/Kg ☼08/11/17 11:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics <3.74 7.20 3.74 mg/Kg ☼08/04/17 10:15 08/09/17 19:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.20 4.32 mg/Kg 08/04/17 10:15 08/09/17 19:40 1☼C9-C10 Aromatics <4.32
7.20 3.60 mg/Kg 08/04/17 10:15 08/09/17 19:40 1☼C9-C12 Aliphatics 6.68 J
2,5-Dibromotoluene (fid)91 70-130 08/04/17 10:15 08/09/17 19:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2,5-Dibromotoluene (pid)89 08/04/17 10:15 08/09/17 19:40 170-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C19-C36 Aliphatics <6.27 12.5 6.27 mg/Kg ☼08/08/17 10:20 08/10/17 22:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
12.5 3.01 mg/Kg 08/08/17 10:20 08/10/17 22:01 1☼C9-C18 Aliphatics <3.01
12.5 6.14 mg/Kg 08/08/17 10:20 08/10/17 21:53 1☼C11-C22 Aromatics 8.10 J
1-Chlorooctadecane 52 40-140 08/08/17 10:20 08/10/17 22:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o-Terphenyl 68 08/08/17 10:20 08/10/17 21:53 140-140
2-Fluorobiphenyl 71 08/08/17 10:20 08/10/17 21:53 140-140
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-1Client Sample ID: EI-EXC-E1
Matrix: SolidDate Collected: 08/04/17 11:15
Percent Solids: 78.5Date Received: 08/05/17 10:00
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
2-Bromonaphthalene 69 40-140 08/08/17 10:20 08/10/17 21:53 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL RL
Percent Moisture 21.5 0.1 0.1 %08/08/17 11:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 11:15 1Percent Solids 78.5
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-2Client Sample ID: SURF-EDGE-1
Matrix: SolidDate Collected: 08/04/17 10:05
Percent Solids: 76.5Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene 0.671 0.436 0.208 mg/Kg ☼08/08/17 10:12 08/10/17 14:38 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.436 0.189 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Acenaphthylene <0.189
0.436 0.189 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Anthracene 1.34
0.436 0.195 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Benzo[a]anthracene 4.87
0.436 0.176 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Benzo[a]pyrene 3.98
0.436 0.182 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Benzo[b]fluoranthene 5.32
0.436 0.215 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Benzo[g,h,i]perylene 2.47
0.436 0.176 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Benzo[k]fluoranthene 2.95
2.17 1.30 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Bis(2-chloroethoxy)methane <1.30
2.17 1.39 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Bis(2-chloroethyl)ether <1.39
2.17 1.29 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼bis (2-chloroisopropyl) ether <1.29
2.17 1.35 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Bis(2-ethylhexyl) phthalate <1.35
2.17 1.34 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼4-Bromophenyl phenyl ether <1.34
2.17 1.40 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Butyl benzyl phthalate <1.40
2.17 1.35 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Carbazole <1.35
2.17 1.48 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼4-Chloroaniline <1.48
2.17 1.09 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼4-Chloro-3-methylphenol <1.09
2.17 1.36 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2-Chloronaphthalene <1.36
2.17 1.24 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2-Chlorophenol <1.24
2.17 1.31 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼4-Chlorophenyl phenyl ether <1.31
0.436 0.241 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Chrysene 5.01
4.34 0.736 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Cresols <0.736
0.436 0.208 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Dibenz(a,h)anthracene 0.721
2.17 1.37 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Dibenzofuran <1.37
2.17 1.24 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼1,2-Dichlorobenzene <1.24
2.17 1.24 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼1,3-Dichlorobenzene <1.24
2.17 1.28 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼1,4-Dichlorobenzene <1.28
4.36 1.33 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼3,3'-Dichlorobenzidine <1.33
2.17 1.14 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2,4-Dichlorophenol <1.14
2.17 1.38 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Diethyl phthalate <1.38
4.36 2.18 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2,4-Dimethylphenol <2.18
2.17 1.35 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Dimethyl phthalate <1.35
2.17 1.37 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Di-n-butyl phthalate <1.37
2.17 1.49 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼4,6-Dinitro-2-methylphenol <1.49
2.17 1.63 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2,4-Dinitrophenol <1.63
2.17 1.35 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2,4-Dinitrotoluene <1.35
2.17 1.45 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2,6-Dinitrotoluene <1.45
2.17 1.16 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Di-n-octyl phthalate <1.16
0.436 0.221 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Fluoranthene 10.6
0.436 0.189 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Fluorene 0.494
2.17 1.63 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Hexachlorobenzene <1.63
2.17 1.09 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Hexachlorobutadiene <1.09
2.17 0.977 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Hexachlorocyclopentadiene <0.977 *
2.17 1.18 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Hexachloroethane <1.18
0.436 0.189 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Indeno[1,2,3-cd]pyrene 2.16
2.17 1.22 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Isophorone <1.22
0.436 0.182 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼1-Methylnaphthalene <0.182
0.436 0.169 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2-Methylnaphthalene <0.169
2.17 1.41 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2-Methylphenol <1.41
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-2Client Sample ID: SURF-EDGE-1
Matrix: SolidDate Collected: 08/04/17 10:05
Percent Solids: 76.5Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <1.32 2.17 1.32 mg/Kg ☼08/08/17 10:12 08/10/17 14:38 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.436 0.189 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Naphthalene <0.189
2.17 1.35 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2-Nitroaniline <1.35
4.36 1.50 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼3-Nitroaniline <1.50
4.36 1.55 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼4-Nitroaniline <1.55
2.17 1.31 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Nitrobenzene <1.31
2.17 1.58 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2-Nitrophenol <1.58
4.36 2.49 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼4-Nitrophenol <2.49
2.17 1.26 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼N-Nitrosodi-n-propylamine <1.26
2.17 0.345 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.345
4.36 1.73 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Pentachlorophenol <1.73
0.436 0.221 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Phenanthrene 7.01
2.17 1.32 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Phenol <1.32
0.436 0.221 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼Pyrene 8.83
2.17 1.18 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼1,2,4-Trichlorobenzene <1.18
2.17 1.42 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2,4,5-Trichlorophenol <1.42
2.17 1.25 mg/Kg 08/08/17 10:12 08/10/17 14:38 5☼2,4,6-Trichlorophenol <1.25
2-Fluorobiphenyl (Surr)86 29-120 08/08/17 10:12 08/10/17 14:38 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)70 08/08/17 10:12 08/10/17 14:38 510-120
Nitrobenzene-d5 (Surr)81 08/08/17 10:12 08/10/17 14:38 527-120
Phenol-d5 (Surr)75 08/08/17 10:12 08/10/17 14:38 510-120
Terphenyl-d14 (Surr)107 08/08/17 10:12 08/10/17 14:38 513-120
2,4,6-Tribromophenol (Surr)116 08/08/17 10:12 08/10/17 14:38 510-120
Method: 6010D - Metals (ICP)
RL MDL
Beryllium <0.261 1.30 0.261 mg/Kg ☼08/09/17 10:33 08/12/17 00:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.30 0.130 mg/Kg 08/09/17 10:33 08/12/17 00:32 1☼Cadmium 0.313 J
1.30 1.17 mg/Kg 08/09/17 10:33 08/12/17 00:32 1☼Chromium 9.60
2.61 1.43 mg/Kg 08/09/17 10:33 08/12/17 00:32 1☼Copper 335
1.30 0.652 mg/Kg 08/09/17 10:33 08/12/17 00:32 1☼Lead 142
3.91 1.30 mg/Kg 08/09/17 10:33 08/12/17 00:32 1☼Manganese 193
2.61 0.782 mg/Kg 08/09/17 10:33 08/12/17 00:32 1☼Nickel 3.23
2.61 1.43 mg/Kg 08/09/17 10:33 08/12/17 00:32 1☼Selenium <1.43
1.30 0.522 mg/Kg 08/09/17 10:33 08/12/17 00:32 1☼Silver <0.522
13.0 6.52 mg/Kg 08/09/17 10:33 08/12/17 00:32 1☼Zinc 228
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony 0.510 J 0.622 0.249 mg/Kg ☼08/09/17 20:35 08/11/17 17:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.622 0.249 mg/Kg 08/09/17 20:35 08/11/17 17:39 1☼Arsenic 5.66
0.622 0.249 mg/Kg 08/09/17 20:35 08/11/17 17:39 1☼Thallium <0.249
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 222 F2 129 38.6 mg/Kg ☼08/08/17 14:17 08/10/17 08:32 1000
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-2Client Sample ID: SURF-EDGE-1
Matrix: SolidDate Collected: 08/04/17 10:05
Percent Solids: 76.5Date Received: 08/05/17 10:00
General Chemistry
RL RL
Percent Moisture 23.5 0.1 0.1 %08/08/17 11:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 11:15 1Percent Solids 76.5
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-3Client Sample ID: SURF-EDGE-2
Matrix: SolidDate Collected: 08/04/17 10:20
Percent Solids: 83.2Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0374 0.0784 0.0374 mg/Kg ☼08/08/17 10:12 08/10/17 14:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Acenaphthylene <0.0339
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Anthracene <0.0339
0.0784 0.0351 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Benzo[a]anthracene 0.0554 J
0.0784 0.0316 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Benzo[a]pyrene 0.0915
0.0784 0.0328 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Benzo[b]fluoranthene 0.0877
0.0784 0.0386 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Benzo[g,h,i]perylene 0.0586 J
0.0784 0.0316 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Benzo[k]fluoranthene 0.0437 J
0.390 0.234 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Bis(2-chloroethoxy)methane <0.234
0.390 0.249 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Bis(2-chloroethyl)ether <0.249
0.390 0.232 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼bis (2-chloroisopropyl) ether <0.232
0.390 0.242 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Bis(2-ethylhexyl) phthalate <0.242
0.390 0.240 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼4-Bromophenyl phenyl ether <0.240
0.390 0.252 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Butyl benzyl phthalate <0.252
0.390 0.242 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Carbazole <0.242
0.390 0.266 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼4-Chloroaniline <0.266
0.390 0.197 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼4-Chloro-3-methylphenol <0.197
0.390 0.244 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2-Chloronaphthalene <0.244
0.390 0.223 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2-Chlorophenol <0.223
0.390 0.235 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼4-Chlorophenyl phenyl ether <0.235
0.0784 0.0433 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Chrysene 0.0538 J
0.779 0.132 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Cresols <0.132
0.0784 0.0374 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Dibenz(a,h)anthracene <0.0374
0.390 0.246 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Dibenzofuran <0.246
0.390 0.222 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼1,2-Dichlorobenzene <0.222
0.390 0.222 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼1,3-Dichlorobenzene <0.222
0.390 0.229 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼1,4-Dichlorobenzene <0.229
0.784 0.239 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼3,3'-Dichlorobenzidine <0.239
0.390 0.205 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2,4-Dichlorophenol <0.205
0.390 0.248 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Diethyl phthalate <0.248
0.784 0.392 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2,4-Dimethylphenol <0.392
0.390 0.242 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Dimethyl phthalate <0.242
0.390 0.247 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Di-n-butyl phthalate <0.247
0.390 0.268 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼4,6-Dinitro-2-methylphenol <0.268
0.390 0.294 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2,4-Dinitrophenol <0.294
0.390 0.243 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2,4-Dinitrotoluene <0.243
0.390 0.261 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2,6-Dinitrotoluene <0.261
0.390 0.208 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Di-n-octyl phthalate <0.208
0.0784 0.0398 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Fluoranthene 0.0798
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Fluorene <0.0339
0.390 0.292 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Hexachlorobenzene <0.292
0.390 0.195 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Hexachlorobutadiene <0.195
0.390 0.175 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Hexachlorocyclopentadiene <0.175 *
0.390 0.212 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Hexachloroethane <0.212
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Indeno[1,2,3-cd]pyrene 0.0522 J
0.390 0.220 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Isophorone <0.220
0.0784 0.0328 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼1-Methylnaphthalene <0.0328
0.0784 0.0304 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2-Methylnaphthalene <0.0304
0.390 0.253 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2-Methylphenol <0.253
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-3Client Sample ID: SURF-EDGE-2
Matrix: SolidDate Collected: 08/04/17 10:20
Percent Solids: 83.2Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <0.237 0.390 0.237 mg/Kg ☼08/08/17 10:12 08/10/17 14:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Naphthalene <0.0339
0.390 0.242 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2-Nitroaniline <0.242
0.784 0.269 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼3-Nitroaniline <0.269
0.784 0.278 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼4-Nitroaniline <0.278
0.390 0.235 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Nitrobenzene <0.235
0.390 0.284 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2-Nitrophenol <0.284
0.784 0.447 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼4-Nitrophenol <0.447
0.390 0.227 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼N-Nitrosodi-n-propylamine <0.227
0.390 0.0620 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0620
0.784 0.311 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Pentachlorophenol <0.311
0.0784 0.0398 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Phenanthrene <0.0398
0.390 0.237 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Phenol <0.237
0.0784 0.0398 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼Pyrene 0.0759 J
0.390 0.212 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼1,2,4-Trichlorobenzene <0.212
0.390 0.255 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2,4,5-Trichlorophenol <0.255
0.390 0.225 mg/Kg 08/08/17 10:12 08/10/17 14:58 1☼2,4,6-Trichlorophenol <0.225
2-Fluorobiphenyl (Surr)81 29-120 08/08/17 10:12 08/10/17 14:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)71 08/08/17 10:12 08/10/17 14:58 110-120
Nitrobenzene-d5 (Surr)77 08/08/17 10:12 08/10/17 14:58 127-120
Phenol-d5 (Surr)74 08/08/17 10:12 08/10/17 14:58 110-120
Terphenyl-d14 (Surr)99 08/08/17 10:12 08/10/17 14:58 113-120
2,4,6-Tribromophenol (Surr)102 08/08/17 10:12 08/10/17 14:58 110-120
Method: 6010D - Metals (ICP)
RL MDL
Beryllium 0.355 J 1.18 0.236 mg/Kg ☼08/09/17 10:33 08/12/17 00:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.18 0.118 mg/Kg 08/09/17 10:33 08/12/17 00:37 1☼Cadmium <0.118
1.18 1.06 mg/Kg 08/09/17 10:33 08/12/17 00:37 1☼Chromium 11.3
2.36 1.30 mg/Kg 08/09/17 10:33 08/12/17 00:37 1☼Copper 23.0
1.18 0.591 mg/Kg 08/09/17 10:33 08/12/17 00:37 1☼Lead 72.1
3.55 1.18 mg/Kg 08/09/17 10:33 08/12/17 00:37 1☼Manganese 185
2.36 0.709 mg/Kg 08/09/17 10:33 08/12/17 00:37 1☼Nickel 2.79
2.36 1.30 mg/Kg 08/09/17 10:33 08/12/17 00:37 1☼Selenium <1.30
1.18 0.473 mg/Kg 08/09/17 10:33 08/12/17 00:37 1☼Silver 0.615 J
11.8 5.91 mg/Kg 08/09/17 10:33 08/12/17 00:37 1☼Zinc 55.3
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony 0.557 J 0.572 0.229 mg/Kg ☼08/09/17 20:35 08/11/17 17:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.86 1.14 mg/Kg 08/09/17 20:35 08/11/17 07:40 5☼Arsenic 5.10
0.572 0.229 mg/Kg 08/09/17 20:35 08/11/17 17:45 1☼Thallium <0.229
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.351 0.119 0.0357 mg/Kg ☼08/08/17 14:17 08/10/17 08:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-3Client Sample ID: SURF-EDGE-2
Matrix: SolidDate Collected: 08/04/17 10:20
Percent Solids: 83.2Date Received: 08/05/17 10:00
General Chemistry
RL RL
Percent Moisture 16.8 0.1 0.1 %08/08/17 11:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 11:15 1Percent Solids 83.2
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-4Client Sample ID: SURF-EDGE-3
Matrix: SolidDate Collected: 08/04/17 10:50
Percent Solids: 85.1Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0374 0.0784 0.0374 mg/Kg ☼08/08/17 10:12 08/10/17 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Acenaphthylene <0.0339
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Anthracene <0.0339
0.0784 0.0351 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Benzo[a]anthracene <0.0351
0.0784 0.0316 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Benzo[a]pyrene 0.0543 J
0.0784 0.0327 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Benzo[b]fluoranthene 0.0348 J
0.0784 0.0386 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Benzo[g,h,i]perylene <0.0386
0.0784 0.0316 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Benzo[k]fluoranthene <0.0316
0.389 0.234 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Bis(2-chloroethoxy)methane <0.234
0.389 0.249 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Bis(2-chloroethyl)ether <0.249
0.389 0.232 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼bis (2-chloroisopropyl) ether <0.232
0.389 0.242 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Bis(2-ethylhexyl) phthalate <0.242
0.389 0.240 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼4-Bromophenyl phenyl ether <0.240
0.389 0.251 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Butyl benzyl phthalate <0.251
0.389 0.242 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Carbazole <0.242
0.389 0.265 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼4-Chloroaniline <0.265
0.389 0.196 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼4-Chloro-3-methylphenol <0.196
0.389 0.244 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2-Chloronaphthalene <0.244
0.389 0.223 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2-Chlorophenol <0.223
0.389 0.235 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼4-Chlorophenyl phenyl ether <0.235
0.0784 0.0433 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Chrysene <0.0433
0.779 0.132 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Cresols <0.132
0.0784 0.0374 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Dibenz(a,h)anthracene <0.0374
0.389 0.246 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Dibenzofuran <0.246
0.389 0.222 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼1,2-Dichlorobenzene <0.222
0.389 0.222 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼1,3-Dichlorobenzene <0.222
0.389 0.229 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼1,4-Dichlorobenzene <0.229
0.784 0.239 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼3,3'-Dichlorobenzidine <0.239
0.389 0.205 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2,4-Dichlorophenol <0.205
0.389 0.248 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Diethyl phthalate <0.248
0.784 0.392 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2,4-Dimethylphenol <0.392
0.389 0.242 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Dimethyl phthalate <0.242
0.389 0.247 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Di-n-butyl phthalate <0.247
0.389 0.268 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼4,6-Dinitro-2-methylphenol <0.268
0.389 0.294 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2,4-Dinitrophenol <0.294
0.389 0.243 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2,4-Dinitrotoluene <0.243
0.389 0.261 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2,6-Dinitrotoluene <0.261
0.389 0.208 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Di-n-octyl phthalate <0.208
0.0784 0.0398 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Fluoranthene <0.0398
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Fluorene <0.0339
0.389 0.292 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Hexachlorobenzene <0.292
0.389 0.195 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Hexachlorobutadiene <0.195
0.389 0.175 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Hexachlorocyclopentadiene <0.175 *
0.389 0.212 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Hexachloroethane <0.212
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Indeno[1,2,3-cd]pyrene <0.0339
0.389 0.220 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Isophorone <0.220
0.0784 0.0327 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼1-Methylnaphthalene <0.0327
0.0784 0.0304 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2-Methylnaphthalene <0.0304
0.389 0.253 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2-Methylphenol <0.253
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-4Client Sample ID: SURF-EDGE-3
Matrix: SolidDate Collected: 08/04/17 10:50
Percent Solids: 85.1Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <0.237 0.389 0.237 mg/Kg ☼08/08/17 10:12 08/10/17 15:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0784 0.0339 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Naphthalene <0.0339
0.389 0.242 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2-Nitroaniline <0.242
0.784 0.269 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼3-Nitroaniline <0.269
0.784 0.278 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼4-Nitroaniline <0.278
0.389 0.235 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Nitrobenzene <0.235
0.389 0.284 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2-Nitrophenol <0.284
0.784 0.447 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼4-Nitrophenol <0.447
0.389 0.227 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼N-Nitrosodi-n-propylamine <0.227
0.389 0.0620 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0620
0.784 0.311 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Pentachlorophenol <0.311
0.0784 0.0398 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Phenanthrene <0.0398
0.389 0.237 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Phenol <0.237
0.0784 0.0398 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼Pyrene <0.0398
0.389 0.212 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼1,2,4-Trichlorobenzene <0.212
0.389 0.255 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2,4,5-Trichlorophenol <0.255
0.389 0.225 mg/Kg 08/08/17 10:12 08/10/17 15:17 1☼2,4,6-Trichlorophenol <0.225
2-Fluorobiphenyl (Surr)78 29-120 08/08/17 10:12 08/10/17 15:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)67 08/08/17 10:12 08/10/17 15:17 110-120
Nitrobenzene-d5 (Surr)72 08/08/17 10:12 08/10/17 15:17 127-120
Phenol-d5 (Surr)70 08/08/17 10:12 08/10/17 15:17 110-120
Terphenyl-d14 (Surr)92 08/08/17 10:12 08/10/17 15:17 113-120
2,4,6-Tribromophenol (Surr)93 08/08/17 10:12 08/10/17 15:17 110-120
Method: 6010D - Metals (ICP)
RL MDL
Beryllium <0.230 1.15 0.230 mg/Kg ☼08/09/17 11:09 08/12/17 02:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.15 0.115 mg/Kg 08/09/17 11:09 08/12/17 02:10 1☼Cadmium <0.115
1.15 1.04 mg/Kg 08/09/17 11:09 08/12/17 02:10 1☼Chromium 3.45
2.30 1.27 mg/Kg 08/09/17 11:09 08/12/17 02:10 1☼Copper 34.2
1.15 0.575 mg/Kg 08/09/17 11:09 08/12/17 02:10 1☼Lead 76.5
3.45 1.15 mg/Kg 08/09/17 11:09 08/12/17 02:10 1☼Manganese 94.5
2.30 0.690 mg/Kg 08/09/17 11:09 08/12/17 02:10 1☼Nickel 1.50 J
2.30 1.27 mg/Kg 08/09/17 11:09 08/12/17 02:10 1☼Selenium <1.27
1.15 0.460 mg/Kg 08/09/17 11:09 08/12/17 02:10 1☼Silver <0.460
11.5 5.75 mg/Kg 08/09/17 11:09 08/12/17 02:10 1☼Zinc 58.7
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony 0.240 J 0.560 0.224 mg/Kg ☼08/09/17 20:35 08/11/17 17:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.560 0.224 mg/Kg 08/09/17 20:35 08/11/17 17:50 1☼Arsenic 2.03
0.560 0.224 mg/Kg 08/09/17 20:35 08/11/17 17:50 1☼Thallium <0.224
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.324 0.114 0.0343 mg/Kg ☼08/08/17 14:17 08/10/17 08:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-4Client Sample ID: SURF-EDGE-3
Matrix: SolidDate Collected: 08/04/17 10:50
Percent Solids: 85.1Date Received: 08/05/17 10:00
General Chemistry
RL RL
Percent Moisture 14.9 0.1 0.1 %08/08/17 11:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 11:15 1Percent Solids 85.1
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-5Client Sample ID: SURF-BASE-1
Matrix: SolidDate Collected: 08/04/17 11:30
Percent Solids: 62.6Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0507 0.106 0.0507 mg/Kg ☼08/08/17 10:12 08/10/17 15:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.106 0.0460 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Acenaphthylene <0.0460
0.106 0.0460 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Anthracene <0.0460
0.106 0.0476 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Benzo[a]anthracene <0.0476
0.106 0.0428 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Benzo[a]pyrene 0.0573 J
0.106 0.0444 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Benzo[b]fluoranthene <0.0444
0.106 0.0523 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Benzo[g,h,i]perylene <0.0523
0.106 0.0428 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Benzo[k]fluoranthene <0.0428
0.528 0.317 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Bis(2-chloroethoxy)methane <0.317
0.528 0.338 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Bis(2-chloroethyl)ether <0.338
0.528 0.314 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼bis (2-chloroisopropyl) ether <0.314
0.528 0.328 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Bis(2-ethylhexyl) phthalate <0.328
0.528 0.325 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼4-Bromophenyl phenyl ether <0.325
0.528 0.341 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Butyl benzyl phthalate <0.341
0.528 0.328 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Carbazole <0.328
0.528 0.360 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼4-Chloroaniline <0.360
0.528 0.266 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼4-Chloro-3-methylphenol <0.266
0.528 0.331 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2-Chloronaphthalene <0.331
0.528 0.303 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2-Chlorophenol <0.303
0.528 0.319 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼4-Chlorophenyl phenyl ether <0.319
0.106 0.0587 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Chrysene <0.0587
1.06 0.179 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Cresols <0.179
0.106 0.0507 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Dibenz(a,h)anthracene <0.0507
0.528 0.333 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Dibenzofuran <0.333
0.528 0.301 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼1,2-Dichlorobenzene <0.301
0.528 0.301 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼1,3-Dichlorobenzene <0.301
0.528 0.311 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼1,4-Dichlorobenzene <0.311
1.06 0.323 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼3,3'-Dichlorobenzidine <0.323
0.528 0.277 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2,4-Dichlorophenol <0.277
0.528 0.336 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Diethyl phthalate <0.336
1.06 0.531 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2,4-Dimethylphenol <0.531
0.528 0.328 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Dimethyl phthalate <0.328
0.528 0.335 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Di-n-butyl phthalate <0.335
0.528 0.363 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼4,6-Dinitro-2-methylphenol <0.363
0.528 0.398 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2,4-Dinitrophenol <0.398
0.528 0.330 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2,4-Dinitrotoluene <0.330
0.528 0.354 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2,6-Dinitrotoluene <0.354
0.528 0.282 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Di-n-octyl phthalate <0.282
0.106 0.0539 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Fluoranthene <0.0539
0.106 0.0460 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Fluorene <0.0460
0.528 0.396 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Hexachlorobenzene <0.396
0.528 0.265 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Hexachlorobutadiene <0.265
0.528 0.238 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Hexachlorocyclopentadiene <0.238 *
0.528 0.287 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Hexachloroethane <0.287
0.106 0.0460 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Indeno[1,2,3-cd]pyrene <0.0460
0.528 0.298 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Isophorone <0.298
0.106 0.0444 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼1-Methylnaphthalene <0.0444
0.106 0.0412 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2-Methylnaphthalene <0.0412
0.528 0.342 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2-Methylphenol <0.342
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-5Client Sample ID: SURF-BASE-1
Matrix: SolidDate Collected: 08/04/17 11:30
Percent Solids: 62.6Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <0.322 0.528 0.322 mg/Kg ☼08/08/17 10:12 08/10/17 15:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.106 0.0460 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Naphthalene <0.0460
0.528 0.328 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2-Nitroaniline <0.328
1.06 0.365 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼3-Nitroaniline <0.365
1.06 0.377 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼4-Nitroaniline <0.377
0.528 0.319 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Nitrobenzene <0.319
0.528 0.385 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2-Nitrophenol <0.385
1.06 0.606 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼4-Nitrophenol <0.606
0.528 0.308 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼N-Nitrosodi-n-propylamine <0.308
0.528 0.0840 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0840
1.06 0.422 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Pentachlorophenol <0.422
0.106 0.0539 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Phenanthrene <0.0539
0.528 0.322 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Phenol <0.322
0.106 0.0539 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼Pyrene <0.0539
0.528 0.287 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼1,2,4-Trichlorobenzene <0.287
0.528 0.346 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2,4,5-Trichlorophenol <0.346
0.528 0.304 mg/Kg 08/08/17 10:12 08/10/17 15:36 1☼2,4,6-Trichlorophenol <0.304
2-Fluorobiphenyl (Surr)76 29-120 08/08/17 10:12 08/10/17 15:36 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)68 08/08/17 10:12 08/10/17 15:36 110-120
Nitrobenzene-d5 (Surr)73 08/08/17 10:12 08/10/17 15:36 127-120
Phenol-d5 (Surr)68 08/08/17 10:12 08/10/17 15:36 110-120
Terphenyl-d14 (Surr)87 08/08/17 10:12 08/10/17 15:36 113-120
2,4,6-Tribromophenol (Surr)89 08/08/17 10:12 08/10/17 15:36 110-120
Method: 6010D - Metals (ICP)
RL MDL
Beryllium 1.49 J 1.59 0.317 mg/Kg ☼08/09/17 10:33 08/12/17 00:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.59 0.159 mg/Kg 08/09/17 10:33 08/12/17 00:53 1☼Cadmium <0.159
1.59 1.43 mg/Kg 08/09/17 10:33 08/12/17 00:53 1☼Chromium 25.0 B
3.17 1.75 mg/Kg 08/09/17 10:33 08/12/17 00:53 1☼Copper 1070
1.59 0.794 mg/Kg 08/09/17 10:33 08/12/17 00:53 1☼Lead 644
4.76 1.59 mg/Kg 08/09/17 10:33 08/12/17 00:53 1☼Manganese 486
3.17 0.952 mg/Kg 08/09/17 10:33 08/12/17 00:53 1☼Nickel 6.67
3.17 1.75 mg/Kg 08/09/17 10:33 08/12/17 00:53 1☼Selenium <1.75
1.59 0.635 mg/Kg 08/09/17 10:33 08/12/17 00:53 1☼Silver 2.70
15.9 7.94 mg/Kg 08/09/17 10:33 08/12/17 00:53 1☼Zinc 131
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony 1.75 0.775 0.310 mg/Kg ☼08/09/17 20:35 08/11/17 17:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.88 1.55 mg/Kg 08/09/17 20:35 08/11/17 08:02 5☼Arsenic 10.4
0.775 0.310 mg/Kg 08/09/17 20:35 08/11/17 17:56 1☼Thallium <0.310
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.432 0.155 0.0464 mg/Kg ☼08/08/17 14:17 08/10/17 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-5Client Sample ID: SURF-BASE-1
Matrix: SolidDate Collected: 08/04/17 11:30
Percent Solids: 62.6Date Received: 08/05/17 10:00
General Chemistry
RL RL
Percent Moisture 37.4 0.1 0.1 %08/08/17 11:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 11:15 1Percent Solids 62.6
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-6Client Sample ID: SURF-BASE-2
Matrix: SolidDate Collected: 08/04/17 11:45
Percent Solids: 74.6Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.212 0.444 0.212 mg/Kg ☼08/08/17 10:12 08/10/17 15:56 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.444 0.192 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Acenaphthylene <0.192
0.444 0.192 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Anthracene <0.192
0.444 0.199 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Benzo[a]anthracene <0.199
0.444 0.179 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Benzo[a]pyrene <0.179
0.444 0.185 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Benzo[b]fluoranthene <0.185
0.444 0.219 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Benzo[g,h,i]perylene <0.219
0.444 0.179 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Benzo[k]fluoranthene <0.179
2.21 1.32 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Bis(2-chloroethoxy)methane <1.32
2.21 1.41 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Bis(2-chloroethyl)ether <1.41
2.21 1.31 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼bis (2-chloroisopropyl) ether <1.31
2.21 1.37 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Bis(2-ethylhexyl) phthalate <1.37
2.21 1.36 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼4-Bromophenyl phenyl ether <1.36
2.21 1.42 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Butyl benzyl phthalate <1.42
2.21 1.37 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Carbazole <1.37
2.21 1.50 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼4-Chloroaniline <1.50
2.21 1.11 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼4-Chloro-3-methylphenol <1.11
2.21 1.38 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2-Chloronaphthalene <1.38
2.21 1.27 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2-Chlorophenol <1.27
2.21 1.33 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼4-Chlorophenyl phenyl ether <1.33
0.444 0.245 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Chrysene <0.245
4.41 0.749 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Cresols <0.749
0.444 0.212 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Dibenz(a,h)anthracene <0.212
2.21 1.39 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Dibenzofuran <1.39
2.21 1.26 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼1,2-Dichlorobenzene <1.26
2.21 1.26 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼1,3-Dichlorobenzene <1.26
2.21 1.30 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼1,4-Dichlorobenzene <1.30
4.44 1.35 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼3,3'-Dichlorobenzidine <1.35
2.21 1.16 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2,4-Dichlorophenol <1.16
2.21 1.40 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Diethyl phthalate <1.40
4.44 2.22 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2,4-Dimethylphenol <2.22
2.21 1.37 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Dimethyl phthalate <1.37
2.21 1.40 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Di-n-butyl phthalate <1.40
2.21 1.52 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼4,6-Dinitro-2-methylphenol <1.52
2.21 1.66 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2,4-Dinitrophenol <1.66
2.21 1.38 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2,4-Dinitrotoluene <1.38
2.21 1.48 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2,6-Dinitrotoluene <1.48
2.21 1.18 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Di-n-octyl phthalate <1.18
0.444 0.225 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Fluoranthene <0.225
0.444 0.192 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Fluorene <0.192
2.21 1.66 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Hexachlorobenzene <1.66
2.21 1.11 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Hexachlorobutadiene <1.11
2.21 0.994 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Hexachlorocyclopentadiene <0.994 *
2.21 1.20 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Hexachloroethane <1.20
0.444 0.192 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Indeno[1,2,3-cd]pyrene <0.192
2.21 1.25 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Isophorone <1.25
0.444 0.185 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼1-Methylnaphthalene <0.185
0.444 0.172 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2-Methylnaphthalene <0.172
2.21 1.43 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2-Methylphenol <1.43
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-6Client Sample ID: SURF-BASE-2
Matrix: SolidDate Collected: 08/04/17 11:45
Percent Solids: 74.6Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <1.34 2.21 1.34 mg/Kg ☼08/08/17 10:12 08/10/17 15:56 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.444 0.192 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Naphthalene <0.192
2.21 1.37 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2-Nitroaniline <1.37
4.44 1.52 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼3-Nitroaniline <1.52
4.44 1.58 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼4-Nitroaniline <1.58
2.21 1.33 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Nitrobenzene <1.33
2.21 1.61 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2-Nitrophenol <1.61
4.44 2.53 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼4-Nitrophenol <2.53
2.21 1.29 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼N-Nitrosodi-n-propylamine <1.29
2.21 0.351 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.351
4.44 1.76 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Pentachlorophenol <1.76
0.444 0.225 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Phenanthrene <0.225
2.21 1.34 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Phenol <1.34
0.444 0.225 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼Pyrene <0.225
2.21 1.20 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼1,2,4-Trichlorobenzene <1.20
2.21 1.44 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2,4,5-Trichlorophenol <1.44
2.21 1.27 mg/Kg 08/08/17 10:12 08/10/17 15:56 5☼2,4,6-Trichlorophenol <1.27
2-Fluorobiphenyl (Surr)67 29-120 08/08/17 10:12 08/10/17 15:56 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)59 08/08/17 10:12 08/10/17 15:56 510-120
Nitrobenzene-d5 (Surr)63 08/08/17 10:12 08/10/17 15:56 527-120
Phenol-d5 (Surr)59 08/08/17 10:12 08/10/17 15:56 510-120
Terphenyl-d14 (Surr)82 08/08/17 10:12 08/10/17 15:56 513-120
2,4,6-Tribromophenol (Surr)97 08/08/17 10:12 08/10/17 15:56 510-120
Method: 6010D - Metals (ICP)
RL MDL
Beryllium 0.618 J 1.29 0.257 mg/Kg ☼08/09/17 10:33 08/12/17 00:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.29 0.129 mg/Kg 08/09/17 10:33 08/12/17 00:58 1☼Cadmium <0.129
1.29 1.16 mg/Kg 08/09/17 10:33 08/12/17 00:58 1☼Chromium 14.3
2.57 1.42 mg/Kg 08/09/17 10:33 08/12/17 00:58 1☼Copper 57.8
1.29 0.644 mg/Kg 08/09/17 10:33 08/12/17 00:58 1☼Lead 86.6
3.86 1.29 mg/Kg 08/09/17 10:33 08/12/17 00:58 1☼Manganese 118
2.57 0.772 mg/Kg 08/09/17 10:33 08/12/17 00:58 1☼Nickel 4.38
2.57 1.42 mg/Kg 08/09/17 10:33 08/12/17 00:58 1☼Selenium <1.42
1.29 0.515 mg/Kg 08/09/17 10:33 08/12/17 00:58 1☼Silver 0.644 J
12.9 6.44 mg/Kg 08/09/17 10:33 08/12/17 00:58 1☼Zinc 92.1
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony 0.367 J 0.639 0.255 mg/Kg ☼08/09/17 20:35 08/11/17 18:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.19 1.28 mg/Kg 08/09/17 20:35 08/11/17 08:07 5☼Arsenic 5.26
0.639 0.255 mg/Kg 08/09/17 20:35 08/11/17 18:01 1☼Thallium <0.255
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.264 0.130 0.0390 mg/Kg ☼08/08/17 14:17 08/10/17 08:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-6Client Sample ID: SURF-BASE-2
Matrix: SolidDate Collected: 08/04/17 11:45
Percent Solids: 74.6Date Received: 08/05/17 10:00
General Chemistry
RL RL
Percent Moisture 25.4 0.1 0.1 %08/08/17 11:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 11:15 1Percent Solids 74.6
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-7Client Sample ID: SURF-BASE-3
Matrix: SolidDate Collected: 08/04/17 12:05
Percent Solids: 72.4Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0430 0.0900 0.0430 mg/Kg ☼08/08/17 10:12 08/10/17 16:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0900 0.0390 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Acenaphthylene <0.0390
0.0900 0.0390 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Anthracene 0.0922
0.0900 0.0403 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Benzo[a]anthracene 0.273
0.0900 0.0363 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Benzo[a]pyrene 0.265
0.0900 0.0376 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Benzo[b]fluoranthene 0.280
0.0900 0.0443 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Benzo[g,h,i]perylene 0.199
0.0900 0.0363 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Benzo[k]fluoranthene 0.173
0.447 0.269 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Bis(2-chloroethoxy)methane <0.269
0.447 0.286 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Bis(2-chloroethyl)ether <0.286
0.447 0.266 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼bis (2-chloroisopropyl) ether <0.266
0.447 0.278 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Bis(2-ethylhexyl) phthalate <0.278
0.447 0.275 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼4-Bromophenyl phenyl ether <0.275
0.447 0.289 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Butyl benzyl phthalate <0.289
0.447 0.278 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Carbazole <0.278
0.447 0.305 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼4-Chloroaniline <0.305
0.447 0.226 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼4-Chloro-3-methylphenol <0.226
0.447 0.281 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2-Chloronaphthalene <0.281
0.447 0.257 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2-Chlorophenol <0.257
0.447 0.270 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼4-Chlorophenyl phenyl ether <0.270
0.0900 0.0497 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Chrysene 0.249
0.895 0.152 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Cresols <0.152
0.0900 0.0430 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Dibenz(a,h)anthracene <0.0430
0.447 0.282 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Dibenzofuran <0.282
0.447 0.255 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼1,2-Dichlorobenzene <0.255
0.447 0.255 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼1,3-Dichlorobenzene <0.255
0.447 0.263 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼1,4-Dichlorobenzene <0.263
0.900 0.274 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼3,3'-Dichlorobenzidine <0.274
0.447 0.235 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2,4-Dichlorophenol <0.235
0.447 0.285 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Diethyl phthalate <0.285
0.900 0.450 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2,4-Dimethylphenol <0.450
0.447 0.278 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Dimethyl phthalate <0.278
0.447 0.283 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Di-n-butyl phthalate <0.283
0.447 0.308 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼4,6-Dinitro-2-methylphenol <0.308
0.447 0.337 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2,4-Dinitrophenol <0.337
0.447 0.279 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2,4-Dinitrotoluene <0.279
0.447 0.300 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2,6-Dinitrotoluene <0.300
0.447 0.239 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Di-n-octyl phthalate <0.239
0.0900 0.0457 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Fluoranthene 0.497
0.0900 0.0390 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Fluorene <0.0390
0.447 0.336 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Hexachlorobenzene <0.336
0.447 0.224 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Hexachlorobutadiene <0.224
0.447 0.202 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Hexachlorocyclopentadiene <0.202 *
0.447 0.243 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Hexachloroethane <0.243
0.0900 0.0390 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Indeno[1,2,3-cd]pyrene 0.161
0.447 0.253 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Isophorone <0.253
0.0900 0.0376 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼1-Methylnaphthalene <0.0376
0.0900 0.0349 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2-Methylnaphthalene <0.0349
0.447 0.290 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2-Methylphenol <0.290
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-7Client Sample ID: SURF-BASE-3
Matrix: SolidDate Collected: 08/04/17 12:05
Percent Solids: 72.4Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <0.273 0.447 0.273 mg/Kg ☼08/08/17 10:12 08/10/17 16:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0900 0.0390 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Naphthalene <0.0390
0.447 0.278 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2-Nitroaniline <0.278
0.900 0.309 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼3-Nitroaniline <0.309
0.900 0.320 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼4-Nitroaniline <0.320
0.447 0.270 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Nitrobenzene <0.270
0.447 0.326 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2-Nitrophenol <0.326
0.900 0.513 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼4-Nitrophenol <0.513
0.447 0.261 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼N-Nitrosodi-n-propylamine <0.261
0.447 0.0712 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0712
0.900 0.357 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Pentachlorophenol <0.357
0.0900 0.0457 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Phenanthrene 0.258
0.447 0.273 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Phenol <0.273
0.0900 0.0457 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼Pyrene 0.493
0.447 0.243 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼1,2,4-Trichlorobenzene <0.243
0.447 0.293 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2,4,5-Trichlorophenol <0.293
0.447 0.258 mg/Kg 08/08/17 10:12 08/10/17 16:15 1☼2,4,6-Trichlorophenol <0.258
2-Fluorobiphenyl (Surr)58 29-120 08/08/17 10:12 08/10/17 16:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)50 08/08/17 10:12 08/10/17 16:15 110-120
Nitrobenzene-d5 (Surr)54 08/08/17 10:12 08/10/17 16:15 127-120
Phenol-d5 (Surr)52 08/08/17 10:12 08/10/17 16:15 110-120
Terphenyl-d14 (Surr)76 08/08/17 10:12 08/10/17 16:15 113-120
2,4,6-Tribromophenol (Surr)72 08/08/17 10:12 08/10/17 16:15 110-120
Method: 6010D - Metals (ICP)
RL MDL
Beryllium <0.274 1.37 0.274 mg/Kg ☼08/09/17 10:33 08/12/17 01:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.37 0.137 mg/Kg 08/09/17 10:33 08/12/17 01:03 1☼Cadmium 2.63
1.37 1.23 mg/Kg 08/09/17 10:33 08/12/17 01:03 1☼Chromium 3.97
2.74 1.51 mg/Kg 08/09/17 10:33 08/12/17 01:03 1☼Copper 174
1.37 0.684 mg/Kg 08/09/17 10:33 08/12/17 01:03 1☼Lead 1240
4.11 1.37 mg/Kg 08/09/17 10:33 08/12/17 01:03 1☼Manganese 204
2.74 0.821 mg/Kg 08/09/17 10:33 08/12/17 01:03 1☼Nickel 2.52 J
2.74 1.51 mg/Kg 08/09/17 10:33 08/12/17 01:03 1☼Selenium <1.51
1.37 0.547 mg/Kg 08/09/17 10:33 08/12/17 01:03 1☼Silver 0.575 J
13.7 6.84 mg/Kg 08/09/17 10:33 08/12/17 01:03 1☼Zinc 750
Method: 6020B - Metals (ICP/MS)
RL MDL
Antimony 1.07 0.680 0.272 mg/Kg ☼08/09/17 20:35 08/11/17 18:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.680 0.272 mg/Kg 08/09/17 20:35 08/11/17 18:07 1☼Arsenic 9.21
0.680 0.272 mg/Kg 08/09/17 20:35 08/11/17 18:07 1☼Thallium <0.272
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury 0.483 0.138 0.0415 mg/Kg ☼08/08/17 14:17 08/10/17 08:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Lab Sample ID: 490-134160-7Client Sample ID: SURF-BASE-3
Matrix: SolidDate Collected: 08/04/17 12:05
Percent Solids: 72.4Date Received: 08/05/17 10:00
General Chemistry
RL RL
Percent Moisture 27.6 0.1 0.1 %08/08/17 11:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 11:15 1Percent Solids 72.4
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-450963/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
RL MDL
Acenaphthene <0.0320 0.0670 0.0320 mg/Kg 08/08/17 10:12 08/10/17 11:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Acenaphthylene
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Anthracene
<0.0300 0.03000.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[a]anthracene
<0.0270 0.02700.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[a]pyrene
<0.0280 0.02800.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[b]fluoranthene
<0.0330 0.03300.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[g,h,i]perylene
<0.0270 0.02700.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[k]fluoranthene
<0.200 0.2000.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Bis(2-chloroethoxy)methane
<0.213 0.2130.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Bis(2-chloroethyl)ether
<0.198 0.1980.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1bis (2-chloroisopropyl) ether
<0.207 0.2070.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Bis(2-ethylhexyl) phthalate
<0.205 0.2050.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Bromophenyl phenyl ether
<0.215 0.2150.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Butyl benzyl phthalate
<0.207 0.2070.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Carbazole
<0.227 0.2270.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Chloroaniline
<0.168 0.1680.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Chloro-3-methylphenol
<0.209 0.2090.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Chloronaphthalene
<0.191 0.1910.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Chlorophenol
<0.201 0.2010.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Chlorophenyl phenyl ether
<0.0370 0.03700.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Chrysene
<0.113 0.1130.666 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Cresols
<0.0320 0.03200.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Dibenz(a,h)anthracene
<0.210 0.2100.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Dibenzofuran
<0.190 0.1900.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 11,2-Dichlorobenzene
<0.190 0.1900.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 11,3-Dichlorobenzene
<0.196 0.1960.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 11,4-Dichlorobenzene
<0.204 0.2040.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 13,3'-Dichlorobenzidine
<0.175 0.1750.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4-Dichlorophenol
<0.212 0.2120.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Diethyl phthalate
<0.335 0.3350.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4-Dimethylphenol
<0.207 0.2070.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Dimethyl phthalate
<0.211 0.2110.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Di-n-butyl phthalate
<0.229 0.2290.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14,6-Dinitro-2-methylphenol
<0.251 0.2510.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4-Dinitrophenol
<0.208 0.2080.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4-Dinitrotoluene
<0.223 0.2230.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,6-Dinitrotoluene
<0.178 0.1780.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Di-n-octyl phthalate
<0.0340 0.03400.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Fluoranthene
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Fluorene
<0.250 0.2500.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Hexachlorobenzene
<0.167 0.1670.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Hexachlorobutadiene
<0.150 0.1500.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Hexachlorocyclopentadiene
<0.181 0.1810.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Hexachloroethane
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Indeno[1,2,3-cd]pyrene
<0.188 0.1880.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Isophorone
<0.0280 0.02800.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 11-Methylnaphthalene
<0.0260 0.02600.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Methylnaphthalene
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-450963/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
RL MDL
2-Methylphenol <0.216 0.333 0.216 mg/Kg 08/08/17 10:12 08/10/17 11:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.203 0.2030.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 13 & 4 Methylphenol
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Naphthalene
<0.207 0.2070.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Nitroaniline
<0.230 0.2300.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 13-Nitroaniline
<0.238 0.2380.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Nitroaniline
<0.201 0.2010.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Nitrobenzene
<0.243 0.2430.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Nitrophenol
<0.382 0.3820.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Nitrophenol
<0.194 0.1940.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1N-Nitrosodi-n-propylamine
<0.0530 0.05300.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1n-Nitrosodiphenylamine(as
diphenylamine)
<0.266 0.2660.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Pentachlorophenol
<0.0340 0.03400.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Phenanthrene
<0.203 0.2030.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Phenol
<0.0340 0.03400.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Pyrene
<0.181 0.1810.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 11,2,4-Trichlorobenzene
<0.218 0.2180.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4,5-Trichlorophenol
<0.192 0.1920.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)91 29-120 08/10/17 11:44 1
MB MB
Surrogate
08/08/17 10:12
Dil FacPreparedAnalyzedQualifierLimits%Recovery
75 08/08/17 10:12 08/10/17 11:44 12-Fluorophenol (Surr)10-120
89 08/08/17 10:12 08/10/17 11:44 1Nitrobenzene-d5 (Surr)27-120
83 08/08/17 10:12 08/10/17 11:44 1Phenol-d5 (Surr)10-120
95 08/08/17 10:12 08/10/17 11:44 1Terphenyl-d14 (Surr)13-120
80 08/08/17 10:12 08/10/17 11:44 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450963/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
Acenaphthene 1.67 1.439 mg/Kg 86 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.410 mg/Kg 85 38-120
Anthracene 1.67 1.481 mg/Kg 89 46-124
Benzo[a]anthracene 1.67 1.562 mg/Kg 94 45-120
Benzo[a]pyrene 1.67 1.452 mg/Kg 87 45-120
Benzo[b]fluoranthene 1.67 1.437 mg/Kg 86 42-120
Benzo[g,h,i]perylene 1.67 1.454 mg/Kg 87 38-120
Benzo[k]fluoranthene 1.67 1.740 mg/Kg 104 42-120
Bis(2-chloroethoxy)methane 1.67 1.193 mg/Kg 72 32-120
Bis(2-chloroethyl)ether 1.67 1.124 mg/Kg 67 31-120
bis (2-chloroisopropyl) ether 1.67 0.8252 mg/Kg 50 32-120
Bis(2-ethylhexyl) phthalate 1.67 1.531 mg/Kg 92 43-120
4-Bromophenyl phenyl ether 1.67 1.464 mg/Kg 88 40-120
Butyl benzyl phthalate 1.67 1.510 mg/Kg 91 43-133
Carbazole 1.67 1.511 mg/Kg 91 44-120
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450963/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
4-Chloroaniline 1.67 0.8331 mg/Kg 50 35-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
4-Chloro-3-methylphenol 1.67 1.522 mg/Kg 91 38-120
2-Chloronaphthalene 1.67 1.376 mg/Kg 83 34-120
2-Chlorophenol 1.67 1.316 mg/Kg 79 32-120
4-Chlorophenyl phenyl ether 1.67 1.453 mg/Kg 87 42-120
Chrysene 1.67 1.588 mg/Kg 95 43-120
Cresols 3.33 2.490 mg/Kg 75 36-129
Dibenz(a,h)anthracene 1.67 1.486 mg/Kg 89 32-128
Dibenzofuran 1.67 1.404 mg/Kg 84 41-120
1,2-Dichlorobenzene 1.67 1.276 mg/Kg 77 33-120
1,3-Dichlorobenzene 1.67 1.262 mg/Kg 76 32-120
1,4-Dichlorobenzene 1.67 1.281 mg/Kg 77 32-120
3,3'-Dichlorobenzidine 1.67 1.463 mg/Kg 88 39-120
2,4-Dichlorophenol 1.67 1.428 mg/Kg 86 32-120
Diethyl phthalate 1.67 1.539 mg/Kg 92 41-122
2,4-Dimethylphenol 1.67 0.9432 mg/Kg 57 32-120
Dimethyl phthalate 1.67 1.532 mg/Kg 92 55-120
Di-n-butyl phthalate 1.67 1.693 mg/Kg 102 46-127
4,6-Dinitro-2-methylphenol 3.33 3.438 mg/Kg 103 27-134
2,4-Dinitrophenol 3.33 3.215 mg/Kg 96 10-142
2,4-Dinitrotoluene 1.67 1.615 mg/Kg 97 43-120
2,6-Dinitrotoluene 1.67 1.693 mg/Kg 102 43-120
Di-n-octyl phthalate 1.67 1.724 mg/Kg 103 40-130
Fluoranthene 1.67 1.635 mg/Kg 98 46-120
Fluorene 1.67 1.457 mg/Kg 87 42-120
Hexachlorobenzene 1.67 1.639 mg/Kg 98 44-120
Hexachlorobutadiene 1.67 1.526 mg/Kg 92 31-120
Hexachlorocyclopentadiene 1.67 <0.150 *mg/Kg 2 24-120
Hexachloroethane 1.67 1.201 mg/Kg 72 33-120
Indeno[1,2,3-cd]pyrene 1.67 1.489 mg/Kg 89 41-121
Isophorone 1.67 0.6517 mg/Kg 39 33-120
1-Methylnaphthalene 1.67 1.358 mg/Kg 81 32-120
2-Methylnaphthalene 1.67 1.361 mg/Kg 82 28-120
2-Methylphenol 1.67 1.215 mg/Kg 73 36-120
3 & 4 Methylphenol 1.67 1.275 mg/Kg 77 37-120
Naphthalene 1.67 1.326 mg/Kg 80 32-120
2-Nitroaniline 1.67 1.443 mg/Kg 87 40-120
3-Nitroaniline 1.67 1.303 mg/Kg 78 42-120
4-Nitroaniline 1.67 1.407 mg/Kg 84 43-120
Nitrobenzene 1.67 1.167 mg/Kg 70 26-120
2-Nitrophenol 1.67 1.628 mg/Kg 98 29-120
4-Nitrophenol 3.33 2.953 mg/Kg 89 32-136
N-Nitrosodi-n-propylamine 1.67 1.168 mg/Kg 70 35-120
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.391 mg/Kg 98 52-140
Pentachlorophenol 3.33 3.161 mg/Kg 95 44-134
Phenanthrene 1.67 1.488 mg/Kg 89 45-120
Phenol 1.67 1.281 mg/Kg 77 30-120
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450963/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
Pyrene 1.67 1.575 mg/Kg 95 43-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2,4-Trichlorobenzene 1.67 1.401 mg/Kg 84 29-120
2,4,5-Trichlorophenol 1.67 1.609 mg/Kg 97 39-120
2,4,6-Trichlorophenol 1.67 1.597 mg/Kg 96 39-120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
88
LCS LCS
Qualifier Limits%Recovery
812-Fluorophenol (Surr)10 -120
88Nitrobenzene-d5 (Surr)27 -120
84Phenol-d5 (Surr)10 -120
107Terphenyl-d14 (Surr)13 -120
1072,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Matrix SpikeLab Sample ID: 490-134155-B-22-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
Acenaphthene <0.0314 1.66 1.306 mg/Kg 79 19-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene <0.0285 1.66 1.294 mg/Kg 78 25-120
Anthracene <0.0285 1.66 1.490 mg/Kg 90 28-125
Benzo[a]anthracene <0.0295 1.66 1.612 mg/Kg 97 23-120
Benzo[a]pyrene <0.0265 1.66 1.479 mg/Kg 89 15-128
Benzo[b]fluoranthene <0.0275 1.66 1.528 mg/Kg 92 12-133
Benzo[g,h,i]perylene <0.0324 1.66 1.533 mg/Kg 92 22-120
Benzo[k]fluoranthene <0.0265 1.66 1.670 mg/Kg 101 28-120
Bis(2-chloroethoxy)methane <0.196 1.66 0.9790 mg/Kg 59 24-120
Bis(2-chloroethyl)ether <0.209 1.66 0.8740 mg/Kg 53 22-120
bis (2-chloroisopropyl) ether <0.194 1.66 0.6447 mg/Kg 39 20-120
Bis(2-ethylhexyl) phthalate <0.203 1.66 1.640 mg/Kg 99 26-120
4-Bromophenyl phenyl ether <0.201 1.66 1.471 mg/Kg 89 31-120
Butyl benzyl phthalate <0.211 1.66 1.618 mg/Kg 98 24-133
Carbazole <0.203 1.66 1.535 mg/Kg 93 25-123
4-Chloroaniline <0.223 1.66 0.7267 mg/Kg 44 26-120
4-Chloro-3-methylphenol <0.165 1.66 1.466 mg/Kg 88 21-120
2-Chloronaphthalene <0.205 1.66 1.207 mg/Kg 73 24-120
2-Chlorophenol <0.188 1.66 1.015 mg/Kg 61 25-120
4-Chlorophenyl phenyl ether <0.197 1.66 1.377 mg/Kg 83 26-120
Chrysene <0.0363 1.66 1.624 mg/Kg 98 20-120
Cresols <0.111 3.31 2.121 mg/Kg 64 10-200
Dibenz(a,h)anthracene <0.0314 1.66 1.559 mg/Kg 94 12-128
Dibenzofuran <0.206 1.66 1.329 mg/Kg 80 21-120
1,2-Dichlorobenzene <0.187 1.66 0.9531 mg/Kg 58 10-120
1,3-Dichlorobenzene <0.187 1.66 0.9261 mg/Kg 56 10-120
1,4-Dichlorobenzene <0.192 1.66 0.9258 mg/Kg 56 10-120
3,3'-Dichlorobenzidine <0.200 1.66 1.441 mg/Kg 87 10-120
2,4-Dichlorophenol <0.172 1.66 1.224 mg/Kg 74 17-120
Diethyl phthalate <0.208 1.66 1.549 mg/Kg 93 29-122
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-134155-B-22-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
2,4-Dimethylphenol <0.329 1.66 0.8543 mg/Kg 52 17-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Dimethyl phthalate <0.203 1.66 1.515 mg/Kg 91 30-120
Di-n-butyl phthalate <0.207 1.66 1.715 mg/Kg 103 29-126
4,6-Dinitro-2-methylphenol <0.225 3.31 1.856 mg/Kg 56 10-134
2,4-Dinitrophenol <0.246 3.31 1.417 mg/Kg 43 10-150
2,4-Dinitrotoluene <0.204 1.66 1.586 mg/Kg 96 24-121
2,6-Dinitrotoluene <0.219 1.66 1.638 mg/Kg 99 24-120
Di-n-octyl phthalate <0.175 1.66 1.858 mg/Kg 112 27-130
Fluoranthene <0.0334 1.66 1.625 mg/Kg 98 10-143
Fluorene <0.0285 1.66 1.406 mg/Kg 85 20-120
Hexachlorobenzene <0.245 1.66 1.650 mg/Kg 100 25-120
Hexachlorobutadiene <0.164 1.66 1.144 mg/Kg 69 10-120
Hexachlorocyclopentadiene <0.147 * F1 1.66 <0.149 F1 mg/Kg 0 10-120
Hexachloroethane <0.178 1.66 0.8796 mg/Kg 53 10-120
Indeno[1,2,3-cd]pyrene <0.0285 1.66 1.556 mg/Kg 94 22-121
Isophorone <0.185 1.66 0.5645 mg/Kg 34 24-120
1-Methylnaphthalene <0.0275 1.66 1.163 mg/Kg 70 10-120
2-Methylnaphthalene <0.0255 1.66 1.149 mg/Kg 69 13-120
2-Methylphenol <0.212 1.66 1.010 mg/Kg 61 23-120
3 & 4 Methylphenol <0.199 1.66 1.111 mg/Kg 67 19-120
Naphthalene <0.0285 1.66 1.042 mg/Kg 63 10-120
2-Nitroaniline <0.203 1.66 1.398 mg/Kg 84 31-120
3-Nitroaniline <0.226 1.66 1.296 mg/Kg 78 31-120
4-Nitroaniline <0.234 1.66 1.410 mg/Kg 85 28-120
Nitrobenzene <0.197 1.66 0.9413 mg/Kg 57 19-120
2-Nitrophenol <0.239 1.66 1.239 mg/Kg 75 23-120
4-Nitrophenol <0.375 3.31 2.877 mg/Kg 87 16-139
N-Nitrosodi-n-propylamine <0.191 1.66 1.001 mg/Kg 60 24-120
n-Nitrosodiphenylamine(as
diphenylamine)
<0.0520 1.41 1.419 mg/Kg 101 26-150
Pentachlorophenol <0.261 3.31 3.099 mg/Kg 94 19-145
Phenanthrene <0.0334 1.66 1.516 mg/Kg 91 21-122
Phenol <0.199 1.66 1.041 mg/Kg 63 15-120
Pyrene <0.0334 1.66 1.702 mg/Kg 103 20-123
1,2,4-Trichlorobenzene <0.178 1.66 1.099 mg/Kg 66 14-120
2,4,5-Trichlorophenol <0.214 1.66 1.541 mg/Kg 93 27-120
2,4,6-Trichlorophenol <0.189 1.66 1.492 mg/Kg 90 24-122
2-Fluorobiphenyl (Surr)29 -120
Surrogate
76
MS MS
Qualifier Limits%Recovery
602-Fluorophenol (Surr)10 -120
67Nitrobenzene-d5 (Surr)27 -120
69Phenol-d5 (Surr)10 -120
117Terphenyl-d14 (Surr)13 -120
1082,4,6-Tribromophenol (Surr)10 -120
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-134155-B-22-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
Acenaphthene <0.0314 1.61 1.031 mg/Kg 64 19-120 24 50
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene <0.0285 1.61 1.025 mg/Kg 64 25-120 23 50
Anthracene <0.0285 1.61 1.185 mg/Kg 73 28-125 23 49
Benzo[a]anthracene <0.0295 1.61 1.267 mg/Kg 79 23-120 24 50
Benzo[a]pyrene <0.0265 1.61 1.180 mg/Kg 73 15-128 22 50
Benzo[b]fluoranthene <0.0275 1.61 1.329 mg/Kg 82 12-133 14 50
Benzo[g,h,i]perylene <0.0324 1.61 1.196 mg/Kg 74 22-120 25 50
Benzo[k]fluoranthene <0.0265 1.61 1.233 mg/Kg 76 28-120 30 45
Bis(2-chloroethoxy)methane <0.196 1.61 0.7630 mg/Kg 47 24-120 25 50
Bis(2-chloroethyl)ether <0.209 1.61 0.6873 mg/Kg 43 22-120 24 50
bis (2-chloroisopropyl) ether <0.194 1.61 0.5166 mg/Kg 32 20-120 22 50
Bis(2-ethylhexyl) phthalate <0.203 1.61 1.288 mg/Kg 80 26-120 24 50
4-Bromophenyl phenyl ether <0.201 1.61 1.170 mg/Kg 73 31-120 23 37
Butyl benzyl phthalate <0.211 1.61 1.304 mg/Kg 81 24-133 21 50
Carbazole <0.203 1.61 1.198 mg/Kg 74 25-123 25 46
4-Chloroaniline <0.223 1.61 0.5653 mg/Kg 35 26-120 25 50
4-Chloro-3-methylphenol <0.165 1.61 1.128 mg/Kg 70 21-120 26 49
2-Chloronaphthalene <0.205 1.61 0.9530 mg/Kg 59 24-120 23 50
2-Chlorophenol <0.188 1.61 0.7986 mg/Kg 49 25-120 24 50
4-Chlorophenyl phenyl ether <0.197 1.61 1.102 mg/Kg 68 26-120 22 50
Chrysene <0.0363 1.61 1.275 mg/Kg 79 20-120 24 49
Cresols <0.111 3.23 1.633 mg/Kg 51 10-200 26 50
Dibenz(a,h)anthracene <0.0314 1.61 1.228 mg/Kg 76 12-128 24 50
Dibenzofuran <0.206 1.61 1.048 mg/Kg 65 21-120 24 50
1,2-Dichlorobenzene <0.187 1.61 0.7693 mg/Kg 48 10-120 21 50
1,3-Dichlorobenzene <0.187 1.61 0.7506 mg/Kg 47 10-120 21 50
1,4-Dichlorobenzene <0.192 1.61 0.7562 mg/Kg 47 10-120 20 50
3,3'-Dichlorobenzidine <0.200 1.61 1.175 mg/Kg 73 10-120 20 50
2,4-Dichlorophenol <0.172 1.61 0.9499 mg/Kg 59 17-120 25 50
Diethyl phthalate <0.208 1.61 1.223 mg/Kg 76 29-122 24 45
2,4-Dimethylphenol <0.329 1.61 0.6258 J mg/Kg 39 17-120 31 50
Dimethyl phthalate <0.203 1.61 1.181 mg/Kg 73 30-120 25 46
Di-n-butyl phthalate <0.207 1.61 1.353 mg/Kg 84 29-126 24 49
4,6-Dinitro-2-methylphenol <0.225 3.23 1.518 mg/Kg 47 10-134 20 50
2,4-Dinitrophenol <0.246 3.23 1.155 mg/Kg 36 10-150 20 50
2,4-Dinitrotoluene <0.204 1.61 1.274 mg/Kg 79 24-121 22 50
2,6-Dinitrotoluene <0.219 1.61 1.295 mg/Kg 80 24-120 23 50
Di-n-octyl phthalate <0.175 1.61 1.492 mg/Kg 92 27-130 22 50
Fluoranthene <0.0334 1.61 1.285 mg/Kg 80 10-143 23 50
Fluorene <0.0285 1.61 1.112 mg/Kg 69 20-120 23 50
Hexachlorobenzene <0.245 1.61 1.302 mg/Kg 81 25-120 24 50
Hexachlorobutadiene <0.164 1.61 0.9239 mg/Kg 57 10-120 21 50
Hexachlorocyclopentadiene <0.147 * F1 1.61 <0.145 F1 mg/Kg 0 10-120 NC 50
Hexachloroethane <0.178 1.61 0.7102 mg/Kg 44 10-120 21 50
Indeno[1,2,3-cd]pyrene <0.0285 1.61 1.219 mg/Kg 76 22-121 24 50
Isophorone <0.185 1.61 0.4369 mg/Kg 27 24-120 25 50
1-Methylnaphthalene <0.0275 1.61 0.8923 mg/Kg 55 10-120 26 50
2-Methylnaphthalene <0.0255 1.61 0.8948 mg/Kg 55 13-120 25 50
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-134155-B-22-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
2-Methylphenol <0.212 1.61 0.7862 mg/Kg 49 23-120 25 50
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
3 & 4 Methylphenol <0.199 1.61 0.8467 mg/Kg 52 19-120 27 50
Naphthalene <0.0285 1.61 0.8203 mg/Kg 51 10-120 24 50
2-Nitroaniline <0.203 1.61 1.125 mg/Kg 70 31-120 22 50
3-Nitroaniline <0.226 1.61 1.042 mg/Kg 65 31-120 22 49
4-Nitroaniline <0.234 1.61 1.118 mg/Kg 69 28-120 23 49
Nitrobenzene <0.197 1.61 0.7380 mg/Kg 46 19-120 24 50
2-Nitrophenol <0.239 1.61 0.9973 mg/Kg 62 23-120 22 50
4-Nitrophenol <0.375 3.23 2.256 mg/Kg 70 16-139 24 45
N-Nitrosodi-n-propylamine <0.191 1.61 0.7750 mg/Kg 48 24-120 25 50
n-Nitrosodiphenylamine(as
diphenylamine)
<0.0520 1.37 1.124 mg/Kg 82 26-150 23 50
Pentachlorophenol <0.261 3.23 2.477 mg/Kg 77 19-145 22 50
Phenanthrene <0.0334 1.61 1.193 mg/Kg 74 21-122 24 50
Phenol <0.199 1.61 0.8136 mg/Kg 50 15-120 24 50
Pyrene <0.0334 1.61 1.379 mg/Kg 85 20-123 21 50
1,2,4-Trichlorobenzene <0.178 1.61 0.8748 mg/Kg 54 14-120 23 50
2,4,5-Trichlorophenol <0.214 1.61 1.226 mg/Kg 76 27-120 23 50
2,4,6-Trichlorophenol <0.189 1.61 1.159 mg/Kg 72 24-122 25 50
2-Fluorobiphenyl (Surr)29 -120
Surrogate
55
MSD MSD
Qualifier Limits%Recovery
432-Fluorophenol (Surr)10 -120
48Nitrobenzene-d5 (Surr)27 -120
49Phenol-d5 (Surr)10 -120
85Terphenyl-d14 (Surr)13 -120
802,4,6-Tribromophenol (Surr)10 -120
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 490-451273/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451273
RL MDL
C5-C8 Aliphatics <2.60 5.00 2.60 mg/Kg 08/09/17 13:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<3.00 3.005.00 mg/Kg 08/09/17 13:14 1C9-C10 Aromatics
<2.50 2.505.00 mg/Kg 08/09/17 13:14 1C9-C12 Aliphatics
2,5-Dibromotoluene (fid)90 70-130 08/09/17 13:14 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
87 08/09/17 13:14 12,5-Dibromotoluene (pid)70-130
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-451273/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451273
C5-C8 Aliphatics 15.0 14.91 mg/Kg 99 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C10 Aromatics 5.00 5.064 mg/Kg 101 70-130
C9-C12 Aliphatics 10.0 9.681 mg/Kg 97 70-130
2,5-Dibromotoluene (fid)70 -130
Surrogate
89
LCS LCS
Qualifier Limits%Recovery
882,5-Dibromotoluene (pid)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-451273/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451273
C5-C8 Aliphatics 15.0 14.59 mg/Kg 97 70-130 2 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C10 Aromatics 5.00 5.060 mg/Kg 101 70-130 0 25
C9-C12 Aliphatics 10.0 9.633 mg/Kg 96 70-130 0 25
2,5-Dibromotoluene (fid)70 -130
Surrogate
96
LCSD LCSD
Qualifier Limits%Recovery
922,5-Dibromotoluene (pid)70 -130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 490-450969/1-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451728 Prep Batch: 450969
RL MDL
C19-C36 Aliphatics <5.00 10.0 5.00 mg/Kg 08/08/17 10:20 08/10/17 17:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<2.40 2.4010.0 mg/Kg 08/08/17 10:20 08/10/17 17:30 1C9-C18 Aliphatics
1-Chlorooctadecane 56 40-140 08/10/17 17:30 1
MB MB
Surrogate
08/08/17 10:20
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 490-450969/1-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451732 Prep Batch: 450969
RL MDL
C11-C22 Aromatics <4.90 10.0 4.90 mg/Kg 08/08/17 10:20 08/10/17 17:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 64 40-140 08/10/17 17:10 1
MB MB
Surrogate
08/08/17 10:20
Dil FacPreparedAnalyzedQualifierLimits%Recovery
70 08/08/17 10:20 08/10/17 17:10 12-Fluorobiphenyl 40-140
68 08/08/17 10:20 08/10/17 17:10 12-Bromonaphthalene 40-140
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450969/2-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451728 Prep Batch: 450969
C19-C36 Aliphatics 20.0 16.23 mg/Kg 81 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C18 Aliphatics 15.0 10.41 mg/Kg 69 40-140
1-Chlorooctadecane 40 -140
Surrogate
61
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450969/2-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451732 Prep Batch: 450969
C11-C22 Aromatics 42.5 34.51 mg/Kg 81 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl 40 -140
Surrogate
71
LCS LCS
Qualifier Limits%Recovery
692-Fluorobiphenyl 40 -140
682-Bromonaphthalene 40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-450969/3-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451728 Prep Batch: 450969
C19-C36 Aliphatics 20.0 16.79 mg/Kg 84 40-140 3 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
C9-C18 Aliphatics 15.0 9.775 J mg/Kg 65 40-140 6 25
1-Chlorooctadecane 40 -140
Surrogate
59
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-450969/3-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451732 Prep Batch: 450969
C11-C22 Aromatics 42.5 37.78 mg/Kg 89 40-140 9 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
o-Terphenyl 40 -140
Surrogate
76
LCSD LCSD
Qualifier Limits%Recovery
752-Fluorobiphenyl 40 -140
742-Bromonaphthalene 40 -140
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-451323/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 452524 Prep Batch: 451323
RL MDL
Beryllium <0.202 1.01 0.202 mg/Kg 08/09/17 10:33 08/11/17 23:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.101 0.1011.01 mg/Kg 08/09/17 10:33 08/11/17 23:57 1Cadmium
<1.11 1.112.02 mg/Kg 08/09/17 10:33 08/11/17 23:57 1Copper
<0.505 0.5051.01 mg/Kg 08/09/17 10:33 08/11/17 23:57 1Lead
<1.01 1.013.03 mg/Kg 08/09/17 10:33 08/11/17 23:57 1Manganese
<0.606 0.6062.02 mg/Kg 08/09/17 10:33 08/11/17 23:57 1Nickel
<1.11 1.112.02 mg/Kg 08/09/17 10:33 08/11/17 23:57 1Selenium
<0.404 0.4041.01 mg/Kg 08/09/17 10:33 08/11/17 23:57 1Silver
Client Sample ID: Method BlankLab Sample ID: MB 490-451323/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 452571 Prep Batch: 451323
RL MDL
Chromium <0.909 1.01 0.909 mg/Kg 08/09/17 10:33 08/14/17 13:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<5.05 5.0510.1 mg/Kg 08/09/17 10:33 08/14/17 13:55 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-451323/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 452524 Prep Batch: 451323
Beryllium 19.6 18.86 mg/Kg 96 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Cadmium 19.6 18.49 mg/Kg 94 80-120
Chromium 19.6 19.04 mg/Kg 97 80-120
Copper 19.6 19.28 mg/Kg 98 80-120
Lead 19.6 18.92 mg/Kg 97 80-120
Manganese 19.6 20.02 mg/Kg 102 80-120
Nickel 19.6 19.14 mg/Kg 98 80-120
Selenium 19.6 18.22 mg/Kg 93 80-120
Silver 19.6 18.47 mg/Kg 94 80-120
Zinc 19.6 19.80 mg/Kg 101 80-120
Client Sample ID: Matrix SpikeLab Sample ID: 490-134168-F-1-C MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 452524 Prep Batch: 451323
Beryllium 0.307 J 21.9 20.36 mg/Kg 91 75-125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Cadmium <0.110 21.9 19.55 mg/Kg 89 75-125☼
Chromium 6.34 F2 F1 21.9 25.98 mg/Kg 89 75-125☼
Copper 5.31 21.9 23.28 mg/Kg 82 75-125☼
Lead 21.6 F1 21.9 32.89 F1 mg/Kg 52 75-125☼
Manganese 267 F2 21.9 128.1 4 mg/Kg -633 75-125☼
Nickel 3.80 21.9 23.57 mg/Kg 90 75-125☼
Selenium <1.21 21.9 18.67 mg/Kg 85 75-125☼
Silver 0.527 J 21.9 20.10 mg/Kg 89 75-125☼
Zinc 20.4 F1 F2 21.9 33.27 F1 mg/Kg 59 75-125☼
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-134168-F-1-D MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 452524 Prep Batch: 451323
Beryllium 0.307 J 22.6 21.23 mg/Kg 92 75-125 4 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Cadmium <0.110 22.6 19.83 mg/Kg 88 75-125 1 20☼
Chromium 6.34 F2 F1 22.6 43.43 F1 F2 mg/Kg 164 75-125 50 20☼
Copper 5.31 22.6 23.49 mg/Kg 80 75-125 1 20☼
Lead 21.6 F1 22.6 36.08 F1 mg/Kg 64 75-125 9 20☼
Manganese 267 F2 22.6 162.7 4 F2 mg/Kg -461 75-125 24 20☼
Nickel 3.80 22.6 28.56 mg/Kg 109 75-125 19 20☼
Selenium <1.21 22.6 18.29 mg/Kg 81 75-125 2 20☼
Silver 0.527 J 22.6 20.91 mg/Kg 90 75-125 4 20☼
Zinc 20.4 F1 F2 22.6 42.46 F2 mg/Kg 97 75-125 24 20☼
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-451524/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451992 Prep Batch: 451524
RL MDL
Antimony <0.200 0.500 0.200 mg/Kg 08/09/17 20:35 08/11/17 06:50 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.200 0.2000.500 mg/Kg 08/09/17 20:35 08/11/17 06:50 1Arsenic
<0.200 0.2000.500 mg/Kg 08/09/17 20:35 08/11/17 06:50 1Thallium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-451524/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451992 Prep Batch: 451524
Antimony 19.5 18.20 mg/Kg 94 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 19.5 18.20 mg/Kg 94 80-120
Thallium 19.5 19.25 mg/Kg 99 80-120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-451524/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451992 Prep Batch: 451524
Antimony 19.2 18.15 mg/Kg 95 80-120 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Arsenic 19.2 18.22 mg/Kg 95 80-120 0 20
Thallium 19.2 19.14 mg/Kg 100 80-120 1 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-134278-G-1-C MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451992 Prep Batch: 451524
Antimony <0.248 25.2 22.38 mg/Kg 89 75-125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 3.10 F1 25.2 21.14 F1 mg/Kg 72 75-125☼
Thallium 0.248 J 25.2 23.37 mg/Kg 92 75-125☼
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-134278-G-1-D MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451992 Prep Batch: 451524
Antimony <0.248 25.6 23.12 mg/Kg 90 75-125 3 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 3.10 F1 25.6 23.30 mg/Kg 79 75-125 10 20☼
Thallium 0.248 J 25.6 24.69 mg/Kg 95 75-125 6 20☼
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-451077/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451811 Prep Batch: 451077
RL MDL
Mercury <0.0300 0.100 0.0300 mg/Kg 08/08/17 14:17 08/10/17 08:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-451077/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451811 Prep Batch: 451077
Mercury 0.162 0.1431 mg/Kg 88 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-451077/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451811 Prep Batch: 451077
Mercury 0.164 0.1383 mg/Kg 84 80-120 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: SURF-EDGE-1Lab Sample ID: 490-134160-2 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451811 Prep Batch: 451077
Mercury 222 F2 0.214 235.3 4 mg/Kg 6190 80-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: SURF-EDGE-1Lab Sample ID: 490-134160-2 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451811 Prep Batch: 451077
Mercury 222 F2 0.214 125.7 J 4 F2 mg/Kg -4507
0
80-120 61 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method: Moisture - Percent Moisture
Client Sample ID: EI-EXC-E1Lab Sample ID: 490-134160-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 450989
Percent Moisture 21.5 20.0 %7 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 78.5 80.0 %2 20
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QC Association Summary
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
GC/MS Semi VOA
Prep Batch: 450963
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550C490-134160-1 EI-EXC-E1 Total/NA
Solid 3550C490-134160-2 SURF-EDGE-1 Total/NA
Solid 3550C490-134160-3 SURF-EDGE-2 Total/NA
Solid 3550C490-134160-4 SURF-EDGE-3 Total/NA
Solid 3550C490-134160-5 SURF-BASE-1 Total/NA
Solid 3550C490-134160-6 SURF-BASE-2 Total/NA
Solid 3550C490-134160-7 SURF-BASE-3 Total/NA
Solid 3550CMB 490-450963/1-A Method Blank Total/NA
Solid 3550CLCS 490-450963/2-A Lab Control Sample Total/NA
Solid 3550C490-134155-B-22-B MS Matrix Spike Total/NA
Solid 3550C490-134155-B-22-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 451551
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 450963490-134160-1 EI-EXC-E1 Total/NA
Solid 8270D 450963490-134160-2 SURF-EDGE-1 Total/NA
Solid 8270D 450963490-134160-3 SURF-EDGE-2 Total/NA
Solid 8270D 450963490-134160-4 SURF-EDGE-3 Total/NA
Solid 8270D 450963490-134160-5 SURF-BASE-1 Total/NA
Solid 8270D 450963490-134160-6 SURF-BASE-2 Total/NA
Solid 8270D 450963490-134160-7 SURF-BASE-3 Total/NA
Solid 8270D 450963MB 490-450963/1-A Method Blank Total/NA
Solid 8270D 450963LCS 490-450963/2-A Lab Control Sample Total/NA
Solid 8270D 450963490-134155-B-22-B MS Matrix Spike Total/NA
Solid 8270D 450963490-134155-B-22-C MSD Matrix Spike Duplicate Total/NA
GC VOA
Prep Batch: 450843
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035490-134160-1 EI-EXC-E1 Total/NA
Analysis Batch: 451273
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAVPH 450843490-134160-1 EI-EXC-E1 Total/NA
Solid MAVPHMB 490-451273/6 Method Blank Total/NA
Solid MAVPHLCS 490-451273/3 Lab Control Sample Total/NA
Solid MAVPHLCSD 490-451273/4 Lab Control Sample Dup Total/NA
Analysis Batch: 452035
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA VPH490-134160-1 EI-EXC-E1 Total/NA
GC Semi VOA
Prep Batch: 450969
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541490-134160-1 EI-EXC-E1 Total/NA
Solid 3541MB 490-450969/1-B Method Blank Total/NA
Solid 3541MB 490-450969/1-C Method Blank Total/NA
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QC Association Summary
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
GC Semi VOA (Continued)
Prep Batch: 450969 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541LCS 490-450969/2-B Lab Control Sample Total/NA
Solid 3541LCS 490-450969/2-C Lab Control Sample Total/NA
Solid 3541LCSD 490-450969/3-B Lab Control Sample Dup Total/NA
Solid 3541LCSD 490-450969/3-C Lab Control Sample Dup Total/NA
Fraction Batch: 451662
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA EPH Frac 450969490-134160-1 EI-EXC-E1 Total/NA
Solid MA EPH Frac 450969490-134160-1 EI-EXC-E1 Total/NA
Solid MA EPH Frac 450969MB 490-450969/1-B Method Blank Total/NA
Solid MA EPH Frac 450969MB 490-450969/1-C Method Blank Total/NA
Solid MA EPH Frac 450969LCS 490-450969/2-B Lab Control Sample Total/NA
Solid MA EPH Frac 450969LCS 490-450969/2-C Lab Control Sample Total/NA
Solid MA EPH Frac 450969LCSD 490-450969/3-B Lab Control Sample Dup Total/NA
Solid MA EPH Frac 450969LCSD 490-450969/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 451728
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA-EPH 451662490-134160-1 EI-EXC-E1 Total/NA
Solid MA-EPH 451662MB 490-450969/1-B Method Blank Total/NA
Solid MA-EPH 451662LCS 490-450969/2-B Lab Control Sample Total/NA
Solid MA-EPH 451662LCSD 490-450969/3-B Lab Control Sample Dup Total/NA
Analysis Batch: 451732
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA-EPH 451662490-134160-1 EI-EXC-E1 Total/NA
Solid MA-EPH 451662MB 490-450969/1-C Method Blank Total/NA
Solid MA-EPH 451662LCS 490-450969/2-C Lab Control Sample Total/NA
Solid MA-EPH 451662LCSD 490-450969/3-C Lab Control Sample Dup Total/NA
Metals
Prep Batch: 451077
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B490-134160-2 SURF-EDGE-1 Total/NA
Solid 7471B490-134160-3 SURF-EDGE-2 Total/NA
Solid 7471B490-134160-4 SURF-EDGE-3 Total/NA
Solid 7471B490-134160-5 SURF-BASE-1 Total/NA
Solid 7471B490-134160-6 SURF-BASE-2 Total/NA
Solid 7471B490-134160-7 SURF-BASE-3 Total/NA
Solid 7471BMB 490-451077/1-A Method Blank Total/NA
Solid 7471BLCS 490-451077/2-A Lab Control Sample Total/NA
Solid 7471BLCSD 490-451077/3-A Lab Control Sample Dup Total/NA
Solid 7471B490-134160-2 MS SURF-EDGE-1 Total/NA
Solid 7471B490-134160-2 MSD SURF-EDGE-1 Total/NA
Prep Batch: 451323
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3051A490-134160-2 SURF-EDGE-1 Total/NA
Solid 3051A490-134160-3 SURF-EDGE-2 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Metals (Continued)
Prep Batch: 451323 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3051A490-134160-4 SURF-EDGE-3 Total/NA
Solid 3051A490-134160-5 SURF-BASE-1 Total/NA
Solid 3051A490-134160-6 SURF-BASE-2 Total/NA
Solid 3051A490-134160-7 SURF-BASE-3 Total/NA
Solid 3051AMB 490-451323/1-A Method Blank Total/NA
Solid 3051ALCS 490-451323/2-A Lab Control Sample Total/NA
Solid 3051A490-134168-F-1-C MS Matrix Spike Total/NA
Solid 3051A490-134168-F-1-D MSD Matrix Spike Duplicate Total/NA
Prep Batch: 451524
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3051A490-134160-2 SURF-EDGE-1 Total/NA
Solid 3051A490-134160-3 SURF-EDGE-2 Total/NA
Solid 3051A490-134160-4 SURF-EDGE-3 Total/NA
Solid 3051A490-134160-5 SURF-BASE-1 Total/NA
Solid 3051A490-134160-6 SURF-BASE-2 Total/NA
Solid 3051A490-134160-7 SURF-BASE-3 Total/NA
Solid 3051AMB 490-451524/1-A Method Blank Total/NA
Solid 3051ALCS 490-451524/2-A Lab Control Sample Total/NA
Solid 3051ALCSD 490-451524/3-A Lab Control Sample Dup Total/NA
Solid 3051A490-134278-G-1-C MS Matrix Spike Total/NA
Solid 3051A490-134278-G-1-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 451811
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B 451077490-134160-2 SURF-EDGE-1 Total/NA
Solid 7471B 451077490-134160-3 SURF-EDGE-2 Total/NA
Solid 7471B 451077490-134160-4 SURF-EDGE-3 Total/NA
Solid 7471B 451077490-134160-5 SURF-BASE-1 Total/NA
Solid 7471B 451077490-134160-6 SURF-BASE-2 Total/NA
Solid 7471B 451077490-134160-7 SURF-BASE-3 Total/NA
Solid 7471B 451077MB 490-451077/1-A Method Blank Total/NA
Solid 7471B 451077LCS 490-451077/2-A Lab Control Sample Total/NA
Solid 7471B 451077LCSD 490-451077/3-A Lab Control Sample Dup Total/NA
Solid 7471B 451077490-134160-2 MS SURF-EDGE-1 Total/NA
Solid 7471B 451077490-134160-2 MSD SURF-EDGE-1 Total/NA
Analysis Batch: 451992
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020B 451524490-134160-3 SURF-EDGE-2 Total/NA
Solid 6020B 451524490-134160-5 SURF-BASE-1 Total/NA
Solid 6020B 451524490-134160-6 SURF-BASE-2 Total/NA
Solid 6020B 451524MB 490-451524/1-A Method Blank Total/NA
Solid 6020B 451524LCS 490-451524/2-A Lab Control Sample Total/NA
Solid 6020B 451524LCSD 490-451524/3-A Lab Control Sample Dup Total/NA
Solid 6020B 451524490-134278-G-1-C MS Matrix Spike Total/NA
Solid 6020B 451524490-134278-G-1-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 452204
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020B 451524490-134160-2 SURF-EDGE-1 Total/NA
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QC Association Summary
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Metals (Continued)
Analysis Batch: 452204 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020B 451524490-134160-3 SURF-EDGE-2 Total/NA
Solid 6020B 451524490-134160-4 SURF-EDGE-3 Total/NA
Solid 6020B 451524490-134160-5 SURF-BASE-1 Total/NA
Solid 6020B 451524490-134160-6 SURF-BASE-2 Total/NA
Solid 6020B 451524490-134160-7 SURF-BASE-3 Total/NA
Analysis Batch: 452524
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010D 451323490-134160-2 SURF-EDGE-1 Total/NA
Solid 6010D 451323490-134160-3 SURF-EDGE-2 Total/NA
Solid 6010D 451323490-134160-4 SURF-EDGE-3 Total/NA
Solid 6010D 451323490-134160-5 SURF-BASE-1 Total/NA
Solid 6010D 451323490-134160-6 SURF-BASE-2 Total/NA
Solid 6010D 451323490-134160-7 SURF-BASE-3 Total/NA
Solid 6010D 451323MB 490-451323/1-A Method Blank Total/NA
Solid 6010D 451323LCS 490-451323/2-A Lab Control Sample Total/NA
Solid 6010D 451323490-134168-F-1-C MS Matrix Spike Total/NA
Solid 6010D 451323490-134168-F-1-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 452571
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010D 451323MB 490-451323/1-A Method Blank Total/NA
General Chemistry
Analysis Batch: 450989
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-134160-1 EI-EXC-E1 Total/NA
Solid Moisture490-134160-2 SURF-EDGE-1 Total/NA
Solid Moisture490-134160-3 SURF-EDGE-2 Total/NA
Solid Moisture490-134160-4 SURF-EDGE-3 Total/NA
Solid Moisture490-134160-5 SURF-BASE-1 Total/NA
Solid Moisture490-134160-6 SURF-BASE-2 Total/NA
Solid Moisture490-134160-7 SURF-BASE-3 Total/NA
Solid Moisture490-134160-1 DU EI-EXC-E1 Total/NA
TestAmerica Nashville
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Lab Chronicle
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134160-1
Project/Site: Eagle Island
Client Sample ID: EI-EXC-E1 Lab Sample ID: 490-134160-1
Matrix: SolidDate Collected: 08/04/17 11:15
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 11:151 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: EI-EXC-E1 Lab Sample ID: 490-134160-1
Matrix: SolidDate Collected: 08/04/17 11:15
Percent Solids: 78.5Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.85 g 1.00 mL
Analysis 8270D 1 451551 08/10/17 12:23 ZLN TAL NSHTotal/NA
Analysis MA VPH 1 452035 08/11/17 11:23 FKG TAL NSHTotal/NA
Prep 5035 450843 08/04/17 10:15 JLP TAL NSHTotal/NA 5.459 g 5.0 mL
Analysis MAVPH 1 451273 08/09/17 19:40 S1S TAL NSHTotal/NA 0.1 mL 5 mL
Prep 3541 450969 08/08/17 10:20 ZXS TAL NSHTotal/NA 10.16 g 2 mL
Fraction MA EPH Frac 451662 08/10/17 10:40 ZXS TAL NSHTotal/NA 2 mL 1 mL
Analysis MA-EPH 1 451732 08/10/17 21:53 A1B TAL NSHTotal/NA
Prep 3541 450969 08/08/17 10:20 ZXS TAL NSHTotal/NA 10.16 g 2 mL
Fraction MA EPH Frac 451662 08/10/17 10:40 ZXS TAL NSHTotal/NA 2 mL 1 mL
Analysis MA-EPH 1 451728 08/10/17 22:01 A1B TAL NSHTotal/NA
Client Sample ID: SURF-EDGE-1 Lab Sample ID: 490-134160-2
Matrix: SolidDate Collected: 08/04/17 10:05
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 11:151 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SURF-EDGE-1 Lab Sample ID: 490-134160-2
Matrix: SolidDate Collected: 08/04/17 10:05
Percent Solids: 76.5Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.09 g 1.00 mL
Analysis 8270D 5 451551 08/10/17 14:38 ZLN TAL NSHTotal/NA
Prep 3051A 451323 08/09/17 10:33 BVH TAL NSHTotal/NA 0.501 g 100 mL
Analysis 6010D 1 452524 08/12/17 00:32 LCS TAL NSHTotal/NA
Prep 3051A 451524 08/09/17 20:35 BVH TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6020B 1 452204 08/11/17 17:39 BLG TAL NSHTotal/NA
Prep 7471B 451077 08/08/17 14:17 RDF TAL NSHTotal/NA 0.609 g 100 mL
Analysis 7471B 1000 451811 08/10/17 08:32 JLJ TAL NSHTotal/NA
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Lab Chronicle
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134160-1
Project/Site: Eagle Island
Client Sample ID: SURF-EDGE-2 Lab Sample ID: 490-134160-3
Matrix: SolidDate Collected: 08/04/17 10:20
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 11:151 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SURF-EDGE-2 Lab Sample ID: 490-134160-3
Matrix: SolidDate Collected: 08/04/17 10:20
Percent Solids: 83.2Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.81 g 1.00 mL
Analysis 8270D 1 451551 08/10/17 14:58 ZLN TAL NSHTotal/NA
Prep 3051A 451323 08/09/17 10:33 BVH TAL NSHTotal/NA 0.508 g 100 mL
Analysis 6010D 1 452524 08/12/17 00:37 LCS TAL NSHTotal/NA
Prep 3051A 451524 08/09/17 20:35 BVH TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6020B 5 451992 08/11/17 07:40 BLG TAL NSHTotal/NA
Prep 3051A 451524 08/09/17 20:35 BVH TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6020B 1 452204 08/11/17 17:45 BLG TAL NSHTotal/NA
Prep 7471B 451077 08/08/17 14:17 RDF TAL NSHTotal/NA 0.605 g 100 mL
Analysis 7471B 1 451811 08/10/17 08:40 JLJ TAL NSHTotal/NA
Client Sample ID: SURF-EDGE-3 Lab Sample ID: 490-134160-4
Matrix: SolidDate Collected: 08/04/17 10:50
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 11:151 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SURF-EDGE-3 Lab Sample ID: 490-134160-4
Matrix: SolidDate Collected: 08/04/17 10:50
Percent Solids: 85.1Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.15 g 1.00 mL
Analysis 8270D 1 451551 08/10/17 15:17 ZLN TAL NSHTotal/NA
Prep 3051A 451323 08/09/17 11:09 BVH TAL NSHTotal/NA 0.511 g 100 mL
Analysis 6010D 1 452524 08/12/17 02:10 LCS TAL NSHTotal/NA
Prep 3051A 451524 08/09/17 20:35 BVH TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6020B 1 452204 08/11/17 17:50 BLG TAL NSHTotal/NA
Prep 7471B 451077 08/08/17 14:17 RDF TAL NSHTotal/NA 0.617 g 100 mL
Analysis 7471B 1 451811 08/10/17 08:43 JLJ TAL NSHTotal/NA
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Lab Chronicle
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134160-1
Project/Site: Eagle Island
Client Sample ID: SURF-BASE-1 Lab Sample ID: 490-134160-5
Matrix: SolidDate Collected: 08/04/17 11:30
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 11:151 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SURF-BASE-1 Lab Sample ID: 490-134160-5
Matrix: SolidDate Collected: 08/04/17 11:30
Percent Solids: 62.6Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.22 g 1.00 mL
Analysis 8270D 1 451551 08/10/17 15:36 ZLN TAL NSHTotal/NA
Prep 3051A 451323 08/09/17 10:33 BVH TAL NSHTotal/NA 0.503 g 100 mL
Analysis 6010D 1 452524 08/12/17 00:53 LCS TAL NSHTotal/NA
Prep 3051A 451524 08/09/17 20:35 BVH TAL NSHTotal/NA 0.515 g 100 mL
Analysis 6020B 5 451992 08/11/17 08:02 BLG TAL NSHTotal/NA
Prep 3051A 451524 08/09/17 20:35 BVH TAL NSHTotal/NA 0.515 g 100 mL
Analysis 6020B 1 452204 08/11/17 17:56 BLG TAL NSHTotal/NA
Prep 7471B 451077 08/08/17 14:17 RDF TAL NSHTotal/NA 0.620 g 100 mL
Analysis 7471B 1 451811 08/10/17 08:45 JLJ TAL NSHTotal/NA
Client Sample ID: SURF-BASE-2 Lab Sample ID: 490-134160-6
Matrix: SolidDate Collected: 08/04/17 11:45
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 11:151 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SURF-BASE-2 Lab Sample ID: 490-134160-6
Matrix: SolidDate Collected: 08/04/17 11:45
Percent Solids: 74.6Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.37 g 1.00 mL
Analysis 8270D 5 451551 08/10/17 15:56 ZLN TAL NSHTotal/NA
Prep 3051A 451323 08/09/17 10:33 BVH TAL NSHTotal/NA 0.521 g 100 mL
Analysis 6010D 1 452524 08/12/17 00:58 LCS TAL NSHTotal/NA
Prep 3051A 451524 08/09/17 20:35 BVH TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6020B 5 451992 08/11/17 08:07 BLG TAL NSHTotal/NA
Prep 3051A 451524 08/09/17 20:35 BVH TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6020B 1 452204 08/11/17 18:01 BLG TAL NSHTotal/NA
Prep 7471B 451077 08/08/17 14:17 RDF TAL NSHTotal/NA 0.619 g 100 mL
Analysis 7471B 1 451811 08/10/17 08:48 JLJ TAL NSHTotal/NA
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Lab Chronicle
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134160-1
Project/Site: Eagle Island
Client Sample ID: SURF-BASE-3 Lab Sample ID: 490-134160-7
Matrix: SolidDate Collected: 08/04/17 12:05
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 11:151 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SURF-BASE-3 Lab Sample ID: 490-134160-7
Matrix: SolidDate Collected: 08/04/17 12:05
Percent Solids: 72.4Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.86 g 1.00 mL
Analysis 8270D 1 451551 08/10/17 16:15 ZLN TAL NSHTotal/NA
Prep 3051A 451323 08/09/17 10:33 BVH TAL NSHTotal/NA 0.505 g 100 mL
Analysis 6010D 1 452524 08/12/17 01:03 LCS TAL NSHTotal/NA
Prep 3051A 451524 08/09/17 20:35 BVH TAL NSHTotal/NA 0.508 g 100 mL
Analysis 6020B 1 452204 08/11/17 18:07 BLG TAL NSHTotal/NA
Prep 7471B 451077 08/08/17 14:17 RDF TAL NSHTotal/NA 0.600 g 100 mL
Analysis 7471B 1 451811 08/10/17 08:56 JLJ TAL NSHTotal/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-134160-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island
Method Method Description LaboratoryProtocol
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
MA DEPMA VPH Massachusetts - Volatile Petroleum Hydrocarbons (GC)TAL NSH
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)TAL NSH
MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467471BMercury (CVAA)TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Accreditation/Certification Summary
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134160-1
Project/Site: Eagle Island
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3874State Program 12-31-17
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
MA VPH Solid C9-C12 Aliphatics (North Carolina)
Moisture Solid Percent Moisture
Moisture Solid Percent Solids
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Login Sample Receipt Checklist
Client: Geosyntec Consultants, Inc.Job Number: 490-134160-1
Login Number: 134160
Question Answer Comment
Creator: Huskey, Adam
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-134180-1
TestAmerica Sample Delivery Group: GN6353
Client Project/Site: Eagle Island Remediation
For:
Geosyntec Consultants, Inc.
2501 Blue Ridge Rd.
Suite 430
Raleigh, North Carolina 27607
Attn: Ms. Kaitlyn S Rhonehouse
Authorized for release by:
8/18/2017 5:21:23 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Remediation
TestAmerica Job ID: 490-134180-1
SDG: GN6353
Page 2 of 32 TestAmerica Nashville8/18/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
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Sample Summary
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-134180-1 EI-EXC-N1 Solid 08/03/17 15:33 08/05/17 10:00
490-134180-2 EI-EXC-S1 Solid 08/03/17 15:58 08/05/17 10:00
490-134180-3 EI-EXC-W1 Solid 08/03/17 16:22 08/05/17 10:00
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Case Narrative
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134180-1
Project/Site: Eagle Island Remediation SDG: GN6353
Job ID: 490-134180-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-134180-1
Comments
No additional comments.
Receipt
The samples were received on 8/5/2017 10:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 4.8º C.
GC/MS Semi VOA
Method 8270D: The continuing calibration verification (CCVIS) associated with batch 490-451551 recovered above the upper control limit
for 2,4-Dinitrophenol, 2,6-Dinitrotoluene and 2-Nitrophenol. The samples associated with this CCVIS were non-detect for the affected
analytes; therefore, the data has been reported. The following sample is impacted: (CCVIS 490-451551/3).
Method 8270D: The continuing calibration verification (CCVIS) analyzed in batch 490-451551 was outside the method criteria for
2,2'oxybis[1-chloropropane]. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is
considered estimated.
Method 8270D: The laboratory control sample (LCS) for preparation batch 490-450963 and analytical batch 490-451551 recovered outside
control limits for Hexachlorocyclopentadiene. This target analyte has been identified as poor performing when analyzed using this
method; therefore, re-extraction/re-analysis was not performed. These results have been reported and qualified.
Method 8270D: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 490-450963 and
analytical batch 490-451551 were outside control limits for Hexachlorocyclopentadiene. This target analyte has been identified as poor
performing when analyzed using this method; therefore, re-extraction/re-analysis was not performed. These results have been reported
and qualified.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Qualifiers
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
*LCS or LCSD is outside acceptance limits.
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID: 490-134180-1Client Sample ID: EI-EXC-N1
Matrix: SolidDate Collected: 08/03/17 15:33
Percent Solids: 64.6Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0480 0.101 0.0480 mg/Kg ☼08/08/17 10:12 08/10/17 16:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.101 0.0435 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Acenaphthylene <0.0435
0.101 0.0435 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Anthracene <0.0435
0.101 0.0450 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Benzo[a]anthracene <0.0450
0.101 0.0405 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Benzo[a]pyrene 0.0674 J
0.101 0.0420 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Benzo[b]fluoranthene <0.0420
0.101 0.0495 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Benzo[g,h,i]perylene <0.0495
0.101 0.0405 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Benzo[k]fluoranthene <0.0405
0.500 0.300 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Bis(2-chloroethoxy)methane <0.300
0.500 0.320 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Bis(2-chloroethyl)ether <0.320
0.500 0.297 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼bis (2-chloroisopropyl) ether <0.297
0.500 0.311 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Bis(2-ethylhexyl) phthalate <0.311
0.500 0.308 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼4-Bromophenyl phenyl ether <0.308
0.500 0.323 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Butyl benzyl phthalate <0.323
0.500 0.311 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Carbazole <0.311
0.500 0.341 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼4-Chloroaniline <0.341
0.500 0.252 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼4-Chloro-3-methylphenol <0.252
0.500 0.314 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2-Chloronaphthalene <0.314
0.500 0.287 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2-Chlorophenol <0.287
0.500 0.302 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼4-Chlorophenyl phenyl ether <0.302
0.101 0.0555 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Chrysene <0.0555
0.999 0.170 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Cresols <0.170
0.101 0.0480 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Dibenz(a,h)anthracene <0.0480
0.500 0.315 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Dibenzofuran <0.315
0.500 0.285 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼1,2-Dichlorobenzene <0.285
0.500 0.285 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼1,3-Dichlorobenzene <0.285
0.500 0.294 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼1,4-Dichlorobenzene <0.294
1.01 0.306 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼3,3'-Dichlorobenzidine <0.306
0.500 0.263 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2,4-Dichlorophenol <0.263
0.500 0.318 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Diethyl phthalate <0.318
1.01 0.503 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2,4-Dimethylphenol <0.503
0.500 0.311 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Dimethyl phthalate <0.311
0.500 0.317 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Di-n-butyl phthalate <0.317
0.500 0.344 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼4,6-Dinitro-2-methylphenol <0.344
0.500 0.377 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2,4-Dinitrophenol <0.377
0.500 0.312 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2,4-Dinitrotoluene <0.312
0.500 0.335 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2,6-Dinitrotoluene <0.335
0.500 0.267 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Di-n-octyl phthalate <0.267
0.101 0.0510 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Fluoranthene <0.0510
0.101 0.0435 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Fluorene <0.0435
0.500 0.375 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Hexachlorobenzene <0.375
0.500 0.251 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Hexachlorobutadiene <0.251
0.500 0.225 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Hexachlorocyclopentadiene <0.225 *
0.500 0.272 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Hexachloroethane <0.272
0.101 0.0435 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Indeno[1,2,3-cd]pyrene <0.0435
0.500 0.282 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Isophorone <0.282
0.101 0.0420 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼1-Methylnaphthalene <0.0420
0.101 0.0390 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2-Methylnaphthalene <0.0390
0.500 0.324 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2-Methylphenol <0.324
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Client Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID: 490-134180-1Client Sample ID: EI-EXC-N1
Matrix: SolidDate Collected: 08/03/17 15:33
Percent Solids: 64.6Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <0.305 0.500 0.305 mg/Kg ☼08/08/17 10:12 08/10/17 16:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.101 0.0435 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Naphthalene <0.0435
0.500 0.311 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2-Nitroaniline <0.311
1.01 0.345 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼3-Nitroaniline <0.345
1.01 0.357 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼4-Nitroaniline <0.357
0.500 0.302 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Nitrobenzene <0.302
0.500 0.365 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2-Nitrophenol <0.365
1.01 0.573 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼4-Nitrophenol <0.573
0.500 0.291 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼N-Nitrosodi-n-propylamine <0.291
0.500 0.0795 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0795
1.01 0.399 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Pentachlorophenol <0.399
0.101 0.0510 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Phenanthrene <0.0510
0.500 0.305 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Phenol <0.305
0.101 0.0510 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼Pyrene <0.0510
0.500 0.272 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼1,2,4-Trichlorobenzene <0.272
0.500 0.327 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2,4,5-Trichlorophenol <0.327
0.500 0.288 mg/Kg 08/08/17 10:12 08/10/17 16:34 1☼2,4,6-Trichlorophenol <0.288
2-Fluorobiphenyl (Surr)67 29-120 08/08/17 10:12 08/10/17 16:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)55 08/08/17 10:12 08/10/17 16:34 110-120
Nitrobenzene-d5 (Surr)61 08/08/17 10:12 08/10/17 16:34 127-120
Phenol-d5 (Surr)60 08/08/17 10:12 08/10/17 16:34 110-120
Terphenyl-d14 (Surr)87 08/08/17 10:12 08/10/17 16:34 113-120
2,4,6-Tribromophenol (Surr)88 08/08/17 10:12 08/10/17 16:34 110-120
Method: MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C9-C12 Aliphatics (North Carolina)8.67 7.74 3.87 mg/Kg ☼08/11/17 11:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics <5.26 10.1 5.26 mg/Kg ☼08/03/17 14:33 08/09/17 22:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.1 6.07 mg/Kg 08/03/17 14:33 08/09/17 22:20 1☼C9-C10 Aromatics <6.07
10.1 5.06 mg/Kg 08/03/17 14:33 08/09/17 22:20 1☼C9-C12 Aliphatics 8.67 J
2,5-Dibromotoluene (fid)93 70-130 08/03/17 14:33 08/09/17 22:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2,5-Dibromotoluene (pid)92 08/03/17 14:33 08/09/17 22:20 170-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C19-C36 Aliphatics <7.48 15.0 7.48 mg/Kg ☼08/08/17 10:20 08/10/17 22:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15.0 3.59 mg/Kg 08/08/17 10:20 08/10/17 22:26 1☼C9-C18 Aliphatics <3.59
15.0 7.33 mg/Kg 08/08/17 10:20 08/11/17 09:15 1☼C11-C22 Aromatics 11.3 J
1-Chlorooctadecane 55 40-140 08/08/17 10:20 08/10/17 22:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o-Terphenyl 65 08/08/17 10:20 08/11/17 09:15 140-140
2-Fluorobiphenyl 65 08/08/17 10:20 08/11/17 09:15 140-140
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Client Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID: 490-134180-1Client Sample ID: EI-EXC-N1
Matrix: SolidDate Collected: 08/03/17 15:33
Percent Solids: 64.6Date Received: 08/05/17 10:00
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
2-Bromonaphthalene 64 40-140 08/08/17 10:20 08/11/17 09:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL RL
Percent Moisture 35.4 0.1 0.1 %08/08/17 10:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 10:52 1Percent Solids 64.6
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Client Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID: 490-134180-2Client Sample ID: EI-EXC-S1
Matrix: SolidDate Collected: 08/03/17 15:58
Percent Solids: 83.0Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0378 0.0792 0.0378 mg/Kg ☼08/08/17 10:12 08/10/17 16:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0792 0.0343 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Acenaphthylene <0.0343
0.0792 0.0343 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Anthracene <0.0343
0.0792 0.0355 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Benzo[a]anthracene 0.319
0.0792 0.0319 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Benzo[a]pyrene 0.311
0.0792 0.0331 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Benzo[b]fluoranthene 0.416
0.0792 0.0390 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Benzo[g,h,i]perylene 0.238
0.0792 0.0319 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Benzo[k]fluoranthene 0.220
0.394 0.237 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Bis(2-chloroethoxy)methane <0.237
0.394 0.252 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Bis(2-chloroethyl)ether <0.252
0.394 0.234 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼bis (2-chloroisopropyl) ether <0.234
0.394 0.245 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Bis(2-ethylhexyl) phthalate <0.245
0.394 0.242 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼4-Bromophenyl phenyl ether <0.242
0.394 0.254 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Butyl benzyl phthalate <0.254
0.394 0.245 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Carbazole <0.245
0.394 0.268 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼4-Chloroaniline <0.268
0.394 0.199 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼4-Chloro-3-methylphenol <0.199
0.394 0.247 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2-Chloronaphthalene <0.247
0.394 0.226 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2-Chlorophenol <0.226
0.394 0.238 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼4-Chlorophenyl phenyl ether <0.238
0.0792 0.0438 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Chrysene 0.321
0.788 0.134 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Cresols <0.134
0.0792 0.0378 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Dibenz(a,h)anthracene 0.0540 J
0.394 0.248 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Dibenzofuran <0.248
0.394 0.225 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼1,2-Dichlorobenzene <0.225
0.394 0.225 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼1,3-Dichlorobenzene <0.225
0.394 0.232 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼1,4-Dichlorobenzene <0.232
0.792 0.241 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼3,3'-Dichlorobenzidine <0.241
0.394 0.207 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2,4-Dichlorophenol <0.207
0.394 0.251 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Diethyl phthalate <0.251
0.792 0.396 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2,4-Dimethylphenol <0.396
0.394 0.245 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Dimethyl phthalate <0.245
0.394 0.250 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Di-n-butyl phthalate <0.250
0.394 0.271 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼4,6-Dinitro-2-methylphenol <0.271
0.394 0.297 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2,4-Dinitrophenol <0.297
0.394 0.246 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2,4-Dinitrotoluene <0.246
0.394 0.264 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2,6-Dinitrotoluene <0.264
0.394 0.211 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Di-n-octyl phthalate <0.211
0.0792 0.0402 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Fluoranthene 0.399
0.0792 0.0343 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Fluorene <0.0343
0.394 0.296 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Hexachlorobenzene <0.296
0.394 0.198 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Hexachlorobutadiene <0.198
0.394 0.177 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Hexachlorocyclopentadiene <0.177 *
0.394 0.214 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Hexachloroethane <0.214
0.0792 0.0343 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Indeno[1,2,3-cd]pyrene 0.176
0.394 0.222 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Isophorone <0.222
0.0792 0.0331 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼1-Methylnaphthalene <0.0331
0.0792 0.0308 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2-Methylnaphthalene <0.0308
0.394 0.255 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2-Methylphenol <0.255
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Client Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID: 490-134180-2Client Sample ID: EI-EXC-S1
Matrix: SolidDate Collected: 08/03/17 15:58
Percent Solids: 83.0Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <0.240 0.394 0.240 mg/Kg ☼08/08/17 10:12 08/10/17 16:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0792 0.0343 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Naphthalene <0.0343
0.394 0.245 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2-Nitroaniline <0.245
0.792 0.272 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼3-Nitroaniline <0.272
0.792 0.281 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼4-Nitroaniline <0.281
0.394 0.238 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Nitrobenzene <0.238
0.394 0.287 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2-Nitrophenol <0.287
0.792 0.452 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼4-Nitrophenol <0.452
0.394 0.229 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼N-Nitrosodi-n-propylamine <0.229
0.394 0.0627 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0627
0.792 0.315 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Pentachlorophenol <0.315
0.0792 0.0402 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Phenanthrene 0.0596 J
0.394 0.240 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Phenol <0.240
0.0792 0.0402 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼Pyrene 0.402
0.394 0.214 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼1,2,4-Trichlorobenzene <0.214
0.394 0.258 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2,4,5-Trichlorophenol <0.258
0.394 0.227 mg/Kg 08/08/17 10:12 08/10/17 16:54 1☼2,4,6-Trichlorophenol <0.227
2-Fluorobiphenyl (Surr)74 29-120 08/08/17 10:12 08/10/17 16:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)55 08/08/17 10:12 08/10/17 16:54 110-120
Nitrobenzene-d5 (Surr)66 08/08/17 10:12 08/10/17 16:54 127-120
Phenol-d5 (Surr)62 08/08/17 10:12 08/10/17 16:54 110-120
Terphenyl-d14 (Surr)92 08/08/17 10:12 08/10/17 16:54 113-120
2,4,6-Tribromophenol (Surr)87 08/08/17 10:12 08/10/17 16:54 110-120
Method: MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C9-C12 Aliphatics (North Carolina)5.70 J 6.02 3.01 mg/Kg ☼08/11/17 11:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics <3.42 6.57 3.42 mg/Kg ☼08/03/17 14:58 08/09/17 22:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.57 3.94 mg/Kg 08/03/17 14:58 08/09/17 22:52 1☼C9-C10 Aromatics <3.94
6.57 3.29 mg/Kg 08/03/17 14:58 08/09/17 22:52 1☼C9-C12 Aliphatics 5.70 J
2,5-Dibromotoluene (fid)94 70-130 08/03/17 14:58 08/09/17 22:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2,5-Dibromotoluene (pid)90 08/03/17 14:58 08/09/17 22:52 170-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C19-C36 Aliphatics 10.7 J 11.1 5.57 mg/Kg ☼08/08/17 10:20 08/10/17 22:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
11.1 2.67 mg/Kg 08/08/17 10:20 08/10/17 22:51 1☼C9-C18 Aliphatics <2.67
11.1 5.46 mg/Kg 08/08/17 10:20 08/10/17 22:44 1☼C11-C22 Aromatics <5.46
1-Chlorooctadecane 54 40-140 08/08/17 10:20 08/10/17 22:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o-Terphenyl 65 08/08/17 10:20 08/10/17 22:44 140-140
2-Fluorobiphenyl 71 08/08/17 10:20 08/10/17 22:44 140-140
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Client Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID: 490-134180-2Client Sample ID: EI-EXC-S1
Matrix: SolidDate Collected: 08/03/17 15:58
Percent Solids: 83.0Date Received: 08/05/17 10:00
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
2-Bromonaphthalene 71 40-140 08/08/17 10:20 08/10/17 22:44 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL RL
Percent Moisture 17.0 0.1 0.1 %08/08/17 10:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 10:52 1Percent Solids 83.0
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Client Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID: 490-134180-3Client Sample ID: EI-EXC-W1
Matrix: SolidDate Collected: 08/03/17 16:22
Percent Solids: 76.1Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0418 0.0874 0.0418 mg/Kg ☼08/08/17 10:12 08/10/17 17:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0874 0.0378 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Acenaphthylene <0.0378
0.0874 0.0378 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Anthracene <0.0378
0.0874 0.0391 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Benzo[a]anthracene <0.0391
0.0874 0.0352 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Benzo[a]pyrene 0.0518 J
0.0874 0.0365 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Benzo[b]fluoranthene <0.0365
0.0874 0.0431 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Benzo[g,h,i]perylene <0.0431
0.0874 0.0352 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Benzo[k]fluoranthene <0.0352
0.435 0.261 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Bis(2-chloroethoxy)methane <0.261
0.435 0.278 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Bis(2-chloroethyl)ether <0.278
0.435 0.258 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼bis (2-chloroisopropyl) ether <0.258
0.435 0.270 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Bis(2-ethylhexyl) phthalate <0.270
0.435 0.268 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼4-Bromophenyl phenyl ether <0.268
0.435 0.281 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Butyl benzyl phthalate <0.281
0.435 0.270 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Carbazole <0.270
0.435 0.296 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼4-Chloroaniline <0.296
0.435 0.219 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼4-Chloro-3-methylphenol <0.219
0.435 0.273 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2-Chloronaphthalene <0.273
0.435 0.249 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2-Chlorophenol <0.249
0.435 0.262 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼4-Chlorophenyl phenyl ether <0.262
0.0874 0.0483 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Chrysene <0.0483
0.869 0.147 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Cresols <0.147
0.0874 0.0418 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Dibenz(a,h)anthracene <0.0418
0.435 0.274 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Dibenzofuran <0.274
0.435 0.248 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼1,2-Dichlorobenzene <0.248
0.435 0.248 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼1,3-Dichlorobenzene <0.248
0.435 0.256 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼1,4-Dichlorobenzene <0.256
0.874 0.266 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼3,3'-Dichlorobenzidine <0.266
0.435 0.228 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2,4-Dichlorophenol <0.228
0.435 0.277 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Diethyl phthalate <0.277
0.874 0.437 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2,4-Dimethylphenol <0.437
0.435 0.270 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Dimethyl phthalate <0.270
0.435 0.275 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Di-n-butyl phthalate <0.275
0.435 0.299 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼4,6-Dinitro-2-methylphenol <0.299
0.435 0.328 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2,4-Dinitrophenol <0.328
0.435 0.271 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2,4-Dinitrotoluene <0.271
0.435 0.291 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2,6-Dinitrotoluene <0.291
0.435 0.232 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Di-n-octyl phthalate <0.232
0.0874 0.0444 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Fluoranthene <0.0444
0.0874 0.0378 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Fluorene <0.0378
0.435 0.326 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Hexachlorobenzene <0.326
0.435 0.218 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Hexachlorobutadiene <0.218
0.435 0.196 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Hexachlorocyclopentadiene <0.196 *
0.435 0.236 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Hexachloroethane <0.236
0.0874 0.0378 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Indeno[1,2,3-cd]pyrene <0.0378
0.435 0.245 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Isophorone <0.245
0.0874 0.0365 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼1-Methylnaphthalene <0.0365
0.0874 0.0339 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2-Methylnaphthalene <0.0339
0.435 0.282 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2-Methylphenol <0.282
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Client Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID: 490-134180-3Client Sample ID: EI-EXC-W1
Matrix: SolidDate Collected: 08/03/17 16:22
Percent Solids: 76.1Date Received: 08/05/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <0.265 0.435 0.265 mg/Kg ☼08/08/17 10:12 08/10/17 17:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0874 0.0378 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Naphthalene <0.0378
0.435 0.270 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2-Nitroaniline <0.270
0.874 0.300 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼3-Nitroaniline <0.300
0.874 0.311 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼4-Nitroaniline <0.311
0.435 0.262 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Nitrobenzene <0.262
0.435 0.317 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2-Nitrophenol <0.317
0.874 0.498 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼4-Nitrophenol <0.498
0.435 0.253 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼N-Nitrosodi-n-propylamine <0.253
0.435 0.0692 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0692
0.874 0.347 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Pentachlorophenol <0.347
0.0874 0.0444 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Phenanthrene <0.0444
0.435 0.265 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Phenol <0.265
0.0874 0.0444 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼Pyrene <0.0444
0.435 0.236 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼1,2,4-Trichlorobenzene <0.236
0.435 0.284 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2,4,5-Trichlorophenol <0.284
0.435 0.251 mg/Kg 08/08/17 10:12 08/10/17 17:13 1☼2,4,6-Trichlorophenol <0.251
2-Fluorobiphenyl (Surr)46 29-120 08/08/17 10:12 08/10/17 17:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)40 08/08/17 10:12 08/10/17 17:13 110-120
Nitrobenzene-d5 (Surr)43 08/08/17 10:12 08/10/17 17:13 127-120
Phenol-d5 (Surr)42 08/08/17 10:12 08/10/17 17:13 110-120
Terphenyl-d14 (Surr)63 08/08/17 10:12 08/10/17 17:13 113-120
2,4,6-Tribromophenol (Surr)60 08/08/17 10:12 08/10/17 17:13 110-120
Method: MA VPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C9-C12 Aliphatics (North Carolina)6.63 6.57 3.28 mg/Kg ☼08/11/17 11:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
RL MDL
C5-C8 Aliphatics <4.06 7.81 4.06 mg/Kg ☼08/03/17 15:22 08/09/17 23:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
7.81 4.69 mg/Kg 08/03/17 15:22 08/09/17 23:24 1☼C9-C10 Aromatics <4.69
7.81 3.91 mg/Kg 08/03/17 15:22 08/09/17 23:24 1☼C9-C12 Aliphatics 6.63 J
2,5-Dibromotoluene (fid)93 70-130 08/03/17 15:22 08/09/17 23:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2,5-Dibromotoluene (pid)89 08/03/17 15:22 08/09/17 23:24 170-130
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
RL MDL
C19-C36 Aliphatics <6.45 12.9 6.45 mg/Kg ☼08/08/17 10:20 08/10/17 23:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
12.9 3.09 mg/Kg 08/08/17 10:20 08/10/17 23:15 1☼C9-C18 Aliphatics <3.09
12.9 6.32 mg/Kg 08/08/17 10:20 08/10/17 23:09 1☼C11-C22 Aromatics 24.8
1-Chlorooctadecane 48 40-140 08/08/17 10:20 08/10/17 23:15 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
o-Terphenyl 53 08/08/17 10:20 08/10/17 23:09 140-140
2-Fluorobiphenyl 54 08/08/17 10:20 08/10/17 23:09 140-140
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Client Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Lab Sample ID: 490-134180-3Client Sample ID: EI-EXC-W1
Matrix: SolidDate Collected: 08/03/17 16:22
Percent Solids: 76.1Date Received: 08/05/17 10:00
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
2-Bromonaphthalene 53 40-140 08/08/17 10:20 08/10/17 23:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
General Chemistry
RL RL
Percent Moisture 23.9 0.1 0.1 %08/08/17 10:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/08/17 10:52 1Percent Solids 76.1
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QC Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-450963/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
RL MDL
Acenaphthene <0.0320 0.0670 0.0320 mg/Kg 08/08/17 10:12 08/10/17 11:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Acenaphthylene
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Anthracene
<0.0300 0.03000.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[a]anthracene
<0.0270 0.02700.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[a]pyrene
<0.0280 0.02800.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[b]fluoranthene
<0.0330 0.03300.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[g,h,i]perylene
<0.0270 0.02700.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Benzo[k]fluoranthene
<0.200 0.2000.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Bis(2-chloroethoxy)methane
<0.213 0.2130.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Bis(2-chloroethyl)ether
<0.198 0.1980.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1bis (2-chloroisopropyl) ether
<0.207 0.2070.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Bis(2-ethylhexyl) phthalate
<0.205 0.2050.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Bromophenyl phenyl ether
<0.215 0.2150.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Butyl benzyl phthalate
<0.207 0.2070.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Carbazole
<0.227 0.2270.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Chloroaniline
<0.168 0.1680.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Chloro-3-methylphenol
<0.209 0.2090.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Chloronaphthalene
<0.191 0.1910.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Chlorophenol
<0.201 0.2010.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Chlorophenyl phenyl ether
<0.0370 0.03700.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Chrysene
<0.113 0.1130.666 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Cresols
<0.0320 0.03200.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Dibenz(a,h)anthracene
<0.210 0.2100.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Dibenzofuran
<0.190 0.1900.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 11,2-Dichlorobenzene
<0.190 0.1900.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 11,3-Dichlorobenzene
<0.196 0.1960.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 11,4-Dichlorobenzene
<0.204 0.2040.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 13,3'-Dichlorobenzidine
<0.175 0.1750.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4-Dichlorophenol
<0.212 0.2120.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Diethyl phthalate
<0.335 0.3350.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4-Dimethylphenol
<0.207 0.2070.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Dimethyl phthalate
<0.211 0.2110.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Di-n-butyl phthalate
<0.229 0.2290.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 14,6-Dinitro-2-methylphenol
<0.251 0.2510.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4-Dinitrophenol
<0.208 0.2080.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4-Dinitrotoluene
<0.223 0.2230.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,6-Dinitrotoluene
<0.178 0.1780.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Di-n-octyl phthalate
<0.0340 0.03400.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Fluoranthene
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Fluorene
<0.250 0.2500.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Hexachlorobenzene
<0.167 0.1670.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Hexachlorobutadiene
<0.150 0.1500.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Hexachlorocyclopentadiene
<0.181 0.1810.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Hexachloroethane
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Indeno[1,2,3-cd]pyrene
<0.188 0.1880.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Isophorone
<0.0280 0.02800.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 11-Methylnaphthalene
<0.0260 0.02600.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Methylnaphthalene
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QC Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-450963/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
RL MDL
2-Methylphenol <0.216 0.333 0.216 mg/Kg 08/08/17 10:12 08/10/17 11:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.203 0.2030.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 13 & 4 Methylphenol
<0.0290 0.02900.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Naphthalene
<0.207 0.2070.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Nitroaniline
<0.230 0.2300.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 13-Nitroaniline
<0.238 0.2380.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Nitroaniline
<0.201 0.2010.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Nitrobenzene
<0.243 0.2430.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12-Nitrophenol
<0.382 0.3820.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 14-Nitrophenol
<0.194 0.1940.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1N-Nitrosodi-n-propylamine
<0.0530 0.05300.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1n-Nitrosodiphenylamine(as
diphenylamine)
<0.266 0.2660.670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Pentachlorophenol
<0.0340 0.03400.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Phenanthrene
<0.203 0.2030.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Phenol
<0.0340 0.03400.0670 mg/Kg 08/08/17 10:12 08/10/17 11:44 1Pyrene
<0.181 0.1810.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 11,2,4-Trichlorobenzene
<0.218 0.2180.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4,5-Trichlorophenol
<0.192 0.1920.333 mg/Kg 08/08/17 10:12 08/10/17 11:44 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)91 29-120 08/10/17 11:44 1
MB MB
Surrogate
08/08/17 10:12
Dil FacPreparedAnalyzedQualifierLimits%Recovery
75 08/08/17 10:12 08/10/17 11:44 12-Fluorophenol (Surr)10-120
89 08/08/17 10:12 08/10/17 11:44 1Nitrobenzene-d5 (Surr)27-120
83 08/08/17 10:12 08/10/17 11:44 1Phenol-d5 (Surr)10-120
95 08/08/17 10:12 08/10/17 11:44 1Terphenyl-d14 (Surr)13-120
80 08/08/17 10:12 08/10/17 11:44 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450963/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
Acenaphthene 1.67 1.439 mg/Kg 86 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.410 mg/Kg 85 38-120
Anthracene 1.67 1.481 mg/Kg 89 46-124
Benzo[a]anthracene 1.67 1.562 mg/Kg 94 45-120
Benzo[a]pyrene 1.67 1.452 mg/Kg 87 45-120
Benzo[b]fluoranthene 1.67 1.437 mg/Kg 86 42-120
Benzo[g,h,i]perylene 1.67 1.454 mg/Kg 87 38-120
Benzo[k]fluoranthene 1.67 1.740 mg/Kg 104 42-120
Bis(2-chloroethoxy)methane 1.67 1.193 mg/Kg 72 32-120
Bis(2-chloroethyl)ether 1.67 1.124 mg/Kg 67 31-120
bis (2-chloroisopropyl) ether 1.67 0.8252 mg/Kg 50 32-120
Bis(2-ethylhexyl) phthalate 1.67 1.531 mg/Kg 92 43-120
4-Bromophenyl phenyl ether 1.67 1.464 mg/Kg 88 40-120
Butyl benzyl phthalate 1.67 1.510 mg/Kg 91 43-133
Carbazole 1.67 1.511 mg/Kg 91 44-120
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QC Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450963/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
4-Chloroaniline 1.67 0.8331 mg/Kg 50 35-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
4-Chloro-3-methylphenol 1.67 1.522 mg/Kg 91 38-120
2-Chloronaphthalene 1.67 1.376 mg/Kg 83 34-120
2-Chlorophenol 1.67 1.316 mg/Kg 79 32-120
4-Chlorophenyl phenyl ether 1.67 1.453 mg/Kg 87 42-120
Chrysene 1.67 1.588 mg/Kg 95 43-120
Cresols 3.33 2.490 mg/Kg 75 36-129
Dibenz(a,h)anthracene 1.67 1.486 mg/Kg 89 32-128
Dibenzofuran 1.67 1.404 mg/Kg 84 41-120
1,2-Dichlorobenzene 1.67 1.276 mg/Kg 77 33-120
1,3-Dichlorobenzene 1.67 1.262 mg/Kg 76 32-120
1,4-Dichlorobenzene 1.67 1.281 mg/Kg 77 32-120
3,3'-Dichlorobenzidine 1.67 1.463 mg/Kg 88 39-120
2,4-Dichlorophenol 1.67 1.428 mg/Kg 86 32-120
Diethyl phthalate 1.67 1.539 mg/Kg 92 41-122
2,4-Dimethylphenol 1.67 0.9432 mg/Kg 57 32-120
Dimethyl phthalate 1.67 1.532 mg/Kg 92 55-120
Di-n-butyl phthalate 1.67 1.693 mg/Kg 102 46-127
4,6-Dinitro-2-methylphenol 3.33 3.438 mg/Kg 103 27-134
2,4-Dinitrophenol 3.33 3.215 mg/Kg 96 10-142
2,4-Dinitrotoluene 1.67 1.615 mg/Kg 97 43-120
2,6-Dinitrotoluene 1.67 1.693 mg/Kg 102 43-120
Di-n-octyl phthalate 1.67 1.724 mg/Kg 103 40-130
Fluoranthene 1.67 1.635 mg/Kg 98 46-120
Fluorene 1.67 1.457 mg/Kg 87 42-120
Hexachlorobenzene 1.67 1.639 mg/Kg 98 44-120
Hexachlorobutadiene 1.67 1.526 mg/Kg 92 31-120
Hexachlorocyclopentadiene 1.67 <0.150 *mg/Kg 2 24-120
Hexachloroethane 1.67 1.201 mg/Kg 72 33-120
Indeno[1,2,3-cd]pyrene 1.67 1.489 mg/Kg 89 41-121
Isophorone 1.67 0.6517 mg/Kg 39 33-120
1-Methylnaphthalene 1.67 1.358 mg/Kg 81 32-120
2-Methylnaphthalene 1.67 1.361 mg/Kg 82 28-120
2-Methylphenol 1.67 1.215 mg/Kg 73 36-120
3 & 4 Methylphenol 1.67 1.275 mg/Kg 77 37-120
Naphthalene 1.67 1.326 mg/Kg 80 32-120
2-Nitroaniline 1.67 1.443 mg/Kg 87 40-120
3-Nitroaniline 1.67 1.303 mg/Kg 78 42-120
4-Nitroaniline 1.67 1.407 mg/Kg 84 43-120
Nitrobenzene 1.67 1.167 mg/Kg 70 26-120
2-Nitrophenol 1.67 1.628 mg/Kg 98 29-120
4-Nitrophenol 3.33 2.953 mg/Kg 89 32-136
N-Nitrosodi-n-propylamine 1.67 1.168 mg/Kg 70 35-120
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.391 mg/Kg 98 52-140
Pentachlorophenol 3.33 3.161 mg/Kg 95 44-134
Phenanthrene 1.67 1.488 mg/Kg 89 45-120
Phenol 1.67 1.281 mg/Kg 77 30-120
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QC Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450963/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
Pyrene 1.67 1.575 mg/Kg 95 43-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2,4-Trichlorobenzene 1.67 1.401 mg/Kg 84 29-120
2,4,5-Trichlorophenol 1.67 1.609 mg/Kg 97 39-120
2,4,6-Trichlorophenol 1.67 1.597 mg/Kg 96 39-120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
88
LCS LCS
Qualifier Limits%Recovery
812-Fluorophenol (Surr)10 -120
88Nitrobenzene-d5 (Surr)27 -120
84Phenol-d5 (Surr)10 -120
107Terphenyl-d14 (Surr)13 -120
1072,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Matrix SpikeLab Sample ID: 490-134155-B-22-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
Acenaphthene <0.0393 2.07 1.635 mg/Kg 79 19-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene <0.0356 2.07 1.619 mg/Kg 78 25-120☼
Anthracene <0.0356 2.07 1.865 mg/Kg 90 28-125☼
Benzo[a]anthracene <0.0369 2.07 2.018 mg/Kg 97 23-120☼
Benzo[a]pyrene <0.0332 2.07 1.851 mg/Kg 89 15-128☼
Benzo[b]fluoranthene <0.0344 2.07 1.912 mg/Kg 92 12-133☼
Benzo[g,h,i]perylene <0.0406 2.07 1.918 mg/Kg 92 22-120☼
Benzo[k]fluoranthene <0.0332 2.07 2.090 mg/Kg 101 28-120☼
Bis(2-chloroethoxy)methane <0.246 2.07 1.225 mg/Kg 59 24-120☼
Bis(2-chloroethyl)ether <0.262 2.07 1.094 mg/Kg 53 22-120☼
bis (2-chloroisopropyl) ether <0.243 2.07 0.8070 mg/Kg 39 20-120☼
Bis(2-ethylhexyl) phthalate <0.254 2.07 2.052 mg/Kg 99 26-120☼
4-Bromophenyl phenyl ether <0.252 2.07 1.841 mg/Kg 89 31-120☼
Butyl benzyl phthalate <0.264 2.07 2.026 mg/Kg 98 24-133☼
Carbazole <0.254 2.07 1.921 mg/Kg 93 25-123☼
4-Chloroaniline <0.279 2.07 0.9095 mg/Kg 44 26-120☼
4-Chloro-3-methylphenol <0.206 2.07 1.835 mg/Kg 88 21-120☼
2-Chloronaphthalene <0.257 2.07 1.510 mg/Kg 73 24-120☼
2-Chlorophenol <0.235 2.07 1.270 mg/Kg 61 25-120☼
4-Chlorophenyl phenyl ether <0.247 2.07 1.723 mg/Kg 83 26-120☼
Chrysene <0.0455 2.07 2.033 mg/Kg 98 20-120☼
Cresols <0.139 4.15 2.655 mg/Kg 64 10-200☼
Dibenz(a,h)anthracene <0.0393 2.07 1.951 mg/Kg 94 12-128☼
Dibenzofuran <0.258 2.07 1.664 mg/Kg 80 21-120☼
1,2-Dichlorobenzene <0.234 2.07 1.193 mg/Kg 58 10-120☼
1,3-Dichlorobenzene <0.234 2.07 1.159 mg/Kg 56 10-120☼
1,4-Dichlorobenzene <0.241 2.07 1.159 mg/Kg 56 10-120☼
3,3'-Dichlorobenzidine <0.251 2.07 1.804 mg/Kg 87 10-120☼
2,4-Dichlorophenol <0.215 2.07 1.532 mg/Kg 74 17-120☼
Diethyl phthalate <0.261 2.07 1.939 mg/Kg 93 29-122☼
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QC Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-134155-B-22-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
2,4-Dimethylphenol <0.412 2.07 1.069 mg/Kg 52 17-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Dimethyl phthalate <0.254 2.07 1.896 mg/Kg 91 30-120☼
Di-n-butyl phthalate <0.259 2.07 2.147 mg/Kg 103 29-126☼
4,6-Dinitro-2-methylphenol <0.281 4.15 2.323 mg/Kg 56 10-134☼
2,4-Dinitrophenol <0.309 4.15 1.774 mg/Kg 43 10-150☼
2,4-Dinitrotoluene <0.256 2.07 1.986 mg/Kg 96 24-121☼
2,6-Dinitrotoluene <0.274 2.07 2.050 mg/Kg 99 24-120☼
Di-n-octyl phthalate <0.219 2.07 2.326 mg/Kg 112 27-130☼
Fluoranthene <0.0418 2.07 2.034 mg/Kg 98 10-143☼
Fluorene <0.0356 2.07 1.760 mg/Kg 85 20-120☼
Hexachlorobenzene <0.307 2.07 2.066 mg/Kg 100 25-120☼
Hexachlorobutadiene <0.205 2.07 1.432 mg/Kg 69 10-120☼
Hexachlorocyclopentadiene <0.184 F1 *2.07 <0.187 F1 mg/Kg 0 10-120☼
Hexachloroethane <0.222 2.07 1.101 mg/Kg 53 10-120☼
Indeno[1,2,3-cd]pyrene <0.0356 2.07 1.948 mg/Kg 94 22-121☼
Isophorone <0.231 2.07 0.7065 mg/Kg 34 24-120☼
1-Methylnaphthalene <0.0344 2.07 1.456 mg/Kg 70 10-120☼
2-Methylnaphthalene <0.0320 2.07 1.438 mg/Kg 69 13-120☼
2-Methylphenol <0.265 2.07 1.264 mg/Kg 61 23-120☼
3 & 4 Methylphenol <0.250 2.07 1.391 mg/Kg 67 19-120☼
Naphthalene <0.0356 2.07 1.304 mg/Kg 63 10-120☼
2-Nitroaniline <0.254 2.07 1.749 mg/Kg 84 31-120☼
3-Nitroaniline <0.283 2.07 1.622 mg/Kg 78 31-120☼
4-Nitroaniline <0.293 2.07 1.765 mg/Kg 85 28-120☼
Nitrobenzene <0.247 2.07 1.178 mg/Kg 57 19-120☼
2-Nitrophenol <0.299 2.07 1.551 mg/Kg 75 23-120☼
4-Nitrophenol <0.470 4.15 3.600 mg/Kg 87 16-139☼
N-Nitrosodi-n-propylamine <0.238 2.07 1.252 mg/Kg 60 24-120☼
n-Nitrosodiphenylamine(as
diphenylamine)
<0.0651 1.76 1.776 mg/Kg 101 26-150☼
Pentachlorophenol <0.327 4.15 3.879 mg/Kg 94 19-145☼
Phenanthrene <0.0418 2.07 1.897 mg/Kg 91 21-122☼
Phenol <0.250 2.07 1.302 mg/Kg 63 15-120☼
Pyrene <0.0418 2.07 2.130 mg/Kg 103 20-123☼
1,2,4-Trichlorobenzene <0.222 2.07 1.376 mg/Kg 66 14-120☼
2,4,5-Trichlorophenol <0.268 2.07 1.929 mg/Kg 93 27-120☼
2,4,6-Trichlorophenol <0.236 2.07 1.868 mg/Kg 90 24-122☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
76
MS MS
Qualifier Limits%Recovery
602-Fluorophenol (Surr)10 -120
67Nitrobenzene-d5 (Surr)27 -120
69Phenol-d5 (Surr)10 -120
117Terphenyl-d14 (Surr)13 -120
1082,4,6-Tribromophenol (Surr)10 -120
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QC Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-134155-B-22-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
Acenaphthene <0.0393 2.02 1.291 mg/Kg 64 19-120 24 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene <0.0356 2.02 1.283 mg/Kg 64 25-120 23 50☼
Anthracene <0.0356 2.02 1.484 mg/Kg 73 28-125 23 49☼
Benzo[a]anthracene <0.0369 2.02 1.586 mg/Kg 79 23-120 24 50☼
Benzo[a]pyrene <0.0332 2.02 1.477 mg/Kg 73 15-128 22 50☼
Benzo[b]fluoranthene <0.0344 2.02 1.663 mg/Kg 82 12-133 14 50☼
Benzo[g,h,i]perylene <0.0406 2.02 1.497 mg/Kg 74 22-120 25 50☼
Benzo[k]fluoranthene <0.0332 2.02 1.543 mg/Kg 76 28-120 30 45☼
Bis(2-chloroethoxy)methane <0.246 2.02 0.9550 mg/Kg 47 24-120 25 50☼
Bis(2-chloroethyl)ether <0.262 2.02 0.8602 mg/Kg 43 22-120 24 50☼
bis (2-chloroisopropyl) ether <0.243 2.02 0.6466 mg/Kg 32 20-120 22 50☼
Bis(2-ethylhexyl) phthalate <0.254 2.02 1.612 mg/Kg 80 26-120 24 50☼
4-Bromophenyl phenyl ether <0.252 2.02 1.465 mg/Kg 73 31-120 23 37☼
Butyl benzyl phthalate <0.264 2.02 1.633 mg/Kg 81 24-133 21 50☼
Carbazole <0.254 2.02 1.499 mg/Kg 74 25-123 25 46☼
4-Chloroaniline <0.279 2.02 0.7075 mg/Kg 35 26-120 25 50☼
4-Chloro-3-methylphenol <0.206 2.02 1.412 mg/Kg 70 21-120 26 49☼
2-Chloronaphthalene <0.257 2.02 1.193 mg/Kg 59 24-120 23 50☼
2-Chlorophenol <0.235 2.02 0.9996 mg/Kg 49 25-120 24 50☼
4-Chlorophenyl phenyl ether <0.247 2.02 1.379 mg/Kg 68 26-120 22 50☼
Chrysene <0.0455 2.02 1.596 mg/Kg 79 20-120 24 49☼
Cresols <0.139 4.04 2.044 mg/Kg 51 10-200 26 50☼
Dibenz(a,h)anthracene <0.0393 2.02 1.537 mg/Kg 76 12-128 24 50☼
Dibenzofuran <0.258 2.02 1.312 mg/Kg 65 21-120 24 50☼
1,2-Dichlorobenzene <0.234 2.02 0.9629 mg/Kg 48 10-120 21 50☼
1,3-Dichlorobenzene <0.234 2.02 0.9395 mg/Kg 47 10-120 21 50☼
1,4-Dichlorobenzene <0.241 2.02 0.9465 mg/Kg 47 10-120 20 50☼
3,3'-Dichlorobenzidine <0.251 2.02 1.471 mg/Kg 73 10-120 20 50☼
2,4-Dichlorophenol <0.215 2.02 1.189 mg/Kg 59 17-120 25 50☼
Diethyl phthalate <0.261 2.02 1.531 mg/Kg 76 29-122 24 45☼
2,4-Dimethylphenol <0.412 2.02 0.7833 J mg/Kg 39 17-120 31 50☼
Dimethyl phthalate <0.254 2.02 1.478 mg/Kg 73 30-120 25 46☼
Di-n-butyl phthalate <0.259 2.02 1.694 mg/Kg 84 29-126 24 49☼
4,6-Dinitro-2-methylphenol <0.281 4.04 1.900 mg/Kg 47 10-134 20 50☼
2,4-Dinitrophenol <0.309 4.04 1.446 mg/Kg 36 10-150 20 50☼
2,4-Dinitrotoluene <0.256 2.02 1.594 mg/Kg 79 24-121 22 50☼
2,6-Dinitrotoluene <0.274 2.02 1.621 mg/Kg 80 24-120 23 50☼
Di-n-octyl phthalate <0.219 2.02 1.868 mg/Kg 92 27-130 22 50☼
Fluoranthene <0.0418 2.02 1.608 mg/Kg 80 10-143 23 50☼
Fluorene <0.0356 2.02 1.391 mg/Kg 69 20-120 23 50☼
Hexachlorobenzene <0.307 2.02 1.629 mg/Kg 81 25-120 24 50☼
Hexachlorobutadiene <0.205 2.02 1.156 mg/Kg 57 10-120 21 50☼
Hexachlorocyclopentadiene <0.184 F1 *2.02 <0.182 F1 mg/Kg 0 10-120 NC 50☼
Hexachloroethane <0.222 2.02 0.8889 mg/Kg 44 10-120 21 50☼
Indeno[1,2,3-cd]pyrene <0.0356 2.02 1.526 mg/Kg 76 22-121 24 50☼
Isophorone <0.231 2.02 0.5469 mg/Kg 27 24-120 25 50☼
1-Methylnaphthalene <0.0344 2.02 1.117 mg/Kg 55 10-120 26 50☼
2-Methylnaphthalene <0.0320 2.02 1.120 mg/Kg 55 13-120 25 50☼
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QC Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-134155-B-22-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451551 Prep Batch: 450963
2-Methylphenol <0.265 2.02 0.9840 mg/Kg 49 23-120 25 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
3 & 4 Methylphenol <0.250 2.02 1.060 mg/Kg 52 19-120 27 50☼
Naphthalene <0.0356 2.02 1.027 mg/Kg 51 10-120 24 50☼
2-Nitroaniline <0.254 2.02 1.408 mg/Kg 70 31-120 22 50☼
3-Nitroaniline <0.283 2.02 1.305 mg/Kg 65 31-120 22 49☼
4-Nitroaniline <0.293 2.02 1.399 mg/Kg 69 28-120 23 49☼
Nitrobenzene <0.247 2.02 0.9237 mg/Kg 46 19-120 24 50☼
2-Nitrophenol <0.299 2.02 1.248 mg/Kg 62 23-120 22 50☼
4-Nitrophenol <0.470 4.04 2.824 mg/Kg 70 16-139 24 45☼
N-Nitrosodi-n-propylamine <0.238 2.02 0.9701 mg/Kg 48 24-120 25 50☼
n-Nitrosodiphenylamine(as
diphenylamine)
<0.0651 1.72 1.406 mg/Kg 82 26-150 23 50☼
Pentachlorophenol <0.327 4.04 3.100 mg/Kg 77 19-145 22 50☼
Phenanthrene <0.0418 2.02 1.493 mg/Kg 74 21-122 24 50☼
Phenol <0.250 2.02 1.018 mg/Kg 50 15-120 24 50☼
Pyrene <0.0418 2.02 1.726 mg/Kg 85 20-123 21 50☼
1,2,4-Trichlorobenzene <0.222 2.02 1.095 mg/Kg 54 14-120 23 50☼
2,4,5-Trichlorophenol <0.268 2.02 1.535 mg/Kg 76 27-120 23 50☼
2,4,6-Trichlorophenol <0.236 2.02 1.451 mg/Kg 72 24-122 25 50☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
55
MSD MSD
Qualifier Limits%Recovery
432-Fluorophenol (Surr)10 -120
48Nitrobenzene-d5 (Surr)27 -120
49Phenol-d5 (Surr)10 -120
85Terphenyl-d14 (Surr)13 -120
802,4,6-Tribromophenol (Surr)10 -120
Method: MAVPH - Massachusetts - Volatile Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 490-451273/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451273
RL MDL
C9-C10 Aromatics <3.00 5.00 3.00 mg/Kg 08/09/17 13:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
2,5-Dibromotoluene (pid)87 70-130 08/09/17 13:14 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC)
Client Sample ID: Method BlankLab Sample ID: MB 490-450969/1-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451728 Prep Batch: 450969
RL MDL
C19-C36 Aliphatics <5.00 10.0 5.00 mg/Kg 08/08/17 10:20 08/10/17 17:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<2.40 2.4010.0 mg/Kg 08/08/17 10:20 08/10/17 17:30 1C9-C18 Aliphatics
1-Chlorooctadecane 56 40-140 08/10/17 17:30 1
MB MB
Surrogate
08/08/17 10:20
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 490-450969/1-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451732 Prep Batch: 450969
RL MDL
C11-C22 Aromatics <4.90 10.0 4.90 mg/Kg 08/08/17 10:20 08/10/17 17:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
o-Terphenyl 64 40-140 08/10/17 17:10 1
MB MB
Surrogate
08/08/17 10:20
Dil FacPreparedAnalyzedQualifierLimits%Recovery
70 08/08/17 10:20 08/10/17 17:10 12-Fluorobiphenyl 40-140
68 08/08/17 10:20 08/10/17 17:10 12-Bromonaphthalene 40-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450969/2-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451728 Prep Batch: 450969
C19-C36 Aliphatics 20.0 16.23 mg/Kg 81 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
C9-C18 Aliphatics 15.0 10.41 mg/Kg 69 40-140
1-Chlorooctadecane 40 -140
Surrogate
61
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-450969/2-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451732 Prep Batch: 450969
C11-C22 Aromatics 42.5 34.51 mg/Kg 81 40-140
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl 40 -140
Surrogate
71
LCS LCS
Qualifier Limits%Recovery
692-Fluorobiphenyl 40 -140
682-Bromonaphthalene 40 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-450969/3-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451728 Prep Batch: 450969
C19-C36 Aliphatics 20.0 16.79 mg/Kg 84 40-140 3 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method: MA-EPH - Massachusetts - Extractable Petroleum Hydrocarbons (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-450969/3-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451728 Prep Batch: 450969
C9-C18 Aliphatics 15.0 9.775 J mg/Kg 65 40-140 6 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1-Chlorooctadecane 40 -140
Surrogate
59
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-450969/3-C
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 451732 Prep Batch: 450969
C11-C22 Aromatics 42.5 37.78 mg/Kg 89 40-140 9 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
o-Terphenyl 40 -140
Surrogate
76
LCSD LCSD
Qualifier Limits%Recovery
752-Fluorobiphenyl 40 -140
742-Bromonaphthalene 40 -140
Method: Moisture - Percent Moisture
Client Sample ID: DuplicateLab Sample ID: 490-134149-I-3 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 450989
Percent Moisture 7.8 9.0 %15 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 92.2 91.0 %1 20
TestAmerica Nashville
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QC Association Summary
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
GC/MS Semi VOA
Prep Batch: 450963
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550C490-134180-1 EI-EXC-N1 Total/NA
Solid 3550C490-134180-2 EI-EXC-S1 Total/NA
Solid 3550C490-134180-3 EI-EXC-W1 Total/NA
Solid 3550CMB 490-450963/1-A Method Blank Total/NA
Solid 3550CLCS 490-450963/2-A Lab Control Sample Total/NA
Solid 3550C490-134155-B-22-B MS Matrix Spike Total/NA
Solid 3550C490-134155-B-22-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 451551
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 450963490-134180-1 EI-EXC-N1 Total/NA
Solid 8270D 450963490-134180-2 EI-EXC-S1 Total/NA
Solid 8270D 450963490-134180-3 EI-EXC-W1 Total/NA
Solid 8270D 450963MB 490-450963/1-A Method Blank Total/NA
Solid 8270D 450963LCS 490-450963/2-A Lab Control Sample Total/NA
Solid 8270D 450963490-134155-B-22-B MS Matrix Spike Total/NA
Solid 8270D 450963490-134155-B-22-C MSD Matrix Spike Duplicate Total/NA
GC VOA
Prep Batch: 450843
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035490-134180-1 EI-EXC-N1 Total/NA
Solid 5035490-134180-2 EI-EXC-S1 Total/NA
Solid 5035490-134180-3 EI-EXC-W1 Total/NA
Analysis Batch: 451273
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MAVPH 450843490-134180-1 EI-EXC-N1 Total/NA
Solid MAVPH 450843490-134180-2 EI-EXC-S1 Total/NA
Solid MAVPH 450843490-134180-3 EI-EXC-W1 Total/NA
Solid MAVPHMB 490-451273/6 Method Blank Total/NA
Analysis Batch: 452035
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA VPH490-134180-1 EI-EXC-N1 Total/NA
Solid MA VPH490-134180-2 EI-EXC-S1 Total/NA
Solid MA VPH490-134180-3 EI-EXC-W1 Total/NA
GC Semi VOA
Prep Batch: 450969
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541490-134180-1 EI-EXC-N1 Total/NA
Solid 3541490-134180-2 EI-EXC-S1 Total/NA
Solid 3541490-134180-3 EI-EXC-W1 Total/NA
Solid 3541MB 490-450969/1-B Method Blank Total/NA
Solid 3541MB 490-450969/1-C Method Blank Total/NA
Solid 3541LCS 490-450969/2-B Lab Control Sample Total/NA
Solid 3541LCS 490-450969/2-C Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
GC Semi VOA (Continued)
Prep Batch: 450969 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541LCSD 490-450969/3-B Lab Control Sample Dup Total/NA
Solid 3541LCSD 490-450969/3-C Lab Control Sample Dup Total/NA
Fraction Batch: 451662
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA EPH Frac 450969490-134180-1 EI-EXC-N1 Total/NA
Solid MA EPH Frac 450969490-134180-1 EI-EXC-N1 Total/NA
Solid MA EPH Frac 450969490-134180-2 EI-EXC-S1 Total/NA
Solid MA EPH Frac 450969490-134180-2 EI-EXC-S1 Total/NA
Solid MA EPH Frac 450969490-134180-3 EI-EXC-W1 Total/NA
Solid MA EPH Frac 450969490-134180-3 EI-EXC-W1 Total/NA
Solid MA EPH Frac 450969MB 490-450969/1-B Method Blank Total/NA
Solid MA EPH Frac 450969MB 490-450969/1-C Method Blank Total/NA
Solid MA EPH Frac 450969LCS 490-450969/2-B Lab Control Sample Total/NA
Solid MA EPH Frac 450969LCS 490-450969/2-C Lab Control Sample Total/NA
Solid MA EPH Frac 450969LCSD 490-450969/3-B Lab Control Sample Dup Total/NA
Solid MA EPH Frac 450969LCSD 490-450969/3-C Lab Control Sample Dup Total/NA
Analysis Batch: 451728
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA-EPH 451662490-134180-1 EI-EXC-N1 Total/NA
Solid MA-EPH 451662490-134180-2 EI-EXC-S1 Total/NA
Solid MA-EPH 451662490-134180-3 EI-EXC-W1 Total/NA
Solid MA-EPH 451662MB 490-450969/1-B Method Blank Total/NA
Solid MA-EPH 451662LCS 490-450969/2-B Lab Control Sample Total/NA
Solid MA-EPH 451662LCSD 490-450969/3-B Lab Control Sample Dup Total/NA
Analysis Batch: 451732
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid MA-EPH 451662490-134180-1 EI-EXC-N1 Total/NA
Solid MA-EPH 451662490-134180-2 EI-EXC-S1 Total/NA
Solid MA-EPH 451662490-134180-3 EI-EXC-W1 Total/NA
Solid MA-EPH 451662MB 490-450969/1-C Method Blank Total/NA
Solid MA-EPH 451662LCS 490-450969/2-C Lab Control Sample Total/NA
Solid MA-EPH 451662LCSD 490-450969/3-C Lab Control Sample Dup Total/NA
General Chemistry
Analysis Batch: 450989
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-134180-1 EI-EXC-N1 Total/NA
Solid Moisture490-134180-2 EI-EXC-S1 Total/NA
Solid Moisture490-134180-3 EI-EXC-W1 Total/NA
Solid Moisture490-134149-I-3 DU Duplicate Total/NA
TestAmerica Nashville
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Lab Chronicle
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134180-1
Project/Site: Eagle Island Remediation SDG: GN6353
Client Sample ID: EI-EXC-N1 Lab Sample ID: 490-134180-1
Matrix: SolidDate Collected: 08/03/17 15:33
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 10:521 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: EI-EXC-N1 Lab Sample ID: 490-134180-1
Matrix: SolidDate Collected: 08/03/17 15:33
Percent Solids: 64.6Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.94 g 1.00 mL
Analysis 8270D 1 451551 08/10/17 16:34 ZLN TAL NSHTotal/NA
Analysis MA VPH 1 452035 08/11/17 11:23 FKG TAL NSHTotal/NA
Prep 5035 450843 08/03/17 14:33 JLP TAL NSHTotal/NA 5.239 g 5.0 mL
Analysis MAVPH 1 451273 08/09/17 22:20 S1S TAL NSHTotal/NA 0.1 mL 5 mL
Prep 3541 450969 08/08/17 10:20 ZXS TAL NSHTotal/NA 10.34 g 2 mL
Fraction MA EPH Frac 451662 08/10/17 10:40 ZXS TAL NSHTotal/NA 2 mL 1 mL
Analysis MA-EPH 1 451732 08/11/17 09:15 A1B TAL NSHTotal/NA
Prep 3541 450969 08/08/17 10:20 ZXS TAL NSHTotal/NA 10.34 g 2 mL
Fraction MA EPH Frac 451662 08/10/17 10:40 ZXS TAL NSHTotal/NA 2 mL 1 mL
Analysis MA-EPH 1 451728 08/10/17 22:26 A1B TAL NSHTotal/NA
Client Sample ID: EI-EXC-S1 Lab Sample ID: 490-134180-2
Matrix: SolidDate Collected: 08/03/17 15:58
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 10:521 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: EI-EXC-S1 Lab Sample ID: 490-134180-2
Matrix: SolidDate Collected: 08/03/17 15:58
Percent Solids: 83.0Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.56 g 1.00 mL
Analysis 8270D 1 451551 08/10/17 16:54 ZLN TAL NSHTotal/NA
Analysis MA VPH 1 452035 08/11/17 11:23 FKG TAL NSHTotal/NA
Prep 5035 450843 08/03/17 14:58 JLP TAL NSHTotal/NA 5.43 g 5.0 mL
Analysis MAVPH 1 451273 08/09/17 22:52 S1S TAL NSHTotal/NA 0.1 mL 5 mL
Prep 3541 450969 08/08/17 10:20 ZXS TAL NSHTotal/NA 10.82 g 2 mL
Fraction MA EPH Frac 451662 08/10/17 10:40 ZXS TAL NSHTotal/NA 2 mL 1 mL
Analysis MA-EPH 1 451732 08/10/17 22:44 A1B TAL NSHTotal/NA
Prep 3541 450969 08/08/17 10:20 ZXS TAL NSHTotal/NA 10.82 g 2 mL
Fraction MA EPH Frac 451662 08/10/17 10:40 ZXS TAL NSHTotal/NA 2 mL 1 mL
Analysis MA-EPH 1 451728 08/10/17 22:51 A1B TAL NSHTotal/NA
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Lab Chronicle
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134180-1
Project/Site: Eagle Island Remediation SDG: GN6353
Client Sample ID: EI-EXC-W1 Lab Sample ID: 490-134180-3
Matrix: SolidDate Collected: 08/03/17 16:22
Date Received: 08/05/17 10:00
Analysis Moisture BAA08/08/17 10:521 TAL NSH450989
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: EI-EXC-W1 Lab Sample ID: 490-134180-3
Matrix: SolidDate Collected: 08/03/17 16:22
Percent Solids: 76.1Date Received: 08/05/17 10:00
Prep 3550C MNM08/08/17 10:12 TAL NSH450963
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.20 g 1.00 mL
Analysis 8270D 1 451551 08/10/17 17:13 ZLN TAL NSHTotal/NA
Analysis MA VPH 1 452035 08/11/17 11:23 FKG TAL NSHTotal/NA
Prep 5035 450843 08/03/17 15:22 JLP TAL NSHTotal/NA 5.258 g 5.0 mL
Analysis MAVPH 1 451273 08/09/17 23:24 S1S TAL NSHTotal/NA 0.1 mL 5 mL
Prep 3541 450969 08/08/17 10:20 ZXS TAL NSHTotal/NA 10.19 g 2 mL
Fraction MA EPH Frac 451662 08/10/17 10:40 ZXS TAL NSHTotal/NA 2 mL 1 mL
Analysis MA-EPH 1 451732 08/10/17 23:09 A1B TAL NSHTotal/NA
Prep 3541 450969 08/08/17 10:20 ZXS TAL NSHTotal/NA 10.19 g 2 mL
Fraction MA EPH Frac 451662 08/10/17 10:40 ZXS TAL NSHTotal/NA 2 mL 1 mL
Analysis MA-EPH 1 451728 08/10/17 23:15 A1B TAL NSHTotal/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-134180-1Client: Geosyntec Consultants, Inc.
SDG: GN6353Project/Site: Eagle Island Remediation
Method Method Description LaboratoryProtocol
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
MA DEPMA VPH Massachusetts - Volatile Petroleum Hydrocarbons (GC)TAL NSH
MA DEPMAVPHMassachusetts - Volatile Petroleum Hydrocarbons (GC)TAL NSH
MA DEPMA-EPH Massachusetts - Extractable Petroleum Hydrocarbons (GC)TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Accreditation/Certification Summary
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134180-1
Project/Site: Eagle Island Remediation SDG: GN6353
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3874State Program 12-31-17
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
MA VPH Solid C9-C12 Aliphatics (North Carolina)
Moisture Solid Percent Moisture
Moisture Solid Percent Solids
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Geosyntec Consultants, Inc.Job Number: 490-134180-1
SDG Number: GN6353
Login Number: 134180
Question Answer Comment
Creator: Huskey, Adam
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-134906-1
Client Project/Site: Eagle Island Leland, NC
For:
Geosyntec Consultants, Inc.
2501 Blue Ridge Rd.
Suite 430
Raleigh, North Carolina 27607
Attn: Ms. Kaitlyn S Rhonehouse
Authorized for release by:
8/24/2017 12:37:22 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
TestAmerica Job ID: 490-134906-1
Page 2 of 27 TestAmerica Nashville8/24/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
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Sample Summary
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-134906-1 SURF-EDGE-4 Solid 08/17/17 10:15 08/18/17 09:35
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Case Narrative
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134906-1
Project/Site: Eagle Island Leland, NC
Job ID: 490-134906-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-134906-1
Comments
No additional comments.
Receipt
The samples were received on 8/18/2017 9:35 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 2.8º C.
GC/MS Semi VOA
Method 8270D: The continuing calibration verification (CCVIS) associated with batch 490-453896 recovered above the upper control limit
for Di-n-octyl phthalate. The samples associated with this CCVIS were non-detect for this analyte; therefore, the data has been reported.
The following sample is impacted: (CCVIS 490-453896/3).
Method 8270D: The continuing calibration verification (CCVIS) analyzed in batch 490-453896 was outside the method criteria for
bis(2-chloroisopropyl)ether. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is
considered estimated.
Method 8270D: The matrix spike (MS) recoveries for preparation batch 490-453767 and analytical batch 490-453896 were outside control
limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS)
recovery was within acceptance limits.
Method 8270D: The continuing calibration verification (CCV) associated with batch 490-454779 recovered above the upper control limit for
2,4-Dinitrophenol. The samples associated with this CCV were non-detects for this analyte; therefore, the data has been reported. The
following sample is impacted: (CCVIS 490-454779/3).
Method 8270D: The continuing calibration verification (CCV) analyzed in batch 490-454779 was outside the method criteria for the
following analyte: bis (2-chloroisopropyl) ether. A CCV standard at or below the reporting limit (RL) was analyzed with the affected
samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the
affected analyte is considered estimated.
Method 8270D: The laboratory control sample and the laboratory control sample duplicate (LCS/LCSD) for preparation batch 490-454604
and 490-454604 and analytical batch 490-454779 recovered outside control limits for the following analyte: Hexachlorocyclopentadiene.
Hexachlorocyclopentadiene has been identified as a poor performing analyte when analyzed using this method; therefore,
re-extraction/re-analysis was not performed.
Method 8270D: The following samples were diluted due to the nature of the sample matrix: (490-135116-I-1-D), (490-135116-I-1-E MS)
and (490-135116-I-1-F MSD). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 6010D: The low level continuing calibration verification (CCVL) associated with batch 490-454496 recovered above the upper
control limit for Antimony. The samples associated with this CCV were non-detects for this analyte; therefore, the data has been reported.
Method 7471B: The following samples were diluted to bring the concentration of target analytes within the calibration range:
(460-139295-C-1-A), (460-139295-C-1-B MS) and (460-139295-C-1-C MSD). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Qualifiers
GC/MS Semi VOA
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
F1 MS and/or MSD Recovery is outside acceptance limits.
Metals
Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Qualifier
^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
F1 MS and/or MSD Recovery is outside acceptance limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Lab Sample ID: 490-134906-1Client Sample ID: SURF-EDGE-4
Matrix: SolidDate Collected: 08/17/17 10:15
Percent Solids: 87.2Date Received: 08/18/17 09:35
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.0358 0.0749 0.0358 mg/Kg ☼08/23/17 09:14 08/23/17 22:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0749 0.0324 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Acenaphthylene <0.0324
0.0749 0.0324 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Anthracene <0.0324
0.0749 0.0336 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Benzo[a]anthracene <0.0336
0.0749 0.0302 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Benzo[a]pyrene <0.0302
0.0749 0.0313 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Benzo[b]fluoranthene <0.0313
0.0749 0.0369 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Benzo[g,h,i]perylene <0.0369
0.0749 0.0302 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Benzo[k]fluoranthene <0.0302
0.372 0.224 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Bis(2-chloroethoxy)methane <0.224
0.372 0.238 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Bis(2-chloroethyl)ether <0.238
0.372 0.221 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼bis (2-chloroisopropyl) ether <0.221
0.372 0.232 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Bis(2-ethylhexyl) phthalate <0.232
0.372 0.229 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼4-Bromophenyl phenyl ether <0.229
0.372 0.240 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Butyl benzyl phthalate <0.240
0.372 0.232 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Carbazole <0.232
0.372 0.254 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼4-Chloroaniline <0.254
0.372 0.188 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼4-Chloro-3-methylphenol <0.188
0.372 0.234 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2-Chloronaphthalene <0.234
0.372 0.214 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2-Chlorophenol <0.214
0.372 0.225 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼4-Chlorophenyl phenyl ether <0.225
0.0749 0.0414 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Chrysene <0.0414
0.745 0.126 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Cresols <0.126
0.0749 0.0358 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Dibenz(a,h)anthracene <0.0358
0.372 0.235 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Dibenzofuran <0.235
0.372 0.213 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼1,2-Dichlorobenzene <0.213
0.372 0.213 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼1,3-Dichlorobenzene <0.213
0.372 0.219 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼1,4-Dichlorobenzene <0.219
0.749 0.228 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼3,3'-Dichlorobenzidine <0.228
0.372 0.196 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2,4-Dichlorophenol <0.196
0.372 0.237 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Diethyl phthalate <0.237
0.749 0.375 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2,4-Dimethylphenol <0.375
0.372 0.232 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Dimethyl phthalate <0.232
0.372 0.236 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Di-n-butyl phthalate <0.236
0.372 0.256 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼4,6-Dinitro-2-methylphenol <0.256
0.372 0.281 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2,4-Dinitrophenol <0.281
0.372 0.233 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2,4-Dinitrotoluene <0.233
0.372 0.249 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2,6-Dinitrotoluene <0.249
0.372 0.199 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Di-n-octyl phthalate <0.199
0.0749 0.0380 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Fluoranthene <0.0380
0.0749 0.0324 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Fluorene <0.0324
0.372 0.280 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Hexachlorobenzene <0.280
0.372 0.187 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Hexachlorobutadiene <0.187
0.372 0.168 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Hexachlorocyclopentadiene <0.168 *
0.372 0.202 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Hexachloroethane <0.202
0.0749 0.0324 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Indeno[1,2,3-cd]pyrene <0.0324
0.372 0.210 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Isophorone <0.210
0.0749 0.0313 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼1-Methylnaphthalene <0.0313
0.0749 0.0291 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2-Methylnaphthalene <0.0291
0.372 0.242 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2-Methylphenol <0.242
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Client Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Lab Sample ID: 490-134906-1Client Sample ID: SURF-EDGE-4
Matrix: SolidDate Collected: 08/17/17 10:15
Percent Solids: 87.2Date Received: 08/18/17 09:35
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3 & 4 Methylphenol <0.227 0.372 0.227 mg/Kg ☼08/23/17 09:14 08/23/17 22:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0749 0.0324 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Naphthalene <0.0324
0.372 0.232 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2-Nitroaniline <0.232
0.749 0.257 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼3-Nitroaniline <0.257
0.749 0.266 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼4-Nitroaniline <0.266
0.372 0.225 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Nitrobenzene <0.225
0.372 0.272 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2-Nitrophenol <0.272
0.749 0.427 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼4-Nitrophenol <0.427
0.372 0.217 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼N-Nitrosodi-n-propylamine <0.217
0.372 0.0593 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼n-Nitrosodiphenylamine(as
diphenylamine)
<0.0593
0.749 0.298 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Pentachlorophenol <0.298
0.0749 0.0380 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Phenanthrene <0.0380
0.372 0.227 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Phenol <0.227
0.0749 0.0380 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼Pyrene <0.0380
0.372 0.202 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼1,2,4-Trichlorobenzene <0.202
0.372 0.244 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2,4,5-Trichlorophenol <0.244
0.372 0.215 mg/Kg 08/23/17 09:14 08/23/17 22:41 1☼2,4,6-Trichlorophenol <0.215
2-Fluorobiphenyl (Surr)50 29-120 08/23/17 09:14 08/23/17 22:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)51 08/23/17 09:14 08/23/17 22:41 110-120
Nitrobenzene-d5 (Surr)50 08/23/17 09:14 08/23/17 22:41 127-120
Phenol-d5 (Surr)56 08/23/17 09:14 08/23/17 22:41 110-120
Terphenyl-d14 (Surr)70 08/23/17 09:14 08/23/17 22:41 113-120
2,4,6-Tribromophenol (Surr)66 08/23/17 09:14 08/23/17 22:41 110-120
Method: 6010D - Metals (ICP)
RL MDL
Antimony <1.09 ^10.9 1.09 mg/Kg ☼08/21/17 17:30 08/22/17 11:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.18 1.31 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Arsenic <1.31
1.09 0.218 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Beryllium <0.218
1.09 0.109 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Cadmium <0.109
1.09 0.983 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Chromium <0.983
2.18 1.20 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Copper <1.20
1.09 0.546 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Lead <0.546
3.28 1.09 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Manganese 3.69
2.18 0.655 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Nickel <0.655
2.18 1.20 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Selenium <1.20
1.09 0.437 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Silver <0.437
2.18 0.655 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Thallium <0.655
10.9 5.46 mg/Kg 08/21/17 17:30 08/22/17 11:32 1☼Zinc <5.46
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury <0.0336 0.112 0.0336 mg/Kg ☼08/21/17 17:27 08/22/17 12:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Moisture 12.8 0.1 0.1 %08/21/17 08:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 %08/21/17 08:40 1Percent Solids 87.2
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-454604/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
RL MDL
Acenaphthene <0.0320 0.0670 0.0320 mg/Kg 08/23/17 09:13 08/23/17 21:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.0290 0.02900.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Acenaphthylene
<0.0290 0.02900.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Anthracene
<0.0300 0.03000.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Benzo[a]anthracene
<0.0270 0.02700.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Benzo[a]pyrene
<0.0280 0.02800.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Benzo[b]fluoranthene
<0.0330 0.03300.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Benzo[g,h,i]perylene
<0.0270 0.02700.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Benzo[k]fluoranthene
<0.200 0.2000.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Bis(2-chloroethoxy)methane
<0.213 0.2130.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Bis(2-chloroethyl)ether
<0.198 0.1980.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1bis (2-chloroisopropyl) ether
<0.207 0.2070.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Bis(2-ethylhexyl) phthalate
<0.205 0.2050.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 14-Bromophenyl phenyl ether
<0.215 0.2150.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Butyl benzyl phthalate
<0.207 0.2070.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Carbazole
<0.227 0.2270.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 14-Chloroaniline
<0.168 0.1680.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 14-Chloro-3-methylphenol
<0.209 0.2090.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12-Chloronaphthalene
<0.191 0.1910.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12-Chlorophenol
<0.201 0.2010.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 14-Chlorophenyl phenyl ether
<0.0370 0.03700.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Chrysene
<0.113 0.1130.666 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Cresols
<0.0320 0.03200.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Dibenz(a,h)anthracene
<0.210 0.2100.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Dibenzofuran
<0.190 0.1900.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 11,2-Dichlorobenzene
<0.190 0.1900.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 11,3-Dichlorobenzene
<0.196 0.1960.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 11,4-Dichlorobenzene
<0.204 0.2040.670 mg/Kg 08/23/17 09:13 08/23/17 21:43 13,3'-Dichlorobenzidine
<0.175 0.1750.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12,4-Dichlorophenol
<0.212 0.2120.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Diethyl phthalate
<0.335 0.3350.670 mg/Kg 08/23/17 09:13 08/23/17 21:43 12,4-Dimethylphenol
<0.207 0.2070.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Dimethyl phthalate
<0.211 0.2110.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Di-n-butyl phthalate
<0.229 0.2290.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 14,6-Dinitro-2-methylphenol
<0.251 0.2510.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12,4-Dinitrophenol
<0.208 0.2080.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12,4-Dinitrotoluene
<0.223 0.2230.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12,6-Dinitrotoluene
<0.178 0.1780.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Di-n-octyl phthalate
<0.0340 0.03400.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Fluoranthene
<0.0290 0.02900.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Fluorene
<0.250 0.2500.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Hexachlorobenzene
<0.167 0.1670.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Hexachlorobutadiene
<0.150 0.1500.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Hexachlorocyclopentadiene
<0.181 0.1810.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Hexachloroethane
<0.0290 0.02900.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Indeno[1,2,3-cd]pyrene
<0.188 0.1880.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Isophorone
<0.0280 0.02800.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 11-Methylnaphthalene
<0.0260 0.02600.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 12-Methylnaphthalene
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-454604/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
RL MDL
2-Methylphenol <0.216 0.333 0.216 mg/Kg 08/23/17 09:13 08/23/17 21:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.203 0.2030.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 13 & 4 Methylphenol
<0.0290 0.02900.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Naphthalene
<0.207 0.2070.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12-Nitroaniline
<0.230 0.2300.670 mg/Kg 08/23/17 09:13 08/23/17 21:43 13-Nitroaniline
<0.238 0.2380.670 mg/Kg 08/23/17 09:13 08/23/17 21:43 14-Nitroaniline
<0.201 0.2010.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Nitrobenzene
<0.243 0.2430.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12-Nitrophenol
<0.382 0.3820.670 mg/Kg 08/23/17 09:13 08/23/17 21:43 14-Nitrophenol
<0.194 0.1940.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1N-Nitrosodi-n-propylamine
<0.0530 0.05300.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1n-Nitrosodiphenylamine(as
diphenylamine)
<0.266 0.2660.670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Pentachlorophenol
<0.0340 0.03400.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Phenanthrene
<0.203 0.2030.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Phenol
<0.0340 0.03400.0670 mg/Kg 08/23/17 09:13 08/23/17 21:43 1Pyrene
<0.181 0.1810.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 11,2,4-Trichlorobenzene
<0.218 0.2180.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12,4,5-Trichlorophenol
<0.192 0.1920.333 mg/Kg 08/23/17 09:13 08/23/17 21:43 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)69 29-120 08/23/17 21:43 1
MB MB
Surrogate
08/23/17 09:13
Dil FacPreparedAnalyzedQualifierLimits%Recovery
52 08/23/17 09:13 08/23/17 21:43 12-Fluorophenol (Surr)10-120
70 08/23/17 09:13 08/23/17 21:43 1Nitrobenzene-d5 (Surr)27-120
60 08/23/17 09:13 08/23/17 21:43 1Phenol-d5 (Surr)10-120
84 08/23/17 09:13 08/23/17 21:43 1Terphenyl-d14 (Surr)13-120
54 08/23/17 09:13 08/23/17 21:43 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-454604/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
Acenaphthene 1.67 1.118 mg/Kg 67 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.199 mg/Kg 72 38-120
Anthracene 1.67 1.230 mg/Kg 74 46-124
Benzo[a]anthracene 1.67 1.291 mg/Kg 77 45-120
Benzo[a]pyrene 1.67 1.176 mg/Kg 71 45-120
Benzo[b]fluoranthene 1.67 1.163 mg/Kg 70 42-120
Benzo[g,h,i]perylene 1.67 1.229 mg/Kg 74 38-120
Benzo[k]fluoranthene 1.67 1.297 mg/Kg 78 42-120
Bis(2-chloroethoxy)methane 1.67 0.9371 mg/Kg 56 32-120
Bis(2-chloroethyl)ether 1.67 0.8964 mg/Kg 54 31-120
bis (2-chloroisopropyl) ether 1.67 0.6890 mg/Kg 41 32-120
Bis(2-ethylhexyl) phthalate 1.67 1.296 mg/Kg 78 43-120
4-Bromophenyl phenyl ether 1.67 1.154 mg/Kg 69 40-120
Butyl benzyl phthalate 1.67 1.260 mg/Kg 76 43-133
Carbazole 1.67 1.222 mg/Kg 73 44-120
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-454604/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
4-Chloroaniline 1.67 1.040 mg/Kg 62 35-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
4-Chloro-3-methylphenol 1.67 1.328 mg/Kg 80 38-120
2-Chloronaphthalene 1.67 1.112 mg/Kg 67 34-120
2-Chlorophenol 1.67 1.066 mg/Kg 64 32-120
4-Chlorophenyl phenyl ether 1.67 1.191 mg/Kg 71 42-120
Chrysene 1.67 1.244 mg/Kg 75 43-120
Cresols 3.33 2.214 mg/Kg 66 36-129
Dibenz(a,h)anthracene 1.67 1.253 mg/Kg 75 32-128
Dibenzofuran 1.67 1.176 mg/Kg 71 41-120
1,2-Dichlorobenzene 1.67 1.007 mg/Kg 60 33-120
1,3-Dichlorobenzene 1.67 0.9810 mg/Kg 59 32-120
1,4-Dichlorobenzene 1.67 0.9850 mg/Kg 59 32-120
3,3'-Dichlorobenzidine 1.67 1.173 mg/Kg 70 39-120
2,4-Dichlorophenol 1.67 1.178 mg/Kg 71 32-120
Diethyl phthalate 1.67 1.245 mg/Kg 75 41-122
2,4-Dimethylphenol 1.67 0.9023 mg/Kg 54 32-120
Dimethyl phthalate 1.67 1.206 mg/Kg 72 55-120
Di-n-butyl phthalate 1.67 1.369 mg/Kg 82 46-127
4,6-Dinitro-2-methylphenol 3.33 1.726 mg/Kg 52 27-134
2,4-Dinitrophenol 3.33 1.461 mg/Kg 44 10-142
2,4-Dinitrotoluene 1.67 1.288 mg/Kg 77 43-120
2,6-Dinitrotoluene 1.67 1.334 mg/Kg 80 43-120
Di-n-octyl phthalate 1.67 1.400 mg/Kg 84 40-130
Fluoranthene 1.67 1.297 mg/Kg 78 46-120
Fluorene 1.67 1.227 mg/Kg 74 42-120
Hexachlorobenzene 1.67 1.276 mg/Kg 77 44-120
Hexachlorobutadiene 1.67 1.103 mg/Kg 66 31-120
Hexachlorocyclopentadiene 1.67 0.1729 J *mg/Kg 10 24-120
Hexachloroethane 1.67 0.9076 mg/Kg 54 33-120
Indeno[1,2,3-cd]pyrene 1.67 1.221 mg/Kg 73 41-121
Isophorone 1.67 0.9429 mg/Kg 57 33-120
1-Methylnaphthalene 1.67 1.115 mg/Kg 67 32-120
2-Methylnaphthalene 1.67 1.107 mg/Kg 66 28-120
2-Methylphenol 1.67 1.084 mg/Kg 65 36-120
3 & 4 Methylphenol 1.67 1.130 mg/Kg 68 37-120
Naphthalene 1.67 1.047 mg/Kg 63 32-120
2-Nitroaniline 1.67 1.177 mg/Kg 71 40-120
3-Nitroaniline 1.67 1.186 mg/Kg 71 42-120
4-Nitroaniline 1.67 1.179 mg/Kg 71 43-120
Nitrobenzene 1.67 0.9202 mg/Kg 55 26-120
2-Nitrophenol 1.67 1.258 mg/Kg 75 29-120
4-Nitrophenol 3.33 2.507 mg/Kg 75 32-136
N-Nitrosodi-n-propylamine 1.67 1.009 mg/Kg 61 35-120
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.125 mg/Kg 79 52-140
Pentachlorophenol 3.33 2.550 mg/Kg 77 44-134
Phenanthrene 1.67 1.213 mg/Kg 73 45-120
Phenol 1.67 1.141 mg/Kg 68 30-120
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-454604/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
Pyrene 1.67 1.291 mg/Kg 77 43-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2,4-Trichlorobenzene 1.67 1.065 mg/Kg 64 29-120
2,4,5-Trichlorophenol 1.67 1.320 mg/Kg 79 39-120
2,4,6-Trichlorophenol 1.67 1.331 mg/Kg 80 39-120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
60
LCS LCS
Qualifier Limits%Recovery
572-Fluorophenol (Surr)10 -120
58Nitrobenzene-d5 (Surr)27 -120
61Phenol-d5 (Surr)10 -120
75Terphenyl-d14 (Surr)13 -120
762,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-454604/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
Acenaphthene 1.67 1.259 mg/Kg 76 36-120 12 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 1.67 1.360 mg/Kg 82 38-120 13 50
Anthracene 1.67 1.411 mg/Kg 85 46-124 14 49
Benzo[a]anthracene 1.67 1.482 mg/Kg 89 45-120 14 50
Benzo[a]pyrene 1.67 1.369 mg/Kg 82 45-120 15 50
Benzo[b]fluoranthene 1.67 1.319 mg/Kg 79 42-120 13 50
Benzo[g,h,i]perylene 1.67 1.429 mg/Kg 86 38-120 15 50
Benzo[k]fluoranthene 1.67 1.541 mg/Kg 92 42-120 17 45
Bis(2-chloroethoxy)methane 1.67 1.069 mg/Kg 64 32-120 13 50
Bis(2-chloroethyl)ether 1.67 1.023 mg/Kg 61 31-120 13 50
bis (2-chloroisopropyl) ether 1.67 0.8073 mg/Kg 48 32-120 16 50
Bis(2-ethylhexyl) phthalate 1.67 1.512 mg/Kg 91 43-120 15 50
4-Bromophenyl phenyl ether 1.67 1.331 mg/Kg 80 40-120 14 37
Butyl benzyl phthalate 1.67 1.492 mg/Kg 90 43-133 17 50
Carbazole 1.67 1.407 mg/Kg 84 44-120 14 46
4-Chloroaniline 1.67 1.192 mg/Kg 71 35-120 14 50
4-Chloro-3-methylphenol 1.67 1.548 mg/Kg 93 38-120 15 49
2-Chloronaphthalene 1.67 1.257 mg/Kg 75 34-120 12 50
2-Chlorophenol 1.67 1.245 mg/Kg 75 32-120 15 50
4-Chlorophenyl phenyl ether 1.67 1.346 mg/Kg 81 42-120 12 50
Chrysene 1.67 1.462 mg/Kg 88 43-120 16 49
Cresols 3.33 2.525 mg/Kg 76 36-129 13 50
Dibenz(a,h)anthracene 1.67 1.440 mg/Kg 86 32-128 14 50
Dibenzofuran 1.67 1.329 mg/Kg 80 41-120 12 50
1,2-Dichlorobenzene 1.67 1.181 mg/Kg 71 33-120 16 50
1,3-Dichlorobenzene 1.67 1.144 mg/Kg 69 32-120 15 50
1,4-Dichlorobenzene 1.67 1.147 mg/Kg 69 32-120 15 50
3,3'-Dichlorobenzidine 1.67 1.331 mg/Kg 80 39-120 13 50
2,4-Dichlorophenol 1.67 1.388 mg/Kg 83 32-120 16 50
Diethyl phthalate 1.67 1.426 mg/Kg 86 41-122 14 45
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-454604/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
2,4-Dimethylphenol 1.67 1.023 mg/Kg 61 32-120 13 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Dimethyl phthalate 1.67 1.385 mg/Kg 83 55-120 14 46
Di-n-butyl phthalate 1.67 1.583 mg/Kg 95 46-127 15 49
4,6-Dinitro-2-methylphenol 3.33 2.037 mg/Kg 61 27-134 17 50
2,4-Dinitrophenol 3.33 1.733 mg/Kg 52 10-142 17 50
2,4-Dinitrotoluene 1.67 1.513 mg/Kg 91 43-120 16 50
2,6-Dinitrotoluene 1.67 1.570 mg/Kg 94 43-120 16 50
Di-n-octyl phthalate 1.67 1.654 mg/Kg 99 40-130 17 50
Fluoranthene 1.67 1.490 mg/Kg 89 46-120 14 50
Fluorene 1.67 1.394 mg/Kg 84 42-120 13 50
Hexachlorobenzene 1.67 1.496 mg/Kg 90 44-120 16 50
Hexachlorobutadiene 1.67 1.296 mg/Kg 78 31-120 16 50
Hexachlorocyclopentadiene 1.67 0.2032 J *mg/Kg 12 24-120 16 50
Hexachloroethane 1.67 1.035 mg/Kg 62 33-120 13 50
Indeno[1,2,3-cd]pyrene 1.67 1.400 mg/Kg 84 41-121 14 50
Isophorone 1.67 1.083 mg/Kg 65 33-120 14 50
1-Methylnaphthalene 1.67 1.294 mg/Kg 78 32-120 15 50
2-Methylnaphthalene 1.67 1.284 mg/Kg 77 28-120 15 50
2-Methylphenol 1.67 1.252 mg/Kg 75 36-120 14 50
3 & 4 Methylphenol 1.67 1.273 mg/Kg 76 37-120 12 50
Naphthalene 1.67 1.193 mg/Kg 72 32-120 13 50
2-Nitroaniline 1.67 1.359 mg/Kg 82 40-120 14 50
3-Nitroaniline 1.67 1.369 mg/Kg 82 42-120 14 49
4-Nitroaniline 1.67 1.386 mg/Kg 83 43-120 16 49
Nitrobenzene 1.67 1.074 mg/Kg 64 26-120 15 50
2-Nitrophenol 1.67 1.441 mg/Kg 86 29-120 14 50
4-Nitrophenol 3.33 2.847 mg/Kg 85 32-136 13 45
N-Nitrosodi-n-propylamine 1.67 1.136 mg/Kg 68 35-120 12 50
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.292 mg/Kg 91 52-140 14 50
Pentachlorophenol 3.33 2.853 mg/Kg 86 44-134 11 50
Phenanthrene 1.67 1.393 mg/Kg 84 45-120 14 50
Phenol 1.67 1.258 mg/Kg 76 30-120 10 50
Pyrene 1.67 1.529 mg/Kg 92 43-120 17 50
1,2,4-Trichlorobenzene 1.67 1.234 mg/Kg 74 29-120 15 50
2,4,5-Trichlorophenol 1.67 1.531 mg/Kg 92 39-120 15 50
2,4,6-Trichlorophenol 1.67 1.497 mg/Kg 90 39-120 12 50
2-Fluorobiphenyl (Surr)29 -120
Surrogate
67
LCSD LCSD
Qualifier Limits%Recovery
662-Fluorophenol (Surr)10 -120
69Nitrobenzene-d5 (Surr)27 -120
73Phenol-d5 (Surr)10 -120
89Terphenyl-d14 (Surr)13 -120
862,4,6-Tribromophenol (Surr)10 -120
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-135116-I-1-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
Acenaphthene 0.166 J 2.37 1.668 mg/Kg 63 19-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene 0.168 J 2.37 1.765 mg/Kg 67 25-120☼
Anthracene 0.363 2.37 1.913 mg/Kg 65 28-125☼
Benzo[a]anthracene 0.730 2.37 2.009 mg/Kg 54 23-120☼
Benzo[a]pyrene 0.755 2.37 1.958 mg/Kg 51 15-128☼
Benzo[b]fluoranthene 0.732 2.37 1.991 mg/Kg 53 12-133☼
Benzo[g,h,i]perylene 0.477 2.37 1.981 mg/Kg 63 22-120☼
Benzo[k]fluoranthene 0.448 2.37 1.987 mg/Kg 65 28-120☼
Bis(2-chloroethoxy)methane <0.561 2.37 1.201 mg/Kg 51 24-120☼
Bis(2-chloroethyl)ether <0.598 2.37 1.153 mg/Kg 49 22-120☼
bis (2-chloroisopropyl) ether <0.556 2.37 0.9354 J mg/Kg 39 20-120☼
Bis(2-ethylhexyl) phthalate <0.581 2.37 1.945 mg/Kg 82 26-120☼
4-Bromophenyl phenyl ether <0.575 2.37 1.693 mg/Kg 71 31-120☼
Butyl benzyl phthalate <0.603 2.37 1.971 mg/Kg 83 24-133☼
Carbazole <0.581 2.37 1.828 mg/Kg 77 25-123☼
4-Chloroaniline <0.637 2.37 1.354 mg/Kg 57 26-120☼
4-Chloro-3-methylphenol <0.471 2.37 1.873 mg/Kg 79 21-120☼
2-Chloronaphthalene <0.586 2.37 1.529 mg/Kg 64 24-120☼
2-Chlorophenol <0.536 2.37 1.397 mg/Kg 59 25-120☼
4-Chlorophenyl phenyl ether <0.564 2.37 1.710 mg/Kg 72 26-120☼
Chrysene 0.680 2.37 2.031 mg/Kg 57 20-120☼
Cresols <0.317 4.75 2.942 mg/Kg 62 10-200☼
Dibenz(a,h)anthracene <0.0898 2.37 1.885 mg/Kg 79 12-128☼
Dibenzofuran <0.589 2.37 1.716 mg/Kg 72 21-120☼
1,2-Dichlorobenzene <0.533 2.37 1.300 mg/Kg 55 10-120☼
1,3-Dichlorobenzene <0.533 2.37 1.242 mg/Kg 52 10-120☼
1,4-Dichlorobenzene <0.550 2.37 1.251 mg/Kg 53 10-120☼
3,3'-Dichlorobenzidine <0.572 2.37 1.855 J mg/Kg 78 10-120☼
2,4-Dichlorophenol <0.491 2.37 1.626 mg/Kg 69 17-120☼
Diethyl phthalate <0.595 2.37 1.792 mg/Kg 76 29-122☼
2,4-Dimethylphenol <0.940 2.37 1.177 J mg/Kg 50 17-120☼
Dimethyl phthalate <0.581 2.37 1.708 mg/Kg 72 30-120☼
Di-n-butyl phthalate <0.592 2.37 2.012 mg/Kg 85 29-126☼
4,6-Dinitro-2-methylphenol <0.642 4.75 1.997 mg/Kg 42 10-134☼
2,4-Dinitrophenol <0.704 4.75 1.616 mg/Kg 34 10-150☼
2,4-Dinitrotoluene <0.584 2.37 1.900 mg/Kg 80 24-121☼
2,6-Dinitrotoluene <0.626 2.37 1.881 mg/Kg 79 24-120☼
Di-n-octyl phthalate <0.499 2.37 2.213 mg/Kg 93 27-130☼
Fluoranthene 1.27 2.37 2.226 mg/Kg 40 10-143☼
Fluorene 0.198 2.37 1.813 mg/Kg 68 20-120☼
Hexachlorobenzene <0.701 2.37 1.846 mg/Kg 78 25-120☼
Hexachlorobutadiene <0.469 2.37 1.476 mg/Kg 62 10-120☼
Hexachlorocyclopentadiene <0.421 F1 *2.37 <0.427 F1 mg/Kg 0 10-120☼
Hexachloroethane <0.508 2.37 1.060 mg/Kg 45 10-120☼
Indeno[1,2,3-cd]pyrene 0.417 2.37 1.945 mg/Kg 64 22-121☼
Isophorone <0.527 2.37 1.234 mg/Kg 52 24-120☼
1-Methylnaphthalene 0.108 J 2.37 1.544 mg/Kg 61 10-120☼
2-Methylnaphthalene <0.0729 2.37 1.483 mg/Kg 62 13-120☼
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-135116-I-1-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
2-Methylphenol <0.606 2.37 1.429 mg/Kg 60 23-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
3 & 4 Methylphenol <0.570 2.37 1.513 mg/Kg 64 19-120☼
Naphthalene 0.221 2.37 1.445 mg/Kg 52 10-120☼
2-Nitroaniline <0.581 2.37 1.780 mg/Kg 75 31-120☼
3-Nitroaniline <0.645 2.37 1.719 J mg/Kg 72 31-120☼
4-Nitroaniline <0.668 2.37 1.771 J mg/Kg 75 28-120☼
Nitrobenzene <0.564 2.37 1.168 mg/Kg 49 19-120☼
2-Nitrophenol <0.682 2.37 1.568 mg/Kg 66 23-120☼
4-Nitrophenol <1.07 4.75 3.414 mg/Kg 72 16-139☼
N-Nitrosodi-n-propylamine <0.544 2.37 1.305 mg/Kg 55 24-120☼
n-Nitrosodiphenylamine(as
diphenylamine)
<0.149 2.02 1.655 mg/Kg 82 26-150☼
Pentachlorophenol <0.746 4.75 3.871 mg/Kg 82 19-145☼
Phenanthrene 0.844 2.37 1.995 mg/Kg 49 21-122☼
Phenol <0.570 2.37 1.471 mg/Kg 62 15-120☼
Pyrene 1.15 2.37 2.222 mg/Kg 45 20-123☼
1,2,4-Trichlorobenzene <0.508 2.37 1.372 mg/Kg 58 14-120☼
2,4,5-Trichlorophenol <0.612 2.37 1.956 mg/Kg 82 27-120☼
2,4,6-Trichlorophenol <0.539 2.37 1.848 mg/Kg 78 24-122☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
58
MS MS
Qualifier Limits%Recovery
492-Fluorophenol (Surr)10 -120
52Nitrobenzene-d5 (Surr)27 -120
56Phenol-d5 (Surr)10 -120
75Terphenyl-d14 (Surr)13 -120
802,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-135116-I-1-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
Acenaphthene 0.166 J 2.33 1.867 mg/Kg 73 19-120 11 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 0.168 J 2.33 1.985 mg/Kg 78 25-120 12 50☼
Anthracene 0.363 2.33 2.167 mg/Kg 77 28-125 12 49☼
Benzo[a]anthracene 0.730 2.33 2.326 mg/Kg 69 23-120 15 50☼
Benzo[a]pyrene 0.755 2.33 2.188 mg/Kg 62 15-128 11 50☼
Benzo[b]fluoranthene 0.732 2.33 2.200 mg/Kg 63 12-133 10 50☼
Benzo[g,h,i]perylene 0.477 2.33 2.162 mg/Kg 72 22-120 9 50☼
Benzo[k]fluoranthene 0.448 2.33 2.227 mg/Kg 76 28-120 11 45☼
Bis(2-chloroethoxy)methane <0.561 2.33 1.437 mg/Kg 62 24-120 18 50☼
Bis(2-chloroethyl)ether <0.598 2.33 1.405 mg/Kg 60 22-120 20 50☼
bis (2-chloroisopropyl) ether <0.556 2.33 1.121 mg/Kg 48 20-120 18 50☼
Bis(2-ethylhexyl) phthalate <0.581 2.33 2.181 mg/Kg 94 26-120 11 50☼
4-Bromophenyl phenyl ether <0.575 2.33 1.911 mg/Kg 82 31-120 12 37☼
Butyl benzyl phthalate <0.603 2.33 2.196 mg/Kg 94 24-133 11 50☼
Carbazole <0.581 2.33 2.047 mg/Kg 88 25-123 11 46☼
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-135116-I-1-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
4-Chloroaniline <0.637 2.33 1.608 mg/Kg 69 26-120 17 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Chloro-3-methylphenol <0.471 2.33 2.125 mg/Kg 91 21-120 13 49☼
2-Chloronaphthalene <0.586 2.33 1.749 mg/Kg 75 24-120 13 50☼
2-Chlorophenol <0.536 2.33 1.661 mg/Kg 71 25-120 17 50☼
4-Chlorophenyl phenyl ether <0.564 2.33 1.932 mg/Kg 83 26-120 12 50☼
Chrysene 0.680 2.33 2.383 mg/Kg 73 20-120 16 49☼
Cresols <0.317 4.66 3.454 mg/Kg 74 10-200 16 50☼
Dibenz(a,h)anthracene <0.0898 2.33 2.115 mg/Kg 91 12-128 11 50☼
Dibenzofuran <0.589 2.33 1.925 mg/Kg 83 21-120 12 50☼
1,2-Dichlorobenzene <0.533 2.33 1.570 mg/Kg 67 10-120 19 50☼
1,3-Dichlorobenzene <0.533 2.33 1.517 mg/Kg 65 10-120 20 50☼
1,4-Dichlorobenzene <0.550 2.33 1.536 mg/Kg 66 10-120 20 50☼
3,3'-Dichlorobenzidine <0.572 2.33 2.076 mg/Kg 89 10-120 11 50☼
2,4-Dichlorophenol <0.491 2.33 1.877 mg/Kg 81 17-120 14 50☼
Diethyl phthalate <0.595 2.33 1.993 mg/Kg 86 29-122 11 45☼
2,4-Dimethylphenol <0.940 2.33 1.403 J mg/Kg 60 17-120 17 50☼
Dimethyl phthalate <0.581 2.33 1.918 mg/Kg 82 30-120 12 46☼
Di-n-butyl phthalate <0.592 2.33 2.254 mg/Kg 97 29-126 11 49☼
4,6-Dinitro-2-methylphenol <0.642 4.66 2.296 mg/Kg 49 10-134 14 50☼
2,4-Dinitrophenol <0.704 4.66 1.839 mg/Kg 39 10-150 13 50☼
2,4-Dinitrotoluene <0.584 2.33 2.117 mg/Kg 91 24-121 11 50☼
2,6-Dinitrotoluene <0.626 2.33 2.122 mg/Kg 91 24-120 12 50☼
Di-n-octyl phthalate <0.499 2.33 2.394 mg/Kg 103 27-130 8 50☼
Fluoranthene 1.27 2.33 2.684 mg/Kg 61 10-143 19 50☼
Fluorene 0.198 2.33 2.061 mg/Kg 80 20-120 13 50☼
Hexachlorobenzene <0.701 2.33 2.079 mg/Kg 89 25-120 12 50☼
Hexachlorobutadiene <0.469 2.33 1.808 mg/Kg 78 10-120 20 50☼
Hexachlorocyclopentadiene <0.421 F1 *2.33 <0.419 F1 mg/Kg 0 10-120 NC 50☼
Hexachloroethane <0.508 2.33 1.318 mg/Kg 57 10-120 22 50☼
Indeno[1,2,3-cd]pyrene 0.417 2.33 2.165 mg/Kg 75 22-121 11 50☼
Isophorone <0.527 2.33 1.456 mg/Kg 63 24-120 17 50☼
1-Methylnaphthalene 0.108 J 2.33 1.861 mg/Kg 75 10-120 19 50☼
2-Methylnaphthalene <0.0729 2.33 1.796 mg/Kg 77 13-120 19 50☼
2-Methylphenol <0.606 2.33 1.682 mg/Kg 72 23-120 16 50☼
3 & 4 Methylphenol <0.570 2.33 1.772 mg/Kg 76 19-120 16 50☼
Naphthalene 0.221 2.33 1.772 mg/Kg 67 10-120 20 50☼
2-Nitroaniline <0.581 2.33 1.983 mg/Kg 85 31-120 11 50☼
3-Nitroaniline <0.645 2.33 1.918 mg/Kg 82 31-120 11 49☼
4-Nitroaniline <0.668 2.33 1.923 mg/Kg 83 28-120 8 49☼
Nitrobenzene <0.564 2.33 1.436 mg/Kg 62 19-120 21 50☼
2-Nitrophenol <0.682 2.33 1.890 mg/Kg 81 23-120 19 50☼
4-Nitrophenol <1.07 4.66 3.928 mg/Kg 84 16-139 14 45☼
N-Nitrosodi-n-propylamine <0.544 2.33 1.553 mg/Kg 67 24-120 17 50☼
n-Nitrosodiphenylamine(as
diphenylamine)
<0.149 1.98 1.888 mg/Kg 95 26-150 13 50☼
Pentachlorophenol <0.746 4.66 4.305 mg/Kg 92 19-145 11 50☼
Phenanthrene 0.844 2.33 2.356 mg/Kg 65 21-122 17 50☼
Phenol <0.570 2.33 1.753 mg/Kg 75 15-120 17 50☼
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-135116-I-1-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454779 Prep Batch: 454604
Pyrene 1.15 2.33 2.674 mg/Kg 65 20-123 18 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2,4-Trichlorobenzene <0.508 2.33 1.705 mg/Kg 73 14-120 22 50☼
2,4,5-Trichlorophenol <0.612 2.33 2.176 mg/Kg 93 27-120 11 50☼
2,4,6-Trichlorophenol <0.539 2.33 2.090 mg/Kg 90 24-122 12 50☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
68
MSD MSD
Qualifier Limits%Recovery
612-Fluorophenol (Surr)10 -120
65Nitrobenzene-d5 (Surr)27 -120
68Phenol-d5 (Surr)10 -120
87Terphenyl-d14 (Surr)13 -120
922,4,6-Tribromophenol (Surr)10 -120
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-454270/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454496 Prep Batch: 454270
RL MDL
Antimony <0.980 ^9.80 0.980 mg/Kg 08/21/17 17:30 08/22/17 10:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.18 1.181.96 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Arsenic
<0.196 0.1960.980 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Beryllium
<0.0980 0.09800.980 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Cadmium
<0.882 0.8820.980 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Chromium
<1.08 1.081.96 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Copper
<0.490 0.4900.980 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Lead
<0.980 0.9802.94 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Manganese
<0.588 0.5881.96 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Nickel
<1.08 1.081.96 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Selenium
<0.392 0.3920.980 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Silver
<0.588 0.5881.96 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Thallium
<4.90 4.909.80 mg/Kg 08/21/17 17:30 08/22/17 10:15 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-454270/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454496 Prep Batch: 454270
Antimony 19.9 20.28 ^mg/Kg 102 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 19.9 19.18 mg/Kg 96 80-120
Beryllium 19.9 20.58 mg/Kg 103 80-120
Cadmium 19.9 19.80 mg/Kg 100 80-120
Chromium 19.9 20.56 mg/Kg 103 80-120
Copper 19.9 19.68 mg/Kg 99 80-120
Lead 19.9 19.44 mg/Kg 98 80-120
Manganese 19.9 20.76 mg/Kg 104 80-120
Nickel 19.9 20.26 mg/Kg 102 80-120
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-454270/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454496 Prep Batch: 454270
Selenium 19.9 20.62 mg/Kg 104 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Silver 19.9 20.74 mg/Kg 104 80-120
Thallium 19.9 20.89 mg/Kg 105 80-120
Zinc 19.9 19.24 mg/Kg 97 80-120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-454270/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454496 Prep Batch: 454270
Antimony 19.6 20.59 ^mg/Kg 105 80-120 2 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Arsenic 19.6 19.27 mg/Kg 98 80-120 0 20
Beryllium 19.6 20.43 mg/Kg 104 80-120 1 20
Cadmium 19.6 19.69 mg/Kg 100 80-120 1 20
Chromium 19.6 19.80 mg/Kg 101 80-120 4 20
Copper 19.6 20.88 mg/Kg 106 80-120 6 20
Lead 19.6 19.71 mg/Kg 100 80-120 1 20
Manganese 19.6 20.02 mg/Kg 102 80-120 4 20
Nickel 19.6 20.02 mg/Kg 102 80-120 1 20
Selenium 19.6 20.53 mg/Kg 105 80-120 0 20
Silver 19.6 19.84 mg/Kg 101 80-120 4 20
Thallium 19.6 20.96 mg/Kg 107 80-120 0 20
Zinc 19.6 18.98 mg/Kg 97 80-120 1 20
Client Sample ID: Matrix SpikeLab Sample ID: 490-134952-B-1-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454496 Prep Batch: 454270
Antimony <0.998 ^19.0 17.45 ^mg/Kg 92 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 3.21 19.0 20.67 mg/Kg 92 75-125
Beryllium <0.200 19.0 18.65 mg/Kg 98 75-125
Cadmium 0.299 J 19.0 17.71 mg/Kg 91 75-125
Chromium 3.77 19.0 21.20 mg/Kg 91 75-125
Copper 11.1 19.0 32.06 mg/Kg 110 75-125
Lead 5.45 19.0 22.55 mg/Kg 90 75-125
Manganese 255 19.0 274.5 4 mg/Kg 102 75-125
Nickel 9.26 19.0 27.50 mg/Kg 96 75-125
Selenium <1.10 19.0 17.28 mg/Kg 91 75-125
Silver <0.399 19.0 17.87 mg/Kg 94 75-125
Thallium <0.599 19.0 17.24 mg/Kg 91 75-125
Zinc 35.3 F1 19.0 55.49 mg/Kg 106 75-125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-134952-B-1-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454496 Prep Batch: 454270
Antimony <0.998 ^19.0 18.17 ^mg/Kg 95 75-125 4 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-134952-B-1-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454496 Prep Batch: 454270
Arsenic 3.21 19.0 22.00 mg/Kg 99 75-125 6 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Beryllium <0.200 19.0 19.12 mg/Kg 100 75-125 3 20
Cadmium 0.299 J 19.0 18.13 mg/Kg 94 75-125 2 20
Chromium 3.77 19.0 22.34 mg/Kg 97 75-125 5 20
Copper 11.1 19.0 32.72 mg/Kg 114 75-125 2 20
Lead 5.45 19.0 23.37 mg/Kg 94 75-125 4 20
Manganese 255 19.0 305.5 4 mg/Kg 265 75-125 11 20
Nickel 9.26 19.0 28.74 mg/Kg 102 75-125 4 20
Selenium <1.10 19.0 17.39 mg/Kg 91 75-125 1 20
Silver <0.399 19.0 18.36 mg/Kg 96 75-125 3 20
Thallium <0.599 19.0 17.89 mg/Kg 94 75-125 4 20
Zinc 35.3 F1 19.0 59.64 F1 mg/Kg 128 75-125 7 20
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-454269/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454481 Prep Batch: 454269
RL MDL
Mercury <0.0301 0.100 0.0301 mg/Kg 08/21/17 17:27 08/22/17 12:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-454269/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454481 Prep Batch: 454269
Mercury 0.168 0.1552 mg/Kg 93 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 460-139295-C-1-B MS ^5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454481 Prep Batch: 454269
Mercury 1.96 0.301 2.351 4 mg/Kg 129 80-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 460-139295-C-1-C MSD ^5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454481 Prep Batch: 454269
Mercury 1.96 0.307 2.568 4 mg/Kg 197 80-120 9 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method: Moisture - Percent Moisture
Client Sample ID: DuplicateLab Sample ID: 490-134867-E-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 454085
Percent Moisture 18.8 16.4 %13 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Percent Solids 81.2 83.6 %3 20
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QC Association Summary
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
GC/MS Semi VOA
Prep Batch: 454604
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550C490-134906-1 SURF-EDGE-4 Total/NA
Solid 3550CMB 490-454604/1-A Method Blank Total/NA
Solid 3550CLCS 490-454604/2-A Lab Control Sample Total/NA
Solid 3550CLCSD 490-454604/3-A Lab Control Sample Dup Total/NA
Solid 3550C490-135116-I-1-E MS Matrix Spike Total/NA
Solid 3550C490-135116-I-1-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 454779
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 454604490-134906-1 SURF-EDGE-4 Total/NA
Solid 8270D 454604MB 490-454604/1-A Method Blank Total/NA
Solid 8270D 454604LCS 490-454604/2-A Lab Control Sample Total/NA
Solid 8270D 454604LCSD 490-454604/3-A Lab Control Sample Dup Total/NA
Solid 8270D 454604490-135116-I-1-E MS Matrix Spike Total/NA
Solid 8270D 454604490-135116-I-1-F MSD Matrix Spike Duplicate Total/NA
Metals
Prep Batch: 454269
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B490-134906-1 SURF-EDGE-4 Total/NA
Solid 7471BMB 490-454269/1-A Method Blank Total/NA
Solid 7471BLCS 490-454269/2-A Lab Control Sample Total/NA
Solid 7471B460-139295-C-1-B MS ^5 Matrix Spike Total/NA
Solid 7471B460-139295-C-1-C MSD ^5 Matrix Spike Duplicate Total/NA
Prep Batch: 454270
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3051A490-134906-1 SURF-EDGE-4 Total/NA
Solid 3051AMB 490-454270/1-A Method Blank Total/NA
Solid 3051ALCS 490-454270/2-A Lab Control Sample Total/NA
Solid 3051ALCSD 490-454270/3-A Lab Control Sample Dup Total/NA
Solid 3051A490-134952-B-1-E MS Matrix Spike Total/NA
Solid 3051A490-134952-B-1-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 454481
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B 454269490-134906-1 SURF-EDGE-4 Total/NA
Solid 7471B 454269MB 490-454269/1-A Method Blank Total/NA
Solid 7471B 454269LCS 490-454269/2-A Lab Control Sample Total/NA
Solid 7471B 454269460-139295-C-1-B MS ^5 Matrix Spike Total/NA
Solid 7471B 454269460-139295-C-1-C MSD ^5 Matrix Spike Duplicate Total/NA
Analysis Batch: 454496
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010D 454270490-134906-1 SURF-EDGE-4 Total/NA
Solid 6010D 454270MB 490-454270/1-A Method Blank Total/NA
Solid 6010D 454270LCS 490-454270/2-A Lab Control Sample Total/NA
Solid 6010D 454270LCSD 490-454270/3-A Lab Control Sample Dup Total/NA
Solid 6010D 454270490-134952-B-1-E MS Matrix Spike Total/NA
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QC Association Summary
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Metals (Continued)
Analysis Batch: 454496 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010D 454270490-134952-B-1-F MSD Matrix Spike Duplicate Total/NA
General Chemistry
Analysis Batch: 454085
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-134906-1 SURF-EDGE-4 Total/NA
Solid Moisture490-134867-E-1 DU Duplicate Total/NA
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Lab Chronicle
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134906-1
Project/Site: Eagle Island Leland, NC
Client Sample ID: SURF-EDGE-4 Lab Sample ID: 490-134906-1
Matrix: SolidDate Collected: 08/17/17 10:15
Date Received: 08/18/17 09:35
Analysis Moisture BAA08/21/17 08:401 TAL NSH454085
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: SURF-EDGE-4 Lab Sample ID: 490-134906-1
Matrix: SolidDate Collected: 08/17/17 10:15
Percent Solids: 87.2Date Received: 08/18/17 09:35
Prep 3550C MNM08/23/17 09:14 TAL NSH454604
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 30.76 g 1.00 mL
Analysis 8270D 1 454779 08/23/17 22:41 RP TAL NSHTotal/NA
Prep 3051A 454270 08/21/17 17:30 BVH TAL NSHTotal/NA 0.525 g 100 mL
Analysis 6010D 1 454496 08/22/17 11:32 LCS TAL NSHTotal/NA
Prep 7471B 454269 08/21/17 17:27 RDF TAL NSHTotal/NA 0.615 g 100 mL
Analysis 7471B 1 454481 08/22/17 12:53 RDF TAL NSHTotal/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-134906-1Client: Geosyntec Consultants, Inc.
Project/Site: Eagle Island Leland, NC
Method Method Description LaboratoryProtocol
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8467471BMercury (CVAA)TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Accreditation/Certification Summary
Client: Geosyntec Consultants, Inc.TestAmerica Job ID: 490-134906-1
Project/Site: Eagle Island Leland, NC
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3874State Program 12-31-17
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
Moisture Solid Percent Moisture
Moisture Solid Percent Solids
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Geosyntec Consultants, Inc.Job Number: 490-134906-1
Login Number: 134906
Question Answer Comment
Creator: Vest, Laura E
List Source: TestAmerica Nashville
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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ATTACHMENT B
T&D DOCUMENTATION
ATTACHMENT C
NCDEQ BACKFILL APPROVAL
COORESPONDANCE
1
Grant Wallace
From:Matthew Jenny
Sent:Wednesday, August 30, 2017 1:52 PM
To:Grant Wallace
Subject:FW: Eagle Island Backfill Source Memorandum

From: Watson, Samuel [mailto:[e-mail]]
Sent: Wednesday, August 23, 2017 2:44 PM
To: Matthew Jenny <[e-mail]>
Cc: Kaitlyn Rhonehouse <[e-mail]>
Subject: RE: Eagle Island Backfill Source Memorandum

Matt,

The Backfill Soil Authorization Memorandum, dated August 23, 2017, has been received and reviewed.

The Brownfields Program concurs with the conclusions presented in the memorandum. As such, the soil from the
potential backfill source may be used as backfill on the site.

Please let me know if there are any questions.

Thanks,

Samuel P. Watson, P.G.
Project Manager
Division of Waste Management - Brownfields
NC Department of Environmental Quality

910 796 7408 office
910 350 2004 fax
[e-mail]

127 Cardinal Drive Ext.
Wilmington, NC 28405

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Matthew Jenny [mailto:[e-mail]]
Sent: Wednesday, August 23, 2017 12:53 PM
To: Watson, Samuel <[e-mail]>